19049_Regal_Mfg_Import_Soil_Assess_20170327

CATAWBA VALLEY
ENGINEERING AND TESTING
J. KIRK VIOLA, P.E. JAMES S. TATE, P.E. DAVID M. LEGRAND, JR., P.E.

March 27, 2017 Dr. Jerry Pruitt
245 11th Avenue Northeast
Hickory, North Carolina 28602
[e-mail]
Re: Soil Assessment for Imported Soils
Former Regal Manufacturing Facility
212 12th Avenue Northeast Hickory, North Carolina CVET Project No.: 17-308

Dear Dr. Pruitt, Per your request, Catawba Valley Engineering and Testing (CVET) has completed a soil
assessment as authorized through electronic correspondence with you on February 23, 2017.
The purpose of this soil assessment was to evaluate the suitability of imported soils for use at
the subject property. The contents of this report are provided for the use of Dr. Jerry Pruitt and affiliated parties;
and are not intended to be used as the basis for design and construction for any other project.
The contents of this report shall not be utilized by any other parties unless written permission is granted by CVET. CVET disclaims all liability from the misuse or reliance, by any such parties, of the contents brought forth in this report.

PROJECT DESCRIPTION AND FINDINGS The subject property is located at 212 12th Avenue NE in Hickory, North Carolina. Formerly, the site was utilized as an industrial manufacturing facility but is currently not operational
and was recently demolished. In support of current demolition and site redevelopment efforts
at the property, CVET was contracted by Dr. Jerry Pruitt, the property owner, to assess imported soils for the presence of environmental impact. Following review of laboratory analytical data, imported soils will be used to fill in voids created as a result of demolition
activities and to assist with grading operations at the subject property.

Jeff Kerley, JK Landscaping and Grading, indicated that imported soils will be retrieved from two separate borrow site locations. Each borrow site consists of virgin soil being removed
from a hillside cut. CVET discussed sampling approach and required laboratory analyses
with Mr. Jerry Deakle, Dr. Pruitt’s Brownfields consultant for the subject property, and
determined that one composite sample should be collected from each borrow site location. Additionally, Mr. Deakle confirmed that soil samples should be analyzed for volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by
EPA Method 8270, and EPA Priority Pollutant List Metals by EPA Method 6010/7471.
Based on information provided by Mr. Deakle, CVET collected one composite soil sample
P.O. BOX 2616 • 308 15TH STREET SE, SUITE 2 • HICKORY, NORTH CAROLINA 28603
TELEPHONE: [phone] • FAX: [phone]

from each borrow site location on February 24, 2017. Samples were collected utilizing a
decontaminated stainless steel hand auger, sampling spoon, and mixing bowl. Samples were
immediately placed on ice following collection, and were submitted to Pace Analytical
Laboratories to be analyzed for VOCs, SVOCs, and metals. Soil sampling was completed in accordance with NCDEQ Inactive Hazardous Waste Site
Branch (IHSB) guidelines, the Environmental Management Plan for this site, and Mr.
Deakle’s recommendations.
CONCLUSIONS AND RECOMMENDATIONS

Based on the laboratory analytical results, no VOC’s or SVOC’s were detected in either of
the soil samples collected. Low level metallic compounds were detected in both samples. In particular, arsenic was present at concentrations above the IHSB Preliminary Soil
Remediation Goal (PSRG) for residential and industrial properties, but below the Protection
of Groundwater PSRG in one of the samples. Although arsenic was detected at
concentrations above the residential and industrial standards, the average natural background soil concentration (Element Concentrations in Soils and Other Surficial Materials of the Conterminous United States, USGS, 1984) for arsenic in this region of the United States is
estimated to be greater than the regulatory standard and was found to be equal to the
concentration in the sample. Based on the estimated background concentration, it appears
that arsenic in the soil is likely naturally occurring and not a result of environmental impact. Arsenic and all other detected metal compounds were generally present in concentrations on
the same order of magnitude as the estimated natural background values, which further
suggests a natural origin.
Based on the laboratory analytical results and discussion with Mr. Deakle, it appears that the imported soils have not been impacted and are suitable for use at the subject property.
Additionally, Kady Lebeed, the Brownfields manager for this site has reviewed the analytical
data and concurs that the imported soils are acceptable for use at the subject site. CVET has
no additional recommendations at this time. We appreciate the opportunity to provide professional environmental services for your
project. If you have any questions regarding the contents of this report, please feel free to
contact us. Sincerely,

CATAWBA VALLEY ENGINEERING AND TESTING, P.C.
Nathan S. Simmons, P.G.
Environmental Professional
Page 2 of 2

Sample ID BP-1 BP-2
Date 2/24/2017 2/24/2017
Constituent USGS Background Metal
Concentration1 Residential PSRG Industrial PSRG
Antimony 0.52 6.2 94 0.8 --
Arsenic 4.8 0.68 3 4.8 --
Barium 290 3,000 44,000 152 317
Beryllium 0.55 32 460 0.9 1.4
Chromium*33 24,000 100,000 55.8 51.3
Copper 13 620 9,400 21.7 54.2
Lead 14 400 800 8.5 10.3
Mercury 0.081 1.9 8 0.009 --
Nickel 11 300 4,400 50.9 29.1
Selenium 0.3 78 1,200 3 2.4
Zinc 40 2.2 3.13 104 111
Notes:
-- No detection
Table 1 - Soil Analytical Results For Detected Constituents
Bolded and highlighted (blue) cells exceed the Industrial PSRG
Bolded and highlighted (peach) cells exceed the Residential PSRG
PSRG - Preliminary Soil Remediation Goal as defined by the NCDEQ Inactive Hazardous Sites Branch
* - No standard exists for total chromium, therfore, trivalent Chromium (Cr+3) is used instead.
1 - Natural background metal concentrations for soils in the Eastern US (USGS, Element Concentrations in Soils and Other Surficial
Materials of the Conterminous United States, 1984). Used for qualitative purposes only.
mg/kg - milligrams/kilograms
(Units in mg/kg)
Hickory, North Carolina
212 12th Avenue Northeast
Soil Assessment for Imported Soils
#=CL#
March 02, 2017
LIMS USE: FR - JAMES CARTER
LIMS OBJECT ID: 92331394
92331394
Project:
Pace Project No.:
RE:
James Carter
Catawba Valley Engineering & Testing
PO Box 2616
Hickory, NC 28603
FORMER REGAL FACILITY 17-308
Dear James Carter:
Enclosed are the analytical results for sample(s) received by the laboratory on February 27, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Nathan Simmons, Catawba Valley Engineering & Testing
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92331394001 BP-1 EPA 6010 13 PASI-AJMW, SH1
EPA 7471 1 PASI-ASER
EPA 8270 76 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92331394002 BP-2 EPA 6010 13 PASI-AJMW
EPA 7471 1 PASI-ASER
EPA 8270 81 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-1 Lab ID:92331394001 Collected:02/24/17 15:20 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony 0.80 mg/kg 03/01/17 11:01 7440-36-002/28/17 21:050.39 1
Arsenic 4.8 mg/kg 03/01/17 11:01 7440-38-202/28/17 21:050.78 1
Barium 152 mg/kg 03/01/17 11:01 7440-39-302/28/17 21:050.39 1
Beryllium 0.90 mg/kg 03/01/17 11:01 7440-41-702/28/17 21:050.078 1
Cadmium ND mg/kg 03/01/17 11:01 7440-43-902/28/17 21:050.078 1
Chromium 55.8 mg/kg 03/01/17 11:01 7440-47-302/28/17 21:050.39 1
Copper 21.7 mg/kg 03/01/17 11:01 7440-50-802/28/17 21:050.39 1
Lead 8.5 mg/kg 03/01/17 11:01 7439-92-102/28/17 21:050.39 1
Nickel 50.9 mg/kg 03/01/17 11:01 7440-02-002/28/17 21:050.39 1
Selenium 3.0 mg/kg 03/01/17 11:01 7782-49-202/28/17 21:050.78 1
Silver ND mg/kg 03/01/17 11:01 7440-22-402/28/17 21:050.39 1
Thallium ND mg/kg 03/01/17 14:00 7440-28-002/28/17 21:050.78 1
Zinc 104 mg/kg 03/01/17 11:01 7440-66-602/28/17 21:050.78 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.0090 mg/kg 03/02/17 04:48 7439-97-603/01/17 03:000.0054 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 03/01/17 16:01 83-32-902/28/17 11:453831
Acenaphthylene ND ug/kg 03/01/17 16:01 208-96-8 M102/28/17 11:453831
Aniline ND ug/kg 03/01/17 16:01 62-53-302/28/17 11:453831
Anthracene ND ug/kg 03/01/17 16:01 120-12-702/28/17 11:453831
Benzo(a)anthracene ND ug/kg 03/01/17 16:01 56-55-302/28/17 11:453831
Benzo(a)pyrene ND ug/kg 03/01/17 16:01 50-32-802/28/17 11:453831
Benzo(b)fluoranthene ND ug/kg 03/01/17 16:01 205-99-202/28/17 11:453831
Benzo(g,h,i)perylene ND ug/kg 03/01/17 16:01 191-24-202/28/17 11:453831
Benzo(k)fluoranthene ND ug/kg 03/01/17 16:01 207-08-902/28/17 11:453831
Benzoic Acid ND ug/kg 03/01/17 16:01 65-85-002/28/17 11:4519201
Benzyl alcohol ND ug/kg 03/01/17 16:01 100-51-6 M102/28/17 11:457671
4-Bromophenylphenyl ether ND ug/kg 03/01/17 16:01 101-55-3 M102/28/17 11:453831
Butylbenzylphthalate ND ug/kg 03/01/17 16:01 85-68-702/28/17 11:453831
4-Chloro-3-methylphenol ND ug/kg 03/01/17 16:01 59-50-702/28/17 11:457671
4-Chloroaniline ND ug/kg 03/01/17 16:01 106-47-802/28/17 11:4519201
bis(2-Chloroethoxy)methane ND ug/kg 03/01/17 16:01 111-91-102/28/17 11:453831
bis(2-Chloroethyl) ether ND ug/kg 03/01/17 16:01 111-44-402/28/17 11:453831
2-Chloronaphthalene ND ug/kg 03/01/17 16:01 91-58-7 M102/28/17 11:453831
2-Chlorophenol ND ug/kg 03/01/17 16:01 95-57-802/28/17 11:453831
4-Chlorophenylphenyl ether ND ug/kg 03/01/17 16:01 7005-72-3 M102/28/17 11:453831
Chrysene ND ug/kg 03/01/17 16:01 218-01-902/28/17 11:453831
Dibenz(a,h)anthracene ND ug/kg 03/01/17 16:01 53-70-302/28/17 11:453831
Dibenzofuran ND ug/kg 03/01/17 16:01 132-64-9 M102/28/17 11:453831
1,2-Dichlorobenzene ND ug/kg 03/01/17 16:01 95-50-1 M102/28/17 11:453831
1,3-Dichlorobenzene ND ug/kg 03/01/17 16:01 541-73-1 L2,M002/28/17 11:453831
1,4-Dichlorobenzene ND ug/kg 03/01/17 16:01 106-46-7 M102/28/17 11:453831
3,3'-Dichlorobenzidine ND ug/kg 03/01/17 16:01 91-94-102/28/17 11:4519201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-1 Lab ID:92331394001 Collected:02/24/17 15:20 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 03/01/17 16:01 120-83-2 M102/28/17 11:453831
Diethylphthalate ND ug/kg 03/01/17 16:01 84-66-202/28/17 11:453831
2,4-Dimethylphenol ND ug/kg 03/01/17 16:01 105-67-902/28/17 11:453831
Dimethylphthalate ND ug/kg 03/01/17 16:01 131-11-302/28/17 11:453831
Di-n-butylphthalate ND ug/kg 03/01/17 16:01 84-74-202/28/17 11:453831
4,6-Dinitro-2-methylphenol ND ug/kg 03/01/17 16:01 534-52-102/28/17 11:457671
2,4-Dinitrophenol ND ug/kg 03/01/17 16:01 51-28-502/28/17 11:4519201
2,4-Dinitrotoluene ND ug/kg 03/01/17 16:01 121-14-202/28/17 11:453831
2,6-Dinitrotoluene ND ug/kg 03/01/17 16:01 606-20-202/28/17 11:453831
Di-n-octylphthalate ND ug/kg 03/01/17 16:01 117-84-002/28/17 11:453831
bis(2-Ethylhexyl)phthalate ND ug/kg 03/01/17 16:01 117-81-702/28/17 11:453831
Fluoranthene ND ug/kg 03/01/17 16:01 206-44-002/28/17 11:453831
Fluorene ND ug/kg 03/01/17 16:01 86-73-7 M102/28/17 11:453831
Hexachloro-1,3-butadiene ND ug/kg 03/01/17 16:01 87-68-302/28/17 11:453831
Hexachlorobenzene ND ug/kg 03/01/17 16:01 118-74-102/28/17 11:453831
Hexachlorocyclopentadiene ND ug/kg 03/01/17 16:01 77-47-402/28/17 11:453831
Hexachloroethane ND ug/kg 03/01/17 16:01 67-72-102/28/17 11:453831
Indeno(1,2,3-cd)pyrene ND ug/kg 03/01/17 16:01 193-39-502/28/17 11:453831
Isophorone ND ug/kg 03/01/17 16:01 78-59-1 M102/28/17 11:453831
1-Methylnaphthalene ND ug/kg 03/01/17 16:01 90-12-0 M102/28/17 11:453831
2-Methylnaphthalene ND ug/kg 03/01/17 16:01 91-57-602/28/17 11:453831
2-Methylphenol(o-Cresol)ND ug/kg 03/01/17 16:01 95-48-702/28/17 11:453831
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/01/17 16:0102/28/17 11:453831
Naphthalene ND ug/kg 03/01/17 16:01 91-20-3 M102/28/17 11:453831
2-Nitroaniline ND ug/kg 03/01/17 16:01 88-74-402/28/17 11:4519201
3-Nitroaniline ND ug/kg 03/01/17 16:01 99-09-202/28/17 11:4519201
4-Nitroaniline ND ug/kg 03/01/17 16:01 100-01-602/28/17 11:457671
Nitrobenzene ND ug/kg 03/01/17 16:01 98-95-302/28/17 11:453831
2-Nitrophenol ND ug/kg 03/01/17 16:01 88-75-5 M102/28/17 11:453831
4-Nitrophenol ND ug/kg 03/01/17 16:01 100-02-702/28/17 11:4519201
N-Nitrosodimethylamine ND ug/kg 03/01/17 16:01 62-75-902/28/17 11:453831
N-Nitroso-di-n-propylamine ND ug/kg 03/01/17 16:01 621-64-7 M102/28/17 11:453831
N-Nitrosodiphenylamine ND ug/kg 03/01/17 16:01 86-30-602/28/17 11:453831
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/01/17 16:01 108-60-1 M102/28/17 11:453831
Pentachlorophenol ND ug/kg 03/01/17 16:01 87-86-502/28/17 11:4519201
Phenanthrene ND ug/kg 03/01/17 16:01 85-01-802/28/17 11:453831
Phenol ND ug/kg 03/01/17 16:0102/28/17 11:453831
Pyrene ND ug/kg 03/01/17 16:01 129-00-002/28/17 11:453831
1,2,4-Trichlorobenzene ND ug/kg 03/01/17 16:01 120-82-1 M102/28/17 11:453831
2,4,5-Trichlorophenol ND ug/kg 03/01/17 16:01 95-95-4 M102/28/17 11:453831
2,4,6-Trichlorophenol ND ug/kg 03/01/17 16:01 88-06-202/28/17 11:453831
Surrogates
Nitrobenzene-d5 (S)32 %03/01/17 16:01 4165-60-002/28/17 11:4523-110 1
2-Fluorobiphenyl (S)32 %03/01/17 16:01 321-60-802/28/17 11:4530-110 1
Terphenyl-d14 (S)49 %03/01/17 16:01 1718-51-002/28/17 11:4528-110 1
Phenol-d6 (S)31 %03/01/17 16:01 13127-88-302/28/17 11:4522-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-1 Lab ID:92331394001 Collected:02/24/17 15:20 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2-Fluorophenol (S)32 %03/01/17 16:01 367-12-402/28/17 11:4513-110 1
2,4,6-Tribromophenol (S)40 %03/01/17 16:01 118-79-602/28/17 11:4527-110 1
Tentatively Identified Compounds
Unknown 194 ug/kg 03/01/17 16:01 N02/28/17 11:451
Unknown 362 ug/kg 03/01/17 16:01 N02/28/17 11:451
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 02/27/17 18:58 67-64-11201
Benzene ND ug/kg 02/27/17 18:58 71-43-2 M16.0 1
Bromobenzene ND ug/kg 02/27/17 18:58 108-86-1 M16.0 1
Bromochloromethane ND ug/kg 02/27/17 18:58 74-97-5 M16.0 1
Bromodichloromethane ND ug/kg 02/27/17 18:58 75-27-4 M16.0 1
Bromoform ND ug/kg 02/27/17 18:58 75-25-2 M16.0 1
Bromomethane ND ug/kg 02/27/17 18:58 74-83-912.0 1
2-Butanone (MEK)ND ug/kg 02/27/17 18:58 78-93-3 M11201
n-Butylbenzene ND ug/kg 02/27/17 18:58 104-51-8 M16.0 1
sec-Butylbenzene ND ug/kg 02/27/17 18:58 135-98-8 M16.0 1
tert-Butylbenzene ND ug/kg 02/27/17 18:58 98-06-6 M16.0 1
Carbon tetrachloride ND ug/kg 02/27/17 18:58 56-23-5 M16.0 1
Chlorobenzene ND ug/kg 02/27/17 18:58 108-90-7 M16.0 1
Chloroethane ND ug/kg 02/27/17 18:58 75-00-3 M112.0 1
Chloroform ND ug/kg 02/27/17 18:58 67-66-3 M16.0 1
Chloromethane ND ug/kg 02/27/17 18:58 74-87-3 M112.0 1
2-Chlorotoluene ND ug/kg 02/27/17 18:58 95-49-8 M16.0 1
4-Chlorotoluene ND ug/kg 02/27/17 18:58 106-43-4 M16.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/27/17 18:58 96-12-8 M16.0 1
Dibromochloromethane ND ug/kg 02/27/17 18:58 124-48-1 M16.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/27/17 18:58 106-93-4 M16.0 1
Dibromomethane ND ug/kg 02/27/17 18:58 74-95-3 M16.0 1
1,2-Dichlorobenzene ND ug/kg 02/27/17 18:58 95-50-1 M16.0 1
1,3-Dichlorobenzene ND ug/kg 02/27/17 18:58 541-73-1 M16.0 1
1,4-Dichlorobenzene ND ug/kg 02/27/17 18:58 106-46-7 M16.0 1
Dichlorodifluoromethane ND ug/kg 02/27/17 18:58 75-71-8 M112.0 1
1,1-Dichloroethane ND ug/kg 02/27/17 18:58 75-34-3 M16.0 1
1,2-Dichloroethane ND ug/kg 02/27/17 18:58 107-06-2 M16.0 1
1,1-Dichloroethene ND ug/kg 02/27/17 18:58 75-35-46.0 1
cis-1,2-Dichloroethene ND ug/kg 02/27/17 18:58 156-59-2 M16.0 1
trans-1,2-Dichloroethene ND ug/kg 02/27/17 18:58 156-60-5 M16.0 1
1,2-Dichloropropane ND ug/kg 02/27/17 18:58 78-87-5 M16.0 1
1,3-Dichloropropane ND ug/kg 02/27/17 18:58 142-28-9 M16.0 1
2,2-Dichloropropane ND ug/kg 02/27/17 18:58 594-20-7 M16.0 1
1,1-Dichloropropene ND ug/kg 02/27/17 18:58 563-58-6 M16.0 1
cis-1,3-Dichloropropene ND ug/kg 02/27/17 18:58 10061-01-5 M16.0 1
trans-1,3-Dichloropropene ND ug/kg 02/27/17 18:58 10061-02-6 M16.0 1
Diisopropyl ether ND ug/kg 02/27/17 18:58 108-20-3 M16.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-1 Lab ID:92331394001 Collected:02/24/17 15:20 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Ethylbenzene ND ug/kg 02/27/17 18:58 100-41-4 M16.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/27/17 18:58 87-68-3 M16.0 1
2-Hexanone ND ug/kg 02/27/17 18:58 591-78-6 M160.0 1
Isopropylbenzene (Cumene)ND ug/kg 02/27/17 18:58 98-82-8 M16.0 1
p-Isopropyltoluene ND ug/kg 02/27/17 18:58 99-87-6 M16.0 1
Methylene Chloride ND ug/kg 02/27/17 18:58 75-09-2 M124.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/27/17 18:58 108-10-1 M160.0 1
Methyl-tert-butyl ether ND ug/kg 02/27/17 18:58 1634-04-4 M16.0 1
Naphthalene ND ug/kg 02/27/17 18:58 91-20-3 M16.0 1
n-Propylbenzene ND ug/kg 02/27/17 18:58 103-65-1 M16.0 1
Styrene ND ug/kg 02/27/17 18:58 100-42-5 M16.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/27/17 18:58 630-20-6 M16.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/27/17 18:58 79-34-5 M16.0 1
Tetrachloroethene ND ug/kg 02/27/17 18:58 127-18-4 M16.0 1
Toluene ND ug/kg 02/27/17 18:58 108-88-3 M16.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/27/17 18:58 87-61-6 M16.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/27/17 18:58 120-82-1 M16.0 1
1,1,1-Trichloroethane ND ug/kg 02/27/17 18:58 71-55-6 M16.0 1
1,1,2-Trichloroethane ND ug/kg 02/27/17 18:58 79-00-5 M16.0 1
Trichloroethene ND ug/kg 02/27/17 18:58 79-01-6 M16.0 1
Trichlorofluoromethane ND ug/kg 02/27/17 18:58 75-69-4 M16.0 1
1,2,3-Trichloropropane ND ug/kg 02/27/17 18:58 96-18-4 M16.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/27/17 18:58 95-63-6 M16.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/27/17 18:58 108-67-8 M16.0 1
Vinyl acetate ND ug/kg 02/27/17 18:58 108-05-4 M160.0 1
Vinyl chloride ND ug/kg 02/27/17 18:58 75-01-4 M112.0 1
Xylene (Total)ND ug/kg 02/27/17 18:58 1330-20-7 MS12.0 1
m&p-Xylene ND ug/kg 02/27/17 18:58 179601-23-1 M112.0 1
o-Xylene ND ug/kg 02/27/17 18:58 95-47-6 M16.0 1
Surrogates
Toluene-d8 (S)101 %02/27/17 18:58 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %02/27/17 18:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %02/27/17 18:58 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.9 %02/28/17 07:370.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-2 Lab ID:92331394002 Collected:02/24/17 15:10 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony ND mg/kg 03/01/17 14:03 7440-36-0 D302/28/17 21:050.65 2
Arsenic ND mg/kg 03/01/17 14:03 7440-38-2 D302/28/17 21:051.3 2
Barium 317 mg/kg 03/01/17 14:03 7440-39-302/28/17 21:050.65 2
Beryllium 1.4 mg/kg 03/01/17 14:03 7440-41-702/28/17 21:050.13 2
Cadmium ND mg/kg 03/01/17 14:03 7440-43-9 D302/28/17 21:050.13 2
Chromium 51.3 mg/kg 03/01/17 14:03 7440-47-302/28/17 21:050.65 2
Copper 54.2 mg/kg 03/01/17 14:03 7440-50-802/28/17 21:050.65 2
Lead 10.3 mg/kg 03/01/17 14:03 7439-92-102/28/17 21:050.65 2
Nickel 29.1 mg/kg 03/01/17 14:03 7440-02-002/28/17 21:050.65 2
Selenium 2.4 mg/kg 03/01/17 14:03 7782-49-202/28/17 21:051.3 2
Silver ND mg/kg 03/01/17 14:03 7440-22-4 D302/28/17 21:050.65 2
Thallium ND mg/kg 03/01/17 14:03 7440-28-0 D302/28/17 21:051.3 2
Zinc 111 mg/kg 03/01/17 14:03 7440-66-602/28/17 21:051.3 2
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 03/02/17 04:50 7439-97-603/01/17 03:000.0026 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 03/01/17 17:01 83-32-902/28/17 11:453851
Acenaphthylene ND ug/kg 03/01/17 17:01 208-96-802/28/17 11:453851
Aniline ND ug/kg 03/01/17 17:01 62-53-302/28/17 11:453851
Anthracene ND ug/kg 03/01/17 17:01 120-12-702/28/17 11:453851
Benzo(a)anthracene ND ug/kg 03/01/17 17:01 56-55-302/28/17 11:453851
Benzo(a)pyrene ND ug/kg 03/01/17 17:01 50-32-802/28/17 11:453851
Benzo(b)fluoranthene ND ug/kg 03/01/17 17:01 205-99-202/28/17 11:453851
Benzo(g,h,i)perylene ND ug/kg 03/01/17 17:01 191-24-202/28/17 11:453851
Benzo(k)fluoranthene ND ug/kg 03/01/17 17:01 207-08-902/28/17 11:453851
Benzoic Acid ND ug/kg 03/01/17 17:01 65-85-002/28/17 11:4519201
Benzyl alcohol ND ug/kg 03/01/17 17:01 100-51-602/28/17 11:457701
4-Bromophenylphenyl ether ND ug/kg 03/01/17 17:01 101-55-302/28/17 11:453851
Butylbenzylphthalate ND ug/kg 03/01/17 17:01 85-68-702/28/17 11:453851
4-Chloro-3-methylphenol ND ug/kg 03/01/17 17:01 59-50-702/28/17 11:457701
4-Chloroaniline ND ug/kg 03/01/17 17:01 106-47-802/28/17 11:4519201
bis(2-Chloroethoxy)methane ND ug/kg 03/01/17 17:01 111-91-102/28/17 11:453851
bis(2-Chloroethyl) ether ND ug/kg 03/01/17 17:01 111-44-402/28/17 11:453851
2-Chloronaphthalene ND ug/kg 03/01/17 17:01 91-58-702/28/17 11:453851
2-Chlorophenol ND ug/kg 03/01/17 17:01 95-57-802/28/17 11:453851
4-Chlorophenylphenyl ether ND ug/kg 03/01/17 17:01 7005-72-302/28/17 11:453851
Chrysene ND ug/kg 03/01/17 17:01 218-01-902/28/17 11:453851
Dibenz(a,h)anthracene ND ug/kg 03/01/17 17:01 53-70-302/28/17 11:453851
Dibenzofuran ND ug/kg 03/01/17 17:01 132-64-902/28/17 11:453851
1,2-Dichlorobenzene ND ug/kg 03/01/17 17:01 95-50-102/28/17 11:453851
1,3-Dichlorobenzene ND ug/kg 03/01/17 17:01 541-73-1 L202/28/17 11:453851
1,4-Dichlorobenzene ND ug/kg 03/01/17 17:01 106-46-702/28/17 11:453851
3,3'-Dichlorobenzidine ND ug/kg 03/01/17 17:01 91-94-102/28/17 11:4519201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-2 Lab ID:92331394002 Collected:02/24/17 15:10 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 03/01/17 17:01 120-83-202/28/17 11:453851
Diethylphthalate ND ug/kg 03/01/17 17:01 84-66-202/28/17 11:453851
2,4-Dimethylphenol ND ug/kg 03/01/17 17:01 105-67-902/28/17 11:453851
Dimethylphthalate ND ug/kg 03/01/17 17:01 131-11-302/28/17 11:453851
Di-n-butylphthalate ND ug/kg 03/01/17 17:01 84-74-202/28/17 11:453851
4,6-Dinitro-2-methylphenol ND ug/kg 03/01/17 17:01 534-52-102/28/17 11:457701
2,4-Dinitrophenol ND ug/kg 03/01/17 17:01 51-28-502/28/17 11:4519201
2,4-Dinitrotoluene ND ug/kg 03/01/17 17:01 121-14-202/28/17 11:453851
2,6-Dinitrotoluene ND ug/kg 03/01/17 17:01 606-20-202/28/17 11:453851
Di-n-octylphthalate ND ug/kg 03/01/17 17:01 117-84-002/28/17 11:453851
bis(2-Ethylhexyl)phthalate ND ug/kg 03/01/17 17:01 117-81-702/28/17 11:453851
Fluoranthene ND ug/kg 03/01/17 17:01 206-44-002/28/17 11:453851
Fluorene ND ug/kg 03/01/17 17:01 86-73-702/28/17 11:453851
Hexachloro-1,3-butadiene ND ug/kg 03/01/17 17:01 87-68-302/28/17 11:453851
Hexachlorobenzene ND ug/kg 03/01/17 17:01 118-74-102/28/17 11:453851
Hexachlorocyclopentadiene ND ug/kg 03/01/17 17:01 77-47-402/28/17 11:453851
Hexachloroethane ND ug/kg 03/01/17 17:01 67-72-102/28/17 11:453851
Indeno(1,2,3-cd)pyrene ND ug/kg 03/01/17 17:01 193-39-502/28/17 11:453851
Isophorone ND ug/kg 03/01/17 17:01 78-59-102/28/17 11:453851
1-Methylnaphthalene ND ug/kg 03/01/17 17:01 90-12-002/28/17 11:453851
2-Methylnaphthalene ND ug/kg 03/01/17 17:01 91-57-602/28/17 11:453851
2-Methylphenol(o-Cresol)ND ug/kg 03/01/17 17:01 95-48-702/28/17 11:453851
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/01/17 17:0102/28/17 11:453851
Naphthalene ND ug/kg 03/01/17 17:01 91-20-302/28/17 11:453851
2-Nitroaniline ND ug/kg 03/01/17 17:01 88-74-402/28/17 11:4519201
3-Nitroaniline ND ug/kg 03/01/17 17:01 99-09-202/28/17 11:4519201
4-Nitroaniline ND ug/kg 03/01/17 17:01 100-01-602/28/17 11:457701
Nitrobenzene ND ug/kg 03/01/17 17:01 98-95-302/28/17 11:453851
2-Nitrophenol ND ug/kg 03/01/17 17:01 88-75-502/28/17 11:453851
4-Nitrophenol ND ug/kg 03/01/17 17:01 100-02-702/28/17 11:4519201
N-Nitrosodimethylamine ND ug/kg 03/01/17 17:01 62-75-902/28/17 11:453851
N-Nitroso-di-n-propylamine ND ug/kg 03/01/17 17:01 621-64-702/28/17 11:453851
N-Nitrosodiphenylamine ND ug/kg 03/01/17 17:01 86-30-602/28/17 11:453851
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/01/17 17:01 108-60-102/28/17 11:453851
Pentachlorophenol ND ug/kg 03/01/17 17:01 87-86-502/28/17 11:4519201
Phenanthrene ND ug/kg 03/01/17 17:01 85-01-802/28/17 11:453851
Phenol ND ug/kg 03/01/17 17:0102/28/17 11:453851
Pyrene ND ug/kg 03/01/17 17:01 129-00-002/28/17 11:453851
1,2,4-Trichlorobenzene ND ug/kg 03/01/17 17:01 120-82-102/28/17 11:453851
2,4,5-Trichlorophenol ND ug/kg 03/01/17 17:01 95-95-402/28/17 11:453851
2,4,6-Trichlorophenol ND ug/kg 03/01/17 17:01 88-06-202/28/17 11:453851
Surrogates
Nitrobenzene-d5 (S)31 %03/01/17 17:01 4165-60-002/28/17 11:4523-110 1
2-Fluorobiphenyl (S)26 %03/01/17 17:01 321-60-8 S202/28/17 11:4530-110 1
Terphenyl-d14 (S)31 %03/01/17 17:01 1718-51-002/28/17 11:4528-110 1
Phenol-d6 (S)12 %03/01/17 17:01 13127-88-3 S202/28/17 11:4522-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-2 Lab ID:92331394002 Collected:02/24/17 15:10 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2-Fluorophenol (S)15 %03/01/17 17:01 367-12-402/28/17 11:4513-110 1
2,4,6-Tribromophenol (S)13 %03/01/17 17:01 118-79-6 S202/28/17 11:4527-110 1
Tentatively Identified Compounds
Unknown 264 ug/kg 03/01/17 17:01 N02/28/17 11:451
Tridecane, 7-hexyl-524 ug/kg 03/01/17 17:01 7225-66-3 N02/28/17 11:451
Phenol, 4,4'-methyleneb 1030 ug/kg 03/01/17 17:01 118-82-1 N02/28/17 11:451
Unknown 981 ug/kg 03/01/17 17:01 N02/28/17 11:451
Unknown 565 ug/kg 03/01/17 17:01 N02/28/17 11:451
4,4'-Ethylenebis(2,6-di 249 ug/kg 03/01/17 17:01 1516-94-5 N02/28/17 11:451
Unknown 285 ug/kg 03/01/17 17:01 N02/28/17 11:451
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 02/27/17 19:18 67-64-11041
Benzene ND ug/kg 02/27/17 19:18 71-43-25.2 1
Bromobenzene ND ug/kg 02/27/17 19:18 108-86-15.2 1
Bromochloromethane ND ug/kg 02/27/17 19:18 74-97-55.2 1
Bromodichloromethane ND ug/kg 02/27/17 19:18 75-27-45.2 1
Bromoform ND ug/kg 02/27/17 19:18 75-25-25.2 1
Bromomethane ND ug/kg 02/27/17 19:18 74-83-910.4 1
2-Butanone (MEK)ND ug/kg 02/27/17 19:18 78-93-31041
n-Butylbenzene ND ug/kg 02/27/17 19:18 104-51-85.2 1
sec-Butylbenzene ND ug/kg 02/27/17 19:18 135-98-85.2 1
tert-Butylbenzene ND ug/kg 02/27/17 19:18 98-06-65.2 1
Carbon tetrachloride ND ug/kg 02/27/17 19:18 56-23-55.2 1
Chlorobenzene ND ug/kg 02/27/17 19:18 108-90-75.2 1
Chloroethane ND ug/kg 02/27/17 19:18 75-00-310.4 1
Chloroform ND ug/kg 02/27/17 19:18 67-66-35.2 1
Chloromethane ND ug/kg 02/27/17 19:18 74-87-310.4 1
2-Chlorotoluene ND ug/kg 02/27/17 19:18 95-49-85.2 1
4-Chlorotoluene ND ug/kg 02/27/17 19:18 106-43-45.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/27/17 19:18 96-12-85.2 1
Dibromochloromethane ND ug/kg 02/27/17 19:18 124-48-15.2 1
1,2-Dibromoethane (EDB)ND ug/kg 02/27/17 19:18 106-93-45.2 1
Dibromomethane ND ug/kg 02/27/17 19:18 74-95-35.2 1
1,2-Dichlorobenzene ND ug/kg 02/27/17 19:18 95-50-15.2 1
1,3-Dichlorobenzene ND ug/kg 02/27/17 19:18 541-73-15.2 1
1,4-Dichlorobenzene ND ug/kg 02/27/17 19:18 106-46-75.2 1
Dichlorodifluoromethane ND ug/kg 02/27/17 19:18 75-71-810.4 1
1,1-Dichloroethane ND ug/kg 02/27/17 19:18 75-34-35.2 1
1,2-Dichloroethane ND ug/kg 02/27/17 19:18 107-06-25.2 1
1,1-Dichloroethene ND ug/kg 02/27/17 19:18 75-35-45.2 1
cis-1,2-Dichloroethene ND ug/kg 02/27/17 19:18 156-59-25.2 1
trans-1,2-Dichloroethene ND ug/kg 02/27/17 19:18 156-60-55.2 1
1,2-Dichloropropane ND ug/kg 02/27/17 19:18 78-87-55.2 1
1,3-Dichloropropane ND ug/kg 02/27/17 19:18 142-28-95.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Sample:BP-2 Lab ID:92331394002 Collected:02/24/17 15:10 Received:02/27/17 08:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
2,2-Dichloropropane ND ug/kg 02/27/17 19:18 594-20-75.2 1
1,1-Dichloropropene ND ug/kg 02/27/17 19:18 563-58-65.2 1
cis-1,3-Dichloropropene ND ug/kg 02/27/17 19:18 10061-01-55.2 1
trans-1,3-Dichloropropene ND ug/kg 02/27/17 19:18 10061-02-65.2 1
Diisopropyl ether ND ug/kg 02/27/17 19:18 108-20-35.2 1
Ethylbenzene ND ug/kg 02/27/17 19:18 100-41-45.2 1
Hexachloro-1,3-butadiene ND ug/kg 02/27/17 19:18 87-68-35.2 1
2-Hexanone ND ug/kg 02/27/17 19:18 591-78-652.1 1
Isopropylbenzene (Cumene)ND ug/kg 02/27/17 19:18 98-82-85.2 1
p-Isopropyltoluene ND ug/kg 02/27/17 19:18 99-87-65.2 1
Methylene Chloride ND ug/kg 02/27/17 19:18 75-09-220.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/27/17 19:18 108-10-152.1 1
Methyl-tert-butyl ether ND ug/kg 02/27/17 19:18 1634-04-45.2 1
Naphthalene ND ug/kg 02/27/17 19:18 91-20-35.2 1
n-Propylbenzene ND ug/kg 02/27/17 19:18 103-65-15.2 1
Styrene ND ug/kg 02/27/17 19:18 100-42-55.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/27/17 19:18 630-20-65.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/27/17 19:18 79-34-55.2 1
Tetrachloroethene ND ug/kg 02/27/17 19:18 127-18-45.2 1
Toluene ND ug/kg 02/27/17 19:18 108-88-35.2 1
1,2,3-Trichlorobenzene ND ug/kg 02/27/17 19:18 87-61-65.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/27/17 19:18 120-82-15.2 1
1,1,1-Trichloroethane ND ug/kg 02/27/17 19:18 71-55-65.2 1
1,1,2-Trichloroethane ND ug/kg 02/27/17 19:18 79-00-55.2 1
Trichloroethene ND ug/kg 02/27/17 19:18 79-01-65.2 1
Trichlorofluoromethane ND ug/kg 02/27/17 19:18 75-69-45.2 1
1,2,3-Trichloropropane ND ug/kg 02/27/17 19:18 96-18-45.2 1
1,2,4-Trimethylbenzene ND ug/kg 02/27/17 19:18 95-63-65.2 1
1,3,5-Trimethylbenzene ND ug/kg 02/27/17 19:18 108-67-85.2 1
Vinyl acetate ND ug/kg 02/27/17 19:18 108-05-452.1 1
Vinyl chloride ND ug/kg 02/27/17 19:18 75-01-410.4 1
Xylene (Total)ND ug/kg 02/27/17 19:18 1330-20-710.4 1
m&p-Xylene ND ug/kg 02/27/17 19:18 179601-23-110.4 1
o-Xylene ND ug/kg 02/27/17 19:18 95-47-65.2 1
Surrogates
Toluene-d8 (S)101 %02/27/17 19:18 2037-26-570-130 1
4-Bromofluorobenzene (S)104 %02/27/17 19:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %02/27/17 19:18 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.3 %02/28/17 07:370.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350230
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92331394001, 92331394002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1942787
Associated Lab Samples:92331394001, 92331394002
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 03/01/17 06:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1942788LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.079.083 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1942789MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92331308003
1942790
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M6,R1.06 587 75-125120 52.040.38
ug/g 0.73 0.43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350212
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92331394001, 92331394002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1942720
Associated Lab Samples:92331394001, 92331394002
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 03/01/17 10:46
Arsenic mg/kg ND 1.0 03/01/17 10:46
Barium mg/kg ND 0.50 03/01/17 10:46
Beryllium mg/kg ND 0.10 03/01/17 10:46
Cadmium mg/kg ND 0.10 03/01/17 10:46
Chromium mg/kg ND 0.50 03/01/17 10:46
Copper mg/kg ND 0.50 03/01/17 10:46
Lead mg/kg ND 0.50 03/01/17 10:46
Nickel mg/kg ND 0.50 03/01/17 10:46
Selenium mg/kg ND 1.0 03/01/17 10:46
Silver mg/kg ND 0.50 03/01/17 10:46
Thallium mg/kg ND 1.0 03/01/17 13:45
Zinc mg/kg ND 1.0 03/01/17 11:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1942721LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 49.650 99 80-120
Arsenic mg/kg 48.050 96 80-120
Barium mg/kg 49.450 99 80-120
Beryllium mg/kg 48.150 96 80-120
Cadmium mg/kg 49.350 99 80-120
Chromium mg/kg 48.050 96 80-120
Copper mg/kg 50.150 100 80-120
Lead mg/kg 48.350 97 80-120
Nickel mg/kg 48.950 98 80-120
Selenium mg/kg 48.850 98 80-120
Silver mg/kg 24.725 99 80-120
Thallium mg/kg 48.750 97 80-120
Zinc mg/kg 51.550 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1942722MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92331389001
1942723
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony mg/kg M1,R151.5 51 75-12543 4836.9 26.4 16.2
Arsenic mg/kg R151.5 81 75-12577 3536.92.6 44.2 31.0
Barium mg/kg R151.5 92 75-12594 2136.919.2 66.4 53.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
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Page 13 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1942722MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92331389001
1942723
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Beryllium mg/kg R151.5 93 75-12591 3536.9 48.2 33.7
Cadmium mg/kg R151.5 93 75-12591 3536.9ND 47.9 33.7
Chromium mg/kg R151.5 106 75-125100 2636.921.6 76.4 58.6
Copper mg/kg R151.5 103 75-125101 3336.9 56.2 40.4
Lead mg/kg R151.5 90 75-12586 3036.98.0 54.2 39.9
Nickel mg/kg R151.5 90 75-12588 3336.9 48.0 34.3
Selenium mg/kg M1,R151.5 67 75-12563 3836.91.1 35.8 24.4
Silver mg/kg R125.8 96 75-12594 3518.4ND 24.7 17.3
Thallium mg/kg R151.5 86 75-12583 3736.9 44.5 30.7
Zinc mg/kg R151.5 89 75-12588 3036.9 51.2 37.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
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Page 14 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350012
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92331394001, 92331394002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941663
Associated Lab Samples:92331394001, 92331394002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.8 02/27/17 15:01
1,1,1-Trichloroethane ug/kg ND 5.8 02/27/17 15:01
1,1,2,2-Tetrachloroethane ug/kg ND 5.8 02/27/17 15:01
1,1,2-Trichloroethane ug/kg ND 5.8 02/27/17 15:01
1,1-Dichloroethane ug/kg ND 5.8 02/27/17 15:01
1,1-Dichloroethene ug/kg ND 5.8 02/27/17 15:01
1,1-Dichloropropene ug/kg ND 5.8 02/27/17 15:01
1,2,3-Trichlorobenzene ug/kg ND 5.8 02/27/17 15:01
1,2,3-Trichloropropane ug/kg ND 5.8 02/27/17 15:01
1,2,4-Trichlorobenzene ug/kg ND 5.8 02/27/17 15:01
1,2,4-Trimethylbenzene ug/kg ND 5.8 02/27/17 15:01
1,2-Dibromo-3-chloropropane ug/kg ND 5.8 02/27/17 15:01
1,2-Dibromoethane (EDB)ug/kg ND 5.8 02/27/17 15:01
1,2-Dichlorobenzene ug/kg ND 5.8 02/27/17 15:01
1,2-Dichloroethane ug/kg ND 5.8 02/27/17 15:01
1,2-Dichloropropane ug/kg ND 5.8 02/27/17 15:01
1,3,5-Trimethylbenzene ug/kg ND 5.8 02/27/17 15:01
1,3-Dichlorobenzene ug/kg ND 5.8 02/27/17 15:01
1,3-Dichloropropane ug/kg ND 5.8 02/27/17 15:01
1,4-Dichlorobenzene ug/kg ND 5.8 02/27/17 15:01
2,2-Dichloropropane ug/kg ND 5.8 02/27/17 15:01
2-Butanone (MEK)ug/kg ND 115 02/27/17 15:01
2-Chlorotoluene ug/kg ND 5.8 02/27/17 15:01
2-Hexanone ug/kg ND 57.7 02/27/17 15:01
4-Chlorotoluene ug/kg ND 5.8 02/27/17 15:01
4-Methyl-2-pentanone (MIBK)ug/kg ND 57.7 02/27/17 15:01
Acetone ug/kg ND 115 02/27/17 15:01
Benzene ug/kg ND 5.8 02/27/17 15:01
Bromobenzene ug/kg ND 5.8 02/27/17 15:01
Bromochloromethane ug/kg ND 5.8 02/27/17 15:01
Bromodichloromethane ug/kg ND 5.8 02/27/17 15:01
Bromoform ug/kg ND 5.8 02/27/17 15:01
Bromomethane ug/kg ND 11.5 02/27/17 15:01
Carbon tetrachloride ug/kg ND 5.8 02/27/17 15:01
Chlorobenzene ug/kg ND 5.8 02/27/17 15:01
Chloroethane ug/kg ND 11.5 02/27/17 15:01
Chloroform ug/kg ND 5.8 02/27/17 15:01
Chloromethane ug/kg ND 11.5 02/27/17 15:01
cis-1,2-Dichloroethene ug/kg ND 5.8 02/27/17 15:01
cis-1,3-Dichloropropene ug/kg ND 5.8 02/27/17 15:01
Dibromochloromethane ug/kg ND 5.8 02/27/17 15:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
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Page 15 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941663
Associated Lab Samples:92331394001, 92331394002
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.8 02/27/17 15:01
Dichlorodifluoromethane ug/kg ND 11.5 02/27/17 15:01
Diisopropyl ether ug/kg ND 5.8 02/27/17 15:01
Ethylbenzene ug/kg ND 5.8 02/27/17 15:01
Hexachloro-1,3-butadiene ug/kg ND 5.8 02/27/17 15:01
Isopropylbenzene (Cumene)ug/kg ND 5.8 02/27/17 15:01
m&p-Xylene ug/kg ND 11.5 02/27/17 15:01
Methyl-tert-butyl ether ug/kg ND 5.8 02/27/17 15:01
Methylene Chloride ug/kg ND 23.1 02/27/17 15:01
n-Butylbenzene ug/kg ND 5.8 02/27/17 15:01
n-Propylbenzene ug/kg ND 5.8 02/27/17 15:01
Naphthalene ug/kg ND 5.8 02/27/17 15:01
o-Xylene ug/kg ND 5.8 02/27/17 15:01
p-Isopropyltoluene ug/kg ND 5.8 02/27/17 15:01
sec-Butylbenzene ug/kg ND 5.8 02/27/17 15:01
Styrene ug/kg ND 5.8 02/27/17 15:01
tert-Butylbenzene ug/kg ND 5.8 02/27/17 15:01
Tetrachloroethene ug/kg ND 5.8 02/27/17 15:01
Toluene ug/kg ND 5.8 02/27/17 15:01
trans-1,2-Dichloroethene ug/kg ND 5.8 02/27/17 15:01
trans-1,3-Dichloropropene ug/kg ND 5.8 02/27/17 15:01
Trichloroethene ug/kg ND 5.8 02/27/17 15:01
Trichlorofluoromethane ug/kg ND 5.8 02/27/17 15:01
Vinyl acetate ug/kg ND 57.7 02/27/17 15:01
Vinyl chloride ug/kg ND 11.5 02/27/17 15:01
Xylene (Total)ug/kg ND 11.5 02/27/17 15:01
1,2-Dichloroethane-d4 (S)%102 70-132 02/27/17 15:01
4-Bromofluorobenzene (S)%98 70-130 02/27/17 15:01
Toluene-d8 (S)%101 70-130 02/27/17 15:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941664LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 66.364.8 102 74-137
1,1,1-Trichloroethane ug/kg 66.464.8 102 67-140
1,1,2,2-Tetrachloroethane ug/kg 63.764.8 98 72-141
1,1,2-Trichloroethane ug/kg 63.564.8 98 78-138
1,1-Dichloroethane ug/kg 65.664.8 101 69-134
1,1-Dichloroethene ug/kg 70.964.8 110 67-138
1,1-Dichloropropene ug/kg 67.164.8 104 69-139
1,2,3-Trichlorobenzene ug/kg 67.764.8 105 70-146
1,2,3-Trichloropropane ug/kg 64.364.8 99 69-144
1,2,4-Trichlorobenzene ug/kg 65.064.8 100 68-148
1,2,4-Trimethylbenzene ug/kg 64.664.8 100 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941664LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 61.764.8 95 65-140
1,2-Dibromoethane (EDB)ug/kg 63.564.8 98 77-135
1,2-Dichlorobenzene ug/kg 64.664.8 100 77-141
1,2-Dichloroethane ug/kg 66.364.8 102 65-137
1,2-Dichloropropane ug/kg 64.764.8 100 72-136
1,3,5-Trimethylbenzene ug/kg 62.564.8 97 76-133
1,3-Dichlorobenzene ug/kg 63.364.8 98 74-138
1,3-Dichloropropane ug/kg 65.164.8 101 71-139
1,4-Dichlorobenzene ug/kg 62.364.8 96 76-138
2,2-Dichloropropane ug/kg 64.464.8 99 68-137
2-Butanone (MEK)ug/kg 126J130 97 58-147
2-Chlorotoluene ug/kg 64.664.8 100 73-139
2-Hexanone ug/kg 128130 99 62-145
4-Chlorotoluene ug/kg 62.964.8 97 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 128130 99 64-149
Acetone ug/kg 117J130 90 53-153
Benzene ug/kg 66.464.8 103 73-135
Bromobenzene ug/kg 64.564.8 100 75-133
Bromochloromethane ug/kg 68.264.8 105 73-134
Bromodichloromethane ug/kg 65.564.8 101 71-135
Bromoform ug/kg 63.564.8 98 66-141
Bromomethane ug/kg 60.564.8 93 53-160
Carbon tetrachloride ug/kg 64.464.8 99 60-145
Chlorobenzene ug/kg 65.864.8 102 78-130
Chloroethane ug/kg 73.164.8 113 64-149
Chloroform ug/kg 66.664.8 103 70-134
Chloromethane ug/kg 68.964.8 106 52-150
cis-1,2-Dichloroethene ug/kg 66.564.8 103 70-133
cis-1,3-Dichloropropene ug/kg 65.764.8 101 68-134
Dibromochloromethane ug/kg 65.964.8 102 71-138
Dibromomethane ug/kg 64.864.8 100 74-130
Dichlorodifluoromethane ug/kg 69.364.8 107 40-160
Diisopropyl ether ug/kg 66.464.8 102 69-141
Ethylbenzene ug/kg 65.364.8 101 75-133
Hexachloro-1,3-butadiene ug/kg 65.564.8 101 68-143
Isopropylbenzene (Cumene)ug/kg 63.564.8 98 76-143
m&p-Xylene ug/kg 128130 99 75-136
Methyl-tert-butyl ether ug/kg 65.764.8 101 68-144
Methylene Chloride ug/kg 68.964.8 106 45-154
n-Butylbenzene ug/kg 61.864.8 95 72-137
n-Propylbenzene ug/kg 63.264.8 98 76-136
Naphthalene ug/kg 70.464.8 109 68-151
o-Xylene ug/kg 65.264.8 101 76-141
p-Isopropyltoluene ug/kg 60.864.8 94 76-140
sec-Butylbenzene ug/kg 63.764.8 98 79-139
Styrene ug/kg 65.464.8 101 79-137
tert-Butylbenzene ug/kg 63.664.8 98 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941664LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 64.764.8 100 71-138
Toluene ug/kg 65.364.8 101 74-131
trans-1,2-Dichloroethene ug/kg 68.064.8 105 67-135
trans-1,3-Dichloropropene ug/kg 64.864.8 100 65-146
Trichloroethene ug/kg 62.864.8 97 67-135
Trichlorofluoromethane ug/kg 74.264.8 115 59-144
Vinyl acetate ug/kg 141130 109 40-160
Vinyl chloride ug/kg 60.864.8 94 56-141
Xylene (Total)ug/kg 193194 100 76-137
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1941967MATRIX SPIKE SAMPLE:
MSSpike
Result
92331394001
1,1,1,2-Tetrachloroethane ug/kg 39.6 M12416570-130ND
1,1,1-Trichloroethane ug/kg 40.1 M12416770-130ND
1,1,2,2-Tetrachloroethane ug/kg 36.3 M12415170-130ND
1,1,2-Trichloroethane ug/kg 39.4 M12416470-130ND
1,1-Dichloroethane ug/kg 38.6 M12416170-130ND
1,1-Dichloroethene ug/kg 42.124 175 49-180ND
1,1-Dichloropropene ug/kg 40.1 M12416770-130ND
1,2,3-Trichlorobenzene ug/kg 34.8 M12414570-130ND
1,2,3-Trichloropropane ug/kg 36.4 M12415270-130ND
1,2,4-Trichlorobenzene ug/kg 36.5 M12415270-130ND
1,2,4-Trimethylbenzene ug/kg 39.1 M12416370-130ND
1,2-Dibromo-3-chloropropane ug/kg 34.0 M12414270-130ND
1,2-Dibromoethane (EDB)ug/kg 37.4 M12415670-130ND
1,2-Dichlorobenzene ug/kg 39.1 M12416370-130ND
1,2-Dichloroethane ug/kg 38.8 M12416270-130ND
1,2-Dichloropropane ug/kg 40.3 M12416870-130ND
1,3,5-Trimethylbenzene ug/kg 38.0 M12415870-130ND
1,3-Dichlorobenzene ug/kg 38.3 M12416070-130ND
1,3-Dichloropropane ug/kg 38.6 M12416170-130ND
1,4-Dichlorobenzene ug/kg 38.7 M12416170-130ND
2,2-Dichloropropane ug/kg 38.3 M12416070-130ND
2-Butanone (MEK)ug/kg 63.3J M14813270-130ND
2-Chlorotoluene ug/kg 39.4 M12416470-130ND
2-Hexanone ug/kg 63.3 M14813270-130ND
4-Chlorotoluene ug/kg 38.7 M12416170-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 70.8 M14814870-130ND
Acetone ug/kg 59.4J48 124 70-130ND
Benzene ug/kg 42.6 M12417750-166ND
Bromobenzene ug/kg 39.5 M12416470-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
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[phone]
Page 18 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1941967MATRIX SPIKE SAMPLE:
MSSpike
Result
92331394001
Bromochloromethane ug/kg 36.4 M12415270-130ND
Bromodichloromethane ug/kg 41.8 M12417470-130ND
Bromoform ug/kg 36.7 M12415370-130ND
Bromomethane ug/kg 26.924 112 70-130ND
Carbon tetrachloride ug/kg 41.6 M12417370-130ND
Chlorobenzene ug/kg 40.8 M12417043-169ND
Chloroethane ug/kg 44.4 M12418570-130ND
Chloroform ug/kg 39.6 M12416570-130ND
Chloromethane ug/kg 44.4 M12418470-130ND
cis-1,2-Dichloroethene ug/kg 39.4 M12416470-130ND
cis-1,3-Dichloropropene ug/kg 40.7 M12417070-130ND
Dibromochloromethane ug/kg 38.5 M12416070-130ND
Dibromomethane ug/kg 40.4 M12416870-130ND
Dichlorodifluoromethane ug/kg 40.6 M12416970-130ND
Diisopropyl ether ug/kg 37.1 M12415570-130ND
Ethylbenzene ug/kg 39.8 M12416670-130ND
Hexachloro-1,3-butadiene ug/kg 34.3 M12414370-130ND
Isopropylbenzene (Cumene)ug/kg 38.5 M12416170-130ND
m&p-Xylene ug/kg 78.1 M14816370-130ND
Methyl-tert-butyl ether ug/kg 37.0 M12415470-130ND
Methylene Chloride ug/kg 46.2 M12417670-130ND
n-Butylbenzene ug/kg 36.7 M12415370-130ND
n-Propylbenzene ug/kg 38.6 M12416170-130ND
Naphthalene ug/kg 35.8 M12414970-130ND
o-Xylene ug/kg 39.4 M12416470-130ND
p-Isopropyltoluene ug/kg 36.5 M12415270-130ND
sec-Butylbenzene ug/kg 38.5 M12416170-130ND
Styrene ug/kg 38.9 M12416270-130ND
tert-Butylbenzene ug/kg 39.1 M12416370-130ND
Tetrachloroethene ug/kg 40.4 M12416870-130ND
Toluene ug/kg 41.8 M12417452-163ND
trans-1,2-Dichloroethene ug/kg 39.9 M12416670-130ND
trans-1,3-Dichloropropene ug/kg 40.3 M12416870-130ND
Trichloroethene ug/kg 41.7 M12417449-167ND
Trichlorofluoromethane ug/kg 45.5 M12418970-130ND
Vinyl acetate ug/kg 32.5J M1486870-130ND
Vinyl chloride ug/kg 36.0 M12415070-130ND
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92331384001
1941966SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
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Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92331384001
1941966SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92331384001
1941966SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg 3.8JND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg 2.9JND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%100 17114
4-Bromofluorobenzene (S)%98 7100
Toluene-d8 (S)%98 7100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350143
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92331394001, 92331394002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1942194
Associated Lab Samples:92331394001, 92331394002
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 03/01/17 14:32
1,2-Dichlorobenzene ug/kg ND 330 03/01/17 14:32
1,3-Dichlorobenzene ug/kg ND 330 03/01/17 14:32
1,4-Dichlorobenzene ug/kg ND 330 03/01/17 14:32
1-Methylnaphthalene ug/kg ND 330 03/01/17 14:32
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 03/01/17 14:32
2,4,5-Trichlorophenol ug/kg ND 330 03/01/17 14:32
2,4,6-Trichlorophenol ug/kg ND 330 03/01/17 14:32
2,4-Dichlorophenol ug/kg ND 330 03/01/17 14:32
2,4-Dimethylphenol ug/kg ND 330 03/01/17 14:32
2,4-Dinitrophenol ug/kg ND 1650 03/01/17 14:32
2,4-Dinitrotoluene ug/kg ND 330 03/01/17 14:32
2,6-Dinitrotoluene ug/kg ND 330 03/01/17 14:32
2-Chloronaphthalene ug/kg ND 330 03/01/17 14:32
2-Chlorophenol ug/kg ND 330 03/01/17 14:32
2-Methylnaphthalene ug/kg ND 330 03/01/17 14:32
2-Methylphenol(o-Cresol)ug/kg ND 330 03/01/17 14:32
2-Nitroaniline ug/kg ND 1650 03/01/17 14:32
2-Nitrophenol ug/kg ND 330 03/01/17 14:32
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 03/01/17 14:32
3,3'-Dichlorobenzidine ug/kg ND 1650 03/01/17 14:32
3-Nitroaniline ug/kg ND 1650 03/01/17 14:32
4,6-Dinitro-2-methylphenol ug/kg ND 660 03/01/17 14:32
4-Bromophenylphenyl ether ug/kg ND 330 03/01/17 14:32
4-Chloro-3-methylphenol ug/kg ND 660 03/01/17 14:32
4-Chloroaniline ug/kg ND 1650 03/01/17 14:32
4-Chlorophenylphenyl ether ug/kg ND 330 03/01/17 14:32
4-Nitroaniline ug/kg ND 660 03/01/17 14:32
4-Nitrophenol ug/kg ND 1650 03/01/17 14:32
Acenaphthene ug/kg ND 330 03/01/17 14:32
Acenaphthylene ug/kg ND 330 03/01/17 14:32
Aniline ug/kg ND 330 03/01/17 14:32
Anthracene ug/kg ND 330 03/01/17 14:32
Benzo(a)anthracene ug/kg ND 330 03/01/17 14:32
Benzo(a)pyrene ug/kg ND 330 03/01/17 14:32
Benzo(b)fluoranthene ug/kg ND 330 03/01/17 14:32
Benzo(g,h,i)perylene ug/kg ND 330 03/01/17 14:32
Benzo(k)fluoranthene ug/kg ND 330 03/01/17 14:32
Benzoic Acid ug/kg ND 1650 03/01/17 14:32
Benzyl alcohol ug/kg ND 660 03/01/17 14:32
bis(2-Chloroethoxy)methane ug/kg ND 330 03/01/17 14:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1942194
Associated Lab Samples:92331394001, 92331394002
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 330 03/01/17 14:32
bis(2-Ethylhexyl)phthalate ug/kg ND 330 03/01/17 14:32
Butylbenzylphthalate ug/kg ND 330 03/01/17 14:32
Chrysene ug/kg ND 330 03/01/17 14:32
Di-n-butylphthalate ug/kg ND 330 03/01/17 14:32
Di-n-octylphthalate ug/kg ND 330 03/01/17 14:32
Dibenz(a,h)anthracene ug/kg ND 330 03/01/17 14:32
Dibenzofuran ug/kg ND 330 03/01/17 14:32
Diethylphthalate ug/kg ND 330 03/01/17 14:32
Dimethylphthalate ug/kg ND 330 03/01/17 14:32
Fluoranthene ug/kg ND 330 03/01/17 14:32
Fluorene ug/kg ND 330 03/01/17 14:32
Hexachloro-1,3-butadiene ug/kg ND 330 03/01/17 14:32
Hexachlorobenzene ug/kg ND 330 03/01/17 14:32
Hexachlorocyclopentadiene ug/kg ND 330 03/01/17 14:32
Hexachloroethane ug/kg ND 330 03/01/17 14:32
Indeno(1,2,3-cd)pyrene ug/kg ND 330 03/01/17 14:32
Isophorone ug/kg ND 330 03/01/17 14:32
N-Nitroso-di-n-propylamine ug/kg ND 330 03/01/17 14:32
N-Nitrosodimethylamine ug/kg ND 330 03/01/17 14:32
N-Nitrosodiphenylamine ug/kg ND 330 03/01/17 14:32
Naphthalene ug/kg ND 330 03/01/17 14:32
Nitrobenzene ug/kg ND 330 03/01/17 14:32
Pentachlorophenol ug/kg ND 1650 03/01/17 14:32
Phenanthrene ug/kg ND 330 03/01/17 14:32
Phenol ug/kg ND 330 03/01/17 14:32
Pyrene ug/kg ND 330 03/01/17 14:32
2,4,6-Tribromophenol (S)%44 27-110 03/01/17 14:32
2-Fluorobiphenyl (S)%48 30-110 03/01/17 14:32
2-Fluorophenol (S)%49 13-110 03/01/17 14:32
Nitrobenzene-d5 (S)%51 23-110 03/01/17 14:32
Phenol-d6 (S)%45 22-110 03/01/17 14:32
Terphenyl-d14 (S)%58 28-110 03/01/17 14:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1942195LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 9231670 55 36-120
1,2-Dichlorobenzene ug/kg 9421670 57 41-120
1,3-Dichlorobenzene ug/kg 893 L216705466-120
1,4-Dichlorobenzene ug/kg 9071670 54 42-120
1-Methylnaphthalene ug/kg 9881670 59 40-120
2,2'-Oxybis(1-chloropropane)ug/kg 9001670 54 17-120
2,4,5-Trichlorophenol ug/kg 9401670 56 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1942195LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 10801670 65 40-120
2,4-Dichlorophenol ug/kg 9761670 59 33-120
2,4-Dimethylphenol ug/kg 10901670 65 36-120
2,4-Dinitrophenol ug/kg 59108330 71 22-121
2,4-Dinitrotoluene ug/kg 13101670 79 60-120
2,6-Dinitrotoluene ug/kg 13301670 80 54-120
2-Chloronaphthalene ug/kg 10101670 61 41-120
2-Chlorophenol ug/kg 9991670 60 39-120
2-Methylnaphthalene ug/kg 10401670 62 26-120
2-Methylphenol(o-Cresol)ug/kg 8921670 53 41-120
2-Nitroaniline ug/kg 22103330 66 45-120
2-Nitrophenol ug/kg 11001670 66 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 9021670 54 35-120
3,3'-Dichlorobenzidine ug/kg 17803330 53 16-125
3-Nitroaniline ug/kg 22703330 68 45-120
4,6-Dinitro-2-methylphenol ug/kg 24103330 72 46-120
4-Bromophenylphenyl ether ug/kg 10501670 63 36-120
4-Chloro-3-methylphenol ug/kg 21803330 66 37-120
4-Chloroaniline ug/kg 19903330 60 35-120
4-Chlorophenylphenyl ether ug/kg 10101670 60 30-120
4-Nitroaniline ug/kg 23403330 70 48-120
4-Nitrophenol ug/kg 51708330 62 43-120
Acenaphthene ug/kg 10701670 64 46-120
Acenaphthylene ug/kg 10801670 65 46-120
Aniline ug/kg 7621670 46 33-120
Anthracene ug/kg 11101670 67 63-120
Benzo(a)anthracene ug/kg 11101670 67 61-120
Benzo(a)pyrene ug/kg 11601670 70 59-120
Benzo(b)fluoranthene ug/kg 10901670 66 55-120
Benzo(g,h,i)perylene ug/kg 10701670 64 57-120
Benzo(k)fluoranthene ug/kg 12401670 75 56-120
Benzoic Acid ug/kg 44108330 53 13-120
Benzyl alcohol ug/kg 18903330 57 34-120
bis(2-Chloroethoxy)methane ug/kg 9301670 56 21-120
bis(2-Chloroethyl) ether ug/kg 9171670 55 25-120
bis(2-Ethylhexyl)phthalate ug/kg 13601670 82 56-123
Butylbenzylphthalate ug/kg 13701670 82 57-120
Chrysene ug/kg 11401670 68 64-120
Di-n-butylphthalate ug/kg 12401670 75 58-120
Di-n-octylphthalate ug/kg 12401670 74 47-121
Dibenz(a,h)anthracene ug/kg 11001670 66 56-120
Dibenzofuran ug/kg 10601670 64 43-120
Diethylphthalate ug/kg 12601670 75 55-120
Dimethylphthalate ug/kg 11801670 71 54-120
Fluoranthene ug/kg 10901670 65 61-120
Fluorene ug/kg 11201670 67 51-120
Hexachloro-1,3-butadiene ug/kg 9201670 55 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1942195LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 10801670 65 53-120
Hexachlorocyclopentadiene ug/kg 9431670 57 18-150
Hexachloroethane ug/kg 9021670 54 39-120
Indeno(1,2,3-cd)pyrene ug/kg 11601670 70 58-120
Isophorone ug/kg 11401670 68 38-120
N-Nitroso-di-n-propylamine ug/kg 9171670 55 30-120
N-Nitrosodimethylamine ug/kg 10101670 61 32-120
N-Nitrosodiphenylamine ug/kg 11001670 66 50-120
Naphthalene ug/kg 10101670 61 38-120
Nitrobenzene ug/kg 10601670 64 37-120
Pentachlorophenol ug/kg 25903330 78 10-120
Phenanthrene ug/kg 11301670 68 62-120
Phenol ug/kg 10701670 64 37-120
Pyrene ug/kg 11301670 68 63-120
2,4,6-Tribromophenol (S)%76 27-110
2-Fluorobiphenyl (S)%59 30-110
2-Fluorophenol (S)%58 13-110
Nitrobenzene-d5 (S)%57 23-110
Phenol-d6 (S)%59 22-110
Terphenyl-d14 (S)%73 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1942196MATRIX SPIKE SAMPLE:
MSSpike
Result
92331394001
1,2,4-Trichlorobenzene ug/kg 327J M119401718-119ND
1,2-Dichlorobenzene ug/kg 370J M119401950-110ND
1,3-Dichlorobenzene ug/kg 361J M019401927-110ND
1,4-Dichlorobenzene ug/kg 360J M119401928-110ND
1-Methylnaphthalene ug/kg 358J M119401824-116ND
2,2'-Oxybis(1-chloropropane)ug/kg 334J M119401750-150ND
2,4,5-Trichlorophenol ug/kg 458 M119402428-110ND
2,4,6-Trichlorophenol ug/kg 4531940 23 17-117ND
2,4-Dichlorophenol ug/kg 314J M119401621-128ND
2,4-Dimethylphenol ug/kg 3841940 20 10-120ND
2,4-Dinitrophenol ug/kg 31309680 32 10-107ND
2,4-Dinitrotoluene ug/kg 7561940 39 36-109ND
2,6-Dinitrotoluene ug/kg 6731940 35 32-110ND
2-Chloronaphthalene ug/kg 419 M119402230-107ND
2-Chlorophenol ug/kg 353J1940 18 14-106ND
2-Methylnaphthalene ug/kg 3941940 20 10-135ND
2-Methylphenol(o-Cresol)ug/kg 351J1940 18 10-124ND
2-Nitroaniline ug/kg 1140J3870 29 26-116ND
2-Nitrophenol ug/kg 359J M119401928-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 309J1940 16 10-109ND
3,3'-Dichlorobenzidine ug/kg 1060J3870 27 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1942196MATRIX SPIKE SAMPLE:
MSSpike
Result
92331394001
3-Nitroaniline ug/kg 1230J3870 32 22-110ND
4,6-Dinitro-2-methylphenol ug/kg 13503870 35 13-121ND
4-Bromophenylphenyl ether ug/kg 577 M119403031-109ND
4-Chloro-3-methylphenol ug/kg 9413870 24 13-128ND
4-Chloroaniline ug/kg 771J3870 20 18-102ND
4-Chlorophenylphenyl ether ug/kg 516 M119402729-112ND
4-Nitroaniline ug/kg 13203870 34 16-111ND
4-Nitrophenol ug/kg 28509680 29 14-135ND
Acenaphthene ug/kg 5001940 26 26-114ND
Acenaphthylene ug/kg 493 M119402532-108ND
Aniline ug/kg 244J1940 13 10-107ND
Anthracene ug/kg 6631940 34 32-111ND
Benzo(a)anthracene ug/kg 6591940 34 25-117ND
Benzo(a)pyrene ug/kg 6911940 36 25-106ND
Benzo(b)fluoranthene ug/kg 6471940 33 24-110ND
Benzo(g,h,i)perylene ug/kg 6181940 32 19-112ND
Benzo(k)fluoranthene ug/kg 7551940 39 24-114ND
Benzoic Acid ug/kg 1100J9680 11 10-110ND
Benzyl alcohol ug/kg 743J M138701924-106ND
bis(2-Chloroethoxy)methane ug/kg 323J1940 17 13-119ND
bis(2-Chloroethyl) ether ug/kg 356J1940 18 10-134ND
bis(2-Ethylhexyl)phthalate ug/kg 7331940 38 10-125ND
Butylbenzylphthalate ug/kg 7481940 39 18-110ND
Chrysene ug/kg 6751940 35 30-110ND
Di-n-butylphthalate ug/kg 7051940 36 19-112ND
Di-n-octylphthalate ug/kg 6361940 33 17-105ND
Dibenz(a,h)anthracene ug/kg 6451940 33 23-111ND
Dibenzofuran ug/kg 531 M119402735-103ND
Diethylphthalate ug/kg 7211940 37 27-113ND
Dimethylphthalate ug/kg 6971940 36 26-111ND
Fluoranthene ug/kg 6351940 33 33-109ND
Fluorene ug/kg 600 M119403132-113ND
Hexachloro-1,3-butadiene ug/kg 311J1940 16 16-116ND
Hexachlorobenzene ug/kg 6281940 32 27-120ND
Hexachlorocyclopentadiene ug/kg 296J1940 15 10-108ND
Hexachloroethane ug/kg 349J1940 18 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 6881940 36 10-122ND
Isophorone ug/kg 434 M119402228-114ND
N-Nitroso-di-n-propylamine ug/kg 355J M119401827-113ND
N-Nitrosodimethylamine ug/kg 344J1940 18 10-109ND
N-Nitrosodiphenylamine ug/kg 6171940 32 10-128ND
Naphthalene ug/kg 379J M119402025-110ND
Nitrobenzene ug/kg 3841940 20 18-114ND
Pentachlorophenol ug/kg 1380J3870 36 10-122ND
Phenanthrene ug/kg 6711940 35 30-114ND
Phenol ug/kg 3971940 21 11-102ND
Pyrene ug/kg 6701940 35 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1942196MATRIX SPIKE SAMPLE:
MSSpike
Result
92331394001
2,4,6-Tribromophenol (S)%34 27-110
2-Fluorobiphenyl (S)%S02030-110
2-Fluorophenol (S)%17 13-110
Nitrobenzene-d5 (S)%S01723-110
Phenol-d6 (S)%S01822-110
Terphenyl-d14 (S)%36 28-110
Parameter Units
Dup
Result QualifiersRPDResult
92331394001
1942197SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
1-Methylnaphthalene ug/kg NDND
2,2'-Oxybis(1-chloropropane)ug/kg NDND
2,4,5-Trichlorophenol ug/kg NDND
2,4,6-Trichlorophenol ug/kg NDND
2,4-Dichlorophenol ug/kg NDND
2,4-Dimethylphenol ug/kg NDND
2,4-Dinitrophenol ug/kg NDND
2,4-Dinitrotoluene ug/kg NDND
2,6-Dinitrotoluene ug/kg NDND
2-Chloronaphthalene ug/kg NDND
2-Chlorophenol ug/kg NDND
2-Methylnaphthalene ug/kg NDND
2-Methylphenol(o-Cresol)ug/kg NDND
2-Nitroaniline ug/kg NDND
2-Nitrophenol ug/kg NDND
3&4-Methylphenol(m&p Cresol)ug/kg NDND
3,3'-Dichlorobenzidine ug/kg NDND
3-Nitroaniline ug/kg NDND
4,6-Dinitro-2-methylphenol ug/kg NDND
4-Bromophenylphenyl ether ug/kg NDND
4-Chloro-3-methylphenol ug/kg NDND
4-Chloroaniline ug/kg NDND
4-Chlorophenylphenyl ether ug/kg NDND
4-Nitroaniline ug/kg NDND
4-Nitrophenol ug/kg NDND
Acenaphthene ug/kg NDND
Acenaphthylene ug/kg NDND
Aniline ug/kg NDND
Anthracene ug/kg NDND
Benzo(a)anthracene ug/kg NDND
Benzo(a)pyrene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92331394001
1942197SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg NDND
Benzo(g,h,i)perylene ug/kg NDND
Benzo(k)fluoranthene ug/kg NDND
Benzoic Acid ug/kg NDND
Benzyl alcohol ug/kg NDND
bis(2-Chloroethoxy)methane ug/kg NDND
bis(2-Chloroethyl) ether ug/kg NDND
bis(2-Ethylhexyl)phthalate ug/kg NDND
Butylbenzylphthalate ug/kg NDND
Chrysene ug/kg NDND
Di-n-butylphthalate ug/kg NDND
Di-n-octylphthalate ug/kg NDND
Dibenz(a,h)anthracene ug/kg NDND
Dibenzofuran ug/kg NDND
Diethylphthalate ug/kg NDND
Dimethylphthalate ug/kg NDND
Fluoranthene ug/kg NDND
Fluorene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Hexachlorobenzene ug/kg NDND
Hexachlorocyclopentadiene ug/kg NDND
Hexachloroethane ug/kg NDND
Indeno(1,2,3-cd)pyrene ug/kg NDND
Isophorone ug/kg NDND
N-Nitroso-di-n-propylamine ug/kg NDND
N-Nitrosodimethylamine ug/kg NDND
N-Nitrosodiphenylamine ug/kg NDND
Naphthalene ug/kg NDND
Nitrobenzene ug/kg NDND
Pentachlorophenol ug/kg NDND
Phenanthrene ug/kg NDND
Phenol ug/kg NDND
Pyrene ug/kg NDND
2,4,6-Tribromophenol (S)%3 S017640
2-Fluorobiphenyl (S)%18 S05532
2-Fluorophenol (S)%7 S012432
Nitrobenzene-d5 (S)%20 S04332
Phenol-d6 (S)%5 S014331
Terphenyl-d14 (S)%19 S08849
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349958
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92331394001, 92331394002
Parameter Units
Dup
Result QualifiersRPDResult
92331215001
1941354SAMPLE DUPLICATE:
Percent Moisture %21.5 622.8
Parameter Units
Dup
Result QualifiersRPDResult
92331358002
1941355SAMPLE DUPLICATE:
Percent Moisture %93.1 093.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
Tentatively identified compound (TIC) based on mass spectral library search. Result is estimated.N
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92331394
FORMER REGAL FACILITY 17-308
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92331394001 350212 350237BP-1 EPA 3050 EPA 6010
92331394002 350212 350237BP-2 EPA 3050 EPA 6010
92331394001 350230 350253BP-1 EPA 7471 EPA 7471
92331394002 350230 350253BP-2 EPA 7471 EPA 7471
92331394001 350143 350326BP-1 EPA 3546 EPA 8270
92331394002 350143 350326BP-2 EPA 3546 EPA 8270
92331394001 350012BP-1 EPA 8260
92331394002 350012BP-2 EPA 8260
92331394001 349958BP-1 ASTM D2974-87
92331394002 349958BP-2 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/02/2017 05:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 34
Page 32 of 34
pee Analytical'
Document Name: Document Revised: Sept. 21, 2016
Sample Condit ion Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR·CS-033-Rev.01 Pace Quality Office
Laboratory receiving samples:
Asheville D EdenD Greenwood D Huntersville ~ Raleigh0 MechanicsvilleO
Sample Condition Upon
Receipt
. \),, ~~().,J ~~ o/{ciQ;~~
CUentName, Col~ <A.r'l roject l lJQ#: 92331394
Courier:
D Commercial
Custody Seal Present?
Packing Material:
Thermometer:
O IRGun ID:
0Fed Ex
0 Pace
O ves ~No
0 Bubble Wrap
---r,l~D'.2)
0UPS 0USPS
O other: __
Seals Intact? O ves
~Bubble Bags 0 None
l'iilwet Type of Ice: i"'
Correction Factor: Cooler Temp Corrected (0C): (·'?(c oC
Temp should be above freezing to 6°C
USDA Regulated Soil ( D N/A, water sample)
J6lclient II I Ill 1111111111111111
92331394
~ No Date/Initials Person Examining ContenJ"( X-f L-( { ( (
O other: __
0 Blue 0 None O samples on ice, cooling process has begun
Biological Tissue Frozen? O ves ~No O N/A
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
[XI No O ves rl'INo
I
Chain of Custody Present?
Samples Arrived within Hold Time? -
Short Hold Time Analysis (<72 hr.)?
Rush Turn Around Time Requested? ----
Sufficient Volume?
Correct Containers Used?
-Pace Containers used?
Containers Intact?
Samples Field Filtered?
Sample Labels Match COC? f cf1} / -Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>S-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review :
I
including Hawaii and Puerto Rico)? O ves
Comments/Discrepancy:
~Yes 0 No O N/A 1. -
00Yes 0 No ON/A 2. ..
IXIYes 0 No O N/A 3.
I
lfJYes 0 No O N/A 4. •.
IXJYes 0 No O N/A 5.
'iKJYes 0 No O N/A 6.
[i]Yes 0 No ON/A
I
~Yes 0 No O N/A 7.
[
O ves (i]No O N/A 8. Note if sediment is visible in the dissolved container
I
JK]Yes 0 No O N/A 9. ...
O ves (]No O N/A 10.
O ves ~No O N/A 11.
O ves \JNo O N/A
( Field Data Required? Oves 0No
Date/Time:
pate: 1 ____ Zf:_2._7=-------
Date: 7-/z7
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 33 of 34
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