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PREPARED FOR:
GRANVILLE COUNTY
SOLID WASTE DEPARTMENT
P.O. BOX 906
OXFORD, NORTH CAROLINA 27565

OXFORD UNIT 2 LANDFILL
PERMIT NO. 39-01 MSWLF 2012

FIRST SEMIANNUAL WATER QUALITY
MONITORING REPORT OF 2016

APRIL 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone] JOYCE PROJECT NO. 660.1601.12

FIRST SEMIANNUAL WATER QUALITY MONITORING REPORT OF 2016
Oxford Landfill, Unit 2 - Granville County - Permit No. 3901-MSWLF-2012

TABLE OF CONTENTS

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
i

1.0 INTRODUCTION ................................................................................................................. 1
1.1 Site Background .................................................................................................................. 1
1.2 Site Conceptual Model ........................................................................................................ 2
1.2.1 Site Geology ................................................................................................................. 2
1.2.2 Site Hydrogeology ........................................................................................................ 2
1.3 Aquifer Characteristics & Groundwater Flow Regime ....................................................... 2
1.4 Monitoring History .............................................................................................................. 4
1.4.1 Monitoring History ....................................................................................................... 4
2.0 FACILITY MONITORING PROGRAM ........................................................................... 4
2.1 Groundwater Monitoring Program ...................................................................................... 4
2.1 Surface Water Monitoring Program .................................................................................... 4
3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2016 .................................................... 4
3.1 Field Work ........................................................................................................................... 4
3.2 Laboratory Analysis and Quality Control ........................................................................... 5
3.3 Data Analysis ...................................................................................................................... 6
3.3.1 Analytical Results for Groundwater ............................................................................. 6
3.3.3 Statistical Methods and Background ............................................................................ 6
3.3.4 Statistical Analyses ...................................................................................................... 6
3.3.5 Analytical Results for Surface Water .......................................................................... 7
4.0 CONCLUSIONS .................................................................................................................... 7
5.0 REFERENCES ...................................................................................................................... 7
7.0 ACRONYMS ......................................................................................................................... 8

FIRST SEMIANNUAL WATER QUALITY MONITORING REPORT OF 2016
Oxford Landfill, Unit 2 - Granville County - Permit No. 3901-MSWLF-2012

TABLE OF CONTENTS

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
ii

TABLES:
Table 1 Well Construction Details
Table 2 Historical Groundwater Elevation Data
Table 3 Groundwater Gradients and Calculated Flow Rates
Table 4 Quantified Detections of Constituents (February 2016)
Table 5 Field Parameters by Location (February 2016)

FIGURE:
Figure 1 Site Location Map (USGS Topographic Map)

DRAWING:
Drawing 1 Groundwater Potentiometric Surface Map (February 2016)

APPENDICES
Appendix A Field Sampling Logs
Appendix B Laboratory Reports with Chains of Custody
Appendix C Historical Detected Groundwater Constituents
Appendix D Historical Detected Surface Water Constituents

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
1

1.0 INTRODUCTION
On behalf of Granville County, Joyce Engineering, (JOYCE) has prepared this Water Quality
Monitoring Report for the Oxford Unit 2 Municipal Solid Waste Landfill, Solid Waste Permit
Number 3901-MSWLF-2012 (facility), in accordance with the North Carolina Solid Waste
Management Rules (NCSWMR) 15A NCAC 13B.1632.

1.1 Site Background
The Oxford Landfill is located at 6584 Landfill Road, Oxford, Granville County, North Carolina,
near the town of Kinton Fork (Figure 1). The facility is owned and operated by Granville
County under Permit Number 3901-MSWLF-2012, issued by the North Carolina Department of
Environmental Quality (NCDEQ) [formerly the Department of Environment and Natural
Resources (DENR)] Solid Waste Section (SWS). The Oxford Landfill consists of two separate
waste disposal units. Unit 1 is a former unlined municipal solid waste (MSW) landfill originally
permitted for disposal of domestic, institutional, industrial, agricultural, and demolition wastes,
with an active C&D landfill on top. Unit 2 is a Subtitle-D MSW landfill. Granville County
received the Unit 2 Permit to Operate from DENR on February 19, 2013. The county began
placing waste in Unit 2 on May 1, 2013.

The groundwater monitoring network for the Unit 2 facility consists of one upgradient well
(MW-7) and five downgradient wells (MW-8, MW-9, MW-10, MW-11 and NES-2S) as shown
on Drawing 1. Monitoring well MW-7 serves as the background well for both the Unit 1 and
Unit 2 landfills. NES-2S is also a performance well for the Unit 1 landfill. The monitoring wells
are screened within the uppermost aquifer underlying the facility. Table 1 presents a summary of
the well construction data for the monitoring wells.

Surface water at the facility is currently monitored semiannually in conjunction with the
groundwater sampling events for Units 1 and 2. Samples are collected from four surface water
monitoring points, SW-1, SW-2, SW-3, and SW-4. SW-1 is located in a sedimentation pond
upstream of the landfill and SW-2 is located immediately downstream of the landfill in a
drainage channel which runs between Unit 1 and Unit 2. Results from SW-1 and SW-2 will be
reported for both units. In addition, two surface water points, SW-3 and SW-4, are monitored for
Unit 2 only. SW-3 is located upstream of Phase 1 of Unit 2, on the perennial creek that runs
along the east side of Phase 1. SW-4 is located on the same perennial creek downstream of
Phase 1, but before the confluence of the perennial creek and the drainage channel from the west
side of Unit 2. The perennial creek eventually flows into Little Grassy Creek, which is classified
“C”, for waters protected for secondary recreation, aquatic life, and wildlife.

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
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1.2 Site Conceptual Model
1.2.1 Site Geology
The Oxford Landfill is located in the Carolina Slate Belt of the Piedmont Physiographic Province
of North Carolina. The geologic province is characterized by rolling topography with a thick
mantle of saprolite overlying late-Proterozoic and Paleozoic igneous and metamorphic bedrock.
The Carolina Slate Belt is comprised of 550 to 650 million year old, metamorphosed
sedimentary and volcanic rocks, intruded by granitic rocks.

The Oxford Landfill is underlain by the Flat River Complex, a shallow intrusive complex of
granitic composition, which comprises a large portion of the northern Carolina Slate Belt (Butler,
1991). The landfill is approximately 18 miles east of the Virgilina Synclinorium, approximately
10 miles west of the Nutbush Creek Fault Zone, and approximately 4 miles northwest of the
Durham Basin (Butler, 1991).

Previous investigations discovered limited exposures of competent, massive, gray to greenish
gray meta-volcanic rock that is moderately fractured. Prominent fractures with near vertical dips
and strike approximately N-20o- E (Joyce, 2009b). Boring logs indicate that the depth to bedrock
at Oxford Landfill ranges from 3 to 35 feet below ground surface. The overlying saprolite
consists of brownish sandy to clayey silt (Joyce, 2009b).

1.2.2 Site Hydrogeology
Groundwater in the Piedmont can occur in substantial volumes where soils and regolith are thick,
but groundwater is typically found in minimal volumes in bedrock, primarily restricted to
fractures. The water table under the area landfill was encountered in the unconfined aquifer that
is mostly in the transition zone that consists of saprolite and highly fractured bedrock. This
unconfined aquifer is pervasive across the site and generally mimics the surface topography.
The saturated portion of the uppermost aquifer beneath the landfill is vertically continuous to
bedrock, and no confining layers have been encountered during permitting. There is a high
degree of connectivity between the saprolite and underlying fractured bedrock such that they
behave as a single continuous aquifer. Depth to water ranged from 3 to 18 feet below grade in
wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S (Table 1). In general, the water
table is near the saprolite/bedrock interface. Drawing 1 presents a groundwater potentiometric
surface map based on static water level data obtained from both Unit 1 and Unit 2 monitoring
wells on August 18, 2015. Drawing 1 depicts groundwater flow to the north beneath Unit 2.

1.3 Aquifer Characteristics & Groundwater Flow Regime
Groundwater in the region generally occurs in the unconfined aquifer that includes both the
saprolite (soil and regolith derived from in-situ weathering of igneous or metamorphic bedrock)
and the underlying fractured bedrock. The transition zone between saprolite and fractured
bedrock is often gradational and can range in thickness from a few inches to several feet.
Typically, the uppermost portion of the fractured bedrock is hydraulically well connected to the

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
3

overlying saprolite such that they act as a single aquifer. The frequency and connectivity of
fractures normally decreases with depth. The unconfined aquifer is pervasive across the site.

Over most of the site, the water table is encountered either slightly above or slightly below the
top of bedrock and generally mimics the surface topography. However, in a few locations at the
site, the water table is as much as 10-15 feet above the top of bedrock.

The bedrock is characterized by very low porosity (less than 10%) but, because it is highly
fractured, the permeability is estimated to be 1.0E-03 cm/sec or higher.

Slug tests were conducted on several piezometers and monitoring wells in the Unit 2 landfill area
in February and March, 2009 to determine the hydraulic conductivity of the aquifer materials.
Most of the piezometers and wells were screened within the fractured bedrock; however, a few
were screened within the saprolite. The average hydraulic conductivity of the fractured bedrock
was 0.87 feet/day. With the exception of the background well (MW-7), all of the monitoring
wells are screened in bedrock. The higher hydraulic conductivity and lower porosity of the
fractured bedrock compared to the saprolite, coupled with the fact that, in most places, only the
upper few feet of the water column are in saprolite, indicate that groundwater flow is going to be
predominantly in the fractured bedrock portion of the aquifer.

Depth to groundwater is measured in all compliance monitoring wells relative to the surveyed
measuring point (top of casing) at the site prior to each sampling event. The groundwater
elevations relative to mean sea level calculated for each monitoring well are summarized in
Table 2. The groundwater elevation contours shown in Drawing 1 are based on data from the
February 2016 sampling event. Groundwater flow beneath the facility is primarily to the north.

Table 3 summarizes the groundwater flow rate calculations for the Unit 2 Landfill. Linear
groundwater flow velocities for wells screened in bedrock were computed using the modified
Darcy equation: V = Ki/ne, where V = average linear velocity (feet/year), K = hydraulic
conductivity (feet/day), i = horizontal hydraulic gradient, and ne = effective porosity.

The mean of hydraulic conductivities (K) from slug-tests conducted in February and March 2009
were used in these calculations, based on the primary lithology of the screened intervals of the
wells or piezometers. The mean hydraulic conductivity of the fractured bedrock was 0.87
feet/day. Horizontal groundwater gradient (i) along the flow path through Unit 2 (i3) shown on
Drawing 1 was estimated from the groundwater potentiometric contours for February 18, 2016.
The gradient across the site was approximately 0.0202 ft/ft. Our flow calculations assumed an
estimated effective porosity (ne) of 0.10 (10%) for the fractured bedrock (Table 3). The linear
flow velocity in the fractured bedrock beneath Unit 2 is estimated at 64 feet per year.

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
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1.4 Monitoring History
1.4.1 Monitoring History
 2012: Pre-waste Background sampling.
 2013: Detection monitoring was initiated.

2.0 FACILITY MONITORING PROGRAM
2.1 Groundwater Monitoring Program
Six groundwater monitoring wells comprise the compliance monitoring network at the Oxford
Unit 2 Landfill. The compliance network includes monitoring wells MW-7 (the current facility
background well), MW-8, MW-9, MW-10, MW-11, and NES-2S. All monitoring wells are
sampled for North Carolina Appendix I list of constituents. MW-7 also serves as the background
well for the Unit 1 landfill and is sampled in accordance to the Unit 1 Groundwater Monitoring
Plan. NES-2S also serves as a performance well and is sampled under the Unit 1 Corrective
Action Plan (CAP) for the facility.

2.1 Surface Water Monitoring Program
There are four surface water sampling points, SW-1, SW-2, SW-3, and SW-4. Sampling point
SW-1 is located in a sedimentation basin near the southeast corner of the waste unit, upgradient
of the waste. Sampling point SW-2 is located northeast of the waste unit along a tributary of
Little Grassy Creek, down-gradient of the waste. SW-3 is located upstream of Unit 2, Phase 1 on
the perennial creek that runs along the east side of the new phase. SW-4 is located on the same
perennial creek downstream of the new phase, but before the confluence of the perennial creek
and the drainage channel from the west side of Unit 2. The surface water samples are analyzed
for the NCSWMR Appendix I list of constituents during both semiannual events.

3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2016
3.1 Field Work
On February 17th and 18th, 2016, JOYCE personnel visited Oxford Landfill to purge and sample
monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S and to collect samples
from surface points SW-2, SW-3 and SW-4. Sample data from SW-1 sampling is covered in the
Oxford Unit 1 Water Quality Monitoring Report.

Monitoring wells were purged and sampled using either a 12 volt pump or disposable bailers.
Field measurements of temperature, pH, specific conductivity, and turbidity were recorded in a
field log for all wells. Prior to sampling, laboratory-supplied containers were prepared with the
following information:

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
5

 Monitoring well ID (completed by laboratory or field personnel);
 Date and time of sample collection (completed by field personnel);
 Initials of sampling personnel (completed by field personnel);
 Project name and number (completed by the laboratory or field personnel);
 Chemical preservative (completed by the laboratory or field personnel); and
 Requested chemical analysis (completed by the laboratory or field personnel).

Groundwater samples from each monitoring well were collected either immediately after purging
or within 24 hours of the final purge volume and were dispensed directly from the pump flow or
bailers into the laboratory-provided containers. Immediately after collection, the samples were
placed in a laboratory-provided cooler and chilled on ice. Field sampling logs are provided in
the Appendix A.

Surface water points SW-1, SW-2, SW-3 and SW-4 were sampled using a decontaminated
graduated dipper. Prepared sampling containers were filled from the dipper, placed in a cooler,
and chilled on ice. Field sampling logs are provided in the Appendix A.

3.2 Laboratory Analysis and Quality Control
The February 2016 groundwater and surface water samples were delivered to Pace Analytical
Services Inc. of Huntersville, North Carolina under chain-of-custody control. Groundwater
samples from the compliance wells and surface points were analyzed for NC Appendix I
constituents. The samples were received by the laboratory February 19,2016, in good condition,
properly preserved, at proper temperatures, and within analysis hold times.

In addition to samples collected for compliance monitoring at the Oxford Landfill, JOYCE
personnel collected a Field Blank as part of the February 2016 sampling event. The Field Blank
was analyzed for both Unit 1 and Unit 2 list of constituents. Also, a Trip Blank that was
prepared by the laboratory accompanied the volatile sampling containers to and from the
laboratory. The Trip Blank was analyzed for both Unit 1 and Unit 2 list of constituents list of
volatile organic compounds.

Upon receipt of the laboratory data package, JOYCE personnel reviewed the following data:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Biased data results based on Matrix Spike, Matrix Spike Duplicate, and Laboratory
Control Samples;
 Blank qualified data (B-flags);
 Detections above the 15A NCAC 2L.0202 (NC 2L) Groundwater Standards or the
SWS Groundwater Water Protection Standards (GWPS), or 15A NCAC 2B (NC 2B)
Surface Water Standards; and
 Detections above historical levels.

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
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6

The complete laboratory analytical reports are included in Appendix B.

3.3 Data Analysis
3.3.1 Analytical Results for Groundwater
The only in inorganic constituent detected in any of the February 2016 groundwater samples at a
quantified concentration above the SWSL was zinc in MW-8. No organic constituents were
detected at quantified concentrations above the SWSL. No constituents were detected above the
NC 2L or GWPS in any groundwater sample. Table 4 summarizes the quantified detections of
constituents for the February 2016 sampling event. The laboratory analytical reports, the
laboratory quality assurance/quality control information, and the chains-of-custody, are included
in Appendix B. Historical groundwater analytical results are presented in Appendix C.

3.3.3 Statistical Methods and Background
Prior to the spring 2001 sampling event, the Oxford Landfill (Unit 1) had two background wells,
MW-1 and MW-1A. MW-1 was damaged by a vehicle and, with the approval of NCDEQ, was
abandoned in early 2001. MW-1A was affected by low water levels and impact from high
turbidity levels; therefore, NCDEQ approved replacing it with MW-7 as the background for the
first semiannual sampling event of 2011. Data from MW-1 between September 1994 and
October 2000, data from MW-1A from September 1994 to June 2010, and data from MW-7 from
June 2011 to present have been used to determine statistical background concentrations for
inorganic constituents detected at the facility. In addition to historical data from MW-1,
MW-1A, and MW-7, pre-waste background sampling data from MW-8, MW-9, MW-10,
MW-11, and MW-12 collected between June and October 2012 may also be included as
background data for statistical analyses.

The background data for inorganic constituents are evaluated in accordance with the procedures
outlined in 15A NCAC 13B.1632 (g) and (h) to determine if the reported concentration exceeded
the facility background concentrations using the Shapiro-Wilk Test, Parametric Prediction
Limits, Parametric Tolerance Intervals, Aitchison’s Adjustment, Non-Parametric Prediction
Limits, and Poisson Prediction Limits as appropriate. Background data, tests for normality,
outliers, Aitchison’s adjustment, tolerance interval, or prediction limits are used, as appropriate
based on the background data. The statistical test by which downgradient data are compared to
facility background data is based upon the nature of the data and the number of data values that
are less than the laboratory limit of detection. All statistical tests are evaluated at the 0.05 level
of significance, 95% confidence level, and are conducted as one-tailed tests.

3.3.4 Statistical Analyses
No inorganic constituents were detected above their NC 2L or GWPS; therefore, statistical
analyses were not required.

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
7

3.3.5 Analytical Results for Surface Water
Sampling point SW-1 is located in a sedimentation basin near the southeast corner of the waste
unit, upgradient of the waste. Sampling point SW-2 is located northeast of the waste unit along a
tributary of Little Grassy Creek, down-gradient of the waste. SW-3 is located upstream of Unit 2,
Phase 1 on the perennial creek that runs along the east side of the new phase. SW-4 is located on
the same perennial creek downstream of the new phase, but before the confluence of the
perennial creek and the drainage channel from the west side of Unit 2. Surface water analytical
results from the site were compared to the 15A-NCAC-2B (NC-2B) surface water standards for
protection of fresh-water aquatic life or human health, whichever is lower (more protective) for a
given constituent.

No constituents were detected above the SWSL in and surface water points during the February
2016 sampling event. The laboratory analytical reports, the laboratory quality assurance/quality
control information, and the chains-of-custody, for SW-2, SW-3 and SW-4 are included in
Appendix B. Historical groundwater analytical results are presented in Appendix D.

4.0 CONCLUSIONS
No inorganic or organic constituents were detected above their NC 2L or GWPS during the
February 2016 monitoring event. The groundwater flow regime is consistent with previous data
and the groundwater monitoring system remains adequate for monitoring the site. Based on
analytical results from the February 2016 event, the Granville County, Oxford Unit 2 Landfill
will remain in the Detection Monitoring program as outlined in Title 15A NCAC 13B .1633.
The next semiannual sampling event is tentatively scheduled for August 2016.

5.0 REFERENCES
The references cited herein were used to prepare this document and may or may not be cited in
the text of this report.

Butler, J. Robert, and Secor, Jr., Donald T., 1991, The Central Piedmont, in Horton, J. W., Jr.,
and Zullo, V. A., eds., The Geology of the Carolinas: The University of Tennessee Press,
p. 59-78.

JOYCE, 2009a. Corrective Action Plan, Granville County Oxford Landfill. March 2009.

JOYCE, 2009b. Hydrogeologic Reports, Granville County Oxford Landfill. October 2009.

JOYCE, 2010a. Request for Background Well Replacement, Granville County Oxford Landfill,
Permit # 39-01. October 25, 2010.

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
8

JOYCE, 2010b. Corrective Action Evaluation Report and Alternate Source
Demonstrations,Granville County Oxford C&D Over MSW Landfill, Permit # 39-01.
November 29, 2010.

JOYCE, 2013. Groundwater Background Monitoring Report Unit 2, Phase 1 MSWLF
Expansion. January 4, 2013

North Carolina Department of Environment, Health, and Natural Resources, 1997. North
Carolina Solid Waste Management Rules. 15 NCAC 13B.1600. January 1, 1997, with
updates through April 2011.

North Carolina Geological Survey, 1985, Geologic map of North Carolina: North Carolina
Department of Natural Resources and Community Development, scale 1:500000.

USEAP, 1992. Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance. July 1992.

Woodward-Clyde Consultants, 1994. Transition Plan, Oxford Landfill Granville County, North
Carolina. April 1994.

7.0 ACRONYMS
ACM Assessment of Corrective Measures (report)
AOC Area of Concern
ASD Alternate Source Demonstration (report)
C&D Construction and Demolition Waste
CAP Corrective Action Plan (report)
CAER Corrective Action Evaluation Report (report)
CPVC Chlorinated Poly Vinyl Chloride
CO2 Carbon Dioxide
COC Contaminant of Concern
DCA Dichloroethane
DCE Dichloroethylene
DENR North Carolina Department of Environment and Natural Resources
DH Dissolved Hydrogen
DL Detection Limit (for laboratory data)
DO Dissolved Oxygen
EPA United States Environmental Protection Agency
Fe2+ Ferrous Iron
GEU Gas Extraction Unit
GWPS Groundwater Protection Standards
HASP Site-specific Health and Safety Plan
HDPE High-density Polyethylene
JE Joyce Engineering

First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Oxford Unit 2 Landfill, Permit No. 3901-MSWLF-2012 April 2016
9

JOYCE Joyce Engineering
LFG Landfill Gas
LEL Lower Explosive Limit
MNA Monitored Natural Attenuation
MSW Municipal Solid Waste
MW Monitoring Well
NC-2B North Carolina Surface Water Standards found in 15A NCAC 2B.0101
NC-2L North Carolina Groundwater Standards found in 15A NCAC 2L.0202
NCAC North Carolina Administrative Code
NCDEQ North Carolina Department of Environmental Quality
NCSWMR North Carolina Solid Waste Management Regulations (15A NCAC 13B.1600)
ND Not Detected (for laboratory data)
NES Nature and Extent Study (report)
O&M Operations and Maintenance
ORP Oxidation-Reduction Potential
OSHA Occupational Health and Safety Association
PCE perchloroethylene (aka – tetrachloroethylene)
PVC Poly Vinyl Chloride
QL Quantitation Limit (for laboratory data)
QRA Quantitative Risk Assessment (report)
RL Reporting Limit (for laboratory data)
SC Specific Conductance
SSI Statistically Significant Increase (over background concentration)
SWQS Surface Water Quality Standards
SWS DENR Division of Waste Management, Solid Waste Section
SWSL North Carolina Solid Waste Section Reporting Limits (for laboratory data)
TCE Trichloroethylene
TDS Total Dissolved Solids
TOC Total Organic Carbon
TSS Total Suspended Solids
VC Vinyl Chloride
VFA Volatile Fatty Acid
VOC Volatile Organic Compound
WQMP Water Quality Monitoring Plan (report)

TABLES

Table 1 Well Construction Details Table 2 Historical Groundwater Elevation Data
Table 3 Groundwater Gradients and Calculated Flow Rates
Table 4 Quantified Detections of Constituents (February 2016)
Table 5 Field Parameters by Location (February 2016)
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Joyce Engineering
TABLE 2: Historical Groundwater Elevation Data
Background
MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S
Well TOC Elev.:534.24 503.31 487.51 484.92 478.72 477.20
Well Total Depth:37.32 28.00 43.00 32.90 22.90 24.20
13-Jun-12 513.48 503.31 479.7 477.42 473.20 468.81
22-Aug-12 509.73 500.82 477.97 475.31 471.50 469.36
25-Sep-12 508.45 499.85 478.1 475.06 471.86 469.30
17-Oct-12 507.95 499.90 478 474.23 471.04 467.98
06-Aug-13 514.33 499.92 478.81 475.32 472.80 469.29
25-Feb-14 511.75 499.91 480.34 476.26 473.47 470.28
12-Aug-14 511.98 500.16 479.91 476.54 473.42 470.29
12-Mar-15 516.39 499.99 479.73 476.47 473.66 470.63
18-Aug-15 512.39 499.86 478.41 474.92 472.17 469.25
16-Feb-16 515.79 499.90 481.44 476.37 474.12 471.15
Notes:
TOC = top of casing.
Water levels are measured from TOC.
All elevations are in feet above mean sea level.
Downgradient
Granville Co. - Oxford Landfill, Unit 2
Permit 3901-MSWLF-2012 Joyce Engineering
Table 4: Quantified Detections of Constituents (February 2016)
WELL ID PARAMETER RESULT UNITS SWSL NC 2L DATE
3901-MW8 Zinc 13.1 µg/L 10 1000 2/18/2016
Notes: µg/L = Micorgrams per liter
SWSL = NC Soild Waste Section Reporting Limit
NC 2L = Groundwater Standard from 15A NCAC 2L.0202
Granville Co. - Oxford Landfill, Unit 2
Permit No. 3901 MSWLF-2012
Joyce Engineering
Table 5: Field Parameters by Location
WELL ID PARAMETER RESULT UNITS COLLECT DATE
3901-MW7 pH 6.89 S.U 2/18/2016
3901-MW7 Temperature 12.8 ºC 2/18/2016
3901-MW7 Conductivity 250 µS/cm 2/18/2016
3901-MW7 Turbidity 8.25 NTU 2/18/2016
3901-MW7 Static Water Level 18.45 ft 2/18/2016
3901-MW7 Well Depth 37.32 ft 2/18/2016
3901-MW8 pH 7.45 S.U 2/17/2016
3901-MW8 Temperature 15.6 ºC 2/17/2016
3901-MW8 Conductivity 195.8 µS/cm 2/17/2016
3901-MW8 Turbidity 10.25 ntu 2/17/2016
3901-MW8 Static Water Level 3.41 ft 2/17/2016
3901-MW8 Well Depth 28.00 ft 2/17/2016
3901-MW9 pH 7.11 S.U 2/18/2016
3901-MW9 Temperature 14.7 ºC 2/18/2016
3901-MW9 Conductivity 290.3 µS/cm 2/18/2016
3901-MW9 Turbidity 11.2 NTU 2/18/2016
3901-MW9 Static Water Level 6.07 ft 2/18/2016
3901-MW9 Well Depth 43.00 ft 2/18/2016
3901-MW10 pH 6.93 S.U 2/18/2016
3901-MW10 Temperature 12.6 ºC 2/18/2016
3901-MW10 Conductivity 166.7 µS/cm 2/18/2016
3901-MW10 Turbidity 11.25 NTU 2/18/2016
3901-MW10 Static Water Level 8.55 ft 2/18/2016
3901-MW10 Well Depth 31.50 ft 2/18/2016
3901-MW11 pH 6.46 S.U 2/18/2016
3901-MW11 Temperature 12.1 ºC 2/18/2016
3901-MW11 Conductivity 122.9 µS/cm 2/18/2016
3901-MW11 Turbidity 25.4 NTU 2/18/2016
3901-MW11 Static Water Level 4.6 ft 2/18/2016
3901-MW11 Well Depth 22.90 ft 2/18/2016
Granville County- Oxford Unit 2 Landfill
Permit No. 3901 MSWLF-2012 Page 1 of 2
Joyce Engineering
Table 5: Field Parameters by Location
WELL ID PARAMETER RESULT UNITS COLLECT DATE
3901-NES2S pH 6.13 S.U 2/18/2016
3901-NES2S Temperature 11.3 ºC 2/18/2016
3901-NES2S Conductivity 95.7 µS/cm 2/18/2016
3901-NES2S Turbidity 8.55 NTU 2/18/2016
3901-NES2S Static Water Level 6.05 ft 2/18/2016
3901-NES2S Well Depth 24.2 ft 2/18/2016
3901-SW3 pH 7.35 S.U 2/17/2016
3901-SW3 Temperature 10.8 ºC 2/17/2016
3901-SW3 Conductivity 33.7 µS/cm 2/17/2016
3901-SW3 Turbidity 13.1 NTU 2/17/2016
3901-SW4 pH 6.88 S.U 2/17/2016
3901-SW4 Temperature 10.2 ºC 2/17/2016
3901-SW4 Conductivity 36.4 µS/cm 2/17/2016
3901-SW4 Turbidity 43.5 NTU 2/17/2016
Notes: ºC= degrees Centigrade
S.U.= Standard Units
µS/cm = microSemens per centimeter
NTU = Nephelometric Turbidity Units
mg/L = milligrams per liter
mV = millivolts.
Granville County- Oxford Unit 2 Landfill
Permit No. 3901 MSWLF-2012 Page 2 of 2
Joyce Engineering

FIGURE

Figure 1 Site Location Map (USGS Topographic Map)

DRAWING

Drawing 1 Groundwater Potentiometric Surface Map

APPENDICES
Appendix A Field Sampling Logs
Appendix B Laboratory Reports with Chains of Custody
Appendix C Historical Detected Groundwater Constituents
Appendix D Historical Detected Surface Water Constituents

Appendix A

Field Sampling Logs

Appendix B

Laboratory Reports with Chains of Custody

#=CL#
February 25, 2016
LIMS USE: FR - VAN BURBACH
LIMS OBJECT ID: 92287200
92287200
Project:
Pace Project No.:
RE:
Mr. Van Burbach
Joyce Engineering-NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
Oxford Compliance Unit 2
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on February 19, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Dale Ingram
[e-mail]
Project Manager
Enclosures
cc: Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 36
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Lab ID Sample ID Matrix Date Collected Date Received
92287200001 3901-MW7 Water 02/18/16 09:35 02/19/16 09:30
92287200002 3901-MW8 Water 02/17/16 12:57 02/19/16 09:30
92287200003 3901-MW9 Water 02/18/16 12:13 02/19/16 09:30
92287200004 3901-MW10 Water 02/18/16 12:08 02/19/16 09:30
92287200005 3901-MW11 Water 02/18/16 11:18 02/19/16 09:30
92287200006 3901-NES2S Water 02/18/16 11:34 02/19/16 09:30
92287200007 3901-SW3 Water 02/17/16 16:25 02/19/16 09:30
92287200008 3901-SW4 Water 02/17/16 15:20 02/19/16 09:30
92287200009 3901-Field Blank Water 02/18/16 12:50 02/19/16 09:30
92287200010 3901-Trip Blank Water 02/16/16 08:00 02/19/16 09:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92287200001 3901-MW7 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200002 3901-MW8 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200003 3901-MW9 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200004 3901-MW10 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200005 3901-MW11 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200006 3901-NES2S EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200007 3901-SW3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200008 3901-SW4 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200009 3901-Field Blank EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92287200010 3901-Trip Blank EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 36
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92287200001 3901-MW7
Barium 14.8J ug/L 02/24/16 00:37100EPA 6010
92287200002 3901-MW8
Barium 59.5J ug/L 02/24/16 00:40100EPA 6010
Copper 7.8J ug/L 02/24/16 00:4010.0EPA 6010
Vanadium 2.9J ug/L 02/24/16 00:4025.0EPA 6010
Zinc 13.1 ug/L 02/24/16 18:1510.0EPA 6010
92287200003 3901-MW9
Arsenic 2.7J ug/L 02/24/16 18:1810.0EPA 6010
Barium 76.1J ug/L 02/24/16 00:43100EPA 6010
92287200004 3901-MW10
Barium 54.2J ug/L 02/24/16 00:46100EPA 6010
92287200005 3901-MW11
Arsenic 3.9J ug/L 02/24/16 18:2410.0EPA 6010
Barium 31.8J ug/L 02/24/16 00:49100EPA 6010
Nickel 2.9J ug/L 02/24/16 00:4950.0EPA 6010
92287200006 3901-NES2S
Barium 28.6J ug/L 02/24/16 00:52100EPA 6010
Chromium 3.0J ug/L 02/24/16 00:5210.0EPA 6010
Zinc 8.6J ug/L 02/24/16 18:2710.0EPA 6010
92287200007 3901-SW3
Barium 22.0J ug/L 02/24/16 00:55100EPA 6010
92287200008 3901-SW4
Barium 26.3J ug/L 02/24/16 00:59100EPA 6010
92287200009 3901-Field Blank
Lead 2.7J ug/L 02/24/16 01:0210.0EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW7 Lab ID: 92287200001 Collected: 02/18/16 09:35 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:11 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:11 7440-38-202/22/16 16:3010.0 2.5 1
Barium 14.8J ug/L 02/24/16 00:37 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:37 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:37 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:37 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:37 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:37 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:37 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:37 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:37 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:37 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:37 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:37 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:11 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 03:27 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 03:27 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 03:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 03:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 03:27 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 03:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 03:27 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 03:27 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 03:27 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 03:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 03:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 03:27 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 03:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 03:27 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 03:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 03:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 03:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 03:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 03:27 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 03:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 03:27 110-57-6 M1100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 03:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 03:27 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 03:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 03:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 03:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 03:27 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 03:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 03:27 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW7 Lab ID: 92287200001 Collected: 02/18/16 09:35 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 03:27 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 03:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 03:27 74-88-4 M110.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 03:27 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 03:27 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 03:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 03:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 03:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 03:27 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 03:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 03:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 03:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 03:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 03:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 03:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 03:27 108-05-4 M150.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 03:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 03:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/23/16 03:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/23/16 03:27 17060-07-070-130 1
Toluene-d8 (S)101 %02/23/16 03:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW8 Lab ID: 92287200002 Collected: 02/17/16 12:57 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:15 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:15 7440-38-202/22/16 16:3010.0 2.5 1
Barium 59.5J ug/L 02/24/16 00:40 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:40 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:40 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:40 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:40 7440-48-402/22/16 16:3010.0 2.5 1
Copper 7.8J ug/L 02/24/16 00:40 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:40 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:40 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:40 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:40 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:40 7440-28-002/22/16 16:305.5 5.0 1
Vanadium 2.9J ug/L 02/24/16 00:40 7440-62-202/22/16 16:3025.0 2.5 1
Zinc 13.1 ug/L 02/24/16 18:15 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 03:44 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 03:44 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 03:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 03:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 03:44 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 03:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 03:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 03:44 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 03:44 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 03:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 03:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 03:44 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 03:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 03:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 03:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 03:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 03:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 03:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 03:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 03:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 03:44 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 03:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 03:44 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 03:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 03:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 03:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 03:44 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 03:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 03:44 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW8 Lab ID: 92287200002 Collected: 02/17/16 12:57 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 03:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 03:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 03:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 03:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 03:44 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 03:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 03:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 03:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 03:44 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 03:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 03:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 03:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 03:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 03:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 03:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 03:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 03:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 03:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/23/16 03:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %02/23/16 03:44 17060-07-070-130 1
Toluene-d8 (S)100 %02/23/16 03:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW9 Lab ID: 92287200003 Collected: 02/18/16 12:13 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:18 7440-36-002/22/16 16:306.0 3.8 1
Arsenic 2.7J ug/L 02/24/16 18:18 7440-38-202/22/16 16:3010.0 2.5 1
Barium 76.1J ug/L 02/24/16 00:43 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:43 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:43 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:43 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:43 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:43 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:43 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:43 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:43 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:43 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:43 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:43 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:18 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 04:17 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 04:17 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 04:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 04:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 04:17 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 04:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 04:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 04:17 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 04:17 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 04:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 04:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 04:17 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 04:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 04:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 04:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 04:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 04:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 04:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 04:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 04:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 04:17 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 04:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 04:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 04:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 04:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 04:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 04:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 04:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 04:17 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW9 Lab ID: 92287200003 Collected: 02/18/16 12:13 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 04:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 04:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 04:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 04:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 04:17 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 04:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 04:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 04:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 04:17 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 04:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 04:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 04:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 04:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 04:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 04:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 04:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 04:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 04:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/23/16 04:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/23/16 04:17 17060-07-070-130 1
Toluene-d8 (S)101 %02/23/16 04:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW10 Lab ID: 92287200004 Collected: 02/18/16 12:08 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:21 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:21 7440-38-202/22/16 16:3010.0 2.5 1
Barium 54.2J ug/L 02/24/16 00:46 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:46 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:46 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:46 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:46 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:46 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:46 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:46 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:46 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:46 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:46 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:46 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:21 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 04:34 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 04:34 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 04:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 04:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 04:34 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 04:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 04:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 04:34 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 04:34 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 04:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 04:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 04:34 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 04:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 04:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 04:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 04:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 04:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 04:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 04:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 04:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 04:34 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 04:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 04:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 04:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 04:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 04:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 04:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 04:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 04:34 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW10 Lab ID: 92287200004 Collected: 02/18/16 12:08 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 04:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 04:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 04:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 04:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 04:34 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 04:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 04:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 04:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 04:34 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 04:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 04:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 04:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 04:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 04:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 04:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 04:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 04:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 04:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/23/16 04:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %02/23/16 04:34 17060-07-070-130 1
Toluene-d8 (S)100 %02/23/16 04:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW11 Lab ID: 92287200005 Collected: 02/18/16 11:18 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:24 7440-36-002/22/16 16:306.0 3.8 1
Arsenic 3.9J ug/L 02/24/16 18:24 7440-38-202/22/16 16:3010.0 2.5 1
Barium 31.8J ug/L 02/24/16 00:49 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:49 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:49 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:49 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:49 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:49 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:49 7439-92-102/22/16 16:3010.0 2.5 1
Nickel 2.9J ug/L 02/24/16 00:49 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:49 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:49 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:49 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:49 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:24 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 04:50 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 04:50 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 04:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 04:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 04:50 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 04:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 04:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 04:50 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 04:50 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 04:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 04:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 04:50 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 04:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 04:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 04:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 04:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 04:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 04:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 04:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 04:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 04:50 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 04:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 04:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 04:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 04:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 04:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 04:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 04:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 04:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-MW11 Lab ID: 92287200005 Collected: 02/18/16 11:18 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 04:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 04:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 04:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 04:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 04:50 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 04:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 04:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 04:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 04:50 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 04:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 04:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 04:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 04:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 04:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 04:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 04:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 04:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 04:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %02/23/16 04:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %02/23/16 04:50 17060-07-070-130 1
Toluene-d8 (S)102 %02/23/16 04:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-NES2S Lab ID: 92287200006 Collected: 02/18/16 11:34 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:27 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:27 7440-38-202/22/16 16:3010.0 2.5 1
Barium 28.6J ug/L 02/24/16 00:52 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:52 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:52 7440-43-902/22/16 16:301.0 0.50 1
Chromium 3.0J ug/L 02/24/16 00:52 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:52 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:52 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:52 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:52 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:52 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:52 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:52 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:52 7440-62-202/22/16 16:3025.0 2.5 1
Zinc 8.6J ug/L 02/24/16 18:27 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 05:07 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 05:07 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 05:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 05:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 05:07 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 05:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 05:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 05:07 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 05:07 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 05:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 05:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 05:07 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 05:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 05:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 05:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 05:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 05:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 05:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 05:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 05:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 05:07 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 05:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 05:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 05:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 05:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 05:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 05:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 05:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 05:07 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-NES2S Lab ID: 92287200006 Collected: 02/18/16 11:34 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 05:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 05:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 05:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 05:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 05:07 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 05:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 05:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 05:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 05:07 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 05:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 05:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 05:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 05:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 05:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 05:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 05:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 05:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 05:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %02/23/16 05:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/23/16 05:07 17060-07-070-130 1
Toluene-d8 (S)101 %02/23/16 05:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-SW3 Lab ID: 92287200007 Collected: 02/17/16 16:25 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:30 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:30 7440-38-202/22/16 16:3010.0 2.5 1
Barium 22.0J ug/L 02/24/16 00:55 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:55 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:55 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:55 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:55 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:55 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:55 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:55 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:55 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:55 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:55 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:55 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:30 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 05:23 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 05:23 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 05:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 05:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 05:23 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 05:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 05:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 05:23 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 05:23 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 05:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 05:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 05:23 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 05:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 05:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 05:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 05:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 05:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 05:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 05:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 05:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 05:23 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 05:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 05:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 05:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 05:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 05:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 05:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 05:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 05:23 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-SW3 Lab ID: 92287200007 Collected: 02/17/16 16:25 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 05:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 05:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 05:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 05:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 05:23 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 05:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 05:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 05:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 05:23 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 05:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 05:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 05:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 05:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 05:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 05:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 05:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 05:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 05:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/23/16 05:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %02/23/16 05:23 17060-07-070-130 1
Toluene-d8 (S)102 %02/23/16 05:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-SW4 Lab ID: 92287200008 Collected: 02/17/16 15:20 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:33 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:33 7440-38-202/22/16 16:3010.0 2.5 1
Barium 26.3J ug/L 02/24/16 00:59 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 00:59 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 00:59 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 00:59 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 00:59 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 00:59 7440-50-802/22/16 16:3010.0 2.5 1
Lead ND ug/L 02/24/16 00:59 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 00:59 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 00:59 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 00:59 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 00:59 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 00:59 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:33 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 05:40 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 05:40 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 05:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 05:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 05:40 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 05:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 05:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 05:40 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 05:40 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 05:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 05:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 05:40 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 05:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 05:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 05:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 05:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 05:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 05:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 05:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 05:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 05:40 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 05:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 05:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 05:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 05:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 05:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 05:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 05:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 05:40 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-SW4 Lab ID: 92287200008 Collected: 02/17/16 15:20 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 05:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 05:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 05:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 05:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 05:40 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 05:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 05:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 05:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 05:40 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 05:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 05:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 05:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 05:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 05:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 05:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 05:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 05:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 05:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %02/23/16 05:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %02/23/16 05:40 17060-07-070-130 1
Toluene-d8 (S)100 %02/23/16 05:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-Field Blank Lab ID: 92287200009 Collected: 02/18/16 12:50 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 02/24/16 18:36 7440-36-002/22/16 16:306.0 3.8 1
Arsenic ND ug/L 02/24/16 18:36 7440-38-202/22/16 16:3010.0 2.5 1
Barium ND ug/L 02/24/16 01:02 7440-39-302/22/16 16:30100 2.5 1
Beryllium ND ug/L 02/24/16 01:02 7440-41-702/22/16 16:301.0 0.50 1
Cadmium ND ug/L 02/24/16 01:02 7440-43-902/22/16 16:301.0 0.50 1
Chromium ND ug/L 02/24/16 01:02 7440-47-302/22/16 16:3010.0 2.5 1
Cobalt ND ug/L 02/24/16 01:02 7440-48-402/22/16 16:3010.0 2.5 1
Copper ND ug/L 02/24/16 01:02 7440-50-802/22/16 16:3010.0 2.5 1
Lead 2.7J ug/L 02/24/16 01:02 7439-92-102/22/16 16:3010.0 2.5 1
Nickel ND ug/L 02/24/16 01:02 7440-02-002/22/16 16:3050.0 2.5 1
Selenium ND ug/L 02/24/16 01:02 7782-49-202/22/16 16:3010.0 5.0 1
Silver ND ug/L 02/24/16 01:02 7440-22-402/22/16 16:3010.0 2.5 1
Thallium ND ug/L 02/24/16 01:02 7440-28-002/22/16 16:305.5 5.0 1
Vanadium ND ug/L 02/24/16 01:02 7440-62-202/22/16 16:3025.0 2.5 1
Zinc ND ug/L 02/24/16 18:36 7440-66-602/22/16 16:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 05:57 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 05:57 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 05:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 05:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 05:57 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 05:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 05:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 05:57 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 05:57 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 05:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 05:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 05:57 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 05:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 05:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 05:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 05:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 05:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 05:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 05:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 05:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 05:57 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 05:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 05:57 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 05:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 05:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 05:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 05:57 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 05:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 05:57 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-Field Blank Lab ID: 92287200009 Collected: 02/18/16 12:50 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 02/23/16 05:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 05:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 05:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 05:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 05:57 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 05:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 05:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 05:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 05:57 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 05:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 05:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 05:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 05:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 05:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 05:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 05:57 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 05:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/23/16 05:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/23/16 05:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %02/23/16 05:57 17060-07-070-130 1
Toluene-d8 (S)100 %02/23/16 05:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-Trip Blank Lab ID: 92287200010 Collected: 02/16/16 08:00 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/23/16 06:13 67-64-1100 10.0 1
Acrylonitrile ND ug/L 02/23/16 06:13 107-13-1200 1.9 1
Benzene ND ug/L 02/23/16 06:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/23/16 06:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/23/16 06:13 75-27-41.0 0.18 1
Bromoform ND ug/L 02/23/16 06:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/23/16 06:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/23/16 06:13 78-93-3100 0.96 1
Carbon disulfide ND ug/L 02/23/16 06:13 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 02/23/16 06:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/23/16 06:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/23/16 06:13 75-00-310.0 0.54 1
Chloroform ND ug/L 02/23/16 06:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/23/16 06:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/23/16 06:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/23/16 06:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/23/16 06:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/23/16 06:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/23/16 06:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/23/16 06:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/23/16 06:13 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 02/23/16 06:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/23/16 06:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/23/16 06:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/23/16 06:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/23/16 06:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/23/16 06:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/23/16 06:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/23/16 06:13 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/23/16 06:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/23/16 06:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/23/16 06:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/23/16 06:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/23/16 06:13 108-10-1100 0.33 1
Styrene ND ug/L 02/23/16 06:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/23/16 06:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/23/16 06:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/23/16 06:13 127-18-41.0 0.46 1
Toluene ND ug/L 02/23/16 06:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/23/16 06:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/23/16 06:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/23/16 06:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/23/16 06:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/23/16 06:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/23/16 06:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/23/16 06:13 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
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Page 24 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Sample: 3901-Trip Blank Lab ID: 92287200010 Collected: 02/16/16 08:00 Received: 02/19/16 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 02/23/16 06:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/23/16 06:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/23/16 06:13 17060-07-070-130 1
Toluene-d8 (S)101 %02/23/16 06:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20757
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92287200001, 92287200002, 92287200003, 92287200004, 92287200005, 92287200006, 92287200007,
92287200008, 92287200009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1670852
Associated Lab Samples: 92287200001, 92287200002, 92287200003, 92287200004, 92287200005, 92287200006, 92287200007,
92287200008, 92287200009
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 6.0 02/24/16 17:373.8
Arsenic ug/L ND 10.0 02/24/16 17:372.5
Barium ug/L ND 100 02/23/16 23:442.5
Beryllium ug/L ND 1.0 02/23/16 23:440.50
Cadmium ug/L ND 1.0 02/23/16 23:440.50
Chromium ug/L ND 10.0 02/23/16 23:442.5
Cobalt ug/L ND 10.0 02/23/16 23:442.5
Copper ug/L ND 10.0 02/23/16 23:442.5
Lead ug/L ND 10.0 02/23/16 23:442.5
Nickel ug/L ND 50.0 02/23/16 23:442.5
Selenium ug/L ND 10.0 02/23/16 23:445.0
Silver ug/L ND 10.0 02/23/16 23:442.5
Thallium ug/L ND 5.5 02/23/16 23:445.0
Vanadium ug/L ND 25.0 02/23/16 23:442.5
Zinc ug/L ND 10.0 02/24/16 17:375.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1670853LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 439500 88 80-120
Arsenic ug/L 498500 100 80-120
Barium ug/L 547500 109 80-120
Beryllium ug/L 527500 105 80-120
Cadmium ug/L 490500 98 80-120
Chromium ug/L 504500 101 80-120
Cobalt ug/L 469500 94 80-120
Copper ug/L 498500 100 80-120
Lead ug/L 472500 94 80-120
Nickel ug/L 491500 98 80-120
Selenium ug/L 471500 94 80-120
Silver ug/L 214250 86 80-120
Thallium ug/L 490500 98 80-120
Vanadium ug/L 520500 104 80-120
Zinc ug/L 490500 98 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
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Huntersville, NC 28078
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Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1670854MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92287261001
1670855
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 88 75-12588 0 255006.5 445 447
Arsenic ug/L 500 100 75-125101 1 25500ND502 508
Barium ug/L 500 87 75-12587 0 2550014901920 1920
Beryllium ug/L 500 100 75-125101 0 25500ND502 503
Cadmium ug/L 500 92 75-12592 0 25500ND462 459
Chromium ug/L 500 94 75-12595 1 25500ND475 478
Cobalt ug/L 500 83 75-12582 1 25500ND415 412
Copper ug/L 500 94 75-12594 0 25500ND472 471
Lead ug/L 500 84 75-12583 1 25500ND418 415
Nickel ug/L 500 86 75-12586 0 25500ND433 432
Selenium ug/L 500 87 75-12586 1 25500ND435 431
Silver ug/L 250 82 75-12582 0 25250ND206 207
Thallium ug/L 500 84 75-12586 2 255008.8 429 438
Vanadium ug/L 500 99 75-125100 1 25500ND497 501
Zinc ug/L 500 93 75-12594 1 2550014.6 482 485
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35665
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92287200001, 92287200002, 92287200003, 92287200004, 92287200005, 92287200006, 92287200007,
92287200008, 92287200009, 92287200010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1670820
Associated Lab Samples: 92287200001, 92287200002, 92287200003, 92287200004, 92287200005, 92287200006, 92287200007,
92287200008, 92287200009, 92287200010
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/23/16 01:480.33
1,1,1-Trichloroethane ug/L ND 1.0 02/23/16 01:480.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/23/16 01:480.40
1,1,2-Trichloroethane ug/L ND 1.0 02/23/16 01:480.29
1,1-Dichloroethane ug/L ND 5.0 02/23/16 01:480.32
1,1-Dichloroethene ug/L ND 5.0 02/23/16 01:480.56
1,2,3-Trichloropropane ug/L ND 1.0 02/23/16 01:480.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/23/16 01:482.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/23/16 01:480.27
1,2-Dichlorobenzene ug/L ND 5.0 02/23/16 01:480.30
1,2-Dichloroethane ug/L ND 1.0 02/23/16 01:480.24
1,2-Dichloropropane ug/L ND 1.0 02/23/16 01:480.27
1,4-Dichlorobenzene ug/L ND 1.0 02/23/16 01:480.33
2-Butanone (MEK)ug/L ND 100 02/23/16 01:480.96
2-Hexanone ug/L ND 50.0 02/23/16 01:480.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/23/16 01:480.33
Acetone ug/L ND 100 02/23/16 01:4810.0
Acrylonitrile ug/L ND 200 02/23/16 01:481.9
Benzene ug/L ND 1.0 02/23/16 01:480.25
Bromochloromethane ug/L ND 3.0 02/23/16 01:480.17
Bromodichloromethane ug/L ND 1.0 02/23/16 01:480.18
Bromoform ug/L ND 3.0 02/23/16 01:480.26
Bromomethane ug/L ND 10.0 02/23/16 01:480.29
Carbon disulfide ug/L ND 100 02/23/16 01:481.2
Carbon tetrachloride ug/L ND 1.0 02/23/16 01:480.25
Chlorobenzene ug/L ND 3.0 02/23/16 01:480.23
Chloroethane ug/L ND 10.0 02/23/16 01:480.54
Chloroform ug/L ND 5.0 02/23/16 01:480.14
Chloromethane ug/L ND 1.0 02/23/16 01:480.11
cis-1,2-Dichloroethene ug/L ND 5.0 02/23/16 01:480.19
cis-1,3-Dichloropropene ug/L ND 1.0 02/23/16 01:480.13
Dibromochloromethane ug/L ND 3.0 02/23/16 01:480.21
Dibromomethane ug/L ND 10.0 02/23/16 01:480.21
Ethylbenzene ug/L ND 1.0 02/23/16 01:480.30
Iodomethane ug/L ND 10.0 02/23/16 01:480.32
Methylene Chloride ug/L ND 1.0 02/23/16 01:480.97
Styrene ug/L ND 1.0 02/23/16 01:480.26
Tetrachloroethene ug/L ND 1.0 02/23/16 01:480.46
Toluene ug/L ND 1.0 02/23/16 01:480.26
trans-1,2-Dichloroethene ug/L ND 5.0 02/23/16 01:480.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1670820
Associated Lab Samples: 92287200001, 92287200002, 92287200003, 92287200004, 92287200005, 92287200006, 92287200007,
92287200008, 92287200009, 92287200010
Matrix: Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 02/23/16 01:480.26
trans-1,4-Dichloro-2-butene ug/L ND 100 02/23/16 01:481.0
Trichloroethene ug/L ND 1.0 02/23/16 01:480.47
Trichlorofluoromethane ug/L ND 1.0 02/23/16 01:480.20
Vinyl acetate ug/L ND 50.0 02/23/16 01:480.35
Vinyl chloride ug/L ND 1.0 02/23/16 01:480.62
Xylene (Total)ug/L ND 5.0 02/23/16 01:480.66
1,2-Dichloroethane-d4 (S)%90 70-130 02/23/16 01:48
4-Bromofluorobenzene (S)%99 70-130 02/23/16 01:48
Toluene-d8 (S)%101 70-130 02/23/16 01:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1670821LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.150 98 80-125
1,1,1-Trichloroethane ug/L 47.350 95 71-129
1,1,2,2-Tetrachloroethane ug/L 47.550 95 79-124
1,1,2-Trichloroethane ug/L 47.850 96 85-125
1,1-Dichloroethane ug/L 45.150 90 73-126
1,1-Dichloroethene ug/L 48.650 97 66-135
1,2,3-Trichloropropane ug/L 47.450 95 75-130
1,2-Dibromo-3-chloropropane ug/L 46.350 93 71-133
1,2-Dibromoethane (EDB)ug/L 49.950 100 83-124
1,2-Dichlorobenzene ug/L 46.750 93 80-133
1,2-Dichloroethane ug/L 43.250 86 67-128
1,2-Dichloropropane ug/L 46.850 94 75-132
1,4-Dichlorobenzene ug/L 48.050 96 78-130
2-Butanone (MEK)ug/L 88.3J100 88 61-144
2-Hexanone ug/L 92.7100 93 68-143
4-Methyl-2-pentanone (MIBK)ug/L 94.2J100 94 72-135
Acetone ug/L 83.6J100 84 48-146
Acrylonitrile ug/L 237250 95 40-160
Benzene ug/L 47.550 95 80-125
Bromochloromethane ug/L 49.050 98 71-125
Bromodichloromethane ug/L 48.850 98 78-124
Bromoform ug/L 51.250 102 71-128
Bromomethane ug/L 35.350 71 40-160
Carbon disulfide ug/L 51.0J50 102 50-160
Carbon tetrachloride ug/L 49.050 98 69-131
Chlorobenzene ug/L 47.150 94 81-122
Chloroethane ug/L 40.050 80 39-148
Chloroform ug/L 46.250 92 73-127
Chloromethane ug/L 37.150 74 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
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Huntersville, NC 28078
[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1670821LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 45.550 91 74-124
cis-1,3-Dichloropropene ug/L 50.050 100 72-132
Dibromochloromethane ug/L 50.450 101 78-125
Dibromomethane ug/L 51.050 102 82-120
Ethylbenzene ug/L 45.450 91 79-121
Iodomethane ug/L 86.2100 86 39-154
Methylene Chloride ug/L 47.250 94 64-133
Styrene ug/L 47.450 95 84-126
Tetrachloroethene ug/L 46.550 93 78-122
Toluene ug/L 47.150 94 80-121
trans-1,2-Dichloroethene ug/L 46.650 93 71-127
trans-1,3-Dichloropropene ug/L 49.850 100 69-141
trans-1,4-Dichloro-2-butene ug/L 46.8J50 94 40-160
Trichloroethene ug/L 48.350 97 78-122
Trichlorofluoromethane ug/L 46.250 92 53-137
Vinyl acetate ug/L 92.6100 93 40-160
Vinyl chloride ug/L 47.050 94 58-137
Xylene (Total)ug/L 135150 90 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1670822MATRIX SPIKE SAMPLE:
MSSpike
Result
92287200001
1,1,1,2-Tetrachloroethane ug/L 19.720 99 70-130ND
1,1,1-Trichloroethane ug/L 20.320 101 70-130ND
1,1,2,2-Tetrachloroethane ug/L 17.920 90 70-130ND
1,1,2-Trichloroethane ug/L 19.120 95 70-130ND
1,1-Dichloroethane ug/L 19.020 95 70-130ND
1,1-Dichloroethene ug/L 21.020 105 70-166ND
1,2,3-Trichloropropane ug/L 18.920 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.120 85 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130ND
1,2-Dichlorobenzene ug/L 18.620 93 70-130ND
1,2-Dichloroethane ug/L 17.120 86 70-130ND
1,2-Dichloropropane ug/L 19.320 96 70-130ND
1,4-Dichlorobenzene ug/L 19.020 95 70-130ND
2-Butanone (MEK)ug/L 31.7J40 79 70-130ND
2-Hexanone ug/L 35.7J40 89 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 36.7J40 92 70-130ND
Acetone ug/L 34.2J40 85 70-130ND
Acrylonitrile ug/L 84.6J100 85 70-130ND
Benzene ug/L 20.420 102 70-148ND
Bromochloromethane ug/L 19.420 97 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
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[phone]
Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1670822MATRIX SPIKE SAMPLE:
MSSpike
Result
92287200001
Bromodichloromethane ug/L 20.320 102 70-130ND
Bromoform ug/L 18.120 91 70-130ND
Bromomethane ug/L 13.3 M12067 70-130ND
Carbon disulfide ug/L 21.7J20 108 70-130ND
Carbon tetrachloride ug/L 21.120 105 70-130ND
Chlorobenzene ug/L 19.520 97 70-146ND
Chloroethane ug/L 19.220 96 70-130ND
Chloroform ug/L 19.320 96 70-130ND
Chloromethane ug/L 16.320 81 70-130ND
cis-1,2-Dichloroethene ug/L 19.120 96 70-130ND
cis-1,3-Dichloropropene ug/L 19.420 97 70-130ND
Dibromochloromethane ug/L 19.520 97 70-130ND
Dibromomethane ug/L 20.920 104 70-130ND
Ethylbenzene ug/L 19.120 96 70-130ND
Iodomethane ug/L 23.6 M14059 70-130ND
Methylene Chloride ug/L 17.320 86 70-130ND
Styrene ug/L 18.720 94 70-130ND
Tetrachloroethene ug/L 20.020 100 70-130ND
Toluene ug/L 19.920 100 70-155ND
trans-1,2-Dichloroethene ug/L 19.620 98 70-130ND
trans-1,3-Dichloropropene ug/L 18.920 95 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.3J M12066 70-130ND
Trichloroethene ug/L 20.320 102 69-151ND
Trichlorofluoromethane ug/L 20.320 101 70-130ND
Vinyl acetate ug/L 25.5J M14064 70-130ND
Vinyl chloride ug/L 20.320 102 70-130ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92287200002
1670823SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92287200002
1670823SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%92 191
4-Bromofluorobenzene (S)%103 3100
Toluene-d8 (S)%102 2100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92287200
Oxford Compliance Unit 2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92287200001 MPRP/20757 ICP/187103901-MW7 EPA 3010A EPA 6010
92287200002 MPRP/20757 ICP/187103901-MW8 EPA 3010A EPA 6010
92287200003 MPRP/20757 ICP/187103901-MW9 EPA 3010A EPA 6010
92287200004 MPRP/20757 ICP/187103901-MW10 EPA 3010A EPA 6010
92287200005 MPRP/20757 ICP/187103901-MW11 EPA 3010A EPA 6010
92287200006 MPRP/20757 ICP/187103901-NES2S EPA 3010A EPA 6010
92287200007 MPRP/20757 ICP/187103901-SW3 EPA 3010A EPA 6010
92287200008 MPRP/20757 ICP/187103901-SW4 EPA 3010A EPA 6010
92287200009 MPRP/20757 ICP/187103901-Field Blank EPA 3010A EPA 6010
92287200001 MSV/356653901-MW7 EPA 8260
92287200002 MSV/356653901-MW8 EPA 8260
92287200003 MSV/356653901-MW9 EPA 8260
92287200004 MSV/356653901-MW10 EPA 8260
92287200005 MSV/356653901-MW11 EPA 8260
92287200006 MSV/356653901-NES2S EPA 8260
92287200007 MSV/356653901-SW3 EPA 8260
92287200008 MSV/356653901-SW4 EPA 8260
92287200009 MSV/356653901-Field Blank EPA 8260
92287200010 MSV/356653901-Trip Blank EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/25/2016 12:13 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 36
Page 35 of 36
Page 36 of 36

Appendix C

Historical Detected Groundwater Constituents

APPENDIX C: HISTORICAL DETECTED GROUNDWATER CONSTITUENTS
Analyte
Sample Collection
Date RL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Blanks
Inorganics
Arsenic 3/12/2015 10.0 4.2 J ND ND ND ND ND ND
NC 2L = 10 µg/L 8/18/2015 10.0 ND ND ND ND ND ND ND
2/18/2016 10.0 ND ND 2.7 J ND 3.9 J ND ND
Barium 13-Jun-12 100 9.2 J 36.8 J 59.2 J 48.2 J 30.6 J 31.4 J ND
22-Aug-12 100 ND 37.3 J 60.9 J 58.9 J 85 J 28.2 J ND
25-Sep-12 100 10.3 J 40.8 J 64.2 J 72.7 J 43.8 J 30.5 J ND
NC 2L = 700 µg/L 17-Oct-12 100 24.2 J 57.3 J 65.1 J 48.7 J 110 28 J ND
6-Aug-13 100 ND 37.1 J 66.5 J 36.8 J 28.5 J 24.8 J ND
25-Feb-14 100 ND 43.6 J 65 J 41.1 J 20.3 J 58.6 J ND
13-Aug-14 100 6.2 J 52.7 J 72.7 J 40.7 J 19.7 J 21.7 J ND
12-Mar-15 100 9.8 J 47.9 J 76.3 J 49.1 J 19.1 J 35.5 J ND
18-Aug-15 100 11.0 J 45.6 J 72.1 J 43.5 J 20.5 J 31.3 J ND
18-Feb-16 100 14.8 J 59.5 J 76.1 J 54.2 J 31.8 J 28.6 J ND
Chromium 13-Jun-12 10.0 ND ND ND 10.9 ND ND ND
22-Aug-12 10.0 ND ND ND 10.4 18.3 ND ND
25-Sep-12 10.0 ND ND ND 10.3 ND ND ND
NC 2L = 10 µg/L 17-Oct-12 10.0 ND ND ND 15.8 20.9 ND ND
6-Aug-13 10.0 ND ND ND ND ND ND ND
25-Feb-14 10.0 ND ND ND ND ND ND ND
13-Aug-14 10.0 ND ND ND 5.1 J ND ND ND
12-Mar-15 10.0 ND 3.0 J ND ND ND ND ND
18-Aug-15 10.0 ND ND ND ND ND ND ND
18-Feb-16 10.0 ND ND ND ND ND 3.00 J ND
Cobalt 13-Jun-12 10.0 ND ND ND ND ND ND ND
22-Aug-12 10.0 ND ND ND ND ND ND ND
25-Sep-12 10.0 ND ND ND ND ND ND ND
GWPS = 1 µg/L 17-Oct-12 10.0 10.3 ND ND ND 12.4 ND ND
6-Aug-13 10.0 ND ND ND ND ND ND ND
25-Feb-14 10.0 ND ND ND ND ND ND ND
13-Aug-14 10.0 ND ND ND ND ND ND ND
12-Mar-15 10.0 ND ND ND ND ND 3.6 J ND
18-Aug-15 10.0 ND ND ND ND ND ND ND
18-Feb-16 10.0 ND ND ND ND ND ND ND
Copper 13-Jun-12 10.0 ND ND ND 46 ND ND ND
22-Aug-12 10.0 ND ND ND 56.2 19.8 ND ND
25-Sep-12 10.0 7.4 J ND ND 63.6 5.7 J ND ND
NC 2L = 1,000 µg/L 17-Oct-12 10.0 19.9 7.6 J ND 35.5 23.1 ND ND
6-Aug-13 10.0 ND ND ND ND ND ND ND
25-Feb-14 10.0 ND ND ND 7.9 J ND ND ND
13-Aug-14 10.0 ND 11.6 ND 13.4 ND ND ND
12-Mar-15 10.0 ND 47.0 ND 6.0 J ND 3.3 J ND
18-Aug-15 10.0 2.8 J 26.6 ND 12.3 ND 4.3 J ND
18-Feb-16 10.0 ND 7.8 J ND ND ND ND ND
Nickel 13-Jun-12 50.0 ND ND ND ND ND ND ND
22-Aug-12 50.0 ND ND ND ND 6.1 J ND ND
25-Sep-12 50.0 ND ND ND ND ND ND ND
NC 2L = 100 µg/L 17-Oct-12 50.0 ND ND ND 6.9 J 8.9 J ND ND
6-Aug-13 50.0 ND ND ND ND ND ND ND
25-Feb-14 50.0 ND ND ND ND ND ND ND
13-Aug-14 50.0 ND ND ND ND ND ND ND
12-Mar-15 50.0 ND ND ND ND ND ND ND
18-Aug-15 50.0 ND ND ND ND 2.7 J ND ND
18-Feb-16 50.0 ND ND ND ND 2.9 J ND ND
Thallium 13-Jun-12 5.5 ND ND ND ND ND ND ND
22-Aug-12 5.5 ND 6.8 6.8 ND ND ND ND
25-Sep-12 5.5 ND ND ND ND ND ND ND
GWPS = 0.28 µg/L 17-Oct-12 5.5 ND ND ND ND ND ND ND
6-Aug-13 5.5 ND ND ND ND ND ND ND
25-Feb-14 5.5 ND ND ND ND ND ND ND
13-Aug-14 5.5 ND ND ND ND ND ND ND
12-Mar-15 5.5 ND ND ND ND ND ND ND
18-Aug-15 5.5 ND ND ND ND ND ND ND
18-Feb-16 5.5 ND ND ND ND ND ND ND
Granville Co. - Oxford Landfill, Unit 2
Permit No. 3901-MSWLF-2012 Page 1 of 2 Joyce Engineering
APPENDIX C: HISTORICAL DETECTED GROUNDWATER CONSTITUENTS
Analyte
Sample Collection
Date RL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Blanks
Vanadium 13-Jun-12 25.0 5.2 J ND ND 27.8 17.3 J 11 J ND
22-Aug-12 25.0 ND ND ND 30.2 69.5 9 J ND
25-Sep-12 25.0 8.3 J ND ND 33.4 16.5 J 8.2 J ND
GWPS = 0.3 µg/L 17-Oct-12 25.0 29.7 ND ND 19.5 J 63.8 6.2 J ND
6-Aug-13 25.0 ND ND ND ND 9.2 J ND ND
25-Feb-14 25.0 ND ND ND 10.2 J ND ND ND
13-Aug-14 25.0 ND ND ND 11.8 J ND ND ND
12-Mar-15 25.0 ND 4.4 J 7.3 J 5.0 J ND 6.7 J ND
18-Aug-15 25.0 6.1 J ND ND 6.5 J 3.6 J 9.1 J ND
18-Feb-16 25.0 ND 2.9 J ND ND ND ND ND
Zinc 13-Jun-12 10.0 ND ND ND 10.5 ND ND ND
22-Aug-12 10.0 ND ND 32 31 21.9 10.6 ND
25-Sep-12 10.0 11.7 ND ND 14.8 ND ND ND
NC 2L = 1,000 µg/L 17-Oct-12 10.0 32.5 ND ND 10.5 29 ND ND
6-Aug-13 10.0 ND ND ND ND ND ND ND
25-Feb-14 10.0 ND ND ND ND ND ND ND
13-Aug-14 10.0 ND ND ND ND ND ND ND
12-Mar-15 10.0 9.8 B 10.9 B 10.7 B 8.7 B 7.8 B 9.9 B 6.1 J
18-Aug-15 10.0 8.9 B ND ND ND ND 5.2 B 11.5 J
18-Feb-16 10.0 ND 13.1 ND ND ND 8.6 J ND
ORGANICS
cis-1,2-Dichloroethene
NC 2L = 70 µg/L * >18-Aug-15 5.0 0.71 J 0.36 J ND ND ND ND ND
18-Feb-16 5.0 ND ND ND ND ND ND ND
Trichlorofluoromethane 13-Jun-12 1.0 ND ND ND ND 0.8 B 0.85 B 0.74 J
22-Aug-12 1.0 ND ND ND ND ND ND ND
NC 2L = 2,000 µg/L 25-Sep-12 1.0 ND ND ND ND ND ND ND
17-Oct-12 1.0 ND ND ND ND ND ND ND
6-Aug-13 1.0 ND ND ND ND ND ND ND
25-Feb-14 1.0 ND ND ND ND ND ND ND
13-Aug-14 2.0 ND ND ND ND ND ND ND
12-Mar-15 1.0 ND ND ND ND ND ND ND
18-Aug-15 1.0 ND ND ND ND ND ND ND
18-Feb-16 1.0 ND ND ND ND ND ND ND
Notes:
All concentrations are in micrograms per liter (µg/L).
RL = Reporting Limit (SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank-qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NC 2L = North Carolina Groundwater Standards from 15A NCAC 2L.0202.
GWPS = Groundwater Protection Standards established by the DENR Solid Waste Section (SWS).
When the NC 2L has not been established, the GWPS will be used.
Bold values for groundwater are above the NC 2L Standards or GWPS.
--- = Well was not monitored and/or not reported.
* Detections of c-1,2-DCE in MW-7 and MW-8 in August 2015 are suspect. The sample collected from MW-7 at the same time for Unit 1 showed no detected c-1,2-DCE.
Granville Co. - Oxford Landfill, Unit 2
Permit No. 3901-MSWLF-2012 Page 2 of 2 Joyce Engineering

Appendix D

Historical Detected Surface Water Constituents

APPENDIX D: HISTORICAL DETECTED SURFACEWATER CONSTITUENTS
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Inorganics
Arsenic 12-Mar-15 2.5 10.0 4.9 J 2.7 J ND ND ND
NC 2B = 50 (05/01/07)19-Aug-15 2.5 10.0 ND Dry ND ND ND
18-Feb-16 2.5 10.0 ND ND ND ND ND
Barium 13-Aug-14 5.0 100 47.4 J 43.9 J 22.1 J 33.9 J ND
12-Mar-15 2.5 100 28.5 J 42 J 22.5 J 24.6 J ND
NC 2B = NE (05/01/07)19-Aug-15 2.5 100 37 J Dry 23.9 J 32.7 J ND
18-Feb-16 2.5 100 58.2 J 55.0 J 22.0 J 26.3 J ND
Chromium 13-Aug-14 5.00 10.0 10.8 10 J ND ND ND
12-Mar-15 2.50 10.0 4.0 J 3.1 J ND 2.6 J ND
NC 2B = 50 µg/L (05/01/07)19-Aug-15 2.50 10.0 ND Dry ND ND ND
18-Feb-16 2.50 10.0 ND ND ND ND ND
Copper 13-Aug-14 5.00 10.0 9.6 J 7.7 J ND ND ND
12-Mar-15 2.50 10.0 3.1 J 2.6 J ND ND ND
NC 2B = 7 µg/L (05/01/07)19-Aug-15 2.50 10.0 ND Dry ND ND ND
18-Feb-16 2.50 10.0 6.3 J 5.7 J ND ND ND
Nickel 13-Aug-14 5.00 50.0 7.5 J 5.4 J ND ND ND
12-Mar-15 2.50 50.0 3 J 2.8 J ND ND ND
NC 2B = 88 µg/L (05/01/07)19-Aug-15 2.50 50.0 ND Dry ND ND ND
18-Feb-16 2.50 50.0 3.3 J 3.0 J ND ND ND
Lead 18-Feb-16 2.50 10.0 4.0 B 2.6 B ND ND 2.7 J
NC 2B = 25 (05/01/07)
Vanadium 13-Aug-14 5.00 25.0 18.0 J 18.2 J ND 9.3 J ND
12-Mar-15 2.50 25.0 7.8 J 8.3 J 3.1 J 6.3 J ND
NC 2B = NE (05/01/07)19-Aug-15 2.50 25.0 2.8 J Dry 2.7 J 4.3 J ND
18-Feb-16 2.50 25.0 6.4 J 6.1 J ND ND ND
Zinc 13-Aug-14 5.00 10.0 14.3 ND ND ND ND
12-Mar-15 5.00 10.0 62.3 11.6 B 8.5 B 10.8 B 6.1 J
NC 2B = 50 µg/L (05/01/07)19-Aug-15 5.00 10.0 ND Dry ND ND 11.5 J
18-Feb-16 5.00 10.0 13.0 11.0 ND ND ND
Notes:
All concentrations are in micrograms per liter (µg/L).
RL = Reporting Limit (SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank-qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NS = Not sampled.
NR = Not Reported.
Dry =Surface water point considered to be dry.
NC 2B = North Carolina Surface Water Standards from 15A NCAC 2B.
NE = Not established.
Bold values for surface water are above the NC 2B.
Surface waters are classified as fresh-water aquatic life.
Granville Co. - Oxford Landfill, Unit 2
Permit No. 3901-MSWLF-2012 Joyce Engineering