5301_LeeCounty_GWMR_DIN27907_20160411

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 

May 18, 2016 

Jaclynne Drummond 
Compliance Hydrogeologist 
NCDEQ, Division of Waste Management  
Solid Waste Section, Asheville Regional Office 
2090 US Highway 70, Swannanoa, NC 28778 

Re: Semi‐Annual Groundwater Monitoring Event (April 2016) 
 Lee County Landfill ‐ Sanford, NC 
 NCDWM – Solid Waste Section Permit # 53‐01 
 Terraquest Project No. 02296 

Dear Ms. Drummond: 

On behalf of the Lee County Department of Public Works, Terraquest Environmental 
Consultants, P.C. is reporting the results of a biannual ground and surface water sampling event 
that took pace at the Lee County Landfill in Sanford, NC on April 11, 2016.  In accordance with 
NCDWM‐SW’s reporting requirements, a Solid Waste Section Environmental Monitoring 
Reporting Form is attached.  The data from the event including analytical results, groundwater 
elevations, and field measured groundwater parameter data is summarized on the attached 
Table 1.  The location of the site is shown of Figure 1, the vicinity of the site on Figure 2, and 
site’s layout on Figure 3.  Figure 4 presents the recent potentiometric surface.  The full 
analytical report is also attached.  The following summarizes the event: 

On April 11, 2016, Terraquest personnel sampled monitoring wells MW5, MW6, MW9, MW10, 
MW12, and MW14, and collected one surface water sample, SW2.  An attempt was made to 
sample the SW1 location, however, no water was available.  All water samples were analyzed 
per SW‐846 8260B (VOCs) and SW‐846 7470A (mercury) and 6010C (RCRA Metals).  All water 
samples were collected following technical methods and standard procedures as outlined on 
the enclosed sheets.  Terraquest personnel also collected dissolved oxygen, pH, temperature, 
and conductivity measurements from each of the sampled monitoring wells following purging 
of the well and directly from the surface water body at the SW2 location.  These measurements 
are listed on the attached Table 1.   

The analytical results revealed detectable concentrations of petroleum‐type compounds in 
monitoring well MW12 only.  Benzene was reported at a concentration in excess of the 
standard set forth under Title 15A of the North Carolina Administrative Code Subchapter 2L 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 
.0202(g).  Results of the RCRA Metals analysis indicate that all of the monitoring wells and the 
surface water sample had a detection of at least one metal.  The analytical results are 
summarized in Table 1.   

A potentiometric surface map (Figure 4) depicting an interpreted groundwater flow direction at 
the site as measured on April 11, 2016 is attached.  Based upon the water levels in monitoring 
wells, the groundwater flow direction is to the southeast toward Mare Brand Creek.  This flow 
direction conforms with historical flow directions.  Table 1 lists the groundwater elevations for 
the monitoring wells. 

If you have any questions regarding the sampling event or analytical report, please contact 
Ryan Kerins at (919)‐563‐9091 or Mr. Joseph Cherry of the Lee County Public Works 
Department at (919)‐774‐8440.  Thank you. 

Sincerely, 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 

Ryan D. Kerins         Michael J. Brown P.G.    
Project Manager       President 

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Pa
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 2  of
 3
FA
C
I
L
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T
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 PE
R
M
I
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W
E
L
L
 ID

C
A
S
 Nu
m
b
e
r

S
W
S
 ID

P
A
R
A
M
E
T
E
R

R
E
S
U
L
T

U
N
I
T
S

Q
U
A
L
I
F
I
E
R
DIL
U
T
I
O
N

FA
C
T
O
R
CO
L
L
E
C
T
 DA
T
E
EXTRACTION  DATE*ANALYSIS  DATE
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
8
4
.
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
9

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

9
.
8
5

f
e
e
t
53
‐01

5
3
0
1
‐MW
9

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

37
4
.
4

f
e
e
t
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

5
.
5
1
53
‐01

5
3
0
1
‐MW
9

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

4
.
9
0

m
g
/
L
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
5
.
2

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
9

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
2
7

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
9

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
9

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
9

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
9

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
1

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

1
5
9

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

<
0
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

<
0
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

<
3
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
1
1
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
9

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
7
7
.
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

8
.
4
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
0

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
6
8
.
6

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

4
.
8
8
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

1
.
8
7

m
g
/
L
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
4
.
6

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
1
0

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
2
7

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
1
0

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
1

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

2
2
7

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

1
.
2
7

u
g
/
L

J

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

<
0
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

<
3
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
7
8
2
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‐2

1
8
3

S
e
l
e
n
i
u
m

<
1
1
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
0

7
4
4
0
‐22
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1
8
4

S
i
l
v
e
r

<
0
.
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
1

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
9
9
.
6

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
1

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

1
0
.
7
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
1

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
8
8
.
9

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
3
7
.
4

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

3
.
9
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
2

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
3
3
.
5

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

6
.
0
4
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

1
.
3
1

m
g
/
L
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
5
.
4

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
1
2

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
,
4
1
7

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
1
2

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

5
.
5
2

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

1
0
0
‐41
‐4

1
1
0

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t
h
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l
b
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n
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n
e

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0
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1
9

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/
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1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

1
3
3
0
‐20
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3
4
6

T
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t
a
l
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n
e
s

<
0
.
1
8

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g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
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1
2

1
0
8
‐90
‐7

3
9

C
h
l
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b
e
n
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2
3
.
9

u
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/
L

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
5
‐34
‐37
5

1
,
1
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h
l
o
r
o
e
t
h
a
n
e

3
.
4
4

u
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/
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1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
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1
2

7
4
3
9
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1
3
2

M
e
r
c
u
r
y

<
0
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0
1

u
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/
L

U

1

4
/
1
1
/
1
6

*

4
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐38
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1
4

A
r
s
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n
i
c

1
1
.
2

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

1
,
5
5
0

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

4
.
0
6

u
g
/
L

J

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

1
.
5
6

u
g
/
L

J

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

6
1
.
9

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
1
1
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
2

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
No
t
e
:
1.  
* Te
c
h
n
i
c
a
l
l
y
,
 th
i
s
 sa
m
p
l
e
 se
t
 di
d
n
'
t
 ha
v
e
 an
y
 ex
t
r
a
c
t
i
o
n
s
.
  Th
e
 me
t
a
l
s
 we
r
e
 pr
e
p
p
e
d
 an
d
 di
g
e
s
t
e
d
.
  Th
e
 vo
l
a
t
i
l
e
s
 ar
e
n
'
t
 in
v
o
l
v
e
d
 in
 an
y
 ex
t
r
a
c
t
i
o
n
 pr
o
c
e
s
s
.
  Th
e
y
 ar
e
 lo
a
d
e
d
 dir
e
c
t
l
y
 on
t
o
 th
e
 in
s
t
r
u
m
e
n
t
.

Ta
b
l
e
 1  ‐

CO
N
T
I
N
U
E
D
GR
O
U
N
D
W
A
T
E
R
 DA
T
A
 4/
1
1
/
1
6
Da
t
e
:
 5/
1
8
/
1
6
Fa
c
i
l
i
t
y
 Na
m
e
:

Le
e
 Co
u
n
t
y
 La
n
d
f
i
l
l
Pa
g
e
 3  of
 3
FA
C
I
L
I
T
Y
 PE
R
M
I
T

W
E
L
L
 ID

C
A
S
 Nu
m
b
e
r

S
W
S
 ID

P
A
R
A
M
E
T
E
R

R
E
S
U
L
T

U
N
I
T
S

Q
U
A
L
I
F
I
E
R

D
I
L
U
T
I
O
N

CO
L
L
E
C
T
 DA
T
E

E
X
T
R
A
C
T
I
O
N
 ANALYSIS  DATE
53
‐01

5
3
0
1
‐MW
1
3

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
6
3
.
9
3

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
3

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

8
.
2
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
3

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
5
5
.
7

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
5
8
.
6
1

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

6
.
4
0

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
5
2
.
2

f
e
e
t
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

5
.
9
7
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

1
.
1
0

m
g
/
L
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
5
.
2

d
e
g
.
 C
53
‐01

5
3
0
1
‐MW
1
4

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

2
3
0

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐MW
1
4

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
1

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
2
0
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

9
.
2
4

u
g
/
L

J

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

2
0
3

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

0
.
3
5

u
g
/
L

J

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

6
.
0
2

u
g
/
L

J

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

5
6
.
3

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
1
1
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐MW
1
4

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

6
.
5
8
53
‐01

5
3
0
1
‐SW
2

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

6
.
6
2

m
g
/
L
53
‐01

5
3
0
1
‐SW
2

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

2
1
.
1

d
e
g
.
 C
53
‐01

5
3
0
1
‐SW
2

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
2
5

m
i
c
r
o
S
/
s
e
c
53
‐01

5
3
0
1
‐SW
2

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐SW
2

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐SW
2

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐SW
2

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
1
8

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
5
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
1

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
2
0
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
4

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

5
6
.
7

u
g
/
L

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

<
0
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

<
0
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

<
3
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
1
1
.
3

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
53
‐01

5
3
0
1
‐SW
2

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
5
0

u
g
/
L

U

1

4
/
1
1
/
1
6

*

4
/
1
9
/
1
6
No
t
e
:
GR
O
U
N
D
W
A
T
E
R
 DA
T
A
 4/
1
1
/
1
6
1.  
* Te
c
h
n
i
c
a
l
l
y
,
 th
i
s
 sa
m
p
l
e
 se
t
 di
d
n
'
t
 ha
v
e
 an
y
 ex
t
r
a
c
t
i
o
n
s
.
  Th
e
 me
t
a
l
s
 we
r
e
 pr
e
p
p
e
d
 an
d
 di
g
e
s
t
e
d
.
  Th
e
 vo
l
a
t
i
l
e
s
 ar
e
n
'
t
 in
v
o
l
v
e
d
 in
 an
y
 ex
t
r
a
c
t
i
o
n
 pr
o
c
e
s
s
.
  Th
e
y
 ar
e
 lo
a
d
e
d
 dir
e
c
t
l
y
 on
t
o
 th
e
 in
s
t
r
u
m
e
n
t
.

Da
t
e
:
 5/
1
8
/
1
6
Fa
c
i
l
i
t
y
 Na
m
e
:

Le
e
 Co
u
n
t
y
 La
n
d
f
i
l
l
Ta
b
l
e
 1  ‐

CO
N
T
I
N
U
E
D
 TECHNICAL METHODS/STANDARD PROCEDURES 

Groundwater Sampling 

Groundwater samples are collected from temporary or permanent monitoring wells according to 
established sampling protocol.  When multiple monitoring wells or sampling points are sampled, 
sampling is completed beginning with the least contaminated well to the most contaminated well, 
if it is known.  When permanent monitoring wells for petroleum sites are sampled, the well is 
purged of a minimum of three well‐bore volumes prior to sample collection in order to assure that 
sampled water is representative of aquifer conditions.  In temporary wells, the first water which 
migrates into the open borehole is sampled.  Samples from both temporary and permanent 
monitoring wells are collected using individually wrapped disposable polyethylene bailers by field 
personnel wearing disposable nitrile gloves.  Only one well is sampled with a given bailer in order to 
prevent sample cross‐contamination.  During both well purging and sampling, proper protective 
clothing and equipment is used and is dependent upon the type and level of contaminants present. 
Also, field personnel change gloves between different samples to reduce the chance of cross‐
contamination. Water samples are transferred from the bailer to laboratory‐prepared sampling 
containers using slow emptying devices to reduce the chance of contamination loss through 
volatilization.  Preservatives, such as acids, are provided by the laboratory in pre‐prepared 
containers in which collected samples are placed if in‐field preservation is necessary.  The samples 
are labeled with the project name, project number, sample identification, required analysis, and 
date and time of collection.  The samples are placed on ice, shipped to a certified laboratory, and 
analyzed before the expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody 
documentation is maintained for each sample collected in the field.   

Surface Water Sampling 

Surface water samples, specifically samples from creeks or streams, are collected from a 
moving/flowing portion of the creek or stream to ensure that stagnant water is not collected.  Field 
personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a 
loss of volatile contaminants which might have been contained in the creek’s/stream’s water.  
Samples are collected by field personnel wearing disposable nitrile gloves.  Field personnel change 
gloves between different locations to reduce the chance of cross‐contamination.  Samples are 
collected directly from the appropriate creek or stream location and placed into the appropriate 
laboratory‐prepared containers.  Preservatives, such as acids, are provided by the laboratory in pre‐
prepared containers in which collected samples are placed if in‐field preservation is necessary. The 
samples are labeled with the project name, project number, sample identification, required 
analysis, and date and time of collection.  The samples are cooled on ice to approximately four 
degrees centigrade, shipped to a certified laboratory, and analyzed before the expiration of an 
analytical method’s prescribed holding time.  Chain‐of‐custody documentation is maintained for 
each sample collected in the field.    

Field Measurements 

Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen 
concentration of a particular groundwater sample are taken directly after a particular monitoring 
well has been adequately purged.  This ensures that the groundwater parameter data collected is 
representative of the aquifer conditions at a given location.  Once purging of the monitoring well is 
complete, the decontaminated probe head and cord of the appropriate unit is lowered into the 
required monitoring well.  If the depth to water in a specific monitoring well is greater than the 
length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate 
monitoring well and a representative groundwater sample is retrieved.  A slow pouring device is 
fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable 
plastic cup.  Groundwater parameter data are then collected from the groundwater in the cup 
using the required unit.   

For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is 
utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s operations 
manual by field personnel.  Prior to data collection, the unit is properly decontaminated to prevent 
cross‐contamination.  The unit is decontaminated between each sample.  The procedure used for 
sample measurement involves lowering the meter’s probe into the new, disposable cup containing 
the groundwater sample to be measured and slowly stirring the probe to force groundwater across 
the probe’s membrane.  The measurements displayed by the meter are then recorded.   

For dissolved oxygen concentration measurements, a YSI® Model 55 Handheld Dissolved Oxygen 
System is utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s 
operations manual by field personnel.  Prior to data collection, the unit is properly decontaminated 
to prevent cross‐contamination.  The unit is decontaminated between each sample.  The procedure 
used for sample measurement involves adjusting the unit for the correct altitude where the 
sampling will take place and adjusting the reported units desired.  Once this is done, the unit’s 
probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to 
force the groundwater across the probe’s membrane.  The measurements displayed by the unit are 
then recorded.   
Analytical Report
A6D0069
Project
Lee County Landfill
Project Number
02296
May 05, 2016
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Mebane, NC 27302
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
6017 Financial Drive Phone #:[phone]
Website:www.ftsanalytical.comNorcross, GA 30071
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
May 05, 2016
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Ryan Kerins
RE: Lee County Landfill
We are reporting the results of the analyses performed on the samples recieved on 4/13/2016 under the
project name referenced above and identified as the lab Work Order A6D0069. All results being reported
under this Report apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontracted lab, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reporting using all other available quality control methods.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed
for at least 5 years in our archives after which time it will be destroyed without further notice, unless
otherwise agreed upon. The samples received, and described as recorded in Work Order A6D0069 will be
filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise
agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard
practices, controlled/regulated substances, etc.)
We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions
concerning this report, please do not hesitate to contact us at any time. We will be happy to help.
Mebane, NC 27302
Sincerely,
Chad A. Bechtold
VP of Client Services
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Samples in this Report
Sample Lab ID Matrix Date Sampled Date Received
MW6 WaterA6D0069-01 13-Apr-2016 09:4511-Apr-2016 11:35
MW9 WaterA6D0069-02 13-Apr-2016 09:4511-Apr-2016 11:20
MW10 WaterA6D0069-03 13-Apr-2016 09:4511-Apr-2016 11:25
MW14 WaterA6D0069-04 13-Apr-2016 09:4511-Apr-2016 11:00
MW5 WaterA6D0069-05 13-Apr-2016 09:4511-Apr-2016 12:25
MW12 WaterA6D0069-06 13-Apr-2016 09:4511-Apr-2016 12:00
SW2 WaterA6D0069-07 13-Apr-2016 09:4511-Apr-2016 12:40
Page 3 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Analysis Case Narrative

SM6200B
Batch B6E0097
The precision (% RPD) of the LCS/LCSD was outside control limits for Tetrachloroethene. The precision (% RPD) was within limits
for the batch Matrix Spike/Matrix Spike Duplicate; therefore, the data was accepted.
Samples affected are: A6D0069-01,-02,-03,-04,-05,-06,-07.
Page 4 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Hit Summary

Sample: MW6
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-01
Sampled: 4/11/16 11:35
Barium 0.0500 mg/L0.00200 1J0.0418 4/19/16 15:29 7440-39-3 EPA 6010C
Sample: MW9
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-02
Sampled: 4/11/16 11:20
Barium 0.0500 mg/L0.00200 10.159 4/19/16 15:30 7440-39-3 EPA 6010C
Sample: MW10
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-03
Sampled: 4/11/16 11:25
Barium 0.0500 mg/L0.00200 10.227 4/19/16 15:32 7440-39-3 EPA 6010C
Cadmium 0.00500 mg/L0.000300 1J0.00127 4/19/16 15:32 7440-43-9 EPA 6010C
Sample: MW14
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-04
Sampled: 4/11/16 11:00
Arsenic 0.0100 mg/L0.00400 1J0.00924 4/19/16 15:34 7440-38-2 EPA 6010C
Barium 0.0500 mg/L0.00200 10.203 4/19/16 15:34 7440-39-3 EPA 6010C
Cadmium 0.00500 mg/L0.000300 1J0.000350 4/19/16 15:34 7440-43-9 EPA 6010C
Chromium 0.0100 mg/L0.000300 1J0.00602 4/19/16 15:34 7440-47-3 EPA 6010C
Lead 0.0100 mg/L0.00330 10.0563 4/19/16 15:34 7439-92-1 EPA 6010C
Sample: MW5
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-05
Sampled: 4/11/16 12:25
Arsenic 0.0100 mg/L0.00400 1J0.00959 4/19/16 15:41 7440-38-2 EPA 6010C
Barium 0.0500 mg/L0.00200 10.344 4/19/16 15:41 7440-39-3 EPA 6010C
Cadmium 0.00500 mg/L0.000300 1J0.00136 4/19/16 15:41 7440-43-9 EPA 6010C
Lead 0.0100 mg/L0.00330 10.0190 4/19/16 15:41 7439-92-1 EPA 6010C
Sample: MW12
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-06
Sampled: 4/11/16 12:00
Page 5 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Hit Summary
(Continued)
Arsenic 0.0100 mg/L0.00400 10.0112 4/19/16 15:43 7440-38-2 EPA 6010C
Barium 0.0500 mg/L0.00200 11.55 4/19/16 15:43 7440-39-3 EPA 6010C
1,1-Dichloroethane 1.00 ug/L0.110 13.44 4/15/16 7:27 75-34-3 EPA 8260B APP I
Cadmium 0.00500 mg/L0.000300 1J0.00406 4/19/16 15:43 7440-43-9 EPA 6010C
Chromium 0.0100 mg/L0.000300 1J0.00156 4/19/16 15:43 7440-47-3 EPA 6010C
Lead 0.0100 mg/L0.00330 10.0619 4/19/16 15:43 7439-92-1 EPA 6010C
Benzene 1.00 ug/L0.160 15.52 4/15/16 7:27 71-43-2 EPA 8260B APP I
Chlorobenzene 1.00 ug/L0.150 123.9 4/15/16 7:27 108-90-7 EPA 8260B APP I
Sample: SW2
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: A6D0069-07
Sampled: 4/11/16 12:40
Barium 0.0500 mg/L0.00200 10.0567 4/19/16 15:45 7440-39-3 EPA 6010C
Page 6 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results

ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-01 (Water)
Client Sample ID: MW6
RL Dil Date Prepared
Sampled: 4/11/16 11:35
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.00400 U 4/19/16 15:294/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 10.0418 J 4/19/16 15:294/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.000300 U 4/19/16 15:294/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.000300 U 4/19/16 15:294/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.00330 U 4/19/16 15:294/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:294/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:294/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 5:144/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 5:144/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 5:144/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 5:144/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 10.110 U 4/15/16 5:144/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 5:144/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 5:144/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 5:144/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 5:144/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 5:144/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 5:144/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 5:144/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 5:144/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 5:144/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 5:144/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 5:144/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 5:144/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 5:144/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 10.160 U 4/15/16 5:144/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 5:144/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 5:144/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 5:144/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 5:144/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 5:144/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 5:144/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 10.150 U 4/15/16 5:144/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 5:144/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 5:144/14/16 21:59 67-66-3
Page 7 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-01 (Water)
Client Sample ID: MW6 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 11:35
CAS #
VOCs by Method 8260B (Continued)
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 5:144/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 5:144/14/16 21:59 156-59-4
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 5:144/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 5:144/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 5:144/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 5:144/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 5:144/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 5:144/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 5:144/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 5:144/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 5:144/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 5:144/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 5:144/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 5:144/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 5:144/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 5:144/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 5:144/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 5:144/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 5:144/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 5:144/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 5:144/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 5:144/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15999%4/15/16 5:14 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186103%4/15/16 5:14 460-00-4
Surrogate: Toluene-D8 (SUR)70-130110%4/15/16 5:14 2037-26-5
Page 8 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-02 (Water)
Client Sample ID: MW9
RL Dil Date Prepared
Sampled: 4/11/16 11:20
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.00400 U 4/19/16 15:304/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 10.159 4/19/16 15:304/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.000300 U 4/19/16 15:304/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.000300 U 4/19/16 15:304/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.00330 U 4/19/16 15:304/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:304/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:304/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 5:404/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 5:404/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 5:404/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 5:404/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 10.110 U 4/15/16 5:404/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 5:404/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 5:404/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 5:404/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 5:404/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 5:404/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 5:404/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 5:404/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 5:404/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 5:404/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 5:404/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 5:404/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 5:404/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 5:404/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 10.160 U 4/15/16 5:404/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 5:404/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 5:404/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 5:404/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 5:404/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 5:404/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 5:404/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 10.150 U 4/15/16 5:404/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 5:404/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 5:404/14/16 21:59 67-66-3
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 5:404/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 5:404/14/16 21:59 156-59-4
Page 9 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-02 (Water)
Client Sample ID: MW9 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 11:20
CAS #
VOCs by Method 8260B (Continued)
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 5:404/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 5:404/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 5:404/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 5:404/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 5:404/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 5:404/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 5:404/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 5:404/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 5:404/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 5:404/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 5:404/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 5:404/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 5:404/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 5:404/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 5:404/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 5:404/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 5:404/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 5:404/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 5:404/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 5:404/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15999%4/15/16 5:40 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186105%4/15/16 5:40 460-00-4
Surrogate: Toluene-D8 (SUR)70-130106%4/15/16 5:40 2037-26-5
Page 10 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-03 (Water)
Client Sample ID: MW10
RL Dil Date Prepared
Sampled: 4/11/16 11:25
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.00400 U 4/19/16 15:324/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 10.227 4/19/16 15:324/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.00127 J 4/19/16 15:324/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.000300 U 4/19/16 15:324/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.00330 U 4/19/16 15:324/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:324/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:324/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 6:074/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 6:074/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 6:074/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 6:074/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 10.110 U 4/15/16 6:074/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 6:074/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 6:074/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 6:074/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 6:074/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 6:074/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 6:074/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 6:074/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 6:074/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 6:074/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 6:074/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 6:074/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 6:074/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 6:074/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 10.160 U 4/15/16 6:074/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 6:074/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 6:074/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 6:074/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 6:074/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 6:074/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 6:074/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 10.150 U 4/15/16 6:074/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 6:074/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 6:074/14/16 21:59 67-66-3
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 6:074/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 6:074/14/16 21:59 156-59-4
Page 11 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-03 (Water)
Client Sample ID: MW10 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 11:25
CAS #
VOCs by Method 8260B (Continued)
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 6:074/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 6:074/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 6:074/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 6:074/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 6:074/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 6:074/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 6:074/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 6:074/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 6:074/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 6:074/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 6:074/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 6:074/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 6:074/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 6:074/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 6:074/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 6:074/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 6:074/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 6:074/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 6:074/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 6:074/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15998%4/15/16 6:07 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186105%4/15/16 6:07 460-00-4
Surrogate: Toluene-D8 (SUR)70-130110%4/15/16 6:07 2037-26-5
Page 12 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-04 (Water)
Client Sample ID: MW14
RL Dil Date Prepared
Sampled: 4/11/16 11:00
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.00924 J 4/19/16 15:344/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 10.203 4/19/16 15:344/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.000350 J 4/19/16 15:344/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.00602 J 4/19/16 15:344/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.0563 4/19/16 15:344/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:344/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:344/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 6:344/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 6:344/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 6:344/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 6:344/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 10.110 U 4/15/16 6:344/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 6:344/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 6:344/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 6:344/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 6:344/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 6:344/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 6:344/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 6:344/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 6:344/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 6:344/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 6:344/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 6:344/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 6:344/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 6:344/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 10.160 U 4/15/16 6:344/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 6:344/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 6:344/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 6:344/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 6:344/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 6:344/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 6:344/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 10.150 U 4/15/16 6:344/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 6:344/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 6:344/14/16 21:59 67-66-3
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 6:344/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 6:344/14/16 21:59 156-59-4
Page 13 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-04 (Water)
Client Sample ID: MW14 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 11:00
CAS #
VOCs by Method 8260B (Continued)
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 6:344/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 6:344/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 6:344/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 6:344/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 6:344/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 6:344/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 6:344/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 6:344/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 6:344/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 6:344/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 6:344/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 6:344/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 6:344/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 6:344/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 6:344/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 6:344/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 6:344/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 6:344/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 6:344/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 6:344/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15998%4/15/16 6:34 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186104%4/15/16 6:34 460-00-4
Surrogate: Toluene-D8 (SUR)70-130109%4/15/16 6:34 2037-26-5
Page 14 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-05 (Water)
Client Sample ID: MW5
RL Dil Date Prepared
Sampled: 4/11/16 12:25
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.00959 J 4/19/16 15:414/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 10.344 4/19/16 15:414/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.00136 J 4/19/16 15:414/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.000300 U 4/19/16 15:414/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.0190 4/19/16 15:414/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:414/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:414/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 7:004/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 7:004/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 7:004/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 7:004/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 10.110 U 4/15/16 7:004/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 7:004/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 7:004/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 7:004/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 7:004/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 7:004/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 7:004/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 7:004/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 7:004/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 7:004/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 7:004/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 7:004/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 7:004/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 7:004/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 10.160 U 4/15/16 7:004/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 7:004/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 7:004/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 7:004/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 7:004/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 7:004/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 7:004/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 10.150 U 4/15/16 7:004/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 7:004/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 7:004/14/16 21:59 67-66-3
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 7:004/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 7:004/14/16 21:59 156-59-4
Page 15 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-05 (Water)
Client Sample ID: MW5 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 12:25
CAS #
VOCs by Method 8260B (Continued)
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 7:004/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 7:004/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 7:004/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 7:004/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 7:004/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 7:004/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 7:004/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 7:004/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 7:004/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 7:004/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 7:004/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 7:004/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 7:004/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 7:004/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 7:004/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 7:004/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 7:004/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 7:004/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 7:004/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 7:004/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15999%4/15/16 7:00 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186107%4/15/16 7:00 460-00-4
Surrogate: Toluene-D8 (SUR)70-130109%4/15/16 7:00 2037-26-5
Page 16 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-06 (Water)
Client Sample ID: MW12
RL Dil Date Prepared
Sampled: 4/11/16 12:00
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.0112 4/19/16 15:434/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 11.55 4/19/16 15:434/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.00406 J 4/19/16 15:434/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.00156 J 4/19/16 15:434/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.0619 4/19/16 15:434/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:434/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:434/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 7:274/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 7:274/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 7:274/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 7:274/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 13.44 4/15/16 7:274/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 7:274/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 7:274/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 7:274/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 7:274/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 7:274/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 7:274/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 7:274/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 7:274/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 7:274/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 7:274/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 7:274/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 7:274/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 7:274/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 15.52 4/15/16 7:274/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 7:274/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 7:274/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 7:274/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 7:274/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 7:274/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 7:274/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 123.9 4/15/16 7:274/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 7:274/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 7:274/14/16 21:59 67-66-3
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 7:274/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 7:274/14/16 21:59 156-59-4
Page 17 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-06 (Water)
Client Sample ID: MW12 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 12:00
CAS #
VOCs by Method 8260B (Continued)
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 7:274/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 7:274/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 7:274/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 7:274/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 7:274/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 7:274/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 7:274/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 7:274/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 7:274/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 7:274/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 7:274/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 7:274/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 7:274/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 7:274/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 7:274/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 7:274/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 7:274/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 7:274/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 7:274/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 7:274/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-159101%4/15/16 7:27 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186103%4/15/16 7:27 460-00-4
Surrogate: Toluene-D8 (SUR)70-130106%4/15/16 7:27 2037-26-5
Page 18 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-07 (Water)
Client Sample ID: SW2
RL Dil Date Prepared
Sampled: 4/11/16 12:40
CAS #
Total Metal Analysis by Method 6010C
Arsenic 0.0100 mg/L0.00400 10.00400 U 4/19/16 15:454/19/16 8:21 7440-38-2
Barium 0.0500 mg/L0.00200 10.0567 4/19/16 15:454/19/16 8:21 7440-39-3
Cadmium 0.00500 mg/L0.000300 10.000300 U 4/19/16 15:454/19/16 8:21 7440-43-9
Chromium 0.0100 mg/L0.000300 10.000300 U 4/19/16 15:454/19/16 8:21 7440-47-3
Lead 0.0100 mg/L0.00330 10.00330 U 4/19/16 15:454/19/16 8:21 7439-92-1
Selenium 0.0500 mg/L0.0113 10.0113 U 4/19/16 15:454/19/16 8:21 7782-49-2
Silver 0.0500 mg/L0.000600 10.000600 U 4/19/16 15:454/19/16 8:21 7440-22-4
Total Metal Analysis by Method 7470
Mercury 0.000200 mg/L0.0000100 10.0000100 U 4/20/16 14:144/19/16 10:53 7439-97-6
VOCs by Method 8260B
1,1,1,2-Tetrachloroethane 1.00 ug/L0.240 10.240 U 4/15/16 7:544/14/16 21:59 630-20-6
1,1,1-Trichloroethane 1.00 ug/L0.160 10.160 U 4/15/16 7:544/14/16 21:59 71-55-6
1,1,2,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 4/15/16 7:544/14/16 21:59 79-34-5
1,1,2-Trichloroethane 1.00 ug/L0.250 10.250 U 4/15/16 7:544/14/16 21:59 79-00-5
1,1-Dichloroethane 1.00 ug/L0.110 10.110 U 4/15/16 7:544/14/16 21:59 75-34-3
1,1-Dichloroethene 1.00 ug/L0.200 10.200 U 4/15/16 7:544/14/16 21:59 75-35-4
1,2,3-Trichloropropane 1.00 ug/L0.210 10.210 U 4/15/16 7:544/14/16 21:59 96-18-4
1,2-Dibromo-3-Chloropropane (DBCP)1.00 ug/L0.190 10.190 U 4/15/16 7:544/14/16 21:59 96-12-8
1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 4/15/16 7:544/14/16 21:59 106-93-4
1,2-Dichlorobenzene 1.00 ug/L0.140 10.140 U 4/15/16 7:544/14/16 21:59 95-50-1
1,2-Dichloroethane 1.00 ug/L0.180 10.180 U 4/15/16 7:544/14/16 21:59 107-06-2
1,2-Dichloropropane 1.00 ug/L0.150 10.150 U 4/15/16 7:544/14/16 21:59 78-87-5
1,4-Dichlorobenzene 1.00 ug/L0.170 10.170 U 4/15/16 7:544/14/16 21:59 106-46-7
2-Butanone (MEK)50.0 ug/L2.52 12.52 U 4/15/16 7:544/14/16 21:59 78-93-3
2-Hexanone 2.00 ug/L0.320 10.320 U 4/15/16 7:544/14/16 21:59 591-78-6
4-Methyl-2-pentanone (MIBK)2.00 ug/L0.260 10.260 U 4/15/16 7:544/14/16 21:59 108-10-1
Acetone 10.0 ug/L0.350 10.350 U 4/15/16 7:544/14/16 21:59 67-64-1
Acrylonitrile 2.00 ug/L0.490 10.490 U 4/15/16 7:544/14/16 21:59 107-13-1
Benzene 1.00 ug/L0.160 10.160 U 4/15/16 7:544/14/16 21:59 71-43-2
Bromochloromethane 1.00 ug/L0.200 10.200 U 4/15/16 7:544/14/16 21:59 74-97-5
Bromodichloromethane 1.00 ug/L0.250 10.250 U 4/15/16 7:544/14/16 21:59 75-27-4
Bromoform 1.00 ug/L0.170 10.170 U 4/15/16 7:544/14/16 21:59 75-25-2
Bromomethane (Methyl Bromide)1.00 ug/L0.250 10.250 U 4/15/16 7:544/14/16 21:59 74-83-9
Carbon disulfide 1.00 ug/L0.260 10.260 U 4/15/16 7:544/14/16 21:59 75-15-0
Carbon tetrachloride 1.00 ug/L0.330 10.330 U 4/15/16 7:544/14/16 21:59 56-23-5
Chlorobenzene 1.00 ug/L0.150 10.150 U 4/15/16 7:544/14/16 21:59 108-90-7
Chloroethane 1.00 ug/L0.260 10.260 U 4/15/16 7:544/14/16 21:59 75-00-3
Chloroform 1.00 ug/L0.160 10.160 U 4/15/16 7:544/14/16 21:59 67-66-3
Chloromethane (Methyl Chloride)1.00 ug/L0.250 10.250 U 4/15/16 7:544/14/16 21:59 74-87-3
cis-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 7:544/14/16 21:59 156-59-4
Page 19 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6D0069-07 (Water)
Client Sample ID: SW2 (Continued)
RL Dil Date Prepared
Sampled: 4/11/16 12:40
CAS #
VOCs by Method 8260B (Continued)
cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 4/15/16 7:544/14/16 21:59 10061-01-5
Dibromochloromethane 1.00 ug/L0.150 10.150 U 4/15/16 7:544/14/16 21:59 124-48-1
Dibromomethane 1.00 ug/L0.240 10.240 U 4/15/16 7:544/14/16 21:59 74-95-3
Ethylbenzene 1.00 ug/L0.190 10.190 U 4/15/16 7:544/14/16 21:59 100-41-4
Iodomethane (Methyl Iodide)1.00 ug/L0.310 10.310 U 4/15/16 7:544/14/16 21:59 74-88-4
m,p-Xylenes 2.00 ug/L0.510 10.510 U 4/15/16 7:544/14/16 21:59 179601-23-1
Methylene Chloride 1.00 ug/L0.420 10.420 U 4/15/16 7:544/14/16 21:59 75-09-2
o-Xylene 1.00 ug/L0.200 10.200 U 4/15/16 7:544/14/16 21:59 95-47-6
Styrene 1.00 ug/L0.180 10.180 U 4/15/16 7:544/14/16 21:59 100-42-5
Tetrachloroethylene 1.00 ug/L0.160 10.160 U 4/15/16 7:544/14/16 21:59 127-18-4
Tetrahydrofuran 5.00 ug/L0.236 10.236 U 4/15/16 7:544/14/16 21:59 109-99-9
Toluene 1.00 ug/L0.140 10.140 U 4/15/16 7:544/14/16 21:59 108-88-3
Total Xylenes 1.00 ug/L0.180 10.180 U 4/15/16 7:544/14/16 21:59 1330-20-7
trans-1,2-Dichloroethene 1.00 ug/L0.210 10.210 U 4/15/16 7:544/14/16 21:59 156-60-5
trans-1,3-Dichloropropene 1.00 ug/L0.110 10.110 U 4/15/16 7:544/14/16 21:59 1006-10-26
trans-1,4-Dichloro-2-butene 1.00 ug/L0.190 10.190 U 4/15/16 7:544/14/16 21:59 110-57-6
Trichloroethylene 1.00 ug/L0.190 10.190 U 4/15/16 7:544/14/16 21:59 79-01-6
Trichlorofluoromethane 1.00 ug/L0.530 10.530 U 4/15/16 7:544/14/16 21:59 75-69-4
Vinyl acetate 1.00 ug/L0.720 10.720 U 4/15/16 7:544/14/16 21:59 108-05-4
Vinyl chloride 1.00 ug/L0.190 10.190 U 4/15/16 7:544/14/16 21:59 75-01-4
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15998%4/15/16 7:54 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-186107%4/15/16 7:54 460-00-4
Surrogate: Toluene-D8 (SUR)70-130109%4/15/16 7:54 2037-26-5
Page 20 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
VOCs by Method 8260B
MDL
Batch: B6E0097
Prepared: 4/14/2016 Analyzed: 4/15/2016Blank (B6E0097-BLK1)
1.00 ug/L0.240 U 0.2401,1,1,2-Tetrachloroethane
1.00 ug/L0.160 U 0.1601,1,1-Trichloroethane
1.00 ug/L0.180 U 0.1801,1,2,2-Tetrachloroethane
1.00 ug/L0.250 U 0.2501,1,2-Trichloroethane
1.00 ug/L0.110 U 0.1101,1-Dichloroethane
1.00 ug/L0.200 U 0.2001,1-Dichloroethene
1.00 ug/L0.210 U 0.2101,2,3-Trichloropropane
1.00 ug/L0.190 U 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB)
1.00 ug/L0.140 U 0.1401,2-Dichlorobenzene
1.00 ug/L0.180 U 0.1801,2-Dichloroethane
1.00 ug/L0.150 U 0.1501,2-Dichloropropane
1.00 ug/L0.170 U 0.1701,4-Dichlorobenzene
50.0 ug/L2.52 U 2.522-Butanone (MEK)
2.00 ug/L0.320 U 0.3202-Hexanone
2.00 ug/L0.260 U 0.2604-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 U 0.350Acetone
2.00 ug/L0.490 U 0.490Acrylonitrile
1.00 ug/L0.160 U 0.160Benzene
1.00 ug/L0.200 U 0.200Bromochloromethane
1.00 ug/L0.250 U 0.250Bromodichloromethane
1.00 ug/L0.170 U 0.170Bromoform
1.00 ug/L0.250 U 0.250Bromomethane (Methyl Bromide)
1.00 ug/L0.260 U 0.260Carbon disulfide
1.00 ug/L0.330 U 0.330Carbon tetrachloride
1.00 ug/L0.150 U 0.150Chlorobenzene
1.00 ug/L0.260 U 0.260Chloroethane
1.00 ug/L0.160 U 0.160Chloroform
1.00 ug/L0.250 U 0.250Chloromethane (Methyl Chloride)
1.00 ug/L0.210 U 0.210cis-1,2-Dichloroethene
1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene
1.00 ug/L0.150 U 0.150Dibromochloromethane
1.00 ug/L0.240 U 0.240Dibromomethane
1.00 ug/L0.190 U 0.190Ethylbenzene
1.00 ug/L0.310 U 0.310Iodomethane (Methyl Iodide)
2.00 ug/L0.510 U 0.510m,p-Xylenes
1.00 ug/L0.420 U 0.420Methylene Chloride
1.00 ug/L0.200 U 0.200o-Xylene
1.00 ug/L0.180 U 0.180Styrene
1.00 ug/L0.160 U 0.160Tetrachloroethylene
1.00 ug/L0.140 U 0.140Toluene
Page 21 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by Method 8260B (Continued)
MDL
Batch: B6E0097 (Continued)
Prepared: 4/14/2016 Analyzed: 4/15/2016Blank (B6E0097-BLK1)
1.00 ug/L0.180 U 0.180Total Xylenes
1.00 ug/L0.210 U 0.210trans-1,2-Dichloroethene
1.00 ug/L0.110 U 0.110trans-1,3-Dichloropropene
1.00 ug/L0.190 U 0.190trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 U 0.190Trichloroethylene
1.00 ug/L0.530 U 0.530Trichlorofluoromethane
1.00 ug/L0.720 U 0.720Vinyl acetate
1.00 ug/L0.190 U 0.190Vinyl chloride
25.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)10125.2 ug/L
25.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)10626.6 ug/L
25.0 70-130Surrogate: Toluene-D8 (SUR)10927.3 ug/L
Prepared & Analyzed: 4/14/2016LCS (B6E0097-BS1)
1.00 25.0 80-130113ug/L28.1 0.2401,1,1,2-Tetrachloroethane
1.00 25.0 65-13089ug/L22.2 0.1601,1,1-Trichloroethane
1.00 25.0 65-130112ug/L28.0 0.1801,1,2,2-Tetrachloroethane
1.00 25.0 75-125105ug/L26.3 0.2501,1,2-Trichloroethane
1.00 25.0 70-13594ug/L23.5 0.1101,1-Dichloroethane
1.00 25.0 70-13090ug/L22.5 0.2001,1-Dichloroethene
1.00 25.0 75-125111ug/L27.9 0.2101,2,3-Trichloropropane
1.00 25.0 50-130114ug/L28.5 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 25.0 80-120105ug/L26.3 0.1801,2-Dibromoethane (EDB)
1.00 25.0 70-120109ug/L27.2 0.1401,2-Dichlorobenzene
1.00 25.0 70-13091ug/L22.7 0.1801,2-Dichloroethane
1.00 25.0 75-125101ug/L25.2 0.1501,2-Dichloropropane
1.00 25.0 75-125108ug/L27.1 0.1701,4-Dichlorobenzene
50.0 50.0 30-15092ug/L46.1 J 2.522-Butanone (MEK)
2.00 50.0 55-130104ug/L52.1 0.3202-Hexanone
2.00 50.0 60-13591ug/L45.4 0.2604-Methyl-2-pentanone (MIBK)
10.0 50.0 40-14099ug/L49.3 0.350Acetone
2.00 50.0 40-14097ug/L48.4 0.490Acrylonitrile
1.00 25.0 80-12099ug/L24.7 0.160Benzene
1.00 25.0 65-130101ug/L25.3 0.200Bromochloromethane
1.00 25.0 75-120102ug/L25.5 0.250Bromodichloromethane
1.00 25.0 70-130123ug/L30.8 0.170Bromoform
1.00 25.0 30-145101ug/L25.3 0.250Bromomethane (Methyl Bromide)
1.00 25.0 35-16093ug/L23.2 0.260Carbon disulfide
1.00 25.0 65-14095ug/L23.8 0.330Carbon tetrachloride
1.00 25.0 80-120107ug/L26.8 0.150Chlorobenzene
1.00 25.0 60-135100ug/L25.0 0.260Chloroethane
Page 22 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by Method 8260B (Continued)
MDL
Batch: B6E0097 (Continued)
Prepared & Analyzed: 4/14/2016LCS (B6E0097-BS1)
1.00 25.0 65-13598ug/L24.4 0.160Chloroform
1.00 25.0 40-12580ug/L19.9 0.250Chloromethane (Methyl Chloride)
1.00 25.0 70-125101ug/L25.2 0.210cis-1,2-Dichloroethene
1.00 25.0 70-130104ug/L25.9 0.100cis-1,3-Dichloropropene
1.00 25.0 60-135114ug/L28.4 0.150Dibromochloromethane
1.00 25.0 75-12599ug/L24.6 0.240Dibromomethane
1.00 25.0 75-125105ug/L26.3 0.190Ethylbenzene
1.00 25.0 65-13072ug/L18.1 0.310Iodomethane (Methyl Iodide)
2.00 50.0 75-130107ug/L53.4 0.510m,p-Xylenes
1.00 25.0 55-14090ug/L22.4 0.420Methylene Chloride
1.00 25.0 80-120107ug/L26.8 0.200o-Xylene
1.00 25.0 65-135114ug/L28.4 0.180Styrene
1.00 25.0 45-15098ug/L24.6 0.160Tetrachloroethylene
1.00 25.0 75-120105ug/L26.3 0.140Toluene
1.00 25.0 60-14097ug/L24.2 0.210trans-1,2-Dichloroethene
1.00 25.0 55-140113ug/L28.3 0.110trans-1,3-Dichloropropene
1.00 25.0 65-135109ug/L27.2 0.190trans-1,4-Dichloro-2-butene
1.00 25.0 70-12594ug/L23.5 0.190Trichloroethylene
1.00 25.0 60-14581ug/L20.3 0.530Trichlorofluoromethane
1.00 25.0 65-13599ug/L24.6 0.720Vinyl acetate
1.00 25.0 50-14585ug/L21.3 0.190Vinyl chloride
25.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9323.1 ug/L
25.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)10225.5 ug/L
25.0 70-130Surrogate: Toluene-D8 (SUR)10927.2 ug/L
Prepared & Analyzed: 4/14/2016LCS Dup (B6E0097-BSD1)
1.00 25.0 2080-130117 4ug/L29.2 0.2401,1,1,2-Tetrachloroethane
1.00 25.0 2065-13095 7ug/L23.7 0.1601,1,1-Trichloroethane
1.00 25.0 2065-130115 2ug/L28.6 0.1801,1,2,2-Tetrachloroethane
1.00 25.0 2075-125113 8ug/L28.3 0.2501,1,2-Trichloroethane
1.00 25.0 2070-13597 3ug/L24.2 0.1101,1-Dichloroethane
1.00 25.0 2070-13098 9ug/L24.6 0.2001,1-Dichloroethene
1.00 25.0 2075-125112 0.5ug/L28.0 0.2101,2,3-Trichloropropane
1.00 25.0 2050-130122 6ug/L30.4 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 25.0 2080-120111 6ug/L27.8 0.1801,2-Dibromoethane (EDB)
1.00 25.0 2070-120112 2ug/L27.9 0.1401,2-Dichlorobenzene
1.00 25.0 2070-13095 5ug/L23.8 0.1801,2-Dichloroethane
1.00 25.0 2075-125104 3ug/L26.0 0.1501,2-Dichloropropane
1.00 25.0 2075-125112 3ug/L27.9 0.1701,4-Dichlorobenzene
50.0 50.0 2030-15095 3ug/L47.5 J 2.522-Butanone (MEK)
Page 23 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by Method 8260B (Continued)
MDL
Batch: B6E0097 (Continued)
Prepared & Analyzed: 4/14/2016LCS Dup (B6E0097-BSD1)
2.00 50.0 2055-130114 9ug/L56.8 0.3202-Hexanone
2.00 50.0 2060-13595 4ug/L47.3 0.2604-Methyl-2-pentanone (MIBK)
10.0 50.0 2040-14094 5ug/L46.8 0.350Acetone
2.00 50.0 2040-14098 0.9ug/L48.8 0.490Acrylonitrile
1.00 25.0 2080-120103 5ug/L25.9 0.160Benzene
1.00 25.0 2065-130104 3ug/L26.1 0.200Bromochloromethane
1.00 25.0 2075-120106 4ug/L26.5 0.250Bromodichloromethane
1.00 25.0 2070-130126 2ug/L31.5 0.170Bromoform
1.00 25.0 2030-145107 5ug/L26.7 0.250Bromomethane (Methyl Bromide)
1.00 25.0 2035-160100 7ug/L25.0 0.260Carbon disulfide
1.00 25.0 2065-140108 13ug/L27.0 0.330Carbon tetrachloride
1.00 25.0 2080-120111 4ug/L27.8 0.150Chlorobenzene
1.00 25.0 2060-135101 1ug/L25.4 0.260Chloroethane
1.00 25.0 2065-13597 0.9ug/L24.2 0.160Chloroform
1.00 25.0 2040-12583 4ug/L20.7 0.250Chloromethane (Methyl Chloride)
1.00 25.0 2070-125103 2ug/L25.8 0.210cis-1,2-Dichloroethene
1.00 25.0 2070-130107 4ug/L26.9 0.100cis-1,3-Dichloropropene
1.00 25.0 2060-135118 4ug/L29.6 0.150Dibromochloromethane
1.00 25.0 2075-125102 4ug/L25.6 0.240Dibromomethane
1.00 25.0 2075-125111 5ug/L27.7 0.190Ethylbenzene
1.00 25.0 2065-13076 4ug/L18.9 0.310Iodomethane (Methyl Iodide)
2.00 50.0 2075-130112 5ug/L56.1 0.510m,p-Xylenes
1.00 25.0 2055-14091 1ug/L22.7 0.420Methylene Chloride
1.00 25.0 2080-120113 5ug/L28.3 0.200o-Xylene
1.00 25.0 2065-135118 4ug/L29.4 0.180Styrene
1.00 25.0 2045-150122 22ug/L30.6 X 0.160Tetrachloroethylene
1.00 25.0 2075-120110 5ug/L27.6 0.140Toluene
1.00 25.0 2060-140102 5ug/L25.5 0.210trans-1,2-Dichloroethene
1.00 25.0 2055-140121 7ug/L30.3 0.110trans-1,3-Dichloropropene
1.00 25.0 2065-135113 3ug/L28.1 0.190trans-1,4-Dichloro-2-butene
1.00 25.0 2070-125100 6ug/L25.0 0.190Trichloroethylene
1.00 25.0 2060-14590 10ug/L22.5 0.530Trichlorofluoromethane
1.00 25.0 2065-13593 6ug/L23.2 0.720Vinyl acetate
1.00 25.0 2050-14593 8ug/L23.2 0.190Vinyl chloride
25.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9423.4 ug/L
25.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)10225.5 ug/L
25.0 70-130Surrogate: Toluene-D8 (SUR)11027.6 ug/L
Page 24 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by Method 8260B (Continued)
MDL
Page 25 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by Method 8260B
MDL
Batch: B6E0097
Prepared: 4/14/2016 Analyzed: 4/15/2016Blank (B6E0097-BLK1)
5.00 ug/L0.236 U 0.236Tetrahydrofuran
Prepared & Analyzed: 4/14/2016LCS (B6E0097-BS1)
5.00 25.0 70-13099ug/L24.9 0.236Tetrahydrofuran
Prepared & Analyzed: 4/14/2016LCS Dup (B6E0097-BSD1)
5.00 25.0 2070-130100 0.5ug/L25.0 0.236Tetrahydrofuran
Page 26 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Total Metal Analysis by Method 6010C
MDL
Batch: B6D0364
Prepared & Analyzed: 4/19/2016Blank (B6D0364-BLK1)
0.0100 mg/L0.00400 U 0.00400Arsenic
0.0500 mg/L0.00200 U 0.00200Barium
0.00500 mg/L0.000300 U 0.000300Cadmium
0.0100 mg/L0.000300 U 0.000300Chromium
0.0100 mg/L0.00330 U 0.00330Lead
0.0500 mg/L0.0113 U 0.0113Selenium
0.0500 mg/L0.000600 U 0.000600Silver
Prepared & Analyzed: 4/19/2016LCS (B6D0364-BS1)
0.0100 1.00 80-120102mg/L1.02 0.00400Arsenic
0.0500 1.00 80-120101mg/L1.01 0.00200Barium
0.00500 1.00 80-120100mg/L0.996 0.000300Cadmium
0.0100 1.00 80-12099mg/L0.989 0.000300Chromium
0.0100 1.00 80-12099mg/L0.988 0.00330Lead
0.0500 1.00 80-120102mg/L1.02 0.0113Selenium
0.0500 1.00 80-12087mg/L0.872 0.000600Silver
Prepared & Analyzed: 4/19/2016LCS Dup (B6D0364-BSD1)
0.0100 1.00 2080-120105 3mg/L1.05 0.00400Arsenic
0.0500 1.00 2080-120105 4mg/L1.05 0.00200Barium
0.00500 1.00 2080-120103 4mg/L1.03 0.000300Cadmium
0.0100 1.00 2080-120103 4mg/L1.03 0.000300Chromium
0.0100 1.00 2080-120103 4mg/L1.03 0.00330Lead
0.0500 1.00 2080-120106 3mg/L1.06 0.0113Selenium
0.0500 1.00 2080-12090 3mg/L0.902 0.000600Silver
Prepared & Analyzed: 4/19/2016Source: L6D0148-01Duplicate (B6D0364-DUP1)
0.0100 0.00854 20mg/L0.00400 U 0.00400Arsenic
0.0500 0.291 200.8mg/L0.289 0.00200Barium
0.00500 0.00245 2059mg/L0.00134 XJ 0.000300Cadmium
0.0100 ND 20mg/L0.000300 U 0.000300Chromium
0.0100 0.0107 2014mg/L0.00923 J 0.00330Lead
0.0500 0.0139 20mg/L0.0113 U 0.0113Selenium
0.0500 ND 20mg/L0.000600 U 0.000600Silver
Page 27 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Total Metal Analysis by Method 6010C (Continued)
MDL
Batch: B6D0364 (Continued)
Prepared & Analyzed: 4/19/2016Source: L6D0148-01Matrix Spike (B6D0364-MS1)
0.0100 1.00 0.00854 80-120102mg/L1.03 0.00400Arsenic
0.0500 1.00 0.291 80-120100mg/L1.29 0.00200Barium
0.00500 1.00 0.00245 80-120100mg/L1.00 0.000300Cadmium
0.0100 1.00 ND 80-12099mg/L0.994 0.000300Chromium
0.0100 1.00 0.0107 80-12098mg/L0.994 0.00330Lead
0.0500 1.00 0.0139 80-120101mg/L1.03 0.0113Selenium
0.0500 1.00 ND 80-12087mg/L0.870 0.000600Silver
Prepared & Analyzed: 4/19/2016Source: L6D0148-01Matrix Spike Dup (B6D0364-MSD1)
0.0100 1.00 0.00854 2080-120105 2mg/L1.06 0.00400Arsenic
0.0500 1.00 0.291 2080-120102 2mg/L1.31 0.00200Barium
0.00500 1.00 0.00245 2080-120101 1mg/L1.01 0.000300Cadmium
0.0100 1.00 ND 2080-120101 1mg/L1.01 0.000300Chromium
0.0100 1.00 0.0107 2080-120100 1mg/L1.01 0.00330Lead
0.0500 1.00 0.0139 2080-120104 2mg/L1.05 0.0113Selenium
0.0500 1.00 ND 2080-12088 1mg/L0.880 0.000600Silver
Page 28 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Total Metal Analysis by Method 7470
MDL
Batch: B6D0373
Prepared: 4/19/2016 Analyzed: 4/20/2016Blank (B6D0373-BLK1)
0.000200 mg/L0.0000100 U 0.0000100Mercury
Prepared: 4/19/2016 Analyzed: 4/20/2016LCS (B6D0373-BS1)
0.000200 0.00300 85-11599mg/L0.00297 0.0000100Mercury
Prepared: 4/19/2016 Analyzed: 4/20/2016LCS Dup (B6D0373-BSD1)
0.000200 0.00300 2085-115102 3mg/L0.00306 0.0000100Mercury
Prepared: 4/19/2016 Analyzed: 4/20/2016Source: A6D0069-01Duplicate (B6D0373-DUP1)
0.000200 ND 20mg/L0.0000100 U 0.0000100Mercury
Prepared: 4/19/2016 Analyzed: 4/20/2016Source: A6D0069-01Matrix Spike (B6D0373-MS1)
0.000200 0.00300 ND 85-115100mg/L0.00300 0.0000100Mercury
Prepared: 4/19/2016 Analyzed: 4/20/2016Source: A6D0069-01Matrix Spike Dup (B6D0373-MSD1)
0.000200 0.00300 ND 2085-115100 0.07mg/L0.00300 0.0000100Mercury
Page 29 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 5/5/16 13:48
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
List of Certifications for FTS Analytical Services - Atlanta
CodeDescriptionNumber ExpiresFacility
LANELAC04176LA CERTICATE 06/30/2016FTSA
ANC483NC CERTIFICATE 12/31/2016FTSA
KENTUKY85KENTUKY CERTICATE FTSA
ASC98015SC CERTIFICATE 06/30/2016FTSA
LFLNELACE84098FL NELAC CERTIFICATE 06/30/2016FTSL
AFLNELACE87429FL NELAC CERTIFICATE 06/30/2016FTSA
DODLI0-135 DoD CERTIFICATE 06/30/2016FTSA
USDAP330-07-00105 USDA CERTIFICATE FTSA
Notes and Definitions
Item Definition
Dry Sample results reported on a dry weight basis.
U Analyte NOT DETECTED at or above the reporting limit.
A Suspected adol-condensation product
B Analyte detected in the method blank
C Confirmed by GC/MS analysis
E Concentration exceeds calibration range
K Hold Time exceeded
N Tentatively Identified Compound
P >25% difference between primary and secondary columns
S Quantitation based on single-point calibration
X General QC Failure see Case Narrative
RPD Relative Percent Difference
%REC Percent Recovery
Source Sample that was matrix spiked or duplicated.
Page 30 of 31
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.