Cenco_Central Transport April 98 GW Mon Rpt-OCR

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Report of April 1998 Semi-Annual Groundwater Monitoring
Honbarrier, Inc. Facility
Charlotte, North Carolina
4.0 ANALYTICAL METHODS AND RESULTS
4.1 Methods
---·-···-··~
June 24, 1998
Page 3
Sample TB-1 was analyzed for volatile organics (SW-846 Method 8260) only.
Samples collected from monitoring wells were analyzed for volatiles (SW-846 Method
8260), semi-volatiles (SW-846 Method 8270), cyanide (SW-846 Method 9010). and
Target Analytical List (TAL) metals (EPA 200 series Methods).
4.2 Results
Laboratory data sheets are presented in Appendix B. A summary of selected
contaminants is provided in Table 4.1. Historical groundwater analytical data is
provided in Table 4.2. A groundwater contaminant plume map, showing total
detectable volatile organic compounds, is provided as Drawing 4.1 .
The laboratory reported the following Quality Assurance\Quality Control (QA/QC)
procedures were out of compliance during analysis of samples:
• Recovery of surrogate toluene exceeded quality control limits during analysis
of the MW-10 sample. Toluene was reported at Below Detection Limit (BOU
for this sample.
• Residual chlorine was reported in the sample from MW-1 3 submitted for
cyanide analysis .
• The volatile analysis for the MW-13 sample was reported as "out of tune time."
It appears the time between laboratory standards analyses and MW-13 analysis
was outside the time window allowed under SW-846 Method 8260 protocol.
When this was discovered, a second analysis performed on the sample from
this well. However, this analysis was performed outside of hold time.
Analytical results from the out of tune run and the out of hold time run were
comparable. Analytical results for this event are similar to analytical results
from previous sampling events at MW-13.
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DRAWINGS
-----.. -iiilil UT -_ 1W oARG = ' 'I ,~a F-I ,~,--'"'Rlf '""" "'":I' '?B
CHAllLOITE, fllORT H CAl!Oll 'IA
Page _L__ of ~ FIELD DATA INFOllMATjON SHEET FOR GROUND-WATER SAM PUNG
--
O ate lyr/m o/day} 4 -:<.8 -'l 8 Casin.g Diameter ..:2. fnche-s
Fi-e-td Perso.n.n el Keu.:i_&Aer J ,S.,/ewa rZ-Top of Ca:;ing Elovation 1/100 +
Facil~y Name Cen/ra C. :J t:. rAnS ;00,-i" Surtace Elavatian 11100 ft ,
.;;? S'-$S EPA 10 II Scteened lnterVaf 11100 ft
Well 10# jrJW-~ Ground water ElevatO,n v 1(100 ft
Weather Co-n di tio n:s Svn,..v, coo/• c.a • ---LoclOng Cap YES NO
Total Woll Depth (TWOJ -.3 $". s:-11100 it Wo~ kttegrity Satisfactory YES i.L:: NO
Depth to Grnund water (OGW J -9. ~I 1£100tt We.U Yield LOW MODERATE v HIGH
length ol Water Column ILWCl = nvo -OGW = ,;2.S • 8 9 Woter Elevation Equipment
1 Casing Volume (OCVJ = LWC x __!/_. / 4 -gal Well Depth Equ ipmeo <
J CasinQ Volumes =-£_..;} • (i_.3 gal = Standard ~ecu•tion Volume Field Measurement Equi pmeiit
Method of We!f Evacuatjon ,;) " a t"-d -1().s_ ~1..1m-n Methcd of Sample Colle-ction &:vft:Y r , /,;/, s-o To taJ Volume of Waler Removed gal
V'cl c/) l/o I (;;i) l/o/{3) 5,.,~r ... . I
Present ative
Bottle
Sampled For .j.--4-,.29-98
Time (mili •ary t J(): JS"°
pH IS.U.) ~-{,,, Z--5"!f'1 :;;-: ~'f -.-t. s .z
Sp. Con d. (µmhos/c mJ 5:;;.o. 0 lf38 0 i/-5'8 0 J./ I CJ
Wal er Temp l'CJ ~ --£,! ~.-b" -~-· I~. 'f
TURBIDITY lsubiectivel • .,..._ 3 -_ ~-~
• 11) Clear (2) Slight !3) Moderate 14) High
COMMENTS/OBSERVAT!ONS:
Revision l August 15, 19 97
~c73 c~c' '-V'• ~75 --"'~. "'1'P '"ft "''7 ~.inti~ ~JErn DA G
>·c;r ,., .• ,,,,, "''illf ,.,.
CHARLOTTE, NORTH CAllOllNA
Page ,;I. of 7 ---
FIELD CATA !NFOAMATjON SHEET FOR GAOllNO-WATER SAMPLING
Date {yr/mo/day) ~ -.;( fh '"' 9g Casing Di am st er
Field Personnel Re u...Sc/ier I Slewt:i re Top of Casing Elevatio.n
Facility N•me C.er1--fraL /ro,,.s &J.Od Surf a ca Efeva tion I .;<9-3'7 EPA ID# Screened lAtarval
Well ID# mw-7 -Groundwater Elevation
Weather Condl rion s • r·-·-Locking Cap YES v NO
Total Well Oep th {TWO I = :39 1/100 It Wd ln!egrily Satisfactory YES v NO
Depth to Groundwater [DG W J = ,, s:. 0 ;l 1 (100 ft Well Yield LOW MODERATE \/
length ol Water Column (LWCI = TVVD • DGW = .:l 3_. 'i. 8 Wat er Elevation Equip m on I
I Cosing Volume IOCV) = LWC x __ 3, IJ4 gal Well Depth Equipment
3 Cci sing Vorumes =-LL. SL gal = Sta11da-rd Evs9.1atioo Vofume Field Measurem.en I Eq:u i p men t
Method of Well Evacuation ,;J " H-a:i .a Method of Sample C-Ollectlon 8&1../ler
I
Total Volume of Wacer Removed
t/> (.;) {s) (4) 5o.1nJJle.. -
Preservative
Bottle
.. 1-;l't-98 Sampled For ·L•'
Time {mili?ary) /t.I: S-j 14: S-? ;if: S-8 ;G :oo 10: I.II:'
pH IS.U.) 5"." 7 s-. "· s-s,/p~ $"".. " s-(R,7'/
Sp. Cond. (µmhos/c mJ :< 31d r,8/S-/, 6 7.2 ·;, 5"70 ;,aeo .
Wai"'" Temp ('CJ --.....-·-... . 17' 0 -
TUR BIOJTY I• ubie<:tive) ' 3 ~ c}, I I
• (1) Clear (2! Slight (3) Moder ace C4J Hjgh
COMMENTS/OBSERVATIONS: Q,./,,y ,,,..h.,,/~,J,.,.. -/,Jw . at: e _./,,,_ k -/,·b-. Sr><!. ~, · 4! rl f'l/ea reeU.
=··--
.2
HIGH
/{;,. t;"
Rav~sion l Augvs! 15, 1997
:c~,. ,,,,,
Inches
11100'
111 00 ..
11100 It
1/1001t
gal
''if'
----------
----a '"'-'5' ,,__, ""'' --<'-,., '"'"'@ ,_,_,,, · :;vff!oATZf?.a -p ____ /-3l1ii1
-.... ~_;.-7_~-~ --'-')' -iliiiiili
CJiA RlO ITE, NORT Ji CAROl!NA
Pago 3 of 7 FIELD DATA lNFOJlMATION SHEET FORGROllNO-WATER SAMPUNG
---
0 ate lyr/mo/day) 4-J3-'i'Sl Caslng Di am 01..-
Fjefd Personnel Re U-Sche,,.. L Slew a r -c-Top of Casing El ovation
Facility Na me (!en f ra L i. n:l n S ,0 O,. t' Surface Elevation • ~:i-~;2. EPA ID II Seteenad Interval
Well 10# mw-& -G:Otind Wa C:e.r El evatKl n
Weather Condtrior.ts .Svnnv, r:,.oo/, ~00 ---locking Cap YES v NO ~ r _,,. v Total Well Depth {TWOI = 32 1/100 il WeU lntegrit y Sa 1i£ factory YES
Depth to Groundwater [OGWJ ..._ / .2~ Z7 1 /100 ft Well Yield LOW v MODERATE
Length o1 Water Column ILWCJ = TWO • DGW = L2~ .2.3 Water Elevation Equjpmenl
1 Casing Volume CCCV) = lWC x _-3., 0 S ga! Well Dei>th Equjpmen t
3 Casing Volumes = ~' .;i4 :9 a I = Standard ~ acuation Vofvme Field Measurement Equ i pm en t
Method ol Well Evacuafon ~ H Pvm= I Method of Sample Colfection .S.al 1e,,.
To taf V alum e a1 Water Removed
(!) (_.;i) (~) 5a.~ ~l-e..
' P .res efY ative
Bottle
Sampled For -E•: 4-,;i. '1-98
Time [mili1oryj 1/f:;l'f 11..f:~& /\,...u1 10: ~,...,
pH !S.U.) LJ;>./3 l~,0~ Q c {g. 81 ..
Sp. Cond. (µmhos/c m) 73;2 75'8' BJ~
Wai.,,-Temp l°C) --I~-. 3
TU flBIDI fY (s ubi ectiveJ ' ~ J "=?
• { 11 Clear 121 Slight !3) Modoraco 14) High
COMMENTS/OBSERVATIONS: r)i:+,.~ \e)iw--l~k~ iadol'
R-evi:sion 1
;e -~a e. -·
_::; Inch.es-
11100.
11100 f<
1/100 ft
11100ft
NO
HIGH
(j, .0 cal
Augusl 1 S. 19S 7
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--------moAfffta 11111 --------
CHARLOTTE, NORTH CAROUNA
Page if of 7 FIELD OAT A !NF OJIMATION SHEET FOR GROllN 0-WATER SAMPLING
---
Dato {yrtmo/davl 4-?iB-98 Casing Dlamoter ~ i-nches
Fie rd Person ner l<eu.. se/,e,, / ._..56u1a,,-C Top of Casing Elevation 1/100 f
Facility Na me Ce,., 1-"""1 L. _____, -6-/ n:r"" S e_or Surface Elevation 11100 ft , .//;;J -S,,2 EPA JO # Scrooned lntatva! 11100 ft
Woll !D# rYJW-9 Groundwater EJevation 11100 ft
Wea th er Conditions :Svl'1nj{_ l warm , 7~ • r•~ --Locking Cap YES v NO '
Total Well Depth (TWO! = s-,;z llfOO It Wd Integrity Sa tis lac tory YES v NO
Depth to Groundwater !DG W) ~ /4.-¥3 1 £100 ft We.II Yield LOW MODERATE v HIGH
Length of Water Column (LWCI = TWO -DGW = 37, S-7 W aier Elw a ti on Eq uipm on t
I Casing Volume IOCVI = LWC x ~ , 0 / ga! Well Dapth fquipment
3 Co'.Jsing Vol-umes ==-18.03 gal = Sta11d21rd EvaCt1.atiQM Vofume Field Measurement Equipment
Method al Well Evacual ion ,;i ,, Pvazp Method of Sample Coll ectlon &, le.--
.Ltf~O Total Volume o1 Water Removed gal
(.1) (;l) /-S,) ~ ... --,..,L~ .
P1eservative
Bottle ..
Sampled For -ir 4 -;;f'-f!J
Time rmilltaryl fl.I: o:Z 1'1: 0 > //f,' 10 C/."'fS-
pH !S.U.) (,, • 3 IJ. (,,.~4-6. /(p ·.·;· 7. O'/
Sp. Cond. (um hos/cm) d&7 ~"14 .;2C, ~ ;zss
Water Temp (•CJ ---/~, ¥
TURBIDITY (s ubj6ctlve) • 3 I I I
• {1 ) Clear 12 ! Slight (3) M oderote C4 I High
COMMENTS/OBSERVATIONS:
Revision l August 15, 199 7
--== -----H'" "T ;·:r .·~a , •. ~'&' c5w • C:"
· FIELD DATA 10G
CHARLOTTE, NORTH CAROLINA
Paga ~of 7 FIELD DATA INFOJlMATjQN SHEET FOA Gi!OU"IO-WATEA SAMPU"IG
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0 ate {yr/mo/day) ~-;!.B-'?8 Casing 0 i am et er
Field Per son nel 8...euscAer / ..skwch,.z-Top of Casing. Elavat:ion
Facility Name C!. ea. f c,,. L _, r-
S<Jrf ace El ova ti on it:JJ. n s "2'2c:~ " 4/-.SI EPA 10 II Seteenad lntelV.U
Well ID# tr:J. w-10 Groundwater EJovatlon
Wea th er Conditions _<:::;..., h. Mf 1 C;._oo { . ~-~ ·• Locking Cap YES y NO
Total Well Depth !TWO! = SI 111QO I! Wo U Integrity Sa tislactory YES v'
Depth to Groundwe!er IDGWI -/0.~0 111 QO It Well Yield LOW MODERATE
Leng !h of Wat er Column l L WC) = TWO -OGW = ~.~ Waier Elevation Equipment
! Casing Vorume IOCVJ = LWC x _kif~ gal_ w.-1 Oopth Equipment
3 Ca sing Volumes = /9, 38 gar ,,,.. Standard Evaszatjan Vorum§ Field Measurement Er;:zuipment
Method of Well Evacuaiion ~ .. ~~tb: -12. ~ I Method of Sample Coll ectlon E.~, /ev
Total V ol~me ol Water Removed
(J) w r-:r) ~4.-.'.l k • Pres-ervati'Ye
Bottle
Sampled For ·• 'i?. 4-29-98
Time (military! 9: ;?(}
pH IS.U.1 (. 1..6 C:..oo l,.02 -G· ¢8 ,.
Sp. Cond. (µm hos/c mJ 1s-1 01 S-8 2>3 ;I~$"
Water Temp ("Cl ---· ,w. /,, 0
TURBIDITY (subjective)• 3 3 ;J., I
• { 1) Clear (21 SUght 13) Modero ca 141 High
COMMENTS/OBS ERV AT IONS:
Aevis1on l
,<•>•
NO
~
'''""' ·-
HIGH
·~·1
.2 inches:
11100 <
l/100ft
11100 ft
]£100 1t
d0.0 gal
August 15, 1S 97
.... ,,
.------,
rm --= lllill liiiiil iill lill llllll mll · BoA~G till IJlllll -liiiiil ----'7F'
CHARLOlTE, NORTH CAROLINA
P.oge {p of 7 FIELD DATA INFORMATION SHEET FOR GROUND-WAl"ER SAMPLING
Oate {yr/mo/day) :-,.Z 8 -9 8 Ca$ing Diameter -;2_ inches
Field Personnel ~=.SC.::6et::: / -5-/e v.Jar t" r op of Casing Elev,;tion 111 00 f
Facility Name C eri Im L
_,
111 (l0 t< I l:4 "' ::..p. {fl r:. 7': &Jrfaoe Elevation
EPA 10 # Screened lntecvat L.9-,;<9 1/100 ft
Woll ID# hlW-13 Groundwater Elevation 11100tt
Weather Cond1tiorts _c;'._,n,.,I!'. 1 C:.0° ( • •"+ . -Looking Cap YES v NO
Tota I Well Depth {TWO I = ;i'9' 11100 11 Wo U Int og<ity Satisfactory YES v NO
Depth to Groundwater IOGWJ -t_3.ol-11100 tt Well Yield LOW ~ MODERATE HIGH
Length of Water Column ILWCJ = TWO • DGW = /S.9? Water Elevation Equipment
I Casing Vofume IOCVJ = LWC x _.El.• 5 s-. gal Well Oa1>th Equi1>me n t
3 Casing Vo!um BS ...,_ 7. ~ 4-;gar = Standa,d Evagy:ation VoTum-e Field Measutement Eq:ul_pmen £
Method of We!I Evacuation ,;) ,, l)v~ Method of Sample Coif action .7? '8.t. 'le ,,-' ~-.o Total V o!u me <>I Wai er llem oved oal
(.;) ~) ('.D <,,~/~
Preservatjve '
Bottle
Sampled For • i?. ,;. -,2. 'J-9~
Time {military! 1!:10
pH IS.U.) i::;-"?Pi ;:;_ Cf'L-.. O<-.. ·.·;· (, (, 5"
Sp. Con<!. tµm hoslc mJ qf{'q 9/J-9 J!.h£, 9s;i
Water Temp (°C) ,f/JA} ~/Vf/ LJJ,;. ;9, &
TU RBIOIT Y (subjective) • .~ ~ ~ I
• {I) C!ear (2J Slight !3) Moderate 14! High I
COMMENTS/OBSERVATIONS:
R-e vision l August 15, 199 7
,__ ---f;5C= ""5' ··2~ne t§ ~. fi"! ,...,. AEro CA Q •c= .... ,,, . ...... .. ~~·· ·<m .. · .• ·"" llliiiiilJllmi .·· .. r
CHARLOTTE. NORTH CAROLINA
Page 7 of 7 --
FIELD DATA INFORMATjON SHEET FOR GROUND-WATER SAMPUNQ
Data (yr/mo/day J .t/-~8 -'t $ Cas;ng Diam oter ;l incfies
Field Personnel 8~.se..h~ L Slewac.-t" Top of Casing. Elevation 11100 t
Facility Name t2e.dra(. -f ra 1:1 s .Oen-C Sur1ace Elevation 1/100 ft y h (;, -7 t{;, EPA 10 b ScreeAad lntBlVal 1/100 It
Wall fD# mw-Jta Ground water Elevat ~n 11100 ft
Wea th er Condl rioos ..$ v n ryy' .,1 ~ Q oJ '1 ;;, 0" -~·· .. locking Cap YES v NO
Total Well Depth {TWOI = "J{J, 1l!QO ft Wd lntegtiCy Satisfacto~ YES V NO
Depth to Groundwater iOGW) ~ /O.;J.I 1!100 f;: Woll Yield LOW MOOEFIA TE HIGH
Length cl Water Column ILWCJ = TWO -OGW = /oS. 7'l. W aier Elevation Equipm"" f
1 Casing Volume iOCVI c LWC x __j0 • £'3 gal Well 0 op th fqulpmen t
3 Casin'1 VoJumas = ~I• &:, .0 :9 al -Standz.rd ~scua!ion Volume Fie la' Measurement Equipment
M ethad cl Well Evac'1alion ,.:;)# ;wv""Y2 M et/iod of Sample Collection f3a£tCY
I Le>. S-Total Volume ol Water Removed 9aj
{1) O) (3) <,,,-,,,(e .
Preserv a6ve
Bottle
Sampled For .j ~: 4--29_'-fP.
Ti me (miljrary I 11: JS"
pH IS.U./ ~Jf'{" /)_,.Fr -.·;· 7, :::o -
Sp. Cond. l;imhos/cm/ &Lt: ./J.J If~'/
Water Temp ("CJ /VW JJ,_ .. J 7, 0
TUR BIOffY (s ubjectiveJ • I 1C /.., I
• {1 J Clear (21 Slight 13) Moderate 141 High (
COMMENTS/OBSERVATIONS:
Revision ] August 15, 1997
I Pace Analytical Services, Inc.
~ai;a .Aaal¥1iQal 9800 Kincey Avenue, Suite 1 oo • Huntersville, NC 28078
Tel: 704"875·9092
Fax: 704-875·9091
I . Mr. Mark Wilkins May 15, 1998
Page 7 PACE Project Number: 680429514
I Client Reference: Central Transport
I PACE Sample Number: 92 0344120
Date Collected: 04/29/98
,.,~, Date Received: 04/29/98
Client Sample ID: MW-7 n Parameter lliill.s. _ERL METHOD QAIE ANA! Y7ED
' I~QBG8MIC 8~81~SIS
' INDIVIDUAL PARAMETERS
Cyanide, Total mg/L 0.002 NO 335.3 05/01/98 • METALS TARGET ANALYTE LIST
Aluminum mg/L 0.10 ND 05/04/98
Antimony mg/L 0.005 NO 05/07/98
B Arsenic mg/L 0.005 ND 05/08/98
Barium mg/L 0.010 0. 17 05/04/98 ' Beryllium mg/L 0.001 NO 05/11/98
H Cadmium mg/L 0.01 0. 32 Ql 05/04/98
Calcium mg/L 0.10 94 05/04/98
Chromium mg/L 0.010 NO 05/04/98
I Cobalt mg/L 0.010 ND 05/04/98
. Copper mg/L 0.010 0.010 05/04/98
Iron mg/L 0.050 l . l 05/04/98
I Lead mg/L 0.005 ND 05/06/98
'" Magnesium mg/L 0.20 62 05/04/98
I Manganese mg/L 0.010 l.8 05/04/98
Mercury mg/L 0.0002 NO 05/06/98
Nickel mg/L 0.005 0.018 05/06/98
Potassium mg/L 1.0 8.3 05/04/98 , Selenium mg/L 0.005 NO 05/07/98
Silver mg/L 0.002 NO 05/08/98
' Sodium mg/L 0.20 93 05/04/98
Thallium mg/L 0.002 NO 05/12/98
Vanadium mg/L 0.010 NO 05/04/98
Zinc mg/L 0.010 0.20 05/04/98 , I ):!
11! •. OBGANIC ANAIYSIS
I VOLATILE ORGANICS 8260
Oichlorodifluoromethane ug/L 10 NO 05/13/98 . Cll1orometllo.ne ug/L 20 ND 05/13/98
1 Vinyl Chloride ug/L 20 100 05113/98
LabQ[a!Q[)'. Q~rti:ll~rui2n IQ!'i L aborat2G'. ~1nr.an20 10~
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Waler !!(1090
~I NC Drinking Wfiler 37706 TN USTUst
SC 99006 This report. shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
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Pace Analytical
Mr, John Reuscher
Page 2
Client Reference: CTI/97R-543
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANAIYSIS
BASE/NEUTRALS AND ACIDS
2-Nitroani line
Acenaphthylene
Dimethyl phthalate
2,6-Dinitrotoluene
Acenaphthene
3-Nitroanlline
2,4-Dinitrophenol
Oibenzofuran
2,4-Dinitrotoluene
4-Nitrophenol
Fluorene
4-Chlorophenyl phenyl ether
Diethyl phthalate
4-Nitroaniline
2-Methyl-4,6-dinltrophenol
N-Nitrosodlphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butyl phthalate
Fluoranthene
Pyrene
Benzyl butyl phthalate
3,3-Dichlorobenzidine
Benz[a]anthracene
Chrysene
bis(2-Ethylhexyl)phthalate
Di-n-octylphthalate
Benzo[bJfluoranthene
Laboratpiy CQrtificatlon IDs
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
---···----------
Pace Analytical Services, Inc.
9800 Kincey Avenue, Surte 100
Huntersville, NC 28078
May 27, 1998
Tel: [phone]
Fax: [phone]
PACE Project Number: 680507515
92 0350642
05/07/98
05107198
MW7
._EHL METHOD DATE ANA! yzrn
50
10
10
10
10 so
50
10
10
25
10
10
10
50
50
10
10
10
50
10
10
10
10
10
10
20
10
10
10
10
10
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
19
ND
ND
8270
05121198
05/21/98
05/21/98
05/2.l /98
05121198
05/21/98
05/21/98
05/21/98
05/21/98
05/21/98
05/21/98
05/21/98
05/21/98
05121198
05/21/98
05/21/98
05121198
05121198
05121198
05/21/98
05121198
05/21/98
05/21/98
05121198
05121198
05/21/98
05/21/98
05/21/98
05/21/98
05/21/98
05121198
NC Wastewaier 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
Labqrator1 Certf6catjan IDs
KV Dlinldfl<J Water SQQOO
TN UST List
This report shall not be reproduced, except in full,
without the written consent of Pace Analytic:al Services, lne.
VA Drinking Water 213
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Pace Analytical
Mr. Mark Wilkins
Page 14
Client Reference: Central Transport
PACE Sample Number:
Date Collected:
Date Received;
Client Sample ID:
Parameter
ORGANIC ANAIYSTS
VOLATILE ORGANICS
Toluene
l, 1,2-Trlchloroethane
Tetrachloroethene
l ,3-Dichloropropane
Chlorodibromomethane
l ,2-Dibromoethane
Chlorobenzene
l ,1 ,1,2-Tetrachloroethane
Ethyl benzene
m-Xylene and p-Xylene
a-Xylene
Styrene
Bromoform
Isopropylbenzene
l ,l ,2,2-Tetrachloroethane
n-Propylbenzene
Bromobenzene
1 ,2,3-Trichloropropane
2-Chlorotoluene
l ,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
l ,2,4-Trlmethylbenzene
sec-Butyl benzene
l ,3-Dlchlorobenzene
p-Isopropyltoluene
l ,4-0ichlorobenzene
n-Butylbenzene
l ,2-Dichlorobenzene
l ,2-Dibromo-3-chloropropane
l ,2,4-Trichlorobenzene
Laboratorv Certificatipn IDs
Unil.s.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Pace Analytical Services. Inc.
9800 Kincey Avenue, Suite 1 oo
Huntersville, NC 28078
May 15, 1998
Tel: [phone]
Fax: [phone]
PACE Project Number: 680429514
92 0344138
04/29/98
04129198
MW~8
_E.RL METHOD DATE ANAi YZED
8260
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 7.4 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND DS/13/98
5.0 ND 05/13/98
5.0 76 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0 ND 05/13/98
5.0
5.0
5.0
5.0
5.0
5.0
lD
ND
NO
ND
NO
ND
ND
ND
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
NC Wastewater 12
NC DMnking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
Laboratorv Certification IDs
KY Drinking Water 90090
TN UST l..ist
This report shall not be reproduced, except in full,
without tl'le written consent of Pace Analytical Services, Jnc.
VA Drinking Water 213
1 .. ,.j,
If ::.1
• I
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Pace Analytical
Mr. Mark Nllkins
Page 20
Client Reference: Central Transport
PACE Sample Number:
Date Collected:
Date Received:
Cl lent Sample ID:
parameter
ORGANIC ANAIYSIS
VOLATILE ORGANICS
Toluene
l,l,2-Trichloroethane
Tetrachloroethene
l ,3-Dichloropropane
Chlorodibromomethane
1,2-Dibromoethane
Chlorobenzene
1,1,l ,2-Tetrachloroethane
Ethyl benzene
m-Xylene and p-Xylene
o-Xylene
Styrene
Bromoform
Isopropylbenzene
l ,l,2,2-Tetrachloroethane
n-Propylbenzene
Bromobenzene
l ,2,3-Trichloropropane
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
l ,2,4-Trimethylbenzene
sec-Butyl benzene
l ,3-Dichlorobenzene
p-Isopropyltoluene
l ,4-Dichlorobenzene
n-Butylbenzene
l , 2-Di ch l orobenzene
l,2-Dibromo-3-chloropropane
l ,2,4-Trlchlorobenzene
Laboratory Certification !Os
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/l
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/l
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/l
ug/l
ug/l
Pace Analytical services. Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May 15, 1998
Tel: [phone]
Fax: 704·875·9091
PACE Project Number: 680429514
92 0344146
04129198
04129198
MN-9
__£&L_ METHOD DATE ANAIYZED
s.o s.o
5.0
5.0 s.o
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 s.o
5.0
5.0
5.0
5.0
5.0 s.o
5.0 s.o
5.0
5.0
5.0 s.o
5.0
5.0
5.0
10
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8260
05/13/98
05113198
05/13/98
05/13/98
05/13/98
05113198
05113198
05113/98
05/13/98
05113198
05113198
05/13/98
05113198
05/13/98
05113198
05/13/98
05/13/98
05/13/98
05/13/98
05113198
05113198
05113198
05/13/98
05/13/ 98
05/13/98
05113198
05/13/98
05/13/98
05/13/98
05/13/98
05113198
NC Wastewater 12
NC Drin•lng Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
Labqratoiy Certjficajion IDs
KY Drinking Water 90090
TN UST List
This report shall not be reproduced, except in full,
wi,hout the written consent of Pace Analytical Services, Inc.
VA Drln•lng Water 21 a
~I
• II
::;_:11
I . .
u
I
I
I
I
Pace Analytical
Mr. Mark Wilkins
Page 22
Client Reference: Central Transport
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Cyanide, Total
METALS TARGET ANALYTE LIST
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Tha 11 i um
Vanadium
Zinc
ORGANIC ANAIYSIS
BASE/NEUTRALS AND ACIDS
bis(2-Chloroethy1>ether
Phenol
2-Chlorophenol
Laboratory Certification IDs
mg/L
mg IL
mg/L
mg/L
mg/L
mg/L
mg!L
mg/L
mg/L
mg IL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg!L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May I 5, I 998
Tel; 704·875·9092
Fax: [phone]
PACE Project Number: 680429514
92 0344154
04129198
04/29/98
MW-10
....£.R.L._ METHOD DATE ANAIYZED
0.002
o. 10
0.005
0.005
0.010
0.001
0.001
0. 10
0.010
0.010
0.010
0.050
0.005
0.20
0.010
0.0002
0.005
1.0 o.oos
0.002
0.20
0.002
0.010
0.010
JO
10
10
ND
0.28
ND
ND
0.014
ND
ND
21
ND
ND
ND
0.36
ND
1 I
0.01 I
ND
ND
ND
ND
ND
14
ND
ND
ND
ND
ND
ND
335.3
8270
05/05/98
05104198
05/07/98
05108198
05/04/98
05/J I 198
05/07/98
05/04/98
05/04/98
05/04/98
05/04/98
05/04/98
05106198
05104198
05/04/98
05/06/98
05106198
05/04/98
05/07/98
05/08/98
05/04/98
05/12/98
05104198
05/04/98
05112198
05/J 2/98
05112/98
NC Wastewater 12
NC Dflnking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
This report shall not be reproduc~d. except in full,
without the written consent of Pace Analytical Services, Inc.
VA Drinking Water 213
-···-l ,
Pace Analytical Services, Inc.
eaca Aaalll:tical 9800 Kincey Avenue, Suite 100
~I Huntersville, NC 28078
Tel; 704-875-9092
Fax: 704·875-9091
~ Mr. Mark Wilkins May 15, 1998 '
Page 23 PACE Project Number: 680429514
' Client Reference: Central Transport
ft PACE Sample Number: 92 0344154
Date Collected: 04/29/98
Date Received: 04129198
'I Client Sample ID: MW-10
Parameter ilOiJ:s. ...£ll.L METHOD DATE ANAi YZFD
OHG8~IC 8~81XSIS
I BASE/NEUTRALS AND ACIDS 8270 '
l ,3-Dichlorobenzene ug/L 10 ND 05/12/98
I 1 ,4-Dichlorobenzene ug/L 10 ND 05/12/98
l,2-Dichlorobenzene ug/L 10 ND 05/12/98 '
Ben zy l a 1 coho l ug/L 20 ND 05/12198
bis(2-Chloroisopropyllether ug/L 10 ND 05/12/98
I 2-Methylphenol ug/L 10 ND 05112/98
,J
Hexachloroethane ug/L 10 ND 05/12/98
I n-Nitrosodl-n-propylamine ug/L 10 ND 05/12/98
3&4-Methylphenol ug/L 10 ND 05/12/98
Nitrobenzene ug/L 10 ND 05112198
' 3,5,5-Trimethyl-2-cyclohexen-l-one ug/L 10 ND 05/12/98
2-Nitrophenol ug/L 10 ND 05/12/98
2,4-Dimethylphenol ug/L 10 ND 05/12/98 g bis(2-Chloroethoxy)methane ug/L 10 ND 05/12/98
' Benzoic acid ug/L 50 ND 05/12/98
2,4-Dichlorophenol ug/L 10 ND 05/12/98
I 1 ,2,4-Trichlorobenzene ug/L 10 ND 05/12/98
Naphthalene ug/L 10 ND 05/12/98
'
I 4-Chloroaniline ug/L 20 ND 05/12/98
Hexachlorobutadiene ug/L 10 ND 05/12/98
4-Chloro-3-methylphenol ug/L 20 ND 05/12/98
2-Methylnaphthalene ug/L 10 ND 05/12/98
I Hexachlorocyclopentadiene ug/L 10 ND 05/12/98
2,4,6-Trichlorophenol ug/L 10 ND 05/12/98
I 2,4,5-Trichlorophenol ug/L lO ND 05/12/98
2-Chloronaphthalene ug/L 10 ND 05/12 /98
2-Nitroaniline ug/L 50 ND 05/12/98
D
Acenaphthylene ug/L 10 ND 05/12/98
Dimethyl phthalate ug/L 10 ND 05/12/98
2,6-Dinitrotoluene ug/L 10 ND 05/12/98
R Acenaphthene ug/L 10 ND 05/12/98
~!2QCal2L'l C§!lltic;atiaa I~ L ab52[WQ~ Q~l11tiC:JlliSlD IQ~
1•
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY DMnk'1ng Waler 90090
NC Drinking Water 37706 TN U$TUst
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace An~lytical Services, Inc.
• :J;I
I
I
I
I
I
I
pace Analytjcal
Mr. Mark Wilkins
Page 37
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May 15, 1998
Tel: 704·875·9092
Fax: 704·875·9091
PACE Project Number: 680429514
Client Reference: Central Transport
PACE Sample Number:
Date collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANAIYSIS
VOLATILE ORGANICS
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
l ,l-Dichloroethane
2,2-Dichloropropane
cis-1,2-Dichloroethene
Chloroform
Bromochloromethane
1,1,l-Trichloroethane
Carbon Tetrachloride
l ,1-Dichloropropene
Benzene
1,2-Dichloroethane
Trichloroethene
l ,2-Dichloropropane
Bromod1chloromethane
Dibromornethane
Toluene
1 ,1,2-Trichloroethane
Tetrachloroethene
1,3-Dichloropropane
Chlorodibromornethane
l ,2-Dibrornoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
I aborajorv Certification !Os
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
ug/L
92 0344189
04129198
04/29/98
TB
_ERL_ METHOD DATE ANAIYZED
5.0
10
10
10
10
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8260 05/13/98
05/13/98
05113/98
05/13/98
05113/98
05113/98
05/13/98
05/13/98
05113/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/98
05/13/9E
05/13/91
05/13/91
05/13/9:
05/13/9
05/13/9
05/13/9
05/13/9
05/13/~
NC Wastewater 12
NC Drinking Waler 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
I abpratorv Certificatiqn If
KY DMnklng Water 900r
TN UST List
This report shall not be reproduced, except in full.
without tne written consent of Pace Analytical Services, Inc.
VA Drinking Water 21 a
• ,:~':I
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Pace Analytical
Mr. Mark Wilkins
Page 39
Client Reference: Central Transport
Metals Target Analytical Methods
Method 200.7
Aluminum -
Calcium
Cobalt
Iron
Manganese
Sodium
Zinc
Barium
Chromium
Copper
Magnesium
Potassium
Vanadium
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May 15, 1998
Tel; 704-875-9092
Fax: [phone]
PACE Project Number: 680429514
Antimony -204.2
Arsenic -206.2
Beryllium -210.2
Cadmium -213.2
Lead -239.2
Mercury -245.1
Nickel -249.2
Selenium -270.2
Silver -272.2
Thallium -279.2
These data have been reviewed and are approved for release.
~'~-"'\-~ N ~-J-~
Margaret S. Harding
Manager, Laboratory Operations
L aborf!torv Cerptjcatinn !Os
NC Wastewater 12
NC Drinking Water 37706
SC 99005
REPORT OF LABORATORY ANALYSIS
This repM shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratorv Certjficyrtjpn IDs
KY Drinking W~et 90090
TN UST List
VA Drinking Water 213
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Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC .28078
Tel: [phone]
Fax: [phone]
Mr. Mark Nllkfns
Page 45
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Cl lent Reference: Central Transport
Cyanide, Total
Batch: 92 72422
Samples: 92 0344 l l l • 92 0344120
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Cyanide, Total
LABORATORY CONTROL SAMPLE:
Parameter
Cyanide, Total
Laboratory Certification !Os
lJ.o.il.s.
mg/L
lJ.o.il.s. mg/L
lli
0.002
lli
0.002
Method
Blank
ND
NC Wastewatet 12
NC Dr'inking Water 37706
SC 99000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. lne.
920345088
0.020
Reference
Value
0.020
Duplicate
of
92 0345088
Q.018
R.e.tJL
95%
RED
11%
Laborajoty Cenjfjc;;rtjon IDs
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
I
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Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: 704·875·9092
Fax: 704-875·9091
Mr. Mark Wilkins
Page 49
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
Nickel
Batch: 92 72530
Samples: 92 0344111, 92 0344120, 92 0344138, 92 0344146, 92 0344154
92 0344162, 92 0344170
METHOO BLANK AND SAMPLE DUPLICATE:
Parameter
Nickel
SPIKE ANO SPIKE DUPLICATE:
Unils.
mg/L
Method
£RL Blank
0.005 ND
Duplicate
of
920340477 .91..Jl3!lil&ll
ND ND
Spike
Spike Dupl
lill2
NC
parameter
Nickel Unils. mg/L
£RL 92 0 3 40540 .5.p1k.e R.e.c.Ji. Re.c.!L lill2
0.005 ND 0.025 108% 108% 0%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Pa ramptpr
Nickel
L aboprtorv Certffigition !Os
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Unils.
mg/L
£.Bl
0.005
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduceo, except in full,
without the written consent of Pace Analytical Services, Inc.
Reference Dupl
Va l 11 e B.e.c.ll Rae.It. B.ffi_
0.025 100% 98% 2%
L.aboratorv Certjfipat!on IDs
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
Ill'' i!::'.I
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• ~·
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Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mark Wilkins
Page 50
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
Selenium
Batch: 92 72586
Samples: 92 0344111, 92 0344120, 92 0344138, 92 0344146, 92 0344154
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter
Selenium
IJ.ni.t.s.
mg/L
£.Bl Blank 920344090 92 0344090 R£.Q
0.005 ND ND ND NC
SPIKE AND SPIKE DUPLICATE:
Parameter
Selenium
IJ.ni.t.s.
mg/L
£.Bl 920344103
0.005 ND
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Parameter
Selenium
L}lbOrfi!lprv Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
IJ.ni.t.s.
mg/L
£.Bl
0.005
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
!iµ,ll.e
0.025
Spike
Spike Dup 1
B.e..c..l! B.e..c..l! R£.[)
90% 78% 14%
MI MI
Reference
Val 11e
0.025
Du pl
B.e..c..l! B.e..c..l! RPO_
104% l 02% 2%
Laboratorv Certjfiqrtjon IDs
KY Drinking water 90090
TN UST List
VA Drinking Water 213
• .. ,, :11
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• :,111
I
I
•
I
I
I
I
I
I
Pace Analytjcal
Mr. Mark W1lkins
Page 53
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May 15, 1998
Tel: [phone]
Fax: [phone]
PACE Project Number: 680429514
Client Reference: Central Transport
S 1 l ver
Batch: 92 72655
Samples: 92 0344120, 92 0344138, 92 0344146, 92 0344154, 92 0344162
92 0344170
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Silver
SPIKE AND SPIKE DUPLICATE:
Parameter
Silver
Units.
mg/L
Units. mg/L
Duplicate
Method 920344120 of
£RL BI a nk .l:JJMW..,-:..17___ 92 0344 I 20
0.002 ND ND ND
920344138
Spike
Spike Dupl
BED
NC
£RL "'MW..,-::.:8.....___ £pike.
0.002 ND 0.010
Re.l:.lL Re.r..ll. BED
667'. 69% 4%
MI MI
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Parameter
Silver
Laboratory Certification IDs
NC Wastewater 12
NC Orinking Water 37706
SC 99006
Units. mg/L
£RL
0.002
REPORT OF LABORATORY ANALYSIS
This report shall not be reprOduced, except in full,
without tl'le written consent of Pace Analytical Services. Inc.
Reference
Va J 11e
0.010
Dupl
Re.l:.lL Re.r..ll. RfD._
93% 93% m
LabQmtpry CertlfiM1ion IDs
KY DrlnKlng Water 90090
TN UST List
VA Drinking Water 213
u
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Pace Aoalytjcal
Mr. Mark Wilkins
Page 55
QUALITY CONTROL DATA
Client Reference: Central Transport
ICP QUALITY CONTROL
Batch: 92 72495
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC .28078
May 15, 1998
Tel: [phone]
Fax: 704-875·9091
PACE Project Number~ 680429514
Samples: 92 0344111, 92 0344120, 92 0344154, 92 0344162, 92 0344170
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920344111 of
Parameter Blank MW-6 92 0344111 RED
INDIVIDUAL PARAMETERS
Barium mg/L 0.010 0.091 0.090 1 i.
Calcium mg/l o. 10 39 39 Oi.
Chromium mg/L 0.010 ND ND NC
Cobalt mg/L 0.010 ND ND NC
Copper mg/L 0.010 ND ND NC
Iron mg/L 0.050 0.88 0.89 Ji.
Magnesium mg/L 0.20 21 21 0%
Manganese mg/L 0.010 0.015 0.014 7%
Potassium mg/l 1.0 2.5 2.6 47.
Sodium mg/L 0.20 26 26 01.
Vanadium mg/L 0.010 ND ND NC
Zinc mg/L 0.010 0.23 0.23 0%
ICP QUALITY CONTROL
Aluminum mg/L 0.10 ND 0.68 0.68 0%
Antimony mg/L 0.20 ND
Arsenic mg/L 0.50 ND
Barium mg/L 0.010 ND
Bery 11 i um mg/L 0.010 ND
Boron mg/L 0.10 ND
Cadmium mg/l 0.010 ND
Calcium mg/L 0. 10 ND
Chromium mg/L 0.010 ND
Cobalt mg/L 0.010 ND
Copper mg/L 0.010 ND
Iron mg/L o.oso ND
Lead mg/l o. 10 ND
Magnesium mg/L 0.20 ND
Manganese mg/l 0.010 ND
Molybdenum mg/L o.os ND
Nickel mg/L 0.05 ND
I ab!2cato~ Q~Oifii:;atioa l~lli LabQud!:!Ol Qlllitlifii;;;at!QD )!Ji:;
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking water 90090
NC Drinking Water 37706 TN UST Lisi
SC 99006 This report shall not be reproduced, except in full, VA Drinking Waler 213
without the written consent of Pace Analytical Services, Inc.
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Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: 704·875-9092
Fax: [phone]
Mr. Mark Wilkins
Page 56
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
ICP QUALITY CONTROL
Batch: 92 72495
Samples: 92 0344111, 92 0344120, 92 0344154, 92 0344162, 92 0344170
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920344111 of
earaweter llnit.s £RL Bl aa~ Mll-6 ~2 031111111 .Rl'..D
Potassium mg/L l .0 ND
Selenium mg/L 0.50 ND
Silver mg/L 0.050 ND
Sodium mg/L 0.20 ND
Thallium mg/L 0.50 ND
Tin mg/L 0.20 ND
Titanium mg/L 0.010 ND
Vanadium mg/L 0.010 NO
Zinc mg/L 0.010 ND
SPIKE AND SPIKE DUPLICATE:
Spike
920344120 Spike Dupl
eai:ametei:: llnit.s £RL t:!W-Z Spik.e. Rac:ll Rs.c!L .Rl'..D
Aluminum mg/L 0.10 ND 50 103% l 021. 1%
Arsenic mg/L 0.50 ND 2.0 991. 96% 31.
Barium mg/L 0.010 0.17 1.0 100% 99% 17.
Beryllium mg/L 0.010 ND 1.0 101% 101% 0%
Boron mg/L o. 10 0.24 l.O 101% 100% 1%
Cadmium mg/L 0.010 0.032 l.O 101% l 021. 1%
Calcium mg/L 0.10 94 50 981. l OrJ'/. 2%
Chromium mg/L 0.010 ND l.O 100% l 001. 0%
Cobalt mg/L 0.010 ND 1.0 981. 98% 0%
Copper mg/L 0.010 0.010 l.O 100% 99% l%
Iron mg/L o.oso l. l 25 981. 97% 17.
Lead mg/L 0. 10 ND 2.0 l 00·1. 99"/. 11.
Magnesium mg/L 0.20 62 25 95% 93% 2%
Manganese mg/L 0.010 1. 8 1.0 941. 941. 0%
Molybdenum mg/L 0.05 ND l . 0 101% 101% 0%
Nickel mg/L 0.05 ND l.O 100% 1011. 1%
Potassium mg/L l.O 8.3 50 103% 1021. 1%
Selenium mg/L 0.50 ND 2.0 107% l 041. 3%
labQ[!Mgt); Q~rlin!;IWiQO IQ~ Latu:~QMQt:x C:rotbtiao !Q~
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN USTUst
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Service$, Inc.
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Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: 704-875·9092
Fax: [phone]
Mr. Mark Wilkins QUALITY CONTROL DATA May 15, 1998
Page 59 PACE Project Number: 680429514
Client Reference: Central Transport
ICP QUALITY CONTROL
Batch: 92 72510
Samples: 92 0344138, 92 0344146
METHOD BLANK AND SAMPLE DUPLICATE:
earameter
INDIVIDUAL PARAMETERS
Barium
Calcium
Chromium
Cobalt
Copper
Iron
Magnesium
Manganese
Potassium
Sodium
Vanadium
Zinc
ICP QUALITY CONTROL
Aluminum
Antimony
Arsenic
Barium
Beryl 11 um
Boron
Cadmium
Cal cl um
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
l..~QgrntQQl Q~Oills;miQO l~S:
Method
lirlits. BJ ank
mg/L 0.010
mg/L 0.10
mg/L 0.010
mg/L 0.010
mg/L 0.010
mg/L 0.050
mg/L 0.20
mg/L 0.010
mg/L 1.0
mg/L 0.20
mg/L 0.010
mg/L 0.010
mg/L o. 10 ND
mg/L 0.20 ND
mg/L 0.50 ND
mg/L 0.010 ND
mg/L 0.010 ND
mg/L o. 10 ND
mg/L 0.010 ND
mg/L 0.10 ND
mg/L 0.010 ND
mg/L 0.010 ND
mg/L 0.010 ND
mg/L 0.050 ND
mg/L 0.10 ND
mg/L 0.20 ND
mg/L 0.010 ND
mg/L 0.05 ND
mg/L 0.05 ND
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS NC Drinking Water 37706
SC 99006 This report shall not be reproduced, except in full,
without the written consent of Pac:e Analytical Services, Inc.
Duplicate
920344138 of
MW-8 92 0344138 BED
o. 18 o. 18 0%
88 81 8%
ND ND NC
ND ND NC
0.011 0.010 10%
9. l 8.9 2%
22 23 4%
l . 7 1. 7 0%
8. l 8.6 6%
66 67 2%
ND ND NC
ND ND NC
0.74 0.74 0%
L.abQOOC~ Q~rtifiQatl2n !Os
KY Drlnldng Water 90090
TN UST List
VA Drinking Water 213
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Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mark Wilkins
Page 65
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
BASE/NEUTRALS AND ACIDS
Batch: 92 72540
Samples: 92 0344111
LABORATORY CONTROL SAMPLE:
Parameter
l ,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Acenaphthylene
Dimethyl phthalate
2,6-Dinitrotoluene
Acenaphthene
3-Nitroanlline
2,4-Dinitrophenol
Dibenzofuran
2,4-Dinitrotoluene
4-Nitrophenol
Fluorene
4-Chlorophenyl phenyl ether
Diethyl phthalate
4-Nitroaniline
2-Methyl-4,6-dinitrophenol
N-Nitrosodiphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butyl phthalate
Laborajorv CertjficQfjon IDs
lln.i.ts. .ERL
ug/L 10
ug/L 10
ug/L 20
ug/L 10
ug/L 20
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 50
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 50
ug/L so
ug/L 10
ug/L 10
ug/L 25
ug/L 10
ug/L 10
ug/L 10
ug/L 50
ug/L 50
ug/L 10
ug/L JO
ug/L 10
ug/l 50
ug/L 10
ug/L 10
ug/L 10
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This repM shall not be reproduced. exoept in full,
without the written consent of Pace Analytical Services, Inc:,
Reference
Value
50
50
50
50
50
50
so so
50
50
50
50
50
50
50
50
50
50
50
50
50 so
50
50
50
50
50
50 so
50
50
50
Rel:ll
54%
60%
62%
52%
80%
65%
22i'.
74'%,
74%
70%
116%
78%
92%
92%
80%
94%
50%
82%
96%
40%
84%
82%
100%
887.
74%
84%
80%
98%
66%
827.
82%
84%
1.a~2rat2ct Qeaifiratis:u1 IQ~
KY Drinking water 90090
TN UST List
VA Drinking Water 213
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Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel; 704-875-9092
Fax: 704 .. 875-9091
Mr. Mark Wilkins
Page 72
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
BASE/NEUTRALS AND ACIDS
Batch: 92 72758
Samples: 92 0344162
METHOD BLANK:
Parameter
bis(2-Chloroethyl)ether
Phenol
2-Chlorophenol
l,3-Dichlorobenzene
1 ,4-Dichlorobenzene
I ,2-Dichlorobenzene
Benzyl alcohol
bis(2-Chloroisopropyl)ether
2-Methylphenol
Hexachloroethane
n-Nitrosodi-n-propylamine
3&4-Methylphenol
Nitrobenzene
3,5,5-Trimethyl-2-cyclohexen-l-one
2-Nitrophenol
2,4-Dimethylphenol
bis<Z-Chloroethoxy>methane
Benzoic acid
2,4-Dichlorophenol
l,2,4-Trichlorobenzene
Naphthalene
4-Chloroanlline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trlchlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Acenaphthylene
Dimethyl phthalate
laboratory Certjficajjon !Os
l.lD.ils.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Method
£RL Bla.nL
10 ND
10 ND
10 ND
10 ND
10 ND
10 ND
20 ND
10 ND
10 ND
10 NO
10 ND
10 ND
10 ND
10 ND
10 ND
10 ND
10 ND
50 ND
10 NO
10 ND
10 ND
20 ND
10 ND
20 NO
10 ND
10 ND
10 ND
10 ND
10 ND
50 ND
10 ND
10 ND
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,
Laboratorv CertfficatiOD !OS
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
!II l!I
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Pace Analytical
Mr. Mark Wilkins
Page 73
Cl lent Reference: Central
BASE/NEUTRALS AND ACIDS
Batch: 92 72758
Samples: 92 0344162
METHOD BLANK:
Parameter
2,6-Dlnltrotoluene
Acenaphthene
3-Nitroaniline
2,4-Dinitrophenol
Dibenzofuran
2,4-Dinitrotoluene
4-Nitrophenol
Fluorene
QUALITY CONTROL DATA
Transport
UnilS. fB.L
ug/L 10
ug/L 10
ug/L 50
ug/l so
ug/L 10
ug/L 10
ug/L 25
ug/L 10
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: 704·875·9092
Fax: 704·875·9091
May 15, 1998
PACE Project Number: 680429514
Method
Bl aok
ND
ND
ND
ND
ND
ND
ND
ND
4-Chlorophenyl phenyl ether ug/L 10 ND
Diethyl phthalate ug/L 10 ND
4-Nitroaniline ug/L so ND
2-Methyl-4,6-dinitrophenol ug/L so ND
N-Nitrosodiphenylamine ug/L 10 ND
4-Bromophenyl phenyl ether ug/L 10 ND
Hexachlorobenzene ug/L 10 ND
Pentachlorophenol ug/L so ND
Phenanthrene ug/L 10 ND
Anthracene ug/L 10 ND
Di-n-butyl phthalate ug/L 10 ND
Fl uoranthene ug/L 10 ND
Pyrene ug/L 10 ND
Benzyl butyl phthalate ug/L 10 ND
3,3-Dichlorobenzidlne ug/L 20 ND
Benz[a]anthracene ug/L 10 ND
Chrysene ug/L 10 ND
bis(2-Ethylhexyllphthalate ug/L 10 ND
Di-n-octylphthalate ug/L 10 ND
Benzo[bJfluoranthene ug/L 10 ND
Benzo[kJfluoranthene ug/L 10 ND
Benzo[alpyrene ug/L 10 ND
Indeno[l,2,3-cdJpyrene ug/L 10 ND
Dibenz[a,h]anthracene ug/L 10 ND
\ aboratorv CertificMion IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Jne.
1 @hgratqry Certification IDs
KY Drinking Water 90090
TN UST Llst
VA Drinking Water 213
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Pace Analytjcal
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC .z8078
Tel: 704-875·9092
Fax: 704·875-9091
Mr. Mark Wilkins
Page 74
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
BASE/NEUTRALS AND ACIDS
Batch: 92 72758
Samples: 92 0344162
METHOD BLANK:
Parameter
Benzo[g,h,ilperylene
Surrogate -2-Fluorophenol
Surrogate -Phenol-d6
Surrogate -Nitrobenzene-d5
Surrogate -2-Fluorobiphenyl
Surrogate -2,4,6-Trlbromophenol
Surrogate -Terphenyl-dl4
LABORATORY CONTROL SAMPLE:
Parameter
bis(2-Chloroethyl>ether
Phenol
2-Chlorophenol
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl alcohol
bis<Z-Chlorolsopropyl)ether
2-Methylphenol
Hexachloroethane
n-Nitrosodl-n-propylamine
3&4-Methylphenol
Nitrobenzene
3,5,5-Trimethyl-2-cyclohexen-l-one
2-Nitrophenol
2,4-Dimethylphenol
bis<2-Chloroethoxy)methane
Benzoic acid
2,4-Dlchlorophenol
l ,2,4-Trichlorobenzene
Naphthalene
L,abo(atory Certjficatjon IDs
.l1a.iJ:.£
ug/L
%
%
%
%
%
%
l1rl.U.s.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Method .eru. Blaa~
10 ND
61
22
62
58
79
67
.eru.
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
50
10
10
10
NC Wastewater 12
NC Drin~ing Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. lnc.
Reference
Value
50 Bac.ll. 72%
30%
60%
547.
547.
561.
50
50
50 so
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
58%
76%
62%
587.
84"/.
58"/.
72°1.
78"/.
62i'.
727.
70%
34%
62%
54i'.
60%
L aboratorv Certjficajjon !Ch;
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
11'.'.1··· )1:\1
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Pace Analytical
Mr. Mark ~ilkins
Page 76
Client Reference: Central
BASE/NEUTRALS AND ACIDS
Batch: 92 72758
samples: 92 0344162
LABORATORY CONTROL SAMPLE:
~ai::awel:er
Benzyl butyl phthalate
3,3-Dichlorobenzidine
Benz[aJanthracene
Chrysene
bis<2-Ethylhexyl)phthalate
Di-n-octylphthalate
Benzo[b]fluoranthene
Benzo[kJfluoranthene
Benzo[aJpyrene
Indeno[l,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
L_aboryrtorv Certificatjon !Os
QUALITY CONTROL DATA
Transport
lJ.n1ts. ill ug/L 10
ug/l 20
ug/l 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville. NC 28078
May 15, 1998
Tel; 704-875·9092
Fax: 704·875-9091
PACE Project Number: 680429514
Reference
lla J 11e Rru:lL
50 88%
100 37%
50 72%
50 72%
50 76%
50 84%
50 80".l
50 80%
50 78%
50 74%
50 74%
50 74%
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
L aborajo'Y Certif!c:atjpn IDs
KY Dnnking Water 90090
TN UST List
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
VA Drinking Water 213
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Pace Analytjcal
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078 -Tel: [phone]
Fax: 704"875-9091
Mr. Mark Wilkins
Page 78
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
VOLATILE ORGANICS
Batch: 92 72748
Samples: 92 0344111, 92 0344120, 92 0344138, 92 0344146, 92 0344154
92 0344162
METHOD BLANK:
Method earameter .llnils. ERL Blaa~
Ethyl benzene ug/L 5.0 ND
m-Xylene and p-Xylene ug/l 5.0 ND
o-Xylene ug/L 5.0 ND Styrene ug/L 5.0 ND
Bromoform ug/L 5,0 ND
Isopropylbenzene ug/L 5.0 ND
l ,l,2,2-Tetrachloroethane ug/L 5.0 ND
n-Propylbenzene ug/L 5.0 ND Bromobenzene ug/L 5.0 NO
l ,2,3-Trichloropropane ug/L 5.0 ND
2-Chlorotoluene ug/L 5.0 ND
1,3,5-Trimethylbenzene ug/L 5.0 ND
4-Chlorotoluene ug/L 5.0 ND
tert-Butylbenzene ug/L 5.0 ND
l ,2,4-Trlmethylbenzene ug/L 5.0 ND
sec-Butyl benzene ug/L 5.0 ND
1,3-Dlchlorobenzene ug/L s.o ND
p-Isopropyltoluene ug/L 5.0 ND
1,4-Dichlorobenzene ug/L 5.0 ND
n-Butylbenzene ug/L 5.0 ND
1,2-Dlchlorobenzene ug/L 5.0 ND
l,2-Dibromo-3-chloropropane ug/L s.o ND
1 ,2,4-Trichlorobenzene ug/L 10 ND
Hexachlorobutadlene ug/L 10 ND
Naphthalene ug/L 10 ND
1 ,2,3-Trichlorobenzene ug/L 5.0 ND
Surrogate -Dibromofluoromethane % l 01
Surrogate -l,2-Dlchloroethane-d4 "!. 93
Surrogate -Toluene-dB % l 02.
Surrogate -4-Bromofluorobenzene % 103
l aborajorv Certtficatjon !Os
NC wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
L.aboratorv Certification !Os :'
KY Drinking Water 9009C I
TN UST List
VA Drinking Water 213
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Pace Analytjcal
Mr. Mark Wilkins
Page 84
Client Reference:
VOLATILE ORGANICS
Batch: 92 72750
Central
QUALITY CONTROL DATA
Transport
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May 15, 1998
Tel: 704-875"9092
Fax: [phone]
PACE Project Number: 680429514
Samples: 92 0344170, 92 0344189
LABORATORY CONTROL SAMPLE:
Parameter Jlnlli £RL
Dichlorodifluoromethane ug/L 5.0
Chloromethane ug/L 10
Vinyl Chloride ug/L 10
Bromomethane ug/l 10
Chloroethane ug/L 10
Trichlorofluoromethane ug/L 5.0
l ,l-Dichloroethene ug/L 5.0
Methylene chloride ug/L 5.0
trans-1,2-Dichloroethene ug/L 5.0
l, 1-Dichloroethane ug/L 5.0
2,2-0ichloropropane ug/L 10
cis-1,2-Dlchloroethene ug/L 5.0
Chloroform ug/L 5.0
Bromochloromethane ug/L 5.0
l, 1,1-Trichloroethane ug/L 5.0
Carbon Tetrachloride ug/L 5.0
1,1-Dichloropropene ug/L 5.0
Benzene ug/L 5.0
1,2-Dichloroethane ug/L 5.0
Trichloroethene ug/L 5.0
1,2-Dichloropropane ug/L 5.0
Bromodichloromethane ug/L 5.0
Dibromomethane ug/L 5.0
Toluene ug/L s.o
l ,l ,2-Trichloroethane ug/L 5.0
Tetrachloroethene ug/L 5.0
1,3-Dichloropropane ug/L s.o
Chlorodibromomethane ug/L 5.0
l ,2-Dibromoethane ug/L 5.0
Chlorobenzene ug/L 5.0
l ,l ,l ,2-Tetrachloroethane Ug/l 5.0
Ethyl benzene ug/L s.o
L_aboratorv Gertlfication !Qs
NC Wastewater 12
NC Orinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Reference
Value
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
R.acY.
45'1.
95%
80%
7(f/.
95%
100%
90%
1057.
90%
100%
120%
100%
115%
105%
115%
115'1.
11 (fl.
100%
105%
105%
105"4
105%
l 05'1.
100%
95'1.
115%
105%
1001.
105%
1051.
1151.
1051.
l WQtalO~ Qlililiifi~miSlD IC~
KY Drinking Water
TN UST List
90091 !
VA Drinking Water 213
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" /'I Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suit• 100
Huntersville, NC 28078
Tel: 704·875·9092
Fax: 704-875·9091
Mr. Mark Wilkins
Page 85
QUALITY CONTROL DATA May 15, 1998
PACE Project Number: 680429514
Client Reference: Central Transport
VOLATILE ORGANICS
Batch: 92 72750
Samples: 92 0344170, 92 0344189
LABORATORY CONTROL SAMPLE:
Ea i:ametei: l.lnil:.s £B.L
m-Xylene and p-Xylene ug/L 5.0
o-Xylene ug/L 5.0
Styrene ug/L 5.0
Bromoform ug/L 5.0
Isopropylbenzene ug/L 5.0
l, 1,2,2-Tetrachloroethane ug/L 5.0
n-Propylbenzene ug/L 5.0
Bromobenzene ug/L 5.0
l ,2,3-Trichloropropane ug/L 5.0
2-Chlorotoluene ug/L s.o
1,3,5-Trimethylbenzene ug/L s.o
4-Chlorotoluene ug/L 5.0
tert-Butylbenzene ug/L 5.0
1,2,4-Trimethylbenzene Ug/L 5.0
sec-Butyl benzene ug/L 5.0
1,3-Dichlorobenzene ug/L 5.0
p-Isopropyltoluene ug/L 5.0
1,4-0ichlorobenzene ug/L 5.0
n-Butylbenzene ug/L 5.0
1,2-Dichlorobenzene 5.0 ug/L
l ,2-Dibromo-3-chloropropane ug/L 5.0
1 ,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
l ab9rMQrv Certjfk:atjon IDs
NC Wastewater 12
NC Drinking Wmer 37706
SC 9900ll
ug/L 10
ug/L 10
ug/L 10
ug/L 5.0
REPORT OF LABORATORY ANALYSIS
This report ~hall not be ~epn~duced, except il"I full,
without the written consent of Pace Analytical Servic;.es, Inc,
Reference
l£al11e Reu
40
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
103%
100%
105%
100%
105%
95%
1007.
100%
95%
100%
105%
100%
105%
105%
105%
11 or.
105%
11 or.
l 057.
105%
100%
135%
1151.
180%
130%
Laboratory CertifiQ!tipn !Os
KY Drinking Wmer 9009C
TN UST List
VA Drinking Wmer 213
Pace Analytjcal
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 1 oo
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. John Reuscher
Page 12
QUALITY CONTROL DATA May 27, 1998
PACE Project Number: 680507515
II l~~ll
u
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I
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I
Client Reference: CTI/97R-543
BASE/NEUTRALS AND ACIDS
Batch: 92 73195
Samples: 92 0350642, 92 0350650
SPIKE:
Parameter
Benzyl butyl phthalate
3,3-D1chlorobenzidlne
Benz[a)anthracene
Chrysene
bis(2-Ethylhexyl)phthalate
Di-n-octylphthalate
Benzo[b)fluoranthene
Benzo[kJfluoranthene
Benzo[aJpyrene
Indeno[l ,2,3-cdlpyrene
Dibenz[a,hJanthracene
Benzo[g,h,iJperylene
LABORATORY CONTROL SAMPLE:
Parameter
bls<2-Chloroethyl)ether
Phenol
2-Chlorophenol
1,3-Dichlorobenzene
l ,4-Dlchlorobenzene
l ,2-Dichlorobenzene
Benzyl alcohol
bis<2-Chloroisopropyl>ether
2-Methylphenol
Hexachloroethane
n-Nitrosodi-n-propylamlne
3&4-Methylphenol
Nitrobenzene
3,5,5-Trimethyl-2-cyclohexen-l-one
2-Nitrophenol
2,4-Dimethylphenol
bis(2-Chloroethoxy)methane
Lru>oratorv Certifitajjon !Os
920350642
LJ.a.1ll ill MW1
ug/L 10 ND
ug/l 20 ND
ug/L 10 ND
ug/l 10 ND
ug/L JO 19
ug/L 10 ND
ug/L 10 ND
ug/L 10 ND
ug/L 10 ND
ug/L 10 ND
ug/L 10 ND
ug/L 10 ND
LJ.a.1ll ill
ug/L 10
ug/l 10
ug/L 10
ug/l 10
ug/L 10
ug/L 10
ug/L 20
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
I NC Wastewater 12
I NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lne.
Spike
Spike fuil:.lL
Reference
\I a 1 11 e fuil:.lL
so 62%
50 24%
50 56%
50 52% so 50%
50 58%
50 56%
50 667.
50 58%
50 50%
50 70%
50 52%
50 6(J'!.
50 747. so 58% so 58%
50 66%
L,abgrajorv Certjficajjon IDs
KY Dfinking Water 90090
TN UST List
VA Drinking Water 213
11,
• .. :11
n. ' '
' • ""
I' " ' •. ~ i ' '.
I 'I I L;
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Pace Analytical
Mr. John Reuscher
Page 14
Client Reference: CTI/97R-543
BASE/NEUTRALS AND ACIDS
Batch: 92 73195
Samples: 92 0350642, 92 0350650
LABORATORY CONTROL SAMPLE:
Parameter
Anthracene
Di-n-butyl phthalate
Fluoranthene
Pyrene
Benzyl butyl phthalate
3,3-Dichlorobenzldine
Senz[a)anthracene
Chrysene
bis(2-Ethylhexyllphthalate
Di-n-octylphthalate
Benzo[b]fluoranthene
Benzo[k]fluoranthene
Benzo[a]pyrene
Indeno[l ,2,3-cdlpyrene
Dibenz[a,hJanthracene
BenzoEg,h,i]perylene
Labora,torv Certification IQs
QUALITY CONTROL DATA
llnlli m
ug/L 10
ug/L 10
ug/L 10
ug/l 10
ug/L 10
ug/L 20
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L lO
ug/L 10
ug/L 10
ug/L 10
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
May 27, 1998
Tel: [phone]
Fax: [phone]
PACE Project Number: 680507515
Reference
~al11e Re.a
50 80%
50 947.
50 84%
50 76%
50 787.
100 40%
50 76%
50 787.
50 86%
50 94%
50 94%
50 927.
50 92%
50 84%
50 84%
50 82%
l aborajorv Certjflcajjon IDs
.. -----,
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090 I
NC Drinking Waler 37706
SC 99006 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
TN USTUst
VA Drinking Water 213
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Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: 704·875·9092
Fax: 704·875·9091
Mr. John Reuscher
Page 15
FOOTNOTES May 27, 1998
for pages 8 through 14 PACE Project Number: 680507515
Client Reference; CTI/97R~543
ND
PRL
Not detected at or above the PRL.
PACE Reporting Limit
Laboratorv Certifi9atjon IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratorv Certificatjoo IDs
KY Drinking Water !:!0090
TN UST List
VA Orinking Water 213