21027_McCall Farms_PHASE II_20170518

TABLE OF CONTENTS
1.0 INTRODUCTION ................................................................................................................. 1
2.0 SUMMARY OF ASSESSMENT ACTIVITIES ................................................................... 3
2.1 Geophysical Assessment ........................................................................................................ 3
2.2 Soil Assessment ..................................................................................................................... 4
2.2.1 Test Pit Soil Assessment ............................................................................................... 4
2.2.2 Soil Boring Assessment ................................................................................................. 5
2.3 Groundwater Assessment....................................................................................................... 5
2.4 Abandonment and Site Clean-up ........................................................................................... 6
3.0 PHYSICAL SITE CHARACTERISTICS ............................................................................. 7
3.1 Topography and Surface Water Drainage.............................................................................. 7
3.2 Site Geology........................................................................................................................... 7
3.3 Site Hydrogeology ................................................................................................................. 7
4.0 ASSESSMENT RESULTS .................................................................................................... 7
4.1 Soil Assessment and Analytical Results ................................................................................ 8
4.1 Groundwater Analytical Results ............................................................................................ 9
5.0 FINDINGS, CONCLUSIONS, AND RECOMMENDATIONS......................................... 10
6.0 REFERENCES .................................................................................................................... 12

DRAWINGS
Drawing 1.1 ............................................................................................... Topographic Site Map
Drawing 1.2 .............................................. Recognized Environmental Condition Summary Map
Drawing 2.1 .................................................... Test Pit Location and Soil Sample Summary Map
Drawing 2.2 ............................... Boring Location and Soil/Groundwater Sample Summary Map

TABLES
Table 4.1 .................................................... Summary of Laboratory Test Detections – Soil Samples
Table 4.2 ..................................... Summary of Laboratory Test Detections – Groundwater Samples

APPENDICES
Appendix A................................. Laboratory Analytical Reports and Chain-of-Custody Records
Appendix B ............................................ Monitoring Well Construction and Abandonment Logs
Appendix C ........................................................................ Monitoring Well Construction Permit

1.0 INTRODUCTION

The John R McAdams Company (McAdams) was retained by Kemira Water Solutions, Inc. to
perform this Phase II Environmental Site Assessment (Phase II ESA) for the former McCall Farms
property located at 2202 Charleston Street SE in Wilson, Wilson County, North Carolina (the
“site” or “subject site”). The subject site consists of Wilson County Tax Parcel, Parcel Identification
Number (PIN) 3721-60-7236. The parcel totals 17 acres in size. The site is depicted on the
topographic map presented as Drawing 1.1.

The subject site was utilized as a sweet potato canning, processing and manufacturing facility from
the 1960s until 2015 when facility operations ceased. The property is currently owned by the City
of Wilson. Kemira Water Solutions, Inc. is interesting is purchasing the property from the City of
Wilson to establish a rail yard onsite and possibly redevelop the site for future manufacturing
purposes.

During a Phase I Environmental Site Assessment (PESA) site reconnaissance, originally
performed by McAdams on October 28, 2016, structures on the site were in the process of being
demolished by others on behalf of the City of Wilson. On February 2, 2017, McAdams returned
to the site to perform Phase II ESA field assessment activities. At the time of the Phase II ESA,
with the exception of a small truck scale house, above ground structures and foundations had been
razed and the property was a graded vacant lot. Subsurface utilities remained in the ground.

The purpose of the Phase II ESA was to the findings identified in the PESA (McAdams, 2017) for
the subject site. These areas are depicted on Drawing 1.2 and summarized below:
• Area A (Above Ground Storage Tank [AST] System/Abandoned-in-Place
Underground Storage Tank [UST], southwest corner of site): A 500-gallon gasoline
above ground storage tank (AST) and a 1,000-gallon diesel AST and associated fueling
pumps were identified in Area A (adjacent to the truck scale) during the site reconnaissance.
Surface staining around the AST system and dispenser pumps was observed by McAdams
during the performance of this PESA. A leaking underground storage tank (LUST) incident
(number 39484) was reported in conjunction with the 1,000-gallon abandoned UST that was
also identified in this area in 2012. Petroleum related groundwater impacts above the 15A
NCAC 02L .0202 North Carolina Groundwater Standards (2L Standards), but below the
Gross Contaminant Levels (GCLs) were identified by Environmental Assessments +
Consulting, Inc. (EAC) in a 2013 Limited Site Assessment (LSA) performed in this area.
Because receptors were not identified in the search radii required by North Carolina
Department of Environmental Quality (NCDEQ), a No Further Action (NFA) and Notice of
Residual Petroleum (NORP) were issued on February 19 and 27, 2014, respectively. • Area B (Former UST Area, near Charleston Street SE, south of former boiler room):
Three former fuel oil USTs measuring 3,000 gallons, 6,000 gallons, and 20,000 gallons each;
a 12,000-gallon gasoline/gasoline mix UST; and, a 500-gallon diesel UST were reported to
have been in Area B. Two LUST incidents (numbers 26380 and 39484) have been linked to
this area. LUST Incident Number 26380 was associated with the removal and closure of the
12,000-gallon gasoline UST in 1990. An assessment of the release was performed that
included soil and groundwater sampling. Soil sample results were reported below the action
level and groundwater impacts were not found. A NFA was issued for the incident on April
25, 1991. LUST Incident Number 39484 was reported in 2012 for impacts associated with
the five USTs in Area B (and the 1,000-gallon abandoned UST in Area A). As documented
in the EAC 2013 LSA, petroleum related compounds were identified above the NCDEQ
UST Section Maximum Soil Contaminant Concentrations (MSCCs) and 2L Standard in soil
and groundwater, respectively. Because receptors were not identified in the search radii
required by NCDEQ, a NFA and NORP were issued on February 19 and 27, 2014,
respectively.
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• Area C (Former Inorganic Compound/Processing Area, central/western portion of
site): The 2013 Phase II ESA performed by EAC indicated that this area contained 1) a
former AST compound that formerly contained potato preservative and treatment chemicals
including a 10,000-gallon reclaimed potassium hydroxide AST, a 10,000-gallon potassium
hydroxide AST, a 10,000-gallon slurry AST, a 10,000-gallon magnesium hydroxide AST,
and, an empty water tank; 2) an area in which potato sorting and washing equipment was
used; and, 3) a process sediment tank and lift station that delivered waste water to a waste
water treatment plant located offsite on the south adjacent parcel (also formerly owned by
Bruce Foods Corporation). Results of the Phase II performed by EAC identified low level
detections of chloride, sulfate, nitrate (as nitrogen), and ammonia in soil and groundwater
below the associated NCDEQ Preliminary Site Remediation Goals (PSRGs) and 2L
Standards. Total dissolved solids (TDS) were identified above the 2L Standards in
groundwater. • Area D (Former Boiler Room, north of Area B): Surface soil staining was observed by
McAdams in the boiler room area in 2016 during the PESA site reconnaissance. The City
of Wilson also reported staining in this area during demolition and grading activities in 2016,
after the former building’s concrete slab was removed. Site observations suggested that the
staining may have potentially originated from decommissioning of the remaining ASTs
during site demolition. • Area E (Northwestern Drum and Debris Area, northwest portion of the site): EAC
performed a Phase II ESA in 2013 in which numerous plastic 55-gallon drums and what
appeared to be used hydraulic oil, petroleum impacted water, and other petroleum waste
products were identified on wood pallets over bare ground, stained surfaces. Results of the
Phase II indicated the presence of total petroleum hydrocarbon (TPH) diesel range organics
(DRO) above the NCDEQ Division of Waste Management (DWM) UST Section Action
Level. In 2014, EAC returned to the site and excavated 54 tons of petroleum impacted soil
and disposed of the material offsite. Confirmation samples revealed concentrations of TPH-
DRO below the NCDEQ DWM UST Section Action Level. The incident was never reported
to the NCDEQ. The equipment storage area and the northwest area of the site in general
(which included the former excavated drum storage area) was identified in the 2016 Phase I
performed by Duncklee and Dunham, P.C. (D&D) as a REC due to the presence, and past
storage of drums and debris scattered throughout the area. • Area F (Onsite Transformer Area, middle portion of the site): Pole-mounted transformers
were identified onsite in the back of the plant by D&D during the 2016 Phase I. The
transformers were not labeled to indicate polychlorinated biphenyl (PCB) content. Evidence
of leakage from the transformers was not observed by D&D. • Site Groundwater: In addition to petroleum related compounds and inorganic compounds
identified in site groundwater during the EAC 2013 Phase II ESA (previously discussed in
Areas A through C), tetrachloroethylene below the 2L Standard was identified in site
groundwater by D&D in the 2016 Phase II assessment. The source of the tetrachloroethylene
was not identified by D&D. D&D did not make recommendations based on the results of
the Phase II assessment. • Water Tank/Chiller Area: The 2016 Phase I ESA performed by D&D identified a pad partially covered by gravel at the northern end of the plant where a Water Tank/Chiller Area was once located. D&D reported having observed an enclosed basin containing stained sediment on the partially covered pad. The use of the basin was not identified. Staining near the pad was not reported. • Unaccounted 500-gallon UST: Records for the site report the presence of a 500-gallon diesel fuel UST onsite that was never accounted for as part of the AST System/Abandoned-in-Place UST area (Area A) or the UST area (Area B). Records are unclear if this UST is still present and unaccounted for or has been misrepresented as the 1,000-gallon gasoline
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Wilson, North Carolina

UST that was closed in-place in Area A. USTs were reportedly not identified by the City of
Wilson during 2016 demolition and grading activities onsite.

Offsite Findings:
• Linamar Forgings/Carolina Forge (Stantonsburg Road): The Linamar
Forgings/Carolina Forge facility located at 2401 Stantonsburg Road SE is identified in the
SHWS under EPA Identification number NCD982084113. This forge is located
approximately 2,000 feet to the east of, and upgradient to, the subject site. The Linamar
Forgings Site is currently in the North Carolina Inactive Hazardous Sites Program with
ongoing remedial investigations occurring onsite. The 2016 RI Work Plan prepared for
the Linamar site included plans to assess several constituents identified on the property
including chlorinated solvents and trihalomethanes above the 2L Standards. Site shallow
and deep groundwater plumes indicate chlorinated solvents are predominantly in the
shallow, unconfined water-bearing zone. Groundwater contour maps prepared for the
Linamar Forgings Site indicated a groundwater flow direction west, towards the Former
McCall Farms Property and the creek the borders the Former McCall Farms Property to
the north and west. • Nine additional sites were located on adjoining or surrounding properties within the
minimum search distances specified by the ASTM E 1527-13 standards. These site listings
included LUST Incidents, leaking above ground storage tank (LAST) Incidents, Solid
Waste Recycling facility (SWRCY), and SHWS. Based on the type of listing, distance in
relationship to the site and local topography, we do not consider these sites to be
environmental concerns connected to the subject site.

The purpose of this Phase II assessment was to evaluate soil and groundwater conditions at the site
in connection with the above referenced findings. This report summarizes the laboratory results of
soil and groundwater samples collected by McAdams at the subject site. The information obtained
from this Phase II assessment will be used to support PESA processes associated with the potential
sale and reuse/redevelopment of the subject site.

2.0 SUMMARY OF ASSESSMENT ACTIVITIES

Phase II activities were performed on February 1 and 2; and March 2, 2017. Prior to field work
being conducted, a Health and Safety Plan (HASP) was prepared by McAdams and North Carolina
811 was contacted to locate utilities to the boundaries subject site.

2.1 Geophysical Assessment

On February 1, 2017, McAdams conducted a private utility locate in order to clear large areas of
utilities where assessment activities were planned and to search for the suspect/misrepresented
500-gallon UST identified during PESA activities. Geophysical equipment used included ground penetrating radar (GPR) electromagnetic (EM) and radio-detection (RD) methods. Utilities identified during the investigation were field mapped in preparation assessment work. The 500-gallon UST was not identified. An anomalous area was, however, identified within Area E (Drawing 1.2). Based on geophysical interpretation it was believed that this area contained fill material inconsistent with what was encountered throughout the site. Metal cans of sweet potatoes were observed at the surface, and based on geophysical results, the potential presence of buried cans in this area was suspected.
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2.2 Soil Assessment

2.2.1 Test Pit Soil Assessment

On February 2, 2017, McAdams supervised Ammons Resource Group, Inc. (ARG) of Zebulon,
North Carolina excavate a total of 51 test pits on the site. Following installation a handheld Global
Positioning System (GPS) unit was utilized to locate the test pits in preparation for mapping each
pit. Insert 2.1 below summarizes the total number of test pits installed by area. Test pit locations are
depicted on Drawing 2.1. In addition to assessing soil in identified RECs, McAdams utilized test
pitting techniques in an attempt to locate the suspect/misrepresented 500-gallon UST. Similar to
geophysical assessment activities, the suspect/misrepresented 500-gallon UST was not identified
during the test pit assessment.

Insert 2.1 Test Pit Summary
Area Number of
Test Pits
Soil Sample
ID
Soil Sample
Analytical Suite*
Former AST System and 1,000-
Gallon UST Area Area A 6 N/A N/A
Boiler Room Area Area D 16 Boiler VOCs, SVOCS,
Pesticide**
Process Water Inorganic
Assessment Area Area C 11 N/A N/A
Transformer Area Area F N/A N/A N/A
Drum Storage and Debris Area Area E 12 TP-5
VOCs, SVOCs,
PCBs, RCRA
Metals, TPH
DRO/GRO,
Pesticides**
Water Chiller Area 6 N/A N/A
*Soil Sample Analytical Suite: • Volatile Organic Compounds (VOCs) using EPA Method 8260B • Semi-Volatile organic Compounds (SVOCs) using EPA Method 8270D (base neutrals and acid
extractables [BNAs]) • Resource Conservation Recovery Act (RCRA) Metals using EPA Method 6010B • TPH DRO and TPH Gasoline Range Organics (GRO) using EPA Method 8015C • Organochlorine Pesticides (Pesticides) using EPA Method 8081B
**Soil analyses for pesticides was not part of the original scope of work however was conducted on the
soil sample “Boiler” and TP-5 after the laboratory notified McAdams of preliminary results for soil sample
“Boiler” indicating the likely presence of pesticides.

Test pits were advanced utilizing a track hoe until native soils were encountered. The maximum
depth of test pit excavation was approximately 10 feet below ground surface (BLS). Soil from the
excavation bucket was field screened for the presence of potential impacts using a photoionization
(PID) and flame ionization detectors (FID) and field observations. Once screening was complete,
debris and soil was placed back into the test pit and the track hoe bucket was used to compact soils
placed back into place.

Based on field screening results (summarized in Section 4.1), a soil sample was collected from
test pit TP-104 (sample identification number “Boiler” in Area D) and TP-5 (identification number
“TP-5” in Area E). Soil samples were collected for laboratory analysis from each test pit at
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approximately 3 feet BLS. Soil samples were placed into laboratory-supplied containers, packed
into an ice-filled cooler, and transported under chain-of-custody from the subject site to Prism
Laboratories, Inc. (Prism) in Charlotte, North Carolina by BeaveEx delivery service. Soil samples
were analyzed for the analyte list summarized in Insert 2.1 above.

The test pit soil sample laboratory report is provided in Appendix A. Test pit field screening and soil
sample results are discussed in Section 4.1.1 of this report.

2.2.2 Soil Boring Assessment

On March 1, 2017, a total of four soil borings (B-1 through B-4) were advanced at the site in the
vicinity of the former onsite transformers to assess Area F. Similar to test pits, soil borings were
located using a handheld GPS unit. Soil boring locations are depicted on Drawing 2.2. Insert 2.2
below summarizes the total number of boring installed in Area F.

Insert 2.2 Soil Boring Summary
Area Number
of Borings Soil Sample ID Soil Sample Analytical
Suite*
Former Transformer Area Area F 4 B-4 VOCs, SVOCs and PCBs
*Soil Sample Analytical Suite: • VOCs using EPA Method 8260B • SVOCs using EPA Method 8270D (BNAs) • PCBs using EPA Method 8082A
Soil borings were advanced by Quantex, Inc. (Quantex) located in Raleigh, North Carolina utilizing a track mounted Geoprobe® direct push drilling rig to approximately 7 feet BLS. Direct-push drilling services were supervised by McAdams. Soil core was collected using five-foot, two-inch diameter, macro-core samplers. Soil core was logged and screened for the presence of potential impacts using a PID and field observations. One soil sample was collected for laboratory analysis from soil boring location B-4 at approximately 4 to 6 feet BLS. Soil sample B-4 was placed into laboratory-supplied containers, packed into an ice-filled cooler, and transported under chain-of-custody from the subject site to Prism in Charlotte, North Carolina by BeaveEx delivery service. Soil sample B-4 was analyzed for the analyte list summarized in Insert 2.2 above. The soil boring sample laboratory report is provided in Appendix A. Soil sample results are discussed in Section 4.1.2 of this report. 2.3 Groundwater Assessment On March 1, 2017, McAdams supervised Quantex in its installation of Type II temporary monitoring wells TW-1 through TW-6 utilizing a track mounted Geoprobe® rig affixed with solid-stem augers. Prior to installing wells, McAdams submit an application to construct monitoring wells on the site with the NCDEQ. Permission was granted for the installation of six wells under NCDEQ permit number WM0501217. The Monitoring Well Construction Permit is included as Appendix C. A summary of the temporary wells installed on the site is included in Insert 2.3 below. Temporary well locations are depicted on Drawing 2.2.
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Insert 2.3 Temporary Wells Summary
Area Temporary
Well Groundwater Analytical Suite*
Former AST System and 1,000-
Gallon UST Area Area A TW-6 VOCs, Cl-, NH3, N, NO3 as N, TDS,
SO4, SVOCs
Boiler Room Area Area D TW-2 VOCs, Cl-, NH3, N, NO3 as N, TDS,
SO4, PCBs
Transformer Area Area F TW-1 VOCs, Cl-, NH3, N, NO3 as N, TDS,
SO4, PCBs
Drum Storage and Debris Area Area E TW-5 VOCs, Cl-, NH3, N, NO3 as N, TDS,
SO4
Water Chiller Area TW-4 VOCs, Cl-, NH3, N, NO3 as N, TDS,
SO4
Beneath the Former Building Footprint TW-3 VOCs, Cl-, NH3, N, NO3 as N, TDS,
SO4
*Groundwater Sample Analytical Suite: • VOCs using EPA Method 6200B • Chloride (Cl-)using EPA Method 9056 • Ammonia (NH3) and nitrogen (N) using EPA Method 350.1 • Nitrate (as NO3) as nitrogen (N) using EPA Method 9056 • Total dissolved solids (TDS) using EPA Method 2540C • Total Sulfate (SO4) using EPA Method 9056 • PCBs using EPA Method 8082A • SVOCs using EPA Method 625 (BNAs)

Borings were advanced to 20 feet BLS. Soil cuttings were field screened using a PID/FID for
evidence of total volatile organic compounds for health and safety purposes and to identify possible
evidence of gross pollution conditions. Temporary wells were constructed using 15 foot sections of
Schedule 40 PVC slotted 0.010-inch well screen and 1-inch diameter Schedule 40 PVC riser pipe to
surface. Annular space around the well was backfilled with sand pack to at least one foot above the
well screen and hydrated bentonite to the land surface. Monitoring well construction records are
presented in Appendix B.

On March 2, 2017, McAdams returned to the site to collect groundwater samples. A water level
measurement was collected from each temporary monitoring well using a decontaminated water level
meter. Following water level collection, three to five well volumes were purging from each temporary
well using a peristaltic pump with dedicated tubing. Groundwater was then decanted directly from
the dedicated tubing into laboratory-supplied containers, packed into an ice-filled cooler, and
transported under chain-of-custody from the subject site to Prism in Charlotte, North Carolina by
BeaveEx delivery service. Groundwater samples were analyzed for the analyte list summarized in
Insert 2.3 above.

The groundwater sample laboratory report is provided in Appendix A. Groundwater sample results
are discussed in Section 4.2 of this report.

2.4 Abandonment and Site Clean-up

Temporary monitoring wells (TW-1 through TW-6) were abandonment in accordance with 15A
NCAC 02C .0100 as documented in the Well Abandonment Records presented in Appendix C.
Borings B-1 through B-4 were backfilled with bentonite chips to surface.
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Because evidence of gross pollution was not observed using field screening techniques, soils and
groundwater (i.e. investigation-derived waste [IDW]) from field assessment activities were spread
on the ground in accordance with NCDEQ guidelines.

3.0 PHYSICAL SITE CHARACTERISTICS

3.1 Topography and Surface Water Drainage

According to United States Geological Survey (USGS) Topographic Quadrangle of Wilson, North
Carolina site elevations range from approximately 90 to 100 feet above mean sea level (Drawing
1.1). Based on topography, surface drainage is expected to flow northwest in the north portion of the
site, and south in the southern portion of the site.

3.2 Site Geology

According to the North Carolina Geological Survey Section of the North Carolina Department of
Natural Resources and Community Development Geology of North Carolina (1985) map the site is
located in the Inner Coastal Plain Province. This province is characterized by stratified sequences
of clays, sand, gravel, and fossil shell layers. Limestone is encountered at depth.

According to the 2013 LSA (EAC), soils in the former UST Area (Area B) consisted of brown silty
sand from land surface to 8 feet BLS. An orange to tan course grained sand was encountered between
10 to 14 feet BLS, beneath which an orange silty clay was encountered at approximately 16 feet
BLS. Soil borings installed as part of this Phase II assessment confirmed these results, however, fill
materially was generally encountered directly below ground surface at depths ranging between 0 to
6 feet BLS.

3.3 Site Hydrogeology

Groundwater elevations and flow directions are site specific. Groundwater flow direction generally
mimics the overlying site topography, flowing from higher to lower land surface elevations. Site-
specific groundwater flow direction can be influenced by impermeable surfaces, the proximity of
nearby drainage features, sinkholes, creeks, swamps, and pumped groundwater wells. Fractures,
joints, bedding planes and other discontinuities in the underlying rock can also affect the
groundwater conditions.

The 2013 LSA (EAC) indicated groundwater was encountered between 12 and 14 feet BLS in Area
B. Groundwater in temporary wells installed as part of this Phase II assessment was encountered
between 11.5 and 14 feet BLS. Based on our limited review of topography and water features, there
is the potential that groundwater flows in multiple directions. The northern portion of the site may
flow to the northwest towards a tributary located along the north and west property boundary. As
documented in the 2013 LSA performed by EAC groundwater in the former UST Area (Area B), located in the southern portion of the site, flows south towards a tributary located to the southeast of the site. 4.0 ASSESSMENT RESULTS The following subsections summarize the test pit field screening and analytical results for soil and groundwater samples collected in association with this Phase II assessment. Laboratory analytical reports and chain-of-custody records for samples collected in conjunction with this Phase II assessment are provided in Appendix A. Table 4.1 provides a summary of soil sample laboratory
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test results compared to the NCDEQ UST Section Action Levels and the NCDEQ Preliminary Site
Remediation Goals (PSRGs). Groundwater analytical results compared to the 2L Standards and the
NCDEQ Division of Waste Management (DWM) Vapor Intrusion Commercial and Residential
Groundwater Screening Levels (VI GWSLs) are summarized in Table 4.2.

4.1 Soil Assessment and Analytical Results

Results of the test pit field screening are summarized as follows:
• Soil staining and petroleum odors were observed in sub-base gravel and soil in 3 of the 16 test pits installed in the former boiler room area (Area D). One soil sample (Boiler) was collected from test pit TP-104. • Soil staining and petroleum odors were observed in soil from 4 of 6 test pits within the former UST/AST area (Area A) near the former facility weigh station. No soils samples were collected for laboratory analysis. • Possible soil impacts were observed in test pit 5 (TP-5) installed in the vicinity of a former loading dock in Area E. One soil sample (TP-5) was collected from test pit TP-5. • No obvious impacts were observed in the field in soil from the remaining test pits. Soil samples collected from test pits TP-104 and TP-5 (sample identification numbers “Boiler” and “TP-5”, respectively) and soil boring B-4 (sample identification number B-4) were analyzed in accordance with the analyte list summarized in Inserts 2.1 and 2.2 (see Sections 2.2.1 and 2.2.2). A summary of the soil analytical results is presented in Table 4.1. A summary of the soil analytical results by Area is provided in Insert 4.1 below. Insert 4.1 Soil Analytical Results Summary
Area Sample
ID
Analytical
Suite Results
Area
D Boiler
VOCs
• Estimated (J) concentrations of acetone and methyl ethyl ketone (MEK)
below the PSRGs.
• Concentrations of petroleum compounds: 1,2,4-trimethylbenzene (LL),
1,3,5-trimethylbenzene, 4-isopropyltoluene, cumene, ethylbenzene, n-
butylbenzene, sec-butylbenzene, tert-butylbenzene, toluene, xylenes (m,p-
and o-), and total xylenes below the PSRGs.
• Concentration of naphthalene above the below the Protection of Groundwater
PSRGs.
SVOCs • Concentrations of 2-methylnaphthalene and polyaromatic hydrocarbons:
fluorene, phenanthrene and pyrene below the PSRGs.
Organochlorine
Pesticides
• Concentration of chlordane above the PSRGs.
• Concentrations of cis-chlordance (A), trans-chlordane (Aa) and heptachlor
above the Unrestricted Use Health and Protection of Groundwater PSRGS.
• Concentration of endosulfan II below the PSRGs.
Area
E TP-5
VOCs • Estimated concentrations of acetone, MEK, and naphthalene below the
PSRGs.
SVOCs • No detectable concentrations above the MDL.
Metals
• Detectable concentrations of total barium and lead below the PSRGs.
• Detectable concentration of total arsenic above the Unrestricted Use Health
based PSRG.
• Total chromium* concentration reported above the PSRGs for hexavalent
chromium, but below the PSRGs for trivalent chromium.
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Area Sample
ID
Analytical
Suite Results
Organochlorine
Pesticides • No detectable concentrations above the MDL.
TPH
DRO/GRO • No detectable concentrations above the MDL.
Area
F B-4
VOCs • Estimated (J) concentrations of petroleum compounds 1,2-dichlorobenzene
and toluene below the PSRGs.
SVOCs • No detectable concentrations above the MDL.
PCBs • No detectable concentrations above the MDL.
Notes:
• “J” flagged concentrations are estimated concentrations reported between the method detection limit (MDL) and
reporting limit (RL)
• “LL” flagged concentrations are medium level analysis results below the RL. Low level analysis reported
estimated above the calibration range.
• “A” flagged concentrations represent concentrations with relative percent difference (RPD) values exceeding the
MDL due to an incomplete patter. The result should be considered as an estimated concentration.
• “Aa” flagged concentrations represent concentrations where midrange continuing calibration verification
standards (CCVs) are analyzed in order to verify that the calibration of the analytical system is still acceptable.
• The NCDEQ does not have a PSRG for total chromium. Rather PSRGs for chromium are broken up between
the isotopic variations of chromium that are present in the environment – trivalent chromium and hexavalent
chromium.

4.1 Groundwater Analytical Results

Groundwater samples (TW-1 through TW-6) were analyzed in accordance with the analyte list
summarized in Insert 2.3 (see Section 2.2.3). A summary of the groundwater analytical results is
presented in Table 4.2. A summary of the groundwater analytical results by Area is provided in
Insert 4.2 below.

Insert 4.2 Groundwater Analytical Results Summary
Area Sample
ID
Analytical
Suite Results
Area A TW-6
Inorganic
Compounds
• Concentrations of ammonia as nitrogen, sulfate, nitrate as nitrogen,
chloride and TDS below the 2L Standards.
VOCs
• Estimated (J flagged) concentration of acetone below the 2L Standards.
• Concentrations of petroleum compounds: n-butylbenzene, sec-
butylbenzene, ethylbenzene, cumene, 4-isopropyltoluene, isopropyl ether,
n-propylbenzene, toluene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, xylenes (m,p- and o-), and total xylenes below the 2 L
Standards.
• Concentrations of benzene, methyl-tert-butyl ether (MTBE) and
naphthalene above the 2L Standards.
SVOCs
• Estimated (J flagged) concentration of 1-methylnaphthalene.
• Concentration of 2-methylnaphthalene below the 2L Standards.
• Concentration of naphthalene above the 2L Standards.
Area D TW-2
Inorganic
Compounds
• Concentrations of nitrate/nitrite as nitrogen, total nitrogen, sulfate, nitrate
as nitrogen, chloride and TDS below the 2L Standards.
VOCs • No detectable concentrations above the MDL.
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Area Sample
ID
Analytical
Suite Results
Area F TW-1
Inorganic
Compounds
• Concentrations of nitrate/nitrite as nitrogen, sulfate, nitrate as nitrogen,
chloride and TDS below the 2L Standards.
VOCs • Concentration of trihalomethane compound - chloromethane – below the
2L Standard.
PCBs • No detectable concentrations above the MDL.
Area E TW-5
Inorganic
Compounds
• Concentrations of nitrate/nitrite as nitrogen, nitrate as nitrogen, chloride
and TDS below the 2L Standards.
VOCs
• Concentration of tetrachloroethylene below the 2L Standards.
• Concentrations of trihalomethanes: bromoform, bromodichloromethane,
chloroform, and dibromochloromethane above the 2L Standards.
Water
Chiller
Area
TW-4
Inorganic
Compounds
• Concentrations of nitrate/nitrite as nitrogen, total nitrogen, ammonia as
nitrogen, sulfate, nitrate as nitrogen, chloride and TDS below the 2L
Standards.
VOCs
• Estimated (J flagged) concentration of acetone below the 2L Standards.
• Concentration of trihalomethanes: bromochloromethane, bromoform,
chloroform, and dibromomethane below the 2L Standards.
• Concentrations of trihalomethanes: bromodichloromethane and
dibromochloromethane above the 2L Standards.
Beneath
Building
Footprint
TW-3 Inorganic
Compounds
• Concentrations of nitrate/nitrite as nitrogen, total nitrogen, sulfate, nitrate
as nitrogen, chloride and TDS below the 2L Standards.
VOCs • No detectable concentrations above the MDL.
Notes:
• “J” flagged concentrations are estimated concentrations reported between the method detection limit (MDL) and
reporting limit (RL)

5.0 FINDINGS AND CONCLUSIONS

Based on the results of this Phase II Assessment McAdams offers the following findings and
conclusions:

Soil Assessment

The Phase II soil assessment included excavation of 51 test pits and the installation of four soil
borings in areas where RECs were identified onsite. Soils were screened for evidence of impact,
and soil samples were collected from two test pits and one soil boring. Below is a summary of the
soil assessment field screening and laboratory analytical results:
• Area A: Petroleum impacted soil was observed using field screening techniques in soil from
4 of 6 test pits within the former UST/AST system area in Area A. Observed impacts
appeared to be consistent with residual impact associated with the NFA status and NORP
associated with a UST release in this area. McAdams did not observe evidence of gross
pollution conditions or the presence of a new release. No soil samples were collected for
laboratory analysis. • Area B: Field screening and laboratory test results indicated impacts that are consistent with
residual petroleum associated with the former UST system release in Area B. No evidence
of new significant releases (i.e. beyond de minimis conditions) were observed. This
information is consistent with the NFA and NORP issued for the release incident onsite.
Phase II Environmental Site Assessment Report May 18, 2017
2202 Charleston Street Page 11
Wilson, North Carolina
• Area C: No soil impacts related to the presence of chloride, sulfate, nitrate (as nitrogen),
ammonia and TDS were observed in test pits installed in the former Inorganic
Compound/Processing Area. No soils samples were collected for laboratory analysis. • Area D: Petroleum impacts were observed in soil from 3 of the 16 test pits installed in the
former boiler room area in Area D. A soil sample was collected from test pit TP-104 in Area
D and submitted for laboratory analyses. Results of the laboratory analysis revealed the
presence petroleum related compounds most notable naphthalene above regulatory
standards. The presence of petroleum related compounds is likely due to leaks associated
with the boiler and heating oil UST systems located in Area B. Soil analyses for pesticides
was not part of the original scope of work, but was conducted on the soil sample collected
from test pit TP-104 after the laboratory notified McAdams of preliminary results indicating
the likely presence of pesticides. Several organochlorine pesticides were reported above the
PSRGs in the soil sample collected in the boiler room. Pesticides were likely used onsite to
control pests from fouling food products. • Area E: Evidence of possible soil impacts was observed in TP-5 installed near a former
loading dock in Area E. Analysis of a soil sample from the test pit indicated low levels of
petroleum below regulatory standards. Total chromium was also identified in soil at this
location with concentrations that were reported above the hexavalent chromium PSRGs, but
below the associated trivalent chromium PSRGs (the laboratory method is unable to speciate
between trivalent and hexavalent chromium). Based on the historical use of the property as
a sweet potato processing and canning facility, it is unlikely that hexavalent chromium was
utilized on the property. Detected total chromium concentrations are likely representative of
the less toxic trivalent chromium which can also be naturally occurring in soils. The presence
of hexavalent chromium can, however, be confirmed through additional analysis. • Area F: Soil collected from boring B-4, installed in the former transformer area (Area F),
did not indicate the presence of PCBs. • Unaccounted 500-gallon UST: Geophysical and test pit assessment techniques were
unsuccessful in locating the suspect/misrepresented 500-gallon UST. Based on the results
of this assessment, the 500-gallon UST is believed to have been misrepresented as the 1,000-
gallon gasoline UST that was closed in-place in Area A. • Site-Wide: No obvious impacts were observed in soil from remaining test pits installed
onsite. No evidence of new releases/sources of impact were identified.

Groundwater Assessment

A total of six temporary monitoring wells were installed and sampled in areas identified as RECs
across the site. Groundwater samples were collected from each temporary well. Below is a
summary of the groundwater assessment laboratory analytical results:
• Area A: Petroleum impacts were detected in groundwater collected from temporary well
TW-6 that was installed in Area A (the former UST/AST System location). The
concentrations of detected constituents were similar to previous groundwater test results performed by others for this area and the test pit observations described above. These data results further support that petroleum impacts are consistent with the NFA status and NORP issued by the NCDEQ for the abandoned in place 1,000-gallon UST. No obvious evidence of gross pollution conditions or indications of a new release were identified in Area A. • Area D: Temporary monitoring well TW-2 was installed in the area of stained soil at the location of the former boiler room. Although soil results indicated the presence of residual petroleum, groundwater collected from temporary well TW-2 did not indicate the presence of petroleum impacts in groundwater. As noted in the soil assessment results, several organochlorine pesticides were detected in soil above the PSRGs in the soil sample collected
Phase II Environmental Site Assessment Report May 18, 2017
2202 Charleston Street Page 12
Wilson, North Carolina

in the former boiler room. Additional groundwater sampling and analysis would be required
to confirm the presence or absence of pesticides in groundwater. • Area E and Water Tank/Chiller Area: Groundwater collected from temporary monitoring
wells TW-4 and TW-5, installed near the former water tank/chiller area (TW-4) and adjacent
to Test Pit TP-5 in Area E (TW-5), respectively, indicated the detection of several
trihalomethane compounds above the 2L Standards. The presence of these compounds in
groundwater could be sourced from historical onsite water use. Tetrachloroethylene was also
detected in groundwater collected in TW-5 (near TP-5) but the reported concentration was
below the associated 2L Standard. The presence of this constituent onsite could be due to the
potential unreported use of this cleaning solvent on former process equipment cleaning, or it
could be due to the offsite chlorinated solvent plume identified on the upgradient Linamar
Forgings/Carolina Forge property. The constituents reported in groundwater collected from
TW-5 were not identified in the soil sample collected in test pit TP-5. Soil samples were not
collected from the water tank/chiller area. • Area F: PCBs were not identified in groundwater collected adjacent to the former
transformer area in Area F. • Unaccounted 500-gallon UST: The groundwater assessment performed onsite did not
indicate the presence of an unknown/additional source of petroleum. This information is
consistent with geophysical and test pit assessment results. • Site-Wide: Outside of the presence of trihalomethanes in groundwater near the water
tank/chiller area, no evidence of new non-petroleum related impacts was identified in site
groundwater. Additionally, analysis of groundwater samples for commons inorganic
compounds found in food preservatives did not indicate the presence of analytes above
applicable 2L Standards.

General Conclusions and Recommendations
• Overall the findings of the Phase II assessment were consistent with previous assessment
results. McAdams did not find evidence of gross pollution conditions in soil or groundwater
or evidence of significant unidentified sources of impact. • In accordance with regulatory requirements, the detection of pesticides in soil; and, inorganic
compounds, trihalomethanes and chlorinated solvent in groundwater are reportable.
Reporting requirements associated with these compounds can be managed under the North
Carolina Brownfields Program. • The risk associated with the detection of impacts identified in the Phase II and those
historically detected at the site in previous investigations can effectively be managed under
the North Carolina Brownfields Program.

6.0 REFERENCES

Duncklee and Dunham, P.C. (D&D), Report of Phase I Environmental Site Assessment McCall
Farms Facility, Wilson, North Carolina, April 7, 2016.

D&D, Letter Report for Phase II Environmental Site Assessment, McCall Farms Facility, Wilson,
North Carolina, May 9, 2016.

EAC, Phase II Environmental Site Assessment – Bruce Foods Plant – 2202 Charleston Street SE,
Wilson, Wilson County, North Carolina, November 26, 2013.

EAC, LSA & Tank Closure with No Further Action – Bruce Foods Plant – 2202 Charleston Street
SE, Wilson, Wilson County, North Carolina, December 12, 2013.
Phase II Environmental Site Assessment Report May 18, 2017
2202 Charleston Street Page 13
Wilson, North Carolina

EAC, Petroleum Contaminated Soil Removal/Excavation – McCall Farms, Inc. (Former Bruce
Foods Plant) – 2202 Charleston Street SE, Wilson, Wilson County, North Carolina,
February 13, 2014.

GHD, Remedial Investigation (RI) Work Plan, Former Carolina Forge Company d/b/a Linamar
Forgings, Wilson, Wilson County, North Carolina, NCD982084113 – Docket NO. 16.-SF-
401, March 2, 2016.

McAdams, Phase I Environmental Site Assessment Report, Former McCall Farms / Bruce Foods
Property, 2202 Charleston Street SE, Wilson, North Carolina, May 18, 2017.

North Carolina Geologic Survey, Geologic Map of North Carolina, 1985.

DRAWINGS
Historical Topo Map
page
SITE NAME:
ADDRESS:
CLIENT:
This report includes information from the
following map sheet(s).
-
EW
SW S SE
NW N NE
2013
0 Miles 0.25 0.5 1 1.5
Kemira PESA
2202 CHARLESTON ST SE
WILSON, NC 27893
The John R. McAdams Co., Inc.
TP, Wilson, 2013, 7.5-minute
E, Saratoga, 2013, 7.5-minute
4762631 4 5
!(
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#*
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TP-200
TP-201
TP-203
TP-202
TP-204
TP-205
TP-13
TP-18
TP-110
TP-102
TP-12
TP-13TP-14TP-15
C H A R L E S T O N S T
TP-9
TP-8
TP-7
TP-6 TP-5
TP-4
TP-3
TP-2
TP-1
TP-17
TP-16
TP-15
TP-14
TP-12
TP-11
TP-10
TP-406
TP-405
TP-404
TP-403
TP-402
TP-401
TP-400
TP-303
TP-302
TP-301
TP-300
TP-111
TP-109
TP-108
TP-107
TP-106
TP-105
TP-104/BOILER
TP-103TP-101
TP-100
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
0 752550Feet1 inch = 75 feet$LEGEND
!(TEST PIT LOCATION
#*TEST PIT SOIL SAMPLE LOCATION
DRAWING 2.1 - TEST PIT LOCATION AND SOIL SAMPLE MAPPHASE II ENVIRONMENTAL SITE ASSESSMENT2202 CHARLESTON STREETWILSON, NORTH CAROLINA
X:\Projects\SPEC\SPEC-16961\GIS\2017-04-18_SPEC16961_Drawing 2.1.mxd, 4/19/2017 10:27:43 AM, roth
4/19/2017
KR
SPEC-16961
DATE:
JOB NO:
DRAWN BY:
DRAFT CHECK:
APPROVAL:JT
SG
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B-2
B-1
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TW-6
TW-4
TW-3
TW-2
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
0 752550Feet1 inch = 75 feet$LEGEND
!(SOIL BORING LOCATION
#*SOIL SAMPLE LOCATION
@A TEMPORARY MONITORING WELL ANDGROUNDWATER SAMPLE LOCATION
DRAWING 2.2 - BORING LOCATION AND SOIL/GROUNDWATER SAMPLE SUMMARY MAPPHASE II ENVIRONMENTAL SITE ASSESSMENT2202 CHARLESTON STREETWILSON, NORTH CAROLINA
X:\Projects\SPEC\SPEC-16961\GIS\2017-04-18_SPEC16961_Drawing 2.2.mxd, 4/18/2017 11:47:27 AM, roth
4/18/2017
KR
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DATE:
JOB NO:
DRAWN BY:
DRAFT CHECK:
APPROVAL:JT
SG

TABLES
TP-5 Boiler Trans - B4
Sample Date 2/2/2017 2/2/2017 3/1/2017
Gasoline Range Organics (GRO)ND NA NA 50
Diesel Range Organics (DRO)ND NA NA 100
cis-Chlordane NA 2.8 NA 1.7 7.7 0.14
Chlordane ND 20 A NA 1.7 7.7 0.14
trans-Chlordane ND 3.7 Aa NA 1.7 7.7 0.14
Endosulfan II ND 0.11 NA 94 1400 5.6
Haptachlor ND 0.25 NA 0.13 0.63 0.0066
Arsenic 2.3 NA NA 0.68 3.0 5.8
Barium 14 NA NA 3000 44000 580
Chromium^^14^^NA NA 24000 (0.3)100000 (6.3)360000 (3.8)
Lead 6.7 NA NA 400 800 270
1,2,4-Trimethylbenzene ND 0.22 LL ND 11.6 48 6.7
1,3,5-Trimethylbenzene ND 0.24 ND 156 182 6.7
4-Isopropyltoluene ND 0.059 ND NL NL 0.68
Acetone 0.0095 J 0.027 J 1.6 12200 100000 24
Cumene ND 0.042 ND 268 268 1.3
1,2-Dichlorobenzene ND ND 0.0021 J 360 376 0.24
Ethylbenzene ND 0.25 ND 5.8 25 8.1
Methyl Ethyl Ketone (MEK)0.0030 J 0.0056 J ND 5400 28400 16
Naphthalene 0.0029 J 1.3 ND 3.8 17 0.21
n-Butylbenzene ND 0.55 ND 108 108 2.4
sec-Butylbenzene ND 0.47 ND 145 145 2.2
tert-Butylbenzene ND 0.022 ND 183 183 1.7
Toluene ND ND 0.0021 J 818 818 5.5
m,p-Xylenes ND 0.058 ND 110 388 NL
o-Xylene ND 0.0086 ND 130 434 NL
Xylenes, total ND 0.067 ND 116 260 6.1
2-Methylnaphthalene ND 2.1 ND 48 600 1.6
Fluorene ND 2.0 ND 480 6000 56
Phenanthrene ND 4.3 ND NL NL 68
Pyrene ND 1.0 ND 360 4600 220
All Aroclors for this Method NA NA ND
Notes:
ppm - parts per million
mg/kg - milligrams per kilogram dry units
NCDEQ DWM UST Section Action Level - North Carolina Department of Environmental Quality, Division of Waste Management, Underground Storage Tank Action Level
PSRG - Preliminary Soil Remediation Goals (October 2016 Inactive Hazardous Sites Branch - IHSB)
ND - Not detected above laboratory detection limit
NL - No standard listed for this analyte
Bold - Indicates exceedance of Unrestricted Use Health Based PSRG or NCDEQ DWM UST Section Action Level
Underlined - Indicates exceedance of Industrial/Commercial Health Based PSRG
Shaded - Indicates exceedance of Protection of Groundwater PSRG
Laboratory Qualifiers:
Aa - The CCV* is above method limits. Result reported with possible high bias
J - Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
A - The RPD value exceeded method limits due to incomplete pattern. The result should be considered as an estimated concentration.
LL - Medium level analysis result below the RL. Low level analysis reported estimated above the calibration range.
*CCV - Continuing calibration verification standards (CCVs) are midrange standards that are analyzed in order to verify that the calibration of the analytical system is still acceptable.
Volatile Organic Compounds (EPA Method 8260B) in mg/kg
NA - Not analyzed for this method
^^Chromium detections are not spectated between total chromium and hexavalent chromium. Both standards are listed in table above. The value in parenthesis indicates the hexavalent chromium standard
Semi-volatile Organic Compounds (EPA Method 8270D) in mg/kg
Poly Chlorinated Biphenyls by Aroclor (EPA Method 8082A) in mg/kg
Organochlorine Pesticides (EPA Method 8081B) in mg/kg
Metals (EPA Method 6010B) in mg/kg
MCADAMS PROJECT NO. SPEC-16961
Sample ID
Unrestricted Use
Health Based
PSRG
Industrial/
Commercial Health
Based PSRG
Protection of
Groundwater
PSRG
Analyte
Total Petroleum Hydrocarbons (EPA Method 8015C) in ppm
NCDEQ DWM
UST Section Action
Level (ppm)
TABLE 4.1
SUMMARY OF LABORATORY DETECTIONS - SOIL SAMPLES
McCALL FARMS - 2202 CHARLESTON STREET
WILSON, NORTH CAROLINA
Regulatory Standards
Regulatory Standards
TW-1 TW-2 TW-3 TW-4 TW-5 TW-6 15A NCAC 02L .0202
(April 1, 2013)
Nitrate/Nitrite as N 0.52 2.0 ND 6.8 8.6 ND 10
Total Nitrogen ND 2.0 ND 6.8 ND ND NL
Ammonia as N ND ND 0.15 0.21 ND 0.20 NL
Sulfate 7.8 85 3.6 3.8 ND 3.2 250
Nitrate as N 0.48 2.0 ND 6.7 8.6 0.12 10
Chloride 47 51 9.1 76 100 11 250
Total Dissolved Solids (TDS)120 240 74 250 310 110 500
Acetone ND ND ND 5.1 J ND 9.8 J 6000
Benzene ND ND ND ND ND 56 1
Bromochloromethane ND ND ND 0.68 ND ND NL
Bromodichloromethane ND ND ND 0.87 14 ND 0.6
Bromoform ND ND ND 3.3 9.0 ND 4
n-Butylbenzene ND ND ND ND ND 1.8 70
sec-Butylbenzene ND ND ND ND ND 2.5 70
Chloroform ND ND ND 8.4 90 ND 70
Chloromethane 0.56 ND ND ND ND ND 3
Dibromochloromethane ND ND ND 1.9 8.9 ND 0.4
Dibromomethane ND ND ND 6.1 ND ND NL
Ethylbenzene ND ND ND ND ND 80 600
Isopropylbenzene (Cumene)ND ND ND ND ND 12 70
Isopropyl Ether ND ND ND ND ND 8.1 70
4-Isopropyltoluene ND ND ND ND ND 0.73 NL
Methyl-tert-Butyl Ether ND ND ND ND ND 50 20
Naphthalene ND ND ND ND ND 77 6
n-Propylbenzene ND ND ND ND ND 18 70
Tetrachloroethylene ND ND ND ND 0.58 ND 0.7
Toluene ND ND ND ND ND 2.8 600
1,2,4-Trimethylbenzene ND ND ND ND ND 200 400
1,3,5-Trimethylbenzene ND ND ND ND ND 1.9 400
m,p-Xylenes ND ND ND ND ND 23 500
o-Xylene ND ND ND ND ND 1.4 500
Xylenes, total ND ND ND ND ND 24 500
1-Methylnaphthalene NA NA NA NA NA 8.7 J NL
2-Methylnaphthalene NA NA NA NA NA 12 30
Naphthalene NA NA NA NA NA 31 6
All compounds for method ND NA NA NA NA NA
Notes:
mg/L - milligrams per liter
ug/L - micrograms per liter
Shaded - Indicates exceedance of 15A NCAC 02L .0202 North Carolina Groundwater Standard
J - Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
ND - Not detected above laboratory detection limit
NA - Not analyzed for this method
PCBs (EPA Method 8082A) in ug/L
MCADAMS PROJECT NO. SPEC-16961
TABLE 4.2
SUMMARY OF LABORATORY DETECTIONS - GROUNDWATER SAMPLES
MARCH 2, 2017
McCALL FARMS - 2202 CHARLESTON STREET
WILSON, NORTH CAROLINA
Sample ID
Analyte
Nitrate/Nitrite as N (EPA Method 300.0) in mg/L
Volatile Organic Compounds (EPA Method 6200B) in ug/L
Semi-Volatile Organic Compounds (EPA Method 625) Including Base Neutrals and Acid Extractables in ug/L
Ammonia and Nitrogen (EPA Method 350.1) in mg/L
Total Dissolved Solids - TDS (EPA Method 2540C) in mg/L
EPA Method 9056A in mg/L

APPENDIX A

LABORATORY ANALYTICAL REPORTS AND
CHAIN-OF-CUSTODY RECORD
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
02/13/2017
McAdams (John R.) Company, Inc.
Jeff Tyburski
2905 Meridian Pkwy
Durham, NC 27713
Project: McCall Farms (Wilson, NC)
Lab Submittal Date: 02/03/2017
Prism Work Order: 7020076
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A The RPD value exceeded method limits due to incomplete pattern. The result should be considered as an
estimated concentration.
Aa The RPD value exceeded method limits due to possible co-eluting peaks on secondary column. The result should
be considered as an estimated concentration.
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
LL Medium level analysis result below the RL. Low level analysis reported estimated above the calibration range.
M Matrix spike outside of the control limits.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 41
Sample Receipt Summary
02/13/2017
Prism Work Order: 7020076
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7020076-01 02/02/17TP-5 02/03/17Solid
7020076-02 02/02/17BOILER 02/03/17Solid
Samples were received in good condition at 1.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 41
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7020076
02/13/2017
Summary of Detections
2.3 mg/kg dry7020076-01 TP-5 Arsenic *6010D
14 mg/kg dry7020076-01 TP-5 Barium *6010D
14 mg/kg dry7020076-01 TP-5 Chromium *6010D
6.7 mg/kg dry7020076-01 TP-5 Lead *6010D
0.0095 J mg/kg dry7020076-01 TP-5 Acetone 8260B
0.0030 J mg/kg dry7020076-01 TP-5 Methyl Ethyl Ketone (2-Butanone)8260B
0.0029 J mg/kg dry7020076-01 TP-5 Naphthalene 8260B
2.8 mg/kg dry7020076-02 BOILER cis-Chlordane 8081B
20 A mg/kg dry7020076-02 BOILER Chlordane 8081B
0.11 mg/kg dry7020076-02 BOILER Endosulfan II 8081B
3.7 Aa mg/kg dry7020076-02 BOILER trans-Chlordane 8081B
0.25 mg/kg dry7020076-02 BOILER Heptachlor 8081B
2.1 mg/kg dry7020076-02 BOILER 2-Methylnaphthalene 8270D
2.0 mg/kg dry7020076-02 BOILER Fluorene 8270D
4.3 mg/kg dry7020076-02 BOILER Phenanthrene 8270D
1.0 mg/kg dry7020076-02 BOILER Pyrene 8270D
0.22 LL mg/kg dry7020076-02 BOILER 1,2,4-Trimethylbenzene 8260B
0.059 mg/kg dry7020076-02 BOILER 4-Isopropyltoluene 8260B
0.027 J mg/kg dry7020076-02 BOILER Acetone 8260B
0.042 mg/kg dry7020076-02 BOILER Isopropylbenzene (Cumene)8260B
0.058 mg/kg dry7020076-02 BOILER m,p-Xylenes 8260B
0.0056 J mg/kg dry7020076-02 BOILER Methyl Ethyl Ketone (2-Butanone)8260B
0.17 mg/kg dry7020076-02 BOILER n-Butylbenzene 8260B
0.0086 mg/kg dry7020076-02 BOILER o-Xylene 8260B
0.022 mg/kg dry7020076-02 BOILER tert-Butylbenzene 8260B
0.067 mg/kg dry7020076-02 BOILER Xylenes, total 8260B
0.24 mg/kg dry7020076-02 BOILER 1,3,5-Trimethylbenzene 8260B
0.25 mg/kg dry7020076-02 BOILER Ethylbenzene 8260B
1.3 mg/kg dry7020076-02 BOILER Naphthalene 8260B
0.55 mg/kg dry7020076-02 BOILER n-Butylbenzene 8260B
0.47 mg/kg dry7020076-02 BOILER sec-Butylbenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: TP-5
Prism Sample ID: 7020076-01
Prism Work Order: 7020076
Time Collected: 02/02/17 20:00
Time Submitted: 02/03/17 15:15
Diesel Range Organics by GC/FID
BRL *8015C P7B011517.8 2/7/17 18:13 ZRCmg/kg dry 3.0Diesel Range Organics
Surrogate Recovery Control Limits
49-12472 %o-Terphenyl
Gasoline Range Organics by GC/FID
BRL *8015C P7B0145504.7 2/8/17 21:03 ANGmg/kg dry 0.70Gasoline Range Organics
Surrogate Recovery Control Limits
50-137107 %a,a,a-Trifluorotoluene
General Chemistry Parameters
88.8 *SM2540 G P7B010910.100 2/6/17 15:03 JLR% by
Weight
0.100% Solids
Organochlorine Pesticides by GC/ECD
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCCCVmg/kg dry 0.000264,4'-DDD
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCCCVmg/kg dry 0.000404,4'-DDE
BRL 8081B P7B016910.0034 2/9/17 16:08 JMCCCVmg/kg dry 0.000924,4'-DDT
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00058Aldrin
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00066alpha-BHC
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00051cis-Chlordane
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00049beta-BHC
BRL 8081B P7B016910.056 2/9/17 16:08 JMCmg/kg dry 0.0047Chlordane
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00036delta-BHC
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCCCVmg/kg dry 0.00035Dieldrin
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00041Endosulfan I
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00031Endosulfan II
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCCCVmg/kg dry 0.00026Endosulfan Sulfate
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00032Endrin
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00049Endrin Aldehyde
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCCCVmg/kg dry 0.00061Endrin Ketone
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00061gamma-BHC
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00046trans-Chlordane
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00056Heptachlor
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCmg/kg dry 0.00043Heptachlor Epoxide
BRL 8081B P7B016910.0022 2/9/17 16:08 JMCCCVmg/kg dry 0.0012Methoxychlor
BRL 8081B P7B016910.056 2/9/17 16:08 JMCmg/kg dry 0.0071Toxaphene
Surrogate Recovery Control Limits
26-20496 %Decachlorobiphenyl
40-16270 %Tetrachloro-m-xylene
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL *8082A P7B011010.056 2/7/17 23:29 JMCmg/kg dry 0.011Aroclor 1016
BRL *8082A P7B011010.11 2/7/17 23:29 JMCmg/kg dry 0.045Aroclor 1221
BRL *8082A P7B011010.11 2/7/17 23:29 JMCmg/kg dry 0.015Aroclor 1232
BRL *8082A P7B011010.056 2/7/17 23:29 JMCmg/kg dry 0.015Aroclor 1242
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: TP-5
Prism Sample ID: 7020076-01
Prism Work Order: 7020076
Time Collected: 02/02/17 20:00
Time Submitted: 02/03/17 15:15
BRL *8082A P7B011010.056 2/7/17 23:29 JMCmg/kg dry 0.011Aroclor 1248
BRL *8082A P7B011010.056 2/7/17 23:29 JMCmg/kg dry 0.014Aroclor 1254
BRL *8082A P7B011010.056 2/7/17 23:29 JMCmg/kg dry 0.015Aroclor 1260
Surrogate Recovery Control Limits
36-18274 %Tetrachloro-m-xylene
34-18283 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0581,2,4-Trichlorobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0561,2-Dichlorobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0521,3-Dichlorobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0541,4-Dichlorobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0702,4,5-Trichlorophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0702,4,6-Trichlorophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0722,4-Dichlorophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0572,4-Dimethylphenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0522,4-Dinitrophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0452,4-Dinitrotoluene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0492,6-Dinitrotoluene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0542-Chloronaphthalene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0532-Chlorophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0592-Methylnaphthalene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0482-Methylphenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0672-Nitroaniline
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0682-Nitrophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0733,3'-Dichlorobenzidine
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0463/4-Methylphenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0643-Nitroaniline
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0644-Bromophenyl phenyl ether
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0524-Chloro-3-methylphenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0454-Chloroaniline
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0484-Chlorophenyl phenyl ether
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0684-Nitroaniline
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.0574-Nitrophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.051Acenaphthene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.054Acenaphthylene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.032Aniline
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.060Anthracene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.049Azobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.049Benzo(a)anthracene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.040Benzo(a)pyrene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.043Benzo(b)fluoranthene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.041Benzo(g,h,i)perylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: TP-5
Prism Sample ID: 7020076-01
Prism Work Order: 7020076
Time Collected: 02/02/17 20:00
Time Submitted: 02/03/17 15:15
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.049Benzo(k)fluoranthene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.031Benzoic Acid
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.049Benzyl alcohol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.065bis(2-Chloroethoxy)methane
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.064Bis(2-chloroisopropyl)ether
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.055Bis(2-Ethylhexyl)phthalate
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.053Butyl benzyl phthalate
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.047Chrysene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.045Dibenzo(a,h)anthracene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.057Dibenzofuran
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.051Diethyl phthalate
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.049Dimethyl phthalate
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.053Di-n-butyl phthalate
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.046Di-n-octyl phthalate
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.047Fluoranthene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.053Fluorene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.059Hexachlorobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.067Hexachlorobutadiene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.066Hexachlorocyclopentadiene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.062Hexachloroethane
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.050Isophorone
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.060Naphthalene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.053Nitrobenzene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.059N-Nitroso-di-n-propylamine
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.057N-Nitrosodiphenylamine
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.044Pentachlorophenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.048Phenanthrene
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.055Phenol
BRL 8270D P7B011410.37 2/7/17 17:53 JMVmg/kg dry 0.049Pyrene
Surrogate Recovery Control Limits
39-13284 %2,4,6-Tribromophenol
44-11579 %2-Fluorobiphenyl
35-11583 %2-Fluorophenol
37-12269 %Nitrobenzene-d5
34-12183 %Phenol-d5
54-12775 %Terphenyl-d14
Total Metals
BRL *7471B P7B012610.024 2/8/17 11:51 JABmg/kg dry 0.0013Mercury
2.3 *6010D P7B010510.28 2/9/17 6:29 bgmmg/kg dry 0.035Arsenic
14 *6010D P7B010510.57 2/9/17 6:29 bgmmg/kg dry 0.083Barium
BRL *6010D P7B010510.28 2/9/17 6:29 bgmmg/kg dry 0.0076Cadmium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: TP-5
Prism Sample ID: 7020076-01
Prism Work Order: 7020076
Time Collected: 02/02/17 20:00
Time Submitted: 02/03/17 15:15
14 *6010D P7B010510.28 2/9/17 6:29 bgmmg/kg dry 0.048Chromium
6.7 *6010D P7B010510.28 2/9/17 6:29 bgmmg/kg dry 0.053Lead
BRL *6010D P7B010510.57 2/9/17 6:29 bgmmg/kg dry 0.13Selenium
BRL *6010D P7B010510.28 2/9/17 6:29 bgmmg/kg dry 0.0071Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000391,1,1,2-Tetrachloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000231,1,1-Trichloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000321,1,2,2-Tetrachloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000421,1,2-Trichloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000131,1-Dichloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000211,1-Dichloroethylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000261,1-Dichloropropylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000271,2,3-Trichlorobenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000601,2,3-Trichloropropane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000351,2,4-Trichlorobenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000361,2,4-Trimethylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000191,2-Dibromoethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000221,2-Dichlorobenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000281,2-Dichloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000291,2-Dichloropropane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000361,3,5-Trimethylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000311,3-Dichlorobenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000241,3-Dichloropropane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000191,4-Dichlorobenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000232,2-Dichloropropane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000242-Chlorotoluene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000284-Chlorotoluene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.000234-Isopropyltoluene
0.0095 8260B P7B009610.047 2/6/17 16:53 ANGJmg/kg dry 0.0012Acetone
BRL 8260B P7B009610.0028 2/6/17 16:53 ANGmg/kg dry 0.00028Benzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00039Bromobenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00026Bromochloromethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00026Bromodichloromethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00054Bromoform
BRL 8260B P7B009610.0095 2/6/17 16:53 ANGmg/kg dry 0.00058Bromomethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00024Carbon Tetrachloride
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00025Chlorobenzene
BRL 8260B P7B009610.0095 2/6/17 16:53 ANGmg/kg dry 0.00039Chloroethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00034Chloroform
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00032Chloromethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00020cis-1,2-Dichloroethylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00016cis-1,3-Dichloropropylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00020Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: TP-5
Prism Sample ID: 7020076-01
Prism Work Order: 7020076
Time Collected: 02/02/17 20:00
Time Submitted: 02/03/17 15:15
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00021Dichlorodifluoromethane
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00018Ethylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00019Isopropyl Ether
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00028Isopropylbenzene (Cumene)
BRL 8260B P7B009610.0095 2/6/17 16:53 ANGmg/kg dry 0.00044m,p-Xylenes
BRL 8260B P7B009610.047 2/6/17 16:53 ANGmg/kg dry 0.00043Methyl Butyl Ketone (2-Hexanone)
0.0030 8260B P7B009610.095 2/6/17 16:53 ANGJmg/kg dry 0.00043Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7B009610.047 2/6/17 16:53 ANGmg/kg dry 0.00040Methyl Isobutyl Ketone
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00027Methylene Chloride
BRL 8260B P7B009610.0095 2/6/17 16:53 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether
0.0029 8260B P7B009610.0095 2/6/17 16:53 ANGJmg/kg dry 0.00015Naphthalene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00024n-Butylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00028n-Propylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00019o-Xylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00023sec-Butylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00029Styrene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00016tert-Butylbenzene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00023Tetrachloroethylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00027Toluene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00028trans-1,2-Dichloroethylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00025trans-1,3-Dichloropropylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00031Trichloroethylene
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00031Trichlorofluoromethane
BRL 8260B P7B009610.024 2/6/17 16:53 ANGmg/kg dry 0.00065Vinyl acetate
BRL 8260B P7B009610.0047 2/6/17 16:53 ANGmg/kg dry 0.00023Vinyl chloride
BRL 8260B P7B009610.014 2/6/17 16:53 ANGmg/kg dry 0.00089Xylenes, total
Surrogate Recovery Control Limits
70-130128 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-129102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: BOILER
Prism Sample ID: 7020076-02
Prism Work Order: 7020076
Time Collected: 02/02/17 16:00
Time Submitted: 02/03/17 15:15
General Chemistry Parameters
84.4 *SM2540 G P7B010910.100 2/6/17 15:03 JLR% by
Weight
0.100% Solids
Organochlorine Pesticides by GC/ECD
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCCCVmg/kg dry 0.00274,4'-DDD
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCCCVmg/kg dry 0.00424,4'-DDE
BRL 8081B P7B0169100.035 2/9/17 16:31 JMCCCVmg/kg dry 0.00974,4'-DDT
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0061Aldrin
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0070alpha-BHC
2.8 8081B P7B01692500.59 2/10/17 11:00 JMCmg/kg dry 0.13cis-Chlordane
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0051beta-BHC
20 8081B P7B0169503.0 2/9/17 16:43 JMCAmg/kg dry 0.25Chlordane
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0038delta-BHC
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCCCVmg/kg dry 0.0037Dieldrin
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0043Endosulfan I
0.11 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0033Endosulfan II
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCCCVmg/kg dry 0.0027Endosulfan Sulfate
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0034Endrin
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0052Endrin Aldehyde
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCCCVmg/kg dry 0.0064Endrin Ketone
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0064gamma-BHC
3.7 8081B P7B01692500.59 2/10/17 11:00 JMCAamg/kg dry 0.12trans-Chlordane
0.25 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0059Heptachlor
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCmg/kg dry 0.0046Heptachlor Epoxide
BRL 8081B P7B0169100.024 2/9/17 16:31 JMCCCVmg/kg dry 0.013Methoxychlor
BRL 8081B P7B0169100.59 2/9/17 16:31 JMCmg/kg dry 0.075Toxaphene
Surrogate Recovery Control Limits
26-20496 %Decachlorobiphenyl
40-16247 %Tetrachloro-m-xylene
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL *8082A P7B011010.059 2/8/17 0:12 JMCmg/kg dry 0.011Aroclor 1016
BRL *8082A P7B011010.12 2/8/17 0:12 JMCmg/kg dry 0.047Aroclor 1221
BRL *8082A P7B011010.12 2/8/17 0:12 JMCmg/kg dry 0.015Aroclor 1232
BRL *8082A P7B011010.059 2/8/17 0:12 JMCmg/kg dry 0.016Aroclor 1242
BRL *8082A P7B011010.059 2/8/17 0:12 JMCmg/kg dry 0.012Aroclor 1248
BRL *8082A P7B011010.059 2/8/17 0:12 JMCmg/kg dry 0.015Aroclor 1254
BRL *8082A P7B011010.059 2/8/17 0:12 JMCmg/kg dry 0.015Aroclor 1260
Surrogate Recovery Control Limits
36-18277 %Tetrachloro-m-xylene
34-18296 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0611,2,4-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: BOILER
Prism Sample ID: 7020076-02
Prism Work Order: 7020076
Time Collected: 02/02/17 16:00
Time Submitted: 02/03/17 15:15
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0591,2-Dichlorobenzene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0551,3-Dichlorobenzene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0571,4-Dichlorobenzene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0732,4,5-Trichlorophenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0732,4,6-Trichlorophenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0762,4-Dichlorophenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0602,4-Dimethylphenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0472,4-Dinitrotoluene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0522,6-Dinitrotoluene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0552-Chlorophenol
2.1 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0632-Methylnaphthalene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0502-Methylphenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0712-Nitroaniline
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0712-Nitrophenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0773,3'-Dichlorobenzidine
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0483/4-Methylphenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0673-Nitroaniline
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0474-Chloroaniline
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0714-Nitroaniline
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.0604-Nitrophenol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.053Acenaphthene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.033Aniline
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.063Anthracene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.052Azobenzene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.051Benzo(a)anthracene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.042Benzo(a)pyrene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.045Benzo(b)fluoranthene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.051Benzo(k)fluoranthene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.052Benzyl alcohol
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.068bis(2-Chloroethoxy)methane
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.067Bis(2-chloroisopropyl)ether
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.056Butyl benzyl phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: BOILER
Prism Sample ID: 7020076-02
Prism Work Order: 7020076
Time Collected: 02/02/17 16:00
Time Submitted: 02/03/17 15:15
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.049Chrysene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.059Dibenzofuran
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.048Di-n-octyl phthalate
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.050Fluoranthene
2.0 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.056Fluorene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.062Hexachlorobenzene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.070Hexachlorobutadiene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.070Hexachlorocyclopentadiene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.053Isophorone
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.063Naphthalene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.059N-Nitrosodiphenylamine
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.046Pentachlorophenol
4.3 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.058Phenol
1.0 8270D P7B011410.39 2/7/17 18:15 JMVmg/kg dry 0.052Pyrene
Surrogate Recovery Control Limits
39-13270 %2,4,6-Tribromophenol
44-11570 %2-Fluorobiphenyl
35-11560 %2-Fluorophenol
37-12270 %Nitrobenzene-d5
34-12167 %Phenol-d5
54-12767 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000381,1,1,2-Tetrachloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000221,1,1-Trichloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000311,1,2,2-Tetrachloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000411,1,2-Trichloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000131,1-Dichloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000201,1-Dichloroethylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000251,1-Dichloropropylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000261,2,3-Trichlorobenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000581,2,3-Trichloropropane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000341,2,4-Trichlorobenzene
0.22 8260B P7B009610.0046 2/6/17 17:26 ANGLLmg/kg dry 0.000351,2,4-Trimethylbenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000181,2-Dibromoethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: BOILER
Prism Sample ID: 7020076-02
Prism Work Order: 7020076
Time Collected: 02/02/17 16:00
Time Submitted: 02/03/17 15:15
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000211,2-Dichlorobenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000271,2-Dichloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000281,2-Dichloropropane
See 8260ML 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000351,3,5-Trimethylbenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000301,3-Dichlorobenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000231,3-Dichloropropane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000181,4-Dichlorobenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000222,2-Dichloropropane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000242-Chlorotoluene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000274-Chlorotoluene
0.059 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.000224-Isopropyltoluene
0.027 8260B P7B009610.046 2/6/17 17:26 ANGJmg/kg dry 0.0011Acetone
BRL 8260B P7B009610.0027 2/6/17 17:26 ANGmg/kg dry 0.00027Benzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00038Bromobenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00025Bromochloromethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00026Bromodichloromethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00052Bromoform
BRL 8260B P7B009610.0091 2/6/17 17:26 ANGmg/kg dry 0.00056Bromomethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00023Carbon Tetrachloride
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00024Chlorobenzene
BRL 8260B P7B009610.0091 2/6/17 17:26 ANGmg/kg dry 0.00038Chloroethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00033Chloroform
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00031Chloromethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00019cis-1,2-Dichloroethylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00015cis-1,3-Dichloropropylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00019Dibromochloromethane
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00021Dichlorodifluoromethane
See 8260ML 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00018Ethylbenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00019Isopropyl Ether
0.042 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00027Isopropylbenzene (Cumene)
0.058 8260B P7B009610.0091 2/6/17 17:26 ANGmg/kg dry 0.00042m,p-Xylenes
BRL 8260B P7B009610.046 2/6/17 17:26 ANGmg/kg dry 0.00041Methyl Butyl Ketone (2-Hexanone)
0.0056 8260B P7B009610.091 2/6/17 17:26 ANGJmg/kg dry 0.00041Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7B009610.046 2/6/17 17:26 ANGmg/kg dry 0.00039Methyl Isobutyl Ketone
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00026Methylene Chloride
BRL 8260B P7B009610.0091 2/6/17 17:26 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether
BRL 8260B P7B009610.0091 2/6/17 17:26 ANGmg/kg dry 0.00014Naphthalene
0.17 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00023n-Butylbenzene
See 8260ML 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00027n-Propylbenzene
0.0086 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00019o-Xylene
See 8260ML 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00022sec-Butylbenzene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00028Styrene
0.022 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00015tert-Butylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 41
Laboratory Report
02/13/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: BOILER
Prism Sample ID: 7020076-02
Prism Work Order: 7020076
Time Collected: 02/02/17 16:00
Time Submitted: 02/03/17 15:15
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00022Tetrachloroethylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00026Toluene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00027trans-1,2-Dichloroethylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00024trans-1,3-Dichloropropylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00030Trichloroethylene
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00030Trichlorofluoromethane
BRL 8260B P7B009610.023 2/6/17 17:26 ANGmg/kg dry 0.00063Vinyl acetate
BRL 8260B P7B009610.0046 2/6/17 17:26 ANGmg/kg dry 0.00022Vinyl chloride
0.067 8260B P7B009610.014 2/6/17 17:26 ANGmg/kg dry 0.00086Xylenes, total
Surrogate Recovery Control Limits
70-130151 %4-Bromofluorobenzene SR
84-123107 %Dibromofluoromethane
76-129107 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
0.24 8260B P7B0133500.24 2/7/17 17:13 ANGmg/kg dry 0.0581,3,5-Trimethylbenzene
0.25 8260B P7B0133500.24 2/7/17 17:13 ANGmg/kg dry 0.054Ethylbenzene
1.3 8260B P7B0133500.47 2/7/17 17:13 ANGmg/kg dry 0.036Naphthalene
0.55 8260B P7B0133500.24 2/7/17 17:13 ANGmg/kg dry 0.047n-Butylbenzene
0.47 8260B P7B0133500.24 2/7/17 17:13 ANGmg/kg dry 0.058sec-Butylbenzene
Surrogate Recovery Control Limits
70-130117 %4-Bromofluorobenzene
70-13092 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
Blank (P7B0096-BLK1)Prepared & Analyzed: 02/06/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
Blank (P7B0096-BLK1)Prepared & Analyzed: 02/06/17
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 12964.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.1
ug/L 50.00 76-129Surrogate: Toluene-d8 10150.6
LCS (P7B0096-BS1)Prepared & Analyzed: 02/06/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0498 0.0050 0.05000 72-115100
1,1,1-Trichloroethane mg/kg wet0.0446 0.0050 0.05000 67-13189
1,1,2,2-Tetrachloroethane mg/kg wet0.0428 0.0050 0.05000 56-12686
1,1,2-Trichloroethane mg/kg wet0.0483 0.0050 0.05000 70-13397
1,1-Dichloroethane mg/kg wet0.0438 0.0050 0.05000 74-12788
1,1-Dichloroethylene mg/kg wet0.0430 0.0050 0.05000 67-14986
1,1-Dichloropropylene mg/kg wet0.0450 0.0050 0.05000 71-13090
1,2,3-Trichlorobenzene mg/kg wet0.0578 0.0050 0.05000 68-130116
1,2,3-Trichloropropane mg/kg wet0.0472 0.0050 0.05000 60-13794
1,2,4-Trichlorobenzene mg/kg wet0.0492 0.0050 0.05000 66-12598
1,2,4-Trimethylbenzene mg/kg wet0.0488 0.0050 0.05000 69-12998
1,2-Dibromoethane mg/kg wet0.0501 0.0050 0.05000 70-132100
1,2-Dichlorobenzene mg/kg wet0.0486 0.0050 0.05000 72-12397
1,2-Dichloroethane mg/kg wet0.0451 0.0050 0.05000 68-12890
1,2-Dichloropropane mg/kg wet0.0423 0.0050 0.05000 73-13085
1,3,5-Trimethylbenzene mg/kg wet0.0471 0.0050 0.05000 69-12894
1,3-Dichlorobenzene mg/kg wet0.0494 0.0050 0.05000 71-12099
1,3-Dichloropropane mg/kg wet0.0457 0.0050 0.05000 75-12491
1,4-Dichlorobenzene mg/kg wet0.0495 0.0050 0.05000 71-12399
2,2-Dichloropropane mg/kg wet0.0473 0.0050 0.05000 50-14295
2-Chlorotoluene mg/kg wet0.0459 0.0050 0.05000 67-12492
4-Chlorotoluene mg/kg wet0.0470 0.0050 0.05000 71-12694
4-Isopropyltoluene mg/kg wet0.0470 0.0050 0.05000 68-12994
Acetone mg/kg wet0.0996 0.050 0.1000 29-198100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
LCS (P7B0096-BS1)Prepared & Analyzed: 02/06/17
Benzene mg/kg wet0.0422 0.0030 0.05000 74-12784
Bromobenzene mg/kg wet0.0452 0.0050 0.05000 73-12590
Bromochloromethane mg/kg wet0.0528 0.0050 0.05000 72-134106
Bromodichloromethane mg/kg wet0.0459 0.0050 0.05000 75-12292
Bromoform mg/kg wet0.0508 0.0050 0.05000 66-135102
Bromomethane mg/kg wet0.0304 0.010 0.05000 20-18061
Carbon Tetrachloride mg/kg wet0.0469 0.0050 0.05000 64-14394
Chlorobenzene mg/kg wet0.0506 0.0050 0.05000 74-118101
Chloroethane mg/kg wet0.0418 0.010 0.05000 33-14984
Chloroform mg/kg wet0.0455 0.0050 0.05000 73-12791
Chloromethane mg/kg wet0.0350 0.0050 0.05000 45-14370
cis-1,2-Dichloroethylene mg/kg wet0.0447 0.0050 0.05000 76-13489
cis-1,3-Dichloropropylene mg/kg wet0.0451 0.0050 0.05000 71-12590
Dibromochloromethane mg/kg wet0.0510 0.0050 0.05000 73-122102
Dichlorodifluoromethane mg/kg wet0.0375 0.0050 0.05000 26-14675
Ethylbenzene mg/kg wet0.0476 0.0050 0.05000 74-12895
Isopropyl Ether mg/kg wet0.0404 0.0050 0.05000 59-15981
Isopropylbenzene (Cumene)mg/kg wet0.0476 0.0050 0.05000 68-12695
m,p-Xylenes mg/kg wet0.0976 0.010 0.1000 75-12498
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0438 0.050 0.05000 J61-15788
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0369 0.10 0.05000 J63-14974
Methyl Isobutyl Ketone mg/kg wet0.0421 0.050 0.05000 J57-16284
Methylene Chloride mg/kg wet0.0392 0.0050 0.05000 74-12978
Methyl-tert-Butyl Ether mg/kg wet0.0444 0.010 0.05000 70-13089
Naphthalene mg/kg wet0.0467 0.010 0.05000 57-15793
n-Butylbenzene mg/kg wet0.0447 0.0050 0.05000 65-13589
n-Propylbenzene mg/kg wet0.0448 0.0050 0.05000 67-13090
o-Xylene mg/kg wet0.0483 0.0050 0.05000 74-12697
sec-Butylbenzene mg/kg wet0.0483 0.0050 0.05000 66-13197
Styrene mg/kg wet0.0527 0.0050 0.05000 77-121105
tert-Butylbenzene mg/kg wet0.0461 0.0050 0.05000 67-13292
Tetrachloroethylene mg/kg wet0.0469 0.0050 0.05000 68-13094
Toluene mg/kg wet0.0429 0.0050 0.05000 71-12986
trans-1,2-Dichloroethylene mg/kg wet0.0458 0.0050 0.05000 73-13292
trans-1,3-Dichloropropylene mg/kg wet0.0446 0.0050 0.05000 68-12389
Trichloroethylene mg/kg wet0.0475 0.0050 0.05000 75-13395
Trichlorofluoromethane mg/kg wet0.0494 0.0050 0.05000 44-14699
Vinyl acetate mg/kg wet0.0480 0.025 0.05000 85-16196
Vinyl chloride mg/kg wet0.0413 0.0050 0.05000 48-14783
Xylenes, total mg/kg wet0.146 0.015 0.1500 74-12697
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10552.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9648.0
ug/L 50.00 76-129Surrogate: Toluene-d8 10250.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
LCS Dup (P7B0096-BSD1)Prepared & Analyzed: 02/06/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0518 0.0050 0.05000 2072-115104 4
1,1,1-Trichloroethane mg/kg wet0.0448 0.0050 0.05000 2067-13190 0.6
1,1,2,2-Tetrachloroethane mg/kg wet0.0459 0.0050 0.05000 2056-12692 7
1,1,2-Trichloroethane mg/kg wet0.0479 0.0050 0.05000 2070-13396 0.8
1,1-Dichloroethane mg/kg wet0.0422 0.0050 0.05000 2074-12784 4
1,1-Dichloroethylene mg/kg wet0.0426 0.0050 0.05000 2067-14985 0.9
1,1-Dichloropropylene mg/kg wet0.0451 0.0050 0.05000 2071-13090 0.2
1,2,3-Trichlorobenzene mg/kg wet0.0594 0.0050 0.05000 2068-130119 3
1,2,3-Trichloropropane mg/kg wet0.0525 0.0050 0.05000 2060-137105 11
1,2,4-Trichlorobenzene mg/kg wet0.0521 0.0050 0.05000 2066-125104 6
1,2,4-Trimethylbenzene mg/kg wet0.0478 0.0050 0.05000 2069-12996 2
1,2-Dibromoethane mg/kg wet0.0528 0.0050 0.05000 2070-132106 5
1,2-Dichlorobenzene mg/kg wet0.0506 0.0050 0.05000 2072-123101 4
1,2-Dichloroethane mg/kg wet0.0469 0.0050 0.05000 2068-12894 4
1,2-Dichloropropane mg/kg wet0.0430 0.0050 0.05000 2073-13086 2
1,3,5-Trimethylbenzene mg/kg wet0.0468 0.0050 0.05000 2069-12894 0.5
1,3-Dichlorobenzene mg/kg wet0.0487 0.0050 0.05000 2071-12097 1
1,3-Dichloropropane mg/kg wet0.0475 0.0050 0.05000 2075-12495 4
1,4-Dichlorobenzene mg/kg wet0.0502 0.0050 0.05000 2071-123100 1
2,2-Dichloropropane mg/kg wet0.0460 0.0050 0.05000 2050-14292 3
2-Chlorotoluene mg/kg wet0.0461 0.0050 0.05000 2067-12492 0.4
4-Chlorotoluene mg/kg wet0.0485 0.0050 0.05000 2071-12697 3
4-Isopropyltoluene mg/kg wet0.0477 0.0050 0.05000 2068-12995 1
Acetone mg/kg wet0.101 0.050 0.1000 2029-198101 2
Benzene mg/kg wet0.0422 0.0030 0.05000 2074-12784 0.05
Bromobenzene mg/kg wet0.0463 0.0050 0.05000 2073-12593 2
Bromochloromethane mg/kg wet0.0511 0.0050 0.05000 2072-134102 3
Bromodichloromethane mg/kg wet0.0455 0.0050 0.05000 2075-12291 0.9
Bromoform mg/kg wet0.0521 0.0050 0.05000 2066-135104 3
Bromomethane mg/kg wet0.0318 0.010 0.05000 2020-18064 4
Carbon Tetrachloride mg/kg wet0.0464 0.0050 0.05000 2064-14393 0.9
Chlorobenzene mg/kg wet0.0505 0.0050 0.05000 2074-118101 0.1
Chloroethane mg/kg wet0.0428 0.010 0.05000 2033-14986 2
Chloroform mg/kg wet0.0452 0.0050 0.05000 2073-12790 0.7
Chloromethane mg/kg wet0.0364 0.0050 0.05000 2045-14373 4
cis-1,2-Dichloroethylene mg/kg wet0.0445 0.0050 0.05000 2076-13489 0.4
cis-1,3-Dichloropropylene mg/kg wet0.0464 0.0050 0.05000 2071-12593 3
Dibromochloromethane mg/kg wet0.0513 0.0050 0.05000 2073-122103 0.5
Dichlorodifluoromethane mg/kg wet0.0366 0.0050 0.05000 2026-14673 3
Ethylbenzene mg/kg wet0.0473 0.0050 0.05000 2074-12895 0.7
Isopropyl Ether mg/kg wet0.0399 0.0050 0.05000 2059-15980 1
Isopropylbenzene (Cumene)mg/kg wet0.0480 0.0050 0.05000 2068-12696 0.7
m,p-Xylenes mg/kg wet0.0932 0.010 0.1000 2075-12493 5
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0472 0.050 0.05000 20 J61-15794 7
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0403 0.10 0.05000 20 J63-14981 9
Methyl Isobutyl Ketone mg/kg wet0.0443 0.050 0.05000 20 J57-16289 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
LCS Dup (P7B0096-BSD1)Prepared & Analyzed: 02/06/17
Methylene Chloride mg/kg wet0.0402 0.0050 0.05000 2074-12980 3
Methyl-tert-Butyl Ether mg/kg wet0.0443 0.010 0.05000 2070-13089 0.2
Naphthalene mg/kg wet0.0484 0.010 0.05000 2057-15797 4
n-Butylbenzene mg/kg wet0.0446 0.0050 0.05000 2065-13589 0.04
n-Propylbenzene mg/kg wet0.0450 0.0050 0.05000 2067-13090 0.6
o-Xylene mg/kg wet0.0475 0.0050 0.05000 2074-12695 2
sec-Butylbenzene mg/kg wet0.0487 0.0050 0.05000 2066-13197 0.9
Styrene mg/kg wet0.0514 0.0050 0.05000 2077-121103 2
tert-Butylbenzene mg/kg wet0.0474 0.0050 0.05000 2067-13295 3
Tetrachloroethylene mg/kg wet0.0479 0.0050 0.05000 2068-13096 2
Toluene mg/kg wet0.0438 0.0050 0.05000 2071-12988 2
trans-1,2-Dichloroethylene mg/kg wet0.0456 0.0050 0.05000 2073-13291 0.5
trans-1,3-Dichloropropylene mg/kg wet0.0446 0.0050 0.05000 2068-12389 0.02
Trichloroethylene mg/kg wet0.0489 0.0050 0.05000 2075-13398 3
Trichlorofluoromethane mg/kg wet0.0473 0.0050 0.05000 2044-14695 4
Vinyl acetate mg/kg wet0.0495 0.025 0.05000 2085-16199 3
Vinyl chloride mg/kg wet0.0407 0.0050 0.05000 2048-14781 1
Xylenes, total mg/kg wet0.141 0.015 0.1500 2074-12694 4
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 76-129Surrogate: Toluene-d8 10050.2
Matrix Spike (P7B0096-MS1)Prepared: 02/06/17 Analyzed: 02/07/17 Source: 7020076-01
1,1,1,2-Tetrachloroethane mg/kg dry0.0390 0.0057 0.05725 BRL 60-12068
1,1,1-Trichloroethane mg/kg dry0.0462 0.0057 0.05725 BRL 52-13981
1,1,2,2-Tetrachloroethane mg/kg dry0.0415 0.0057 0.05725 BRL 39-13572
1,1,2-Trichloroethane mg/kg dry0.0440 0.0057 0.05725 BRL 44-14077
1,1-Dichloroethane mg/kg dry0.0449 0.0057 0.05725 BRL 59-13778
1,1-Dichloroethylene mg/kg dry0.0449 0.0057 0.05725 BRL 54-16278
1,1-Dichloropropylene mg/kg dry0.0485 0.0057 0.05725 BRL 55-13785
1,2,3-Trichlorobenzene mg/kg dry0.0401 0.0057 0.05725 BRL 34-12070
1,2,3-Trichloropropane mg/kg dry0.0456 0.0057 0.05725 BRL 45-13980
1,2,4-Trichlorobenzene mg/kg dry0.0346 0.0057 0.05725 BRL 35-11660
1,2,4-Trimethylbenzene mg/kg dry0.0452 0.0057 0.05725 BRL 38-14279
1,2-Dibromoethane mg/kg dry0.0446 0.0057 0.05725 BRL 49-13278
1,2-Dichlorobenzene mg/kg dry0.0447 0.0057 0.05725 BRL 42-13078
1,2-Dichloroethane mg/kg dry0.0388 0.0057 0.05725 BRL 51-13168
1,2-Dichloropropane mg/kg dry0.0422 0.0057 0.05725 BRL 55-13874
1,3,5-Trimethylbenzene mg/kg dry0.0480 0.0057 0.05725 BRL 44-14084
1,3-Dichlorobenzene mg/kg dry0.0442 0.0057 0.05725 BRL 41-12977
1,3-Dichloropropane mg/kg dry0.0453 0.0057 0.05725 BRL 53-12979
1,4-Dichlorobenzene mg/kg dry0.0431 0.0057 0.05725 BRL 44-13475
2,2-Dichloropropane mg/kg dry0.0475 0.0057 0.05725 BRL 30-14783
2-Chlorotoluene mg/kg dry0.0456 0.0057 0.05725 BRL 46-13280
4-Chlorotoluene mg/kg dry0.0434 0.0057 0.05725 BRL 44-13576
4-Isopropyltoluene mg/kg dry0.0455 0.0057 0.05725 BRL 32-14480
Acetone mg/kg dry0.0580 0.057 0.1145 0.00954 34-14342
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
Matrix Spike (P7B0096-MS1)Prepared: 02/06/17 Analyzed: 02/07/17 Source: 7020076-01
Benzene mg/kg dry0.0446 0.0034 0.05725 BRL 60-13578
Bromobenzene mg/kg dry0.0417 0.0057 0.05725 BRL 45-13573
Bromochloromethane mg/kg dry0.0468 0.0057 0.05725 BRL 55-13682
Bromodichloromethane mg/kg dry0.0408 0.0057 0.05725 BRL 55-12771
Bromoform mg/kg dry0.0396 0.0057 0.05725 BRL 40-13669
Bromomethane mg/kg dry0.0271 0.011 0.05725 BRL 30-13747
Carbon Tetrachloride mg/kg dry0.0466 0.0057 0.05725 BRL 48-15381
Chlorobenzene mg/kg dry0.0478 0.0057 0.05725 BRL 57-12583
Chloroethane mg/kg dry0.0416 0.011 0.05725 BRL 16-17773
Chloroform mg/kg dry0.0449 0.0057 0.05725 BRL 56-13778
Chloromethane mg/kg dry0.0350 0.0057 0.05725 BRL 40-14561
cis-1,2-Dichloroethylene mg/kg dry0.0439 0.0057 0.05725 BRL 58-14077
cis-1,3-Dichloropropylene mg/kg dry0.0380 0.0057 0.05725 BRL 42-13566
Dibromochloromethane mg/kg dry0.0436 0.0057 0.05725 BRL 49-12776
Dichlorodifluoromethane mg/kg dry0.0364 0.0057 0.05725 BRL 25-15164
Ethylbenzene mg/kg dry0.0475 0.0057 0.05725 BRL 44-14483
Isopropyl Ether mg/kg dry0.0393 0.0057 0.05725 BRL 51-15569
Isopropylbenzene (Cumene)mg/kg dry0.0513 0.0057 0.05725 BRL 41-14090
m,p-Xylenes mg/kg dry0.0929 0.011 0.1145 BRL 36-14881
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0137 0.057 0.05725 BRL M, J30-14724
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0212 0.11 0.05725 0.00295 J24-16032
Methyl Isobutyl Ketone mg/kg dry0.0301 0.057 0.05725 BRL J25-16353
Methylene Chloride mg/kg dry0.0397 0.0057 0.05725 BRL 53-14469
Methyl-tert-Butyl Ether mg/kg dry0.0401 0.011 0.05725 BRL 49-13570
Naphthalene mg/kg dry0.0307 0.011 0.05725 0.00286 32-12749
n-Butylbenzene mg/kg dry0.0415 0.0057 0.05725 BRL 23-14872
n-Propylbenzene mg/kg dry0.0466 0.0057 0.05725 BRL 35-14481
o-Xylene mg/kg dry0.0468 0.0057 0.05725 BRL 43-14382
sec-Butylbenzene mg/kg dry0.0499 0.0057 0.05725 BRL 34-14487
Styrene mg/kg dry0.0434 0.0057 0.05725 BRL 42-13276
tert-Butylbenzene mg/kg dry0.0495 0.0057 0.05725 BRL 36-15086
Tetrachloroethylene mg/kg dry0.0478 0.0057 0.05725 BRL 47-14284
Toluene mg/kg dry0.0447 0.0057 0.05725 BRL 57-13578
trans-1,2-Dichloroethylene mg/kg dry0.0467 0.0057 0.05725 BRL 58-14182
trans-1,3-Dichloropropylene mg/kg dry0.0358 0.0057 0.05725 BRL 41-12463
Trichloroethylene mg/kg dry0.0487 0.0057 0.05725 BRL 38-16485
Trichlorofluoromethane mg/kg dry0.0463 0.0057 0.05725 BRL 30-15781
Vinyl acetate mg/kg dryBRL0.029 0.05725 BRL M61-154
Vinyl chloride mg/kg dry0.0437 0.0057 0.05725 BRL 40-15676
Xylenes, total mg/kg dry0.140 0.017 0.1718 BRL 36-14881
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10853.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 76-129Surrogate: Toluene-d8 10954.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
Matrix Spike Dup (P7B0096-MSD1)Prepared: 02/06/17 Analyzed: 02/07/17 Source: 7020076-01
1,1,1,2-Tetrachloroethane mg/kg dry0.0519 0.0057 0.05714 BRL 15 D60-12091 28
1,1,1-Trichloroethane mg/kg dry0.0533 0.0057 0.05714 BRL 2152-13993 14
1,1,2,2-Tetrachloroethane mg/kg dry0.0473 0.0057 0.05714 BRL 2239-13583 13
1,1,2-Trichloroethane mg/kg dry0.0506 0.0057 0.05714 BRL 2144-14089 14
1,1-Dichloroethane mg/kg dry0.0521 0.0057 0.05714 BRL 2159-13791 15
1,1-Dichloroethylene mg/kg dry0.0534 0.0057 0.05714 BRL 2254-16293 17
1,1-Dichloropropylene mg/kg dry0.0559 0.0057 0.05714 BRL 1955-13798 14
1,2,3-Trichlorobenzene mg/kg dry0.0429 0.0057 0.05714 BRL 4134-12075 7
1,2,3-Trichloropropane mg/kg dry0.0601 0.0057 0.05714 BRL 25 D45-139105 27
1,2,4-Trichlorobenzene mg/kg dry0.0379 0.0057 0.05714 BRL 6235-11666 9
1,2,4-Trimethylbenzene mg/kg dry0.0494 0.0057 0.05714 BRL 2438-14287 9
1,2-Dibromoethane mg/kg dry0.0526 0.0057 0.05714 BRL 15 D49-13292 16
1,2-Dichlorobenzene mg/kg dry0.0477 0.0057 0.05714 BRL 2142-13083 6
1,2-Dichloroethane mg/kg dry0.0454 0.0057 0.05714 BRL 13 D51-13179 16
1,2-Dichloropropane mg/kg dry0.0500 0.0057 0.05714 BRL 16 D55-13887 17
1,3,5-Trimethylbenzene mg/kg dry0.0514 0.0057 0.05714 BRL 2944-14090 7
1,3-Dichlorobenzene mg/kg dry0.0495 0.0057 0.05714 BRL 2441-12987 11
1,3-Dichloropropane mg/kg dry0.0498 0.0057 0.05714 BRL 1553-12987 9
1,4-Dichlorobenzene mg/kg dry0.0483 0.0057 0.05714 BRL 2144-13485 11
2,2-Dichloropropane mg/kg dry0.0545 0.0057 0.05714 BRL 2030-14795 14
2-Chlorotoluene mg/kg dry0.0511 0.0057 0.05714 BRL 2946-13289 11
4-Chlorotoluene mg/kg dry0.0495 0.0057 0.05714 BRL 2344-13587 13
4-Isopropyltoluene mg/kg dry0.0504 0.0057 0.05714 BRL 2232-14488 10
Acetone mg/kg dry0.0698 0.057 0.1143 0.00954 4934-14353 18
Benzene mg/kg dry0.0516 0.0034 0.05714 BRL 2060-13590 15
Bromobenzene mg/kg dry0.0486 0.0057 0.05714 BRL 2545-13585 15
Bromochloromethane mg/kg dry0.0559 0.0057 0.05714 BRL 1855-13698 18
Bromodichloromethane mg/kg dry0.0488 0.0057 0.05714 BRL 17 D55-12785 18
Bromoform mg/kg dry0.0453 0.0057 0.05714 BRL 3540-13679 13
Bromomethane mg/kg dry0.0297 0.011 0.05714 BRL 3030-13752 9
Carbon Tetrachloride mg/kg dry0.0546 0.0057 0.05714 BRL 2348-15396 16
Chlorobenzene mg/kg dry0.0547 0.0057 0.05714 BRL 1457-12596 14
Chloroethane mg/kg dry0.0475 0.011 0.05714 BRL 4716-17783 13
Chloroform mg/kg dry0.0520 0.0057 0.05714 BRL 1856-13791 15
Chloromethane mg/kg dry0.0398 0.0057 0.05714 BRL 2640-14570 13
cis-1,2-Dichloroethylene mg/kg dry0.0516 0.0057 0.05714 BRL 2858-14090 16
cis-1,3-Dichloropropylene mg/kg dry0.0429 0.0057 0.05714 BRL 3242-13575 12
Dibromochloromethane mg/kg dry0.0503 0.0057 0.05714 BRL 2449-12788 14
Dichlorodifluoromethane mg/kg dry0.0398 0.0057 0.05714 BRL 3725-15170 9
Ethylbenzene mg/kg dry0.0546 0.0057 0.05714 BRL 1944-14496 14
Isopropyl Ether mg/kg dry0.0469 0.0057 0.05714 BRL 13 D51-15582 18
Isopropylbenzene (Cumene)mg/kg dry0.0559 0.0057 0.05714 BRL 2741-14098 9
m,p-Xylenes mg/kg dry0.106 0.011 0.1143 BRL 2036-14893 13
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0191 0.057 0.05714 BRL 42 J30-14733 33
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0225 0.11 0.05714 0.00295 42 J24-16034 6
Methyl Isobutyl Ketone mg/kg dry0.0346 0.057 0.05714 BRL 44 J25-16361 14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7B0096 - 5035
Matrix Spike Dup (P7B0096-MSD1)Prepared: 02/06/17 Analyzed: 02/07/17 Source: 7020076-01
Methylene Chloride mg/kg dry0.0446 0.0057 0.05714 BRL 1453-14478 12
Methyl-tert-Butyl Ether mg/kg dry0.0474 0.011 0.05714 BRL 2249-13583 17
Naphthalene mg/kg dry0.0359 0.011 0.05714 0.00286 4432-12758 16
n-Butylbenzene mg/kg dry0.0476 0.0057 0.05714 BRL 3923-14883 14
n-Propylbenzene mg/kg dry0.0525 0.0057 0.05714 BRL 2735-14492 12
o-Xylene mg/kg dry0.0530 0.0057 0.05714 BRL 1743-14393 12
sec-Butylbenzene mg/kg dry0.0546 0.0057 0.05714 BRL 2834-14496 9
Styrene mg/kg dry0.0508 0.0057 0.05714 BRL 2842-13289 16
tert-Butylbenzene mg/kg dry0.0547 0.0057 0.05714 BRL 2936-15096 10
Tetrachloroethylene mg/kg dry0.0543 0.0057 0.05714 BRL 2647-14295 13
Toluene mg/kg dry0.0508 0.0057 0.05714 BRL 2257-13589 13
trans-1,2-Dichloroethylene mg/kg dry0.0563 0.0057 0.05714 BRL 18 D58-14199 19
trans-1,3-Dichloropropylene mg/kg dry0.0407 0.0057 0.05714 BRL 2041-12471 13
Trichloroethylene mg/kg dry0.0551 0.0057 0.05714 BRL 1838-16496 12
Trichlorofluoromethane mg/kg dry0.0524 0.0057 0.05714 BRL 2730-15792 12
Vinyl acetate mg/kg dryBRL0.029 0.05714 BRL 35 M61-154
Vinyl chloride mg/kg dry0.0474 0.0057 0.05714 BRL 3540-15683 8
Xylenes, total mg/kg dry0.159 0.017 0.1714 BRL 2036-14893 13
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10854.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9547.6
ug/L 50.00 76-129Surrogate: Toluene-d8 10552.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
Blank (P7B0114-BLK1)Prepared & Analyzed: 02/07/17
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
2,4,5-Trichlorophenol mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitroaniline mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
3-Nitroaniline mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitroaniline mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Aniline mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
Blank (P7B0114-BLK1)Prepared & Analyzed: 02/07/17
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.329 39-132Surrogate: 2,4,6-Tribromophenol 862.87
mg/kg wet 1.664 44-115Surrogate: 2-Fluorobiphenyl 811.34
mg/kg wet 3.329 35-115Surrogate: 2-Fluorophenol 832.75
mg/kg wet 1.664 37-122Surrogate: Nitrobenzene-d5 701.17
mg/kg wet 3.329 34-121Surrogate: Phenol-d5 862.86
mg/kg wet 1.664 54-127Surrogate: Terphenyl-d14 871.45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
LCS (P7B0114-BS1)Prepared & Analyzed: 02/07/17
1,2,4-Trichlorobenzene mg/kg wet1.10 0.33 1.666 34-11866
1,2-Dichlorobenzene mg/kg wet1.11 0.33 1.666 33-11767
1,3-Dichlorobenzene mg/kg wet1.10 0.33 1.666 30-11566
1,4-Dichlorobenzene mg/kg wet1.03 0.33 1.666 31-11562
2,4,5-Trichlorophenol mg/kg wet1.39 0.33 1.666 41-12483
2,4,6-Trichlorophenol mg/kg wet1.40 0.33 1.666 39-12684
2,4-Dichlorophenol mg/kg wet1.26 0.33 1.666 40-12275
2,4-Dimethylphenol mg/kg wet1.47 0.33 1.666 30-12788
2,4-Dinitrophenol mg/kg wet1.28 0.33 1.666 27-12977
2,4-Dinitrotoluene mg/kg wet1.38 0.33 1.666 48-12683
2,6-Dinitrotoluene mg/kg wet1.42 0.33 1.666 46-12485
2-Chloronaphthalene mg/kg wet1.31 0.33 1.666 41-11479
2-Chlorophenol mg/kg wet1.29 0.33 1.666 34-12178
2-Methylnaphthalene mg/kg wet1.12 0.33 1.666 38-12267
2-Methylphenol mg/kg wet1.45 0.33 1.666 32-12287
2-Nitroaniline mg/kg wet1.31 0.33 1.666 44-12779
2-Nitrophenol mg/kg wet1.16 0.33 1.666 36-12369
3,3'-Dichlorobenzidine mg/kg wet1.37 0.33 1.666 22-12183
3/4-Methylphenol mg/kg wet1.26 0.33 1.666 34-11976
3-Nitroaniline mg/kg wet1.22 0.33 1.666 33-11974
4,6-Dinitro-2-methylphenol mg/kg wet1.32 0.33 1.666 29-13279
4-Bromophenyl phenyl ether mg/kg wet1.37 0.33 1.666 46-12482
4-Chloro-3-methylphenol mg/kg wet1.28 0.33 1.666 45-12277
4-Chloroaniline mg/kg wet1.11 0.33 1.666 17-10666
4-Chlorophenyl phenyl ether mg/kg wet1.33 0.33 1.666 45-12180
4-Nitroaniline mg/kg wet1.16 0.33 1.666 63-14769
4-Nitrophenol mg/kg wet1.34 0.33 1.666 30-13280
Acenaphthene mg/kg wet1.36 0.33 1.666 40-12382
Acenaphthylene mg/kg wet1.32 0.33 1.666 32-13279
Aniline mg/kg wet1.79 0.33 1.666 12-197107
Anthracene mg/kg wet1.46 0.33 1.666 47-12388
Azobenzene mg/kg wet1.42 0.33 1.666 39-12586
Benzo(a)anthracene mg/kg wet1.32 0.33 1.666 49-12679
Benzo(a)pyrene mg/kg wet1.14 0.33 1.666 45-12969
Benzo(b)fluoranthene mg/kg wet1.16 0.33 1.666 45-13269
Benzo(g,h,i)perylene mg/kg wet1.13 0.33 1.666 43-13468
Benzo(k)fluoranthene mg/kg wet1.05 0.33 1.666 47-13263
Benzoic Acid mg/kg wet0.752 0.33 1.666 10-8345
Benzyl alcohol mg/kg wet1.32 0.33 1.666 29-12279
bis(2-Chloroethoxy)methane mg/kg wet1.13 0.33 1.666 36-12168
Bis(2-Chloroethyl)ether mg/kg wet1.05 0.33 1.666 31-12063
Bis(2-chloroisopropyl)ether mg/kg wet1.09 0.33 1.666 33-13165
Bis(2-Ethylhexyl)phthalate mg/kg wet1.42 0.33 1.666 51-13385
Butyl benzyl phthalate mg/kg wet1.40 0.33 1.666 48-13284
Chrysene mg/kg wet1.50 0.33 1.666 50-12490
Dibenzo(a,h)anthracene mg/kg wet0.773 0.33 1.666 45-13446
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
LCS (P7B0114-BS1)Prepared & Analyzed: 02/07/17
Dibenzofuran mg/kg wet1.37 0.33 1.666 44-12083
Diethyl phthalate mg/kg wet1.22 0.33 1.666 50-12473
Dimethyl phthalate mg/kg wet1.40 0.33 1.666 48-12484
Di-n-butyl phthalate mg/kg wet1.49 0.33 1.666 51-12889
Di-n-octyl phthalate mg/kg wet1.24 0.33 1.666 45-14074
Fluoranthene mg/kg wet1.46 0.33 1.666 50-12787
Fluorene mg/kg wet1.34 0.33 1.666 43-12581
Hexachlorobenzene mg/kg wet1.38 0.33 1.666 45-12283
Hexachlorobutadiene mg/kg wet1.15 0.33 1.666 32-12369
Hexachlorocyclopentadiene mg/kg wet0.716 0.33 1.666 32-11743
Hexachloroethane mg/kg wet1.00 0.33 1.666 28-11760
Indeno(1,2,3-cd)pyrene mg/kg wet1.37 0.33 1.666 45-13382
Isophorone mg/kg wet1.20 0.33 1.666 30-12272
Naphthalene mg/kg wet1.04 0.33 1.666 35-12362
Nitrobenzene mg/kg wet1.14 0.33 1.666 34-12269
N-Nitroso-di-n-propylamine mg/kg wet1.21 0.33 1.666 36-12073
N-Nitrosodiphenylamine mg/kg wet1.73 0.33 1.666 38-127104
Pentachlorophenol mg/kg wet1.65 0.33 1.666 25-13399
Phenanthrene mg/kg wet1.36 0.33 1.666 50-12182
Phenol mg/kg wet1.32 0.33 1.666 34-12179
Pyrene mg/kg wet1.34 0.33 1.666 47-12780
mg/kg wet 3.331 39-132Surrogate: 2,4,6-Tribromophenol 782.61
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 761.27
mg/kg wet 3.331 35-115Surrogate: 2-Fluorophenol 742.47
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 621.03
mg/kg wet 3.331 34-121Surrogate: Phenol-d5 782.58
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 731.22
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
LCS Dup (P7B0114-BSD1)Prepared & Analyzed: 02/07/17
1,2,4-Trichlorobenzene mg/kg wet1.09 0.33 1.659 2034-11866 1
1,2-Dichlorobenzene mg/kg wet1.10 0.33 1.659 2033-11766 0.6
1,3-Dichlorobenzene mg/kg wet1.07 0.33 1.659 2030-11565 2
1,4-Dichlorobenzene mg/kg wet1.05 0.33 1.659 2031-11563 2
2,4,5-Trichlorophenol mg/kg wet1.40 0.33 1.659 2041-12485 1
2,4,6-Trichlorophenol mg/kg wet1.42 0.33 1.659 2039-12685 1
2,4-Dichlorophenol mg/kg wet1.24 0.33 1.659 2040-12275 0.9
2,4-Dimethylphenol mg/kg wet1.50 0.33 1.659 2030-12791 2
2,4-Dinitrophenol mg/kg wet1.24 0.33 1.659 2027-12975 3
2,4-Dinitrotoluene mg/kg wet1.31 0.33 1.659 2048-12679 5
2,6-Dinitrotoluene mg/kg wet1.32 0.33 1.659 2046-12479 7
2-Chloronaphthalene mg/kg wet1.26 0.33 1.659 2041-11476 3
2-Chlorophenol mg/kg wet1.33 0.33 1.659 2034-12180 3
2-Methylnaphthalene mg/kg wet1.18 0.33 1.659 2038-12271 5
2-Methylphenol mg/kg wet1.37 0.33 1.659 2032-12283 5
2-Nitroaniline mg/kg wet1.06 0.33 1.659 20 D44-12764 21
2-Nitrophenol mg/kg wet1.18 0.33 1.659 2036-12371 2
3,3'-Dichlorobenzidine mg/kg wet1.34 0.33 1.659 2022-12181 3
3/4-Methylphenol mg/kg wet1.21 0.33 1.659 2034-11973 4
3-Nitroaniline mg/kg wet1.19 0.33 1.659 2033-11972 3
4,6-Dinitro-2-methylphenol mg/kg wet1.29 0.33 1.659 2029-13278 2
4-Bromophenyl phenyl ether mg/kg wet1.23 0.33 1.659 2046-12474 11
4-Chloro-3-methylphenol mg/kg wet1.32 0.33 1.659 2045-12280 3
4-Chloroaniline mg/kg wet1.07 0.33 1.659 2017-10664 3
4-Chlorophenyl phenyl ether mg/kg wet1.30 0.33 1.659 2045-12178 2
4-Nitroaniline mg/kg wet1.20 0.33 1.659 2063-14772 4
4-Nitrophenol mg/kg wet1.27 0.33 1.659 2030-13277 5
Acenaphthene mg/kg wet1.32 0.33 1.659 2040-12379 3
Acenaphthylene mg/kg wet1.32 0.33 1.659 2032-13279 0.3
Aniline mg/kg wet1.71 0.33 1.659 2012-197103 4
Anthracene mg/kg wet1.44 0.33 1.659 2047-12387 1
Azobenzene mg/kg wet1.45 0.33 1.659 2039-12587 2
Benzo(a)anthracene mg/kg wet1.33 0.33 1.659 2049-12680 0.7
Benzo(a)pyrene mg/kg wet0.971 0.33 1.659 2045-12959 16
Benzo(b)fluoranthene mg/kg wet1.17 0.33 1.659 2045-13271 1
Benzo(g,h,i)perylene mg/kg wet1.21 0.33 1.659 2043-13473 7
Benzo(k)fluoranthene mg/kg wet1.06 0.33 1.659 2047-13264 1
Benzoic Acid mg/kg wet0.719 0.33 1.659 2010-8343 5
Benzyl alcohol mg/kg wet1.26 0.33 1.659 2029-12276 5
bis(2-Chloroethoxy)methane mg/kg wet1.16 0.33 1.659 2036-12170 3
Bis(2-Chloroethyl)ether mg/kg wet0.950 0.33 1.659 2031-12057 10
Bis(2-chloroisopropyl)ether mg/kg wet1.09 0.33 1.659 2033-13166 0.5
Bis(2-Ethylhexyl)phthalate mg/kg wet1.41 0.33 1.659 2051-13385 0.8
Butyl benzyl phthalate mg/kg wet1.56 0.33 1.659 2048-13294 11
Chrysene mg/kg wet1.48 0.33 1.659 2050-12489 1
Dibenzo(a,h)anthracene mg/kg wet0.882 0.33 1.659 2045-13453 13
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
LCS Dup (P7B0114-BSD1)Prepared & Analyzed: 02/07/17
Dibenzofuran mg/kg wet1.31 0.33 1.659 2044-12079 4
Diethyl phthalate mg/kg wet1.24 0.33 1.659 2050-12475 2
Dimethyl phthalate mg/kg wet1.22 0.33 1.659 2048-12473 14
Di-n-butyl phthalate mg/kg wet1.52 0.33 1.659 2051-12891 2
Di-n-octyl phthalate mg/kg wet1.29 0.33 1.659 2045-14078 4
Fluoranthene mg/kg wet1.40 0.33 1.659 2050-12784 4
Fluorene mg/kg wet1.37 0.33 1.659 2043-12583 2
Hexachlorobenzene mg/kg wet1.30 0.33 1.659 2045-12278 6
Hexachlorobutadiene mg/kg wet1.16 0.33 1.659 2032-12370 1
Hexachlorocyclopentadiene mg/kg wet0.765 0.33 1.659 2032-11746 7
Hexachloroethane mg/kg wet1.06 0.33 1.659 2028-11764 5
Indeno(1,2,3-cd)pyrene mg/kg wet1.52 0.33 1.659 2045-13392 10
Isophorone mg/kg wet1.20 0.33 1.659 2030-12273 0.3
Naphthalene mg/kg wet1.06 0.33 1.659 2035-12364 3
Nitrobenzene mg/kg wet1.13 0.33 1.659 2034-12268 1
N-Nitroso-di-n-propylamine mg/kg wet1.19 0.33 1.659 2036-12072 2
N-Nitrosodiphenylamine mg/kg wet1.73 0.33 1.659 2038-127104 0.2
Pentachlorophenol mg/kg wet1.57 0.33 1.659 2025-13395 5
Phenanthrene mg/kg wet1.41 0.33 1.659 2050-12185 4
Phenol mg/kg wet1.30 0.33 1.659 2034-12179 1
Pyrene mg/kg wet1.61 0.33 1.659 2047-12797 19
mg/kg wet 3.318 39-132Surrogate: 2,4,6-Tribromophenol 802.65
mg/kg wet 1.659 44-115Surrogate: 2-Fluorobiphenyl 761.25
mg/kg wet 3.318 35-115Surrogate: 2-Fluorophenol 692.30
mg/kg wet 1.659 37-122Surrogate: Nitrobenzene-d5 621.04
mg/kg wet 3.318 34-121Surrogate: Phenol-d5 742.47
mg/kg wet 1.659 54-127Surrogate: Terphenyl-d14 831.38
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
Matrix Spike (P7B0114-MS1)Prepared & Analyzed: 02/07/17 Source: 7020076-01
1,2,4-Trichlorobenzene mg/kg dry1.19 0.37 1.856 BRL 34-11864
1,2-Dichlorobenzene mg/kg dry1.24 0.37 1.856 BRL 33-11767
1,3-Dichlorobenzene mg/kg dry1.18 0.37 1.856 BRL 30-11563
1,4-Dichlorobenzene mg/kg dry1.19 0.37 1.856 BRL 31-11564
2,4,5-Trichlorophenol mg/kg dry1.55 0.37 1.856 BRL 41-12483
2,4,6-Trichlorophenol mg/kg dry1.56 0.37 1.856 BRL 39-12684
2,4-Dichlorophenol mg/kg dry1.37 0.37 1.856 BRL 40-12274
2,4-Dimethylphenol mg/kg dry1.67 0.37 1.856 BRL 30-12790
2,4-Dinitrophenol mg/kg dry1.55 0.37 1.856 BRL 27-12983
2,4-Dinitrotoluene mg/kg dry1.58 0.37 1.856 BRL 48-12685
2,6-Dinitrotoluene mg/kg dry1.54 0.37 1.856 BRL 46-12483
2-Chloronaphthalene mg/kg dry1.42 0.37 1.856 BRL 41-11476
2-Chlorophenol mg/kg dry1.49 0.37 1.856 BRL 34-12180
2-Methylnaphthalene mg/kg dry1.29 0.37 1.856 BRL 38-12269
2-Methylphenol mg/kg dry1.53 0.37 1.856 BRL 32-12282
2-Nitroaniline mg/kg dry1.44 0.37 1.856 BRL 44-12777
2-Nitrophenol mg/kg dry1.31 0.37 1.856 BRL 36-12370
3,3'-Dichlorobenzidine mg/kg dry1.52 0.37 1.856 BRL 22-12182
3/4-Methylphenol mg/kg dry1.39 0.37 1.856 BRL 34-11975
3-Nitroaniline mg/kg dry1.33 0.37 1.856 BRL 33-11972
4,6-Dinitro-2-methylphenol mg/kg dry1.46 0.37 1.856 BRL 29-13278
4-Bromophenyl phenyl ether mg/kg dry1.53 0.37 1.856 BRL 46-12482
4-Chloro-3-methylphenol mg/kg dry1.48 0.37 1.856 BRL 45-12280
4-Chloroaniline mg/kg dry1.24 0.37 1.856 BRL 17-10667
4-Chlorophenyl phenyl ether mg/kg dry1.46 0.37 1.856 BRL 45-12179
4-Nitroaniline mg/kg dry1.33 0.37 1.856 BRL 63-14772
4-Nitrophenol mg/kg dry1.52 0.37 1.856 BRL 30-13282
Acenaphthene mg/kg dry1.52 0.37 1.856 BRL 40-12382
Acenaphthylene mg/kg dry1.49 0.37 1.856 BRL 32-13280
Aniline mg/kg dry1.88 0.37 1.856 BRL 12-197101
Anthracene mg/kg dry1.57 0.37 1.856 BRL 47-12385
Azobenzene mg/kg dry1.56 0.37 1.856 BRL 39-12584
Benzo(a)anthracene mg/kg dry1.53 0.37 1.856 BRL 49-12682
Benzo(a)pyrene mg/kg dry1.13 0.37 1.856 BRL 45-12961
Benzo(b)fluoranthene mg/kg dry1.17 0.37 1.856 BRL 45-13263
Benzo(g,h,i)perylene mg/kg dry1.15 0.37 1.856 BRL 43-13462
Benzo(k)fluoranthene mg/kg dry1.05 0.37 1.856 BRL 47-13256
Benzoic Acid mg/kg dry1.25 0.37 1.856 BRL 10-8368
Benzyl alcohol mg/kg dry1.42 0.37 1.856 BRL 29-12276
bis(2-Chloroethoxy)methane mg/kg dry1.26 0.37 1.856 BRL 36-12168
Bis(2-Chloroethyl)ether mg/kg dry1.16 0.37 1.856 BRL 31-12062
Bis(2-chloroisopropyl)ether mg/kg dry1.22 0.37 1.856 BRL 33-13166
Bis(2-Ethylhexyl)phthalate mg/kg dry1.63 0.37 1.856 BRL 51-13388
Butyl benzyl phthalate mg/kg dry1.61 0.37 1.856 BRL 48-13287
Chrysene mg/kg dry1.63 0.37 1.856 BRL 50-12488
Dibenzo(a,h)anthracene mg/kg dry0.841 0.37 1.856 BRL 45-13445
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
Matrix Spike (P7B0114-MS1)Prepared & Analyzed: 02/07/17 Source: 7020076-01
Dibenzofuran mg/kg dry1.51 0.37 1.856 BRL 44-12081
Diethyl phthalate mg/kg dry1.56 0.37 1.856 BRL 50-12484
Dimethyl phthalate mg/kg dry1.56 0.37 1.856 BRL 48-12484
Di-n-butyl phthalate mg/kg dry1.65 0.37 1.856 BRL 51-12889
Di-n-octyl phthalate mg/kg dry1.26 0.37 1.856 BRL 45-14068
Fluoranthene mg/kg dry1.52 0.37 1.856 BRL 50-12782
Fluorene mg/kg dry1.51 0.37 1.856 BRL 43-12581
Hexachlorobenzene mg/kg dry1.46 0.37 1.856 BRL 45-12279
Hexachlorobutadiene mg/kg dry1.33 0.37 1.856 BRL 32-12371
Hexachlorocyclopentadiene mg/kg dry0.659 0.37 1.856 BRL 32-11736
Hexachloroethane mg/kg dry1.18 0.37 1.856 BRL 28-11764
Indeno(1,2,3-cd)pyrene mg/kg dry1.51 0.37 1.856 BRL 45-13381
Isophorone mg/kg dry1.33 0.37 1.856 BRL 30-12272
Naphthalene mg/kg dry1.24 0.37 1.856 BRL 35-12367
Nitrobenzene mg/kg dry1.27 0.37 1.856 BRL 34-12268
N-Nitroso-di-n-propylamine mg/kg dry1.35 0.37 1.856 BRL 36-12073
N-Nitrosodiphenylamine mg/kg dry1.86 0.37 1.856 BRL 38-127100
Pentachlorophenol mg/kg dry1.76 0.37 1.856 BRL 25-13395
Phenanthrene mg/kg dry1.56 0.37 1.856 BRL 50-12184
Phenol mg/kg dry1.46 0.37 1.856 BRL 34-12179
Pyrene mg/kg dry1.55 0.37 1.856 BRL 47-12784
mg/kg dry 3.711 39-132Surrogate: 2,4,6-Tribromophenol 812.99
mg/kg dry 1.856 44-115Surrogate: 2-Fluorobiphenyl 751.40
mg/kg dry 3.711 35-115Surrogate: 2-Fluorophenol 762.81
mg/kg dry 1.856 37-122Surrogate: Nitrobenzene-d5 651.21
mg/kg dry 3.711 34-121Surrogate: Phenol-d5 762.81
mg/kg dry 1.856 54-127Surrogate: Terphenyl-d14 731.35
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
Matrix Spike Dup (P7B0114-MSD1)Prepared & Analyzed: 02/07/17 Source: 7020076-01
1,2,4-Trichlorobenzene mg/kg dry1.22 0.37 1.873 BRL 2034-11865 2
1,2-Dichlorobenzene mg/kg dry1.28 0.37 1.873 BRL 2033-11768 4
1,3-Dichlorobenzene mg/kg dry1.22 0.37 1.873 BRL 2030-11565 4
1,4-Dichlorobenzene mg/kg dry1.19 0.37 1.873 BRL 2031-11564 0.3
2,4,5-Trichlorophenol mg/kg dry1.49 0.37 1.873 BRL 2041-12479 4
2,4,6-Trichlorophenol mg/kg dry1.57 0.37 1.873 BRL 2039-12684 0.7
2,4-Dichlorophenol mg/kg dry1.37 0.37 1.873 BRL 2040-12273 0.2
2,4-Dimethylphenol mg/kg dry1.70 0.37 1.873 BRL 2030-12791 2
2,4-Dinitrophenol mg/kg dry1.60 0.37 1.873 BRL 2027-12985 3
2,4-Dinitrotoluene mg/kg dry1.55 0.37 1.873 BRL 2048-12683 1
2,6-Dinitrotoluene mg/kg dry1.53 0.37 1.873 BRL 2046-12482 0.8
2-Chloronaphthalene mg/kg dry1.44 0.37 1.873 BRL 2041-11477 2
2-Chlorophenol mg/kg dry1.51 0.37 1.873 BRL 2034-12181 1
2-Methylnaphthalene mg/kg dry1.33 0.37 1.873 BRL 2038-12271 3
2-Methylphenol mg/kg dry1.54 0.37 1.873 BRL 2032-12282 1
2-Nitroaniline mg/kg dry1.40 0.37 1.873 BRL 2044-12775 2
2-Nitrophenol mg/kg dry1.32 0.37 1.873 BRL 2036-12371 1
3,3'-Dichlorobenzidine mg/kg dry1.47 0.37 1.873 BRL 2022-12179 3
3/4-Methylphenol mg/kg dry1.40 0.37 1.873 BRL 2034-11975 0.4
3-Nitroaniline mg/kg dry1.35 0.37 1.873 BRL 2033-11972 1
4,6-Dinitro-2-methylphenol mg/kg dry1.42 0.37 1.873 BRL 2029-13276 2
4-Bromophenyl phenyl ether mg/kg dry1.48 0.37 1.873 BRL 2046-12479 3
4-Chloro-3-methylphenol mg/kg dry1.51 0.37 1.873 BRL 2045-12281 2
4-Chloroaniline mg/kg dry1.24 0.37 1.873 BRL 2017-10666 0.4
4-Chlorophenyl phenyl ether mg/kg dry1.47 0.37 1.873 BRL 2045-12179 1
4-Nitroaniline mg/kg dry1.32 0.37 1.873 BRL 2063-14771 0.6
4-Nitrophenol mg/kg dry1.48 0.37 1.873 BRL 2030-13279 3
Acenaphthene mg/kg dry1.52 0.37 1.873 BRL 2040-12381 0.06
Acenaphthylene mg/kg dry1.51 0.37 1.873 BRL 2032-13281 2
Aniline mg/kg dry1.92 0.37 1.873 BRL 2012-197102 2
Anthracene mg/kg dry1.53 0.37 1.873 BRL 2047-12382 3
Azobenzene mg/kg dry1.55 0.37 1.873 BRL 2039-12583 0.8
Benzo(a)anthracene mg/kg dry1.49 0.37 1.873 BRL 2049-12680 2
Benzo(a)pyrene mg/kg dry1.11 0.37 1.873 BRL 2045-12959 2
Benzo(b)fluoranthene mg/kg dry1.12 0.37 1.873 BRL 2045-13260 4
Benzo(g,h,i)perylene mg/kg dry1.16 0.37 1.873 BRL 2043-13462 0.7
Benzo(k)fluoranthene mg/kg dry1.03 0.37 1.873 BRL 2047-13255 1
Benzoic Acid mg/kg dry1.26 0.37 1.873 BRL 2010-8367 0.8
Benzyl alcohol mg/kg dry1.47 0.37 1.873 BRL 2029-12278 3
bis(2-Chloroethoxy)methane mg/kg dry1.27 0.37 1.873 BRL 2036-12168 0.9
Bis(2-Chloroethyl)ether mg/kg dry1.17 0.37 1.873 BRL 2031-12063 1
Bis(2-chloroisopropyl)ether mg/kg dry1.22 0.37 1.873 BRL 2033-13165 0.1
Bis(2-Ethylhexyl)phthalate mg/kg dry1.60 0.37 1.873 BRL 2051-13385 2
Butyl benzyl phthalate mg/kg dry1.57 0.37 1.873 BRL 2048-13284 3
Chrysene mg/kg dry1.59 0.37 1.873 BRL 2050-12485 2
Dibenzo(a,h)anthracene mg/kg dry0.846 0.37 1.873 BRL 2045-13445 0.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7B0114 - 3546
Matrix Spike Dup (P7B0114-MSD1)Prepared & Analyzed: 02/07/17 Source: 7020076-01
Dibenzofuran mg/kg dry1.53 0.37 1.873 BRL 2044-12082 2
Diethyl phthalate mg/kg dry1.55 0.37 1.873 BRL 2050-12483 0.6
Dimethyl phthalate mg/kg dry1.57 0.37 1.873 BRL 2048-12484 0.3
Di-n-butyl phthalate mg/kg dry1.59 0.37 1.873 BRL 2051-12885 4
Di-n-octyl phthalate mg/kg dry1.24 0.37 1.873 BRL 2045-14066 2
Fluoranthene mg/kg dry1.50 0.37 1.873 BRL 2050-12780 2
Fluorene mg/kg dry1.52 0.37 1.873 BRL 2043-12581 0.4
Hexachlorobenzene mg/kg dry1.48 0.37 1.873 BRL 2045-12279 1
Hexachlorobutadiene mg/kg dry1.32 0.37 1.873 BRL 2032-12371 0.2
Hexachlorocyclopentadiene mg/kg dry0.721 0.37 1.873 BRL 2032-11738 9
Hexachloroethane mg/kg dry1.19 0.37 1.873 BRL 2028-11764 0.5
Indeno(1,2,3-cd)pyrene mg/kg dry1.50 0.37 1.873 BRL 2045-13380 0.5
Isophorone mg/kg dry1.33 0.37 1.873 BRL 2030-12271 0.4
Naphthalene mg/kg dry1.28 0.37 1.873 BRL 2035-12368 3
Nitrobenzene mg/kg dry1.28 0.37 1.873 BRL 2034-12268 0.6
N-Nitroso-di-n-propylamine mg/kg dry1.36 0.37 1.873 BRL 2036-12072 0.5
N-Nitrosodiphenylamine mg/kg dry1.84 0.37 1.873 BRL 2038-12798 1
Pentachlorophenol mg/kg dry1.70 0.37 1.873 BRL 2025-13391 4
Phenanthrene mg/kg dry1.54 0.37 1.873 BRL 2050-12182 1
Phenol mg/kg dry1.47 0.37 1.873 BRL 2034-12178 0.6
Pyrene mg/kg dry1.52 0.37 1.873 BRL 2047-12781 2
mg/kg dry 3.746 39-132Surrogate: 2,4,6-Tribromophenol 782.92
mg/kg dry 1.873 44-115Surrogate: 2-Fluorobiphenyl 751.40
mg/kg dry 3.746 35-115Surrogate: 2-Fluorophenol 762.85
mg/kg dry 1.873 37-122Surrogate: Nitrobenzene-d5 651.21
mg/kg dry 3.746 34-121Surrogate: Phenol-d5 762.83
mg/kg dry 1.873 54-127Surrogate: Terphenyl-d14 711.32
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Organochlorine Pesticides by GC/ECD - Quality Control
Batch P7B0169 - 3546
Blank (P7B0169-BLK1)Prepared & Analyzed: 02/09/17
4,4'-DDD mg/kg wetBRL0.0020
4,4'-DDE mg/kg wetBRL0.0020
4,4'-DDT mg/kg wetBRL0.0030
Aldrin mg/kg wetBRL0.0020
alpha-BHC mg/kg wetBRL0.0020
cis-Chlordane mg/kg wetBRL0.0020
beta-BHC mg/kg wetBRL0.0020
Chlordane mg/kg wetBRL0.050
delta-BHC mg/kg wetBRL0.0020
Dieldrin mg/kg wetBRL0.0020
Endosulfan I mg/kg wetBRL0.0020
Endosulfan II mg/kg wetBRL0.0020
Endosulfan Sulfate mg/kg wetBRL0.0020
Endrin mg/kg wetBRL0.0020
Endrin Aldehyde mg/kg wetBRL0.0020
Endrin Ketone mg/kg wetBRL0.0020
gamma-BHC mg/kg wetBRL0.0020
trans-Chlordane mg/kg wetBRL0.0020
Heptachlor mg/kg wetBRL0.0020
Heptachlor Epoxide mg/kg wetBRL0.0020
Methoxychlor mg/kg wetBRL0.0020
Toxaphene mg/kg wetBRL0.050
mg/kg wet 0.03332 26-204Surrogate: Decachlorobiphenyl 950.0318
mg/kg wet 0.03332 40-162Surrogate: Tetrachloro-m-xylene 760.0254
LCS (P7B0169-BS1)Prepared & Analyzed: 02/09/17
4,4'-DDD mg/kg wet0.0331 0.0020 0.03331 56-13999
4,4'-DDE mg/kg wet0.0326 0.0020 0.03331 56-13498
4,4'-DDT mg/kg wet0.0349 0.0030 0.03331 50-145105
Aldrin mg/kg wet0.0276 0.0020 0.03331 45-13683
alpha-BHC mg/kg wet0.0254 0.0020 0.03331 45-13776
cis-Chlordane mg/kg wet0.0294 0.0020 0.03331 54-13388
beta-BHC mg/kg wet0.0280 0.0020 0.03331 50-13684
delta-BHC mg/kg wet0.0266 0.0020 0.03331 47-13980
Dieldrin mg/kg wet0.0299 0.0020 0.03331 56-13690
Endosulfan I mg/kg wet0.0280 0.0020 0.03331 53-13284
Endosulfan II mg/kg wet0.0316 0.0020 0.03331 53-13495
Endosulfan Sulfate mg/kg wet0.0320 0.0020 0.03331 55-13696
Endrin mg/kg wet0.0307 0.0020 0.03331 57-14092
Endrin Aldehyde mg/kg wet0.0301 0.0020 0.03331 35-13790
Endrin Ketone mg/kg wet0.0320 0.0020 0.03331 55-13696
gamma-BHC mg/kg wet0.0267 0.0020 0.03331 49-13580
trans-Chlordane mg/kg wet0.0296 0.0020 0.03331 53-13589
Heptachlor mg/kg wet0.0272 0.0020 0.03331 47-13682
Heptachlor Epoxide mg/kg wet0.0284 0.0020 0.03331 52-13685
Methoxychlor mg/kg wet0.0349 0.0020 0.03331 52-143105
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Organochlorine Pesticides by GC/ECD - Quality Control
Batch P7B0169 - 3546
LCS (P7B0169-BS1)Prepared & Analyzed: 02/09/17
mg/kg wet 0.03331 26-204Surrogate: Decachlorobiphenyl 980.0327
mg/kg wet 0.03331 40-162Surrogate: Tetrachloro-m-xylene 740.0245
LCS (P7B0169-BS2)Prepared & Analyzed: 02/09/17
Chlordane mg/kg wet0.263 0.050 0.3327 43-14979
mg/kg wet 0.03327 26-204Surrogate: Decachlorobiphenyl 940.0314
mg/kg wet 0.03327 40-162Surrogate: Tetrachloro-m-xylene 810.0269
LCS (P7B0169-BS3)Prepared & Analyzed: 02/09/17
Toxaphene mg/kg wet0.257 0.050 0.3332 33-14177
mg/kg wet 0.03332 26-204Surrogate: Decachlorobiphenyl 840.0279
mg/kg wet 0.03332 40-162Surrogate: Tetrachloro-m-xylene 810.0269
LCS Dup (P7B0169-BSD1)Prepared & Analyzed: 02/09/17
4,4'-DDD mg/kg wet0.0357 0.0020 0.03332 2056-139107 7
4,4'-DDE mg/kg wet0.0344 0.0020 0.03332 2056-134103 6
4,4'-DDT mg/kg wet0.0380 0.0030 0.03332 2050-145114 9
Aldrin mg/kg wet0.0284 0.0020 0.03332 2045-13685 3
alpha-BHC mg/kg wet0.0260 0.0020 0.03332 2045-13778 2
cis-Chlordane mg/kg wet0.0309 0.0020 0.03332 2054-13393 5
beta-BHC mg/kg wet0.0287 0.0020 0.03332 2050-13686 2
delta-BHC mg/kg wet0.0271 0.0020 0.03332 2047-13981 2
Dieldrin mg/kg wet0.0312 0.0020 0.03332 2056-13694 4
Endosulfan I mg/kg wet0.0291 0.0020 0.03332 2053-13287 4
Endosulfan II mg/kg wet0.0333 0.0020 0.03332 2053-134100 5
Endosulfan Sulfate mg/kg wet0.0342 0.0020 0.03332 2055-136103 7
Endrin mg/kg wet0.0323 0.0020 0.03332 2057-14097 5
Endrin Aldehyde mg/kg wet0.0300 0.0020 0.03332 2035-13790 0.5
Endrin Ketone mg/kg wet0.0347 0.0020 0.03332 2055-136104 8
gamma-BHC mg/kg wet0.0273 0.0020 0.03332 2049-13582 2
trans-Chlordane mg/kg wet0.0309 0.0020 0.03332 2053-13593 4
Heptachlor mg/kg wet0.0280 0.0020 0.03332 2047-13684 3
Heptachlor Epoxide mg/kg wet0.0294 0.0020 0.03332 2052-13688 3
Methoxychlor mg/kg wet0.0388 0.0020 0.03332 2052-143116 11
mg/kg wet 0.03332 26-204Surrogate: Decachlorobiphenyl 1080.0360
mg/kg wet 0.03332 40-162Surrogate: Tetrachloro-m-xylene 740.0248
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P7B0110 - 3546
Blank (P7B0110-BLK1)Prepared & Analyzed: 02/07/17
Aroclor 1016 mg/kg wetBRL0.050
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.050
Aroclor 1248 mg/kg wetBRL0.050
Aroclor 1254 mg/kg wetBRL0.050
Aroclor 1260 mg/kg wetBRL0.050
mg/kg wet 0.03333 36-182Surrogate: Tetrachloro-m-xylene 760.0252
mg/kg wet 0.03333 34-182Surrogate: Decachlorobiphenyl 950.0315
LCS (P7B0110-BS1)Prepared & Analyzed: 02/07/17
Aroclor 1016 mg/kg wet0.389 0.050 0.3324 64-151117
Aroclor 1260 mg/kg wet0.400 0.050 0.3324 45-166120
mg/kg wet 0.03324 36-182Surrogate: Tetrachloro-m-xylene 860.0284
mg/kg wet 0.03324 34-182Surrogate: Decachlorobiphenyl 970.0323
LCS Dup (P7B0110-BSD1)Prepared & Analyzed: 02/07/17
Aroclor 1016 mg/kg wet0.369 0.050 0.3331 5064-151111 5
Aroclor 1260 mg/kg wet0.367 0.050 0.3331 5045-166110 9
mg/kg wet 0.03331 36-182Surrogate: Tetrachloro-m-xylene 780.0261
mg/kg wet 0.03331 34-182Surrogate: Decachlorobiphenyl 840.0281
Matrix Spike (P7B0110-MS1)Prepared & Analyzed: 02/07/17 Source: 7020076-01
Aroclor 1016 mg/kg dry0.402 0.055 0.3673 BRL 14-192109
Aroclor 1260 mg/kg dry0.412 0.055 0.3673 BRL 10-192112
mg/kg dry 0.03673 36-182Surrogate: Tetrachloro-m-xylene 810.0299
mg/kg dry 0.03673 34-182Surrogate: Decachlorobiphenyl 900.0330
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P7B0110 - 3546
Matrix Spike Dup (P7B0110-MSD1)Prepared & Analyzed: 02/07/17 Source: 7020076-01
Aroclor 1016 mg/kg dry0.422 0.056 0.3751 BRL 5014-192112 5
Aroclor 1260 mg/kg dry0.433 0.056 0.3751 BRL 5010-192116 5
mg/kg dry 0.03751 36-182Surrogate: Tetrachloro-m-xylene 800.0299
mg/kg dry 0.03751 34-182Surrogate: Decachlorobiphenyl 850.0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Gasoline Range Organics by GC/FID - Quality Control
Batch P7B0145 - 5035
Blank (P7B0145-BLK1)Prepared & Analyzed: 02/08/17
Gasoline Range Organics mg/kg wetBRL5.0
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1025.10
LCS (P7B0145-BS1)Prepared & Analyzed: 02/08/17
Gasoline Range Organics mg/kg wet62.4 5.0 50.00 41-138125
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1055.25
LCS Dup (P7B0145-BSD1)Prepared & Analyzed: 02/08/17
Gasoline Range Organics mg/kg wet64.6 5.0 50.00 2041-138129 3
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1105.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Diesel Range Organics by GC/FID - Quality Control
Batch P7B0115 - 3546
Blank (P7B0115-BLK1)Prepared & Analyzed: 02/07/17
Diesel Range Organics mg/kg wetBRL7.0
mg/kg wet 1.327 49-124Surrogate: o-Terphenyl 650.864
LCS (P7B0115-BS1)Prepared & Analyzed: 02/07/17
Diesel Range Organics mg/kg wet67.8 7.0 66.53 55-109102
mg/kg wet 1.331 49-124Surrogate: o-Terphenyl 761.01
LCS Dup (P7B0115-BSD1)Prepared & Analyzed: 02/07/17
Diesel Range Organics mg/kg wet68.6 7.0 66.64 2055-109103 1
mg/kg wet 1.333 49-124Surrogate: o-Terphenyl 730.972
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7B0105 - 3050B
Blank (P7B0105-BLK1)Prepared: 02/07/17 Analyzed: 02/09/17
Arsenic mg/kg wetBRL0.25
Barium mg/kg wetBRL0.50
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wetBRL0.25
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL0.50
Silver mg/kg wetBRL0.25
LCS (P7B0105-BS1)Prepared: 02/07/17 Analyzed: 02/09/17
Arsenic mg/kg wet24.1 0.25 25.00 80-12096
Barium mg/kg wet24.2 0.50 25.00 80-12097
Cadmium mg/kg wet23.8 0.25 25.00 80-12095
Chromium mg/kg wet23.9 0.25 25.00 80-12095
Lead mg/kg wet23.4 0.25 25.00 80-12094
Selenium mg/kg wet23.5 0.50 25.00 80-12094
Silver mg/kg wet9.40 0.25 10.00 80-12094
Batch P7B0126 - 7471B
Blank (P7B0126-BLK1)Prepared & Analyzed: 02/08/17
Mercury mg/kg wetBRL0.020
LCS (P7B0126-BS1)Prepared & Analyzed: 02/08/17
Mercury mg/kg wet0.440 0.020 0.4167 80-120106
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 41
2/13/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 7020076
Time Submitted: 2/3/2017 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7B0109 - Solids, Dry Weight
Duplicate (P7B0109-DUP3)Prepared & Analyzed: 02/06/17 Source: 7020076-01
% Solids % by Weight89.0 0.100 88.8 200.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7B01157020076-01 02/07/17 10:4030.31 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7B01457020076-01 02/08/17 15:376.01 5g mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P7B01097020076-01 02/06/17 15:0330 30g g
P7B01097020076-02 02/06/17 15:0330 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7B01697020076-01 02/09/17 11:2030.05 10g mL
P7B01697020076-02 02/09/17 11:2030.05 10g mL
P7B01697020076-02 02/09/17 11:2030.05 10g mL
P7B01697020076-02 02/09/17 11:2030.05 10g mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7B01107020076-01 02/07/17 9:5630.16 10g mL
P7B01107020076-02 02/07/17 9:5630.37 10g mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7B01147020076-01 02/07/17 10:3830 1g mL
P7B01147020076-02 02/07/17 10:3830.02 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P7B01057020076-01 02/07/17 9:291.98 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P7B01267020076-01 02/08/17 7:550.57 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7B00967020076-01 02/06/17 14:235.95 5g mL
P7B00967020076-02 02/06/17 14:236.48 5g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7B01337020076-02 02/07/17 9:426.3 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Page 41 of 41
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
03/10/2017
McAdams (John R.) Company, Inc.
Sean Gallagher
2905 Meridian Pkwy
Durham, NC 27713
Project: McCall Farms (Wilson, NC)
Lab Submittal Date: 03/03/2017
Prism Work Order: 7030045
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
SE Surrogate recovery outside the QC limits due to emulsion.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Sample Receipt Summary
03/10/2017
Prism Work Order: 7030045
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030045-01 03/02/17TW-1 03/03/17Water
7030045-02 03/02/17TW-2 03/03/17Water
7030045-03 03/02/17TW-3 03/03/17Water
7030045-04 03/02/17TW-4 03/03/17Water
7030045-05 03/02/17TW-5 03/03/17Water
7030045-06 03/02/17TW-6 03/03/17Water
7030045-07 03/01/17Trans-B4 03/03/17Solid
Samples were received in good condition at 1.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 50
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030045
03/10/2017
Summary of Detections
47 mg/L7030045-01 TW-1 Chloride *9056A
0.52 mg/L7030045-01 TW-1 Nitrate/Nitrite as N *300.0
0.48 mg/L7030045-01 TW-1 Nitrate as N *9056A
7.8 mg/L7030045-01 TW-1 Sulfate *9056A
120 mg/L7030045-01 TW-1 Total Dissolved Solids *SM2540 C
0.56 ug/L7030045-01 TW-1 Chloromethane SM6200 B
51 mg/L7030045-02 TW-2 Chloride *9056A
2.0 mg/L7030045-02 TW-2 Nitrate/Nitrite as N *300.0
2.0 mg/L7030045-02 TW-2 Nitrate as N *9056A
85 mg/L7030045-02 TW-2 Sulfate *9056A
240 mg/L7030045-02 TW-2 Total Dissolved Solids *SM2540 C
2.0 mg/L7030045-02 TW-2 Total Nitrogen *Total Nitrogen
9.1 mg/L7030045-03 TW-3 Chloride *9056A
3.6 mg/L7030045-03 TW-3 Sulfate *9056A
74 mg/L7030045-03 TW-3 Total Dissolved Solids *SM2540 C
0.15 mg/L7030045-03 TW-3 Ammonia as N *SM4500-NH3 G
76 mg/L7030045-04 TW-4 Chloride *9056A
6.8 mg/L7030045-04 TW-4 Nitrate/Nitrite as N *300.0
6.7 mg/L7030045-04 TW-4 Nitrate as N *9056A
3.8 mg/L7030045-04 TW-4 Sulfate *9056A
250 mg/L7030045-04 TW-4 Total Dissolved Solids *SM2540 C
6.8 mg/L7030045-04 TW-4 Total Nitrogen *Total Nitrogen
0.21 mg/L7030045-04 TW-4 Ammonia as N *SM4500-NH3 G
5.1 J ug/L7030045-04 TW-4 Acetone SM6200 B
0.68 ug/L7030045-04 TW-4 Bromochloromethane SM6200 B
0.87 ug/L7030045-04 TW-4 Bromodichloromethane SM6200 B
3.3 ug/L7030045-04 TW-4 Bromoform SM6200 B
8.4 ug/L7030045-04 TW-4 Chloroform SM6200 B
1.9 ug/L7030045-04 TW-4 Dibromochloromethane SM6200 B
6.1 ug/L7030045-04 TW-4 Dibromomethane SM6200 B
100 mg/L7030045-05 TW-5 Chloride *9056A
8.6 mg/L7030045-05 TW-5 Nitrate/Nitrite as N *300.0
8.6 mg/L7030045-05 TW-5 Nitrate as N *9056A
310 mg/L7030045-05 TW-5 Total Dissolved Solids *SM2540 C
8.6 mg/L7030045-05 TW-5 Total Nitrogen *Total Nitrogen
14 ug/L7030045-05 TW-5 Bromodichloromethane SM6200 B
9.0 ug/L7030045-05 TW-5 Bromoform SM6200 B
90 ug/L7030045-05 TW-5 Chloroform SM6200 B
8.9 ug/L7030045-05 TW-5 Dibromochloromethane SM6200 B
0.58 ug/L7030045-05 TW-5 Tetrachloroethylene SM6200 B
11 mg/L7030045-06 TW-6 Chloride *9056A
0.12 mg/L7030045-06 TW-6 Nitrate as N *9056A
3.2 mg/L7030045-06 TW-6 Sulfate *9056A
110 mg/L7030045-06 TW-6 Total Dissolved Solids *SM2540 C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030045
03/10/2017
Summary of Detections
0.20 mg/L7030045-06 TW-6 Ammonia as N *SM4500-NH3 G
8.7 J ug/L7030045-06 TW-6 1-Methylnaphthalene 625
12 ug/L7030045-06 TW-6 2-Methylnaphthalene 625
31 ug/L7030045-06 TW-6 Naphthalene 625
200 ug/L7030045-06 TW-6 1,2,4-Trimethylbenzene SM6200 B
1.9 ug/L7030045-06 TW-6 1,3,5-Trimethylbenzene SM6200 B
0.73 ug/L7030045-06 TW-6 4-Isopropyltoluene SM6200 B
9.8 J ug/L7030045-06 TW-6 Acetone SM6200 B
56 ug/L7030045-06 TW-6 Benzene SM6200 B
80 ug/L7030045-06 TW-6 Ethylbenzene SM6200 B
8.1 ug/L7030045-06 TW-6 Isopropyl Ether SM6200 B
12 ug/L7030045-06 TW-6 Isopropylbenzene (Cumene)SM6200 B
23 ug/L7030045-06 TW-6 m,p-Xylenes SM6200 B
50 ug/L7030045-06 TW-6 Methyl-tert-Butyl Ether SM6200 B
77 ug/L7030045-06 TW-6 Naphthalene SM6200 B
1.8 ug/L7030045-06 TW-6 n-Butylbenzene SM6200 B
18 ug/L7030045-06 TW-6 n-Propylbenzene SM6200 B
1.4 ug/L7030045-06 TW-6 o-Xylene SM6200 B
2.5 ug/L7030045-06 TW-6 sec-Butylbenzene SM6200 B
2.8 ug/L7030045-06 TW-6 Toluene SM6200 B
24 ug/L7030045-06 TW-6 Xylenes, total SM6200 B
0.0021 J mg/kg dry7030045-07 Trans-B4 1,2-Dichlorobenzene 8260B
0.0021 J mg/kg dry7030045-07 Trans-B4 Toluene 8260B
1.6 mg/kg dry7030045-07 Trans-B4 Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 7030045-01
Prism Work Order: 7030045
Time Collected: 03/02/17 11:00
Time Submitted: 03/03/17 08:15
Anions by Ion Chromatography
47 *9056A P7C008711.0 3/3/17 14:15 EGCmg/L 0.044Chloride
0.52 *300.0 P7C008710.20 3/3/17 14:15 EGCmg/L 0.026Nitrate/Nitrite as N
0.48 *9056A P7C008710.10 3/3/17 14:15 EGCmg/L 0.017Nitrate as N
7.8 *9056A P7C008711.0 3/3/17 14:15 EGCmg/L 0.32Sulfate
General Chemistry Parameters
120 *SM2540 C P7C00981503/6/17 14:45 SLSmg/L 1.4Total Dissolved Solids
BRL *351.2 P7C010610.50 3/8/17 9:51 CLBmg/L 0.17Total Kjeldahl Nitrogen
BRL *Total Nitrogen [CALC]10.70 3/8/17 9:51 CLBmg/L 0.20Total Nitrogen
BRL *SM4500-NH3 G P7C010110.10 3/7/17 10:12 CLBmg/L 0.0046Ammonia as N
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL *8082A P7C015510.56 3/9/17 16:39 JMCug/L 0.28Aroclor 1016
BRL *8082A P7C015511.1 3/9/17 16:39 JMCug/L 0.12Aroclor 1221
BRL *8082A P7C015510.56 3/9/17 16:39 JMCug/L 0.18Aroclor 1232
BRL *8082A P7C015510.56 3/9/17 16:39 JMCug/L 0.16Aroclor 1242
BRL *8082A P7C015510.56 3/9/17 16:39 JMCug/L 0.16Aroclor 1248
BRL *8082A P7C015510.56 3/9/17 16:39 JMCug/L 0.18Aroclor 1254
BRL *8082A P7C015510.56 3/9/17 16:39 JMCCCVug/L 0.33Aroclor 1260
Surrogate Recovery Control Limits
30-16184 %Tetrachloro-m-xylene
32-178103 %Decachlorobiphenyl
Volatile Organic Compounds by GC/MS
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 16:58 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0501,4-Dichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 7030045-01
Prism Work Order: 7030045
Time Collected: 03/02/17 11:00
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012012.0 3/7/17 16:58 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P7C01201103/7/17 16:58 KDMug/L 0.31Acetone
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.048Benzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.057Bromobenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.040Bromoform
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.18Bromomethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.22Chloroethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.076Chloroform
0.56 SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.079Chloromethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.065Dibromomethane
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P7C012012003/7/17 16:58 KDMug/L 27Ethanol
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 16:58 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P7C012015.0 3/7/17 16:58 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P7C012012.0 3/7/17 16:58 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P7C012011.0 3/7/17 16:58 KDMug/L 0.19Naphthalene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.044o-Xylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.047Styrene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.044Toluene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.12trans-1,3-Dichloropropylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 7030045-01
Prism Work Order: 7030045
Time Collected: 03/02/17 11:00
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P7C012015.0 3/7/17 16:58 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P7C012010.50 3/7/17 16:58 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P7C012011.5 3/7/17 16:58 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13090 %4-Bromofluorobenzene
70-13090 %Dibromofluoromethane
70-13084 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-2
Prism Sample ID: 7030045-02
Prism Work Order: 7030045
Time Collected: 03/02/17 12:00
Time Submitted: 03/03/17 08:15
Anions by Ion Chromatography
51 *9056A P7C008711.0 3/3/17 14:31 EGCmg/L 0.044Chloride
2.0 *300.0 P7C008710.20 3/3/17 14:31 EGCmg/L 0.026Nitrate/Nitrite as N
2.0 *9056A P7C008710.10 3/3/17 14:31 EGCmg/L 0.017Nitrate as N
85 *9056A P7C008711.0 3/3/17 14:31 EGCmg/L 0.32Sulfate
General Chemistry Parameters
240 *SM2540 C P7C00981503/6/17 14:45 SLSmg/L 1.4Total Dissolved Solids
BRL *351.2 P7C010610.50 3/8/17 9:51 CLBmg/L 0.17Total Kjeldahl Nitrogen
2.0 *Total Nitrogen [CALC]10.70 3/8/17 9:51 CLBmg/L 0.20Total Nitrogen
BRL *SM4500-NH3 G P7C010110.10 3/7/17 10:12 CLBmg/L 0.0046Ammonia as N
Volatile Organic Compounds by GC/MS
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 17:24 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P7C012012.0 3/7/17 17:24 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P7C01201103/7/17 17:24 KDMug/L 0.31Acetone
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.048Benzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.057Bromobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.040Bromoform
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.18Bromomethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-2
Prism Sample ID: 7030045-02
Prism Work Order: 7030045
Time Collected: 03/02/17 12:00
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.22Chloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.076Chloroform
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.079Chloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.065Dibromomethane
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P7C012012003/7/17 17:24 KDMug/L 27Ethanol
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 17:24 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P7C012015.0 3/7/17 17:24 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P7C012012.0 3/7/17 17:24 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P7C012011.0 3/7/17 17:24 KDMug/L 0.19Naphthalene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.044o-Xylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.047Styrene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.044Toluene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P7C012015.0 3/7/17 17:24 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P7C012010.50 3/7/17 17:24 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P7C012011.5 3/7/17 17:24 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13090 %4-Bromofluorobenzene
70-13092 %Dibromofluoromethane
70-13083 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-3
Prism Sample ID: 7030045-03
Prism Work Order: 7030045
Time Collected: 03/02/17 12:30
Time Submitted: 03/03/17 08:15
Anions by Ion Chromatography
9.1 *9056A P7C008711.0 3/3/17 15:19 EGCmg/L 0.044Chloride
BRL *300.0 P7C008710.20 3/3/17 15:19 EGCmg/L 0.026Nitrate/Nitrite as N
BRL *9056A P7C008710.10 3/3/17 15:19 EGCmg/L 0.017Nitrate as N
3.6 *9056A P7C008711.0 3/3/17 15:19 EGCmg/L 0.32Sulfate
General Chemistry Parameters
74 *SM2540 C P7C00981503/6/17 14:45 SLSmg/L 1.4Total Dissolved Solids
BRL *351.2 P7C010610.50 3/8/17 9:51 CLBmg/L 0.17Total Kjeldahl Nitrogen
BRL *Total Nitrogen [CALC]10.70 3/8/17 9:51 CLBmg/L 0.20Total Nitrogen
0.15 *SM4500-NH3 G P7C010110.10 3/7/17 10:12 CLBmg/L 0.0046Ammonia as N
Volatile Organic Compounds by GC/MS
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 17:50 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P7C012012.0 3/7/17 17:50 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P7C01201103/7/17 17:50 KDMug/L 0.31Acetone
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.048Benzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.057Bromobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.040Bromoform
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.18Bromomethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-3
Prism Sample ID: 7030045-03
Prism Work Order: 7030045
Time Collected: 03/02/17 12:30
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.22Chloroethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.076Chloroform
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.079Chloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.065Dibromomethane
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P7C012012003/7/17 17:50 KDMug/L 27Ethanol
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 17:50 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P7C012015.0 3/7/17 17:50 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P7C012012.0 3/7/17 17:50 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P7C012011.0 3/7/17 17:50 KDMug/L 0.19Naphthalene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.044o-Xylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.047Styrene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.044Toluene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P7C012015.0 3/7/17 17:50 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P7C012010.50 3/7/17 17:50 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P7C012011.5 3/7/17 17:50 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13088 %4-Bromofluorobenzene
70-13093 %Dibromofluoromethane
70-13082 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-4
Prism Sample ID: 7030045-04
Prism Work Order: 7030045
Time Collected: 03/02/17 13:00
Time Submitted: 03/03/17 08:15
Anions by Ion Chromatography
76 *9056A P7C008711.0 3/3/17 15:34 EGCmg/L 0.044Chloride
6.8 *300.0 P7C008710.20 3/3/17 15:34 EGCmg/L 0.026Nitrate/Nitrite as N
6.7 *9056A P7C008710.10 3/3/17 15:34 EGCmg/L 0.017Nitrate as N
3.8 *9056A P7C008711.0 3/3/17 15:34 EGCmg/L 0.32Sulfate
General Chemistry Parameters
250 *SM2540 C P7C00981503/6/17 15:06 SLSmg/L 1.4Total Dissolved Solids
BRL *351.2 P7C010610.50 3/8/17 9:51 CLBmg/L 0.17Total Kjeldahl Nitrogen
6.8 *Total Nitrogen [CALC]10.70 3/8/17 9:51 CLBmg/L 0.20Total Nitrogen
0.21 *SM4500-NH3 G P7C010110.10 3/7/17 10:12 CLBmg/L 0.0046Ammonia as N
Volatile Organic Compounds by GC/MS
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 18:16 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P7C012012.0 3/7/17 18:16 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.0894-Isopropyltoluene
5.1 SM6200 B P7C01201103/7/17 18:16 KDMJug/L 0.31Acetone
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.048Benzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.057Bromobenzene
0.68 SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.14Bromochloromethane
0.87 SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.062Bromodichloromethane
3.3 SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.040Bromoform
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.18Bromomethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-4
Prism Sample ID: 7030045-04
Prism Work Order: 7030045
Time Collected: 03/02/17 13:00
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.22Chloroethane
8.4 SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.076Chloroform
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.079Chloromethane
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.079cis-1,3-Dichloropropylene
1.9 SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.081Dibromochloromethane
6.1 SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.065Dibromomethane
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P7C012012003/7/17 18:16 KDMug/L 27Ethanol
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 18:16 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P7C012015.0 3/7/17 18:16 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P7C012012.0 3/7/17 18:16 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P7C012011.0 3/7/17 18:16 KDMug/L 0.19Naphthalene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.044o-Xylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.047Styrene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.044Toluene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P7C012015.0 3/7/17 18:16 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P7C012010.50 3/7/17 18:16 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P7C012011.5 3/7/17 18:16 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13088 %4-Bromofluorobenzene
70-13093 %Dibromofluoromethane
70-13082 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-5
Prism Sample ID: 7030045-05
Prism Work Order: 7030045
Time Collected: 03/02/17 13:30
Time Submitted: 03/03/17 08:15
Anions by Ion Chromatography
100 *9056A P7C008711.0 3/3/17 15:50 EGCmg/L 0.044Chloride
8.6 *300.0 P7C008710.20 3/3/17 15:50 EGCmg/L 0.026Nitrate/Nitrite as N
8.6 *9056A P7C008710.10 3/3/17 15:50 EGCmg/L 0.017Nitrate as N
BRL *9056A P7C008711.0 3/3/17 15:50 EGCmg/L 0.32Sulfate
General Chemistry Parameters
310 *SM2540 C P7C00981503/6/17 15:06 SLSmg/L 1.4Total Dissolved Solids
BRL *351.2 P7C010610.50 3/8/17 9:51 CLBmg/L 0.17Total Kjeldahl Nitrogen
8.6 *Total Nitrogen [CALC]10.70 3/8/17 9:51 CLBmg/L 0.20Total Nitrogen
BRL *SM4500-NH3 G P7C010110.10 3/7/17 10:12 CLBmg/L 0.0046Ammonia as N
Volatile Organic Compounds by GC/MS
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 18:42 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P7C012012.0 3/7/17 18:42 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P7C01201103/7/17 18:42 KDMug/L 0.31Acetone
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.048Benzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.057Bromobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.14Bromochloromethane
14 SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.062Bromodichloromethane
9.0 SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.040Bromoform
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.18Bromomethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-5
Prism Sample ID: 7030045-05
Prism Work Order: 7030045
Time Collected: 03/02/17 13:30
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.22Chloroethane
90 SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.076Chloroform
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.079Chloromethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.079cis-1,3-Dichloropropylene
8.9 SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.065Dibromomethane
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P7C012012003/7/17 18:42 KDMug/L 27Ethanol
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 18:42 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P7C012015.0 3/7/17 18:42 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P7C012012.0 3/7/17 18:42 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P7C012011.0 3/7/17 18:42 KDMug/L 0.19Naphthalene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.044o-Xylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.047Styrene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.088tert-Butylbenzene
0.58 SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.044Toluene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P7C012015.0 3/7/17 18:42 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P7C012010.50 3/7/17 18:42 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P7C012011.5 3/7/17 18:42 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13091 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13085 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-6
Prism Sample ID: 7030045-06
Prism Work Order: 7030045
Time Collected: 03/02/17 12:00
Time Submitted: 03/03/17 08:15
Anions by Ion Chromatography
11 *9056A P7C008711.0 3/3/17 16:06 EGCmg/L 0.044Chloride
BRL *300.0 P7C008710.20 3/3/17 16:06 EGCmg/L 0.026Nitrate/Nitrite as N
0.12 *9056A P7C008710.10 3/3/17 16:06 EGCmg/L 0.017Nitrate as N
3.2 *9056A P7C008711.0 3/3/17 16:06 EGCmg/L 0.32Sulfate
General Chemistry Parameters
110 *SM2540 C P7C00981503/6/17 15:06 SLSmg/L 1.4Total Dissolved Solids
BRL *351.2 P7C010610.50 3/8/17 9:51 CLBmg/L 0.17Total Kjeldahl Nitrogen
BRL *Total Nitrogen [CALC]10.70 3/8/17 9:51 CLBmg/L 0.20Total Nitrogen
0.20 *SM4500-NH3 G P7C010110.10 3/7/17 10:12 CLBmg/L 0.0046Ammonia as N
Semivolatile Organic Compounds by GC/MS
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.51,2,4-Trichlorobenzene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.41,2-Dichlorobenzene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.31,3-Dichlorobenzene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.41,4-Dichlorobenzene
8.7 625 P7C00551103/6/17 14:00 JMVJug/L 2.11-Methylnaphthalene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.82,4,6-Trichlorophenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.62,4-Dichlorophenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.12,4-Dimethylphenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.22,4-Dinitrophenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.92,4-Dinitrotoluene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.92,6-Dinitrotoluene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.32-Chloronaphthalene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.12-Chlorophenol
12 625 P7C00551103/6/17 14:00 JMVug/L 1.82-Methylnaphthalene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.42-Nitrophenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.83,3'-Dichlorobenzidine
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.23/4-Methylphenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.94,6-Dinitro-2-methylphenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.24-Bromophenyl phenyl ether
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.34-Chloro-3-methylphenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.74-Chloroaniline
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.24-Chlorophenyl phenyl ether
BRL 625 P7C00551503/6/17 14:00 JMVug/L 1.74-Nitrophenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.3Acenaphthene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.3Acenaphthylene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.2Anthracene
BRL 625 P7C005511003/6/17 14:00 JMVug/L 14Benzidine
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.1Benzo(a)anthracene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.6Benzo(a)pyrene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.5Benzo(b)fluoranthene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.5Benzo(g,h,i)perylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-6
Prism Sample ID: 7030045-06
Prism Work Order: 7030045
Time Collected: 03/02/17 12:00
Time Submitted: 03/03/17 08:15
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.8Benzo(k)fluoranthene
BRL 625 P7C005511003/6/17 14:00 JMVug/L 0.74Benzoic Acid
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.6Benzyl alcohol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.8bis(2-Chloroethoxy)methane
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.6Bis(2-Chloroethyl)ether
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.7Bis(2-chloroisopropyl)ether
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.1Bis(2-Ethylhexyl)phthalate
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.6Butyl benzyl phthalate
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.4Chrysene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.4Dibenzo(a,h)anthracene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.3Dibenzofuran
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.3Diethyl phthalate
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.5Dimethyl phthalate
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.4Di-n-butyl phthalate
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.6Di-n-octyl phthalate
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.5Fluoranthene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.8Fluorene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.5Hexachlorobenzene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.0Hexachlorobutadiene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.6Hexachlorocyclopentadiene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.5Hexachloroethane
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.1Indeno(1,2,3-cd)pyrene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.1Isophorone
31 625 P7C00551103/6/17 14:00 JMVug/L 2.1Naphthalene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 1.4Nitrobenzene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 0.83N-Nitrosodimethylamine
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.0N-Nitroso-di-n-propylamine
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.9N-Nitrosodiphenylamine
BRL 625 P7C00551103/6/17 14:00 JMVug/L 2.1Pentachlorophenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.2Phenanthrene
BRL 625 P7C00551103/6/17 14:00 JMVug/L 0.48Phenol
BRL 625 P7C00551103/6/17 14:00 JMVug/L 3.5Pyrene
Surrogate Recovery Control Limits
31-14414 %2,4,6-Tribromophenol SE
49-11848 %2-Fluorobiphenyl SE
22-842 %2-Fluorophenol SE
43-12346 %Nitrobenzene-d5
10-631 %Phenol-d5 SE
49-15153 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0361,1,2,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-6
Prism Sample ID: 7030045-06
Prism Work Order: 7030045
Time Collected: 03/02/17 12:00
Time Submitted: 03/03/17 08:15
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.131,2,4-Trichlorobenzene
200 SM6200 B P7C0120105.0 3/7/17 23:27 KDMug/L 0.541,2,4-Trimethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 23:01 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.111,2-Dichloropropane
1.9 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P7C012012.0 3/7/17 23:01 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0504-Chlorotoluene
0.73 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.0894-Isopropyltoluene
9.8 SM6200 B P7C01201103/7/17 23:01 KDMJug/L 0.31Acetone
56 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.048Benzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.057Bromobenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.040Bromoform
BRL SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.18Bromomethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.22Chloroethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.076Chloroform
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.079Chloromethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.065Dibromomethane
BRL SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P7C012012003/7/17 23:01 KDMug/L 27Ethanol
80 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P7C012012.0 3/7/17 23:01 KDMug/L 0.16Hexachlorobutadiene
8.1 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.050Isopropyl Ether
12 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.054Isopropylbenzene (Cumene)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Water
Client Sample ID: TW-6
Prism Sample ID: 7030045-06
Prism Work Order: 7030045
Time Collected: 03/02/17 12:00
Time Submitted: 03/03/17 08:15
23 SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P7C012015.0 3/7/17 23:01 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P7C012012.0 3/7/17 23:01 KDMug/L 0.083Methylene Chloride
50 SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.042Methyl-tert-Butyl Ether
77 SM6200 B P7C012011.0 3/7/17 23:01 KDMug/L 0.19Naphthalene
1.8 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.076n-Butylbenzene
18 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.087n-Propylbenzene
1.4 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.044o-Xylene
2.5 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.047Styrene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.098Tetrachloroethylene
2.8 SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.044Toluene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P7C012015.0 3/7/17 23:01 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P7C012010.50 3/7/17 23:01 KDMug/L 0.097Vinyl chloride
24 SM6200 B P7C012011.5 3/7/17 23:01 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13091 %4-Bromofluorobenzene
70-13092 %Dibromofluoromethane
70-13085 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Solid
Client Sample ID: Trans-B4
Prism Sample ID: 7030045-07
Prism Work Order: 7030045
Time Collected: 03/01/17 20:00
Time Submitted: 03/03/17 08:15
General Chemistry Parameters
90.6 *SM2540 G P7C008810.100 3/3/17 14:51 JLB% by
Weight
0.100% Solids
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL *8082A P7C013010.055 3/9/17 13:07 JMCmg/kg dry 0.011Aroclor 1016
BRL *8082A P7C013010.11 3/9/17 13:07 JMCmg/kg dry 0.044Aroclor 1221
BRL *8082A P7C013010.11 3/9/17 13:07 JMCmg/kg dry 0.014Aroclor 1232
BRL *8082A P7C013010.055 3/9/17 13:07 JMCmg/kg dry 0.015Aroclor 1242
BRL *8082A P7C013010.055 3/9/17 13:07 JMCmg/kg dry 0.011Aroclor 1248
BRL *8082A P7C013010.055 3/9/17 13:07 JMCmg/kg dry 0.014Aroclor 1254
BRL *8082A P7C013010.055 3/9/17 13:07 JMCCCVmg/kg dry 0.014Aroclor 1260
Surrogate Recovery Control Limits
36-18273 %Tetrachloro-m-xylene
34-182116 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0571,2,4-Trichlorobenzene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0551,2-Dichlorobenzene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0511,3-Dichlorobenzene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0531,4-Dichlorobenzene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0701-Methylnaphthalene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0682,4,6-Trichlorophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0702,4-Dichlorophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0562,4-Dimethylphenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0512,4-Dinitrophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0442,4-Dinitrotoluene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0482,6-Dinitrotoluene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0532-Chloronaphthalene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0522-Chlorophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0582-Methylnaphthalene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0472-Methylphenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0662-Nitrophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0723,3'-Dichlorobenzidine
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0453/4-Methylphenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0554,6-Dinitro-2-methylphenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0634-Bromophenyl phenyl ether
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0514-Chloro-3-methylphenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0444-Chloroaniline
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0474-Chlorophenyl phenyl ether
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.0564-Nitrophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.050Acenaphthene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.053Acenaphthylene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.059Anthracene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.048Azobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Solid
Client Sample ID: Trans-B4
Prism Sample ID: 7030045-07
Prism Work Order: 7030045
Time Collected: 03/01/17 20:00
Time Submitted: 03/03/17 08:15
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.048Benzo(a)anthracene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.039Benzo(a)pyrene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.042Benzo(b)fluoranthene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.040Benzo(g,h,i)perylene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.048Benzo(k)fluoranthene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.031Benzoic Acid
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.048Benzyl alcohol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.063bis(2-Chloroethoxy)methane
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.051Bis(2-Chloroethyl)ether
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.062Bis(2-chloroisopropyl)ether
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.054Bis(2-Ethylhexyl)phthalate
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.052Butyl benzyl phthalate
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.046Chrysene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.044Dibenzo(a,h)anthracene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.055Dibenzofuran
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.050Diethyl phthalate
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.048Dimethyl phthalate
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.052Di-n-butyl phthalate
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.045Di-n-octyl phthalate
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.046Fluoranthene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.052Fluorene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.058Hexachlorobenzene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.065Hexachlorobutadiene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.065Hexachlorocyclopentadiene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.061Hexachloroethane
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.042Indeno(1,2,3-cd)pyrene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.049Isophorone
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.059Naphthalene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.052Nitrobenzene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.057N-Nitroso-di-n-propylamine
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.055N-Nitrosodiphenylamine
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.043Pentachlorophenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.047Phenanthrene
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.054Phenol
BRL 8270D P7C012910.36 3/8/17 16:03 JMVmg/kg dry 0.048Pyrene
Surrogate Recovery Control Limits
39-132100 %2,4,6-Tribromophenol
44-11592 %2-Fluorobiphenyl
35-11595 %2-Fluorophenol
37-12287 %Nitrobenzene-d5
34-12194 %Phenol-d5
54-127107 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Solid
Client Sample ID: Trans-B4
Prism Sample ID: 7030045-07
Prism Work Order: 7030045
Time Collected: 03/01/17 20:00
Time Submitted: 03/03/17 08:15
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000381,1,1,2-Tetrachloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000221,1,1-Trichloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000311,1,2,2-Tetrachloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000411,1,2-Trichloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000131,1-Dichloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000201,1-Dichloroethylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000251,1-Dichloropropylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000261,2,3-Trichlorobenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000581,2,3-Trichloropropane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000341,2,4-Trichlorobenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000351,2,4-Trimethylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000181,2-Dibromoethane
0.0021 8260B P7C008910.0046 3/3/17 18:22 ANGJmg/kg dry 0.000221,2-Dichlorobenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000271,2-Dichloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000281,2-Dichloropropane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000351,3,5-Trimethylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000301,3-Dichlorobenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000231,3-Dichloropropane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000181,4-Dichlorobenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000222,2-Dichloropropane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000242-Chlorotoluene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000274-Chlorotoluene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.000224-Isopropyltoluene
See 8260ML 8260B P7C008910.046 3/3/17 18:22 ANGmg/kg dry 0.0011Acetone
BRL 8260B P7C008910.0027 3/3/17 18:22 ANGmg/kg dry 0.00027Benzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00038Bromobenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00025Bromochloromethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00026Bromodichloromethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00052Bromoform
BRL 8260B P7C008910.0092 3/3/17 18:22 ANGmg/kg dry 0.00057Bromomethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00023Carbon Tetrachloride
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00024Chlorobenzene
BRL 8260B P7C008910.0092 3/3/17 18:22 ANGmg/kg dry 0.00038Chloroethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00033Chloroform
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00031Chloromethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00020cis-1,2-Dichloroethylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00015cis-1,3-Dichloropropylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00019Dibromochloromethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00021Dichlorodifluoromethane
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00018Ethylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00019Isopropyl Ether
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00027Isopropylbenzene (Cumene)
BRL 8260B P7C008910.0092 3/3/17 18:22 ANGmg/kg dry 0.00042m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 50
Laboratory Report
03/10/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Sample Matrix: Solid
Client Sample ID: Trans-B4
Prism Sample ID: 7030045-07
Prism Work Order: 7030045
Time Collected: 03/01/17 20:00
Time Submitted: 03/03/17 08:15
BRL 8260B P7C008910.046 3/3/17 18:22 ANGmg/kg dry 0.00041Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7C008910.092 3/3/17 18:22 ANGmg/kg dry 0.00041Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7C008910.046 3/3/17 18:22 ANGmg/kg dry 0.00039Methyl Isobutyl Ketone
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00026Methylene Chloride
BRL 8260B P7C008910.0092 3/3/17 18:22 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether
BRL 8260B P7C008910.0092 3/3/17 18:22 ANGmg/kg dry 0.00014Naphthalene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00023n-Butylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00027n-Propylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00019o-Xylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00022sec-Butylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00028Styrene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00015tert-Butylbenzene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00022Tetrachloroethylene
0.0021 8260B P7C008910.0046 3/3/17 18:22 ANGJmg/kg dry 0.00026Toluene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00027trans-1,2-Dichloroethylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00024trans-1,3-Dichloropropylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00030Trichloroethylene
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00030Trichlorofluoromethane
BRL 8260B P7C008910.023 3/3/17 18:22 ANGmg/kg dry 0.00063Vinyl acetate
BRL 8260B P7C008910.0046 3/3/17 18:22 ANGmg/kg dry 0.00022Vinyl chloride
BRL 8260B P7C008910.014 3/3/17 18:22 ANGmg/kg dry 0.00086Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-129102 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
1.6 8260B P7C0104500.91 3/7/17 1:11 ANGmg/kg dry 0.17Acetone
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130129 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0089 - 5035
Blank (P7C0089-BLK1)Prepared & Analyzed: 03/03/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0089 - 5035
Blank (P7C0089-BLK1)Prepared & Analyzed: 03/03/17
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10552.6
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.6
LCS (P7C0089-BS1)Prepared & Analyzed: 03/03/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0470 0.0050 0.05000 72-11594
1,1,1-Trichloroethane mg/kg wet0.0546 0.0050 0.05000 67-131109
1,1,2,2-Tetrachloroethane mg/kg wet0.0511 0.0050 0.05000 56-126102
1,1,2-Trichloroethane mg/kg wet0.0514 0.0050 0.05000 70-133103
1,1-Dichloroethane mg/kg wet0.0501 0.0050 0.05000 74-127100
1,1-Dichloroethylene mg/kg wet0.0514 0.0050 0.05000 67-149103
1,1-Dichloropropylene mg/kg wet0.0534 0.0050 0.05000 71-130107
1,2,3-Trichlorobenzene mg/kg wet0.0465 0.0050 0.05000 68-13093
1,2,3-Trichloropropane mg/kg wet0.0478 0.0050 0.05000 60-13796
1,2,4-Trichlorobenzene mg/kg wet0.0463 0.0050 0.05000 66-12593
1,2,4-Trimethylbenzene mg/kg wet0.0492 0.0050 0.05000 69-12998
1,2-Dibromoethane mg/kg wet0.0546 0.0050 0.05000 70-132109
1,2-Dichlorobenzene mg/kg wet0.0479 0.0050 0.05000 72-12396
1,2-Dichloroethane mg/kg wet0.0499 0.0050 0.05000 68-128100
1,2-Dichloropropane mg/kg wet0.0518 0.0050 0.05000 73-130104
1,3,5-Trimethylbenzene mg/kg wet0.0486 0.0050 0.05000 69-12897
1,3-Dichlorobenzene mg/kg wet0.0475 0.0050 0.05000 71-12095
1,3-Dichloropropane mg/kg wet0.0517 0.0050 0.05000 75-124103
1,4-Dichlorobenzene mg/kg wet0.0475 0.0050 0.05000 71-12395
2,2-Dichloropropane mg/kg wet0.0478 0.0050 0.05000 50-14296
2-Chlorotoluene mg/kg wet0.0485 0.0050 0.05000 67-12497
4-Chlorotoluene mg/kg wet0.0488 0.0050 0.05000 71-12698
4-Isopropyltoluene mg/kg wet0.0477 0.0050 0.05000 68-12995
Acetone mg/kg wet0.0897 0.050 0.1000 29-19890
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0089 - 5035
LCS (P7C0089-BS1)Prepared & Analyzed: 03/03/17
Benzene mg/kg wet0.0514 0.0030 0.05000 74-127103
Bromobenzene mg/kg wet0.0476 0.0050 0.05000 73-12595
Bromochloromethane mg/kg wet0.0497 0.0050 0.05000 72-13499
Bromodichloromethane mg/kg wet0.0512 0.0050 0.05000 75-122102
Bromoform mg/kg wet0.0489 0.0050 0.05000 66-13598
Bromomethane mg/kg wet0.0512 0.010 0.05000 20-180102
Carbon Tetrachloride mg/kg wet0.0485 0.0050 0.05000 64-14397
Chlorobenzene mg/kg wet0.0515 0.0050 0.05000 74-118103
Chloroethane mg/kg wet0.0579 0.010 0.05000 33-149116
Chloroform mg/kg wet0.0515 0.0050 0.05000 73-127103
Chloromethane mg/kg wet0.0458 0.0050 0.05000 45-14392
cis-1,2-Dichloroethylene mg/kg wet0.0517 0.0050 0.05000 76-134103
cis-1,3-Dichloropropylene mg/kg wet0.0500 0.0050 0.05000 71-125100
Dibromochloromethane mg/kg wet0.0466 0.0050 0.05000 73-12293
Dichlorodifluoromethane mg/kg wet0.0448 0.0050 0.05000 26-14690
Ethylbenzene mg/kg wet0.0521 0.0050 0.05000 74-128104
Isopropyl Ether mg/kg wet0.0491 0.0050 0.05000 59-15998
Isopropylbenzene (Cumene)mg/kg wet0.0488 0.0050 0.05000 68-12698
m,p-Xylenes mg/kg wet0.106 0.010 0.1000 75-124106
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0512 0.050 0.05000 61-157102
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0481 0.10 0.05000 J63-14996
Methyl Isobutyl Ketone mg/kg wet0.0525 0.050 0.05000 57-162105
Methylene Chloride mg/kg wet0.0489 0.0050 0.05000 74-12998
Methyl-tert-Butyl Ether mg/kg wet0.0501 0.010 0.05000 70-130100
Naphthalene mg/kg wet0.0474 0.010 0.05000 57-15795
n-Butylbenzene mg/kg wet0.0494 0.0050 0.05000 65-13599
n-Propylbenzene mg/kg wet0.0497 0.0050 0.05000 67-13099
o-Xylene mg/kg wet0.0517 0.0050 0.05000 74-126103
sec-Butylbenzene mg/kg wet0.0492 0.0050 0.05000 66-13198
Styrene mg/kg wet0.0522 0.0050 0.05000 77-121104
tert-Butylbenzene mg/kg wet0.0472 0.0050 0.05000 67-13294
Tetrachloroethylene mg/kg wet0.0501 0.0050 0.05000 68-130100
Toluene mg/kg wet0.0519 0.0050 0.05000 71-129104
trans-1,2-Dichloroethylene mg/kg wet0.0514 0.0050 0.05000 73-132103
trans-1,3-Dichloropropylene mg/kg wet0.0490 0.0050 0.05000 68-12398
Trichloroethylene mg/kg wet0.0510 0.0050 0.05000 75-133102
Trichlorofluoromethane mg/kg wet0.0549 0.0050 0.05000 44-146110
Vinyl acetate mg/kg wet0.0465 0.025 0.05000 85-16193
Vinyl chloride mg/kg wet0.0490 0.0050 0.05000 48-14798
Xylenes, total mg/kg wet0.158 0.015 0.1500 74-126105
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.3
ug/L 50.00 76-129Surrogate: Toluene-d8 10049.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0089 - 5035
LCS Dup (P7C0089-BSD1)Prepared & Analyzed: 03/03/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0468 0.0050 0.05000 2072-11594 0.4
1,1,1-Trichloroethane mg/kg wet0.0534 0.0050 0.05000 2067-131107 2
1,1,2,2-Tetrachloroethane mg/kg wet0.0510 0.0050 0.05000 2056-126102 0.1
1,1,2-Trichloroethane mg/kg wet0.0507 0.0050 0.05000 2070-133101 1
1,1-Dichloroethane mg/kg wet0.0486 0.0050 0.05000 2074-12797 3
1,1-Dichloroethylene mg/kg wet0.0498 0.0050 0.05000 2067-149100 3
1,1-Dichloropropylene mg/kg wet0.0516 0.0050 0.05000 2071-130103 3
1,2,3-Trichlorobenzene mg/kg wet0.0476 0.0050 0.05000 2068-13095 2
1,2,3-Trichloropropane mg/kg wet0.0492 0.0050 0.05000 2060-13798 3
1,2,4-Trichlorobenzene mg/kg wet0.0474 0.0050 0.05000 2066-12595 2
1,2,4-Trimethylbenzene mg/kg wet0.0481 0.0050 0.05000 2069-12996 2
1,2-Dibromoethane mg/kg wet0.0540 0.0050 0.05000 2070-132108 1
1,2-Dichlorobenzene mg/kg wet0.0478 0.0050 0.05000 2072-12396 0.3
1,2-Dichloroethane mg/kg wet0.0500 0.0050 0.05000 2068-128100 0.3
1,2-Dichloropropane mg/kg wet0.0510 0.0050 0.05000 2073-130102 2
1,3,5-Trimethylbenzene mg/kg wet0.0473 0.0050 0.05000 2069-12895 3
1,3-Dichlorobenzene mg/kg wet0.0465 0.0050 0.05000 2071-12093 2
1,3-Dichloropropane mg/kg wet0.0506 0.0050 0.05000 2075-124101 2
1,4-Dichlorobenzene mg/kg wet0.0472 0.0050 0.05000 2071-12394 0.5
2,2-Dichloropropane mg/kg wet0.0468 0.0050 0.05000 2050-14294 2
2-Chlorotoluene mg/kg wet0.0469 0.0050 0.05000 2067-12494 3
4-Chlorotoluene mg/kg wet0.0476 0.0050 0.05000 2071-12695 2
4-Isopropyltoluene mg/kg wet0.0465 0.0050 0.05000 2068-12993 3
Acetone mg/kg wet0.0908 0.050 0.1000 2029-19891 1
Benzene mg/kg wet0.0498 0.0030 0.05000 2074-127100 3
Bromobenzene mg/kg wet0.0464 0.0050 0.05000 2073-12593 3
Bromochloromethane mg/kg wet0.0488 0.0050 0.05000 2072-13498 2
Bromodichloromethane mg/kg wet0.0510 0.0050 0.05000 2075-122102 0.2
Bromoform mg/kg wet0.0509 0.0050 0.05000 2066-135102 4
Bromomethane mg/kg wet0.0529 0.010 0.05000 2020-180106 3
Carbon Tetrachloride mg/kg wet0.0478 0.0050 0.05000 2064-14396 1
Chlorobenzene mg/kg wet0.0501 0.0050 0.05000 2074-118100 3
Chloroethane mg/kg wet0.0597 0.010 0.05000 2033-149119 3
Chloroform mg/kg wet0.0507 0.0050 0.05000 2073-127101 2
Chloromethane mg/kg wet0.0490 0.0050 0.05000 2045-14398 7
cis-1,2-Dichloroethylene mg/kg wet0.0504 0.0050 0.05000 2076-134101 3
cis-1,3-Dichloropropylene mg/kg wet0.0496 0.0050 0.05000 2071-12599 0.6
Dibromochloromethane mg/kg wet0.0470 0.0050 0.05000 2073-12294 0.9
Dichlorodifluoromethane mg/kg wet0.0432 0.0050 0.05000 2026-14686 4
Ethylbenzene mg/kg wet0.0500 0.0050 0.05000 2074-128100 4
Isopropyl Ether mg/kg wet0.0485 0.0050 0.05000 2059-15997 1
Isopropylbenzene (Cumene)mg/kg wet0.0469 0.0050 0.05000 2068-12694 4
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 2075-124102 4
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0517 0.050 0.05000 2061-157103 1
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0486 0.10 0.05000 20 J63-14997 1
Methyl Isobutyl Ketone mg/kg wet0.0527 0.050 0.05000 2057-162105 0.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0089 - 5035
LCS Dup (P7C0089-BSD1)Prepared & Analyzed: 03/03/17
Methylene Chloride mg/kg wet0.0483 0.0050 0.05000 2074-12997 1
Methyl-tert-Butyl Ether mg/kg wet0.0503 0.010 0.05000 2070-130101 0.4
Naphthalene mg/kg wet0.0486 0.010 0.05000 2057-15797 3
n-Butylbenzene mg/kg wet0.0480 0.0050 0.05000 2065-13596 3
n-Propylbenzene mg/kg wet0.0480 0.0050 0.05000 2067-13096 3
o-Xylene mg/kg wet0.0498 0.0050 0.05000 2074-126100 4
sec-Butylbenzene mg/kg wet0.0472 0.0050 0.05000 2066-13194 4
Styrene mg/kg wet0.0508 0.0050 0.05000 2077-121102 3
tert-Butylbenzene mg/kg wet0.0461 0.0050 0.05000 2067-13292 2
Tetrachloroethylene mg/kg wet0.0486 0.0050 0.05000 2068-13097 3
Toluene mg/kg wet0.0505 0.0050 0.05000 2071-129101 3
trans-1,2-Dichloroethylene mg/kg wet0.0504 0.0050 0.05000 2073-132101 2
trans-1,3-Dichloropropylene mg/kg wet0.0496 0.0050 0.05000 2068-12399 1
Trichloroethylene mg/kg wet0.0494 0.0050 0.05000 2075-13399 3
Trichlorofluoromethane mg/kg wet0.0512 0.0050 0.05000 2044-146102 7
Vinyl acetate mg/kg wet0.0478 0.025 0.05000 2085-16196 3
Vinyl chloride mg/kg wet0.0468 0.0050 0.05000 2048-14794 5
Xylenes, total mg/kg wet0.152 0.015 0.1500 2074-126101 4
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.5
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10250.8
ug/L 50.00 76-129Surrogate: Toluene-d8 10049.8
Batch P7C0120 - SM6200 B
Blank (P7C0120-BLK1)Prepared & Analyzed: 03/07/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0120 - SM6200 B
Blank (P7C0120-BLK1)Prepared & Analyzed: 03/07/17
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0120 - SM6200 B
Blank (P7C0120-BLK1)Prepared & Analyzed: 03/07/17
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9145.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9346.7
ug/L 50.00 70-130Surrogate: Toluene-d8 8442.0
LCS (P7C0120-BS1)Prepared & Analyzed: 03/07/17
1,1,1,2-Tetrachloroethane ug/L20.3 0.50 20.00 70-130102
1,1,1-Trichloroethane ug/L22.1 0.50 20.00 70-130111
1,1,2,2-Tetrachloroethane ug/L16.6 0.50 20.00 70-13083
1,1,2-Trichloroethane ug/L20.9 0.50 20.00 70-130105
1,1-Dichloroethane ug/L21.7 0.50 20.00 70-130109
1,1-Dichloroethylene ug/L20.8 0.50 20.00 70-130104
1,1-Dichloropropylene ug/L22.1 0.50 20.00 70-130110
1,2,3-Trichlorobenzene ug/L18.1 0.50 20.00 70-13090
1,2,3-Trichloropropane ug/L16.3 0.50 20.00 70-13082
1,2,4-Trichlorobenzene ug/L17.9 0.50 20.00 70-13090
1,2,4-Trimethylbenzene ug/L18.6 0.50 20.00 70-13093
1,2-Dibromo-3-chloropropane ug/L14.5 2.0 20.00 70-13073
1,2-Dibromoethane ug/L18.9 0.50 20.00 70-13095
1,2-Dichlorobenzene ug/L18.4 0.50 20.00 70-13092
1,2-Dichloroethane ug/L21.9 0.50 20.00 70-130110
1,2-Dichloropropane ug/L21.6 0.50 20.00 70-130108
1,3,5-Trimethylbenzene ug/L18.6 0.50 20.00 70-13093
1,3-Dichlorobenzene ug/L18.2 0.50 20.00 70-13091
1,3-Dichloropropane ug/L19.2 0.50 20.00 70-13096
1,4-Dichlorobenzene ug/L17.9 0.50 20.00 70-13090
2,2-Dichloropropane ug/L22.5 2.0 20.00 70-130112
2-Chlorotoluene ug/L17.9 0.50 20.00 70-13089
4-Chlorotoluene ug/L18.0 0.50 20.00 70-13090
4-Isopropyltoluene ug/L18.8 0.50 20.00 70-13094
Acetone ug/L29.8 10 40.00 40-16074
Benzene ug/L22.2 0.50 20.00 70-130111
Bromobenzene ug/L17.4 0.50 20.00 70-13087
Bromochloromethane ug/L22.3 0.50 20.00 70-130112
Bromodichloromethane ug/L22.8 0.50 20.00 70-130114
Bromoform ug/L16.6 0.50 20.00 70-13083
Bromomethane ug/L22.5 1.0 20.00 60-140113
Carbon Tetrachloride ug/L19.3 0.50 20.00 70-13097
Chlorobenzene ug/L20.0 0.50 20.00 70-130100
Chloroethane ug/L26.2 0.50 20.00 60-140131
Chloroform ug/L21.8 0.50 20.00 70-130109
Chloromethane ug/L16.4 0.50 20.00 60-14082
cis-1,2-Dichloroethylene ug/L21.9 0.50 20.00 70-130109
cis-1,3-Dichloropropylene ug/L22.1 0.50 20.00 70-130110
Dibromochloromethane ug/L18.2 0.50 20.00 70-13091
Dibromomethane ug/L21.1 0.50 20.00 70-130106
Dichlorodifluoromethane ug/L18.9 1.0 20.00 60-14095
Ethanol ug/L375 200 500.0 60-14075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0120 - SM6200 B
LCS (P7C0120-BS1)Prepared & Analyzed: 03/07/17
Ethylbenzene ug/L20.6 0.50 20.00 70-130103
Hexachlorobutadiene ug/L18.4 2.0 20.00 70-13092
Isopropyl Ether ug/L22.5 0.50 20.00 70-130113
Isopropylbenzene (Cumene)ug/L19.1 0.50 20.00 70-13095
m,p-Xylenes ug/L41.9 1.0 40.00 70-130105
Methyl Butyl Ketone (2-Hexanone)ug/L16.2 1.0 20.00 60-14081
Methyl Ethyl Ketone (2-Butanone)ug/L17.1 5.0 20.00 60-14085
Methyl Isobutyl Ketone ug/L18.4 1.0 20.00 60-14092
Methylene Chloride ug/L21.1 2.0 20.00 70-130106
Methyl-tert-Butyl Ether ug/L21.1 1.0 20.00 70-130106
Naphthalene ug/L16.5 1.0 20.00 70-13082
n-Butylbenzene ug/L18.8 0.50 20.00 70-13094
n-Propylbenzene ug/L19.1 0.50 20.00 70-13095
o-Xylene ug/L20.2 0.50 20.00 70-130101
sec-Butylbenzene ug/L19.0 0.50 20.00 70-13095
Styrene ug/L20.2 0.50 20.00 70-130101
tert-Butylbenzene ug/L18.3 0.50 20.00 70-13092
Tetrachloroethylene ug/L20.6 0.50 20.00 70-130103
Toluene ug/L22.5 0.50 20.00 70-130113
trans-1,2-Dichloroethylene ug/L21.3 0.50 20.00 70-130106
trans-1,3-Dichloropropylene ug/L21.7 0.50 20.00 70-130108
Trichloroethylene ug/L22.8 0.50 20.00 70-130114
Trichlorofluoromethane ug/L28.9 0.50 20.00 L160-140145
Vinyl acetate ug/L21.8 5.0 20.00 60-140109
Vinyl chloride ug/L20.1 0.50 20.00 60-140100
Xylenes, total ug/L62.2 1.5 60.00 70-130104
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9246.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.9
ug/L 50.00 70-130Surrogate: Toluene-d8 8743.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0120 - SM6200 B
LCS Dup (P7C0120-BSD1)Prepared & Analyzed: 03/07/17
1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 2070-13098 4
1,1,1-Trichloroethane ug/L21.1 0.50 20.00 2070-130106 5
1,1,2,2-Tetrachloroethane ug/L17.5 0.50 20.00 2070-13087 5
1,1,2-Trichloroethane ug/L21.3 0.50 20.00 2070-130106 2
1,1-Dichloroethane ug/L21.0 0.50 20.00 2070-130105 3
1,1-Dichloroethylene ug/L20.2 0.50 20.00 2070-130101 3
1,1-Dichloropropylene ug/L21.2 0.50 20.00 2070-130106 4
1,2,3-Trichlorobenzene ug/L18.3 0.50 20.00 2070-13091 0.9
1,2,3-Trichloropropane ug/L16.9 0.50 20.00 2070-13085 4
1,2,4-Trichlorobenzene ug/L17.8 0.50 20.00 2070-13089 0.7
1,2,4-Trimethylbenzene ug/L17.9 0.50 20.00 2070-13090 4
1,2-Dibromo-3-chloropropane ug/L16.2 2.0 20.00 2070-13081 11
1,2-Dibromoethane ug/L19.4 0.50 20.00 2070-13097 2
1,2-Dichlorobenzene ug/L17.7 0.50 20.00 2070-13089 4
1,2-Dichloroethane ug/L22.0 0.50 20.00 2070-130110 0.6
1,2-Dichloropropane ug/L21.3 0.50 20.00 2070-130106 1
1,3,5-Trimethylbenzene ug/L18.0 0.50 20.00 2070-13090 4
1,3-Dichlorobenzene ug/L17.8 0.50 20.00 2070-13089 2
1,3-Dichloropropane ug/L19.2 0.50 20.00 2070-13096 0.5
1,4-Dichlorobenzene ug/L17.5 0.50 20.00 2070-13088 2
2,2-Dichloropropane ug/L21.6 2.0 20.00 2070-130108 4
2-Chlorotoluene ug/L17.1 0.50 20.00 2070-13086 4
4-Chlorotoluene ug/L17.4 0.50 20.00 2070-13087 3
4-Isopropyltoluene ug/L18.1 0.50 20.00 2070-13090 4
Acetone ug/L35.4 10 40.00 2040-16088 17
Benzene ug/L21.4 0.50 20.00 2070-130107 4
Bromobenzene ug/L17.0 0.50 20.00 2070-13085 3
Bromochloromethane ug/L22.4 0.50 20.00 2070-130112 0.3
Bromodichloromethane ug/L22.4 0.50 20.00 2070-130112 2
Bromoform ug/L17.3 0.50 20.00 2070-13087 4
Bromomethane ug/L20.3 1.0 20.00 2060-140101 10
Carbon Tetrachloride ug/L18.8 0.50 20.00 2070-13094 3
Chlorobenzene ug/L19.3 0.50 20.00 2070-13097 4
Chloroethane ug/L23.9 0.50 20.00 2060-140120 9
Chloroform ug/L21.1 0.50 20.00 2070-130106 3
Chloromethane ug/L15.8 0.50 20.00 2060-14079 4
cis-1,2-Dichloroethylene ug/L21.0 0.50 20.00 2070-130105 4
cis-1,3-Dichloropropylene ug/L21.9 0.50 20.00 2070-130110 0.8
Dibromochloromethane ug/L18.0 0.50 20.00 2070-13090 1
Dibromomethane ug/L21.6 0.50 20.00 2070-130108 2
Dichlorodifluoromethane ug/L17.3 1.0 20.00 2060-14087 9
Ethanol ug/L520 200 500.0 20 D60-140104 32
Ethylbenzene ug/L19.9 0.50 20.00 2070-130100 4
Hexachlorobutadiene ug/L17.7 2.0 20.00 2070-13088 4
Isopropyl Ether ug/L22.1 0.50 20.00 2070-130110 2
Isopropylbenzene (Cumene)ug/L18.0 0.50 20.00 2070-13090 6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0120 - SM6200 B
LCS Dup (P7C0120-BSD1)Prepared & Analyzed: 03/07/17
m,p-Xylenes ug/L40.5 1.0 40.00 2070-130101 3
Methyl Butyl Ketone (2-Hexanone)ug/L18.5 1.0 20.00 2060-14093 13
Methyl Ethyl Ketone (2-Butanone)ug/L19.7 5.0 20.00 2060-14098 14
Methyl Isobutyl Ketone ug/L20.6 1.0 20.00 2060-140103 11
Methylene Chloride ug/L20.7 2.0 20.00 2070-130103 2
Methyl-tert-Butyl Ether ug/L21.2 1.0 20.00 2070-130106 0.2
Naphthalene ug/L17.5 1.0 20.00 2070-13088 6
n-Butylbenzene ug/L17.9 0.50 20.00 2070-13090 5
n-Propylbenzene ug/L18.2 0.50 20.00 2070-13091 5
o-Xylene ug/L19.5 0.50 20.00 2070-13097 4
sec-Butylbenzene ug/L18.1 0.50 20.00 2070-13090 5
Styrene ug/L19.7 0.50 20.00 2070-13099 3
tert-Butylbenzene ug/L17.6 0.50 20.00 2070-13088 4
Tetrachloroethylene ug/L19.7 0.50 20.00 2070-13098 4
Toluene ug/L21.8 0.50 20.00 2070-130109 3
trans-1,2-Dichloroethylene ug/L20.5 0.50 20.00 2070-130103 4
trans-1,3-Dichloropropylene ug/L22.1 0.50 20.00 2070-130110 2
Trichloroethylene ug/L22.1 0.50 20.00 2070-130111 3
Trichlorofluoromethane ug/L26.3 0.50 20.00 2060-140132 9
Vinyl acetate ug/L23.0 5.0 20.00 2060-140115 5
Vinyl chloride ug/L19.3 0.50 20.00 2060-14096 4
Xylenes, total ug/L60.0 1.5 60.00 2070-130100 4
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9145.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.9
ug/L 50.00 70-130Surrogate: Toluene-d8 8643.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7C0104 - 5035
Blank (P7C0104-BLK1)Prepared & Analyzed: 03/06/17
Acetone mg/kg wetBRL0.020
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.2
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 11055.1
ug/L 50.00 70-130Surrogate: Toluene-d8 11858.9
LCS (P7C0104-BS1)Prepared & Analyzed: 03/06/17
Acetone mg/kg wet0.0728 0.020 0.1000 12-19673
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10652.8
ug/L 50.00 70-130Surrogate: Toluene-d8 11758.6
LCS Dup (P7C0104-BSD1)Prepared & Analyzed: 03/06/17
Acetone mg/kg wet0.0771 0.020 0.1000 2012-19677 6
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10753.4
ug/L 50.00 70-130Surrogate: Toluene-d8 11658.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0055 - 625
Blank (P7C0055-BLK1)Prepared: 03/03/17 Analyzed: 03/06/17
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1-Methylnaphthalene ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3'-Dichlorobenzidine ug/LBRL10
3/4-Methylphenol ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitrophenol ug/LBRL50
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Anthracene ug/LBRL10
Benzidine ug/LBRL100
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzoic Acid ug/LBRL100
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chrysene ug/LBRL10
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0055 - 625
Blank (P7C0055-BLK1)Prepared: 03/03/17 Analyzed: 03/06/17
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isophorone ug/LBRL10
Naphthalene ug/LBRL10
Nitrobenzene ug/LBRL10
N-Nitrosodimethylamine ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Pyrene ug/LBRL10
ug/L 100.0 31-144Surrogate: 2,4,6-Tribromophenol 8786.7
ug/L 50.00 49-118Surrogate: 2-Fluorobiphenyl 8643.0
ug/L 100.0 22-84Surrogate: 2-Fluorophenol 6059.9
ug/L 50.00 43-123Surrogate: Nitrobenzene-d5 8341.6
ug/L 100.0 10-63Surrogate: Phenol-d5 3838.4
ug/L 50.00 49-151Surrogate: Terphenyl-d14 10351.3
LCS (P7C0055-BS1)Prepared: 03/03/17 Analyzed: 03/06/17
1,2,4-Trichlorobenzene ug/L66.0 10 100.0 44-14266
1,2-Dichlorobenzene ug/L71.8 10 100.0 32-12972
1,3-Dichlorobenzene ug/L72.3 10 100.0 20-12472
1,4-Dichlorobenzene ug/L71.6 10 100.0 20-12472
1-Methylnaphthalene ug/L76.5 10 100.0 40-13577
2,4,6-Trichlorophenol ug/L94.6 10 100.0 37-14495
2,4-Dichlorophenol ug/L70.0 10 100.0 39-13570
2,4-Dimethylphenol ug/L81.5 10 100.0 32-11982
2,4-Dinitrophenol ug/L97.8 10 100.0 10-19198
2,4-Dinitrotoluene ug/L10410 100.0 39-139104
2,6-Dinitrotoluene ug/L10110 100.0 50-158101
2-Chloronaphthalene ug/L91.4 10 100.0 60-11891
2-Chlorophenol ug/L81.9 10 100.0 23-13482
2-Methylnaphthalene ug/L72.7 10 100.0 18-12173
2-Nitrophenol ug/L71.3 10 100.0 29-18271
3,3'-Dichlorobenzidine ug/L96.5 10 100.0 10-26297
3/4-Methylphenol ug/L65.4 10 100.0 L76-10765
4,6-Dinitro-2-methylphenol ug/L10610 100.0 10-181106
4-Bromophenyl phenyl ether ug/L10110 100.0 53-127101
4-Chloro-3-methylphenol ug/L76.9 10 100.0 22-14777
4-Chloroaniline ug/L70.4 10 100.0 44-16370
4-Chlorophenyl phenyl ether ug/L94.2 10 100.0 25-15894
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0055 - 625
LCS (P7C0055-BS1)Prepared: 03/03/17 Analyzed: 03/06/17
4-Nitrophenol ug/L40.2 50 100.0 J10-13240
Acenaphthene ug/L97.7 10 100.0 47-14598
Acenaphthylene ug/L95.1 10 100.0 33-14595
Anthracene ug/L99.9 10 100.0 27-133100
Benzidine ug/L70.4 100 100.0 J15-15070
Benzo(a)anthracene ug/L90.2 10 100.0 33-14390
Benzo(a)pyrene ug/L99.4 10 100.0 17-16399
Benzo(b)fluoranthene ug/L10010 100.0 24-159100
Benzo(g,h,i)perylene ug/L96.6 10 100.0 10-21997
Benzo(k)fluoranthene ug/L94.4 10 100.0 11-16294
Benzoic Acid ug/L14.4 100 100.0 J10-12514
Benzyl alcohol ug/L77.4 10 100.0 16-10777
bis(2-Chloroethoxy)methane ug/L74.0 10 100.0 33-18474
Bis(2-Chloroethyl)ether ug/L81.0 10 100.0 12-15881
Bis(2-chloroisopropyl)ether ug/L79.4 10 100.0 36-16679
Bis(2-Ethylhexyl)phthalate ug/L93.8 10 100.0 10-15894
Butyl benzyl phthalate ug/L89.6 10 100.0 10-15290
Chrysene ug/L10110 100.0 17-168101
Dibenzo(a,h)anthracene ug/L61.5 10 100.0 10-22761
Dibenzofuran ug/L98.7 10 100.0 39-11499
Diethyl phthalate ug/L94.4 10 100.0 10-11494
Dimethyl phthalate ug/L79.6 10 100.0 10-11280
Di-n-butyl phthalate ug/L10110 100.0 10-118101
Di-n-octyl phthalate ug/L10210 100.0 10-146102
Fluoranthene ug/L97.6 10 100.0 26-13798
Fluorene ug/L96.4 10 100.0 59-12196
Hexachlorobenzene ug/L10110 100.0 10-152101
Hexachlorobutadiene ug/L70.5 10 100.0 24-11670
Hexachlorocyclopentadiene ug/L61.9 10 100.0 32-11762
Hexachloroethane ug/L69.1 10 100.0 40-11369
Indeno(1,2,3-cd)pyrene ug/L10510 100.0 10-171105
Isophorone ug/L79.0 10 100.0 21-19679
Naphthalene ug/L67.9 10 100.0 21-13368
Nitrobenzene ug/L72.4 10 100.0 35-18072
N-Nitrosodimethylamine ug/L53.5 10 100.0 10-11953
N-Nitroso-di-n-propylamine ug/L87.6 10 100.0 10-23088
N-Nitrosodiphenylamine ug/L12210 100.0 69-152122
Pentachlorophenol ug/L114 10 100.0 14-176114
Phenanthrene ug/L10010 100.0 54-120100
Phenol ug/L38.9 10 100.0 10-11239
Pyrene ug/L90.3 10 100.0 52-11590
ug/L 100.0 31-144Surrogate: 2,4,6-Tribromophenol 9897.5
ug/L 50.00 49-118Surrogate: 2-Fluorobiphenyl 9447.1
ug/L 100.0 22-84Surrogate: 2-Fluorophenol 5555.0
ug/L 50.00 43-123Surrogate: Nitrobenzene-d5 6834.0
ug/L 100.0 10-63Surrogate: Phenol-d5 3838.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0055 - 625
LCS (P7C0055-BS1)Prepared: 03/03/17 Analyzed: 03/06/17
ug/L 50.00 49-151Surrogate: Terphenyl-d14 10552.6
LCS Dup (P7C0055-BSD1)Prepared: 03/03/17 Analyzed: 03/06/17
1,2,4-Trichlorobenzene ug/L66.0 10 100.0 2044-14266 0.06
1,2-Dichlorobenzene ug/L73.7 10 100.0 2032-12974 3
1,3-Dichlorobenzene ug/L73.4 10 100.0 2020-12473 1
1,4-Dichlorobenzene ug/L72.6 10 100.0 2020-12473 1
1-Methylnaphthalene ug/L76.0 10 100.0 2040-13576 0.7
2,4,6-Trichlorophenol ug/L95.0 10 100.0 2037-14495 0.4
2,4-Dichlorophenol ug/L70.8 10 100.0 2039-13571 1
2,4-Dimethylphenol ug/L84.3 10 100.0 2032-11984 3
2,4-Dinitrophenol ug/L10010 100.0 2010-191100 3
2,4-Dinitrotoluene ug/L10410 100.0 2039-139104 0.2
2,6-Dinitrotoluene ug/L10110 100.0 2050-158101 0.6
2-Chloronaphthalene ug/L91.1 10 100.0 2060-11891 0.3
2-Chlorophenol ug/L84.2 10 100.0 2023-13484 3
2-Methylnaphthalene ug/L73.4 10 100.0 2018-12173 1
2-Nitrophenol ug/L72.6 10 100.0 2029-18273 2
3,3'-Dichlorobenzidine ug/L96.4 10 100.0 2010-26296 0.08
3/4-Methylphenol ug/L67.8 10 100.0 20 L76-10768 3
4,6-Dinitro-2-methylphenol ug/L99.7 10 100.0 2010-181100 6
4-Bromophenyl phenyl ether ug/L97.9 10 100.0 2053-12798 4
4-Chloro-3-methylphenol ug/L77.5 10 100.0 2022-14778 0.8
4-Chloroaniline ug/L71.2 10 100.0 2044-16371 1
4-Chlorophenyl phenyl ether ug/L94.8 10 100.0 2025-15895 0.6
4-Nitrophenol ug/L41.3 50 100.0 20 J10-13241 3
Acenaphthene ug/L96.8 10 100.0 2047-14597 1
Acenaphthylene ug/L94.2 10 100.0 2033-14594 1
Anthracene ug/L97.1 10 100.0 2027-13397 3
Benzidine ug/L73.2 100 100.0 20 J15-15073 4
Benzo(a)anthracene ug/L89.0 10 100.0 2033-14389 1
Benzo(a)pyrene ug/L96.8 10 100.0 2017-16397 3
Benzo(b)fluoranthene ug/L98.8 10 100.0 2024-15999 1
Benzo(g,h,i)perylene ug/L94.6 10 100.0 2010-21995 2
Benzo(k)fluoranthene ug/L93.8 10 100.0 2011-16294 0.7
Benzoic Acid ug/L23.2 100 100.0 20 D, J10-12523 47
Benzyl alcohol ug/L77.9 10 100.0 2016-10778 0.6
bis(2-Chloroethoxy)methane ug/L73.1 10 100.0 2033-18473 1
Bis(2-Chloroethyl)ether ug/L78.0 10 100.0 2012-15878 4
Bis(2-chloroisopropyl)ether ug/L78.8 10 100.0 2036-16679 0.7
Bis(2-Ethylhexyl)phthalate ug/L91.7 10 100.0 2010-15892 2
Butyl benzyl phthalate ug/L89.0 10 100.0 2010-15289 0.8
Chrysene ug/L97.6 10 100.0 2017-16898 3
Dibenzo(a,h)anthracene ug/L61.1 10 100.0 2010-22761 0.6
Dibenzofuran ug/L98.1 10 100.0 2039-11498 0.6
Diethyl phthalate ug/L95.7 10 100.0 2010-11496 1
Dimethyl phthalate ug/L83.3 10 100.0 2010-11283 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0055 - 625
LCS Dup (P7C0055-BSD1)Prepared: 03/03/17 Analyzed: 03/06/17
Di-n-butyl phthalate ug/L98.5 10 100.0 2010-11899 2
Di-n-octyl phthalate ug/L10010 100.0 2010-146100 2
Fluoranthene ug/L94.4 10 100.0 2026-13794 3
Fluorene ug/L96.2 10 100.0 2059-12196 0.2
Hexachlorobenzene ug/L97.8 10 100.0 2010-15298 3
Hexachlorobutadiene ug/L72.1 10 100.0 2024-11672 2
Hexachlorocyclopentadiene ug/L63.3 10 100.0 2032-11763 2
Hexachloroethane ug/L71.4 10 100.0 2040-11371 3
Indeno(1,2,3-cd)pyrene ug/L10410 100.0 2010-171104 0.8
Isophorone ug/L78.9 10 100.0 2021-19679 0.09
Naphthalene ug/L68.0 10 100.0 2021-13368 0.01
Nitrobenzene ug/L72.8 10 100.0 2035-18073 0.6
N-Nitrosodimethylamine ug/L55.3 10 100.0 2010-11955 3
N-Nitroso-di-n-propylamine ug/L85.4 10 100.0 2010-23085 3
N-Nitrosodiphenylamine ug/L118 10 100.0 2069-152118 3
Pentachlorophenol ug/L10910 100.0 2014-176109 4
Phenanthrene ug/L97.1 10 100.0 2054-12097 3
Phenol ug/L41.0 10 100.0 2010-11241 5
Pyrene ug/L89.0 10 100.0 2052-11589 1
ug/L 100.0 31-144Surrogate: 2,4,6-Tribromophenol 9090.1
ug/L 50.00 49-118Surrogate: 2-Fluorobiphenyl 9044.8
ug/L 100.0 22-84Surrogate: 2-Fluorophenol 5454.5
ug/L 50.00 43-123Surrogate: Nitrobenzene-d5 6532.4
ug/L 100.0 10-63Surrogate: Phenol-d5 3736.9
ug/L 50.00 49-151Surrogate: Terphenyl-d14 9849.0
Batch P7C0129 - 3546
Blank (P7C0129-BLK1)Prepared & Analyzed: 03/08/17
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0129 - 3546
Blank (P7C0129-BLK1)Prepared & Analyzed: 03/08/17
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.332 39-132Surrogate: 2,4,6-Tribromophenol 882.92
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0129 - 3546
Blank (P7C0129-BLK1)Prepared & Analyzed: 03/08/17
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 871.45
mg/kg wet 3.332 35-115Surrogate: 2-Fluorophenol 933.08
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 821.37
mg/kg wet 3.332 34-121Surrogate: Phenol-d5 903.01
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 921.54
LCS (P7C0129-BS1)Prepared & Analyzed: 03/08/17
1,2,4-Trichlorobenzene mg/kg wet1.17 0.33 1.665 34-11870
1,2-Dichlorobenzene mg/kg wet1.23 0.33 1.665 33-11774
1,3-Dichlorobenzene mg/kg wet1.21 0.33 1.665 30-11573
1,4-Dichlorobenzene mg/kg wet1.20 0.33 1.665 31-11572
1-Methylnaphthalene mg/kg wet1.33 0.33 1.665 40-11980
2,4,6-Trichlorophenol mg/kg wet1.46 0.33 1.665 39-12688
2,4-Dichlorophenol mg/kg wet1.31 0.33 1.665 40-12279
2,4-Dimethylphenol mg/kg wet1.52 0.33 1.665 30-12791
2,4-Dinitrophenol mg/kg wet1.81 0.33 1.665 27-129109
2,4-Dinitrotoluene mg/kg wet1.56 0.33 1.665 48-12694
2,6-Dinitrotoluene mg/kg wet1.52 0.33 1.665 46-12491
2-Chloronaphthalene mg/kg wet1.40 0.33 1.665 41-11484
2-Chlorophenol mg/kg wet1.51 0.33 1.665 34-12191
2-Methylnaphthalene mg/kg wet1.26 0.33 1.665 38-12276
2-Methylphenol mg/kg wet1.52 0.33 1.665 32-12292
2-Nitrophenol mg/kg wet1.25 0.33 1.665 36-12375
3,3'-Dichlorobenzidine mg/kg wet1.28 0.33 1.665 22-12177
3/4-Methylphenol mg/kg wet1.35 0.33 1.665 34-11981
4,6-Dinitro-2-methylphenol mg/kg wet1.67 0.33 1.665 29-132100
4-Bromophenyl phenyl ether mg/kg wet1.48 0.33 1.665 46-12489
4-Chloro-3-methylphenol mg/kg wet1.40 0.33 1.665 45-12284
4-Chloroaniline mg/kg wet1.10 0.33 1.665 17-10666
4-Chlorophenyl phenyl ether mg/kg wet1.43 0.33 1.665 45-12186
4-Nitrophenol mg/kg wet1.63 0.33 1.665 30-13298
Acenaphthene mg/kg wet1.49 0.33 1.665 40-12390
Acenaphthylene mg/kg wet1.46 0.33 1.665 32-13287
Anthracene mg/kg wet1.52 0.33 1.665 47-12391
Azobenzene mg/kg wet1.61 0.33 1.665 39-12597
Benzo(a)anthracene mg/kg wet1.37 0.33 1.665 49-12682
Benzo(a)pyrene mg/kg wet1.42 0.33 1.665 45-12986
Benzo(b)fluoranthene mg/kg wet1.37 0.33 1.665 45-13282
Benzo(g,h,i)perylene mg/kg wet1.37 0.33 1.665 43-13482
Benzo(k)fluoranthene mg/kg wet1.42 0.33 1.665 47-13285
Benzoic Acid mg/kg wet1.01 0.33 1.665 10-8361
Benzyl alcohol mg/kg wet1.45 0.33 1.665 29-12287
bis(2-Chloroethoxy)methane mg/kg wet1.29 0.33 1.665 36-12178
Bis(2-Chloroethyl)ether mg/kg wet1.58 0.33 1.665 31-12095
Bis(2-chloroisopropyl)ether mg/kg wet1.29 0.33 1.665 33-13178
Bis(2-Ethylhexyl)phthalate mg/kg wet1.44 0.33 1.665 51-13386
Butyl benzyl phthalate mg/kg wet1.44 0.33 1.665 48-13287
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0129 - 3546
LCS (P7C0129-BS1)Prepared & Analyzed: 03/08/17
Chrysene mg/kg wet1.59 0.33 1.665 50-12496
Dibenzo(a,h)anthracene mg/kg wet0.958 0.33 1.665 45-13458
Dibenzofuran mg/kg wet1.51 0.33 1.665 44-12091
Diethyl phthalate mg/kg wet1.51 0.33 1.665 50-12491
Dimethyl phthalate mg/kg wet1.51 0.33 1.665 48-12490
Di-n-butyl phthalate mg/kg wet1.58 0.33 1.665 51-12895
Di-n-octyl phthalate mg/kg wet1.46 0.33 1.665 45-14088
Fluoranthene mg/kg wet1.49 0.33 1.665 50-12790
Fluorene mg/kg wet1.47 0.33 1.665 43-12588
Hexachlorobenzene mg/kg wet1.48 0.33 1.665 45-12289
Hexachlorobutadiene mg/kg wet1.25 0.33 1.665 32-12375
Hexachlorocyclopentadiene mg/kg wet0.864 0.33 1.665 32-11752
Hexachloroethane mg/kg wet1.20 0.33 1.665 28-11772
Indeno(1,2,3-cd)pyrene mg/kg wet1.52 0.33 1.665 45-13392
Isophorone mg/kg wet1.33 0.33 1.665 30-12280
Naphthalene mg/kg wet1.21 0.33 1.665 35-12373
Nitrobenzene mg/kg wet1.29 0.33 1.665 34-12278
N-Nitroso-di-n-propylamine mg/kg wet1.32 0.33 1.665 36-12079
N-Nitrosodiphenylamine mg/kg wet1.83 0.33 1.665 38-127110
Pentachlorophenol mg/kg wet1.91 0.33 1.665 25-133114
Phenanthrene mg/kg wet1.52 0.33 1.665 50-12191
Phenol mg/kg wet1.61 0.33 1.665 34-12197
Pyrene mg/kg wet1.40 0.33 1.665 47-12784
mg/kg wet 3.330 39-132Surrogate: 2,4,6-Tribromophenol 832.77
mg/kg wet 1.665 44-115Surrogate: 2-Fluorobiphenyl 801.33
mg/kg wet 3.330 35-115Surrogate: 2-Fluorophenol 832.78
mg/kg wet 1.665 37-122Surrogate: Nitrobenzene-d5 691.14
mg/kg wet 3.330 34-121Surrogate: Phenol-d5 832.77
mg/kg wet 1.665 54-127Surrogate: Terphenyl-d14 891.48
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0129 - 3546
LCS Dup (P7C0129-BSD1)Prepared & Analyzed: 03/08/17
1,2,4-Trichlorobenzene mg/kg wet1.30 0.33 1.666 2034-11878 11
1,2-Dichlorobenzene mg/kg wet1.38 0.33 1.666 2033-11783 11
1,3-Dichlorobenzene mg/kg wet1.35 0.33 1.666 2030-11581 11
1,4-Dichlorobenzene mg/kg wet1.31 0.33 1.666 2031-11579 9
1-Methylnaphthalene mg/kg wet1.47 0.33 1.666 2040-11988 10
2,4,6-Trichlorophenol mg/kg wet1.66 0.33 1.666 2039-126100 13
2,4-Dichlorophenol mg/kg wet1.44 0.33 1.666 2040-12286 9
2,4-Dimethylphenol mg/kg wet1.67 0.33 1.666 2030-127100 9
2,4-Dinitrophenol mg/kg wet1.98 0.33 1.666 2027-129119 9
2,4-Dinitrotoluene mg/kg wet1.71 0.33 1.666 2048-126103 9
2,6-Dinitrotoluene mg/kg wet1.73 0.33 1.666 2046-124104 13
2-Chloronaphthalene mg/kg wet1.58 0.33 1.666 2041-11495 12
2-Chlorophenol mg/kg wet1.65 0.33 1.666 2034-12199 9
2-Methylnaphthalene mg/kg wet1.38 0.33 1.666 2038-12283 9
2-Methylphenol mg/kg wet1.67 0.33 1.666 2032-122100 9
2-Nitrophenol mg/kg wet1.43 0.33 1.666 2036-12386 14
3,3'-Dichlorobenzidine mg/kg wet1.39 0.33 1.666 2022-12183 8
3/4-Methylphenol mg/kg wet1.47 0.33 1.666 2034-11989 9
4,6-Dinitro-2-methylphenol mg/kg wet1.88 0.33 1.666 2029-132113 12
4-Bromophenyl phenyl ether mg/kg wet1.62 0.33 1.666 2046-12497 9
4-Chloro-3-methylphenol mg/kg wet1.53 0.33 1.666 2045-12292 8
4-Chloroaniline mg/kg wet1.24 0.33 1.666 2017-10674 12
4-Chlorophenyl phenyl ether mg/kg wet1.61 0.33 1.666 2045-12197 12
4-Nitrophenol mg/kg wet1.84 0.33 1.666 2030-132110 12
Acenaphthene mg/kg wet1.67 0.33 1.666 2040-123100 11
Acenaphthylene mg/kg wet1.62 0.33 1.666 2032-13297 11
Anthracene mg/kg wet1.66 0.33 1.666 2047-123100 9
Azobenzene mg/kg wet1.76 0.33 1.666 2039-125106 9
Benzo(a)anthracene mg/kg wet1.50 0.33 1.666 2049-12690 9
Benzo(a)pyrene mg/kg wet1.53 0.33 1.666 2045-12992 7
Benzo(b)fluoranthene mg/kg wet1.51 0.33 1.666 2045-13291 9
Benzo(g,h,i)perylene mg/kg wet1.47 0.33 1.666 2043-13489 8
Benzo(k)fluoranthene mg/kg wet1.53 0.33 1.666 2047-13292 7
Benzoic Acid mg/kg wet1.05 0.33 1.666 2010-8363 3
Benzyl alcohol mg/kg wet1.56 0.33 1.666 2029-12294 8
bis(2-Chloroethoxy)methane mg/kg wet1.41 0.33 1.666 2036-12185 9
Bis(2-Chloroethyl)ether mg/kg wet1.28 0.33 1.666 20 D31-12077 21
Bis(2-chloroisopropyl)ether mg/kg wet1.43 0.33 1.666 2033-13186 11
Bis(2-Ethylhexyl)phthalate mg/kg wet1.54 0.33 1.666 2051-13392 7
Butyl benzyl phthalate mg/kg wet1.57 0.33 1.666 2048-13294 8
Chrysene mg/kg wet1.73 0.33 1.666 2050-124104 8
Dibenzo(a,h)anthracene mg/kg wet1.04 0.33 1.666 2045-13462 8
Dibenzofuran mg/kg wet1.68 0.33 1.666 2044-120101 11
Diethyl phthalate mg/kg wet1.69 0.33 1.666 2050-124102 11
Dimethyl phthalate mg/kg wet1.69 0.33 1.666 2048-124102 12
Di-n-butyl phthalate mg/kg wet1.72 0.33 1.666 2051-128103 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7C0129 - 3546
LCS Dup (P7C0129-BSD1)Prepared & Analyzed: 03/08/17
Di-n-octyl phthalate mg/kg wet1.57 0.33 1.666 2045-14094 7
Fluoranthene mg/kg wet1.63 0.33 1.666 2050-12798 9
Fluorene mg/kg wet1.64 0.33 1.666 2043-12598 11
Hexachlorobenzene mg/kg wet1.63 0.33 1.666 2045-12298 10
Hexachlorobutadiene mg/kg wet1.43 0.33 1.666 2032-12386 13
Hexachlorocyclopentadiene mg/kg wet0.997 0.33 1.666 2032-11760 14
Hexachloroethane mg/kg wet1.33 0.33 1.666 2028-11780 10
Indeno(1,2,3-cd)pyrene mg/kg wet1.63 0.33 1.666 2045-13398 7
Isophorone mg/kg wet1.45 0.33 1.666 2030-12287 9
Naphthalene mg/kg wet1.33 0.33 1.666 2035-12380 9
Nitrobenzene mg/kg wet1.45 0.33 1.666 2034-12287 11
N-Nitroso-di-n-propylamine mg/kg wet1.51 0.33 1.666 2036-12091 14
N-Nitrosodiphenylamine mg/kg wet2.00 0.33 1.666 2038-127120 9
Pentachlorophenol mg/kg wet2.00 0.33 1.666 2025-133120 5
Phenanthrene mg/kg wet1.67 0.33 1.666 2050-121100 10
Phenol mg/kg wet1.76 0.33 1.666 2034-121106 9
Pyrene mg/kg wet1.51 0.33 1.666 2047-12791 8
mg/kg wet 3.331 39-132Surrogate: 2,4,6-Tribromophenol 943.15
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 911.51
mg/kg wet 3.331 35-115Surrogate: 2-Fluorophenol 933.10
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 771.28
mg/kg wet 3.331 34-121Surrogate: Phenol-d5 923.06
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 961.60
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P7C0130 - 3546
Blank (P7C0130-BLK1)Prepared: 03/08/17 Analyzed: 03/09/17
Aroclor 1016 mg/kg wetBRL0.049
Aroclor 1221 mg/kg wetBRL0.099
Aroclor 1232 mg/kg wetBRL0.099
Aroclor 1242 mg/kg wetBRL0.049
Aroclor 1248 mg/kg wetBRL0.049
Aroclor 1254 mg/kg wetBRL0.049
Aroclor 1260 mg/kg wetBRL0.049
mg/kg wet 0.03289 36-182Surrogate: Tetrachloro-m-xylene 780.0256
mg/kg wet 0.03289 34-182Surrogate: Decachlorobiphenyl 1110.0365
LCS (P7C0130-BS1)Prepared: 03/08/17 Analyzed: 03/09/17
Aroclor 1016 mg/kg wet0.296 0.050 0.3331 64-15189
Aroclor 1260 mg/kg wet0.367 0.050 0.3331 45-166110
mg/kg wet 0.03331 36-182Surrogate: Tetrachloro-m-xylene 850.0284
mg/kg wet 0.03331 34-182Surrogate: Decachlorobiphenyl 1150.0384
LCS Dup (P7C0130-BSD1)Prepared: 03/08/17 Analyzed: 03/09/17
Aroclor 1016 mg/kg wet0.268 0.050 0.3320 5064-15181 10
Aroclor 1260 mg/kg wet0.328 0.050 0.3320 5045-16699 11
mg/kg wet 0.03320 36-182Surrogate: Tetrachloro-m-xylene 780.0259
mg/kg wet 0.03320 34-182Surrogate: Decachlorobiphenyl 1030.0342
Matrix Spike (P7C0130-MS1)Prepared: 03/08/17 Analyzed: 03/09/17 Source: 7030045-07
Aroclor 1016 mg/kg dry0.307 0.055 0.3676 BRL 14-19283
Aroclor 1260 mg/kg dry0.355 0.055 0.3676 BRL 10-19297
mg/kg dry 0.03676 36-182Surrogate: Tetrachloro-m-xylene 720.0263
mg/kg dry 0.03676 34-182Surrogate: Decachlorobiphenyl 1010.0372
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P7C0130 - 3546
Matrix Spike Dup (P7C0130-MSD1)Prepared: 03/08/17 Analyzed: 03/09/17 Source: 7030045-07
Aroclor 1016 mg/kg dry0.298 0.055 0.3636 BRL 5014-19282 3
Aroclor 1260 mg/kg dry0.383 0.055 0.3636 BRL 5010-192105 8
mg/kg dry 0.03636 36-182Surrogate: Tetrachloro-m-xylene 720.0262
mg/kg dry 0.03636 34-182Surrogate: Decachlorobiphenyl 1050.0382
Batch P7C0155 - 3510C GC
Blank (P7C0155-BLK1)Prepared & Analyzed: 03/09/17
Aroclor 1016 ug/LBRL0.50
Aroclor 1221 ug/LBRL1.0
Aroclor 1232 ug/LBRL0.50
Aroclor 1242 ug/LBRL0.50
Aroclor 1248 ug/LBRL0.50
Aroclor 1254 ug/LBRL0.50
Aroclor 1260 ug/LBRL0.50
ug/L 1.000 30-161Surrogate: Tetrachloro-m-xylene 730.729
ug/L 1.000 32-178Surrogate: Decachlorobiphenyl 1131.13
LCS (P7C0155-BS1)Prepared & Analyzed: 03/09/17
Aroclor 1016 ug/L7.63 0.50 10.00 50-11476
Aroclor 1260 ug/L10.1 0.50 10.00 10-127101
ug/L 1.000 30-161Surrogate: Tetrachloro-m-xylene 640.642
ug/L 1.000 32-178Surrogate: Decachlorobiphenyl 1141.14
LCS Dup (P7C0155-BSD1)Prepared & Analyzed: 03/09/17
Aroclor 1016 ug/L6.95 0.50 10.00 5050-11470 9
Aroclor 1260 ug/L9.34 0.50 10.00 5010-12793 8
ug/L 1.000 30-161Surrogate: Tetrachloro-m-xylene 660.657
ug/L 1.000 32-178Surrogate: Decachlorobiphenyl 970.970
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7C0087 - NO PREP
Blank (P7C0087-BLK1)Prepared & Analyzed: 03/03/17
Chloride mg/LBRL1.0
Nitrate/Nitrite as N mg/LBRL0.20
Nitrate as N mg/LBRL0.10
Sulfate mg/LBRL1.0
LCS (P7C0087-BS1)Prepared & Analyzed: 03/03/17
Chloride mg/L39.2 1.0 40.00 80-12098
Nitrate/Nitrite as N mg/L7.99 0.21 8.000 90-110100
Nitrate as N mg/L3.84 0.10 4.000 80-12096
Sulfate mg/L39.0 1.0 40.00 80-12098
Matrix Spike (P7C0087-MS1)Prepared & Analyzed: 03/03/17 Source: 7030045-02
Chloride mg/L91.7 1.0 40.00 50.8 80-120102
Nitrate/Nitrite as N mg/L10.4 0.21 8.000 2.01 90-110105
Nitrate as N mg/L6.04 0.10 4.000 1.97 80-120102
Sulfate mg/L1261.0 40.00 84.6 80-120103
Matrix Spike Dup (P7C0087-MSD1)Prepared & Analyzed: 03/03/17 Source: 7030045-02
Chloride mg/L91.0 1.0 40.00 50.8 1580-120101 0.8
Nitrate/Nitrite as N mg/L10.2 0.21 8.000 2.01 1590-110103 1
Nitrate as N mg/L5.97 0.10 4.000 1.97 1580-120100 1
Sulfate mg/L1261.0 40.00 84.6 1580-120102 0.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 50
3/10/17
Level II QC Report
2905 Meridian Pkwy
Project: McCall Farms (Wilson, NC)McAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Sean Gallagher
Prism Work Order: 7030045
Time Submitted: 3/3/2017 8:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0098 - NO PREP
Blank (P7C0098-BLK1)Prepared & Analyzed: 03/06/17
Total Dissolved Solids mg/LBRL50
LCS (P7C0098-BS1)Prepared & Analyzed: 03/06/17
Total Dissolved Solids mg/L1000 50 1000 90-110100
Duplicate (P7C0098-DUP1)Prepared & Analyzed: 03/06/17 Source: 7030045-04
Total Dissolved Solids mg/L25250 252 200
Batch P7C0101 - NO PREP
Blank (P7C0101-BLK1)Prepared & Analyzed: 03/07/17
Ammonia as N mg/LBRL0.10
LCS (P7C0101-BS1)Prepared & Analyzed: 03/07/17
Ammonia as N mg/L2.47 0.10 2.500 90-11099
Batch P7C0106 - 351.2
Blank (P7C0106-BLK1)Prepared: 03/07/17 Analyzed: 03/08/17
Total Kjeldahl Nitrogen mg/LBRL0.50
LCS (P7C0106-BS1)Prepared: 03/07/17 Analyzed: 03/08/17
Total Kjeldahl Nitrogen mg/L10.0 2.0 10.00 90-110100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 50
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Date/TimeInitialFinal
P7C01067030045-01 03/07/17 10:0025 25mL mL
P7C01067030045-02 03/07/17 10:0025 25mL mL
P7C01067030045-03 03/07/17 10:0025 25mL mL
P7C01067030045-04 03/07/17 10:0025 25mL mL
P7C01067030045-05 03/07/17 10:0025 25mL mL
P7C01067030045-06 03/07/17 10:0025 25mL mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P7C00887030045-07 03/03/17 14:5130 30g g
Prep Method: 3510C GC
Lab Number Batch Date/TimeInitialFinal
P7C01557030045-01 03/09/17 11:0089010mL mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7C01307030045-07 03/08/17 11:5430.03 10g mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7C01297030045-07 03/08/17 11:4630 1g mL
Prep Method: 625
Lab Number Batch Date/TimeInitialFinal
P7C00557030045-06 03/03/17 12:251000 1mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7C00897030045-07 03/03/17 11:406.02 5g mL
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P7C01207030045-01 03/07/17 8:4210 10mL mL
P7C01207030045-02 03/07/17 8:4210 10mL mL
P7C01207030045-03 03/07/17 8:4210 10mL mL
P7C01207030045-04 03/07/17 8:4210 10mL mL
P7C01207030045-05 03/07/17 8:4210 10mL mL
P7C01207030045-06 03/07/17 8:4210 10mL mL
P7C01207030045-06 03/07/17 8:4210 10mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7C01047030045-07 03/06/17 12:256.09 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 50
Page 50 of 50

APPENDIX B

MONITORING WELL CONSTRUCTION AND
ABANDONMENT LOGS


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By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
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copy of this record has been provided to the well owner.



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James D. Barker3106AQuantex, Inc.WM050121743/1/17 TW-1,2,3,4,5,6 Former McCall Farms NA2202 Charleston Street SE, Wilson, NC 27893Wilson NA35.696256 77.8988464 4Six Temp Wells 20' NA 2.25" Direct Push - Temp Well 6 7 Gray Cayey SAND 0 5 1 Sch 40 PVC 5 20 1 0.010 Sch 40 PVC 0 3 neat cement 45 lbs. pour 3 4 Bentonite 20 lbs. pour 4 20 #2 sand Pour 0 20 Sand, Gray Clayey SAND some SILT temp well propely abandoned per 2C rules, same day.3/8/17
W E L L A B AND ON M E N T R E C O R D
This form can be used for single or multiple wells
Form GW-30 North Carolina Department of Environment and Natural Resources
Division of Water Quality Revised March 2013

1. Well Contractor Information:

Well Contractor Name (or well owner personally abandoning well on his/her property)

NC Well Contractor Certification Number

Company Name

2. Well Construction Permit #:
List all applicable well construction permits (i.e. County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under 7g)

4. Date well(s) abandoned:
5a. Well location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W
CONST RUCTI O N DE TA ILS OF W EL L(S) BEING AB ANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply
wells ONLY with the same construction/abandonment, you can submit one form.

6a. Well ID#:

6b. Total well depth: (ft.)

6c. Borehole diameter: (in.)

6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)

6f. Inner casing/tubing length (if known): (ft.)

6g. Screen length (if known): (ft.)

W ELL ABA NDONMENT DET AILS

7a. Number of wells being abandoned:
For multiple injection or non-water supply wells ONLY with the same
construction/abandonment, you can submit one form.

7b. Approximate volume of water remaining in well(s): (gal.) F OR W AT ER SUPPLY WEL LS ONL Y:

7c. Type of disinfectant used:

7d. Amount of disinfectant used:

7e. Sealing materials used (check all that apply):
 Neat Cement Grout  Bentonite Chips or Pellets
 Sand Cement Grout  Dry Clay
 Concrete Grout  Drill Cuttings
 Specialty Grout  Gravel
 Bentonite Slurry  Other (explain under 7g)

7f. For each material selected above, provide amount of materials used:

7g. Provide a brief description of the abandonment procedure:

8. Certification:

Signature of Certified Well Contractor or Well Owner Date

By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.

9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.

SUBMITT AL INSTRUC TIONS

10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Quality, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617!
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:

Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636!

10c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well abandonment to the county health department of the county
where abandoned.
For Internal Use ONLY:
James D. Barker3106-AQuantex, Inc. WM050121743/1/17Former McCall Farms NA2202 Charleston Street SE, Wilson, NC 27893Wilson NA35.696256 77.898846TW-1,2,3,4,5,6 20' 1" pvc ~ 5' to 6' NA 5' 15' Six None NA NA430 lbs. of Neat Cement For ea. Temp WellSix temp wells totalNeat cement was poured into 1" pvc screenand riser. Cement was also placed in boreholeannulas from land surface to 3' below grade.3/8/17

APPENDIX C

MONITORING WELL CONSTRUCTION PERMIT