Cenco_Analytical Results-OCR

January 09, 2008
LIMS USE: FR - JOHN REUSCHER
LIMS OBJECT ID: 9210724
9210724
Project:
Pace Project No.:
RE:
John Reuscher
Delta Environmental Consultant
8008 Corp. Center Drive
Suite 100
Charlotte, NC 28226
HONBARRIER ANNUAL 5E0711711P
Dear John Reuscher:
Enclosed are the analytical results for sample(s) received by the laboratory on December 28, 2007.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Charlotte Certification IDs
Florida/NELAP Certification Number: E87627Kansas Certification Number: E-10364
Louisiana/LELAP Certification Number: 04034North Carolina Drinking Water Certification Number: 37706North Carolina Wastewater Certification Number: 12
North Carolina Field Services Certification Number: 5342South Carolina Certification Number: 990060001
South Carolina Bioassay Certification Number: 990060003Tennessee Certification Number: 04010Virginia Certification Number: 00213
Asheville Certification IDs
Florida/NELAP Certification Number: E87648
Louisiana/LELAP Certification Number: 03095New Jersey Certification Number: NC011
North Carolina Drinking Water Certification Number: 37712North Carolina Wastewater Certification Number: 40North Carolina Bioassay Certification Number: 9
Pennsylvania Certification Number: 68-03578
South Carolina Certification Number: 99030001South Carolina Bioassay Certification Number: 99030002
Tennessee Certification Number: 2980Virginia Certification Number: 00072
Eden Certification IDs
North Carolina Drinking Water Certification Number: 37738
Virginia Drinking Water Certification Number: 00424
North Carolina Wastewater Certification Number: 633
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Lab ID Sample ID Matrix Date Collected Date Received
9210724001 MW-2 Water 12/27/07 12:08 12/28/07 14:30
9210724002 MW-7 Water 12/27/07 12:36 12/28/07 14:30
9210724003 MW-13 Water 12/27/07 13:10 12/28/07 14:30
9210724004 MW-19 Water 12/27/07 11:30 12/28/07 14:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Lab ID Sample ID Method
Analytes
Reported
9210724001 MW-2 EPA 601 31
9210724002 MW-7 EPA 601/602 40
9210724003 MW-13 EPA 601 31
9210724004 MW-19 EPA 601 31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Sample:MW-2 Lab ID:9210724001 Collected:12/27/07 12:08 Received:12/28/07 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
601 Volatiles Analytical Method: EPA 601
Bromodichloromethane ND ug/L 1.0 1 01/03/08 22:54 75-27-4
Bromoform ND ug/L 1.0 1 01/03/08 22:54 75-25-2
Bromomethane ND ug/L 1.0 1 01/03/08 22:54 74-83-9
Carbon tetrachloride ND ug/L 1.0 1 01/03/08 22:54 56-23-5
Chlorobenzene ND ug/L 1.0 1 01/03/08 22:54 108-90-7
Chloroethane ND ug/L 1.0 1 01/03/08 22:54 75-00-3
Chloroform ND ug/L 1.0 1 01/03/08 22:54 67-66-3
Chloromethane ND ug/L 2.0 1 01/03/08 22:54 74-87-3
Dibromochloromethane ND ug/L 1.0 1 01/03/08 22:54 124-48-1
1,2-Dibromoethane (EDB)ND ug/L 1.0 1 01/03/08 22:54 106-93-4
1,2-Dichlorobenzene ND ug/L 1.0 1 01/03/08 22:54 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 01/03/08 22:54 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 01/03/08 22:54 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 01/03/08 22:54 75-71-8
1,1-Dichloroethane 5.7 ug/L 1.0 1 01/03/08 22:54 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 01/03/08 22:54 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 01/03/08 22:54 75-35-4
cis-1,2-Dichloroethene 38.0 ug/L 1.0 1 01/03/08 22:54 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 01/03/08 22:54 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 01/03/08 22:54 78-87-5
cis-1,3-Dichloropropene ND ug/L 1.0 1 01/03/08 22:54 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 01/03/08 22:54 10061-02-6
Methylene Chloride ND ug/L 2.0 1 01/03/08 22:54 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 01/03/08 22:54 79-34-5
Tetrachloroethene ND ug/L 1.0 1 01/03/08 22:54 127-18-4
1,1,1-Trichloroethane ND ug/L 1.0 1 01/03/08 22:54 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 01/03/08 22:54 79-00-5
Trichloroethene ND ug/L 1.0 1 01/03/08 22:54 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 01/03/08 22:54 75-69-4
Vinyl chloride 1.8 ug/L 1.0 1 01/03/08 22:54 75-01-4
1-Chloro-3-fluorobenzene (S)90 %65-137 1 01/03/08 22:54 625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 5 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Sample:MW-7 Lab ID:9210724002 Collected:12/27/07 12:36 Received:12/28/07 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
601/602 Volatiles Analytical Method: EPA 601/602
Benzene 134 ug/L 5.0 5 01/03/08 22:13 71-43-2
Bromodichloromethane ND ug/L 5.0 5 01/03/08 22:13 75-27-4
Bromoform ND ug/L 5.0 5 01/03/08 22:13 75-25-2
Bromomethane ND ug/L 5.0 5 01/03/08 22:13 74-83-9
Carbon tetrachloride ND ug/L 5.0 5 01/03/08 22:13 56-23-5
Chlorobenzene 518 ug/L 25.0 25 01/08/08 23:12 108-90-7
Chloroethane ND ug/L 5.0 5 01/03/08 22:13 75-00-3
Chloroform ND ug/L 5.0 5 01/03/08 22:13 67-66-3
Chloromethane ND ug/L 10.0 5 01/03/08 22:13 74-87-3
Dibromochloromethane ND ug/L 5.0 5 01/03/08 22:13 124-48-1
1,2-Dibromoethane (EDB)ND ug/L 5.0 5 01/03/08 22:13 106-93-4
1,2-Dichlorobenzene ND ug/L 5.0 5 01/03/08 22:13 95-50-1
1,3-Dichlorobenzene 11.0 ug/L 5.0 5 01/03/08 22:13 541-73-1
1,4-Dichlorobenzene 33.5 ug/L 5.0 5 01/03/08 22:13 106-46-7
Dichlorodifluoromethane ND ug/L 5.0 5 01/03/08 22:13 75-71-8
1,1-Dichloroethane ND ug/L 5.0 5 01/03/08 22:13 75-34-3
1,2-Dichloroethane ND ug/L 5.0 5 01/03/08 22:13 107-06-2
1,1-Dichloroethene ND ug/L 5.0 5 01/03/08 22:13 75-35-4
cis-1,2-Dichloroethene 49.9 ug/L 5.0 5 01/03/08 22:13 156-59-2
trans-1,2-Dichloroethene ND ug/L 5.0 5 01/03/08 22:13 156-60-5
1,2-Dichloropropane ND ug/L 5.0 5 01/03/08 22:13 78-87-5
cis-1,3-Dichloropropene ND ug/L 5.0 5 01/03/08 22:13 10061-01-5
trans-1,3-Dichloropropene ND ug/L 5.0 5 01/03/08 22:13 10061-02-6
Diisopropyl ether ND ug/L 5.0 5 01/03/08 22:13 108-20-3
Ethylbenzene ND ug/L 5.0 5 01/03/08 22:13 100-41-4
Methylene Chloride ND ug/L 10.0 5 01/03/08 22:13 75-09-2
Methyl-tert-butyl ether ND ug/L 5.0 5 01/03/08 22:13 1634-04-4
Naphthalene ND ug/L 10.0 5 01/03/08 22:13 91-20-3
1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 01/03/08 22:13 79-34-5
Tetrachloroethene ND ug/L 5.0 5 01/03/08 22:13 127-18-4
Toluene ND ug/L 5.0 5 01/03/08 22:13 108-88-3
1,1,1-Trichloroethane ND ug/L 5.0 5 01/03/08 22:13 71-55-6
1,1,2-Trichloroethane ND ug/L 5.0 5 01/03/08 22:13 79-00-5
Trichloroethene ND ug/L 5.0 5 01/03/08 22:13 79-01-6
Trichlorofluoromethane ND ug/L 5.0 5 01/03/08 22:13 75-69-4
Vinyl chloride 11.3 ug/L 5.0 5 01/03/08 22:13 75-01-4
Xylene (Total)91.3 ug/L 10.0 5 01/03/08 22:13 1330-20-7
m&p-Xylene 91.3 ug/L 10.0 5 01/03/08 22:13 1330-20-7
o-Xylene ND ug/L 5.0 5 01/03/08 22:13 95-47-6
1-Chloro-3-fluorobenzene (S)81 %65-137 5 01/03/08 22:13 625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 6 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Sample:MW-13 Lab ID:9210724003 Collected:12/27/07 13:10 Received:12/28/07 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
601 Volatiles Analytical Method: EPA 601
Bromodichloromethane ND ug/L 5.0 5 01/03/08 23:36 75-27-4
Bromoform ND ug/L 5.0 5 01/03/08 23:36 75-25-2
Bromomethane ND ug/L 5.0 5 01/03/08 23:36 74-83-9
Carbon tetrachloride ND ug/L 5.0 5 01/03/08 23:36 56-23-5
Chlorobenzene 19.8 ug/L 5.0 5 01/03/08 23:36 108-90-7
Chloroethane ND ug/L 5.0 5 01/03/08 23:36 75-00-3
Chloroform ND ug/L 5.0 5 01/03/08 23:36 67-66-3
Chloromethane ND ug/L 10.0 5 01/03/08 23:36 74-87-3
Dibromochloromethane ND ug/L 5.0 5 01/03/08 23:36 124-48-1
1,2-Dibromoethane (EDB)ND ug/L 5.0 5 01/03/08 23:36 106-93-4
1,2-Dichlorobenzene ND ug/L 5.0 5 01/03/08 23:36 95-50-1
1,3-Dichlorobenzene ND ug/L 5.0 5 01/03/08 23:36 541-73-1
1,4-Dichlorobenzene ND ug/L 5.0 5 01/03/08 23:36 106-46-7
Dichlorodifluoromethane ND ug/L 5.0 5 01/03/08 23:36 75-71-8
1,1-Dichloroethane ND ug/L 5.0 5 01/03/08 23:36 75-34-3
1,2-Dichloroethane ND ug/L 5.0 5 01/03/08 23:36 107-06-2
1,1-Dichloroethene ND ug/L 5.0 5 01/03/08 23:36 75-35-4
cis-1,2-Dichloroethene 223 ug/L 5.0 5 01/03/08 23:36 156-59-2
trans-1,2-Dichloroethene 9.6 ug/L 5.0 5 01/03/08 23:36 156-60-5
1,2-Dichloropropane ND ug/L 5.0 5 01/03/08 23:36 78-87-5
cis-1,3-Dichloropropene ND ug/L 5.0 5 01/03/08 23:36 10061-01-5
trans-1,3-Dichloropropene ND ug/L 5.0 5 01/03/08 23:36 10061-02-6
Methylene Chloride ND ug/L 10.0 5 01/03/08 23:36 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 01/03/08 23:36 79-34-5
Tetrachloroethene ND ug/L 5.0 5 01/03/08 23:36 127-18-4
1,1,1-Trichloroethane ND ug/L 5.0 5 01/03/08 23:36 71-55-6
1,1,2-Trichloroethane ND ug/L 5.0 5 01/03/08 23:36 79-00-5
Trichloroethene ND ug/L 5.0 5 01/03/08 23:36 79-01-6
Trichlorofluoromethane ND ug/L 5.0 5 01/03/08 23:36 75-69-4
Vinyl chloride 32.2 ug/L 5.0 5 01/03/08 23:36 75-01-4
1-Chloro-3-fluorobenzene (S)96 %65-137 5 01/03/08 23:36 625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 7 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Sample:MW-19 Lab ID:9210724004 Collected:12/27/07 11:30 Received:12/28/07 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
601 Volatiles Analytical Method: EPA 601
Bromodichloromethane ND ug/L 1.0 1 01/04/08 00:17 75-27-4
Bromoform ND ug/L 1.0 1 01/04/08 00:17 75-25-2
Bromomethane ND ug/L 1.0 1 01/04/08 00:17 74-83-9
Carbon tetrachloride ND ug/L 1.0 1 01/04/08 00:17 56-23-5
Chlorobenzene ND ug/L 1.0 1 01/04/08 00:17 108-90-7
Chloroethane ND ug/L 1.0 1 01/04/08 00:17 75-00-3
Chloroform ND ug/L 1.0 1 01/04/08 00:17 67-66-3
Chloromethane ND ug/L 2.0 1 01/04/08 00:17 74-87-3
Dibromochloromethane ND ug/L 1.0 1 01/04/08 00:17 124-48-1
1,2-Dibromoethane (EDB)ND ug/L 1.0 1 01/04/08 00:17 106-93-4
1,2-Dichlorobenzene ND ug/L 1.0 1 01/04/08 00:17 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 01/04/08 00:17 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 01/04/08 00:17 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 01/04/08 00:17 75-71-8
1,1-Dichloroethane 1.9 ug/L 1.0 1 01/04/08 00:17 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 01/04/08 00:17 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 01/04/08 00:17 75-35-4
cis-1,2-Dichloroethene 4.7 ug/L 1.0 1 01/04/08 00:17 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 01/04/08 00:17 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 01/04/08 00:17 78-87-5
cis-1,3-Dichloropropene ND ug/L 1.0 1 01/04/08 00:17 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 01/04/08 00:17 10061-02-6
Methylene Chloride ND ug/L 2.0 1 01/04/08 00:17 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 01/04/08 00:17 79-34-5
Tetrachloroethene ND ug/L 1.0 1 01/04/08 00:17 127-18-4
1,1,1-Trichloroethane ND ug/L 1.0 1 01/04/08 00:17 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 01/04/08 00:17 79-00-5
Trichloroethene ND ug/L 1.0 1 01/04/08 00:17 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 01/04/08 00:17 75-69-4
Vinyl chloride ND ug/L 1.0 1 01/04/08 00:17 75-01-4
1-Chloro-3-fluorobenzene (S)86 %65-137 1 01/04/08 00:17 625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 8 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/1555
EPA 601/602
EPA 601/602
601/602 GCV Water
Associated Lab Samples:9210724002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:59925
Associated Lab Samples:9210724002
1,1,1-Trichloroethane ug/L ND 1.0
1,1,2,2-Tetrachloroethane ug/L ND 1.0
1,1,2-Trichloroethane ug/L ND 1.0
1,1-Dichloroethane ug/L ND 1.0
1,1-Dichloroethene ug/L ND 1.0
1,2-Dibromoethane (EDB)ug/L ND 1.0
1,2-Dichlorobenzene ug/L ND 1.0
1,2-Dichloroethane ug/L ND 1.0
1,2-Dichloropropane ug/L ND 1.0
1,3-Dichlorobenzene ug/L ND 1.0
1,4-Dichlorobenzene ug/L ND 1.0
Benzene ug/L ND 1.0
Bromodichloromethane ug/L ND 1.0
Bromoform ug/L ND 1.0
Bromomethane ug/L ND 1.0
Carbon tetrachloride ug/L ND 1.0
Chlorobenzene ug/L ND 1.0
Chloroethane ug/L ND 1.0
Chloroform ug/L ND 1.0
Chloromethane ug/L ND 2.0
cis-1,2-Dichloroethene ug/L ND 1.0
cis-1,3-Dichloropropene ug/L ND 1.0
Dibromochloromethane ug/L ND 1.0
Dichlorodifluoromethane ug/L ND 1.0
Diisopropyl ether ug/L ND 1.0
Ethylbenzene ug/L ND 1.0
m&p-Xylene ug/L ND 2.0
Methyl-tert-butyl ether ug/L ND 1.0
Methylene Chloride ug/L ND 2.0
Naphthalene ug/L ND 2.0
o-Xylene ug/L ND 1.0
Tetrachloroethene ug/L ND 1.0
Toluene ug/L ND 1.0
trans-1,2-Dichloroethene ug/L ND 1.0
trans-1,3-Dichloropropene ug/L ND 1.0
Trichloroethene ug/L ND 1.0
Trichlorofluoromethane ug/L ND 1.0
Vinyl chloride ug/L ND 1.0
Xylene (Total)ug/L ND 2.0
1-Chloro-3-fluorobenzene (S)%94 65-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 9 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
59926LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 15.920 79 41-138
1,1,2,2-Tetrachloroethane ug/L 24.320 121 8-184
1,1,2-Trichloroethane ug/L 21.020 105 39-136
1,1-Dichloroethane ug/L 25.320 126 47-132
1,1-Dichloroethene ug/L 18.520 93 28-167
1,2-Dibromoethane (EDB)ug/L 21.220 106 50-150
1,2-Dichlorobenzene ug/L 20.920 105 1-208
1,2-Dichloroethane ug/L 22.220 111 51-147
1,2-Dichloropropane ug/L 21.420 107 44-156
1,3-Dichlorobenzene ug/L 21.020 105 7-187
1,4-Dichlorobenzene ug/L 20.320 101 42-143
Benzene ug/L 23.420 117 39-150
Bromodichloromethane ug/L 20.420 102 42-172
Bromoform ug/L 21.020 105 13-159
Bromomethane ug/L 28.320 141 1-144
Carbon tetrachloride ug/L 15.620 78 43-143
Chlorobenzene ug/L 19.620 98 38-150
Chloroethane ug/L 23.920 119 46-137
Chloroform ug/L 21.820 109 49-133
Chloromethane ug/L 22.720 114 1-193
cis-1,2-Dichloroethene ug/L 20.720 103 38-155
cis-1,3-Dichloropropene ug/L 19.820 99 22-178
Dibromochloromethane ug/L 21.820 109 24-191
Dichlorodifluoromethane ug/L 21.720 109 48-157
Diisopropyl ether ug/L 20.220 101 89-108
Ethylbenzene ug/L 21.920 110 32-160
m&p-Xylene ug/L 41.640 104 82-115
Methyl-tert-butyl ether ug/L 19.020 95 88-110
Methylene Chloride ug/L 23.720 118 25-162
Naphthalene ug/L 21.620 108 50-150
o-Xylene ug/L 21.420 107 91-110
Tetrachloroethene ug/L 21.420 107 26-162
Toluene ug/L 21.320 107 46-148
trans-1,2-Dichloroethene ug/L 20.320 101 38-155
trans-1,3-Dichloropropene ug/L 20.220 101 22-178
Trichloroethene ug/L 23.220 116 35-146
Trichlorofluoromethane ug/L 26.220 131 21-156
Vinyl chloride ug/L 24.720 123 28-163
Xylene (Total)ug/L 63.160 105 50-150
1-Chloro-3-fluorobenzene (S)%104 65-137
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
59928MATRIX SPIKE SAMPLE:
MSSpike
Result
9210661006
1,1,1-Trichloroethane ug/L 14.620 73 41-138ND
1,1,2,2-Tetrachloroethane ug/L 22.920 114 8-184ND
1,1,2-Trichloroethane ug/L 18.720 93 39-136ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 10 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
59928MATRIX SPIKE SAMPLE:
MSSpike
Result
9210661006
1,1-Dichloroethane ug/L 23.620 118 47-132ND
1,1-Dichloroethene ug/L 18.020 90 28-167ND
1,2-Dibromoethane (EDB)ug/L 16.020 80 50-150ND
1,2-Dichlorobenzene ug/L 19.720 99 1-208ND
1,2-Dichloroethane ug/L 19.420 97 51-147ND
1,2-Dichloropropane ug/L 19.920 100 44-156ND
1,3-Dichlorobenzene ug/L 19.520 98 7-187ND
1,4-Dichlorobenzene ug/L 19.820 99 42-143ND
Benzene ug/L 23.120 116 39-150ND
Bromodichloromethane ug/L 20.820 104 42-172ND
Bromoform ug/L 19.620 98 13-159ND
Bromomethane ug/L 21.120 105 1-144ND
Carbon tetrachloride ug/L 14.920 75 43-143ND
Chlorobenzene ug/L 17.720 89 38-150ND
Chloroethane ug/L 21.620 108 46-137ND
Chloroform ug/L 20.620 103 49-133ND
Chloromethane ug/L 21.820 109 1-193ND
cis-1,2-Dichloroethene ug/L 19.320 97 38-155ND
cis-1,3-Dichloropropene ug/L 14.920 75 22-178ND
Dibromochloromethane ug/L 18.020 90 24-191ND
Dichlorodifluoromethane ug/L 21.520 108 48-157ND
Diisopropyl ether ug/L 19.920 99 89-108ND
Ethylbenzene ug/L 21.120 106 32-160ND
m&p-Xylene ug/L 39.940 100 82-115ND
Methyl-tert-butyl ether ug/L 18.920 95 88-110ND
Methylene Chloride ug/L 23.420 117 25-162ND
Naphthalene ug/L 20.620 103 50-150ND
o-Xylene ug/L 21.820 109 91-110ND
Tetrachloroethene ug/L 17.820 89 26-162ND
Toluene ug/L 21.220 106 46-148ND
trans-1,2-Dichloroethene ug/L 19.920 99 38-155ND
trans-1,3-Dichloropropene ug/L 16.820 84 22-178ND
Trichloroethene ug/L 20.620 103 35-146ND
Trichlorofluoromethane ug/L 22.520 113 21-156ND
Vinyl chloride ug/L 22.720 113 28-163ND
Xylene (Total)ug/L 61.760 103 50-150ND
1-Chloro-3-fluorobenzene (S)%100 65-137
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9210661005
59927SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 0 30ND
1,1,2,2-Tetrachloroethane ug/L ND 0 30ND
1,1,2-Trichloroethane ug/L ND 0 30ND
1,1-Dichloroethane ug/L ND 0 30ND
1,1-Dichloroethene ug/L ND 0 30ND
1,2-Dibromoethane (EDB)ug/L ND 0 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 11 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9210661005
59927SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 0 30ND
1,2-Dichloroethane ug/L ND 0 30ND
1,2-Dichloropropane ug/L ND 0 30ND
1,3-Dichlorobenzene ug/L ND 0 30ND
1,4-Dichlorobenzene ug/L ND 0 30ND
Benzene ug/L ND 0 30ND
Bromodichloromethane ug/L ND 0 30ND
Bromoform ug/L ND 0 30ND
Bromomethane ug/L ND 0 30ND
Carbon tetrachloride ug/L ND 0 30ND
Chlorobenzene ug/L ND 0 30ND
Chloroethane ug/L ND 0 30ND
Chloroform ug/L ND 0 30ND
Chloromethane ug/L ND 0 30ND
cis-1,2-Dichloroethene ug/L ND 0 30ND
cis-1,3-Dichloropropene ug/L ND 0 30ND
Dibromochloromethane ug/L ND 0 30ND
Dichlorodifluoromethane ug/L ND 0 30ND
Diisopropyl ether ug/L ND 0 30ND
Ethylbenzene ug/L ND 0 30ND
m&p-Xylene ug/L ND 0 30ND
Methyl-tert-butyl ether ug/L ND 0 30ND
Methylene Chloride ug/L ND 0 30ND
Naphthalene ug/L ND 0 30ND
o-Xylene ug/L ND 0 30ND
Tetrachloroethene ug/L ND 0 30ND
Toluene ug/L ND 0 30ND
trans-1,2-Dichloroethene ug/L ND 0 30ND
trans-1,3-Dichloropropene ug/L ND 0 30ND
Trichloroethene ug/L ND 0 30ND
Trichlorofluoromethane ug/L ND 0 30ND
Vinyl chloride ug/L ND 0 30ND
Xylene (Total)ug/L ND 0 30ND
1-Chloro-3-fluorobenzene (S)%93 .193
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 12 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/1556
EPA 601
EPA 601
601 GCV Water
Associated Lab Samples:9210724001, 9210724003, 9210724004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:59954
Associated Lab Samples:9210724001, 9210724003, 9210724004
1,1,1-Trichloroethane ug/L ND 1.0
1,1,2,2-Tetrachloroethane ug/L ND 1.0
1,1,2-Trichloroethane ug/L ND 1.0
1,1-Dichloroethane ug/L ND 1.0
1,1-Dichloroethene ug/L ND 1.0
1,2-Dibromoethane (EDB)ug/L ND 1.0
1,2-Dichlorobenzene ug/L ND 1.0
1,2-Dichloroethane ug/L ND 1.0
1,2-Dichloropropane ug/L ND 1.0
1,3-Dichlorobenzene ug/L ND 1.0
1,4-Dichlorobenzene ug/L ND 1.0
Bromodichloromethane ug/L ND 1.0
Bromoform ug/L ND 1.0
Bromomethane ug/L ND 1.0
Carbon tetrachloride ug/L ND 1.0
Chlorobenzene ug/L ND 1.0
Chloroethane ug/L ND 1.0
Chloroform ug/L ND 1.0
Chloromethane ug/L ND 2.0
cis-1,2-Dichloroethene ug/L ND 1.0
cis-1,3-Dichloropropene ug/L ND 1.0
Dibromochloromethane ug/L ND 1.0
Dichlorodifluoromethane ug/L ND 1.0
Methylene Chloride ug/L ND 2.0
Tetrachloroethene ug/L ND 1.0
trans-1,2-Dichloroethene ug/L ND 1.0
trans-1,3-Dichloropropene ug/L ND 1.0
Trichloroethene ug/L ND 1.0
Trichlorofluoromethane ug/L ND 1.0
Vinyl chloride ug/L ND 1.0
1-Chloro-3-fluorobenzene (S)%94 65-137
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
59955LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 15.920 79 41-138
1,1,2,2-Tetrachloroethane ug/L 24.320 121 8-184
1,1,2-Trichloroethane ug/L 21.020 105 39-136
1,1-Dichloroethane ug/L 25.320 126 47-132
1,1-Dichloroethene ug/L 18.520 93 28-167
1,2-Dibromoethane (EDB)ug/L 21.220 106 50-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 13 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
59955LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 20.920 105 1-208
1,2-Dichloroethane ug/L 22.220 111 51-147
1,2-Dichloropropane ug/L 21.420 107 44-156
1,3-Dichlorobenzene ug/L 21.020 105 7-187
1,4-Dichlorobenzene ug/L 20.320 101 42-143
Bromodichloromethane ug/L 20.420 102 42-172
Bromoform ug/L 21.020 105 13-159
Bromomethane ug/L 28.320 141 1-144
Carbon tetrachloride ug/L 15.620 78 43-143
Chlorobenzene ug/L 19.620 98 38-150
Chloroethane ug/L 23.920 119 46-137
Chloroform ug/L 21.820 109 49-133
Chloromethane ug/L 22.720 114 1-193
cis-1,2-Dichloroethene ug/L 20.720 103 38-155
cis-1,3-Dichloropropene ug/L 19.820 99 22-178
Dibromochloromethane ug/L 21.820 109 24-191
Dichlorodifluoromethane ug/L 21.720 109 48-157
Methylene Chloride ug/L 23.720 118 25-162
Tetrachloroethene ug/L 21.420 107 26-162
trans-1,2-Dichloroethene ug/L 20.320 101 38-155
trans-1,3-Dichloropropene ug/L 20.220 101 22-178
Trichloroethene ug/L 23.220 116 35-146
Trichlorofluoromethane ug/L 26.220 131 21-156
Vinyl chloride ug/L 24.720 123 28-163
1-Chloro-3-fluorobenzene (S)%104 65-137
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
59968MATRIX SPIKE SAMPLE:
MSSpike
Result
9210724004
1,1,1-Trichloroethane ug/L 13.920 70 41-138ND
1,1,2,2-Tetrachloroethane ug/L 24.820 124 8-184ND
1,1,2-Trichloroethane ug/L 22.720 113 39-136ND
1,1-Dichloroethane ug/L 25.820 120 47-1321.9
1,1-Dichloroethene ug/L 19.520 97 28-167ND
1,2-Dibromoethane (EDB)ug/L 22.920 115 50-150ND
1,2-Dichlorobenzene ug/L 21.820 109 1-208ND
1,2-Dichloroethane ug/L 22.220 111 51-147ND
1,2-Dichloropropane ug/L 20.920 105 44-156ND
1,3-Dichlorobenzene ug/L 21.620 108 7-187ND
1,4-Dichlorobenzene ug/L 21.120 105 42-143ND
Bromodichloromethane ug/L 21.520 108 42-172ND
Bromoform ug/L 23.420 117 13-159ND
Bromomethane ug/L 25.120 125 1-144ND
Carbon tetrachloride ug/L 13.420 67 43-143ND
Chlorobenzene ug/L 20.420 102 38-150ND
Chloroethane ug/L 24.920 124 46-137ND
Chloroform ug/L 17.120 85 49-133ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 14 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
59968MATRIX SPIKE SAMPLE:
MSSpike
Result
9210724004
Chloromethane ug/L 24.820 124 1-193ND
cis-1,2-Dichloroethene ug/L 26.320 108 38-1554.7
cis-1,3-Dichloropropene ug/L 19.020 95 22-178ND
Dibromochloromethane ug/L 21.720 109 24-191ND
Dichlorodifluoromethane ug/L 19.620 98 48-157ND
Methylene Chloride ug/L 23.120 116 25-162ND
Tetrachloroethene ug/L 20.720 103 26-162ND
trans-1,2-Dichloroethene ug/L 19.520 98 38-155ND
trans-1,3-Dichloropropene ug/L 19.620 98 22-178ND
Trichloroethene ug/L 23.920 120 35-146ND
Trichlorofluoromethane ug/L 23.820 119 21-156ND
Vinyl chloride ug/L 25.220 126 28-163ND
1-Chloro-3-fluorobenzene (S)%103 65-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 15 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9210724
HONBARRIER ANNUAL 5E0711711P
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/09/2008 05:34 PM Page 16 of 16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
.,,,4:)
Pace Analytical '
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Report To: :JD),,.., J<'rzu.f c A .e-r-Attention: :ro ( ~ '°ReM.-.S c ~ 1138578
Ad~oag 6,.,,,nife &YJ/u ~r.1capyTa Company Name: REGULATORY AGENCY
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