5504_LakeNormanCDLF_GWMR_DIN27924

 
10 Quiet Brook Court 314-496-4654
St. Charles, MO 63303 www.jettenviro.com

September 2, 2016 Submitted via Electronic Mail

Ms. Jackie Drummond
North Carolina Department of Environmental Quality
Division of Waste Management - Solid Waste Section
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

Dear Ms. Drummond:

Re: Submittal of Groundwater and Surface Water Monitoring Results
First Semi-Annual 2016 Event
Lake Norman Construction & Demolition Landfill
North Carolina, Permit # 55-04

On behalf of BFI Lake Norman Landfill, Inc., Jett Environmental Consulting is providing a water quality summary
for the First Semi-Annual 2016 sampling event for the Lake Norman Construction & Demolition Landfill.
Groundwater and surface water sampling was performed by Pace Analytical Services, Inc. (formerly Analytical
Services, Inc.) and analytical testing was performed by Pace Analytical Services, Inc. The groundwater and
surface water samples were analyzed for the Detection Monitoring parameters listed in 15A North Carolina
Administrative Code (NCAC) 13B .0544(b)(1)(D), which included the constituents listed in Appendix I of 40 CFR
Part 258 (15 heavy metals and 47 organics), mercury, chloride, manganese, sulfate, iron, specific conductance,
pH, temperature, alkalinity, and total dissolved solids. In accordance with a North Carolina Department of
Environmental Quality (NCDEQ) memorandum for C&D landfills dated June 25, 2010, tetrahydrofuran was also
monitored for each of the samples collected. Included in Attachment A is a copy of the laboratory analytical
report and field information forms.

Assessment Monitoring Program

A Groundwater Assessment Monitoring Work Plan was compiled in accordance with 15A NCAC 13B .0545, due to
confirmed methylene chloride detections at MW-4 above the North Carolina 15A NCAC 2L Water Quality Standard
during the Second Semi-Annual 2014 event. The Groundwater Monitoring Assessment Work Plan was submitted on
March 9, 2015 by Jett Environmental Consulting and approved by NCDEQ in correspondence dated March 16, 2015.
Well MW-5 was installed downgradient of MW-4 on March 25, 2015. The sampling activities associated with the Work
Plan were completed during the May 2015 event. A summary of the May 2015 event data was provided to NCDEQ
in correspondence dated July 27, 2015.

No volatile organic compounds (VOCs) have been confirmed detected above NC Solid Waste Section Limits
(SWSLs) or NC 2L Standards at MW-5. Per a March 8, 2016 NCDEQ letter, MW-4 was approved for abandonment
and replaced with MW-5 in the groundwater monitoring program. The NCDEQ letter requested the site continue
in Assessment Monitoring at this time. Well MW-4 was abandoned on July 25, 2016, as documented in a Well
Abandonment Report submitted to NCDEQ on August 12, 2016 by SCS Engineers.

Groundwater Flow Rate & Direction

The attached Figure 1 provides a potentiometric surface map utilizing water level data from the First Semi-
Annual 2016 event. Groundwater flow direction for the First Semi-Annual 2016 event was generally to the
northwest, consistent with past reports.

2 

To calculate the average linear groundwater velocity, the hydraulic gradients were measured from the
potentiometric surface map. The groundwater velocities are then calculated from the following equation:
v = [ Ki/n ] * 365

where:
v = groundwater flow velocity (ft/year)
K = hydraulic conductivity (ft/day)
i = hydraulic gradient (ft/ft)
n = effective porosity (dimensionless)

Based on information provided in the “Construction Plan Application” by S&ME, Inc. dated February 20, 1998,
hydraulic conductivity measurements average 1.13 ft/day and the effective porosity measurements average
33%.

During the First Semi-Annual 2016 event, the hydraulic gradient from the southeast to northwest portion of the
site was estimated at 0.0238 ft/ft.

Using the hydraulic conductivity of 1.13 ft/day, the effective porosity of 0.33, and a hydraulic gradient of 0.0238
ft/ft, the calculated groundwater velocity was 0.081 ft/day (30 ft/yr) for the First Semi-Annual 2016 event.

Effectiveness of the Monitoring Systems

The groundwater monitoring well network is designed to detect potential effects on groundwater from the facility.
The designated upgradient monitoring well, MW-1, is positioned to monitor background groundwater quality for
the facility. The remaining three wells (MW-2, MW-3, and MW-5) are positioned in the downgradient position
around the base of the landfill footprint. Each of the wells was sampled during the First Semi-Annual 2016
event.

The surface water monitoring network is designed to detect potential effects on surface water from the facility.
The designated upgradient point, SW-1, is positioned to monitor background surface water quality for the facility.
The designated downgradient point, SW-2, is positioned to monitor surface water quality downgradient from
the landfill. Both surface water monitoring points were sampled during the First Semi-Annual 2016 event.

Based on a review of well and surface water locations, groundwater flow directions, flow gradients, flow rates,
and sampling availability, the present monitoring program is considered sufficient to monitor groundwater and
surface water quality surrounding the facility.

Monitoring Summary

A summary of the inorganic results and organic detections for the First Semi-Annual 2016 event is available on
Table 1. The following is a brief summary of the monitoring data from the First Semi-Annual 2016 event:

Groundwater

 The NC SWSL is the lowest amount of analyte in a sample that can be quantitatively determined with
suitable precision and accuracy. The SWSL is the concentration below which reported analytical results
must be qualified as estimated. No VOCs were detected above an SWSL during the First Semi-Annual
2016 event.

 Three inorganic constituents were reported above the NC 2L Standards: total chromium at MW-5; total
iron at MW-2, MW-3, and MW-5; and total manganese at MW-2, MW-3, and MW-5.

3 

Total Chromium, Iron, and Manganese at MW-5

Review of the Pace Analytical Services, Inc. field sampling form for well MW-5 indicates that the well went dry
after 4.75 gallons were removed. The field turbidity was increasing as the well was approaching dryness.
Therefore it appears that suspended sediment was the likely cause of the increase in total chromium, iron, and
manganese at MW-5. It is recommended that MW-5 be redeveloped in an attempt to lower field turbidity
(suspended sediment) and total metals (i.e. chromium, iron, and manganese). Total metals at well MW-5 will
then be resampled with a peristaltic pump, supplemented with dissolved metals analysis.

Total Iron and Manganese at MW-2 and MW-3

The First Semi-Annual 2016 total iron concentrations at MW-2 (335 ug/L) and MW-3 (2,110 ug/L) are consistent with
the historical total iron concentrations at MW-2 (72.8 to 968 ug/L) and MW-3 (84.2 to 10,500 ug/L), respectively.

The First Semi-Annual 2016 total manganese concentrations at MW-2 (54.3ug/L) and MW-3 (137 ug/L) are consistent
with the historical total manganese concentrations at MW-2 (5.2 to 113 ug/L) and MW-3 (17.3 to 989 ug/L),
respectively.

The total iron and total manganese concentrations in groundwater wells MW-2 and MW-3 appear to be attributable to
naturally occurring conditions at the site and not related to the landfill.

Surface Water

 No VOCs were detected above an SWSL in surface water samples.

 Four inorganic constituents were reported above the NC 2B Standards: total copper at SW-2; total iron
and total manganese at SW-1 and SW-2; and total zinc at SW-2.

Total Iron and Manganese at SW-1

SW-1 is located upgradient to the facility. The First Semi-Annual 2016 concentration of total iron at SW-1 (1,800 ug/L)
is consistent with historical total iron concentrations at upgradient surface water point SW-1 (474 to 2,920 ug/L).

The First Semi-Annual 2016 concentration of total manganese at SW-1 (288 ug/L) is consistent with historical total
manganese concentrations at upgradient surface water point SW-1 (97.3 to 674 ug/L).

The total iron and total manganese concentrations in upgradient surface water point SW-1 appear to be attributable
to naturally occurring conditions at the site and not related to the landfill.

Total Copper, Iron, Manganese, and Zinc at SW-2

Review of the Pace Analytical Services, Inc. field sampling form for surface water point SW-2 indicates that the
field turbidity was >800 NTU during sampling. Therefore it appears that suspended sediment was the likely
cause of the increase in total metals (i.e. copper, iron, manganese, and zinc) at SW-2. It is recommended that
SW-2 be resampled in an attempt to collect a lower field turbidity (i.e. lower suspended sediment) sample. The
SW-2 resample will be analyzed for total metals, supplemented with dissolved metals analysis.

Assessment Activities Summary

In order to delineate the extent of methylene chloride in the vicinity of MW-4, one additional well (MW-5) was
installed downgradient of MW-4 in March 2015 (see Figure 1). Delineation well MW-5 allowed collection of
groundwater samples in the direction of any potential migration.
4 

The only organic compounds that had been confirmed detected above SWSLs at MW-4 are methylene chloride,
tetrahydrofuran, and trichlorofluoromethane. Methylene chloride and trichlorofluoromethane are commonly
found in landfill gas (LFG). Since new downgradient well MW-5 indicated no confirmed VOCs above applicable
NC SWSLs or NC 2L Standards (May and November 2015 events), then the extent of VOC impact had been
considered defined on the landfill property by MW-5. Per a March 8, 2016 NCDEQ letter, MW-4 was approved for
abandonment and replaced with MW-5 in the groundwater monitoring program. The NCDEQ letter requested the
site continue in Assessment Monitoring at this time.

Recommendations

During the First Semi-Annual 2016 event, no VOCs were detected above an SWSL at the groundwater
monitoring wells or surface water samples.

Due to 2L exceedances for total chromium at MW-5, the site will continue in Assessment Monitoring through
the next semi-annual event. Well MW-5 went dry during sampling using a Grundfos submersible pump. During
the week of September 12, 2016, the site plans to redevelop MW-5 and collect a resample utilizing a peristaltic
pump for low flow purging/sampling. Dissolved metals will be collected to supplement the total metal sample
results at MW-5. The site will also attempt to resample surface water point SW-2 for total/dissolved metals,
which exhibited elevated field turbidity and total metals during the First Semi-Annual 2016 event. The MW-5
and SW-2 resampling results will be submitted to NCDEQ upon receipt and review.

The next semi-annual sampling event is tentatively scheduled for November 2016.

Should you have any questions or concerns, please contact Mr. Mike Gurley at [phone] or Steve Jett at
[phone].

Sincerely,

Steve Jett, LG #1825
Owner
Jett Environmental Consulting, PLLC (C-517)

Attachment: Figure 1 – Potentiometric Surface Map
Table 1 – Data Compared to NC Standards, First Semi-Annual 2016 Event
Attachment A - Laboratory Analytical Report & Field Information Forms

cc: Mike Gurley, Republic Services, Inc. (PDF via Email)
Lake Norman Landfill (1 Hardcopy)
Figure

Well Gradient Status
Top of PVC
Casing
Elevation
(fmsl)1
Depth to
Water (ft)2
Groundwater
Elevation (fmsl)
MW-1 Upgradient 745.77 35.32 710.45
MW-2 Downgradient 680.37 11.94 668.43
MW-3 Downgradient 679.60 11.72 667.88
MW-5 Downgradient 680.24 13.5 666.74
Note 1: Top of PVC Casing Elevations from correspondence dated 5/10/02 by S&ME, Inc.
with the exception of MW-5, which was provided by Lawrence Associates on 6/22/15.
Note 2: Depth to water measured by Analytical Services, Inc. on 5/16/16.
Groundwater Elevation Summary Table
Lake Norman Landfill
Table
Constituent Units MDL SWSL NC 2L Std MW-1 MW-2 MW-3 MW-5
Alkalinity as CaCO3 ug/L 1000 1000 NE 85000 25000 30000 60000
Antimony, Total ug/L 0.25 6 NE J 1.32 J 0.43 J 0.28 J 0.3
Arsenic, Total ug/L 0.75 10 10 <10.0 <10.0 <10.0 <10.0
Barium, Total ug/L 0.3 100 700 J 68.4 120 J 36.8 J 73.8
Beryllium, Total ug/L 0.09 1 NE <1.00 <1.00 <1.00 J 0.16
Cadmium, Total ug/L 0.1 1 2 <1.00 <1.00 <1.00 <1.00
Chloride ug/L 1000 1000 250,000 3600 6200 16000 4700
Chromium, Total ug/L 0.43 10 10 <10.0 <10.0 J 1.34 23.9
Cobalt, Total ug/L 0.29 10 NE <10.0 J 1.67 J 2.75 J 5.4
Copper, Total ug/L 0.41 10 1,000 J 1.03 J 0.78 J 4.67 J 2.93
Iron, Total ug/L 5.72 40 300 J 37.8 335 2110 9530
Lead, Total ug/L 0.08 10 15 <10.0 J 0.17 J 0.55 J 1.58
Manganese, Total ug/L 1.04 10 50 J 6.13 54.3 137 763
Mercury, Total ug/L 0.132 0.2 1 <0.200 <0.200 <0.200 <0.200
Nickel, Total ug/L 0.48 50 100 <50.0 <50.0 J 1.59 J 16
pH (Field)su NE NE NE 5.93 5.08 4.94 6.1
Selenium, Total ug/L 0.85 10 20 J 0.95 <10.0 <10.0 J 1.5
Silver, Total ug/L 0.22 10 20 <10.0 <10.0 <10.0 <10.0
Specific Conductance (Field)umhos/cm 1 1 NE 240 198 144 149
Sulfate as SO4 ug/L 5000 5000 250,000 7600 46000 <5000 <5000
Temperature (Field)Deg-C NE NE NE 15.5 14.8 14.1 18.4
Thallium, Total ug/L 0.06 5.5 NE J 0.12 <5.50 <5.50 J 0.11
Total Dissolved Solids (TDS)ug/L 10000 10000 500,000 154000 147000 103000 117000
Turbidity (Field)NTU NE NE NE 0.8 1.21 3.81 8.21
Vanadium, Total ug/L 1.57 25 NE J 4.1 J 2.19 J 7.57 J 17.4
Zinc, Total ug/L 1.3 10 1,000 <10.0 <10.0 J 2.7 21.6
Constituent (ug/L) Units MDL SWSL NC 2B Std SW-1 SW-2
Alkalinity as CaCO3 ug/L 1000 1000 NE 45000 55000
Antimony, Total ug/L 0.25 6 NE <6.00 J 0.32
Arsenic, Total ug/L 0.75 10 10 <10.0 J 2.68
Barium, Total ug/L 0.3 100 1,000 J 43.8 323
Beryllium, Total ug/L 0.09 1 6.5 <1.00 J 0.55
Cadmium, Total ug/L 0.1 1 2 <1.00 <1.00
Chloride ug/L 1000 1000 230,000 5000 3700
Chromium, Total ug/L 0.43 10 20 <10.0 16.2
Cobalt, Total ug/L 0.29 10 NE J 1.02 12.6
Copper, Total ug/L 0.41 10 3 J 0.71 30.5
Dissolved Oxygen (Field)ug/L NE NE NE 7070 5380
Iron, Total ug/L 5.72 40 1,000 1800 40100
Lead, Total ug/L 0.08 10 25 J 0.16 14.7
Manganese, Total ug/L 1.04 10 200 288 801
Mercury, Total ug/L 0.132 0.2 0.012 <0.200 <0.200
Nickel, Total ug/L 0.48 50 8.3 <50.0 J 8.77
pH (Field)su NE NE NE 4.13 5.62
Selenium, Total ug/L 0.85 10 5 <10.0 J 2.8
Silver, Total ug/L 0.22 10 0.06 <10.0 <10.0
Specific Conductance (Field)umhos/cm 1 1 NE 110 131
Sulfate as SO4 ug/L 51 5000 NE J 3300 23000
Temperature (Field)Deg-C NE NE NE 14.5 15.4
Thallium, Total ug/L 0.06 5.5 NE <5.50 <5.50
Total Dissolved Solids (TDS)ug/L 10000 10000 NE 80000 128000
Turbidity (Field)NTU NE NE NE 5.91 >800
Vanadium, Total ug/L 1.57 25 NE J 2.27 105
Zinc, Total ug/L 1.3 10 50 J 3.51 94
Acetone ug/L 4.9 100 2,000 <100 J 6.8
NE: Denotes a NC 2L or 2B Standard is not established.
Only the VOCs detected during this event are displayed on the table.
J: Denotes Sample result above the MDL but below the SWSL; estimated value; value may not be accurate.
Denotes result above an SWSL is also above the NC 2L or 2B Standard:
For NC 2B Standard, lowest value utilized from the classifications from the 2B Table published May 15, 2013.
TABLE 1
FIRST SEMI-ANNUAL 2016 EVENT DATA COMPARED TO NC STANDARDS
LAKE NORMAN C&D LANDFILL
GROUNDWATER SAMPLES
SURFACE WATER SAMPLES
Attachment A
Laboratory Analytical Report
&
Field Information Forms

PACE ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
BFI Waste Systems of North America, LLC
Project: Lake Norman C&D Landfill
Concord, NC 28027
5105 Morehead Rd.
Mr. Mike Gurley
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, Inc. certifies
that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the
samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
June 08, 2016
Report Number:AZE0540
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
5504-MW1 AZE0540-01 05/17/16 11:47 05/18/16 12:45Ground Water
5504-MW2 AZE0540-02 05/17/16 10:08 05/18/16 12:45Ground Water
5504-MW3 AZE0540-03 05/17/16 08:57 05/18/16 12:45Ground Water
5504-MW5 AZE0540-04 05/16/16 15:19 05/18/16 12:45Ground Water
5504-Duplicate AZE0540-05 05/16/16 00:00 05/18/16 12:45Ground Water
5504-Field Blank AZE0540-06 05/17/16 10:10 05/18/16 12:45Water
5504-Trip Blank AZE0540-07 05/16/16 00:00 05/18/16 12:45Water
5504-Equipment Blank AZE0540-08 05/18/16 12:00 05/18/16 12:45Water
5504-SW1 AZE0540-09 05/17/16 08:54 05/18/16 12:45Surface Water
5504-SW2 AZE0540-10 05/17/16 10:21 05/18/16 12:45Surface Water
Page 2 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AZE0540-01 AZE054005/17/16 11:47
Project:Lake Norman C&D Landfill
05/18/16 12:45
On Site
EPA 9050A 240 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 11:4705/17/16 11:47
EPA 9040C 5.93 pH Units1Field - pH 6050530NAPH05/17/16 11:4705/17/16 11:47
SM 2550 B 15.5 °C1Field - Temperature 6050530NATEMP05/17/16 11:4705/17/16 11:47
EPA 180.1 0.80 NTU1Field - Turbidity 6050530NATURB05/17/16 11:4705/17/16 11:47
NA 35.32 feet1Field - Water Level 6050530NAWL05/17/16 11:4705/17/16 11:47
General Chemistry
SM 2320 B 85000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 154000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 3600 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/25/16 23:0605/25/16 13:58
EPA 9056A 7600 ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/25/16 23:0605/25/16 13:58
Metals, Total
EPA 6020B 1.32 ug/L1Antimony6.00 J 6050611EPA 3005A 0.25 7440-36-0 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 13:3805/26/16 08:15
EPA 6020B 68.4 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6050611EPA 3005A 0.29 7440-48-4 05/26/16 13:3805/26/16 08:15
Page 3 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AZE0540-01 AZE054005/17/16 11:47
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 1.03 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Lead10.0 6050611EPA 3005A 0.08 7439-92-1 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6050611EPA 3005A 0.48 7440-02-0 05/26/16 13:3805/26/16 08:15
EPA 6020B 0.95 ug/L1Selenium10.0 J 6050611EPA 3005A 0.85 7782-49-2 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 13:3805/26/16 08:15
EPA 6020B 0.12 ug/L1Thallium5.50 J 6050611EPA 3005A 0.06 7440-28-0 05/26/16 13:3805/26/16 08:15
EPA 6020B 4.10 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 13:3805/26/16 08:15
NDEPA 6020B ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 13:3805/26/16 08:15
EPA 6020B 37.8 ug/L1Iron40.0 J 6050611EPA 3005A 5.72 7439-89-6 05/26/16 13:3805/26/16 08:15
EPA 6020B 6.13 ug/L1Manganese10.0 J 6050611EPA 3005A 1.04 7439-96-5 05/26/16 13:3805/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:0606/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 15:0605/20/16 05:15
Page 4 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AZE0540-01 AZE054005/17/16 11:47
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 15:0605/20/16 05:15
Page 5 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AZE0540-01 AZE054005/17/16 11:47
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 15:0605/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 15:0605/20/16 05:15
EPA 8260B 92 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 15:0605/20/16 05:1580-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 15:0605/20/16 05:1578-120
EPA 8260B 103 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 15:0605/20/16 05:1580-120
EPA 8260B 108 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 15:0605/20/16 05:1580-120
Page 6 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AZE0540-02 AZE054005/17/16 10:08
Project:Lake Norman C&D Landfill
05/18/16 12:45
On Site
EPA 9050A 198 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 10:0805/17/16 10:08
EPA 9040C 5.08 pH Units1Field - pH 6050530NAPH05/17/16 10:0805/17/16 10:08
SM 2550 B 14.8 °C1Field - Temperature 6050530NATEMP05/17/16 10:0805/17/16 10:08
EPA 180.1 1.21 NTU1Field - Turbidity 6050530NATURB05/17/16 10:0805/17/16 10:08
NA 11.94 feet1Field - Water Level 6050530NAWL05/17/16 10:0805/17/16 10:08
General Chemistry
SM 2320 B 25000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 147000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 6200 ug/L2Chloride2000 6050603EPA 9056A 2000 16887-00-6 05/25/16 23:2705/25/16 13:58
EPA 9056A 46000 ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 06/01/16 16:4905/25/16 13:58
Metals, Total
EPA 6020B 0.43 ug/L1Antimony6.00 J 6050611EPA 3005A 0.25 7440-36-0 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 13:4305/26/16 08:15
EPA 6020B 120 ug/L1Barium100 6050611EPA 3005A 0.30 7440-39-3 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 13:4305/26/16 08:15
EPA 6020B 1.67 ug/L1Cobalt10.0 J 6050611EPA 3005A 0.29 7440-48-4 05/26/16 13:4305/26/16 08:15
Page 7 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AZE0540-02 AZE054005/17/16 10:08
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 0.78 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 13:4305/26/16 08:15
EPA 6020B 0.17 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6050611EPA 3005A 0.48 7440-02-0 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6050611EPA 3005A 0.85 7782-49-2 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 13:4305/26/16 08:15
EPA 6020B 2.19 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 13:4305/26/16 08:15
NDEPA 6020B ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 13:4305/26/16 08:15
EPA 6020B 335 ug/L1Iron40.0 6050611EPA 3005A 5.72 7439-89-6 05/26/16 13:4305/26/16 08:15
EPA 6020B 54.3 ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 13:4305/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:0806/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 15:3105/20/16 05:15
Page 8 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AZE0540-02 AZE054005/17/16 10:08
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 15:3105/20/16 05:15
Page 9 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AZE0540-02 AZE054005/17/16 10:08
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 15:3105/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 15:3105/20/16 05:15
EPA 8260B 93 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 15:3105/20/16 05:1580-120
EPA 8260B 104 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 15:3105/20/16 05:1578-120
EPA 8260B 101 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 15:3105/20/16 05:1580-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 15:3105/20/16 05:1580-120
Page 10 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AZE0540-03 AZE054005/17/16 08:57
Project:Lake Norman C&D Landfill
05/18/16 12:45
On Site
EPA 9050A 144 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 08:5705/17/16 08:57
EPA 9040C 4.94 pH Units1Field - pH 6050530NAPH05/17/16 08:5705/17/16 08:57
SM 2550 B 14.1 °C1Field - Temperature 6050530NATEMP05/17/16 08:5705/17/16 08:57
EPA 180.1 3.81 NTU1Field - Turbidity 6050530NATURB05/17/16 08:5705/17/16 08:57
NA 11.72 feet1Field - Water Level 6050530NAWL05/17/16 08:5705/17/16 08:57
General Chemistry
SM 2320 B 30000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 103000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 16000 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/25/16 23:4705/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/25/16 23:4705/25/16 13:58
Metals, Total
EPA 6020B 0.28 ug/L1Antimony6.00 J 6050611EPA 3005A 0.25 7440-36-0 05/26/16 13:4805/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 13:4805/26/16 08:15
EPA 6020B 36.8 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 13:4805/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 13:4805/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 13:4805/26/16 08:15
EPA 6020B 1.34 ug/L1Chromium10.0 J 6050611EPA 3005A 0.43 7440-47-3 05/26/16 13:4805/26/16 08:15
EPA 6020B 2.75 ug/L1Cobalt10.0 J 6050611EPA 3005A 0.29 7440-48-4 05/26/16 13:4805/26/16 08:15
Page 11 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AZE0540-03 AZE054005/17/16 08:57
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 4.67 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 13:4805/26/16 08:15
EPA 6020B 0.55 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 13:4805/26/16 08:15
EPA 6020B 1.59 ug/L1Nickel50.0 J 6050611EPA 3005A 0.48 7440-02-0 05/26/16 13:4805/26/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6050611EPA 3005A 0.85 7782-49-2 05/26/16 13:4805/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 13:4805/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 13:4805/26/16 08:15
EPA 6020B 7.57 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 13:4805/26/16 08:15
EPA 6020B 2.70 ug/L1Zinc10.0 J 6050611EPA 3005A 1.30 7440-66-6 05/26/16 13:4805/26/16 08:15
EPA 6020B 2110 ug/L1Iron40.0 6050611EPA 3005A 5.72 7439-89-6 05/26/16 13:4805/26/16 08:15
EPA 6020B 137 ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 13:4805/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:1106/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 15:5705/20/16 05:15
Page 12 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AZE0540-03 AZE054005/17/16 08:57
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 15:5705/20/16 05:15
Page 13 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AZE0540-03 AZE054005/17/16 08:57
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 15:5705/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 15:5705/20/16 05:15
EPA 8260B 91 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 15:5705/20/16 05:1580-120
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 15:5705/20/16 05:1578-120
EPA 8260B 99 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 15:5705/20/16 05:1580-120
EPA 8260B 107 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 15:5705/20/16 05:1580-120
Page 14 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AZE0540-04 AZE054005/16/16 15:19
Project:Lake Norman C&D Landfill
05/18/16 12:45
On Site
EPA 9050A 149 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/16/16 15:1905/16/16 15:19
EPA 9040C 6.10 pH Units1Field - pH 6050530NAPH05/16/16 15:1905/16/16 15:19
SM 2550 B 18.4 °C1Field - Temperature 6050530NATEMP05/16/16 15:1905/16/16 15:19
EPA 180.1 8.21 NTU1Field - Turbidity 6050530NATURB05/16/16 15:1905/16/16 15:19
NA 13.50 feet1Field - Water Level 6050530NAWL05/16/16 15:1905/16/16 15:19
General Chemistry
SM 2320 B 60000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 117000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 4700 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 00:0805/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 00:0805/25/16 13:58
Metals, Total
EPA 6020B 0.30 ug/L1Antimony6.00 J 6050611EPA 3005A 0.25 7440-36-0 05/26/16 13:5305/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 13:5305/26/16 08:15
EPA 6020B 73.8 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 13:5305/26/16 08:15
EPA 6020B 0.16 ug/L1Beryllium1.00 J 6050611EPA 3005A 0.09 7440-41-7 05/26/16 13:5305/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 13:5305/26/16 08:15
EPA 6020B 23.9 ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 13:5305/26/16 08:15
EPA 6020B 5.40 ug/L1Cobalt10.0 J 6050611EPA 3005A 0.29 7440-48-4 05/26/16 13:5305/26/16 08:15
Page 15 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AZE0540-04 AZE054005/16/16 15:19
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 2.93 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 13:5305/26/16 08:15
EPA 6020B 1.58 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 13:5305/26/16 08:15
EPA 6020B 16.0 ug/L1Nickel50.0 J 6050611EPA 3005A 0.48 7440-02-0 05/26/16 13:5305/26/16 08:15
EPA 6020B 1.50 ug/L1Selenium10.0 J 6050611EPA 3005A 0.85 7782-49-2 05/26/16 13:5305/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 13:5305/26/16 08:15
EPA 6020B 0.11 ug/L1Thallium5.50 J 6050611EPA 3005A 0.06 7440-28-0 05/26/16 13:5305/26/16 08:15
EPA 6020B 17.4 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 13:5305/26/16 08:15
EPA 6020B 21.6 ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 13:5305/26/16 08:15
EPA 6020B 9530 ug/L5Iron200 6050611EPA 3005A 28.6 7439-89-6 06/03/16 17:1705/26/16 08:15
EPA 6020B 763 ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 13:5305/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:1306/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 16:2205/20/16 05:15
Page 16 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AZE0540-04 AZE054005/16/16 15:19
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 16:2205/20/16 05:15
Page 17 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AZE0540-04 AZE054005/16/16 15:19
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 16:2205/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 16:2205/20/16 05:15
EPA 8260B 92 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 16:2205/20/16 05:1580-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 16:2205/20/16 05:1578-120
EPA 8260B 102 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 16:2205/20/16 05:1580-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 16:2205/20/16 05:1580-120
Page 18 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AZE0540-05 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
General Chemistry
SM 2320 B 55000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 90000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 4700 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 00:2905/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 00:2905/25/16 13:58
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050611EPA 3005A 0.25 7440-36-0 05/26/16 13:5805/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 13:5805/26/16 08:15
EPA 6020B 76.4 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 13:5805/26/16 08:15
EPA 6020B 0.16 ug/L1Beryllium1.00 J 6050611EPA 3005A 0.09 7440-41-7 05/26/16 13:5805/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 13:5805/26/16 08:15
EPA 6020B 25.0 ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 13:5805/26/16 08:15
EPA 6020B 5.60 ug/L1Cobalt10.0 J 6050611EPA 3005A 0.29 7440-48-4 05/26/16 13:5805/26/16 08:15
EPA 6020B 3.05 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 13:5805/26/16 08:15
EPA 6020B 1.69 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 13:5805/26/16 08:15
EPA 6020B 16.4 ug/L1Nickel50.0 J 6050611EPA 3005A 0.48 7440-02-0 05/26/16 13:5805/26/16 08:15
EPA 6020B 1.22 ug/L1Selenium10.0 J 6050611EPA 3005A 0.85 7782-49-2 05/26/16 13:5805/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 13:5805/26/16 08:15
EPA 6020B 0.11 ug/L1Thallium5.50 J 6050611EPA 3005A 0.06 7440-28-0 05/26/16 13:5805/26/16 08:15
EPA 6020B 18.2 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 13:5805/26/16 08:15
Page 19 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AZE0540-05 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 22.8 ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 13:5805/26/16 08:15
EPA 6020B 10200 ug/L5Iron200 6050611EPA 3005A 28.6 7439-89-6 05/26/16 17:2205/26/16 08:15
EPA 6020B 820 ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 13:5805/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:1506/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 16:4705/20/16 05:15
Page 20 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AZE0540-05 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 16:4705/20/16 05:15
Page 21 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AZE0540-05 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 16:4705/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 16:4705/20/16 05:15
EPA 8260B 90 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 16:4705/20/16 05:1580-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 16:4705/20/16 05:1578-120
EPA 8260B 101 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 16:4705/20/16 05:1580-120
EPA 8260B 107 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 16:4705/20/16 05:1580-120
Page 22 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AZE0540-06 AZE054005/17/16 10:10
Project:Lake Norman C&D Landfill
05/18/16 12:45
General Chemistry
NDSM 2320 B ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 47000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
NDEPA 9056A ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 02:1205/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 02:1205/25/16 13:58
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050611EPA 3005A 0.25 7440-36-0 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Barium100 6050611EPA 3005A 0.30 7440-39-3 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6050611EPA 3005A 0.29 7440-48-4 05/26/16 14:1205/26/16 08:15
EPA 6020B 6.11 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Lead10.0 6050611EPA 3005A 0.08 7439-92-1 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6050611EPA 3005A 0.48 7440-02-0 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6050611EPA 3005A 0.85 7782-49-2 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6050611EPA 3005A 1.57 7440-62-2 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 14:1205/26/16 08:15
Page 23 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AZE0540-06 AZE054005/17/16 10:10
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 10.3 ug/L1Iron40.0 J 6050611EPA 3005A 5.72 7439-89-6 05/26/16 14:1205/26/16 08:15
NDEPA 6020B ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 14:1205/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:1806/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 07:0605/20/16 05:15
Page 24 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AZE0540-06 AZE054005/17/16 10:10
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 07:0605/20/16 05:15
EPA 8260B 0.7 ug/L1Methylene Chloride 1.0 J 6050502EPA 5030B 0.5 75-09-2 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 07:0605/20/16 05:15
Page 25 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AZE0540-06 AZE054005/17/16 10:10
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 07:0605/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 07:0605/20/16 05:15
EPA 8260B 92 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 07:0605/20/16 05:1580-120
EPA 8260B 98 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 07:0605/20/16 05:1578-120
EPA 8260B 102 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 07:0605/20/16 05:1580-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 07:0605/20/16 05:1580-120
Page 26 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Trip Blank
Water
AZE0540-07 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 07:3105/20/16 05:15
Page 27 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Trip Blank
Water
AZE0540-07 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 07:3105/20/16 05:15
Page 28 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Trip Blank
Water
AZE0540-07 AZE054005/16/16 00:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 07:3105/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 07:3105/20/16 05:15
EPA 8260B 91 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 07:3105/20/16 05:1580-120
EPA 8260B 99 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 07:3105/20/16 05:1578-120
EPA 8260B 101 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 07:3105/20/16 05:1580-120
EPA 8260B 108 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 07:3105/20/16 05:1580-120
Page 29 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AZE0540-08 AZE054005/18/16 12:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
General Chemistry
NDSM 2320 B ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 27000 ug/L1Total Dissolved Solids 10000 6050523SM 2540 C 10000 E-10173 05/24/16 18:5005/24/16 18:50
Inorganic Anions
NDEPA 9056A ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 02:3305/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 02:3305/25/16 13:58
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050611EPA 3005A 0.25 7440-36-0 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 14:1705/26/16 08:15
EPA 6020B 0.34 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6050611EPA 3005A 0.29 7440-48-4 05/26/16 14:1705/26/16 08:15
EPA 6020B 6.51 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 14:1705/26/16 08:15
EPA 6020B 0.11 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6050611EPA 3005A 0.48 7440-02-0 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6050611EPA 3005A 0.85 7782-49-2 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6050611EPA 3005A 1.57 7440-62-2 05/26/16 14:1705/26/16 08:15
Page 30 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AZE0540-08 AZE054005/18/16 12:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
NDEPA 6020B ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 14:1705/26/16 08:15
EPA 6020B 15.7 ug/L1Iron40.0 J 6050611EPA 3005A 5.72 7439-89-6 05/26/16 14:1705/26/16 08:15
NDEPA 6020B ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 14:1705/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:2006/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 07:5605/20/16 05:15
Page 31 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AZE0540-08 AZE054005/18/16 12:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 07:5605/20/16 05:15
EPA 8260B 1.0 ug/L1Methylene Chloride 1.0 J 6050502EPA 5030B 0.5 75-09-2 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 07:5605/20/16 05:15
Page 32 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AZE0540-08 AZE054005/18/16 12:00
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 07:5605/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 07:5605/20/16 05:15
EPA 8260B 93 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 07:5605/20/16 05:1580-120
EPA 8260B 99 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 07:5605/20/16 05:1578-120
EPA 8260B 102 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 07:5605/20/16 05:1580-120
EPA 8260B 109 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 07:5605/20/16 05:1580-120
Page 33 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AZE0540-09 AZE054005/17/16 08:54
Project:Lake Norman C&D Landfill
05/18/16 12:45
On Site
EPA 9050A 110 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 08:5405/17/16 08:54
SM 4500-O G 7070 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 08:5405/17/16 08:54
EPA 9040C 4.13 pH Units1Field - pH 6050530NAPH05/17/16 08:5405/17/16 08:54
SM 2550 B 14.5 °C1Field - Temperature 6050530NATEMP05/17/16 08:5405/17/16 08:54
EPA 180.1 5.91 NTU1Field - Turbidity 6050530NATURB05/17/16 08:5405/17/16 08:54
General Chemistry
SM 2320 B 45000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 80000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 5000 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 02:5305/25/16 13:58
EPA 9056A 3300 ug/L1Sulfate5000 J 6050603EPA 9056A 51 14808-79-8 05/26/16 02:5305/25/16 13:58
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050611EPA 3005A 0.25 7440-36-0 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 14:2205/26/16 08:15
EPA 6020B 43.8 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 14:2205/26/16 08:15
EPA 6020B 1.02 ug/L1Cobalt10.0 J 6050611EPA 3005A 0.29 7440-48-4 05/26/16 14:2205/26/16 08:15
Page 34 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AZE0540-09 AZE054005/17/16 08:54
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 0.71 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 14:2205/26/16 08:15
EPA 6020B 0.16 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6050611EPA 3005A 0.48 7440-02-0 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6050611EPA 3005A 0.85 7782-49-2 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 14:2205/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 14:2205/26/16 08:15
EPA 6020B 2.27 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 14:2205/26/16 08:15
EPA 6020B 3.51 ug/L1Zinc10.0 J 6050611EPA 3005A 1.30 7440-66-6 05/26/16 14:2205/26/16 08:15
EPA 6020B 1800 ug/L1Iron40.0 6050611EPA 3005A 5.72 7439-89-6 05/26/16 14:2205/26/16 08:15
EPA 6020B 288 ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 14:2205/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:5706/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 17:1305/20/16 05:15
Page 35 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AZE0540-09 AZE054005/17/16 08:54
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 17:1305/20/16 05:15
Page 36 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AZE0540-09 AZE054005/17/16 08:54
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050502EPA 5030B 1.7 108-10-1 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 4.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 17:1305/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 17:1305/20/16 05:15
EPA 8260B 93 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 17:1305/20/16 05:1580-120
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 17:1305/20/16 05:1578-120
EPA 8260B 102 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 17:1305/20/16 05:1580-120
EPA 8260B 108 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 17:1305/20/16 05:1580-120
Page 37 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AZE0540-10 AZE054005/17/16 10:21
Project:Lake Norman C&D Landfill
05/18/16 12:45
On Site
EPA 9050A 131 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 10:2105/17/16 10:21
SM 4500-O G 5380 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 10:2105/17/16 10:21
EPA 9040C 5.62 pH Units1Field - pH 6050530NAPH05/17/16 10:2105/17/16 10:21
SM 2550 B 15.4 °C1Field - Temperature 6050530NATEMP05/17/16 10:2105/17/16 10:21
EPA 180.1 800 NTU1Field - Turbidity >6050530NATURB05/17/16 10:2105/17/16 10:21
General Chemistry
SM 2320 B 55000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 128000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 3700 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 03:3505/25/16 13:58
EPA 9056A 23000 ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 06/01/16 18:1205/25/16 13:58
Metals, Total
EPA 6020B 0.32 ug/L1Antimony6.00 J 6050611EPA 3005A 0.25 7440-36-0 05/26/16 14:2705/26/16 08:15
EPA 6020B 2.68 ug/L1Arsenic10.0 J 6050611EPA 3005A 0.75 7440-38-2 05/26/16 14:2705/26/16 08:15
EPA 6020B 323 ug/L1Barium100 6050611EPA 3005A 0.30 7440-39-3 05/26/16 14:2705/26/16 08:15
EPA 6020B 0.55 ug/L5Beryllium1.00 J 6050611EPA 3005A 0.47 7440-41-7 06/03/16 15:5505/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 14:2705/26/16 08:15
EPA 6020B 16.2 ug/L1Chromium10.0 6050611EPA 3005A 0.43 7440-47-3 05/26/16 14:2705/26/16 08:15
EPA 6020B 12.6 ug/L1Cobalt10.0 6050611EPA 3005A 0.29 7440-48-4 05/26/16 14:2705/26/16 08:15
Page 38 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AZE0540-10 AZE054005/17/16 10:21
Project:Lake Norman C&D Landfill
05/18/16 12:45
Metals, Total
EPA 6020B 30.5 ug/L1Copper10.0 6050611EPA 3005A 0.41 7440-50-8 05/26/16 14:2705/26/16 08:15
EPA 6020B 14.7 ug/L1Lead10.0 6050611EPA 3005A 0.08 7439-92-1 05/26/16 14:2705/26/16 08:15
EPA 6020B 8.77 ug/L1Nickel50.0 J 6050611EPA 3005A 0.48 7440-02-0 05/26/16 14:2705/26/16 08:15
EPA 6020B 2.80 ug/L1Selenium10.0 J 6050611EPA 3005A 0.85 7782-49-2 05/26/16 14:2705/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 14:2705/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 14:2705/26/16 08:15
EPA 6020B 105 ug/L1Vanadium25.0 6050611EPA 3005A 1.57 7440-62-2 05/26/16 14:2705/26/16 08:15
EPA 6020B 94.0 ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 14:2705/26/16 08:15
EPA 6020B 40100 ug/L10Iron400 6050611EPA 3005A 57.2 7439-89-6 06/03/16 16:0005/26/16 08:15
EPA 6020B 801 ug/L1Manganese10.0 6050611EPA 3005A 1.04 7439-96-5 05/26/16 14:2705/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 15:5906/01/16 15:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 6.8 ug/L1Acetone100 J 6050503EPA 5030B 4.9 67-64-1 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6050503EPA 5030B 1.8 107-13-1 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6050503EPA 5030B 0.2 71-43-2 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6050503EPA 5030B 0.7 74-97-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050503EPA 5030B 0.6 75-27-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6050503EPA 5030B 0.7 75-25-2 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6050503EPA 5030B 0.8 74-83-9 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6050503EPA 5030B 0.6 75-15-0 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050503EPA 5030B 0.6 56-23-5 05/20/16 17:3805/20/16 12:00
Page 39 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AZE0540-10 AZE054005/17/16 10:21
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 6050503EPA 5030B 0.4 108-90-7 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6050503EPA 5030B 0.4 75-00-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6050503EPA 5030B 0.3 67-66-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6050503EPA 5030B 0.4 74-87-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050503EPA 5030B 0.7 124-48-1 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050503EPA 5030B 2.0 96-12-8 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050503EPA 5030B 0.7 106-93-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6050503EPA 5030B 0.7 74-95-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050503EPA 5030B 0.5 95-50-1 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050503EPA 5030B 0.3 106-46-7 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050503EPA 5030B 1.5 110-57-6 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050503EPA 5030B 0.4 75-34-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050503EPA 5030B 0.3 107-06-2 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050503EPA 5030B 0.5 75-35-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050503EPA 5030B 0.5 156-59-2 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050503EPA 5030B 0.4 156-60-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050503EPA 5030B 0.5 78-87-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050503EPA 5030B 0.4 10061-01-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050503EPA 5030B 0.4 10061-02-6 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6050503EPA 5030B 0.2 100-41-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6050503EPA 5030B 0.6 74-88-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050503EPA 5030B 0.9 591-78-6 05/20/16 17:3805/20/16 12:00
Page 40 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AZE0540-10 AZE054005/17/16 10:21
Project:Lake Norman C&D Landfill
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050503EPA 5030B 0.5 75-09-2 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050503EPA 5030B 1.1 78-93-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 6050503EPA 5030B 1.7 108-10-1 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6050503EPA 5030B 0.4 100-42-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050503EPA 5030B 0.6 630-20-6 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050503EPA 5030B 0.5 79-34-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050503EPA 5030B 0.4 127-18-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6050503EPA 5030B 0.3 108-88-3 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050503EPA 5030B 0.4 71-55-6 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050503EPA 5030B 0.8 79-00-5 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6050503EPA 5030B 0.4 79-01-6 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050503EPA 5030B 0.5 75-69-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050503EPA 5030B 0.7 96-18-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6050503EPA 5030B 0.8 108-05-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050503EPA 5030B 0.7 75-01-4 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Xylenes, total 4.0 6050503EPA 5030B 0.4 1330-20-7 05/20/16 17:3805/20/16 12:00
NDEPA 8260B ug/L1Tetrahydrofuran10 6050503EPA 5030B 1.5 109-99-9 05/20/16 17:3805/20/16 12:00
EPA 8260B 93 %Surr: Dibromofluoromethane 6050503EPA 5030B 1868-53-7 05/20/16 17:3805/20/16 12:0080-120
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6050503EPA 5030B 17060-07-0 05/20/16 17:3805/20/16 12:0078-120
EPA 8260B 100 %Surr: Toluene-d8 6050503EPA 5030B 2037-26-5 05/20/16 17:3805/20/16 12:0080-120
EPA 8260B 108 %Surr: 4-Bromofluorobenzene 6050503EPA 5030B 460-00-4 05/20/16 17:3805/20/16 12:0080-120
Page 41 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6050450 - SM 2320 B
Blank (6050450-BLK1)Prepared & Analyzed: 05/19/16
Alkalinity as CaCO3 ug/LND1000
LCS (6050450-BS1)Prepared & Analyzed: 05/19/16
Alkalinity as CaCO3 ug/L1000001000 100000 85-115100
Duplicate (6050450-DUP1)Prepared & Analyzed: 05/19/16 Source: AZE0540-01
Alkalinity as CaCO3 ug/L850001000 85000 100
Batch 6050522 - SM 2540 C
Blank (6050522-BLK1)Prepared & Analyzed: 05/23/16
Total Dissolved Solids ug/LND10000
LCS (6050522-BS1)Prepared & Analyzed: 05/23/16
Total Dissolved Solids ug/L40000010000 400000 84-108100
Duplicate (6050522-DUP1)Prepared & Analyzed: 05/23/16 Source: AZE0540-03
Total Dissolved Solids ug/L9600010000 103000 107
Duplicate (6050522-DUP2)Prepared & Analyzed: 05/23/16 Source: AZE0540-10
Total Dissolved Solids ug/L14100010000 128000 1010
Batch 6050523 - SM 2540 C
Blank (6050523-BLK1)Prepared & Analyzed: 05/24/16
Total Dissolved Solids ug/LND10000
Page 42 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6050523 - SM 2540 C
LCS (6050523-BS1)Prepared & Analyzed: 05/24/16
Total Dissolved Solids ug/L40100010000 400000 84-108100
Duplicate (6050523-DUP1)Prepared & Analyzed: 05/24/16 Source: AZE0546-11
Total Dissolved Solids ug/L23000050000 215000 107
Page 43 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 6050603 - EPA 9056A
Blank (6050603-BLK1)Prepared & Analyzed: 05/25/16
Chloride ug/LND1000
Sulfate ug/LND5000
LCS (6050603-BS1)Prepared & Analyzed: 05/25/16
Chloride ug/L96701000 10010 90-11097
Sulfate ug/L97705000 10010 90-11098
Matrix Spike (6050603-MS1)Prepared & Analyzed: 05/25/16 Source: AZE0694-01
Chloride ug/L731001000 10010 86100 QM-0290-1100
Sulfate ug/L183005000 10010 ND QM-0590-110183
Matrix Spike (6050603-MS2)Prepared: 05/25/16 Analyzed: 05/26/16 Source: AZE0540-09
Chloride ug/L149001000 10010 5010 90-11099
Sulfate ug/L128005000 10010 3330 90-11094
Matrix Spike Dup (6050603-MSD1)Prepared & Analyzed: 05/25/16 Source: AZE0694-01
Chloride ug/L730001000 10010 86100 15 QM-0290-1100 0.1
Sulfate ug/L183005000 10010 ND 15 QM-0590-110183 0.1
Page 44 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
Blank (6050611-BLK1)Prepared & Analyzed: 05/26/16
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Iron ug/LND40.0
Lead ug/LND10.0
Manganese ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6050611-BS1)Prepared & Analyzed: 05/26/16
Antimony ug/L98.6 6.00 100.00 80-12099
Arsenic ug/L98.7 10.0 100.00 80-12099
Barium ug/L99.8 100 100.00 J80-120100
Beryllium ug/L98.6 1.00 100.00 80-12099
Cadmium ug/L96.9 1.00 100.00 80-12097
Chromium ug/L10010.0 100.00 80-120100
Cobalt ug/L97.2 10.0 100.00 80-12097
Copper ug/L96.4 10.0 100.00 80-12096
Page 45 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
LCS (6050611-BS1)Prepared & Analyzed: 05/26/16
Iron ug/L100040.0 1000.0 80-120100
Lead ug/L95.9 10.0 100.00 80-12096
Manganese ug/L10410.0 100.00 80-120104
Nickel ug/L99.2 50.0 100.00 80-12099
Selenium ug/L10210.0 100.00 80-120102
Silver ug/L10010.0 100.00 80-120100
Thallium ug/L97.4 5.50 100.00 80-12097
Vanadium ug/L99.9 25.0 100.00 80-120100
Zinc ug/L99.1 10.0 100.00 80-12099
Matrix Spike (6050611-MS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Antimony ug/L99.4 6.00 100.00 1.32 75-12598
Arsenic ug/L95.9 10.0 100.00 ND 75-12596
Barium ug/L176100 100.00 68.4 75-125107
Beryllium ug/L98.7 1.00 100.00 ND 75-12599
Cadmium ug/L93.9 1.00 100.00 ND 75-12594
Chromium ug/L10210.0 100.00 ND 75-125102
Cobalt ug/L98.3 10.0 100.00 ND 75-12598
Copper ug/L96.5 10.0 100.00 1.03 75-12595
Iron ug/L101040.0 1000.0 37.8 75-12597
Lead ug/L96.0 10.0 100.00 ND 75-12596
Manganese ug/L10810.0 100.00 6.13 75-125102
Nickel ug/L95.9 50.0 100.00 ND 75-12596
Selenium ug/L95.5 10.0 100.00 0.95 75-12595
Silver ug/L98.9 10.0 100.00 ND 75-12599
Thallium ug/L98.2 5.50 100.00 0.12 75-12598
Vanadium ug/L10525.0 100.00 4.10 75-125101
Page 46 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
Matrix Spike (6050611-MS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Zinc ug/L98.6 10.0 100.00 ND 75-12599
Matrix Spike Dup (6050611-MSD1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Antimony ug/L96.1 6.00 100.00 1.32 2075-12595 3
Arsenic ug/L96.7 10.0 100.00 ND 2075-12597 0.8
Barium ug/L173100 100.00 68.4 2075-125105 1
Beryllium ug/L1021.00 100.00 ND 2075-125102 4
Cadmium ug/L97.7 1.00 100.00 ND 2075-12598 4
Chromium ug/L10510.0 100.00 ND 2075-125105 3
Cobalt ug/L10210.0 100.00 ND 2075-125102 3
Copper ug/L97.9 10.0 100.00 1.03 2075-12597 1
Iron ug/L104040.0 1000.0 37.8 2075-125100 3
Lead ug/L96.7 10.0 100.00 ND 2075-12597 0.8
Manganese ug/L10910.0 100.00 6.13 2075-125103 1
Nickel ug/L10050.0 100.00 ND 2075-125100 4
Selenium ug/L98.7 10.0 100.00 0.95 2075-12598 3
Silver ug/L99.2 10.0 100.00 ND 2075-12599 0.3
Thallium ug/L98.2 5.50 100.00 0.12 2075-12598 0.06
Vanadium ug/L10625.0 100.00 4.10 2075-125101 0.7
Zinc ug/L97.6 10.0 100.00 ND 2075-12598 1
Post Spike (6050611-PS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Antimony ug/L90.5 100.00 1.32 80-12089
Arsenic ug/L95.0 100.00 0.58 80-12094
Barium ug/L174 100.00 68.4 80-120105
Beryllium ug/L104 100.00 0.02 80-120104
Cadmium ug/L97.7 100.00 0.007 80-12098
Page 47 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
Post Spike (6050611-PS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Chromium ug/L101 100.00 0.15 80-120101
Cobalt ug/L102 100.00 0.03 80-120102
Copper ug/L96.9 100.00 1.03 80-12096
Iron ug/L1020 1000.0 37.8 80-12098
Lead ug/L95.0 100.00 0.01 80-12095
Manganese ug/L109 100.00 6.13 80-120103
Nickel ug/L99.3 100.00 0.11 80-12099
Selenium ug/L99.5 100.00 0.95 80-12099
Silver ug/L99.4 100.00 0.10 80-12099
Thallium ug/L97.1 100.00 0.12 80-12097
Vanadium ug/L107 100.00 4.10 80-120103
Zinc ug/L97.4 100.00 0.52 80-12097
Batch 6060013 - EPA 7470A
Blank (6060013-BLK1)Prepared: 06/01/16 Analyzed: 06/02/16
Mercury ug/LND0.200
LCS (6060013-BS1)Prepared: 06/01/16 Analyzed: 06/02/16
Mercury ug/L2.13 0.200 2.5000 80-12085
Duplicate (6060013-DUP1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0475-19RE1
Mercury ug/L1.35 0.200 1.19 2012
Duplicate (6060013-DUP2)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0475-57RE1
Mercury ug/L0.659 0.200 0.675 202
Page 48 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6060013 - EPA 7470A
Matrix Spike (6060013-MS1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0546-06
Mercury ug/L1.84 0.200 2.5000 ND QM-0575-12574
Matrix Spike Dup (6060013-MSD1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0546-06
Mercury ug/L1.77 0.200 2.5000 ND 20 QM-0575-12571 4
Post Spike (6060013-PS1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0546-06
Mercury ug/L1.30 1.6667 0.074 QM-0580-12073
Page 49 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
Blank (6050502-BLK1)Prepared & Analyzed: 05/20/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND1.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Page 50 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
Blank (6050502-BLK1)Prepared & Analyzed: 05/20/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND50
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND1.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND4.0
Tetrahydrofuran ug/LND10
ug/L 50.000 80-120Surr: Dibromofluoromethane 9346
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10050
ug/L 50.000 80-120Surr: Toluene-d8 10251
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Page 51 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
LCS (6050502-BS1)Prepared & Analyzed: 05/20/16
Benzene ug/L51 50.000 67-134101
Chlorobenzene ug/L51 50.000 69-122103
1,1-Dichloroethene ug/L49 50.000 58-14298
Toluene ug/L50 50.000 68-127101
Trichloroethene ug/L53 50.000 72-132106
Tetrahydrofuran ug/LND10 62-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 9548
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10150
ug/L 50.000 80-120Surr: Toluene-d8 10151
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Matrix Spike (6050502-MS1)Prepared & Analyzed: 05/20/16 Source: AZE0496-20
Benzene ug/L51 50.000 ND 67-134101
Chlorobenzene ug/L50 50.000 ND 69-122101
1,1-Dichloroethene ug/L52 50.000 ND 58-142103
Toluene ug/L50 50.000 ND 68-127100
Trichloroethene ug/L53 50.000 ND 72-132107
Tetrahydrofuran ug/LND10 ND 62-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 9146
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10151
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Matrix Spike Dup (6050502-MSD1)Prepared & Analyzed: 05/20/16 Source: AZE0496-20
Benzene ug/L52 50.000 ND 967-134104 3
Page 52 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
Matrix Spike Dup (6050502-MSD1)Prepared & Analyzed: 05/20/16 Source: AZE0496-20
Chlorobenzene ug/L52 50.000 ND 1369-122104 3
1,1-Dichloroethene ug/L53 50.000 ND 958-142105 2
Toluene ug/L50 50.000 ND 968-127101 0.6
Trichloroethene ug/L54 50.000 ND 1172-132109 2
Tetrahydrofuran ug/LND10 ND 5362-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 9347
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10150
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Batch 6050503 - EPA 5030B
Blank (6050503-BLK1)Prepared & Analyzed: 05/20/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Page 53 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050503 - EPA 5030B
Blank (6050503-BLK1)Prepared & Analyzed: 05/20/16
Dibromochloromethane ug/LND1.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND50
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND1.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
Page 54 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050503 - EPA 5030B
Blank (6050503-BLK1)Prepared & Analyzed: 05/20/16
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND4.0
Tetrahydrofuran ug/LND10
ug/L 50.000 80-120Surr: Dibromofluoromethane 9447
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10151
ug/L 50.000 80-120Surr: Toluene-d8 10351
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10553
LCS (6050503-BS1)Prepared & Analyzed: 05/20/16
Benzene ug/L52 50.000 67-134104
Chlorobenzene ug/L55 50.000 69-122109
1,1-Dichloroethene ug/L53 50.000 58-142105
Toluene ug/L51 50.000 68-127101
Trichloroethene ug/L53 50.000 72-132106
Tetrahydrofuran ug/LND10 62-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 9447
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10151
ug/L 50.000 80-120Surr: Toluene-d8 10351
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Page 55 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050503 - EPA 5030B
Matrix Spike (6050503-MS1)Prepared & Analyzed: 05/20/16 Source: AZE0540-10
Benzene ug/L51 50.000 ND 67-134103
Chlorobenzene ug/L52 50.000 ND 69-122104
1,1-Dichloroethene ug/L51 50.000 ND 58-142103
Toluene ug/L50 50.000 ND 68-127100
Trichloroethene ug/L53 50.000 ND 72-132105
Tetrahydrofuran ug/LND10 ND 62-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 9346
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10251
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10553
Matrix Spike Dup (6050503-MSD1)Prepared & Analyzed: 05/20/16 Source: AZE0540-10
Benzene ug/L51 50.000 ND 967-134102 0.9
Chlorobenzene ug/L51 50.000 ND 1369-122103 0.7
1,1-Dichloroethene ug/L51 50.000 ND 958-142102 0.4
Toluene ug/L49 50.000 ND 968-12799 1
Trichloroethene ug/L52 50.000 ND 1172-132105 0.8
Tetrahydrofuran ug/LND10 ND 5362-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 9347
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10251
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10754
Page 56 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
E87315FL DOH NELAC (Drinking Water) Eff: 07/01/2015 06/30/2016NELDW
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2017TX
1340Virginia 12/14/2016VA
Page 57 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix interference. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
>Greater than the result value reported.
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 58 of 59
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley June 08, 2016
COC Goes Here
Page 59 of 59
LOG-IN CHECKLIST
BFI Waste Systems of North America, LLC
Lake Norman C&D LandfillProject:
Client:
Printed: 6/8/2016 7:08:40AM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, INC.
Date Received:05/18/16 12:45 Logged In By:Charles Hawks
Work Order:AZE0540
OBSERVATIONS
Attn: Mr. Mike Gurley
#Samples: 10 #Containers: 48
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
NO
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:No
Comments:
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