4502_HendersonKimberlyClark_GWMR_DIN27875_20160304

#=CL#
May 17, 2016
LIMS USE: FR - MICHAEL BALDWIN
LIMS OBJECT ID: 92288936
92288936
Project:
Pace Project No.:
RE:
Mr. Michael Baldwin
Kimberly Clark
32 Smyth Avenue
Hendersonville, NC 28793
South LF MW 3/4
Dear Mr. Baldwin:
Enclosed are the analytical results for sample(s) received by the laboratory on March 04, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Revised Report: Report revised to correct flag settings
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc:Tana Black, Kimberly Clark
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92288936
South LF MW 3/4
Lab ID Sample ID Matrix Date Collected Date Received
92288936001 MW-1S Water 03/04/16 14:15 03/04/16 16:45
92288936002 MW-2S Water 03/03/16 12:55 03/04/16 16:45
92288936003 MW-3S Water 03/03/16 13:05 03/04/16 16:45
92288936004 MW-4S Water 03/04/16 15:15 03/04/16 16:45
92288936005 MW-5S Water 03/04/16 15:30 03/04/16 16:45
92288936006 MW-6S Water 03/04/16 15:00 03/04/16 16:45
92288936007 MW-7S Water 03/04/16 14:45 03/04/16 16:45
92288936008 TVL BLK Water 03/04/16 10:30 03/04/16 16:45
92288936009 EQUIP BLK Water 03/04/16 14:00 03/04/16 16:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92288936
South LF MW 3/4
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92288936001 MW-1S EPA 8260 63 PASI-CNB
92288936004 MW-4S EPA 8260 63 PASI-CNB
92288936005 MW-5S EPA 8260 63 PASI-CNB
92288936006 MW-6S EPA 8260 63 PASI-CNB
92288936007 MW-7S EPA 8260 63 PASI-CNB
92288936008 TVL BLK EPA 8260 63 PASI-CNB
92288936009 EQUIP BLK EPA 8260 63 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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2225 Riverside Dr.
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[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-1S Lab ID:92288936001 Collected:03/04/16 14:15 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:341
Collected Date 3/4/16 03/07/16 17:341
Collected Time 14:15 03/07/16 17:341
Field pH 6.4 Std. Units 03/07/16 17:340.10 0.10 1
Field Temperature 12.7 deg C 03/07/16 17:340.50 0.50 1
Static Water Level 10.79 feet 03/07/16 17:341
Field Specific Conductance 133 umhos/cm 03/07/16 17:341.0 1.0 1
Turbidity 5.66 NTU 03/07/16 17:341.0 1.0 1
Odor No Odor 03/07/16 17:341
Appearance Clear 03/07/16 17:341
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 19:02 67-64-125.0 10.0 1
Benzene ND ug/L 03/06/16 19:02 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 19:02 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 19:02 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 19:02 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 19:02 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 19:02 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 19:02 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 19:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 19:02 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/06/16 19:02 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 19:02 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 19:02 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 19:02 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 19:02 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 19:02 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 19:02 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 19:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 19:02 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 19:02 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 19:02 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 19:02 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 19:02 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/06/16 19:02 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 19:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 19:02 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 19:02 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 19:02 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 19:02 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 19:02 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 19:02 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 19:02 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/06/16 19:02 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-1S Lab ID:92288936001 Collected:03/04/16 14:15 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 03/06/16 19:02 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 19:02 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 19:02 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 19:02 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 19:02 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 19:02 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 19:02 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 19:02 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 19:02 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 19:02 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 19:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 19:02 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 19:02 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/06/16 19:02 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 19:02 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 19:02 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 19:02 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 19:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 19:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 19:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 19:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 19:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 19:02 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 19:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 19:02 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 19:02 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 19:02 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)93 %03/06/16 19:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %03/06/16 19:02 17060-07-070-130 1
Toluene-d8 (S)99 %03/06/16 19:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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2225 Riverside Dr.
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Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-2S Lab ID:92288936002 Collected:03/03/16 12:55 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:351
Collected Date 3/4/16 03/07/16 17:351
Collected Time 12:55 03/07/16 17:351
Field pH 6.8 Std. Units 03/07/16 17:350.10 0.10 1
Field Temperature 9.9 deg C 03/07/16 17:350.50 0.50 1
Static Water Level 2.57 feet 03/07/16 17:351
Field Specific Conductance 76 umhos/cm 03/07/16 17:351.0 1.0 1
Turbidity 33.12 NTU 03/07/16 17:351.0 1.0 1
Odor No Odor 03/07/16 17:351
Appearance Clear 03/07/16 17:351
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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2225 Riverside Dr.
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[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-3S Lab ID:92288936003 Collected:03/03/16 13:05 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:361
Collected Date 3/4/16 03/07/16 17:361
Collected Time 13:05 03/07/16 17:361
Field pH 6.4 Std. Units 03/07/16 17:360.10 0.10 1
Field Temperature 10.5 deg C 03/07/16 17:360.50 0.50 1
Static Water Level 5.15 feet 03/07/16 17:361
Field Specific Conductance 119 umhos/cm 03/07/16 17:361.0 1.0 1
Turbidity 27.68 NTU 03/07/16 17:361.0 1.0 1
Odor No Odor 03/07/16 17:361
Appearance Clear 03/07/16 17:361
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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2225 Riverside Dr.
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Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-4S Lab ID:92288936004 Collected:03/04/16 15:15 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:371
Collected Date 3/4/16 03/07/16 17:371
Collected Time 15:15 03/07/16 17:371
Field pH 6.1 Std. Units 03/07/16 17:370.10 0.10 1
Field Temperature 9.8 deg C 03/07/16 17:370.50 0.50 1
Static Water Level 3.92 feet 03/07/16 17:371
Field Specific Conductance 550 umhos/cm 03/07/16 17:371.0 1.0 1
Turbidity 5.12 NTU 03/07/16 17:371.0 1.0 1
Odor Organic
Odor 03/07/16 17:371
Appearance Clear 03/07/16 17:371
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 19:35 67-64-125.0 10.0 1
Benzene 0.57J ug/L 03/06/16 19:35 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 19:35 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 19:35 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 19:35 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 19:35 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 19:35 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 19:35 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 19:35 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 19:35 108-90-71.0 0.23 1
Chloroethane 1.9 ug/L 03/06/16 19:35 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 19:35 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 19:35 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 19:35 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 19:35 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 19:35 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 19:35 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 19:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 19:35 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 19:35 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 19:35 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 19:35 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 19:35 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/06/16 19:35 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 19:35 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 19:35 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 19:35 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 19:35 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 19:35 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 19:35 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 19:35 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 19:35 563-58-61.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-4S Lab ID:92288936004 Collected:03/04/16 15:15 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
cis-1,3-Dichloropropene ND ug/L 03/06/16 19:35 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/06/16 19:35 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 19:35 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 19:35 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 19:35 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 19:35 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 19:35 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 19:35 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 19:35 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 19:35 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 19:35 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 19:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 19:35 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 19:35 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/06/16 19:35 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 19:35 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 19:35 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 19:35 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 19:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 19:35 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 19:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 19:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 19:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 19:35 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 19:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 19:35 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 19:35 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 19:35 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %03/06/16 19:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %03/06/16 19:35 17060-07-070-130 1
Toluene-d8 (S)99 %03/06/16 19:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-5S Lab ID:92288936005 Collected:03/04/16 15:30 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:381
Collected Date 3/4/16 03/07/16 17:381
Collected Time 15:30 03/07/16 17:381
Field pH 6.2 Std. Units 03/07/16 17:380.10 0.10 1
Field Temperature 9.2 deg C 03/07/16 17:380.50 0.50 1
Static Water Level 3.85 feet 03/07/16 17:381
Field Specific Conductance 127 umhos/cm 03/07/16 17:381.0 1.0 1
Turbidity 9.66 NTU 03/07/16 17:381.0 1.0 1
Odor Organic
Odor 03/07/16 17:381
Appearance Clear 03/07/16 17:381
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 19:52 67-64-125.0 10.0 1
Benzene ND ug/L 03/06/16 19:52 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 19:52 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 19:52 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 19:52 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 19:52 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 19:52 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 19:52 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 19:52 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 19:52 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/06/16 19:52 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 19:52 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 19:52 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 19:52 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 19:52 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 19:52 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 19:52 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 19:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 19:52 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 19:52 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 19:52 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 19:52 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 19:52 75-71-81.0 0.21 1
1,1-Dichloroethane 0.53J ug/L 03/06/16 19:52 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 19:52 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 19:52 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 19:52 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 19:52 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 19:52 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 19:52 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 19:52 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 19:52 563-58-61.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-5S Lab ID:92288936005 Collected:03/04/16 15:30 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
cis-1,3-Dichloropropene ND ug/L 03/06/16 19:52 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/06/16 19:52 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 19:52 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 19:52 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 19:52 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 19:52 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 19:52 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 19:52 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 19:52 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 19:52 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 19:52 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 19:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 19:52 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 19:52 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/06/16 19:52 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 19:52 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 19:52 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 19:52 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 19:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 19:52 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 19:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 19:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 19:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 19:52 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 19:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 19:52 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 19:52 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 19:52 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)94 %03/06/16 19:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %03/06/16 19:52 17060-07-070-130 1
Toluene-d8 (S)99 %03/06/16 19:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-6S Lab ID:92288936006 Collected:03/04/16 15:00 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:391
Collected Date 3/4/16 03/07/16 17:391
Collected Time 15:00 03/07/16 17:391
Field pH 6.9 Std. Units 03/07/16 17:390.10 0.10 1
Field Temperature 9.7 deg C 03/07/16 17:390.50 0.50 1
Static Water Level 7.45 feet 03/07/16 17:391
Field Specific Conductance 77 umhos/cm 03/07/16 17:391.0 1.0 1
Turbidity 9.50 NTU 03/07/16 17:391.0 1.0 1
Odor No Odor 03/07/16 17:391
Appearance Clear 03/07/16 17:391
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 20:08 67-64-125.0 10.0 1
Benzene ND ug/L 03/06/16 20:08 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 20:08 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 20:08 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 20:08 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 20:08 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 20:08 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 20:08 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 20:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 20:08 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/06/16 20:08 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 20:08 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 20:08 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 20:08 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 20:08 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 20:08 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 20:08 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 20:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 20:08 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 20:08 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 20:08 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 20:08 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 20:08 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/06/16 20:08 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 20:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 20:08 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 20:08 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 20:08 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 20:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 20:08 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 20:08 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 20:08 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/06/16 20:08 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-6S Lab ID:92288936006 Collected:03/04/16 15:00 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 03/06/16 20:08 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 20:08 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 20:08 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 20:08 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 20:08 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 20:08 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 20:08 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 20:08 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 20:08 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 20:08 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 20:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 20:08 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 20:08 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/06/16 20:08 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 20:08 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 20:08 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 20:08 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 20:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 20:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 20:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 20:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 20:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 20:08 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 20:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 20:08 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 20:08 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 20:08 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)95 %03/06/16 20:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %03/06/16 20:08 17060-07-070-130 1
Toluene-d8 (S)100 %03/06/16 20:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-7S Lab ID:92288936007 Collected:03/04/16 14:45 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/07/16 17:411
Collected Date 3/4/16 03/07/16 17:411
Collected Time 14:45 03/07/16 17:411
Field pH 6.5 Std. Units 03/07/16 17:410.10 0.10 1
Field Temperature 9.6 deg C 03/07/16 17:410.50 0.50 1
Static Water Level 4.60 feet 03/07/16 17:411
Field Specific Conductance 118 umhos/cm 03/07/16 17:411.0 1.0 1
Turbidity 12.89 NTU 03/07/16 17:411.0 1.0 1
Odor No Odor 03/07/16 17:411
Appearance Clear 03/07/16 17:411
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 20:25 67-64-125.0 10.0 1
Benzene ND ug/L 03/06/16 20:25 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 20:25 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 20:25 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 20:25 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 20:25 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 20:25 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 20:25 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 20:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 20:25 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/06/16 20:25 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 20:25 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 20:25 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 20:25 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 20:25 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 20:25 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 20:25 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 20:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 20:25 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 20:25 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 20:25 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 20:25 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 20:25 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/06/16 20:25 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 20:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 20:25 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 20:25 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 20:25 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 20:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 20:25 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 20:25 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 20:25 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/06/16 20:25 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:MW-7S Lab ID:92288936007 Collected:03/04/16 14:45 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 03/06/16 20:25 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 20:25 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 20:25 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 20:25 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 20:25 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 20:25 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 20:25 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 20:25 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 20:25 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 20:25 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 20:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 20:25 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 20:25 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/06/16 20:25 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 20:25 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 20:25 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 20:25 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 20:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 20:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 20:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 20:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 20:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 20:25 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 20:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 20:25 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 20:25 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 20:25 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)95 %03/06/16 20:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %03/06/16 20:25 17060-07-070-130 1
Toluene-d8 (S)100 %03/06/16 20:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:TVL BLK Lab ID:92288936008 Collected:03/04/16 10:30 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 18:12 67-64-125.0 10.0 1
Benzene ND ug/L 03/06/16 18:12 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 18:12 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 18:12 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 18:12 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 18:12 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 18:12 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 18:12 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 18:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 18:12 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/06/16 18:12 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 18:12 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 18:12 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 18:12 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 18:12 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 18:12 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 18:12 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 18:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 18:12 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 18:12 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 18:12 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 18:12 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 18:12 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/06/16 18:12 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 18:12 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 18:12 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 18:12 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 18:12 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 18:12 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 18:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 18:12 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 18:12 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/06/16 18:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/06/16 18:12 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 18:12 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 18:12 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 18:12 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 18:12 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 18:12 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 18:12 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 18:12 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 18:12 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 18:12 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 18:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 18:12 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 18:12 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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Page 17 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:TVL BLK Lab ID:92288936008 Collected:03/04/16 10:30 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 03/06/16 18:12 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 18:12 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 18:12 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 18:12 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 18:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 18:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 18:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 18:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 18:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 18:12 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 18:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 18:12 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 18:12 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 18:12 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)95 %03/06/16 18:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %03/06/16 18:12 17060-07-070-130 1
Toluene-d8 (S)98 %03/06/16 18:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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Page 18 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:EQUIP BLK Lab ID:92288936009 Collected:03/04/16 14:00 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/06/16 18:29 67-64-125.0 10.0 1
Benzene ND ug/L 03/06/16 18:29 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/06/16 18:29 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/06/16 18:29 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/06/16 18:29 75-27-41.0 0.18 1
Bromoform ND ug/L 03/06/16 18:29 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/06/16 18:29 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/06/16 18:29 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/06/16 18:29 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/06/16 18:29 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/06/16 18:29 75-00-31.0 0.54 1
Chloroform ND ug/L 03/06/16 18:29 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/06/16 18:29 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/06/16 18:29 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/06/16 18:29 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/06/16 18:29 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/06/16 18:29 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/06/16 18:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/06/16 18:29 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/06/16 18:29 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/06/16 18:29 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/06/16 18:29 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/06/16 18:29 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/06/16 18:29 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/06/16 18:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/06/16 18:29 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/06/16 18:29 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/06/16 18:29 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/06/16 18:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/06/16 18:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/06/16 18:29 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/06/16 18:29 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/06/16 18:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/06/16 18:29 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/06/16 18:29 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/06/16 18:29 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/06/16 18:29 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/06/16 18:29 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/06/16 18:29 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/06/16 18:29 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/06/16 18:29 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/06/16 18:29 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/06/16 18:29 91-20-31.0 0.24 1
Styrene ND ug/L 03/06/16 18:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/06/16 18:29 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/06/16 18:29 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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Page 19 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92288936
South LF MW 3/4
Sample:EQUIP BLK Lab ID:92288936009 Collected:03/04/16 14:00 Received:03/04/16 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 03/06/16 18:29 127-18-41.0 0.46 1
Toluene ND ug/L 03/06/16 18:29 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/06/16 18:29 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/06/16 18:29 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/06/16 18:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/06/16 18:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/06/16 18:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/06/16 18:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/06/16 18:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/06/16 18:29 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/06/16 18:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/06/16 18:29 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/06/16 18:29 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/06/16 18:29 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)96 %03/06/16 18:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/06/16 18:29 17060-07-070-130 1
Toluene-d8 (S)99 %03/06/16 18:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
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[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92288936
South LF MW 3/4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35846
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92288936001, 92288936004, 92288936005, 92288936006, 92288936007, 92288936008, 92288936009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1679922
Associated Lab Samples:92288936001, 92288936004, 92288936005, 92288936006, 92288936007, 92288936008, 92288936009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/06/16 15:430.33
1,1,1-Trichloroethane ug/L ND 1.0 03/06/16 15:430.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/06/16 15:430.40
1,1,2-Trichloroethane ug/L ND 1.0 03/06/16 15:430.29
1,1-Dichloroethane ug/L ND 1.0 03/06/16 15:430.32
1,1-Dichloroethene ug/L ND 1.0 03/06/16 15:430.56
1,1-Dichloropropene ug/L ND 1.0 03/06/16 15:430.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/06/16 15:430.33
1,2,3-Trichloropropane ug/L ND 1.0 03/06/16 15:430.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/06/16 15:430.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/06/16 15:432.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/06/16 15:430.27
1,2-Dichlorobenzene ug/L ND 1.0 03/06/16 15:430.30
1,2-Dichloroethane ug/L ND 1.0 03/06/16 15:430.24
1,2-Dichloropropane ug/L ND 1.0 03/06/16 15:430.27
1,3-Dichlorobenzene ug/L ND 1.0 03/06/16 15:430.24
1,3-Dichloropropane ug/L ND 1.0 03/06/16 15:430.28
1,4-Dichlorobenzene ug/L ND 1.0 03/06/16 15:430.33
2,2-Dichloropropane ug/L ND 1.0 03/06/16 15:430.13
2-Butanone (MEK)ug/L ND 5.0 03/06/16 15:430.96
2-Chlorotoluene ug/L ND 1.0 03/06/16 15:430.35
2-Hexanone ug/L ND 5.0 03/06/16 15:430.46
4-Chlorotoluene ug/L ND 1.0 03/06/16 15:430.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/06/16 15:430.33
Acetone ug/L ND 25.0 03/06/16 15:4310.0
Benzene ug/L ND 1.0 03/06/16 15:430.25
Bromobenzene ug/L ND 1.0 03/06/16 15:430.30
Bromochloromethane ug/L ND 1.0 03/06/16 15:430.17
Bromodichloromethane ug/L ND 1.0 03/06/16 15:430.18
Bromoform ug/L ND 1.0 03/06/16 15:430.26
Bromomethane ug/L ND 2.0 03/06/16 15:430.29
Carbon tetrachloride ug/L ND 1.0 03/06/16 15:430.25
Chlorobenzene ug/L ND 1.0 03/06/16 15:430.23
Chloroethane ug/L ND 1.0 03/06/16 15:430.54
Chloroform ug/L ND 1.0 03/06/16 15:430.14
Chloromethane ug/L ND 1.0 03/06/16 15:430.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/06/16 15:430.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/06/16 15:430.13
Dibromochloromethane ug/L ND 1.0 03/06/16 15:430.21
Dibromomethane ug/L ND 1.0 03/06/16 15:430.21
Dichlorodifluoromethane ug/L ND 1.0 03/06/16 15:430.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92288936
South LF MW 3/4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1679922
Associated Lab Samples:92288936001, 92288936004, 92288936005, 92288936006, 92288936007, 92288936008, 92288936009
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/06/16 15:430.12
Ethylbenzene ug/L ND 1.0 03/06/16 15:430.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/06/16 15:430.71
m&p-Xylene ug/L ND 2.0 03/06/16 15:430.66
Methyl-tert-butyl ether ug/L ND 1.0 03/06/16 15:430.21
Methylene Chloride ug/L ND 2.0 03/06/16 15:430.97
Naphthalene ug/L ND 1.0 03/06/16 15:430.24
o-Xylene ug/L ND 1.0 03/06/16 15:430.23
p-Isopropyltoluene ug/L ND 1.0 03/06/16 15:430.31
Styrene ug/L ND 1.0 03/06/16 15:430.26
Tetrachloroethene ug/L ND 1.0 03/06/16 15:430.46
Toluene ug/L ND 1.0 03/06/16 15:430.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/06/16 15:430.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/06/16 15:430.26
Trichloroethene ug/L ND 1.0 03/06/16 15:430.47
Trichlorofluoromethane ug/L ND 1.0 03/06/16 15:430.20
Vinyl acetate ug/L ND 2.0 03/06/16 15:430.35
Vinyl chloride ug/L ND 1.0 03/06/16 15:430.62
Xylene (Total)ug/L ND 2.0 03/06/16 15:430.66
1,2-Dichloroethane-d4 (S)%99 70-130 03/06/16 15:43
4-Bromofluorobenzene (S)%94 70-130 03/06/16 15:43
Toluene-d8 (S)%98 70-130 03/06/16 15:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1679923LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.450 99 70-130
1,1,1-Trichloroethane ug/L 50.050 100 70-130
1,1,2,2-Tetrachloroethane ug/L 46.350 93 70-130
1,1,2-Trichloroethane ug/L 48.650 97 70-130
1,1-Dichloroethane ug/L 49.150 98 70-130
1,1-Dichloroethene ug/L 52.850 106 70-132
1,1-Dichloropropene ug/L 52.150 104 70-130
1,2,3-Trichlorobenzene ug/L 41.250 82 70-135
1,2,3-Trichloropropane ug/L 51.450 103 70-130
1,2,4-Trichlorobenzene ug/L 43.750 87 70-134
1,2-Dibromo-3-chloropropane ug/L 48.250 96 70-130
1,2-Dibromoethane (EDB)ug/L 51.050 102 70-130
1,2-Dichlorobenzene ug/L 48.250 96 70-130
1,2-Dichloroethane ug/L 47.650 95 70-130
1,2-Dichloropropane ug/L 48.850 98 70-130
1,3-Dichlorobenzene ug/L 50.350 101 70-130
1,3-Dichloropropane ug/L 50.150 100 70-130
1,4-Dichlorobenzene ug/L 51.150 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92288936
South LF MW 3/4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1679923LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 50.350 101 58-145
2-Butanone (MEK)ug/L 90.4100 90 70-145
2-Chlorotoluene ug/L 48.150 96 70-130
2-Hexanone ug/L 90.5100 91 70-144
4-Chlorotoluene ug/L 47.750 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-140
Acetone ug/L 84.3100 84 50-175
Benzene ug/L 50.150 100 70-130
Bromobenzene ug/L 49.850 100 70-130
Bromochloromethane ug/L 51.850 104 70-130
Bromodichloromethane ug/L 50.050 100 70-130
Bromoform ug/L 46.050 92 70-130
Bromomethane ug/L 42.050 84 54-130
Carbon tetrachloride ug/L 49.050 98 70-132
Chlorobenzene ug/L 49.850 100 70-130
Chloroethane ug/L 49.450 99 64-134
Chloroform ug/L 48.450 97 70-130
Chloromethane ug/L 37.250 74 64-130
cis-1,2-Dichloroethene ug/L 50.150 100 70-131
cis-1,3-Dichloropropene ug/L 49.050 98 70-130
Dibromochloromethane ug/L 49.050 98 70-130
Dibromomethane ug/L 50.950 102 70-131
Dichlorodifluoromethane ug/L 43.350 87 56-130
Diisopropyl ether ug/L 50.850 102 70-130
Ethylbenzene ug/L 49.550 99 70-130
Hexachloro-1,3-butadiene ug/L 38.550 77 70-130
m&p-Xylene ug/L 95.5100 96 70-130
Methyl-tert-butyl ether ug/L 51.050 102 70-130
Methylene Chloride ug/L 46.650 93 63-130
Naphthalene ug/L 43.150 86 70-138
o-Xylene ug/L 46.850 94 70-130
p-Isopropyltoluene ug/L 45.850 92 70-130
Styrene ug/L 49.450 99 70-130
Tetrachloroethene ug/L 50.350 101 70-130
Toluene ug/L 48.950 98 70-130
trans-1,2-Dichloroethene ug/L 50.050 100 70-130
trans-1,3-Dichloropropene ug/L 48.650 97 70-132
Trichloroethene ug/L 49.550 99 70-130
Trichlorofluoromethane ug/L 50.850 102 62-133
Vinyl acetate ug/L 95.0100 95 66-157
Vinyl chloride ug/L 50.050 100 50-150
Xylene (Total)ug/L 142150 95 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92288936
South LF MW 3/4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1679924MATRIX SPIKE SAMPLE:
MSSpike
Result
92288825001
1,1,1,2-Tetrachloroethane ug/L 20.620 103 70-130ND
1,1,1-Trichloroethane ug/L 21.420 107 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 20.520 103 70-130ND
1,1-Dichloroethane ug/L 21.320 106 70-130ND
1,1-Dichloroethene ug/L 23.220 116 70-166ND
1,1-Dichloropropene ug/L 22.720 114 70-130ND
1,2,3-Trichlorobenzene ug/L 16.320 81 70-130ND
1,2,3-Trichloropropane ug/L 20.520 102 70-130ND
1,2,4-Trichlorobenzene ug/L 16.220 81 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.320 107 70-130ND
1,2-Dichlorobenzene ug/L 19.620 98 70-130ND
1,2-Dichloroethane ug/L 19.620 98 70-130ND
1,2-Dichloropropane ug/L 21.320 106 70-130ND
1,3-Dichlorobenzene ug/L 21.720 108 70-130ND
1,3-Dichloropropane ug/L 20.620 103 70-130ND
1,4-Dichlorobenzene ug/L 21.320 106 70-130ND
2,2-Dichloropropane ug/L 20.620 103 70-130ND
2-Butanone (MEK)ug/L 37.340 93 70-130ND
2-Chlorotoluene ug/L 20.520 102 70-130ND
2-Hexanone ug/L 37.140 93 70-130ND
4-Chlorotoluene ug/L 20.320 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.140 108 70-130ND
Acetone ug/L 39.040 97 70-130ND
Benzene ug/L 22.120 108 70-148ND
Bromobenzene ug/L 21.020 105 70-130ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 21.120 106 70-130ND
Bromoform ug/L 18.020 90 70-130ND
Bromomethane ug/L 14.220 71 70-130ND
Carbon tetrachloride ug/L 21.720 108 70-130ND
Chlorobenzene ug/L 21.020 105 70-146ND
Chloroethane ug/L 23.120 115 70-130ND
Chloroform ug/L 20.920 104 70-130ND
Chloromethane ug/L 15.820 79 70-130ND
cis-1,2-Dichloroethene ug/L 22.020 110 70-130ND
cis-1,3-Dichloropropene ug/L 20.520 103 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Dichlorodifluoromethane ug/L 18.820 94 70-130ND
Diisopropyl ether ug/L 21.020 105 70-130ND
Ethylbenzene ug/L 20.820 104 70-130ND
Hexachloro-1,3-butadiene ug/L 14.820 74 70-130ND
m&p-Xylene ug/L 40.340 100 70-130ND
Methyl-tert-butyl ether ug/L 21.120 105 70-130ND
Methylene Chloride ug/L 20.020 100 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92288936
South LF MW 3/4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1679924MATRIX SPIKE SAMPLE:
MSSpike
Result
92288825001
Naphthalene ug/L 18.020 90 70-130ND
o-Xylene ug/L 19.620 98 70-130ND
p-Isopropyltoluene ug/L 19.020 95 70-130ND
Styrene ug/L 18.620 93 70-130ND
Tetrachloroethene ug/L 21.820 108 70-130ND
Toluene ug/L 21.320 106 70-155ND
trans-1,2-Dichloroethene ug/L 22.220 111 70-130ND
trans-1,3-Dichloropropene ug/L 19.520 97 70-130ND
Trichloroethene ug/L 21.920 110 69-151ND
Trichlorofluoromethane ug/L 22.520 113 70-130ND
Vinyl acetate ug/L 33.340 83 70-130ND
Vinyl chloride ug/L 22.520 113 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92288936001
1679925SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92288936
South LF MW 3/4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92288936001
1679925SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%97 3100
4-Bromofluorobenzene (S)%95 393
Toluene-d8 (S)%99 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92288936
South LF MW 3/4
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92288936
South LF MW 3/4
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92288936001 FLD/MW-1S
92288936002 FLD/MW-2S
92288936003 FLD/MW-3S
92288936004 FLD/MW-4S
92288936005 FLD/MW-5S
92288936006 FLD/MW-6S
92288936007 FLD/MW-7S
92288936001 MSV/35846MW-1S EPA 8260
92288936004 MSV/35846MW-4S EPA 8260
92288936005 MSV/35846MW-5S EPA 8260
92288936006 MSV/35846MW-6S EPA 8260
92288936007 MSV/35846MW-7S EPA 8260
92288936008 MSV/35846TVL BLK EPA 8260
92288936009 MSV/35846EQUIP BLK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/17/2016 12:33 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 31
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