07005_Bouligny LSI 20141121

Limited Site Investigation

Former Bouligny Site
2300 North Davidson Street and 628 East 27th Street
Charlotte, North Carolina
November 21, 2014
Terracon Project No. 71147763

Prepared for:
Southern Apartment Group
Charlotte, North Carolina

Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina

Terracon Consultants, Inc. 2020-E Starita Road Charlotte, North Carolina 28206
P [704] 509 1777 F [704] 509 1888 terracon.com

November 21, 2014

Southern Apartment Group
1435 West Morehead Street, Suite 130
Charlotte, North Carolina 28208

Attn. Mr. Eric Applefield

Telephone: [phone]
E-mail: [e-mail]

Re: Limited Site Investigation
Former Bouligny Site
2300 North Davidson Street and 628 East 27th Street
Charlotte, Mecklenburg County, North Carolina
Terracon Project No. 71147763

Dear Mr. Applefield,

Terracon Consultants, Inc. (Terracon) is pleased to submit the enclosed Limited Site
Investigation (LSI) report for the above-referenced site. The LSI activities were completed
to evaluate current environmental conditions at the site and to fulfill certain requirements
established by the Brownfields Agreement (No. 07005-03-60) for the former Bouligny site.
Terracon conducted the LSI in general accordance with our proposal 71147E095, dated
September 30, 2014 (Revised October 1, 2014) and our Supplemental Change Order
71147E106, dated November 17, 2014.

We appreciate the opportunity to perform these services for you. Please contact us if you
have questions regarding this information or if we can provide any other services.

Sincerely,
Terracon Consultants, Inc.

Stephen C. Brown Christopher L. Corbitt, PG
Project Geologist Senior Project Manager

TABLE OF CONTENTS

1.0 INTRODUCTION ......................................................................................................... 1 
1.1 Site Description .................................................................................................. 1 
1.2 Scope of Services .............................................................................................. 1 
1.3 Standard of Care ................................................................................................ 2 
1.4 Additional Scope Limitations .............................................................................. 2 
1.5 Reliance ............................................................................................................. 3 
2.0 FIELD ACTIVITIES ..................................................................................................... 3 
2.1 Groundwater Sampling ...................................................................................... 3 
2.2 Soil Gas Sampling ............................................................................................. 3 
3.0 ANALYTICAL DATA .................................................................................................. 5 
3.1 Groundwater Sample Analysis ........................................................................... 5 
3.2 Soil Gas Sample Analysis .................................................................................. 6 
4.0 CONCLUSIONS .......................................................................................................... 6 

APPENDICES

APPENDIX A Figure 1 – Topographic Map
Figure 2 – Sample Location Plan
APPENDIX B Photographs
APPENDIX C Table 1 – Soil Gas Sampling Analytical Results Summary
APPENDIX D Laboratory Analytical Reports

Responsive ■ Resourceful ■ Reliable 1
LIMITED SITE INVESTIGATION
FORMER BOULIGNY SITE
2300 NORTH DAVIDSON STREET AND 628 EAST 27TH STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA

Project No. 71147763
Report Date: November 21, 2014
1.0 INTRODUCTION
1.1 Site Description
Site Description
Site Name Former Bouligny Site
Site Location/Address 2300 North Davidson Street and 628 East 27th Street
Charlotte, Mecklenburg County, North Carolina
Land Area Approximately 3.627 acres
Site Improvements
The site is occupied by two buildings, an automotive repair
shop (6537 sq. ft.) and a private recycling center (12,436 sq.
ft.). Remaining portions of the site are gravel covered or
grass covered.

The site location is depicted on Exhibit 1 of Appendix A which was reproduced from a
portion of the USGS 7.5-minute series topographic map.
1.2 Scope of Services
Terracon recently completed a Phase I Environmental Site Assessment for the property.
A report of our findings was issued as Terracon Project No. 71147763 on September 4,
2014. In our report, Terracon identified four on-site Leaking Underground Storage Tank
(LUST) incidents as current or historical Recognized Environmental Conditions (RECs).
We also identified releases on two adjacent properties as RECs associated with the site.

Based on a telephone conversation on September 25, 2014 between our Messrs. Chris
Corbitt and Stephen Brown and Ms. Susan Cooper of Womble Carlyle Sandridge & Rice,
LLP (client’s attorney), the client requested Terracon to evaluate impact to the site by the
adjacent Safety Kleen facility and potential vapor encroachment at the site.

As a result of a meeting on November 5, 2014 with the North Carolina Brownfields
Program, Terracon was requested to conduct supplemental environmental services
including a water supply well receptor survey in accordance with the established
Limited Site Investigation
Former Bouligny Site ■ Charlotte, North Carolina
November 21, 2014 ■ Terracon Project No. 71147763

Responsive ■ Resourceful ■ Reliable 2
Brownfields Agreement and soil sampling at the site in order to provide additional
information regarding potential on-site environmental impacts.

The objective of the LSI was to:
 evaluate the potential impact to the site by the adjacent Safety Kleen facility,
 evaluate potential vapor encroachment in soils,
 evaluate potential soil contaminant concentrations at the site to identify potential
“hot spots” (high concentrations) of documented constituents beneath the former
truck maintenance shop as a result of recent sub-slab sampling results and at a
known area near the southern exterior corner of the shop building where high
levels of 1,1,2,2-tetrachloroethane (TCA) was historically detected; and,
 conduct a water supply well receptor survey in accordance with the established
Brownfields Agreement for the site.
1.3 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted
practices of the profession undertaken in similar studies in the same geographical area
during the same time period. Terracon makes no warranties, either expressed or implied,
regarding the findings, conclusions or recommendations. Please note that Terracon does
not warrant the work of laboratories, regulatory agencies or other third parties supplying
information used in the preparation of the report. These LSI services were performed in
accordance with the scope of work authorized by you, our client, as reflected in our
proposal and were not restricted by ASTM E1903-97.
1.4 Additional Scope Limitations
Findings, conclusions and recommendations resulting from these services are based
upon information derived from the on-site activities and other services performed under
this scope of work; such information is subject to change over time. Certain indicators of
the presence of hazardous substances, petroleum products, or other constituents may
have been latent, inaccessible, unobservable, non-detectable or not present during these
services; thus, we cannot represent that the site is free of hazardous substances, toxic
materials, petroleum products, or other latent conditions beyond those identified during
this LSI. Subsurface conditions may vary from those encountered at specific borings or
wells or during other surveys, tests, assessments, investigations or exploratory services;
the data, interpretations, findings, and our recommendations are based solely upon data
obtained at the time and within the scope of these services.
Limited Site Investigation
Former Bouligny Site ■ Charlotte, North Carolina
November 21, 2014 ■ Terracon Project No. 71147763

Responsive ■ Resourceful ■ Reliable 3
1.5 Reliance
This report has been prepared for the exclusive use of Southern Apartment Group. Any
authorization for use or reliance by any other party (except a governmental entity having
jurisdiction over the site) is prohibited without the expressed written authorization of
Southern Apartment Group and Terracon. Any unauthorized distribution or reuse is at the
client’s sole risk. Reliance by authorized parties will be subject to the terms, conditions
and limitations stated in the Agreement For Services (AFS), subsequent task orders and
the LSI report. The limitation of liability defined in the terms and conditions is the
aggregate limit of Terracon’s liability to the client and all relying parties unless otherwise
agreed in writing.
2.0 FIELD ACTIVITIES
Prior to initiating field activities, Terracon engaged Priority Underground Locating, a
private utility locating company, to identify on-site underground utilities in the specific
areas planned for drilling. Terracon mobilized to the site on October 16 and 21, 2014 and
November 12, 2014 to conduct our field activities.
2.1 Soil Gas Sampling
Terracon installed sub-slab vapor sampling points in the Junk Rescue building (SG-1) and
the auto repair shop building (SG-2) to evaluate the presence of volatile vapors beneath
the on-site buildings. We also installed a soil vapor sampling point (SG-3) in the
northwestern portion of the site near North Davidson Street to evaluate impacts to the
soils by chlorinated compounds in groundwater at the site. Sampling points SG-1 and
SG-2 were installed using a rotary hammer drill to advance a small diameter hole through
the floor slabs to approximately 6 to 12 inches below the slab. Each vapor sampling point
was constructed using a new, non-reactive Teflon® soil gas implant attached to Teflon
tubing was inserted into the boring and the annular space between the implant and the
boring was backfilled with well sand and bentonite hydrated with de-ionized water to form
a competent seal. A water dam was maintained on each bentonite seal for the duration of
sample collection.

Prior to sample collection, the ambient air in each sampling point was purged a minimum
of four volumes using a new, disposable 60ml syringe connected in-line with the sampling
train. Once purging was complete, a laboratory supplied, pre-cleaned Summa canister,
with a flow controller set for 2 hours, was connected to the purge hose for collection of the
sub-slab vapor sample.

Each canister was filled using a dedicated, 2-hour flow controller set to a sample rate less
than or equal to 50 milliliters (mL) per min (50 mL/min x 120 min = 6 L sample volume).
An “in line” vacuum gauge was installed at the sample controller to verify initial vacuum
Limited Site Investigation
Former Bouligny Site ■ Charlotte, North Carolina
November 21, 2014 ■ Terracon Project No. 71147763

Responsive ■ Resourceful ■ Reliable 4
levels within the canister and as an indicator that final pressure equalization had been
reached (sampling was complete). General weather conditions at the time of sampling
activities (temperature, humidity, barometric pressure) were recorded before, during and
after the collection of the sample. Weather conditions (clear and mild) remained relatively
consistent throughout the sample collection period.

An outdoor, ambient air sample (AA-1) was also collected using a Summa canister with a
flow controller set for 2 hours. The ambient sample was obtained outside the auto repair
shop building (see Exhibit 2) to limit potential interference from volatile organic
compounds (VOCs) commonly found inside commercial and industrial settings, such as
paints, paint thinners, gasoline-powered machinery, certain building materials and
cleaning products.

Following completion of the field activities, the Summa canisters, along with chain-of-
custody documentation, were shipped via Federal Express to Pace Analytical Services,
Inc., in Minneapolis, Minnesota for analysis of VOCs by EPA Method TO-15 and helium
on a standard laboratory schedule.

A Sample Location Plan showing the approximate locations of the soil vapor sampling
points is included as Figure 2 of Appendix A. Photographic documentation of our
sampling activities is included in Appendix B.
2.2 Groundwater Sampling
In order to evaluate the potential impact from nearby upgradient properties to the east,
Terracon advanced one soil boring (TMW-1) to an estimated depth of 23 feet below
ground surface (bgs) utilizing a Geoprobe® drill rig equipped with a hollow stem rotary
auger in the southeastern portion of the site along Yadkin Avenue. Drilling services were
performed by a North Carolina licensed monitoring well driller using a Geoprobe© drilling
rig under the supervision of a Terracon environmental professional on October 16, 2014l.
The down-hole drilling equipment was decontaminated prior to advancing the boring. The
boring was subsequently converted to a temporary Type II groundwater monitoring well.
A Sample Location Plan showing the approximate location of temporary monitoring well
TMW-1 is included as Figure 2 of Appendix A.

Terracon returned to the site on October 21, 2014 to collect a groundwater sample. Prior
to sampling, the well was developed by purging. Once the measured parameters of
temperature, pH and conductivity remained relatively stable, the well was considered
developed. A water sample was collected using a new, disposable bailer. The
groundwater sample was placed in laboratory-supplied glassware, labeled and stored in
an ice-packed cooler. The sample, along with chain-of-custody documentation, was
delivered to Pace Analytical Services, Inc., in Huntersville, North Carolina for analysis of
volatile organic compounds (VOCs) by Standard Method 6200.
Limited Site Investigation
Former Bouligny Site ■ Charlotte, North Carolina
November 21, 2014 ■ Terracon Project No. 71147763

Responsive ■ Resourceful ■ Reliable 5
2.3 Soil Sampling
One November 12, 2014, four borings were advanced using a track-mounted Geoprobe®
direct-push drill rig at the auto repair shop building. The soil sampling was conducted as a
result of recent sub-slab vapor analysis to document current conditions in soils where
previous constituents of concern were detected. The down-hole drilling rods were
decontaminated prior to advancing each boring. Six soil samples were collected at
selected depths from the four soil borings for laboratory analysis. A Sample Location Plan
showing the approximate location of the soil borings is included as Figure 2 of Appendix
A.

The soil samples were placed in laboratory-supplied glassware, labeled and stored in an
ice-packed cooler. The samples, along with chain-of-custody documentation, were
delivered to Pace Analytical Services, Inc., in Huntersville, North Carolina for analysis of
VOCs by EPA Method 8260.
2.4 Receptor Survey
To comply with Land Use Restrictions (LURs) established in the Brownfields Agreement,
Terracon conducted a water supply well survey in the vicinity of the project site. A
walking/driving reconnaissance in the project area was conducted by Terracon as part of
this assessment. Based on the information obtained from the reconnaissance, historical
information from Charlotte Mecklenburg Utilities (water meter connections) and review of
the Mecklenburg LUESA Well Information System website, one permanently abandoned
water supply well was identified within 1,500 feet of the source area. The abandoned well
is located at 2201 North Davidson Street and was reportedly use for irrigation purposes
only. The surrounding properties are connected to municipal water supplies.
3.0 ANALYTICAL DATA
3.1 Soil Gas Sample Analysis
According to the laboratory analytical report, twenty-seven (27) volatile organic
compounds were detected in the vapor samples. Analysis of sample SG-2 detected
1,1,2,2-tetrachloroethane at a concentration of 17,200 micrograms per cubic meter
(µg/m³), tetrachloroethene at a concentration of 503 µg/m³, trichloroethene at a
concentration of 4,480 µg/m³, 1,2,4-trimethylbenzene at a concentration of 2,830 µg/m³
and o-xylenes at a concentration of 701 µg/m³. These five constituent detections
exceeded their respective North Carolina Division of Waste Management (DWM)
Residential Vapor Intrusion Screening Levels of 16.1 µg/m³, 278 µg/m³, 13.9 µg/m³, 48.7
µg/m³ and 695 µg/m³. The remaining detected constituent concentrations identified in the
various samples were below regulatory levels. The laboratory analytical results are
Limited Site Investigation
Former Bouligny Site ■ Charlotte, North Carolina
November 21, 2014 ■ Terracon Project No. 71147763

Responsive ■ Resourceful ■ Reliable 6
summarized in Table 1 of Appendix C. A copy of the laboratory analytical report is
included in Appendix D.
3.2 Groundwater Sample Analysis
According to the laboratory analytical report, 1,1-dichloroethane was detected at a
concentration of 0.61 micrograms per liter (µg/L) in groundwater sample TMW-1 collected
in the southeastern portion of the site along Yadkin Avenue. The North Carolina
Administrative Code (NCAC) 2L water quality standard for 1,1-dichloroethane is 6 µg/L.
A copy of the laboratory analytical report is included in Appendix D.
3.3 Soil Sample Analysis
Based on the laboratory analytical report, low (estimated) levels of methylene chloride
were detected in soil samples GP-1(0-5), GP-1(10-15), GP-2(10-15), GP-3(15-20) and
GP-4(15-20) at concentrations below its North Carolina Preliminary Soil Remediation Goal
(PSRG). This constituent is typically used in laboratory procedures and is considered to
be a laboratory artifact. Naphthalene was detected at a concentration of 467J
micrograms per kilogram (µg/kg) in soil sample GP-4(5-10). The established Protection of
Groundwater PSRG for naphthalene in 210 µg/kg. Naphthalene does not exceed the
North Carolina Residential PSRG (3,800 µg/kg). The detected constituent concentration
noted above with a “J” indicates the concentration is an estimated value that is above the
method detection limit (MDL) but below the method reporting limit. Low levels of the
petroleum constituents: n-butylbenzene, sec-butylbenzene, isoproylbenzene (cumene)
and n-propylbenzene were also detected in soil sample GP-4(5-10) at concentrations
below regulatory levels. Trichloroethene, a chlorinated compound, was detected at a
concentration of 5.7 µg/kg in sample GP-2(10-15) which is below its North Carolina
Residential and Protection of Groundwater PSRGs. The laboratory analytical results are
summarized in Table 2 of Appendix C. A copy of the laboratory analytical report is
included in Appendix D.
4.0 CONCLUSIONS
Based on the findings of this limited site investigation, Terracon concludes the following.

 Twenty-seven VOCs were detected in the vapor samples. Analysis of sample SG-
2 (obtained beneath the floor slab of the auto repair shop) detected 1,1,2,2-
tetrachloroethane at a concentration of 17,200 µg/m³, tetrachloroethene at a
concentration of 503 µg/m³, trichloroethene at a concentration of 4,480 µg/m³,
1,2,4-trimethylbenzene at a concentration of 2,830 µg/m³ and o-xylenes at a
concentration of 701 µg/m³. These five constituent detections exceeded their
respective North Carolina DWM Residential Vapor Intrusion Screening Levels.
Limited Site Investigation
Former Bouligny Site ■ Charlotte, North Carolina
November 21, 2014 ■ Terracon Project No. 71147763

Responsive ■ Resourceful ■ Reliable 7
The remaining VOC detections, including samples SG-1 and SG-3, were below
regulatory levels.
 According to the laboratory analytical report, 1,1-dichloroethane was detected at a
concentration of 0.61 µg/L in groundwater sample TMW-1 collected in the
southeastern portion of the site. The North Carolina 2L water quality standard for
this constituent is 6 µg/L.
 According to the laboratory analytical report for soil samples collected at the site,
low levels of the petroleum constituents: n-butylbenzene, sec-butylbenzene,
isoproylbenzene (cumene) and n-propylbenzene were detected in soil sample GP-
4(5-10) at concentrations below regulatory levels. Trichloroethene, a chlorinated
compound, was detected at a concentration of 5.7 µg/kg which is below its North
Carolina Residential and Protection of Groundwater PSRGs. Naphthalene was
detected at a concentration of 467J µg/kg in soil sample GP-4(5-10) which is
above the established Protection of Groundwater PSRG for naphthalene but below
the established North Carolina Residential PSRG.

 Well receptor information identified one water-supply well within a 1,500-ft radius
of the source area. The abandoned well was located at 2201 North Davidson
Street and was reportedly used for irrigation purposes. Surrounding properties are
connected to municipal water supplies.

APPENDIX A

Figure 1 - Topographic Map
Figure 2 – Sample Location Plan
PROJECT NO.: 71147763
DATE: September 2014
DRAWN BY: MGS
SCALE: 1” = 2000’FIGURE NO. 1
REFERENCE: USGS Topographic Map; Charlotte East, North Carolina Quadrangle; dated 1967 (photo-revised 1988).
TOPOGRAPHIC MAP
FORMER BOULIGNY SITE
2300 NORTH DAVIDSON STEET AND
628 EAST 27TH STREET
CHARLOTTE, NORTH CAROLINA
SITE
PROJECT NO.: 71147763
DATE: November 2014
DRAWN BY: MGS
FIGURE NO. 2B
REFERENCE: Site Plan generated from field notes during site reconnaissance
SAMPLE LOCATION PLAN
FORMER BOULIGNY SITE
2300 NORTH DAVIDSON STEET AND 628
EAST 27TH STREET
CHARLOTTE, NORTH CAROLINA NOT TO SCALE
denotes approximate site boundary.
TIME OUT YOUTH CENTER
PARTY PEDALER
GRAVEL COVERED LOT
THE CENTER FOR
COMMUNITY
TRANSITIONS
TEXTILE RUBBER &
CHEMICAL CO. INC.
CHARLOTTE
ARRANGEMENTS
historical monitoring well
GRAVEL
PARKED CARS
GRAVEL
COVERED
OPEN LOT
MASONRY BLOCK.
LINED SUMP.
SUMP
WITH
PIPING
MW-6
MW-3MW-2 MW-7
MW-9
MW-8
MW-10
MW-5
MW-4
MW-1 MW-1A
MW-5A
FORMER 550-
GAL. GAS UST
(Incident
#20598)
FORMER
550-GAL.
WASTE
OIL UST
(Incident
#12011)
TW-1
FORMER
6,000 GAL.
HEATING
OIL UST
(Incident
#20659)
OIL/WATER
SEPARATOR
Incident
#20659
SG-3
AA-1
SG-1
temporary monitoring well
soil sampling point
GP-4
GP-3
GP-2
SG-2/GP-1
soil-gas sampling point

APPENDIX B

Photographs
Project No. 71147763
Date Photos Taken: October 16 and November 12, 2014

Former Bouligny Site – Charlotte, North Carolina

Photo 1 View of soil vapor sample location SG-1.

Photo 2 View of soil vapor sample location SG-2.
Project No. 71147763
Date Photos Taken: October 16 and November 12, 2014

Former Bouligny Site – Charlotte, North Carolina

Photo 3 View of soil vapor sample location SG-3.

Photo 4 View of ambient air sampling.

Project No. 71147763
Date Photos Taken: October 16 and November 12, 2014

Former Bouligny Site – Charlotte, North Carolina

Photo 5 View of soil sampling activities inside the auto repair shop building.

Photo 6 View of soil sampling activities outside the auto repair shop building.

APPENDIX C

Table 1 – Soil Gas Sampling Analytical Results Summary
Table 2 – Soil Sampling Analytical Results Summary
TA
B
L
E

1
Su
b
-
S
l
a
b
/
S
o
i
l

V
a
p
o
r

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s

S
u
m
m
a
r
y
Fo
r
m
e
r

B
o
u
l
i
g
n
y

S
i
t
e
23
0
0

N
o
r
t
h

D
a
v
i
d
s
o
n

S
t
r
e
e
t

a
n
d

6
2
8

E
a
s
t

2
7
t
h

S
t
r
e
e
t
Ch
a
r
l
o
t
t
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Pr
o
j
e
c
t

N
u
m
b
e
r
:

7
1
1
4
7
7
6
3
TO
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-
1
5

T
O
-15

T
O
-
1
5
Co
n
t
a
m
i
n
a
n
t

o
f

C
o
n
c
e
r
n

→
Da
t
e

C
o
l
l
e
c
t
e
d
(m
m
/
d
d
/
y
y
)
SG
-
1

1
0
/
1
6
/
1
4

2
1
2

1
.
5

4
7
1

6
.
1

3
.
8

1
.
4
J

0
.
9
1
J

5
.
4

3
7
.
4

5
.
4

3
3

8

N
D

1
.
6
J

N
D

2
.
1

N
D

3
5
.
1

1
7
.
1

5
.
6

N
D

N
D

4
8

4
.
9

0
.
8
9
J

5
.
8

2
.
8
SG
-
2

1
0
/
1
6
/
1
4

6
1
1

3
6
.
5

3
4
2

5
0
.
3

N
D

5
0
.
1
J

8
4
5

1
0
8

2
5
.
4
J

N
D

N
D

6
7
.
7

N
D

N
D

3
8
4

N
D
17
,
2
0
0

5
0
3
ND

5
9
.
6

4
6
.
6
J
4,480 ND 2,830 1800

N
D
701
SG
-
3

1
0
/
1
6
/
1
4

3
0
1

2
.
8

9
8
.
8

8
.
2

2
.
3

3
.
3

1
.
2
J

5
.
8

3
.
5

1
3
.
8

2
.
2
J

1
0
.
5

1
.
4

2
.
4
J

4
.
6

2
.
6

N
D

2
1
.
4

N
D

1
2
.
4

N
D

N
D

1
.
1
J

2

0
.
9
3
J

1
2
.
9

4
.
9
AA
-
1

1
0
/
1
6
/
1
4

1
5
.
8

2
.
6

2
.
9

N
D

2
.
5

1
.
8

0
.
7
4
J

1
0
1

9
.
6

N
D

1
.
3
J

N
D

N
D

1
.
1
J

N
D

N
D

N
D

N
D

N
D

7
.
6

N
D

N
D

1
.
7

1
.
8

N
D

5
.
5

1
.
9
21
6
,
0
0
0

1
2
0

3
4
,
8
0
0

4
,
8
7
0

6
9
5

3
7
4

N
L

N
L

4
,
8
7
0

2
0
9

4
,
1
7
0

2
0
,
9
0
0

3
,
6
0
0

2
0
.
9

2
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C
h
l
o
r
i
d
e

APPENDIX D

Laboratory Analytical Reports

#=CL#
October 28, 2014
LIMS USE: FR - STEPHEN BROWN
LIMS OBJECT ID: 92222006
92222006
Project:
Pace Project No.:
RE:
Mr. Stephen Brown
Terracon
2020 E Starita Road
Charlotte, NC 28206
FORMER BOULIGNY SITE
Dear Mr. Brown:
Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
This report was revised to remove THC as Gas by TO15.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414A2LA Certification #: 2926.01
Alaska Certification #: UST-078Alaska Certification #MN00064Alabama Certification #40770Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680
California Certification #: 01155CAColorado Certification #PaceConnecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-LFlorida/NELAP Certification #: E87605
Guam Certification #:14-008rGeorgia Certification #: 959Georgia EPD #: PaceIdaho Certification #: MN00064Hawaii Certification #MN00064
Illinois Certification #: 200011Indiana Certification#C-MN-01Iowa Certification #: 368Kansas Certification #: E-10167Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086Louisiana DHH #: LA140001Maine Certification #: 2013011Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Minnesota Certification #: 027-053-137Mississippi Certification #: Pace
Montana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: PaceNew Jersey Certification #: MN-002New York Certification #: 11647
North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036Ohio EPA #: 4150Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001Pennsylvania Certification #: 68-00563Puerto Rico Certification
Saipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192Tennessee Certification #: 02818Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486West Virginia Certification #: 382West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Lab ID Sample ID Matrix Date Collected Date Received
92222006001 SG-1 Air 10/16/14 16:38 10/17/14 16:10
92222006002 SG-2 Air 10/16/14 17:07 10/17/14 16:10
92222006003 SG-3 Air 10/16/14 20:02 10/17/14 16:10
92222006004 AA-1 Air 10/16/14 17:02 10/17/14 16:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92222006001 SG-1 TO-15 58 PASI-MMJL
92222006002 SG-2 TO-15 58 PASI-MMJL
92222006003 SG-3 TO-15 58 PASI-MMJL
92222006004 AA-1 TO-15 58 PASI-MMJL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:SG-1 Lab ID:92222006001 Collected:10/16/14 16:38 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 212 ug/m3 10/23/14 20:30 67-64-1 E4.2 2.1 1.75
Benzene 1.5 ug/m3 10/23/14 20:30 71-43-20.57 0.21 1.75
Bromodichloromethane ND ug/m3 10/23/14 20:30 75-27-42.4 0.32 1.75
Bromoform ND ug/m3 10/23/14 20:30 75-25-23.7 0.57 1.75
Bromomethane ND ug/m3 10/23/14 20:30 74-83-91.4 0.47 1.75
1,3-Butadiene ND ug/m3 10/23/14 20:30 106-99-00.79 0.15 1.75
2-Butanone (MEK)471 ug/m3 10/24/14 12:09 78-93-352.5 23.9 87.5
Carbon disulfide 6.1 ug/m3 10/23/14 20:30 75-15-01.1 0.13 1.75
Carbon tetrachloride ND ug/m3 10/23/14 20:30 56-23-51.1 0.56 1.75
Chlorobenzene ND ug/m3 10/23/14 20:30 108-90-71.6 0.19 1.75
Chloroethane ND ug/m3 10/23/14 20:30 75-00-30.94 0.28 1.75
Chloroform ND ug/m3 10/23/14 20:30 67-66-30.87 0.31 1.75
Chloromethane ND ug/m3 10/23/14 20:30 74-87-30.74 0.34 1.75
Cyclohexane ND ug/m3 10/23/14 20:30 110-82-71.2 0.22 1.75
Dibromochloromethane ND ug/m3 10/23/14 20:30 124-48-13.0 1.5 1.75
1,2-Dibromoethane (EDB)ND ug/m3 10/23/14 20:30 106-93-42.7 0.41 1.75
1,2-Dichlorobenzene ND ug/m3 10/23/14 20:30 95-50-12.1 0.25 1.75
1,3-Dichlorobenzene ND ug/m3 10/23/14 20:30 541-73-12.1 0.41 1.75
1,4-Dichlorobenzene ND ug/m3 10/23/14 20:30 106-46-72.1 0.35 1.75
Dichlorodifluoromethane 3.8 ug/m3 10/23/14 20:30 75-71-81.8 0.19 1.75
1,1-Dichloroethane ND ug/m3 10/23/14 20:30 75-34-31.4 0.24 1.75
1,2-Dichloroethane ND ug/m3 10/23/14 20:30 107-06-20.72 0.21 1.75
1,1-Dichloroethene ND ug/m3 10/23/14 20:30 75-35-41.4 0.18 1.75
cis-1,2-Dichloroethene ND ug/m3 10/23/14 20:30 156-59-21.4 0.34 1.75
trans-1,2-Dichloroethene ND ug/m3 10/23/14 20:30 156-60-51.4 0.29 1.75
1,2-Dichloropropane ND ug/m3 10/23/14 20:30 78-87-51.6 0.27 1.75
cis-1,3-Dichloropropene ND ug/m3 10/23/14 20:30 10061-01-51.6 0.24 1.75
trans-1,3-Dichloropropene ND ug/m3 10/23/14 20:30 10061-02-61.6 0.26 1.75
Dichlorotetrafluoroethane ND ug/m3 10/23/14 20:30 76-14-22.5 0.44 1.75
Ethyl acetate ND ug/m3 10/23/14 20:30 141-78-61.3 0.22 1.75
Ethylbenzene 1.4J ug/m3 10/23/14 20:30 100-41-41.5 0.31 1.75
4-Ethyltoluene 0.91J ug/m3 10/23/14 20:30 622-96-81.8 0.30 1.75
n-Heptane 5.4 ug/m3 10/23/14 20:30 142-82-51.5 0.28 1.75
Hexachloro-1,3-butadiene ND ug/m3 10/23/14 20:30 87-68-33.8 0.72 1.75
n-Hexane 37.4 ug/m3 10/23/14 20:30 110-54-31.3 0.18 1.75
2-Hexanone 5.4 ug/m3 10/23/14 20:30 591-78-61.5 0.37 1.75
Methylene Chloride 33.0 ug/m3 10/23/14 20:30 75-09-26.2 0.40 1.75
4-Methyl-2-pentanone (MIBK)8.0 ug/m3 10/23/14 20:30 108-10-11.5 0.30 1.75
Methyl-tert-butyl ether ND ug/m3 10/23/14 20:30 1634-04-41.3 0.16 1.75
Naphthalene 1.6J ug/m3 10/23/14 20:30 91-20-3 SS4.7 0.45 1.75
Propylene ND ug/m3 10/23/14 20:30 115-07-10.61 0.19 1.75
Styrene 2.1 ug/m3 10/23/14 20:30 100-42-51.5 0.24 1.75
1,1,2,2-Tetrachloroethane ND ug/m3 10/23/14 20:30 79-34-51.2 0.41 1.75
Tetrachloroethene 35.1 ug/m3 10/23/14 20:30 127-18-41.2 0.33 1.75
Tetrahydrofuran 17.1 ug/m3 10/23/14 20:30 109-99-91.0 0.24 1.75
Toluene 5.6 ug/m3 10/23/14 20:30 108-88-31.3 0.24 1.75
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:SG-1 Lab ID:92222006001 Collected:10/16/14 16:38 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 10/23/14 20:30 120-82-12.6 0.64 1.75
1,1,1-Trichloroethane ND ug/m3 10/23/14 20:30 71-55-61.9 0.24 1.75
1,1,2-Trichloroethane ND ug/m3 10/23/14 20:30 79-00-50.96 0.43 1.75
Trichloroethene ND ug/m3 10/23/14 20:30 79-01-60.96 0.31 1.75
Trichlorofluoromethane 48.0 ug/m3 10/23/14 20:30 75-69-42.0 0.24 1.75
1,1,2-Trichlorotrifluoroethane ND ug/m3 10/23/14 20:30 76-13-12.8 0.28 1.75
1,2,4-Trimethylbenzene 4.9 ug/m3 10/23/14 20:30 95-63-61.7 0.21 1.75
1,3,5-Trimethylbenzene 0.89J ug/m3 10/23/14 20:30 108-67-81.7 0.36 1.75
Vinyl acetate ND ug/m3 10/23/14 20:30 108-05-41.3 0.61 1.75
Vinyl chloride ND ug/m3 10/23/14 20:30 75-01-40.46 0.16 1.75
m&p-Xylene 5.8 ug/m3 10/23/14 20:30 179601-23-13.1 0.24 1.75
o-Xylene 2.8 ug/m3 10/23/14 20:30 95-47-61.5 0.77 1.75
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:SG-2 Lab ID:92222006002 Collected:10/16/14 17:07 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 611 ug/m3 10/24/14 08:16 67-64-116280.9 67
Benzene 36.5 ug/m3 10/24/14 08:16 71-43-221.8 7.9 67
Bromodichloromethane ND ug/m3 10/24/14 08:16 75-27-491.1 12.2 67
Bromoform ND ug/m3 10/24/14 08:16 75-25-214121.6 67
Bromomethane ND ug/m3 10/24/14 08:16 74-83-952.9 18.1 67
1,3-Butadiene ND ug/m3 10/24/14 08:16 106-99-030.2 5.7 67
2-Butanone (MEK)342 ug/m3 10/24/14 08:16 78-93-340.2 18.3 67
Carbon disulfide 50.3 ug/m3 10/24/14 08:16 75-15-042.2 4.8 67
Carbon tetrachloride ND ug/m3 10/24/14 08:16 56-23-542.9 21.4 67
Chlorobenzene ND ug/m3 10/24/14 08:16 108-90-763.0 7.1 67
Chloroethane ND ug/m3 10/24/14 08:16 75-00-336.2 10.8 67
Chloroform ND ug/m3 10/24/14 08:16 67-66-333.2 12.0 67
Chloromethane ND ug/m3 10/24/14 08:16 74-87-328.1 12.9 67
Cyclohexane ND ug/m3 10/24/14 08:16 110-82-746.9 8.4 67
Dibromochloromethane ND ug/m3 10/24/14 08:16 124-48-111658.0 67
1,2-Dibromoethane (EDB)ND ug/m3 10/24/14 08:16 106-93-410515.7 67
1,2-Dichlorobenzene ND ug/m3 10/24/14 08:16 95-50-181.7 9.4 67
1,3-Dichlorobenzene ND ug/m3 10/24/14 08:16 541-73-181.7 15.5 67
1,4-Dichlorobenzene ND ug/m3 10/24/14 08:16 106-46-781.7 13.3 67
Dichlorodifluoromethane ND ug/m3 10/24/14 08:16 75-71-867.7 7.3 67
1,1-Dichloroethane ND ug/m3 10/24/14 08:16 75-34-354.9 9.4 67
1,2-Dichloroethane ND ug/m3 10/24/14 08:16 107-06-227.5 8.0 67
1,1-Dichloroethene ND ug/m3 10/24/14 08:16 75-35-454.3 6.9 67
cis-1,2-Dichloroethene ND ug/m3 10/24/14 08:16 156-59-254.3 13.1 67
trans-1,2-Dichloroethene ND ug/m3 10/24/14 08:16 156-60-554.3 10.9 67
1,2-Dichloropropane ND ug/m3 10/24/14 08:16 78-87-563.0 10.2 67
cis-1,3-Dichloropropene ND ug/m3 10/24/14 08:16 10061-01-561.6 9.1 67
trans-1,3-Dichloropropene ND ug/m3 10/24/14 08:16 10061-02-661.6 10.1 67
Dichlorotetrafluoroethane ND ug/m3 10/24/14 08:16 76-14-295.1 16.7 67
Ethyl acetate ND ug/m3 10/24/14 08:16 141-78-648.9 8.4 67
Ethylbenzene 50.1J ug/m3 10/24/14 08:16 100-41-459.0 12.0 67
4-Ethyltoluene 845 ug/m3 10/24/14 08:16 622-96-867.0 11.7 67
n-Heptane 108 ug/m3 10/24/14 08:16 142-82-555.6 10.9 67
Hexachloro-1,3-butadiene ND ug/m3 10/24/14 08:16 87-68-314727.5 67
n-Hexane 25.4J ug/m3 10/24/14 08:16 110-54-348.2 6.8 67
2-Hexanone ND ug/m3 10/24/14 08:16 591-78-655.6 14.3 67
Methylene Chloride ND ug/m3 10/24/14 08:16 75-09-223715.5 67
4-Methyl-2-pentanone (MIBK)67.7 ug/m3 10/24/14 08:16 108-10-155.6 11.5 67
Methyl-tert-butyl ether ND ug/m3 10/24/14 08:16 1634-04-448.9 6.0 67
Naphthalene ND ug/m3 10/24/14 08:16 91-20-317817.3 67
Propylene 384 ug/m3 10/24/14 08:16 115-07-123.4 7.4 67
Styrene ND ug/m3 10/24/14 08:16 100-42-558.3 9.0 67
1,1,2,2-Tetrachloroethane 17200 ug/m3 10/24/14 13:57 79-34-5 A3599200857.6
Tetrachloroethene 503 ug/m3 10/24/14 08:16 127-18-446.2 12.6 67
Tetrahydrofuran ND ug/m3 10/24/14 08:16 109-99-940.2 9.3 67
Toluene 59.6 ug/m3 10/24/14 08:16 108-88-351.6 9.0 67
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:SG-2 Lab ID:92222006002 Collected:10/16/14 17:07 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 10/24/14 08:16 120-82-110124.4 67
1,1,1-Trichloroethane 46.6J ug/m3 10/24/14 08:16 71-55-674.4 9.3 67
1,1,2-Trichloroethane ND ug/m3 10/24/14 08:16 79-00-536.8 16.3 67
Trichloroethene 4480 ug/m3 10/24/14 08:16 79-01-636.8 11.9 67
Trichlorofluoromethane ND ug/m3 10/24/14 08:16 75-69-476.4 9.2 67
1,1,2-Trichlorotrifluoroethane ND ug/m3 10/24/14 08:16 76-13-110710.7 67
1,2,4-Trimethylbenzene 2830 ug/m3 10/24/14 08:16 95-63-666.9 8.2 67
1,3,5-Trimethylbenzene 1800 ug/m3 10/24/14 08:16 108-67-866.9 13.9 67
Vinyl acetate ND ug/m3 10/24/14 08:16 108-05-448.0 23.3 67
Vinyl chloride ND ug/m3 10/24/14 08:16 75-01-417.4 6.2 67
m&p-Xylene ND ug/m3 10/24/14 08:16 179601-23-11189.4 67
o-Xylene 701 ug/m3 10/24/14 08:16 95-47-659.0 29.5 67
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:SG-3 Lab ID:92222006003 Collected:10/16/14 20:02 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 301 ug/m3 10/23/14 21:16 67-64-1 E4.1 2.0 1.68
Benzene 2.8 ug/m3 10/23/14 21:16 71-43-20.55 0.20 1.68
Bromodichloromethane ND ug/m3 10/23/14 21:16 75-27-42.3 0.31 1.68
Bromoform ND ug/m3 10/23/14 21:16 75-25-23.5 0.54 1.68
Bromomethane ND ug/m3 10/23/14 21:16 74-83-91.3 0.45 1.68
1,3-Butadiene ND ug/m3 10/23/14 21:16 106-99-00.76 0.14 1.68
2-Butanone (MEK)98.8 ug/m3 10/23/14 21:16 78-93-31.0 0.46 1.68
Carbon disulfide 8.2 ug/m3 10/23/14 21:16 75-15-01.1 0.12 1.68
Carbon tetrachloride ND ug/m3 10/23/14 21:16 56-23-51.1 0.54 1.68
Chlorobenzene ND ug/m3 10/23/14 21:16 108-90-71.6 0.18 1.68
Chloroethane ND ug/m3 10/23/14 21:16 75-00-30.91 0.27 1.68
Chloroform ND ug/m3 10/23/14 21:16 67-66-30.83 0.30 1.68
Chloromethane ND ug/m3 10/23/14 21:16 74-87-30.71 0.32 1.68
Cyclohexane ND ug/m3 10/23/14 21:16 110-82-71.2 0.21 1.68
Dibromochloromethane ND ug/m3 10/23/14 21:16 124-48-12.9 1.5 1.68
1,2-Dibromoethane (EDB)ND ug/m3 10/23/14 21:16 106-93-42.6 0.39 1.68
1,2-Dichlorobenzene ND ug/m3 10/23/14 21:16 95-50-12.0 0.24 1.68
1,3-Dichlorobenzene ND ug/m3 10/23/14 21:16 541-73-12.0 0.39 1.68
1,4-Dichlorobenzene ND ug/m3 10/23/14 21:16 106-46-72.0 0.33 1.68
Dichlorodifluoromethane 2.3 ug/m3 10/23/14 21:16 75-71-81.7 0.18 1.68
1,1-Dichloroethane ND ug/m3 10/23/14 21:16 75-34-31.4 0.24 1.68
1,2-Dichloroethane ND ug/m3 10/23/14 21:16 107-06-20.69 0.20 1.68
1,1-Dichloroethene ND ug/m3 10/23/14 21:16 75-35-41.4 0.17 1.68
cis-1,2-Dichloroethene ND ug/m3 10/23/14 21:16 156-59-21.4 0.33 1.68
trans-1,2-Dichloroethene ND ug/m3 10/23/14 21:16 156-60-51.4 0.27 1.68
1,2-Dichloropropane ND ug/m3 10/23/14 21:16 78-87-51.6 0.26 1.68
cis-1,3-Dichloropropene ND ug/m3 10/23/14 21:16 10061-01-51.5 0.23 1.68
trans-1,3-Dichloropropene ND ug/m3 10/23/14 21:16 10061-02-61.5 0.25 1.68
Dichlorotetrafluoroethane ND ug/m3 10/23/14 21:16 76-14-22.4 0.42 1.68
Ethyl acetate ND ug/m3 10/23/14 21:16 141-78-61.2 0.21 1.68
Ethylbenzene 3.3 ug/m3 10/23/14 21:16 100-41-41.5 0.30 1.68
4-Ethyltoluene 1.2J ug/m3 10/23/14 21:16 622-96-81.7 0.29 1.68
n-Heptane 5.8 ug/m3 10/23/14 21:16 142-82-51.4 0.27 1.68
Hexachloro-1,3-butadiene ND ug/m3 10/23/14 21:16 87-68-33.7 0.69 1.68
n-Hexane 3.5 ug/m3 10/23/14 21:16 110-54-31.2 0.17 1.68
2-Hexanone 13.8 ug/m3 10/23/14 21:16 591-78-61.4 0.36 1.68
Methylene Chloride 2.2J ug/m3 10/23/14 21:16 75-09-25.9 0.39 1.68
4-Methyl-2-pentanone (MIBK)10.5 ug/m3 10/23/14 21:16 108-10-11.4 0.29 1.68
Methyl-tert-butyl ether 1.4 ug/m3 10/23/14 21:16 1634-04-41.2 0.15 1.68
Naphthalene 2.4J ug/m3 10/23/14 21:16 91-20-3 SS4.5 0.43 1.68
Propylene 4.6 ug/m3 10/23/14 21:16 115-07-10.59 0.18 1.68
Styrene 2.6 ug/m3 10/23/14 21:16 100-42-51.5 0.23 1.68
1,1,2,2-Tetrachloroethane ND ug/m3 10/23/14 21:16 79-34-51.2 0.39 1.68
Tetrachloroethene 21.4 ug/m3 10/23/14 21:16 127-18-41.2 0.32 1.68
Tetrahydrofuran ND ug/m3 10/23/14 21:16 109-99-91.0 0.23 1.68
Toluene 12.4 ug/m3 10/23/14 21:16 108-88-31.3 0.23 1.68
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:SG-3 Lab ID:92222006003 Collected:10/16/14 20:02 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 10/23/14 21:16 120-82-12.5 0.61 1.68
1,1,1-Trichloroethane ND ug/m3 10/23/14 21:16 71-55-61.9 0.23 1.68
1,1,2-Trichloroethane ND ug/m3 10/23/14 21:16 79-00-50.92 0.41 1.68
Trichloroethene ND ug/m3 10/23/14 21:16 79-01-60.92 0.30 1.68
Trichlorofluoromethane 1.1J ug/m3 10/23/14 21:16 75-69-41.9 0.23 1.68
1,1,2-Trichlorotrifluoroethane ND ug/m3 10/23/14 21:16 76-13-12.7 0.27 1.68
1,2,4-Trimethylbenzene 2.0 ug/m3 10/23/14 21:16 95-63-61.7 0.20 1.68
1,3,5-Trimethylbenzene 0.93J ug/m3 10/23/14 21:16 108-67-81.7 0.35 1.68
Vinyl acetate ND ug/m3 10/23/14 21:16 108-05-41.2 0.58 1.68
Vinyl chloride ND ug/m3 10/23/14 21:16 75-01-40.44 0.16 1.68
m&p-Xylene 12.9 ug/m3 10/23/14 21:16 179601-23-13.0 0.24 1.68
o-Xylene 4.9 ug/m3 10/23/14 21:16 95-47-61.5 0.74 1.68
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:AA-1 Lab ID:92222006004 Collected:10/16/14 17:02 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 15.8 ug/m3 10/23/14 20:53 67-64-13.5 1.7 1.44
Benzene 2.6 ug/m3 10/23/14 20:53 71-43-20.47 0.17 1.44
Bromodichloromethane ND ug/m3 10/23/14 20:53 75-27-42.0 0.26 1.44
Bromoform ND ug/m3 10/23/14 20:53 75-25-23.0 0.47 1.44
Bromomethane ND ug/m3 10/23/14 20:53 74-83-91.1 0.39 1.44
1,3-Butadiene ND ug/m3 10/23/14 20:53 106-99-00.65 0.12 1.44
2-Butanone (MEK)2.9 ug/m3 10/23/14 20:53 78-93-30.86 0.39 1.44
Carbon disulfide ND ug/m3 10/23/14 20:53 75-15-00.91 0.10 1.44
Carbon tetrachloride ND ug/m3 10/23/14 20:53 56-23-50.92 0.46 1.44
Chlorobenzene ND ug/m3 10/23/14 20:53 108-90-71.4 0.15 1.44
Chloroethane ND ug/m3 10/23/14 20:53 75-00-30.78 0.23 1.44
Chloroform ND ug/m3 10/23/14 20:53 67-66-30.71 0.26 1.44
Chloromethane ND ug/m3 10/23/14 20:53 74-87-30.60 0.28 1.44
Cyclohexane ND ug/m3 10/23/14 20:53 110-82-71.0 0.18 1.44
Dibromochloromethane ND ug/m3 10/23/14 20:53 124-48-12.5 1.2 1.44
1,2-Dibromoethane (EDB)ND ug/m3 10/23/14 20:53 106-93-42.2 0.34 1.44
1,2-Dichlorobenzene ND ug/m3 10/23/14 20:53 95-50-11.8 0.20 1.44
1,3-Dichlorobenzene ND ug/m3 10/23/14 20:53 541-73-11.8 0.33 1.44
1,4-Dichlorobenzene ND ug/m3 10/23/14 20:53 106-46-71.8 0.29 1.44
Dichlorodifluoromethane 2.5 ug/m3 10/23/14 20:53 75-71-81.5 0.16 1.44
1,1-Dichloroethane ND ug/m3 10/23/14 20:53 75-34-31.2 0.20 1.44
1,2-Dichloroethane ND ug/m3 10/23/14 20:53 107-06-20.59 0.17 1.44
1,1-Dichloroethene ND ug/m3 10/23/14 20:53 75-35-41.2 0.15 1.44
cis-1,2-Dichloroethene ND ug/m3 10/23/14 20:53 156-59-21.2 0.28 1.44
trans-1,2-Dichloroethene ND ug/m3 10/23/14 20:53 156-60-51.2 0.23 1.44
1,2-Dichloropropane ND ug/m3 10/23/14 20:53 78-87-51.4 0.22 1.44
cis-1,3-Dichloropropene ND ug/m3 10/23/14 20:53 10061-01-51.3 0.20 1.44
trans-1,3-Dichloropropene ND ug/m3 10/23/14 20:53 10061-02-61.3 0.22 1.44
Dichlorotetrafluoroethane ND ug/m3 10/23/14 20:53 76-14-22.0 0.36 1.44
Ethyl acetate ND ug/m3 10/23/14 20:53 141-78-61.1 0.18 1.44
Ethylbenzene 1.8 ug/m3 10/23/14 20:53 100-41-41.3 0.26 1.44
4-Ethyltoluene 0.74J ug/m3 10/23/14 20:53 622-96-81.4 0.25 1.44
n-Heptane 101 ug/m3 10/23/14 20:53 142-82-51.2 0.23 1.44
Hexachloro-1,3-butadiene ND ug/m3 10/23/14 20:53 87-68-33.2 0.59 1.44
n-Hexane 9.6 ug/m3 10/23/14 20:53 110-54-31.0 0.15 1.44
2-Hexanone ND ug/m3 10/23/14 20:53 591-78-61.2 0.31 1.44
Methylene Chloride 1.3J ug/m3 10/23/14 20:53 75-09-25.1 0.33 1.44
4-Methyl-2-pentanone (MIBK)ND ug/m3 10/23/14 20:53 108-10-11.2 0.25 1.44
Methyl-tert-butyl ether ND ug/m3 10/23/14 20:53 1634-04-41.1 0.13 1.44
Naphthalene 1.1J ug/m3 10/23/14 20:53 91-20-3 SS3.8 0.37 1.44
Propylene ND ug/m3 10/23/14 20:53 115-07-10.50 0.16 1.44
Styrene ND ug/m3 10/23/14 20:53 100-42-51.3 0.19 1.44
1,1,2,2-Tetrachloroethane ND ug/m3 10/23/14 20:53 79-34-51.0 0.34 1.44
Tetrachloroethene ND ug/m3 10/23/14 20:53 127-18-40.99 0.27 1.44
Tetrahydrofuran ND ug/m3 10/23/14 20:53 109-99-90.86 0.20 1.44
Toluene 7.6 ug/m3 10/23/14 20:53 108-88-31.1 0.19 1.44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Sample:AA-1 Lab ID:92222006004 Collected:10/16/14 17:02 Received:10/17/14 16:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 10/23/14 20:53 120-82-12.2 0.52 1.44
1,1,1-Trichloroethane ND ug/m3 10/23/14 20:53 71-55-61.6 0.20 1.44
1,1,2-Trichloroethane ND ug/m3 10/23/14 20:53 79-00-50.79 0.35 1.44
Trichloroethene ND ug/m3 10/23/14 20:53 79-01-60.79 0.26 1.44
Trichlorofluoromethane 1.7 ug/m3 10/23/14 20:53 75-69-41.6 0.20 1.44
1,1,2-Trichlorotrifluoroethane ND ug/m3 10/23/14 20:53 76-13-12.3 0.23 1.44
1,2,4-Trimethylbenzene 1.8 ug/m3 10/23/14 20:53 95-63-61.4 0.18 1.44
1,3,5-Trimethylbenzene ND ug/m3 10/23/14 20:53 108-67-81.4 0.30 1.44
Vinyl acetate ND ug/m3 10/23/14 20:53 108-05-41.0 0.50 1.44
Vinyl chloride ND ug/m3 10/23/14 20:53 75-01-40.37 0.13 1.44
m&p-Xylene 5.5 ug/m3 10/23/14 20:53 179601-23-12.5 0.20 1.44
o-Xylene 1.9 ug/m3 10/23/14 20:53 95-47-61.3 0.64 1.44
REPORT OF LABORATORY ANALYSIS
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Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/21644
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92222006001, 92222006002, 92222006003, 92222006004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1825298
Associated Lab Samples:92222006001, 92222006002, 92222006003, 92222006004
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 10/23/14 15:51
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 10/23/14 15:51
1,1,2-Trichloroethane ug/m3 ND 0.55 10/23/14 15:51
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 10/23/14 15:51
1,1-Dichloroethane ug/m3 ND 0.82 10/23/14 15:51
1,1-Dichloroethene ug/m3 ND 0.81 10/23/14 15:51
1,2,4-Trichlorobenzene ug/m3 ND 1.5 10/23/14 15:51
1,2,4-Trimethylbenzene ug/m3 ND 1.0 10/23/14 15:51
1,2-Dibromoethane (EDB)ug/m3 ND 1.6 10/23/14 15:51
1,2-Dichlorobenzene ug/m3 ND 1.2 10/23/14 15:51
1,2-Dichloroethane ug/m3 ND 0.41 10/23/14 15:51
1,2-Dichloropropane ug/m3 ND 0.94 10/23/14 15:51
1,3,5-Trimethylbenzene ug/m3 ND 1.0 10/23/14 15:51
1,3-Butadiene ug/m3 ND 0.45 10/23/14 15:51
1,3-Dichlorobenzene ug/m3 ND 1.2 10/23/14 15:51
1,4-Dichlorobenzene ug/m3 ND 1.2 10/23/14 15:51
2-Butanone (MEK)ug/m3 ND 0.60 10/23/14 15:51
2-Hexanone ug/m3 ND 0.83 10/23/14 15:51
4-Ethyltoluene ug/m3 ND 1.0 10/23/14 15:51
4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 10/23/14 15:51
Acetone ug/m3 ND 2.4 10/23/14 15:51
Benzene ug/m3 ND 0.32 10/23/14 15:51
Bromodichloromethane ug/m3 ND 1.4 10/23/14 15:51
Bromoform ug/m3 ND 2.1 10/23/14 15:51
Bromomethane ug/m3 ND 0.79 10/23/14 15:51
Carbon disulfide ug/m3 ND 0.63 10/23/14 15:51
Carbon tetrachloride ug/m3 ND 0.64 10/23/14 15:51
Chlorobenzene ug/m3 ND 0.94 10/23/14 15:51
Chloroethane ug/m3 ND 0.54 10/23/14 15:51
Chloroform ug/m3 ND 0.50 10/23/14 15:51
Chloromethane ug/m3 ND 0.42 10/23/14 15:51
cis-1,2-Dichloroethene ug/m3 ND 0.81 10/23/14 15:51
cis-1,3-Dichloropropene ug/m3 ND 0.92 10/23/14 15:51
Cyclohexane ug/m3 ND 0.70 10/23/14 15:51
Dibromochloromethane ug/m3 ND 1.7 10/23/14 15:51
Dichlorodifluoromethane ug/m3 ND 1.0 10/23/14 15:51
Dichlorotetrafluoroethane ug/m3 ND 1.4 10/23/14 15:51
Ethyl acetate ug/m3 ND 0.73 10/23/14 15:51
Ethylbenzene ug/m3 ND 0.88 10/23/14 15:51
Hexachloro-1,3-butadiene ug/m3 ND 2.2 10/23/14 15:51
m&p-Xylene ug/m3 ND 1.8 10/23/14 15:51
REPORT OF LABORATORY ANALYSIS
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Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1825298
Associated Lab Samples:92222006001, 92222006002, 92222006003, 92222006004
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 0.73 10/23/14 15:51
Methylene Chloride ug/m3 ND 3.5 10/23/14 15:51
n-Heptane ug/m3 ND 0.83 10/23/14 15:51
n-Hexane ug/m3 ND 0.72 10/23/14 15:51
Naphthalene ug/m3 ND 2.7 10/23/14 15:51
o-Xylene ug/m3 ND 0.88 10/23/14 15:51
Propylene ug/m3 ND 0.35 10/23/14 15:51
Styrene ug/m3 ND 0.87 10/23/14 15:51
Tetrachloroethene ug/m3 ND 0.69 10/23/14 15:51
Tetrahydrofuran ug/m3 ND 0.60 10/23/14 15:51
Toluene ug/m3 ND 0.77 10/23/14 15:51
trans-1,2-Dichloroethene ug/m3 ND 0.81 10/23/14 15:51
trans-1,3-Dichloropropene ug/m3 ND 0.92 10/23/14 15:51
Trichloroethene ug/m3 ND 0.55 10/23/14 15:51
Trichlorofluoromethane ug/m3 ND 1.1 10/23/14 15:51
Vinyl acetate ug/m3 ND 0.72 10/23/14 15:51
Vinyl chloride ug/m3 ND 0.26 10/23/14 15:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1825299LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 46.655.5 84 72-128
1,1,2,2-Tetrachloroethane ug/m3 57.069.8 82 72-136
1,1,2-Trichloroethane ug/m3 49.155.5 88 72-130
1,1,2-Trichlorotrifluoroethane ug/m3 69.077.9 89 68-126
1,1-Dichloroethane ug/m3 35.441.2 86 68-128
1,1-Dichloroethene ug/m3 37.240.3 92 68-130
1,2,4-Trichlorobenzene ug/m3 64.075.5 85 30-150
1,2,4-Trimethylbenzene ug/m3 55.450 111 71-140
1,2-Dibromoethane (EDB)ug/m3 74.678.1 95 73-136
1,2-Dichlorobenzene ug/m3 54.961.2 90 63-150
1,2-Dichloroethane ug/m3 34.441.2 84 71-132
1,2-Dichloropropane ug/m3 41.247 88 72-130
1,3,5-Trimethylbenzene ug/m3 55.550 111 73-136
1,3-Butadiene ug/m3 22.122.5 98 72-130
1,3-Dichlorobenzene ug/m3 55.561.2 91 69-142
1,4-Dichlorobenzene ug/m3 55.061.2 90 65-142
2-Butanone (MEK)ug/m3 29.630 99 71-135
2-Hexanone ug/m3 48.141.7 115 75-133
4-Ethyltoluene ug/m3 56.150 112 73-134
4-Methyl-2-pentanone (MIBK)ug/m3 46.341.7 111 72-137
Acetone ug/m3 23.224.2 96 68-136
Benzene ug/m3 32.532.5 100 69-134
Bromodichloromethane ug/m3 59.368.2 87 74-129
REPORT OF LABORATORY ANALYSIS
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Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1825299LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 97.8105 93 69-138
Bromomethane ug/m3 41.339.5 105 68-127
Carbon disulfide ug/m3 29.431.7 93 68-130
Carbon tetrachloride ug/m3 56.664 88 66-134
Chlorobenzene ug/m3 47.646.8 102 72-137
Chloroethane ug/m3 26.526.8 99 69-128
Chloroform ug/m3 44.849.7 90 72-127
Chloromethane ug/m3 17.221 82 69-125
cis-1,2-Dichloroethene ug/m3 40.840.3 101 71-135
cis-1,3-Dichloropropene ug/m3 47.546.2 103 74-134
Cyclohexane ug/m3 29.135 83 72-130
Dibromochloromethane ug/m3 82.086.6 95 73-133
Dichlorodifluoromethane ug/m3 44.850.3 89 69-125
Dichlorotetrafluoroethane ug/m3 60.071.1 84 68-128
Ethyl acetate ug/m3 34.436.6 94 71-134
Ethylbenzene ug/m3 42.144.2 95 73-139
Hexachloro-1,3-butadiene ug/m3 87.3108 80 30-150
m&p-Xylene ug/m3 94.088.3 106 73-139
Methyl-tert-butyl ether ug/m3 41.436.7 113 72-132
Methylene Chloride ug/m3 32.435.3 92 64-134
n-Heptane ug/m3 42.741.7 102 70-130
n-Hexane ug/m3 40.035.8 112 69-128
Naphthalene ug/m3 50.4 SS53.3 95 61-150
o-Xylene ug/m3 50.844.2 115 71-138
Propylene ug/m3 16.717.5 95 69-133
Styrene ug/m3 43.443.3 100 74-136
Tetrachloroethene ug/m3 74.969 109 69-136
Tetrahydrofuran ug/m3 27.430 91 73-131
Toluene ug/m3 38.338.3 100 67-133
trans-1,2-Dichloroethene ug/m3 37.140.3 92 70-131
trans-1,3-Dichloropropene ug/m3 45.346.2 98 72-135
Trichloroethene ug/m3 59.454.6 109 70-135
Trichlorofluoromethane ug/m3 45.657.1 80 67-125
Vinyl acetate ug/m3 37.935.8 106 72-133
Vinyl chloride ug/m3 27.826 107 69-132
REPORT OF LABORATORY ANALYSIS
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Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
This result is reported from a serial dilution.A3
Analyte concentration exceeded the calibration range. The reported result is estimated.E
This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be
considered an estimated value.SS
REPORT OF LABORATORY ANALYSIS
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Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92222006
FORMER BOULIGNY SITE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92222006001 AIR/21644SG-1 TO-15
92222006002 AIR/21644SG-2 TO-15
92222006003 AIR/21644SG-3 TO-15
92222006004 AIR/21644AA-1 TO-15
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/28/2014 05:43 PM
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Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
October 31, 2014
LIMS USE: FR - CHRIS CORBITT
LIMS OBJECT ID: 92222333
92222333
Project:
Pace Project No.:
RE:
Mr. Chris Corbitt
Terracon
2020 E-Starita Road
Charlotte, NC 28206
NODA Site - 71147763
Dear Mr. Corbitt:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
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[phone]
Page 1 of 15
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Lab ID Sample ID Matrix Date Collected Date Received
92222333001 TMW-1 Water 10/21/14 11:05 10/21/14 17:10
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92222333001 TMW-1 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Sample:TMW-1 Lab ID:92222333001 Collected:10/21/14 11:05 Received:10/21/14 17:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/29/14 17:22 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/29/14 17:22 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/29/14 17:22 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/29/14 17:22 75-27-40.50 0.25 1
Bromoform ND ug/L 10/29/14 17:22 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/29/14 17:22 74-83-95.0 0.50 1
n-Butylbenzene ND ug/L 10/29/14 17:22 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/29/14 17:22 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/29/14 17:22 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/29/14 17:22 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/29/14 17:22 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/29/14 17:22 75-00-31.0 0.50 1
Chloroform ND ug/L 10/29/14 17:22 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/29/14 17:22 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/29/14 17:22 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/29/14 17:22 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/29/14 17:22 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/29/14 17:22 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/29/14 17:22 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/29/14 17:22 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 10/29/14 17:22 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/29/14 17:22 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/29/14 17:22 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/29/14 17:22 75-71-80.50 0.25 1
1,1-Dichloroethane 0.61 ug/L 10/29/14 17:22 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/29/14 17:22 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/29/14 17:22 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/29/14 17:22 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/29/14 17:22 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/29/14 17:22 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/29/14 17:22 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 10/29/14 17:22 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/29/14 17:22 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/29/14 17:22 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/29/14 17:22 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/29/14 17:22 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/29/14 17:22 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/29/14 17:22 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/29/14 17:22 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/29/14 17:22 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 10/29/14 17:22 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/29/14 17:22 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/29/14 17:22 103-65-10.50 0.25 1
Styrene ND ug/L 10/29/14 17:22 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/29/14 17:22 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/29/14 17:22 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Sample:TMW-1 Lab ID:92222333001 Collected:10/21/14 11:05 Received:10/21/14 17:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 10/29/14 17:22 127-18-40.50 0.25 1
Toluene ND ug/L 10/29/14 17:22 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/29/14 17:22 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/29/14 17:22 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/29/14 17:22 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/29/14 17:22 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/29/14 17:22 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/29/14 17:22 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/29/14 17:22 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/29/14 17:22 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/29/14 17:22 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/29/14 17:22 75-01-41.0 0.25 1
m&p-Xylene ND ug/L 10/29/14 17:22 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/29/14 17:22 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %10/29/14 17:22 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %10/29/14 17:22 460-00-470-130 1
Toluene-d8 (S)101 %10/29/14 17:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/31/2014 11:48 AM
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Page 6 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/28972
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92222333001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1317804
Associated Lab Samples:92222333001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/29/14 15:59
1,1,1-Trichloroethane ug/L ND 0.50 10/29/14 15:59
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/29/14 15:59
1,1,2-Trichloroethane ug/L ND 0.50 10/29/14 15:59
1,1-Dichloroethane ug/L ND 0.50 10/29/14 15:59
1,1-Dichloroethene ug/L ND 0.50 10/29/14 15:59
1,1-Dichloropropene ug/L ND 0.50 10/29/14 15:59
1,2,3-Trichlorobenzene ug/L ND 2.0 10/29/14 15:59
1,2,3-Trichloropropane ug/L ND 0.50 10/29/14 15:59
1,2,4-Trichlorobenzene ug/L ND 2.0 10/29/14 15:59
1,2,4-Trimethylbenzene ug/L ND 0.50 10/29/14 15:59
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/29/14 15:59
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/29/14 15:59
1,2-Dichlorobenzene ug/L ND 0.50 10/29/14 15:59
1,2-Dichloroethane ug/L ND 0.50 10/29/14 15:59
1,2-Dichloropropane ug/L ND 0.50 10/29/14 15:59
1,3,5-Trimethylbenzene ug/L ND 0.50 10/29/14 15:59
1,3-Dichlorobenzene ug/L ND 0.50 10/29/14 15:59
1,3-Dichloropropane ug/L ND 0.50 10/29/14 15:59
1,4-Dichlorobenzene ug/L ND 0.50 10/29/14 15:59
2,2-Dichloropropane ug/L ND 0.50 10/29/14 15:59
2-Chlorotoluene ug/L ND 0.50 10/29/14 15:59
4-Chlorotoluene ug/L ND 0.50 10/29/14 15:59
Benzene ug/L ND 0.50 10/29/14 15:59
Bromobenzene ug/L ND 0.50 10/29/14 15:59
Bromochloromethane ug/L ND 0.50 10/29/14 15:59
Bromodichloromethane ug/L ND 0.50 10/29/14 15:59
Bromoform ug/L ND 0.50 10/29/14 15:59
Bromomethane ug/L ND 5.0 10/29/14 15:59
Carbon tetrachloride ug/L ND 0.50 10/29/14 15:59
Chlorobenzene ug/L ND 0.50 10/29/14 15:59
Chloroethane ug/L ND 1.0 10/29/14 15:59
Chloroform ug/L ND 0.50 10/29/14 15:59
Chloromethane ug/L ND 1.0 10/29/14 15:59
cis-1,2-Dichloroethene ug/L ND 0.50 10/29/14 15:59
cis-1,3-Dichloropropene ug/L ND 0.50 10/29/14 15:59
Dibromochloromethane ug/L ND 0.50 10/29/14 15:59
Dibromomethane ug/L ND 0.50 10/29/14 15:59
Dichlorodifluoromethane ug/L ND 0.50 10/29/14 15:59
Diisopropyl ether ug/L ND 0.50 10/29/14 15:59
Ethylbenzene ug/L ND 0.50 10/29/14 15:59
REPORT OF LABORATORY ANALYSIS
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Page 7 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1317804
Associated Lab Samples:92222333001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 10/29/14 15:59
Isopropylbenzene (Cumene)ug/L ND 0.50 10/29/14 15:59
m&p-Xylene ug/L ND 1.0 10/29/14 15:59
Methyl-tert-butyl ether ug/L ND 0.50 10/29/14 15:59
Methylene Chloride ug/L ND 2.0 10/29/14 15:59
n-Butylbenzene ug/L ND 0.50 10/29/14 15:59
n-Propylbenzene ug/L ND 0.50 10/29/14 15:59
Naphthalene ug/L ND 2.0 10/29/14 15:59
o-Xylene ug/L ND 0.50 10/29/14 15:59
sec-Butylbenzene ug/L ND 0.50 10/29/14 15:59
Styrene ug/L ND 0.50 10/29/14 15:59
tert-Butylbenzene ug/L ND 0.50 10/29/14 15:59
Tetrachloroethene ug/L ND 0.50 10/29/14 15:59
Toluene ug/L ND 0.50 10/29/14 15:59
trans-1,2-Dichloroethene ug/L ND 0.50 10/29/14 15:59
trans-1,3-Dichloropropene ug/L ND 0.50 10/29/14 15:59
Trichloroethene ug/L ND 0.50 10/29/14 15:59
Trichlorofluoromethane ug/L ND 1.0 10/29/14 15:59
Vinyl chloride ug/L ND 1.0 10/29/14 15:59
1,2-Dichloroethane-d4 (S)%93 70-130 10/29/14 15:59
4-Bromofluorobenzene (S)%100 70-130 10/29/14 15:59
Toluene-d8 (S)%100 70-130 10/29/14 15:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1317805LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 60-140
1,1,1-Trichloroethane ug/L 53.950 108 60-140
1,1,2,2-Tetrachloroethane ug/L 50.550 101 60-140
1,1,2-Trichloroethane ug/L 50.650 101 60-140
1,1-Dichloroethane ug/L 53.550 107 60-140
1,1-Dichloroethene ug/L 52.550 105 60-140
1,1-Dichloropropene ug/L 54.250 108 60-140
1,2,3-Trichlorobenzene ug/L 51.150 102 60-140
1,2,3-Trichloropropane ug/L 51.550 103 60-140
1,2,4-Trichlorobenzene ug/L 51.350 103 60-140
1,2,4-Trimethylbenzene ug/L 51.450 103 60-140
1,2-Dibromo-3-chloropropane ug/L 51.150 102 60-140
1,2-Dibromoethane (EDB)ug/L 51.050 102 60-140
1,2-Dichlorobenzene ug/L 50.850 102 60-140
1,2-Dichloroethane ug/L 49.750 99 60-140
1,2-Dichloropropane ug/L 52.950 106 60-140
1,3,5-Trimethylbenzene ug/L 51.850 104 60-140
1,3-Dichlorobenzene ug/L 50.950 102 60-140
REPORT OF LABORATORY ANALYSIS
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Page 8 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1317805LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.950 104 60-140
1,4-Dichlorobenzene ug/L 50.950 102 60-140
2,2-Dichloropropane ug/L 53.350 107 60-140
2-Chlorotoluene ug/L 53.250 106 60-140
4-Chlorotoluene ug/L 50.750 101 60-140
Benzene ug/L 52.150 104 60-140
Bromobenzene ug/L 52.050 104 60-140
Bromochloromethane ug/L 54.450 109 60-140
Bromodichloromethane ug/L 50.050 100 60-140
Bromoform ug/L 44.450 89 60-140
Bromomethane ug/L 49.150 98 60-140
Carbon tetrachloride ug/L 55.850 112 60-140
Chlorobenzene ug/L 51.350 103 60-140
Chloroethane ug/L 42.050 84 60-140
Chloroform ug/L 48.150 96 60-140
Chloromethane ug/L 43.850 88 60-140
cis-1,2-Dichloroethene ug/L 53.250 106 60-140
cis-1,3-Dichloropropene ug/L 54.350 109 60-140
Dibromochloromethane ug/L 52.750 105 60-140
Dibromomethane ug/L 50.350 101 60-140
Dichlorodifluoromethane ug/L 42.850 86 60-140
Diisopropyl ether ug/L 49.950 100 60-140
Ethylbenzene ug/L 51.350 103 60-140
Hexachloro-1,3-butadiene ug/L 51.050 102 60-140
Isopropylbenzene (Cumene)ug/L 52.550 105 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 47.350 95 60-140
Methylene Chloride ug/L 52.550 105 60-140
n-Butylbenzene ug/L 52.050 104 60-140
n-Propylbenzene ug/L 51.150 102 60-140
Naphthalene ug/L 49.150 98 60-140
o-Xylene ug/L 50.350 101 60-140
sec-Butylbenzene ug/L 52.350 105 60-140
Styrene ug/L 53.350 107 60-140
tert-Butylbenzene ug/L 44.550 89 60-140
Tetrachloroethene ug/L 49.950 100 60-140
Toluene ug/L 50.350 101 60-140
trans-1,2-Dichloroethene ug/L 52.250 104 60-140
trans-1,3-Dichloropropene ug/L 55.850 112 60-140
Trichloroethene ug/L 49.050 98 60-140
Trichlorofluoromethane ug/L 45.050 90 60-140
Vinyl chloride ug/L 40.750 81 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 9 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1317806MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92221975005
1317807
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 114 60-140109 4 3020ND22.8 21.9
1,1,1-Trichloroethane ug/L 20 122 60-140116 5 3020ND24.4 23.3
1,1,2,2-Tetrachloroethane ug/L 20 109 60-140107 2 3020ND21.7 21.3
1,1,2-Trichloroethane ug/L 20 110 60-140103 7 3020ND22.0 20.6
1,1-Dichloroethane ug/L 20 119 60-140111 6 3020ND23.7 22.3
1,1-Dichloroethene ug/L 20 122 60-140116 5 3020ND24.4 23.2
1,1-Dichloropropene ug/L 20 122 60-140116 4 3020ND24.3 23.3
1,2,3-Trichlorobenzene ug/L 20 107 60-140103 3 3020ND21.4 20.8
1,2,3-Trichloropropane ug/L 20 110 60-140110 0 3020ND22.0 22.0
1,2,4-Trichlorobenzene ug/L 20 107 60-140104 2 3020ND21.5 21.0
1,2,4-Trimethylbenzene ug/L 20 114 60-140107 7 3020ND22.9 21.4
1,2-Dibromo-3-
chloropropane ug/L 20 106 60-14099 7 3020ND21.2 19.8
1,2-Dibromoethane (EDB)ug/L 20 114 60-140107 6 3020ND22.9 21.5
1,2-Dichlorobenzene ug/L 20 109 60-140104 5 3020ND21.9 20.8
1,2-Dichloroethane ug/L 20 104 60-140100 4 3020ND20.8 20.0
1,2-Dichloropropane ug/L 20 114 60-140109 5 3020ND22.8 21.7
1,3,5-Trimethylbenzene ug/L 20 115 60-140109 5 3020ND22.9 21.9
1,3-Dichlorobenzene ug/L 20 111 60-140104 7 3020ND22.1 20.7
1,3-Dichloropropane ug/L 20 112 60-140107 5 3020ND22.4 21.3
1,4-Dichlorobenzene ug/L 20 110 60-140104 5 3020ND22.1 21.0
2,2-Dichloropropane ug/L 20 116 60-140111 4 3020ND23.2 22.3
2-Chlorotoluene ug/L 20 113 60-140107 5 3020ND22.6 21.4
4-Chlorotoluene ug/L 20 113 60-140106 6 3020ND22.5 21.2
Benzene ug/L 20 116 60-140111 4 3020ND23.2 22.2
Bromobenzene ug/L 20 113 60-140106 7 3020ND22.6 21.2
Bromochloromethane ug/L 20 113 60-140108 4 3020ND22.6 21.6
Bromodichloromethane ug/L 20 105 60-140101 4 3020ND20.9 20.1
Bromoform ug/L 20 86 60-14084 2 3020ND17.1 16.9
Bromomethane ug/L 20 89 60-14097 9 3020ND17.7 19.5
Carbon tetrachloride ug/L 20 123 60-140122 1 3020ND24.6 24.4
Chlorobenzene ug/L 20 113 60-140107 5 3020ND22.7 21.5
Chloroethane ug/L 20 111 60-140107 4 3020ND22.3 21.4
Chloroform ug/L 20 104 60-140102 2 3020ND20.7 20.3
Chloromethane ug/L 20 86 60-14085 1 3020ND17.2 17.0
cis-1,2-Dichloroethene ug/L 20 119 60-140113 5 3020ND23.8 22.5
cis-1,3-Dichloropropene ug/L 20 113 60-140109 4 3020ND22.7 21.7
Dibromochloromethane ug/L 20 90 60-14087 4 3020ND18.1 17.4
Dibromomethane ug/L 20 114 60-140109 5 3020ND22.8 21.7
Dichlorodifluoromethane ug/L 20 86 60-14081 7 3020ND17.3 16.1
Diisopropyl ether ug/L 20 108 60-140102 5 3020ND21.5 20.4
Ethylbenzene ug/L 20 116 60-140110 5 3020ND23.2 22.0
Hexachloro-1,3-butadiene ug/L 20 108 60-140105 3 3020ND21.6 21.0
Isopropylbenzene (Cumene)ug/L 20 116 60-140111 5 3020ND23.3 22.2
m&p-Xylene ug/L 40 117 60-140112 5 3040ND46.8 44.6
Methyl-tert-butyl ether ug/L 20 105 60-14098 6 3020ND20.9 19.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/31/2014 11:48 AM
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Page 10 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1317806MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92221975005
1317807
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 112 60-140104 8 3020ND22.4 20.8
n-Butylbenzene ug/L 20 112 60-140108 4 3020ND22.4 21.6
n-Propylbenzene ug/L 20 117 60-140110 6 3020ND23.3 21.9
Naphthalene ug/L 20 101 60-140100 1 3020ND20.3 20.1
o-Xylene ug/L 20 111 60-140107 4 3020ND22.3 21.4
sec-Butylbenzene ug/L 20 115 60-140109 5 3020ND23.0 21.9
Styrene ug/L 20 118 60-140113 5 3020ND23.6 22.5
tert-Butylbenzene ug/L 20 98 60-14092 7 3020ND19.7 18.3
Tetrachloroethene ug/L 20 115 60-140111 4 3020ND23.1 22.1
Toluene ug/L 20 113 60-140107 5 3020ND22.5 21.5
trans-1,2-Dichloroethene ug/L 20 121 60-140114 6 3020ND24.2 22.8
trans-1,3-Dichloropropene ug/L 20 101 60-14099 2 3020ND20.2 19.9
Trichloroethene ug/L 20 111 60-140106 5 3020ND22.3 21.3
Trichlorofluoromethane ug/L 20 111 60-140106 5 3020ND22.3 21.2
Vinyl chloride ug/L 20 93 60-14089 5 3020ND18.6 17.7
1,2-Dichloroethane-d4 (S)%102 70-13099
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/31/2014 11:48 AM
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Page 11 of 15
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92222333
NODA Site - 71147763
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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Page 12 of 15
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92222333
NODA Site - 71147763
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92222333001 MSV/28972TMW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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Page 13 of 15
Page 14 of 15
Page 15 of 15
#=CL#
November 14, 2014
LIMS USE: FR - CHRIS CORBITT
LIMS OBJECT ID: 92225255
92225255
Project:
Pace Project No.:
RE:
Mr. Chris Corbitt
Terracon
2020 E-Starita Road
Charlotte, NC 28206
Noda Site 71147763
Dear Mr. Corbitt:
Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92225255
Noda Site 71147763
Lab ID Sample ID Matrix Date Collected Date Received
92225255001 GP-1 (0-5)Solid 11/12/14 10:58 11/12/14 13:55
92225255002 GP-1 (10-15)Solid 11/12/14 11:06 11/12/14 13:55
92225255003 GP-2 (10-15)Solid 11/12/14 11:42 11/12/14 13:55
92225255004 GP-3 (15-20)Solid 11/12/14 12:08 11/12/14 13:55
92225255005 GP-4 (5-10)Solid 11/12/14 12:39 11/12/14 13:55
92225255006 GP-4 (15-20)Solid 11/12/14 12:49 11/12/14 13:55
REPORT OF LABORATORY ANALYSIS
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Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92225255
Noda Site 71147763
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92225255001 GP-1 (0-5)EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CACS
92225255002 GP-1 (10-15)EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CACS
92225255003 GP-2 (10-15)EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CACS
92225255004 GP-3 (15-20)EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CACS
92225255005 GP-4 (5-10)EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CACS
92225255006 GP-4 (15-20)EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CACS
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-1 (0-5)Lab ID:92225255001 Collected:11/12/14 10:58 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/13/14 23:31 67-64-110710.7 1
Benzene ND ug/kg 11/13/14 23:31 71-43-25.3 1.7 1
Bromobenzene ND ug/kg 11/13/14 23:31 108-86-1 L35.3 2.1 1
Bromochloromethane ND ug/kg 11/13/14 23:31 74-97-55.3 1.8 1
Bromodichloromethane ND ug/kg 11/13/14 23:31 75-27-45.3 2.0 1
Bromoform ND ug/kg 11/13/14 23:31 75-25-25.3 2.5 1
Bromomethane ND ug/kg 11/13/14 23:31 74-83-910.7 2.7 1
2-Butanone (MEK)ND ug/kg 11/13/14 23:31 78-93-31073.1 1
n-Butylbenzene ND ug/kg 11/13/14 23:31 104-51-85.3 1.9 1
sec-Butylbenzene ND ug/kg 11/13/14 23:31 135-98-85.3 1.7 1
tert-Butylbenzene ND ug/kg 11/13/14 23:31 98-06-65.3 2.1 1
Carbon tetrachloride ND ug/kg 11/13/14 23:31 56-23-55.3 2.8 1
Chlorobenzene ND ug/kg 11/13/14 23:31 108-90-75.3 2.0 1
Chloroethane ND ug/kg 11/13/14 23:31 75-00-310.7 2.6 1
Chloroform ND ug/kg 11/13/14 23:31 67-66-35.3 1.7 1
Chloromethane ND ug/kg 11/13/14 23:31 74-87-310.7 2.6 1
2-Chlorotoluene ND ug/kg 11/13/14 23:31 95-49-85.3 1.8 1
4-Chlorotoluene ND ug/kg 11/13/14 23:31 106-43-45.3 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/13/14 23:31 96-12-85.3 3.8 1
Dibromochloromethane ND ug/kg 11/13/14 23:31 124-48-15.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 11/13/14 23:31 106-93-45.3 1.9 1
Dibromomethane ND ug/kg 11/13/14 23:31 74-95-35.3 2.7 1
1,2-Dichlorobenzene ND ug/kg 11/13/14 23:31 95-50-15.3 2.0 1
1,3-Dichlorobenzene ND ug/kg 11/13/14 23:31 541-73-15.3 2.1 1
1,4-Dichlorobenzene ND ug/kg 11/13/14 23:31 106-46-75.3 1.8 1
Dichlorodifluoromethane ND ug/kg 11/13/14 23:31 75-71-810.7 3.8 1
1,1-Dichloroethane ND ug/kg 11/13/14 23:31 75-34-35.3 1.6 1
1,2-Dichloroethane ND ug/kg 11/13/14 23:31 107-06-25.3 2.3 1
1,1-Dichloroethene ND ug/kg 11/13/14 23:31 75-35-45.3 1.9 1
cis-1,2-Dichloroethene ND ug/kg 11/13/14 23:31 156-59-25.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 11/13/14 23:31 156-60-55.3 2.0 1
1,2-Dichloropropane ND ug/kg 11/13/14 23:31 78-87-55.3 1.8 1
1,3-Dichloropropane ND ug/kg 11/13/14 23:31 142-28-95.3 2.0 1
2,2-Dichloropropane ND ug/kg 11/13/14 23:31 594-20-75.3 1.8 1
1,1-Dichloropropene ND ug/kg 11/13/14 23:31 563-58-65.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 11/13/14 23:31 10061-01-55.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 11/13/14 23:31 10061-02-65.3 1.6 1
Diisopropyl ether ND ug/kg 11/13/14 23:31 108-20-35.3 1.8 1
Ethylbenzene ND ug/kg 11/13/14 23:31 100-41-45.3 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 11/13/14 23:31 87-68-35.3 2.1 1
2-Hexanone ND ug/kg 11/13/14 23:31 591-78-653.4 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 11/13/14 23:31 98-82-85.3 2.0 1
p-Isopropyltoluene ND ug/kg 11/13/14 23:31 99-87-65.3 1.8 1
Methylene Chloride 6.8J ug/kg 11/13/14 23:31 75-09-221.4 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/13/14 23:31 108-10-153.4 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-1 (0-5)Lab ID:92225255001 Collected:11/12/14 10:58 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/13/14 23:31 1634-04-45.3 1.6 1
Naphthalene ND ug/kg 11/13/14 23:31 91-20-35.3 1.3 1
n-Propylbenzene ND ug/kg 11/13/14 23:31 103-65-15.3 1.8 1
Styrene ND ug/kg 11/13/14 23:31 100-42-55.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/13/14 23:31 630-20-65.3 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/13/14 23:31 79-34-55.3 2.0 1
Tetrachloroethene ND ug/kg 11/13/14 23:31 127-18-45.3 1.8 1
Toluene ND ug/kg 11/13/14 23:31 108-88-35.3 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 11/13/14 23:31 87-61-65.3 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 11/13/14 23:31 120-82-15.3 1.7 1
1,1,1-Trichloroethane ND ug/kg 11/13/14 23:31 71-55-65.3 1.9 1
1,1,2-Trichloroethane ND ug/kg 11/13/14 23:31 79-00-55.3 2.2 1
Trichloroethene ND ug/kg 11/13/14 23:31 79-01-65.3 2.2 1
Trichlorofluoromethane ND ug/kg 11/13/14 23:31 75-69-45.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 11/13/14 23:31 96-18-45.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 11/13/14 23:31 95-63-65.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 11/13/14 23:31 108-67-85.3 1.9 1
Vinyl acetate ND ug/kg 11/13/14 23:31 108-05-453.4 9.4 1
Vinyl chloride ND ug/kg 11/13/14 23:31 75-01-410.7 1.9 1
Xylene (Total)ND ug/kg 11/13/14 23:31 1330-20-710.7 3.8 1
m&p-Xylene ND ug/kg 11/13/14 23:31 179601-23-110.7 3.8 1
o-Xylene ND ug/kg 11/13/14 23:31 95-47-65.3 2.0 1
Surrogates
Toluene-d8 (S)101 %11/13/14 23:31 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %11/13/14 23:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)117 %11/13/14 23:31 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.3 %11/14/14 13:300.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-1 (10-15)Lab ID:92225255002 Collected:11/12/14 11:06 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/13/14 23:51 67-64-110610.6 1
Benzene ND ug/kg 11/13/14 23:51 71-43-25.3 1.7 1
Bromobenzene ND ug/kg 11/13/14 23:51 108-86-1 L35.3 2.1 1
Bromochloromethane ND ug/kg 11/13/14 23:51 74-97-55.3 1.8 1
Bromodichloromethane ND ug/kg 11/13/14 23:51 75-27-45.3 2.0 1
Bromoform ND ug/kg 11/13/14 23:51 75-25-25.3 2.4 1
Bromomethane ND ug/kg 11/13/14 23:51 74-83-910.6 2.6 1
2-Butanone (MEK)ND ug/kg 11/13/14 23:51 78-93-31063.1 1
n-Butylbenzene ND ug/kg 11/13/14 23:51 104-51-85.3 1.9 1
sec-Butylbenzene ND ug/kg 11/13/14 23:51 135-98-85.3 1.7 1
tert-Butylbenzene ND ug/kg 11/13/14 23:51 98-06-65.3 2.1 1
Carbon tetrachloride ND ug/kg 11/13/14 23:51 56-23-55.3 2.8 1
Chlorobenzene ND ug/kg 11/13/14 23:51 108-90-75.3 2.0 1
Chloroethane ND ug/kg 11/13/14 23:51 75-00-310.6 2.5 1
Chloroform ND ug/kg 11/13/14 23:51 67-66-35.3 1.7 1
Chloromethane ND ug/kg 11/13/14 23:51 74-87-310.6 2.5 1
2-Chlorotoluene ND ug/kg 11/13/14 23:51 95-49-85.3 1.8 1
4-Chlorotoluene ND ug/kg 11/13/14 23:51 106-43-45.3 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/13/14 23:51 96-12-85.3 3.8 1
Dibromochloromethane ND ug/kg 11/13/14 23:51 124-48-15.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 11/13/14 23:51 106-93-45.3 1.9 1
Dibromomethane ND ug/kg 11/13/14 23:51 74-95-35.3 2.6 1
1,2-Dichlorobenzene ND ug/kg 11/13/14 23:51 95-50-15.3 2.0 1
1,3-Dichlorobenzene ND ug/kg 11/13/14 23:51 541-73-15.3 2.1 1
1,4-Dichlorobenzene ND ug/kg 11/13/14 23:51 106-46-75.3 1.8 1
Dichlorodifluoromethane ND ug/kg 11/13/14 23:51 75-71-810.6 3.8 1
1,1-Dichloroethane ND ug/kg 11/13/14 23:51 75-34-35.3 1.6 1
1,2-Dichloroethane ND ug/kg 11/13/14 23:51 107-06-25.3 2.3 1
1,1-Dichloroethene ND ug/kg 11/13/14 23:51 75-35-45.3 1.9 1
cis-1,2-Dichloroethene ND ug/kg 11/13/14 23:51 156-59-25.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 11/13/14 23:51 156-60-55.3 2.0 1
1,2-Dichloropropane ND ug/kg 11/13/14 23:51 78-87-55.3 1.8 1
1,3-Dichloropropane ND ug/kg 11/13/14 23:51 142-28-95.3 2.0 1
2,2-Dichloropropane ND ug/kg 11/13/14 23:51 594-20-75.3 1.8 1
1,1-Dichloropropene ND ug/kg 11/13/14 23:51 563-58-65.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 11/13/14 23:51 10061-01-55.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 11/13/14 23:51 10061-02-65.3 1.6 1
Diisopropyl ether ND ug/kg 11/13/14 23:51 108-20-35.3 1.8 1
Ethylbenzene ND ug/kg 11/13/14 23:51 100-41-45.3 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 11/13/14 23:51 87-68-35.3 2.1 1
2-Hexanone ND ug/kg 11/13/14 23:51 591-78-652.9 4.1 1
Isopropylbenzene (Cumene)ND ug/kg 11/13/14 23:51 98-82-85.3 2.0 1
p-Isopropyltoluene ND ug/kg 11/13/14 23:51 99-87-65.3 1.8 1
Methylene Chloride 6.3J ug/kg 11/13/14 23:51 75-09-221.2 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/13/14 23:51 108-10-152.9 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-1 (10-15)Lab ID:92225255002 Collected:11/12/14 11:06 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/13/14 23:51 1634-04-45.3 1.6 1
Naphthalene ND ug/kg 11/13/14 23:51 91-20-35.3 1.3 1
n-Propylbenzene ND ug/kg 11/13/14 23:51 103-65-15.3 1.8 1
Styrene ND ug/kg 11/13/14 23:51 100-42-55.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/13/14 23:51 630-20-65.3 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/13/14 23:51 79-34-55.3 2.0 1
Tetrachloroethene ND ug/kg 11/13/14 23:51 127-18-45.3 1.8 1
Toluene ND ug/kg 11/13/14 23:51 108-88-35.3 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 11/13/14 23:51 87-61-65.3 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 11/13/14 23:51 120-82-15.3 1.7 1
1,1,1-Trichloroethane ND ug/kg 11/13/14 23:51 71-55-65.3 1.9 1
1,1,2-Trichloroethane ND ug/kg 11/13/14 23:51 79-00-55.3 2.2 1
Trichloroethene ND ug/kg 11/13/14 23:51 79-01-65.3 2.2 1
Trichlorofluoromethane ND ug/kg 11/13/14 23:51 75-69-45.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 11/13/14 23:51 96-18-45.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 11/13/14 23:51 95-63-65.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 11/13/14 23:51 108-67-85.3 1.9 1
Vinyl acetate ND ug/kg 11/13/14 23:51 108-05-452.9 9.3 1
Vinyl chloride ND ug/kg 11/13/14 23:51 75-01-410.6 1.9 1
Xylene (Total)ND ug/kg 11/13/14 23:51 1330-20-710.6 3.8 1
m&p-Xylene ND ug/kg 11/13/14 23:51 179601-23-110.6 3.8 1
o-Xylene ND ug/kg 11/13/14 23:51 95-47-65.3 2.0 1
Surrogates
Toluene-d8 (S)101 %11/13/14 23:51 2037-26-570-130 1
4-Bromofluorobenzene (S)92 %11/13/14 23:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)117 %11/13/14 23:51 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.3 %11/14/14 13:300.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-2 (10-15)Lab ID:92225255003 Collected:11/12/14 11:42 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/14/14 00:10 67-64-198.4 9.8 1
Benzene ND ug/kg 11/14/14 00:10 71-43-24.9 1.6 1
Bromobenzene ND ug/kg 11/14/14 00:10 108-86-1 L34.9 2.0 1
Bromochloromethane ND ug/kg 11/14/14 00:10 74-97-54.9 1.7 1
Bromodichloromethane ND ug/kg 11/14/14 00:10 75-27-44.9 1.9 1
Bromoform ND ug/kg 11/14/14 00:10 75-25-24.9 2.3 1
Bromomethane ND ug/kg 11/14/14 00:10 74-83-99.8 2.5 1
2-Butanone (MEK)ND ug/kg 11/14/14 00:10 78-93-398.4 2.9 1
n-Butylbenzene ND ug/kg 11/14/14 00:10 104-51-84.9 1.8 1
sec-Butylbenzene ND ug/kg 11/14/14 00:10 135-98-84.9 1.6 1
tert-Butylbenzene ND ug/kg 11/14/14 00:10 98-06-64.9 2.0 1
Carbon tetrachloride ND ug/kg 11/14/14 00:10 56-23-54.9 2.6 1
Chlorobenzene ND ug/kg 11/14/14 00:10 108-90-74.9 1.9 1
Chloroethane ND ug/kg 11/14/14 00:10 75-00-39.8 2.4 1
Chloroform ND ug/kg 11/14/14 00:10 67-66-34.9 1.6 1
Chloromethane ND ug/kg 11/14/14 00:10 74-87-39.8 2.4 1
2-Chlorotoluene ND ug/kg 11/14/14 00:10 95-49-84.9 1.7 1
4-Chlorotoluene ND ug/kg 11/14/14 00:10 106-43-44.9 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/14/14 00:10 96-12-84.9 3.5 1
Dibromochloromethane ND ug/kg 11/14/14 00:10 124-48-14.9 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 11/14/14 00:10 106-93-44.9 1.8 1
Dibromomethane ND ug/kg 11/14/14 00:10 74-95-34.9 2.5 1
1,2-Dichlorobenzene ND ug/kg 11/14/14 00:10 95-50-14.9 1.9 1
1,3-Dichlorobenzene ND ug/kg 11/14/14 00:10 541-73-14.9 2.0 1
1,4-Dichlorobenzene ND ug/kg 11/14/14 00:10 106-46-74.9 1.7 1
Dichlorodifluoromethane ND ug/kg 11/14/14 00:10 75-71-89.8 3.5 1
1,1-Dichloroethane ND ug/kg 11/14/14 00:10 75-34-34.9 1.5 1
1,2-Dichloroethane ND ug/kg 11/14/14 00:10 107-06-24.9 2.2 1
1,1-Dichloroethene ND ug/kg 11/14/14 00:10 75-35-44.9 1.8 1
cis-1,2-Dichloroethene ND ug/kg 11/14/14 00:10 156-59-24.9 1.4 1
trans-1,2-Dichloroethene ND ug/kg 11/14/14 00:10 156-60-54.9 1.9 1
1,2-Dichloropropane ND ug/kg 11/14/14 00:10 78-87-54.9 1.7 1
1,3-Dichloropropane ND ug/kg 11/14/14 00:10 142-28-94.9 1.9 1
2,2-Dichloropropane ND ug/kg 11/14/14 00:10 594-20-74.9 1.7 1
1,1-Dichloropropene ND ug/kg 11/14/14 00:10 563-58-64.9 1.5 1
cis-1,3-Dichloropropene ND ug/kg 11/14/14 00:10 10061-01-54.9 1.8 1
trans-1,3-Dichloropropene ND ug/kg 11/14/14 00:10 10061-02-64.9 1.5 1
Diisopropyl ether ND ug/kg 11/14/14 00:10 108-20-34.9 1.7 1
Ethylbenzene ND ug/kg 11/14/14 00:10 100-41-44.9 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 11/14/14 00:10 87-68-34.9 2.0 1
2-Hexanone ND ug/kg 11/14/14 00:10 591-78-649.2 3.8 1
Isopropylbenzene (Cumene)ND ug/kg 11/14/14 00:10 98-82-84.9 1.9 1
p-Isopropyltoluene ND ug/kg 11/14/14 00:10 99-87-64.9 1.7 1
Methylene Chloride 5.9J ug/kg 11/14/14 00:10 75-09-219.7 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/14/14 00:10 108-10-149.2 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-2 (10-15)Lab ID:92225255003 Collected:11/12/14 11:42 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/14/14 00:10 1634-04-44.9 1.5 1
Naphthalene ND ug/kg 11/14/14 00:10 91-20-34.9 1.2 1
n-Propylbenzene ND ug/kg 11/14/14 00:10 103-65-14.9 1.7 1
Styrene ND ug/kg 11/14/14 00:10 100-42-54.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/14/14 00:10 630-20-64.9 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/14/14 00:10 79-34-54.9 1.9 1
Tetrachloroethene ND ug/kg 11/14/14 00:10 127-18-44.9 1.7 1
Toluene ND ug/kg 11/14/14 00:10 108-88-34.9 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 11/14/14 00:10 87-61-64.9 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 11/14/14 00:10 120-82-14.9 1.6 1
1,1,1-Trichloroethane ND ug/kg 11/14/14 00:10 71-55-64.9 1.8 1
1,1,2-Trichloroethane ND ug/kg 11/14/14 00:10 79-00-54.9 2.1 1
Trichloroethene 5.7 ug/kg 11/14/14 00:10 79-01-64.9 2.1 1
Trichlorofluoromethane ND ug/kg 11/14/14 00:10 75-69-44.9 2.2 1
1,2,3-Trichloropropane ND ug/kg 11/14/14 00:10 96-18-44.9 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 11/14/14 00:10 95-63-64.9 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 11/14/14 00:10 108-67-84.9 1.8 1
Vinyl acetate ND ug/kg 11/14/14 00:10 108-05-449.2 8.7 1
Vinyl chloride ND ug/kg 11/14/14 00:10 75-01-49.8 1.8 1
Xylene (Total)ND ug/kg 11/14/14 00:10 1330-20-79.8 3.5 1
m&p-Xylene ND ug/kg 11/14/14 00:10 179601-23-19.8 3.5 1
o-Xylene ND ug/kg 11/14/14 00:10 95-47-64.9 1.9 1
Surrogates
Toluene-d8 (S)101 %11/14/14 00:10 2037-26-570-130 1
4-Bromofluorobenzene (S)91 %11/14/14 00:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %11/14/14 00:10 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %11/14/14 13:300.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-3 (15-20)Lab ID:92225255004 Collected:11/12/14 12:08 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/14/14 00:30 67-64-192.1 9.2 1
Benzene ND ug/kg 11/14/14 00:30 71-43-24.6 1.5 1
Bromobenzene ND ug/kg 11/14/14 00:30 108-86-1 L34.6 1.8 1
Bromochloromethane ND ug/kg 11/14/14 00:30 74-97-54.6 1.6 1
Bromodichloromethane ND ug/kg 11/14/14 00:30 75-27-44.6 1.8 1
Bromoform ND ug/kg 11/14/14 00:30 75-25-24.6 2.1 1
Bromomethane ND ug/kg 11/14/14 00:30 74-83-99.2 2.3 1
2-Butanone (MEK)ND ug/kg 11/14/14 00:30 78-93-392.1 2.7 1
n-Butylbenzene ND ug/kg 11/14/14 00:30 104-51-84.6 1.7 1
sec-Butylbenzene ND ug/kg 11/14/14 00:30 135-98-84.6 1.5 1
tert-Butylbenzene ND ug/kg 11/14/14 00:30 98-06-64.6 1.8 1
Carbon tetrachloride ND ug/kg 11/14/14 00:30 56-23-54.6 2.4 1
Chlorobenzene ND ug/kg 11/14/14 00:30 108-90-74.6 1.8 1
Chloroethane ND ug/kg 11/14/14 00:30 75-00-39.2 2.2 1
Chloroform ND ug/kg 11/14/14 00:30 67-66-34.6 1.5 1
Chloromethane ND ug/kg 11/14/14 00:30 74-87-39.2 2.2 1
2-Chlorotoluene ND ug/kg 11/14/14 00:30 95-49-84.6 1.6 1
4-Chlorotoluene ND ug/kg 11/14/14 00:30 106-43-44.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/14/14 00:30 96-12-84.6 3.3 1
Dibromochloromethane ND ug/kg 11/14/14 00:30 124-48-14.6 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 11/14/14 00:30 106-93-44.6 1.7 1
Dibromomethane ND ug/kg 11/14/14 00:30 74-95-34.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 11/14/14 00:30 95-50-14.6 1.8 1
1,3-Dichlorobenzene ND ug/kg 11/14/14 00:30 541-73-14.6 1.8 1
1,4-Dichlorobenzene ND ug/kg 11/14/14 00:30 106-46-74.6 1.6 1
Dichlorodifluoromethane ND ug/kg 11/14/14 00:30 75-71-89.2 3.3 1
1,1-Dichloroethane ND ug/kg 11/14/14 00:30 75-34-34.6 1.4 1
1,2-Dichloroethane ND ug/kg 11/14/14 00:30 107-06-24.6 2.0 1
1,1-Dichloroethene ND ug/kg 11/14/14 00:30 75-35-44.6 1.7 1
cis-1,2-Dichloroethene ND ug/kg 11/14/14 00:30 156-59-24.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 11/14/14 00:30 156-60-54.6 1.8 1
1,2-Dichloropropane ND ug/kg 11/14/14 00:30 78-87-54.6 1.6 1
1,3-Dichloropropane ND ug/kg 11/14/14 00:30 142-28-94.6 1.8 1
2,2-Dichloropropane ND ug/kg 11/14/14 00:30 594-20-74.6 1.6 1
1,1-Dichloropropene ND ug/kg 11/14/14 00:30 563-58-64.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 11/14/14 00:30 10061-01-54.6 1.7 1
trans-1,3-Dichloropropene ND ug/kg 11/14/14 00:30 10061-02-64.6 1.4 1
Diisopropyl ether ND ug/kg 11/14/14 00:30 108-20-34.6 1.6 1
Ethylbenzene ND ug/kg 11/14/14 00:30 100-41-44.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 11/14/14 00:30 87-68-34.6 1.8 1
2-Hexanone ND ug/kg 11/14/14 00:30 591-78-646.1 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 11/14/14 00:30 98-82-84.6 1.8 1
p-Isopropyltoluene ND ug/kg 11/14/14 00:30 99-87-64.6 1.6 1
Methylene Chloride 4.5J ug/kg 11/14/14 00:30 75-09-218.4 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/14/14 00:30 108-10-146.1 3.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-3 (15-20)Lab ID:92225255004 Collected:11/12/14 12:08 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/14/14 00:30 1634-04-44.6 1.4 1
Naphthalene ND ug/kg 11/14/14 00:30 91-20-34.6 1.1 1
n-Propylbenzene ND ug/kg 11/14/14 00:30 103-65-14.6 1.6 1
Styrene ND ug/kg 11/14/14 00:30 100-42-54.6 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/14/14 00:30 630-20-64.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/14/14 00:30 79-34-54.6 1.8 1
Tetrachloroethene ND ug/kg 11/14/14 00:30 127-18-44.6 1.6 1
Toluene ND ug/kg 11/14/14 00:30 108-88-34.6 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 11/14/14 00:30 87-61-64.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 11/14/14 00:30 120-82-14.6 1.5 1
1,1,1-Trichloroethane ND ug/kg 11/14/14 00:30 71-55-64.6 1.7 1
1,1,2-Trichloroethane ND ug/kg 11/14/14 00:30 79-00-54.6 1.9 1
Trichloroethene ND ug/kg 11/14/14 00:30 79-01-64.6 1.9 1
Trichlorofluoromethane ND ug/kg 11/14/14 00:30 75-69-44.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 11/14/14 00:30 96-18-44.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 11/14/14 00:30 95-63-64.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 11/14/14 00:30 108-67-84.6 1.7 1
Vinyl acetate ND ug/kg 11/14/14 00:30 108-05-446.1 8.1 1
Vinyl chloride ND ug/kg 11/14/14 00:30 75-01-49.2 1.7 1
Xylene (Total)ND ug/kg 11/14/14 00:30 1330-20-79.2 3.3 1
m&p-Xylene ND ug/kg 11/14/14 00:30 179601-23-19.2 3.3 1
o-Xylene ND ug/kg 11/14/14 00:30 95-47-64.6 1.8 1
Surrogates
Toluene-d8 (S)102 %11/14/14 00:30 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %11/14/14 00:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %11/14/14 00:30 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.7 %11/14/14 13:310.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-4 (5-10)Lab ID:92225255005 Collected:11/12/14 12:39 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/14/14 00:50 67-64-1119001190100
Benzene ND ug/kg 11/14/14 00:50 71-43-2594190100
Bromobenzene ND ug/kg 11/14/14 00:50 108-86-1 L3594238100
Bromochloromethane ND ug/kg 11/14/14 00:50 74-97-5594202100
Bromodichloromethane ND ug/kg 11/14/14 00:50 75-27-4594226100
Bromoform ND ug/kg 11/14/14 00:50 75-25-2594273100
Bromomethane ND ug/kg 11/14/14 00:50 74-83-91190297100
2-Butanone (MEK)ND ug/kg 11/14/14 00:50 78-93-311900345100
n-Butylbenzene 1750 ug/kg 11/14/14 00:50 104-51-8594214100
sec-Butylbenzene 1970 ug/kg 11/14/14 00:50 135-98-8594190100
tert-Butylbenzene ND ug/kg 11/14/14 00:50 98-06-6594238100
Carbon tetrachloride ND ug/kg 11/14/14 00:50 56-23-5594309100
Chlorobenzene ND ug/kg 11/14/14 00:50 108-90-7594226100
Chloroethane ND ug/kg 11/14/14 00:50 75-00-31190285100
Chloroform ND ug/kg 11/14/14 00:50 67-66-3594190100
Chloromethane ND ug/kg 11/14/14 00:50 74-87-31190285100
2-Chlorotoluene ND ug/kg 11/14/14 00:50 95-49-8594202100
4-Chlorotoluene ND ug/kg 11/14/14 00:50 106-43-4594214100
1,2-Dibromo-3-chloropropane ND ug/kg 11/14/14 00:50 96-12-8594428100
Dibromochloromethane ND ug/kg 11/14/14 00:50 124-48-1594214100
1,2-Dibromoethane (EDB)ND ug/kg 11/14/14 00:50 106-93-4594214100
Dibromomethane ND ug/kg 11/14/14 00:50 74-95-3594297100
1,2-Dichlorobenzene ND ug/kg 11/14/14 00:50 95-50-1594226100
1,3-Dichlorobenzene ND ug/kg 11/14/14 00:50 541-73-1594238100
1,4-Dichlorobenzene ND ug/kg 11/14/14 00:50 106-46-7594202100
Dichlorodifluoromethane ND ug/kg 11/14/14 00:50 75-71-81190428100
1,1-Dichloroethane ND ug/kg 11/14/14 00:50 75-34-3594178100
1,2-Dichloroethane ND ug/kg 11/14/14 00:50 107-06-2594262100
1,1-Dichloroethene ND ug/kg 11/14/14 00:50 75-35-4594214100
cis-1,2-Dichloroethene ND ug/kg 11/14/14 00:50 156-59-2594166100
trans-1,2-Dichloroethene ND ug/kg 11/14/14 00:50 156-60-5594226100
1,2-Dichloropropane ND ug/kg 11/14/14 00:50 78-87-5594202100
1,3-Dichloropropane ND ug/kg 11/14/14 00:50 142-28-9594226100
2,2-Dichloropropane ND ug/kg 11/14/14 00:50 594-20-7594202100
1,1-Dichloropropene ND ug/kg 11/14/14 00:50 563-58-6594178100
cis-1,3-Dichloropropene ND ug/kg 11/14/14 00:50 10061-01-5594214100
trans-1,3-Dichloropropene ND ug/kg 11/14/14 00:50 10061-02-6594178100
Diisopropyl ether ND ug/kg 11/14/14 00:50 108-20-3594202100
Ethylbenzene ND ug/kg 11/14/14 00:50 100-41-4594214100
Hexachloro-1,3-butadiene ND ug/kg 11/14/14 00:50 87-68-3594238100
2-Hexanone ND ug/kg 11/14/14 00:50 591-78-65940464100
Isopropylbenzene (Cumene)424J ug/kg 11/14/14 00:50 98-82-8594226100
p-Isopropyltoluene ND ug/kg 11/14/14 00:50 99-87-6594202100
Methylene Chloride ND ug/kg 11/14/14 00:50 75-09-22380357100
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/14/14 00:50 108-10-15940440100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-4 (5-10)Lab ID:92225255005 Collected:11/12/14 12:39 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/14/14 00:50 1634-04-4594178100
Naphthalene 467J ug/kg 11/14/14 00:50 91-20-3594143100
n-Propylbenzene 1050 ug/kg 11/14/14 00:50 103-65-1594202100
Styrene ND ug/kg 11/14/14 00:50 100-42-5594214100
1,1,1,2-Tetrachloroethane ND ug/kg 11/14/14 00:50 630-20-6594250100
1,1,2,2-Tetrachloroethane ND ug/kg 11/14/14 00:50 79-34-5594226100
Tetrachloroethene ND ug/kg 11/14/14 00:50 127-18-4594202100
Toluene ND ug/kg 11/14/14 00:50 108-88-3594214100
1,2,3-Trichlorobenzene ND ug/kg 11/14/14 00:50 87-61-6594262100
1,2,4-Trichlorobenzene ND ug/kg 11/14/14 00:50 120-82-1594190100
1,1,1-Trichloroethane ND ug/kg 11/14/14 00:50 71-55-6594214100
1,1,2-Trichloroethane ND ug/kg 11/14/14 00:50 79-00-5594250100
Trichloroethene ND ug/kg 11/14/14 00:50 79-01-6594250100
Trichlorofluoromethane ND ug/kg 11/14/14 00:50 75-69-4594262100
1,2,3-Trichloropropane ND ug/kg 11/14/14 00:50 96-18-4594190100
1,2,4-Trimethylbenzene ND ug/kg 11/14/14 00:50 95-63-6594238100
1,3,5-Trimethylbenzene ND ug/kg 11/14/14 00:50 108-67-8594214100
Vinyl acetate ND ug/kg 11/14/14 00:50 108-05-459401050100
Vinyl chloride ND ug/kg 11/14/14 00:50 75-01-41190214100
Xylene (Total)ND ug/kg 11/14/14 00:50 1330-20-71190428100
m&p-Xylene ND ug/kg 11/14/14 00:50 179601-23-11190428100
o-Xylene ND ug/kg 11/14/14 00:50 95-47-6594226100
Surrogates
Toluene-d8 (S)105 %11/14/14 00:50 2037-26-5 D370-130 100
4-Bromofluorobenzene (S)102 %11/14/14 00:50 460-00-470-130 100
1,2-Dichloroethane-d4 (S)104 %11/14/14 00:50 17060-07-070-132 100
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.0 %11/14/14 13:310.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-4 (15-20)Lab ID:92225255006 Collected:11/12/14 12:49 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/14/14 01:10 67-64-110910.9 1
Benzene ND ug/kg 11/14/14 01:10 71-43-25.4 1.7 1
Bromobenzene ND ug/kg 11/14/14 01:10 108-86-1 L35.4 2.2 1
Bromochloromethane ND ug/kg 11/14/14 01:10 74-97-55.4 1.9 1
Bromodichloromethane ND ug/kg 11/14/14 01:10 75-27-45.4 2.1 1
Bromoform ND ug/kg 11/14/14 01:10 75-25-25.4 2.5 1
Bromomethane ND ug/kg 11/14/14 01:10 74-83-910.9 2.7 1
2-Butanone (MEK)ND ug/kg 11/14/14 01:10 78-93-31093.2 1
n-Butylbenzene ND ug/kg 11/14/14 01:10 104-51-85.4 2.0 1
sec-Butylbenzene ND ug/kg 11/14/14 01:10 135-98-85.4 1.7 1
tert-Butylbenzene ND ug/kg 11/14/14 01:10 98-06-65.4 2.2 1
Carbon tetrachloride ND ug/kg 11/14/14 01:10 56-23-55.4 2.8 1
Chlorobenzene ND ug/kg 11/14/14 01:10 108-90-75.4 2.1 1
Chloroethane ND ug/kg 11/14/14 01:10 75-00-310.9 2.6 1
Chloroform ND ug/kg 11/14/14 01:10 67-66-35.4 1.7 1
Chloromethane ND ug/kg 11/14/14 01:10 74-87-310.9 2.6 1
2-Chlorotoluene ND ug/kg 11/14/14 01:10 95-49-85.4 1.9 1
4-Chlorotoluene ND ug/kg 11/14/14 01:10 106-43-45.4 2.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/14/14 01:10 96-12-85.4 3.9 1
Dibromochloromethane ND ug/kg 11/14/14 01:10 124-48-15.4 2.0 1
1,2-Dibromoethane (EDB)ND ug/kg 11/14/14 01:10 106-93-45.4 2.0 1
Dibromomethane ND ug/kg 11/14/14 01:10 74-95-35.4 2.7 1
1,2-Dichlorobenzene ND ug/kg 11/14/14 01:10 95-50-15.4 2.1 1
1,3-Dichlorobenzene ND ug/kg 11/14/14 01:10 541-73-15.4 2.2 1
1,4-Dichlorobenzene ND ug/kg 11/14/14 01:10 106-46-75.4 1.9 1
Dichlorodifluoromethane ND ug/kg 11/14/14 01:10 75-71-810.9 3.9 1
1,1-Dichloroethane ND ug/kg 11/14/14 01:10 75-34-35.4 1.6 1
1,2-Dichloroethane ND ug/kg 11/14/14 01:10 107-06-25.4 2.4 1
1,1-Dichloroethene ND ug/kg 11/14/14 01:10 75-35-45.4 2.0 1
cis-1,2-Dichloroethene ND ug/kg 11/14/14 01:10 156-59-25.4 1.5 1
trans-1,2-Dichloroethene ND ug/kg 11/14/14 01:10 156-60-55.4 2.1 1
1,2-Dichloropropane ND ug/kg 11/14/14 01:10 78-87-55.4 1.9 1
1,3-Dichloropropane ND ug/kg 11/14/14 01:10 142-28-95.4 2.1 1
2,2-Dichloropropane ND ug/kg 11/14/14 01:10 594-20-75.4 1.9 1
1,1-Dichloropropene ND ug/kg 11/14/14 01:10 563-58-65.4 1.6 1
cis-1,3-Dichloropropene ND ug/kg 11/14/14 01:10 10061-01-55.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 11/14/14 01:10 10061-02-65.4 1.6 1
Diisopropyl ether ND ug/kg 11/14/14 01:10 108-20-35.4 1.9 1
Ethylbenzene ND ug/kg 11/14/14 01:10 100-41-45.4 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 11/14/14 01:10 87-68-35.4 2.2 1
2-Hexanone ND ug/kg 11/14/14 01:10 591-78-654.4 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 11/14/14 01:10 98-82-85.4 2.1 1
p-Isopropyltoluene ND ug/kg 11/14/14 01:10 99-87-65.4 1.9 1
Methylene Chloride 10.1J ug/kg 11/14/14 01:10 75-09-221.8 3.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/14/14 01:10 108-10-154.4 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92225255
Noda Site 71147763
Sample:GP-4 (15-20)Lab ID:92225255006 Collected:11/12/14 12:49 Received:11/12/14 13:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/14/14 01:10 1634-04-45.4 1.6 1
Naphthalene ND ug/kg 11/14/14 01:10 91-20-35.4 1.3 1
n-Propylbenzene ND ug/kg 11/14/14 01:10 103-65-15.4 1.9 1
Styrene ND ug/kg 11/14/14 01:10 100-42-55.4 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/14/14 01:10 630-20-65.4 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/14/14 01:10 79-34-55.4 2.1 1
Tetrachloroethene ND ug/kg 11/14/14 01:10 127-18-45.4 1.9 1
Toluene ND ug/kg 11/14/14 01:10 108-88-35.4 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 11/14/14 01:10 87-61-65.4 2.4 1
1,2,4-Trichlorobenzene ND ug/kg 11/14/14 01:10 120-82-15.4 1.7 1
1,1,1-Trichloroethane ND ug/kg 11/14/14 01:10 71-55-65.4 2.0 1
1,1,2-Trichloroethane ND ug/kg 11/14/14 01:10 79-00-55.4 2.3 1
Trichloroethene ND ug/kg 11/14/14 01:10 79-01-65.4 2.3 1
Trichlorofluoromethane ND ug/kg 11/14/14 01:10 75-69-45.4 2.4 1
1,2,3-Trichloropropane ND ug/kg 11/14/14 01:10 96-18-45.4 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 11/14/14 01:10 95-63-65.4 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 11/14/14 01:10 108-67-85.4 2.0 1
Vinyl acetate ND ug/kg 11/14/14 01:10 108-05-454.4 9.6 1
Vinyl chloride ND ug/kg 11/14/14 01:10 75-01-410.9 2.0 1
Xylene (Total)ND ug/kg 11/14/14 01:10 1330-20-710.9 3.9 1
m&p-Xylene ND ug/kg 11/14/14 01:10 179601-23-110.9 3.9 1
o-Xylene ND ug/kg 11/14/14 01:10 95-47-65.4 2.1 1
Surrogates
Toluene-d8 (S)100 %11/14/14 01:10 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %11/14/14 01:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %11/14/14 01:10 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.3 %11/14/14 13:310.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/29238
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92225255001, 92225255002, 92225255003, 92225255004, 92225255005, 92225255006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1329214
Associated Lab Samples:92225255001, 92225255002, 92225255003, 92225255004, 92225255005, 92225255006
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.8 11/13/14 17:54
1,1,1-Trichloroethane ug/kg ND 5.8 11/13/14 17:54
1,1,2,2-Tetrachloroethane ug/kg ND 5.8 11/13/14 17:54
1,1,2-Trichloroethane ug/kg ND 5.8 11/13/14 17:54
1,1-Dichloroethane ug/kg ND 5.8 11/13/14 17:54
1,1-Dichloroethene ug/kg ND 5.8 11/13/14 17:54
1,1-Dichloropropene ug/kg ND 5.8 11/13/14 17:54
1,2,3-Trichlorobenzene ug/kg ND 5.8 11/13/14 17:54
1,2,3-Trichloropropane ug/kg ND 5.8 11/13/14 17:54
1,2,4-Trichlorobenzene ug/kg ND 5.8 11/13/14 17:54
1,2,4-Trimethylbenzene ug/kg ND 5.8 11/13/14 17:54
1,2-Dibromo-3-chloropropane ug/kg ND 5.8 11/13/14 17:54
1,2-Dibromoethane (EDB)ug/kg ND 5.8 11/13/14 17:54
1,2-Dichlorobenzene ug/kg ND 5.8 11/13/14 17:54
1,2-Dichloroethane ug/kg ND 5.8 11/13/14 17:54
1,2-Dichloropropane ug/kg ND 5.8 11/13/14 17:54
1,3,5-Trimethylbenzene ug/kg ND 5.8 11/13/14 17:54
1,3-Dichlorobenzene ug/kg ND 5.8 11/13/14 17:54
1,3-Dichloropropane ug/kg ND 5.8 11/13/14 17:54
1,4-Dichlorobenzene ug/kg ND 5.8 11/13/14 17:54
2,2-Dichloropropane ug/kg ND 5.8 11/13/14 17:54
2-Butanone (MEK)ug/kg ND 116 11/13/14 17:54
2-Chlorotoluene ug/kg ND 5.8 11/13/14 17:54
2-Hexanone ug/kg ND 58.1 11/13/14 17:54
4-Chlorotoluene ug/kg ND 5.8 11/13/14 17:54
4-Methyl-2-pentanone (MIBK)ug/kg ND 58.1 11/13/14 17:54
Acetone ug/kg 11.8J 116 11/13/14 17:54
Benzene ug/kg ND 5.8 11/13/14 17:54
Bromobenzene ug/kg ND 5.8 11/13/14 17:54
Bromochloromethane ug/kg ND 5.8 11/13/14 17:54
Bromodichloromethane ug/kg ND 5.8 11/13/14 17:54
Bromoform ug/kg ND 5.8 11/13/14 17:54
Bromomethane ug/kg ND 11.6 11/13/14 17:54
Carbon tetrachloride ug/kg ND 5.8 11/13/14 17:54
Chlorobenzene ug/kg ND 5.8 11/13/14 17:54
Chloroethane ug/kg ND 11.6 11/13/14 17:54
Chloroform ug/kg ND 5.8 11/13/14 17:54
Chloromethane ug/kg ND 11.6 11/13/14 17:54
cis-1,2-Dichloroethene ug/kg ND 5.8 11/13/14 17:54
cis-1,3-Dichloropropene ug/kg ND 5.8 11/13/14 17:54
Dibromochloromethane ug/kg ND 5.8 11/13/14 17:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1329214
Associated Lab Samples:92225255001, 92225255002, 92225255003, 92225255004, 92225255005, 92225255006
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.8 11/13/14 17:54
Dichlorodifluoromethane ug/kg ND 11.6 11/13/14 17:54
Diisopropyl ether ug/kg ND 5.8 11/13/14 17:54
Ethylbenzene ug/kg ND 5.8 11/13/14 17:54
Hexachloro-1,3-butadiene ug/kg ND 5.8 11/13/14 17:54
Isopropylbenzene (Cumene)ug/kg ND 5.8 11/13/14 17:54
m&p-Xylene ug/kg ND 11.6 11/13/14 17:54
Methyl-tert-butyl ether ug/kg ND 5.8 11/13/14 17:54
Methylene Chloride ug/kg ND 23.3 11/13/14 17:54
n-Butylbenzene ug/kg ND 5.8 11/13/14 17:54
n-Propylbenzene ug/kg ND 5.8 11/13/14 17:54
Naphthalene ug/kg ND 5.8 11/13/14 17:54
o-Xylene ug/kg ND 5.8 11/13/14 17:54
p-Isopropyltoluene ug/kg ND 5.8 11/13/14 17:54
sec-Butylbenzene ug/kg ND 5.8 11/13/14 17:54
Styrene ug/kg ND 5.8 11/13/14 17:54
tert-Butylbenzene ug/kg ND 5.8 11/13/14 17:54
Tetrachloroethene ug/kg ND 5.8 11/13/14 17:54
Toluene ug/kg ND 5.8 11/13/14 17:54
trans-1,2-Dichloroethene ug/kg ND 5.8 11/13/14 17:54
trans-1,3-Dichloropropene ug/kg ND 5.8 11/13/14 17:54
Trichloroethene ug/kg ND 5.8 11/13/14 17:54
Trichlorofluoromethane ug/kg ND 5.8 11/13/14 17:54
Vinyl acetate ug/kg ND 58.1 11/13/14 17:54
Vinyl chloride ug/kg ND 11.6 11/13/14 17:54
Xylene (Total)ug/kg ND 11.6 11/13/14 17:54
1,2-Dichloroethane-d4 (S)%109 70-132 11/13/14 17:54
4-Bromofluorobenzene (S)%95 70-130 11/13/14 17:54
Toluene-d8 (S)%100 70-130 11/13/14 17:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1329215LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.341.1 120 74-137
1,1,1-Trichloroethane ug/kg 52.541.1 128 67-140
1,1,2,2-Tetrachloroethane ug/kg 46.341.1 113 72-141
1,1,2-Trichloroethane ug/kg 49.741.1 121 78-138
1,1-Dichloroethane ug/kg 51.541.1 125 69-134
1,1-Dichloroethene ug/kg 51.341.1 125 67-138
1,1-Dichloropropene ug/kg 56.541.1 138 69-139
1,2,3-Trichlorobenzene ug/kg 55.141.1 134 70-146
1,2,3-Trichloropropane ug/kg 53.641.1 131 69-144
1,2,4-Trichlorobenzene ug/kg 56.041.1 136 68-148
1,2,4-Trimethylbenzene ug/kg 54.341.1 132 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1329215LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 52.641.1 128 65-140
1,2-Dibromoethane (EDB)ug/kg 52.141.1 127 77-135
1,2-Dichlorobenzene ug/kg 52.641.1 128 77-141
1,2-Dichloroethane ug/kg 47.741.1 116 65-137
1,2-Dichloropropane ug/kg 51.741.1 126 72-136
1,3,5-Trimethylbenzene ug/kg 53.441.1 130 76-133
1,3-Dichlorobenzene ug/kg 52.241.1 127 74-138
1,3-Dichloropropane ug/kg 51.741.1 126 71-139
1,4-Dichlorobenzene ug/kg 52.441.1 128 76-138
2,2-Dichloropropane ug/kg 52.541.1 128 68-137
2-Butanone (MEK)ug/kg 11382.1 138 58-147
2-Chlorotoluene ug/kg 52.641.1 128 73-139
2-Hexanone ug/kg 10782.1 131 62-145
4-Chlorotoluene ug/kg 53.841.1 131 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 11582.1 140 64-149
Acetone ug/kg 11282.1 137 53-153
Benzene ug/kg 52.941.1 129 73-135
Bromobenzene ug/kg 58.0 L041.1 141 75-133
Bromochloromethane ug/kg 52.941.1 129 73-134
Bromodichloromethane ug/kg 46.241.1 113 71-135
Bromoform ug/kg 48.041.1 117 66-141
Bromomethane ug/kg 50.241.1 122 53-160
Carbon tetrachloride ug/kg 53.041.1 129 60-145
Chlorobenzene ug/kg 50.141.1 122 78-130
Chloroethane ug/kg 49.941.1 122 64-149
Chloroform ug/kg 48.241.1 117 70-134
Chloromethane ug/kg 51.841.1 126 52-150
cis-1,2-Dichloroethene ug/kg 53.541.1 130 70-133
cis-1,3-Dichloropropene ug/kg 52.641.1 128 68-134
Dibromochloromethane ug/kg 47.641.1 116 71-138
Dibromomethane ug/kg 51.841.1 126 74-130
Dichlorodifluoromethane ug/kg 51.141.1 124 40-160
Diisopropyl ether ug/kg 51.941.1 126 69-141
Ethylbenzene ug/kg 51.641.1 126 75-133
Hexachloro-1,3-butadiene ug/kg 54.241.1 132 68-143
Isopropylbenzene (Cumene)ug/kg 51.841.1 126 76-143
m&p-Xylene ug/kg 97.382.1 119 75-136
Methyl-tert-butyl ether ug/kg 50.241.1 122 68-144
Methylene Chloride ug/kg 50.041.1 122 45-154
n-Butylbenzene ug/kg 55.341.1 135 72-137
n-Propylbenzene ug/kg 51.241.1 125 76-136
Naphthalene ug/kg 57.541.1 140 68-151
o-Xylene ug/kg 50.741.1 123 76-141
p-Isopropyltoluene ug/kg 52.641.1 128 76-140
sec-Butylbenzene ug/kg 51.541.1 125 79-139
Styrene ug/kg 52.741.1 128 79-137
tert-Butylbenzene ug/kg 47.741.1 116 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1329215LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 47.141.1 115 71-138
Toluene ug/kg 50.841.1 124 74-131
trans-1,2-Dichloroethene ug/kg 52.041.1 127 67-135
trans-1,3-Dichloropropene ug/kg 54.341.1 132 65-146
Trichloroethene ug/kg 53.141.1 129 67-135
Trichlorofluoromethane ug/kg 49.741.1 121 59-144
Vinyl acetate ug/kg 57.1 F382.1 70 40-160
Vinyl chloride ug/kg 48.841.1 119 56-141
Xylene (Total)ug/kg 148123 120 76-137
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1330102MATRIX SPIKE SAMPLE:
MSSpike
Result
92225178001
1,1,1,2-Tetrachloroethane ug/kg 19.123.4 82 70-130ND
1,1,1-Trichloroethane ug/kg 18.623.4 80 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 20.923.4 89 70-130ND
1,1,2-Trichloroethane ug/kg 20.423.4 87 70-130ND
1,1-Dichloroethane ug/kg 19.423.4 83 70-130ND
1,1-Dichloroethene ug/kg 17.023.4 73 49-180ND
1,1-Dichloropropene ug/kg 18.723.4 80 70-130ND
1,2,3-Trichlorobenzene ug/kg 10.9 M123.4 46 70-130ND
1,2,3-Trichloropropane ug/kg 20.723.4 89 70-130ND
1,2,4-Trichlorobenzene ug/kg 11.0 M123.4 47 70-130ND
1,2,4-Trimethylbenzene ug/kg 17.123.4 73 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 21.923.4 93 70-130ND
1,2-Dibromoethane (EDB)ug/kg 21.523.4 92 70-130ND
1,2-Dichlorobenzene ug/kg 16.2 M123.4 69 70-130ND
1,2-Dichloroethane ug/kg 19.823.4 84 70-130ND
1,2-Dichloropropane ug/kg 19.423.4 83 70-130ND
1,3,5-Trimethylbenzene ug/kg 17.023.4 73 70-130ND
1,3-Dichlorobenzene ug/kg 16.2 M123.4 69 70-130ND
1,3-Dichloropropane ug/kg 21.523.4 92 70-130ND
1,4-Dichlorobenzene ug/kg 16.623.4 71 70-130ND
2,2-Dichloropropane ug/kg 18.023.4 77 70-130ND
2-Butanone (MEK)ug/kg 42.1J46.8 90 70-130ND
2-Chlorotoluene ug/kg 17.023.4 73 70-130ND
2-Hexanone ug/kg 45.6J46.8 97 70-130ND
4-Chlorotoluene ug/kg 17.223.4 74 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 45.1J46.8 96 70-130ND
Acetone ug/kg 37.2J46.8 80 70-130ND
Benzene ug/kg 18.423.4 79 50-166ND
Bromobenzene ug/kg 17.023.4 73 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1330102MATRIX SPIKE SAMPLE:
MSSpike
Result
92225178001
Bromochloromethane ug/kg 20.223.4 86 70-130ND
Bromodichloromethane ug/kg 17.623.4 75 70-130ND
Bromoform ug/kg 19.023.4 81 70-130ND
Bromomethane ug/kg 16.623.4 71 70-130ND
Carbon tetrachloride ug/kg 18.123.4 77 70-130ND
Chlorobenzene ug/kg 19.023.4 81 43-169ND
Chloroethane ug/kg 16.323.4 70 70-130ND
Chloroform ug/kg 18.223.4 78 70-130ND
Chloromethane ug/kg 11.2J M123.4 48 70-130ND
cis-1,2-Dichloroethene ug/kg 21.623.4 86 70-130ND
cis-1,3-Dichloropropene ug/kg 18.723.4 80 70-130ND
Dibromochloromethane ug/kg 18.823.4 80 70-130ND
Dibromomethane ug/kg 19.923.4 85 70-130ND
Dichlorodifluoromethane ug/kg 8.6J M123.4 37 70-130ND
Diisopropyl ether ug/kg 20.423.4 87 70-130ND
Ethylbenzene ug/kg 19.123.4 82 70-130ND
Hexachloro-1,3-butadiene ug/kg 11.2 M123.4 48 70-130ND
Isopropylbenzene (Cumene)ug/kg 18.123.4 78 70-130ND
m&p-Xylene ug/kg 38.046.8 81 70-130ND
Methyl-tert-butyl ether ug/kg 20.223.4 87 70-130ND
Methylene Chloride ug/kg 34.123.4 99 70-130ND
n-Butylbenzene ug/kg 14.4 M123.4 62 70-130ND
n-Propylbenzene ug/kg 17.523.4 75 70-130ND
Naphthalene ug/kg 13.9 M123.4 60 70-130ND
o-Xylene ug/kg 18.023.4 77 70-130ND
p-Isopropyltoluene ug/kg 16.0 M123.4 68 70-130ND
sec-Butylbenzene ug/kg 16.423.4 70 70-130ND
Styrene ug/kg 18.323.4 78 70-130ND
tert-Butylbenzene ug/kg 15.6 M123.4 67 70-130ND
Tetrachloroethene ug/kg 149 M123.4 189 70-130104
Toluene ug/kg 18.823.4 80 52-163ND
trans-1,2-Dichloroethene ug/kg 18.723.4 80 70-130ND
trans-1,3-Dichloropropene ug/kg 20.223.4 86 70-130ND
Trichloroethene ug/kg 21.023.4 78 49-167ND
Trichlorofluoromethane ug/kg 16.923.4 72 70-130ND
Vinyl acetate ug/kg 21.3J M146.8 46 70-130ND
Vinyl chloride ug/kg 14.3 M123.4 61 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92224775002
1330635SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92224775002
1330635SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 43.6J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92224775002
1330635SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%125 33116
4-Bromofluorobenzene (S)%78 2777
Toluene-d8 (S)%99 1g2798
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92225255
Noda Site 71147763
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7233
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92225255001, 92225255002, 92225255003, 92225255004, 92225255005, 92225255006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92225178001
1329003SAMPLE DUPLICATE:
Percent Moisture %13.5 7 2514.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92224987002
1329004SAMPLE DUPLICATE:
Percent Moisture %9.9 1 2510
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92225255
Noda Site 71147763
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92225255
Noda Site 71147763
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92225255001 MSV/29238GP-1 (0-5)EPA 8260
92225255002 MSV/29238GP-1 (10-15)EPA 8260
92225255003 MSV/29238GP-2 (10-15)EPA 8260
92225255004 MSV/29238GP-3 (15-20)EPA 8260
92225255005 MSV/29238GP-4 (5-10)EPA 8260
92225255006 MSV/29238GP-4 (15-20)EPA 8260
92225255001 PMST/7233GP-1 (0-5)ASTM D2974-87
92225255002 PMST/7233GP-1 (10-15)ASTM D2974-87
92225255003 PMST/7233GP-2 (10-15)ASTM D2974-87
92225255004 PMST/7233GP-3 (15-20)ASTM D2974-87
92225255005 PMST/7233GP-4 (5-10)ASTM D2974-87
92225255006 PMST/7233GP-4 (15-20)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 04:17 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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