0201_AlexanderCoMSWLF_GWMR_DIN27738_20170107

Alexander County Active C&D and Closed MSWLF
Taylorsville, North Carolina
July 2016
MESCO Project Number: G16003.0
Semi-Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
Permit Number: 02-01
P.O. Box 97
Garner, NC 27529
P.E. License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 3
Groundwater Samples Page 3
Surface Water Samples Page 3
Groundwater and Surface Water Characterization Page 3
Corrective Action Update Page 4
MNA Analysis (AOCs MW-16, MW-24, MW-26) Page 3
Phytoremediation (AOC MW-24) Page 4
Enhanced Bioremediation via Substrate Injection (AOC MW-26) Page 4
Landfill Gas Extraction (AOC MW-1B) Page 5
Findings Page 5
Closing Page 6
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards Figure 2
Total VOCs and Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26 Figure 3
Histograms of Dissolved Methane Concentrations Figure 4
Histograms of Total VOC Concentrations Figure 5
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections in Water Samples Above SWSL, GWP, 2L, 2B or MCL (Appendix I) Table 5
Detections in Water Samples Above MDL (Appendix II Exclusive) Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
MNA Parameter Data Summary Table 8
Phytoremediation Tree Measurement Summary Table 9
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
January 16, 2017Ms. Jaclynne DrummondSolid Waste Section (SWS)Division of Waste Management/ NCDEQ2090 US Highway 70 Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update Alexander County Active C&D and Closed MSWLF Permit No. 02-01 MESCO Project No. G16003.0 Event Date(s): July 1, 5-6 and September 22, 2016
Introduction
On behalf of Alexander County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to
present this Semi-Annual Water Quality Monitoring Report with Corrective Action Update for events
performed at the Alexander County active construction and demolition (C&D) and closed municipal
solid waste landfill (MSWLF) on July 1, 5-6 and September 22, 2016. A small number of samples were
collected during the additional September event since the laboratory failed to report the results from the
July event. NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Alexander County provide
this report to the NC Solid Waste Section (SWS) on a semi-annual basis. Laboratory analytical results,
which included targeting Appendix II constituents, indicate one or more volatile organic compounds
(VOCs) continue to persist at levels above the 2L Standard in samples collected from 9 wells that monitor
the uppermost aquifer but concentrations continue to decrease over time and distance. Surface water
samples did not contain contaminant concentrations in excess of the 2B Surface Water Standard.
Corrective action to remediate VOCs in groundwater is ongoing within the four areas of concern (AOC)
with updated information presented herein.
Background
The Alexander County active C&D and closed MSWLF, is located at 2500 Paynes Dairy Road near
Taylorsville North Carolina. The total waste footprint encompasses approximately 24 acres situated on
283 contiguous acres. The site location topographic map is depicted in the attached Figure 1.
The closed MSWLF ceased operation prior to 1998 and the C&D landfill continues operation owo
Assessment and Corrective Action (ACM) reports dated August 27, 2002 and April 11, 2008. MESCO
then developed a Corrective Action Plan-Revision 1 (CAP-Rev 1) on February 6, 2009. In response to
improved water quality and changing geochemical conditions the originally selected remediation
approach was amended by MESCO in a Corrective Action Plan-Addendum (CAP-Add) dated December
20, 2010. Groundwater remediation efforts have been implemented at the four distinct areas of concern
(AOCs) which are identified as MW-1B, MW-16, MW-24 and MW-26. Remediation technologies
initiated to date with reference to their respective AOC include monitored natural attenuation (MNA)
(MW-16, MW-24, MW-26), phytoremediation (MW-24), enhanced bioremediation via substrate injection
(MW-26) and landfill gas (LFG) extraction (MW-1B). Following establishment of the two year MNA
baseline MESCO completed a Corrective Action Evaluation Report (CAER) (DIN 13596) on March 22,
2011. Based on improved water quality conditions as demonstrated in the CAER the parameters and
frequencies of future monitoring events were established by the SWS CAER review response (DIN
14150) dated June 16, 2011.
A second CAP-Add was submitted by MESCO dated May 30, 2013 as requested by the SWS in a letter

entitled Compliance Boundary (Relevant Point of Compliance) (DIN 18502) dated February 18, 2013. A
Request for Appendix II Groundwater Monitoring Modification (DIN 20137) was submitted by MESCO
dated November 8, 2013 which was subsequently approved by the SWS (DIN 20144) on November 13,
2013.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, corrective action
update, ground/surface water characterization, and findings. Well construction summary table, field
observations table, field parameter data table, sampling and analysis summary table, detections compared
to Standards tables, a groundwater flow directions/rates table, potentiometric map, time-series graph,
quality assurance/quality control data, and laboratory analytical data results are enclosed herein.
Sampling Procedures
MESCO personnel performed this sampling event following the parameters and frequency established by
the SWS review response to the (CAER) (Doc ID 14150) dated June 16, 2011 and the SWS approved
Request for Appendix II Groundwater Monitoring Modification (DIN 20137). The water quality
monitoring program includes a combination of detection, assessment and corrective action monitoring
with specifically defined analysis.
Water samples were collected from all monitoring locations outlined in the CAP-Add and CAER with the
exception of MW-1A; which has been chronically dry and MW-7 which is exempt during the summer
event. Monitoring locations are depicted on the potentiometric map (Figure 2).
Sampling was performed per the protocols outlined in the Groundwater and Surface Water Sampling and
Analysis Plan included as Appendix B of the approved CAP-Add. A summary detailing the construction of
the water monitoring wells is presented on Table 1. The function and integrity of all monitoring locations
were visually evaluated with deficiencies rectified as documented on Table 2. The depth to water in each
well was electronically gaged prior to purging to quantify the static water level elevation. Submersible
pumping or bailing was utilized to purge the wells a minimum of three times the volume of standing water
in the well or until dry. Surface water samples were collected from previously designated locations along
discharge features. During well purging and surface water sample collection the required field parameters
were recorded. The samples were then placed into laboratory-prepared, pre-preserved containers via a new
disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-certified
laboratory under proper chain of custody (C-O-C) protocols and within the specified hold times for each
analysis.
Field Parameter Data
Field parameters were recorded including depth to water, pH, specific conductance, temperature, dissolved
oxygen (DO), oxidation reduction potential (ORP) and turbidity. A summary of the field parameter data is
presented in Table 3 and the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Services Inc. (PACE) of Huntersville/Asheville, NC performed the laboratory analyses.
All water samples were tested for at least the constituents listed in 40CFR258 Appendix I. Assessment
monitoring (full suite of constituents listed in 40CFR258 Appendix II) was performed on a subset
consisting of 11 wells (MW-1, MW-1B, MW-2, MW-4R, MW-5, MW-9, MW-11, MW-12, MW-16,
MW-26 and background well MW-18) as previously approved. Corrective action monitoring (Appendix I
or II plus a subset of MNA parameters previously approved by SWS) was also performed on 9 wells
(MW-3, MW-5, MW-6, MW-11, MW-12, MW-12D, MW-24, MW-26 and MW-31). Additionally;
supplemental samples MW-1 and MW-1B were analyzed for dissolved methane to assess remediation
progress. Quality control measures implemented during this event included submittal and subsequent
quantification of equipment (EB), field (FB), and travel (TB) blanks. A sampling and analysis table
summarizing the locations, laboratory, target analytes and methods is presented as Table 4. Laboratory
results and C-O-Cs are presented in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at
2
or below the current Solid Waste Section Limit (SWSL). Table 5 summarizes App I constituents detected
in groundwater and surface water samples that attain or were above the current SWSL, Groundwater
Protection Standards (GWP), North Carolina Groundwater Standards (2L), the applicable North Carolina
Surface Water Standards (2B) for a class C waterbody and Maximum Contaminant Levels (MCL) also
known as “Federal Primary Drinking Water Standards”. Table 6 shows the Appendix II exclusive
(defined in this report as not also listed in Appendix I) constituents detected above the MDL.
Quality Control Samples
No constituents were detected above the SWSL in any of the quality control blanks (EB, FB or TB). Low
(“j-qualified”) levels of cyanide were detected in every sample collected in July 2016 and was also
detected in their respective associated laboratory method blank, therefore, the detections are believed to be
false positives.
Groundwater Samples
The number of metal detections and concentrations were significantly elevated compared to previous
events. Total metals detected above their respective 2L/GWP Standard included arsenic (MW-14),
cadmium (MW-2), chromium (MW-5, MW-11, MW-13, MW-17), cobalt (MW-1B, MW-2, MW-4R, MW-
9, MW-11, MW-14, MW-16), mercury (MW-1B), thallium (MW-2, MW-9, MW-11) and vanadium (MW-
1, MW-5, MW-13, MW-14, MW-17, MW-21, MW-22, MW-23, MW-24, MW-25, MW-31, MW-32, MW-
34). The upgradient background well MW-18 also contained levels of chromium, thallium and vanadium
above their respective GWP/2L Standard.
The VOCs detected in concentrations which exceeds their respective 2L Standard during this event were:
Benzene ranging from (1.1 – 5.3 µg/L) at (MW-1, MW-3, MW-4R, MW-5, MW-11, MW-12, MW-15,
MW-16 and MW-26) above the 2L of 1.0 µg/L.
Para-dichlorobenzene at MW-3 (7.1 µg/L) and MW-11 (7.8 µg/L) which is above the 2L (6.0 µg/L).
Tetrachloroethene at MW-16 (1.3 µg/L) which is above the 2L (0.7 µg/L).
1,2-dichlroethane at MW-3 (0.47 µg/L) and MW-16 (0.45 µg/L) which is above the 2L (0.4 µg/L) but
below the SWSL (1.0 µg/L) thus “j-qualified”.
Sample MW-16 also contained 1,1-dichloroethane (8.7 µg/L) and 1,2-dichloropropane (0.89 µg/L) which
is above their respective Standards (6.0 µg/L and 0.6 µg/L).
A site map depicting the spatial distribution of VOC concentrations exceeding the 2L Standard during this
sampling event is shown in Figure 2.
Surface Water Samples
None of the targeted constituents were detected in any surface water sample in levels above the NC 2B
Surface Water Standards.
Groundwater and Surface Water Characterization
At the landfill, groundwater flow direction generally mirrors topography, thus flow direction is from higher
to lower elevations as shown on the potentiometric map included as Figure 2. Locally, groundwater flow is
expected to be generally westerly toward the Lower Little River, and southerly toward the Catawba River
(Figure 1). Groundwater linear velocity rates calculated using modified Darcy's equation varied greatly
and were slower in the upper bedrock fracture system than the less prominent regolith (Table 7). Streams
at designated monitoring points were visually observed to be of normal seasonal volume, flow rate and low
turbidity. Hydrogeologic parameters appear generally consistent with historical observations.
3
Corrective Action Update
Groundwater remediation continues to be implemented at the four AOCs designated in the CAP-Add.
Groundwater remediation per the CAP-Add is expected to continue until the SWS authorizes a change. General
background information and activities performed since the CAER and last semi-annual event are briefly
presented in the following sections.
MNA Analysis (AOCs MW-16, MW-24, MW-26)
Semi-annual MNA monitoring of 14 wells for the full suite of SWS recommended parameters was initiated
on June 30, 2009 and performed for four consecutive semi-annual events to establish a baseline per the
CAP-Revision 1. The number of wells requiring MNA analysis was reduced to 10 and the parameters and
frequency were also amended per the SWS CAER review response (DIN 14150) dated June 16, 2011.
Establishment of the MNA baseline concluded in December 2012 at MW-33 and MW-34. MNA data
collected during this period is presented on Table 8.
Following the acquisition of a 15.7 acre parcel from Crescent Resources on March 3, 2011, extension of
the eastern relative point of compliance downgradient of AOC MW-16 has been approved with conditions
by the SWS on February 18, 2013 (DIN:18502). Recordation of Survey Plat titled Survey For Notice of
Contaminated Site Alexander County Landfill and A Notice and SWS approved Declaration of Perpetual
Land Use Restrictions for this parcel has remained at the Alexander County Register of Deeds Office since
November 13, 2012. The SWS approved CAP-Add dated May 30, 2013 clarifies that groundwater
remediation of AOC MW-16 will remain as only MNA, rather than any other technologies described in the
preceding CAP-Add.
Phytoremediation (AOC MW-24)
County personnel planted about 200 hybrid poplar trees over an approximate one acre area between MW-7
and MW-12 in May 2010 in an effort to phytoremediate groundwater in the MW-24 AOC. The County
continued to maintain the fence-enclosed stand during this semi-annual period which included continuous
supplemental watering and eradication of competing vegetation. MESCO personnel continued quarterly
tree growth monitoring by recording measurements of ten designated sample trees on March 25, 2016 and
August 1, 2016. The trees were dormant but had buds in March. The foliage appeared healthy with slight
yellowing over the summer. Standing water was not observed within the premeditation area on either
visit. The average tree has grown considerably (245” or 645%) over the past 5+ years (Table 9 and
Figure 3).
MESCO personnel deployed dedicated pressure transducers in MW-7 and MW-12 on August 12, 2010 to
record daily water levels. Groundwater level fluctuations were downloaded and transducers re-zeroed on
August 1, 2016 and September 22, 2016. In addition, daily precipitation amounts are periodically
obtained from the National Weather Services Cooperative Observer Program Station 318519 database.
Data continues to suggest both MW-7 and MW-12 water level variations mirror each other and both
respond quickly to precipitation events. Total cumulative VOC concentrations in AOC MW-24 during
this event have have decreased 63% compared to its respective 2 year baseline established in 2010 and
statistical trend analysis indicates that an increasing trend is not evident. The phytoremediation zone has
not been established long enough to make a valid assessment of the effectiveness as a remediation
measure. The phytoremediation area will continue to be maintained and monitored on a quarterly basis.
Enhanced Bioremediation via Substrate Injection (AOC MW-26)
In an attempt to remediate benzene as detected in MW-26, Bac-9 was injected 50 ft upgradient in IW-1 on
February 17, 2011 following conditions in the Underground Injection Control (UIC) Permit WI0300160.
The UIC permit was renewed on January 31, 2013 and as directed by the UIC post-injection water quality
monitoring of MW-3, MW-11, MW-26, MW-27 and MW-31 is required on a semi-annual basis.
Benzene was detected above the 2L Standard in a sample collected from MW-26 after being below 6
months ago. Contaminants remain absent from MW-31 located along MW-26 flow path beyond the
compliance boundary. Most recent levels of total VOCs compared to the baseline established during the
four events prior to injection exhibited a reduction both upgradient (-31%) and downgradient (-42%) of the
4
injection point. Most recently, total cumulative VOCs from all samples in AOC MW-26 decreased 42%
and benzene concentrations decreased 26% compared to the baseline averages established during the four
events performed over the two years preceding the injection (Figure 3). Further injections are not planned
at this time.
Landfill Gas Extraction (AOC MW-1B)
Three LFG extraction wells (MEW-1, MEW-2, MEW-3) were installed screening the majority of the
vadose zone at the northern border of the closed landfill in the vicinity of the scalehouse. MEW-1 was
installed on August 17, 2010 with MEW-2 and MEW-3 installed on October 20, 2010. Well control heads
were plumbed to a header pipe by the County which was connected to a soil vacuum extraction (SVE) unit
on July 5, 2012. An active LFG blower system pilot study was performed by MESCO between June 14,
2012 and July 12, 2012 to evaluate the effectiveness a vacuum would have on reducing levels of LFG in
the soil which may remediate the low level VOCs detected in groundwater hydraulically upgradient of the
landfill. A comparison of LFG concentrations and pressures before and after vacuum start-up indicated the
system is capable of eliminating LFG migration at all locations monitored within AOC MW-1B. The
active LFG Collection Control System (LFGCCS) has been in continuous operation since November 1,
2012 and been verified and documented by MESCO personnel on at least a quarterly basis to be
eliminating LFG migration through the vadose at all locations monitored beyond the extraction wells.
Improvement in groundwater quality has also been observed in response to implementation of the LFG
extraction system. Dissolved methane levels in groundwater have decreased considerably within MW-1 (-
99%) and MW-1B (-82%) in the 3.5+ years of operation (Figure 4). During this event total cumulative
VOC concentrations within AOC MW-1B have also exhibited a significant reduction (-88%) and exhibited
a statistically significant decreasing trend compared to the baseline established prior to initiation of
remediation via LFG extraction (Figure 5). Levels of benzene have remained below 2L Standards at MW-
1B for three consecutive events following consistent detections the previous 13 years. The LFGCCS is
planned to continue operation and will continue to be monitored and assessed on a quarterly basis.
Findings
The proliferation of metals detected during this event is very inconsistent with historical events. During
this event there were 35 instances of metal exceedances compared to only 1 during the previous event.
The source of metals is believed to be a product of erosion of natural deposits and not anthropogenic.
The semi-annual laboratory results indicate that low level (<24.4 µg/L) dissolved phase VOCs, consisting
primarily of benzene and a few chlorinated solvents, continue to be detected in groundwater samples
collected within 270 feet of the waste boundary. All constituents detected during this event remain within
their own respective historically identified range. Very few Appendix II exclusive parameters were
detected with mercury in sample MW-1B being the only constituent found above the 2L Standard. Total
VOC concentrations continue to not exhibit an increasing trend over time site-wide and in each of the
AOCs (Figure 6). Statistical Sen's Slope trend analysis performed at both a 90% and 95% confidence
interval indicates a downward trend of total VOC concentrations at AOC MW-1B, AOC MW-26 and
cumulative of all wells site-wide since corrective action was initiated. (Figure 6). The same statistical
analysis indicates no trend at AOC MW-16 or AOC MW-24. Total VOC concentrations during this event,
compared to their own respective averages calculated during the two year baseline period (ended in 2010),
indicate a reduction site-wide (-38%), AOC MW-1B (-88%), AOC MW-24 (-63%), AOC MW-26 (-34%),
aggregate of all other wells not located within designated remediation areas (-40%) and a slight increase of
(1%) in AOC MW-16 (Figure 6).
Laboratory data continues to indicate that all surface water samples remain unimpacted.
Evaluation of the most current water quality data continues to support assertions drawn in previous reports.
VOCs persist in the upper portion of the aquifer but concentrations continue to decrease over time and
distance away from the landfill. MNA data and previous screening models indicate that the plumes within
each AOC are stabilizing and/or decreasing and there is evidence that natural attenuation is ongoing at the
facility. Implementation of the corrective action measures coupled with natural attenuation is expected to
decrease VOC concentrations in groundwater over time.
5
Figures
Topographic Map with Site Location
FIGURE 1
QUADRANGLE LEGEND
Alexander County Active C&D and Closed MSWLF
1/20 1 MILE
LANDFILL PROPERTY
N
2500 Paynes Dairy Road
Taylorsville, NC 28681
Lat:35-15-18.7246
Long:-81-08-51.51.32
Northing:767009.09
Easting:1363506.43
IW-1MW-24
MW-25
MW-26
MW-27
MW-21
MW-23
MW-20
MW-22
MW-5Benzene 3.3 ug/l
MW-1Benzene - 1.1 ug/l
MW-16
Benzene - 2.9 ug/l
Tetrachloroethene - 1.3 ug/l
1,1-Dichloroethane - 8.7 ug/l1,2-Dichloroethane - 0.45(j)
1,8-Dichloropropane - 0.89(j)
MW-31,4-Dichlorobenzene - 7.1 ug/l
Benzene - 5.3 ug/l
1,2-Dichloroethane - 0.47(j)
MW-11
Benzene - 3.0 ug/l
1,4-Dichlorobenzene - 7.8 ug/l
MW-12
Benzene - 1.1 ug/l
MW-15
Benzene - 3.8 ug/l
July 1, 2016
WELL #
15A NCAC 2L Groundwater Quality Standard 1.0 6.0 0.7 6.0 0.4 0.6
MW-1B
MW-1 1080.54 35.62 1044.92 1.1
MW-1A 1085.32 >47.34 <1037.98
MW-1B 1082.56 42.12 1040.44
MW-18 1084.33 49.18 1035.15
MW-19 1071.48 50.60 1020.88
MW-16
MW-5 1051.26 41.20 1010.06 3.3
MW-10 1040.80 37.34 1003.46
MW-16 1037.56 30.48 1007.08 2.9 1.3 8.7 0.45 (j)0.89 (j)
MW-32 1025.26 31.86 993.40
MW-33 1007.40 13.67 993.73
MW-34 1014.60 8.11 1006.49
MW-24
MW-7 1009.24 45.23 964.01 NOT SAMPLED
MW-12 1007.35 51.35 956.00 1.1
MW-12D 1008.46 59.15 949.31
MW-24 974.04 29.91 944.13
MW-25 981.93 27.45 954.48
MW-26
MW-3 1024.73 25.75 998.98 5.3 7.1 0.47 (j)MW-11 1011.96 42.22 969.74 3.0 7.8
MW-26 990.69 28.88 961.81 1.4
MW-27 992.19 22.29 969.90
MW-31 985.42 11.25 974.17
MW-2 1004.48 21.75 982.73
MW-4R 1012.64 16.01 996.63 1.7
MW-6 1010.79 31.63 979.16
MW-9 996.27 11.75 984.52
MW-13 1004.56 42.28 962.28
MW-14 997.44 38.94 958.50
MW-15 1023.44 24.87 998.57 3.8
MW-17 991.16 19.22 971.94
MW-20 1046.92 39.38 1007.54
MW-21 990.00 31.29 958.71MW-22 958.97 15.52 943.45
MW-23 950.48 17.96 932.52
* = Deep well(s) not used for groundwater contouring
M ³M´4XDOLILHGFRQFHQWUDWLRQ6:6/FRQVLGHUHGDQHVWLPDWH
Groundwater Levels & VOCs Detected Above 2L Standards
AREA OF
CONCERN per CAP
TOP OF
CASING ELEVATION (FT AMSL)
DEPTH TO
WATER (FT BTOC)
GROUNDWATER
POTENTIOMETRIC ELEVATION (FT AMSL)
BENZENE
(ug/L)
1,4-
DCB (ug/L)
PCE
(ug/L)
1,1-
DCA (ug/L)
1,2-
DCA (ug/L)
1,2-
DCP (ug/L)MW-26
Benzene - 1.4 ug/l
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Figure 3
June 30, 2009 – July & September, 2016
Well ID Benzene Benzene Benzene Benzene Benzene Benzene
Up MW-3 61.66 8.10 43.03 7.20 31.50 6.00 37.04 6.10 43.31 6.85 30.20 5.30 -13.11 -1.55 -30 -23
Up MW-11 53.28 5.00 46.25 4.50 40.81 5.90 43.20 4.20 45.89 4.90 26.40 3.00 -19.49 -1.90 -42 -39
Up MW-27 23.70 0.00 20.20 0.00 24.60 0.00 28.00 0.00 24.13 0.00 21.30 0.00 -2.83 0.00 -12 0
138.64 13.10 109.48 11.70 96.91 11.90 108.24 10.30 113.32 11.75 77.90 8.30 -35.42 -3.45 -31 -29
Down MW-26 39.40 1.40 20.00 1.40 39.50 3.20 29.00 1.60 31.98 1.90 18.60 1.40 -13.38 -0.50 -42 -26
Down MW-31 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 0
39.40 1.40 20.00 1.40 39.50 3.20 29.00 1.60 31.98 1.90 18.60 1.40 -13.38 -0.50 -42 -26
Up&Down Gradient Total 178.04 14.50 129.48 13.10 136.41 15.10 137.24 11.90 145.29 13.65 96.50 9.70 -48.79 -3.95 -34 -29
Total VOCs and Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26
Total VOCs & Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26
Hydraulic
Gradient In
Relation to
Injection
Well (IW-1)
June 2009 (ug/L)Dec. 2009 (ug/L)July 2010 (ug/L)Dec. 2010 (ug/L)
Average of Four Events Preceding Injection (ug/L)July or Sept. 2016 (ug/L)
Difference Between Current and Baseline (ug/L)
Difference Between Current and Baseline (%)
All
VOCs
All
VOCs
All
VOCs
Benzen
e
All
VOCs
Benzen
e All VOCs
All
VOCs
All
VOCs
All
VOCs
Subtotal Upgradient
Subtotal Downgradient
2L
2 /1 7 /2 0 1 1
2 /1 7 /2 0 1 1
B a c -9 I n j e c t e d
B a c -9 I n j e c t e d
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Figure 4
Histograms of Dissolved Methane Concentrations
AOC ID WELL ID
DISSOLVED DISSOLVED DISSOLVED DISSOLVED DISSOLVED DISSOLVED
METHANE METHANE METHANE METHANE METHANE METHANE REDUCTION
Post-Start Up Post-Start Up Post-Start Up Post-Start Up Post-Start Up SINCE
06/15/12 06/27/13 06/26/14 06/16/15 01/06/16 07/05/16 START-UP
(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(%)
MW-1B
MW-1 6.78 0.08 0.00153 0.07580 0.0332 0.0903 -99
MW-1A NS NS NS NS NS NS NA
MW-1B 1.90 0.69 ND<0.0004 0.099 0.0511 0.3430 -82
MW-18 NS NS NS NS NS NS NA
MW-19 NS NS NS NS NS NS NA
AOC AVG 4.34 0.39 0.0009 0.0873 0.0422 0.2167 -95
NS = Not sampled since not impacted
Pre-LFGCCS (June 15, 2012) Compared to Post-LFGGCCS (July 5, 2016)
Pre-Start Up
0
1
2
3
4
5
6
7
8
DISSOLVED METHANE IN GROUNDWATER
MW-1
MW-1B
DATES
m g /L
E x t r a c t i o n S t a r t e d
NOV. 2012
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Figure 5
Histograms of Total VOC Concentrations
Baseline (June 24, 2009-December 9, 2010) Compared to July 2016
AOC ID WELL ID
MW-1B
MW-1 25.22 4.20 -21.02 -83
MW-1A NS NS NA NA
MW-1B 15.66 1.20 -14.46 -92
MW-18 0.00 0.00 0.00 0
MW-19 3.48 0.00 -3.48 -100
AOC AVG 11.09 1.35 -9.74 -88
MW-16
MW-5 18.39 22.30 3.91 21
MW-10 2.17 0.00 -2.17 -100
MW-16 44.14 43.34 -0.80 -2
MW-32 0.00 0.00 0.00 0MW-33 0.00 0.00 0.00 0MW-34 0.00 0.00 0.00 0
AOC AVG 10.78 10.94 0.16 1
MW-24
MW-7 12.69 -8.99 -71
MW-12 30.94 13.30 -17.64 -57
MW-12D 0.00 0.00 0.00 0
MW-24 1.56 0.00 -1.56 -100
MW-25 0.30 0.00 -0.30 -100
AOC AVG 9.10 3.40 -5.70 -63
MW-26
MW-3 43.31 30.20 -13.11 -30
MW-11 45.89 26.40 -19.49 -42
MW-26 31.98 18.60 -13.38 -42
MW-27 24.13 21.30 -2.83 -12
MW-31 0.00 0.00 0.00 0
AOC AVG 29.06 19.30 -9.76 -34
MW-2 27.19 0.00 -27.19 -100
MW-4R 25.00 21.30 -3.70 -15
MW-6 0.00 0.00 0.00 0
MW-9 18.51 15.10 -3.41 -18
MW-13 0.00 0.00 0.00 0
MW-14 11.93 7.20 -4.73 -40
MW-15 12.83 17.80 4.97 39
MW-17 2.27 0.00 -2.27 -100
MW-20 0.59 0.00 -0.59 -100
MW-21 0.28 0.00 -0.28 -100
MW-22 2.70 0.00 -2.70 -100
MW-23 0.51 0.00 -0.51 -100AOC AVG 8.48 5.12 -3.37 -40ALL WELLS ALL WELLS AVG 12.55 7.81 -4.74 -38
NS = Not sampled since dry
TOTAL VOC(s) BASELINE
AVERAGE
(June 2009-
Dec. 2010)
(ug/l)
TOTAL VOC(s)
LATEST
July 2016
(ug/l)
DIFFERENCE BETWEEN
LATEST AND
BASELINE (ug/L)
DIFFERENCE BETWEEN
LATEST AND
BASELINE
(%)

STATISTICAL
TREND*
Between June
2009 – July
2016
DownwardNo TrendDownwardNo TrendNo TrendDownwardNo TrendNo TrendNo TrendNo TrendNo TrendNo Trend
No Trend
3.7 1/16 No TrendDownwardNo TrendNo TrendNo TrendNo TrendDownwardDownwardNo TrendDownwardNo TrendDownward
Undesignated
(No
Remediation)
DownwardDownwardNo TrendDownwardNo TrendNo TrendNo TrendNo TrendNo TrendNo TrendNo TrendNo TrendDownwardDownward
* = Statistical trend analysis of all events between June 2009 and July 2016 via Sen's Slope Estimator at both a 90% or 95% Confidence Level
1/16 = Result from Jan 2016 event since exempt from sampling in July 2016
MW-1B MW-16 MW-26 MW-24 UNDESIGNATED SITEWIDE
0
5
10
15
20
25
30
35
TOTAL VOC(s) BASELINE AVERAGE COMPARED TO JULY 2016
BASELINE AVERAGE
JULY 2016AREA OF CONCERN
u g /L
Tables
Alexander County Active C10/14/2016 and Closed MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
July 1,5-6, 2016
Latitude Longitude
(inches)(ft)
MW-1 9/14/90 2 40.00 25.00 15 Soil & Rock 1080.54 1077.98 1054.92 25.62 35.8389 -81.1478
MW-1A 9/30/94 2 47.50 32.50 15 Soil & Rock 1085.32 1083.28 <1035.78 Dry (>49.54)35.8389 -81.1478
MW-1B 5/21/03 2 61.00 46.00 15 Rock 1082.56 1079.56 1040.44 42.12 35.8391 -81.1478
MW-2 9/6/90 2 30.00 15.00 15 Soil 1004.48 1002.28 982.73 21.75 35.8376 -81.1524
MW-3 9/19/90 2 33.00 13.00 20 Soil & Rock 1024.73 1024.23 998.98 25.75 35.8365 -81.1503
MW-4R 9/30/94 2 20.50 5.50 15 Soil & Rock 1012.64 1008.54 996.63 16.01 35.8366 -81.1479
MW-5 9/16/94 2 48.80 33.80 15 Soil & Rock 1051.26 1049.01 1010.06 41.20 35.8373 -81.1465
MW-6 9/29/94 2 41.00 26.00 15 Rock 1010.79 1008.29 979.16 31.63 35.8369 -81.1364
MW-7 9/29/94 2 53.00 38.00 15 Rock 1009.24 1005.84 964.01 45.23 35.8364 -81.1522
MW-9 10/24/00 2 31.50 16.50 15 Rock 996.27 993.76 984.52 11.75 35.8361 -81.1481
MW-10 10/25/00 2 91.00 76.00 15 Rock 1040.80 1037.83 1003.46 37.34 35.8366 -81.1469
MW-11 10/24/00 2 56.00 41.00 15 Rock 1011.96 1008.98 969.74 42.22 35.8359 -81.1505
MW-12 10/23/00 2 66.50 51.50 15 Soil 1007.35 1004.46 956.00 51.35 35.3577 -81.1525
MW-12D 6/9/00 2 100.00 90.00 10 Rock 1008.46 1006.03 949.31 59.15 35.3577 -81.1525
MW-13 10/25/00 2 60.50 45.50 15 Rock 1004.56 1001.63 962.28 42.28 35.8368 -81.1532
MW-14 10/26/00 2 40.50 25.50 15 Soil & Rock 997.44 994.06 958.50 38.94 35.8376 -81.1525
MW-15 10/25/00 2 35.00 20.00 15 Soil & Rock 1023.44 1020.81 998.57 24.87 35.8385 -81.1508
MW-16 12/20/07 2 40.25 25.25 15 Rock 1037.56 1034.94 1007.08 30.48 35.8371 -81.1465
MW-17 6/10/03 2 22.30 7.30 15 Rock 991.16 988.36 971.94 19.22 35.8386 -81.1511
MW-18 12/19/07 2 56.70 41.70 15 Rock 1084.33 1081.52 1035.15 49.18 35.8392 -81.1467
MW-19 12/20/07 2 63.92 48.92 15 Rock 1071.48 1068.67 1020.88 50.60 35.8391 -81.1487
MW-20 12/20/07 2 63.55 48.55 15 Rock 1046.92 1044.19 1007.54 39.38 35.8391 -81.1502
MW-21 12/19/07 2 41.05 26.05 15 Rock 990.00 987.08 958.71 31.29 35.8386 -81.1514
MW-22 12/19/07 2 18.12 8.12 10 Rock 958.97 956.21 943.45 15.52 35.8381 -81.1524
MW-23 12/19/07 2 21.54 6.54 15 Soil 950.48 947.83 932.52 17.96 35.8376 -81.1529
MW-24 12/20/07 2 35.35 20.35 15 Soil 974.04 971.29 944.13 29.91 35.8356 -81.1533
MW-25 12/19/07 2 44.48 29.48 15 Rock 981.93 979.93 954.48 27.45 35.8353 -81.1528
MW-26 12/20/07 2 49.80 34.80 15 Rock 990.69 988.08 961.81 28.88 35.8354 -81.1504
MW-27 12/20/07 2 49.82 34.82 15 Rock 992.19 989.19 969.90 22.29 35.8356 -81.1493
MW-31 8/16/10 2 32.56 17.56 15 Soil 985.42 982.42 974.17 11.25 35.8348 -81.1506
MW-32 8/16/10 2 42.70 27.7 15 Rock 1025.26 1022.26 993.40 31.86 35.8361 -81.1469
MW-33 4/27/13 2 21.38 6.38 15 PWR 1007.40 1004.40 993.73 13.67 35.8367 -81.1462
MW-34 4/27/13 2 21.19 6.19 15 PWR 1014.60 1011.60 1006.49 8.11 35.8373 -81.1459
IW-1 2/14/11 4 52.44 37.44 15 Rock 990.44 987.44 NR NR 35.8356 -81.1504
NOTE:
PWR = partially weathered rock
Monitoring
Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
July 1,5 & 6, 2016
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-1A No Yes Yes Yes Yes Yes Dry which is typical
MW-1B Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-3 Yes Yes Yes Yes Yes Yes Slow recharge
MW-4R Yes Yes Yes Yes Yes Yes Purge water has sulfur smell.
MW-5 Yes Yes Yes Yes Yes Yes Well damaged by MESCO*; Needs MNA tubing
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes
MW-9 Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes Purge water has sulfur smell. Very slow recharge
MW-11 Yes Yes Yes Yes Yes Yes
MW-12 Yes Yes Yes Yes Yes Yes
MW-12D Yes Yes Yes Yes Yes Yes
MW-13 Yes Yes Yes Yes Yes Yes
MW-14 Yes Yes Yes Yes Yes ?Surface pad cracked
MW-15 Yes Yes Yes Yes Yes Yes
MW-16 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19 Yes Yes Yes Yes Yes Yes
MW-20 Yes Yes Yes Yes Yes Yes
MW-21 Yes Yes Yes Yes Yes Yes
MW-22 Yes Yes Yes Yes Yes Yes
MW-23 Yes Yes Yes Yes Yes Yes
MW-24 Yes Yes Yes Yes Yes Yes
MW-25 Yes Yes Yes Yes Yes Yes
MW-26 Yes Yes Yes Yes Yes Yes
MW-27 Yes Yes Yes Yes Yes Yes
MW-31 Yes Yes Yes Yes Yes Yes Purge water very turbid
MW-32 Yes Yes Yes Yes Yes Yes
MW-33 Yes Yes Yes Yes Yes Yes
MW-34 Yes Yes Yes Yes Yes Yes Path to well recently improved by County
IW-1 Yes Yes Yes Yes Yes Yes Injection well. Not sampled this event.
SW-3 Yes -----
SW-4R Yes -----
SW-5 Yes -----
SW-6 Yes -----
Any unusual field conditions, observations, or events:
LFG extraction system operating in AOC MW-1B which is typical.
*MW-5 was damaged by MESCO but repaired by MESCO. Stickup elevation attempted to be maintained but should be re-surveyed for accuracy.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface
Pad
Effective
Phytoremediation transducer data downloaded
Phytoremediation transducer data downloaded
Low gage height and flow rate
Low gage height and flow rate
Low gage height and flow rate
Low gage height and flow rate
Alexander County Active C12/07/2016 and Closed MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
July 1,5-6, 2016
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L % Vol.Visual or NTU
MW-1 35.62 1044.92 1080.54 17.7 NR NR 6.1 468 NR NR Clear
MW-1B 42.12 1040.44 1082.56 15.8 NR NR 5.32 290 NR NR Clear
MW-2 21.75 982.73 1004.48 18.6 NR NR 5.3 152 NR NR Clear
MW-3 25.75 998.98 1024.73 18.7 NR NR 5.5 376 NR NR Clear
MW-4R 16.01 996.63 1012.64 16.2 NR NR 5.81 81 NR NR Clear
MW-5 41.20 1010.06 1051.26 19.2 -91 0.2 6.1 428 NR NR 63
MW-6 31.63 979.16 1010.79 14.9 178 0.9 5.2 62 NR NR 19
MW-7 45.23 964.01 1009.24 -----NR NR -
MW-9 11.75 984.52 996.27 17.7 NR NR 6 603 NR NR Clear
MW-10 37.34 1003.46 1040.80 18.2 NR NR 6.99 60 NR NR Slight
MW-11 42.22 969.74 1011.96 16.8 77 0.1 5.8 684 NR NR 33
MW-12 51.35 956.00 1007.35 17.3 71 0.6 5.81 61 NR NR 19
MW-12D 59.15 949.31 1008.46 16.8 75 0.9 5.21 48 NR NR 26
MW-13 42.28 962.28 1004.56 14.9 NR NR 5.6 210 NR NR Clear
MW-14 38.94 958.50 997.44 16.1 NR NR 6.11 123 NR NR Slight
MW-15 24.87 998.57 1023.44 14.8 NR NR 5.4 254 NR NR Clear
MW-16 30.48 1007.08 1037.56 15.5 219 0.7 5.17 163 NR NR Clear
MW-17 19.22 971.94 991.16 14.6 NR NR 5.1 82 NR NR Clear
MW-18 49.18 1035.15 1084.33 17.1 303 2.4 6.81 33 NR NR Slight
MW-19 50.60 1020.88 1071.48 17.3 NR NR 6.72 86 NR NR Clear
MW-20 39.38 1007.54 1046.92 15.9 NR NR 6.21 143 NR NR Clear
MW-21 31.29 958.71 990.00 14.8 NR NR 5.6 56 NR NR Clear
MW-22 15.52 943.45 958.97 14.6 NR NR 5.2 44 NR NR Clear
MW-23 17.96 932.52 950.48 13.5 NR NR 5.3 78 NR NR Slight
MW-24 29.91 944.13 974.04 14.6 307 0.4 5.7 160 NR NR Slight
MW-25 27.45 954.48 981.93 14.0 197 0.5 5.3 72 NR NR Clear
MW-26 28.88 961.81 990.69 16.3 133 2.8 5.69 403 NR NR Clear
MW-27 22.29 969.90 992.19 16.9 191 2.9 6.2 162 NR NR 38
MW-31 11.25 974.17 985.42 15.9 201 0.9 5.20 135 NR NR Moderate
MW-32 31.86 993.40 1025.26 14.1 NR NR 5.4 23 NR NR Clear
MW-33 13.67 993.73 1007.40 16.1 NR NR 6.13 127 NR NR Moderate
MW-34 8.11 1006.49 1014.60 15.2 NR NR 5.1 36 NR NR Clear
Minimum 8.11 932.52 950.48 13.5 -91 0.1 5.1 23 NR NR Clear
Average 31.07 983.58 1014.65 16.1 155 1.1 5.71 184 NR NR Slight
Maximum 59.15 1044.92 1084.33 19.2 307 2.9 6.99 684 NR NR Moderate
SW-3 ---20.1 NR NR 6.89 83 NR NR Clear
SW-4R ---18.6 NR NR 6.3 65 NR NR Clear
SW-5 ---20.2 NR NR 6.91 91 NR NR Clear
SW-6 ---20.7 NR NR 6.92 103 NR NR Clear
Minimum ---18.6 NR NR 6.3 65 NR NR Clear
Average ---19.9 NR NR 6.76 86 NR NR Clear
Maximum ---20.7 NR NR 6.92 103 NR NR Clear
NR = No Reading Attempted
Water
Depth
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane Gas in
Headspace
Turbidity of
Metal Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
July 1,5 & 6, 2016 & September 22 , 2016
App. I App. II MNA
C o n s t i t u e n t
T o t a l M e t a l s
T o t a l M e t a l s A p p I I
H e r b i c i d e s -C h l o r i n a t e d A p p I I
P e s t i c i d e s A p p I I
T o t a l C y a n i d e
S u l f i d e
V F A
H y d r o g e n
M e t h a n e , D i s s o l v e d
C a r b o n D i o x i d e
A l k a l i n i t y
S u l f a t e
S u l f i d e
C h l o r i d e
T O C
C O D
B O D
I r o n , D i s s o l v e d
N i t r a t e
Laboratory P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
F I E L D
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
P A C E
Method L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b S W 8 1 5 1 A
L a b E P A 8 0 8 2 A
L a b E P A 8 2 7 0 D
L a b E P A 8 0 8 1 B
L a b E P A 9 0 1 4
L a b S M 1 8 4 5 0 0 -S D
A M 2 3 G
A M 2 0 G A X
R S K 1 7 5
A M 2 0 G A X
L a b S M 2 3 2 0 B
E P A 3 0 0 .0
L a b S M 1 8 4 5 0 0 -S D
S M 5 3 1 0 B
S M 5 2 2 0 D
S M 5 2 1 0 B
L a b E P A 6 0 1 0
L a b 3 5 3 .2
MW-1 x x x x x x x x x
MW-1A Dry so not sampled which is typical
MW-1B x x x x x x x x x
MW-2 x x x x x x x x
MW-3 x x x x x x x x
MW-4R x x x x x x x x
MW-5 x x x x x x x x x x x x x x x x x x
MW-6 x x x x x x x x x x x x
MW-7 Not sampled since exempt during summer event (DIN:14150)
MW-9 x x x x x x x x
MW-10 x x
MW-11 x x x x x x x x x x x x x x x x x x
MW-12 x x x x x x x x x x x x x x x x x x
MW-12D x x x x x x x x x x x x
MW-13 x x
MW-14 x x
MW-15 x x
MW-16 x x x x x x x x x
MW-17 x x
MW-18 x x x x x x x x x
MW-19 x x
MW-20 x x
MW-21 x x
MW-22 x x
MW-23 x x
MW-24 x x x x x x x x x x x x
MW-25 x x x x
MW-26 x x x x x x x x x x x x x x x x x x
MW-27 x x x
MW-31 x x x x x x x x x x x x
MW-32 x x
MW-33 x x
MW-34 x x
SW-3 x x
SW-4R x x
SW-5 x x
SW-6 x x
EB x x
TB x
FB x x
App I & II = Appendix I Listed in current 40 CFR 258
V O C s
V O C s A p p I I
P o l y c h l o r i n a t e d b i p h e n y l (P C B ) A p p I I
S e m i v o l a t i l e O r g a n i c s (S V O C s ) A p p I I
E t h e n e /E t h a n e
H a c h K i t
L a b S M 4 5 0 0 -C l -E
Alexander Co. Active CDLF over MSW Page 1 of 4
Table 5
July 1-6, 2016 and September 22, 2016
Sample ID Result Unit
MW-1 7/05/16 3.1 0.33 1 6 75
MW-1 Benzene 7/05/16 1.1 0.25 1 1 5 L &/or LFG
MW-1 Cobalt, total 7/05/16 10.1 2.5 10 NE 70 NE
MW-1 Vanadium, total 7/05/16 4.7J 2.5 25 NE 0.3 NE N
MW-1 Zinc, total 7/05/16 44.3 5 10 1000 5000
MW-1B 7/05/16 1.2 0.33 1 6 75
MW-1B Barium, total 7/05/16 176 2.5 100 700 1300
MW-1B Cobalt, total 7/05/16 107 2.5 10 NE 70 NE N
MW-1B Zinc, total 7/05/16 26.6 5 10 1000 5000
MW-2 Barium, total 7/06/16 106 2.5 100 700 1300
MW-2 Cadmium, total 7/06/16 2.9 0.5 1 2 5 N
MW-2 Cobalt, total 7/06/16 820 2.5 10 NE 70 NE N
MW-2 Thallium, total 7/06/16 6.6 5 5.5 NE 0.28 2 N
MW-2 Zinc, total 7/06/16 471 5 10 1000 5000
MW-3 7/05/16 0.47J 0.24 1 0.4 5 L &/or LFG
MW-3 7/05/16 7.1 0.33 1 6 75 L &/or LFG
MW-3 Benzene 7/05/16 5.3 0.25 1 1 5 L &/or LFG
MW-3 7/05/16 5.9 0.19 5 70 70
MW-3 Cobalt, total 7/05/16 10 2.5 10 NE 70 NE
MW-3 7/05/16 2.2 0.3 1 600 700
MW-3 Toluene 7/05/16 1 0.26 1 600 1000
MW-3 7/05/16 8.7 0.66 5 530 10000
MW-4R 7/05/16 4.2 0.33 1 6 75
MW-4R Barium, total 7/05/16 114 2.5 100 700 1300
MW-4R Benzene 7/05/16 1.7 0.25 1 1 5 L &/or LFG
MW-4R 7/05/16 15.4 0.19 5 70 70
MW-4R Cobalt, total 7/05/16 378 2.5 10 NE 70 NE N
MW-5 7/05/16 2.8 0.33 1 6 75
MW-5 Barium, total 7/05/16 120 2.5 100 700 1300
MW-5 Benzene 7/05/16 3.3 0.25 1 1 5 L &/or LFG
MW-5 Beryllium, total 7/05/16 1.5 0.5 1 NE 4 4
MW-5 Chromium, total 7/05/16 35.8 2.5 10 10 100 N
MW-5 7/05/16 16.2 0.19 5 70 70
MW-5 Copper, total 7/05/16 16.3 2.5 10 1000 1300
MW-5 Vanadium, total 7/05/16 24.2J 2.5 25 NE 0.3 NE N
MW-5 Zinc, total 7/05/16 83.3 5 10 1000 5000
Detections in Water Samples Above Established SWSL, GWP, 2L, 2B, or MCL (Appendix I)
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
Ethylbenzene ug/L
ug/L
Xylene (Total)ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
Alexander Co. Active CDLF over MSW Page 2 of 4
Sample ID Result UnitParameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
MW-6 Cobalt, total 7/06/16 13.6 2.5 10 NE 70 NE
MW-9 7/06/16 2.2 0.33 1 6 75
MW-9 Barium, total 7/06/16 152 2.5 100 700 1300
MW-9 7/06/16 12.9 0.19 5 70 70
MW-9 Cobalt, total 7/06/16 247 2.5 10 NE 70 NE N
MW-9 Nickel, total 7/06/16 65.7 2.5 50 100 100
MW-9 Thallium, total 7/06/16 6.2 5 5.5 NE 0.28 2 N
MW-9 Zinc, total 7/06/16 19.4 5 10 1000 5000
MW-11 7/06/16 7.8 0.33 1 6 75 L &/or LFG
MW-11 Barium, total 7/06/16 175 2.5 100 700 1300
MW-11 Benzene 7/06/16 3 0.25 1 1 5 L &/or LFG
MW-11 Chromium, total 7/06/16 13.2 2.5 10 10 100 N
MW-11 7/06/16 15.6 0.19 5 70 70
MW-11 Cobalt, total 7/06/16 120 2.5 10 NE 70 NE N
MW-11 Thallium, total 7/06/16 5J 5 5.5 NE 0.28 2 N
MW-11 Zinc, total 7/06/16 161 5 10 1000 5000
MW-12 7/05/16 3.7 0.33 1 6 75
MW-12 Barium, total 7/05/16 112 2.5 100 700 1300
MW-12 Benzene 7/05/16 1.1 0.25 1 1 5 L &/or LFG
MW-12 7/05/16 7.4 0.19 5 70 70
MW-12 Cobalt, total 7/05/16 68.8 2.5 10 NE 70 NE
MW-12 7/05/16 1.1 0.47 1 3 5
MW-12 Zinc, total 7/05/16 45.1 5 10 1000 5000
MW-13 Chromium, total 7/01/16 18.7 2.5 10 10 100 N
MW-13 Vanadium, total 7/01/16 19.8J 2.5 25 NE 0.3 NE N
MW-13 Copper, total 7/01/16 41.6 2.5 10 1000 1300
MW-13 Lead, total 7/01/16 10.6 2.5 10 15 15
MW-13 Zinc, total 7/01/16 28.6 5 10 1000 5000
MW-14 Arsenic, total 7/01/16 12.3 2.5 10 10 10 N
MW-14 Cobalt, total 7/01/16 92.5 2.5 10 NE 70 NE N
MW-14 Vanadium, total 7/01/16 7.3J 2.5 25 NE 0.3 NE N
MW-14 7/01/16 1.6 0.33 1 6 75
MW-14 Barium, total 7/01/16 175 2.5 100 700 1300
MW-14 7/01/16 5.6 0.19 5 70 70
MW-14 Copper, total 7/01/16 14 2.5 10 1000 1300
MW-14 Zinc, total 7/01/16 32.2 5 10 1000 5000
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
Trichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
Alexander Co. Active CDLF over MSW Page 3 of 4
Sample ID Result UnitParameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
MW-15 Benzene 7/01/16 3.8 0.25 1 1 5 L &/or LFG
MW-15 7/01/16 1.3 0.33 1 6 75
MW-15 Cadmium, total 7/01/16 1.6 0.5 1 2 5
MW-15 7/01/16 11.5 0.19 5 70 70
MW-15 Cobalt, total 7/01/16 29.7 2.5 10 NE 70 NE
MW-15 7/01/16 1.2 0.47 1 3 5
MW-15 Zinc, total 7/01/16 26.6 5 10 1000 5000
MW-16 7/05/16 8.7 0.32 5 6 7 L &/or LFG
MW-16 7/05/16 0.45J 0.24 1 0.4 5 L &/or LFG
MW-16 7/05/16 0.89J 0.27 1 0.6 5 L &/or LFG
MW-16 Benzene 7/05/16 2.9 0.25 1 1 5 L &/or LFG
MW-16 7/05/16 1.3 0.46 1 0.7 5 L &/or LFG
MW-16 Cobalt, total 7/05/16 91 2.5 10 NE 70 NE N
MW-16 7/05/16 2.6 0.33 1 6 75
MW-16 7/05/16 24.4 0.19 5 70 70
MW-16 7/05/16 2.1 0.47 1 3 5
MW-17 Chromium, total 7/01/16 31.3 2.5 10 10 100 N
MW-17 Vanadium, total 7/01/16 48.7 2.5 25 NE 0.3 NE N
MW-17 Barium, total 7/01/16 178 2.5 100 700 1300
MW-17 Cobalt, total 7/01/16 51.4 2.5 10 NE 70 NE
MW-17 Copper, total 7/01/16 22.5 2.5 10 1000 1300
MW-17 Lead, total 7/01/16 10.6 2.5 10 15 15
MW-17 Zinc, total 7/01/16 53.7 5 10 1000 5000
MW-18 Chromium, total 9/22/16 29.2 2.5 10 10 100 N
MW-18 Vanadium, total 9/22/16 43.3 2.5 25 NE 0.3 NE N
MW-18 Cobalt, total 9/22/16 47.1 2.5 10 NE 70 NE
MW-18 Copper, total 9/22/16 69.6 2.5 10 1000 1300
MW-18 Thallium, total 9/22/16 5.1J 5 5.5 NE 0.28 2 N
MW-18 Zinc, total 9/22/16 58.2 5 10 1000 5000
MW-20 Cadmium, total 7/01/16 1.2 0.5 1 2 5
MW-21 Vanadium, total 7/01/16 20.2J 12.5 25 NE 0.3 NE N
MW-22 Cadmium, total 7/01/16 1.2 0.5 1 2 5
MW-22 Vanadium, total 7/01/16 4.8J 2.5 25 NE 0.3 NE N
MW-22 Zinc, total 7/01/16 13.8 5 10 1000 5000
MW-23 Chromium, total 7/01/16 10.8 2.5 10 10 100 N
MW-23 Vanadium, total 7/01/16 12.2J 2.5 25 NE 0.3 NE N
MW-23 Cobalt, total 7/01/16 23.6 2.5 10 NE 70 NE
MW-23 Zinc, total 7/01/16 16.5 5 10 1000 5000
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
Trichloroethene ug/L
ug/L
1,1-Dichloroethane ug/L
1,2-Dichloroethane ug/L
1,2-Dichloropropane ug/L
ug/L
Tetrachloroethene ug/L
ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
Trichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Alexander Co. Active CDLF over MSW Page 4 of 4
Sample ID Result UnitParameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
MW-24 Chromium, total 7/06/16 16.7 2.5 10 10 100 N
MW-24 Vanadium, total 7/06/16 10.4J 2.5 25 NE 0.3 NE N
MW-24 Barium, total 7/06/16 207 2.5 100 700 1300
MW-24 Cobalt, total 7/06/16 15.6 2.5 10 NE 70 NE
MW-24 Zinc, total 7/06/16 29.2 5 10 1000 5000
MW-25 Vanadium, total 7/06/16 3.5J 2.5 25 NE 0.3 NE N
MW-25 Zinc, total 7/06/16 13.6 5 10 1000 5000
MW-26 Benzene 9/22/16 1.4 0.25 1 1 5 L &/or LFG
MW-26 9/22/16 4.9 0.33 1 6 75
MW-26 9/22/16 12.3 0.19 5 70 70
MW-26 Cobalt, total 9/22/16 23 2.5 10 NE 70 NE
MW-26 Zinc, total 9/22/16 18 5 10 1000 5000
MW-27 7/05/16 21.3 0.19 5 70 70
MW-31 Barium, total 7/05/16 100 2.5 100 700 1300
MW-31 Vanadium, total 7/05/16 3.7J 2.5 25 NE 0.3 NE N
MW-31 Zinc, total 7/05/16 13.5 5 10 1000 5000
MW-32 Vanadium, total 7/01/16 4.9J 2.5 25 NE 0.3 NE N
MW-32 Zinc, total 7/01/16 23.7 5 10 1000 5000
MW-34 Copper, total 7/01/16 10.1 2.5 10 1000 1300
MW-34 Vanadium, total 7/01/16 16.7J 2.5 25 NE 0.3 NE N
MW-34 Zinc, total 7/01/16 21 5 10 1000 5000
SW-3 Cobalt, total 7/01/16 32.2 2.5 10 270 NE
SW-5 Cobalt, total 7/01/16 32 2.5 10 270 NE
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
J=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
NE = Not Established
LFG = Landfill Gas
Concentration > 2L, 2B, GWP or MCL Standard
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains Appendix I constituents detected at or above SWSL, GWP, 2L, 2B or MCL Standards
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
BOLD =
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 6
July 1-6, 2016 and September 22, 2016
Sample ID Result Unit
MW-1 Cyanide 7/05/16 4.2J(B)4 10 70 200
MW-1B Cyanide 7/05/16 5.2J(B)4 10 70 200
MW-1B Mercury, total 7/05/16 1.3 0.1 0.2 1 2 LFG
MW-2 Cyanide 7/06/16 8.5J(B)4 10 70 200
MW-2 Mercury, total 9/22/16 0.44 0.1 0.2 1 2
MW-4R Cyanide 7/05/16 4J(B)4 10 70 200
MW-5 Cyanide 7/05/16 4.8J(B)4 10 70 200
MW-9 Cyanide 7/06/16 6.4J(B)4 10 70 200
MW-9 Mercury, total 9/22/16 0.36 0.1 0.2 1 2
MW-11 7/06/16 1.7J 0.85 15 NE NE NE
MW-11 Cyanide 7/06/16 5J(B)4 10 70 200
MW-11 Mercury, total 9/22/16 0.43 0.1 0.2 1 2
MW-11 7/06/16 1.3J 1.2 20 NE NE NE
MW-12 Cyanide 7/05/16 5J(B)4 10 70 200
MW-12 7/05/16 0.45J 0.35 10 70 70
MW-16 Cyanide 7/05/16 4.7J(B)4 10 70 200
MW-26 9/22/16 0.05J 0.05 2 50 50
MW-26 Aldrin 9/22/16 0.11 0.05 0.05 NE NE 1
A definitive source of the detection was not determined as part of this report.
NE = Not Established
LFG = Landfill Gas
Adjusted for actual sample preparation data and moisture content
(B) = Also detected in associated method Blank and flagged by the laboratory as such. Likely false positive or high bias originating in the laboratory.
Concentration > 2L, GWP or MCL Standard
Detections in Water Samples above MDL (Appendix II Exclusive)
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 GWP 5 MCL 6 Preliminary
Cause 7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
bis(2-Ethylhexyl)phthalate ug/L
ug/L
ug/L
Thionazin ug/L
ug/L
1,2,4-Trichlorobenzene ug/L
ug/L
2,4,5-TP (Silvex)ug/L
ug/L
1 Table contains App II exclusive constituents detected over MDL. (Parameters not also listed in Appendix I)
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 GWP = Groundwater Protection Standard
6 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
7 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
j = The reported value is estimated & between the laboratory MDL & the SWSL,
BOLD =
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 7
July 1, 2016
MW-2 3.70E-06 28 0.098 1 N76W 21.75 982.73 UC
MW-12 n/a 28 0.032 n/a S41W 51.35 956.00 UC
MW-16 8.72E-04 17 0.032 171 S07E 30.48 1007.08 UC
MW-17 n/a 17 0.117 n/a N56W 19.22 971.94 UC
MW-21 3.77E-03 28 0.273 3799 N54W 31.29 958.71 UC
MW-22 6.04E-04 28 0.055 123 N51W 15.52 943.45 UC
MW-23 9.83E-04 28 0.310 1127 N41W 17.96 932.52 UC
MW-24 1.33E-02 28 0.076 3733 N63W 29.91 944.13 UC
MW-31 n/a 28 0.173 n/a n/a 11.25 974.17 UC
MW-33 n/a 28 0.060 n/a S35E 13.67 993.73 UC
MW-34 n/a 28 0.032 n/a S27E 8.11 1006.49 UC
Minimum 3.70E-06 17 0.032 1 -8.11 932.52 -
Average 3.26E-03 26 0.114 1493 -22.77 970.09 -
Maximum 1.33E-02 28 0.310 3799 -51.35 1007.08 -
MW-1 5.60E-05 10 0.086 50 N51W 35.62 1044.92 UC/UBR
MW-3 3.90E-06 10 0.020 1 S23W 25.75 998.98 UC/UBR
MW-4R 4.90E-04 10 0.053 271 S07W 16.01 996.63 UC/UBR
MW-5 6.40E-05 28 0.071 17 S03E 41.20 1010.06 UC/UBR
MW-14 n/a 10 0.372 n/a N54W 38.94 958.50 UC/UBR
MW-15 n/a 10 0.044 n/a N84W 24.87 998.57 UC/UBR
Minimum 3.90E-06 10 0.020 1 -16.01 958.50 -
Average 1.53E-04 13 0.108 85 -30.40 1001.28 -
Maximum 4.90E-04 28 0.372 271 -41.2 1044.92 -
MW-1B n/a 10 0.054 n/a N11W 42.12 1040.44 UBR
MW-6 2.40E-05 10 0.004 1 S80W 26.27 979.16 UBR
MW-7 1.60E-06 10 0.032 1 S31W 45.23 964.01 UBR
MW-9 n/a 10 0.251 n/a S05E 11.75 984.52 UBR
MW-11 n/a 10 0.061 n/a S22W 42.22 969.74 UBR
MW-13 n/a 10 0.075 n/a S72W 42.28 962.28 UBR
MW-19 1.92E-06 10 0.042 1 N46W 50.60 1020.88 UBR
MW-20 5.49E-05 10 0.029 17 S74W 39.38 1007.54 UBR
MW-25 5.41E-05 10 0.056 31 N64W 27.45 954.48 UBR
MW-26 1.16E-04 10 0.027 33 S32W 28.88 961.81 UBR
MW-27 2.83E-05 10 0.018 5 S15W 22.29 969.90 UBR
MW-32 n/a 10 0.114 n/a S15E 31.86 993.40 UBR
Minimum 1.60E-06 10 0.004 1 -11.75 954.48 -
Average 4.01E-05 10 0.064 13 -34.19 984.01 -
Maximum 1.16E-04 10 0.251 33 -50.60 1040.44 -
MW-10 n/a 10 0.095 n/a n/a 37.34 1003.46 LBR
MW-12D n/a 10 0.088 n/a n/a 59.15 949.31 LBR
MW-18 1.19E-04 10 0.083 n/a n/a 49.18 1035.15 LBR
Minimum 1.19E-04 10 0.083 --37.34 949.31 -
Average 1.19E-04 10 0.089 --48.56 995.97 -
Maximum 1.19E-04 10 0.095 --59.15 1035.15 -
NOTE:Values for hydraulic conductivity obtained from GAI Consultants Sampling Report (April, 1995) & MESCO ACM Report (2008).
Average Linear Groundwater Velocities calculated only for UC & UBR wells with hydraulic conductivity values.
Wells screened in LBR not utilized for flow directions/gradients.
Flow rate (Q) calculated via modified Darcy's equation:
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity
(%)
Hydraulic
Gradient
(ft/ft)
Average Linear
Velocity Rate
(ft/yr)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation (ft amsl)
Screened
Interval
Lithology
K= hydraulic conductivity
UC = Unconfined/saprolite; UBR = Upper Bedrock fracture system; LBR = Lower Bedrock fracture system.ne = effective porosity
dh= head difference
Hydrologic Gradient taken from water elevations recorded between July 1, 2016.dl= horizontal distance
dl
dh
n
KQ
e

Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 8
MNA Parameter Data Summary
July 1, 5-6, 2016
Parameters Method MDL*Units MW-18 MW-3 MW-5 MW-6 MW-7 MW-11 MW-12 MW-12D MW-16 MW-24 MW-25 MW-26 MW-27 MW-31 MW-33 MW-34
7/05/16 7/05/16 7/05/16 7/06/16 NS 7/06/16 7/05/16 7/05/16 7/06/16 7/06/16 7/06/16 7/05/16 7/05/16 7/05/16 7/01/16 7/01/16
VFA – Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Lactic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Methane RSK175 10 ug/L <10 19000 NS NS NS NS NS NS 8380 NS NS 2610 52.8 <10 NS NS
Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
CO2-Dissolved Field HACH Kit NS mg/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Alkalinity SM 2320B 1000 ug/L NS 104000 112000 11200 NS 210000 125000 381000 46100 36600 17400 211000 35900 35100 NS NS
Sulfate EPA 300.0 1000 ug/L NS 1320j 4480j 3670j NS 2330j 3660j 1290j 6860j 4920j 4710j 4150j 4230j 1760j NS NS
Sulfide SM 4500-S2D 100 ug/L NS NS <100 <100 NS <100 <100 <100 <100 <100 <100 <100 <100 <100 NS NS
Chloride SM 4500-Cl-E 1000 ug/L 1360 23900 4480 4230 NS 67200 10300 56600 6020 18300 3800 31400 23100 16000 NS NS
TOC SM 5310B 500 ug/L 1570 5240 2440 2840 NS 5930 1640 3160 1310 2210 1990 2880 1800 2160 NS NS
COD SM 5220D 12500 ug/L <12500 46000 50000 <12500 NS 91000 36000 <12500 <12500 26000 <12500 25000 <12500 <12500 NS NS
BOD SM5210B NS ug/L <2000 6600 2770 <2000 NS 3770 2300 <2000 <2000 <2000 <2000 <2000 <2000 <2000 NS NS
Iron (total-dissolved)EPA 6010 25 ug/L NS NS 13100 <25 NS 25500 18000 283j <25 333 465 1250 <25 68.2j NS NS
Nitrate EPA 353.2 10 ug/L 51.5j NS <10 365j NS <10 <10 <10 83.2j 309j 1130j <10 472j 1350j NS NS
Temperature Field Instrument 0 C 17.1 18.7 19.2 14.9 NS 16.8 17.3 16.8 15.5 14.6 14 16.3 16.9 15.9 16.1 15.2
ORP Field Instrument -900 mV 303 NS -91 178 NS 71 71 75 219 307 197 133 191 201 NS NS
DO Field Instrument 0 mg/L 2.4 NS 0.2 0.9 NS 0.6 0.6 0.9 0.7 0.4 0.5 2.8 2.9 0.9 NS NS
pH Field Instrument 0 SU 6.81 5.50 6.1 5.20 NS 5.81 5.81 5.21 5.17 5.7 5.3 5.69 6.2 5.2 6.13 5.1
Sp. Conductance Field Instrument 0 us/cm 33 376 428 603 NS 61 61 48 163 160 72 403 162 135 127 36
Turbidity Field Instrument 0 NTU NS NS 63 NS NS 19 19 26 NS NS NS NS NS NS NS NS
Notes:
VFA = Volatile Fatty Acids
MDL* = Lab Method Detection Limit or lowest field measurement possible
< = Not Detected above MDL value
MNA monitoring not required for MW-31 by SWS but recorded per NC Underground Injection Control (UIC) Permit requirement
NS = Not Sampled since not required during this specific event
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 9
August 1, 2016
March 25, 2016 August 1, 2016 March 25, 2015 compared to Aug. 1, 2016
Notes Notes
1 5/25/10 244 195 16.8 456 Dormant 5/25/10 263 205 17.5 486 25% yellow 19 10 0.7 30
2 5/22/13 87 68 3.5 159 Dormant 5/22/13 99 73 4.2 176 0% yellow 12 5 0.7 18
3 5/25/10 199 133 8.4 340 Dormant 5/25/10 216 145 9.1 370 50% yellow 17 12 0.7 30
4 5/25/10 221 86 7.9 315 Dormant 5/25/10 235 93 8.1 336 10% yellow 14 7 0.2 21
5 5/25/10 159 72 6.3 237 Dormant 5/25/10 162 76 7.5 246 10% yellow 3 4 1.2 8
6 5/25/10 136 61 5.2 202 Dormant 5/25/10 142 68 6.3 216 10% yellow 6 7 1.1 14
7 5/25/10 133 87 4.6 225 Dormant 5/25/10 136 91 5.2 232 33% yellow 3 4 0.6 8
8 5/25/10 191 71 6.8 269 Dormant 5/25/10 212 85 7.2 304 33% yellow 21 14 0.4 35
9 5/25/10 172 75 4.9 252 Dormant 5/25/10 195 88 5.5 289 10% yellow 23 13 0.6 37
10 5/22/13 91 50 3.5 145 Dormant 5/22/13 103 66 4.2 173 0% yellow 12 16 0.7 29
Min.-87 50 3.5 145 --99 66 4.2 173 -3 4 0.2 8
Avg.-163 90 6.8 260 --176 99 7.5 283 -13 9 0.7 23
Max.-244 195 16.8 456 --263 205 17.5 486 -23 16 1.2 37
NOTES:
All trees except for those replaced in 2013 exhibited yellowing of foliage on August 1, 2016.
Phytoremediation Tree Measurement Summary
Tree
ID
Date
Planted
Date
Planted
Height
(in)
Width
Middle
(in)
Trunk
Circ.
(in)
Total (Ht +
Width +
Circ.)
(in)
Height
(in)
Width
Middle
(in)
Trunk
Circ.
(in)
Total (Ht
+ Width +
Circ.) (in)
Height
(in)
Width
Middle
(in)
Trunk Circ.
(in)
Total (Ht +
Width + Circ.)
(in)
0
50
100
150
200
250
300
Average Tree Size
Average Tree Size (Inches)Date
I n c h e s
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
July 22, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92304133
92304133
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
ALEXANDER LF- METHANE
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 06, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Lab ID Sample ID Matrix Date Collected Date Received
92304133001 MW-1 Water 07/05/16 13:45 07/06/16 08:55
92304133002 MW-1B Water 07/05/16 13:40 07/06/16 08:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92304133001 MW-1 RSK 175 Modified 1 PASI-CZDO
92304133002 MW-1B RSK 175 Modified 1 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Sample:MW-1 Lab ID:92304133001 Collected:07/05/16 13:45 Received:07/06/16 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 90.3 ug/L 07/20/16 17:02 74-82-8 H510.0 10.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/22/2016 12:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Sample:MW-1B Lab ID:92304133002 Collected:07/05/16 13:40 Received:07/06/16 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 343 ug/L 07/20/16 17:17 74-82-8 H510.0 10.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/22/2016 12:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321519
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Associated Lab Samples:92304133001, 92304133002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1781804
Associated Lab Samples:92304133001, 92304133002
Matrix:Water
AnalyzedMDL
Methane ug/L ND 10.0 N207/20/16 14:4810.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1781805LABORATORY CONTROL SAMPLE:
LCSSpike
Methane ug/L 454 N239611570-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1783837MATRIX SPIKE SAMPLE:
MSSpike
Result
92304098010
Methane ug/L 10700 H5,M1,N239614370-13010100
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304098012
1783838SAMPLE DUPLICATE:
Methane ug/L 7530 H5,N211208380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/22/2016 12:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/22/2016 12:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92304133
ALEXANDER LF- METHANE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92304133001 321519MW-1 RSK 175 Modified
92304133002 321519MW-1B RSK 175 Modified
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/22/2016 12:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 11
Page 10 of 11
Page 11 of 11
#=CL#
July 25, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92304304
92304304
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
ALEXANDER LF (MNA)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 07, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Lab ID Sample ID Matrix Date Collected Date Received
92304304001 MW-6 Water 07/06/16 11:00 07/07/16 10:17
92304304002 MW-16 Water 07/06/16 13:25 07/07/16 10:17
92304304003 MW-5 Water 07/06/16 13:00 07/07/16 10:17
92304304004 MW-24 Water 07/06/16 12:00 07/07/16 10:17
92304304005 MW-25 Water 07/06/16 12:20 07/07/16 10:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92304304001 MW-6 EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AWRC
SM 5210B 1 PASI-ACJH
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ABRJ
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92304304002 MW-16 EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AKDF
SM 5210B 1 PASI-AEWS
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ABRJ
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92304304003 MW-5 EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AKDF
SM 5210B 1 PASI-ACJH
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ABRJ
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92304304004 MW-24 SM 5210B 1 PASI-ACJH
92304304005 MW-25 SM 5210B 1 PASI-ACJH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Sample:MW-6 Lab ID:92304304001 Collected:07/06/16 11:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved ND ug/L 07/14/16 11:12 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 11200 ug/L 07/16/16 00:34500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/13/16 16:00 18496-25-8 M310001001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 07/12/16 22:2607/08/16 04:00200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3670J ug/L 07/08/16 19:53 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 365J ug/L 07/08/16 08:111000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4230 ug/L 07/16/16 02:42 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 07/22/16 15:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2840 ug/L 07/23/16 12:58 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Sample:MW-16 Lab ID:92304304002 Collected:07/06/16 13:25 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved ND ug/L 07/14/16 11:15 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 46100 ug/L 07/16/16 00:45500010001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 07/13/16 09:1007/08/16 06:22200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 6860J ug/L 07/08/16 20:04 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 83.2J ug/L 07/08/16 08:251000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 6020 ug/L 07/16/16 02:43 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 07/22/16 15:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1310 ug/L 07/23/16 13:08 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Sample:MW-5 Lab ID:92304304003 Collected:07/06/16 13:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 13100 ug/L 07/14/16 11:18 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 112000 ug/L 07/16/16 00:57500010001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 2770 ug/L 07/12/16 22:2607/08/16 04:00200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4480J ug/L 07/08/16 20:14 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 07/08/16 08:241000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4480 ug/L 07/16/16 02:44 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 50000 ug/L 07/22/16 15:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2440 ug/L 07/23/16 13:26 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Sample:MW-24 Lab ID:92304304004 Collected:07/06/16 12:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 07/12/16 22:2607/08/16 04:00200020001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Sample:MW-25 Lab ID:92304304005 Collected:07/06/16 12:20 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 07/12/16 22:2607/08/16 04:00200020001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320919
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1778357
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Iron, Dissolved ug/L ND 50.0 07/14/16 10:3225.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1778358LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Dissolved ug/L 49505000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1778359MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098001
1778360
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron, Dissolved ug/L 5000 86 75-12586 0 205000180002230022300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321357
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1780858
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 07/15/16 20:021000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1780859LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4950050000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780860MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304615003
1780861
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M15000013080-120130 0 255000012.6 mg/L 77600 77800
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780862MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304785002
1780863
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 118 80-12087 8 2550000130 mg/L 189000 174000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321057
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92304304001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779211
Associated Lab Samples:92304304001
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 07/13/16 16:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779212LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 511J500 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779213MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304304001
1779214
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M3500690-1106 10500NDNDND
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779215MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930034
1779216
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M150012090-110120 0 10500ND603J603J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320362
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92304304001, 92304304003, 92304304004, 92304304005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775308
Associated Lab Samples:92304304001, 92304304003, 92304304004, 92304304005
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 B207/12/16 22:262000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775309LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 211000198000 107 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304000001
1775310SAMPLE DUPLICATE:
BOD, 5 day ug/L ND 10ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320385
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92304304002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775341
Associated Lab Samples:92304304002
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 07/13/16 09:102000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775342LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 202000198000 102 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304304002
1775343SAMPLE DUPLICATE:
BOD, 5 day ug/L ND 10ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320518
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1776040
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 07/08/16 18:221000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1776041LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19100J20000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1776042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92302775001
1776043
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 91 90-11091 0 102000025.2 mg/L 43400J 43500J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320395
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775344
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 07/08/16 08:0810.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775345LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24302500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1775346MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304304001
1775347
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 98 90-11099 0 102500365J28302830
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321256
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1780514
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 07/16/16 02:22500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1780515LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2020020000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780516MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304120001
1780517
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000014590-110154 2 101000033.5 mg/L 47900 48900
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780518MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930032
1780519
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000011590-110116 0 1010000183002980029900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
322212
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1785501
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 07/22/16 15:3012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1785502LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 383000375000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1785503MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304578001
1785504
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M3375000090-1100 0 33750001240 mg/L 1240000 1240000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1785505MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930035
1785506
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M13750008390-11083 0 337500091000404000404000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
322299
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92304304001, 92304304002, 92304304003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1786055
Associated Lab Samples:92304304001, 92304304002, 92304304003
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 07/23/16 02:03500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1786056LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2310025000 93 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1786057MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098001
1786058
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250008690-11094 8 102500016402310025000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1786059MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304304003
1786060
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 101 90-11091 10 102500024402770025200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92304304
ALEXANDER LF (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92304304001 320919 321096MW-6 EPA 3010 EPA 6010
92304304002 320919 321096MW-16 EPA 3010 EPA 6010
92304304003 320919 321096MW-5 EPA 3010 EPA 6010
92304304001 321357MW-6 SM 2320B
92304304002 321357MW-16 SM 2320B
92304304003 321357MW-5 SM 2320B
92304304001 321057MW-6 SM 4500-S2D
92304304001 320362 320386MW-6 SM 5210B SM 5210B
92304304002 320385 320388MW-16 SM 5210B SM 5210B
92304304003 320362 320386MW-5 SM 5210B SM 5210B
92304304004 320362 320386MW-24 SM 5210B SM 5210B
92304304005 320362 320386MW-25 SM 5210B SM 5210B
92304304001 320518MW-6 EPA 300.0
92304304002 320518MW-16 EPA 300.0
92304304003 320518MW-5 EPA 300.0
92304304001 320395MW-6 EPA 353.2
92304304002 320395MW-16 EPA 353.2
92304304003 320395MW-5 EPA 353.2
92304304001 321256MW-6 SM 4500-Cl-E
92304304002 321256MW-16 SM 4500-Cl-E
92304304003 321256MW-5 SM 4500-Cl-E
92304304001 322212MW-6 SM 5220D
92304304002 322212MW-16 SM 5220D
92304304003 322212MW-5 SM 5220D
92304304001 322299MW-6 SM 5310B
92304304002 322299MW-16 SM 5310B
92304304003 322299MW-5 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 04:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
July 26, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92303930
92303930
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
ALEXANDER LF (SWS)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between July 05, 2016
and July 07, 2016. The results relate only to the samples included in this report. Results reported
herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 190
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 190
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID Matrix Date Collected Date Received
92303930002 MW-10 Water 07/01/16 02:00 07/05/16 12:30
92303930003 MW-13 Water 07/01/16 05:00 07/05/16 12:30
92303930004 MW-14 Water 07/01/16 16:45 07/05/16 12:30
92303930005 MW-15 Water 07/01/16 17:50 07/05/16 12:30
92303930006 MW-17 Water 07/01/16 14:30 07/05/16 12:30
92303930007 MW-19 Water 07/01/16 15:00 07/05/16 12:30
92303930008 MW-20 Water 07/01/16 14:35 07/05/16 12:30
92303930009 MW-21 Water 07/01/16 14:17 07/05/16 12:30
92303930010 MW-22 Water 07/01/16 17:25 07/05/16 12:30
92303930011 MW-23 Water 07/01/16 17:30 07/05/16 12:30
92303930012 MW-32 Water 07/01/16 15:27 07/05/16 12:30
92303930013 MW-33 Water 07/01/16 16:00 07/05/16 12:30
92303930014 MW-34 Water 07/01/16 17:20 07/05/16 12:30
92303930015 SW-3 Water 07/01/16 13:30 07/05/16 12:30
92303930016 SW-4R Water 07/01/16 14:01 07/05/16 12:30
92303930017 SW-5 Water 07/01/16 14:00 07/05/16 12:30
92303930018 SW-6 Water 07/01/16 16:05 07/05/16 12:30
92304098001 MW-12 Water 07/05/16 11:30 07/06/16 08:56
92304098002 MW-12D Water 07/05/16 11:45 07/06/16 08:56
92304098003 MW-16 Water 07/05/16 11:00 07/06/16 08:56
92304098004 EB Water 07/05/16 18:00 07/06/16 08:56
92304098005 FB Water 07/05/16 18:05 07/06/16 08:56
92304098006 TB Water 07/05/16 00:00 07/06/16 08:56
92304098007 MW-1 Water 07/05/16 13:45 07/06/16 08:56
92304098008 MW-1B Water 07/05/16 13:40 07/06/16 08:56
92304098009 MW-4R Water 07/05/16 16:00 07/06/16 08:56
92304098010 MW-5 Water 07/05/16 16:20 07/06/16 08:56
92304098011 MW-12 Water 07/05/16 11:30 07/06/16 08:56
92304098012 MW-16 Water 07/05/16 11:00 07/06/16 08:56
92303930031 MW-6 Water 07/06/16 11:00 07/07/16 10:17
92303930032 MW-24 Water 07/06/16 12:00 07/07/16 10:17
92303930034 MW-25 Water 07/06/16 12:20 07/07/16 10:17
92303930036 MW-9 Water 07/06/16 09:30 07/07/16 10:17
92303930037 MW-2 Water 07/06/16 11:40 07/07/16 10:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 190
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92303930002 MW-10 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930003 MW-13 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930004 MW-14 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930005 MW-15 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930006 MW-17 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930007 MW-19 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930008 MW-20 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930009 MW-21 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930010 MW-22 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930011 MW-23 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930012 MW-32 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930013 MW-33 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930014 MW-34 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
92303930015 SW-3 EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92303930016 SW-4R EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92303930017 SW-5 EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92303930018 SW-6 EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92304098001 MW-12 RSK 175 Modified 1 PASI-CZDO
EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 190
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AWRC
SM 5210B 1 PASI-ASER
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-AAES2
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92304098002 MW-12D RSK 175 Modified 1 PASI-CZDO
EPA 6010 15 PASI-ASH1
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CGAW
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AWRC
SM 5210B 1 PASI-ASER
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-AAES2
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92304098003 MW-16 EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
92304098004 EB EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
92304098005 FB EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
92304098006 TB EPA 8260 67 PASI-CGAW
92304098007 MW-1 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 190
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-CN-E 1 PASI-AAES2
92304098008 MW-1B EPA 8081 20 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92304098009 MW-4R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92304098010 MW-5 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
RSK 175 Modified 1 PASI-CZDO
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-CN-E 1 PASI-AAES2
92304098011 MW-12 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 190
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92304098012 MW-16 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
RSK 175 Modified 1 PASI-CZDO
EPA 8270 111 PASI-CBPJ
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92303930031 MW-6 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92303930032 MW-24 EPA 6010 15 PASI-ASH1
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AWRC
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ABRJ
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92303930034 MW-25 EPA 6010 15 PASI-ASH1
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AWRC
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ABRJ
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92303930036 MW-9 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 190
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92303930037 MW-2 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-10 Lab ID:92303930002 Collected:07/01/16 02:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 19:55 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 19:55 7440-38-207/07/16 18:4010.0 2.5 1
Barium 25.4J ug/L 07/08/16 19:55 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 19:55 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 19:55 7440-43-907/07/16 18:401.0 0.50 1
Chromium ND ug/L 07/08/16 19:55 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt ND ug/L 07/08/16 19:55 7440-48-407/07/16 18:4010.0 2.5 1
Copper ND ug/L 07/08/16 19:55 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 19:55 7439-92-107/07/16 18:4010.0 2.5 1
Nickel ND ug/L 07/08/16 19:55 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 19:55 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 19:55 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 19:55 7440-28-007/07/16 18:405.5 5.0 1
Vanadium ND ug/L 07/08/16 19:55 7440-62-207/07/16 18:4025.0 2.5 1
Zinc ND ug/L 07/08/16 19:55 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 00:15 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 00:15 107-13-12001.9 1
Benzene ND ug/L 07/08/16 00:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 00:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 00:15 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 00:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 00:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 00:15 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 00:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 00:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 00:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 00:15 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 00:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 00:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 00:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 00:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 00:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 00:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 00:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 00:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 00:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 00:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 00:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 00:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.27J ug/L 07/08/16 00:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 00:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 00:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 00:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 00:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-10 Lab ID:92303930002 Collected:07/01/16 02:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 00:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 00:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 00:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 00:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 00:15 108-10-11000.33 1
Styrene ND ug/L 07/08/16 00:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 00:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 00:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 00:15 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 00:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 00:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 00:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 00:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 00:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 00:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 00:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 00:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 00:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %07/08/16 00:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 00:15 17060-07-070-130 1
Toluene-d8 (S)102 %07/08/16 00:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-13 Lab ID:92303930003 Collected:07/01/16 05:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 19:59 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 19:59 7440-38-207/07/16 18:4010.0 2.5 1
Barium 58.1J ug/L 07/08/16 19:59 7440-39-307/07/16 18:401002.5 1
Beryllium 0.73J ug/L 07/08/16 19:59 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 19:59 7440-43-907/07/16 18:401.0 0.50 1
Chromium 18.7 ug/L 07/08/16 19:59 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 7.5J ug/L 07/08/16 19:59 7440-48-407/07/16 18:4010.0 2.5 1
Copper 41.6 ug/L 07/08/16 19:59 7440-50-807/07/16 18:4010.0 2.5 1
Lead 10.6 ug/L 07/08/16 19:59 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 26.2J ug/L 07/08/16 19:59 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 19:59 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 19:59 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 19:59 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 19.8J ug/L 07/08/16 19:59 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 28.6 ug/L 07/08/16 19:59 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 00:32 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 00:32 107-13-12001.9 1
Benzene ND ug/L 07/08/16 00:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 00:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 00:32 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 00:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 00:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 00:32 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 00:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 00:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 00:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 00:32 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 00:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 00:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 00:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 00:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 00:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 00:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 00:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 00:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 00:32 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 00:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 00:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 00:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 00:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 00:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 00:32 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 00:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 00:32 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-13 Lab ID:92303930003 Collected:07/01/16 05:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 00:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 00:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 00:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 00:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 00:32 108-10-11000.33 1
Styrene ND ug/L 07/08/16 00:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 00:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 00:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 00:32 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 00:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 00:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 00:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 00:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 00:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 00:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 00:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 00:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 00:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 00:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 00:32 17060-07-070-130 1
Toluene-d8 (S)102 %07/08/16 00:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-14 Lab ID:92303930004 Collected:07/01/16 16:45 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:02 7440-36-007/07/16 18:406.0 3.8 1
Arsenic 12.3 ug/L 07/08/16 20:02 7440-38-207/07/16 18:4010.0 2.5 1
Barium 175 ug/L 07/08/16 20:02 7440-39-307/07/16 18:401002.5 1
Beryllium 0.90J ug/L 07/08/16 20:02 7440-41-707/07/16 18:401.0 0.50 1
Cadmium 0.89J ug/L 07/08/16 20:02 7440-43-907/07/16 18:401.0 0.50 1
Chromium 6.6J ug/L 07/08/16 20:02 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 92.5 ug/L 07/08/16 20:02 7440-48-407/07/16 18:4010.0 2.5 1
Copper 14.0 ug/L 07/08/16 20:02 7440-50-807/07/16 18:4010.0 2.5 1
Lead 7.5J ug/L 07/08/16 20:02 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 19.2J ug/L 07/08/16 20:02 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:02 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:02 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:02 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 7.3J ug/L 07/08/16 20:02 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 32.2 ug/L 07/08/16 20:02 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 00:49 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 00:49 107-13-12001.9 1
Benzene 0.34J ug/L 07/08/16 00:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 00:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 00:49 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 00:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 00:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 00:49 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 00:49 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 00:49 56-23-51.0 0.25 1
Chlorobenzene 0.63J ug/L 07/08/16 00:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 00:49 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 00:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 00:49 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 00:49 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 00:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 00:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 00:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 00:49 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.6 ug/L 07/08/16 00:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 00:49 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 00:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 00:49 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 00:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 5.6 ug/L 07/08/16 00:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 00:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 00:49 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 00:49 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 00:49 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-14 Lab ID:92303930004 Collected:07/01/16 16:45 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 00:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 00:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 00:49 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 00:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 00:49 108-10-11000.33 1
Styrene ND ug/L 07/08/16 00:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 00:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 00:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 00:49 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 00:49 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 00:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 00:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 00:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 00:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 00:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 00:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 00:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 00:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %07/08/16 00:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)116 %07/08/16 00:49 17060-07-070-130 1
Toluene-d8 (S)99 %07/08/16 00:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-15 Lab ID:92303930005 Collected:07/01/16 17:50 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:14 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:14 7440-38-207/07/16 18:4010.0 2.5 1
Barium 52.2J ug/L 07/08/16 20:14 7440-39-307/07/16 18:401002.5 1
Beryllium 0.90J ug/L 07/08/16 20:14 7440-41-707/07/16 18:401.0 0.50 1
Cadmium 1.6 ug/L 07/08/16 20:14 7440-43-907/07/16 18:401.0 0.50 1
Chromium ND ug/L 07/08/16 20:14 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 29.7 ug/L 07/08/16 20:14 7440-48-407/07/16 18:4010.0 2.5 1
Copper 4.3J ug/L 07/08/16 20:14 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:14 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 3.9J ug/L 07/08/16 20:14 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:14 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:14 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:14 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 2.5J ug/L 07/08/16 20:14 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 26.6 ug/L 07/08/16 20:14 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 01:06 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 01:06 107-13-12001.9 1
Benzene 3.8 ug/L 07/08/16 01:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 01:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 01:06 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 01:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 01:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 01:06 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 01:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 01:06 56-23-51.0 0.25 1
Chlorobenzene 0.66J ug/L 07/08/16 01:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 01:06 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 01:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 01:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 01:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 01:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 01:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 01:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 01:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.3 ug/L 07/08/16 01:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 01:06 110-57-61001.0 1
1,1-Dichloroethane 2.3J ug/L 07/08/16 01:06 75-34-35.0 0.32 1
1,2-Dichloroethane 0.37J ug/L 07/08/16 01:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 01:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 11.5 ug/L 07/08/16 01:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 01:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 01:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 01:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 01:06 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-15 Lab ID:92303930005 Collected:07/01/16 17:50 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 01:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 01:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 01:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 01:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 01:06 108-10-11000.33 1
Styrene ND ug/L 07/08/16 01:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 01:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 01:06 79-34-53.0 0.40 1
Tetrachloroethene 0.66J ug/L 07/08/16 01:06 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 01:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 01:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 01:06 79-00-51.0 0.29 1
Trichloroethene 1.2 ug/L 07/08/16 01:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 01:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 01:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 01:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 01:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 01:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 01:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 01:06 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 01:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-17 Lab ID:92303930006 Collected:07/01/16 14:30 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:17 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:17 7440-38-207/07/16 18:4010.0 2.5 1
Barium 178 ug/L 07/08/16 20:17 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:17 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 20:17 7440-43-907/07/16 18:401.0 0.50 1
Chromium 31.3 ug/L 07/08/16 20:17 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 51.4 ug/L 07/08/16 20:17 7440-48-407/07/16 18:4010.0 2.5 1
Copper 22.5 ug/L 07/08/16 20:17 7440-50-807/07/16 18:4010.0 2.5 1
Lead 10.6 ug/L 07/08/16 20:17 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 12.4J ug/L 07/08/16 20:17 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:17 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:17 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:17 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 48.7 ug/L 07/08/16 20:17 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 53.7 ug/L 07/08/16 20:17 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 01:24 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 01:24 107-13-12001.9 1
Benzene 0.80J ug/L 07/08/16 01:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 01:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 01:24 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 01:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 01:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 01:24 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 01:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 01:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 01:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 01:24 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 01:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 01:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 01:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 01:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 01:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 01:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 01:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.45J ug/L 07/08/16 01:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 01:24 110-57-61001.0 1
1,1-Dichloroethane 0.91J ug/L 07/08/16 01:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 01:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 01:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.3J ug/L 07/08/16 01:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 01:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 01:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 01:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 01:24 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-17 Lab ID:92303930006 Collected:07/01/16 14:30 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 01:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 01:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 01:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 01:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 01:24 108-10-11000.33 1
Styrene ND ug/L 07/08/16 01:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 01:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 01:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 01:24 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 01:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 01:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 01:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 01:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 01:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 01:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 01:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 01:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 01:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 01:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 01:24 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 01:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-19 Lab ID:92303930007 Collected:07/01/16 15:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:20 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:20 7440-38-207/07/16 18:4010.0 2.5 1
Barium 16.9J ug/L 07/08/16 20:20 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:20 7440-41-707/07/16 18:401.0 0.50 1
Cadmium 0.62J ug/L 07/08/16 20:20 7440-43-907/07/16 18:401.0 0.50 1
Chromium ND ug/L 07/08/16 20:20 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt ND ug/L 07/08/16 20:20 7440-48-407/07/16 18:4010.0 2.5 1
Copper 2.6J ug/L 07/08/16 20:20 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:20 7439-92-107/07/16 18:4010.0 2.5 1
Nickel ND ug/L 07/08/16 20:20 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:20 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:20 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:20 7440-28-007/07/16 18:405.5 5.0 1
Vanadium ND ug/L 07/08/16 20:20 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 7.5J ug/L 07/08/16 20:20 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 01:41 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 01:41 107-13-12001.9 1
Benzene ND ug/L 07/08/16 01:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 01:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 01:41 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 01:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 01:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 01:41 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 01:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 01:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 01:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 01:41 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 01:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 01:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 01:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 01:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 01:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 01:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 01:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 01:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 01:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 01:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 01:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 01:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 01:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 01:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 01:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 01:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 01:41 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-19 Lab ID:92303930007 Collected:07/01/16 15:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 01:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 01:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 01:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 01:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 01:41 108-10-11000.33 1
Styrene ND ug/L 07/08/16 01:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 01:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 01:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 01:41 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 01:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 01:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 01:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 01:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 01:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 01:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 01:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 01:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 01:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %07/08/16 01:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 01:41 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 01:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-20 Lab ID:92303930008 Collected:07/01/16 14:35 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:23 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:23 7440-38-207/07/16 18:4010.0 2.5 1
Barium 44.5J ug/L 07/08/16 20:23 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:23 7440-41-707/07/16 18:401.0 0.50 1
Cadmium 1.2 ug/L 07/08/16 20:23 7440-43-907/07/16 18:401.0 0.50 1
Chromium ND ug/L 07/08/16 20:23 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt ND ug/L 07/08/16 20:23 7440-48-407/07/16 18:4010.0 2.5 1
Copper ND ug/L 07/08/16 20:23 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:23 7439-92-107/07/16 18:4010.0 2.5 1
Nickel ND ug/L 07/08/16 20:23 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:23 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:23 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:23 7440-28-007/07/16 18:405.5 5.0 1
Vanadium ND ug/L 07/08/16 20:23 7440-62-207/07/16 18:4025.0 2.5 1
Zinc ND ug/L 07/08/16 20:23 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 01:58 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 01:58 107-13-12001.9 1
Benzene ND ug/L 07/08/16 01:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 01:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 01:58 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 01:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 01:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 01:58 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 01:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 01:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 01:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 01:58 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 01:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 01:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 01:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 01:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 01:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 01:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 01:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 01:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 01:58 110-57-61001.0 1
1,1-Dichloroethane 0.36J ug/L 07/08/16 01:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 01:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 01:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 01:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 01:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 01:58 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 01:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 01:58 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-20 Lab ID:92303930008 Collected:07/01/16 14:35 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 01:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 01:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 01:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 01:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 01:58 108-10-11000.33 1
Styrene ND ug/L 07/08/16 01:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 01:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 01:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 01:58 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 01:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 01:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 01:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 01:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 01:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 01:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 01:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 01:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 01:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 01:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %07/08/16 01:58 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 01:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-21 Lab ID:92303930009 Collected:07/01/16 14:17 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/09/16 13:56 7440-36-0 D307/07/16 18:4030.0 19.0 5
Arsenic ND ug/L 07/09/16 13:56 7440-38-2 D307/07/16 18:4050.0 12.5 5
Barium 161J ug/L 07/09/16 13:56 7440-39-307/07/16 18:4050012.5 5
Beryllium ND ug/L 07/09/16 13:56 7440-41-7 D307/07/16 18:405.0 2.5 5
Cadmium ND ug/L 07/09/16 13:56 7440-43-9 D307/07/16 18:405.0 2.5 5
Chromium 21.0J ug/L 07/09/16 13:56 7440-47-3 D307/07/16 18:4050.0 12.5 5
Cobalt 23.1J ug/L 07/09/16 13:56 7440-48-4 D307/07/16 18:4050.0 12.5 5
Copper 18.0J ug/L 07/09/16 13:56 7440-50-8 D307/07/16 18:4050.0 12.5 5
Lead ND ug/L 07/09/16 13:56 7439-92-1 D307/07/16 18:4050.0 12.5 5
Nickel 23.5J ug/L 07/09/16 13:56 7440-02-0 D307/07/16 18:4025012.5 5
Selenium ND ug/L 07/09/16 13:56 7782-49-2 D307/07/16 18:4050.0 25.0 5
Silver ND ug/L 07/09/16 13:56 7440-22-4 D307/07/16 18:4050.0 12.5 5
Thallium ND ug/L 07/09/16 13:56 7440-28-0 D307/07/16 18:4027.5 25.0 5
Vanadium 20.2J ug/L 07/09/16 13:56 7440-62-2 D307/07/16 18:4012512.5 5
Zinc 26.8J ug/L 07/09/16 13:56 7440-66-6 D307/07/16 18:4050.0 25.0 5
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 02:15 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 02:15 107-13-12001.9 1
Benzene ND ug/L 07/08/16 02:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 02:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 02:15 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 02:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 02:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 02:15 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 02:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 02:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 02:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 02:15 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 02:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 02:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 02:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 02:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 02:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 02:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 02:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 02:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 02:15 110-57-61001.0 1
1,1-Dichloroethane 0.40J ug/L 07/08/16 02:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 02:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 02:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.64J ug/L 07/08/16 02:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 02:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 02:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 02:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 02:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-21 Lab ID:92303930009 Collected:07/01/16 14:17 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 02:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 02:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 02:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 02:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 02:15 108-10-11000.33 1
Styrene ND ug/L 07/08/16 02:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 02:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 02:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 02:15 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 02:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 02:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 02:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 02:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 02:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 02:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 02:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 02:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 02:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 02:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 02:15 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 02:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-22 Lab ID:92303930010 Collected:07/01/16 17:25 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:30 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:30 7440-38-207/07/16 18:4010.0 2.5 1
Barium 76.6J ug/L 07/08/16 20:30 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:30 7440-41-707/07/16 18:401.0 0.50 1
Cadmium 1.2 ug/L 07/08/16 20:30 7440-43-907/07/16 18:401.0 0.50 1
Chromium 5.1J ug/L 07/08/16 20:30 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 5.4J ug/L 07/08/16 20:30 7440-48-407/07/16 18:4010.0 2.5 1
Copper 3.3J ug/L 07/08/16 20:30 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:30 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 5.3J ug/L 07/08/16 20:30 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:30 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:30 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:30 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 4.8J ug/L 07/08/16 20:30 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 13.8 ug/L 07/08/16 20:30 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 02:32 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 02:32 107-13-12001.9 1
Benzene ND ug/L 07/08/16 02:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 02:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 02:32 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 02:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 02:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 02:32 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 02:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 02:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 02:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 02:32 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 02:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 02:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 02:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 02:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 02:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 02:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 02:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 02:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 02:32 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 02:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 02:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 02:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 02:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 02:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 02:32 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 02:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 02:32 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-22 Lab ID:92303930010 Collected:07/01/16 17:25 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 02:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 02:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 02:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 02:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 02:32 108-10-11000.33 1
Styrene ND ug/L 07/08/16 02:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 02:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 02:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 02:32 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 02:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 02:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 02:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 02:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 02:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 02:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 02:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 02:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 02:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %07/08/16 02:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %07/08/16 02:32 17060-07-070-130 1
Toluene-d8 (S)98 %07/08/16 02:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-23 Lab ID:92303930011 Collected:07/01/16 17:30 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:33 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:33 7440-38-207/07/16 18:4010.0 2.5 1
Barium 90.5J ug/L 07/08/16 20:33 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:33 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 20:33 7440-43-907/07/16 18:401.0 0.50 1
Chromium 10.8 ug/L 07/08/16 20:33 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 23.6 ug/L 07/08/16 20:33 7440-48-407/07/16 18:4010.0 2.5 1
Copper 6.1J ug/L 07/08/16 20:33 7440-50-807/07/16 18:4010.0 2.5 1
Lead 3.1J ug/L 07/08/16 20:33 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 13.6J ug/L 07/08/16 20:33 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:33 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:33 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:33 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 12.2J ug/L 07/08/16 20:33 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 16.5 ug/L 07/08/16 20:33 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 02:50 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 02:50 107-13-12001.9 1
Benzene ND ug/L 07/08/16 02:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 02:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 02:50 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 02:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 02:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 02:50 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 02:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 02:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 02:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 02:50 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 02:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 02:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 02:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 02:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 02:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 02:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 02:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 02:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 02:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 02:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 02:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 02:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.94J ug/L 07/08/16 02:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 02:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 02:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 02:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 02:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-23 Lab ID:92303930011 Collected:07/01/16 17:30 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 02:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 02:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 02:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 02:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 02:50 108-10-11000.33 1
Styrene ND ug/L 07/08/16 02:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 02:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 02:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 02:50 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 02:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 02:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 02:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 02:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 02:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 02:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 02:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 02:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 02:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %07/08/16 02:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 02:50 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 02:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-32 Lab ID:92303930012 Collected:07/01/16 15:27 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:36 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:36 7440-38-207/07/16 18:4010.0 2.5 1
Barium 21.5J ug/L 07/08/16 20:36 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:36 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 20:36 7440-43-907/07/16 18:401.0 0.50 1
Chromium 8.0J ug/L 07/08/16 20:36 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt ND ug/L 07/08/16 20:36 7440-48-407/07/16 18:4010.0 2.5 1
Copper ND ug/L 07/08/16 20:36 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:36 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 7.3J ug/L 07/08/16 20:36 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:36 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:36 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:36 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 4.9J ug/L 07/08/16 20:36 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 23.7 ug/L 07/08/16 20:36 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 03:07 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 03:07 107-13-12001.9 1
Benzene ND ug/L 07/08/16 03:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 03:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 03:07 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 03:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 03:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 03:07 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 03:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 03:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 03:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 03:07 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 03:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 03:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 03:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 03:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 03:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 03:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 03:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 03:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 03:07 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 03:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 03:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 03:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 03:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 03:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 03:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 03:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 03:07 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-32 Lab ID:92303930012 Collected:07/01/16 15:27 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 03:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 03:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 03:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 03:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 03:07 108-10-11000.33 1
Styrene ND ug/L 07/08/16 03:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 03:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 03:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 03:07 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 03:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 03:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 03:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 03:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 03:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 03:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 03:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 03:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 03:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 03:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 03:07 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 03:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-33 Lab ID:92303930013 Collected:07/01/16 16:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:39 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:39 7440-38-207/07/16 18:4010.0 2.5 1
Barium 19.8J ug/L 07/08/16 20:39 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:39 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 20:39 7440-43-907/07/16 18:401.0 0.50 1
Chromium ND ug/L 07/08/16 20:39 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt 6.1J ug/L 07/08/16 20:39 7440-48-407/07/16 18:4010.0 2.5 1
Copper ND ug/L 07/08/16 20:39 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:39 7439-92-107/07/16 18:4010.0 2.5 1
Nickel ND ug/L 07/08/16 20:39 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:39 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:39 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:39 7440-28-007/07/16 18:405.5 5.0 1
Vanadium ND ug/L 07/08/16 20:39 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 5.8J ug/L 07/08/16 20:39 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 03:24 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 03:24 107-13-12001.9 1
Benzene ND ug/L 07/08/16 03:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 03:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 03:24 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 03:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 03:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 03:24 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 03:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 03:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 03:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 03:24 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 03:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 03:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 03:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 03:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 03:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 03:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 03:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 03:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 03:24 110-57-61001.0 1
1,1-Dichloroethane 0.43J ug/L 07/08/16 03:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 03:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 03:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.91J ug/L 07/08/16 03:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 03:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 03:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 03:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 03:24 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-33 Lab ID:92303930013 Collected:07/01/16 16:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 03:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 03:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 03:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 03:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 03:24 108-10-11000.33 1
Styrene ND ug/L 07/08/16 03:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 03:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 03:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 03:24 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 03:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 03:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 03:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 03:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 03:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 03:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 03:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 03:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 03:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %07/08/16 03:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %07/08/16 03:24 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 03:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-34 Lab ID:92303930014 Collected:07/01/16 17:20 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/08/16 20:42 7440-36-007/07/16 18:406.0 3.8 1
Arsenic ND ug/L 07/08/16 20:42 7440-38-207/07/16 18:4010.0 2.5 1
Barium 49.0J ug/L 07/08/16 20:42 7440-39-307/07/16 18:401002.5 1
Beryllium ND ug/L 07/08/16 20:42 7440-41-707/07/16 18:401.0 0.50 1
Cadmium ND ug/L 07/08/16 20:42 7440-43-907/07/16 18:401.0 0.50 1
Chromium 8.1J ug/L 07/08/16 20:42 7440-47-307/07/16 18:4010.0 2.5 1
Cobalt ND ug/L 07/08/16 20:42 7440-48-407/07/16 18:4010.0 2.5 1
Copper 10.1 ug/L 07/08/16 20:42 7440-50-807/07/16 18:4010.0 2.5 1
Lead ND ug/L 07/08/16 20:42 7439-92-107/07/16 18:4010.0 2.5 1
Nickel 4.3J ug/L 07/08/16 20:42 7440-02-007/07/16 18:4050.0 2.5 1
Selenium ND ug/L 07/08/16 20:42 7782-49-207/07/16 18:4010.0 5.0 1
Silver ND ug/L 07/08/16 20:42 7440-22-407/07/16 18:4010.0 2.5 1
Thallium ND ug/L 07/08/16 20:42 7440-28-007/07/16 18:405.5 5.0 1
Vanadium 16.7J ug/L 07/08/16 20:42 7440-62-207/07/16 18:4025.0 2.5 1
Zinc 21.0 ug/L 07/08/16 20:42 7440-66-607/07/16 18:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 03:41 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 03:41 107-13-12001.9 1
Benzene ND ug/L 07/08/16 03:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 03:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 03:41 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 03:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 03:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 03:41 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 03:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 03:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 03:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 03:41 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 03:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 03:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 03:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 03:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 03:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 03:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 03:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 03:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 03:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 03:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 03:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 03:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 03:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 03:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 03:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 03:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 03:41 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-34 Lab ID:92303930014 Collected:07/01/16 17:20 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 03:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 03:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 03:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 03:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 03:41 108-10-11000.33 1
Styrene ND ug/L 07/08/16 03:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 03:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 03:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 03:41 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 03:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 03:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 03:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 03:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 03:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 03:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 03:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 03:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 03:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %07/08/16 03:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 03:41 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 03:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-3 Lab ID:92303930015 Collected:07/01/16 13:30 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/10/16 18:26 7440-36-007/07/16 23:006.0 3.8 1
Arsenic ND ug/L 07/10/16 18:26 7440-38-207/07/16 23:0010.0 2.5 1
Barium 32.9J ug/L 07/10/16 18:26 7440-39-307/07/16 23:001002.5 1
Beryllium ND ug/L 07/10/16 18:26 7440-41-707/07/16 23:001.0 0.50 1
Cadmium ND ug/L 07/10/16 18:26 7440-43-907/07/16 23:001.0 0.50 1
Chromium ND ug/L 07/10/16 18:26 7440-47-307/07/16 23:0010.0 2.5 1
Cobalt 32.2 ug/L 07/10/16 18:26 7440-48-407/07/16 23:0010.0 2.5 1
Copper ND ug/L 07/10/16 18:26 7440-50-807/07/16 23:0010.0 2.5 1
Lead ND ug/L 07/10/16 18:26 7439-92-107/07/16 23:0010.0 2.5 1
Nickel ND ug/L 07/10/16 18:26 7440-02-007/07/16 23:0050.0 2.5 1
Selenium ND ug/L 07/10/16 18:26 7782-49-207/07/16 23:0010.0 5.0 1
Silver ND ug/L 07/10/16 18:26 7440-22-407/07/16 23:0010.0 2.5 1
Thallium ND ug/L 07/10/16 18:26 7440-28-007/07/16 23:005.5 5.0 1
Vanadium ND ug/L 07/10/16 18:26 7440-62-207/07/16 23:0025.0 2.5 1
Zinc ND ug/L 07/10/16 18:26 7440-66-607/07/16 23:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 04:51 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 04:51 107-13-12001.9 1
Benzene ND ug/L 07/08/16 04:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 04:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 04:51 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 04:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 04:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 04:51 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 04:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 04:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 04:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 04:51 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 04:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 04:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 04:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 04:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 04:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 04:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 04:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.37J ug/L 07/08/16 04:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 04:51 110-57-61001.0 1
1,1-Dichloroethane 0.37J ug/L 07/08/16 04:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 04:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 04:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.3J ug/L 07/08/16 04:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 04:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 04:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 04:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 04:51 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-3 Lab ID:92303930015 Collected:07/01/16 13:30 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 04:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 04:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 04:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 04:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 04:51 108-10-11000.33 1
Styrene ND ug/L 07/08/16 04:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 04:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 04:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 04:51 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 04:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 04:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 04:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 04:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 04:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 04:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 04:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 04:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 04:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 04:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 04:51 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 04:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-4R Lab ID:92303930016 Collected:07/01/16 14:01 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/10/16 18:35 7440-36-007/07/16 23:006.0 3.8 1
Arsenic ND ug/L 07/10/16 18:35 7440-38-207/07/16 23:0010.0 2.5 1
Barium 40.9J ug/L 07/10/16 18:35 7440-39-307/07/16 23:001002.5 1
Beryllium ND ug/L 07/10/16 18:35 7440-41-707/07/16 23:001.0 0.50 1
Cadmium ND ug/L 07/10/16 18:35 7440-43-907/07/16 23:001.0 0.50 1
Chromium ND ug/L 07/10/16 18:35 7440-47-307/07/16 23:0010.0 2.5 1
Cobalt ND ug/L 07/10/16 18:35 7440-48-407/07/16 23:0010.0 2.5 1
Copper ND ug/L 07/10/16 18:35 7440-50-807/07/16 23:0010.0 2.5 1
Lead ND ug/L 07/10/16 18:35 7439-92-107/07/16 23:0010.0 2.5 1
Nickel ND ug/L 07/10/16 18:35 7440-02-007/07/16 23:0050.0 2.5 1
Selenium ND ug/L 07/10/16 18:35 7782-49-207/07/16 23:0010.0 5.0 1
Silver ND ug/L 07/10/16 18:35 7440-22-407/07/16 23:0010.0 2.5 1
Thallium ND ug/L 07/10/16 18:35 7440-28-007/07/16 23:005.5 5.0 1
Vanadium ND ug/L 07/10/16 18:35 7440-62-207/07/16 23:0025.0 2.5 1
Zinc ND ug/L 07/10/16 18:35 7440-66-607/07/16 23:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 05:08 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 05:08 107-13-12001.9 1
Benzene ND ug/L 07/08/16 05:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 05:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 05:08 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 05:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 05:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 05:08 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 05:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 05:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 05:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 05:08 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 05:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 05:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 05:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 05:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 05:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 05:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 05:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 05:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 05:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 05:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 05:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 05:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 05:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 05:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 05:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 05:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 05:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-4R Lab ID:92303930016 Collected:07/01/16 14:01 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 05:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 05:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 05:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 05:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 05:08 108-10-11000.33 1
Styrene ND ug/L 07/08/16 05:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 05:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 05:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 05:08 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 05:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 05:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 05:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 05:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 05:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 05:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 05:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 05:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 05:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %07/08/16 05:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/08/16 05:08 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 05:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-5 Lab ID:92303930017 Collected:07/01/16 14:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/10/16 18:39 7440-36-007/07/16 23:006.0 3.8 1
Arsenic ND ug/L 07/10/16 18:39 7440-38-207/07/16 23:0010.0 2.5 1
Barium 33.5J ug/L 07/10/16 18:39 7440-39-307/07/16 23:001002.5 1
Beryllium ND ug/L 07/10/16 18:39 7440-41-707/07/16 23:001.0 0.50 1
Cadmium ND ug/L 07/10/16 18:39 7440-43-907/07/16 23:001.0 0.50 1
Chromium ND ug/L 07/10/16 18:39 7440-47-307/07/16 23:0010.0 2.5 1
Cobalt 32.0 ug/L 07/10/16 18:39 7440-48-407/07/16 23:0010.0 2.5 1
Copper ND ug/L 07/10/16 18:39 7440-50-807/07/16 23:0010.0 2.5 1
Lead ND ug/L 07/10/16 18:39 7439-92-107/07/16 23:0010.0 2.5 1
Nickel 3.7J ug/L 07/10/16 18:39 7440-02-007/07/16 23:0050.0 2.5 1
Selenium ND ug/L 07/10/16 18:39 7782-49-207/07/16 23:0010.0 5.0 1
Silver ND ug/L 07/10/16 18:39 7440-22-407/07/16 23:0010.0 2.5 1
Thallium ND ug/L 07/10/16 18:39 7440-28-007/07/16 23:005.5 5.0 1
Vanadium ND ug/L 07/10/16 18:39 7440-62-207/07/16 23:0025.0 2.5 1
Zinc ND ug/L 07/10/16 18:39 7440-66-607/07/16 23:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 03:59 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 03:59 107-13-12001.9 1
Benzene ND ug/L 07/08/16 03:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 03:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 03:59 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 03:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 03:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 03:59 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 03:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 03:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 03:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 03:59 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 03:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 03:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 03:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 03:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 03:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 03:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 03:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.40J ug/L 07/08/16 03:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 03:59 110-57-61001.0 1
1,1-Dichloroethane 0.33J ug/L 07/08/16 03:59 75-34-35.0 0.32 1
1,2-Dichloroethane 0.24J ug/L 07/08/16 03:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 03:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.4J ug/L 07/08/16 03:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 03:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 03:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 03:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 03:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-5 Lab ID:92303930017 Collected:07/01/16 14:00 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 03:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 03:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 03:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 03:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 03:59 108-10-11000.33 1
Styrene ND ug/L 07/08/16 03:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 03:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 03:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 03:59 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 03:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 03:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 03:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 03:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 03:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 03:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 03:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 03:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 03:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 03:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 03:59 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 03:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-6 Lab ID:92303930018 Collected:07/01/16 16:05 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/10/16 18:42 7440-36-007/07/16 23:006.0 3.8 1
Arsenic ND ug/L 07/10/16 18:42 7440-38-207/07/16 23:0010.0 2.5 1
Barium 20.6J ug/L 07/10/16 18:42 7440-39-307/07/16 23:001002.5 1
Beryllium ND ug/L 07/10/16 18:42 7440-41-707/07/16 23:001.0 0.50 1
Cadmium ND ug/L 07/10/16 18:42 7440-43-907/07/16 23:001.0 0.50 1
Chromium ND ug/L 07/10/16 18:42 7440-47-307/07/16 23:0010.0 2.5 1
Cobalt 5.1J ug/L 07/10/16 18:42 7440-48-407/07/16 23:0010.0 2.5 1
Copper ND ug/L 07/10/16 18:42 7440-50-807/07/16 23:0010.0 2.5 1
Lead ND ug/L 07/10/16 18:42 7439-92-107/07/16 23:0010.0 2.5 1
Nickel ND ug/L 07/10/16 18:42 7440-02-007/07/16 23:0050.0 2.5 1
Selenium ND ug/L 07/10/16 18:42 7782-49-207/07/16 23:0010.0 5.0 1
Silver ND ug/L 07/10/16 18:42 7440-22-407/07/16 23:0010.0 2.5 1
Thallium ND ug/L 07/10/16 18:42 7440-28-007/07/16 23:005.5 5.0 1
Vanadium ND ug/L 07/10/16 18:42 7440-62-207/07/16 23:0025.0 2.5 1
Zinc ND ug/L 07/10/16 18:42 7440-66-607/07/16 23:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 04:33 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 04:33 107-13-12001.9 1
Benzene ND ug/L 07/08/16 04:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 04:33 74-97-5 M13.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 04:33 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 04:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 04:33 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 04:33 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 04:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 04:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 04:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 04:33 75-00-3 M110.0 0.54 1
Chloroform ND ug/L 07/08/16 04:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 04:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 04:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 04:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 04:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 04:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 04:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 04:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 04:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/08/16 04:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 04:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 04:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/08/16 04:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 04:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 04:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 04:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 04:33 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:SW-6 Lab ID:92303930018 Collected:07/01/16 16:05 Received:07/05/16 12:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/08/16 04:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 04:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 04:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 04:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 04:33 108-10-11000.33 1
Styrene ND ug/L 07/08/16 04:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 04:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 04:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 04:33 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 04:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 04:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 04:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 04:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 04:33 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 04:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 04:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 04:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 04:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %07/08/16 04:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 04:33 17060-07-070-130 1
Toluene-d8 (S)100 %07/08/16 04:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098001 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 12800 ug/L 07/20/16 15:18 74-82-8 H510.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 18000 ug/L 07/14/16 10:38 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 125000 ug/L 07/14/16 20:37500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 2300 ug/L 07/12/16 02:0007/07/16 04:18200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3660J ug/L 07/07/16 19:02 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 07/07/16 08:341000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 10300 ug/L 07/14/16 13:21 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 36000 ug/L 07/13/16 17:4525000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1640 ug/L 07/23/16 10:11 7440-44-0 M110005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12D Lab ID:92304098002 Collected:07/05/16 11:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 5980 ug/L 07/20/16 15:46 74-82-8 H510.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:00 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:00 7440-38-207/11/16 20:3010.0 2.5 1
Barium 9.9J ug/L 07/18/16 20:00 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:00 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:00 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 20:00 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt ND ug/L 07/18/16 20:00 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 20:00 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:00 7439-92-107/11/16 20:3010.0 2.5 1
Nickel ND ug/L 07/18/16 20:00 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:00 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:00 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:00 7440-28-007/11/16 20:305.5 5.0 1
Vanadium ND ug/L 07/18/16 20:00 7440-62-207/11/16 20:3025.0 2.5 1
Zinc ND ug/L 07/18/16 20:00 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 283 ug/L 07/14/16 10:47 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 05:25 67-64-110010.0 1
Acrylonitrile ND ug/L 07/08/16 05:25 107-13-12001.9 1
Benzene 0.44J ug/L 07/08/16 05:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 05:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 05:25 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 05:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 05:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 05:25 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 05:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 05:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 05:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 05:25 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 05:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 05:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 05:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 05:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 05:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 05:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 05:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/08/16 05:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 05:25 110-57-61001.0 1
1,1-Dichloroethane 0.38J ug/L 07/08/16 05:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 05:25 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12D Lab ID:92304098002 Collected:07/05/16 11:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 07/08/16 05:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.75J ug/L 07/08/16 05:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 05:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 05:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 05:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 05:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 05:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/08/16 05:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 05:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/08/16 05:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 05:25 108-10-11000.33 1
Styrene ND ug/L 07/08/16 05:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 05:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 05:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 05:25 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 05:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/08/16 05:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 05:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 05:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 05:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 05:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 05:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 05:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 05:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 05:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %07/08/16 05:25 17060-07-070-130 1
Toluene-d8 (S)103 %07/08/16 05:25 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 381000 ug/L 07/14/16 20:51500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 07/12/16 02:0007/07/16 04:18200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1290J ug/L 07/07/16 19:34 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 07/07/16 08:351000010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12D Lab ID:92304098002 Collected:07/05/16 11:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 56600 ug/L 07/14/16 13:22 16887-00-6200010002
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 07/13/16 17:4525000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 3160 ug/L 07/23/16 11:08 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-16 Lab ID:92304098003 Collected:07/05/16 11:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:09 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:09 7440-38-207/11/16 20:3010.0 2.5 1
Barium 58.2J ug/L 07/18/16 20:09 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:09 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:09 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 20:09 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 91.0 ug/L 07/18/16 20:09 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 20:09 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:09 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 7.1J ug/L 07/18/16 20:09 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:09 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:09 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:09 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:09 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 20:09 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 9.3J ug/L 07/18/16 20:09 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:25 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 05:42 67-64-110010.0 1
Acetonitrile ND ug/L 07/08/16 05:42 75-05-855.0 2.2 1
Acrolein ND ug/L 07/08/16 05:42 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/08/16 05:42 107-13-12001.9 1
Allyl chloride ND ug/L 07/08/16 05:42 107-05-110.0 1.5 1
Benzene 2.9 ug/L 07/08/16 05:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 05:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 05:42 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 05:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 05:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 05:42 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 05:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 05:42 56-23-51.0 0.25 1
Chlorobenzene 0.66J ug/L 07/08/16 05:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 05:42 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 05:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 05:42 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/08/16 05:42 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 05:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 05:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 05:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 05:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 05:42 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/08/16 05:42 541-73-15.0 0.24 1
1,4-Dichlorobenzene 2.6 ug/L 07/08/16 05:42 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-16 Lab ID:92304098003 Collected:07/05/16 11:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 05:42 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/08/16 05:42 75-71-85.0 0.21 1
1,1-Dichloroethane 8.7 ug/L 07/08/16 05:42 75-34-35.0 0.32 1
1,2-Dichloroethane 0.45J ug/L 07/08/16 05:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 05:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 24.4 ug/L 07/08/16 05:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 05:42 156-60-55.0 0.49 1
1,2-Dichloropropane 0.89J ug/L 07/08/16 05:42 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/08/16 05:42 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/08/16 05:42 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/08/16 05:42 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 05:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 05:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 05:42 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/08/16 05:42 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/08/16 05:42 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/08/16 05:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 05:42 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/08/16 05:42 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/08/16 05:42 126-98-71000.93 1
Methylene Chloride ND ug/L 07/08/16 05:42 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 07/08/16 05:42 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 05:42 108-10-11000.33 1
Naphthalene ND ug/L 07/08/16 05:42 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/08/16 05:42 107-12-01503.6 1
Styrene ND ug/L 07/08/16 05:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 05:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 05:42 79-34-53.0 0.40 1
Tetrachloroethene 1.3 ug/L 07/08/16 05:42 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 05:42 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/08/16 05:42 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/08/16 05:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 05:42 79-00-51.0 0.29 1
Trichloroethene 2.1 ug/L 07/08/16 05:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 05:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 05:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 05:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 05:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 05:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %07/08/16 05:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 05:42 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 05:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:EB Lab ID:92304098004 Collected:07/05/16 18:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:12 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:12 7440-38-207/11/16 20:3010.0 2.5 1
Barium ND ug/L 07/18/16 20:12 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:12 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:12 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 20:12 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt ND ug/L 07/18/16 20:12 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 20:12 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:12 7439-92-107/11/16 20:3010.0 2.5 1
Nickel ND ug/L 07/18/16 20:12 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:12 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:12 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:12 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:12 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 20:12 7440-62-207/11/16 20:3025.0 2.5 1
Zinc ND ug/L 07/18/16 20:12 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:32 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/07/16 23:06 67-64-110010.0 1
Acetonitrile ND ug/L 07/07/16 23:06 75-05-855.0 2.2 1
Acrolein ND ug/L 07/07/16 23:06 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/07/16 23:06 107-13-12001.9 1
Allyl chloride ND ug/L 07/07/16 23:06 107-05-110.0 1.5 1
Benzene ND ug/L 07/07/16 23:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/07/16 23:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/07/16 23:06 75-27-41.0 0.18 1
Bromoform ND ug/L 07/07/16 23:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/07/16 23:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/07/16 23:06 78-93-31000.96 1
Carbon disulfide ND ug/L 07/07/16 23:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/07/16 23:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/07/16 23:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/07/16 23:06 75-00-310.0 0.54 1
Chloroform ND ug/L 07/07/16 23:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/07/16 23:06 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/07/16 23:06 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/07/16 23:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/07/16 23:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/07/16 23:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/07/16 23:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/07/16 23:06 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/07/16 23:06 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 07/07/16 23:06 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:EB Lab ID:92304098004 Collected:07/05/16 18:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 07/07/16 23:06 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/07/16 23:06 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 07/07/16 23:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/07/16 23:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/07/16 23:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/07/16 23:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/07/16 23:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/07/16 23:06 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/07/16 23:06 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/07/16 23:06 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/07/16 23:06 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/07/16 23:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/07/16 23:06 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/07/16 23:06 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/07/16 23:06 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/07/16 23:06 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/07/16 23:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/07/16 23:06 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/07/16 23:06 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/07/16 23:06 126-98-71000.93 1
Methylene Chloride ND ug/L 07/07/16 23:06 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 07/07/16 23:06 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/07/16 23:06 108-10-11000.33 1
Naphthalene ND ug/L 07/07/16 23:06 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/07/16 23:06 107-12-01503.6 1
Styrene ND ug/L 07/07/16 23:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/07/16 23:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/07/16 23:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/07/16 23:06 127-18-41.0 0.46 1
Toluene 0.35J ug/L 07/07/16 23:06 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/07/16 23:06 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/07/16 23:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/07/16 23:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/07/16 23:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/07/16 23:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/07/16 23:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/07/16 23:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/07/16 23:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/07/16 23:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %07/07/16 23:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/07/16 23:06 17060-07-070-130 1
Toluene-d8 (S)101 %07/07/16 23:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:FB Lab ID:92304098005 Collected:07/05/16 18:05 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:15 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:15 7440-38-207/11/16 20:3010.0 2.5 1
Barium ND ug/L 07/18/16 20:15 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:15 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:15 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 20:15 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt ND ug/L 07/18/16 20:15 7440-48-407/11/16 20:3010.0 2.5 1
Copper 2.6J ug/L 07/18/16 20:15 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:15 7439-92-107/11/16 20:3010.0 2.5 1
Nickel ND ug/L 07/18/16 20:15 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:15 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:15 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:15 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:15 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 20:15 7440-62-207/11/16 20:3025.0 2.5 1
Zinc ND ug/L 07/18/16 20:15 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:34 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/07/16 23:23 67-64-110010.0 1
Acetonitrile ND ug/L 07/07/16 23:23 75-05-855.0 2.2 1
Acrolein ND ug/L 07/07/16 23:23 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/07/16 23:23 107-13-12001.9 1
Allyl chloride ND ug/L 07/07/16 23:23 107-05-110.0 1.5 1
Benzene ND ug/L 07/07/16 23:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/07/16 23:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/07/16 23:23 75-27-41.0 0.18 1
Bromoform ND ug/L 07/07/16 23:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/07/16 23:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/07/16 23:23 78-93-31000.96 1
Carbon disulfide ND ug/L 07/07/16 23:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/07/16 23:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/07/16 23:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/07/16 23:23 75-00-310.0 0.54 1
Chloroform ND ug/L 07/07/16 23:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/07/16 23:23 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/07/16 23:23 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/07/16 23:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/07/16 23:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/07/16 23:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/07/16 23:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/07/16 23:23 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/07/16 23:23 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 07/07/16 23:23 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:FB Lab ID:92304098005 Collected:07/05/16 18:05 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 07/07/16 23:23 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/07/16 23:23 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 07/07/16 23:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/07/16 23:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/07/16 23:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/07/16 23:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/07/16 23:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/07/16 23:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/07/16 23:23 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/07/16 23:23 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/07/16 23:23 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/07/16 23:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/07/16 23:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/07/16 23:23 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/07/16 23:23 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/07/16 23:23 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/07/16 23:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/07/16 23:23 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/07/16 23:23 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/07/16 23:23 126-98-71000.93 1
Methylene Chloride ND ug/L 07/07/16 23:23 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 07/07/16 23:23 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/07/16 23:23 108-10-11000.33 1
Naphthalene ND ug/L 07/07/16 23:23 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/07/16 23:23 107-12-01503.6 1
Styrene ND ug/L 07/07/16 23:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/07/16 23:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/07/16 23:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/07/16 23:23 127-18-41.0 0.46 1
Toluene 0.37J ug/L 07/07/16 23:23 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/07/16 23:23 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/07/16 23:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/07/16 23:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/07/16 23:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/07/16 23:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/07/16 23:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/07/16 23:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/07/16 23:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/07/16 23:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %07/07/16 23:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %07/07/16 23:23 17060-07-070-130 1
Toluene-d8 (S)101 %07/07/16 23:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:TB Lab ID:92304098006 Collected:07/05/16 00:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/07/16 23:40 67-64-110010.0 1
Acetonitrile ND ug/L 07/07/16 23:40 75-05-855.0 2.2 1
Acrolein ND ug/L 07/07/16 23:40 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/07/16 23:40 107-13-12001.9 1
Allyl chloride ND ug/L 07/07/16 23:40 107-05-110.0 1.5 1
Benzene ND ug/L 07/07/16 23:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/07/16 23:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/07/16 23:40 75-27-41.0 0.18 1
Bromoform ND ug/L 07/07/16 23:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/07/16 23:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/07/16 23:40 78-93-31000.96 1
Carbon disulfide ND ug/L 07/07/16 23:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/07/16 23:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/07/16 23:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/07/16 23:40 75-00-310.0 0.54 1
Chloroform ND ug/L 07/07/16 23:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/07/16 23:40 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/07/16 23:40 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/07/16 23:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/07/16 23:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/07/16 23:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/07/16 23:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/07/16 23:40 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/07/16 23:40 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 07/07/16 23:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/07/16 23:40 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/07/16 23:40 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 07/07/16 23:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/07/16 23:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/07/16 23:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/07/16 23:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/07/16 23:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/07/16 23:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/07/16 23:40 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/07/16 23:40 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/07/16 23:40 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/07/16 23:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/07/16 23:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/07/16 23:40 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/07/16 23:40 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/07/16 23:40 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/07/16 23:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/07/16 23:40 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/07/16 23:40 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/07/16 23:40 126-98-71000.93 1
Methylene Chloride ND ug/L 07/07/16 23:40 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:TB Lab ID:92304098006 Collected:07/05/16 00:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 07/07/16 23:40 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/07/16 23:40 108-10-11000.33 1
Naphthalene ND ug/L 07/07/16 23:40 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/07/16 23:40 107-12-01503.6 1
Styrene ND ug/L 07/07/16 23:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/07/16 23:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/07/16 23:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/07/16 23:40 127-18-41.0 0.46 1
Toluene ND ug/L 07/07/16 23:40 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/07/16 23:40 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/07/16 23:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/07/16 23:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/07/16 23:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/07/16 23:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/07/16 23:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/07/16 23:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/07/16 23:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/07/16 23:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/07/16 23:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %07/07/16 23:40 17060-07-070-130 1
Toluene-d8 (S)100 %07/07/16 23:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1 Lab ID:92304098007 Collected:07/05/16 13:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 22:43 309-00-207/07/16 13:190.050 0.050 1
alpha-BHC ND ug/L 07/12/16 22:43 319-84-607/07/16 13:190.050 0.050 1
beta-BHC ND ug/L 07/12/16 22:43 319-85-707/07/16 13:190.050 0.050 1
delta-BHC ND ug/L 07/12/16 22:43 319-86-807/07/16 13:190.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 22:43 58-89-907/07/16 13:190.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 22:43 57-74-907/07/16 13:190.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 22:43 72-54-807/07/16 13:190.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 22:43 72-55-907/07/16 13:190.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 22:43 50-29-307/07/16 13:190.10 0.050 1
Dieldrin ND ug/L 07/12/16 22:43 60-57-107/07/16 13:190.075 0.050 1
Endosulfan I ND ug/L 07/12/16 22:43 959-98-807/07/16 13:190.10 0.050 1
Endosulfan II ND ug/L 07/12/16 22:43 33213-65-907/07/16 13:190.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 22:43 1031-07-807/07/16 13:190.10 0.050 1
Endrin ND ug/L 07/12/16 22:43 72-20-807/07/16 13:190.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 22:43 7421-93-407/07/16 13:190.10 0.050 1
Heptachlor ND ug/L 07/12/16 22:43 76-44-807/07/16 13:190.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 22:43 1024-57-307/07/16 13:190.075 0.050 1
Methoxychlor ND ug/L 07/12/16 22:43 72-43-507/07/16 13:191.0 0.15 1
Toxaphene ND ug/L 07/12/16 22:43 8001-35-207/07/16 13:191.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)91 %07/12/16 22:43 877-09-807/07/16 13:1920-130 1
Decachlorobiphenyl (S)85 %07/12/16 22:43 2051-24-307/07/16 13:1920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/08/16 10:51 12674-11-207/07/16 13:190.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/08/16 10:51 11104-28-207/07/16 13:190.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/08/16 10:51 11141-16-507/07/16 13:190.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/08/16 10:51 53469-21-907/07/16 13:190.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/08/16 10:51 12672-29-607/07/16 13:190.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/08/16 10:51 11097-69-107/07/16 13:190.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/08/16 10:51 11096-82-507/07/16 13:190.50 0.50 1
Surrogates
Decachlorobiphenyl (S)73 %07/08/16 10:51 2051-24-307/07/16 13:1910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 07/13/16 00:54 25057-89-007/11/16 08:250.095 0.047 1
2,4-D ND ug/L 07/13/16 00:54 94-75-707/11/16 08:250.95 0.23 1
Dalapon ND ug/L 07/13/16 00:54 75-99-007/11/16 08:250.92 0.43 1
2,4-DB ND ug/L 07/13/16 00:54 94-82-607/11/16 08:251.9 0.51 1
Dicamba ND ug/L 07/13/16 00:54 1918-00-907/11/16 08:250.095 0.030 1
Dichlorprop ND ug/L 07/13/16 00:54 120-36-507/11/16 08:250.66 0.19 1
Dinoseb ND ug/L 07/13/16 00:54 88-85-707/11/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 07/13/16 00:54 87-86-507/11/16 08:250.029 0.017 1
Picloram ND ug/L 07/13/16 00:54 1918-02-107/11/16 08:250.095 0.019 1
2,4,5-T ND ug/L 07/13/16 00:54 93-76-507/11/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 00:54 93-72-107/11/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1 Lab ID:92304098007 Collected:07/05/16 13:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)79 %07/13/16 00:54 19719-28-907/11/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:18 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:18 7440-38-207/11/16 20:3010.0 2.5 1
Barium 40.9J ug/L 07/18/16 20:18 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:18 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:18 7440-43-907/11/16 20:301.0 0.50 1
Chromium 4.3J ug/L 07/18/16 20:18 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 10.1 ug/L 07/18/16 20:18 7440-48-407/11/16 20:3010.0 2.5 1
Copper 7.1J ug/L 07/18/16 20:18 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:18 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 10.5J ug/L 07/18/16 20:18 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:18 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:18 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:18 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:18 7440-31-507/11/16 20:301002.5 1
Vanadium 4.7J ug/L 07/18/16 20:18 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 44.3 ug/L 07/18/16 20:18 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:37 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 13:44 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 13:44 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 13:44 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 13:44 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 13:44 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 13:44 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 13:44 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 13:44 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 13:44 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 13:44 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 13:44 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 13:44 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 13:44 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 13:44 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 13:44 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 13:44 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 13:44 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 13:44 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 13:44 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 13:44 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 13:44 95-57-807/08/16 12:0610.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1 Lab ID:92304098007 Collected:07/05/16 13:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 07/12/16 13:44 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 13:44 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 13:44 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 13:44 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 13:44 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 13:44 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 13:44 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 13:44 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 13:44 84-66-207/08/16 12:0660001.3 1
Dimethoate ND ug/L 07/12/16 13:44 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 13:44 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 13:44 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 13:44 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 13:44 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 13:44 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 13:44 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 13:44 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 13:44 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/12/16 13:44 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 13:44 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 13:44 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 13:44 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 13:44 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 13:44 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 13:44 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 13:44 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 13:44 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 13:44 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 13:44 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 13:44 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 13:44 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 13:44 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 13:44 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 13:44 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 13:44 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 13:44 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 13:44 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 13:44 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 13:44 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 13:44 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 13:44 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 13:44 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/12/16 13:44 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 13:44 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 13:4407/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 13:44 134-32-707/08/16 12:0610.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1 Lab ID:92304098007 Collected:07/05/16 13:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 07/12/16 13:44 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 13:44 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 13:44 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 13:44 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 13:44 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 13:44 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 13:44 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 13:44 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 13:44 99-55-807/08/16 12:0610.0 1.2 1
N-Nitrosodiethylamine ND ug/L 07/12/16 13:44 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 13:44 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 13:44 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 13:44 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 13:44 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 13:44 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 13:44 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 13:44 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 13:44 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 13:44 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 13:44 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 13:44 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 13:44 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 13:44 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 13:44 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 13:44 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 13:4407/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 13:44 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 13:44 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 13:44 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 13:44 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 13:44 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 13:44 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 13:44 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 13:44 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 13:44 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 13:44 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 13:44 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 13:44 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)80 %07/12/16 13:44 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)74 %07/12/16 13:44 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)86 %07/12/16 13:44 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)33 %07/12/16 13:44 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)42 %07/12/16 13:44 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)76 %07/12/16 13:44 118-79-607/08/16 12:0627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1 Lab ID:92304098007 Collected:07/05/16 13:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 06:00 67-64-110010.0 1
Acetonitrile ND ug/L 07/08/16 06:00 75-05-855.0 2.2 1
Acrolein ND ug/L 07/08/16 06:00 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/08/16 06:00 107-13-12001.9 1
Allyl chloride ND ug/L 07/08/16 06:00 107-05-110.0 1.5 1
Benzene 1.1 ug/L 07/08/16 06:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 06:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 06:00 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 06:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 06:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 06:00 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 06:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 06:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 06:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 06:00 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 06:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 06:00 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/08/16 06:00 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 06:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 06:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 06:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 06:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 06:00 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/08/16 06:00 541-73-15.0 0.24 1
1,4-Dichlorobenzene 3.1 ug/L 07/08/16 06:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 06:00 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/08/16 06:00 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 07/08/16 06:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 06:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 06:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.7J ug/L 07/08/16 06:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 06:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 06:00 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/08/16 06:00 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/08/16 06:00 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/08/16 06:00 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 06:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 06:00 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 06:00 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/08/16 06:00 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/08/16 06:00 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/08/16 06:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 06:00 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/08/16 06:00 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/08/16 06:00 126-98-71000.93 1
Methylene Chloride ND ug/L 07/08/16 06:00 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1 Lab ID:92304098007 Collected:07/05/16 13:45 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 07/08/16 06:00 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 06:00 108-10-11000.33 1
Naphthalene ND ug/L 07/08/16 06:00 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/08/16 06:00 107-12-01503.6 1
Styrene ND ug/L 07/08/16 06:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 06:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 06:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 06:00 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 06:00 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/08/16 06:00 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/08/16 06:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 06:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 06:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 06:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 06:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 06:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 06:00 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 06:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %07/08/16 06:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %07/08/16 06:00 17060-07-070-130 1
Toluene-d8 (S)102 %07/08/16 06:00 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.2J ug/L 07/12/16 17:23 57-12-5 B,M110.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1B Lab ID:92304098008 Collected:07/05/16 13:40 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 23:01 309-00-207/07/16 13:190.050 0.050 1
alpha-BHC ND ug/L 07/12/16 23:01 319-84-607/07/16 13:190.050 0.050 1
beta-BHC ND ug/L 07/12/16 23:01 319-85-707/07/16 13:190.050 0.050 1
delta-BHC ND ug/L 07/12/16 23:01 319-86-807/07/16 13:190.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 23:01 58-89-907/07/16 13:190.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 23:01 57-74-907/07/16 13:190.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 23:01 72-54-807/07/16 13:190.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 23:01 72-55-907/07/16 13:190.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 23:01 50-29-307/07/16 13:190.10 0.050 1
Dieldrin ND ug/L 07/12/16 23:01 60-57-107/07/16 13:190.075 0.050 1
Endosulfan I ND ug/L 07/12/16 23:01 959-98-807/07/16 13:190.10 0.050 1
Endosulfan II ND ug/L 07/12/16 23:01 33213-65-907/07/16 13:190.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 23:01 1031-07-807/07/16 13:190.10 0.050 1
Endrin ND ug/L 07/12/16 23:01 72-20-807/07/16 13:190.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 23:01 7421-93-407/07/16 13:190.10 0.050 1
Heptachlor ND ug/L 07/12/16 23:01 76-44-807/07/16 13:190.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 23:01 1024-57-307/07/16 13:190.075 0.050 1
Methoxychlor ND ug/L 07/12/16 23:01 72-43-507/07/16 13:191.0 0.15 1
Toxaphene ND ug/L 07/12/16 23:01 8001-35-207/07/16 13:191.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)133 %07/12/16 23:01 877-09-8 S307/07/16 13:1920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/08/16 11:31 12674-11-207/07/16 13:190.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/08/16 11:31 11104-28-207/07/16 13:190.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/08/16 11:31 11141-16-507/07/16 13:190.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/08/16 11:31 53469-21-907/07/16 13:190.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/08/16 11:31 12672-29-607/07/16 13:190.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/08/16 11:31 11097-69-107/07/16 13:190.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/08/16 11:31 11096-82-507/07/16 13:190.50 0.50 1
Surrogates
Decachlorobiphenyl (S)49 %07/08/16 11:31 2051-24-307/07/16 13:1910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 07/13/16 01:24 25057-89-007/11/16 08:250.096 0.048 1
2,4-D ND ug/L 07/13/16 01:24 94-75-707/11/16 08:250.95 0.23 1
Dalapon ND ug/L 07/13/16 01:24 75-99-007/11/16 08:250.92 0.44 1
2,4-DB ND ug/L 07/13/16 01:24 94-82-607/11/16 08:251.9 0.52 1
Dicamba ND ug/L 07/13/16 01:24 1918-00-907/11/16 08:250.095 0.030 1
Dichlorprop ND ug/L 07/13/16 01:24 120-36-507/11/16 08:250.66 0.19 1
Dinoseb ND ug/L 07/13/16 01:24 88-85-707/11/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 07/13/16 01:24 87-86-507/11/16 08:250.029 0.017 1
Picloram ND ug/L 07/13/16 01:24 1918-02-107/11/16 08:250.096 0.019 1
2,4,5-T ND ug/L 07/13/16 01:24 93-76-507/11/16 08:250.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 01:24 93-72-107/11/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1B Lab ID:92304098008 Collected:07/05/16 13:40 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)88 %07/13/16 01:24 19719-28-907/11/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:30 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:30 7440-38-207/11/16 20:3010.0 2.5 1
Barium 176 ug/L 07/18/16 20:30 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:30 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:30 7440-43-907/11/16 20:301.0 0.50 1
Chromium 2.6J ug/L 07/18/16 20:30 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 107 ug/L 07/18/16 20:30 7440-48-407/11/16 20:3010.0 2.5 1
Copper 7.7J ug/L 07/18/16 20:30 7440-50-807/11/16 20:3010.0 2.5 1
Lead 3.1J ug/L 07/18/16 20:30 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 10.5J ug/L 07/18/16 20:30 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:30 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:30 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:30 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:30 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 20:30 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 26.6 ug/L 07/18/16 20:30 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 1.3 ug/L 07/15/16 12:39 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 14:12 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 14:12 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 14:12 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 14:12 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 14:12 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 14:12 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 14:12 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 14:12 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 14:12 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 14:12 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 14:12 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 14:12 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 14:12 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 14:12 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 14:12 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 14:12 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 14:12 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 14:12 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 14:12 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 14:12 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 14:12 95-57-807/08/16 12:0610.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1B Lab ID:92304098008 Collected:07/05/16 13:40 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 07/12/16 14:12 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 14:12 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 14:12 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 14:12 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 14:12 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 14:12 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 14:12 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 14:12 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 14:12 84-66-207/08/16 12:0660001.3 1
Dimethoate ND ug/L 07/12/16 14:12 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 14:12 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 14:12 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 14:12 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 14:12 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 14:12 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 14:12 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 14:12 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 14:12 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/12/16 14:12 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 14:12 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 14:12 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 14:12 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 14:12 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 14:12 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 14:12 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 14:12 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 14:12 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 14:12 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 14:12 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 14:12 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 14:12 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 14:12 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 14:12 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 14:12 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 14:12 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 14:12 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 14:12 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 14:12 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 14:12 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 14:12 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 14:12 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 14:12 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/12/16 14:12 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 14:12 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 14:1207/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 14:12 134-32-707/08/16 12:0610.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1B Lab ID:92304098008 Collected:07/05/16 13:40 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 07/12/16 14:12 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 14:12 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 14:12 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 14:12 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 14:12 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 14:12 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 14:12 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 14:12 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 14:12 99-55-807/08/16 12:0610.0 1.2 1
N-Nitrosodiethylamine ND ug/L 07/12/16 14:12 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 14:12 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 14:12 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 14:12 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 14:12 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 14:12 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 14:12 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 14:12 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 14:12 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 14:12 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 14:12 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 14:12 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 14:12 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 14:12 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 14:12 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 14:12 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 14:1207/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 14:12 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 14:12 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 14:12 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 14:12 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 14:12 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 14:12 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 14:12 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 14:12 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 14:12 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 14:12 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 14:12 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 14:12 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)77 %07/12/16 14:12 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)72 %07/12/16 14:12 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)87 %07/12/16 14:12 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)27 %07/12/16 14:12 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)36 %07/12/16 14:12 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)66 %07/12/16 14:12 118-79-607/08/16 12:0627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1B Lab ID:92304098008 Collected:07/05/16 13:40 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 06:17 67-64-110010.0 1
Acetonitrile ND ug/L 07/08/16 06:17 75-05-855.0 2.2 1
Acrolein ND ug/L 07/08/16 06:17 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/08/16 06:17 107-13-12001.9 1
Allyl chloride ND ug/L 07/08/16 06:17 107-05-110.0 1.5 1
Benzene ND ug/L 07/08/16 06:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 06:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 06:17 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 06:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 06:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 06:17 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 06:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 06:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/08/16 06:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 06:17 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 06:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 06:17 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/08/16 06:17 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 06:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 06:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 06:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 06:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 06:17 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/08/16 06:17 541-73-15.0 0.24 1
1,4-Dichlorobenzene 1.2 ug/L 07/08/16 06:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 06:17 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/08/16 06:17 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 07/08/16 06:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 06:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 06:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.68J ug/L 07/08/16 06:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 06:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 06:17 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/08/16 06:17 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/08/16 06:17 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/08/16 06:17 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 06:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 06:17 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 06:17 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/08/16 06:17 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/08/16 06:17 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/08/16 06:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 06:17 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/08/16 06:17 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/08/16 06:17 126-98-71000.93 1
Methylene Chloride ND ug/L 07/08/16 06:17 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-1B Lab ID:92304098008 Collected:07/05/16 13:40 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 07/08/16 06:17 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 06:17 108-10-11000.33 1
Naphthalene ND ug/L 07/08/16 06:17 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/08/16 06:17 107-12-01503.6 1
Styrene ND ug/L 07/08/16 06:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 06:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 06:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 06:17 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 06:17 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/08/16 06:17 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/08/16 06:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 06:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 06:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 06:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 06:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 06:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 06:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 06:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 06:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %07/08/16 06:17 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 06:17 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.2J ug/L 07/12/16 17:26 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-4R Lab ID:92304098009 Collected:07/05/16 16:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 23:19 309-00-207/07/16 13:190.050 0.050 1
alpha-BHC ND ug/L 07/12/16 23:19 319-84-607/07/16 13:190.050 0.050 1
beta-BHC ND ug/L 07/12/16 23:19 319-85-707/07/16 13:190.050 0.050 1
delta-BHC ND ug/L 07/12/16 23:19 319-86-807/07/16 13:190.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 23:19 58-89-907/07/16 13:190.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 23:19 57-74-907/07/16 13:190.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 23:19 72-54-807/07/16 13:190.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 23:19 72-55-907/07/16 13:190.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 23:19 50-29-307/07/16 13:190.10 0.050 1
Dieldrin ND ug/L 07/12/16 23:19 60-57-107/07/16 13:190.075 0.050 1
Endosulfan I ND ug/L 07/12/16 23:19 959-98-807/07/16 13:190.10 0.050 1
Endosulfan II ND ug/L 07/12/16 23:19 33213-65-907/07/16 13:190.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 23:19 1031-07-807/07/16 13:190.10 0.050 1
Endrin ND ug/L 07/12/16 23:19 72-20-807/07/16 13:190.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 23:19 7421-93-407/07/16 13:190.10 0.050 1
Heptachlor ND ug/L 07/12/16 23:19 76-44-807/07/16 13:190.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 23:19 1024-57-307/07/16 13:190.075 0.050 1
Methoxychlor ND ug/L 07/12/16 23:19 72-43-507/07/16 13:191.0 0.15 1
Toxaphene ND ug/L 07/12/16 23:19 8001-35-207/07/16 13:191.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)74 %07/12/16 23:19 877-09-807/07/16 13:1920-130 1
Decachlorobiphenyl (S)88 %07/12/16 23:19 2051-24-307/07/16 13:1920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/08/16 11:51 12674-11-207/07/16 13:190.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/08/16 11:51 11104-28-207/07/16 13:190.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/08/16 11:51 11141-16-507/07/16 13:190.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/08/16 11:51 53469-21-907/07/16 13:190.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/08/16 11:51 12672-29-607/07/16 13:190.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/08/16 11:51 11097-69-107/07/16 13:190.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/08/16 11:51 11096-82-507/07/16 13:190.50 0.50 1
Surrogates
Decachlorobiphenyl (S)61 %07/08/16 11:51 2051-24-307/07/16 13:1910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 07/13/16 01:54 25057-89-007/11/16 08:250.097 0.048 1
2,4-D ND ug/L 07/13/16 01:54 94-75-707/11/16 08:250.96 0.23 1
Dalapon ND ug/L 07/13/16 01:54 75-99-007/11/16 08:250.93 0.44 1
2,4-DB ND ug/L 07/13/16 01:54 94-82-607/11/16 08:251.9 0.52 1
Dicamba ND ug/L 07/13/16 01:54 1918-00-907/11/16 08:250.096 0.031 1
Dichlorprop ND ug/L 07/13/16 01:54 120-36-507/11/16 08:250.67 0.20 1
Dinoseb ND ug/L 07/13/16 01:54 88-85-707/11/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 07/13/16 01:54 87-86-507/11/16 08:250.029 0.017 1
Picloram ND ug/L 07/13/16 01:54 1918-02-107/11/16 08:250.097 0.019 1
2,4,5-T ND ug/L 07/13/16 01:54 93-76-507/11/16 08:250.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 01:54 93-72-107/11/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-4R Lab ID:92304098009 Collected:07/05/16 16:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)50 %07/13/16 01:54 19719-28-907/11/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:34 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:34 7440-38-207/11/16 20:3010.0 2.5 1
Barium 114 ug/L 07/18/16 20:34 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:34 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:34 7440-43-907/11/16 20:301.0 0.50 1
Chromium 2.6J ug/L 07/18/16 20:34 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 378 ug/L 07/18/16 20:34 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 20:34 7440-50-807/11/16 20:3010.0 2.5 1
Lead 3.8J ug/L 07/18/16 20:34 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 13.0J ug/L 07/18/16 20:34 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:34 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:34 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:34 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:34 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 20:34 7440-62-207/11/16 20:3025.0 2.5 1
Zinc ND ug/L 07/18/16 20:34 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:42 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 14:40 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 14:40 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 14:40 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 14:40 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 14:40 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 14:40 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 14:40 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 14:40 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 14:40 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 14:40 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 14:40 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 14:40 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 14:40 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 14:40 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 14:40 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 14:40 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 14:40 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 14:40 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 14:40 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 14:40 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 14:40 95-57-807/08/16 12:0610.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-4R Lab ID:92304098009 Collected:07/05/16 16:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 07/12/16 14:40 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 14:40 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 14:40 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 14:40 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 14:40 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 14:40 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 14:40 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 14:40 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 14:40 84-66-207/08/16 12:0660001.3 1
Dimethoate ND ug/L 07/12/16 14:40 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 14:40 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 14:40 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 14:40 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 14:40 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 14:40 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 14:40 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 14:40 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 14:40 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/12/16 14:40 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 14:40 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 14:40 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 14:40 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 14:40 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 14:40 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 14:40 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 14:40 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 14:40 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 14:40 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 14:40 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 14:40 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 14:40 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 14:40 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 14:40 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 14:40 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 14:40 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 14:40 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 14:40 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 14:40 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 14:40 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 14:40 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 14:40 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 14:40 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/12/16 14:40 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 14:40 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 14:4007/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 14:40 134-32-707/08/16 12:0610.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-4R Lab ID:92304098009 Collected:07/05/16 16:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 07/12/16 14:40 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 14:40 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 14:40 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 14:40 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 14:40 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 14:40 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 14:40 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 14:40 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 14:40 99-55-807/08/16 12:0610.0 1.2 1
N-Nitrosodiethylamine ND ug/L 07/12/16 14:40 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 14:40 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 14:40 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 14:40 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 14:40 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 14:40 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 14:40 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 14:40 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 14:40 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 14:40 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 14:40 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 14:40 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 14:40 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 14:40 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 14:40 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 14:40 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 14:4007/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 14:40 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 14:40 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 14:40 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 14:40 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 14:40 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 14:40 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 14:40 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 14:40 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 14:40 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 14:40 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 14:40 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 14:40 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)77 %07/12/16 14:40 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)72 %07/12/16 14:40 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)88 %07/12/16 14:40 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)32 %07/12/16 14:40 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)42 %07/12/16 14:40 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)80 %07/12/16 14:40 118-79-607/08/16 12:0627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-4R Lab ID:92304098009 Collected:07/05/16 16:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 06:34 67-64-110010.0 1
Acetonitrile ND ug/L 07/08/16 06:34 75-05-855.0 2.2 1
Acrolein ND ug/L 07/08/16 06:34 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/08/16 06:34 107-13-12001.9 1
Allyl chloride ND ug/L 07/08/16 06:34 107-05-110.0 1.5 1
Benzene 1.7 ug/L 07/08/16 06:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 06:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 06:34 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 06:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 06:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 06:34 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 06:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 06:34 56-23-51.0 0.25 1
Chlorobenzene 1.7J ug/L 07/08/16 06:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 06:34 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 06:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 06:34 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/08/16 06:34 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 06:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 06:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 06:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 06:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 06:34 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/08/16 06:34 541-73-15.0 0.24 1
1,4-Dichlorobenzene 4.2 ug/L 07/08/16 06:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 06:34 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/08/16 06:34 75-71-85.0 0.21 1
1,1-Dichloroethane 2.5J ug/L 07/08/16 06:34 75-34-35.0 0.32 1
1,2-Dichloroethane 0.36J ug/L 07/08/16 06:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 06:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 15.4 ug/L 07/08/16 06:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 06:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 06:34 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/08/16 06:34 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/08/16 06:34 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/08/16 06:34 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 06:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 06:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 06:34 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/08/16 06:34 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/08/16 06:34 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/08/16 06:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 06:34 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/08/16 06:34 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/08/16 06:34 126-98-71000.93 1
Methylene Chloride ND ug/L 07/08/16 06:34 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-4R Lab ID:92304098009 Collected:07/05/16 16:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 07/08/16 06:34 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 06:34 108-10-11000.33 1
Naphthalene ND ug/L 07/08/16 06:34 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/08/16 06:34 107-12-01503.6 1
Styrene ND ug/L 07/08/16 06:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 06:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 06:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 06:34 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 06:34 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/08/16 06:34 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/08/16 06:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 06:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/08/16 06:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 06:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 06:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 06:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 06:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 06:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 06:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %07/08/16 06:34 17060-07-070-130 1
Toluene-d8 (S)103 %07/08/16 06:34 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.0J ug/L 07/12/16 17:27 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-5 Lab ID:92304098010 Collected:07/05/16 16:20 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 23:36 309-00-207/07/16 13:190.050 0.050 1
alpha-BHC ND ug/L 07/12/16 23:36 319-84-607/07/16 13:190.050 0.050 1
beta-BHC ND ug/L 07/12/16 23:36 319-85-707/07/16 13:190.050 0.050 1
delta-BHC ND ug/L 07/12/16 23:36 319-86-807/07/16 13:190.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 23:36 58-89-907/07/16 13:190.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 23:36 57-74-907/07/16 13:190.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 23:36 72-54-807/07/16 13:190.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 23:36 72-55-907/07/16 13:190.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 23:36 50-29-307/07/16 13:190.10 0.050 1
Dieldrin ND ug/L 07/12/16 23:36 60-57-107/07/16 13:190.075 0.050 1
Endosulfan I ND ug/L 07/12/16 23:36 959-98-807/07/16 13:190.10 0.050 1
Endosulfan II ND ug/L 07/12/16 23:36 33213-65-907/07/16 13:190.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 23:36 1031-07-807/07/16 13:190.10 0.050 1
Endrin ND ug/L 07/12/16 23:36 72-20-807/07/16 13:190.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 23:36 7421-93-407/07/16 13:190.10 0.050 1
Heptachlor ND ug/L 07/12/16 23:36 76-44-807/07/16 13:190.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 23:36 1024-57-307/07/16 13:190.075 0.050 1
Methoxychlor ND ug/L 07/12/16 23:36 72-43-507/07/16 13:191.0 0.15 1
Toxaphene ND ug/L 07/12/16 23:36 8001-35-207/07/16 13:191.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)97 %07/12/16 23:36 877-09-807/07/16 13:1920-130 1
Decachlorobiphenyl (S)94 %07/12/16 23:36 2051-24-307/07/16 13:1920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/08/16 12:11 12674-11-207/07/16 13:190.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/08/16 12:11 11104-28-207/07/16 13:190.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/08/16 12:11 11141-16-507/07/16 13:190.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/08/16 12:11 53469-21-907/07/16 13:190.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/08/16 12:11 12672-29-607/07/16 13:190.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/08/16 12:11 11097-69-107/07/16 13:190.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/08/16 12:11 11096-82-507/07/16 13:190.50 0.50 1
Surrogates
Decachlorobiphenyl (S)52 %07/08/16 12:11 2051-24-307/07/16 13:1910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 07/13/16 02:24 25057-89-007/11/16 08:250.096 0.048 1
2,4-D ND ug/L 07/13/16 02:24 94-75-707/11/16 08:250.95 0.23 1
Dalapon ND ug/L 07/13/16 02:24 75-99-007/11/16 08:250.92 0.44 1
2,4-DB ND ug/L 07/13/16 02:24 94-82-607/11/16 08:251.9 0.52 1
Dicamba ND ug/L 07/13/16 02:24 1918-00-907/11/16 08:250.095 0.030 1
Dichlorprop ND ug/L 07/13/16 02:24 120-36-507/11/16 08:250.66 0.19 1
Dinoseb ND ug/L 07/13/16 02:24 88-85-707/11/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 07/13/16 02:24 87-86-507/11/16 08:250.029 0.017 1
Picloram ND ug/L 07/13/16 02:24 1918-02-107/11/16 08:250.096 0.019 1
2,4,5-T ND ug/L 07/13/16 02:24 93-76-507/11/16 08:250.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 02:24 93-72-107/11/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-5 Lab ID:92304098010 Collected:07/05/16 16:20 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)85 %07/13/16 02:24 19719-28-907/11/16 08:2539-139 1
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 10100 ug/L 07/20/16 16:01 74-82-8 H5,M1,
N2
10.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:37 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:37 7440-38-207/11/16 20:3010.0 2.5 1
Barium 120 ug/L 07/18/16 20:37 7440-39-307/11/16 20:301002.5 1
Beryllium 1.5 ug/L 07/18/16 20:37 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:37 7440-43-907/11/16 20:301.0 0.50 1
Chromium 35.8 ug/L 07/18/16 20:37 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 8.9J ug/L 07/18/16 20:37 7440-48-407/11/16 20:3010.0 2.5 1
Copper 16.3 ug/L 07/18/16 20:37 7440-50-807/11/16 20:3010.0 2.5 1
Lead 5.7J ug/L 07/18/16 20:37 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 19.4J ug/L 07/18/16 20:37 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:37 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:37 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:37 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:37 7440-31-507/11/16 20:301002.5 1
Vanadium 24.2J ug/L 07/18/16 20:37 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 83.3 ug/L 07/18/16 20:37 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:44 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 15:08 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 15:08 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 15:08 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 15:08 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 15:08 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 15:08 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 15:08 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 15:08 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 15:08 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 15:08 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 15:08 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 15:08 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 15:08 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 15:08 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 15:08 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 15:08 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 15:08 510-15-607/08/16 12:0610.0 0.72 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-5 Lab ID:92304098010 Collected:07/05/16 16:20 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 15:08 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 15:08 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 15:08 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 15:08 95-57-807/08/16 12:0610.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 07/12/16 15:08 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 15:08 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 15:08 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 15:08 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 15:08 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 15:08 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 15:08 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 15:08 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 15:08 84-66-207/08/16 12:0660001.3 1
Dimethoate ND ug/L 07/12/16 15:08 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 15:08 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 15:08 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 15:08 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 15:08 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 15:08 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 15:08 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 15:08 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 15:08 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/12/16 15:08 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 15:08 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 15:08 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 15:08 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 15:08 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 15:08 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 15:08 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 15:08 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 15:08 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 15:08 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 15:08 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 15:08 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 15:08 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 15:08 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 15:08 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 15:08 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 15:08 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 15:08 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 15:08 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 15:08 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 15:08 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 15:08 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 15:08 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 15:08 91-57-607/08/16 12:0610.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-5 Lab ID:92304098010 Collected:07/05/16 16:20 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Methyl parathion ND ug/L 07/12/16 15:08 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 15:08 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 15:0807/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 15:08 134-32-707/08/16 12:0610.0 0.96 1
2-Naphthalenamine ND ug/L 07/12/16 15:08 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 15:08 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 15:08 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 15:08 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 15:08 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 15:08 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 15:08 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 15:08 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 15:08 99-55-807/08/16 12:0610.0 1.2 1
N-Nitrosodiethylamine ND ug/L 07/12/16 15:08 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 15:08 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 15:08 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 15:08 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 15:08 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 15:08 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 15:08 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 15:08 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 15:08 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 15:08 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 15:08 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 15:08 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 15:08 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 15:08 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 15:08 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 15:08 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 15:0807/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 15:08 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 15:08 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 15:08 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 15:08 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 15:08 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 15:08 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 15:08 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 15:08 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 15:08 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 15:08 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 15:08 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 15:08 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)77 %07/12/16 15:08 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)72 %07/12/16 15:08 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)79 %07/12/16 15:08 1718-51-007/08/16 12:0631-107 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-5 Lab ID:92304098010 Collected:07/05/16 16:20 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Phenol-d6 (S)32 %07/12/16 15:08 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)43 %07/12/16 15:08 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)77 %07/12/16 15:08 118-79-607/08/16 12:0627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 06:51 67-64-110010.0 1
Acetonitrile ND ug/L 07/08/16 06:51 75-05-855.0 2.2 1
Acrolein ND ug/L 07/08/16 06:51 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 07/08/16 06:51 107-13-12001.9 1
Allyl chloride ND ug/L 07/08/16 06:51 107-05-110.0 1.5 1
Benzene 3.3 ug/L 07/08/16 06:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 06:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 06:51 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 06:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 06:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 06:51 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 06:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 06:51 56-23-51.0 0.25 1
Chlorobenzene 0.92J ug/L 07/08/16 06:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 06:51 75-00-310.0 0.54 1
Chloroform ND ug/L 07/08/16 06:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 06:51 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/08/16 06:51 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 06:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 06:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 06:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 06:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 06:51 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/08/16 06:51 541-73-15.0 0.24 1
1,4-Dichlorobenzene 2.8 ug/L 07/08/16 06:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 06:51 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/08/16 06:51 75-71-85.0 0.21 1
1,1-Dichloroethane 4.1J ug/L 07/08/16 06:51 75-34-35.0 0.32 1
1,2-Dichloroethane 0.26J ug/L 07/08/16 06:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 06:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 16.2 ug/L 07/08/16 06:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 06:51 156-60-55.0 0.49 1
1,2-Dichloropropane 0.43J ug/L 07/08/16 06:51 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/08/16 06:51 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/08/16 06:51 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/08/16 06:51 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 06:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 06:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 06:51 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/08/16 06:51 97-63-210.0 0.20 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-5 Lab ID:92304098010 Collected:07/05/16 16:20 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Hexachloro-1,3-butadiene ND ug/L 07/08/16 06:51 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/08/16 06:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 06:51 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/08/16 06:51 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/08/16 06:51 126-98-71000.93 1
Methylene Chloride ND ug/L 07/08/16 06:51 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 07/08/16 06:51 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 06:51 108-10-11000.33 1
Naphthalene ND ug/L 07/08/16 06:51 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/08/16 06:51 107-12-01503.6 1
Styrene ND ug/L 07/08/16 06:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 06:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 06:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 06:51 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 06:51 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/08/16 06:51 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/08/16 06:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 06:51 79-00-51.0 0.29 1
Trichloroethene 0.55J ug/L 07/08/16 06:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 06:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 06:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 06:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 06:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 06:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %07/08/16 06:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %07/08/16 06:51 17060-07-070-130 1
Toluene-d8 (S)103 %07/08/16 06:51 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.8J ug/L 07/12/16 17:28 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098011 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 23:54 309-00-207/07/16 13:190.050 0.050 1
alpha-BHC ND ug/L 07/12/16 23:54 319-84-607/07/16 13:190.050 0.050 1
beta-BHC ND ug/L 07/12/16 23:54 319-85-707/07/16 13:190.050 0.050 1
delta-BHC ND ug/L 07/12/16 23:54 319-86-807/07/16 13:190.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 23:54 58-89-907/07/16 13:190.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 23:54 57-74-907/07/16 13:190.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 23:54 72-54-807/07/16 13:190.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 23:54 72-55-907/07/16 13:190.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 23:54 50-29-307/07/16 13:190.10 0.050 1
Dieldrin ND ug/L 07/12/16 23:54 60-57-107/07/16 13:190.075 0.050 1
Endosulfan I ND ug/L 07/12/16 23:54 959-98-807/07/16 13:190.10 0.050 1
Endosulfan II ND ug/L 07/12/16 23:54 33213-65-907/07/16 13:190.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 23:54 1031-07-807/07/16 13:190.10 0.050 1
Endrin ND ug/L 07/12/16 23:54 72-20-807/07/16 13:190.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 23:54 7421-93-407/07/16 13:190.10 0.050 1
Heptachlor ND ug/L 07/12/16 23:54 76-44-807/07/16 13:190.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 23:54 1024-57-307/07/16 13:190.075 0.050 1
Methoxychlor ND ug/L 07/12/16 23:54 72-43-507/07/16 13:191.0 0.15 1
Toxaphene ND ug/L 07/12/16 23:54 8001-35-207/07/16 13:191.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)75 %07/12/16 23:54 877-09-807/07/16 13:1920-130 1
Decachlorobiphenyl (S)60 %07/12/16 23:54 2051-24-307/07/16 13:1920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/08/16 12:31 12674-11-207/07/16 13:190.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/08/16 12:31 11104-28-207/07/16 13:190.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/08/16 12:31 11141-16-507/07/16 13:190.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/08/16 12:31 53469-21-907/07/16 13:190.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/08/16 12:31 12672-29-607/07/16 13:190.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/08/16 12:31 11097-69-107/07/16 13:190.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/08/16 12:31 11096-82-507/07/16 13:190.50 0.50 1
Surrogates
Decachlorobiphenyl (S)46 %07/08/16 12:31 2051-24-307/07/16 13:1910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 07/13/16 02:54 25057-89-0 M107/11/16 08:250.095 0.047 1
2,4-D ND ug/L 07/13/16 02:54 94-75-707/11/16 08:250.95 0.23 1
Dalapon ND ug/L 07/13/16 02:54 75-99-0 M1,R107/11/16 08:250.92 0.43 1
2,4-DB ND ug/L 07/13/16 02:54 94-82-607/11/16 08:251.9 0.51 1
Dicamba ND ug/L 07/13/16 02:54 1918-00-9 M107/11/16 08:250.095 0.030 1
Dichlorprop ND ug/L 07/13/16 02:54 120-36-5 M107/11/16 08:250.66 0.19 1
Dinoseb ND ug/L 07/13/16 02:54 88-85-707/11/16 08:250.19 0.057 1
Pentachlorophenol ND ug/L 07/13/16 02:54 87-86-507/11/16 08:250.029 0.017 1
Picloram ND ug/L 07/13/16 02:54 1918-02-107/11/16 08:250.095 0.019 1
2,4,5-T ND ug/L 07/13/16 02:54 93-76-507/11/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 02:54 93-72-107/11/16 08:250.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098011 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)46 %07/13/16 02:54 19719-28-907/11/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:40 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:40 7440-38-207/11/16 20:3010.0 2.5 1
Barium 112 ug/L 07/18/16 20:40 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:40 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:40 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 20:40 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 68.8 ug/L 07/18/16 20:40 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 20:40 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:40 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 8.4J ug/L 07/18/16 20:40 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:40 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:40 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:40 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 20:40 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 20:40 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 45.1 ug/L 07/18/16 20:40 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 07/15/16 12:46 7439-97-607/14/16 22:550.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/19/16 13:50 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/19/16 13:50 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/19/16 13:50 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/19/16 13:50 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/19/16 13:50 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/19/16 13:50 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/19/16 13:50 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/19/16 13:50 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/19/16 13:50 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/19/16 13:50 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/19/16 13:50 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/19/16 13:50 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/19/16 13:50 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/19/16 13:50 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/19/16 13:50 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/19/16 13:50 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/19/16 13:50 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/19/16 13:50 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/19/16 13:50 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/19/16 13:50 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/19/16 13:50 95-57-807/08/16 12:0610.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098011 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 07/19/16 13:50 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/19/16 13:50 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/19/16 13:50 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/19/16 13:50 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/19/16 13:50 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/19/16 13:50 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/19/16 13:50 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/19/16 13:50 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/19/16 13:50 84-66-207/08/16 12:0660001.3 1
Dimethoate ND ug/L 07/19/16 13:50 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/19/16 13:50 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/19/16 13:50 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/19/16 13:50 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/19/16 13:50 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/19/16 13:50 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/19/16 13:50 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/19/16 13:50 534-52-1 L207/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/19/16 13:50 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/19/16 13:50 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/19/16 13:50 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/19/16 13:50 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/19/16 13:50 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/19/16 13:50 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/19/16 13:50 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/19/16 13:50 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/19/16 13:50 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/19/16 13:50 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/19/16 13:50 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/19/16 13:50 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/19/16 13:50 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/19/16 13:50 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/19/16 13:50 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/19/16 13:50 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/19/16 13:50 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/19/16 13:50 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/19/16 13:50 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/19/16 13:50 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/19/16 13:50 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/19/16 13:50 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/19/16 13:50 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/19/16 13:50 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/19/16 13:50 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/19/16 13:50 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/19/16 13:50 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/19/16 13:5007/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/19/16 13:50 134-32-707/08/16 12:0610.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098011 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 07/19/16 13:50 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/19/16 13:50 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/19/16 13:50 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/19/16 13:50 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/19/16 13:50 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/19/16 13:50 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/19/16 13:50 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/19/16 13:50 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/19/16 13:50 99-55-807/08/16 12:0610.0 1.2 1
N-Nitrosodiethylamine ND ug/L 07/19/16 13:50 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/19/16 13:50 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/19/16 13:50 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/19/16 13:50 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/19/16 13:50 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/19/16 13:50 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/19/16 13:50 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/19/16 13:50 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/19/16 13:50 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/19/16 13:50 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/19/16 13:50 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/19/16 13:50 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/19/16 13:50 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/19/16 13:50 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/19/16 13:50 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/19/16 13:50 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/19/16 13:5007/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/19/16 13:50 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/19/16 13:50 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/19/16 13:50 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/19/16 13:50 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/19/16 13:50 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/19/16 13:50 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/19/16 13:50 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/19/16 13:50 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/19/16 13:50 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/19/16 13:50 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/19/16 13:50 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/19/16 13:50 99-35-4 L307/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)57 %07/19/16 13:50 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)53 %07/19/16 13:50 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)80 %07/19/16 13:50 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)18 %07/19/16 13:50 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)26 %07/19/16 13:50 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)66 %07/19/16 13:50 118-79-607/08/16 12:0627-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098011 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/08/16 07:26 67-64-110010.0 1
Acetonitrile ND ug/L 07/08/16 07:26 75-05-8 M155.0 2.2 1
Acrolein ND ug/L 07/08/16 07:26 107-02-8 M153.0 1.6 1
Acrylonitrile ND ug/L 07/08/16 07:26 107-13-12001.9 1
Allyl chloride ND ug/L 07/08/16 07:26 107-05-110.0 1.5 1
Benzene 1.1 ug/L 07/08/16 07:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/08/16 07:26 74-97-5 M13.0 0.17 1
Bromodichloromethane ND ug/L 07/08/16 07:26 75-27-41.0 0.18 1
Bromoform ND ug/L 07/08/16 07:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/08/16 07:26 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 07/08/16 07:26 78-93-31000.96 1
Carbon disulfide ND ug/L 07/08/16 07:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/08/16 07:26 56-23-51.0 0.25 1
Chlorobenzene 1.3J ug/L 07/08/16 07:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/08/16 07:26 75-00-3 M110.0 0.54 1
Chloroform ND ug/L 07/08/16 07:26 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/08/16 07:26 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/08/16 07:26 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/08/16 07:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/08/16 07:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/08/16 07:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/08/16 07:26 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/08/16 07:26 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/08/16 07:26 541-73-15.0 0.24 1
1,4-Dichlorobenzene 3.7 ug/L 07/08/16 07:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/08/16 07:26 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/08/16 07:26 75-71-8 M15.0 0.21 1
1,1-Dichloroethane 0.92J ug/L 07/08/16 07:26 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/08/16 07:26 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/08/16 07:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.4 ug/L 07/08/16 07:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/08/16 07:26 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/08/16 07:26 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/08/16 07:26 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/08/16 07:26 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/08/16 07:26 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/08/16 07:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/08/16 07:26 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/08/16 07:26 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/08/16 07:26 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/08/16 07:26 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/08/16 07:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/08/16 07:26 74-88-4 M110.0 0.32 1
Isobutanol ND ug/L 07/08/16 07:26 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/08/16 07:26 126-98-71000.93 1
Methylene Chloride ND ug/L 07/08/16 07:26 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-12 Lab ID:92304098011 Collected:07/05/16 11:30 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 07/08/16 07:26 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/08/16 07:26 108-10-11000.33 1
Naphthalene ND ug/L 07/08/16 07:26 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/08/16 07:26 107-12-01503.6 1
Styrene ND ug/L 07/08/16 07:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/08/16 07:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/08/16 07:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/08/16 07:26 127-18-41.0 0.46 1
Toluene ND ug/L 07/08/16 07:26 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene 0.45J ug/L 07/08/16 07:26 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/08/16 07:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/08/16 07:26 79-00-51.0 0.29 1
Trichloroethene 1.1 ug/L 07/08/16 07:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/08/16 07:26 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/08/16 07:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/08/16 07:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/08/16 07:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/08/16 07:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/08/16 07:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %07/08/16 07:26 17060-07-070-130 1
Toluene-d8 (S)101 %07/08/16 07:26 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.0J ug/L 07/12/16 17:28 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-16 Lab ID:92304098012 Collected:07/05/16 11:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/13/16 00:12 309-00-207/07/16 13:190.050 0.050 1
alpha-BHC ND ug/L 07/13/16 00:12 319-84-607/07/16 13:190.050 0.050 1
beta-BHC ND ug/L 07/13/16 00:12 319-85-707/07/16 13:190.050 0.050 1
delta-BHC ND ug/L 07/13/16 00:12 319-86-807/07/16 13:190.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/13/16 00:12 58-89-907/07/16 13:190.050 0.050 1
Chlordane (Technical)ND ug/L 07/13/16 00:12 57-74-907/07/16 13:190.50 0.20 1
4,4'-DDD ND ug/L 07/13/16 00:12 72-54-807/07/16 13:190.10 0.050 1
4,4'-DDE ND ug/L 07/13/16 00:12 72-55-907/07/16 13:190.10 0.050 1
4,4'-DDT ND ug/L 07/13/16 00:12 50-29-307/07/16 13:190.10 0.050 1
Dieldrin ND ug/L 07/13/16 00:12 60-57-107/07/16 13:190.075 0.050 1
Endosulfan I ND ug/L 07/13/16 00:12 959-98-807/07/16 13:190.10 0.050 1
Endosulfan II ND ug/L 07/13/16 00:12 33213-65-907/07/16 13:190.10 0.050 1
Endosulfan sulfate ND ug/L 07/13/16 00:12 1031-07-807/07/16 13:190.10 0.050 1
Endrin ND ug/L 07/13/16 00:12 72-20-807/07/16 13:190.10 0.050 1
Endrin aldehyde ND ug/L 07/13/16 00:12 7421-93-407/07/16 13:190.10 0.050 1
Heptachlor ND ug/L 07/13/16 00:12 76-44-807/07/16 13:190.050 0.050 1
Heptachlor epoxide ND ug/L 07/13/16 00:12 1024-57-307/07/16 13:190.075 0.050 1
Methoxychlor ND ug/L 07/13/16 00:12 72-43-507/07/16 13:191.0 0.15 1
Toxaphene ND ug/L 07/13/16 00:12 8001-35-207/07/16 13:191.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)61 %07/13/16 00:12 877-09-807/07/16 13:1920-130 1
Decachlorobiphenyl (S)61 %07/13/16 00:12 2051-24-307/07/16 13:1920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/08/16 12:51 12674-11-207/07/16 13:190.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/08/16 12:51 11104-28-207/07/16 13:190.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/08/16 12:51 11141-16-507/07/16 13:190.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/08/16 12:51 53469-21-907/07/16 13:190.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/08/16 12:51 12672-29-607/07/16 13:190.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/08/16 12:51 11097-69-107/07/16 13:190.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/08/16 12:51 11096-82-507/07/16 13:190.50 0.50 1
Surrogates
Decachlorobiphenyl (S)54 %07/08/16 12:51 2051-24-307/07/16 13:1910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 07/13/16 04:23 25057-89-007/11/16 08:250.096 0.048 1
2,4-D ND ug/L 07/13/16 04:23 94-75-707/11/16 08:250.95 0.23 1
Dalapon ND ug/L 07/13/16 04:23 75-99-007/11/16 08:250.92 0.44 1
2,4-DB ND ug/L 07/13/16 04:23 94-82-607/11/16 08:251.9 0.52 1
Dicamba ND ug/L 07/13/16 04:23 1918-00-907/11/16 08:250.095 0.030 1
Dichlorprop ND ug/L 07/13/16 04:23 120-36-507/11/16 08:250.66 0.19 1
Dinoseb ND ug/L 07/13/16 04:23 88-85-707/11/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 07/13/16 04:23 87-86-507/11/16 08:250.029 0.017 1
Picloram ND ug/L 07/13/16 04:23 1918-02-107/11/16 08:250.096 0.019 1
2,4,5-T ND ug/L 07/13/16 04:23 93-76-507/11/16 08:250.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 04:23 93-72-107/11/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-16 Lab ID:92304098012 Collected:07/05/16 11:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)69 %07/13/16 04:23 19719-28-907/11/16 08:2539-139 1
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 8380 ug/L 07/20/16 16:32 74-82-8 H5,N210.0 10.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 16:04 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 16:04 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 16:04 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 16:04 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 16:04 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 16:04 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 16:04 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 16:04 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 16:04 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 16:04 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 16:04 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 16:04 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 16:04 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 16:04 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 16:04 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 16:04 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 16:04 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 16:04 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 16:04 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 16:04 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 16:04 95-57-807/08/16 12:0610.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 07/12/16 16:04 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 16:04 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 16:04 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 16:04 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 16:04 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 16:04 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 16:04 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 16:04 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 16:04 84-66-207/08/16 12:0660001.3 1
Dimethoate ND ug/L 07/12/16 16:04 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 16:04 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 16:04 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 16:04 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 16:04 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 16:04 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 16:04 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 16:04 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 16:04 99-65-007/08/16 12:0620.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-16 Lab ID:92304098012 Collected:07/05/16 11:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dinitrophenol ND ug/L 07/12/16 16:04 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 16:04 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 16:04 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 16:04 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 16:04 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 16:04 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 16:04 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 16:04 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 16:04 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 16:04 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 16:04 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 16:04 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 16:04 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 16:04 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 16:04 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 16:04 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 16:04 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 16:04 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 16:04 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 16:04 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 16:04 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 16:04 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 16:04 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 16:04 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/12/16 16:04 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 16:04 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 16:0407/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 16:04 134-32-707/08/16 12:0610.0 0.96 1
2-Naphthalenamine ND ug/L 07/12/16 16:04 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 16:04 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 16:04 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 16:04 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 16:04 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 16:04 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 16:04 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 16:04 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 16:04 99-55-807/08/16 12:0610.0 1.2 1
N-Nitrosodiethylamine ND ug/L 07/12/16 16:04 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 16:04 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 16:04 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 16:04 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 16:04 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 16:04 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 16:04 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 16:04 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 16:04 126-68-107/08/16 12:0610.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-16 Lab ID:92304098012 Collected:07/05/16 11:00 Received:07/06/16 08:56 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 16:04 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 16:04 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 16:04 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 16:04 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 16:04 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 16:04 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 16:04 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 16:0407/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 16:04 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 16:04 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 16:04 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 16:04 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 16:04 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 16:04 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 16:04 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 16:04 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 16:04 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 16:04 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 16:04 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 16:04 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)78 %07/12/16 16:04 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)73 %07/12/16 16:04 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)87 %07/12/16 16:04 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)31 %07/12/16 16:04 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)42 %07/12/16 16:04 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)76 %07/12/16 16:04 118-79-607/08/16 12:0627-110 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.7J ug/L 07/12/16 17:29 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-6 Lab ID:92303930031 Collected:07/06/16 11:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:52 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:52 7440-38-207/11/16 20:3010.0 2.5 1
Barium 36.0J ug/L 07/18/16 20:52 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 20:52 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:52 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 20:52 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 13.6 ug/L 07/18/16 20:52 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 20:52 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 20:52 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 6.7J ug/L 07/18/16 20:52 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:52 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:52 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:52 7440-28-007/11/16 20:305.5 5.0 1
Vanadium ND ug/L 07/18/16 20:52 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 9.1J ug/L 07/18/16 20:52 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/14/16 05:23 67-64-110010.0 1
Acrylonitrile ND ug/L 07/14/16 05:23 107-13-12001.9 1
Benzene ND ug/L 07/14/16 05:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/14/16 05:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/14/16 05:23 75-27-41.0 0.18 1
Bromoform ND ug/L 07/14/16 05:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/14/16 05:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/14/16 05:23 78-93-31000.96 1
Carbon disulfide ND ug/L 07/14/16 05:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/14/16 05:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/14/16 05:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/14/16 05:23 75-00-310.0 0.54 1
Chloroform ND ug/L 07/14/16 05:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/14/16 05:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 05:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/14/16 05:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/14/16 05:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/14/16 05:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/14/16 05:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/14/16 05:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/14/16 05:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/14/16 05:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/14/16 05:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/14/16 05:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/14/16 05:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/14/16 05:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/14/16 05:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/14/16 05:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/14/16 05:23 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-6 Lab ID:92303930031 Collected:07/06/16 11:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 07/14/16 05:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/14/16 05:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/14/16 05:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/14/16 05:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 05:23 108-10-11000.33 1
Styrene ND ug/L 07/14/16 05:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 05:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 05:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/14/16 05:23 127-18-41.0 0.46 1
Toluene ND ug/L 07/14/16 05:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/14/16 05:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/14/16 05:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/14/16 05:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/14/16 05:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/14/16 05:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/14/16 05:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/14/16 05:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/14/16 05:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %07/14/16 05:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %07/14/16 05:23 17060-07-070-130 1
Toluene-d8 (S)99 %07/14/16 05:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-24 Lab ID:92303930032 Collected:07/06/16 12:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 20:55 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 20:55 7440-38-207/11/16 20:3010.0 2.5 1
Barium 207 ug/L 07/18/16 20:55 7440-39-307/11/16 20:301002.5 1
Beryllium 0.81J ug/L 07/18/16 20:55 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 20:55 7440-43-907/11/16 20:301.0 0.50 1
Chromium 16.7 ug/L 07/18/16 20:55 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 15.6 ug/L 07/18/16 20:55 7440-48-407/11/16 20:3010.0 2.5 1
Copper 4.4J ug/L 07/18/16 20:55 7440-50-807/11/16 20:3010.0 2.5 1
Lead 5.2J ug/L 07/18/16 20:55 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 11.3J ug/L 07/18/16 20:55 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 20:55 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 20:55 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 20:55 7440-28-007/11/16 20:305.5 5.0 1
Vanadium 10.4J ug/L 07/18/16 20:55 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 29.2 ug/L 07/18/16 20:55 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 333 ug/L 07/14/16 11:09 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/14/16 05:41 67-64-110010.0 1
Acrylonitrile ND ug/L 07/14/16 05:41 107-13-12001.9 1
Benzene ND ug/L 07/14/16 05:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/14/16 05:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/14/16 05:41 75-27-41.0 0.18 1
Bromoform ND ug/L 07/14/16 05:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/14/16 05:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/14/16 05:41 78-93-31000.96 1
Carbon disulfide ND ug/L 07/14/16 05:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/14/16 05:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/14/16 05:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/14/16 05:41 75-00-310.0 0.54 1
Chloroform ND ug/L 07/14/16 05:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/14/16 05:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 05:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/14/16 05:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/14/16 05:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/14/16 05:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/14/16 05:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/14/16 05:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/14/16 05:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/14/16 05:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/14/16 05:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/14/16 05:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.83J ug/L 07/14/16 05:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/14/16 05:41 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-24 Lab ID:92303930032 Collected:07/06/16 12:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 07/14/16 05:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/14/16 05:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/14/16 05:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/14/16 05:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/14/16 05:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/14/16 05:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/14/16 05:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 05:41 108-10-11000.33 1
Styrene ND ug/L 07/14/16 05:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 05:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 05:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/14/16 05:41 127-18-41.0 0.46 1
Toluene ND ug/L 07/14/16 05:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/14/16 05:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/14/16 05:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/14/16 05:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/14/16 05:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/14/16 05:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/14/16 05:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/14/16 05:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/14/16 05:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %07/14/16 05:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %07/14/16 05:41 17060-07-070-130 1
Toluene-d8 (S)100 %07/14/16 05:41 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 36600 ug/L 07/16/16 00:22500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/12/16 13:30 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4920J ug/L 07/08/16 19:42 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 309J ug/L 07/08/16 08:171000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 18300 ug/L 07/16/16 02:39 16887-00-6 M110005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 26000 ug/L 07/22/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-24 Lab ID:92303930032 Collected:07/06/16 12:00 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2210 ug/L 07/23/16 12:45 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-25 Lab ID:92303930034 Collected:07/06/16 12:20 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 21:11 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 21:11 7440-38-207/11/16 20:3010.0 2.5 1
Barium 62.6J ug/L 07/18/16 21:11 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 21:11 7440-41-707/11/16 20:301.0 0.50 1
Cadmium 0.94J ug/L 07/18/16 21:11 7440-43-907/11/16 20:301.0 0.50 1
Chromium 4.7J ug/L 07/18/16 21:11 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 5.5J ug/L 07/18/16 21:11 7440-48-407/11/16 20:3010.0 2.5 1
Copper 3.2J ug/L 07/18/16 21:11 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 21:11 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 5.1J ug/L 07/18/16 21:11 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 21:11 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 21:11 7440-22-407/11/16 20:3010.0 2.5 1
Thallium ND ug/L 07/18/16 21:11 7440-28-007/11/16 20:305.5 5.0 1
Vanadium 3.5J ug/L 07/18/16 21:11 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 13.6 ug/L 07/18/16 21:11 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 465 ug/L 07/14/16 11:22 7439-89-607/13/16 19:4950.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/14/16 06:15 67-64-110010.0 1
Acrylonitrile ND ug/L 07/14/16 06:15 107-13-12001.9 1
Benzene ND ug/L 07/14/16 06:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/14/16 06:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/14/16 06:15 75-27-41.0 0.18 1
Bromoform ND ug/L 07/14/16 06:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/14/16 06:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/14/16 06:15 78-93-31000.96 1
Carbon disulfide ND ug/L 07/14/16 06:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/14/16 06:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/14/16 06:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/14/16 06:15 75-00-310.0 0.54 1
Chloroform ND ug/L 07/14/16 06:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/14/16 06:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 06:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/14/16 06:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/14/16 06:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/14/16 06:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/14/16 06:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/14/16 06:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/14/16 06:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/14/16 06:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/14/16 06:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/14/16 06:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/14/16 06:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/14/16 06:15 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-25 Lab ID:92303930034 Collected:07/06/16 12:20 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 07/14/16 06:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 07/14/16 06:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/14/16 06:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/14/16 06:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/14/16 06:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/14/16 06:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/14/16 06:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 06:15 108-10-11000.33 1
Styrene ND ug/L 07/14/16 06:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 06:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 06:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/14/16 06:15 127-18-41.0 0.46 1
Toluene ND ug/L 07/14/16 06:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/14/16 06:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/14/16 06:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/14/16 06:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/14/16 06:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/14/16 06:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/14/16 06:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/14/16 06:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/14/16 06:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %07/14/16 06:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %07/14/16 06:15 17060-07-070-130 1
Toluene-d8 (S)99 %07/14/16 06:15 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 17400 ug/L 07/16/16 01:29500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/13/16 16:00 18496-25-8 M110001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4710J ug/L 07/08/16 20:25 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 1130J ug/L 07/08/16 08:181000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3800 ug/L 07/16/16 02:49 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 07/22/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-25 Lab ID:92303930034 Collected:07/06/16 12:20 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1990 ug/L 07/23/16 14:04 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-9 Lab ID:92303930036 Collected:07/06/16 09:30 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 20:21 309-00-207/12/16 08:050.050 0.050 1
alpha-BHC ND ug/L 07/12/16 20:21 319-84-607/12/16 08:050.050 0.050 1
beta-BHC ND ug/L 07/12/16 20:21 319-85-707/12/16 08:050.050 0.050 1
delta-BHC ND ug/L 07/12/16 20:21 319-86-807/12/16 08:050.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 20:21 58-89-907/12/16 08:050.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 20:21 57-74-907/12/16 08:050.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 20:21 72-54-807/12/16 08:050.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 20:21 72-55-907/12/16 08:050.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 20:21 50-29-307/12/16 08:050.10 0.050 1
Dieldrin ND ug/L 07/12/16 20:21 60-57-107/12/16 08:050.075 0.050 1
Endosulfan I ND ug/L 07/12/16 20:21 959-98-807/12/16 08:050.10 0.050 1
Endosulfan II ND ug/L 07/12/16 20:21 33213-65-907/12/16 08:050.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 20:21 1031-07-807/12/16 08:050.10 0.050 1
Endrin ND ug/L 07/12/16 20:21 72-20-807/12/16 08:050.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 20:21 7421-93-407/12/16 08:050.10 0.050 1
Heptachlor ND ug/L 07/12/16 20:21 76-44-807/12/16 08:050.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 20:21 1024-57-307/12/16 08:050.075 0.050 1
Methoxychlor ND ug/L 07/12/16 20:21 72-43-507/12/16 08:051.0 0.15 1
Toxaphene ND ug/L 07/12/16 20:21 8001-35-207/12/16 08:051.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %07/12/16 20:21 877-09-807/12/16 08:0520-130 1
Decachlorobiphenyl (S)134 %07/12/16 20:21 2051-24-3 S307/12/16 08:0520-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/09/16 18:31 12674-11-207/08/16 13:240.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/09/16 18:31 11104-28-207/08/16 13:240.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/09/16 18:31 11141-16-507/08/16 13:240.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/09/16 18:31 53469-21-907/08/16 13:240.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/09/16 18:31 12672-29-607/08/16 13:240.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/09/16 18:31 11097-69-107/08/16 13:240.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/09/16 18:31 11096-82-507/08/16 13:240.50 0.50 1
Surrogates
Decachlorobiphenyl (S)58 %07/09/16 18:31 2051-24-307/08/16 13:2410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 07/13/16 04:53 94-75-707/11/16 08:250.95 0.23 1
Dinoseb ND ug/L 07/13/16 04:53 88-85-707/11/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 07/13/16 04:53 87-86-507/11/16 08:250.029 0.017 1
2,4,5-T ND ug/L 07/13/16 04:53 93-76-507/11/16 08:250.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 04:53 93-72-107/11/16 08:250.19 0.050 1
Surrogates
2,4-DCAA (S)76 %07/13/16 04:53 19719-28-907/11/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 21:14 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 21:14 7440-38-207/11/16 20:3010.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-9 Lab ID:92303930036 Collected:07/06/16 09:30 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 152 ug/L 07/18/16 21:14 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 21:14 7440-41-707/11/16 20:301.0 0.50 1
Cadmium ND ug/L 07/18/16 21:14 7440-43-907/11/16 20:301.0 0.50 1
Chromium 4.6J ug/L 07/18/16 21:14 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 247 ug/L 07/18/16 21:14 7440-48-407/11/16 20:3010.0 2.5 1
Copper ND ug/L 07/18/16 21:14 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 21:14 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 65.7 ug/L 07/18/16 21:14 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 21:14 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 21:14 7440-22-407/11/16 20:3010.0 2.5 1
Thallium 6.2 ug/L 07/18/16 21:14 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 21:14 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 21:14 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 19.4 ug/L 07/18/16 21:14 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 17:00 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 17:00 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 17:00 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 17:00 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 17:00 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 17:00 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 17:00 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 17:00 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 17:00 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 17:00 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 17:00 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 17:00 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 17:00 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 17:00 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 17:00 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 17:00 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 17:00 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 17:00 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 17:00 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 17:00 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 17:00 95-57-807/08/16 12:0610.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 07/12/16 17:00 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 17:00 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 17:00 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 17:00 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 17:00 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 17:00 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 17:00 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 17:00 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 17:00 84-66-207/08/16 12:0660001.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-9 Lab ID:92303930036 Collected:07/06/16 09:30 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dimethoate ND ug/L 07/12/16 17:00 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 17:00 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 17:00 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 17:00 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 17:00 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 17:00 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 17:00 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 17:00 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 17:00 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/12/16 17:00 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 17:00 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 17:00 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 17:00 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 17:00 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 17:00 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 17:00 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 17:00 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 17:00 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 17:00 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 17:00 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 17:00 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 17:00 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 17:00 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 17:00 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 17:00 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 17:00 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 17:00 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 17:00 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 17:00 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 17:00 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 17:00 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 17:00 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 17:00 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/12/16 17:00 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 17:00 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 17:0007/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 17:00 134-32-707/08/16 12:0610.0 0.96 1
2-Naphthalenamine ND ug/L 07/12/16 17:00 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 17:00 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 17:00 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 17:00 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 17:00 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 17:00 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 17:00 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 17:00 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 17:00 99-55-807/08/16 12:0610.0 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-9 Lab ID:92303930036 Collected:07/06/16 09:30 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
N-Nitrosodiethylamine ND ug/L 07/12/16 17:00 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 17:00 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 17:00 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 17:00 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 17:00 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 17:00 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 17:00 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 17:00 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 17:00 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 17:00 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 17:00 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 17:00 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 17:00 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 17:00 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 17:00 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 17:00 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 17:0007/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 17:00 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 17:00 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 17:00 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 17:00 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 17:00 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 17:00 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 17:00 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 17:00 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 17:00 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 17:00 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 17:00 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 17:00 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)73 %07/12/16 17:00 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)70 %07/12/16 17:00 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)87 %07/12/16 17:00 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)32 %07/12/16 17:00 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)41 %07/12/16 17:00 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)81 %07/12/16 17:00 118-79-607/08/16 12:0627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/14/16 06:32 67-64-110010.0 1
Acetonitrile ND ug/L 07/14/16 06:32 75-05-855.0 2.2 1
Acrolein ND ug/L 07/14/16 06:32 107-02-8 L353.0 1.6 1
Acrylonitrile ND ug/L 07/14/16 06:32 107-13-12001.9 1
Allyl chloride ND ug/L 07/14/16 06:32 107-05-110.0 1.5 1
Benzene 0.89J ug/L 07/14/16 06:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/14/16 06:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/14/16 06:32 75-27-41.0 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-9 Lab ID:92303930036 Collected:07/06/16 09:30 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Bromoform ND ug/L 07/14/16 06:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/14/16 06:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/14/16 06:32 78-93-31000.96 1
Carbon disulfide ND ug/L 07/14/16 06:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/14/16 06:32 56-23-51.0 0.25 1
Chlorobenzene 1.2J ug/L 07/14/16 06:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/14/16 06:32 75-00-310.0 0.54 1
Chloroform ND ug/L 07/14/16 06:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/14/16 06:32 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/14/16 06:32 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 06:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/14/16 06:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/14/16 06:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/14/16 06:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/14/16 06:32 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/14/16 06:32 541-73-15.0 0.24 1
1,4-Dichlorobenzene 2.2 ug/L 07/14/16 06:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/14/16 06:32 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/14/16 06:32 75-71-85.0 0.21 1
1,1-Dichloroethane 0.59J ug/L 07/14/16 06:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/14/16 06:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/14/16 06:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 12.9 ug/L 07/14/16 06:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/14/16 06:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/14/16 06:32 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/14/16 06:32 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/14/16 06:32 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/14/16 06:32 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/14/16 06:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/14/16 06:32 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/14/16 06:32 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/14/16 06:32 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/14/16 06:32 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/14/16 06:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/14/16 06:32 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/14/16 06:32 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/14/16 06:32 126-98-71000.93 1
Methylene Chloride ND ug/L 07/14/16 06:32 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 07/14/16 06:32 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 06:32 108-10-11000.33 1
Naphthalene ND ug/L 07/14/16 06:32 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/14/16 06:32 107-12-01503.6 1
Styrene ND ug/L 07/14/16 06:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 06:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 06:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/14/16 06:32 127-18-41.0 0.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-9 Lab ID:92303930036 Collected:07/06/16 09:30 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Toluene ND ug/L 07/14/16 06:32 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/14/16 06:32 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/14/16 06:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/14/16 06:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/14/16 06:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/14/16 06:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/14/16 06:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/14/16 06:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/14/16 06:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/14/16 06:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %07/14/16 06:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %07/14/16 06:32 17060-07-070-130 1
Toluene-d8 (S)100 %07/14/16 06:32 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/13/16 16:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 6.4J ug/L 07/12/16 17:41 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-2 Lab ID:92303930037 Collected:07/06/16 11:40 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 07/12/16 22:25 309-00-207/12/16 08:050.050 0.050 1
alpha-BHC ND ug/L 07/12/16 22:25 319-84-607/12/16 08:050.050 0.050 1
beta-BHC ND ug/L 07/12/16 22:25 319-85-707/12/16 08:050.050 0.050 1
delta-BHC ND ug/L 07/12/16 22:25 319-86-807/12/16 08:050.050 0.050 1
gamma-BHC (Lindane)ND ug/L 07/12/16 22:25 58-89-907/12/16 08:050.050 0.050 1
Chlordane (Technical)ND ug/L 07/12/16 22:25 57-74-907/12/16 08:050.50 0.20 1
4,4'-DDD ND ug/L 07/12/16 22:25 72-54-807/12/16 08:050.10 0.050 1
4,4'-DDE ND ug/L 07/12/16 22:25 72-55-907/12/16 08:050.10 0.050 1
4,4'-DDT ND ug/L 07/12/16 22:25 50-29-307/12/16 08:050.10 0.050 1
Dieldrin ND ug/L 07/12/16 22:25 60-57-107/12/16 08:050.075 0.050 1
Endosulfan I ND ug/L 07/12/16 22:25 959-98-807/12/16 08:050.10 0.050 1
Endosulfan II ND ug/L 07/12/16 22:25 33213-65-907/12/16 08:050.10 0.050 1
Endosulfan sulfate ND ug/L 07/12/16 22:25 1031-07-807/12/16 08:050.10 0.050 1
Endrin ND ug/L 07/12/16 22:25 72-20-807/12/16 08:050.10 0.050 1
Endrin aldehyde ND ug/L 07/12/16 22:25 7421-93-407/12/16 08:050.10 0.050 1
Heptachlor ND ug/L 07/12/16 22:25 76-44-807/12/16 08:050.050 0.050 1
Heptachlor epoxide ND ug/L 07/12/16 22:25 1024-57-307/12/16 08:050.075 0.050 1
Methoxychlor ND ug/L 07/12/16 22:25 72-43-507/12/16 08:051.0 0.15 1
Toxaphene ND ug/L 07/12/16 22:25 8001-35-207/12/16 08:051.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %07/12/16 22:25 877-09-807/12/16 08:0520-130 1
Decachlorobiphenyl (S)86 %07/12/16 22:25 2051-24-307/12/16 08:0520-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 07/09/16 18:51 12674-11-207/08/16 13:240.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 07/09/16 18:51 11104-28-207/08/16 13:240.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 07/09/16 18:51 11141-16-507/08/16 13:240.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 07/09/16 18:51 53469-21-907/08/16 13:240.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 07/09/16 18:51 12672-29-607/08/16 13:240.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 07/09/16 18:51 11097-69-107/08/16 13:240.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 07/09/16 18:51 11096-82-507/08/16 13:240.50 0.50 1
Surrogates
Decachlorobiphenyl (S)50 %07/09/16 18:51 2051-24-307/08/16 13:2410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 07/13/16 05:23 94-75-707/11/16 08:250.98 0.23 1
Dinoseb ND ug/L 07/13/16 05:23 88-85-707/11/16 08:250.20 0.059 1
Pentachlorophenol ND ug/L 07/13/16 05:23 87-86-507/11/16 08:250.030 0.018 1
2,4,5-T ND ug/L 07/13/16 05:23 93-76-507/11/16 08:250.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 07/13/16 05:23 93-72-107/11/16 08:250.20 0.051 1
Surrogates
2,4-DCAA (S)84 %07/13/16 05:23 19719-28-907/11/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 07/18/16 21:18 7440-36-007/11/16 20:306.0 3.8 1
Arsenic ND ug/L 07/18/16 21:18 7440-38-207/11/16 20:3010.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-2 Lab ID:92303930037 Collected:07/06/16 11:40 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 106 ug/L 07/18/16 21:18 7440-39-307/11/16 20:301002.5 1
Beryllium ND ug/L 07/18/16 21:18 7440-41-707/11/16 20:301.0 0.50 1
Cadmium 2.9 ug/L 07/18/16 21:18 7440-43-907/11/16 20:301.0 0.50 1
Chromium ND ug/L 07/18/16 21:18 7440-47-307/11/16 20:3010.0 2.5 1
Cobalt 820 ug/L 07/18/16 21:18 7440-48-407/11/16 20:3010.0 2.5 1
Copper 2.7J ug/L 07/18/16 21:18 7440-50-807/11/16 20:3010.0 2.5 1
Lead ND ug/L 07/18/16 21:18 7439-92-107/11/16 20:3010.0 2.5 1
Nickel 39.3J ug/L 07/18/16 21:18 7440-02-007/11/16 20:3050.0 2.5 1
Selenium ND ug/L 07/18/16 21:18 7782-49-207/11/16 20:3010.0 5.0 1
Silver ND ug/L 07/18/16 21:18 7440-22-407/11/16 20:3010.0 2.5 1
Thallium 6.6 ug/L 07/18/16 21:18 7440-28-007/11/16 20:305.5 5.0 1
Tin ND ug/L 07/18/16 21:18 7440-31-507/11/16 20:301002.5 1
Vanadium ND ug/L 07/18/16 21:18 7440-62-207/11/16 20:3025.0 2.5 1
Zinc 471 ug/L 07/18/16 21:18 7440-66-607/11/16 20:3010.0 5.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 07/12/16 17:28 83-32-907/08/16 12:0610.0 0.25 1
Acenaphthylene ND ug/L 07/12/16 17:28 208-96-807/08/16 12:0610.0 0.21 1
Acetophenone ND ug/L 07/12/16 17:28 98-86-207/08/16 12:0610.0 2.0 1
2-Acetylaminofluorene ND ug/L 07/12/16 17:28 53-96-307/08/16 12:0620.0 0.84 1
4-Aminobiphenyl ND ug/L 07/12/16 17:28 92-67-107/08/16 12:0620.0 0.92 1
Anthracene ND ug/L 07/12/16 17:28 120-12-707/08/16 12:0610.0 0.14 1
Benzo(a)anthracene ND ug/L 07/12/16 17:28 56-55-307/08/16 12:0610.0 0.33 1
Benzo(a)pyrene ND ug/L 07/12/16 17:28 50-32-807/08/16 12:0610.0 0.30 1
Benzo(b)fluoranthene ND ug/L 07/12/16 17:28 205-99-207/08/16 12:0610.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 07/12/16 17:28 191-24-207/08/16 12:0610.0 0.38 1
Benzo(k)fluoranthene ND ug/L 07/12/16 17:28 207-08-907/08/16 12:0610.0 0.43 1
Benzyl alcohol ND ug/L 07/12/16 17:28 100-51-607/08/16 12:0620.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 07/12/16 17:28 101-55-307/08/16 12:0610.0 1.3 1
Butylbenzylphthalate ND ug/L 07/12/16 17:28 85-68-707/08/16 12:0610.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 07/12/16 17:28 59-50-707/08/16 12:0620.0 4.2 1
4-Chloroaniline ND ug/L 07/12/16 17:28 106-47-807/08/16 12:0620.0 3.4 1
Chlorobenzilate ND ug/L 07/12/16 17:28 510-15-607/08/16 12:0610.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/16 17:28 111-91-107/08/16 12:0610.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/12/16 17:28 111-44-407/08/16 12:0610.0 1.5 1
2-Chloronaphthalene ND ug/L 07/12/16 17:28 91-58-707/08/16 12:0610.0 2.2 1
2-Chlorophenol ND ug/L 07/12/16 17:28 95-57-807/08/16 12:0610.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 07/12/16 17:28 7005-72-307/08/16 12:0610.0 2.1 1
Chrysene ND ug/L 07/12/16 17:28 218-01-907/08/16 12:0610.0 0.21 1
Diallate ND ug/L 07/12/16 17:28 2303-16-407/08/16 12:0610.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/16 17:28 53-70-307/08/16 12:0610.0 0.55 1
Dibenzofuran ND ug/L 07/12/16 17:28 132-64-907/08/16 12:0610.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 07/12/16 17:28 91-94-107/08/16 12:0620.0 1.4 1
2,4-Dichlorophenol ND ug/L 07/12/16 17:28 120-83-207/08/16 12:0610.0 1.7 1
2,6-Dichlorophenol ND ug/L 07/12/16 17:28 87-65-007/08/16 12:0610.0 1.8 1
Diethylphthalate ND ug/L 07/12/16 17:28 84-66-207/08/16 12:0660001.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-2 Lab ID:92303930037 Collected:07/06/16 11:40 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dimethoate ND ug/L 07/12/16 17:28 60-51-507/08/16 12:0620.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 07/12/16 17:28 60-11-707/08/16 12:0610.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 07/12/16 17:28 57-97-607/08/16 12:0610.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 07/12/16 17:28 119-93-707/08/16 12:0610.0 2.1 1
2,4-Dimethylphenol ND ug/L 07/12/16 17:28 105-67-907/08/16 12:0610.0 2.2 1
Dimethylphthalate ND ug/L 07/12/16 17:28 131-11-307/08/16 12:0610.0 1.5 1
Di-n-butylphthalate ND ug/L 07/12/16 17:28 84-74-207/08/16 12:0610.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/16 17:28 534-52-107/08/16 12:0650.0 1.7 1
1,3-Dinitrobenzene ND ug/L 07/12/16 17:28 99-65-007/08/16 12:0620.0 1.5 1
2,4-Dinitrophenol ND ug/L 07/12/16 17:28 51-28-507/08/16 12:0650.0 6.5 1
2,4-Dinitrotoluene ND ug/L 07/12/16 17:28 121-14-207/08/16 12:0610.0 1.2 1
2,6-Dinitrotoluene ND ug/L 07/12/16 17:28 606-20-207/08/16 12:0610.0 1.7 1
Di-n-octylphthalate ND ug/L 07/12/16 17:28 117-84-007/08/16 12:0610.0 0.86 1
Diphenylamine ND ug/L 07/12/16 17:28 122-39-407/08/16 12:0610.0 1.3 1
Disulfoton ND ug/L 07/12/16 17:28 298-04-407/08/16 12:0610.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/16 17:28 117-81-707/08/16 12:0615.0 0.85 1
Ethyl methanesulfonate ND ug/L 07/12/16 17:28 62-50-007/08/16 12:0620.0 1.8 1
Famphur ND ug/L 07/12/16 17:28 52-85-707/08/16 12:0620.0 1.7 1
Fluoranthene ND ug/L 07/12/16 17:28 206-44-007/08/16 12:0610.0 0.21 1
Fluorene ND ug/L 07/12/16 17:28 86-73-707/08/16 12:0610.0 0.21 1
Hexachlorobenzene ND ug/L 07/12/16 17:28 118-74-107/08/16 12:0610.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/16 17:28 77-47-407/08/16 12:0610.0 1.8 1
Hexachloroethane ND ug/L 07/12/16 17:28 67-72-107/08/16 12:0610.0 1.5 1
Hexachloropropene ND ug/L 07/12/16 17:28 1888-71-707/08/16 12:0610.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/16 17:28 193-39-507/08/16 12:0610.0 0.29 1
Isodrin ND ug/L 07/12/16 17:28 465-73-607/08/16 12:0620.0 2.0 1
Isophorone ND ug/L 07/12/16 17:28 78-59-107/08/16 12:0610.0 1.8 1
Isosafrole ND ug/L 07/12/16 17:28 120-58-107/08/16 12:0610.0 1.8 1
Kepone ND ug/L 07/12/16 17:28 143-50-007/08/16 12:0620.0 3.1 1
Methapyrilene ND ug/L 07/12/16 17:28 91-80-507/08/16 12:061002.7 1
3-Methylcholanthrene ND ug/L 07/12/16 17:28 56-49-507/08/16 12:0610.0 0.82 1
Methyl methanesulfonate ND ug/L 07/12/16 17:28 66-27-307/08/16 12:0610.0 1.3 1
2-Methylnaphthalene ND ug/L 07/12/16 17:28 91-57-607/08/16 12:0610.0 0.28 1
Methyl parathion ND ug/L 07/12/16 17:28 298-00-007/08/16 12:0610.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/16 17:28 95-48-707/08/16 12:0610.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/16 17:2807/08/16 12:0610.0 1.7 1
1-Naphthalenamine ND ug/L 07/12/16 17:28 134-32-707/08/16 12:0610.0 0.96 1
2-Naphthalenamine ND ug/L 07/12/16 17:28 91-59-807/08/16 12:0610.0 0.98 1
1,4-Naphthoquinone ND ug/L 07/12/16 17:28 130-15-407/08/16 12:0610.0 1.8 1
2-Nitroaniline ND ug/L 07/12/16 17:28 88-74-407/08/16 12:0650.0 2.8 1
3-Nitroaniline ND ug/L 07/12/16 17:28 99-09-207/08/16 12:0650.0 2.4 1
4-Nitroaniline ND ug/L 07/12/16 17:28 100-01-607/08/16 12:0620.0 2.5 1
Nitrobenzene ND ug/L 07/12/16 17:28 98-95-307/08/16 12:0610.0 1.7 1
2-Nitrophenol ND ug/L 07/12/16 17:28 88-75-507/08/16 12:0610.0 1.7 1
4-Nitrophenol ND ug/L 07/12/16 17:28 100-02-707/08/16 12:0650.0 5.8 1
5-Nitro-o-toluidine ND ug/L 07/12/16 17:28 99-55-807/08/16 12:0610.0 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-2 Lab ID:92303930037 Collected:07/06/16 11:40 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
N-Nitrosodiethylamine ND ug/L 07/12/16 17:28 55-18-507/08/16 12:0620.0 1.8 1
N-Nitrosodimethylamine ND ug/L 07/12/16 17:28 62-75-907/08/16 12:0610.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 07/12/16 17:28 924-16-307/08/16 12:0610.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/16 17:28 621-64-707/08/16 12:0610.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/16 17:28 86-30-607/08/16 12:0610.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 07/12/16 17:28 10595-95-607/08/16 12:0610.0 1.8 1
N-Nitrosopiperidine ND ug/L 07/12/16 17:28 100-75-407/08/16 12:0620.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 07/12/16 17:28 930-55-207/08/16 12:0610.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 07/12/16 17:28 126-68-107/08/16 12:0610.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/16 17:28 108-60-107/08/16 12:0610.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 07/12/16 17:28 56-38-207/08/16 12:0610.0 1.1 1
Pentachlorobenzene ND ug/L 07/12/16 17:28 608-93-507/08/16 12:0610.0 2.0 1
Pentachloronitrobenzene ND ug/L 07/12/16 17:28 82-68-807/08/16 12:0620.0 1.0 1
Pentachlorophenol ND ug/L 07/12/16 17:28 87-86-507/08/16 12:0625.0 2.3 1
Phenacetin ND ug/L 07/12/16 17:28 62-44-207/08/16 12:0620.0 0.97 1
Phenanthrene ND ug/L 07/12/16 17:28 85-01-807/08/16 12:0610.0 0.22 1
Phenol ND ug/L 07/12/16 17:2807/08/16 12:0610.0 1.7 1
p-Phenylenediamine ND ug/L 07/12/16 17:28 106-50-307/08/16 12:0610.0 0.96 1
Phorate ND ug/L 07/12/16 17:28 298-02-207/08/16 12:0610.0 1.1 1
Pronamide ND ug/L 07/12/16 17:28 23950-58-507/08/16 12:0610.0 0.97 1
Pyrene ND ug/L 07/12/16 17:28 129-00-007/08/16 12:0610.0 0.19 1
Safrole ND ug/L 07/12/16 17:28 94-59-707/08/16 12:0610.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 07/12/16 17:28 95-94-307/08/16 12:0610.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 07/12/16 17:28 58-90-207/08/16 12:0610.0 2.3 1
Thionazin ND ug/L 07/12/16 17:28 297-97-207/08/16 12:0620.0 1.2 1
O-Toluidine ND ug/L 07/12/16 17:28 95-53-407/08/16 12:0610.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/12/16 17:28 95-95-407/08/16 12:0610.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 07/12/16 17:28 88-06-207/08/16 12:0610.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 07/12/16 17:28 99-35-407/08/16 12:0610.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)78 %07/12/16 17:28 4165-60-007/08/16 12:0621-110 1
2-Fluorobiphenyl (S)71 %07/12/16 17:28 321-60-807/08/16 12:0627-110 1
Terphenyl-d14 (S)89 %07/12/16 17:28 1718-51-007/08/16 12:0631-107 1
Phenol-d6 (S)33 %07/12/16 17:28 13127-88-307/08/16 12:0610-110 1
2-Fluorophenol (S)43 %07/12/16 17:28 367-12-407/08/16 12:0612-110 1
2,4,6-Tribromophenol (S)78 %07/12/16 17:28 118-79-607/08/16 12:0627-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/14/16 06:49 67-64-110010.0 1
Acetonitrile ND ug/L 07/14/16 06:49 75-05-855.0 2.2 1
Acrolein ND ug/L 07/14/16 06:49 107-02-8 L353.0 1.6 1
Acrylonitrile ND ug/L 07/14/16 06:49 107-13-12001.9 1
Allyl chloride ND ug/L 07/14/16 06:49 107-05-110.0 1.5 1
Benzene 0.41J ug/L 07/14/16 06:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/14/16 06:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/14/16 06:49 75-27-41.0 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-2 Lab ID:92303930037 Collected:07/06/16 11:40 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Bromoform ND ug/L 07/14/16 06:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/14/16 06:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/14/16 06:49 78-93-31000.96 1
Carbon disulfide ND ug/L 07/14/16 06:49 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/14/16 06:49 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/14/16 06:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/14/16 06:49 75-00-310.0 0.54 1
Chloroform ND ug/L 07/14/16 06:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/14/16 06:49 74-87-31.0 0.11 1
Chloroprene ND ug/L 07/14/16 06:49 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 06:49 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/14/16 06:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/14/16 06:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/14/16 06:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/14/16 06:49 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 07/14/16 06:49 541-73-15.0 0.24 1
1,4-Dichlorobenzene 0.78J ug/L 07/14/16 06:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/14/16 06:49 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 07/14/16 06:49 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 07/14/16 06:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/14/16 06:49 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/14/16 06:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.0J ug/L 07/14/16 06:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/14/16 06:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/14/16 06:49 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/14/16 06:49 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/14/16 06:49 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 07/14/16 06:49 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 07/14/16 06:49 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/14/16 06:49 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/14/16 06:49 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 07/14/16 06:49 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 07/14/16 06:49 87-68-310.0 0.71 1
2-Hexanone ND ug/L 07/14/16 06:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/14/16 06:49 74-88-410.0 0.32 1
Isobutanol ND ug/L 07/14/16 06:49 78-83-110035.0 1
Methacrylonitrile ND ug/L 07/14/16 06:49 126-98-71000.93 1
Methylene Chloride ND ug/L 07/14/16 06:49 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 07/14/16 06:49 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 06:49 108-10-11000.33 1
Naphthalene ND ug/L 07/14/16 06:49 91-20-310.0 0.24 1
Propionitrile ND ug/L 07/14/16 06:49 107-12-01503.6 1
Styrene ND ug/L 07/14/16 06:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 06:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 06:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/14/16 06:49 127-18-41.0 0.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 190
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Sample:MW-2 Lab ID:92303930037 Collected:07/06/16 11:40 Received:07/07/16 10:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Toluene ND ug/L 07/14/16 06:49 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 07/14/16 06:49 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 07/14/16 06:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/14/16 06:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/14/16 06:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/14/16 06:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/14/16 06:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/14/16 06:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/14/16 06:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/14/16 06:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %07/14/16 06:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %07/14/16 06:49 17060-07-070-130 1
Toluene-d8 (S)100 %07/14/16 06:49 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 07/13/16 16:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 8.5J ug/L 07/12/16 17:42 57-12-5 B10.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321519
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Associated Lab Samples:92304098001, 92304098002, 92304098010, 92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1781804
Associated Lab Samples:92304098001, 92304098002, 92304098010, 92304098012
Matrix:Water
AnalyzedMDL
Methane ug/L ND 10.0 N207/20/16 14:4810.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1781805LABORATORY CONTROL SAMPLE:
LCSSpike
Methane ug/L 454 N239611570-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1783837MATRIX SPIKE SAMPLE:
MSSpike
Result
92304098010
Methane ug/L 10700 H5,M1,N239614370-13010100
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304098012
1783838SAMPLE DUPLICATE:
Methane ug/L 7530 H5,N211208380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320770
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92304098003, 92304098004, 92304098005, 92304098007, 92304098008, 92304098009, 92304098010,
92304098011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1777274
Associated Lab Samples:92304098003, 92304098004, 92304098005, 92304098007, 92304098008, 92304098009, 92304098010,
92304098011
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 07/15/16 11:450.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1777275LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777276MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303393001
1777277
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 103 75-125102 1 252.5ND 2.6 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320140
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92303930002, 92303930003, 92303930004, 92303930005, 92303930006, 92303930007, 92303930008,
92303930009, 92303930010, 92303930011, 92303930012, 92303930013, 92303930014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1774122
Associated Lab Samples:92303930002, 92303930003, 92303930004, 92303930005, 92303930006, 92303930007, 92303930008,
92303930009, 92303930010, 92303930011, 92303930012, 92303930013, 92303930014
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 07/08/16 19:123.8
Arsenic ug/L ND 10.0 07/08/16 19:122.5
Barium ug/L ND 100 07/08/16 19:122.5
Beryllium ug/L ND 1.0 07/08/16 19:120.50
Cadmium ug/L ND 1.0 07/08/16 19:120.50
Chromium ug/L ND 10.0 07/08/16 19:122.5
Cobalt ug/L ND 10.0 07/08/16 19:122.5
Copper ug/L ND 10.0 07/08/16 19:122.5
Lead ug/L ND 10.0 07/08/16 19:122.5
Nickel ug/L ND 50.0 07/08/16 19:122.5
Selenium ug/L ND 10.0 07/08/16 19:125.0
Silver ug/L ND 10.0 07/08/16 19:122.5
Thallium ug/L ND 5.5 07/08/16 19:125.0
Vanadium ug/L ND 25.0 07/08/16 19:122.5
Zinc ug/L ND 10.0 07/08/16 19:125.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774123LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 491500 98 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 498500 100 80-120
Beryllium ug/L 501500 100 80-120
Cadmium ug/L 494500 99 80-120
Chromium ug/L 502500 100 80-120
Cobalt ug/L 489500 98 80-120
Copper ug/L 495500 99 80-120
Lead ug/L 488500 98 80-120
Nickel ug/L 494500 99 80-120
Selenium ug/L 486500 97 80-120
Silver ug/L 248250 99 80-120
Thallium ug/L 490500 98 80-120
Vanadium ug/L 496500 99 80-120
Zinc ug/L 492500 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1774124MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303571012
1774125
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12598 0 25500ND490492
Arsenic ug/L 500 95 75-12596 1 25500ND474479
Barium ug/L 500 98 75-12598 0 25500146637635
Beryllium ug/L 500 99 75-12599 0 25500ND496498
Cadmium ug/L 500 97 75-12598 1 25500ND486489
Chromium ug/L 500 97 75-125100 3 25500ND488501
Cobalt ug/L 500 95 75-12595 0 25500ND474475
Copper ug/L 500 98 75-12599 1 25500ND490494
Lead ug/L 500 94 75-12594 0 25500ND471473
Nickel ug/L 500 95 75-12596 2 25500ND474482
Selenium ug/L 500 97 75-12597 1 25500ND483486
Silver ug/L 250 98 75-12598 0 25250ND244245
Thallium ug/L 500 94 75-12595 1 25500ND471477
Vanadium ug/L 500 98 75-12598 0 25500ND491493
Zinc ug/L 500 95 75-125100 5 25500ND478503
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320141
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92303930015, 92303930016, 92303930017, 92303930018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1774126
Associated Lab Samples:92303930015, 92303930016, 92303930017, 92303930018
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 07/10/16 18:113.8
Arsenic ug/L ND 10.0 07/10/16 18:112.5
Barium ug/L ND 100 07/10/16 18:112.5
Beryllium ug/L ND 1.0 07/10/16 18:110.50
Cadmium ug/L ND 1.0 07/10/16 18:110.50
Chromium ug/L ND 10.0 07/10/16 18:112.5
Cobalt ug/L ND 10.0 07/10/16 18:112.5
Copper ug/L ND 10.0 07/10/16 18:112.5
Lead ug/L ND 10.0 07/10/16 18:112.5
Nickel ug/L ND 50.0 07/10/16 18:112.5
Selenium ug/L ND 10.0 07/10/16 18:115.0
Silver ug/L ND 10.0 07/10/16 18:112.5
Thallium ug/L ND 5.5 07/10/16 18:115.0
Vanadium ug/L ND 25.0 07/10/16 18:112.5
Zinc ug/L ND 10.0 07/10/16 18:115.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774127LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 478500 96 80-120
Arsenic ug/L 450500 90 80-120
Barium ug/L 506500 101 80-120
Beryllium ug/L 511500 102 80-120
Cadmium ug/L 485500 97 80-120
Chromium ug/L 501500 100 80-120
Cobalt ug/L 473500 95 80-120
Copper ug/L 497500 99 80-120
Lead ug/L 471500 94 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 470500 94 80-120
Silver ug/L 247250 99 80-120
Thallium ug/L 475500 95 80-120
Vanadium ug/L 490500 98 80-120
Zinc ug/L 463500 93 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1774128MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930015
1774129
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12595 1 25500ND472477
Arsenic ug/L 500 90 75-12591 2 25500ND450458
Barium ug/L 500 102 75-125102 0 2550032.9J 542 544
Beryllium ug/L 500 103 75-125104 0 25500ND516518
Cadmium ug/L 500 96 75-12597 1 25500ND482487
Chromium ug/L 500 101 75-125102 1 25500ND504510
Cobalt ug/L 500 94 75-12595 1 2550032.2 503 506
Copper ug/L 500 99 75-125100 1 25500ND494499
Lead ug/L 500 93 75-12594 1 25500ND467470
Nickel ug/L 500 96 75-12597 1 25500ND481487
Selenium ug/L 500 93 75-12593 1 25500ND466469
Silver ug/L 250 98 75-12598 1 25250ND244246
Thallium ug/L 500 95 75-12596 1 25500ND476481
Vanadium ug/L 500 98 75-12599 1 25500ND490493
Zinc ug/L 500 92 75-12595 3 25500ND466479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320532
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92303930031, 92303930032, 92303930034, 92303930036, 92303930037, 92304098002, 92304098003,
92304098004, 92304098005, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1776172
Associated Lab Samples:92303930031, 92303930032, 92303930034, 92303930036, 92303930037, 92304098002, 92304098003,
92304098004, 92304098005, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 07/18/16 19:543.8
Arsenic ug/L ND 10.0 07/18/16 19:542.5
Barium ug/L ND 100 07/18/16 19:542.5
Beryllium ug/L ND 1.0 07/18/16 19:540.50
Cadmium ug/L ND 1.0 07/18/16 19:540.50
Chromium ug/L ND 10.0 07/18/16 19:542.5
Cobalt ug/L ND 10.0 07/18/16 19:542.5
Copper ug/L ND 10.0 07/18/16 19:542.5
Lead ug/L ND 10.0 07/18/16 19:542.5
Nickel ug/L ND 50.0 07/18/16 19:542.5
Selenium ug/L ND 10.0 07/18/16 19:545.0
Silver ug/L ND 10.0 07/18/16 19:542.5
Thallium ug/L ND 5.5 07/18/16 19:545.0
Tin ug/L ND 100 07/18/16 19:542.5
Vanadium ug/L ND 25.0 07/18/16 19:542.5
Zinc ug/L ND 10.0 07/18/16 19:545.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1776173LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 524500 105 80-120
Arsenic ug/L 499500 100 80-120
Barium ug/L 514500 103 80-120
Beryllium ug/L 507500 101 80-120
Cadmium ug/L 520500 104 80-120
Chromium ug/L 507500 101 80-120
Cobalt ug/L 516500 103 80-120
Copper ug/L 517500 103 80-120
Lead ug/L 510500 102 80-120
Nickel ug/L 519500 104 80-120
Selenium ug/L 507500 101 80-120
Silver ug/L 257250 103 80-120
Thallium ug/L 499500 100 80-120
Tin ug/L 525500 105 80-120
Vanadium ug/L 514500 103 80-120
Zinc ug/L 505500 101 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1776174MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098002
1776175
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 106 75-125105 0 25500ND531528
Arsenic ug/L 500 101 75-125101 0 25500ND506505
Barium ug/L 500 103 75-125102 1 255009.9J 527 522
Beryllium ug/L 500 103 75-125103 1 25500ND516513
Cadmium ug/L 500 105 75-125105 0 25500ND527526
Chromium ug/L 500 101 75-125101 0 25500ND508505
Cobalt ug/L 500 100 75-125100 0 25500ND500498
Copper ug/L 500 105 75-125104 1 25500ND525521
Lead ug/L 500 100 75-125100 1 25500ND500498
Nickel ug/L 500 101 75-125100 0 25500ND504503
Selenium ug/L 500 104 75-125103 0 25500ND520518
Silver ug/L 250 104 75-125103 1 25250ND260258
Thallium ug/L 500 96 75-12596 0 25500ND481480
Tin ug/L 500 104 75-125104 0 25500ND520519
Vanadium ug/L 500 104 75-125104 0 25500ND520519
Zinc ug/L 500 99 75-12599 0 25500ND498497
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320919
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92303930032, 92303930034, 92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1778357
Associated Lab Samples:92303930032, 92303930034, 92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Iron, Dissolved ug/L ND 50.0 07/14/16 10:3225.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1778358LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Dissolved ug/L 49505000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1778359MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098001
1778360
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron, Dissolved ug/L 5000 86 75-12586 0 205000180002230022300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320327
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92303930002, 92303930003, 92303930004, 92303930005, 92303930006, 92303930007, 92303930008,
92303930009, 92303930010, 92303930011, 92303930012, 92303930013, 92303930014, 92303930017,
92303930018, 92304098004, 92304098005, 92304098006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775014
Associated Lab Samples:92303930002, 92303930003, 92303930004, 92303930005, 92303930006, 92303930007, 92303930008,
92303930009, 92303930010, 92303930011, 92303930012, 92303930013, 92303930014, 92303930017,
92303930018, 92304098004, 92304098005, 92304098006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/07/16 22:490.33
1,1,1-Trichloroethane ug/L ND 1.0 07/07/16 22:490.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/07/16 22:490.40
1,1,2-Trichloroethane ug/L ND 1.0 07/07/16 22:490.29
1,1-Dichloroethane ug/L ND 5.0 07/07/16 22:490.32
1,1-Dichloroethene ug/L ND 5.0 07/07/16 22:490.56
1,1-Dichloropropene ug/L ND 5.0 07/07/16 22:490.49
1,2,3-Trichloropropane ug/L ND 1.0 07/07/16 22:490.41
1,2,4-Trichlorobenzene ug/L ND 10.0 07/07/16 22:490.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/07/16 22:492.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/07/16 22:490.27
1,2-Dichlorobenzene ug/L ND 5.0 07/07/16 22:490.30
1,2-Dichloroethane ug/L ND 1.0 07/07/16 22:490.24
1,2-Dichloropropane ug/L ND 1.0 07/07/16 22:490.27
1,3-Dichlorobenzene ug/L ND 5.0 07/07/16 22:490.24
1,3-Dichloropropane ug/L ND 1.0 07/07/16 22:490.28
1,4-Dichlorobenzene ug/L ND 1.0 07/07/16 22:490.33
2,2-Dichloropropane ug/L ND 15.0 07/07/16 22:490.13
2-Butanone (MEK)ug/L ND 100 07/07/16 22:490.96
2-Hexanone ug/L ND 50.0 07/07/16 22:490.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/07/16 22:490.33
Acetone ug/L ND 100 07/07/16 22:4910.0
Acetonitrile ug/L ND 55.0 07/07/16 22:492.2
Acrolein ug/L ND 53.0 07/07/16 22:491.6
Acrylonitrile ug/L ND 200 07/07/16 22:491.9
Allyl chloride ug/L ND 10.0 07/07/16 22:491.5
Benzene ug/L ND 1.0 07/07/16 22:490.25
Bromochloromethane ug/L ND 3.0 07/07/16 22:490.17
Bromodichloromethane ug/L ND 1.0 07/07/16 22:490.18
Bromoform ug/L ND 3.0 07/07/16 22:490.26
Bromomethane ug/L ND 10.0 07/07/16 22:490.29
Carbon disulfide ug/L ND 100 07/07/16 22:491.2
Carbon tetrachloride ug/L ND 1.0 07/07/16 22:490.25
Chlorobenzene ug/L ND 3.0 07/07/16 22:490.23
Chloroethane ug/L ND 10.0 07/07/16 22:490.54
Chloroform ug/L ND 5.0 07/07/16 22:490.14
Chloromethane ug/L ND 1.0 07/07/16 22:490.11
Chloroprene ug/L ND 20.0 07/07/16 22:490.27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775014
Associated Lab Samples:92303930002, 92303930003, 92303930004, 92303930005, 92303930006, 92303930007, 92303930008,
92303930009, 92303930010, 92303930011, 92303930012, 92303930013, 92303930014, 92303930017,
92303930018, 92304098004, 92304098005, 92304098006
Matrix:Water
AnalyzedMDL
cis-1,2-Dichloroethene ug/L ND 5.0 07/07/16 22:490.19
cis-1,3-Dichloropropene ug/L ND 1.0 07/07/16 22:490.13
Dibromochloromethane ug/L ND 3.0 07/07/16 22:490.21
Dibromomethane ug/L ND 10.0 07/07/16 22:490.21
Dichlorodifluoromethane ug/L ND 5.0 07/07/16 22:490.21
Ethyl methacrylate ug/L ND 10.0 07/07/16 22:490.20
Ethylbenzene ug/L ND 1.0 07/07/16 22:490.30
Hexachloro-1,3-butadiene ug/L ND 10.0 07/07/16 22:490.71
Iodomethane ug/L ND 10.0 07/07/16 22:490.32
Isobutanol ug/L ND 100 07/07/16 22:4935.0
Methacrylonitrile ug/L ND 100 07/07/16 22:490.93
Methyl methacrylate ug/L ND 30.0 07/07/16 22:492.0
Methylene Chloride ug/L ND 1.0 07/07/16 22:490.97
Naphthalene ug/L ND 10.0 07/07/16 22:490.24
Propionitrile ug/L ND 150 07/07/16 22:493.6
Styrene ug/L ND 1.0 07/07/16 22:490.26
Tetrachloroethene ug/L ND 1.0 07/07/16 22:490.46
Toluene ug/L ND 1.0 07/07/16 22:490.26
trans-1,2-Dichloroethene ug/L ND 5.0 07/07/16 22:490.49
trans-1,3-Dichloropropene ug/L ND 1.0 07/07/16 22:490.26
trans-1,4-Dichloro-2-butene ug/L ND 100 07/07/16 22:491.0
Trichloroethene ug/L ND 1.0 07/07/16 22:490.47
Trichlorofluoromethane ug/L ND 1.0 07/07/16 22:490.20
Vinyl acetate ug/L ND 50.0 07/07/16 22:490.35
Vinyl chloride ug/L ND 1.0 07/07/16 22:490.62
Xylene (Total)ug/L ND 5.0 07/07/16 22:490.66
1,2-Dichloroethane-d4 (S)%115 70-130 07/07/16 22:49
4-Bromofluorobenzene (S)%99 70-130 07/07/16 22:49
Toluene-d8 (S)%100 70-130 07/07/16 22:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775015LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.550 95 80-125
1,1,1-Trichloroethane ug/L 50.250 100 71-129
1,1,2,2-Tetrachloroethane ug/L 48.950 98 79-124
1,1,2-Trichloroethane ug/L 45.850 92 85-125
1,1-Dichloroethane ug/L 50.450 101 73-126
1,1-Dichloroethene ug/L 52.950 106 66-135
1,1-Dichloropropene ug/L 47.050 94 74-135
1,2,3-Trichloropropane ug/L 48.150 96 75-130
1,2,4-Trichlorobenzene ug/L 47.350 95 75-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775015LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 51.350 103 71-133
1,2-Dibromoethane (EDB)ug/L 52.350 105 83-124
1,2-Dichlorobenzene ug/L 51.850 104 80-133
1,2-Dichloroethane ug/L 48.650 97 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,3-Dichlorobenzene ug/L 51.550 103 77-130
1,3-Dichloropropane ug/L 47.350 95 76-131
1,4-Dichlorobenzene ug/L 49.650 99 78-130
2,2-Dichloropropane ug/L 47.050 94 40-160
2-Butanone (MEK)ug/L 98.0J100 98 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 103100 103 48-146
Acetonitrile ug/L 510500 102 62-150
Acrolein ug/L 330250 132 24-160
Acrylonitrile ug/L 246250 98 40-160
Allyl chloride ug/L 47.050 94 66-137
Benzene ug/L 51.150 102 80-125
Bromochloromethane ug/L 58.150 116 71-125
Bromodichloromethane ug/L 49.850 100 78-124
Bromoform ug/L 42.750 85 71-128
Bromomethane ug/L 43.350 87 40-160
Carbon disulfide ug/L 49.8J50 100 50-160
Carbon tetrachloride ug/L 50.250 100 69-131
Chlorobenzene ug/L 48.650 97 81-122
Chloroethane ug/L 49.550 99 39-148
Chloroform ug/L 51.050 102 73-127
Chloromethane ug/L 45.150 90 44-146
Chloroprene ug/L 46.850 94 75-145
cis-1,2-Dichloroethene ug/L 49.350 99 74-124
cis-1,3-Dichloropropene ug/L 50.050 100 72-132
Dibromochloromethane ug/L 44.650 89 78-125
Dibromomethane ug/L 47.750 95 82-120
Dichlorodifluoromethane ug/L 56.350 113 34-157
Ethyl methacrylate ug/L 47.050 94 82-121
Ethylbenzene ug/L 48.750 97 79-121
Hexachloro-1,3-butadiene ug/L 45.450 91 72-131
Iodomethane ug/L 81.3100 81 39-154
Isobutanol ug/L 8641000 86 34-160
Methacrylonitrile ug/L 475500 95 74-134
Methyl methacrylate ug/L 51.250 102 84-124
Methylene Chloride ug/L 54.350 109 64-133
Naphthalene ug/L 45.650 91 73-133
Propionitrile ug/L 518500 104 73-140
Styrene ug/L 50.150 100 84-126
Tetrachloroethene ug/L 44.150 88 78-122
Toluene ug/L 51.350 103 80-121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775015LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,2-Dichloroethene ug/L 51.450 103 71-127
trans-1,3-Dichloropropene ug/L 48.450 97 69-141
trans-1,4-Dichloro-2-butene ug/L 45.0J50 90 40-160
Trichloroethene ug/L 49.050 98 78-122
Trichlorofluoromethane ug/L 58.550 117 53-137
Vinyl acetate ug/L 92.6100 93 40-160
Vinyl chloride ug/L 47.950 96 58-137
Xylene (Total)ug/L 143150 96 81-126
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775017MATRIX SPIKE SAMPLE:
MSSpike
Result
92303930018
1,1,1,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,1-Trichloroethane ug/L 25.320 126 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.220 106 70-130ND
1,1,2-Trichloroethane ug/L 20.920 105 70-130ND
1,1-Dichloroethane ug/L 25.020 125 70-130ND
1,1-Dichloroethene ug/L 27.720 139 70-166ND
1,1-Dichloropropene ug/L 24.220 121 70-130ND
1,2,3-Trichloropropane ug/L 20.720 104 70-130ND
1,2,4-Trichlorobenzene ug/L 20.720 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.320 112 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.920 120 70-130ND
1,2-Dichlorobenzene ug/L 22.920 115 70-130ND
1,2-Dichloroethane ug/L 22.720 113 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,3-Dichlorobenzene ug/L 23.420 117 70-130ND
1,3-Dichloropropane ug/L 21.020 105 70-130ND
1,4-Dichlorobenzene ug/L 22.320 111 70-130ND
2,2-Dichloropropane ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 46.9J40 117 70-130ND
2-Hexanone ug/L 44.6J40 111 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.3J40 108 70-130ND
Acetone ug/L 50.7J40 121 70-130ND
Acetonitrile ug/L 22.2J M12001170-130ND
Acrolein ug/L 145 M110014570-130ND
Acrylonitrile ug/L 115J100 115 70-130ND
Allyl chloride ug/L 23.020 115 70-130ND
Benzene ug/L 23.820 119 70-148ND
Bromochloromethane ug/L 28.3 M12014170-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 18.320 92 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775017MATRIX SPIKE SAMPLE:
MSSpike
Result
92303930018
Bromomethane ug/L 9.1J M1204570-130ND
Carbon disulfide ug/L 25.2J20 126 70-130ND
Carbon tetrachloride ug/L 25.120 126 70-130ND
Chlorobenzene ug/L 23.420 117 70-146ND
Chloroethane ug/L 29.2 M12014670-130ND
Chloroform ug/L 24.520 123 70-130ND
Chloromethane ug/L 20.020 100 70-130ND
Chloroprene ug/L 23.520 118 70-130ND
cis-1,2-Dichloroethene ug/L 24.520 123 70-130ND
cis-1,3-Dichloropropene ug/L 21.720 109 70-130ND
Dibromochloromethane ug/L 20.520 102 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Dichlorodifluoromethane ug/L 31.0 M12015570-130ND
Ethyl methacrylate ug/L 20.520 103 70-130ND
Ethylbenzene ug/L 23.820 119 70-130ND
Hexachloro-1,3-butadiene ug/L 20.320 101 70-130ND
Iodomethane ug/L 32.240 80 70-130ND
Isobutanol ug/L 373400 93 70-130ND
Methacrylonitrile ug/L 219200 110 70-130ND
Methyl methacrylate ug/L 23.2J20 116 70-130ND
Methylene Chloride ug/L 22.120 110 70-130ND
Naphthalene ug/L 20.020 100 70-130ND
Propionitrile ug/L 230200 115 70-130ND
Styrene ug/L 23.320 117 70-130ND
Tetrachloroethene ug/L 21.820 109 70-130ND
Toluene ug/L 23.920 120 70-155ND
trans-1,2-Dichloroethene ug/L 23.720 119 70-130ND
trans-1,3-Dichloropropene ug/L 20.820 104 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.6J20 78 70-130ND
Trichloroethene ug/L 22.920 115 69-151ND
Trichlorofluoromethane ug/L 29.3 M12014670-130ND
Vinyl acetate ug/L 36.3J40 91 70-130ND
Vinyl chloride ug/L 24.320 121 70-130ND
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930017
1775016SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.38J 300.33J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930017
1775016SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 300.24J
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.35J 300.40J
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 1.4J 5 301.4J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930017
1775016SAMPLE DUPLICATE:
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%110 1109
4-Bromofluorobenzene (S)%98 098
Toluene-d8 (S)%102 1101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320331
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92303930015, 92303930016, 92304098002, 92304098003, 92304098007, 92304098008, 92304098009,
92304098010, 92304098011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775096
Associated Lab Samples:92303930015, 92303930016, 92304098002, 92304098003, 92304098007, 92304098008, 92304098009,
92304098010, 92304098011
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/07/16 22:310.33
1,1,1-Trichloroethane ug/L ND 1.0 07/07/16 22:310.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/07/16 22:310.40
1,1,2-Trichloroethane ug/L ND 1.0 07/07/16 22:310.29
1,1-Dichloroethane ug/L ND 5.0 07/07/16 22:310.32
1,1-Dichloroethene ug/L ND 5.0 07/07/16 22:310.56
1,1-Dichloropropene ug/L ND 5.0 07/07/16 22:310.49
1,2,3-Trichloropropane ug/L ND 1.0 07/07/16 22:310.41
1,2,4-Trichlorobenzene ug/L ND 10.0 07/07/16 22:310.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/07/16 22:312.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/07/16 22:310.27
1,2-Dichlorobenzene ug/L ND 5.0 07/07/16 22:310.30
1,2-Dichloroethane ug/L ND 1.0 07/07/16 22:310.24
1,2-Dichloropropane ug/L ND 1.0 07/07/16 22:310.27
1,3-Dichlorobenzene ug/L ND 5.0 07/07/16 22:310.24
1,3-Dichloropropane ug/L ND 1.0 07/07/16 22:310.28
1,4-Dichlorobenzene ug/L ND 1.0 07/07/16 22:310.33
2,2-Dichloropropane ug/L ND 15.0 07/07/16 22:310.13
2-Butanone (MEK)ug/L ND 100 07/07/16 22:310.96
2-Hexanone ug/L ND 50.0 07/07/16 22:310.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/07/16 22:310.33
Acetone ug/L ND 100 07/07/16 22:3110.0
Acetonitrile ug/L ND 55.0 07/07/16 22:312.2
Acrolein ug/L ND 53.0 07/07/16 22:311.6
Acrylonitrile ug/L ND 200 07/07/16 22:311.9
Allyl chloride ug/L ND 10.0 07/07/16 22:311.5
Benzene ug/L ND 1.0 07/07/16 22:310.25
Bromochloromethane ug/L ND 3.0 07/07/16 22:310.17
Bromodichloromethane ug/L ND 1.0 07/07/16 22:310.18
Bromoform ug/L ND 3.0 07/07/16 22:310.26
Bromomethane ug/L ND 10.0 07/07/16 22:310.29
Carbon disulfide ug/L ND 100 07/07/16 22:311.2
Carbon tetrachloride ug/L ND 1.0 07/07/16 22:310.25
Chlorobenzene ug/L ND 3.0 07/07/16 22:310.23
Chloroethane ug/L ND 10.0 07/07/16 22:310.54
Chloroform ug/L ND 5.0 07/07/16 22:310.14
Chloromethane ug/L ND 1.0 07/07/16 22:310.11
Chloroprene ug/L ND 20.0 07/07/16 22:310.27
cis-1,2-Dichloroethene ug/L ND 5.0 07/07/16 22:310.19
cis-1,3-Dichloropropene ug/L ND 1.0 07/07/16 22:310.13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775096
Associated Lab Samples:92303930015, 92303930016, 92304098002, 92304098003, 92304098007, 92304098008, 92304098009,
92304098010, 92304098011
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 3.0 07/07/16 22:310.21
Dibromomethane ug/L ND 10.0 07/07/16 22:310.21
Dichlorodifluoromethane ug/L ND 5.0 07/07/16 22:310.21
Ethyl methacrylate ug/L ND 10.0 07/07/16 22:310.20
Ethylbenzene ug/L ND 1.0 07/07/16 22:310.30
Hexachloro-1,3-butadiene ug/L 0.84J 10.0 07/07/16 22:310.71
Iodomethane ug/L ND 10.0 07/07/16 22:310.32
Isobutanol ug/L ND 100 07/07/16 22:3135.0
Methacrylonitrile ug/L ND 100 07/07/16 22:310.93
Methyl methacrylate ug/L ND 30.0 07/07/16 22:312.0
Methylene Chloride ug/L ND 1.0 07/07/16 22:310.97
Naphthalene ug/L ND 10.0 07/07/16 22:310.24
Propionitrile ug/L ND 150 07/07/16 22:313.6
Styrene ug/L ND 1.0 07/07/16 22:310.26
Tetrachloroethene ug/L ND 1.0 07/07/16 22:310.46
Toluene ug/L ND 1.0 07/07/16 22:310.26
trans-1,2-Dichloroethene ug/L ND 5.0 07/07/16 22:310.49
trans-1,3-Dichloropropene ug/L ND 1.0 07/07/16 22:310.26
trans-1,4-Dichloro-2-butene ug/L ND 100 07/07/16 22:311.0
Trichloroethene ug/L ND 1.0 07/07/16 22:310.47
Trichlorofluoromethane ug/L ND 1.0 07/07/16 22:310.20
Vinyl acetate ug/L ND 50.0 07/07/16 22:310.35
Vinyl chloride ug/L ND 1.0 07/07/16 22:310.62
Xylene (Total)ug/L ND 5.0 07/07/16 22:310.66
1,2-Dichloroethane-d4 (S)%108 70-130 07/07/16 22:31
4-Bromofluorobenzene (S)%98 70-130 07/07/16 22:31
Toluene-d8 (S)%100 70-130 07/07/16 22:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775097LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.750 97 80-125
1,1,1-Trichloroethane ug/L 51.550 103 71-129
1,1,2,2-Tetrachloroethane ug/L 51.250 102 79-124
1,1,2-Trichloroethane ug/L 47.050 94 85-125
1,1-Dichloroethane ug/L 52.250 104 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,1-Dichloropropene ug/L 50.750 101 74-135
1,2,3-Trichloropropane ug/L 49.950 100 75-130
1,2,4-Trichlorobenzene ug/L 50.550 101 75-134
1,2-Dibromo-3-chloropropane ug/L 53.350 107 71-133
1,2-Dibromoethane (EDB)ug/L 52.750 105 83-124
1,2-Dichlorobenzene ug/L 55.150 110 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775097LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 50.550 101 67-128
1,2-Dichloropropane ug/L 49.550 99 75-132
1,3-Dichlorobenzene ug/L 53.850 108 77-130
1,3-Dichloropropane ug/L 48.650 97 76-131
1,4-Dichlorobenzene ug/L 52.250 104 78-130
2,2-Dichloropropane ug/L 50.650 101 40-160
2-Butanone (MEK)ug/L 96.6J100 97 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 104100 104 72-135
Acetone ug/L 110100 110 48-146
Acetonitrile ug/L 519500 104 62-150
Acrolein ug/L 338250 135 24-160
Acrylonitrile ug/L 247250 99 40-160
Allyl chloride ug/L 53.250 106 66-137
Benzene ug/L 53.850 108 80-125
Bromochloromethane ug/L 59.750 119 71-125
Bromodichloromethane ug/L 51.950 104 78-124
Bromoform ug/L 44.050 88 71-128
Bromomethane ug/L 45.850 92 40-160
Carbon disulfide ug/L 52.8J50 106 50-160
Carbon tetrachloride ug/L 53.250 106 69-131
Chlorobenzene ug/L 52.250 104 81-122
Chloroethane ug/L 58.350 117 39-148
Chloroform ug/L 53.550 107 73-127
Chloromethane ug/L 48.350 97 44-146
Chloroprene ug/L 48.650 97 75-145
cis-1,2-Dichloroethene ug/L 52.150 104 74-124
cis-1,3-Dichloropropene ug/L 51.150 102 72-132
Dibromochloromethane ug/L 46.650 93 78-125
Dibromomethane ug/L 49.750 99 82-120
Dichlorodifluoromethane ug/L 58.050 116 34-157
Ethyl methacrylate ug/L 49.550 99 82-121
Ethylbenzene ug/L 52.450 105 79-121
Hexachloro-1,3-butadiene ug/L 48.650 97 72-131
Iodomethane ug/L 91.4100 91 39-154
Isobutanol ug/L 8971000 90 34-160
Methacrylonitrile ug/L 495500 99 74-134
Methyl methacrylate ug/L 53.050 106 84-124
Methylene Chloride ug/L 57.150 114 64-133
Naphthalene ug/L 47.750 95 73-133
Propionitrile ug/L 520500 104 73-140
Styrene ug/L 52.250 104 84-126
Tetrachloroethene ug/L 45.550 91 78-122
Toluene ug/L 53.850 108 80-121
trans-1,2-Dichloroethene ug/L 53.750 107 71-127
trans-1,3-Dichloropropene ug/L 50.350 101 69-141
trans-1,4-Dichloro-2-butene ug/L 44.0J50 88 40-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775097LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 51.450 103 78-122
Trichlorofluoromethane ug/L 62.550 125 53-137
Vinyl acetate ug/L 96.4100 96 40-160
Vinyl chloride ug/L 50.550 101 58-137
Xylene (Total)ug/L 152150 101 81-126
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775099MATRIX SPIKE SAMPLE:
MSSpike
Result
92304098011
1,1,1,2-Tetrachloroethane ug/L 21.620 108 70-130ND
1,1,1-Trichloroethane ug/L 25.320 127 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.220 106 70-130ND
1,1,2-Trichloroethane ug/L 20.920 104 70-130ND
1,1-Dichloroethane ug/L 25.720 124 70-1300.92J
1,1-Dichloroethene ug/L 27.920 140 70-166ND
1,1-Dichloropropene ug/L 23.920 119 70-130ND
1,2,3-Trichloropropane ug/L 20.820 104 70-130ND
1,2,4-Trichlorobenzene ug/L 20.920 102 70-1300.45J
1,2-Dibromo-3-chloropropane ug/L 22.320 112 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.120 116 70-130ND
1,2-Dichlorobenzene ug/L 23.320 117 70-130ND
1,2-Dichloroethane ug/L 23.520 116 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,3-Dichlorobenzene ug/L 23.020 115 70-130ND
1,3-Dichloropropane ug/L 22.220 111 70-130ND
1,4-Dichlorobenzene ug/L 25.720 110 70-1303.7
2,2-Dichloropropane ug/L 22.020 110 70-130ND
2-Butanone (MEK)ug/L 46.7J40 117 70-130ND
2-Hexanone ug/L 43.5J40 109 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.7J40 109 70-130ND
Acetone ug/L 49.3J40 114 70-130ND
Acetonitrile ug/L 29.0J M12001570-130ND
Acrolein ug/L 137 M110013770-130ND
Acrylonitrile ug/L 110J100 110 70-130ND
Allyl chloride ug/L 21.520 108 70-130ND
Benzene ug/L 25.120 120 70-1481.1
Bromochloromethane ug/L 27.0 M12013570-130ND
Bromodichloromethane ug/L 23.520 118 70-130ND
Bromoform ug/L 17.920 90 70-130ND
Bromomethane ug/L 5.9J M1202970-130ND
Carbon disulfide ug/L 25.7J20 129 70-130ND
Carbon tetrachloride ug/L 24.320 122 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775099MATRIX SPIKE SAMPLE:
MSSpike
Result
92304098011
Chlorobenzene ug/L 24.320 115 70-1461.3J
Chloroethane ug/L 28.6 M12014370-130ND
Chloroform ug/L 24.720 124 70-130ND
Chloromethane ug/L 17.420 87 70-130ND
Chloroprene ug/L 22.520 112 70-130ND
cis-1,2-Dichloroethene ug/L 31.120 118 70-1307.4
cis-1,3-Dichloropropene ug/L 22.020 110 70-130ND
Dibromochloromethane ug/L 20.520 102 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Dichlorodifluoromethane ug/L 30.0 M12015070-130ND
Ethyl methacrylate ug/L 19.720 98 70-130ND
Ethylbenzene ug/L 23.420 117 70-130ND
Hexachloro-1,3-butadiene ug/L 19.120 95 70-130ND
Iodomethane ug/L 23.4 M1405970-130ND
Isobutanol ug/L 338400 85 70-130ND
Methacrylonitrile ug/L 220200 110 70-130ND
Methyl methacrylate ug/L 21.5J20 108 70-130ND
Methylene Chloride ug/L 21.720 108 70-130ND
Naphthalene ug/L 20.320 102 70-130ND
Propionitrile ug/L 219200 109 70-130ND
Styrene ug/L 22.720 113 70-130ND
Tetrachloroethene ug/L 20.520 102 70-130ND
Toluene ug/L 23.720 118 70-155ND
trans-1,2-Dichloroethene ug/L 23.620 118 70-130ND
trans-1,3-Dichloropropene ug/L 21.520 107 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.3J20 72 70-130ND
Trichloroethene ug/L 23.520 112 69-1511.1
Trichlorofluoromethane ug/L 31.6 M12015870-130ND
Vinyl acetate ug/L 37.1J40 93 70-130ND
Vinyl chloride ug/L 24.520 122 70-130ND
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304098010
1775098SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 4.1J 1 304.1J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304098010
1775098SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.25J 300.26J
1,2-Dichloropropane ug/L 0.39J 300.43J
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 2.6 8 302.8
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L 3.2 6 303.3
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.86J 300.92J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 15.6 4 3016.2
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304098010
1775098SAMPLE DUPLICATE:
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 0.65J 300.55J
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%111 2109
4-Bromofluorobenzene (S)%93 194
Toluene-d8 (S)%101 2103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321048
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92303930031, 92303930032, 92303930034, 92303930036, 92303930037
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779147
Associated Lab Samples:92303930031, 92303930032, 92303930034, 92303930036, 92303930037
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/14/16 02:320.33
1,1,1-Trichloroethane ug/L ND 1.0 07/14/16 02:320.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/14/16 02:320.40
1,1,2-Trichloroethane ug/L ND 1.0 07/14/16 02:320.29
1,1-Dichloroethane ug/L ND 5.0 07/14/16 02:320.32
1,1-Dichloroethene ug/L ND 5.0 07/14/16 02:320.56
1,1-Dichloropropene ug/L ND 5.0 07/14/16 02:320.49
1,2,3-Trichloropropane ug/L ND 1.0 07/14/16 02:320.41
1,2,4-Trichlorobenzene ug/L ND 10.0 07/14/16 02:320.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/14/16 02:322.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/14/16 02:320.27
1,2-Dichlorobenzene ug/L ND 5.0 07/14/16 02:320.30
1,2-Dichloroethane ug/L ND 1.0 07/14/16 02:320.24
1,2-Dichloropropane ug/L ND 1.0 07/14/16 02:320.27
1,3-Dichlorobenzene ug/L ND 5.0 07/14/16 02:320.24
1,3-Dichloropropane ug/L ND 1.0 07/14/16 02:320.28
1,4-Dichlorobenzene ug/L ND 1.0 07/14/16 02:320.33
2,2-Dichloropropane ug/L ND 15.0 07/14/16 02:320.13
2-Butanone (MEK)ug/L ND 100 07/14/16 02:320.96
2-Hexanone ug/L ND 50.0 07/14/16 02:320.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/14/16 02:320.33
Acetone ug/L ND 100 07/14/16 02:3210.0
Acetonitrile ug/L ND 55.0 07/14/16 02:322.2
Acrolein ug/L ND 53.0 07/14/16 02:321.6
Acrylonitrile ug/L ND 200 07/14/16 02:321.9
Allyl chloride ug/L ND 10.0 07/14/16 02:321.5
Benzene ug/L ND 1.0 07/14/16 02:320.25
Bromochloromethane ug/L ND 3.0 07/14/16 02:320.17
Bromodichloromethane ug/L ND 1.0 07/14/16 02:320.18
Bromoform ug/L ND 3.0 07/14/16 02:320.26
Bromomethane ug/L ND 10.0 07/14/16 02:320.29
Carbon disulfide ug/L ND 100 07/14/16 02:321.2
Carbon tetrachloride ug/L ND 1.0 07/14/16 02:320.25
Chlorobenzene ug/L ND 3.0 07/14/16 02:320.23
Chloroethane ug/L ND 10.0 07/14/16 02:320.54
Chloroform ug/L ND 5.0 07/14/16 02:320.14
Chloromethane ug/L ND 1.0 07/14/16 02:320.11
Chloroprene ug/L ND 20.0 07/14/16 02:320.27
cis-1,2-Dichloroethene ug/L ND 5.0 07/14/16 02:320.19
cis-1,3-Dichloropropene ug/L ND 1.0 07/14/16 02:320.13
Dibromochloromethane ug/L ND 3.0 07/14/16 02:320.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779147
Associated Lab Samples:92303930031, 92303930032, 92303930034, 92303930036, 92303930037
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 07/14/16 02:320.21
Dichlorodifluoromethane ug/L ND 5.0 07/14/16 02:320.21
Ethyl methacrylate ug/L ND 10.0 07/14/16 02:320.20
Ethylbenzene ug/L ND 1.0 07/14/16 02:320.30
Hexachloro-1,3-butadiene ug/L ND 10.0 07/14/16 02:320.71
Iodomethane ug/L ND 10.0 07/14/16 02:320.32
Isobutanol ug/L ND 100 07/14/16 02:3235.0
Methacrylonitrile ug/L ND 100 07/14/16 02:320.93
Methyl methacrylate ug/L ND 30.0 07/14/16 02:322.0
Methylene Chloride ug/L ND 1.0 07/14/16 02:320.97
Naphthalene ug/L ND 10.0 07/14/16 02:320.24
Propionitrile ug/L ND 150 07/14/16 02:323.6
Styrene ug/L ND 1.0 07/14/16 02:320.26
Tetrachloroethene ug/L ND 1.0 07/14/16 02:320.46
Toluene ug/L ND 1.0 07/14/16 02:320.26
trans-1,2-Dichloroethene ug/L ND 5.0 07/14/16 02:320.49
trans-1,3-Dichloropropene ug/L ND 1.0 07/14/16 02:320.26
trans-1,4-Dichloro-2-butene ug/L ND 100 07/14/16 02:321.0
Trichloroethene ug/L ND 1.0 07/14/16 02:320.47
Trichlorofluoromethane ug/L ND 1.0 07/14/16 02:320.20
Vinyl acetate ug/L ND 50.0 07/14/16 02:320.35
Vinyl chloride ug/L ND 1.0 07/14/16 02:320.62
Xylene (Total)ug/L ND 5.0 07/14/16 02:320.66
1,2-Dichloroethane-d4 (S)%101 70-130 07/14/16 02:32
4-Bromofluorobenzene (S)%99 70-130 07/14/16 02:32
Toluene-d8 (S)%100 70-130 07/14/16 02:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779148LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.450 97 80-125
1,1,1-Trichloroethane ug/L 48.150 96 71-129
1,1,2,2-Tetrachloroethane ug/L 46.550 93 79-124
1,1,2-Trichloroethane ug/L 46.550 93 85-125
1,1-Dichloroethane ug/L 46.850 94 73-126
1,1-Dichloroethene ug/L 48.550 97 66-135
1,1-Dichloropropene ug/L 45.450 91 74-135
1,2,3-Trichloropropane ug/L 45.950 92 75-130
1,2,4-Trichlorobenzene ug/L 49.950 100 75-134
1,2-Dibromo-3-chloropropane ug/L 51.550 103 71-133
1,2-Dibromoethane (EDB)ug/L 50.450 101 83-124
1,2-Dichlorobenzene ug/L 50.850 102 80-133
1,2-Dichloroethane ug/L 46.150 92 67-128
1,2-Dichloropropane ug/L 45.750 91 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779148LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.250 96 77-130
1,3-Dichloropropane ug/L 45.750 91 76-131
1,4-Dichlorobenzene ug/L 48.450 97 78-130
2,2-Dichloropropane ug/L 43.450 87 40-160
2-Butanone (MEK)ug/L 95.1J100 95 61-144
2-Hexanone ug/L 98.3100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 96.7J100 97 72-135
Acetone ug/L 96.9J100 97 48-146
Acetonitrile ug/L 479500 96 62-150
Acrolein ug/L 409 L025016424-160
Acrylonitrile ug/L 250250 100 40-160
Allyl chloride ug/L 47.650 95 66-137
Benzene ug/L 47.550 95 80-125
Bromochloromethane ug/L 49.150 98 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 42.650 85 71-128
Bromomethane ug/L 52.650 105 40-160
Carbon disulfide ug/L 52.8J50 106 50-160
Carbon tetrachloride ug/L 48.850 98 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 49.650 99 39-148
Chloroform ug/L 46.850 94 73-127
Chloromethane ug/L 53.950 108 44-146
Chloroprene ug/L 48.150 96 75-145
cis-1,2-Dichloroethene ug/L 47.750 95 74-124
cis-1,3-Dichloropropene ug/L 46.750 93 72-132
Dibromochloromethane ug/L 48.350 97 78-125
Dibromomethane ug/L 48.450 97 82-120
Dichlorodifluoromethane ug/L 52.650 105 34-157
Ethyl methacrylate ug/L 47.850 96 82-121
Ethylbenzene ug/L 47.450 95 79-121
Hexachloro-1,3-butadiene ug/L 48.950 98 72-131
Iodomethane ug/L 106100 106 39-154
Isobutanol ug/L 10201000 102 34-160
Methacrylonitrile ug/L 477500 95 74-134
Methyl methacrylate ug/L 49.150 98 84-124
Methylene Chloride ug/L 46.850 94 64-133
Naphthalene ug/L 46.450 93 73-133
Propionitrile ug/L 497500 99 73-140
Styrene ug/L 50.150 100 84-126
Tetrachloroethene ug/L 44.050 88 78-122
Toluene ug/L 47.750 95 80-121
trans-1,2-Dichloroethene ug/L 48.450 97 71-127
trans-1,3-Dichloropropene ug/L 46.250 92 69-141
trans-1,4-Dichloro-2-butene ug/L 60.4J50 121 40-160
Trichloroethene ug/L 46.550 93 78-122
Trichlorofluoromethane ug/L 52.250 104 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779148LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 89.1100 89 40-160
Vinyl chloride ug/L 49.650 99 58-137
Xylene (Total)ug/L 140150 93 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1779149MATRIX SPIKE SAMPLE:
MSSpike
Result
92304768001
1,1,1,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,1-Trichloroethane ug/L 21.020 105 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.120 96 70-130ND
1,1,2-Trichloroethane ug/L 19.320 97 70-130ND
1,1-Dichloroethane ug/L 20.520 103 70-130ND
1,1-Dichloroethene ug/L 21.520 107 70-166ND
1,1-Dichloropropene ug/L 20.220 101 70-130ND
1,2,3-Trichloropropane ug/L 19.020 95 70-130ND
1,2,4-Trichlorobenzene ug/L 20.420 102 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 100 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.020 105 70-130ND
1,2-Dichlorobenzene ug/L 20.820 104 70-130ND
1,2-Dichloroethane ug/L 19.420 97 70-130ND
1,2-Dichloropropane ug/L 19.520 98 70-130ND
1,3-Dichlorobenzene ug/L 20.520 103 70-130ND
1,3-Dichloropropane ug/L 19.220 96 70-130ND
1,4-Dichlorobenzene ug/L 20.120 100 70-130ND
2,2-Dichloropropane ug/L 17.220 86 70-130ND
2-Butanone (MEK)ug/L 38.0J40 95 70-130ND
2-Hexanone ug/L 38.9J40 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 38.9J40 97 70-130ND
Acetone ug/L 40.2J40 101 70-130ND
Acetonitrile ug/L 198200 99 70-130ND
Acrolein ug/L 148 M010014870-130ND
Acrylonitrile ug/L 102J100 102 70-130ND
Allyl chloride ug/L 19.320 97 70-130ND
Benzene ug/L 20.220 101 70-148ND
Bromochloromethane ug/L 21.020 105 70-130ND
Bromodichloromethane ug/L 20.120 100 70-130ND
Bromoform ug/L 17.720 89 70-130ND
Bromomethane ug/L 19.520 98 70-130ND
Carbon disulfide ug/L 18.5J20 93 70-130ND
Carbon tetrachloride ug/L 21.820 109 70-130ND
Chlorobenzene ug/L 21.020 105 70-146ND
Chloroethane ug/L 22.720 113 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1779149MATRIX SPIKE SAMPLE:
MSSpike
Result
92304768001
Chloroform ug/L 20.120 101 70-130ND
Chloromethane ug/L 22.920 114 70-130ND
Chloroprene ug/L 20.520 103 70-130ND
cis-1,2-Dichloroethene ug/L 20.620 103 70-130ND
cis-1,3-Dichloropropene ug/L 18.820 94 70-130ND
Dibromochloromethane ug/L 20.120 100 70-130ND
Dibromomethane ug/L 19.920 99 70-130ND
Dichlorodifluoromethane ug/L 22.320 112 70-130ND
Ethyl methacrylate ug/L 19.920 99 70-130ND
Ethylbenzene ug/L 20.620 103 70-130ND
Hexachloro-1,3-butadiene ug/L 19.820 99 70-130ND
Iodomethane ug/L 29.240 73 70-130ND
Isobutanol ug/L 381400 95 70-130ND
Methacrylonitrile ug/L 196200 98 70-130ND
Methyl methacrylate ug/L 19.8J20 99 70-130ND
Methylene Chloride ug/L 19.320 96 70-130ND
Naphthalene ug/L 18.420 92 70-130ND
Propionitrile ug/L 191200 96 70-130ND
Styrene ug/L 20.920 104 70-130ND
Tetrachloroethene ug/L 18.920 95 70-130ND
Toluene ug/L 20.520 102 70-155ND
trans-1,2-Dichloroethene ug/L 21.320 107 70-130ND
trans-1,3-Dichloropropene ug/L 18.320 92 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.3J20 87 70-130ND
Trichloroethene ug/L 19.920 100 69-151ND
Trichlorofluoromethane ug/L 24.520 122 70-130ND
Vinyl acetate ug/L 29.3J40 73 70-130ND
Vinyl chloride ug/L 22.720 113 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304768002
1779150SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304768002
1779150SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304768002
1779150SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%102 0102
4-Bromofluorobenzene (S)%97 2100
Toluene-d8 (S)%100 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320316
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92304098007, 92304098008, 92304098009, 92304098010, 92304098011, 92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1774965
Associated Lab Samples:92304098007, 92304098008, 92304098009, 92304098010, 92304098011, 92304098012
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 07/09/16 17:320.050
4,4'-DDE ug/L ND 0.10 07/09/16 17:320.050
4,4'-DDT ug/L ND 0.10 07/09/16 17:320.050
Aldrin ug/L ND 0.050 07/09/16 17:320.050
alpha-BHC ug/L ND 0.050 07/09/16 17:320.050
beta-BHC ug/L ND 0.050 07/09/16 17:320.050
Chlordane (Technical)ug/L ND 0.50 07/09/16 17:320.20
delta-BHC ug/L ND 0.050 07/09/16 17:320.050
Dieldrin ug/L ND 0.075 07/09/16 17:320.050
Endosulfan I ug/L ND 0.10 07/09/16 17:320.050
Endosulfan II ug/L ND 0.10 07/09/16 17:320.050
Endosulfan sulfate ug/L ND 0.10 07/09/16 17:320.050
Endrin ug/L ND 0.10 07/09/16 17:320.050
Endrin aldehyde ug/L ND 0.10 07/09/16 17:320.050
gamma-BHC (Lindane)ug/L ND 0.050 07/09/16 17:320.050
Heptachlor ug/L ND 0.050 07/09/16 17:320.050
Heptachlor epoxide ug/L ND 0.075 07/09/16 17:320.050
Methoxychlor ug/L ND 1.0 07/09/16 17:320.15
Toxaphene ug/L ND 1.5 07/09/16 17:320.20
Decachlorobiphenyl (S)%59 20-130 07/09/16 17:32
Tetrachloro-m-xylene (S)%79 20-130 07/09/16 17:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774966LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1774967
4,4'-DDD ug/L 0.24.25 96 20-150910.22 6 30
4,4'-DDE ug/L 0.25.25 101 20-150950.23 6 30
4,4'-DDT ug/L 0.26.25 105 20-150980.24 7 30
Aldrin ug/L 0.20.25 80 20-150770.19 4 30
alpha-BHC ug/L 0.20.25 82 20-150810.20 2 30
beta-BHC ug/L 0.24.25 97 20-150930.23 3 30
delta-BHC ug/L 0.33.25 134 20-1501050.26 24 30
Dieldrin ug/L 0.23.25 92 20-150880.22 5 30
Endosulfan I ug/L 0.26.25 105 20-1501000.25 4 30
Endosulfan II ug/L 0.25.25 103 20-150980.24 5 30
Endosulfan sulfate ug/L 0.26.25 105 20-150990.25 5 30
Endrin ug/L 0.27.25 107 20-1501020.25 5 30
Endrin aldehyde ug/L 0.22.25 90 20-150880.22 2 30
gamma-BHC (Lindane)ug/L 0.22.25 88 20-150870.21 2 30
Heptachlor ug/L 0.21.25 86 20-150840.21 2 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774966LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1774967
Heptachlor epoxide ug/L 0.23.25 94 20-150910.22 3 30
Methoxychlor ug/L 0.85J.74 115 20-1501080.81J 6 30
Decachlorobiphenyl (S)%71 20-13064
Tetrachloro-m-xylene (S)%80 20-13077
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320774
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92303930036, 92303930037
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1777288
Associated Lab Samples:92303930036, 92303930037
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 07/12/16 20:390.050
4,4'-DDE ug/L ND 0.10 07/12/16 20:390.050
4,4'-DDT ug/L ND 0.10 07/12/16 20:390.050
Aldrin ug/L ND 0.050 07/12/16 20:390.050
alpha-BHC ug/L ND 0.050 07/12/16 20:390.050
beta-BHC ug/L ND 0.050 07/12/16 20:390.050
Chlordane (Technical)ug/L ND 0.50 07/12/16 20:390.20
delta-BHC ug/L ND 0.050 07/12/16 20:390.050
Dieldrin ug/L ND 0.075 07/12/16 20:390.050
Endosulfan I ug/L ND 0.10 07/12/16 20:390.050
Endosulfan II ug/L ND 0.10 07/12/16 20:390.050
Endosulfan sulfate ug/L ND 0.10 07/12/16 20:390.050
Endrin ug/L ND 0.10 07/12/16 20:390.050
Endrin aldehyde ug/L ND 0.10 07/12/16 20:390.050
gamma-BHC (Lindane)ug/L ND 0.050 07/12/16 20:390.050
Heptachlor ug/L ND 0.050 07/12/16 20:390.050
Heptachlor epoxide ug/L ND 0.075 07/12/16 20:390.050
Methoxychlor ug/L ND 1.0 07/12/16 20:390.15
Toxaphene ug/L ND 1.5 07/12/16 20:390.20
Decachlorobiphenyl (S)%108 20-130 07/12/16 20:39
Tetrachloro-m-xylene (S)%105 20-130 07/12/16 20:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1777289LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.27.25 109 20-150
4,4'-DDE ug/L 0.25.25 102 20-150
4,4'-DDT ug/L 0.29.25 115 20-150
Aldrin ug/L 0.21.25 85 20-150
alpha-BHC ug/L 0.23.25 94 20-150
beta-BHC ug/L 0.25.25 103 20-150
delta-BHC ug/L 0.27.25 109 20-150
Dieldrin ug/L 0.25.25 102 20-150
Endosulfan I ug/L 0.26.25 105 20-150
Endosulfan II ug/L 0.28.25 113 20-150
Endosulfan sulfate ug/L 0.29.25 117 20-150
Endrin ug/L 0.28.25 112 20-150
Endrin aldehyde ug/L 0.25.25 103 20-150
gamma-BHC (Lindane)ug/L 0.24.25 98 20-150
Heptachlor ug/L 0.23.25 95 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1777289LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.26.25 104 20-150
Methoxychlor ug/L 0.95J.74 128 20-150
Decachlorobiphenyl (S)%92 20-130
Tetrachloro-m-xylene (S)%103 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1777290MATRIX SPIKE SAMPLE:
MSSpike
Result
92304445002
4,4'-DDD ug/L 0.26.25 104 20-150ND
4,4'-DDE ug/L 0.24.25 96 20-150ND
4,4'-DDT ug/L 0.26.25 105 20-150ND
Aldrin ug/L 0.21.25 84 20-150ND
alpha-BHC ug/L 0.22.25 89 20-150ND
beta-BHC ug/L 0.24.25 98 20-150ND
delta-BHC ug/L 0.26.25 104 20-150ND
Dieldrin ug/L 0.37.25 96 20-1500.13
Endosulfan I ug/L 0.25.25 103 20-150ND
Endosulfan II ug/L 0.27.25 108 20-150ND
Endosulfan sulfate ug/L 0.27.25 110 20-150ND
Endrin ug/L 0.27.25 109 20-150ND
Endrin aldehyde ug/L 0.24.25 98 20-150ND
gamma-BHC (Lindane)ug/L 0.23.25 92 20-150ND
Heptachlor ug/L 0.23.25 93 20-150ND
Heptachlor epoxide ug/L 0.25.25 100 20-150ND
Methoxychlor ug/L 0.87J.74 117 20-150ND
Decachlorobiphenyl (S)%95 20-130
Tetrachloro-m-xylene (S)%97 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304445012
1777291SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304445012
1777291SAMPLE DUPLICATE:
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%97 5102
Tetrachloro-m-xylene (S)%103 1104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320263
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92304098007, 92304098008, 92304098009, 92304098010, 92304098011, 92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1774649
Associated Lab Samples:92304098007, 92304098008, 92304098009, 92304098010, 92304098011, 92304098012
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 07/08/16 13:310.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 07/08/16 13:310.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 07/08/16 13:310.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 07/08/16 13:310.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 07/08/16 13:310.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 07/08/16 13:310.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 07/08/16 13:310.50
Decachlorobiphenyl (S)%60 10-132 07/08/16 13:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774650LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 3.35 66 50-150
PCB-1260 (Aroclor 1260)ug/L 4.15 82 50-150
Decachlorobiphenyl (S)%66 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1774652MATRIX SPIKE SAMPLE:
MSSpike
Result
92304098007
PCB-1016 (Aroclor 1016)ug/L 4.25 84 50-150ND
PCB-1260 (Aroclor 1260)ug/L 4.45 87 50-150ND
Decachlorobiphenyl (S)%76 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304098012
1774653SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%47 1454
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320469
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92303930036, 92303930037
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775709
Associated Lab Samples:92303930036, 92303930037
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 07/09/16 19:120.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 07/09/16 19:120.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 07/09/16 19:120.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 07/09/16 19:120.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 07/09/16 19:120.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 07/09/16 19:120.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 07/09/16 19:120.50
Decachlorobiphenyl (S)%57 10-132 07/09/16 19:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775710LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1775711
PCB-1016 (Aroclor 1016)ug/L 3.65 73 50-150713.5 3 30
PCB-1260 (Aroclor 1260)ug/L 3.95 79 50-150794.0 1 30
Decachlorobiphenyl (S)%53 10-13248
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
307840
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92303930036, 92303930037, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011,
92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1631444
Associated Lab Samples:92303930036, 92303930037, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011,
92304098012
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 07/12/16 23:540.042
2,4,5-TP (Silvex)ug/L ND 0.19 07/12/16 23:540.049
2,4-D ug/L ND 0.94 07/12/16 23:540.22
2,4-DB ug/L ND 1.9 07/12/16 23:540.51
Bentazon ug/L ND 0.094 07/12/16 23:540.047
Dalapon ug/L ND 0.91 07/12/16 23:540.43
Dicamba ug/L ND 0.094 07/12/16 23:540.030
Dichlorprop ug/L ND 0.65 07/12/16 23:540.19
Dinoseb ug/L ND 0.19 07/12/16 23:540.057
Pentachlorophenol ug/L ND 0.028 07/12/16 23:540.017
Picloram ug/L ND 0.094 07/12/16 23:540.019
2,4-DCAA (S)%84 39-139 07/12/16 23:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1631445LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.31.2 107 37-133
2,4,5-TP (Silvex)ug/L 1.31.2 112 53-134
2,4-D ug/L 4.46 73 35-124
2,4-DB ug/L 12.512 104 31-132
Bentazon ug/L 0.52.6 87 51-125
Dalapon ug/L 7.36 122 10-122
Dicamba ug/L 0.61.6 101 44-125
Dichlorprop ug/L 4.24.2 99 70-130
Dinoseb ug/L 1.11.2 91 13-116
Pentachlorophenol ug/L 0.19.18 105 39-170
Picloram ug/L 0.40.6 67 10-127
2,4-DCAA (S)%90 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1632331MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098011
1632332
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 2.4 103 37-13378 27 402.4ND 2.5 1.9
2,4,5-TP (Silvex)ug/L 2.4 111 53-13491 20 402.4ND 2.7 2.2
2,4-D ug/L 12 70 35-12463 10 4012ND8.4 7.6
2,4-DB ug/L 24 89 31-13277 14 4024ND21.3 18.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1632331MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098011
1632332
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bentazon ug/L M11.2 27 51-1259 401.2ND 0.32 0.11J
Dalapon ug/L M1,R11220910-122127 48 4012ND25.1 15.3
Dicamba ug/L M11.2 151 44-125121 22 401.2ND 1.8 1.5
Dichlorprop ug/L M18.4 66 70-13056 17 408.4ND 5.6 4.7
Dinoseb ug/L 2.4 81 13-11655 38 402.4ND 1.9 1.3
Pentachlorophenol ug/L .36 68 39-17081 17 40.36ND 0.24 0.29
Picloram ug/L 1.2 88 10-12781 8 401.2ND 1.1 0.98
2,4-DCAA (S)%97 39-139131 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320460
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92303930036, 92303930037, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011,
92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775636
Associated Lab Samples:92303930036, 92303930037, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011,
92304098012
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 07/12/16 13:161.7
1,3,5-Trinitrobenzene ug/L ND 10.0 07/12/16 13:161.1
1,3-Dinitrobenzene ug/L ND 20.0 07/12/16 13:161.5
1,4-Naphthoquinone ug/L ND 10.0 07/12/16 13:161.8
1-Naphthalenamine ug/L ND 10.0 07/12/16 13:160.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/12/16 13:161.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 07/12/16 13:162.3
2,4,5-Trichlorophenol ug/L ND 10.0 07/12/16 13:162.2
2,4,6-Trichlorophenol ug/L ND 10.0 07/12/16 13:161.9
2,4-Dichlorophenol ug/L ND 10.0 07/12/16 13:161.7
2,4-Dimethylphenol ug/L ND 10.0 07/12/16 13:162.2
2,4-Dinitrophenol ug/L ND 50.0 07/12/16 13:166.5
2,4-Dinitrotoluene ug/L ND 10.0 07/12/16 13:161.2
2,6-Dichlorophenol ug/L ND 10.0 07/12/16 13:161.8
2,6-Dinitrotoluene ug/L ND 10.0 07/12/16 13:161.7
2-Acetylaminofluorene ug/L ND 20.0 07/12/16 13:160.84
2-Chloronaphthalene ug/L ND 10.0 07/12/16 13:162.2
2-Chlorophenol ug/L ND 10.0 07/12/16 13:161.5
2-Methylnaphthalene ug/L ND 10.0 07/12/16 13:160.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/12/16 13:161.7
2-Naphthalenamine ug/L ND 10.0 07/12/16 13:160.98
2-Nitroaniline ug/L ND 50.0 07/12/16 13:162.8
2-Nitrophenol ug/L ND 10.0 07/12/16 13:161.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/12/16 13:161.7
3,3'-Dichlorobenzidine ug/L ND 20.0 07/12/16 13:161.4
3,3'-Dimethylbenzidine ug/L ND 10.0 07/12/16 13:162.1
3-Methylcholanthrene ug/L ND 10.0 07/12/16 13:160.82
3-Nitroaniline ug/L ND 50.0 07/12/16 13:162.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 07/12/16 13:161.7
4-Aminobiphenyl ug/L ND 20.0 07/12/16 13:160.92
4-Bromophenylphenyl ether ug/L ND 10.0 07/12/16 13:161.3
4-Chloro-3-methylphenol ug/L ND 20.0 07/12/16 13:164.2
4-Chloroaniline ug/L ND 20.0 07/12/16 13:163.4
4-Chlorophenylphenyl ether ug/L ND 10.0 07/12/16 13:162.1
4-Nitroaniline ug/L ND 20.0 07/12/16 13:162.5
4-Nitrophenol ug/L ND 50.0 07/12/16 13:165.8
5-Nitro-o-toluidine ug/L ND 10.0 07/12/16 13:161.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 07/12/16 13:160.77
Acenaphthene ug/L ND 10.0 07/12/16 13:160.25
Acenaphthylene ug/L ND 10.0 07/12/16 13:160.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775636
Associated Lab Samples:92303930036, 92303930037, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011,
92304098012
Matrix:Water
AnalyzedMDL
Acetophenone ug/L ND 10.0 07/12/16 13:162.0
Anthracene ug/L ND 10.0 07/12/16 13:160.14
Benzo(a)anthracene ug/L ND 10.0 07/12/16 13:160.33
Benzo(a)pyrene ug/L ND 10.0 07/12/16 13:160.30
Benzo(b)fluoranthene ug/L ND 10.0 07/12/16 13:160.28
Benzo(g,h,i)perylene ug/L ND 10.0 07/12/16 13:160.38
Benzo(k)fluoranthene ug/L ND 10.0 07/12/16 13:160.43
Benzyl alcohol ug/L ND 20.0 07/12/16 13:163.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/12/16 13:161.7
bis(2-Chloroethyl) ether ug/L ND 10.0 07/12/16 13:161.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 07/12/16 13:160.85
Butylbenzylphthalate ug/L ND 10.0 07/12/16 13:160.75
Chlorobenzilate ug/L ND 10.0 07/12/16 13:160.72
Chrysene ug/L ND 10.0 07/12/16 13:160.21
Di-n-butylphthalate ug/L ND 10.0 07/12/16 13:161.1
Di-n-octylphthalate ug/L ND 10.0 07/12/16 13:160.86
Diallate ug/L ND 10.0 07/12/16 13:161.3
Dibenz(a,h)anthracene ug/L ND 10.0 07/12/16 13:160.55
Dibenzofuran ug/L ND 10.0 07/12/16 13:161.8
Diethylphthalate ug/L ND 6000 07/12/16 13:161.3
Dimethoate ug/L ND 20.0 07/12/16 13:160.92
Dimethylphthalate ug/L ND 10.0 07/12/16 13:161.5
Diphenylamine ug/L ND 10.0 07/12/16 13:161.3
Disulfoton ug/L ND 10.0 07/12/16 13:161.4
Ethyl methanesulfonate ug/L ND 20.0 07/12/16 13:161.8
Famphur ug/L ND 20.0 07/12/16 13:161.7
Fluoranthene ug/L ND 10.0 07/12/16 13:160.21
Fluorene ug/L ND 10.0 07/12/16 13:160.21
Hexachlorobenzene ug/L ND 10.0 07/12/16 13:161.1
Hexachlorocyclopentadiene ug/L ND 10.0 07/12/16 13:161.8
Hexachloroethane ug/L ND 10.0 07/12/16 13:161.5
Hexachloropropene ug/L ND 10.0 07/12/16 13:161.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/12/16 13:160.29
Isodrin ug/L ND 20.0 07/12/16 13:162.0
Isophorone ug/L ND 10.0 07/12/16 13:161.8
Isosafrole ug/L ND 10.0 07/12/16 13:161.8
Kepone ug/L ND 20.0 07/12/16 13:163.1
Methapyrilene ug/L ND 100 07/12/16 13:162.7
Methyl methanesulfonate ug/L ND 10.0 07/12/16 13:161.3
Methyl parathion ug/L ND 10.0 07/12/16 13:161.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 07/12/16 13:162.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/12/16 13:162.1
N-Nitrosodiethylamine ug/L ND 20.0 07/12/16 13:161.8
N-Nitrosodimethylamine ug/L ND 10.0 07/12/16 13:161.3
N-Nitrosodiphenylamine ug/L ND 10.0 07/12/16 13:161.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775636
Associated Lab Samples:92303930036, 92303930037, 92304098007, 92304098008, 92304098009, 92304098010, 92304098011,
92304098012
Matrix:Water
AnalyzedMDL
N-Nitrosomethylethylamine ug/L ND 10.0 07/12/16 13:161.8
N-Nitrosopiperidine ug/L ND 20.0 07/12/16 13:161.9
N-Nitrosopyrrolidine ug/L ND 10.0 07/12/16 13:162.5
Nitrobenzene ug/L ND 10.0 07/12/16 13:161.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 07/12/16 13:161.8
O-Toluidine ug/L ND 10.0 07/12/16 13:161.6
P-Dimethylaminoazobenzene ug/L ND 10.0 07/12/16 13:160.35
p-Phenylenediamine ug/L ND 10.0 07/12/16 13:160.96
Parathion (Ethyl parathion)ug/L ND 10.0 07/12/16 13:161.1
Pentachlorobenzene ug/L ND 10.0 07/12/16 13:162.0
Pentachloronitrobenzene ug/L ND 20.0 07/12/16 13:161.0
Pentachlorophenol ug/L ND 25.0 07/12/16 13:162.3
Phenacetin ug/L ND 20.0 07/12/16 13:160.97
Phenanthrene ug/L ND 10.0 07/12/16 13:160.22
Phenol ug/L ND 10.0 07/12/16 13:161.7
Phorate ug/L ND 10.0 07/12/16 13:161.1
Pronamide ug/L ND 10.0 07/12/16 13:160.97
Pyrene ug/L ND 10.0 07/12/16 13:160.19
Safrole ug/L ND 10.0 07/12/16 13:161.5
Thionazin ug/L ND 20.0 07/12/16 13:161.2
2,4,6-Tribromophenol (S)%68 27-110 07/12/16 13:16
2-Fluorobiphenyl (S)%66 27-110 07/12/16 13:16
2-Fluorophenol (S)%39 12-110 07/12/16 13:16
Nitrobenzene-d5 (S)%74 21-110 07/12/16 13:16
Phenol-d6 (S)%30 10-110 07/12/16 13:16
Terphenyl-d14 (S)%88 31-107 07/12/16 13:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775637LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 33.250 66 16-129
1,3,5-Trinitrobenzene ug/L 50.950 102 55-125
1,3-Dinitrobenzene ug/L 39.550 79 30-122
1,4-Naphthoquinone ug/L 41.350 83 31-120
1-Naphthalenamine ug/L 34.250 68 37-126
2,2'-Oxybis(1-chloropropane)ug/L 42.950 86 18-120
2,3,4,6-Tetrachlorophenol ug/L 54.250 108 54-276
2,4,5-Trichlorophenol ug/L 41.050 82 43-113
2,4,6-Trichlorophenol ug/L 40.050 80 42-120
2,4-Dichlorophenol ug/L 40.850 82 30-120
2,4-Dimethylphenol ug/L 40.450 81 29-111
2,4-Dinitrophenol ug/L 155250 62 19-132
2,4-Dinitrotoluene ug/L 45.650 91 58-128
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775637LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dichlorophenol ug/L 43.050 86 54-128
2,6-Dinitrotoluene ug/L 47.450 95 54-129
2-Acetylaminofluorene ug/L 53.650 107 81-160
2-Chloronaphthalene ug/L 38.550 77 43-117
2-Chlorophenol ug/L 36.750 73 37-120
2-Methylnaphthalene ug/L 40.150 80 33-120
2-Methylphenol(o-Cresol)ug/L 35.450 71 31-120
2-Naphthalenamine ug/L 41.050 82 41-136
2-Nitroaniline ug/L 89.0100 89 48-121
2-Nitrophenol ug/L 39.350 79 25-116
3&4-Methylphenol(m&p Cresol)ug/L 32.450 65 23-120
3,3'-Dichlorobenzidine ug/L 91.1250 36 10-154
3,3'-Dimethylbenzidine ug/L 51.7100 52 10-157
3-Methylcholanthrene ug/L 42.750 85 65-130
3-Nitroaniline ug/L 87.7100 88 43-115
4,6-Dinitro-2-methylphenol ug/L 91.8100 92 44-124
4-Aminobiphenyl ug/L 35.350 71 21-125
4-Bromophenylphenyl ether ug/L 40.350 81 34-113
4-Chloro-3-methylphenol ug/L 93.5100 93 31-110
4-Chloroaniline ug/L 85.0100 85 20-120
4-Chlorophenylphenyl ether ug/L 39.450 79 34-116
4-Nitroaniline ug/L 85.8100 86 46-128
4-Nitrophenol ug/L 106250 42 11-120
5-Nitro-o-toluidine ug/L 50.850 102 78-160
7,12-Dimethylbenz(a)anthracene ug/L 43.850 88 47-124
Acenaphthene ug/L 37.750 75 48-114
Acenaphthylene ug/L 39.550 79 48-112
Acetophenone ug/L 49.450 99 24-120
Anthracene ug/L 39.550 79 57-118
Benzo(a)anthracene ug/L 41.450 83 56-121
Benzo(a)pyrene ug/L 43.850 88 55-127
Benzo(b)fluoranthene ug/L 44.950 90 53-128
Benzo(g,h,i)perylene ug/L 42.850 86 54-125
Benzo(k)fluoranthene ug/L 43.350 87 51-123
Benzyl alcohol ug/L 87.6100 88 27-120
bis(2-Chloroethoxy)methane ug/L 41.350 83 32-120
bis(2-Chloroethyl) ether ug/L 41.050 82 33-111
bis(2-Ethylhexyl)phthalate ug/L 49.350 99 50-145
Butylbenzylphthalate ug/L 50.150 100 54-138
Chlorobenzilate ug/L 45.850 92 65-132
Chrysene ug/L 38.850 78 58-127
Di-n-butylphthalate ug/L 44.450 89 56-125
Di-n-octylphthalate ug/L 45.050 90 50-134
Diallate ug/L 41.250 82 47-123
Dibenz(a,h)anthracene ug/L 41.850 84 53-129
Dibenzofuran ug/L 42.050 84 45-120
Diethylphthalate ug/L 41.1J50 82 53-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775637LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethoate ug/L 40.350 81 57-139
Dimethylphthalate ug/L 40.250 80 55-116
Diphenylamine ug/L 41.050 82 42-120
Disulfoton ug/L 41.250 82 49-156
Ethyl methanesulfonate ug/L 42.650 85 43-120
Famphur ug/L 68.5100 69 40-160
Fluoranthene ug/L 40.750 81 57-125
Fluorene ug/L 41.050 82 53-118
Hexachlorobenzene ug/L 36.850 74 49-116
Hexachlorocyclopentadiene ug/L 28.050 56 26-158
Hexachloroethane ug/L 30.350 61 30-114
Hexachloropropene ug/L 29.350 59 13-137
Indeno(1,2,3-cd)pyrene ug/L 42.250 84 55-128
Isodrin ug/L 46.050 92 68-129
Isophorone ug/L 46.950 94 31-118
Isosafrole ug/L 39.850 80 48-107
Kepone ug/L 74.9100 75 10-124
Methapyrilene ug/L 28.9J50 58 40-160
Methyl methanesulfonate ug/L 32.650 65 25-114
Methyl parathion ug/L 44.950 90 58-137
N-Nitroso-di-n-butylamine ug/L 41.050 82 36-115
N-Nitroso-di-n-propylamine ug/L 50.550 101 32-119
N-Nitrosodiethylamine ug/L 45.250 90 47-115
N-Nitrosodimethylamine ug/L 20.850 42 13-120
N-Nitrosodiphenylamine ug/L 41.050 82 43-120
N-Nitrosomethylethylamine ug/L 41.350 83 39-120
N-Nitrosopiperidine ug/L 46.250 92 43-113
N-Nitrosopyrrolidine ug/L 46.950 94 32-110
Nitrobenzene ug/L 40.950 82 33-110
O,O,O-Triethylphosphorothioate ug/L 38.850 78 51-127
O-Toluidine ug/L 40.350 81 27-120
P-Dimethylaminoazobenzene ug/L 23.4100 23 10-120
p-Phenylenediamine ug/L 55.750 111 72-143
Parathion (Ethyl parathion)ug/L 47.450 95 56-140
Pentachlorobenzene ug/L 36.050 72 30-137
Pentachloronitrobenzene ug/L 48.950 98 70-124
Pentachlorophenol ug/L 85.4250 34 10-137
Phenacetin ug/L 47.950 96 60-130
Phenanthrene ug/L 38.850 78 57-117
Phenol ug/L 21.350 43 10-120
Phorate ug/L 45.350 91 55-126
Pronamide ug/L 44.950 90 75-124
Pyrene ug/L 43.250 86 55-122
Safrole ug/L 40.850 82 41-120
Thionazin ug/L 44.550 89 63-137
2,4,6-Tribromophenol (S)%81 27-110
2-Fluorobiphenyl (S)%69 27-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775637LABORATORY CONTROL SAMPLE:
LCSSpike
2-Fluorophenol (S)%44 12-110
Nitrobenzene-d5 (S)%77 21-110
Phenol-d6 (S)%36 10-110
Terphenyl-d14 (S)%89 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775638MATRIX SPIKE SAMPLE:
MSSpike
Result
92303930033
1,2,4,5-Tetrachlorobenzene ug/L 35.050 70 50-150ND
1,3,5-Trinitrobenzene ug/L 49.950 100 50-150ND
1,3-Dinitrobenzene ug/L 40.250 80 50-150ND
1,4-Naphthoquinone ug/L 42.950 86 50-150ND
1-Naphthalenamine ug/L 34.850 70 50-150ND
2,2'-Oxybis(1-chloropropane)ug/L 43.150 86 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 47.750 95 50-150ND
2,4,5-Trichlorophenol ug/L 41.150 82 19-105ND
2,4,6-Trichlorophenol ug/L 40.850 82 13-108ND
2,4-Dichlorophenol ug/L 41.350 83 29-111ND
2,4-Dimethylphenol ug/L 41.550 83 21-103ND
2,4-Dinitrophenol ug/L 162250 65 10-109ND
2,4-Dinitrotoluene ug/L 45.350 91 27-104ND
2,6-Dichlorophenol ug/L 41.850 84 50-150ND
2,6-Dinitrotoluene ug/L 47.450 95 28-101ND
2-Acetylaminofluorene ug/L 55.450 110 50-150ND
2-Chloronaphthalene ug/L 39.950 80 14-102ND
2-Chlorophenol ug/L 38.250 76 16-110ND
2-Methylnaphthalene ug/L 40.350 81 13-110ND
2-Methylphenol(o-Cresol)ug/L 36.450 73 19-110ND
2-Naphthalenamine ug/L 45.250 90 50-150ND
2-Nitroaniline ug/L 85.9100 86 26-103ND
2-Nitrophenol ug/L 41.250 82 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 32.950 66 20-110ND
3,3'-Dichlorobenzidine ug/L 86.1250 34 25-112ND
3,3'-Dimethylbenzidine ug/L 34.7 M11003550-150ND
3-Methylcholanthrene ug/L 43.550 86 50-150ND
3-Nitroaniline ug/L 50.8100 51 29-110ND
4,6-Dinitro-2-methylphenol ug/L 91.3100 91 10-117ND
4-Aminobiphenyl ug/L 34.550 69 50-150ND
4-Bromophenylphenyl ether ug/L 40.350 81 20-105ND
4-Chloro-3-methylphenol ug/L 91.6100 92 22-110ND
4-Chloroaniline ug/L 85.0100 85 20-100ND
4-Chlorophenylphenyl ether ug/L 40.150 80 19-102ND
4-Nitroaniline ug/L 78.3100 78 29-110ND
4-Nitrophenol ug/L 113250 45 10-110ND
5-Nitro-o-toluidine ug/L 43.950 88 50-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 153 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775638MATRIX SPIKE SAMPLE:
MSSpike
Result
92303930033
7,12-Dimethylbenz(a)anthracene ug/L 43.250 86 50-150ND
Acenaphthene ug/L 38.450 77 17-100ND
Acenaphthylene ug/L 40.350 81 21-100ND
Acetophenone ug/L 48.150 96 50-150ND
Anthracene ug/L 39.650 79 24-109ND
Benzo(a)anthracene ug/L 40.550 81 22-117ND
Benzo(a)pyrene ug/L 42.850 86 23-104ND
Benzo(b)fluoranthene ug/L 44.250 88 23-103ND
Benzo(g,h,i)perylene ug/L 41.650 83 18-111ND
Benzo(k)fluoranthene ug/L 40.150 80 22-113ND
Benzyl alcohol ug/L 88.0100 88 19-101ND
bis(2-Chloroethoxy)methane ug/L 41.850 84 22-110ND
bis(2-Chloroethyl) ether ug/L 42.050 84 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 48.550 94 23-1021.7J
Butylbenzylphthalate ug/L 49.550 99 25-110ND
Chlorobenzilate ug/L 44.850 90 50-150ND
Chrysene ug/L 38.850 78 23-115ND
Di-n-butylphthalate ug/L 43.450 87 26-110ND
Di-n-octylphthalate ug/L 50.950 102 22-110ND
Diallate ug/L 41.250 82 50-150ND
Dibenz(a,h)anthracene ug/L 41.350 83 21-112ND
Dibenzofuran ug/L 42.750 85 19-102ND
Diethylphthalate ug/L 41.8J50 84 29-110ND
Dimethoate ug/L 40.450 81 50-150ND
Dimethylphthalate ug/L 40.450 81 27-110ND
Diphenylamine ug/L 41.350 83 50-150ND
Disulfoton ug/L 42.150 83 50-150ND
Ethyl methanesulfonate ug/L 42.850 86 50-150ND
Famphur ug/L 42.7 M11004350-150ND
Fluoranthene ug/L 39.150 78 23-112ND
Fluorene ug/L 40.850 82 22-104ND
Hexachlorobenzene ug/L 36.550 73 21-116ND
Hexachlorocyclopentadiene ug/L 32.150 64 10-110ND
Hexachloroethane ug/L 32.850 66 10-110ND
Hexachloropropene ug/L 33.250 66 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 41.750 83 20-113ND
Isodrin ug/L 46.550 93 50-150ND
Isophorone ug/L 46.150 92 50-150ND
Isosafrole ug/L 40.850 82 50-150ND
Kepone ug/L 70.7100 71 50-150ND
Methapyrilene ug/L 33.4J50 67 50-150ND
Methyl methanesulfonate ug/L 35.250 70 50-150ND
Methyl parathion ug/L 44.350 89 50-150ND
N-Nitroso-di-n-butylamine ug/L 44.050 88 50-150ND
N-Nitroso-di-n-propylamine ug/L 48.950 98 21-105ND
N-Nitrosodiethylamine ug/L 47.550 95 50-150ND
N-Nitrosodimethylamine ug/L 24.350 49 10-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 154 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1775638MATRIX SPIKE SAMPLE:
MSSpike
Result
92303930033
N-Nitrosodiphenylamine ug/L 41.350 83 23-107ND
N-Nitrosomethylethylamine ug/L 43.050 86 50-150ND
N-Nitrosopiperidine ug/L 46.550 93 50-150ND
N-Nitrosopyrrolidine ug/L 47.050 94 50-150ND
Nitrobenzene ug/L 42.150 84 20-110ND
O,O,O-Triethylphosphorothioate ug/L 39.150 78 50-150ND
O-Toluidine ug/L 41.750 83 50-150ND
P-Dimethylaminoazobenzene ug/L 22.6 M11002350-150ND
p-Phenylenediamine ug/L 53.850 108 50-150ND
Parathion (Ethyl parathion)ug/L 47.350 95 50-150ND
Pentachlorobenzene ug/L 36.350 73 50-150ND
Pentachloronitrobenzene ug/L 49.250 98 50-150ND
Pentachlorophenol ug/L 86.1250 34 10-118ND
Phenacetin ug/L 48.050 96 50-150ND
Phenanthrene ug/L 38.250 76 24-106ND
Phenol ug/L 22.650 45 12-110ND
Phorate ug/L 45.950 92 50-150ND
Pronamide ug/L 44.050 88 50-150ND
Pyrene ug/L 42.350 85 24-114ND
Safrole ug/L 41.250 82 50-150ND
Thionazin ug/L 45.750 89 50-1501.3J
2,4,6-Tribromophenol (S)%82 27-110
2-Fluorobiphenyl (S)%72 27-110
2-Fluorophenol (S)%49 12-110
Nitrobenzene-d5 (S)%81 21-110
Phenol-d6 (S)%38 10-110
Terphenyl-d14 (S)%77 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930036
1775639SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 155 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930036
1775639SAMPLE DUPLICATE:
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 156 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930036
1775639SAMPLE DUPLICATE:
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%72 1281
2-Fluorobiphenyl (S)%64 970
2-Fluorophenol (S)%39 541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 157 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92303930036
1775639SAMPLE DUPLICATE:
Nitrobenzene-d5 (S)%67 873
Phenol-d6 (S)%30 932
Terphenyl-d14 (S)%81 687
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 158 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321132
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779577
Associated Lab Samples:92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 07/14/16 17:061000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779578LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4840050000 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779579MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304420005
1779580
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 85 80-12087 1 255000036.9 mg/L 79600 80400
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779581MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304520002
1779582
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 91 80-12090 1 255000033.0 mg/L 78500 78100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 159 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321357
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92303930032, 92303930034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1780858
Associated Lab Samples:92303930032, 92303930034
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 07/15/16 20:021000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1780859LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4950050000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780860MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304615003
1780861
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M15000013080-120130 0 255000012.6 mg/L 77600 77800
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780862MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304785002
1780863
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 118 80-12087 8 2550000130 mg/L 189000 174000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 160 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320825
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92303930032, 92304098001, 92304098002, 92304098007, 92304098008, 92304098009, 92304098011,
92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1777612
Associated Lab Samples:92303930032, 92304098001, 92304098002, 92304098007, 92304098008, 92304098009, 92304098011,
92304098012
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 07/12/16 13:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1777613LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 483J500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777614MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303850002
1777615
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 90-110100 0 10500ND542J542J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777616MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303965001
1777617
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 99 90-11099 0 10500ND505J505J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 161 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321057
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92303930034, 92303930036, 92303930037
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779211
Associated Lab Samples:92303930034, 92303930036, 92303930037
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 07/13/16 16:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779212LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 511J500 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779213MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304304001
1779214
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M3500690-1106 10500NDNDND
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779215MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930034
1779216
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M150012090-110120 0 10500ND603J603J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 162 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320133
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1774098
Associated Lab Samples:92304098001, 92304098002
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 07/12/16 02:002000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774099LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 203000198000 103 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92304109002
1774100SAMPLE DUPLICATE:
BOD, 5 day ug/L 97800 2 1099.3 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 163 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320345
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775199
Associated Lab Samples:92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 07/07/16 18:361000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775200LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19300J20000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1775201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098001
1775202
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 95 90-11095 0 10200003660J22600J22600J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 164 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320518
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92303930032, 92303930034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1776040
Associated Lab Samples:92303930032, 92303930034
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 07/08/16 18:221000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1776041LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19100J20000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1776042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92302775001
1776043
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 91 90-11091 0 102000025.2 mg/L 43400J 43500J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 165 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320181
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1774240
Associated Lab Samples:92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 07/07/16 08:2510.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1774241LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24602500 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1774242MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304131002
1774243
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125008490-11084 0 102500ND21002100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 166 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320395
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92303930032, 92303930034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1775344
Associated Lab Samples:92303930032, 92303930034
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 07/08/16 08:0810.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1775345LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24302500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1775346MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304304001
1775347
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 98 90-11099 0 102500365J28302830
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 167 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321155
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779647
Associated Lab Samples:92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 07/14/16 12:17500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779648LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1970020000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779649MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304706001
1779650
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 99 90-110101 0 101000024.4 mg/L 34300 34400
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779651MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304282001
1779652
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M1200007790-11074 2 102000026.5 mg/L 41900 41200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 168 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321256
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92303930032, 92303930034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1780514
Associated Lab Samples:92303930032, 92303930034
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 07/16/16 02:22500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1780515LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2020020000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780516MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304120001
1780517
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000014590-110154 2 101000033.5 mg/L 47900 48900
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1780518MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930032
1780519
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000011590-110116 0 1010000183002980029900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 169 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320783
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92304098007, 92304098008, 92304098009, 92304098010, 92304098011, 92304098012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1777340
Associated Lab Samples:92304098007, 92304098008, 92304098009, 92304098010, 92304098011, 92304098012
Matrix:Water
AnalyzedMDL
Cyanide ug/L 4.8J 10.0 07/12/16 17:074.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1777341LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 108100 108 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777342MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304589002
1777343
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 91 75-12594 3 10100ND98.9 102
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098007
1777345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11005875-12559 2 101004.2J 62.1 63.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 170 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
320784
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92303930036, 92303930037
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1777346
Associated Lab Samples:92303930036, 92303930037
Matrix:Water
AnalyzedMDL
Cyanide ug/L 4.2J 10.0 07/12/16 17:364.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1777347LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 103100 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777348MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930033
1777349
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11006375-12564 2 101005.0J 68.2 69.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1777350MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304483003
1777351
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 101 75-125102 1 10100ND109110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 171 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
321038
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1779019
Associated Lab Samples:92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 07/13/16 17:4512500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1779020LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 740000750000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779021MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303853001
1779022
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 30000000 95 90-11095 0 3300000003220 mg/L 3170000
0
3170000
0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1779023MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304058001
1779024
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M675000007990-11079 0 375000004250 mg/L 1020000
0
1020000
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 172 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
322212
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92303930032, 92303930034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1785501
Associated Lab Samples:92303930032, 92303930034
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 07/22/16 15:3012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1785502LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 383000375000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1785503MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304578001
1785504
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M3375000090-1100 0 33750001240 mg/L 1240000 1240000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1785505MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92303930035
1785506
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M13750008390-11083 0 337500091000404000404000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 173 of 190
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
322299
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92303930032, 92303930034, 92304098001, 92304098002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1786055
Associated Lab Samples:92303930032, 92303930034, 92304098001, 92304098002
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 07/23/16 02:03500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1786056LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2310025000 93 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1786057MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304098001
1786058
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250008690-11094 8 102500016402310025000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1786059MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92304304003
1786060
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 101 90-11091 10 102500024402770025200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 174 of 190
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 175 of 190
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
ANALYTE QUALIFIERS
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 176 of 190
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92304098007 320316 320403MW-1 EPA 3510 EPA 8081
92304098008 320316 320403MW-1B EPA 3510 EPA 8081
92304098009 320316 320403MW-4R EPA 3510 EPA 8081
92304098010 320316 320403MW-5 EPA 3510 EPA 8081
92304098011 320316 320403MW-12 EPA 3510 EPA 8081
92304098012 320316 320403MW-16 EPA 3510 EPA 8081
92303930036 320774 320874MW-9 EPA 3510 EPA 8081
92303930037 320774 320874MW-2 EPA 3510 EPA 8081
92304098007 320263 320402MW-1 EPA 3510 EPA 8082
92304098008 320263 320402MW-1B EPA 3510 EPA 8082
92304098009 320263 320402MW-4R EPA 3510 EPA 8082
92304098010 320263 320402MW-5 EPA 3510 EPA 8082
92304098011 320263 320402MW-12 EPA 3510 EPA 8082
92304098012 320263 320402MW-16 EPA 3510 EPA 8082
92303930036 320469 320584MW-9 EPA 3510 EPA 8082
92303930037 320469 320584MW-2 EPA 3510 EPA 8082
92304098007 307840 308354MW-1 EPA 8151 EPA 8151
92304098008 307840 308354MW-1B EPA 8151 EPA 8151
92304098009 307840 308354MW-4R EPA 8151 EPA 8151
92304098010 307840 308354MW-5 EPA 8151 EPA 8151
92304098011 307840 308354MW-12 EPA 8151 EPA 8151
92304098012 307840 308354MW-16 EPA 8151 EPA 8151
92303930036 307840 308354MW-9 EPA 8151 EPA 8151
92303930037 307840 308354MW-2 EPA 8151 EPA 8151
92304098001 321519MW-12 RSK 175 Modified
92304098002 321519MW-12D RSK 175 Modified
92304098010 321519MW-5 RSK 175 Modified
92304098012 321519MW-16 RSK 175 Modified
92303930002 320140 320384MW-10 EPA 3010A EPA 6010
92303930003 320140 320384MW-13 EPA 3010A EPA 6010
92303930004 320140 320384MW-14 EPA 3010A EPA 6010
92303930005 320140 320384MW-15 EPA 3010A EPA 6010
92303930006 320140 320384MW-17 EPA 3010A EPA 6010
92303930007 320140 320384MW-19 EPA 3010A EPA 6010
92303930008 320140 320384MW-20 EPA 3010A EPA 6010
92303930009 320140 320384MW-21 EPA 3010A EPA 6010
92303930010 320140 320384MW-22 EPA 3010A EPA 6010
92303930011 320140 320384MW-23 EPA 3010A EPA 6010
92303930012 320140 320384MW-32 EPA 3010A EPA 6010
92303930013 320140 320384MW-33 EPA 3010A EPA 6010
92303930014 320140 320384MW-34 EPA 3010A EPA 6010
92303930015 320141 320562SW-3 EPA 3010A EPA 6010
92303930016 320141 320562SW-4R EPA 3010A EPA 6010
92303930017 320141 320562SW-5 EPA 3010A EPA 6010
92303930018 320141 320562SW-6 EPA 3010A EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 177 of 190
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92304098002 320532 320766MW-12D EPA 3010A EPA 6010
92304098003 320532 320766MW-16 EPA 3010A EPA 6010
92304098004 320532 320766EBEPA 3010A EPA 6010
92304098005 320532 320766FBEPA 3010A EPA 6010
92304098007 320532 320766MW-1 EPA 3010A EPA 6010
92304098008 320532 320766MW-1B EPA 3010A EPA 6010
92304098009 320532 320766MW-4R EPA 3010A EPA 6010
92304098010 320532 320766MW-5 EPA 3010A EPA 6010
92304098011 320532 320766MW-12 EPA 3010A EPA 6010
92303930031 320532 320766MW-6 EPA 3010A EPA 6010
92303930032 320532 320766MW-24 EPA 3010A EPA 6010
92303930034 320532 320766MW-25 EPA 3010A EPA 6010
92303930036 320532 320766MW-9 EPA 3010A EPA 6010
92303930037 320532 320766MW-2 EPA 3010A EPA 6010
92304098001 320919 321096MW-12 EPA 3010 EPA 6010
92304098002 320919 321096MW-12D EPA 3010 EPA 6010
92303930032 320919 321096MW-24 EPA 3010 EPA 6010
92303930034 320919 321096MW-25 EPA 3010 EPA 6010
92304098003 320770 321289MW-16 EPA 7470 EPA 7470
92304098004 320770 321289EBEPA 7470 EPA 7470
92304098005 320770 321289FBEPA 7470 EPA 7470
92304098007 320770 321289MW-1 EPA 7470 EPA 7470
92304098008 320770 321289MW-1B EPA 7470 EPA 7470
92304098009 320770 321289MW-4R EPA 7470 EPA 7470
92304098010 320770 321289MW-5 EPA 7470 EPA 7470
92304098011 320770 321289MW-12 EPA 7470 EPA 7470
92304098007 320460 320668MW-1 EPA 3510 EPA 8270
92304098008 320460 320668MW-1B EPA 3510 EPA 8270
92304098009 320460 320668MW-4R EPA 3510 EPA 8270
92304098010 320460 320668MW-5 EPA 3510 EPA 8270
92304098011 320460 321682MW-12 EPA 3510 EPA 8270
92304098012 320460 320668MW-16 EPA 3510 EPA 8270
92303930036 320460 320668MW-9 EPA 3510 EPA 8270
92303930037 320460 320668MW-2 EPA 3510 EPA 8270
92303930002 320327MW-10 EPA 8260
92303930003 320327MW-13 EPA 8260
92303930004 320327MW-14 EPA 8260
92303930005 320327MW-15 EPA 8260
92303930006 320327MW-17 EPA 8260
92303930007 320327MW-19 EPA 8260
92303930008 320327MW-20 EPA 8260
92303930009 320327MW-21 EPA 8260
92303930010 320327MW-22 EPA 8260
92303930011 320327MW-23 EPA 8260
92303930012 320327MW-32 EPA 8260
92303930013 320327MW-33 EPA 8260
92303930014 320327MW-34 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 178 of 190
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92303930015 320331SW-3 EPA 8260
92303930016 320331SW-4R EPA 8260
92303930017 320327SW-5 EPA 8260
92303930018 320327SW-6 EPA 8260
92304098002 320331MW-12D EPA 8260
92304098003 320331MW-16 EPA 8260
92304098004 320327EBEPA 8260
92304098005 320327FBEPA 8260
92304098006 320327TBEPA 8260
92304098007 320331MW-1 EPA 8260
92304098008 320331MW-1B EPA 8260
92304098009 320331MW-4R EPA 8260
92304098010 320331MW-5 EPA 8260
92304098011 320331MW-12 EPA 8260
92303930031 321048MW-6 EPA 8260
92303930032 321048MW-24 EPA 8260
92303930034 321048MW-25 EPA 8260
92303930036 321048MW-9 EPA 8260
92303930037 321048MW-2 EPA 8260
92304098001 321132MW-12 SM 2320B
92304098002 321132MW-12D SM 2320B
92303930032 321357MW-24 SM 2320B
92303930034 321357MW-25 SM 2320B
92304098001 320825MW-12 SM 4500-S2D
92304098002 320825MW-12D SM 4500-S2D
92304098007 320825MW-1 SM 4500-S2D
92304098008 320825MW-1B SM 4500-S2D
92304098009 320825MW-4R SM 4500-S2D
92304098011 320825MW-12 SM 4500-S2D
92304098012 320825MW-16 SM 4500-S2D
92303930032 320825MW-24 SM 4500-S2D
92303930034 321057MW-25 SM 4500-S2D
92303930036 321057MW-9 SM 4500-S2D
92303930037 321057MW-2 SM 4500-S2D
92304098001 320133 320168MW-12 SM 5210B SM 5210B
92304098002 320133 320168MW-12D SM 5210B SM 5210B
92304098001 320345MW-12 EPA 300.0
92304098002 320345MW-12D EPA 300.0
92303930032 320518MW-24 EPA 300.0
92303930034 320518MW-25 EPA 300.0
92304098001 320181MW-12 EPA 353.2
92304098002 320181MW-12D EPA 353.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 179 of 190
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92303930
ALEXANDER LF (SWS)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92303930032 320395MW-24 EPA 353.2
92303930034 320395MW-25 EPA 353.2
92304098001 321155MW-12 SM 4500-Cl-E
92304098002 321155MW-12D SM 4500-Cl-E
92303930032 321256MW-24 SM 4500-Cl-E
92303930034 321256MW-25 SM 4500-Cl-E
92304098007 320783MW-1 SM 4500-CN-E
92304098008 320783MW-1B SM 4500-CN-E
92304098009 320783MW-4R SM 4500-CN-E
92304098010 320783MW-5 SM 4500-CN-E
92304098011 320783MW-12 SM 4500-CN-E
92304098012 320783MW-16 SM 4500-CN-E
92303930036 320784MW-9 SM 4500-CN-E
92303930037 320784MW-2 SM 4500-CN-E
92304098001 321038MW-12 SM 5220D
92304098002 321038MW-12D SM 5220D
92303930032 322212MW-24 SM 5220D
92303930034 322212MW-25 SM 5220D
92304098001 322299MW-12 SM 5310B
92304098002 322299MW-12D SM 5310B
92303930032 322299MW-24 SM 5310B
92303930034 322299MW-25 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 09:49 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 180 of 190
Page 181 of 190
Page 182 of 190
Page 183 of 190
Page 184 of 190
Page 185 of 190
Page 186 of 190
Page 187 of 190
Page 188 of 190
Page 189 of 190
Page 190 of 190
Appendix B
Field Sampling Parameter Data Sheet(s)