5301_LeeCounty_GWMR_DIN27908_20161012

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 

November 2, 2016 

Jaclynne Drummond 
Compliance Hydrogeologist 
NCDEQ, Division of Waste Management  
Solid Waste Section, Asheville Regional Office 
2090 US Highway 70, Swannanoa, NC 28778 

Re: Semi‐Annual Groundwater Monitoring Event (October 2016) 
 Lee County Landfill ‐ Sanford, NC 
 NCDWM – Solid Waste Section Permit # 53‐01 
 Terraquest Project No. 02296 

Dear Ms. Drummond: 

On behalf of the Lee County Department of Public Works, Terraquest Environmental 
Consultants, P.C. is reporting the results of a biannual ground and surface water sampling event 
that took pace at the Lee County Landfill in Sanford, NC on October 12, 2016.  In accordance 
with NCDWM‐SW’s reporting requirements, a Solid Waste Section Environmental Monitoring 
Reporting Form is attached.  The data from the event including analytical results, groundwater 
elevations, and field measured groundwater parameter data is summarized on the attached 
Table 1.  The location of the site is shown of Figure 1, the vicinity of the site on Figure 2, and 
site’s layout on Figure 3.  Figure 4 presents the recent potentiometric surface.  The full 
analytical report is also attached.  The following summarizes the event: 

On October 12, 2016, Terraquest personnel sampled monitoring wells MW5, MW6, MW9, 
MW10, MW12, and MW14, and collected one surface water sample, SW2.  All water samples 
were analyzed per SW‐846 8260B (VOCs) and SW‐846 7470A (mercury) and 6010C (RCRA 
Metals).  All water samples were collected following technical methods and standard 
procedures as outlined on the enclosed sheets.  Terraquest personnel also collected dissolved 
oxygen, pH, temperature, and conductivity measurements from each of the sampled 
monitoring wells following purging of the well and directly from the surface water body at the 
SW2 location.  These measurements are listed on the attached Table 1.   

The analytical results revealed detectable concentrations of petroleum‐type compounds in 
monitoring well MW12 only.  Results of the RCRA Metals analysis indicate that all of the 
monitoring wells and the surface water sample had a detection of at least one metal.  The 
analytical results are summarized in Table 1.   

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 

A potentiometric surface map (Figure 4) depicting an interpreted groundwater flow direction at 
the site as measured on October 12, 2016 is attached.  Based upon the water levels in 
monitoring wells, the groundwater flow direction is to the southeast toward Mare Brand Creek.  
This flow direction conforms with historical flow directions.  Table 1 lists the groundwater 
elevations for the monitoring wells. 

If you have any questions regarding the sampling event or analytical report, please contact 
Ryan Kerins at (919)‐563‐9091 or Mr. Joseph Cherry of the Lee County Public Works 
Department at (919)‐774‐8440.  Thank you. 

Sincerely, 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 

Ryan D. Kerins         Michael J. Brown P.G.    
Project Manager       President 

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 Na
m
e
:
  Le
e
 Co
u
n
t
y
 La
n
d
f
i
l
l
Ta
b
l
e
 1
Da
t
e
:
 11
/
2
/
1
6
1.  * Te
c
h
n
i
c
a
l
l
y
,
 th
i
s
 sa
m
p
l
e
 se
t
 di
d
n
'
t
 ha
v
e
 an
y
 ex
t
r
a
c
t
i
o
n
s
.
  Th
e
 me
t
a
l
s
 we
r
e
 pr
e
p
p
e
d
 an
d
 dig
e
s
t
e
d
.
  Th
e
 vo
l
a
t
i
l
e
s
 ar
e
n
'
t
 in
v
o
l
v
e
d
 in
 an
y
 ex
t
r
a
c
t
i
o
n
 pr
o
c
e
s
s
.

Th
e
y
 ar
e
 lo
a
d
e
d
 di
r
e
c
t
l
y
 on
t
o
 th
e
 in
s
t
r
u
m
e
n
t
.

Pa
g
e
 2  of
 3
FA
C
I
L
I
T
Y

PE
R
M
I
T
WE
L
L
 ID

C
A
S
 Nu
m
b
e
r

S
W
S
 ID

P
A
R
A
M
E
T
E
R

R
E
S
U
L
T

U
N
I
T
S

Q
U
A
L
I
F
I
E
R
DIL
U
T
I
O
N

FA
C
T
O
R
CO
L
L
E
C
T
 DA
T
E
EX
T
R
A
C
T
I
O
N
 DATE*ANALYSIS  DATE
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
8
4
.
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
9

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

5
.
2
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
9

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

37
9
.
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

4
.
6
6
53
‐01

5
3
0
1
‐MW
9

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

6
.
2
5

m
g
/
L
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

2
0
.
0

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

9
4

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
9

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
9

1
0
8
‐88
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1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
9

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
9

1
3
3
0
‐20
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3
4
6

T
o
t
a
l
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l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
9

T
e
t
r
a
h
y
d
r
o
f
u
r
a
n

<
0
.
2
3
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
0
0
0
1
0
0

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
5
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
0
.
0
0
4
0
0

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

0
.
1
4
8

m
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

<
0
.
0
0
0
3
0
0

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

0
.
0
0
1
1
7

m
g
/
L

J

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

0
.
0
0
4
1
4

m
g
/
L

J

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
0
.
0
1
1
3

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
0
0
0
6
0
0

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
7
7
.
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

8
.
1
8

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
0

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
6
8
.
8

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

4
.
5
8
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

3
.
5
7

m
g
/
L
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

2
0
.
2

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

9
9

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
1
0

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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1
0

1
0
8
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1
9
6

T
o
l
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e

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0
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1
4

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/
L

U

1

1
0
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1
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1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

1
0
0
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‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
2
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1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

1
3
3
0
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3
4
6

T
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t
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l
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n
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s

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0
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1
8

u
g
/
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1

1
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1
2
/
1
6

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1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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1
0

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1

1
0
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1
6

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1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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1
0

7
4
3
9
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1
3
2

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e
r
c
u
r
y

<
0
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0
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0
0

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g
/
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U

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1
0
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1
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6

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1
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2
5
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1
6
53
‐01

5
3
0
1
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0
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g
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1
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6

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1
0
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1
7
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1
6
53
‐01

5
3
0
1
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4
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1
5

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m

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1
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6
53
‐01

5
3
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1
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1
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7
4
4
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3
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C
a
d
m
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m

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0
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0
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g
/
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U

1

1
0
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1
2
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1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
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1
0

7
4
4
0
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5
1

C
h
r
o
m
i
u
m

0
.
0
0
0
6
3
8

m
g
/
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J

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
3
9
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1
3
1

L
e
a
d

<
0
.
0
0
3
3
0

m
g
/
L

U

1

1
0
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1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
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1
0

7
7
8
2
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1
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3

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l
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m

<
0
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1
1
3

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g
/
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1

1
0
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1
2
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1
6

*

1
0
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1
7
/
1
6
53
‐01

5
3
0
1
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1
0

7
4
4
0
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1
8
4

S
i
l
v
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r

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0
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0
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6
0
0

m
g
/
L

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1

1
0
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1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
1

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
9
9
.
6

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
1

S
W
3
1
8

3
1
8

D
e
p
t
h
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t
e
r

5
.
4
3

f
e
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t
53
‐01

5
3
0
1
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1
1

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
9
4
.
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
3
7
.
4

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
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t
e
r

3
.
3
9

f
e
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t
53
‐01

5
3
0
1
‐MW
1
2

4
2
7

G
r
o
u
n
d
w
a
t
e
r
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v
a
t
i
o
n

3
3
4
.
0

f
e
e
t
53
‐01

5
3
0
1
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1
2

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

6
.
3
5
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

1
.
3
5

m
g
/
L
53
‐01

5
3
0
1
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1
2

S
W
3
2
5

3
2
5

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e
m
p
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t
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e

2
1
.
0

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
,
6
2
5

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
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1
2

7
1
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1
6

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e
n
z
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n
e

<
0
.
1
6
0

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g
/
L

U

1

1
0
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1
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/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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1
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0
8
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1
9
6

T
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l
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0
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4
5

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1

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6

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1
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/
2
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1
6
53
‐01

5
3
0
1
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1
2

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0
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1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

1
0
/
1
2
/
1
6

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1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

T
e
t
r
a
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y
d
r
o
f
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a
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9
.
1
7

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

1
0
8
‐90
‐7

3
9

C
h
l
o
r
o
b
e
n
z
e
n
e

2
4
.
7

u
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
5
‐00
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4
1

C
h
l
o
r
o
e
t
h
a
n
e

2
6
.
3

u
g
/
L

L

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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1
2

1
0
6
‐46
‐77
1

1
‐4 ‐Dic
h
l
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o
b
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e

4
.
8
7

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1

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0
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1
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6

*

1
0
/
2
0
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1
6
53
‐01

5
3
0
1
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1
2

7
5
‐34
‐37
5

1
,
1
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h
l
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t
h
a
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e

3
.
5
5

u
g
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1

1
0
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1
2
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6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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1
2

9
5
‐50
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9

1
,
2
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c
h
l
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o
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n
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e
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e

0
.
4
9

u
g
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L

J

1

1
0
/
1
2
/
1
6

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1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
3
9
‐97
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1
3
2

M
e
r
c
u
r
y

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0
.
0
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1
0
0

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g
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L

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0
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2
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1
6

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1
0
/
2
5
/
1
6
53
‐01

5
3
0
1
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2

7
4
4
0
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4

A
r
s
e
n
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c

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0
0
4
5
7

m
g
/
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1

1
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2
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6

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1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
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‐3

1
5

B
a
r
i
u
m

0
.
2
5

m
g
/
L

1

1
0
/
1
2
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6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
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1
2

7
4
4
0
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3
4

C
a
d
m
i
u
m

0
.
0
0
0
5
6
7

m
g
/
L

J

1

1
0
/
1
2
/
1
6

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1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐47
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5
1

C
h
r
o
m
i
u
m

0
.
0
2
1
5

m
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

0
.
0
8
4
2

m
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
0
.
0
1
1
3

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
0
0
0
6
0
0

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
No
t
e
:
1.  * Te
c
h
n
i
c
a
l
l
y
,
 th
i
s
 sa
m
p
l
e
 se
t
 di
d
n
'
t
 ha
v
e
 an
y
 ex
t
r
a
c
t
i
o
n
s
.
  Th
e
 me
t
a
l
s
 we
r
e
 pr
e
p
p
e
d
 an
d
 dig
e
s
t
e
d
.
  Th
e
 vo
l
a
t
i
l
e
s
 ar
e
n
'
t
 in
v
o
l
v
e
d
 in
 an
y
 ex
t
r
a
c
t
i
o
n
 pr
o
c
e
s
s
.

Th
e
y
 ar
e
 lo
a
d
e
d
 di
r
e
c
t
l
y
 on
t
o
 th
e
 in
s
t
r
u
m
e
n
t
.

Ta
b
l
e
 1  ‐ 
CO
N
T
I
N
U
E
D
GR
O
U
N
D
W
A
T
E
R
 DA
T
A
 10
/
1
2
/
1
6
Da
t
e
:
 11
/
2
/
1
6
Fa
c
i
l
i
t
y
 Na
m
e
:
  Le
e
 Co
u
n
t
y
 La
n
d
f
i
l
l
Pa
g
e
 3  of
 3
FA
C
I
L
I
T
Y

WE
L
L
 ID

C
A
S
 Nu
m
b
e
r

S
W
S
 ID

P
A
R
A
M
E
T
E
R

R
E
S
U
L
T

U
N
I
T
S

Q
U
A
L
I
F
I
E
R

D
I
L
U
T
I
O
N

CO
L
L
E
C
T
 DA
T
E

E
X
T
R
A
C
T
I
O
N
 ANALYSIS  DATE
53
‐01

5
3
0
1
‐MW
1
3

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
6
3
.
9
3

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
3

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

7
.
6
3

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
3

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
5
6
.
3

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
5
8
.
6
1

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
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t
e
r

6
.
3
7

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

4
2
7

G
r
o
u
n
d
w
a
t
e
r
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v
a
t
i
o
n

3
5
2
.
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

5
.
8
9
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

1
.
5
8

m
g
/
L
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
8
.
6

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

9
5

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
1
4

7
1
‐43
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1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

1
0
8
‐88
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1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

1
3
3
0
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3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

T
e
t
r
a
h
y
d
r
o
f
u
r
a
n

<
0
.
2
3
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
0
0
0
1
0
0

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
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1
4

A
r
s
e
n
i
c

0
.
0
0
0
4
5
7

m
g
/
L

J

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
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1
4

7
4
4
0
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‐3

1
5

B
a
r
i
u
m

0
.
2
5
0

m
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

0
.
0
0
0
5
6
7

m
g
/
L

J

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

0
.
0
2
1
5

m
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

0
.
0
8
4
2

m
g
/
L

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
7
8
2
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‐2

1
8
3

S
e
l
e
n
i
u
m

<
0
.
0
1
1
3

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐22
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1
8
4

S
i
l
v
e
r

<
0
.
0
0
0
6
0
0

m
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
1
7
/
1
6
53
‐01

5
3
0
1
‐SW
2

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

6
.
0
7
53
‐01

5
3
0
1
‐SW
2

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

6
.
2
0

m
g
/
L
53
‐01

5
3
0
1
‐SW
2

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
8
.
8

d
e
g
.
 C
53
‐01

5
3
0
1
‐SW
2

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

8
0

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐SW
2

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐SW
2

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
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2

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐SW
2

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

T
e
t
r
a
h
y
d
r
o
f
u
r
a
n

<
0
.
2
3
6

u
g
/
L

U

1

1
0
/
1
2
/
1
6

*

1
0
/
2
0
/
1
6
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Analytical Report
A6J0040
Project
Lee County Landfill
Project Number
02296
November 01, 2016
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Mebane, NC 27302
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
6017 Financial Drive Phone #:[phone]
Website:www.ftsanalytical.comNorcross, GA 30071
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
November 01, 2016
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Ryan Kerins
RE: Lee County Landfill
We are reporting the results of the analyses performed on the samples recieved on 10/14/2016 under the
project name referenced above and identified as the lab Work Order A6J0040. All results being reported
under this Report apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontracted lab, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reporting using all other available quality control methods.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed
for at least 5 years in our archives after which time it will be destroyed without further notice, unless
otherwise agreed upon. The samples received, and described as recorded in Work Order A6J0040 will be
filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise
agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard
practices, controlled/regulated substances, etc.)
We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions
concerning this report, please do not hesitate to contact us at any time. We will be happy to help.
Mebane, NC 27302
Sincerely,
Chad A. Bechtold
VP of Client Services
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Samples in this Report
Sample Lab ID Matrix Date Sampled Date Received
MW5 WaterA6J0040-01 14-Oct-2016 10:0012-Oct-2016 12:45
MW6 WaterA6J0040-02 14-Oct-2016 10:0012-Oct-2016 11:35
MW9 WaterA6J0040-03 14-Oct-2016 10:0012-Oct-2016 11:10
MW10 WaterA6J0040-04 14-Oct-2016 10:0012-Oct-2016 11:25
MW12 WaterA6J0040-05 14-Oct-2016 10:0012-Oct-2016 12:30
MW14 WaterA6J0040-06 14-Oct-2016 10:0012-Oct-2016 10:40
SW2 WaterA6J0040-07 14-Oct-2016 10:0012-Oct-2016 13:00
Page 3 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Analysis Case Narrative

SW8260B
Batch B6I0420
The percent recovery of the Blank Spike Duplicate was outside QC limits for Chloroethane. The RPD of the BS/BSD was
outside QC limits for Chloroform. Acceptable per NELAC, Appendix D, Marginal Exceedances.
Samples affected: A6J0040-01,-02,-03,-04,-05,-06,-07.
Page 4 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Hits Summary
Sample: MW5
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-01
0.0500 mg/L0.00200 10.273 10/17/16 14:53 7440-39-3 EPA 6010CBarium
0.00500 mg/L0.000300 1J0.000623 10/17/16 14:53 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 1J0.00560 10/17/16 14:53 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 10.0113 10/17/16 14:53 7439-92-1 EPA 6010CLead
Sample: MW6
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-02
0.0500 mg/L0.00200 1J0.0459 10/17/16 14:55 7440-39-3 EPA 6010CBarium
0.0100 mg/L0.000300 1J0.000711 10/17/16 14:55 7440-47-3 EPA 6010CChromium
Sample: MW9
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-03
0.0500 mg/L0.00200 10.148 10/17/16 14:57 7440-39-3 EPA 6010CBarium
0.0100 mg/L0.000300 1J0.00117 10/17/16 14:57 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 1J0.00414 10/17/16 14:57 7439-92-1 EPA 6010CLead
Sample: MW10
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-04
0.0500 mg/L0.00200 10.137 10/17/16 15:05 7440-39-3 EPA 6010CBarium
0.0100 mg/L0.000300 1J0.000638 10/17/16 15:05 7440-47-3 EPA 6010CChromium
Page 5 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Hits Summary
(Continued)
Sample: MW12
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-05
0.0500 mg/L0.00200 11.24 10/17/16 15:07 7440-39-3 EPA 6010CBarium
1.00 ug/L0.110 13.55 10/20/16 20:04 75-34-3 EPA 8260B APP I1,1-Dichloroethane
0.00500 mg/L0.000300 1J0.00236 10/17/16 15:07 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 1J0.00364 10/17/16 15:07 7440-47-3 EPA 6010CChromium
1.00 ug/L0.140 1J0.490 10/20/16 20:04 95-50-1 EPA 8260B APP I1,2-Dichlorobenzene
0.0100 mg/L0.00330 10.0165 10/17/16 15:07 7439-92-1 EPA 6010CLead
1.00 ug/L0.170 14.87 10/20/16 20:04 106-46-7 EPA 8260B APP I1,4-Dichlorobenzene
0.0500 mg/L0.0113 1J0.0121 10/17/16 15:07 7782-49-2 EPA 6010CSelenium
1.00 ug/L0.150 124.7 10/20/16 20:04 108-90-7 EPA 8260B APP IChlorobenzene
1.00 ug/L0.260 1L26.3 10/20/16 20:04 75-00-3 EPA 8260B APP IChloroethane
5.00 ug/L0.236 19.17 10/20/16 20:04 109-99-9 EPA 8260BTetrahydrofuran
1.00 ug/L0.140 1J0.450 10/20/16 20:04 108-88-3 EPA 8260B APP IToluene
Sample: MW14
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-06
0.0100 mg/L0.00400 1J0.00457 10/17/16 15:09 7440-38-2 EPA 6010CArsenic
0.0500 mg/L0.00200 10.250 10/17/16 15:09 7440-39-3 EPA 6010CBarium
0.00500 mg/L0.000300 1J0.000567 10/17/16 15:09 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 10.0215 10/17/16 15:09 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 10.0842 10/17/16 15:09 7439-92-1 EPA 6010CLead
Sample: SW2
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6J0040-07
0.0500 mg/L0.00200 10.0563 10/17/16 15:17 7440-39-3 EPA 6010CBarium
0.0100 mg/L0.000300 1J0.00181 10/17/16 15:17 7440-47-3 EPA 6010CChromium
Page 6 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results

ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-01 (Water)
Client Sample ID: MW5
RL Dil Date Prepared
Sampled: 10/12/16 12:45
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00400 U 10/17/16 14:5310/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 10.273 10/17/16 14:5310/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.000623 J 10/17/16 14:5310/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.00560 J 10/17/16 14:5310/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.0113 10/17/16 14:5310/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/17/16 14:5310/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 14:5310/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 18:3810/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 18:3810/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 18:3810/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 18:3810/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/16 18:3810/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 18:3810/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 18:3810/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 18:3810/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 18:3810/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/16 18:3810/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 18:3810/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 18:3810/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/16 18:3810/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 18:3810/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 18:3810/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 18:3810/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 18:3810/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 18:3810/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 18:3810/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 18:3810/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 18:3810/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 18:3810/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 18:3810/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 18:3810/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 18:3810/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/16 18:3810/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U, L 10/20/16 18:3810/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 18:3810/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 18:3810/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 18:3810/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 18:3810/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 18:3810/20/16 13:58 124-48-1Dibromochloromethane
Page 7 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-01 (Water)
Client Sample ID: MW5 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 12:45
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.240 10.240 U 10/20/16 18:3810/20/16 13:58 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/16 18:3810/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 18:3810/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 18:3810/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 18:3810/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 18:3810/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 18:3810/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 18:3810/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/16 18:3810/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 18:3810/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 18:3810/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 18:3810/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 18:3810/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 18:3810/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 18:3810/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 18:3810/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 18:3810/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15997%10/20/16 18:38 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18686%10/20/16 18:38 460-00-4
Surrogate: Toluene-D8 (SUR)70-13099%10/20/16 18:38 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 10.236 U 10/20/16 18:3810/20/16 13:58 109-99-9Tetrahydrofuran
Page 8 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-02 (Water)
Client Sample ID: MW6
RL Dil Date Prepared
Sampled: 10/12/16 11:35
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00400 U 10/17/16 14:5510/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 10.0459 J 10/17/16 14:5510/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.000300 U 10/17/16 14:5510/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.000711 J 10/17/16 14:5510/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.00330 U 10/17/16 14:5510/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/17/16 14:5510/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 14:5510/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 18:5910/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 18:5910/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 18:5910/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 18:5910/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/16 18:5910/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 18:5910/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 18:5910/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 18:5910/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 18:5910/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/16 18:5910/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 18:5910/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 18:5910/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/16 18:5910/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 18:5910/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 18:5910/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 18:5910/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 18:5910/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 18:5910/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 18:5910/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 18:5910/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 18:5910/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 18:5910/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 18:5910/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 18:5910/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 18:5910/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/16 18:5910/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U, L 10/20/16 18:5910/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 18:5910/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 18:5910/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 18:5910/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 18:5910/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 18:5910/20/16 13:58 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/16 18:5910/20/16 13:58 74-95-3Dibromomethane
Page 9 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-02 (Water)
Client Sample ID: MW6 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 11:35
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.190 10.190 U 10/20/16 18:5910/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 18:5910/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 18:5910/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 18:5910/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 18:5910/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 18:5910/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 18:5910/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/16 18:5910/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 18:5910/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 18:5910/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 18:5910/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 18:5910/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 18:5910/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 18:5910/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 18:5910/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 18:5910/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15999%10/20/16 18:59 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18686%10/20/16 18:59 460-00-4
Surrogate: Toluene-D8 (SUR)70-13099%10/20/16 18:59 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 10.236 U 10/20/16 18:5910/20/16 13:58 109-99-9Tetrahydrofuran
Page 10 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-03 (Water)
Client Sample ID: MW9
RL Dil Date Prepared
Sampled: 10/12/16 11:10
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00400 U 10/17/16 14:5710/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 10.148 10/17/16 14:5710/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.000300 U 10/17/16 14:5710/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.00117 J 10/17/16 14:5710/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.00414 J 10/17/16 14:5710/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/17/16 14:5710/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 14:5710/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 19:2110/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 19:2110/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 19:2110/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 19:2110/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/16 19:2110/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 19:2110/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 19:2110/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 19:2110/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 19:2110/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/16 19:2110/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 19:2110/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 19:2110/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/16 19:2110/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 19:2110/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 19:2110/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 19:2110/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 19:2110/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 19:2110/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 19:2110/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 19:2110/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 19:2110/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 19:2110/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 19:2110/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 19:2110/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 19:2110/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/16 19:2110/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U, L 10/20/16 19:2110/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 19:2110/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 19:2110/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 19:2110/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 19:2110/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 19:2110/20/16 13:58 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/16 19:2110/20/16 13:58 74-95-3Dibromomethane
Page 11 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-03 (Water)
Client Sample ID: MW9 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 11:10
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.190 10.190 U 10/20/16 19:2110/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 19:2110/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 19:2110/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 19:2110/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 19:2110/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 19:2110/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 19:2110/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/16 19:2110/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 19:2110/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 19:2110/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 19:2110/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 19:2110/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 19:2110/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 19:2110/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 19:2110/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 19:2110/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-159101%10/20/16 19:21 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18684%10/20/16 19:21 460-00-4
Surrogate: Toluene-D8 (SUR)70-13099%10/20/16 19:21 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 10.236 U 10/20/16 19:2110/20/16 13:58 109-99-9Tetrahydrofuran
Page 12 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-04 (Water)
Client Sample ID: MW10
RL Dil Date Prepared
Sampled: 10/12/16 11:25
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00400 U 10/17/16 15:0510/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 10.137 10/17/16 15:0510/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.000300 U 10/17/16 15:0510/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.000638 J 10/17/16 15:0510/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.00330 U 10/17/16 15:0510/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/17/16 15:0510/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 15:0510/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 19:4210/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 19:4210/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 19:4210/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 19:4210/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/16 19:4210/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 19:4210/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 19:4210/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 19:4210/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 19:4210/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/16 19:4210/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 19:4210/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 19:4210/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/16 19:4210/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 19:4210/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 19:4210/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 19:4210/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 19:4210/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 19:4210/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 19:4210/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 19:4210/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 19:4210/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 19:4210/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 19:4210/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 19:4210/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 19:4210/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/16 19:4210/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U, L 10/20/16 19:4210/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 19:4210/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 19:4210/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 19:4210/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 19:4210/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 19:4210/20/16 13:58 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/16 19:4210/20/16 13:58 74-95-3Dibromomethane
Page 13 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-04 (Water)
Client Sample ID: MW10 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 11:25
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.190 10.190 U 10/20/16 19:4210/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 19:4210/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 19:4210/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 19:4210/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 19:4210/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 19:4210/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 19:4210/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/16 19:4210/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 19:4210/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 19:4210/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 19:4210/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 19:4210/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 19:4210/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 19:4210/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 19:4210/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 19:4210/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15999%10/20/16 19:42 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18684%10/20/16 19:42 460-00-4
Surrogate: Toluene-D8 (SUR)70-13098%10/20/16 19:42 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 10.236 U 10/20/16 19:4210/20/16 13:58 109-99-9Tetrahydrofuran
Page 14 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-05 (Water)
Client Sample ID: MW12
RL Dil Date Prepared
Sampled: 10/12/16 12:30
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00400 U 10/17/16 15:0710/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 11.24 10/17/16 15:0710/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.00236 J 10/17/16 15:0710/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.00364 J 10/17/16 15:0710/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.0165 10/17/16 15:0710/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0121 J 10/17/16 15:0710/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 15:0710/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 20:0410/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 20:0410/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 20:0410/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 20:0410/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 13.55 10/20/16 20:0410/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 20:0410/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 20:0410/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 20:0410/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 20:0410/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.490 J 10/20/16 20:0410/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 20:0410/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 20:0410/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 14.87 10/20/16 20:0410/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 20:0410/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 20:0410/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 20:0410/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 20:0410/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 20:0410/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 20:0410/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 20:0410/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 20:0410/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 20:0410/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 20:0410/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 20:0410/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 20:0410/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 124.7 10/20/16 20:0410/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 126.3 L 10/20/16 20:0410/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 20:0410/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 20:0410/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 20:0410/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 20:0410/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 20:0410/20/16 13:58 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/16 20:0410/20/16 13:58 74-95-3Dibromomethane
Page 15 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-05 (Water)
Client Sample ID: MW12 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 12:30
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.190 10.190 U 10/20/16 20:0410/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 20:0410/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 20:0410/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 20:0410/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 20:0410/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 20:0410/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 20:0410/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.450 J 10/20/16 20:0410/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 20:0410/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 20:0410/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 20:0410/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 20:0410/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 20:0410/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 20:0410/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 20:0410/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 20:0410/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15999%10/20/16 20:04 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18685%10/20/16 20:04 460-00-4
Surrogate: Toluene-D8 (SUR)70-13096%10/20/16 20:04 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 19.17 10/20/16 20:0410/20/16 13:58 109-99-9Tetrahydrofuran
Page 16 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-06 (Water)
Client Sample ID: MW14
RL Dil Date Prepared
Sampled: 10/12/16 10:40
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00457 J 10/17/16 15:0910/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 10.250 10/17/16 15:0910/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.000567 J 10/17/16 15:0910/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.0215 10/17/16 15:0910/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.0842 10/17/16 15:0910/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/17/16 15:0910/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 15:0910/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 20:2610/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 20:2610/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 20:2610/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 20:2610/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/16 20:2610/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 20:2610/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 20:2610/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 20:2610/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 20:2610/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/16 20:2610/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 20:2610/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 20:2610/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/16 20:2610/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 20:2610/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 20:2610/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 20:2610/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 20:2610/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 20:2610/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 20:2610/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 20:2610/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 20:2610/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 20:2610/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 20:2610/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 20:2610/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 20:2610/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/16 20:2610/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U, L 10/20/16 20:2610/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 20:2610/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 20:2610/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 20:2610/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 20:2610/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 20:2610/20/16 13:58 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/16 20:2610/20/16 13:58 74-95-3Dibromomethane
Page 17 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-06 (Water)
Client Sample ID: MW14 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 10:40
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.190 10.190 U 10/20/16 20:2610/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 20:2610/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 20:2610/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 20:2610/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 20:2610/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 20:2610/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 20:2610/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/16 20:2610/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 20:2610/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 20:2610/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 20:2610/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 20:2610/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 20:2610/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 20:2610/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 20:2610/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 20:2610/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-159100%10/20/16 20:26 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18685%10/20/16 20:26 460-00-4
Surrogate: Toluene-D8 (SUR)70-13098%10/20/16 20:26 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 10.236 U 10/20/16 20:2610/20/16 13:58 109-99-9Tetrahydrofuran
Page 18 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-07 (Water)
Client Sample ID: SW2
RL Dil Date Prepared
Sampled: 10/12/16 13:00
CAS #
7 RCRA Metals by Method 6010C
0.0100 mg/L0.00400 10.00400 U 10/17/16 15:1710/17/16 8:20 7440-38-2Arsenic
0.0500 mg/L0.00200 10.0563 10/17/16 15:1710/17/16 8:20 7440-39-3Barium
0.00500 mg/L0.000300 10.000300 U 10/17/16 15:1710/17/16 8:20 7440-43-9Cadmium
0.0100 mg/L0.000300 10.00181 J 10/17/16 15:1710/17/16 8:20 7440-47-3Chromium
0.0100 mg/L0.00330 10.00330 U 10/17/16 15:1710/17/16 8:20 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/17/16 15:1710/17/16 8:20 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/17/16 15:1710/17/16 8:20 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
1.00 ug/L0.240 10.240 U 10/20/16 20:4710/20/16 13:58 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/16 20:4710/20/16 13:58 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/16 20:4710/20/16 13:58 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/16 20:4710/20/16 13:58 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/16 20:4710/20/16 13:58 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/16 20:4710/20/16 13:58 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/16 20:4710/20/16 13:58 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/16 20:4710/20/16 13:58 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/16 20:4710/20/16 13:58 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/16 20:4710/20/16 13:58 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/16 20:4710/20/16 13:58 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/16 20:4710/20/16 13:58 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/16 20:4710/20/16 13:58 106-46-71,4-Dichlorobenzene
50.0 ug/L2.52 12.52 U 10/20/16 20:4710/20/16 13:58 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/16 20:4710/20/16 13:58 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/16 20:4710/20/16 13:58 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/16 20:4710/20/16 13:58 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/16 20:4710/20/16 13:58 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/16 20:4710/20/16 13:58 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/16 20:4710/20/16 13:58 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/16 20:4710/20/16 13:58 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/16 20:4710/20/16 13:58 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/16 20:4710/20/16 13:58 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/16 20:4710/20/16 13:58 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/16 20:4710/20/16 13:58 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/16 20:4710/20/16 13:58 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U, L 10/20/16 20:4710/20/16 13:58 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U, F 10/20/16 20:4710/20/16 13:58 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/16 20:4710/20/16 13:58 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/16 20:4710/20/16 13:58 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/16 20:4710/20/16 13:58 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/16 20:4710/20/16 13:58 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/16 20:4710/20/16 13:58 74-95-3Dibromomethane
Page 19 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6J0040-07 (Water)
Client Sample ID: SW2 (Continued)
RL Dil Date Prepared
Sampled: 10/12/16 13:00
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
1.00 ug/L0.190 10.190 U 10/20/16 20:4710/20/16 13:58 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/16 20:4710/20/16 13:58 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/16 20:4710/20/16 13:58 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/16 20:4710/20/16 13:58 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/16 20:4710/20/16 13:58 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/16 20:4710/20/16 13:58 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/16 20:4710/20/16 13:58 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/16 20:4710/20/16 13:58 108-88-3Toluene
1.00 ug/L0.180 10.180 U 10/20/16 20:4710/20/16 13:58 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/16 20:4710/20/16 13:58 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/16 20:4710/20/16 13:58 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/16 20:4710/20/16 13:58 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/16 20:4710/20/16 13:58 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/16 20:4710/20/16 13:58 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/16 20:4710/20/16 13:58 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/16 20:4710/20/16 13:58 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-159101%10/20/16 20:47 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18685%10/20/16 20:47 460-00-4
Surrogate: Toluene-D8 (SUR)70-13098%10/20/16 20:47 2037-26-5
Total Mercury Analysis by Method 7470A
0.000200 mg/L0.0000100 10.0000100 U 10/25/16 12:1110/24/16 13:00 7439-97-6Mercury
VOCs by Method 8260B
5.00 ug/L0.236 10.236 U 10/20/16 20:4710/20/16 13:58 109-99-9Tetrahydrofuran
Page 20 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
VOCs by Method 8260B
MDL
Batch: B6I0420
Prepared & Analyzed: 10/20/2016Blank (B6I0420-BLK1)
5.00 ug/L0.236 U 0.236Tetrahydrofuran
Prepared & Analyzed: 10/20/2016LCS (B6I0420-BS1)
5.00 50.0 70-130116ug/L57.8 0.236Tetrahydrofuran
Prepared & Analyzed: 10/20/2016LCS Dup (B6I0420-BSD1)
5.00 50.0 2070-130113 2ug/L56.5 0.236Tetrahydrofuran
Page 21 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B
MDL
Batch: B6I0420
Prepared & Analyzed: 10/20/2016Blank (B6I0420-BLK1)
1.00 ug/L0.240 U 0.2401,1,1,2-Tetrachloroethane
1.00 ug/L0.160 U 0.1601,1,1-Trichloroethane
1.00 ug/L0.180 U 0.1801,1,2,2-Tetrachloroethane
1.00 ug/L0.250 U 0.2501,1,2-Trichloroethane
1.00 ug/L0.110 U 0.1101,1-Dichloroethane
1.00 ug/L0.200 U 0.2001,1-Dichloroethene
1.00 ug/L0.210 U 0.2101,2,3-Trichloropropane
1.00 ug/L0.190 U 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB)
1.00 ug/L0.750 J 0.1401,2-Dichlorobenzene
1.00 ug/L0.180 U 0.1801,2-Dichloroethane
1.00 ug/L0.150 U 0.1501,2-Dichloropropane
1.00 ug/L0.900 J 0.1701,4-Dichlorobenzene
50.0 ug/L2.52 U 2.522-Butanone (MEK)
2.00 ug/L0.320 U 0.3202-Hexanone
2.00 ug/L0.260 U 0.2604-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 U 0.350Acetone
2.00 ug/L0.490 U 0.490Acrylonitrile
1.00 ug/L0.160 U 0.160Benzene
1.00 ug/L0.200 U 0.200Bromochloromethane
1.00 ug/L0.250 U 0.250Bromodichloromethane
1.00 ug/L0.170 U 0.170Bromoform
1.00 ug/L0.250 U 0.250Bromomethane (Methyl Bromide)
1.00 ug/L0.260 U 0.260Carbon disulfide
1.00 ug/L0.330 U 0.330Carbon tetrachloride
1.00 ug/L0.150 U 0.150Chlorobenzene
1.00 ug/L0.260 U 0.260Chloroethane
1.00 ug/L0.160 U 0.160Chloroform
1.00 ug/L0.250 U 0.250Chloromethane (Methyl Chloride)
1.00 ug/L0.210 U 0.210cis-1,2-Dichloroethene
1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene
1.00 ug/L0.150 U 0.150Dibromochloromethane
1.00 ug/L0.240 U 0.240Dibromomethane
1.00 ug/L0.190 U 0.190Ethylbenzene
1.00 ug/L0.310 U 0.310Iodomethane (Methyl Iodide)
2.00 ug/L0.510 U 0.510m,p-Xylenes
1.00 ug/L0.420 U 0.420Methylene Chloride
1.00 ug/L0.200 U 0.200o-Xylene
1.00 ug/L0.180 U 0.180Styrene
1.00 ug/L0.160 U 0.160Tetrachloroethylene
1.00 ug/L0.140 U 0.140Toluene
Page 22 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B (Continued)
MDL
Batch: B6I0420 (Continued)
Prepared & Analyzed: 10/20/2016Blank (B6I0420-BLK1)
1.00 ug/L0.180 U 0.180Total Xylenes
1.00 ug/L0.210 U 0.210trans-1,2-Dichloroethene
1.00 ug/L0.110 U 0.110trans-1,3-Dichloropropene
1.00 ug/L0.190 U 0.190trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 U 0.190Trichloroethylene
1.00 ug/L0.530 U 0.530Trichlorofluoromethane
1.00 ug/L0.720 U 0.720Vinyl acetate
1.00 ug/L0.190 U 0.190Vinyl chloride
50.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9748.6 ug/L
50.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)8442.2 ug/L
50.0 70-130Surrogate: Toluene-D8 (SUR)9849.2 ug/L
Prepared & Analyzed: 10/20/2016LCS (B6I0420-BS1)
1.00 50.0 80-13096ug/L47.8 0.2401,1,1,2-Tetrachloroethane
1.00 50.0 65-13086ug/L43.0 0.1601,1,1-Trichloroethane
1.00 50.0 65-13086ug/L43.0 0.1801,1,2,2-Tetrachloroethane
1.00 50.0 75-12596ug/L48.1 0.2501,1,2-Trichloroethane
1.00 50.0 70-13598ug/L49.0 0.1101,1-Dichloroethane
1.00 50.0 70-13089ug/L44.5 0.2001,1-Dichloroethene
1.00 50.0 75-12586ug/L42.8 0.2101,2,3-Trichloropropane
1.00 50.0 50-13068ug/L34.2 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 50.0 80-12098ug/L48.9 0.1801,2-Dibromoethane (EDB)
1.00 50.0 70-12094ug/L47.2 0.1401,2-Dichlorobenzene
1.00 50.0 70-13097ug/L48.7 0.1801,2-Dichloroethane
1.00 50.0 75-125119ug/L59.6 0.1501,2-Dichloropropane
1.00 50.0 75-12593ug/L46.6 0.1701,4-Dichlorobenzene
50.0 100 30-15096ug/L95.9 2.522-Butanone (MEK)
2.00 100 55-130100ug/L1000.3202-Hexanone
2.00 100 60-135103ug/L1030.2604-Methyl-2-pentanone (MIBK)
10.0 100 40-14081ug/L81.0 0.350Acetone
2.00 125 40-14076ug/L94.4 0.490Acrylonitrile
1.00 50.0 80-120104ug/L51.8 0.160Benzene
1.00 50.0 65-13093ug/L46.4 0.200Bromochloromethane
1.00 50.0 75-12089ug/L44.4 0.250Bromodichloromethane
1.00 50.0 70-13082ug/L40.9 0.170Bromoform
1.00 50.0 30-14589ug/L44.3 0.250Bromomethane (Methyl Bromide)
1.00 50.0 35-16088ug/L43.8 0.260Carbon disulfide
1.00 50.0 65-14083ug/L41.7 0.330Carbon tetrachloride
1.00 50.0 80-120107ug/L53.7 0.150Chlorobenzene
1.00 50.0 60-13561ug/L30.4 0.260Chloroethane
Page 23 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B (Continued)
MDL
Batch: B6I0420 (Continued)
Prepared & Analyzed: 10/20/2016LCS (B6I0420-BS1)
1.00 50.0 65-13595ug/L47.4 0.160Chloroform
1.00 50.0 40-125115ug/L57.6 0.250Chloromethane (Methyl Chloride)
1.00 50.0 70-12588ug/L44.1 0.210cis-1,2-Dichloroethene
1.00 50.0 70-130106ug/L53.2 0.100cis-1,3-Dichloropropene
1.00 50.0 60-13591ug/L45.3 0.150Dibromochloromethane
1.00 50.0 75-12596ug/L47.8 0.240Dibromomethane
1.00 50.0 75-125105ug/L52.4 0.190Ethylbenzene
1.00 50.0 65-13089ug/L44.7 0.310Iodomethane (Methyl Iodide)
2.00 100 75-130111ug/L1110.510m,p-Xylenes
1.00 50.0 55-14085ug/L42.7 0.420Methylene Chloride
1.00 50.0 80-120111ug/L55.4 0.200o-Xylene
1.00 50.0 65-135112ug/L55.8 0.180Styrene
1.00 50.0 45-150105ug/L52.3 0.160Tetrachloroethylene
1.00 50.0 75-120105ug/L52.5 0.140Toluene
1.00 50.0 60-14091ug/L45.5 0.210trans-1,2-Dichloroethene
1.00 50.0 55-140105ug/L52.5 0.110trans-1,3-Dichloropropene
1.00 50.0 65-13591ug/L45.7 0.190trans-1,4-Dichloro-2-butene
1.00 50.0 70-12596ug/L48.0 0.190Trichloroethylene
1.00 50.0 60-14586ug/L43.1 0.530Trichlorofluoromethane
1.00 50.0 65-13593ug/L46.4 0.720Vinyl acetate
1.00 50.0 50-145105ug/L52.3 0.190Vinyl chloride
50.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9547.6 ug/L
50.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)8542.4 ug/L
50.0 70-130Surrogate: Toluene-D8 (SUR)9748.6 ug/L
Prepared & Analyzed: 10/20/2016LCS Dup (B6I0420-BSD1)
1.00 50.0 2080-13093 2ug/L46.7 0.2401,1,1,2-Tetrachloroethane
1.00 50.0 2065-13081 6ug/L40.7 0.1601,1,1-Trichloroethane
1.00 50.0 2065-13086 0.2ug/L43.0 0.1801,1,2,2-Tetrachloroethane
1.00 50.0 2075-12595 1ug/L47.5 0.2501,1,2-Trichloroethane
1.00 50.0 2070-13595 3ug/L47.5 0.1101,1-Dichloroethane
1.00 50.0 2070-13085 5ug/L42.5 0.2001,1-Dichloroethene
1.00 50.0 2075-12587 1ug/L43.3 0.2101,2,3-Trichloropropane
1.00 50.0 2050-13072 5ug/L36.1 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 50.0 2080-12094 4ug/L47.1 0.1801,2-Dibromoethane (EDB)
1.00 50.0 2070-12094 0.4ug/L47.1 0.1401,2-Dichlorobenzene
1.00 50.0 2070-13093 5ug/L46.6 0.1801,2-Dichloroethane
1.00 50.0 2075-125115 3ug/L57.6 0.1501,2-Dichloropropane
1.00 50.0 2075-12592 2ug/L45.8 0.1701,4-Dichlorobenzene
50.0 100 2030-15092 4ug/L92.3 2.522-Butanone (MEK)
Page 24 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B (Continued)
MDL
Batch: B6I0420 (Continued)
Prepared & Analyzed: 10/20/2016LCS Dup (B6I0420-BSD1)
2.00 100 2055-13094 6ug/L94.3 0.3202-Hexanone
2.00 100 2060-13597 6ug/L97.4 0.2604-Methyl-2-pentanone (MIBK)
10.0 100 2040-14074 9ug/L73.7 0.350Acetone
2.00 125 2040-14074 2ug/L92.6 0.490Acrylonitrile
1.00 50.0 2080-12098 6ug/L48.8 0.160Benzene
1.00 50.0 2065-13088 5ug/L44.2 0.200Bromochloromethane
1.00 50.0 2075-12086 4ug/L42.8 0.250Bromodichloromethane
1.00 50.0 2070-13082 0.3ug/L41.0 0.170Bromoform
1.00 50.0 2030-14581 9ug/L40.4 0.250Bromomethane (Methyl Bromide)
1.00 50.0 2035-16087 1ug/L43.3 0.260Carbon disulfide
1.00 50.0 2065-14069 19ug/L34.4 0.330Carbon tetrachloride
1.00 50.0 2080-120102 5ug/L50.9 0.150Chlorobenzene
1.00 50.0 2060-13557 6ug/L28.5 X 0.260Chloroethane
1.00 50.0 2065-13576 22ug/L37.9 X 0.160Chloroform
1.00 50.0 2040-125106 8ug/L53.0 0.250Chloromethane (Methyl Chloride)
1.00 50.0 2070-12583 6ug/L41.4 0.210cis-1,2-Dichloroethene
1.00 50.0 2070-130101 6ug/L50.3 0.100cis-1,3-Dichloropropene
1.00 50.0 2060-13587 4ug/L43.6 0.150Dibromochloromethane
1.00 50.0 2075-12592 3ug/L46.2 0.240Dibromomethane
1.00 50.0 2075-12599 6ug/L49.5 0.190Ethylbenzene
1.00 50.0 2065-130104 15ug/L52.0 0.310Iodomethane (Methyl Iodide)
2.00 100 2075-130105 5ug/L1050.510m,p-Xylenes
1.00 50.0 2055-14086 0.3ug/L42.8 0.420Methylene Chloride
1.00 50.0 2080-120104 7ug/L51.8 0.200o-Xylene
1.00 50.0 2065-135105 7ug/L52.3 0.180Styrene
1.00 50.0 2045-15098 7ug/L48.9 0.160Tetrachloroethylene
1.00 50.0 2075-12099 6ug/L49.3 0.140Toluene
1.00 50.0 2060-14088 3ug/L44.2 0.210trans-1,2-Dichloroethene
1.00 50.0 2055-14098 7ug/L49.0 0.110trans-1,3-Dichloropropene
1.00 50.0 2065-13596 5ug/L48.0 0.190trans-1,4-Dichloro-2-butene
1.00 50.0 2070-12590 6ug/L45.2 0.190Trichloroethylene
1.00 50.0 2060-14587 1ug/L43.6 0.530Trichlorofluoromethane
1.00 50.0 2065-13590 3ug/L44.9 0.720Vinyl acetate
1.00 50.0 2050-14596 9ug/L47.8 0.190Vinyl chloride
50.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9547.6 ug/L
50.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)8341.6 ug/L
50.0 70-130Surrogate: Toluene-D8 (SUR)9748.3 ug/L
Page 25 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
7 RCRA Metals by Method 6010C
MDL
Batch: B6J0314
Prepared & Analyzed: 10/17/2016Blank (B6J0314-BLK1)
0.0100 mg/L0.00400 U 0.00400Arsenic
0.0500 mg/L0.00200 U 0.00200Barium
0.00500 mg/L0.000300 U 0.000300Cadmium
0.0100 mg/L0.000430 J 0.000300Chromium
0.0100 mg/L0.00330 U 0.00330Lead
0.0500 mg/L0.0113 U 0.0113Selenium
0.0500 mg/L0.000600 U 0.000600Silver
Prepared & Analyzed: 10/17/2016LCS (B6J0314-BS1)
0.0100 1.00 80-12096mg/L0.960 0.00400Arsenic
0.0500 1.00 80-12096mg/L0.958 0.00200Barium
0.00500 1.00 80-12095mg/L0.950 0.000300Cadmium
0.0100 1.00 80-12096mg/L0.964 0.000300Chromium
0.0100 1.00 80-12094mg/L0.940 0.00330Lead
0.0500 1.00 80-12096mg/L0.956 0.0113Selenium
0.0500 1.00 80-12095mg/L0.948 0.000600Silver
Prepared & Analyzed: 10/17/2016LCS Dup (B6J0314-BSD1)
0.0100 1.00 2080-12092 4mg/L0.921 0.00400Arsenic
0.0500 1.00 2080-12092 4mg/L0.924 0.00200Barium
0.00500 1.00 2080-12092 3mg/L0.917 0.000300Cadmium
0.0100 1.00 2080-12093 4mg/L0.930 0.000300Chromium
0.0100 1.00 2080-12091 3mg/L0.911 0.00330Lead
0.0500 1.00 2080-12092 4mg/L0.922 0.0113Selenium
0.0500 1.00 2080-12091 4mg/L0.914 0.000600Silver
Prepared & Analyzed: 10/17/2016Source: A6J0040-03Duplicate (B6J0314-DUP1)
0.0100 ND 20mg/L0.00400 U 0.00400Arsenic
0.0500 0.148 200.9mg/L0.149 0.00200Barium
0.00500 ND 20mg/L0.000300 U 0.000300Cadmium
0.0100 0.00117 208mg/L0.00108 J 0.000300Chromium
0.0100 0.00414 2023mg/L0.00519 XJ 0.00330Lead
0.0500 ND 20mg/L0.0113 U 0.0113Selenium
0.0500 ND 20mg/L0.000600 U 0.000600Silver
Page 26 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
7 RCRA Metals by Method 6010C (Continued)
MDL
Batch: B6J0314 (Continued)
Prepared & Analyzed: 10/17/2016Source: A6J0040-03Matrix Spike (B6J0314-MS1)
0.0100 1.00 ND 80-12092mg/L0.921 0.00400Arsenic
0.0500 1.00 0.148 80-12091mg/L1.06 0.00200Barium
0.00500 1.00 ND 80-12091mg/L0.911 0.000300Cadmium
0.0100 1.00 0.00117 80-12093mg/L0.928 0.000300Chromium
0.0100 1.00 0.00414 80-12091mg/L0.910 0.00330Lead
0.0500 1.00 ND 80-12092mg/L0.916 0.0113Selenium
0.0500 1.00 ND 80-12091mg/L0.906 0.000600Silver
Prepared & Analyzed: 10/17/2016Source: A6J0040-03Matrix Spike Dup (B6J0314-MSD1)
0.0100 1.00 ND 2080-12095 3mg/L0.945 0.00400Arsenic
0.0500 1.00 0.148 2080-12094 2mg/L1.08 0.00200Barium
0.00500 1.00 ND 2080-12094 3mg/L0.938 0.000300Cadmium
0.0100 1.00 0.00117 2080-12095 3mg/L0.953 0.000300Chromium
0.0100 1.00 0.00414 2080-12093 2mg/L0.931 0.00330Lead
0.0500 1.00 ND 2080-12094 3mg/L0.940 0.0113Selenium
0.0500 1.00 ND 2080-12093 3mg/L0.929 0.000600Silver
Page 27 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Total Mercury Analysis by Method 7470A
MDL
Batch: B6J0485
Prepared: 10/24/2016 Analyzed: 10/25/2016Blank (B6J0485-BLK1)
0.000200 mg/L0.0000840 J 0.0000100Mercury
Prepared: 10/24/2016 Analyzed: 10/25/2016LCS (B6J0485-BS1)
0.000200 0.00300 85-11592mg/L0.00277 0.0000100Mercury
Prepared: 10/24/2016 Analyzed: 10/25/2016LCS Dup (B6J0485-BSD1)
0.000200 0.00300 2085-11593 0.1mg/L0.00278 0.0000100Mercury
Prepared: 10/24/2016 Analyzed: 10/25/2016Source: A6J0040-02Duplicate (B6J0485-DUP1)
0.000200 ND 20mg/L0.0000100 U 0.0000100Mercury
Prepared: 10/24/2016 Analyzed: 10/25/2016Source: A6J0040-02Matrix Spike (B6J0485-MS1)
0.000200 0.00300 ND 85-11591mg/L0.00274 0.0000100Mercury
Prepared: 10/24/2016 Analyzed: 10/25/2016Source: A6J0040-02Matrix Spike Dup (B6J0485-MSD1)
0.000200 0.00300 ND 2085-11589 2mg/L0.00268 0.0000100Mercury
Page 28 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 11/1/16 14:31
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
List of Certifications for FTS Analytical Services - Atlanta
CodeDescriptionNumber ExpiresFacility
LANELAC04176LA CERTIFICATE 06/30/2016FTSA
ANC483NC CERTIFICATE 12/31/2016FTSA
KENTUKY85KENTUKY CERTIFICATE FTSA
ASC98015SC CERTIFICATE 06/30/2017FTSA
LFLNELACE84098FL NELAC CERTIFICATE 06/30/2017FTSL
AFLNELACE87429FL NELAC CERTIFICATE 06/30/2017FTSA
DODLI0-135 DoD CERTIFICATE 06/30/2016FTSA
USDAP330-07-00105 USDA CERTIFICATE FTSA
Notes and Definitions
Item Definition
The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. L
RPD Failure in the BKS/BSD.F
Dry Sample results reported on a dry weight basis.
U Analyte NOT DETECTED at or above the reporting limit.
A Suspected adol-condensation product.
B Analyte detected in the method blank.
C Confirmed by GC/MS analysis.
E Concentration exceeds calibration range.
K Hold Time exceeded.
N Tentatively Identified Compound.
P >25% difference between primary and secondary columns.
S Quantitation based on single-point calibration.
X General QC Failure see Case Narrative.
J The target analyte was positively identified below the Reporting Limit and above the Method Detection Limit.
RPD Relative Percent Difference
%REC Percent Recovery
Source Sample that was matrix spiked or duplicated.
Page 29 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
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