20054_Carolina Foundry_Brownfields Assessment Report_20170314

BROWNFIELDS ASSESSMENT
REPORT
Carolina Foundry Brownfields Site
NCBP #20054-16-60
224-232 West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
March 14, 2017
Terracon Project No. 71167563
Prepared for:
Barringer Capital, LLC
Charlotte, North Carolina
Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina
Artist’s rendition of completed project:
TABLE OF CONTENTS
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1.0 SITE DESCRIPTION ....................................................................................................... 1
1.1 General Site Description ...................................................................................... 1
1.2 Site History .......................................................................................................... 1
1.3 Preliminary Redevelopment Plans ....................................................................... 3
2.0 SCOPE OF SERVICES ................................................................................................... 3
2.1 Reliance ............................................................................................................... 4
3.0 FIELD INVESTIGATION METHODS ............................................................................... 4
3.1 Temporary Well Installation .................................................................................. 4
3.2 Groundwater Sampling ........................................................................................ 5
3.3 Soil Sampling ....................................................................................................... 6
3.4 Soil Vapor Sample Point Installation .................................................................... 7
3.5 Soil Vapor Sampling ............................................................................................ 8
3.6 Brownfields Receptor Survey ............................................................................... 8
4.0 RESULTS ....................................................................................................................... 9
4.1 Site Hydrogeology ................................................................................................ 9
4.2 Groundwater Sample Results .............................................................................. 9
4.3 Soil Sample Results ........................................................................................... 10
4.4 Soil Vapor Sample Results ................................................................................ 12
5.0 CONCLUSIONS AND RECOMMENDATIONS ............................................................. 13
Tables
Table 1 – Sampling and Analysis Plan
Table 2 – Soil Sample Analytical Results
Table 3 – Groundwater Elevations
Table 4 – Groundwater Sample Analytical Results
Table 5 – Soil Vapor Sample Analytical Results
Figures
Figure 1 – Site Overview Map
Figure 2 – Historical Site Layout and Sample Location Map
Figure 3 – Groundwater Elevation Map
Figure 4 – Soil Sample Analytical Results Map
Figure 5 – Groundwater Sample Analytical Results Map
Figure 6 – Soil Vapor Sample Analytical Results Map
Figure 7 – Preliminary Future Site Layout Map
Appendices
APPENDIX A – FIELD FORMS, SOIL BORING LOGS, AND RECEPTOR SURVEY
Soil Boring Logs
Groundwater Sample Collection Records
Soil Vapor Sample Collection Record
Brownfields Receptor Survey Form
APPENDIX B – LABORATORY ANALYTICAL REPORTS
Groundwater Sample Analytical Report – Pace Analytical
Soil Sample Analytical Report – Pace Analytical
Soil Vapor Sample Analytical Report – Eurofins AirToxics
TABLE OF CONTENTS (CONTINUED)
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APPENDIX C – BROWNFIELDS RISK CALCULATORS
Brownfields Soil Risk Calculators (Residential)
Brownfields Groundwater Concentration to Indoor Air Risk Calculator (Residential)
Brownfields Soil Vapor Concentration to Indoor Air Concentration Risk Calculator
(Residential)
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BROWNFIELDS ASSESSMENT REPORT
CAROLINA FOUNDRY BROWNFIELDS SITE
NCBP #20054-16-60
224-232 WEST TREMONT AVENUE
CHARLOTTE, NORTH CAROLINA
Terracon Project No. 71167563
March 14, 2017
1.0 SITE DESCRIPTION
1.1 General Site Description
The Carolina Foundry Brownfields site is located at 224-232 West Tremont Avenue in Charlotte,
North Carolina. The site encompasses three contiguous parcels (Mecklenburg County Tax Parcel
Nos. 12103308, 12103309 and 12103310) for a total area of approximately 0.75 acres. The
Carolina Foundry site is generally bound to the south by West Tremont Avenue while the
surrounding properties are developed as industrial/commercial. According to the National
Wetland Inventory (NWI) online database, the nearest surface water feature is an unnamed
tributary of Irwin Creek, located approximately 600 feet north of the site. The site as shown on
Figure 1 was accepted into the North Carolina Brownfields Program on August 2, 2016 with
Barringer Capital, LLC identified as the prospective developer (PD).
1.2 Site History
Terracon performed a review of historical documents available for the site, including a Phase I
Environmental Site Assessment (ESA) completed by Geoscience Group, Inc. (Geoscience) in
2015 for the former foundry facility. Terracon also reviewed available aerial photographs to gain
a general understanding of the development history of the property. The history of the site is
discussed below.
Two of the on-site parcels (12103309 and 12103310) consist of a single-story building that was
formerly occupied by Carolina Foundry, which operated as an aluminum, brass, and copper
casting facility. The third parcel (12103308) contains a separate single-story building that was
used for storage. According to the 2015 Phase I ESA by Geoscience, the storage building was
constructed in the early 1990s and the foundry building was built in the mid-1950s. The foundry
was active from at least 1949. According to the historical information, the property was
undeveloped prior to approximately 1930.
In conjunction with the 2015 Phase I ESA, Geoscience collected nine soil samples beneath the
concrete floor slab of the foundry building. Samples were collected from areas of the building that
included two machine shops, adjacent to an underground heating oil storage tank, adjacent to the
foundry furnaces, and within the air compressor room where ponded oil was observed on the
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concrete floor. The 2015 sample locations are shown on Figure 2, and the sampling results are
included in Table 2 (taken from the Geoscience Phase I ESA). Note that samples were not
collected from sample locations S-3 (near the heating oil UST) and S-8 (casting area) due to
obstructions, and two samples were obtained from sample location S-5 at different depths (S-5
and S-5A).
The nine soil samples (S-1, S-2, S-4, S-5, S-5A, S-6, S-7, S-9 and S-10), were collected at depths
ranging from 1.5 to 8 feet below ground surface (bgs), and were analyzed for volatile organic
compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA
Method 8270 and RCRA metals. Petroleum-related VOCs were detected in soils near the
furnaces and the former heating oil UST at concentrations that did not exceed the Residential
Health Based Preliminary Soil Remediation Goals (PSRGs). Various SVOC constituents were
also detected in samples S-1 through S-5A. Benzo(a)pyrene, benzo(a)anthracene,
benzo(b)fluoranthene, and indeno(1,2,3-cd)pyrene) were detected in samples S-1 and S-2 above
Residential PSRGs. Samples S-1 and S-2 were obtained in the machine shop area (eastern
portion of foundry building) which is currently planned for development as an access
driveway/road (Figures 2 and 7). Other PAH compounds (naphthalene, 1-methylnaphthalene,
and 2-methylnaphthalene) were detected near the former UST and the furnaces (S-4 and/or S-
5/5A) above Protection of Groundwater PSRGs but below Residential PSRGs. Various RCRA
metals were detected in the soils at the site below residential PSRGs; however, arsenic was
detected in each sample at concentrations that exceeded the Residential or Non-Residential
PSRGs. The elevated arsenic concentrations are within the typical range of naturally occurring
arsenic in the Charlotte area (Geochemical Landscapes of the Conterminous United States —
New Map Presentations for 22 Elements, USGS, 2001).
As part of the Phase I ESA, Geoscience also collected two representative samples from the waste
foundry sand stockpiled inside the former foundry building to characterize the foundry sand for
disposal. One sample was obtained from the foundry sand stockpiled in the casting area, and
one composite sample was taken from the waste foundry sand stockpile (labeled as “Former
Waste Sand Stockpile” on Figure 2). The samples contained diesel range organics (DRO) at
2,900 mg/kg (foundry floor) and 2,000 mg/kg (waste sand stockpile). Gasoline range organics
(GRO) at 23 mg/kg and benzene, toluene, ethylbenzene, and xylenes (BTEX) were detected in
the foundry floor sample. BTEX and GRO constituents were not detected in the waste pile
sample. Toxicity Characteristic Leachate Procedure (TCLP) metals analyses from both stockpiles
indicated the presence of cadmium and lead at levels below characteristic hazardous waste
criteria. Terracon understands that the stockpiled foundry sands have been removed from the
site.
A 1,000-gallon underground heating oil storage tank was formerly located inside the foundry
building as shown on Figure 2. The tank was removed in January 2016 by Environmental
Compliance Services of NC (ECS). ECS submitted an Initial Abatement Action Report describing
the tank removal activities to the UST Section of the North Carolina Department of Environmental
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Quality (NCDEQ). According to the report, petroleum-impacted soils were detected near the tank.
After removal of the tank and impacted soils, confirmation samples were collected from the
excavation to confirm the removal of the impacted soils. Groundwater was not encountered
during the tank removal activities. Laboratory analyses of samples collected at the bottom of the
excavation approximately six feet below ground surface (bgs), detected DRO constituents at
concentrations above the current regulatory action level of 100 milligrams/kilogram (mg/kg).
VOCs and several other petroleum compounds were present in the confirmation soil samples at
levels below their respective Residential Maximum Soil Contaminant Concentrations (MSCCs).
The confirmation sample locations (SS-1 and SS-2) are shown on Figure 2, and the sampling
results are included in Table 2 (taken from the ECS Initial Abatement Action Report). Following
tank removal activities, ECS filed a Notice of Residual Petroleum for the release at the UST at
the Mecklenburg County Register of Deeds. The Notice of Residual Petroleum included a land
use restriction that prohibits the use of groundwater at the site. The NCDEQ issued a No Further
Action Letter for the UST release on March 1, 2016.
Off-Site Environmental Concerns
The former Carolina Foundry is bordered by multiple facilities that have entered into the NC
Brownfields Program. Based on topography and its location relative to the site, it is possible that
impacted groundwater from the nearby Tremont Redevelopment property (NC Brownfields
#18004-14-060) could migrate towards the site.
1.3 Preliminary Redevelopment Plans
The PD’s current redevelopment plans are to demolish the existing on-site buildings and construct
as many as 18 residential townhome units, grouped into three buildings. Redevelopment plans
also include paved access driveways, as shown on Figures 2 and 7.
2.0 SCOPE OF SERVICES
Terracon conducted the Brownfields Assessment activities in general accordance with the
Brownfields Assessment Work Plan, revised November 29, 2016, approved by the NC
Brownfields Program Project Manager on December 1, 2016. Several minor scope modifications
regarding the collection of soil samples were discussed during a meeting at the site on January
9, 2017 with Brownfields Project Managers Ms. Jordan Thompson and Ms. Carolyn Minnich due
to conditions encountered at the site. These scope modifications were approved by the
Brownfields Project Manager and documented in an addendum letter dated January 12, 2017.
The scope of services conducted at the facility included:
§Preparation of a Health and Safety Plan and underground utility clearance;
§Installation of three temporary groundwater monitoring wells;
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§Groundwater sample collection from the temporary monitoring wells;
§Collection of eight soil samples at the site;
§Installation of seven sub-slab soil vapor sample points at locations inside the buildings
near the former UST, the furnace area, the mold preparation area, the sand mixer, the
southern machine shop and storage areas for collection of soil vapor samples; and,
§Completion of a Brownfields Receptor Survey.
Sample locations are shown on Figure 2 and are summarized in Table 1. Field methods are
discussed in Section 3 of this report.
2.1 Reliance
This report has been prepared for the exclusive use of Barringer Capital, LLC and the North
Carolina Brownfields Program. Any authorization for use or reliance by another party (except a
governmental entity having jurisdiction over the site) is prohibited without the expressed written
authorization of Barringer Capital, LLC and Terracon. Any unauthorized distribution or reuse is
at the sole risk of Barringer Capital, LLC. Reliance by authorized parties will be subject to the
terms, conditions, and limitations stated in the proposal, report, and Terracon’s Agreement for
Services. The limitation of liability defined in the terms and conditions is the aggregate limit of
Terracon’s liability to Barringer Capital, LLC and all relying parties unless otherwise agreed in
writing.
3.0 FIELD INVESTIGATION METHODS
Terracon conducted the field work in accordance with a health and safety plan developed for this
project. Work was performed using United States Environmental Protection Agency (USEPA)
Level D work attire consisting of hard hats, safety glasses, protective gloves, and protective boots.
3.1 Temporary Well Installation
Prior to intrusive activities, Terracon submitted a locate request to the public utility locator [NC
811] to arrange for location of underground public utilities from the street to the utility meter. As
an added measure of safety, Terracon subcontracted Probe Utility Locating of Huntersville, North
Carolina, a private utility locator, to identify and mark public utilities beyond the meter as well as
additional site utilities identified near the proposed boring locations on January 9, 2017.
Terracon mobilized to the site on January 9, 2017 to install three temporary groundwater
monitoring wells GW-01, GW-02, and GW-03 (Figure 2 and Table 3) to evaluate groundwater
quality and determine the groundwater flow direction and hydraulic gradient at the site in the
general areas outlined in the Brownfields Assessment Work Plan. Redevelopment plans for the
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site do not include the use of on-site groundwater for any purpose and it is not anticipated that
groundwater will be encountered during redevelopment activities.
The boreholes were drilled by Innovative Environmental Technologies (IET) using Direct Push
Technology (DPT) drilling methods. Prior to advancing each boring, the drill tooling was cleaned
to prevent cross-contamination of samples. Boreholes for the wells were advanced to the water
table or DPT refusal, whichever was encountered first. The wells were constructed with a 1-inch
diameter PVC riser and a 10-foot screen to a total depth between 20 and 24 feet bgs. A sand
filter pack was placed in the annulus, extending from the bottom of the well screen to about one
foot above the top of the well screen. Hydrated bentonite was then used to create a 2-foot thick
seal above the filter pack. Well construction details are provided in Table 3. Terracon surveyed
the horizontal and vertical locations of the temporary monitoring wells so the groundwater flow
direction and hydraulic gradient could be calculated.
3.2 Groundwater Sampling
Terracon collected groundwater samples from two of the three temporary monitoring wells (GW-
02 and GW-03) on January 11, 2017. After multiple attempts to develop temporary well GW-01
due to the presence of mud clogging the well, Terracon re-mobilized to the site on January 16,
2017 to install a replacement for well GW-01 using a 4-inch diameter borehole and placement of
a thicker sand pack around the well screen.
Prior to sample collection, Terracon gauged the groundwater elevations in the monitoring wells
using a clean electronic water level indicator. Depth to groundwater ranged from 7.08 feet below
ground surface (bgs) in well GW-02 to 13.19 feet bgs in well GW-03. Groundwater elevation
measurements and monitoring well construction information are provided in Table 3. Based on
the water level measurements, groundwater flow direction is generally towards the northeast.
The wells were purged using a peristaltic pump and low-flow sampling methods until field
parameters of temperature, pH, oxidation-reduction potential, specific conductance, and
dissolved oxygen had stabilized. Groundwater sample collection records are provided in
Appendix A. The wells were generally purged at least two well volumes using low-flow methods
prior to sampling. Due to the physical properties of the 1-inch diameter temporary monitoring
wells with groundwater sample collection from temporary monitoring wells, development to less
than 10 NTU for turbidity was not feasible for temporary well GW-03, which was collected at 24
NTU. A duplicate groundwater sample (DUP-02-011117) was collected at well GW-02
The groundwater samples were placed in laboratory-supplied glassware, labeled and stored in
an ice-packed cooler. The samples, a trip blank for QA/QC purposes, and the chain-of-custody
documentation, were delivered to Pace Analytical Services, Inc. in Huntersville, North Carolina
for analysis of volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic
compounds (SVOCs) by EPA Method 8270, and RCRA metals by EPA Methods 6010 and 7470,
including aluminum, copper, and zinc.
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3.3 Soil Sampling
Prior to intrusive activities for collecting soil samples, Terracon conducted underground public
utility locating activities similar to the procedures described in Section 3.1 for the installation of
temporary monitoring wells. The soil sample locations are shown on Figure 2.
On January 10, 2017, Terracon mobilized to the site to collect eight soil samples (S-11 through
S-16, BG-01, and BG-02). Terracon also collected a duplicate sample (DUP-01-011017) at the
same sample location as sample S-15. Soil sample BG-01 was advanced to a depth of 2.5 feet
bgs and soil borings BG-02 and S-11 through S-16 were advanced to a depth of 5 feet bgs. Soil
sampling activities were conducted in the unsaturated zone only. Samples were collected in
areas of the site where existing surface soils may be disturbed during redevelopment (see Figure
2 for soil sample locations and Figure 7 for the preliminary future site layout). Grading plans are
not yet available but reportedly, grade cuts will be limited to less than 5 feet bgs in these areas.
Soil borings were located between the storage building and the foundry building (S-11), in the
paved driveway to the south of the former foundry building (S-12), between the former waste sand
stockpile and the sand mixer in the foundry building (S-13), near a trench drain with containing
ponded water within the former foundry building (S-14), near a large pit with a sump located in
the former mold preparation area (S-15), and near a small pit located near the former machine
shop (S-16). Soil samples BG-01 and BG-02 were collected to establish background metals
concentrations on the site.
Terracon subcontracted Innovative Environmental Technologies (IET), Inc., a North Carolina
licensed drilling company to advance the borings using direct-push drilling technology and Macro-
Core® samplers. IET utilized an AMS PowerProbe track-mounted drill rig. Since the location of
background sample BG-01 was not accessible by the drill rig, IET used a clean, de-contaminated
hand-auger to advance the boring to 2.5 feet bgs. Soil type, relative moisture content, and other
lithologic characteristics documented in the field are depicted on boring logs (Appendix A). Soils
consisted predominantly of red, orange and brown silty clay and clayey silt with moderate to low
moisture. Groundwater was not present in the shallow soil borings; however, three of the borings
were advanced to the water table. Photo-ionization detector (PID) readings did not indicate VOC
impacts in the recovered soils. Terracon collected a sample from the 0 to 2 foot interval from
samples S-11, S-12, S-13, BG-01, and BG-02. Terracon collected a sample from the 3 to 5 foot
interval from samples S-15, S-16, and DUP-01-011017 and a sample from the 1-3 foot interval
from S-14. Additional soils were collected at the locations of the four interior soil borings (S-13
through S-16) for analysis of metals by the Toxicity Characteristic Leachate Procedure (TCLP) to
evaluate the soils at the facility for hazardous characteristics. The TCLP samples were placed on
hold at the laboratory pending the results of the total metals analyses. After review of the total
metals analyses results, the Brownfields program did not require TCLP analysis. The boreholes
were abandoned using hydrated bentonite and concrete grout after the sampling activities were
completed.
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The soil samples were placed in laboratory-prepared glass containers, labeled with pertinent
sample information and stored in an ice-packed cooler pending submittal to a North Carolina
certified laboratory for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270 and
the eight RCRA metals by EPA Methods 6010/7471, including aluminum, copper, and zinc in
accordance with requirements by the North Carolina Brownfields Program. Chain of custody
documentation accompanied the samples to the laboratory.
3.4 Soil Vapor Sample Point Installation
The Brownfields Assessment Work Plan for the foundry site included the collection of seven sub-
slab soil vapor samples and one blind duplicate sample collected at the location of SV-04, near
the former sand mixer. The locations of the sub-slab soil vapor samples are shown on Figure 2
as SV-01 through SV-07 and are discussed below:
§SV-01 and SV-07 in the building formerly used as a warehouse;
§SV-02 in the mold preparation/casting area where waste sand was stockpiled;
§SV-03 in the furnace area;
§SV-04 adjacent to the sand mixer;
§SV-05 in the southern machine shop area; and
§SV-06 in the area of the kerosene AST and the former heating oil UST.
Updated sample identifications, locations, and analytical methods are shown in the Sampling and
Analysis Plan (Table 1) and on Figure 2. Technical approaches and methods used for the soil
vapor investigation are in general accordance with the Interstate Technical and Regulatory
Council’s Vapor Intrusion: A Practical Guideline (2007) and Vapor Intrusion Pathway:
Investigative Approaches for Typical Scenarios (2007), as well as the NCDEQ Division of Waste
Management (DWM)Vapor Intrusion Guidance (2014).
On January 9, 2017, two temporary sub-slab soil vapor (SV) sampling points were installed within
the storage building and five sub-slab SV sampling points were installed within the former foundry
building (Figure 2). Each temporary SV sampling point was installed by drilling a 5/8-inch
diameter hole through the floor slab to a depth of approximately 1 to 2 inches into the underlying
soils. The concrete slab was approximately eight inches thick at sampling points SV-01 and SV-
07 and about 14 to 15 inches at sampling points SV-02 through SV-06. The existence of a
moisture barrier beneath the building slab could not be verified by Terracon. The SV sampling
points were completed with a Vapor Pin™ assembly consisting of a brass barb fitting with a
silicone sleeve to seal the 5/8-inch diameter hole. A silicone cap was placed over the vapor pin
to keep it sealed and the sample points were allowed to equilibrate overnight prior to sampling.
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3.5 Soil Vapor Sampling
Terracon mobilized to the site on January 10, 2017 to collect the seven sub-slab soil vapor
samples and a blind duplicate sample. In order to test the integrity of the sampling point seal,
both a shut-in test and a helium tracer test were conducted at each sample point. A MGD-2000
helium detector was used to verify the presence and concentration of tracer gas.
The protocol for using a tracer gas is to enclose the sample manifold, tubing and ground interface
with a shroud and enrich the shroud atmosphere with helium. Prior to sample collection, at least
three volumes of the vapor point annulus and attached Teflon® lined tubing and sample train were
purged using a vacuum canister. Purge samples were then screened for helium to assess the
presence of leaks in the seal and fittings and with a PID to assess for the presence of VOCs.
Sample collection was started if the tracer testing indicated the helium concentration in the vapor
point was less than 10 percent of the helium concentration in the shroud, indicating an
appropriately sealed vapor point annulus.
Samples were collected with 1.0-liter Summa® canisters equipped with 170 ml/min flow controllers
for analysis of VOCs per EPA Method TO-15. In addition to the tracer test performed in the field,
one sample (SV-07) was analyzed for helium by Method ASTM-1946 to quantify leakage. None
of the seven SV points exhibited leakage during field leak testing. A blind duplicate sample was
collected at sample point SV-04. The vacuum pressure of the sample canisters was monitored
and recorded at regular intervals throughout the sampling period. Field sample collection records
for soil vapor samples are provided in Appendix A. After completion of soil vapor sampling
activities, the vapor sample points were abandoned by removal of the vapor pin and silicone
sleeve and filling the borehole with neat cement grout to the slab surface.
Following completion of the field activities, the Summa canisters (eight samples including the
duplicate), along with chain-of-custody documentation, were shipped to Eurofins AirToxics in
Folsom, California for laboratory analysis of VOCs by United States Environmental Protection
Agency (EPA) Method TO-15 and ASTM-1946 (SV-07 only).
3.6 Brownfields Receptor Survey
Terracon completed a Brownfields Receptor Survey which was completed on the form provided
by the NC Brownfields Program as a part of the additional assessment for the site. The Brownfield
Program’s “Brownfields Receptor Survey” form was used to conduct the field- and office-based
portions of the receptor survey. Terracon did not identify private or public water supply wells or
private irrigation wells within 1,500 feet of the site. The nearest surface water is an unnamed
tributary of Irwin Creek, located approximately 600 feet north of the site. The completed form is
included in Appendix A.
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4.0 RESULTS
The laboratory analytical reports and chain-of-custody record are attached in Appendix D. The
following sections describe the sample results.
4.1 Site Hydrogeology
Groundwater levels measured in the three on-site temporary monitoring wells ranged from 7.08
feet bgs (GW-02) to 13.19 feet bgs (GW-03). Groundwater elevations were calculated using the
field measurements and the top of casing and ground elevation data. Groundwater depths and
elevations are reported in Table 3. A groundwater elevation contour map is provided as Figure
3.
Groundwater in the surficial aquifer appears to be flowing towards the northeast. The horizontal
hydraulic gradient is approximately 0.054 ft./ft. at the former foundry site.
4.2 Groundwater Sample Results
On January 10, 11, and 17, 2017, groundwater samples were collected from three temporary
monitoring wells at the site. Laboratory analytical results for VOCs, SVOCs, and RCRA metals
are discussed separately below. Groundwater sample analytical results are summarized in Table
4 and on Figure 5. The laboratory analytical reports are included in Appendix B. Groundwater
sample results were compared to the North Carolina Administrative Code Subchapter 2L
Groundwater Quality Standards (2L Standard), effective April 1, 2013.
VOCs
Methylene chloride was detected in samples GW-02 (2.0 micrograms per liter [µg/L]), GW-03
(1.9J µg/L), and DUP-02-011117 (2.0 µg/L) at concentrations below the 2L Standard of 5 µg/L.
Styrene was also detected in samples GW-02 (0.30J) and DUP-02-011117 (0.39J) below the 2L
Standard. Styrene and methylene chloride are also below the DWM Residential Groundwater
Vapor Intrusion Screening Level of 1,860 µg/L and 942 µg/L, respectively. Sample GW-01 did not
contain VOC constituents above laboratory reporting limits.
SVOCs
Diethylphthalate was detected in samples GW-01 (7.9J µg/L) and DUP-02-011117 (2.2J µg/L) at
concentrations below its 2L Standard of 6,000 µg/L. SVOCs were not detected above laboratory
reporting limits or the 2L Standard in samples GW-02 or GW-03.
RCRA Metals
As discussed in Section 3.2, the groundwater sample from temporary monitoring well GW-03 had
elevated turbidity. Terracon considers the elevated metals concentrations in the sample collected
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from well GW-03 to be a result of high turbidity rather than actual concentrations representative
of the conditions at the site.
Various metals were detected in the four (including the duplicate) groundwater samples above
the laboratory reporting limits but none of the detected metals exceeded their respective 2L
Standard. The following RCRA metals were detected in the groundwater samples:
§Aluminum was detected in each of the four groundwater samples. Currently, a 2L
Standard for aluminum has not been established.
§Barium was detected in each of the four samples at concentrations well below the 2L
Standard of 700 µg/L.
§Copper was detected in each of the four samples at levels that are well below its 2L
Standard of 1,000 µg/L.
§Chromium was only detected in sample GW-03 (4.5J µg/L), below its 2L Standard of 10
µg/L.
§Lead was only detected in sample GW-03 (2.7J µg/L), below its 2L Standard of 15 µg/L.
§Zinc was detected in each of the four samples at concentrations that are well below its 2L
Standard of 1,000 µg/L.
In addition to comparing VOCs to the 2L Standards and DWM Residential Groundwater Vapor
Intrusion Screening Levels, Terracon also used the Brownfields Vapor Intrusion Groundwater
Concentration to Indoor Air Concentration (GWC-IAC) Calculator, Version 3.45 to assess the
potential vapor intrusion risk due to off-gassing from groundwater. The metals detected in the four
groundwater samples collected at the site and diethylphthalate (SVOC) do not readily volatilize
and are not included in the list of compounds of the GWC-IAC Calculator. As such, the risk
calculations were performed for samples GW-02, GW-03, and DUP-02-011117, the only
groundwater samples with detected VOCs. According to the calculator, cumulative carcinogenic
risk and the non-carcinogenic hazard quotient for samples GW-02, GW-03, and DUP-02-011117
are below the acceptable threshold value under a residential exposure scenario. The residential
risk calculator summary sheets are included in Appendix C.
4.3 Soil Sample Results
Nine soil samples (including the two background samples and one blind duplicate) were collected
for laboratory analysis at the site (Figure 2). Laboratory results are summarized below by
analytical method. Soil sample analytical results are summarized in Table 2 and on Figure 4 and
the laboratory analytical reports are included in Appendix B. Detected concentrations were
compared to the IHSB Residential and Non-Residential Preliminary Soil Remediation Goals
(PSRGs), October 2016 version. Concentrations were also evaluated using the Brownfields Soil
Risk Calculators.
Brownfields Assessment Report
Carolina Foundry Brownfields Site ■ Charlotte, NC
March 14, 2017 ■ Terracon Project No. 71167563
Responsive ■Resourceful ■Reliable 11
VOCs
Acetone was detected in sample S-16 at a concentration exceeding the laboratory reporting limit
but below the Residential PSRG. Naphthalene was detected in sample S-11 above the laboratory
reporting limit but below the residential and non-residential PSRGs. Methylene chloride was
detected in samples S-11 through S-16 and the blind duplicate sample at concentrations
exceeding the laboratory reporting limit but below the residential and non-residential PSRGs.
SVOCs
SVOCs were detected in soil samples S-12 and S-15:
§Sample S-12, collected southeast of the foundry building, contained 10 PAH constituents
at concentrations above laboratory reporting limits. Benzo(a)anthracene (0.172J
milligrams per kilogram [mg/kg]), benzo(b)fluoranthene (0.239J mg/kg) and
benzo(a)pyrene (0.179J mg/kg) exceeded their respective Residential PSRGs. The
remaining SVOCs detected in sample S-12 were below their respective residential
PSRGs.
§Sample SB-15 contained fluoranthene at a concentration that exceeded the laboratory
reporting limit but is below the residential PSRGs.
§The following soil samples did not contain SVOCs above laboratory reporting limits: S-11,
S-13, S-14, S-16, and DUP-01-011017.
RCRA Metals
Various metals were detected above laboratory reporting limits in each of the soil samples. The
metals are summarized below:
§Arsenic was detected in each soil sample at concentrations ranging from 2.9 to 4.6 mg/kg
that exceeded either the Residential or Non-Residential PSRG. The concentrations of
arsenic detected at the site are consistent with the on-site background samples and are
within the range of published naturally occurring metal concentrations for the site area
(Geochemical Landscapes of the Conterminous United States — New Map Presentations
for 22 Elements, USGS, 2001).
§Copper was detected in background soil sample BG-01 at a concentration of 1,270 mg/kg
which exceeds the Residential PSRG of 620 mg/kg. Copper concentrations detected in
the remaining eight soil samples below the PSRGs. The reason for the presence of
elevated copper and other metals detected in background sample BG-01 is unknown at
this time.
§The remaining metals were detected at concentrations below their respective PSRGs:
o Aluminum: 9 of 9 samples (7650 to 15,300 mg/kg);
o Barium: 9 of 9 samples (16.7 to 88.0 mg/kg);
o Cadmium: 2 of 9 samples (0.069J and 0.74 mg/kg);
o Chromium: 9 of 9 samples (23.2 to 45.3 mg/kg);
o Lead: 9 of 9 samples (8.5 to 201 mg/kg);
Brownfields Assessment Report
Carolina Foundry Brownfields Site ■ Charlotte, NC
March 14, 2017 ■ Terracon Project No. 71167563
Responsive ■Resourceful ■Reliable 12
o Mercury: 9 of 9 samples (0.011 to 0.12 mg/kg);
o Silver: 7 of 9 samples (0.26J to 0.59 mg/kg); and
o Zinc: 9 of 9 samples (8.4 to 586 mg/kg).
Detected concentrations of VOCs, SVOCs, and metals in soil samples were evaluated using the
NC Brownfields Program Soil Risk Calculator. Cumulative carcinogenic risk and the non-
carcinogenic hazard quotient for all of the samples are below the unacceptable threshold value
under a residential exposure scenario. The residential risk calculator summary sheets for each of
the 9 soil samples is included in Appendix C.
4.4 Soil Vapor Sample Results
Soil vapor sample results are shown on Figure 6 and summarized on Table 5. The laboratory
analytical reports are included in Appendix B.
No leaks were detected in the sample manifolds during the initial dead-head or shut-in tests. After
purging, the purge tubing was screened for helium and VOCs. VOCs were not detected within the
purge tubing for each of the seven soil vapor samples above ambient air PID readings. During
purging, helium was detected in six of the seven SV samples (SV-01, SV-02, SV-04, SV-05, SV-
06, and SV-07). Although helium was present in the line, the leaks are considered to be minor,
as helium within the line was far less than what was detected within the shroud. Therefore,
Terracon does not consider the minor leaks to be a QA/QC concern. Sample SV-07 was also
analyzed for helium by the analytical laboratory to obtain a more reliable leak quantification.
Based on the laboratory analytical result for sample SV-07 helium (0.37%) was detected above
the reporting limit of 0.12%. This corresponds to a 3% leak which is well below the 10% leak
threshold specified in the NCDEQ Vapor Intrusion Guidance (2014); therefore, the QA/QC helium
sample supports the integrity of the soil vapor sample results. A level 2 QA/QC data package is
provided with the soil vapor laboratory results in Appendix B.
Laboratory analytical results for the soil vapor samples were compared to the NCDEQ DWM Soil
Gas Screening Levels (SGSL) for a residential exposure scenario, updated October 2016. VOCs
were not detected above non-residential SGSLs. Only 1,2,4-trimethylbenzene was detected
above the residential SGSL in one sample (SV-06). The following compounds were present in
soil vapor above laboratory reporting limits:
§Acetone (5 samples), benzene (2 samples), 2-butanone (methyl ethyl ketone; 2 samples),
carbon disulfide (2 samples), cyclohexane (2 samples), 1,2-dichloropropane (1 sample),
ethanol (7 samples), ethyl benzene (2 samples), 4-ethyltoluene (4 samples), Freon 11 (2
samples), heptane (2 samples), hexane (3 samples), 2-hexanone (2 samples), 4-methyl-
2-pentanone (2 samples), 2-propanol (2 samples), propylbenzene (2 samples), styrene (2
samples), toluene (5 samples), 1,2,4-trimethylbenzene (4 samples), 1,3,5-
trimethylbenzene (3 samples), m,p-xylene (3 samples), and o-xylene (2 samples).
Brownfields Assessment Report
Carolina Foundry Brownfields Site ■ Charlotte, NC
March 14, 2017 ■ Terracon Project No. 71167563
Responsive ■Resourceful ■Reliable 13
Blind duplicate sample DUP-1-10-17 was collected at location SV-04. The duplicate sample
results generally correlate with the primary sample (SV-04) results. Soil vapor sample results
were also evaluated using the NC Brownfields Program Sub-Slab or Exterior Soil Gas
Concentration to Indoor Air Concentration (SGC-IAC) Calculator, version 3.45. Under a residential
exposure scenario, the cumulative vapor intrusion carcinogenic risk and hazard quotient are
below the acceptable threshold value for the seven soil vapor samples and the duplicate sample.
The risk calculators are included in Appendix C.
5.0 CONCLUSIONS AND RECOMMENDATIONS
Based on the scope of services described in this report and subject to the limitations described
herein, Terracon provides the following conclusions.
Soil
§Investigation activities have determined that the upper five feet of soils at the boring
locations consist of silty clays and clayey silts.
§Overall, environmental impacts in soils appear to be limited. Analytical results of soil
samples from previous assessments (S-1 and S-2), and from our assessment (S-12),
detected benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene) at
concentrations above their respective Residential PSRGs. Soil samples S-1 and S-2 by
GeoScience also detected ideno(1,2,3-cd)pyrene above its Residential PSRG. Although
SVOCs were detected in samples S-1 and S-2 above their respective Residential PSRGs,
the Brownfields soil risk calculator did not identify the SVOCs as exceeding the cumulative
value for carcinogenic risk or the target hazard quotient for non-carcinogens.
§According to the Brownfields soil risk calculator, the cumulative carcinogenic risk and the
target quotient for non-carcinogens for the detected constituents (SVOCs, VOCs and
metals) in sample S-12 do not exceed the residential carcinogenic risk or the target hazard
quotient threshold limit.
§Samples collected near the former furnaces inside the foundry building contained various
VOCs and SVOCs above their respective Protection of Groundwater PSRGs. According
to the Brownfields soil risk calculator, the cumulative carcinogenic risk value and the target
hazard quotient are within acceptable risk levels.
§Elevated concentrations of copper and other metals were detected in background sample
BG-01. Copper exceeded its Residential PSRG. The reason for the presence of elevated
copper and other metals detected in background sample BG-01 is unknown at this time.
§Although arsenic was detected in each of the soil samples collected from the former
foundry building at concentrations that exceed either its Residential or Non-Residential
PSRGs, arsenic was also detected above its Non-Residential PSRG in the two
background samples. The elevated detected concentrations of arsenic at the site are
within the range of published naturally occurring metal concentrations for the site area.
Brownfields Assessment Report
Carolina Foundry Brownfields Site ■ Charlotte, NC
March 14, 2017 ■ Terracon Project No. 71167563
Responsive ■Resourceful ■Reliable 14
Groundwater
§Depth to groundwater at the site ranged between 7.08 and 13.19 feet bgs and the
groundwater flow direction is generally towards the northeast.
§Although VOCs, SVOCs, and metals were detected in the groundwater, none of the
detected constituents exceeded the 2L Standards.
§The Brownfields GWC-IAC Calculator confirms that under a residential-use scenario, off-
gassing from groundwater at the site does not represent a vapor intrusion concern.
§Groundwater will not be used for any purpose at the site, and it is not anticipated that
groundwater will be encountered during redevelopment activities.
Soil Vapor
§Soil vapor sample SV-06 collected from the former Carolina Foundry contained 1,2,4-
trimethylbenzene above its Residential SGSL. The remaining soil vapor samples collected
at the former foundry did not detect VOCs above the SGSLs. Cumulative risk evaluations
using the Brownfields Program SGC-IAC Calculator confirm vapor intrusion risks are
acceptable under a residential scenario.
§Soil vapor sample results do not indicate vapor intrusion problems at the site; therefore,
vapor mitigation is not required based on soil vapor sample results.
TABLES
Table 1
Sampling and Analysis Plan
Carolina Foundry Brownfields Site
224 - 232 West Tremont Avenue
Charlotte, Mecklenburg County, NC
Terracon Project No. 71167563
SAMPLE ID SAMPLE MEDIUM GENERAL AREA SAMPLE INTERVAL (ft bgs)ANALYTICAL METHODS
GW-01 Groundwater Northeastern Corner of Storage Building 10-20 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7470 (RCRA Metals); Plus Aluminum Copper, and Zinc
GW-02 Groundwater Southeastern Corner of Storage Building 14-24 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7470 (RCRA Metals); Plus Aluminum Copper, and Zinc
GW-03 Groundwater Southeast of Machine Shop 13-23 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7470 (RCRA Metals); Plus Aluminum Copper, and Zinc
DUP-02-011117 Groundwater Southeastern Corner of Storage Building 14-24 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7470 (RCRA Metals); Plus Aluminum Copper, and Zinc
S-11 Soil Northeastern Corner of Storage Building 0-2 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
S-12 Soil Southeast of Machine Shop 0-2 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
S-13 Soil Former Sand Mixer 0-2 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
S-14 Soil Trench Drain with Standing Water 1-3 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
S-15 Soil Large Pit with Sump 3-5 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
S-16 Soil Small Pit 3-5 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
BG-01 Soil Northern Exterior Wall of Storage Building 0-2 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
BG-02 Soil Southeastern Corner of Storage Building 0-2 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
DUP-01-011017 Soil Large Pit with Sump 3-5 EPA 8260 (VOCs); EPA 8270 (SVOCs); 6010/7471 (RCRA Metals); Plus Aluminum, Copper, and Zinc
SV-01 Sub-Slab Soil Vapor (Gas)Southern Extent of Storage Building Sub-Slab EPA TO-15
SV-02 Sub-Slab Soil Vapor (Gas)Mold Preparation Area Sub-Slab EPA TO-15
SV-03 Sub-Slab Soil Vapor (Gas)Furnace Area Sub-Slab EPA TO-15
SV-04 Sub-Slab Soil Vapor (Gas)Former Sand Mixer Sub-Slab EPA TO-15
SV-05 Sub-Slab Soil Vapor (Gas)Former Machine Shop Sub-Slab EPA TO-15
SV-06 Sub-Slab Soil Vapor (Gas)Former USTs Sub-Slab EPA TO-15
SV-07 Sub-Slab Soil Vapor (Gas)Northern Extent of Storage Building Sub-Slab EPA TO-15; ASTM-1946
DUP-1-10-17 Sub-Slab Soil Vapor (Gas)Former Sand Mixer Sub-Slab EPA TO-15
Notes:
ft als - feet above ground surface
ft bgs - feet below ground surface
Table 2
Soil Sample Analytical Results
Carolina Foundry Brownfields Site
224 - 232 West Tremont Avenue
Charlotte, Mecklenburg County, NC
Terracon Project No. 71167563
Sample ID:S-1 S-2 S-4 S-5 S-5A S-6 S-7 S-9 S-10 SS-1 SS-2 S-11 S-12 S-13 S-14 S-15 S-16 DUP-01-011017 BG-01 BG-02
Sample Date: 7/30/2015 7/30/2015 7/30/2015 7/30/2015 7/30/2015 7/30/2015 7/30/2015 7/30/2015 7/30/2015 1/11/2016 1/11/2016 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17
PoG PSRG Location/Area:Eastern
Machine Shop
Eastern
Machine Shop
Former UST
Area Furnace Area Furnace Area
Compressor
Room
Compressor
Room
Western
Machine Shop
Western
Machine Shop Below UST Below UST
Northeastern
Corner of Storage
Building
Southeast of
Machine Shop
Former Sand
Mixer Trench Drain Large Pit with
Sump Small Pit Large Pit with Sump
Northern Exterior
Wall of Storage
Building
Southeastern
Corner of Storage
Building
Sample Interval (ft
bgs):1.5 1.5 8 2 7 2 2 2 2 6 6 0-2 0-2 0-2 1-3 3-5 3-5 3-5 0-2 0-2
Acetone 24 12,200 100,000 ND 0.12 ND ND ND ND ND 0.15 0.053J 0.0151J <0.303 <0.0096 <0.0076 <0.0101 <0.0101 <0.0097 0.0110J <0.0124
n-Butylbenzene 2.4 108 108 ND ND 0.16J ND ND ND ND ND ND <0.0022 0.139J <0.0017 <0.0014 <0.0018 <0.0018 <0.0017 <0.0017 <0.0022
sec-Butylbenzene 2.2 145 145 ND ND 0.13J 0.012 0.13J ND ND ND ND <0.0019 0.0927J <0.0015 <0.0012 <0.0016 <0.0016 <0.0016 <0.0015 <0.0020
4-Isopropylbenzene 0.68 NS NS ND ND 0.11J ND 0.10J ND ND ND ND 0.0033J 0.225 <0.0016 <0.0013 <0.0017 <0.0017 <0.0016 <0.0016 <0.0021
MEK 16 5,400 28,400 ND ND ND ND ND ND ND 0.017J ND ND ND NA NA NA NA NA NA NA
0.023 57 640 ND ND ND ND ND ND ND ND ND 0.0568 <0.0909 0.0063J 0.0043J 0.0063J 0.0063J 0.0057J 0.0114J 0.0081J
0.21 3.8 17 ND ND 0.54J ND 0.50J ND ND ND ND 0.0121 0.456 0.0039J <0.00092 <0.0012 <0.0012 <0.0012 <0.0011 <0.0015
n-Propylbenzene 1.5 264 264 ND ND ND ND 0.097J ND ND ND ND <0.002 0.0646J <0.0016 <0.0013 <0.0017 <0.0017 <0.0016 <0.0016 <0.0021
1,2,4-Trimethylbenzene 6.7 11.6 48 ND ND 0.85 ND 0.60 ND ND ND ND 0.0056J 0.635 <0.0019 <0.0015 <0.002 <0.002 <0.0019 <0.0019 <0.0025
1,3,5-Trimethylbenzene 6.7 156 182 ND ND 0.29J ND 0.20J ND ND ND ND <0.0022 0.169 <0.0017 <0.0014 <0.0018 <0.0018 <0.0017 <0.0017 <0.0022
o-Xylene NS 130 434 ND ND 0.091J ND 0.089J ND ND ND ND ND ND <0.0018 <0.0015 <0.0019 <0.0019 <0.0018 <0.0018 <0.0024
Xylenes (Total)6.1 116 260 ND ND ND ND ND ND ND ND ND <0.0043 0.0641J <0.0035 <0.0027 <0.0036 <0.0036 <0.0035 <0.0034 <0.0045
Acenaphthalene 8.4 720 9,000 ND 0.23J ND ND ND ND ND ND ND ND ND <0.091 <0.0918 <0.094 <0.0954 <0.095 <0.0978 <0.0938
Anthracene 660 3,600 46,000 ND 0.23J ND ND ND ND ND ND ND ND ND <0.0886 <0.0894 <0.0915 <0.092 <0.0925 <0.0952 <91.3
Benzo(a)anthracene 0.18 0.16 2.9 0.30J 0.65 ND ND ND ND ND ND ND ND ND <0.0731 0.172J <0.0755 <0.0759 <0.0762 <0.0785 <0.0753
Benzo(a)pyrene 0.052 0.016 0.29 0.33J 0.71 ND ND ND ND ND ND ND ND ND <0.0755 0.179J <0.0779 <0.0783 <0.0787 <0.0811 <0.0778
Benzo(b)fluoranthene 0.6 0.16 2.9 0.41J 0.89 ND ND ND ND ND ND ND ND ND <0.0683 0.239J <0.0705 <0.0709 <0.0712 <0.0733 <0.0703
Benzo(g,h,i)perylene 7,800 NS NS 0.21J 0.53 ND ND ND ND ND ND ND ND ND <0.101 0.133J <0.104 <0.104 <0.105 <0.108 <0.104
Benzo(k)fluoranthene 5.9 1.6 29 0.20J 0.45 ND ND ND ND ND ND ND ND ND <0.0779 0.106J <0.0804 <0.0808 <0.0812 <0.0836 <0.0802
Chrysene 18 16 290 0.31J 0.67 ND ND ND ND ND ND ND ND ND <0.0527 0.172J <0.0544 <0.0547 <0.055 <0.0566 <0.0543
Fluoranthene 330 480 6,000 0.59 1.2 ND ND ND ND ND ND ND ND ND <0.0575 0.354J <0.0594 <0.0597 0.0737J <0.0618 <0.0592
Fluorene 330 480 6,000 ND ND 0.35J ND ND ND ND ND ND <0.0936 0.202J <0.0815 <0.0821 <0.0841 <0.0846 <0.085 <0.0875 <0.0839
Ideno(1,2,3-cd)pyrene 2 0.16 2.9 0.21J 0.44 ND ND ND ND ND ND ND ND ND <0.0815 0.112J <0.0841 <0.0846 <0.085 <0.0875 <0.0839
1-Methylnaphthalene 0.052 18 73 ND ND 1.9 0.37J 0.61 ND ND ND ND <0.118 0.616 <0.103 <0.104 <0.106 <0.107 <0.107 <0.111 <0.106
2-Methylnaphthalene 1.6 48 600 ND ND 2.7 ND 0.86 ND ND ND ND 0.164J 0.727 <0.0851 <0.0858 <0.0878 <0.0883 <0.0887 <0.0914 <0.0876
Naphthalene 0.21 3.8 17 ND ND 0.54 ND 0.17J ND ND ND ND <0.111 0.17J <0.097 <0.0978 <0.100 <0.101 <0.101 <0.104 <0.100
Phenanthrene 68 NS NS 0.31J 0.5 0.84 0.68 0.41J ND ND ND ND 0.135J 0.261J <0.0659 0.237J <0.0680 <0.0684 <0.0687 <0.0708 <0.0679
Pyrene 220 360 4,600 0.54 1.2 0.16J 0.13J ND ND ND ND ND <0.0771 0.132J <0.0671 0.278J <0.0693 <0.0696 <0.070 <0.0721 <0.0691
Aluminum NS 15,400 100,000 NA NA NA NA NA NA NA NA NA NA NA 11000 11000 15300 10500 9880 14300 9670 7650 8900
5.8 0.68 3.0 5.1 5.7 1.9 2.1 3.1 2.3 2.4 4.9 3.3 NA NA 3.9 4.6 2.9 3.6 3.6 3.3 2.9 4.2 4.4
580 3,000 44,000 74 94 49 25 100 24 40 150 47 NA NA 44.1 72.9 59.9 17.5 22.9 24.1 25.7 88.0 16.7
3.0 14.2 196 ND 0.30 ND ND ND ND ND ND ND NA NA <0.057 0.069J <0.077 <0.084 <0.092 0.088 <0.092 0.74 <0.11
360,000 24,000 100,000 31 69 32 30 46 31 38 41 38 NA NA 23.2 26.2 24.1 35.7 25.2 30.8 45.3 32.5 32.7
Copper 700 620 9,400 NA NA NA NA NA NA NA NA NA NA NA 69.6 57.1 12.3 19 18.1 21.0 13.6 1270 17.0
270 400 800 65 120 4.7 11 15 11 9.7 17 11 NA NA 15.9 81.8 11.5 11.3 21.8 15.6 11.0 201 8.5
1.00 2.20 3.13 0.90 0.41 ND ND ND ND 0.037 ND ND NA NA 0.044 0.063 0.011 0.10 0.065 0.051 0.045 0.12 0.071
3.4 78 1,160 NA NA NA NA NA NA NA NA NA NA NA <0.28 0.26J <0.39 0.38J 0.37J 0.47 0.31J 0.59 0.40J
Zinc 1,200 4,600 70,000 NA NA NA NA NA NA NA NA NA NA NA 67.3 74.2 8.4 14.3 13.7 12.2 14.0 586 9.0
NA NA NA NA NA NA NA NA NA 131 1860 NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA <7.2 <7.6 NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
EPH C9-C18 Aliphatics NS NS NS NA NA NA NA NA NA NA NA NA 48.7 <674 NA NA NA NA NA NA NA NA NA
EPH C11-C22Aromatics NS NS NS NA NA NA NA NA NA NA NA NA 34.6 415 NA NA NA NA NA NA NA NA NA
Notes:
All results are shown in milograms per kilogram (mg/kg).
ft bgs - Feet Below Ground Surface
NA-Not Analyzed
NS - No Standard
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
Total chromium is assumed to consist exclusively of trivalent chromium. Historical site operations do not indicate the use of hexavalent chromium.
PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals, updated October, 2016.
Concentrations highlighted in grey exceed their respective Protection of Groundater level.
Concentrations highlighted in yellow exceed their respective residential PSRG.
Concentrations highlighted in orange exceed their respective non-residential PSRG.
Concentrations highlighted in blue exceed their respective TPH Action level.
VPH Aromatics and Alphatics
were not detected
EPH
VPH
Diesel-Range Organics (EPA Method 8015)
Gasoline-Range Organics (EPA Method 8015)
TPH Action
100
50
Barium
Analyte Residential
PSRGs
Non-
Residential
PSRGs
Volatile Organic Compounds by EPA Method 8260
Methylene Chloride
Naphthalene
NA NA
Semi-Volatile Organic Compounds by EPA Method 8270
Metals by EPA Methods 6010 and 7471
Arsenic
NA NA
Cadmium
Chromium
Lead
Mercury
Silver
Table 3
Groundwater Elevations
Carolina Foundry Brownfields Site
224 - 232 West Tremont Avenue
Charlotte, Mecklenburg County, NC
Terracon Project No. 71167563
GW-01 20.21 1.48 99.33 97.85 11.09
GW-02 24.21 0.47 100.00 99.53 7.08
GW-03 23.40 0.51 102.14 101.63 13.19
Notes:
Water levels were measured on Janaury 10, 11, and 17, 2017. Measurements were made to top of well casing and later converted to ft bgs.
ft - feet
ft bgs - feet below ground surface
Temporary wells were constructed using one-inch diameter PVC casing and 10 ft of 0.01-inch slot well screens.
Temporary Well ID
Top of Casing
Elevation
(ft)
Ground Elevation
(ft)
Total Depth
(ft bgs)
PVC Stickup Height
(ft)
92.45
88.44
Groundwater
Elevation
(ft)
86.76
Depth to Water
(ft bgs)
Table 4
Groundwater Sample Analytical Results
Carolina Foundry Brownfields Site
224 - 232 West Tremont Avenue
Charlotte, Mecklenburg County, NC
Terracon Project No. 71167563
Sample ID:GW-01 GW-02 GW-03 DUP-02-011117
Sample Date: 01/17/17 01/11/17 01/10/17 01/11/17
Screen Interval (ft bgs):10-20 14-24 13-23 14-24
Methylene Chloride 942 3,960 5 <0.97 2.0 1.9J 2.0
Styrene 1,860 7,790 70 <0.26 0.30J <0.26 0.39J
Diethylphthalate NS NS 6,000 7.9J <1.3 <1.3 2.2J
Metals by EPA Method 6010
Aluminum NS NS NS 497 401 950 420
Barium NS NS 700 67.2 55.8 37.0 55.6
Copper NS NS 1,000 4.5J 48.8 6.3 50.3
Chromium NS NS 10 <2.5 <2.5 4.5J <2.5
Lead NS NS 15 <2.5 <2.5 2.7J <2.5
Zinc NS NS 1,000 137 108 15.9 103
Notes:
Concentrations are reported in micrograms per liter (µg/L).
Only detected compounds are shown.
NCAC 2L GWQS - North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards (April 1, 2013).
NS - No Standard
Concentrations highlighted in grey exceed their respective NCAC 2L GWQS
Analyte NCAC 2L
GWQS
Volatile Organic Compounds by EPA Method 8260
Semi-Volatile Organic Compounds by EPA Method 8270
Residential GWSL Non-Residential
GWSL
Table 5
Soil Vapor Sample Analytical Results
Carolina Foundry Brownfields Site
224 - 232 West Tremont Avenue
Charlotte, Mecklenburg County, NC
Terracon Project No. 71167563
Sample ID:SV-01 SV-02 SV-03 SV-04 SV-05 SV-06 SV-07 DUP-1-10-17
Sample Date:01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17 01/10/17
Type:Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab
216,000 2,720,000 18J 71 16J 1200E 28J 55 100 1100E
Benzene 120 1,570 <0.37 <0.39 2.6J 83 <0.35 <0.37 1.3J 78
34,800 438,000 <2.1 5.8J 2.6J 280 <2.0 11J <2.0 270
4,870 61,300 1.3J 2.2J 2.2J 100 2.7J 6.6J 1.7J 100
Cumene 177 745 <0.72 <0.75 <0.69 4.0J <0.68 1.6J <0.68 4.0J
Cyclohexane 6,950 526,000 <0.77 <0.80 <0.74 6.8 <0.72 <0.77 <0.72 <0.70
1,2-Dichloroethane 22 98 3.4J <1.1 <0.98 <0.97 <0.97 1.9J <0.92 <0.94
1,2-Dichloropropane 27.8 350 7.2 <1.1 <0.98 <0.97 <0.97 4.2J <0.94 <0.94
NS NS 39 22 5.0J 52 13 14 26 51
Ethyl Benzene 374 4,910 <0.66 <0.69 <0.63 45 <0.62 <0.66 1.2J 43
4-Ethyltoluene NS NS <1.4 <1.5 <1.4 54 <1.4 32 11 51
Freon 11 NS NS 16 <1.4 <1.2 <1.2 <1.2 1.4J 31 <1.2
Freon 12 NS NS 1.6J 2.0J 2.3J 2.0J <1.2 2.1J 2.0J 1.7J
Heptane NS NS 1.5J <1.0 <0.95 55 <0.94 1.5J 1.8J 54
Hexane 4,870 61,300 <0.30 <0.31 <0.29 53 <0.28 3.2J 6.5 53
2-Hexanone 209 2,630 <0.91 <0.95 <0.87 49 <0.86 <0.91 <0.84 47
4-Methyl-2-pentanone 20,900 263,000 <1.4 <1.4 <1.3 32 <1.3 <1.4 <1.3 31
1,390 17,500 <0.90 7.0J <0.87 25 <0.85 <0.90 <0.83 23
Propylbenzene 6,950 87,600 <0.70 <0.74 <0.67 11 <0.66 4.9J 2.4J 11
6,950 87,600 <1.2 <1.2 1.7J 9.1 1.8J <1.2 3.8J 7.9
Tetrachloroethene 11.5 48.4 6.9J 2.5J <1.1 3.9J 6.6J 6.6J 3.2J 3.4J
34,800 438,000 9.3 0.87J 3.7J 180 1.2J 6.9 13 170
48.7 613 2.4J <2.0 2.2J 40 2.1J 80 9.4 40
1,3,5-Trimethylbenzene NS NS <1.3 <1.4 <1.2 14 <1.2 20 4.5J 13
2,2,4-Trimethylpentane NS NS 0.70J <0.56 1.7J 2.6J <0.50 <0.53 1.7J 2.5J
695 8,760 1.3J <0.86 1.5J 110 <0.78 3.3J 5.8 100
o-Xylene 695 8,760 <0.66 <0.69 0.67J 54 <0.63 2.5J 2.2J 51
NS NS NA NA NA NA NA NA 0.37 (%)NA
Notes:
Concentrations are reported in micrograms per cubic meter (μg/m3) unless otherwise noted.
Only detected compounds are shown.
Concentrations detected above the laboratory reporting limit are shown in bold.
E - exceeds instrument calibration range
NA - not analyzed
NS - no standard
DWM - North Carolina Department of Environmental Quality, Division of Waste Management
SGSL - DWM Sub-slab and Exterior Soil Gas Screening Level, updated October 2016
Concentrations highlighted in yellow exceed their respective residential SGSL.
Residential
Screening Levels
SGSL
2-Propanol
Non-
Residential
Screening
Levels SGSL
Analyte
ASTM-1946
Helium
EPA Method TO-15
2-Butanone (Methyl Ethyl Ketone)
m,p-Xylene
Toluene
Styrene
Acetone
1,2,4-Trimethylbenzene
Carbon Disulfide
Ethanol
FIGURES
SITE OVERVIEW MAP
Carolina Foundry Brownfields Site
224-232 W Tremont Ave
Charlotte, NC
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY
QUADRANGLES INCLUDE: CHARLOTTE WEST, NC (1/1/1993) and CHARLOTTE EAST, NC (1/1/1988).
2020 Starita Rd Ste E
Charlotte, NC 28206-1298
71167563
Project Manager:
Drawn by:
Checked by:
Approved by:
HEH
CLC
CLC
1”=2,000’
71167563.1
March 2017
Project No.
Scale:
File Name:
Date:
1
FIGUREHEH
APPROXIMATE
SITE BOUNDARY
#0
#0
#0
#0
#0#0
#0
$+
$+
")
")
")
")
")
")
@A
@A
@A
")
")
")
")
")
")
")")
")
")
")
")
STORAGE
AREA
MACHINE
SHOP
OFFICE
MACHINE SHOP
FURNACE
AREA
COMPRESSORROOM
CASTING AREA
MOLD
PREPARATION
AREA
STORAGE
AREA
FORMER
WASTE SAND STOCKPILE
SAND
MIXER
AST
FORMER
UST
FU
R
N
A
C
E
S
Open
Space
S-3
NS
S-8
NS
BG-01
S-9
S-7
S-6
S-4
S-2
S-1
SS-2
SS-1
S-10
S-5 / S-5A
S-13
GW-01 / S-11
GW-03 / S-12
GW-02 / BG-02
SV-07
SV-01
SV-04
SV-02
SV-03
SV-05
SV-06
S-16
S-14
S-15
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
2
HISTORICAL SITE LAYOUT AND SAMPLE LOCATION MAP
CAROLINA FOUNDRY BROWNFIELDS SITE
224-232 W. TREMONT AVE.
CHARLOTTE, NC
71167563
HEH
CLC
MARCH 2017
Project No.:
Drawn By:
Checked By:
Date:
N
:
\
P
r
o
j
e
c
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s
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2
0
1
6
\
7
1
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o
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R
e
s
u
l
t
s
.
m
x
d
³
0 25 5012.5
Feet
1 inch = 25 feet
Legend
Brownfields Site Boundary
Site Features
")Historical Soil Boring Location
A@ Groundwater Sample Location
)"Soil Sample Location
$Background Soil Sample Location0
# Soil Vapor Sample Location
Approximate Extent of Future Residential Units
Existing Buildings
Notes:
- Locations of building footprints and site features are approximate.
- Locations of interior features and soil sample locations are approximate
and based on a 2015 Phase 1 ESA for the site by Geoscience Group.
- NS indicates that no sample was submitted for laboratory analysis.
- Redevelopment Plans were provided by Barringer Capital, LLC.
- 2015 aerial imagery obtained from NC OneMap.
- Parcel data obtained from Mecklenburg County GIS website.
TREMONT AVE
N
U
E
#0
#0
#0
#0
#0#0
#0
$+
$+
")
")
")
")
")
")
@A
@A
")
")
")
")
")
")
")")
")
")
")
")
STORAGE
AREA
MACHINE
SHOP
OFFICE
MACHINE SHOP
FURNACE
AREA
COMPRESSORROOM
CASTING AREA
MOLD
PREPARATION
AREA
STORAGE
AREA
FORMER
WASTE SAND STOCKPILE
SAND
MIXER
AST
FORMER
UST
FU
R
N
A
C
E
S
Open
Space
S-3
NS
S-8
NS
BG-01
S-9
S-7
S-6
S-4
S-2
S-1
SS-2
SS-1
S-10
S-5 / S-5A
S-13
GW-01 / S-11
GW-03 / S-12
GW-02 / BG-02
SV-07
SV-01
SV-04
SV-02
SV-03
SV-05
SV-06
S-16
S-14
S-15
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
3
GROUNDWATER ELEVATION MAP
CAROLINA FOUNDRY BROWNFIELDS SITE
224-232 W. TREMONT AVE.
CHARLOTTE, NC
71167563
HEH
CLC
MARCH 2017
Project No.:
Drawn By:
Checked By:
Date:
N
:
\
P
r
o
j
e
c
t
s
\
2
0
1
6
\
7
1
1
6
7
5
6
3
\
W
o
r
k
i
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F
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\
3
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S
o
i
l

R
e
s
u
l
t
s
.
m
x
d
³
0 25 5012.5
Feet
1 inch = 25 feet
Legend
Brownfields Site Boundary
Site Features
")Historical Soil Boring Location
A@ Groundwater Sample Location
)"Soil Sample Location
$ Background Soil Sample Location0
# Soil Vapor Sample Location
Approximate Extent of Future Residential Units
Existing Buildings
Notes:
- Locations of building footprints and site features are approximate.
- Locations of interior features and soil sample locations are approximate
and based on a 2015 Phase 1 ESA for the site by Geoscience Group.
- NS indicates that no sample was submitted for laboratory analysis.
- Redevelopment Plans were provided by Barringer Capital, LLC.
- 2015 aerial imagery obtained from NC OneMap.
- Parcel data obtained from Mecklenburg County GIS website.
TREMONT AVE
N
U
E
#0
#0
#0
#0
#0#0
#0
$+
$+
")
")
")
")
")
")
@A
@A
@A
")
")
")
")
")
")
")")
")
")
")
")
STORAGE
AREA
MACHINE
SHOP
OFFICE
MACHINE SHOP
FURNACE
AREA
COMPRESSORROOM
CASTING AREA
MOLD
PREPARATION
AREA
STORAGE
AREA
FORMER
WASTE SAND STOCKPILE
SAND
MIXER
AST
FORMER
UST
FU
R
N
A
C
E
S
Open
Space
S-3
NS
S-8
NS
BG-01
S-9
S-7
S-6
S-4
S-2
S-1
SS-2
SS-1
S-10
S-5 / S-5A
S-13
GW-01 / S-11
GW-03 / S-12
GW-02 / BG-02
SV-07
SV-01
SV-04
SV-02
SV-03
SV-05
SV-06
S-16
S-14
S-15
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
4
SOIL SAMPLE ANALYTICAL RESULTS MAP
CAROLINA FOUNDRY BROWNFIELDS SITE
224-232 W. TREMONT AVE.
CHARLOTTE, NC
71167563
HEH
CLC
MARCH 2017
Project No.:
Drawn By:
Checked By:
Date:
N
:
\
P
r
o
j
e
c
t
s
\
2
0
1
6
\
7
1
1
6
7
5
6
3
\
W
o
r
k
i
n
g

F
i
l
e
s
\
G
I
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\
3
-
S
o
i
l

R
e
s
u
l
t
s
.
m
x
d
³
0 25 5012.5
Feet
1 inch = 25 feet
Legend
Brownfields Site Boundary
Site Features
")Historical Soil Boring Location
A@ Groundwater Sample Location
)"Soil Sample Location
$Background Soil Sample Location
#Soil Vapor Sample Location
Approximate Extent of Future Residential Units
Existing Buildings
Notes:
- Locations of building footprints and site features are approximate.- Locations of interior features and soil sample locations are approximate
and based on a 2015 Phase 1 ESA for the site by Geoscience Group.- NS indicates that no sample was submitted for laboratory analysis.- Redevelopment Plans were provided by Barringer Capital, LLC.- 2015 aerial imagery obtained from NC OneMap.
- Parcel data obtained from Mecklenburg County GIS website.
TREMONT AVE
N
U
E
#0
#0
#0
#0
#0#0
#0
$+
$+
")
")
")
")
")
")
@A
@A
@A
")
")
")
")
")
")
")")
")
")
")
")
STORAGE
AREA
MACHINE
SHOP
OFFICE
MACHINE SHOP
FURNACE
AREA
COMPRESSORROOM
CASTING AREA
MOLD
PREPARATION
AREA
STORAGE
AREA
FORMER
WASTE SAND STOCKPILE
SAND
MIXER
AST
FORMER
UST
FU
R
N
A
C
E
S
Open
Space
S-3
NS
S-8
NS
BG-01
S-9
S-7
S-6
S-4
S-2
S-1
SS-2
SS-1
S-10
S-5 / S-5A
S-13
GW-01 / S-11
GW-03 / S-12
GW-02 / BG-02
SV-07
SV-01
SV-04
SV-02
SV-03
SV-05
SV-06
S-16
S-14
S-15
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
5
GROUNDWATER ANALYTICALRESULTS MAP
CAROLINA FOUNDRY BROWNFIELDS SITE
224-232 W. TREMONT AVE.
CHARLOTTE, NC
71167563
HEH
CLC
MARCH 2017
Project No.:
Drawn By:
Checked By:
Date:
N
:
\
P
r
o
j
e
c
t
s
\
2
0
1
6
\
7
1
1
6
7
5
6
3
\
W
o
r
k
i
n
g

F
i
l
e
s
\
G
I
S
\
3
-
S
o
i
l

R
e
s
u
l
t
s
.
m
x
d
³
0 25 5012.5
Feet
1 inch = 25 feet
Legend
Brownfields Site Boundary
Site Features
")Historical Soil Boring Location
A@ Groundwater Sample Location
)" Soil Sample Location
$ Background Soil Sample Location0
#Soil Vapor Sample Location
Approximate Extent of Future Residential Units
Existing Buildings
Notes:
- Locations of building footprints and site features are approximate.
- Locations of interior features and soil sample locations are approximate
and based on a 2015 Phase 1 ESA for the site by Geoscience Group.
- NS indicates that no sample was submitted for laboratory analysis.
- Redevelopment Plans were provided by Barringer Capital, LLC.
- 2015 aerial imagery obtained from NC OneMap.
- Parcel data obtained from Mecklenburg County GIS website.
TREMONT AVE
N
U
E
#0
#0
#0
#0
#0#0
#0
$+
$+
")
")
")
")
")
")
@A
@A
@A
")
")
")
")
")
")
")")
")
")
")
")
STORAGE
AREA
MACHINE
SHOP
OFFICE
MACHINE SHOP
FURNACE
AREA
COMPRESSORROOM
CASTING AREA
MOLD
PREPARATION
AREA
STORAGE
AREA
FORMER
WASTE SAND STOCKPILE
SAND
MIXER
AST
FORMER
UST
FU
R
N
A
C
E
S
Open
Space
S-3
NS
S-8
NS
BG-01
S-9
S-7
S-6
S-4
S-2
S-1
SS-2
SS-1
S-10
S-5 / S-5A
S-13
GW-01 / S-11
GW-03 / S-12
GW-02 / BG-02
SV-07
SV-01
SV-04
SV-02
SV-03
SV-05
SV-06
S-16
S-14
S-15
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
CAROLINA FOUNDRY BROWNFIELDS SITE 6224-232 W. TREMONT AVE.
CHARLOTTE, NC
71167563
HEH
CLC
MARCH 2017
Project No.:
Drawn By:
Checked By:
Date:
N
:
\
P
r
o
j
e
c
t
s
\
2
0
1
6
\
7
1
1
6
7
5
6
3
\
W
o
r
k
i
n
g

F
i
l
e
s
\
G
I
S
\
3
-
S
o
i
l

R
e
s
u
l
t
s
.
m
x
d
³
0 25 5012.5
Feet
1 inch = 25 feet
Legend
Brownfields Site Boundary
Site Features
")Historical Soil Boring Location
A@ Groundwater Sample Location
)"Soil Sample Location
$ Background Soil Sample Location 0
#Soil Vapor Sample Location
Approximate Extent of Future Residential Units
Existing Buildings
Notes:
- Locations of building footprints and site features are approximate.
- Locations of interior features and soil sample locations are approximate
and based on a 2015 Phase 1 ESA for the site by Geoscience Group.
- NS indicates that no sample was submitted for laboratory analysis.
- Redevelopment Plans were provided by Barringer Capital, LLC.
- 2015 aerial imagery obtained from NC OneMap.
- Parcel data obtained from Mecklenburg County GIS website.
TREMONT AVE
N
U
E
1
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
7
PRELIMINARY FUTURE SITE LAYOUT MAP
CAROLINA FOUNDRY BROWNFIELDS SITE
224-232 W. TREMONT AVE.
CHARLOTTE, NC
71167563
HEH
CLC
March 2017
Project No.:
Drawn By:
Checked By:
Date:
N
:
\
7
1

E
n
v
i
r
o
n
m
e
n
t
a
l
\
B
u
s

D
e
v
\
P
r
o
p
o
s
a
l
s
\
2
0
1
6

P
r
o
p
o
s
a
l
s
\
7
1
1
6
7
E
1
3
5

C
a
r
o
l
i
n
a

F
o
u
n
d
r
y

B
r
o
w
n
f
i
e
l
d
s
\
G
I
S
\
M
X
D
\
3
-
P
r
e
l
i
m
S
i
t
e
P
l
a
n
.
m
x
d
³
0 25 5012.5
Feet
1 inch = 25 feet
Notes:
- Future site layout drawing provided by Barringer Capital, LLC
APPENDIX A – FIELD FORMS, SOIL BORING LOGS, AND
RECEPTOR SURVEY
Soil Boring Logs
Groundwater Sample Collection Records
Soil Vapor Sample Collection Record
Brownfields Receptor Survey Form
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 2.5 feet bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
Boring terminated at 2.5 feet.
NOTES: *soil sample interval
Checked by _CLC__________________Date:___March 2017_____
Well ID:BG 01
71167563 Rig make / type:AMS Power
Probe 11:30
Depth (ft)Description of Drill Cuttings
Ha
n
d

A
u
g
e
r
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
0-2.5: Brown CLAYEY SILT; low moisture*
2.5 0.3
26
28
30
32
14
16
18
20
22
24
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 24 feet bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
G 0-0.5: GRAVEL
0.5-2: Red SILTY CLAY; low to moderate moisture*
2-5: Same as above
5-10: Red/Orange SILTY CLAY; low moisture
10-15: Grey/Orange SILTY CLAY; low to moderate moisture
15-16: Red CLAY; low moisture
16-20: Grey CLAYEY SILT; low moisture
20-24: Red/Brown CLAY; saturated
Boring terminated at 24 feet bgs due to refusal.
NOTES:Well set at 24 ft bgs, *soil sample interval
Checked by _CLC__________________Date:___March 2017_____
CL
ML/CL
Sa
p
r
o
l
i
t
e
5
5
5
5
4 Saturated
0.9
1.0
1.1
0.2
0.6
Well ID:BG-02/GW-02
71167563 Rig make / type:AMS Power
Probe
10:15
10:37
Depth (ft)Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
26
28
30
32
14
16
18
20
22
24
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 16 feet bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
0-2: Grey/Black top soil and CLAY,SOME ODOR; high moisture*
2-5: Red/Brown CLAY, no odor; high moisture
5-10: Tan CLAYEY SILT; low moisture
10-14: Red CLAY; saturated
14-15: Red/Orange CLAYEY SILT; saturated
1
Boring terminated at 16 feet bgs due to saturated soils.
NOTES: Well set at 16 ft bgs, *soil sample interval
Checked by _CLC__________________Date:___March 2017_____
CL/ML
Sa
p
r
o
l
i
t
e
Depth (ft)
Well ID:S-11/GW-01
71167563 Rig make / type:AMS Power
Probe
10:55
11:16
Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
33.8
6.8
4.0
5
5
5 Saturated
26
28
30
32
14
16
18
20
22
24
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 25 ft bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
Fil
l 0-0.5: Concrete
0.5-2: Red SILTY CLAY; moderate moisture*
2-5: Same as above
5-9: Red CLAY; low mositure
9-10: Red/tan CLAY; low moisture
10-15: Red/tan/orange, SILTY CLAY; low moisture
15-17: Same as above
17-20: Red/orange/tan CLAY; saturated
20-23: Same as above
Boring terminated at 25 feet bgs due to saturated soils.
NOTES:Well set at 23 ft bgs, *soil sample interval
Checked by _CLC__________________Date:___March 2017_____
Sa
p
r
o
l
i
t
e
5
5
5
5
Saturated5
Well ID:S-12/GW-03
71167563 Rig make / type:AMS Power
Probe
9:30
10:00
Depth (ft)Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
0.9
0.6
1.0
0.5
1.3
CL/ML
26
28
30
32
14
16
18
20
22
24
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 5 ft bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)
PID
(ppm)
Geologic
ID U.S.C.S.
Fi
l
l 0-0.5: Concrete
0.5-5: Red SILTY CLAY; low moisture*
Boring terminated at 5 ft bgs.
NOTES: *soil sample interval
Checked by _CLC__________________Date:___March 2017_____
Well ID:S-13
71167563 Rig make / type:AMS Power
Probe
12:10
12:15
Depth (ft)Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
Sa
p
r
o
l
i
t
e
5
0.0
0.0 ML/CL
26
28
30
32
14
16
18
20
22
24
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 5 ft bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)
PID
(ppm)
Geologic
ID U.S.C.S.
Fi
l
l 0-0.5: Concrete
0.5-5: Red SILTY CLAY; low moisture*
Boring terminated at 5 ft bgs.
NOTES: *soil sample interval 1-3 feet
Checked by _CLC__________________Date:___March 2017_____
Well ID:S-14
71167563 Rig make / type:AMS Power
Probe
12:23
12:25
Depth (ft)Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
5
Sa
p
r
o
l
i
t
e
0.0
0.0 ML/CL
26
28
30
32
14
16
18
20
22
24
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 5 ft bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)
PID
(ppm)
Geologic
ID U.S.C.S.
Fi
l
l 0-1: Concrete
S/G 1-1.5: Black stained SANDY GRAVEL; moderate moisture
1.5-5 Red SILTY CLAY; low moisture*
Boring terminated at 5 ft bgs.
NOTES: *sampled interval from 3 to 5 feet
Checked by _CLC__________________Date:___March 2017_____
26
28
30
32
14
16
18
20
22
24
Depth (ft)Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
5
0.0
0.0 Sa
p
r
o
l
i
t
e
ML/CL
Well ID:S-15
71167563 Rig make / type:AMS Power
Probe
12:18
12:21
Client:David Smith Drilling Co:IET
Site:Carolina Foundry Lead Driller:John Allen
Project No:Time Started:
Site Address:224-232 West Tremont Time Finished:
Charlotte, NC Logged By:HEH
Weather:Sunny, cold Depth of Boring: 5 ft bgs
Drilling
Method /
Dia.
Blow
Counts
(per 6 in)
Recovery
(ft)
PID
(ppm)
Geologic
ID U.S.C.S.
Fi
l
l 0-0.5: Concrete
0.5-5: Red SILTY CLAY; low moisture*
Boring terminated at 5 ft bgs.
NOTES: *soil sample interval 3 to 5 feet
Checked by _CLC__________________Date:___March 2017_____
Well ID:S-16
71167563 Rig make / type:AMS Power
Probe
11:54
12:09
Depth (ft)Description of Drill Cuttings
2-
i
n
c
h

d
i
a
m
e
t
e
r

m
a
c
r
o
c
o
r
e
No
t

A
p
p
l
i
c
a
b
l
e
2
4
6
8
10
12
5
0.0
0.0 ML/CLSa
p
r
o
l
i
t
e
26
28
30
32
14
16
18
20
22
24
Carolina Foundry
224-232 West Tremont Avenue
Charlotte
Mecklenburg
20054-16-60
0%
0.75 Acres
The former foundry building (19,687 sq. ft.) was constructed
2%
73%
1%
10% Gravel Cover
14% Grass Cover
General Industrial/GFP International Inc.
Commercial/ Carolina Prepress Inc.
General Industrial/Carolina Parent Magazine
General Industrial/Dilworth Mattress Factory
Unchanged
Unchanged
Unchanged
Unchanged
N
Piedmont Natural Gas
City of Charlotte
Duke Energy
Y 10 Southeast
Y
N N/A N/A N/A
Y
N N/A N/A N/A
N N/A N/A
Additional Information:
-Power and telephone lines are overhead at the former foundry building.
-Underground power lines extend from the storage building to West Tremont Avenue.
-An underground water line main appears to parallel West Tremont Avenue.
-Stormwater piping parallels West Tremont Avenue.
-The natural gas line parallels West Tremont Avenue.
N N/A N/A
20 South
Y
Y 0 South
5 South
Y 0 South
X
Not applicable.
N
N
N N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
There are no surface water features on the subject
property.
N/A
N/A
N/A
N/A
No wetlands are present on the subject property
or adjacent properties.
The nearest surface water feature is an unnamed
tributary of Irwin Creek, located approximately 600
feet north of the site.
1
Figure
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES 2020-E Starita Road
Charlotte, NC
SITE DIAGRAMProject Manager:
Drawn by:
Checked by:
Approved by:
HEH Project No.
File Name:
Date:
Scale:
71167563
HEH
March 2016CLC
CLC
1 in = 650 feet
Receptor Map
Carolina Foundry Brownfields
224-232 West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
denotes approximate 1,000
foot radius
denotes residential properties
APPENDIX B – LABORATORY ANALYTICAL REPORTS
Groundwater Sample Analytical Report – Pace Analytical
Soil Sample Analytical Report – Pace Analytical
Soil Vapor Sample Analytical Report – Eurofins AirToxics
#=CL#
January 30, 2017
LIMS USE: FR - HALEY HINDES
LIMS OBJECT ID: 92326590
92326590
Project:
Pace Project No.:
RE:
Haley Hindes
Terracon NC
2020 Starita Rd
Suite E
Charlotte, NC 28206
CAROLINA FOUNDRY 71167563
Dear Haley Hindes:
Enclosed are the analytical results for sample(s) received by the laboratory on January 17, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Report revised 1/30/17 to add MDLs and J-flags.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 26
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 26
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Lab ID Sample ID Matrix Date Collected Date Received
92326590001 GW-01 Water 01/17/17 14:50 01/17/17 16:16
92326590002 TRIP BLANK Water 01/17/17 00:00 01/17/17 16:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 26
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92326590001 GW-01 EPA 6010 10 PASI-ASER
EPA 7470 1 PASI-AWAB
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92326590002 TRIP BLANK EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Sample:GW-01 Lab ID:92326590001 Collected:01/17/17 14:50 Received:01/17/17 16:16 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Aluminum 497 ug/L 01/20/17 18:44 7429-90-501/19/17 22:0510050.0 1
Arsenic ND ug/L 01/20/17 18:44 7440-38-201/19/17 22:0510.0 5.0 1
Barium 67.2 ug/L 01/20/17 18:44 7440-39-301/19/17 22:055.0 2.5 1
Cadmium ND ug/L 01/20/17 18:44 7440-43-901/19/17 22:051.0 0.50 1
Chromium ND ug/L 01/20/17 18:44 7440-47-301/19/17 22:055.0 2.5 1
Copper 4.5J ug/L 01/20/17 18:44 7440-50-801/19/17 22:055.0 2.5 1
Lead ND ug/L 01/20/17 18:44 7439-92-101/19/17 22:055.0 2.5 1
Selenium ND ug/L 01/20/17 18:44 7782-49-201/19/17 22:0510.0 5.0 1
Silver ND ug/L 01/20/17 18:44 7440-22-401/19/17 22:055.0 2.5 1
Zinc 137 ug/L 01/20/17 18:44 7440-66-601/19/17 22:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/23/17 11:27 7439-97-601/21/17 02:200.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/19/17 14:27 83-32-901/18/17 09:0510.0 0.25 1
Acenaphthylene ND ug/L 01/19/17 14:27 208-96-801/18/17 09:0510.0 0.21 1
Aniline ND ug/L 01/19/17 14:27 62-53-301/18/17 09:0510.0 1.3 1
Anthracene ND ug/L 01/19/17 14:27 120-12-701/18/17 09:0510.0 0.14 1
Benzo(a)anthracene ND ug/L 01/19/17 14:27 56-55-301/18/17 09:0510.0 0.33 1
Benzo(a)pyrene ND ug/L 01/19/17 14:27 50-32-801/18/17 09:0510.0 0.30 1
Benzo(b)fluoranthene ND ug/L 01/19/17 14:27 205-99-201/18/17 09:0510.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 01/19/17 14:27 191-24-201/18/17 09:0510.0 0.38 1
Benzo(k)fluoranthene ND ug/L 01/19/17 14:27 207-08-901/18/17 09:0510.0 0.43 1
Benzoic Acid ND ug/L 01/19/17 14:27 65-85-001/18/17 09:0550.0 11.1 1
Benzyl alcohol ND ug/L 01/19/17 14:27 100-51-601/18/17 09:0520.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 01/19/17 14:27 101-55-301/18/17 09:0510.0 1.3 1
Butylbenzylphthalate ND ug/L 01/19/17 14:27 85-68-701/18/17 09:0510.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 01/19/17 14:27 59-50-701/18/17 09:0520.0 4.2 1
4-Chloroaniline ND ug/L 01/19/17 14:27 106-47-801/18/17 09:0520.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 01/19/17 14:27 111-91-101/18/17 09:0510.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 01/19/17 14:27 111-44-401/18/17 09:0510.0 1.5 1
2-Chloronaphthalene ND ug/L 01/19/17 14:27 91-58-701/18/17 09:0510.0 2.2 1
2-Chlorophenol ND ug/L 01/19/17 14:27 95-57-801/18/17 09:0510.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 01/19/17 14:27 7005-72-301/18/17 09:0510.0 2.1 1
Chrysene ND ug/L 01/19/17 14:27 218-01-901/18/17 09:0510.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 01/19/17 14:27 53-70-301/18/17 09:0510.0 0.55 1
Dibenzofuran ND ug/L 01/19/17 14:27 132-64-901/18/17 09:0510.0 1.8 1
1,2-Dichlorobenzene ND ug/L 01/19/17 14:27 95-50-101/18/17 09:0510.0 1.2 1
1,3-Dichlorobenzene ND ug/L 01/19/17 14:27 541-73-101/18/17 09:0510.0 1.1 1
1,4-Dichlorobenzene ND ug/L 01/19/17 14:27 106-46-701/18/17 09:0510.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 01/19/17 14:27 91-94-101/18/17 09:0520.0 1.4 1
2,4-Dichlorophenol ND ug/L 01/19/17 14:27 120-83-201/18/17 09:0510.0 1.7 1
Diethylphthalate 7.9J ug/L 01/19/17 14:27 84-66-201/18/17 09:0510.0 1.3 1
2,4-Dimethylphenol ND ug/L 01/19/17 14:27 105-67-901/18/17 09:0510.0 2.2 1
Dimethylphthalate ND ug/L 01/19/17 14:27 131-11-301/18/17 09:0510.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Sample:GW-01 Lab ID:92326590001 Collected:01/17/17 14:50 Received:01/17/17 16:16 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Di-n-butylphthalate ND ug/L 01/19/17 14:27 84-74-201/18/17 09:0510.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 01/19/17 14:27 534-52-101/18/17 09:0520.0 1.7 1
2,4-Dinitrophenol ND ug/L 01/19/17 14:27 51-28-501/18/17 09:0550.0 6.5 1
2,4-Dinitrotoluene ND ug/L 01/19/17 14:27 121-14-201/18/17 09:0510.0 1.2 1
2,6-Dinitrotoluene ND ug/L 01/19/17 14:27 606-20-201/18/17 09:0510.0 1.7 1
Di-n-octylphthalate ND ug/L 01/19/17 14:27 117-84-001/18/17 09:0510.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/19/17 14:27 117-81-701/18/17 09:056.0 0.85 1
Fluoranthene ND ug/L 01/19/17 14:27 206-44-001/18/17 09:0510.0 0.21 1
Fluorene ND ug/L 01/19/17 14:27 86-73-701/18/17 09:0510.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 01/19/17 14:27 87-68-301/18/17 09:0510.0 1.8 1
Hexachlorobenzene ND ug/L 01/19/17 14:27 118-74-101/18/17 09:0510.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 01/19/17 14:27 77-47-401/18/17 09:0510.0 1.8 1
Hexachloroethane ND ug/L 01/19/17 14:27 67-72-101/18/17 09:0510.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/19/17 14:27 193-39-501/18/17 09:0510.0 0.29 1
Isophorone ND ug/L 01/19/17 14:27 78-59-101/18/17 09:0510.0 1.8 1
1-Methylnaphthalene ND ug/L 01/19/17 14:27 90-12-001/18/17 09:0510.0 0.32 1
2-Methylnaphthalene ND ug/L 01/19/17 14:27 91-57-601/18/17 09:0510.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 01/19/17 14:27 95-48-701/18/17 09:0510.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/19/17 14:2701/18/17 09:0510.0 1.7 1
Naphthalene ND ug/L 01/19/17 14:27 91-20-301/18/17 09:0510.0 0.34 1
2-Nitroaniline ND ug/L 01/19/17 14:27 88-74-401/18/17 09:0550.0 2.8 1
3-Nitroaniline ND ug/L 01/19/17 14:27 99-09-201/18/17 09:0550.0 2.4 1
4-Nitroaniline ND ug/L 01/19/17 14:27 100-01-601/18/17 09:0520.0 2.5 1
Nitrobenzene ND ug/L 01/19/17 14:27 98-95-301/18/17 09:0510.0 1.7 1
2-Nitrophenol ND ug/L 01/19/17 14:27 88-75-501/18/17 09:0510.0 1.7 1
4-Nitrophenol ND ug/L 01/19/17 14:27 100-02-701/18/17 09:0550.0 5.8 1
N-Nitrosodimethylamine ND ug/L 01/19/17 14:27 62-75-901/18/17 09:0510.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 01/19/17 14:27 621-64-701/18/17 09:0510.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 01/19/17 14:27 86-30-601/18/17 09:0510.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/19/17 14:27 108-60-101/18/17 09:0510.0 1.6 1
Pentachlorophenol ND ug/L 01/19/17 14:27 87-86-501/18/17 09:0525.0 2.3 1
Phenanthrene ND ug/L 01/19/17 14:27 85-01-801/18/17 09:0510.0 0.22 1
Phenol ND ug/L 01/19/17 14:2701/18/17 09:0510.0 1.7 1
Pyrene ND ug/L 01/19/17 14:27 129-00-001/18/17 09:0510.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 01/19/17 14:27 120-82-101/18/17 09:0510.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 01/19/17 14:27 95-95-401/18/17 09:0510.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 01/19/17 14:27 88-06-201/18/17 09:0510.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)71 %01/19/17 14:27 4165-60-001/18/17 09:0521-110 1
2-Fluorobiphenyl (S)70 %01/19/17 14:27 321-60-801/18/17 09:0527-110 1
Terphenyl-d14 (S)79 %01/19/17 14:27 1718-51-001/18/17 09:0531-107 1
Phenol-d6 (S)29 %01/19/17 14:27 13127-88-301/18/17 09:0510-110 1
2-Fluorophenol (S)41 %01/19/17 14:27 367-12-401/18/17 09:0512-110 1
2,4,6-Tribromophenol (S)71 %01/19/17 14:27 118-79-601/18/17 09:0527-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Sample:GW-01 Lab ID:92326590001 Collected:01/17/17 14:50 Received:01/17/17 16:16 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 01/18/17 17:57 67-64-125.0 10.0 1
Benzene ND ug/L 01/18/17 17:57 71-43-21.0 0.25 1
Bromobenzene ND ug/L 01/18/17 17:57 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 01/18/17 17:57 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 01/18/17 17:57 75-27-41.0 0.18 1
Bromoform ND ug/L 01/18/17 17:57 75-25-21.0 0.26 1
Bromomethane ND ug/L 01/18/17 17:57 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 01/18/17 17:57 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 01/18/17 17:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/18/17 17:57 108-90-71.0 0.23 1
Chloroethane ND ug/L 01/18/17 17:57 75-00-31.0 0.54 1
Chloroform ND ug/L 01/18/17 17:57 67-66-31.0 0.14 1
Chloromethane ND ug/L 01/18/17 17:57 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 01/18/17 17:57 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 01/18/17 17:57 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 01/18/17 17:57 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 01/18/17 17:57 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/18/17 17:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/18/17 17:57 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/18/17 17:57 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 01/18/17 17:57 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 01/18/17 17:57 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 01/18/17 17:57 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 01/18/17 17:57 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 01/18/17 17:57 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/18/17 17:57 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/18/17 17:57 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/18/17 17:57 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 01/18/17 17:57 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 01/18/17 17:57 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 01/18/17 17:57 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 01/18/17 17:57 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 01/18/17 17:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/18/17 17:57 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 01/18/17 17:57 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 01/18/17 17:57 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 01/18/17 17:57 87-68-31.0 0.71 1
2-Hexanone ND ug/L 01/18/17 17:57 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 01/18/17 17:57 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 01/18/17 17:57 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/18/17 17:57 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 01/18/17 17:57 1634-04-41.0 0.21 1
Naphthalene ND ug/L 01/18/17 17:57 91-20-31.0 0.24 1
Styrene ND ug/L 01/18/17 17:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/18/17 17:57 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/18/17 17:57 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 7 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Sample:GW-01 Lab ID:92326590001 Collected:01/17/17 14:50 Received:01/17/17 16:16 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 01/18/17 17:57 127-18-41.0 0.46 1
Toluene ND ug/L 01/18/17 17:57 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 01/18/17 17:57 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 01/18/17 17:57 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 01/18/17 17:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/18/17 17:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/18/17 17:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/18/17 17:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/18/17 17:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/18/17 17:57 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 01/18/17 17:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/18/17 17:57 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 01/18/17 17:57 179601-23-12.0 0.66 1
o-Xylene ND ug/L 01/18/17 17:57 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)96 %01/18/17 17:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %01/18/17 17:57 17060-07-070-130 1
Toluene-d8 (S)104 %01/18/17 17:57 2037-26-570-130 1
Sample:TRIP BLANK Lab ID:92326590002 Collected:01/17/17 00:00 Received:01/17/17 16:16 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 01/18/17 13:13 67-64-125.0 10.0 1
Benzene ND ug/L 01/18/17 13:13 71-43-21.0 0.25 1
Bromobenzene ND ug/L 01/18/17 13:13 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 01/18/17 13:13 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 01/18/17 13:13 75-27-41.0 0.18 1
Bromoform ND ug/L 01/18/17 13:13 75-25-21.0 0.26 1
Bromomethane ND ug/L 01/18/17 13:13 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 01/18/17 13:13 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 01/18/17 13:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/18/17 13:13 108-90-71.0 0.23 1
Chloroethane ND ug/L 01/18/17 13:13 75-00-31.0 0.54 1
Chloroform ND ug/L 01/18/17 13:13 67-66-31.0 0.14 1
Chloromethane ND ug/L 01/18/17 13:13 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 01/18/17 13:13 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 01/18/17 13:13 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 01/18/17 13:13 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 01/18/17 13:13 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/18/17 13:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/18/17 13:13 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/18/17 13:13 95-50-11.0 0.30 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 8 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Sample:TRIP BLANK Lab ID:92326590002 Collected:01/17/17 00:00 Received:01/17/17 16:16 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,3-Dichlorobenzene ND ug/L 01/18/17 13:13 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 01/18/17 13:13 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 01/18/17 13:13 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 01/18/17 13:13 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 01/18/17 13:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/18/17 13:13 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/18/17 13:13 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/18/17 13:13 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 01/18/17 13:13 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 01/18/17 13:13 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 01/18/17 13:13 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 01/18/17 13:13 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 01/18/17 13:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/18/17 13:13 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 01/18/17 13:13 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 01/18/17 13:13 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 01/18/17 13:13 87-68-31.0 0.71 1
2-Hexanone ND ug/L 01/18/17 13:13 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 01/18/17 13:13 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 01/18/17 13:13 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/18/17 13:13 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 01/18/17 13:13 1634-04-41.0 0.21 1
Naphthalene ND ug/L 01/18/17 13:13 91-20-31.0 0.24 1
Styrene ND ug/L 01/18/17 13:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/18/17 13:13 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/18/17 13:13 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 01/18/17 13:13 127-18-41.0 0.46 1
Toluene ND ug/L 01/18/17 13:13 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 01/18/17 13:13 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 01/18/17 13:13 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 01/18/17 13:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/18/17 13:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/18/17 13:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/18/17 13:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/18/17 13:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/18/17 13:13 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 01/18/17 13:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/18/17 13:13 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 01/18/17 13:13 179601-23-12.0 0.66 1
o-Xylene ND ug/L 01/18/17 13:13 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)94 %01/18/17 13:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %01/18/17 13:13 17060-07-070-130 1
Toluene-d8 (S)107 %01/18/17 13:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
345129
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92326590001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1915074
Associated Lab Samples:92326590001
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/23/17 11:130.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1915075LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1915076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324858001
1915077
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 50 84 75-12586 2 2550ND42.0 42.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344820
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92326590001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1913223
Associated Lab Samples:92326590001
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 10.0 01/20/17 18:285.0
Barium ug/L ND 5.0 01/20/17 18:282.5
Cadmium ug/L ND 1.0 01/20/17 18:280.50
Chromium ug/L ND 5.0 01/20/17 18:282.5
Copper ug/L ND 5.0 01/20/17 18:282.5
Lead ug/L ND 5.0 01/20/17 18:282.5
Selenium ug/L ND 10.0 01/20/17 18:285.0
Silver ug/L ND 5.0 01/20/17 18:282.5
Zinc ug/L ND 10.0 01/20/17 18:285.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913224LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 461500 92 80-120
Barium ug/L 478500 96 80-120
Cadmium ug/L 468500 94 80-120
Chromium ug/L 463500 93 80-120
Copper ug/L 475500 95 80-120
Lead ug/L 469500 94 80-120
Selenium ug/L 471500 94 80-120
Silver ug/L 242250 97 80-120
Zinc ug/L 485500 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1913225MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92326202001
1913226
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 91 75-12592 1 20500ND463469
Barium ug/L 500 89 75-125106 3 20500197024202500
Cadmium ug/L 500 93 75-12594 1 20500ND465470
Chromium ug/L 500 91 75-12591 1 2050046.6 500 504
Copper ug/L 500 100 75-125100 0 20500124624624
Lead ug/L 500 82 75-12583 1 2050021.8 434 437
Selenium ug/L M15005675-12557 2 20500ND285289
Silver ug/L 250 98 75-12599 2 20250ND246250
Zinc ug/L 500 98 75-12599 0 2050055710501050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344697
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92326590001, 92326590002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1912355
Associated Lab Samples:92326590001, 92326590002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 01/18/17 11:440.33
1,1,1-Trichloroethane ug/L ND 1.0 01/18/17 11:440.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 01/18/17 11:440.40
1,1,2-Trichloroethane ug/L ND 1.0 01/18/17 11:440.29
1,1-Dichloroethane ug/L ND 1.0 01/18/17 11:440.32
1,1-Dichloroethene ug/L ND 1.0 01/18/17 11:440.56
1,1-Dichloropropene ug/L ND 1.0 01/18/17 11:440.49
1,2,3-Trichlorobenzene ug/L ND 1.0 01/18/17 11:440.33
1,2,3-Trichloropropane ug/L ND 1.0 01/18/17 11:440.41
1,2,4-Trichlorobenzene ug/L ND 1.0 01/18/17 11:440.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 01/18/17 11:442.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/18/17 11:440.27
1,2-Dichlorobenzene ug/L ND 1.0 01/18/17 11:440.30
1,2-Dichloroethane ug/L ND 1.0 01/18/17 11:440.24
1,2-Dichloropropane ug/L ND 1.0 01/18/17 11:440.27
1,3-Dichlorobenzene ug/L ND 1.0 01/18/17 11:440.24
1,3-Dichloropropane ug/L ND 1.0 01/18/17 11:440.28
1,4-Dichlorobenzene ug/L ND 1.0 01/18/17 11:440.33
2,2-Dichloropropane ug/L ND 1.0 01/18/17 11:440.13
2-Butanone (MEK)ug/L ND 5.0 01/18/17 11:440.96
2-Chlorotoluene ug/L ND 1.0 01/18/17 11:440.35
2-Hexanone ug/L ND 5.0 01/18/17 11:440.46
4-Chlorotoluene ug/L ND 1.0 01/18/17 11:440.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 01/18/17 11:440.33
Acetone ug/L ND 25.0 01/18/17 11:4410.0
Benzene ug/L ND 1.0 01/18/17 11:440.25
Bromobenzene ug/L ND 1.0 01/18/17 11:440.30
Bromochloromethane ug/L ND 1.0 01/18/17 11:440.17
Bromodichloromethane ug/L ND 1.0 01/18/17 11:440.18
Bromoform ug/L ND 1.0 01/18/17 11:440.26
Bromomethane ug/L ND 2.0 01/18/17 11:440.29
Carbon tetrachloride ug/L ND 1.0 01/18/17 11:440.25
Chlorobenzene ug/L ND 1.0 01/18/17 11:440.23
Chloroethane ug/L ND 1.0 01/18/17 11:440.54
Chloroform ug/L ND 1.0 01/18/17 11:440.14
Chloromethane ug/L ND 1.0 01/18/17 11:440.11
cis-1,2-Dichloroethene ug/L ND 1.0 01/18/17 11:440.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/18/17 11:440.13
Dibromochloromethane ug/L ND 1.0 01/18/17 11:440.21
Dibromomethane ug/L ND 1.0 01/18/17 11:440.21
Dichlorodifluoromethane ug/L ND 1.0 01/18/17 11:440.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1912355
Associated Lab Samples:92326590001, 92326590002
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 01/18/17 11:440.12
Ethylbenzene ug/L ND 1.0 01/18/17 11:440.30
Hexachloro-1,3-butadiene ug/L ND 1.0 01/18/17 11:440.71
m&p-Xylene ug/L ND 2.0 01/18/17 11:440.66
Methyl-tert-butyl ether ug/L ND 1.0 01/18/17 11:440.21
Methylene Chloride ug/L ND 2.0 01/18/17 11:440.97
Naphthalene ug/L ND 1.0 01/18/17 11:440.24
o-Xylene ug/L ND 1.0 01/18/17 11:440.23
p-Isopropyltoluene ug/L ND 1.0 01/18/17 11:440.31
Styrene ug/L ND 1.0 01/18/17 11:440.26
Tetrachloroethene ug/L ND 1.0 01/18/17 11:440.46
Toluene ug/L ND 1.0 01/18/17 11:440.26
trans-1,2-Dichloroethene ug/L ND 1.0 01/18/17 11:440.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/18/17 11:440.26
Trichloroethene ug/L ND 1.0 01/18/17 11:440.47
Trichlorofluoromethane ug/L ND 1.0 01/18/17 11:440.20
Vinyl acetate ug/L ND 2.0 01/18/17 11:440.35
Vinyl chloride ug/L ND 1.0 01/18/17 11:440.62
Xylene (Total)ug/L ND 1.0 01/18/17 11:440.66
1,2-Dichloroethane-d4 (S)%86 70-130 01/18/17 11:44
4-Bromofluorobenzene (S)%92 70-130 01/18/17 11:44
Toluene-d8 (S)%103 70-130 01/18/17 11:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1912356LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.650 107 70-130
1,1,1-Trichloroethane ug/L 52.650 105 70-130
1,1,2,2-Tetrachloroethane ug/L 48.850 98 70-130
1,1,2-Trichloroethane ug/L 50.250 100 70-130
1,1-Dichloroethane ug/L 48.250 96 70-130
1,1-Dichloroethene ug/L 52.550 105 70-132
1,1-Dichloropropene ug/L 56.350 113 70-130
1,2,3-Trichlorobenzene ug/L 49.950 100 70-135
1,2,3-Trichloropropane ug/L 49.450 99 70-130
1,2,4-Trichlorobenzene ug/L 53.050 106 70-134
1,2-Dibromo-3-chloropropane ug/L 46.950 94 70-130
1,2-Dibromoethane (EDB)ug/L 53.450 107 70-130
1,2-Dichlorobenzene ug/L 52.050 104 70-130
1,2-Dichloroethane ug/L 47.050 94 70-130
1,2-Dichloropropane ug/L 49.750 99 70-130
1,3-Dichlorobenzene ug/L 53.050 106 70-130
1,3-Dichloropropane ug/L 53.450 107 70-130
1,4-Dichlorobenzene ug/L 51.650 103 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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[phone]
Page 13 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1912356LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 55.350 111 58-145
2-Butanone (MEK)ug/L 83.2100 83 70-145
2-Chlorotoluene ug/L 51.450 103 70-130
2-Hexanone ug/L 83.6100 84 70-144
4-Chlorotoluene ug/L 50.450 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 78.8100 79 70-140
Acetone ug/L 85.1100 85 50-175
Benzene ug/L 53.550 107 70-130
Bromobenzene ug/L 51.950 104 70-130
Bromochloromethane ug/L 49.050 98 70-130
Bromodichloromethane ug/L 50.750 101 70-130
Bromoform ug/L 43.250 86 70-130
Bromomethane ug/L 49.150 98 54-130
Carbon tetrachloride ug/L 55.450 111 70-132
Chlorobenzene ug/L 52.450 105 70-130
Chloroethane ug/L 54.750 109 64-134
Chloroform ug/L 48.250 96 70-130
Chloromethane ug/L 49.750 99 64-130
cis-1,2-Dichloroethene ug/L 46.150 92 70-131
cis-1,3-Dichloropropene ug/L 51.750 103 70-130
Dibromochloromethane ug/L 55.050 110 70-130
Dibromomethane ug/L 51.750 103 70-131
Dichlorodifluoromethane ug/L 60.550 121 56-130
Diisopropyl ether ug/L 45.750 91 70-130
Ethylbenzene ug/L 51.050 102 70-130
Hexachloro-1,3-butadiene ug/L 59.250 118 70-130
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 49.750 99 70-130
Methylene Chloride ug/L 49.650 99 63-130
Naphthalene ug/L 48.650 97 70-138
o-Xylene ug/L 50.850 102 70-130
p-Isopropyltoluene ug/L 52.650 105 70-130
Styrene ug/L 51.750 103 70-130
Tetrachloroethene ug/L 52.850 106 70-130
Toluene ug/L 48.450 97 70-130
trans-1,2-Dichloroethene ug/L 49.250 98 70-130
trans-1,3-Dichloropropene ug/L 51.350 103 70-132
Trichloroethene ug/L 56.350 113 70-130
Trichlorofluoromethane ug/L 60.250 120 62-133
Vinyl acetate ug/L 98.8100 99 66-157
Vinyl chloride ug/L 47.850 96 50-150
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%92 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 14 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1912357MATRIX SPIKE SAMPLE:
MSSpike
Result
92326419001
1,1,1,2-Tetrachloroethane ug/L 22.520 113 70-130ND
1,1,1-Trichloroethane ug/L 23.320 117 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.020 105 70-130ND
1,1,2-Trichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethane ug/L 20.920 105 70-130ND
1,1-Dichloroethene ug/L 22.620 113 70-166ND
1,1-Dichloropropene ug/L 23.920 119 70-130ND
1,2,3-Trichlorobenzene ug/L 21.320 106 70-130ND
1,2,3-Trichloropropane ug/L 21.320 107 70-130ND
1,2,4-Trichlorobenzene ug/L 23.120 115 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.220 101 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.320 107 70-130ND
1,2-Dichlorobenzene ug/L 23.320 116 70-130ND
1,2-Dichloroethane ug/L 19.220 96 70-130ND
1,2-Dichloropropane ug/L 22.420 112 70-130ND
1,3-Dichlorobenzene ug/L 23.520 117 70-130ND
1,3-Dichloropropane ug/L 21.620 108 70-130ND
1,4-Dichlorobenzene ug/L 22.620 113 70-130ND
2,2-Dichloropropane ug/L 21.520 107 70-130ND
2-Butanone (MEK)ug/L 33.640 84 70-130ND
2-Chlorotoluene ug/L 23.320 116 70-130ND
2-Hexanone ug/L 36.440 91 70-130ND
4-Chlorotoluene ug/L 23.520 117 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 86 70-130ND
Acetone ug/L 29.640 74 70-130ND
Benzene ug/L 23.320 116 70-148ND
Bromobenzene ug/L 23.420 117 70-130ND
Bromochloromethane ug/L 20.520 102 70-130ND
Bromodichloromethane ug/L 22.220 111 70-130ND
Bromoform ug/L 19.220 96 70-130ND
Bromomethane ug/L 16.820 84 70-130ND
Carbon tetrachloride ug/L 24.920 124 70-130ND
Chlorobenzene ug/L 23.520 117 70-146ND
Chloroethane ug/L 22.220 111 70-130ND
Chloroform ug/L 21.120 106 70-130ND
Chloromethane ug/L 17.820 89 70-130ND
cis-1,2-Dichloroethene ug/L 19.720 98 70-130ND
cis-1,3-Dichloropropene ug/L 20.620 103 70-130ND
Dibromochloromethane ug/L 21.020 105 70-130ND
Dibromomethane ug/L 22.720 113 70-130ND
Dichlorodifluoromethane ug/L 14.020 70 70-130ND
Diisopropyl ether ug/L 18.620 93 70-130ND
Ethylbenzene ug/L 23.520 118 70-130ND
Hexachloro-1,3-butadiene ug/L 23.820 119 70-130ND
m&p-Xylene ug/L 46.440 116 70-130ND
Methyl-tert-butyl ether ug/L 19.720 98 70-130ND
Methylene Chloride ug/L 20.920 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 15 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1912357MATRIX SPIKE SAMPLE:
MSSpike
Result
92326419001
Naphthalene ug/L 20.720 104 70-130ND
o-Xylene ug/L 23.120 115 70-130ND
p-Isopropyltoluene ug/L 22.320 111 70-130ND
Styrene ug/L 23.020 115 70-130ND
Tetrachloroethene ug/L 23.420 117 70-130ND
Toluene ug/L 23.120 115 70-155ND
trans-1,2-Dichloroethene ug/L 21.620 108 70-130ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-130ND
Trichloroethene ug/L 24.920 124 69-151ND
Trichlorofluoromethane ug/L 25.020 125 70-130ND
Vinyl acetate ug/L 31.340 78 70-130ND
Vinyl chloride ug/L 17.720 88 70-130ND
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92326419002
1912358SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 16 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92326419002
1912358SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%84 084
4-Bromofluorobenzene (S)%91 596
Toluene-d8 (S)%104 2105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344509
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92326590001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1911411
Associated Lab Samples:92326590001
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 01/17/17 12:231.9
1,2-Dichlorobenzene ug/L ND 10.0 01/17/17 12:231.2
1,3-Dichlorobenzene ug/L ND 10.0 01/17/17 12:231.1
1,4-Dichlorobenzene ug/L ND 10.0 01/17/17 12:231.2
1-Methylnaphthalene ug/L ND 10.0 01/17/17 12:230.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 01/17/17 12:231.6
2,4,5-Trichlorophenol ug/L ND 10.0 01/17/17 12:232.2
2,4,6-Trichlorophenol ug/L ND 10.0 01/17/17 12:231.9
2,4-Dichlorophenol ug/L ND 10.0 01/17/17 12:231.7
2,4-Dimethylphenol ug/L ND 10.0 01/17/17 12:232.2
2,4-Dinitrophenol ug/L ND 50.0 01/17/17 12:236.5
2,4-Dinitrotoluene ug/L ND 10.0 01/17/17 12:231.2
2,6-Dinitrotoluene ug/L ND 10.0 01/17/17 12:231.7
2-Chloronaphthalene ug/L ND 10.0 01/17/17 12:232.2
2-Chlorophenol ug/L ND 10.0 01/17/17 12:231.5
2-Methylnaphthalene ug/L ND 10.0 01/17/17 12:230.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 01/17/17 12:231.7
2-Nitroaniline ug/L ND 50.0 01/17/17 12:232.8
2-Nitrophenol ug/L ND 10.0 01/17/17 12:231.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 01/17/17 12:231.7
3,3'-Dichlorobenzidine ug/L ND 20.0 01/17/17 12:231.4
3-Nitroaniline ug/L ND 50.0 01/17/17 12:232.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/17/17 12:231.7
4-Bromophenylphenyl ether ug/L ND 10.0 01/17/17 12:231.3
4-Chloro-3-methylphenol ug/L ND 20.0 01/17/17 12:234.2
4-Chloroaniline ug/L ND 20.0 01/17/17 12:233.4
4-Chlorophenylphenyl ether ug/L ND 10.0 01/17/17 12:232.1
4-Nitroaniline ug/L ND 20.0 01/17/17 12:232.5
4-Nitrophenol ug/L ND 50.0 01/17/17 12:235.8
Acenaphthene ug/L ND 10.0 01/17/17 12:230.25
Acenaphthylene ug/L ND 10.0 01/17/17 12:230.21
Aniline ug/L ND 10.0 01/17/17 12:231.3
Anthracene ug/L ND 10.0 01/17/17 12:230.14
Benzo(a)anthracene ug/L ND 10.0 01/17/17 12:230.33
Benzo(a)pyrene ug/L ND 10.0 01/17/17 12:230.30
Benzo(b)fluoranthene ug/L ND 10.0 01/17/17 12:230.28
Benzo(g,h,i)perylene ug/L ND 10.0 01/17/17 12:230.38
Benzo(k)fluoranthene ug/L ND 10.0 01/17/17 12:230.43
Benzoic Acid ug/L ND 50.0 01/17/17 12:2311.1
Benzyl alcohol ug/L ND 20.0 01/17/17 12:233.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/17/17 12:231.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1911411
Associated Lab Samples:92326590001
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 01/17/17 12:231.5
bis(2-Ethylhexyl)phthalate ug/L 1.6J 6.0 01/17/17 12:230.85
Butylbenzylphthalate ug/L 1.1J 10.0 01/17/17 12:230.75
Chrysene ug/L ND 10.0 01/17/17 12:230.21
Di-n-butylphthalate ug/L ND 10.0 01/17/17 12:231.1
Di-n-octylphthalate ug/L ND 10.0 01/17/17 12:230.86
Dibenz(a,h)anthracene ug/L ND 10.0 01/17/17 12:230.55
Dibenzofuran ug/L ND 10.0 01/17/17 12:231.8
Diethylphthalate ug/L ND 10.0 01/17/17 12:231.3
Dimethylphthalate ug/L ND 10.0 01/17/17 12:231.5
Fluoranthene ug/L ND 10.0 01/17/17 12:230.21
Fluorene ug/L ND 10.0 01/17/17 12:230.21
Hexachloro-1,3-butadiene ug/L ND 10.0 01/17/17 12:231.8
Hexachlorobenzene ug/L ND 10.0 01/17/17 12:231.1
Hexachlorocyclopentadiene ug/L ND 10.0 01/17/17 12:231.8
Hexachloroethane ug/L ND 10.0 01/17/17 12:231.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 01/17/17 12:230.29
Isophorone ug/L ND 10.0 01/17/17 12:231.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 01/17/17 12:232.1
N-Nitrosodimethylamine ug/L ND 10.0 01/17/17 12:231.3
N-Nitrosodiphenylamine ug/L ND 10.0 01/17/17 12:231.3
Naphthalene ug/L ND 10.0 01/17/17 12:230.34
Nitrobenzene ug/L ND 10.0 01/17/17 12:231.7
Pentachlorophenol ug/L ND 25.0 01/17/17 12:232.3
Phenanthrene ug/L ND 10.0 01/17/17 12:230.22
Phenol ug/L ND 10.0 01/17/17 12:231.7
Pyrene ug/L ND 10.0 01/17/17 12:230.19
2,4,6-Tribromophenol (S)%57 27-110 01/17/17 12:23
2-Fluorobiphenyl (S)%56 27-110 01/17/17 12:23
2-Fluorophenol (S)%35 12-110 01/17/17 12:23
Nitrobenzene-d5 (S)%57 21-110 01/17/17 12:23
Phenol-d6 (S)%22 10-110 01/17/17 12:23
Terphenyl-d14 (S)%66 31-107 01/17/17 12:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1911412LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1911413
1,2,4-Trichlorobenzene ug/L 28.750 57 31-1205427.1 6 30
1,2-Dichlorobenzene ug/L 26.950 54 38-1205225.9 4 30
1,3-Dichlorobenzene ug/L 26.150 52 30-1225025.0 4 30
1,4-Dichlorobenzene ug/L 25.850 52 37-1204824.2 7 30
1-Methylnaphthalene ug/L 31.350 63 34-1135829.1 7 30
2,2'-Oxybis(1-chloropropane)ug/L 34.650 69 18-1206532.5 6 30
2,4,5-Trichlorophenol ug/L 29.650 59 43-1135628.2 5 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1911412LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1911413
2,4,6-Trichlorophenol ug/L 38.450 77 42-1207336.5 5 30
2,4-Dichlorophenol ug/L 35.250 70 30-1206633.1 6 30
2,4-Dimethylphenol ug/L 36.350 73 29-1116834.2 6 30
2,4-Dinitrophenol ug/L 157250 63 19-13259147 7 30
2,4-Dinitrotoluene ug/L 34.850 70 58-1286834.0 3 30
2,6-Dinitrotoluene ug/L 34.850 70 54-1296733.6 4 30
2-Chloronaphthalene ug/L 32.950 66 43-1176231.1 6 30
2-Chlorophenol ug/L 32.350 65 37-1206231.1 4 30
2-Methylnaphthalene ug/L 31.950 64 33-1206130.3 5 30
2-Methylphenol(o-Cresol)ug/L 25.450 51 31-1204924.5 4 30
2-Nitroaniline ug/L 74.1100 74 48-1216968.9 7 30
2-Nitrophenol ug/L 35.050 70 25-1166834.0 3 30
3&4-Methylphenol(m&p Cresol)ug/L 23.550 47 23-1204522.3 5 30
3,3'-Dichlorobenzidine ug/L 69.0100 69 10-1546766.7 3 30
3-Nitroaniline ug/L 72.0100 72 43-1156969.1 4 30
4,6-Dinitro-2-methylphenol ug/L 86.8100 87 44-1248382.5 5 30
4-Bromophenylphenyl ether ug/L 31.850 64 34-1136030.0 6 30
4-Chloro-3-methylphenol ug/L 71.6100 72 31-1106766.6 7 30
4-Chloroaniline ug/L 66.5100 67 20-1206161.2 8 30
4-Chlorophenylphenyl ether ug/L 31.450 63 34-1166030.1 5 30
4-Nitroaniline ug/L 77.9100 78 46-1287473.8 5 30
4-Nitrophenol ug/L 93.4250 37 11-1203689.9 4 30
Acenaphthene ug/L 32.450 65 48-1146130.6 6 30
Acenaphthylene ug/L 33.650 67 48-1126431.8 6 30
Aniline ug/L 26.050 52 26-1204823.8 9 30
Anthracene ug/L 33.350 67 57-1186432.0 4 30
Benzo(a)anthracene ug/L 35.150 70 56-1216934.6 1 30
Benzo(a)pyrene ug/L 34.350 69 55-1276633.2 3 30
Benzo(b)fluoranthene ug/L 35.550 71 53-1286934.3 3 30
Benzo(g,h,i)perylene ug/L 35.150 70 54-1256733.6 4 30
Benzo(k)fluoranthene ug/L 34.550 69 51-1236733.7 2 30
Benzoic Acid ug/L 63.7250 25 10-1202563.7 0 30
Benzyl alcohol ug/L 60.5100 60 27-1205656.0 8 30
bis(2-Chloroethoxy)methane ug/L 32.750 65 32-1206130.5 7 30
bis(2-Chloroethyl) ether ug/L 29.750 59 33-1115829.2 2 30
bis(2-Ethylhexyl)phthalate ug/L 41.250 82 50-1458040.2 2 30
Butylbenzylphthalate ug/L 39.650 79 54-1387638.1 4 30
Chrysene ug/L 34.250 68 58-1276733.3 3 30
Di-n-butylphthalate ug/L 40.550 81 56-1257638.1 6 30
Di-n-octylphthalate ug/L 42.350 85 50-1348341.4 2 30
Dibenz(a,h)anthracene ug/L 38.550 77 53-1297236.0 7 30
Dibenzofuran ug/L 32.050 64 45-1206130.5 5 30
Diethylphthalate ug/L 38.150 76 53-1207336.5 4 30
Dimethylphthalate ug/L 36.150 72 55-1166833.9 6 30
Fluoranthene ug/L 36.250 72 57-1256934.6 4 30
Fluorene ug/L 33.550 67 53-1186331.5 6 30
Hexachloro-1,3-butadiene ug/L 27.050 54 23-1205225.8 5 30
REPORT OF LABORATORY ANALYSIS
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Page 20 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1911412LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1911413
Hexachlorobenzene ug/L 33.050 66 49-1166431.9 3 30
Hexachlorocyclopentadiene ug/L 33.950 68 26-1586532.5 4 30
Hexachloroethane ug/L 26.050 52 30-1144924.7 5 30
Indeno(1,2,3-cd)pyrene ug/L 36.350 73 55-1287135.4 3 30
Isophorone ug/L 34.550 69 31-1186331.4 10 30
N-Nitroso-di-n-propylamine ug/L 36.850 74 32-1196733.6 9 30
N-Nitrosodimethylamine ug/L 23.150 46 13-1204321.4 8 30
N-Nitrosodiphenylamine ug/L 32.950 66 43-1206231.2 5 30
Naphthalene ug/L 29.950 60 32-1205628.0 7 30
Nitrobenzene ug/L 33.450 67 33-1106331.5 6 30
Pentachlorophenol ug/L 87.4100 87 10-1378685.7 2 30
Phenanthrene ug/L 34.450 69 57-1176532.6 5 30
Phenol ug/L 14.650 29 10-1202814.0 4 30
Pyrene ug/L 33.150 66 55-1226331.7 4 30
2,4,6-Tribromophenol (S)%69 27-11065
2-Fluorobiphenyl (S)%63 27-11061
2-Fluorophenol (S)%41 12-11039
Nitrobenzene-d5 (S)%66 21-11063
Phenol-d6 (S)%28 10-11027
Terphenyl-d14 (S)%67 31-10761
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 21 of 26
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 22 of 26
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92326590
CAROLINA FOUNDRY 71167563
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92326590001 344820 345007GW-01 EPA 3010A EPA 6010
92326590001 345129 345182GW-01 EPA 7470 EPA 7470
92326590001 344509 344558GW-01 EPA 3510 EPA 8270
92326590001 344697GW-01 EPA 8260
92326590002 344697TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:03 AM
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Page 23 of 26
Page 24 of 26
Page 25 of 26
Page 26 of 26
#=CL#
January 30, 2017
LIMS USE: FR - HALEY HINDES
LIMS OBJECT ID: 92325998
92325998
Project:
Pace Project No.:
RE:
Haley Hindes
Terracon NC
2020 Starita Rd
Suite E
Charlotte, NC 28206
71167563
Dear Haley Hindes:
Enclosed are the analytical results for sample(s) received by the laboratory on January 11, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Report revised 1/30/17 to add MDLs and J-flags.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325998
71167563
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 34
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325998
71167563
Lab ID Sample ID Matrix Date Collected Date Received
92325998001 GW-03 Water 01/10/17 15:45 01/11/17 15:57
92325998002 GW-02 Water 01/11/17 10:45 01/11/17 15:57
92325998003 DUP-02-011117 Water 01/11/17 00:00 01/11/17 15:57
92325998004 TRIP BLANK Water 01/03/17 00:00 01/11/17 15:57
REPORT OF LABORATORY ANALYSIS
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Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325998
71167563
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325998001 GW-03 EPA 6010 10 PASI-ASER
EPA 7470 1 PASI-AWAB
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92325998002 GW-02 EPA 6010 10 PASI-ASER
EPA 7470 1 PASI-AWAB
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92325998003 DUP-02-011117 EPA 6010 10 PASI-ASER
EPA 7470 1 PASI-AWAB
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92325998004 TRIP BLANK EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-03 Lab ID: 92325998001 Collected: 01/10/17 15:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Aluminum 950 ug/L 01/17/17 02:21 7429-90-5 M101/13/17 00:45100 50.0 1
Arsenic ND ug/L 01/17/17 02:21 7440-38-201/13/17 00:4510.0 5.0 1
Barium 37.0 ug/L 01/17/17 02:21 7440-39-301/13/17 00:455.0 2.5 1
Cadmium ND ug/L 01/17/17 02:21 7440-43-901/13/17 00:451.0 0.50 1
Chromium 4.5J ug/L 01/17/17 02:21 7440-47-301/13/17 00:455.0 2.5 1
Copper 6.3 ug/L 01/17/17 02:21 7440-50-801/13/17 00:455.0 2.5 1
Lead 2.7J ug/L 01/17/17 02:21 7439-92-101/13/17 00:455.0 2.5 1
Selenium ND ug/L 01/17/17 02:21 7782-49-201/13/17 00:4510.0 5.0 1
Silver ND ug/L 01/17/17 02:21 7440-22-401/13/17 00:455.0 2.5 1
Zinc 15.9 ug/L 01/17/17 02:21 7440-66-601/13/17 00:4510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/16/17 12:18 7439-97-601/13/17 12:350.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/17/17 14:08 83-32-901/13/17 15:1910.0 0.25 1
Acenaphthylene ND ug/L 01/17/17 14:08 208-96-801/13/17 15:1910.0 0.21 1
Aniline ND ug/L 01/17/17 14:08 62-53-301/13/17 15:1910.0 1.3 1
Anthracene ND ug/L 01/17/17 14:08 120-12-701/13/17 15:1910.0 0.14 1
Benzo(a)anthracene ND ug/L 01/17/17 14:08 56-55-301/13/17 15:1910.0 0.33 1
Benzo(a)pyrene ND ug/L 01/17/17 14:08 50-32-801/13/17 15:1910.0 0.30 1
Benzo(b)fluoranthene ND ug/L 01/17/17 14:08 205-99-201/13/17 15:1910.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 01/17/17 14:08 191-24-201/13/17 15:1910.0 0.38 1
Benzo(k)fluoranthene ND ug/L 01/17/17 14:08 207-08-901/13/17 15:1910.0 0.43 1
Benzoic Acid ND ug/L 01/17/17 14:08 65-85-001/13/17 15:1950.0 11.1 1
Benzyl alcohol ND ug/L 01/17/17 14:08 100-51-601/13/17 15:1920.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 01/17/17 14:08 101-55-301/13/17 15:1910.0 1.3 1
Butylbenzylphthalate ND ug/L 01/17/17 14:08 85-68-701/13/17 15:1910.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 01/17/17 14:08 59-50-701/13/17 15:1920.0 4.2 1
4-Chloroaniline ND ug/L 01/17/17 14:08 106-47-801/13/17 15:1920.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 01/17/17 14:08 111-91-101/13/17 15:1910.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 01/17/17 14:08 111-44-401/13/17 15:1910.0 1.5 1
2-Chloronaphthalene ND ug/L 01/17/17 14:08 91-58-701/13/17 15:1910.0 2.2 1
2-Chlorophenol ND ug/L 01/17/17 14:08 95-57-801/13/17 15:1910.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 01/17/17 14:08 7005-72-301/13/17 15:1910.0 2.1 1
Chrysene ND ug/L 01/17/17 14:08 218-01-901/13/17 15:1910.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 01/17/17 14:08 53-70-301/13/17 15:1910.0 0.55 1
Dibenzofuran ND ug/L 01/17/17 14:08 132-64-901/13/17 15:1910.0 1.8 1
1,2-Dichlorobenzene ND ug/L 01/17/17 14:08 95-50-101/13/17 15:1910.0 1.2 1
1,3-Dichlorobenzene ND ug/L 01/17/17 14:08 541-73-101/13/17 15:1910.0 1.1 1
1,4-Dichlorobenzene ND ug/L 01/17/17 14:08 106-46-701/13/17 15:1910.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 01/17/17 14:08 91-94-101/13/17 15:1920.0 1.4 1
2,4-Dichlorophenol ND ug/L 01/17/17 14:08 120-83-201/13/17 15:1910.0 1.7 1
Diethylphthalate ND ug/L 01/17/17 14:08 84-66-201/13/17 15:1910.0 1.3 1
2,4-Dimethylphenol ND ug/L 01/17/17 14:08 105-67-901/13/17 15:1910.0 2.2 1
Dimethylphthalate ND ug/L 01/17/17 14:08 131-11-301/13/17 15:1910.0 1.5 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-03 Lab ID: 92325998001 Collected: 01/10/17 15:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Di-n-butylphthalate ND ug/L 01/17/17 14:08 84-74-201/13/17 15:1910.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 01/17/17 14:08 534-52-101/13/17 15:1920.0 1.7 1
2,4-Dinitrophenol ND ug/L 01/17/17 14:08 51-28-501/13/17 15:1950.0 6.5 1
2,4-Dinitrotoluene ND ug/L 01/17/17 14:08 121-14-201/13/17 15:1910.0 1.2 1
2,6-Dinitrotoluene ND ug/L 01/17/17 14:08 606-20-201/13/17 15:1910.0 1.7 1
Di-n-octylphthalate ND ug/L 01/17/17 14:08 117-84-001/13/17 15:1910.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/17/17 14:08 117-81-701/13/17 15:196.0 0.85 1
Fluoranthene ND ug/L 01/17/17 14:08 206-44-001/13/17 15:1910.0 0.21 1
Fluorene ND ug/L 01/17/17 14:08 86-73-701/13/17 15:1910.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 01/17/17 14:08 87-68-301/13/17 15:1910.0 1.8 1
Hexachlorobenzene ND ug/L 01/17/17 14:08 118-74-101/13/17 15:1910.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 01/17/17 14:08 77-47-401/13/17 15:1910.0 1.8 1
Hexachloroethane ND ug/L 01/17/17 14:08 67-72-101/13/17 15:1910.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/17/17 14:08 193-39-501/13/17 15:1910.0 0.29 1
Isophorone ND ug/L 01/17/17 14:08 78-59-101/13/17 15:1910.0 1.8 1
1-Methylnaphthalene ND ug/L 01/17/17 14:08 90-12-001/13/17 15:1910.0 0.32 1
2-Methylnaphthalene ND ug/L 01/17/17 14:08 91-57-601/13/17 15:1910.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 01/17/17 14:08 95-48-701/13/17 15:1910.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/17/17 14:0801/13/17 15:1910.0 1.7 1
Naphthalene ND ug/L 01/17/17 14:08 91-20-301/13/17 15:1910.0 0.34 1
2-Nitroaniline ND ug/L 01/17/17 14:08 88-74-401/13/17 15:1950.0 2.8 1
3-Nitroaniline ND ug/L 01/17/17 14:08 99-09-201/13/17 15:1950.0 2.4 1
4-Nitroaniline ND ug/L 01/17/17 14:08 100-01-601/13/17 15:1920.0 2.5 1
Nitrobenzene ND ug/L 01/17/17 14:08 98-95-301/13/17 15:1910.0 1.7 1
2-Nitrophenol ND ug/L 01/17/17 14:08 88-75-501/13/17 15:1910.0 1.7 1
4-Nitrophenol ND ug/L 01/17/17 14:08 100-02-701/13/17 15:1950.0 5.8 1
N-Nitrosodimethylamine ND ug/L 01/17/17 14:08 62-75-901/13/17 15:1910.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 01/17/17 14:08 621-64-701/13/17 15:1910.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 01/17/17 14:08 86-30-601/13/17 15:1910.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/17/17 14:08 108-60-101/13/17 15:1910.0 1.6 1
Pentachlorophenol ND ug/L 01/17/17 14:08 87-86-501/13/17 15:1925.0 2.3 1
Phenanthrene ND ug/L 01/17/17 14:08 85-01-801/13/17 15:1910.0 0.22 1
Phenol ND ug/L 01/17/17 14:0801/13/17 15:1910.0 1.7 1
Pyrene ND ug/L 01/17/17 14:08 129-00-001/13/17 15:1910.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 01/17/17 14:08 120-82-101/13/17 15:1910.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 01/17/17 14:08 95-95-401/13/17 15:1910.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 01/17/17 14:08 88-06-201/13/17 15:1910.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)46 %01/17/17 14:08 4165-60-001/13/17 15:1921-110 1
2-Fluorobiphenyl (S)48 %01/17/17 14:08 321-60-801/13/17 15:1927-110 1
Terphenyl-d14 (S)66 %01/17/17 14:08 1718-51-001/13/17 15:1931-107 1
Phenol-d6 (S)18 %01/17/17 14:08 13127-88-301/13/17 15:1910-110 1
2-Fluorophenol (S)27 %01/17/17 14:08 367-12-401/13/17 15:1912-110 1
2,4,6-Tribromophenol (S)60 %01/17/17 14:08 118-79-601/13/17 15:1927-110 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-03 Lab ID: 92325998001 Collected: 01/10/17 15:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 01/12/17 18:58 67-64-125.0 10.0 1
Benzene ND ug/L 01/12/17 18:58 71-43-21.0 0.25 1
Bromobenzene ND ug/L 01/12/17 18:58 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 01/12/17 18:58 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 01/12/17 18:58 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/17 18:58 75-25-21.0 0.26 1
Bromomethane ND ug/L 01/12/17 18:58 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/17 18:58 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 01/12/17 18:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/17 18:58 108-90-71.0 0.23 1
Chloroethane ND ug/L 01/12/17 18:58 75-00-31.0 0.54 1
Chloroform ND ug/L 01/12/17 18:58 67-66-31.0 0.14 1
Chloromethane ND ug/L 01/12/17 18:58 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 01/12/17 18:58 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 01/12/17 18:58 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/17 18:58 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 01/12/17 18:58 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/17 18:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/17 18:58 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/17 18:58 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 01/12/17 18:58 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 01/12/17 18:58 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 01/12/17 18:58 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 01/12/17 18:58 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/17 18:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/17 18:58 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/17 18:58 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/12/17 18:58 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/17 18:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 01/12/17 18:58 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 01/12/17 18:58 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 01/12/17 18:58 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 01/12/17 18:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/17 18:58 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 01/12/17 18:58 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 01/12/17 18:58 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 01/12/17 18:58 87-68-31.0 0.71 1
2-Hexanone ND ug/L 01/12/17 18:58 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 01/12/17 18:58 99-87-61.0 0.31 1
Methylene Chloride 1.9J ug/L 01/12/17 18:58 75-09-2 C92.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/17 18:58 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 01/12/17 18:58 1634-04-41.0 0.21 1
Naphthalene ND ug/L 01/12/17 18:58 91-20-31.0 0.24 1
Styrene ND ug/L 01/12/17 18:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/17 18:58 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/17 18:58 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-03 Lab ID: 92325998001 Collected: 01/10/17 15:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 01/12/17 18:58 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/17 18:58 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 01/12/17 18:58 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 01/12/17 18:58 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 01/12/17 18:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/17 18:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/17 18:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/17 18:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/17 18:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/17 18:58 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 01/12/17 18:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/17 18:58 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 01/12/17 18:58 179601-23-12.0 0.66 1
o-Xylene ND ug/L 01/12/17 18:58 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)101 %01/12/17 18:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %01/12/17 18:58 17060-07-070-130 1
Toluene-d8 (S)107 %01/12/17 18:58 2037-26-570-130 1
Sample: GW-02 Lab ID: 92325998002 Collected: 01/11/17 10:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Aluminum 401 ug/L 01/17/17 02:39 7429-90-501/13/17 00:45100 50.0 1
Arsenic ND ug/L 01/17/17 02:39 7440-38-201/13/17 00:4510.0 5.0 1
Barium 55.8 ug/L 01/17/17 02:39 7440-39-301/13/17 00:455.0 2.5 1
Cadmium ND ug/L 01/17/17 02:39 7440-43-901/13/17 00:451.0 0.50 1
Chromium ND ug/L 01/17/17 02:39 7440-47-301/13/17 00:455.0 2.5 1
Copper 48.8 ug/L 01/17/17 02:39 7440-50-801/13/17 00:455.0 2.5 1
Lead ND ug/L 01/17/17 02:39 7439-92-101/13/17 00:455.0 2.5 1
Selenium ND ug/L 01/17/17 02:39 7782-49-201/13/17 00:4510.0 5.0 1
Silver ND ug/L 01/17/17 02:39 7440-22-401/13/17 00:455.0 2.5 1
Zinc 108 ug/L 01/17/17 02:39 7440-66-601/13/17 00:4510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/16/17 12:25 7439-97-601/13/17 12:350.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/17/17 14:33 83-32-901/13/17 15:1910.0 0.25 1
Acenaphthylene ND ug/L 01/17/17 14:33 208-96-801/13/17 15:1910.0 0.21 1
Aniline ND ug/L 01/17/17 14:33 62-53-301/13/17 15:1910.0 1.3 1
Anthracene ND ug/L 01/17/17 14:33 120-12-701/13/17 15:1910.0 0.14 1
Benzo(a)anthracene ND ug/L 01/17/17 14:33 56-55-301/13/17 15:1910.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-02 Lab ID: 92325998002 Collected: 01/11/17 10:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)pyrene ND ug/L 01/17/17 14:33 50-32-801/13/17 15:1910.0 0.30 1
Benzo(b)fluoranthene ND ug/L 01/17/17 14:33 205-99-201/13/17 15:1910.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 01/17/17 14:33 191-24-201/13/17 15:1910.0 0.38 1
Benzo(k)fluoranthene ND ug/L 01/17/17 14:33 207-08-901/13/17 15:1910.0 0.43 1
Benzoic Acid ND ug/L 01/17/17 14:33 65-85-001/13/17 15:1950.0 11.1 1
Benzyl alcohol ND ug/L 01/17/17 14:33 100-51-601/13/17 15:1920.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 01/17/17 14:33 101-55-301/13/17 15:1910.0 1.3 1
Butylbenzylphthalate ND ug/L 01/17/17 14:33 85-68-701/13/17 15:1910.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 01/17/17 14:33 59-50-701/13/17 15:1920.0 4.2 1
4-Chloroaniline ND ug/L 01/17/17 14:33 106-47-801/13/17 15:1920.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 01/17/17 14:33 111-91-101/13/17 15:1910.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 01/17/17 14:33 111-44-401/13/17 15:1910.0 1.5 1
2-Chloronaphthalene ND ug/L 01/17/17 14:33 91-58-701/13/17 15:1910.0 2.2 1
2-Chlorophenol ND ug/L 01/17/17 14:33 95-57-801/13/17 15:1910.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 01/17/17 14:33 7005-72-301/13/17 15:1910.0 2.1 1
Chrysene ND ug/L 01/17/17 14:33 218-01-901/13/17 15:1910.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 01/17/17 14:33 53-70-301/13/17 15:1910.0 0.55 1
Dibenzofuran ND ug/L 01/17/17 14:33 132-64-901/13/17 15:1910.0 1.8 1
1,2-Dichlorobenzene ND ug/L 01/17/17 14:33 95-50-101/13/17 15:1910.0 1.2 1
1,3-Dichlorobenzene ND ug/L 01/17/17 14:33 541-73-101/13/17 15:1910.0 1.1 1
1,4-Dichlorobenzene ND ug/L 01/17/17 14:33 106-46-701/13/17 15:1910.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 01/17/17 14:33 91-94-101/13/17 15:1920.0 1.4 1
2,4-Dichlorophenol ND ug/L 01/17/17 14:33 120-83-201/13/17 15:1910.0 1.7 1
Diethylphthalate ND ug/L 01/17/17 14:33 84-66-201/13/17 15:1910.0 1.3 1
2,4-Dimethylphenol ND ug/L 01/17/17 14:33 105-67-901/13/17 15:1910.0 2.2 1
Dimethylphthalate ND ug/L 01/17/17 14:33 131-11-301/13/17 15:1910.0 1.5 1
Di-n-butylphthalate ND ug/L 01/17/17 14:33 84-74-201/13/17 15:1910.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 01/17/17 14:33 534-52-101/13/17 15:1920.0 1.7 1
2,4-Dinitrophenol ND ug/L 01/17/17 14:33 51-28-501/13/17 15:1950.0 6.5 1
2,4-Dinitrotoluene ND ug/L 01/17/17 14:33 121-14-201/13/17 15:1910.0 1.2 1
2,6-Dinitrotoluene ND ug/L 01/17/17 14:33 606-20-201/13/17 15:1910.0 1.7 1
Di-n-octylphthalate ND ug/L 01/17/17 14:33 117-84-001/13/17 15:1910.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/17/17 14:33 117-81-701/13/17 15:196.0 0.85 1
Fluoranthene ND ug/L 01/17/17 14:33 206-44-001/13/17 15:1910.0 0.21 1
Fluorene ND ug/L 01/17/17 14:33 86-73-701/13/17 15:1910.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 01/17/17 14:33 87-68-301/13/17 15:1910.0 1.8 1
Hexachlorobenzene ND ug/L 01/17/17 14:33 118-74-101/13/17 15:1910.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 01/17/17 14:33 77-47-401/13/17 15:1910.0 1.8 1
Hexachloroethane ND ug/L 01/17/17 14:33 67-72-101/13/17 15:1910.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/17/17 14:33 193-39-501/13/17 15:1910.0 0.29 1
Isophorone ND ug/L 01/17/17 14:33 78-59-101/13/17 15:1910.0 1.8 1
1-Methylnaphthalene ND ug/L 01/17/17 14:33 90-12-001/13/17 15:1910.0 0.32 1
2-Methylnaphthalene ND ug/L 01/17/17 14:33 91-57-601/13/17 15:1910.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 01/17/17 14:33 95-48-701/13/17 15:1910.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/17/17 14:3301/13/17 15:1910.0 1.7 1
Naphthalene ND ug/L 01/17/17 14:33 91-20-301/13/17 15:1910.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-02 Lab ID: 92325998002 Collected: 01/11/17 10:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitroaniline ND ug/L 01/17/17 14:33 88-74-401/13/17 15:1950.0 2.8 1
3-Nitroaniline ND ug/L 01/17/17 14:33 99-09-201/13/17 15:1950.0 2.4 1
4-Nitroaniline ND ug/L 01/17/17 14:33 100-01-601/13/17 15:1920.0 2.5 1
Nitrobenzene ND ug/L 01/17/17 14:33 98-95-301/13/17 15:1910.0 1.7 1
2-Nitrophenol ND ug/L 01/17/17 14:33 88-75-501/13/17 15:1910.0 1.7 1
4-Nitrophenol ND ug/L 01/17/17 14:33 100-02-701/13/17 15:1950.0 5.8 1
N-Nitrosodimethylamine ND ug/L 01/17/17 14:33 62-75-901/13/17 15:1910.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 01/17/17 14:33 621-64-701/13/17 15:1910.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 01/17/17 14:33 86-30-601/13/17 15:1910.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/17/17 14:33 108-60-101/13/17 15:1910.0 1.6 1
Pentachlorophenol ND ug/L 01/17/17 14:33 87-86-501/13/17 15:1925.0 2.3 1
Phenanthrene ND ug/L 01/17/17 14:33 85-01-801/13/17 15:1910.0 0.22 1
Phenol ND ug/L 01/17/17 14:3301/13/17 15:1910.0 1.7 1
Pyrene ND ug/L 01/17/17 14:33 129-00-001/13/17 15:1910.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 01/17/17 14:33 120-82-101/13/17 15:1910.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 01/17/17 14:33 95-95-401/13/17 15:1910.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 01/17/17 14:33 88-06-201/13/17 15:1910.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)74 %01/17/17 14:33 4165-60-001/13/17 15:1921-110 1
2-Fluorobiphenyl (S)76 %01/17/17 14:33 321-60-801/13/17 15:1927-110 1
Terphenyl-d14 (S)73 %01/17/17 14:33 1718-51-001/13/17 15:1931-107 1
Phenol-d6 (S)27 %01/17/17 14:33 13127-88-301/13/17 15:1910-110 1
2-Fluorophenol (S)42 %01/17/17 14:33 367-12-401/13/17 15:1912-110 1
2,4,6-Tribromophenol (S)86 %01/17/17 14:33 118-79-601/13/17 15:1927-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 01/12/17 19:16 67-64-125.0 10.0 1
Benzene ND ug/L 01/12/17 19:16 71-43-21.0 0.25 1
Bromobenzene ND ug/L 01/12/17 19:16 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 01/12/17 19:16 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 01/12/17 19:16 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/17 19:16 75-25-21.0 0.26 1
Bromomethane ND ug/L 01/12/17 19:16 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/17 19:16 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 01/12/17 19:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/17 19:16 108-90-71.0 0.23 1
Chloroethane ND ug/L 01/12/17 19:16 75-00-31.0 0.54 1
Chloroform ND ug/L 01/12/17 19:16 67-66-31.0 0.14 1
Chloromethane ND ug/L 01/12/17 19:16 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 01/12/17 19:16 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 01/12/17 19:16 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/17 19:16 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 01/12/17 19:16 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/17 19:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/17 19:16 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/17 19:16 95-50-11.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: GW-02 Lab ID: 92325998002 Collected: 01/11/17 10:45 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,3-Dichlorobenzene ND ug/L 01/12/17 19:16 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 01/12/17 19:16 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 01/12/17 19:16 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 01/12/17 19:16 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/17 19:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/17 19:16 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/17 19:16 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/12/17 19:16 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/17 19:16 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 01/12/17 19:16 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 01/12/17 19:16 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 01/12/17 19:16 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 01/12/17 19:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/17 19:16 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 01/12/17 19:16 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 01/12/17 19:16 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 01/12/17 19:16 87-68-31.0 0.71 1
2-Hexanone ND ug/L 01/12/17 19:16 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 01/12/17 19:16 99-87-61.0 0.31 1
Methylene Chloride 2.0 ug/L 01/12/17 19:16 75-09-2 C92.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/17 19:16 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 01/12/17 19:16 1634-04-41.0 0.21 1
Naphthalene ND ug/L 01/12/17 19:16 91-20-31.0 0.24 1
Styrene 0.30J ug/L 01/12/17 19:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/17 19:16 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/17 19:16 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 01/12/17 19:16 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/17 19:16 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 01/12/17 19:16 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 01/12/17 19:16 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 01/12/17 19:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/17 19:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/17 19:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/17 19:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/17 19:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/17 19:16 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 01/12/17 19:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/17 19:16 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 01/12/17 19:16 179601-23-12.0 0.66 1
o-Xylene ND ug/L 01/12/17 19:16 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)101 %01/12/17 19:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %01/12/17 19:16 17060-07-070-130 1
Toluene-d8 (S)105 %01/12/17 19:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: DUP-02-011117 Lab ID: 92325998003 Collected: 01/11/17 00:00 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Aluminum 420 ug/L 01/17/17 02:42 7429-90-501/13/17 00:45100 50.0 1
Arsenic ND ug/L 01/17/17 02:42 7440-38-201/13/17 00:4510.0 5.0 1
Barium 55.6 ug/L 01/17/17 02:42 7440-39-301/13/17 00:455.0 2.5 1
Cadmium ND ug/L 01/17/17 02:42 7440-43-901/13/17 00:451.0 0.50 1
Chromium ND ug/L 01/17/17 02:42 7440-47-301/13/17 00:455.0 2.5 1
Copper 50.3 ug/L 01/17/17 02:42 7440-50-801/13/17 00:455.0 2.5 1
Lead ND ug/L 01/17/17 02:42 7439-92-101/13/17 00:455.0 2.5 1
Selenium ND ug/L 01/17/17 02:42 7782-49-201/13/17 00:4510.0 5.0 1
Silver ND ug/L 01/17/17 02:42 7440-22-401/13/17 00:455.0 2.5 1
Zinc 103 ug/L 01/17/17 02:42 7440-66-601/13/17 00:4510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/16/17 12:27 7439-97-601/13/17 12:350.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/17/17 15:00 83-32-901/13/17 15:1910.0 0.25 1
Acenaphthylene ND ug/L 01/17/17 15:00 208-96-801/13/17 15:1910.0 0.21 1
Aniline ND ug/L 01/17/17 15:00 62-53-301/13/17 15:1910.0 1.3 1
Anthracene ND ug/L 01/17/17 15:00 120-12-701/13/17 15:1910.0 0.14 1
Benzo(a)anthracene ND ug/L 01/17/17 15:00 56-55-301/13/17 15:1910.0 0.33 1
Benzo(a)pyrene ND ug/L 01/17/17 15:00 50-32-801/13/17 15:1910.0 0.30 1
Benzo(b)fluoranthene ND ug/L 01/17/17 15:00 205-99-201/13/17 15:1910.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 01/17/17 15:00 191-24-201/13/17 15:1910.0 0.38 1
Benzo(k)fluoranthene ND ug/L 01/17/17 15:00 207-08-901/13/17 15:1910.0 0.43 1
Benzoic Acid ND ug/L 01/17/17 15:00 65-85-001/13/17 15:1950.0 11.1 1
Benzyl alcohol ND ug/L 01/17/17 15:00 100-51-601/13/17 15:1920.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 01/17/17 15:00 101-55-301/13/17 15:1910.0 1.3 1
Butylbenzylphthalate ND ug/L 01/17/17 15:00 85-68-701/13/17 15:1910.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 01/17/17 15:00 59-50-701/13/17 15:1920.0 4.2 1
4-Chloroaniline ND ug/L 01/17/17 15:00 106-47-801/13/17 15:1920.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 01/17/17 15:00 111-91-101/13/17 15:1910.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 01/17/17 15:00 111-44-401/13/17 15:1910.0 1.5 1
2-Chloronaphthalene ND ug/L 01/17/17 15:00 91-58-701/13/17 15:1910.0 2.2 1
2-Chlorophenol ND ug/L 01/17/17 15:00 95-57-801/13/17 15:1910.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 01/17/17 15:00 7005-72-301/13/17 15:1910.0 2.1 1
Chrysene ND ug/L 01/17/17 15:00 218-01-901/13/17 15:1910.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 01/17/17 15:00 53-70-301/13/17 15:1910.0 0.55 1
Dibenzofuran ND ug/L 01/17/17 15:00 132-64-901/13/17 15:1910.0 1.8 1
1,2-Dichlorobenzene ND ug/L 01/17/17 15:00 95-50-101/13/17 15:1910.0 1.2 1
1,3-Dichlorobenzene ND ug/L 01/17/17 15:00 541-73-101/13/17 15:1910.0 1.1 1
1,4-Dichlorobenzene ND ug/L 01/17/17 15:00 106-46-701/13/17 15:1910.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 01/17/17 15:00 91-94-101/13/17 15:1920.0 1.4 1
2,4-Dichlorophenol ND ug/L 01/17/17 15:00 120-83-201/13/17 15:1910.0 1.7 1
Diethylphthalate 2.2J ug/L 01/17/17 15:00 84-66-201/13/17 15:1910.0 1.3 1
2,4-Dimethylphenol ND ug/L 01/17/17 15:00 105-67-901/13/17 15:1910.0 2.2 1
Dimethylphthalate ND ug/L 01/17/17 15:00 131-11-301/13/17 15:1910.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
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Page 12 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: DUP-02-011117 Lab ID: 92325998003 Collected: 01/11/17 00:00 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Di-n-butylphthalate ND ug/L 01/17/17 15:00 84-74-201/13/17 15:1910.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 01/17/17 15:00 534-52-101/13/17 15:1920.0 1.7 1
2,4-Dinitrophenol ND ug/L 01/17/17 15:00 51-28-501/13/17 15:1950.0 6.5 1
2,4-Dinitrotoluene ND ug/L 01/17/17 15:00 121-14-201/13/17 15:1910.0 1.2 1
2,6-Dinitrotoluene ND ug/L 01/17/17 15:00 606-20-201/13/17 15:1910.0 1.7 1
Di-n-octylphthalate ND ug/L 01/17/17 15:00 117-84-001/13/17 15:1910.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/17/17 15:00 117-81-701/13/17 15:196.0 0.85 1
Fluoranthene ND ug/L 01/17/17 15:00 206-44-001/13/17 15:1910.0 0.21 1
Fluorene ND ug/L 01/17/17 15:00 86-73-701/13/17 15:1910.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 01/17/17 15:00 87-68-301/13/17 15:1910.0 1.8 1
Hexachlorobenzene ND ug/L 01/17/17 15:00 118-74-101/13/17 15:1910.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 01/17/17 15:00 77-47-401/13/17 15:1910.0 1.8 1
Hexachloroethane ND ug/L 01/17/17 15:00 67-72-101/13/17 15:1910.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/17/17 15:00 193-39-501/13/17 15:1910.0 0.29 1
Isophorone ND ug/L 01/17/17 15:00 78-59-101/13/17 15:1910.0 1.8 1
1-Methylnaphthalene ND ug/L 01/17/17 15:00 90-12-001/13/17 15:1910.0 0.32 1
2-Methylnaphthalene ND ug/L 01/17/17 15:00 91-57-601/13/17 15:1910.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 01/17/17 15:00 95-48-701/13/17 15:1910.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/17/17 15:0001/13/17 15:1910.0 1.7 1
Naphthalene ND ug/L 01/17/17 15:00 91-20-301/13/17 15:1910.0 0.34 1
2-Nitroaniline ND ug/L 01/17/17 15:00 88-74-401/13/17 15:1950.0 2.8 1
3-Nitroaniline ND ug/L 01/17/17 15:00 99-09-201/13/17 15:1950.0 2.4 1
4-Nitroaniline ND ug/L 01/17/17 15:00 100-01-601/13/17 15:1920.0 2.5 1
Nitrobenzene ND ug/L 01/17/17 15:00 98-95-301/13/17 15:1910.0 1.7 1
2-Nitrophenol ND ug/L 01/17/17 15:00 88-75-501/13/17 15:1910.0 1.7 1
4-Nitrophenol ND ug/L 01/17/17 15:00 100-02-701/13/17 15:1950.0 5.8 1
N-Nitrosodimethylamine ND ug/L 01/17/17 15:00 62-75-901/13/17 15:1910.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 01/17/17 15:00 621-64-701/13/17 15:1910.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 01/17/17 15:00 86-30-601/13/17 15:1910.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/17/17 15:00 108-60-101/13/17 15:1910.0 1.6 1
Pentachlorophenol ND ug/L 01/17/17 15:00 87-86-501/13/17 15:1925.0 2.3 1
Phenanthrene ND ug/L 01/17/17 15:00 85-01-801/13/17 15:1910.0 0.22 1
Phenol ND ug/L 01/17/17 15:0001/13/17 15:1910.0 1.7 1
Pyrene ND ug/L 01/17/17 15:00 129-00-001/13/17 15:1910.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 01/17/17 15:00 120-82-101/13/17 15:1910.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 01/17/17 15:00 95-95-401/13/17 15:1910.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 01/17/17 15:00 88-06-201/13/17 15:1910.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)75 %01/17/17 15:00 4165-60-001/13/17 15:1921-110 1
2-Fluorobiphenyl (S)78 %01/17/17 15:00 321-60-801/13/17 15:1927-110 1
Terphenyl-d14 (S)87 %01/17/17 15:00 1718-51-001/13/17 15:1931-107 1
Phenol-d6 (S)28 %01/17/17 15:00 13127-88-301/13/17 15:1910-110 1
2-Fluorophenol (S)43 %01/17/17 15:00 367-12-401/13/17 15:1912-110 1
2,4,6-Tribromophenol (S)79 %01/17/17 15:00 118-79-601/13/17 15:1927-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: DUP-02-011117 Lab ID: 92325998003 Collected: 01/11/17 00:00 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 01/12/17 19:33 67-64-125.0 10.0 1
Benzene ND ug/L 01/12/17 19:33 71-43-21.0 0.25 1
Bromobenzene ND ug/L 01/12/17 19:33 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 01/12/17 19:33 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 01/12/17 19:33 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/17 19:33 75-25-21.0 0.26 1
Bromomethane ND ug/L 01/12/17 19:33 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/17 19:33 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 01/12/17 19:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/17 19:33 108-90-71.0 0.23 1
Chloroethane ND ug/L 01/12/17 19:33 75-00-31.0 0.54 1
Chloroform ND ug/L 01/12/17 19:33 67-66-31.0 0.14 1
Chloromethane ND ug/L 01/12/17 19:33 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 01/12/17 19:33 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 01/12/17 19:33 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/17 19:33 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 01/12/17 19:33 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/17 19:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/17 19:33 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/17 19:33 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 01/12/17 19:33 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 01/12/17 19:33 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 01/12/17 19:33 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 01/12/17 19:33 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/17 19:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/17 19:33 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/17 19:33 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/12/17 19:33 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/17 19:33 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 01/12/17 19:33 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 01/12/17 19:33 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 01/12/17 19:33 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 01/12/17 19:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/17 19:33 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 01/12/17 19:33 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 01/12/17 19:33 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 01/12/17 19:33 87-68-31.0 0.71 1
2-Hexanone ND ug/L 01/12/17 19:33 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 01/12/17 19:33 99-87-61.0 0.31 1
Methylene Chloride 2.0 ug/L 01/12/17 19:33 75-09-2 C92.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/17 19:33 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 01/12/17 19:33 1634-04-41.0 0.21 1
Naphthalene ND ug/L 01/12/17 19:33 91-20-31.0 0.24 1
Styrene 0.39J ug/L 01/12/17 19:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/17 19:33 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/17 19:33 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: DUP-02-011117 Lab ID: 92325998003 Collected: 01/11/17 00:00 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 01/12/17 19:33 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/17 19:33 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 01/12/17 19:33 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 01/12/17 19:33 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 01/12/17 19:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/17 19:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/17 19:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/17 19:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/17 19:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/17 19:33 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 01/12/17 19:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/17 19:33 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 01/12/17 19:33 179601-23-12.0 0.66 1
o-Xylene ND ug/L 01/12/17 19:33 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)101 %01/12/17 19:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %01/12/17 19:33 17060-07-070-130 1
Toluene-d8 (S)105 %01/12/17 19:33 2037-26-570-130 1
Sample: TRIP BLANK Lab ID: 92325998004 Collected: 01/03/17 00:00 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 01/12/17 16:04 67-64-125.0 10.0 1
Benzene ND ug/L 01/12/17 16:04 71-43-21.0 0.25 1
Bromobenzene ND ug/L 01/12/17 16:04 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 01/12/17 16:04 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 01/12/17 16:04 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/17 16:04 75-25-21.0 0.26 1
Bromomethane ND ug/L 01/12/17 16:04 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/17 16:04 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 01/12/17 16:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/17 16:04 108-90-71.0 0.23 1
Chloroethane ND ug/L 01/12/17 16:04 75-00-31.0 0.54 1
Chloroform ND ug/L 01/12/17 16:04 67-66-31.0 0.14 1
Chloromethane ND ug/L 01/12/17 16:04 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 01/12/17 16:04 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 01/12/17 16:04 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/17 16:04 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 01/12/17 16:04 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/17 16:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/17 16:04 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/17 16:04 95-50-11.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 15 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325998
71167563
Sample: TRIP BLANK Lab ID: 92325998004 Collected: 01/03/17 00:00 Received: 01/11/17 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,3-Dichlorobenzene ND ug/L 01/12/17 16:04 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 01/12/17 16:04 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 01/12/17 16:04 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 01/12/17 16:04 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/17 16:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/17 16:04 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/17 16:04 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/12/17 16:04 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/17 16:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 01/12/17 16:04 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 01/12/17 16:04 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 01/12/17 16:04 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 01/12/17 16:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/17 16:04 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 01/12/17 16:04 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 01/12/17 16:04 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 01/12/17 16:04 87-68-31.0 0.71 1
2-Hexanone ND ug/L 01/12/17 16:04 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 01/12/17 16:04 99-87-61.0 0.31 1
Methylene Chloride 2.6 ug/L 01/12/17 16:04 75-09-2 C92.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/17 16:04 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 01/12/17 16:04 1634-04-41.0 0.21 1
Naphthalene ND ug/L 01/12/17 16:04 91-20-31.0 0.24 1
Styrene ND ug/L 01/12/17 16:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/17 16:04 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/17 16:04 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 01/12/17 16:04 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/17 16:04 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 01/12/17 16:04 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 01/12/17 16:04 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 01/12/17 16:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/17 16:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/17 16:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/17 16:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/17 16:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/17 16:04 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 01/12/17 16:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/17 16:04 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 01/12/17 16:04 179601-23-12.0 0.66 1
o-Xylene ND ug/L 01/12/17 16:04 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %01/12/17 16:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %01/12/17 16:04 17060-07-070-130 1
Toluene-d8 (S)107 %01/12/17 16:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344218
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples: 92325998001, 92325998002, 92325998003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1909631
Associated Lab Samples:92325998001, 92325998002, 92325998003
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/16/17 12:130.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909632LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1909633MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325998001
1909634
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 89 75-12589 1 252.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Page 17 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344184
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples: 92325998001, 92325998002, 92325998003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1909426
Associated Lab Samples:92325998001, 92325998002, 92325998003
Matrix: Water
AnalyzedMDL
Aluminum ug/L ND 100 01/17/17 02:1550.0
Arsenic ug/L ND 10.0 01/17/17 02:155.0
Barium ug/L ND 5.0 01/17/17 02:152.5
Cadmium ug/L ND 1.0 01/17/17 02:150.50
Chromium ug/L ND 5.0 01/17/17 02:152.5
Copper ug/L ND 5.0 01/17/17 02:152.5
Lead ug/L ND 5.0 01/17/17 02:152.5
Selenium ug/L ND 10.0 01/17/17 02:155.0
Silver ug/L ND 5.0 01/17/17 02:152.5
Zinc ug/L ND 10.0 01/17/17 02:155.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909427LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 54305000 109 80-120
Arsenic ug/L 524500 105 80-120
Barium ug/L 542500 108 80-120
Cadmium ug/L 537500 107 80-120
Chromium ug/L 533500 107 80-120
Copper ug/L 553500 111 80-120
Lead ug/L 530500 106 80-120
Selenium ug/L 541500 108 80-120
Silver ug/L 240250 96 80-120
Zinc ug/L 536500 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1909428MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325998001
1909429
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L M1500012875-125128 0 2050009507340 7340
Arsenic ug/L 500 99 75-12599 1 20500ND494 497
Barium ug/L 500 101 75-125102 0 2050037.0 544 547
Cadmium ug/L 500 101 75-125101 0 20500ND506 504
Chromium ug/L 500 100 75-125100 0 205004.5J 505 505
Copper ug/L 500 104 75-125104 0 205006.3 527 527
Lead ug/L 500 98 75-12598 1 205002.7J 491 494
Selenium ug/L 500 101 75-125101 0 20500ND507 509
Silver ug/L 250 90 75-12590 1 20250ND226 224
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Huntersville, NC 28078
[phone]
Page 18 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1909428MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325998001
1909429
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Zinc ug/L 500 100 75-125100 0 2050015.9 516 517
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344139
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92325998001, 92325998002, 92325998003, 92325998004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1909126
Associated Lab Samples:92325998001, 92325998002, 92325998003, 92325998004
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 01/12/17 13:110.33
1,1,1-Trichloroethane ug/L ND 1.0 01/12/17 13:110.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 01/12/17 13:110.40
1,1,2-Trichloroethane ug/L ND 1.0 01/12/17 13:110.29
1,1-Dichloroethane ug/L ND 1.0 01/12/17 13:110.32
1,1-Dichloroethene ug/L ND 1.0 01/12/17 13:110.56
1,1-Dichloropropene ug/L ND 1.0 01/12/17 13:110.49
1,2,3-Trichlorobenzene ug/L ND 1.0 01/12/17 13:110.33
1,2,3-Trichloropropane ug/L ND 1.0 01/12/17 13:110.41
1,2,4-Trichlorobenzene ug/L ND 1.0 01/12/17 13:110.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 01/12/17 13:112.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/12/17 13:110.27
1,2-Dichlorobenzene ug/L ND 1.0 01/12/17 13:110.30
1,2-Dichloroethane ug/L ND 1.0 01/12/17 13:110.24
1,2-Dichloropropane ug/L ND 1.0 01/12/17 13:110.27
1,3-Dichlorobenzene ug/L ND 1.0 01/12/17 13:110.24
1,3-Dichloropropane ug/L ND 1.0 01/12/17 13:110.28
1,4-Dichlorobenzene ug/L ND 1.0 01/12/17 13:110.33
2,2-Dichloropropane ug/L ND 1.0 01/12/17 13:110.13
2-Butanone (MEK)ug/L ND 5.0 01/12/17 13:110.96
2-Chlorotoluene ug/L ND 1.0 01/12/17 13:110.35
2-Hexanone ug/L ND 5.0 01/12/17 13:110.46
4-Chlorotoluene ug/L ND 1.0 01/12/17 13:110.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 01/12/17 13:110.33
Acetone ug/L ND 25.0 01/12/17 13:1110.0
Benzene ug/L ND 1.0 01/12/17 13:110.25
Bromobenzene ug/L ND 1.0 01/12/17 13:110.30
Bromochloromethane ug/L ND 1.0 01/12/17 13:110.17
Bromodichloromethane ug/L ND 1.0 01/12/17 13:110.18
Bromoform ug/L ND 1.0 01/12/17 13:110.26
Bromomethane ug/L ND 2.0 01/12/17 13:110.29
Carbon tetrachloride ug/L ND 1.0 01/12/17 13:110.25
Chlorobenzene ug/L ND 1.0 01/12/17 13:110.23
Chloroethane ug/L ND 1.0 01/12/17 13:110.54
Chloroform ug/L ND 1.0 01/12/17 13:110.14
Chloromethane ug/L ND 1.0 01/12/17 13:110.11
cis-1,2-Dichloroethene ug/L ND 1.0 01/12/17 13:110.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/12/17 13:110.13
Dibromochloromethane ug/L ND 1.0 01/12/17 13:110.21
Dibromomethane ug/L ND 1.0 01/12/17 13:110.21
Dichlorodifluoromethane ug/L ND 1.0 01/12/17 13:110.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Huntersville, NC 28078
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Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1909126
Associated Lab Samples:92325998001, 92325998002, 92325998003, 92325998004
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 01/12/17 13:110.12
Ethylbenzene ug/L ND 1.0 01/12/17 13:110.30
Hexachloro-1,3-butadiene ug/L ND 1.0 01/12/17 13:110.71
m&p-Xylene ug/L ND 2.0 01/12/17 13:110.66
Methyl-tert-butyl ether ug/L ND 1.0 01/12/17 13:110.21
Methylene Chloride ug/L 1.9J 2.0 C901/12/17 13:110.97
Naphthalene ug/L ND 1.0 01/12/17 13:110.24
o-Xylene ug/L ND 1.0 01/12/17 13:110.23
p-Isopropyltoluene ug/L ND 1.0 01/12/17 13:110.31
Styrene ug/L ND 1.0 01/12/17 13:110.26
Tetrachloroethene ug/L ND 1.0 01/12/17 13:110.46
Toluene ug/L ND 1.0 01/12/17 13:110.26
trans-1,2-Dichloroethene ug/L ND 1.0 01/12/17 13:110.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/12/17 13:110.26
Trichloroethene ug/L ND 1.0 01/12/17 13:110.47
Trichlorofluoromethane ug/L ND 1.0 01/12/17 13:110.20
Vinyl acetate ug/L ND 2.0 01/12/17 13:110.35
Vinyl chloride ug/L ND 1.0 01/12/17 13:110.62
Xylene (Total)ug/L ND 1.0 01/12/17 13:110.66
1,2-Dichloroethane-d4 (S)%95 70-130 01/12/17 13:11
4-Bromofluorobenzene (S)%103 70-130 01/12/17 13:11
Toluene-d8 (S)%105 70-130 01/12/17 13:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909128LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 70-130
1,1,1-Trichloroethane ug/L 50.250 100 70-130
1,1,2,2-Tetrachloroethane ug/L 48.150 96 70-130
1,1,2-Trichloroethane ug/L 48.650 97 70-130
1,1-Dichloroethane ug/L 46.950 94 70-130
1,1-Dichloroethene ug/L 52.050 104 70-132
1,1-Dichloropropene ug/L 53.850 108 70-130
1,2,3-Trichlorobenzene ug/L 49.750 99 70-135
1,2,3-Trichloropropane ug/L 48.650 97 70-130
1,2,4-Trichlorobenzene ug/L 49.250 98 70-134
1,2-Dibromo-3-chloropropane ug/L 46.550 93 70-130
1,2-Dibromoethane (EDB)ug/L 49.050 98 70-130
1,2-Dichlorobenzene ug/L 50.050 100 70-130
1,2-Dichloroethane ug/L 45.450 91 70-130
1,2-Dichloropropane ug/L 47.750 95 70-130
1,3-Dichlorobenzene ug/L 49.250 98 70-130
1,3-Dichloropropane ug/L 50.450 101 70-130
1,4-Dichlorobenzene ug/L 48.950 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909128LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.650 103 58-145
2-Butanone (MEK)ug/L 87.4100 87 70-145
2-Chlorotoluene ug/L 48.150 96 70-130
2-Hexanone ug/L 87.7100 88 70-144
4-Chlorotoluene ug/L 49.550 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 89.2100 89 70-140
Acetone ug/L 83.5100 83 50-175
Benzene ug/L 50.050 100 70-130
Bromobenzene ug/L 49.050 98 70-130
Bromochloromethane ug/L 46.450 93 70-130
Bromodichloromethane ug/L 47.950 96 70-130
Bromoform ug/L 47.850 96 70-130
Bromomethane ug/L 51.250 102 54-130
Carbon tetrachloride ug/L 52.150 104 70-132
Chlorobenzene ug/L 51.450 103 70-130
Chloroethane ug/L 48.050 96 64-134
Chloroform ug/L 46.250 92 70-130
Chloromethane ug/L 49.150 98 64-130
cis-1,2-Dichloroethene ug/L 46.050 92 70-131
cis-1,3-Dichloropropene ug/L 51.150 102 70-130
Dibromochloromethane ug/L 52.450 105 70-130
Dibromomethane ug/L 47.750 95 70-131
Dichlorodifluoromethane ug/L 50.150 100 56-130
Diisopropyl ether ug/L 48.850 98 70-130
Ethylbenzene ug/L 50.850 102 70-130
Hexachloro-1,3-butadiene ug/L 55.650 111 70-130
m&p-Xylene ug/L 100100 100 70-130
Methyl-tert-butyl ether ug/L 50.150 100 70-130
Methylene Chloride ug/L 50.550 101 63-130
Naphthalene ug/L 48.850 98 70-138
o-Xylene ug/L 49.950 100 70-130
p-Isopropyltoluene ug/L 48.950 98 70-130
Styrene ug/L 50.450 101 70-130
Tetrachloroethene ug/L 49.650 99 70-130
Toluene ug/L 47.950 96 70-130
trans-1,2-Dichloroethene ug/L 50.650 101 70-130
trans-1,3-Dichloropropene ug/L 50.250 100 70-132
Trichloroethene ug/L 51.450 103 70-130
Trichlorofluoromethane ug/L 54.550 109 62-133
Vinyl acetate ug/L 94.6100 95 66-157
Vinyl chloride ug/L 42.550 85 50-150
Xylene (Total)ug/L 150150 100 70-130
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909129MATRIX SPIKE SAMPLE:
MSSpike
Result
92325943001
1,1,1,2-Tetrachloroethane ug/L 22.720 113 70-130ND
1,1,1-Trichloroethane ug/L 23.920 120 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,2-Trichloroethane ug/L 21.720 109 70-130ND
1,1-Dichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethene ug/L 25.020 125 70-166ND
1,1-Dichloropropene ug/L 25.920 129 70-130ND
1,2,3-Trichlorobenzene ug/L 22.220 111 70-130ND
1,2,3-Trichloropropane ug/L 19.520 97 70-130ND
1,2,4-Trichlorobenzene ug/L 21.620 108 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.520 98 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.920 105 70-130ND
1,2-Dichlorobenzene ug/L 21.620 108 70-130ND
1,2-Dichloroethane ug/L 21.420 107 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,3-Dichlorobenzene ug/L 22.320 111 70-130ND
1,3-Dichloropropane ug/L 21.520 107 70-130ND
1,4-Dichlorobenzene ug/L 22.520 113 70-130ND
2,2-Dichloropropane ug/L 25.220 126 70-130ND
2-Butanone (MEK)ug/L 37.940 95 70-130ND
2-Chlorotoluene ug/L 22.120 111 70-130ND
2-Hexanone ug/L 37.640 94 70-130ND
4-Chlorotoluene ug/L 22.320 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 38.340 96 70-130ND
Acetone ug/L 30.440 70 70-130ND
Benzene ug/L 26.120 130 70-148ND
Bromobenzene ug/L 22.220 111 70-130ND
Bromochloromethane ug/L 21.220 106 70-130ND
Bromodichloromethane ug/L 22.720 113 70-130ND
Bromoform ug/L 19.920 99 70-130ND
Bromomethane ug/L 17.120 86 70-130ND
Carbon tetrachloride ug/L 25.120 125 70-130ND
Chlorobenzene ug/L 22.620 113 70-146ND
Chloroethane ug/L 22.220 111 70-130ND
Chloroform ug/L 21.520 107 70-130ND
Chloromethane ug/L 21.820 108 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 23.120 116 70-130ND
Dibromochloromethane ug/L 21.820 109 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Dichlorodifluoromethane ug/L 21.520 107 70-130ND
Diisopropyl ether ug/L 88.8 M120444 70-130ND
Ethylbenzene ug/L 22.720 114 70-130ND
Hexachloro-1,3-butadiene ug/L 26.120 130 70-130ND
m&p-Xylene ug/L 46.040 115 70-130ND
Methyl-tert-butyl ether ug/L 76.9 M120384 70-130ND
Methylene Chloride ug/L 23.620 107 70-1302.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
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Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909129MATRIX SPIKE SAMPLE:
MSSpike
Result
92325943001
Naphthalene ug/L 21.620 108 70-130ND
o-Xylene ug/L 22.220 111 70-130ND
p-Isopropyltoluene ug/L 22.320 112 70-130ND
Styrene ug/L 22.320 112 70-130ND
Tetrachloroethene ug/L 21.920 109 70-130ND
Toluene ug/L 22.620 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.620 118 70-130ND
trans-1,3-Dichloropropene ug/L 22.520 112 70-130ND
Trichloroethene ug/L 24.320 121 69-151ND
Trichlorofluoromethane ug/L 26.2 M120131 70-130ND
Vinyl acetate ug/L 40.040 100 70-130ND
Vinyl chloride ug/L 19.720 99 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325883004
1909803SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
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Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325883004
1909803SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L 2.2 9 302.4
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%95 095
4-Bromofluorobenzene (S)%103 1102
Toluene-d8 (S)%103 3106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344313
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples: 92325998001, 92325998002, 92325998003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1910349
Associated Lab Samples:92325998001, 92325998002, 92325998003
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 01/17/17 13:181.9
1,2-Dichlorobenzene ug/L ND 10.0 01/17/17 13:181.2
1,3-Dichlorobenzene ug/L ND 10.0 01/17/17 13:181.1
1,4-Dichlorobenzene ug/L ND 10.0 01/17/17 13:181.2
1-Methylnaphthalene ug/L ND 10.0 01/17/17 13:180.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 01/17/17 13:181.6
2,4,5-Trichlorophenol ug/L ND 10.0 01/17/17 13:182.2
2,4,6-Trichlorophenol ug/L ND 10.0 01/17/17 13:181.9
2,4-Dichlorophenol ug/L ND 10.0 01/17/17 13:181.7
2,4-Dimethylphenol ug/L ND 10.0 01/17/17 13:182.2
2,4-Dinitrophenol ug/L ND 50.0 01/17/17 13:186.5
2,4-Dinitrotoluene ug/L ND 10.0 01/17/17 13:181.2
2,6-Dinitrotoluene ug/L ND 10.0 01/17/17 13:181.7
2-Chloronaphthalene ug/L ND 10.0 01/17/17 13:182.2
2-Chlorophenol ug/L ND 10.0 01/17/17 13:181.5
2-Methylnaphthalene ug/L ND 10.0 01/17/17 13:180.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 01/17/17 13:181.7
2-Nitroaniline ug/L ND 50.0 01/17/17 13:182.8
2-Nitrophenol ug/L ND 10.0 01/17/17 13:181.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 01/17/17 13:181.7
3,3'-Dichlorobenzidine ug/L ND 20.0 01/17/17 13:181.4
3-Nitroaniline ug/L ND 50.0 01/17/17 13:182.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/17/17 13:181.7
4-Bromophenylphenyl ether ug/L ND 10.0 01/17/17 13:181.3
4-Chloro-3-methylphenol ug/L ND 20.0 01/17/17 13:184.2
4-Chloroaniline ug/L ND 20.0 01/17/17 13:183.4
4-Chlorophenylphenyl ether ug/L ND 10.0 01/17/17 13:182.1
4-Nitroaniline ug/L ND 20.0 01/17/17 13:182.5
4-Nitrophenol ug/L ND 50.0 01/17/17 13:185.8
Acenaphthene ug/L ND 10.0 01/17/17 13:180.25
Acenaphthylene ug/L ND 10.0 01/17/17 13:180.21
Aniline ug/L ND 10.0 01/17/17 13:181.3
Anthracene ug/L ND 10.0 01/17/17 13:180.14
Benzo(a)anthracene ug/L ND 10.0 01/17/17 13:180.33
Benzo(a)pyrene ug/L ND 10.0 01/17/17 13:180.30
Benzo(b)fluoranthene ug/L ND 10.0 01/17/17 13:180.28
Benzo(g,h,i)perylene ug/L ND 10.0 01/17/17 13:180.38
Benzo(k)fluoranthene ug/L ND 10.0 01/17/17 13:180.43
Benzoic Acid ug/L ND 50.0 01/17/17 13:1811.1
Benzyl alcohol ug/L ND 20.0 01/17/17 13:183.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/17/17 13:181.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1910349
Associated Lab Samples:92325998001, 92325998002, 92325998003
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 01/17/17 13:181.5
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 01/17/17 13:180.85
Butylbenzylphthalate ug/L ND 10.0 01/17/17 13:180.75
Chrysene ug/L ND 10.0 01/17/17 13:180.21
Di-n-butylphthalate ug/L ND 10.0 01/17/17 13:181.1
Di-n-octylphthalate ug/L ND 10.0 01/17/17 13:180.86
Dibenz(a,h)anthracene ug/L ND 10.0 01/17/17 13:180.55
Dibenzofuran ug/L ND 10.0 01/17/17 13:181.8
Diethylphthalate ug/L ND 10.0 01/17/17 13:181.3
Dimethylphthalate ug/L ND 10.0 01/17/17 13:181.5
Fluoranthene ug/L ND 10.0 01/17/17 13:180.21
Fluorene ug/L ND 10.0 01/17/17 13:180.21
Hexachloro-1,3-butadiene ug/L ND 10.0 01/17/17 13:181.8
Hexachlorobenzene ug/L ND 10.0 01/17/17 13:181.1
Hexachlorocyclopentadiene ug/L ND 10.0 01/17/17 13:181.8
Hexachloroethane ug/L ND 10.0 01/17/17 13:181.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 01/17/17 13:180.29
Isophorone ug/L ND 10.0 01/17/17 13:181.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 01/17/17 13:182.1
N-Nitrosodimethylamine ug/L ND 10.0 01/17/17 13:181.3
N-Nitrosodiphenylamine ug/L ND 10.0 01/17/17 13:181.3
Naphthalene ug/L ND 10.0 01/17/17 13:180.34
Nitrobenzene ug/L ND 10.0 01/17/17 13:181.7
Pentachlorophenol ug/L ND 25.0 01/17/17 13:182.3
Phenanthrene ug/L ND 10.0 01/17/17 13:180.22
Phenol ug/L ND 10.0 01/17/17 13:181.7
Pyrene ug/L ND 10.0 01/17/17 13:180.19
2,4,6-Tribromophenol (S)%90 27-110 01/17/17 13:18
2-Fluorobiphenyl (S)%72 27-110 01/17/17 13:18
2-Fluorophenol (S)%42 12-110 01/17/17 13:18
Nitrobenzene-d5 (S)%69 21-110 01/17/17 13:18
Phenol-d6 (S)%30 10-110 01/17/17 13:18
Terphenyl-d14 (S)%91 31-107 01/17/17 13:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1910350LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1910351
1,2,4-Trichlorobenzene ug/L 33.950 68 31-1206532.5 4 30
1,2-Dichlorobenzene ug/L 33.050 66 38-1206934.4 4 30
1,3-Dichlorobenzene ug/L 32.050 64 30-1226633.0 3 30
1,4-Dichlorobenzene ug/L 31.750 63 37-1206733.5 6 30
1-Methylnaphthalene ug/L 38.950 78 34-1138040.2 3 30
2,2'-Oxybis(1-chloropropane)ug/L 55.450 111 18-12011457.1 3 30
2,4,5-Trichlorophenol ug/L 34.450 69 43-1136834.2 1 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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[phone]
Page 27 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1910350LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1910351
2,4,6-Trichlorophenol ug/L 40.050 80 42-1208542.5 6 30
2,4-Dichlorophenol ug/L 43.150 86 30-1209044.8 4 30
2,4-Dimethylphenol ug/L 45.150 90 29-1119547.6 5 30
2,4-Dinitrophenol ug/L 176250 71 19-13278196 11 30
2,4-Dinitrotoluene ug/L 43.950 88 58-1288944.3 1 30
2,6-Dinitrotoluene ug/L 45.050 90 54-1299145.6 1 30
2-Chloronaphthalene ug/L 46.550 93 43-1179145.4 2 30
2-Chlorophenol ug/L 40.250 80 37-1208944.6 11 30
2-Methylnaphthalene ug/L 40.750 81 33-1208341.5 2 30
2-Methylphenol(o-Cresol)ug/L 30.550 61 31-1206733.7 10 30
2-Nitroaniline ug/L 101100 101 48-121101101 1 30
2-Nitrophenol ug/L 43.650 87 25-1168442.1 3 30
3&4-Methylphenol(m&p Cresol)ug/L 29.150 58 23-1206733.3 13 30
3,3'-Dichlorobenzidine ug/L 102100 102 10-1549999.4 2 30
3-Nitroaniline ug/L 95.4100 95 43-1159998.6 3 30
4,6-Dinitro-2-methylphenol ug/L 113100 113 44-124118118 5 30
4-Bromophenylphenyl ether ug/L 40.350 81 34-1137939.7 1 30
4-Chloro-3-methylphenol ug/L 91.7100 92 31-1109998.5 7 30
4-Chloroaniline ug/L 88.6100 89 20-1209493.5 5 30
4-Chlorophenylphenyl ether ug/L 37.450 75 34-1167436.9 1 30
4-Nitroaniline ug/L 108100 108 46-128110110 2 30
4-Nitrophenol ug/L 94.3250 38 11-1203996.5 2 30
Acenaphthene ug/L 42.450 85 48-1148542.6 0 30
Acenaphthylene ug/L 41.450 83 48-1128442.1 2 30
Aniline ug/L 30.150 60 26-1206733.3 10 30
Anthracene ug/L 46.050 92 57-1189447.1 2 30
Benzo(a)anthracene ug/L 45.050 90 56-1219045.1 0 30
Benzo(a)pyrene ug/L 48.350 97 55-12710150.3 4 30
Benzo(b)fluoranthene ug/L 51.350 103 53-12810653.1 3 30
Benzo(g,h,i)perylene ug/L 54.950 110 54-12510552.3 5 30
Benzo(k)fluoranthene ug/L 48.650 97 51-12310552.5 8 30
Benzoic Acid ug/L 81.6 R12503310-12045113 33 30
Benzyl alcohol ug/L 70.7100 71 27-1207979.2 11 30
bis(2-Chloroethoxy)methane ug/L 41.850 84 32-1208642.9 3 30
bis(2-Chloroethyl) ether ug/L 40.350 81 33-1118743.7 8 30
bis(2-Ethylhexyl)phthalate ug/L 44.850 90 50-1459145.7 2 30
Butylbenzylphthalate ug/L 47.850 96 54-1389849.2 3 30
Chrysene ug/L 45.850 92 58-1279446.9 2 30
Di-n-butylphthalate ug/L 51.950 104 56-12510753.3 3 30
Di-n-octylphthalate ug/L 51.050 102 50-1349949.5 3 30
Dibenz(a,h)anthracene ug/L 54.250 108 53-12910853.9 1 30
Dibenzofuran ug/L 41.150 82 45-1208341.3 0 30
Diethylphthalate ug/L 44.150 88 53-1208844.2 0 30
Dimethylphthalate ug/L 43.750 87 55-1168843.9 1 30
Fluoranthene ug/L 46.150 92 57-1259547.7 4 30
Fluorene ug/L 42.350 85 53-1188542.6 1 30
Hexachloro-1,3-butadiene ug/L 26.650 53 23-1204924.7 7 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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[phone]
Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325998
71167563
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1910350LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1910351
Hexachlorobenzene ug/L 47.350 95 49-1169547.7 1 30
Hexachlorocyclopentadiene ug/L 36.750 73 26-1587035.1 4 30
Hexachloroethane ug/L 27.650 55 30-1145628.0 1 30
Indeno(1,2,3-cd)pyrene ug/L 55.050 110 55-12810753.6 3 30
Isophorone ug/L 41.250 82 31-1188643.1 4 30
N-Nitroso-di-n-propylamine ug/L 36.750 73 32-1198643.1 16 30
N-Nitrosodimethylamine ug/L 30.750 61 13-1207135.3 14 30
N-Nitrosodiphenylamine ug/L 43.150 86 43-1208542.3 2 30
Naphthalene ug/L 39.550 79 32-1207738.6 2 30
Nitrobenzene ug/L 39.450 79 33-1107638.1 3 30
Pentachlorophenol ug/L 125100 125 10-137132132 6 30
Phenanthrene ug/L 46.750 93 57-1179447.1 1 30
Phenol ug/L 22.250 44 10-1204824.1 8 30
Pyrene ug/L 41.450 83 55-1228140.7 2 30
2,4,6-Tribromophenol (S)%106 27-110108
2-Fluorobiphenyl (S)%71 27-11072
2-Fluorophenol (S)%52 12-11055
Nitrobenzene-d5 (S)%77 21-11075
Phenol-d6 (S)%35 10-11040
Terphenyl-d14 (S)%90 31-10788
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Page 29 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325998
71167563
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Page 30 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325998
71167563
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325998001 344184 344334GW-03 EPA 3010A EPA 6010
92325998002 344184 344334GW-02 EPA 3010A EPA 6010
92325998003 344184 344334DUP-02-011117 EPA 3010A EPA 6010
92325998001 344218 344413GW-03 EPA 7470 EPA 7470
92325998002 344218 344413GW-02 EPA 7470 EPA 7470
92325998003 344218 344413DUP-02-011117 EPA 7470 EPA 7470
92325998001 344313 344546GW-03 EPA 3510 EPA 8270
92325998002 344313 344546GW-02 EPA 3510 EPA 8270
92325998003 344313 344546DUP-02-011117 EPA 3510 EPA 8270
92325998001 344139GW-03 EPA 8260
92325998002 344139GW-02 EPA 8260
92325998003 344139DUP-02-011117 EPA 8260
92325998004 344139TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 10:12 AM
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Page 31 of 34
Page 32 of 34
Page 33 of 34
Page 34 of 34
#=CL#
January 30, 2017
LIMS USE: FR - HALEY HINDES
LIMS OBJECT ID: 92325933
92325933
Project:
Pace Project No.:
RE:
Haley Hindes
Terracon NC
2020 Starita Rd
Suite E
Charlotte, NC 28206
71167563 CAROLINA FOUNDRY
Dear Haley Hindes:
Enclosed are the analytical results for sample(s) received by the laboratory on January 11, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Report revised 1/30/17 to add MDLs and J-flags.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Page 1 of 57
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 57
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Lab ID Sample ID Matrix Date Collected Date Received
92325933001 S-11 Solid 01/10/17 11:30 01/11/17 13:25
92325933002 S-12 Solid 01/10/17 10:10 01/11/17 13:25
92325933003 S-13 Solid 01/10/17 14:15 01/11/17 13:25
92325933004 S-14 Solid 01/10/17 14:00 01/11/17 13:25
92325933005 S-15 Solid 01/10/17 13:15 01/11/17 13:25
92325933006 S-16 Solid 01/10/17 13:55 01/11/17 13:25
92325933007 DUP-01-011017 Solid 01/10/17 00:00 01/11/17 13:25
92325933008 BG-01 Solid 01/10/17 11:50 01/11/17 13:25
92325933009 BG-02 Solid 01/10/17 10:40 01/11/17 13:25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 57
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325933001 S-11 EPA 6010 10 PASI-ASER
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933002 S-12 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933003 S-13 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933004 S-14 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933005 S-15 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933006 S-16 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933007 DUP-01-011017 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92325933008 BG-01 EPA 6010 10 PASI-ASER, SH1
EPA 7471 1 PASI-AWAB
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 57
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CCLW
92325933009 BG-02 EPA 6010 10 PASI-ASER
EPA 7471 1 PASI-AWAB
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
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Page 5 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-11 Lab ID: 92325933001 Collected: 01/10/17 11:30 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 11000 mg/kg 01/13/17 19:42 7429-90-501/12/17 23:1511.3 5.7 1
Arsenic 3.9 mg/kg 01/13/17 19:42 7440-38-201/12/17 23:151.1 0.57 1
Barium 44.1 mg/kg 01/13/17 19:42 7440-39-301/12/17 23:150.57 0.28 1
Cadmium ND mg/kg 01/13/17 19:42 7440-43-901/12/17 23:150.11 0.057 1
Chromium 23.2 mg/kg 01/13/17 19:42 7440-47-301/12/17 23:150.57 0.28 1
Copper 69.6 mg/kg 01/13/17 19:42 7440-50-801/12/17 23:150.57 0.28 1
Lead 15.9 mg/kg 01/13/17 19:42 7439-92-101/12/17 23:150.57 0.28 1
Selenium ND mg/kg 01/13/17 19:42 7782-49-201/12/17 23:151.1 0.57 1
Silver ND mg/kg 01/13/17 19:42 7440-22-401/12/17 23:150.57 0.28 1
Zinc 67.3 mg/kg 01/13/17 19:42 7440-66-601/12/17 23:151.1 0.57 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.044 mg/kg 01/13/17 09:13 7439-97-601/12/17 13:110.0039 0.0020 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 17:41 83-32-901/12/17 09:00395 91.0 1
Acenaphthylene ND ug/kg 01/13/17 17:41 208-96-801/12/17 09:00395 93.4 1
Aniline ND ug/kg 01/13/17 17:41 62-53-301/12/17 09:00395 107 1
Anthracene ND ug/kg 01/13/17 17:41 120-12-701/12/17 09:00395 88.6 1
Benzo(a)anthracene ND ug/kg 01/13/17 17:41 56-55-301/12/17 09:00395 73.1 1
Benzo(a)pyrene ND ug/kg 01/13/17 17:41 50-32-801/12/17 09:00395 75.5 1
Benzo(b)fluoranthene ND ug/kg 01/13/17 17:41 205-99-201/12/17 09:00395 68.3 1
Benzo(g,h,i)perylene ND ug/kg 01/13/17 17:41 191-24-201/12/17 09:00395 101 1
Benzo(k)fluoranthene ND ug/kg 01/13/17 17:41 207-08-901/12/17 09:00395 77.9 1
Benzoic Acid ND ug/kg 01/13/17 17:41 65-85-001/12/17 09:001980 71.9 1
Benzyl alcohol ND ug/kg 01/13/17 17:41 100-51-601/12/17 09:00791 79.1 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 17:41 101-55-301/12/17 09:00395 71.9 1
Butylbenzylphthalate ND ug/kg 01/13/17 17:41 85-68-701/12/17 09:00395 83.9 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 17:41 59-50-701/12/17 09:00791 81.5 1
4-Chloroaniline ND ug/kg 01/13/17 17:41 106-47-801/12/17 09:001980 110 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 17:41 111-91-101/12/17 09:00395 92.2 1
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 17:41 111-44-401/12/17 09:00395 101 1
2-Chloronaphthalene ND ug/kg 01/13/17 17:41 91-58-701/12/17 09:00395 77.9 1
2-Chlorophenol ND ug/kg 01/13/17 17:41 95-57-801/12/17 09:00395 108 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 17:41 7005-72-301/12/17 09:00395 81.5 1
Chrysene ND ug/kg 01/13/17 17:41 218-01-901/12/17 09:00395 52.7 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 17:41 53-70-301/12/17 09:00395 83.9 1
Dibenzofuran ND ug/kg 01/13/17 17:41 132-64-901/12/17 09:00395 64.7 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 17:41 95-50-1 M101/12/17 09:00395 105 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 17:41 541-73-1 L201/12/17 09:00395 89.8 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 17:41 106-46-701/12/17 09:00395 111 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 17:41 91-94-101/12/17 09:001980 86.3 1
2,4-Dichlorophenol ND ug/kg 01/13/17 17:41 120-83-201/12/17 09:00395 86.3 1
Diethylphthalate ND ug/kg 01/13/17 17:41 84-66-201/12/17 09:00395 61.1 1
2,4-Dimethylphenol ND ug/kg 01/13/17 17:41 105-67-901/12/17 09:00395 156 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-11 Lab ID: 92325933001 Collected: 01/10/17 11:30 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Dimethylphthalate ND ug/kg 01/13/17 17:41 131-11-301/12/17 09:00395 80.3 1
Di-n-butylphthalate ND ug/kg 01/13/17 17:41 84-74-201/12/17 09:00395 64.7 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 17:41 534-52-101/12/17 09:00791 79.1 1
2,4-Dinitrophenol ND ug/kg 01/13/17 17:41 51-28-5 M101/12/17 09:001980 64.7 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 17:41 121-14-201/12/17 09:00395 74.3 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 17:41 606-20-201/12/17 09:00395 82.7 1
Di-n-octylphthalate ND ug/kg 01/13/17 17:41 117-84-001/12/17 09:00395 82.7 1
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 17:41 117-81-701/12/17 09:00395 108 1
Fluoranthene ND ug/kg 01/13/17 17:41 206-44-001/12/17 09:00395 57.5 1
Fluorene ND ug/kg 01/13/17 17:41 86-73-701/12/17 09:00395 81.5 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 17:41 87-68-301/12/17 09:00395 68.3 1
Hexachlorobenzene ND ug/kg 01/13/17 17:41 118-74-101/12/17 09:00395 50.3 1
Hexachlorocyclopentadiene ND ug/kg 01/13/17 17:41 77-47-401/12/17 09:00395 73.1 1
Hexachloroethane ND ug/kg 01/13/17 17:41 67-72-101/12/17 09:00395 104 1
Indeno(1,2,3-cd)pyrene ND ug/kg 01/13/17 17:41 193-39-501/12/17 09:00395 81.5 1
Isophorone ND ug/kg 01/13/17 17:41 78-59-101/12/17 09:00395 88.6 1
1-Methylnaphthalene ND ug/kg 01/13/17 17:41 90-12-001/12/17 09:00395 103 1
2-Methylnaphthalene ND ug/kg 01/13/17 17:41 91-57-601/12/17 09:00395 85.1 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 17:41 95-48-701/12/17 09:00395 120 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 17:4101/12/17 09:00395 156 1
Naphthalene ND ug/kg 01/13/17 17:41 91-20-301/12/17 09:00395 97.0 1
2-Nitroaniline ND ug/kg 01/13/17 17:41 88-74-401/12/17 09:001980 122 1
3-Nitroaniline ND ug/kg 01/13/17 17:41 99-09-201/12/17 09:001980 108 1
4-Nitroaniline ND ug/kg 01/13/17 17:41 100-01-601/12/17 09:00791 111 1
Nitrobenzene ND ug/kg 01/13/17 17:41 98-95-301/12/17 09:00395 108 1
2-Nitrophenol ND ug/kg 01/13/17 17:41 88-75-501/12/17 09:00395 95.8 1
4-Nitrophenol ND ug/kg 01/13/17 17:41 100-02-701/12/17 09:001980 70.7 1
N-Nitrosodimethylamine ND ug/kg 01/13/17 17:41 62-75-901/12/17 09:00395 128 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 17:41 621-64-701/12/17 09:00395 75.5 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 17:41 86-30-601/12/17 09:00395 117 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 17:41 108-60-1 M101/12/17 09:00395 105 1
Pentachlorophenol ND ug/kg 01/13/17 17:41 87-86-501/12/17 09:001980 71.9 1
Phenanthrene ND ug/kg 01/13/17 17:41 85-01-801/12/17 09:00395 65.9 1
Phenol ND ug/kg 01/13/17 17:4101/12/17 09:00395 119 1
Pyrene ND ug/kg 01/13/17 17:41 129-00-001/12/17 09:00395 67.1 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 17:41 120-82-101/12/17 09:00395 76.7 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 17:41 95-95-401/12/17 09:00395 122 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 17:41 88-06-201/12/17 09:00395 87.4 1
Surrogates
Nitrobenzene-d5 (S)40 %01/13/17 17:41 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)38 %01/13/17 17:41 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)63 %01/13/17 17:41 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)28 %01/13/17 17:41 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)26 %01/13/17 17:41 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)21 %01/13/17 17:41 118-79-6 S001/12/17 09:0027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-11 Lab ID: 92325933001 Collected: 01/10/17 11:30 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/12/17 13:29 67-64-196.0 9.6 1
Benzene ND ug/kg 01/12/17 13:29 71-43-24.8 1.5 1
Bromobenzene ND ug/kg 01/12/17 13:29 108-86-14.8 1.9 1
Bromochloromethane ND ug/kg 01/12/17 13:29 74-97-54.8 1.6 1
Bromodichloromethane ND ug/kg 01/12/17 13:29 75-27-44.8 1.8 1
Bromoform ND ug/kg 01/12/17 13:29 75-25-24.8 2.2 1
Bromomethane ND ug/kg 01/12/17 13:29 74-83-99.6 2.4 1
2-Butanone (MEK)ND ug/kg 01/12/17 13:29 78-93-396.0 2.8 1
n-Butylbenzene ND ug/kg 01/12/17 13:29 104-51-84.8 1.7 1
sec-Butylbenzene ND ug/kg 01/12/17 13:29 135-98-84.8 1.5 1
tert-Butylbenzene ND ug/kg 01/12/17 13:29 98-06-64.8 1.9 1
Carbon tetrachloride ND ug/kg 01/12/17 13:29 56-23-54.8 2.5 1
Chlorobenzene ND ug/kg 01/12/17 13:29 108-90-74.8 1.8 1
Chloroethane ND ug/kg 01/12/17 13:29 75-00-39.6 2.3 1
Chloroform ND ug/kg 01/12/17 13:29 67-66-34.8 1.5 1
Chloromethane ND ug/kg 01/12/17 13:29 74-87-39.6 2.3 1
2-Chlorotoluene ND ug/kg 01/12/17 13:29 95-49-84.8 1.6 1
4-Chlorotoluene ND ug/kg 01/12/17 13:29 106-43-44.8 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 13:29 96-12-84.8 3.5 1
Dibromochloromethane ND ug/kg 01/12/17 13:29 124-48-14.8 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 13:29 106-93-44.8 1.7 1
Dibromomethane ND ug/kg 01/12/17 13:29 74-95-34.8 2.4 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 13:29 95-50-14.8 1.8 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 13:29 541-73-14.8 1.9 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 13:29 106-46-74.8 1.6 1
Dichlorodifluoromethane ND ug/kg 01/12/17 13:29 75-71-89.6 3.5 1
1,1-Dichloroethane ND ug/kg 01/12/17 13:29 75-34-34.8 1.4 1
1,2-Dichloroethane ND ug/kg 01/12/17 13:29 107-06-24.8 2.1 1
1,1-Dichloroethene ND ug/kg 01/12/17 13:29 75-35-44.8 1.7 1
cis-1,2-Dichloroethene ND ug/kg 01/12/17 13:29 156-59-24.8 1.3 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 13:29 156-60-54.8 1.8 1
1,2-Dichloropropane ND ug/kg 01/12/17 13:29 78-87-54.8 1.6 1
1,3-Dichloropropane ND ug/kg 01/12/17 13:29 142-28-94.8 1.8 1
2,2-Dichloropropane ND ug/kg 01/12/17 13:29 594-20-74.8 1.6 1
1,1-Dichloropropene ND ug/kg 01/12/17 13:29 563-58-64.8 1.4 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 13:29 10061-01-54.8 1.7 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 13:29 10061-02-64.8 1.4 1
Diisopropyl ether ND ug/kg 01/12/17 13:29 108-20-34.8 1.6 1
Ethylbenzene ND ug/kg 01/12/17 13:29 100-41-44.8 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 13:29 87-68-34.8 1.9 1
2-Hexanone ND ug/kg 01/12/17 13:29 591-78-648.0 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 13:29 98-82-84.8 1.8 1
p-Isopropyltoluene ND ug/kg 01/12/17 13:29 99-87-64.8 1.6 1
Methylene Chloride 6.3J ug/kg 01/12/17 13:29 75-09-219.2 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 13:29 108-10-148.0 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-11 Lab ID: 92325933001 Collected: 01/10/17 11:30 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 01/12/17 13:29 1634-04-44.8 1.4 1
Naphthalene 3.9J ug/kg 01/12/17 13:29 91-20-34.8 1.2 1
n-Propylbenzene ND ug/kg 01/12/17 13:29 103-65-14.8 1.6 1
Styrene ND ug/kg 01/12/17 13:29 100-42-54.8 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 13:29 630-20-64.8 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 13:29 79-34-54.8 1.8 1
Tetrachloroethene ND ug/kg 01/12/17 13:29 127-18-44.8 1.6 1
Toluene ND ug/kg 01/12/17 13:29 108-88-34.8 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 13:29 87-61-64.8 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 13:29 120-82-14.8 1.5 1
1,1,1-Trichloroethane ND ug/kg 01/12/17 13:29 71-55-64.8 1.7 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 13:29 79-00-54.8 2.0 1
Trichloroethene ND ug/kg 01/12/17 13:29 79-01-64.8 2.0 1
Trichlorofluoromethane ND ug/kg 01/12/17 13:29 75-69-44.8 2.1 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 13:29 96-18-44.8 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 13:29 95-63-64.8 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 13:29 108-67-84.8 1.7 1
Vinyl acetate ND ug/kg 01/12/17 13:29 108-05-448.0 8.4 1
Vinyl chloride ND ug/kg 01/12/17 13:29 75-01-49.6 1.7 1
Xylene (Total)ND ug/kg 01/12/17 13:29 1330-20-79.6 3.5 1
m&p-Xylene ND ug/kg 01/12/17 13:29 179601-23-19.6 3.5 1
o-Xylene ND ug/kg 01/12/17 13:29 95-47-64.8 1.8 1
Surrogates
Toluene-d8 (S)99 %01/12/17 13:29 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %01/12/17 13:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %01/12/17 13:29 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.5 %01/13/17 07:250.10 0.10 1
Sample: S-12 Lab ID: 92325933002 Collected: 01/10/17 10:10 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 11000 mg/kg 01/14/17 08:38 7429-90-501/12/17 23:1571.0 35.5 10
Arsenic 4.6 mg/kg 01/13/17 19:45 7440-38-201/12/17 23:150.71 0.36 1
Barium 72.9 mg/kg 01/13/17 19:45 7440-39-301/12/17 23:150.36 0.18 1
Cadmium 0.069J mg/kg 01/13/17 19:45 7440-43-901/12/17 23:150.071 0.036 1
Chromium 26.2 mg/kg 01/13/17 19:45 7440-47-301/12/17 23:150.36 0.18 1
Copper 57.1 mg/kg 01/13/17 19:45 7440-50-801/12/17 23:150.36 0.18 1
Lead 81.8 mg/kg 01/13/17 19:45 7439-92-101/12/17 23:150.36 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-12 Lab ID: 92325933002 Collected: 01/10/17 10:10 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Selenium ND mg/kg 01/13/17 19:45 7782-49-201/12/17 23:150.71 0.36 1
Silver 0.26J mg/kg 01/13/17 19:45 7440-22-401/12/17 23:150.36 0.18 1
Zinc 74.2 mg/kg 01/13/17 19:45 7440-66-601/12/17 23:150.71 0.36 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.063 mg/kg 01/13/17 09:15 7439-97-601/12/17 13:110.0028 0.0014 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 18:35 83-32-901/12/17 09:00399 91.8 1
Acenaphthylene ND ug/kg 01/13/17 18:35 208-96-801/12/17 09:00399 94.2 1
Aniline ND ug/kg 01/13/17 18:35 62-53-301/12/17 09:00399 107 1
Anthracene ND ug/kg 01/13/17 18:35 120-12-701/12/17 09:00399 89.4 1
Benzo(a)anthracene 172J ug/kg 01/13/17 18:35 56-55-301/12/17 09:00399 73.7 1
Benzo(a)pyrene 179J ug/kg 01/13/17 18:35 50-32-801/12/17 09:00399 76.1 1
Benzo(b)fluoranthene 239J ug/kg 01/13/17 18:35 205-99-201/12/17 09:00399 68.8 1
Benzo(g,h,i)perylene 133J ug/kg 01/13/17 18:35 191-24-201/12/17 09:00399 101 1
Benzo(k)fluoranthene 106J ug/kg 01/13/17 18:35 207-08-901/12/17 09:00399 78.5 1
Benzoic Acid ND ug/kg 01/13/17 18:35 65-85-001/12/17 09:001990 72.5 1
Benzyl alcohol ND ug/kg 01/13/17 18:35 100-51-601/12/17 09:00797 79.7 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 18:35 101-55-301/12/17 09:00399 72.5 1
Butylbenzylphthalate ND ug/kg 01/13/17 18:35 85-68-701/12/17 09:00399 84.5 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 18:35 59-50-701/12/17 09:00797 82.1 1
4-Chloroaniline ND ug/kg 01/13/17 18:35 106-47-801/12/17 09:001990 111 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 18:35 111-91-101/12/17 09:00399 93.0 1
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 18:35 111-44-401/12/17 09:00399 101 1
2-Chloronaphthalene ND ug/kg 01/13/17 18:35 91-58-701/12/17 09:00399 78.5 1
2-Chlorophenol ND ug/kg 01/13/17 18:35 95-57-801/12/17 09:00399 109 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 18:35 7005-72-301/12/17 09:00399 82.1 1
Chrysene 172J ug/kg 01/13/17 18:35 218-01-901/12/17 09:00399 53.1 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 18:35 53-70-301/12/17 09:00399 84.5 1
Dibenzofuran ND ug/kg 01/13/17 18:35 132-64-901/12/17 09:00399 65.2 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 18:35 95-50-101/12/17 09:00399 106 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 18:35 541-73-1 L201/12/17 09:00399 90.6 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 18:35 106-46-701/12/17 09:00399 112 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 18:35 91-94-101/12/17 09:001990 87.0 1
2,4-Dichlorophenol ND ug/kg 01/13/17 18:35 120-83-201/12/17 09:00399 87.0 1
Diethylphthalate ND ug/kg 01/13/17 18:35 84-66-201/12/17 09:00399 61.6 1
2,4-Dimethylphenol ND ug/kg 01/13/17 18:35 105-67-901/12/17 09:00399 157 1
Dimethylphthalate ND ug/kg 01/13/17 18:35 131-11-301/12/17 09:00399 80.9 1
Di-n-butylphthalate ND ug/kg 01/13/17 18:35 84-74-201/12/17 09:00399 65.2 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 18:35 534-52-101/12/17 09:00797 79.7 1
2,4-Dinitrophenol ND ug/kg 01/13/17 18:35 51-28-501/12/17 09:001990 65.2 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 18:35 121-14-201/12/17 09:00399 74.9 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 18:35 606-20-201/12/17 09:00399 83.3 1
Di-n-octylphthalate ND ug/kg 01/13/17 18:35 117-84-001/12/17 09:00399 83.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-12 Lab ID: 92325933002 Collected: 01/10/17 10:10 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 18:35 117-81-701/12/17 09:00399 109 1
Fluoranthene 354J ug/kg 01/13/17 18:35 206-44-001/12/17 09:00399 58.0 1
Fluorene ND ug/kg 01/13/17 18:35 86-73-701/12/17 09:00399 82.1 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 18:35 87-68-301/12/17 09:00399 68.8 1
Hexachlorobenzene ND ug/kg 01/13/17 18:35 118-74-101/12/17 09:00399 50.7 1
Hexachlorocyclopentadiene ND ug/kg 01/13/17 18:35 77-47-401/12/17 09:00399 73.7 1
Hexachloroethane ND ug/kg 01/13/17 18:35 67-72-101/12/17 09:00399 105 1
Indeno(1,2,3-cd)pyrene 112J ug/kg 01/13/17 18:35 193-39-501/12/17 09:00399 82.1 1
Isophorone ND ug/kg 01/13/17 18:35 78-59-101/12/17 09:00399 89.4 1
1-Methylnaphthalene ND ug/kg 01/13/17 18:35 90-12-001/12/17 09:00399 104 1
2-Methylnaphthalene ND ug/kg 01/13/17 18:35 91-57-601/12/17 09:00399 85.8 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 18:35 95-48-701/12/17 09:00399 121 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 18:3501/12/17 09:00399 157 1
Naphthalene ND ug/kg 01/13/17 18:35 91-20-301/12/17 09:00399 97.8 1
2-Nitroaniline ND ug/kg 01/13/17 18:35 88-74-401/12/17 09:001990 123 1
3-Nitroaniline ND ug/kg 01/13/17 18:35 99-09-201/12/17 09:001990 109 1
4-Nitroaniline ND ug/kg 01/13/17 18:35 100-01-601/12/17 09:00797 112 1
Nitrobenzene ND ug/kg 01/13/17 18:35 98-95-301/12/17 09:00399 109 1
2-Nitrophenol ND ug/kg 01/13/17 18:35 88-75-501/12/17 09:00399 96.6 1
4-Nitrophenol ND ug/kg 01/13/17 18:35 100-02-701/12/17 09:001990 71.3 1
N-Nitrosodimethylamine ND ug/kg 01/13/17 18:35 62-75-901/12/17 09:00399 129 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 18:35 621-64-701/12/17 09:00399 76.1 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 18:35 86-30-601/12/17 09:00399 118 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 18:35 108-60-101/12/17 09:00399 106 1
Pentachlorophenol ND ug/kg 01/13/17 18:35 87-86-501/12/17 09:001990 72.5 1
Phenanthrene 237J ug/kg 01/13/17 18:35 85-01-801/12/17 09:00399 66.4 1
Phenol ND ug/kg 01/13/17 18:3501/12/17 09:00399 120 1
Pyrene 278J ug/kg 01/13/17 18:35 129-00-001/12/17 09:00399 67.6 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 18:35 120-82-101/12/17 09:00399 77.3 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 18:35 95-95-401/12/17 09:00399 123 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 18:35 88-06-201/12/17 09:00399 88.2 1
Surrogates
Nitrobenzene-d5 (S)64 %01/13/17 18:35 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)55 %01/13/17 18:35 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)78 %01/13/17 18:35 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)50 %01/13/17 18:35 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)42 %01/13/17 18:35 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)45 %01/13/17 18:35 118-79-601/12/17 09:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/12/17 13:49 67-64-176.3 7.6 1
Benzene ND ug/kg 01/12/17 13:49 71-43-23.8 1.2 1
Bromobenzene ND ug/kg 01/12/17 13:49 108-86-13.8 1.5 1
Bromochloromethane ND ug/kg 01/12/17 13:49 74-97-53.8 1.3 1
Bromodichloromethane ND ug/kg 01/12/17 13:49 75-27-43.8 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-12 Lab ID: 92325933002 Collected: 01/10/17 10:10 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Bromoform ND ug/kg 01/12/17 13:49 75-25-23.8 1.8 1
Bromomethane ND ug/kg 01/12/17 13:49 74-83-97.6 1.9 1
2-Butanone (MEK)ND ug/kg 01/12/17 13:49 78-93-376.3 2.2 1
n-Butylbenzene ND ug/kg 01/12/17 13:49 104-51-83.8 1.4 1
sec-Butylbenzene ND ug/kg 01/12/17 13:49 135-98-83.8 1.2 1
tert-Butylbenzene ND ug/kg 01/12/17 13:49 98-06-63.8 1.5 1
Carbon tetrachloride ND ug/kg 01/12/17 13:49 56-23-53.8 2.0 1
Chlorobenzene ND ug/kg 01/12/17 13:49 108-90-73.8 1.5 1
Chloroethane ND ug/kg 01/12/17 13:49 75-00-37.6 1.8 1
Chloroform ND ug/kg 01/12/17 13:49 67-66-33.8 1.2 1
Chloromethane ND ug/kg 01/12/17 13:49 74-87-37.6 1.8 1
2-Chlorotoluene ND ug/kg 01/12/17 13:49 95-49-83.8 1.3 1
4-Chlorotoluene ND ug/kg 01/12/17 13:49 106-43-43.8 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 13:49 96-12-83.8 2.7 1
Dibromochloromethane ND ug/kg 01/12/17 13:49 124-48-13.8 1.4 1
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 13:49 106-93-43.8 1.4 1
Dibromomethane ND ug/kg 01/12/17 13:49 74-95-33.8 1.9 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 13:49 95-50-13.8 1.5 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 13:49 541-73-13.8 1.5 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 13:49 106-46-73.8 1.3 1
Dichlorodifluoromethane ND ug/kg 01/12/17 13:49 75-71-87.6 2.7 1
1,1-Dichloroethane ND ug/kg 01/12/17 13:49 75-34-33.8 1.1 1
1,2-Dichloroethane ND ug/kg 01/12/17 13:49 107-06-23.8 1.7 1
1,1-Dichloroethene ND ug/kg 01/12/17 13:49 75-35-43.8 1.4 1
cis-1,2-Dichloroethene ND ug/kg 01/12/17 13:49 156-59-23.8 1.1 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 13:49 156-60-53.8 1.5 1
1,2-Dichloropropane ND ug/kg 01/12/17 13:49 78-87-53.8 1.3 1
1,3-Dichloropropane ND ug/kg 01/12/17 13:49 142-28-93.8 1.5 1
2,2-Dichloropropane ND ug/kg 01/12/17 13:49 594-20-73.8 1.3 1
1,1-Dichloropropene ND ug/kg 01/12/17 13:49 563-58-63.8 1.1 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 13:49 10061-01-53.8 1.4 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 13:49 10061-02-63.8 1.1 1
Diisopropyl ether ND ug/kg 01/12/17 13:49 108-20-33.8 1.3 1
Ethylbenzene ND ug/kg 01/12/17 13:49 100-41-43.8 1.4 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 13:49 87-68-33.8 1.5 1
2-Hexanone ND ug/kg 01/12/17 13:49 591-78-638.2 3.0 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 13:49 98-82-83.8 1.5 1
p-Isopropyltoluene ND ug/kg 01/12/17 13:49 99-87-63.8 1.3 1
Methylene Chloride 4.3J ug/kg 01/12/17 13:49 75-09-215.3 2.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 13:49 108-10-138.2 2.8 1
Methyl-tert-butyl ether ND ug/kg 01/12/17 13:49 1634-04-43.8 1.1 1
Naphthalene ND ug/kg 01/12/17 13:49 91-20-33.8 0.92 1
n-Propylbenzene ND ug/kg 01/12/17 13:49 103-65-13.8 1.3 1
Styrene ND ug/kg 01/12/17 13:49 100-42-53.8 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 13:49 630-20-63.8 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-12 Lab ID: 92325933002 Collected: 01/10/17 10:10 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 13:49 79-34-53.8 1.5 1
Tetrachloroethene ND ug/kg 01/12/17 13:49 127-18-43.8 1.3 1
Toluene ND ug/kg 01/12/17 13:49 108-88-33.8 1.4 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 13:49 87-61-63.8 1.7 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 13:49 120-82-13.8 1.2 1
1,1,1-Trichloroethane ND ug/kg 01/12/17 13:49 71-55-63.8 1.4 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 13:49 79-00-53.8 1.6 1
Trichloroethene ND ug/kg 01/12/17 13:49 79-01-63.8 1.6 1
Trichlorofluoromethane ND ug/kg 01/12/17 13:49 75-69-43.8 1.7 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 13:49 96-18-43.8 1.2 1
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 13:49 95-63-63.8 1.5 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 13:49 108-67-83.8 1.4 1
Vinyl acetate ND ug/kg 01/12/17 13:49 108-05-4 M138.2 6.7 1
Vinyl chloride ND ug/kg 01/12/17 13:49 75-01-47.6 1.4 1
Xylene (Total)ND ug/kg 01/12/17 13:49 1330-20-77.6 2.7 1
m&p-Xylene ND ug/kg 01/12/17 13:49 179601-23-17.6 2.7 1
o-Xylene ND ug/kg 01/12/17 13:49 95-47-63.8 1.5 1
Surrogates
Toluene-d8 (S)99 %01/12/17 13:49 2037-26-570-130 1
4-Bromofluorobenzene (S)103 %01/12/17 13:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %01/12/17 13:49 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.2 %01/13/17 07:250.10 0.10 1
Sample: S-13 Lab ID: 92325933003 Collected: 01/10/17 14:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 15300 mg/kg 01/14/17 08:41 7429-90-501/12/17 23:1577.3 38.7 10
Arsenic 2.9 mg/kg 01/13/17 19:48 7440-38-201/12/17 23:150.77 0.39 1
Barium 59.9 mg/kg 01/13/17 19:48 7440-39-301/12/17 23:150.39 0.19 1
Cadmium ND mg/kg 01/13/17 19:48 7440-43-901/12/17 23:150.077 0.039 1
Chromium 24.1 mg/kg 01/13/17 19:48 7440-47-301/12/17 23:150.39 0.19 1
Copper 12.3 mg/kg 01/13/17 19:48 7440-50-801/12/17 23:150.39 0.19 1
Lead 11.5 mg/kg 01/13/17 19:48 7439-92-101/12/17 23:150.39 0.19 1
Selenium ND mg/kg 01/13/17 19:48 7782-49-201/12/17 23:150.77 0.39 1
Silver ND mg/kg 01/13/17 19:48 7440-22-401/12/17 23:150.39 0.19 1
Zinc 8.4 mg/kg 01/13/17 19:48 7440-66-601/12/17 23:150.77 0.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-13 Lab ID: 92325933003 Collected: 01/10/17 14:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.011 mg/kg 01/13/17 09:18 7439-97-601/12/17 13:110.0032 0.0016 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 19:01 83-32-901/12/17 09:00408 94.0 1
Acenaphthylene ND ug/kg 01/13/17 19:01 208-96-801/12/17 09:00408 96.5 1
Aniline ND ug/kg 01/13/17 19:01 62-53-301/12/17 09:00408 110 1
Anthracene ND ug/kg 01/13/17 19:01 120-12-701/12/17 09:00408 91.5 1
Benzo(a)anthracene ND ug/kg 01/13/17 19:01 56-55-301/12/17 09:00408 75.5 1
Benzo(a)pyrene ND ug/kg 01/13/17 19:01 50-32-801/12/17 09:00408 77.9 1
Benzo(b)fluoranthene ND ug/kg 01/13/17 19:01 205-99-201/12/17 09:00408 70.5 1
Benzo(g,h,i)perylene ND ug/kg 01/13/17 19:01 191-24-201/12/17 09:00408 104 1
Benzo(k)fluoranthene ND ug/kg 01/13/17 19:01 207-08-901/12/17 09:00408 80.4 1
Benzoic Acid ND ug/kg 01/13/17 19:01 65-85-001/12/17 09:002040 74.2 1
Benzyl alcohol ND ug/kg 01/13/17 19:01 100-51-601/12/17 09:00816 81.6 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 19:01 101-55-301/12/17 09:00408 74.2 1
Butylbenzylphthalate ND ug/kg 01/13/17 19:01 85-68-701/12/17 09:00408 86.6 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 19:01 59-50-701/12/17 09:00816 84.1 1
4-Chloroaniline ND ug/kg 01/13/17 19:01 106-47-801/12/17 09:002040 114 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 19:01 111-91-101/12/17 09:00408 95.3 1
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 19:01 111-44-401/12/17 09:00408 104 1
2-Chloronaphthalene ND ug/kg 01/13/17 19:01 91-58-701/12/17 09:00408 80.4 1
2-Chlorophenol ND ug/kg 01/13/17 19:01 95-57-801/12/17 09:00408 111 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 19:01 7005-72-301/12/17 09:00408 84.1 1
Chrysene ND ug/kg 01/13/17 19:01 218-01-901/12/17 09:00408 54.4 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 19:01 53-70-301/12/17 09:00408 86.6 1
Dibenzofuran ND ug/kg 01/13/17 19:01 132-64-901/12/17 09:00408 66.8 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 19:01 95-50-101/12/17 09:00408 109 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 19:01 541-73-1 L201/12/17 09:00408 92.8 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 19:01 106-46-701/12/17 09:00408 115 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 19:01 91-94-101/12/17 09:002040 89.1 1
2,4-Dichlorophenol ND ug/kg 01/13/17 19:01 120-83-201/12/17 09:00408 89.1 1
Diethylphthalate ND ug/kg 01/13/17 19:01 84-66-201/12/17 09:00408 63.1 1
2,4-Dimethylphenol ND ug/kg 01/13/17 19:01 105-67-901/12/17 09:00408 161 1
Dimethylphthalate ND ug/kg 01/13/17 19:01 131-11-301/12/17 09:00408 82.9 1
Di-n-butylphthalate ND ug/kg 01/13/17 19:01 84-74-201/12/17 09:00408 66.8 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 19:01 534-52-101/12/17 09:00816 81.6 1
2,4-Dinitrophenol ND ug/kg 01/13/17 19:01 51-28-501/12/17 09:002040 66.8 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 19:01 121-14-201/12/17 09:00408 76.7 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 19:01 606-20-201/12/17 09:00408 85.4 1
Di-n-octylphthalate ND ug/kg 01/13/17 19:01 117-84-001/12/17 09:00408 85.4 1
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 19:01 117-81-701/12/17 09:00408 111 1
Fluoranthene ND ug/kg 01/13/17 19:01 206-44-001/12/17 09:00408 59.4 1
Fluorene ND ug/kg 01/13/17 19:01 86-73-701/12/17 09:00408 84.1 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 19:01 87-68-301/12/17 09:00408 70.5 1
Hexachlorobenzene ND ug/kg 01/13/17 19:01 118-74-101/12/17 09:00408 52.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-13 Lab ID: 92325933003 Collected: 01/10/17 14:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Hexachlorocyclopentadiene ND ug/kg 01/13/17 19:01 77-47-401/12/17 09:00408 75.5 1
Hexachloroethane ND ug/kg 01/13/17 19:01 67-72-101/12/17 09:00408 108 1
Indeno(1,2,3-cd)pyrene ND ug/kg 01/13/17 19:01 193-39-501/12/17 09:00408 84.1 1
Isophorone ND ug/kg 01/13/17 19:01 78-59-101/12/17 09:00408 91.5 1
1-Methylnaphthalene ND ug/kg 01/13/17 19:01 90-12-001/12/17 09:00408 106 1
2-Methylnaphthalene ND ug/kg 01/13/17 19:01 91-57-601/12/17 09:00408 87.8 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 19:01 95-48-701/12/17 09:00408 124 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 19:0101/12/17 09:00408 161 1
Naphthalene ND ug/kg 01/13/17 19:01 91-20-301/12/17 09:00408 100 1
2-Nitroaniline ND ug/kg 01/13/17 19:01 88-74-401/12/17 09:002040 126 1
3-Nitroaniline ND ug/kg 01/13/17 19:01 99-09-201/12/17 09:002040 111 1
4-Nitroaniline ND ug/kg 01/13/17 19:01 100-01-601/12/17 09:00816 115 1
Nitrobenzene ND ug/kg 01/13/17 19:01 98-95-301/12/17 09:00408 111 1
2-Nitrophenol ND ug/kg 01/13/17 19:01 88-75-501/12/17 09:00408 99.0 1
4-Nitrophenol ND ug/kg 01/13/17 19:01 100-02-701/12/17 09:002040 73.0 1
N-Nitrosodimethylamine ND ug/kg 01/13/17 19:01 62-75-901/12/17 09:00408 132 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 19:01 621-64-701/12/17 09:00408 77.9 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 19:01 86-30-601/12/17 09:00408 121 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 19:01 108-60-101/12/17 09:00408 109 1
Pentachlorophenol ND ug/kg 01/13/17 19:01 87-86-501/12/17 09:002040 74.2 1
Phenanthrene ND ug/kg 01/13/17 19:01 85-01-801/12/17 09:00408 68.0 1
Phenol ND ug/kg 01/13/17 19:0101/12/17 09:00408 122 1
Pyrene ND ug/kg 01/13/17 19:01 129-00-001/12/17 09:00408 69.3 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 19:01 120-82-101/12/17 09:00408 79.2 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 19:01 95-95-401/12/17 09:00408 126 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 19:01 88-06-201/12/17 09:00408 90.3 1
Surrogates
Nitrobenzene-d5 (S)53 %01/13/17 19:01 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)48 %01/13/17 19:01 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)70 %01/13/17 19:01 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)48 %01/13/17 19:01 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)35 %01/13/17 19:01 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)42 %01/13/17 19:01 118-79-601/12/17 09:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/12/17 14:09 67-64-1101 10.1 1
Benzene ND ug/kg 01/12/17 14:09 71-43-25.0 1.6 1
Bromobenzene ND ug/kg 01/12/17 14:09 108-86-15.0 2.0 1
Bromochloromethane ND ug/kg 01/12/17 14:09 74-97-55.0 1.7 1
Bromodichloromethane ND ug/kg 01/12/17 14:09 75-27-45.0 1.9 1
Bromoform ND ug/kg 01/12/17 14:09 75-25-25.0 2.3 1
Bromomethane ND ug/kg 01/12/17 14:09 74-83-910.1 2.5 1
2-Butanone (MEK)ND ug/kg 01/12/17 14:09 78-93-3101 2.9 1
n-Butylbenzene ND ug/kg 01/12/17 14:09 104-51-85.0 1.8 1
sec-Butylbenzene ND ug/kg 01/12/17 14:09 135-98-85.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-13 Lab ID: 92325933003 Collected: 01/10/17 14:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
tert-Butylbenzene ND ug/kg 01/12/17 14:09 98-06-65.0 2.0 1
Carbon tetrachloride ND ug/kg 01/12/17 14:09 56-23-55.0 2.6 1
Chlorobenzene ND ug/kg 01/12/17 14:09 108-90-75.0 1.9 1
Chloroethane ND ug/kg 01/12/17 14:09 75-00-310.1 2.4 1
Chloroform ND ug/kg 01/12/17 14:09 67-66-35.0 1.6 1
Chloromethane ND ug/kg 01/12/17 14:09 74-87-310.1 2.4 1
2-Chlorotoluene ND ug/kg 01/12/17 14:09 95-49-85.0 1.7 1
4-Chlorotoluene ND ug/kg 01/12/17 14:09 106-43-45.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 14:09 96-12-85.0 3.6 1
Dibromochloromethane ND ug/kg 01/12/17 14:09 124-48-15.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 14:09 106-93-45.0 1.8 1
Dibromomethane ND ug/kg 01/12/17 14:09 74-95-35.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 14:09 95-50-15.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 14:09 541-73-15.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 14:09 106-46-75.0 1.7 1
Dichlorodifluoromethane ND ug/kg 01/12/17 14:09 75-71-810.1 3.6 1
1,1-Dichloroethane ND ug/kg 01/12/17 14:09 75-34-35.0 1.5 1
1,2-Dichloroethane ND ug/kg 01/12/17 14:09 107-06-25.0 2.2 1
1,1-Dichloroethene ND ug/kg 01/12/17 14:09 75-35-45.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 01/12/17 14:09 156-59-25.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 14:09 156-60-55.0 1.9 1
1,2-Dichloropropane ND ug/kg 01/12/17 14:09 78-87-55.0 1.7 1
1,3-Dichloropropane ND ug/kg 01/12/17 14:09 142-28-95.0 1.9 1
2,2-Dichloropropane ND ug/kg 01/12/17 14:09 594-20-75.0 1.7 1
1,1-Dichloropropene ND ug/kg 01/12/17 14:09 563-58-65.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 14:09 10061-01-55.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 14:09 10061-02-65.0 1.5 1
Diisopropyl ether ND ug/kg 01/12/17 14:09 108-20-35.0 1.7 1
Ethylbenzene ND ug/kg 01/12/17 14:09 100-41-45.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 14:09 87-68-35.0 2.0 1
2-Hexanone ND ug/kg 01/12/17 14:09 591-78-650.5 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 14:09 98-82-85.0 1.9 1
p-Isopropyltoluene ND ug/kg 01/12/17 14:09 99-87-65.0 1.7 1
Methylene Chloride 6.3J ug/kg 01/12/17 14:09 75-09-220.2 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 14:09 108-10-150.5 3.7 1
Methyl-tert-butyl ether ND ug/kg 01/12/17 14:09 1634-04-45.0 1.5 1
Naphthalene ND ug/kg 01/12/17 14:09 91-20-35.0 1.2 1
n-Propylbenzene ND ug/kg 01/12/17 14:09 103-65-15.0 1.7 1
Styrene ND ug/kg 01/12/17 14:09 100-42-55.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 14:09 630-20-65.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 14:09 79-34-55.0 1.9 1
Tetrachloroethene ND ug/kg 01/12/17 14:09 127-18-45.0 1.7 1
Toluene ND ug/kg 01/12/17 14:09 108-88-35.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 14:09 87-61-65.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 14:09 120-82-15.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-13 Lab ID: 92325933003 Collected: 01/10/17 14:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 01/12/17 14:09 71-55-65.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 14:09 79-00-55.0 2.1 1
Trichloroethene ND ug/kg 01/12/17 14:09 79-01-65.0 2.1 1
Trichlorofluoromethane ND ug/kg 01/12/17 14:09 75-69-45.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 14:09 96-18-45.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 14:09 95-63-65.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 14:09 108-67-85.0 1.8 1
Vinyl acetate ND ug/kg 01/12/17 14:09 108-05-450.5 8.9 1
Vinyl chloride ND ug/kg 01/12/17 14:09 75-01-410.1 1.8 1
Xylene (Total)ND ug/kg 01/12/17 14:09 1330-20-710.1 3.6 1
m&p-Xylene ND ug/kg 01/12/17 14:09 179601-23-110.1 3.6 1
o-Xylene ND ug/kg 01/12/17 14:09 95-47-65.0 1.9 1
Surrogates
Toluene-d8 (S)98 %01/12/17 14:09 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %01/12/17 14:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %01/12/17 14:09 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.2 %01/13/17 07:250.10 0.10 1
Sample: S-14 Lab ID: 92325933004 Collected: 01/10/17 14:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 10500 mg/kg 01/14/17 08:54 7429-90-501/12/17 23:1584.0 42.0 10
Arsenic 3.6 mg/kg 01/13/17 19:51 7440-38-201/12/17 23:150.84 0.42 1
Barium 17.5 mg/kg 01/13/17 19:51 7440-39-301/12/17 23:150.42 0.21 1
Cadmium ND mg/kg 01/13/17 19:51 7440-43-901/12/17 23:150.084 0.042 1
Chromium 35.7 mg/kg 01/13/17 19:51 7440-47-301/12/17 23:150.42 0.21 1
Copper 19.0 mg/kg 01/13/17 19:51 7440-50-801/12/17 23:150.42 0.21 1
Lead 11.3 mg/kg 01/13/17 19:51 7439-92-101/12/17 23:150.42 0.21 1
Selenium ND mg/kg 01/13/17 19:51 7782-49-201/12/17 23:150.84 0.42 1
Silver 0.38J mg/kg 01/13/17 19:51 7440-22-401/12/17 23:150.42 0.21 1
Zinc 14.3 mg/kg 01/13/17 19:51 7440-66-601/12/17 23:150.84 0.42 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.10 mg/kg 01/13/17 09:20 7439-97-601/12/17 13:110.0039 0.0019 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 19:28 83-32-901/12/17 09:00410 94.5 1
Acenaphthylene ND ug/kg 01/13/17 19:28 208-96-801/12/17 09:00410 97.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-14 Lab ID: 92325933004 Collected: 01/10/17 14:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Aniline ND ug/kg 01/13/17 19:28 62-53-301/12/17 09:00410 111 1
Anthracene ND ug/kg 01/13/17 19:28 120-12-701/12/17 09:00410 92.0 1
Benzo(a)anthracene ND ug/kg 01/13/17 19:28 56-55-301/12/17 09:00410 75.9 1
Benzo(a)pyrene ND ug/kg 01/13/17 19:28 50-32-801/12/17 09:00410 78.3 1
Benzo(b)fluoranthene ND ug/kg 01/13/17 19:28 205-99-201/12/17 09:00410 70.9 1
Benzo(g,h,i)perylene ND ug/kg 01/13/17 19:28 191-24-201/12/17 09:00410 104 1
Benzo(k)fluoranthene ND ug/kg 01/13/17 19:28 207-08-901/12/17 09:00410 80.8 1
Benzoic Acid ND ug/kg 01/13/17 19:28 65-85-001/12/17 09:002050 74.6 1
Benzyl alcohol ND ug/kg 01/13/17 19:28 100-51-601/12/17 09:00821 82.1 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 19:28 101-55-301/12/17 09:00410 74.6 1
Butylbenzylphthalate ND ug/kg 01/13/17 19:28 85-68-701/12/17 09:00410 87.0 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 19:28 59-50-701/12/17 09:00821 84.6 1
4-Chloroaniline ND ug/kg 01/13/17 19:28 106-47-801/12/17 09:002050 114 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 19:28 111-91-101/12/17 09:00410 95.8 1
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 19:28 111-44-401/12/17 09:00410 104 1
2-Chloronaphthalene ND ug/kg 01/13/17 19:28 91-58-701/12/17 09:00410 80.8 1
2-Chlorophenol ND ug/kg 01/13/17 19:28 95-57-801/12/17 09:00410 112 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 19:28 7005-72-301/12/17 09:00410 84.6 1
Chrysene ND ug/kg 01/13/17 19:28 218-01-901/12/17 09:00410 54.7 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 19:28 53-70-301/12/17 09:00410 87.0 1
Dibenzofuran ND ug/kg 01/13/17 19:28 132-64-901/12/17 09:00410 67.2 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 19:28 95-50-101/12/17 09:00410 109 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 19:28 541-73-1 L201/12/17 09:00410 93.3 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 19:28 106-46-701/12/17 09:00410 116 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 19:28 91-94-101/12/17 09:002050 89.5 1
2,4-Dichlorophenol ND ug/kg 01/13/17 19:28 120-83-201/12/17 09:00410 89.5 1
Diethylphthalate ND ug/kg 01/13/17 19:28 84-66-201/12/17 09:00410 63.4 1
2,4-Dimethylphenol ND ug/kg 01/13/17 19:28 105-67-901/12/17 09:00410 162 1
Dimethylphthalate ND ug/kg 01/13/17 19:28 131-11-301/12/17 09:00410 83.3 1
Di-n-butylphthalate ND ug/kg 01/13/17 19:28 84-74-201/12/17 09:00410 67.2 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 19:28 534-52-101/12/17 09:00821 82.1 1
2,4-Dinitrophenol ND ug/kg 01/13/17 19:28 51-28-501/12/17 09:002050 67.2 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 19:28 121-14-201/12/17 09:00410 77.1 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 19:28 606-20-201/12/17 09:00410 85.8 1
Di-n-octylphthalate ND ug/kg 01/13/17 19:28 117-84-001/12/17 09:00410 85.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 19:28 117-81-701/12/17 09:00410 112 1
Fluoranthene ND ug/kg 01/13/17 19:28 206-44-001/12/17 09:00410 59.7 1
Fluorene ND ug/kg 01/13/17 19:28 86-73-701/12/17 09:00410 84.6 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 19:28 87-68-301/12/17 09:00410 70.9 1
Hexachlorobenzene ND ug/kg 01/13/17 19:28 118-74-101/12/17 09:00410 52.2 1
Hexachlorocyclopentadiene ND ug/kg 01/13/17 19:28 77-47-401/12/17 09:00410 75.9 1
Hexachloroethane ND ug/kg 01/13/17 19:28 67-72-101/12/17 09:00410 108 1
Indeno(1,2,3-cd)pyrene ND ug/kg 01/13/17 19:28 193-39-501/12/17 09:00410 84.6 1
Isophorone ND ug/kg 01/13/17 19:28 78-59-101/12/17 09:00410 92.0 1
1-Methylnaphthalene ND ug/kg 01/13/17 19:28 90-12-001/12/17 09:00410 107 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-14 Lab ID: 92325933004 Collected: 01/10/17 14:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2-Methylnaphthalene ND ug/kg 01/13/17 19:28 91-57-601/12/17 09:00410 88.3 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 19:28 95-48-701/12/17 09:00410 124 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 19:2801/12/17 09:00410 162 1
Naphthalene ND ug/kg 01/13/17 19:28 91-20-301/12/17 09:00410 101 1
2-Nitroaniline ND ug/kg 01/13/17 19:28 88-74-401/12/17 09:002050 127 1
3-Nitroaniline ND ug/kg 01/13/17 19:28 99-09-201/12/17 09:002050 112 1
4-Nitroaniline ND ug/kg 01/13/17 19:28 100-01-601/12/17 09:00821 116 1
Nitrobenzene ND ug/kg 01/13/17 19:28 98-95-301/12/17 09:00410 112 1
2-Nitrophenol ND ug/kg 01/13/17 19:28 88-75-501/12/17 09:00410 99.5 1
4-Nitrophenol ND ug/kg 01/13/17 19:28 100-02-701/12/17 09:002050 73.4 1
N-Nitrosodimethylamine ND ug/kg 01/13/17 19:28 62-75-901/12/17 09:00410 133 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 19:28 621-64-701/12/17 09:00410 78.3 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 19:28 86-30-601/12/17 09:00410 122 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 19:28 108-60-101/12/17 09:00410 109 1
Pentachlorophenol ND ug/kg 01/13/17 19:28 87-86-501/12/17 09:002050 74.6 1
Phenanthrene ND ug/kg 01/13/17 19:28 85-01-801/12/17 09:00410 68.4 1
Phenol ND ug/kg 01/13/17 19:2801/12/17 09:00410 123 1
Pyrene ND ug/kg 01/13/17 19:28 129-00-001/12/17 09:00410 69.6 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 19:28 120-82-101/12/17 09:00410 79.6 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 19:28 95-95-401/12/17 09:00410 127 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 19:28 88-06-201/12/17 09:00410 90.8 1
Surrogates
Nitrobenzene-d5 (S)38 %01/13/17 19:28 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)48 %01/13/17 19:28 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)68 %01/13/17 19:28 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)55 %01/13/17 19:28 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)53 %01/13/17 19:28 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)52 %01/13/17 19:28 118-79-601/12/17 09:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/12/17 14:28 67-64-1101 10.1 1
Benzene ND ug/kg 01/12/17 14:28 71-43-25.0 1.6 1
Bromobenzene ND ug/kg 01/12/17 14:28 108-86-15.0 2.0 1
Bromochloromethane ND ug/kg 01/12/17 14:28 74-97-55.0 1.7 1
Bromodichloromethane ND ug/kg 01/12/17 14:28 75-27-45.0 1.9 1
Bromoform ND ug/kg 01/12/17 14:28 75-25-25.0 2.3 1
Bromomethane ND ug/kg 01/12/17 14:28 74-83-910.1 2.5 1
2-Butanone (MEK)ND ug/kg 01/12/17 14:28 78-93-3101 2.9 1
n-Butylbenzene ND ug/kg 01/12/17 14:28 104-51-85.0 1.8 1
sec-Butylbenzene ND ug/kg 01/12/17 14:28 135-98-85.0 1.6 1
tert-Butylbenzene ND ug/kg 01/12/17 14:28 98-06-65.0 2.0 1
Carbon tetrachloride ND ug/kg 01/12/17 14:28 56-23-55.0 2.6 1
Chlorobenzene ND ug/kg 01/12/17 14:28 108-90-75.0 1.9 1
Chloroethane ND ug/kg 01/12/17 14:28 75-00-310.1 2.4 1
Chloroform ND ug/kg 01/12/17 14:28 67-66-35.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-14 Lab ID: 92325933004 Collected: 01/10/17 14:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 01/12/17 14:28 74-87-310.1 2.4 1
2-Chlorotoluene ND ug/kg 01/12/17 14:28 95-49-85.0 1.7 1
4-Chlorotoluene ND ug/kg 01/12/17 14:28 106-43-45.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 14:28 96-12-85.0 3.6 1
Dibromochloromethane ND ug/kg 01/12/17 14:28 124-48-15.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 14:28 106-93-45.0 1.8 1
Dibromomethane ND ug/kg 01/12/17 14:28 74-95-35.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 14:28 95-50-15.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 14:28 541-73-15.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 14:28 106-46-75.0 1.7 1
Dichlorodifluoromethane ND ug/kg 01/12/17 14:28 75-71-810.1 3.6 1
1,1-Dichloroethane ND ug/kg 01/12/17 14:28 75-34-35.0 1.5 1
1,2-Dichloroethane ND ug/kg 01/12/17 14:28 107-06-25.0 2.2 1
1,1-Dichloroethene ND ug/kg 01/12/17 14:28 75-35-45.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 01/12/17 14:28 156-59-25.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 14:28 156-60-55.0 1.9 1
1,2-Dichloropropane ND ug/kg 01/12/17 14:28 78-87-55.0 1.7 1
1,3-Dichloropropane ND ug/kg 01/12/17 14:28 142-28-95.0 1.9 1
2,2-Dichloropropane ND ug/kg 01/12/17 14:28 594-20-75.0 1.7 1
1,1-Dichloropropene ND ug/kg 01/12/17 14:28 563-58-65.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 14:28 10061-01-55.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 14:28 10061-02-65.0 1.5 1
Diisopropyl ether ND ug/kg 01/12/17 14:28 108-20-35.0 1.7 1
Ethylbenzene ND ug/kg 01/12/17 14:28 100-41-45.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 14:28 87-68-35.0 2.0 1
2-Hexanone ND ug/kg 01/12/17 14:28 591-78-650.5 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 14:28 98-82-85.0 1.9 1
p-Isopropyltoluene ND ug/kg 01/12/17 14:28 99-87-65.0 1.7 1
Methylene Chloride 6.3J ug/kg 01/12/17 14:28 75-09-220.2 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 14:28 108-10-150.5 3.7 1
Methyl-tert-butyl ether ND ug/kg 01/12/17 14:28 1634-04-45.0 1.5 1
Naphthalene ND ug/kg 01/12/17 14:28 91-20-35.0 1.2 1
n-Propylbenzene ND ug/kg 01/12/17 14:28 103-65-15.0 1.7 1
Styrene ND ug/kg 01/12/17 14:28 100-42-55.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 14:28 630-20-65.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 14:28 79-34-55.0 1.9 1
Tetrachloroethene ND ug/kg 01/12/17 14:28 127-18-45.0 1.7 1
Toluene ND ug/kg 01/12/17 14:28 108-88-35.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 14:28 87-61-65.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 14:28 120-82-15.0 1.6 1
1,1,1-Trichloroethane ND ug/kg 01/12/17 14:28 71-55-65.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 14:28 79-00-55.0 2.1 1
Trichloroethene ND ug/kg 01/12/17 14:28 79-01-65.0 2.1 1
Trichlorofluoromethane ND ug/kg 01/12/17 14:28 75-69-45.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 14:28 96-18-45.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-14 Lab ID: 92325933004 Collected: 01/10/17 14:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 14:28 95-63-65.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 14:28 108-67-85.0 1.8 1
Vinyl acetate ND ug/kg 01/12/17 14:28 108-05-450.5 8.9 1
Vinyl chloride ND ug/kg 01/12/17 14:28 75-01-410.1 1.8 1
Xylene (Total)ND ug/kg 01/12/17 14:28 1330-20-710.1 3.6 1
m&p-Xylene ND ug/kg 01/12/17 14:28 179601-23-110.1 3.6 1
o-Xylene ND ug/kg 01/12/17 14:28 95-47-65.0 1.9 1
Surrogates
Toluene-d8 (S)97 %01/12/17 14:28 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %01/12/17 14:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %01/12/17 14:28 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.6 %01/13/17 07:270.10 0.10 1
Sample: S-15 Lab ID: 92325933005 Collected: 01/10/17 13:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 9880 mg/kg 01/14/17 08:57 7429-90-501/12/17 23:1591.9 45.9 10
Arsenic 3.6 mg/kg 01/13/17 19:54 7440-38-201/12/17 23:150.92 0.46 1
Barium 22.9 mg/kg 01/13/17 19:54 7440-39-301/12/17 23:150.46 0.23 1
Cadmium ND mg/kg 01/13/17 19:54 7440-43-901/12/17 23:150.092 0.046 1
Chromium 25.2 mg/kg 01/13/17 19:54 7440-47-301/12/17 23:150.46 0.23 1
Copper 18.1 mg/kg 01/13/17 19:54 7440-50-801/12/17 23:150.46 0.23 1
Lead 21.8 mg/kg 01/13/17 19:54 7439-92-101/12/17 23:150.46 0.23 1
Selenium ND mg/kg 01/13/17 19:54 7782-49-201/12/17 23:150.92 0.46 1
Silver 0.37J mg/kg 01/13/17 19:54 7440-22-401/12/17 23:150.46 0.23 1
Zinc 13.7 mg/kg 01/13/17 19:54 7440-66-601/12/17 23:150.92 0.46 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.065 mg/kg 01/13/17 09:22 7439-97-601/12/17 13:110.0037 0.0019 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 19:55 83-32-901/12/17 09:00412 95.0 1
Acenaphthylene ND ug/kg 01/13/17 19:55 208-96-801/12/17 09:00412 97.5 1
Aniline ND ug/kg 01/13/17 19:55 62-53-301/12/17 09:00412 111 1
Anthracene ND ug/kg 01/13/17 19:55 120-12-701/12/17 09:00412 92.5 1
Benzo(a)anthracene ND ug/kg 01/13/17 19:55 56-55-301/12/17 09:00412 76.2 1
Benzo(a)pyrene ND ug/kg 01/13/17 19:55 50-32-801/12/17 09:00412 78.7 1
Benzo(b)fluoranthene ND ug/kg 01/13/17 19:55 205-99-201/12/17 09:00412 71.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-15 Lab ID: 92325933005 Collected: 01/10/17 13:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Benzo(g,h,i)perylene ND ug/kg 01/13/17 19:55 191-24-201/12/17 09:00412 105 1
Benzo(k)fluoranthene ND ug/kg 01/13/17 19:55 207-08-901/12/17 09:00412 81.2 1
Benzoic Acid ND ug/kg 01/13/17 19:55 65-85-001/12/17 09:002060 75.0 1
Benzyl alcohol ND ug/kg 01/13/17 19:55 100-51-601/12/17 09:00825 82.5 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 19:55 101-55-301/12/17 09:00412 75.0 1
Butylbenzylphthalate ND ug/kg 01/13/17 19:55 85-68-701/12/17 09:00412 87.5 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 19:55 59-50-701/12/17 09:00825 85.0 1
4-Chloroaniline ND ug/kg 01/13/17 19:55 106-47-801/12/17 09:002060 115 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 19:55 111-91-101/12/17 09:00412 96.2 1
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 19:55 111-44-401/12/17 09:00412 105 1
2-Chloronaphthalene ND ug/kg 01/13/17 19:55 91-58-701/12/17 09:00412 81.2 1
2-Chlorophenol ND ug/kg 01/13/17 19:55 95-57-801/12/17 09:00412 112 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 19:55 7005-72-301/12/17 09:00412 85.0 1
Chrysene ND ug/kg 01/13/17 19:55 218-01-901/12/17 09:00412 55.0 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 19:55 53-70-301/12/17 09:00412 87.5 1
Dibenzofuran ND ug/kg 01/13/17 19:55 132-64-901/12/17 09:00412 67.5 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 19:55 95-50-101/12/17 09:00412 110 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 19:55 541-73-1 L201/12/17 09:00412 93.7 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 19:55 106-46-701/12/17 09:00412 116 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 19:55 91-94-101/12/17 09:002060 90.0 1
2,4-Dichlorophenol ND ug/kg 01/13/17 19:55 120-83-201/12/17 09:00412 90.0 1
Diethylphthalate ND ug/kg 01/13/17 19:55 84-66-201/12/17 09:00412 63.7 1
2,4-Dimethylphenol ND ug/kg 01/13/17 19:55 105-67-901/12/17 09:00412 162 1
Dimethylphthalate ND ug/kg 01/13/17 19:55 131-11-301/12/17 09:00412 83.7 1
Di-n-butylphthalate ND ug/kg 01/13/17 19:55 84-74-201/12/17 09:00412 67.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 19:55 534-52-101/12/17 09:00825 82.5 1
2,4-Dinitrophenol ND ug/kg 01/13/17 19:55 51-28-501/12/17 09:002060 67.5 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 19:55 121-14-201/12/17 09:00412 77.5 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 19:55 606-20-201/12/17 09:00412 86.2 1
Di-n-octylphthalate ND ug/kg 01/13/17 19:55 117-84-001/12/17 09:00412 86.2 1
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 19:55 117-81-701/12/17 09:00412 112 1
Fluoranthene 73.7J ug/kg 01/13/17 19:55 206-44-001/12/17 09:00412 60.0 1
Fluorene ND ug/kg 01/13/17 19:55 86-73-701/12/17 09:00412 85.0 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 19:55 87-68-301/12/17 09:00412 71.2 1
Hexachlorobenzene ND ug/kg 01/13/17 19:55 118-74-101/12/17 09:00412 52.5 1
Hexachlorocyclopentadiene ND ug/kg 01/13/17 19:55 77-47-401/12/17 09:00412 76.2 1
Hexachloroethane ND ug/kg 01/13/17 19:55 67-72-101/12/17 09:00412 109 1
Indeno(1,2,3-cd)pyrene ND ug/kg 01/13/17 19:55 193-39-501/12/17 09:00412 85.0 1
Isophorone ND ug/kg 01/13/17 19:55 78-59-101/12/17 09:00412 92.5 1
1-Methylnaphthalene ND ug/kg 01/13/17 19:55 90-12-001/12/17 09:00412 107 1
2-Methylnaphthalene ND ug/kg 01/13/17 19:55 91-57-601/12/17 09:00412 88.7 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 19:55 95-48-701/12/17 09:00412 125 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 19:5501/12/17 09:00412 162 1
Naphthalene ND ug/kg 01/13/17 19:55 91-20-301/12/17 09:00412 101 1
2-Nitroaniline ND ug/kg 01/13/17 19:55 88-74-401/12/17 09:002060 127 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-15 Lab ID: 92325933005 Collected: 01/10/17 13:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3-Nitroaniline ND ug/kg 01/13/17 19:55 99-09-201/12/17 09:002060 112 1
4-Nitroaniline ND ug/kg 01/13/17 19:55 100-01-601/12/17 09:00825 116 1
Nitrobenzene ND ug/kg 01/13/17 19:55 98-95-301/12/17 09:00412 112 1
2-Nitrophenol ND ug/kg 01/13/17 19:55 88-75-501/12/17 09:00412 100 1
4-Nitrophenol ND ug/kg 01/13/17 19:55 100-02-701/12/17 09:002060 73.7 1
N-Nitrosodimethylamine ND ug/kg 01/13/17 19:55 62-75-901/12/17 09:00412 134 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 19:55 621-64-701/12/17 09:00412 78.7 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 19:55 86-30-601/12/17 09:00412 122 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 19:55 108-60-101/12/17 09:00412 110 1
Pentachlorophenol ND ug/kg 01/13/17 19:55 87-86-501/12/17 09:002060 75.0 1
Phenanthrene ND ug/kg 01/13/17 19:55 85-01-801/12/17 09:00412 68.7 1
Phenol ND ug/kg 01/13/17 19:5501/12/17 09:00412 124 1
Pyrene ND ug/kg 01/13/17 19:55 129-00-001/12/17 09:00412 70.0 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 19:55 120-82-101/12/17 09:00412 80.0 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 19:55 95-95-401/12/17 09:00412 127 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 19:55 88-06-201/12/17 09:00412 91.2 1
Surrogates
Nitrobenzene-d5 (S)35 %01/13/17 19:55 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)37 %01/13/17 19:55 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)61 %01/13/17 19:55 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)44 %01/13/17 19:55 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)44 %01/13/17 19:55 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)61 %01/13/17 19:55 118-79-601/12/17 09:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/12/17 14:48 67-64-197.0 9.7 1
Benzene ND ug/kg 01/12/17 14:48 71-43-24.9 1.6 1
Bromobenzene ND ug/kg 01/12/17 14:48 108-86-14.9 1.9 1
Bromochloromethane ND ug/kg 01/12/17 14:48 74-97-54.9 1.6 1
Bromodichloromethane ND ug/kg 01/12/17 14:48 75-27-44.9 1.8 1
Bromoform ND ug/kg 01/12/17 14:48 75-25-24.9 2.2 1
Bromomethane ND ug/kg 01/12/17 14:48 74-83-99.7 2.4 1
2-Butanone (MEK)ND ug/kg 01/12/17 14:48 78-93-397.0 2.8 1
n-Butylbenzene ND ug/kg 01/12/17 14:48 104-51-84.9 1.7 1
sec-Butylbenzene ND ug/kg 01/12/17 14:48 135-98-84.9 1.6 1
tert-Butylbenzene ND ug/kg 01/12/17 14:48 98-06-64.9 1.9 1
Carbon tetrachloride ND ug/kg 01/12/17 14:48 56-23-54.9 2.5 1
Chlorobenzene ND ug/kg 01/12/17 14:48 108-90-74.9 1.8 1
Chloroethane ND ug/kg 01/12/17 14:48 75-00-39.7 2.3 1
Chloroform ND ug/kg 01/12/17 14:48 67-66-34.9 1.6 1
Chloromethane ND ug/kg 01/12/17 14:48 74-87-39.7 2.3 1
2-Chlorotoluene ND ug/kg 01/12/17 14:48 95-49-84.9 1.6 1
4-Chlorotoluene ND ug/kg 01/12/17 14:48 106-43-44.9 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 14:48 96-12-84.9 3.5 1
Dibromochloromethane ND ug/kg 01/12/17 14:48 124-48-14.9 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-15 Lab ID: 92325933005 Collected: 01/10/17 13:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 14:48 106-93-44.9 1.7 1
Dibromomethane ND ug/kg 01/12/17 14:48 74-95-34.9 2.4 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 14:48 95-50-14.9 1.8 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 14:48 541-73-14.9 1.9 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 14:48 106-46-74.9 1.6 1
Dichlorodifluoromethane ND ug/kg 01/12/17 14:48 75-71-89.7 3.5 1
1,1-Dichloroethane ND ug/kg 01/12/17 14:48 75-34-34.9 1.5 1
1,2-Dichloroethane ND ug/kg 01/12/17 14:48 107-06-24.9 2.1 1
1,1-Dichloroethene ND ug/kg 01/12/17 14:48 75-35-44.9 1.7 1
cis-1,2-Dichloroethene ND ug/kg 01/12/17 14:48 156-59-24.9 1.4 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 14:48 156-60-54.9 1.8 1
1,2-Dichloropropane ND ug/kg 01/12/17 14:48 78-87-54.9 1.6 1
1,3-Dichloropropane ND ug/kg 01/12/17 14:48 142-28-94.9 1.8 1
2,2-Dichloropropane ND ug/kg 01/12/17 14:48 594-20-74.9 1.6 1
1,1-Dichloropropene ND ug/kg 01/12/17 14:48 563-58-64.9 1.5 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 14:48 10061-01-54.9 1.7 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 14:48 10061-02-64.9 1.5 1
Diisopropyl ether ND ug/kg 01/12/17 14:48 108-20-34.9 1.6 1
Ethylbenzene ND ug/kg 01/12/17 14:48 100-41-44.9 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 14:48 87-68-34.9 1.9 1
2-Hexanone ND ug/kg 01/12/17 14:48 591-78-648.5 3.8 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 14:48 98-82-84.9 1.8 1
p-Isopropyltoluene ND ug/kg 01/12/17 14:48 99-87-64.9 1.6 1
Methylene Chloride 5.7J ug/kg 01/12/17 14:48 75-09-219.4 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 14:48 108-10-148.5 3.6 1
Methyl-tert-butyl ether ND ug/kg 01/12/17 14:48 1634-04-44.9 1.5 1
Naphthalene ND ug/kg 01/12/17 14:48 91-20-34.9 1.2 1
n-Propylbenzene ND ug/kg 01/12/17 14:48 103-65-14.9 1.6 1
Styrene ND ug/kg 01/12/17 14:48 100-42-54.9 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 14:48 630-20-64.9 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 14:48 79-34-54.9 1.8 1
Tetrachloroethene ND ug/kg 01/12/17 14:48 127-18-44.9 1.6 1
Toluene ND ug/kg 01/12/17 14:48 108-88-34.9 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 14:48 87-61-64.9 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 14:48 120-82-14.9 1.6 1
1,1,1-Trichloroethane ND ug/kg 01/12/17 14:48 71-55-64.9 1.7 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 14:48 79-00-54.9 2.0 1
Trichloroethene ND ug/kg 01/12/17 14:48 79-01-64.9 2.0 1
Trichlorofluoromethane ND ug/kg 01/12/17 14:48 75-69-44.9 2.1 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 14:48 96-18-44.9 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 14:48 95-63-64.9 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 14:48 108-67-84.9 1.7 1
Vinyl acetate ND ug/kg 01/12/17 14:48 108-05-448.5 8.5 1
Vinyl chloride ND ug/kg 01/12/17 14:48 75-01-49.7 1.7 1
Xylene (Total)ND ug/kg 01/12/17 14:48 1330-20-79.7 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-15 Lab ID: 92325933005 Collected: 01/10/17 13:15 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
m&p-Xylene ND ug/kg 01/12/17 14:48 179601-23-19.7 3.5 1
o-Xylene ND ug/kg 01/12/17 14:48 95-47-64.9 1.8 1
Surrogates
Toluene-d8 (S)99 %01/12/17 14:48 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %01/12/17 14:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %01/12/17 14:48 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.0 %01/13/17 07:270.10 0.10 1
Sample: S-16 Lab ID: 92325933006 Collected: 01/10/17 13:55 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 14300 mg/kg 01/14/17 09:00 7429-90-501/12/17 23:1588.1 44.1 10
Arsenic 3.3 mg/kg 01/13/17 19:58 7440-38-201/12/17 23:150.88 0.44 1
Barium 24.1 mg/kg 01/13/17 19:58 7440-39-301/12/17 23:150.44 0.22 1
Cadmium ND mg/kg 01/13/17 19:58 7440-43-901/12/17 23:150.088 0.044 1
Chromium 30.8 mg/kg 01/13/17 19:58 7440-47-301/12/17 23:150.44 0.22 1
Copper 21.0 mg/kg 01/13/17 19:58 7440-50-801/12/17 23:150.44 0.22 1
Lead 15.6 mg/kg 01/13/17 19:58 7439-92-101/12/17 23:150.44 0.22 1
Selenium ND mg/kg 01/13/17 19:58 7782-49-201/12/17 23:150.88 0.44 1
Silver 0.47 mg/kg 01/13/17 19:58 7440-22-401/12/17 23:150.44 0.22 1
Zinc 12.2 mg/kg 01/13/17 19:58 7440-66-601/12/17 23:150.88 0.44 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.051 mg/kg 01/13/17 09:30 7439-97-601/12/17 13:110.0041 0.0020 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 20:48 83-32-901/12/17 09:00425 97.8 1
Acenaphthylene ND ug/kg 01/13/17 20:48 208-96-801/12/17 09:00425 100 1
Aniline ND ug/kg 01/13/17 20:48 62-53-301/12/17 09:00425 115 1
Anthracene ND ug/kg 01/13/17 20:48 120-12-701/12/17 09:00425 95.2 1
Benzo(a)anthracene ND ug/kg 01/13/17 20:48 56-55-301/12/17 09:00425 78.5 1
Benzo(a)pyrene ND ug/kg 01/13/17 20:48 50-32-801/12/17 09:00425 81.1 1
Benzo(b)fluoranthene ND ug/kg 01/13/17 20:48 205-99-201/12/17 09:00425 73.3 1
Benzo(g,h,i)perylene ND ug/kg 01/13/17 20:48 191-24-201/12/17 09:00425 108 1
Benzo(k)fluoranthene ND ug/kg 01/13/17 20:48 207-08-901/12/17 09:00425 83.6 1
Benzoic Acid ND ug/kg 01/13/17 20:48 65-85-001/12/17 09:002120 77.2 1
Benzyl alcohol ND ug/kg 01/13/17 20:48 100-51-601/12/17 09:00849 84.9 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 20:48 101-55-301/12/17 09:00425 77.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-16 Lab ID: 92325933006 Collected: 01/10/17 13:55 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Butylbenzylphthalate ND ug/kg 01/13/17 20:48 85-68-701/12/17 09:00425 90.1 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 20:48 59-50-701/12/17 09:00849 87.5 1
4-Chloroaniline ND ug/kg 01/13/17 20:48 106-47-801/12/17 09:002120 118 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 20:48 111-91-101/12/17 09:00425 99.1 1
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 20:48 111-44-401/12/17 09:00425 108 1
2-Chloronaphthalene ND ug/kg 01/13/17 20:48 91-58-701/12/17 09:00425 83.6 1
2-Chlorophenol ND ug/kg 01/13/17 20:48 95-57-801/12/17 09:00425 116 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 20:48 7005-72-301/12/17 09:00425 87.5 1
Chrysene ND ug/kg 01/13/17 20:48 218-01-901/12/17 09:00425 56.6 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 20:48 53-70-301/12/17 09:00425 90.1 1
Dibenzofuran ND ug/kg 01/13/17 20:48 132-64-901/12/17 09:00425 69.5 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 20:48 95-50-101/12/17 09:00425 113 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 20:48 541-73-1 L201/12/17 09:00425 96.5 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 20:48 106-46-701/12/17 09:00425 120 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 20:48 91-94-101/12/17 09:002120 92.6 1
2,4-Dichlorophenol ND ug/kg 01/13/17 20:48 120-83-201/12/17 09:00425 92.6 1
Diethylphthalate ND ug/kg 01/13/17 20:48 84-66-201/12/17 09:00425 65.6 1
2,4-Dimethylphenol ND ug/kg 01/13/17 20:48 105-67-901/12/17 09:00425 167 1
Dimethylphthalate ND ug/kg 01/13/17 20:48 131-11-301/12/17 09:00425 86.2 1
Di-n-butylphthalate ND ug/kg 01/13/17 20:48 84-74-201/12/17 09:00425 69.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 20:48 534-52-101/12/17 09:00849 84.9 1
2,4-Dinitrophenol ND ug/kg 01/13/17 20:48 51-28-501/12/17 09:002120 69.5 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 20:48 121-14-201/12/17 09:00425 79.8 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 20:48 606-20-201/12/17 09:00425 88.8 1
Di-n-octylphthalate ND ug/kg 01/13/17 20:48 117-84-001/12/17 09:00425 88.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 20:48 117-81-701/12/17 09:00425 116 1
Fluoranthene ND ug/kg 01/13/17 20:48 206-44-001/12/17 09:00425 61.8 1
Fluorene ND ug/kg 01/13/17 20:48 86-73-701/12/17 09:00425 87.5 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 20:48 87-68-301/12/17 09:00425 73.3 1
Hexachlorobenzene ND ug/kg 01/13/17 20:48 118-74-101/12/17 09:00425 54.0 1
Hexachlorocyclopentadiene ND ug/kg 01/13/17 20:48 77-47-401/12/17 09:00425 78.5 1
Hexachloroethane ND ug/kg 01/13/17 20:48 67-72-101/12/17 09:00425 112 1
Indeno(1,2,3-cd)pyrene ND ug/kg 01/13/17 20:48 193-39-501/12/17 09:00425 87.5 1
Isophorone ND ug/kg 01/13/17 20:48 78-59-101/12/17 09:00425 95.2 1
1-Methylnaphthalene ND ug/kg 01/13/17 20:48 90-12-001/12/17 09:00425 111 1
2-Methylnaphthalene ND ug/kg 01/13/17 20:48 91-57-601/12/17 09:00425 91.4 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 20:48 95-48-701/12/17 09:00425 129 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 20:4801/12/17 09:00425 167 1
Naphthalene ND ug/kg 01/13/17 20:48 91-20-301/12/17 09:00425 104 1
2-Nitroaniline ND ug/kg 01/13/17 20:48 88-74-401/12/17 09:002120 131 1
3-Nitroaniline ND ug/kg 01/13/17 20:48 99-09-201/12/17 09:002120 116 1
4-Nitroaniline ND ug/kg 01/13/17 20:48 100-01-601/12/17 09:00849 120 1
Nitrobenzene ND ug/kg 01/13/17 20:48 98-95-301/12/17 09:00425 116 1
2-Nitrophenol ND ug/kg 01/13/17 20:48 88-75-501/12/17 09:00425 103 1
4-Nitrophenol ND ug/kg 01/13/17 20:48 100-02-701/12/17 09:002120 75.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-16 Lab ID: 92325933006 Collected: 01/10/17 13:55 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
N-Nitrosodimethylamine ND ug/kg 01/13/17 20:48 62-75-901/12/17 09:00425 138 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 20:48 621-64-701/12/17 09:00425 81.1 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 20:48 86-30-601/12/17 09:00425 126 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 20:48 108-60-101/12/17 09:00425 113 1
Pentachlorophenol ND ug/kg 01/13/17 20:48 87-86-501/12/17 09:002120 77.2 1
Phenanthrene ND ug/kg 01/13/17 20:48 85-01-801/12/17 09:00425 70.8 1
Phenol ND ug/kg 01/13/17 20:4801/12/17 09:00425 127 1
Pyrene ND ug/kg 01/13/17 20:48 129-00-001/12/17 09:00425 72.1 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 20:48 120-82-101/12/17 09:00425 82.4 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 20:48 95-95-401/12/17 09:00425 131 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 20:48 88-06-201/12/17 09:00425 93.9 1
Surrogates
Nitrobenzene-d5 (S)40 %01/13/17 20:48 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)45 %01/13/17 20:48 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)58 %01/13/17 20:48 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)32 %01/13/17 20:48 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)31 %01/13/17 20:48 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)34 %01/13/17 20:48 118-79-601/12/17 09:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 11.0J ug/kg 01/12/17 15:08 67-64-193.6 9.4 1
Benzene ND ug/kg 01/12/17 15:08 71-43-24.7 1.5 1
Bromobenzene ND ug/kg 01/12/17 15:08 108-86-14.7 1.9 1
Bromochloromethane ND ug/kg 01/12/17 15:08 74-97-54.7 1.6 1
Bromodichloromethane ND ug/kg 01/12/17 15:08 75-27-44.7 1.8 1
Bromoform ND ug/kg 01/12/17 15:08 75-25-24.7 2.2 1
Bromomethane ND ug/kg 01/12/17 15:08 74-83-99.4 2.3 1
2-Butanone (MEK)ND ug/kg 01/12/17 15:08 78-93-393.6 2.7 1
n-Butylbenzene ND ug/kg 01/12/17 15:08 104-51-84.7 1.7 1
sec-Butylbenzene ND ug/kg 01/12/17 15:08 135-98-84.7 1.5 1
tert-Butylbenzene ND ug/kg 01/12/17 15:08 98-06-64.7 1.9 1
Carbon tetrachloride ND ug/kg 01/12/17 15:08 56-23-54.7 2.4 1
Chlorobenzene ND ug/kg 01/12/17 15:08 108-90-74.7 1.8 1
Chloroethane ND ug/kg 01/12/17 15:08 75-00-39.4 2.2 1
Chloroform ND ug/kg 01/12/17 15:08 67-66-34.7 1.5 1
Chloromethane ND ug/kg 01/12/17 15:08 74-87-39.4 2.2 1
2-Chlorotoluene ND ug/kg 01/12/17 15:08 95-49-84.7 1.6 1
4-Chlorotoluene ND ug/kg 01/12/17 15:08 106-43-44.7 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 15:08 96-12-84.7 3.4 1
Dibromochloromethane ND ug/kg 01/12/17 15:08 124-48-14.7 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 15:08 106-93-44.7 1.7 1
Dibromomethane ND ug/kg 01/12/17 15:08 74-95-34.7 2.3 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 15:08 95-50-14.7 1.8 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 15:08 541-73-14.7 1.9 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 15:08 106-46-74.7 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-16 Lab ID: 92325933006 Collected: 01/10/17 13:55 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Dichlorodifluoromethane ND ug/kg 01/12/17 15:08 75-71-89.4 3.4 1
1,1-Dichloroethane ND ug/kg 01/12/17 15:08 75-34-34.7 1.4 1
1,2-Dichloroethane ND ug/kg 01/12/17 15:08 107-06-24.7 2.1 1
1,1-Dichloroethene ND ug/kg 01/12/17 15:08 75-35-44.7 1.7 1
cis-1,2-Dichloroethene ND ug/kg 01/12/17 15:08 156-59-24.7 1.3 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 15:08 156-60-54.7 1.8 1
1,2-Dichloropropane ND ug/kg 01/12/17 15:08 78-87-54.7 1.6 1
1,3-Dichloropropane ND ug/kg 01/12/17 15:08 142-28-94.7 1.8 1
2,2-Dichloropropane ND ug/kg 01/12/17 15:08 594-20-74.7 1.6 1
1,1-Dichloropropene ND ug/kg 01/12/17 15:08 563-58-64.7 1.4 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 15:08 10061-01-54.7 1.7 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 15:08 10061-02-64.7 1.4 1
Diisopropyl ether ND ug/kg 01/12/17 15:08 108-20-34.7 1.6 1
Ethylbenzene ND ug/kg 01/12/17 15:08 100-41-44.7 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 15:08 87-68-34.7 1.9 1
2-Hexanone ND ug/kg 01/12/17 15:08 591-78-646.8 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 15:08 98-82-84.7 1.8 1
p-Isopropyltoluene ND ug/kg 01/12/17 15:08 99-87-64.7 1.6 1
Methylene Chloride 11.4J ug/kg 01/12/17 15:08 75-09-218.7 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 15:08 108-10-146.8 3.5 1
Methyl-tert-butyl ether ND ug/kg 01/12/17 15:08 1634-04-44.7 1.4 1
Naphthalene ND ug/kg 01/12/17 15:08 91-20-34.7 1.1 1
n-Propylbenzene ND ug/kg 01/12/17 15:08 103-65-14.7 1.6 1
Styrene ND ug/kg 01/12/17 15:08 100-42-54.7 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 15:08 630-20-64.7 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 15:08 79-34-54.7 1.8 1
Tetrachloroethene ND ug/kg 01/12/17 15:08 127-18-44.7 1.6 1
Toluene ND ug/kg 01/12/17 15:08 108-88-34.7 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 15:08 87-61-64.7 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 15:08 120-82-14.7 1.5 1
1,1,1-Trichloroethane ND ug/kg 01/12/17 15:08 71-55-64.7 1.7 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 15:08 79-00-54.7 2.0 1
Trichloroethene ND ug/kg 01/12/17 15:08 79-01-64.7 2.0 1
Trichlorofluoromethane ND ug/kg 01/12/17 15:08 75-69-44.7 2.1 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 15:08 96-18-44.7 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 15:08 95-63-64.7 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 15:08 108-67-84.7 1.7 1
Vinyl acetate ND ug/kg 01/12/17 15:08 108-05-446.8 8.2 1
Vinyl chloride ND ug/kg 01/12/17 15:08 75-01-49.4 1.7 1
Xylene (Total)ND ug/kg 01/12/17 15:08 1330-20-79.4 3.4 1
m&p-Xylene ND ug/kg 01/12/17 15:08 179601-23-19.4 3.4 1
o-Xylene ND ug/kg 01/12/17 15:08 95-47-64.7 1.8 1
Surrogates
Toluene-d8 (S)98 %01/12/17 15:08 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %01/12/17 15:08 460-00-470-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: S-16 Lab ID: 92325933006 Collected: 01/10/17 13:55 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Surrogates
1,2-Dichloroethane-d4 (S)97 %01/12/17 15:08 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.3 %01/13/17 07:280.10 0.10 1
Sample: DUP-01-011017 Lab ID: 92325933007 Collected: 01/10/17 00:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 9670 mg/kg 01/14/17 09:03 7429-90-501/12/17 23:1592.1 46.0 10
Arsenic 2.9 mg/kg 01/13/17 20:01 7440-38-201/12/17 23:150.92 0.46 1
Barium 25.7 mg/kg 01/13/17 20:01 7440-39-301/12/17 23:150.46 0.23 1
Cadmium ND mg/kg 01/13/17 20:01 7440-43-901/12/17 23:150.092 0.046 1
Chromium 45.3 mg/kg 01/13/17 20:01 7440-47-301/12/17 23:150.46 0.23 1
Copper 13.6 mg/kg 01/13/17 20:01 7440-50-801/12/17 23:150.46 0.23 1
Lead 11.0 mg/kg 01/13/17 20:01 7439-92-101/12/17 23:150.46 0.23 1
Selenium ND mg/kg 01/13/17 20:01 7782-49-201/12/17 23:150.92 0.46 1
Silver 0.31J mg/kg 01/13/17 20:01 7440-22-401/12/17 23:150.46 0.23 1
Zinc 14.0 mg/kg 01/13/17 20:01 7440-66-601/12/17 23:150.92 0.46 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.045 mg/kg 01/13/17 09:32 7439-97-601/12/17 13:110.0033 0.0017 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/13/17 21:15 83-32-901/12/17 09:00407 93.8 1
Acenaphthylene ND ug/kg 01/13/17 21:15 208-96-801/12/17 09:00407 96.3 1
Aniline ND ug/kg 01/13/17 21:15 62-53-301/12/17 09:00407 110 1
Anthracene ND ug/kg 01/13/17 21:15 120-12-701/12/17 09:00407 91.3 1
Benzo(a)anthracene ND ug/kg 01/13/17 21:15 56-55-301/12/17 09:00407 75.3 1
Benzo(a)pyrene ND ug/kg 01/13/17 21:15 50-32-801/12/17 09:00407 77.8 1
Benzo(b)fluoranthene ND ug/kg 01/13/17 21:15 205-99-201/12/17 09:00407 70.3 1
Benzo(g,h,i)perylene ND ug/kg 01/13/17 21:15 191-24-201/12/17 09:00407 104 1
Benzo(k)fluoranthene ND ug/kg 01/13/17 21:15 207-08-901/12/17 09:00407 80.2 1
Benzoic Acid ND ug/kg 01/13/17 21:15 65-85-001/12/17 09:002040 74.0 1
Benzyl alcohol ND ug/kg 01/13/17 21:15 100-51-601/12/17 09:00815 81.5 1
4-Bromophenylphenyl ether ND ug/kg 01/13/17 21:15 101-55-301/12/17 09:00407 74.0 1
Butylbenzylphthalate ND ug/kg 01/13/17 21:15 85-68-701/12/17 09:00407 86.4 1
4-Chloro-3-methylphenol ND ug/kg 01/13/17 21:15 59-50-701/12/17 09:00815 83.9 1
4-Chloroaniline ND ug/kg 01/13/17 21:15 106-47-801/12/17 09:002040 114 1
bis(2-Chloroethoxy)methane ND ug/kg 01/13/17 21:15 111-91-101/12/17 09:00407 95.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: DUP-01-011017 Lab ID: 92325933007 Collected: 01/10/17 00:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 01/13/17 21:15 111-44-401/12/17 09:00407 104 1
2-Chloronaphthalene ND ug/kg 01/13/17 21:15 91-58-701/12/17 09:00407 80.2 1
2-Chlorophenol ND ug/kg 01/13/17 21:15 95-57-801/12/17 09:00407 111 1
4-Chlorophenylphenyl ether ND ug/kg 01/13/17 21:15 7005-72-301/12/17 09:00407 83.9 1
Chrysene ND ug/kg 01/13/17 21:15 218-01-901/12/17 09:00407 54.3 1
Dibenz(a,h)anthracene ND ug/kg 01/13/17 21:15 53-70-301/12/17 09:00407 86.4 1
Dibenzofuran ND ug/kg 01/13/17 21:15 132-64-901/12/17 09:00407 66.6 1
1,2-Dichlorobenzene ND ug/kg 01/13/17 21:15 95-50-101/12/17 09:00407 109 1
1,3-Dichlorobenzene ND ug/kg 01/13/17 21:15 541-73-1 L201/12/17 09:00407 92.6 1
1,4-Dichlorobenzene ND ug/kg 01/13/17 21:15 106-46-701/12/17 09:00407 115 1
3,3'-Dichlorobenzidine ND ug/kg 01/13/17 21:15 91-94-101/12/17 09:002040 88.9 1
2,4-Dichlorophenol ND ug/kg 01/13/17 21:15 120-83-201/12/17 09:00407 88.9 1
Diethylphthalate ND ug/kg 01/13/17 21:15 84-66-201/12/17 09:00407 62.9 1
2,4-Dimethylphenol ND ug/kg 01/13/17 21:15 105-67-901/12/17 09:00407 160 1
Dimethylphthalate ND ug/kg 01/13/17 21:15 131-11-301/12/17 09:00407 82.7 1
Di-n-butylphthalate ND ug/kg 01/13/17 21:15 84-74-201/12/17 09:00407 66.6 1
4,6-Dinitro-2-methylphenol ND ug/kg 01/13/17 21:15 534-52-101/12/17 09:00815 81.5 1
2,4-Dinitrophenol ND ug/kg 01/13/17 21:15 51-28-501/12/17 09:002040 66.6 1
2,4-Dinitrotoluene ND ug/kg 01/13/17 21:15 121-14-201/12/17 09:00407 76.5 1
2,6-Dinitrotoluene ND ug/kg 01/13/17 21:15 606-20-201/12/17 09:00407 85.2 1
Di-n-octylphthalate ND ug/kg 01/13/17 21:15 117-84-001/12/17 09:00407 85.2 1
bis(2-Ethylhexyl)phthalate ND ug/kg 01/13/17 21:15 117-81-701/12/17 09:00407 111 1
Fluoranthene ND ug/kg 01/13/17 21:15 206-44-001/12/17 09:00407 59.2 1
Fluorene ND ug/kg 01/13/17 21:15 86-73-701/12/17 09:00407 83.9 1
Hexachloro-1,3-butadiene ND ug/kg 01/13/17 21:15 87-68-301/12/17 09:00407 70.3 1
Hexachlorobenzene ND ug/kg 01/13/17 21:15 118-74-101/12/17 09:00407 51.8 1
Hexachlorocyclopentadiene ND ug/kg 01/13/17 21:15 77-47-401/12/17 09:00407 75.3 1
Hexachloroethane ND ug/kg 01/13/17 21:15 67-72-101/12/17 09:00407 107 1
Indeno(1,2,3-cd)pyrene ND ug/kg 01/13/17 21:15 193-39-501/12/17 09:00407 83.9 1
Isophorone ND ug/kg 01/13/17 21:15 78-59-101/12/17 09:00407 91.3 1
1-Methylnaphthalene ND ug/kg 01/13/17 21:15 90-12-001/12/17 09:00407 106 1
2-Methylnaphthalene ND ug/kg 01/13/17 21:15 91-57-601/12/17 09:00407 87.6 1
2-Methylphenol(o-Cresol)ND ug/kg 01/13/17 21:15 95-48-701/12/17 09:00407 123 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/13/17 21:1501/12/17 09:00407 160 1
Naphthalene ND ug/kg 01/13/17 21:15 91-20-301/12/17 09:00407 100 1
2-Nitroaniline ND ug/kg 01/13/17 21:15 88-74-401/12/17 09:002040 126 1
3-Nitroaniline ND ug/kg 01/13/17 21:15 99-09-201/12/17 09:002040 111 1
4-Nitroaniline ND ug/kg 01/13/17 21:15 100-01-601/12/17 09:00815 115 1
Nitrobenzene ND ug/kg 01/13/17 21:15 98-95-301/12/17 09:00407 111 1
2-Nitrophenol ND ug/kg 01/13/17 21:15 88-75-501/12/17 09:00407 98.7 1
4-Nitrophenol ND ug/kg 01/13/17 21:15 100-02-701/12/17 09:002040 72.8 1
N-Nitrosodimethylamine ND ug/kg 01/13/17 21:15 62-75-901/12/17 09:00407 132 1
N-Nitroso-di-n-propylamine ND ug/kg 01/13/17 21:15 621-64-701/12/17 09:00407 77.8 1
N-Nitrosodiphenylamine ND ug/kg 01/13/17 21:15 86-30-601/12/17 09:00407 121 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/13/17 21:15 108-60-101/12/17 09:00407 109 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: DUP-01-011017 Lab ID: 92325933007 Collected: 01/10/17 00:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 01/13/17 21:15 87-86-501/12/17 09:002040 74.0 1
Phenanthrene ND ug/kg 01/13/17 21:15 85-01-801/12/17 09:00407 67.9 1
Phenol ND ug/kg 01/13/17 21:1501/12/17 09:00407 122 1
Pyrene ND ug/kg 01/13/17 21:15 129-00-001/12/17 09:00407 69.1 1
1,2,4-Trichlorobenzene ND ug/kg 01/13/17 21:15 120-82-101/12/17 09:00407 79.0 1
2,4,5-Trichlorophenol ND ug/kg 01/13/17 21:15 95-95-401/12/17 09:00407 126 1
2,4,6-Trichlorophenol ND ug/kg 01/13/17 21:15 88-06-201/12/17 09:00407 90.1 1
Surrogates
Nitrobenzene-d5 (S)50 %01/13/17 21:15 4165-60-001/12/17 09:0023-110 1
2-Fluorobiphenyl (S)58 %01/13/17 21:15 321-60-801/12/17 09:0030-110 1
Terphenyl-d14 (S)68 %01/13/17 21:15 1718-51-001/12/17 09:0028-110 1
Phenol-d6 (S)40 %01/13/17 21:15 13127-88-301/12/17 09:0022-110 1
2-Fluorophenol (S)37 %01/13/17 21:15 367-12-401/12/17 09:0013-110 1
2,4,6-Tribromophenol (S)28 %01/13/17 21:15 118-79-601/12/17 09:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/12/17 15:28 67-64-1124 12.4 1
Benzene ND ug/kg 01/12/17 15:28 71-43-26.2 2.0 1
Bromobenzene ND ug/kg 01/12/17 15:28 108-86-16.2 2.5 1
Bromochloromethane ND ug/kg 01/12/17 15:28 74-97-56.2 2.1 1
Bromodichloromethane ND ug/kg 01/12/17 15:28 75-27-46.2 2.4 1
Bromoform ND ug/kg 01/12/17 15:28 75-25-26.2 2.9 1
Bromomethane ND ug/kg 01/12/17 15:28 74-83-912.4 3.1 1
2-Butanone (MEK)ND ug/kg 01/12/17 15:28 78-93-3124 3.6 1
n-Butylbenzene ND ug/kg 01/12/17 15:28 104-51-86.2 2.2 1
sec-Butylbenzene ND ug/kg 01/12/17 15:28 135-98-86.2 2.0 1
tert-Butylbenzene ND ug/kg 01/12/17 15:28 98-06-66.2 2.5 1
Carbon tetrachloride ND ug/kg 01/12/17 15:28 56-23-56.2 3.2 1
Chlorobenzene ND ug/kg 01/12/17 15:28 108-90-76.2 2.4 1
Chloroethane ND ug/kg 01/12/17 15:28 75-00-312.4 3.0 1
Chloroform ND ug/kg 01/12/17 15:28 67-66-36.2 2.0 1
Chloromethane ND ug/kg 01/12/17 15:28 74-87-312.4 3.0 1
2-Chlorotoluene ND ug/kg 01/12/17 15:28 95-49-86.2 2.1 1
4-Chlorotoluene ND ug/kg 01/12/17 15:28 106-43-46.2 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/12/17 15:28 96-12-86.2 4.5 1
Dibromochloromethane ND ug/kg 01/12/17 15:28 124-48-16.2 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 01/12/17 15:28 106-93-46.2 2.2 1
Dibromomethane ND ug/kg 01/12/17 15:28 74-95-36.2 3.1 1
1,2-Dichlorobenzene ND ug/kg 01/12/17 15:28 95-50-16.2 2.4 1
1,3-Dichlorobenzene ND ug/kg 01/12/17 15:28 541-73-16.2 2.5 1
1,4-Dichlorobenzene ND ug/kg 01/12/17 15:28 106-46-76.2 2.1 1
Dichlorodifluoromethane ND ug/kg 01/12/17 15:28 75-71-812.4 4.5 1
1,1-Dichloroethane ND ug/kg 01/12/17 15:28 75-34-36.2 1.9 1
1,2-Dichloroethane ND ug/kg 01/12/17 15:28 107-06-26.2 2.7 1
1,1-Dichloroethene ND ug/kg 01/12/17 15:28 75-35-46.2 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: DUP-01-011017 Lab ID: 92325933007 Collected: 01/10/17 00:00 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 01/12/17 15:28 156-59-26.2 1.7 1
trans-1,2-Dichloroethene ND ug/kg 01/12/17 15:28 156-60-56.2 2.4 1
1,2-Dichloropropane ND ug/kg 01/12/17 15:28 78-87-56.2 2.1 1
1,3-Dichloropropane ND ug/kg 01/12/17 15:28 142-28-96.2 2.4 1
2,2-Dichloropropane ND ug/kg 01/12/17 15:28 594-20-76.2 2.1 1
1,1-Dichloropropene ND ug/kg 01/12/17 15:28 563-58-66.2 1.9 1
cis-1,3-Dichloropropene ND ug/kg 01/12/17 15:28 10061-01-56.2 2.2 1
trans-1,3-Dichloropropene ND ug/kg 01/12/17 15:28 10061-02-66.2 1.9 1
Diisopropyl ether ND ug/kg 01/12/17 15:28 108-20-36.2 2.1 1
Ethylbenzene ND ug/kg 01/12/17 15:28 100-41-46.2 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 01/12/17 15:28 87-68-36.2 2.5 1
2-Hexanone ND ug/kg 01/12/17 15:28 591-78-662.1 4.8 1
Isopropylbenzene (Cumene)ND ug/kg 01/12/17 15:28 98-82-86.2 2.4 1
p-Isopropyltoluene ND ug/kg 01/12/17 15:28 99-87-66.2 2.1 1
Methylene Chloride 8.1J ug/kg 01/12/17 15:28 75-09-224.8 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/12/17 15:28 108-10-162.1 4.6 1
Methyl-tert-butyl ether ND ug/kg 01/12/17 15:28 1634-04-46.2 1.9 1
Naphthalene ND ug/kg 01/12/17 15:28 91-20-36.2 1.5 1
n-Propylbenzene ND ug/kg 01/12/17 15:28 103-65-16.2 2.1 1
Styrene ND ug/kg 01/12/17 15:28 100-42-56.2 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/12/17 15:28 630-20-66.2 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/12/17 15:28 79-34-56.2 2.4 1
Tetrachloroethene ND ug/kg 01/12/17 15:28 127-18-46.2 2.1 1
Toluene ND ug/kg 01/12/17 15:28 108-88-36.2 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 01/12/17 15:28 87-61-66.2 2.7 1
1,2,4-Trichlorobenzene ND ug/kg 01/12/17 15:28 120-82-16.2 2.0 1
1,1,1-Trichloroethane ND ug/kg 01/12/17 15:28 71-55-66.2 2.2 1
1,1,2-Trichloroethane ND ug/kg 01/12/17 15:28 79-00-56.2 2.6 1
Trichloroethene ND ug/kg 01/12/17 15:28 79-01-66.2 2.6 1
Trichlorofluoromethane ND ug/kg 01/12/17 15:28 75-69-46.2 2.7 1
1,2,3-Trichloropropane ND ug/kg 01/12/17 15:28 96-18-46.2 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 01/12/17 15:28 95-63-66.2 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 01/12/17 15:28 108-67-86.2 2.2 1
Vinyl acetate ND ug/kg 01/12/17 15:28 108-05-462.1 10.9 1
Vinyl chloride ND ug/kg 01/12/17 15:28 75-01-412.4 2.2 1
Xylene (Total)ND ug/kg 01/12/17 15:28 1330-20-712.4 4.5 1
m&p-Xylene ND ug/kg 01/12/17 15:28 179601-23-112.4 4.5 1
o-Xylene ND ug/kg 01/12/17 15:28 95-47-66.2 2.4 1
Surrogates
Toluene-d8 (S)99 %01/12/17 15:28 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %01/12/17 15:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %01/12/17 15:28 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.0 %01/13/17 07:290.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Sample: BG-01 Lab ID: 92325933008 Collected: 01/10/17 11:50 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 7650 mg/kg 01/13/17 20:04 7429-90-501/12/17 23:1511.0 5.5 1
Arsenic 4.2 mg/kg 01/13/17 20:04 7440-38-201/12/17 23:151.1 0.55 1
Barium 88.0 mg/kg 01/13/17 20:04 7440-39-301/12/17 23:150.55 0.27 1
Cadmium 0.74 mg/kg 01/13/17 20:04 7440-43-901/12/17 23:150.11 0.055 1
Chromium 32.5 mg/kg 01/13/17 20:04 7440-47-301/12/17 23:150.55 0.27 1
Copper 1270 mg/kg 01/14/17 09:06 7440-50-801/12/17 23:155.5 2.7 10
Lead 201 mg/kg 01/13/17 20:04 7439-92-101/12/17 23:150.55 0.27 1
Selenium ND mg/kg 01/13/17 20:04 7782-49-201/12/17 23:151.1 0.55 1
Silver 0.59 mg/kg 01/13/17 20:04 7440-22-401/12/17 23:150.55 0.27 1
Zinc 586 mg/kg 01/13/17 20:04 7440-66-601/12/17 23:151.1 0.55 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.12 mg/kg 01/13/17 10:06 7439-97-601/12/17 13:110.0060 0.0030 2
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.5 %01/18/17 16:040.10 0.10 1
Sample: BG-02 Lab ID: 92325933009 Collected: 01/10/17 10:40 Received: 01/11/17 13:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Aluminum 8900 mg/kg 01/13/17 20:07 7429-90-501/12/17 23:1511.3 5.6 1
Arsenic 4.4 mg/kg 01/13/17 20:07 7440-38-201/12/17 23:151.1 0.56 1
Barium 16.7 mg/kg 01/13/17 20:07 7440-39-301/12/17 23:150.56 0.28 1
Cadmium ND mg/kg 01/13/17 20:07 7440-43-901/12/17 23:150.11 0.056 1
Chromium 32.7 mg/kg 01/13/17 20:07 7440-47-301/12/17 23:150.56 0.28 1
Copper 17.0 mg/kg 01/13/17 20:07 7440-50-801/12/17 23:150.56 0.28 1
Lead 8.5 mg/kg 01/13/17 20:07 7439-92-101/12/17 23:150.56 0.28 1
Selenium ND mg/kg 01/13/17 20:07 7782-49-201/12/17 23:151.1 0.56 1
Silver 0.40J mg/kg 01/13/17 20:07 7440-22-401/12/17 23:150.56 0.28 1
Zinc 9.0 mg/kg 01/13/17 20:07 7440-66-601/12/17 23:151.1 0.56 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.071 mg/kg 01/13/17 09:38 7439-97-601/12/17 13:110.0054 0.0027 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.6 %01/18/17 16:040.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344075
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007,
92325933008, 92325933009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1908749
Associated Lab Samples: 92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007,
92325933008, 92325933009
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 01/13/17 09:010.0030
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908750LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.076.083 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1908751MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325877001
1908752
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg .044 77 75-12586 8 20.0440.010 0.044 0.048
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344177
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007,
92325933008, 92325933009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1909396
Associated Lab Samples: 92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007,
92325933008, 92325933009
Matrix: Solid
AnalyzedMDL
Aluminum mg/kg ND 10.0 01/13/17 19:185.0
Arsenic mg/kg ND 1.0 01/13/17 19:180.50
Barium mg/kg ND 0.50 01/13/17 19:180.25
Cadmium mg/kg ND 0.10 01/13/17 19:180.050
Chromium mg/kg ND 0.50 01/13/17 19:180.25
Copper mg/kg ND 0.50 01/13/17 19:180.25
Lead mg/kg ND 0.50 01/13/17 19:180.25
Selenium mg/kg ND 1.0 01/13/17 19:180.50
Silver mg/kg ND 0.50 01/13/17 19:180.25
Zinc mg/kg ND 1.0 01/14/17 08:350.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909397LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum mg/kg 481500 96 80-120
Arsenic mg/kg 48.150 96 80-120
Barium mg/kg 48.850 98 80-120
Cadmium mg/kg 49.150 98 80-120
Chromium mg/kg 48.750 97 80-120
Copper mg/kg 50.550 101 80-120
Lead mg/kg 49.850 100 80-120
Selenium mg/kg 50.450 101 80-120
Silver mg/kg 24.925 99 80-120
Zinc mg/kg 52.150 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1909398MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325852001
1909399
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum mg/kg 397 97 75-12596 14 20463ND386 444
Arsenic mg/kg 39.7 99 75-12597 14 2046.3ND 39.5 45.4
Barium mg/kg 39.7 99 75-12596 13 2046.3ND 39.1 44.6
Cadmium mg/kg 39.7 99 75-12597 14 2046.3ND 39.3 45.0
Chromium mg/kg 39.7 97 75-12596 14 2046.3ND 38.6 44.5
Copper mg/kg 39.7 103 75-125101 14 2046.3ND 40.7 46.7
Lead mg/kg 39.7 100 75-12597 12 2046.3ND 39.8 45.1
Selenium mg/kg 39.7 108 75-125105 13 2046.3ND 43.3 49.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
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Page 35 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1909398MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325852001
1909399
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Silver mg/kg 19.8 99 75-12598 15 2023.1ND 19.7 22.7
Zinc mg/kg 39.7 101 75-12599 13 2046.3ND 40.0 45.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344113
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1908891
Associated Lab Samples:92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 6.6 01/12/17 11:302.8
1,1,1-Trichloroethane ug/kg ND 6.6 01/12/17 11:302.4
1,1,2,2-Tetrachloroethane ug/kg ND 6.6 01/12/17 11:302.5
1,1,2-Trichloroethane ug/kg ND 6.6 01/12/17 11:302.8
1,1-Dichloroethane ug/kg ND 6.6 01/12/17 11:302.0
1,1-Dichloroethene ug/kg ND 6.6 01/12/17 11:302.4
1,1-Dichloropropene ug/kg ND 6.6 01/12/17 11:302.0
1,2,3-Trichlorobenzene ug/kg ND 6.6 01/12/17 11:302.9
1,2,3-Trichloropropane ug/kg ND 6.6 01/12/17 11:302.1
1,2,4-Trichlorobenzene ug/kg ND 6.6 01/12/17 11:302.1
1,2,4-Trimethylbenzene ug/kg ND 6.6 01/12/17 11:302.7
1,2-Dibromo-3-chloropropane ug/kg ND 6.6 01/12/17 11:304.8
1,2-Dibromoethane (EDB)ug/kg ND 6.6 01/12/17 11:302.4
1,2-Dichlorobenzene ug/kg ND 6.6 01/12/17 11:302.5
1,2-Dichloroethane ug/kg ND 6.6 01/12/17 11:302.9
1,2-Dichloropropane ug/kg ND 6.6 01/12/17 11:302.3
1,3,5-Trimethylbenzene ug/kg ND 6.6 01/12/17 11:302.4
1,3-Dichlorobenzene ug/kg ND 6.6 01/12/17 11:302.7
1,3-Dichloropropane ug/kg ND 6.6 01/12/17 11:302.5
1,4-Dichlorobenzene ug/kg ND 6.6 01/12/17 11:302.3
2,2-Dichloropropane ug/kg ND 6.6 01/12/17 11:302.3
2-Butanone (MEK)ug/kg ND 133 01/12/17 11:303.9
2-Chlorotoluene ug/kg ND 6.6 01/12/17 11:302.3
2-Hexanone ug/kg ND 66.5 01/12/17 11:305.2
4-Chlorotoluene ug/kg ND 6.6 01/12/17 11:302.4
4-Methyl-2-pentanone (MIBK)ug/kg ND 66.5 01/12/17 11:304.9
Acetone ug/kg ND 133 01/12/17 11:3013.3
Benzene ug/kg ND 6.6 01/12/17 11:302.1
Bromobenzene ug/kg ND 6.6 01/12/17 11:302.7
Bromochloromethane ug/kg ND 6.6 01/12/17 11:302.3
Bromodichloromethane ug/kg ND 6.6 01/12/17 11:302.5
Bromoform ug/kg ND 6.6 01/12/17 11:303.1
Bromomethane ug/kg ND 13.3 01/12/17 11:303.3
Carbon tetrachloride ug/kg ND 6.6 01/12/17 11:303.5
Chlorobenzene ug/kg ND 6.6 01/12/17 11:302.5
Chloroethane ug/kg ND 13.3 01/12/17 11:303.2
Chloroform ug/kg ND 6.6 01/12/17 11:302.1
Chloromethane ug/kg ND 13.3 01/12/17 11:303.2
cis-1,2-Dichloroethene ug/kg ND 6.6 01/12/17 11:301.9
cis-1,3-Dichloropropene ug/kg ND 6.6 01/12/17 11:302.4
Dibromochloromethane ug/kg ND 6.6 01/12/17 11:302.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 37 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1908891
Associated Lab Samples:92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 6.6 01/12/17 11:303.3
Dichlorodifluoromethane ug/kg ND 13.3 01/12/17 11:304.8
Diisopropyl ether ug/kg ND 6.6 01/12/17 11:302.3
Ethylbenzene ug/kg ND 6.6 01/12/17 11:302.4
Hexachloro-1,3-butadiene ug/kg ND 6.6 01/12/17 11:302.7
Isopropylbenzene (Cumene)ug/kg ND 6.6 01/12/17 11:302.5
m&p-Xylene ug/kg ND 13.3 01/12/17 11:304.8
Methyl-tert-butyl ether ug/kg ND 6.6 01/12/17 11:302.0
Methylene Chloride ug/kg ND 26.6 01/12/17 11:304.0
n-Butylbenzene ug/kg ND 6.6 01/12/17 11:302.4
n-Propylbenzene ug/kg ND 6.6 01/12/17 11:302.3
Naphthalene ug/kg 3.6J 6.6 01/12/17 11:301.6
o-Xylene ug/kg ND 6.6 01/12/17 11:302.5
p-Isopropyltoluene ug/kg ND 6.6 01/12/17 11:302.3
sec-Butylbenzene ug/kg ND 6.6 01/12/17 11:302.1
Styrene ug/kg ND 6.6 01/12/17 11:302.4
tert-Butylbenzene ug/kg ND 6.6 01/12/17 11:302.7
Tetrachloroethene ug/kg ND 6.6 01/12/17 11:302.3
Toluene ug/kg ND 6.6 01/12/17 11:302.4
trans-1,2-Dichloroethene ug/kg ND 6.6 01/12/17 11:302.5
trans-1,3-Dichloropropene ug/kg ND 6.6 01/12/17 11:302.0
Trichloroethene ug/kg ND 6.6 01/12/17 11:302.8
Trichlorofluoromethane ug/kg ND 6.6 01/12/17 11:302.9
Vinyl acetate ug/kg ND 66.5 01/12/17 11:3011.7
Vinyl chloride ug/kg ND 13.3 01/12/17 11:302.4
Xylene (Total)ug/kg ND 13.3 01/12/17 11:304.8
1,2-Dichloroethane-d4 (S)%100 70-132 01/12/17 11:30
4-Bromofluorobenzene (S)%100 70-130 01/12/17 11:30
Toluene-d8 (S)%98 70-130 01/12/17 11:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908892LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 71.767.9 106 74-137
1,1,1-Trichloroethane ug/kg 68.567.9 101 67-140
1,1,2,2-Tetrachloroethane ug/kg 70.367.9 103 72-141
1,1,2-Trichloroethane ug/kg 73.367.9 108 78-138
1,1-Dichloroethane ug/kg 68.267.9 100 69-134
1,1-Dichloroethene ug/kg 70.967.9 104 67-138
1,1-Dichloropropene ug/kg 70.167.9 103 69-139
1,2,3-Trichlorobenzene ug/kg 78.567.9 116 70-146
1,2,3-Trichloropropane ug/kg 69.367.9 102 69-144
1,2,4-Trichlorobenzene ug/kg 79.267.9 117 68-148
1,2,4-Trimethylbenzene ug/kg 73.867.9 109 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908892LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 69.267.9 102 65-140
1,2-Dibromoethane (EDB)ug/kg 71.567.9 105 77-135
1,2-Dichlorobenzene ug/kg 71.567.9 105 77-141
1,2-Dichloroethane ug/kg 67.467.9 99 65-137
1,2-Dichloropropane ug/kg 73.467.9 108 72-136
1,3,5-Trimethylbenzene ug/kg 71.467.9 105 76-133
1,3-Dichlorobenzene ug/kg 73.367.9 108 74-138
1,3-Dichloropropane ug/kg 74.467.9 110 71-139
1,4-Dichlorobenzene ug/kg 71.367.9 105 76-138
2,2-Dichloropropane ug/kg 67.067.9 99 68-137
2-Butanone (MEK)ug/kg 126J136 93 58-147
2-Chlorotoluene ug/kg 78.667.9 116 73-139
2-Hexanone ug/kg 137136 101 62-145
4-Chlorotoluene ug/kg 72.167.9 106 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 145136 107 64-149
Acetone ug/kg 132J136 97 53-153
Benzene ug/kg 75.867.9 112 73-135
Bromobenzene ug/kg 71.067.9 105 75-133
Bromochloromethane ug/kg 65.467.9 96 73-134
Bromodichloromethane ug/kg 74.867.9 110 71-135
Bromoform ug/kg 60.667.9 89 66-141
Bromomethane ug/kg 68.067.9 100 53-160
Carbon tetrachloride ug/kg 73.967.9 109 60-145
Chlorobenzene ug/kg 74.467.9 110 78-130
Chloroethane ug/kg 80.467.9 118 64-149
Chloroform ug/kg 71.967.9 106 70-134
Chloromethane ug/kg 64.767.9 95 52-150
cis-1,2-Dichloroethene ug/kg 68.367.9 100 70-133
cis-1,3-Dichloropropene ug/kg 74.567.9 110 68-134
Dibromochloromethane ug/kg 72.867.9 107 71-138
Dibromomethane ug/kg 74.367.9 109 74-130
Dichlorodifluoromethane ug/kg 67.667.9 100 40-160
Diisopropyl ether ug/kg 68.167.9 100 69-141
Ethylbenzene ug/kg 74.467.9 110 75-133
Hexachloro-1,3-butadiene ug/kg 74.567.9 110 68-143
Isopropylbenzene (Cumene)ug/kg 73.567.9 108 76-143
m&p-Xylene ug/kg 147136 108 75-136
Methyl-tert-butyl ether ug/kg 66.767.9 98 68-144
Methylene Chloride ug/kg 70.067.9 103 45-154
n-Butylbenzene ug/kg 74.667.9 110 72-137
n-Propylbenzene ug/kg 73.767.9 109 76-136
Naphthalene ug/kg 89.367.9 131 68-151
o-Xylene ug/kg 72.367.9 106 76-141
p-Isopropyltoluene ug/kg 70.367.9 104 76-140
sec-Butylbenzene ug/kg 72.567.9 107 79-139
Styrene ug/kg 74.567.9 110 79-137
tert-Butylbenzene ug/kg 66.367.9 98 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908892LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 66.967.9 98 71-138
Toluene ug/kg 73.767.9 109 74-131
trans-1,2-Dichloroethene ug/kg 70.067.9 103 67-135
trans-1,3-Dichloropropene ug/kg 73.767.9 108 65-146
Trichloroethene ug/kg 73.267.9 108 67-135
Trichlorofluoromethane ug/kg 74.167.9 109 59-144
Vinyl acetate ug/kg 144136 106 40-160
Vinyl chloride ug/kg 62.367.9 92 56-141
Xylene (Total)ug/kg 219204 108 76-137
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909216MATRIX SPIKE SAMPLE:
MSSpike
Result
92325933002
1,1,1,2-Tetrachloroethane ug/kg 42.240.6 104 70-130ND
1,1,1-Trichloroethane ug/kg 41.240.6 102 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 41.040.6 101 70-130ND
1,1,2-Trichloroethane ug/kg 44.840.6 111 70-130ND
1,1-Dichloroethane ug/kg 41.340.6 102 70-130ND
1,1-Dichloroethene ug/kg 42.440.6 105 49-180ND
1,1-Dichloropropene ug/kg 41.640.6 103 70-130ND
1,2,3-Trichlorobenzene ug/kg 35.940.6 89 70-130ND
1,2,3-Trichloropropane ug/kg 39.540.6 97 70-130ND
1,2,4-Trichlorobenzene ug/kg 34.540.6 85 70-130ND
1,2,4-Trimethylbenzene ug/kg 41.240.6 101 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 37.040.6 91 70-130ND
1,2-Dibromoethane (EDB)ug/kg 40.640.6 100 70-130ND
1,2-Dichlorobenzene ug/kg 37.440.6 92 70-130ND
1,2-Dichloroethane ug/kg 42.140.6 104 70-130ND
1,2-Dichloropropane ug/kg 45.840.6 113 70-130ND
1,3,5-Trimethylbenzene ug/kg 41.440.6 102 70-130ND
1,3-Dichlorobenzene ug/kg 37.540.6 93 70-130ND
1,3-Dichloropropane ug/kg 44.340.6 109 70-130ND
1,4-Dichlorobenzene ug/kg 35.340.6 87 70-130ND
2,2-Dichloropropane ug/kg 40.540.6 100 70-130ND
2-Butanone (MEK)ug/kg 76.7J81 95 70-130ND
2-Chlorotoluene ug/kg 39.540.6 97 70-130ND
2-Hexanone ug/kg 83.381 103 70-130ND
4-Chlorotoluene ug/kg 39.740.6 98 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 87.581 108 70-130ND
Acetone ug/kg 82.681 96 70-130ND
Benzene ug/kg 45.540.6 112 50-166ND
Bromobenzene ug/kg 39.040.6 96 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 40 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909216MATRIX SPIKE SAMPLE:
MSSpike
Result
92325933002
Bromochloromethane ug/kg 41.740.6 103 70-130ND
Bromodichloromethane ug/kg 44.940.6 111 70-130ND
Bromoform ug/kg 33.440.6 82 70-130ND
Bromomethane ug/kg 39.340.6 97 70-130ND
Carbon tetrachloride ug/kg 43.640.6 108 70-130ND
Chlorobenzene ug/kg 41.340.6 102 43-169ND
Chloroethane ug/kg 47.140.6 116 70-130ND
Chloroform ug/kg 43.740.6 108 70-130ND
Chloromethane ug/kg 39.040.6 96 70-130ND
cis-1,2-Dichloroethene ug/kg 40.740.6 100 70-130ND
cis-1,3-Dichloropropene ug/kg 42.740.6 105 70-130ND
Dibromochloromethane ug/kg 41.340.6 102 70-130ND
Dibromomethane ug/kg 42.240.6 104 70-130ND
Dichlorodifluoromethane ug/kg 41.040.6 101 70-130ND
Diisopropyl ether ug/kg 42.540.6 105 70-130ND
Ethylbenzene ug/kg 42.740.6 105 70-130ND
Hexachloro-1,3-butadiene ug/kg 39.140.6 97 70-130ND
Isopropylbenzene (Cumene)ug/kg 42.040.6 104 70-130ND
m&p-Xylene ug/kg 84.281 104 70-130ND
Methyl-tert-butyl ether ug/kg 41.140.6 101 70-130ND
Methylene Chloride ug/kg 43.640.6 97 70-1304.3J
n-Butylbenzene ug/kg 40.840.6 101 70-130ND
n-Propylbenzene ug/kg 41.840.6 103 70-130ND
Naphthalene ug/kg 42.840.6 104 70-130ND
o-Xylene ug/kg 41.940.6 103 70-130ND
p-Isopropyltoluene ug/kg 39.940.6 99 70-130ND
sec-Butylbenzene ug/kg 42.140.6 104 70-130ND
Styrene ug/kg 40.440.6 100 70-130ND
tert-Butylbenzene ug/kg 39.840.6 98 70-130ND
Tetrachloroethene ug/kg 38.440.6 95 70-130ND
Toluene ug/kg 44.040.6 109 52-163ND
trans-1,2-Dichloroethene ug/kg 41.440.6 102 70-130ND
trans-1,3-Dichloropropene ug/kg 40.440.6 100 70-130ND
Trichloroethene ug/kg 42.740.6 105 49-167ND
Trichlorofluoromethane ug/kg 45.740.6 113 70-130ND
Vinyl acetate ug/kg 48.0 M18159 70-130ND
Vinyl chloride ug/kg 37.040.6 91 70-130ND
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325944001
1909215SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325944001
1909215SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 42 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325944001
1909215SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 25.9 C930ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%99 298
4-Bromofluorobenzene (S)%98 499
Toluene-d8 (S)%98 499
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344099
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1908842
Associated Lab Samples:92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 330 01/13/17 13:1364.0
1,2-Dichlorobenzene ug/kg ND 330 01/13/17 13:1388.0
1,3-Dichlorobenzene ug/kg ND 330 01/13/17 13:1375.0
1,4-Dichlorobenzene ug/kg ND 330 01/13/17 13:1393.0
1-Methylnaphthalene ug/kg ND 330 01/13/17 13:1386.0
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 01/13/17 13:1388.0
2,4,5-Trichlorophenol ug/kg ND 330 01/13/17 13:13102
2,4,6-Trichlorophenol ug/kg ND 330 01/13/17 13:1373.0
2,4-Dichlorophenol ug/kg ND 330 01/13/17 13:1372.0
2,4-Dimethylphenol ug/kg ND 330 01/13/17 13:13130
2,4-Dinitrophenol ug/kg ND 1650 01/13/17 13:1354.0
2,4-Dinitrotoluene ug/kg ND 330 01/13/17 13:1362.0
2,6-Dinitrotoluene ug/kg ND 330 01/13/17 13:1369.0
2-Chloronaphthalene ug/kg ND 330 01/13/17 13:1365.0
2-Chlorophenol ug/kg ND 330 01/13/17 13:1390.0
2-Methylnaphthalene ug/kg ND 330 01/13/17 13:1371.0
2-Methylphenol(o-Cresol)ug/kg ND 330 01/13/17 13:13100
2-Nitroaniline ug/kg ND 1650 01/13/17 13:13102
2-Nitrophenol ug/kg ND 330 01/13/17 13:1380.0
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 01/13/17 13:13130
3,3'-Dichlorobenzidine ug/kg ND 1650 01/13/17 13:1372.0
3-Nitroaniline ug/kg ND 1650 01/13/17 13:1390.0
4,6-Dinitro-2-methylphenol ug/kg ND 660 01/13/17 13:1366.0
4-Bromophenylphenyl ether ug/kg ND 330 01/13/17 13:1360.0
4-Chloro-3-methylphenol ug/kg ND 660 01/13/17 13:1368.0
4-Chloroaniline ug/kg ND 1650 01/13/17 13:1392.0
4-Chlorophenylphenyl ether ug/kg ND 330 01/13/17 13:1368.0
4-Nitroaniline ug/kg ND 660 01/13/17 13:1393.0
4-Nitrophenol ug/kg ND 1650 01/13/17 13:1359.0
Acenaphthene ug/kg ND 330 01/13/17 13:1376.0
Acenaphthylene ug/kg ND 330 01/13/17 13:1378.0
Aniline ug/kg ND 330 01/13/17 13:1389.0
Anthracene ug/kg ND 330 01/13/17 13:1374.0
Benzo(a)anthracene ug/kg ND 330 01/13/17 13:1361.0
Benzo(a)pyrene ug/kg ND 330 01/13/17 13:1363.0
Benzo(b)fluoranthene ug/kg ND 330 01/13/17 13:1357.0
Benzo(g,h,i)perylene ug/kg ND 330 01/13/17 13:1384.0
Benzo(k)fluoranthene ug/kg ND 330 01/13/17 13:1365.0
Benzoic Acid ug/kg ND 1650 01/13/17 13:1360.0
Benzyl alcohol ug/kg ND 660 01/13/17 13:1366.0
bis(2-Chloroethoxy)methane ug/kg ND 330 01/13/17 13:1377.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1908842
Associated Lab Samples:92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 330 01/13/17 13:1384.0
bis(2-Ethylhexyl)phthalate ug/kg ND 330 01/13/17 13:1390.0
Butylbenzylphthalate ug/kg ND 330 01/13/17 13:1370.0
Chrysene ug/kg ND 330 01/13/17 13:1344.0
Di-n-butylphthalate ug/kg ND 330 01/13/17 13:1354.0
Di-n-octylphthalate ug/kg ND 330 01/13/17 13:1369.0
Dibenz(a,h)anthracene ug/kg ND 330 01/13/17 13:1370.0
Dibenzofuran ug/kg ND 330 01/13/17 13:1354.0
Diethylphthalate ug/kg ND 330 01/13/17 13:1351.0
Dimethylphthalate ug/kg ND 330 01/13/17 13:1367.0
Fluoranthene ug/kg ND 330 01/13/17 13:1348.0
Fluorene ug/kg ND 330 01/13/17 13:1368.0
Hexachloro-1,3-butadiene ug/kg ND 330 01/13/17 13:1357.0
Hexachlorobenzene ug/kg ND 330 01/13/17 13:1342.0
Hexachlorocyclopentadiene ug/kg ND 330 01/13/17 13:1361.0
Hexachloroethane ug/kg ND 330 01/13/17 13:1387.0
Indeno(1,2,3-cd)pyrene ug/kg ND 330 01/13/17 13:1368.0
Isophorone ug/kg ND 330 01/13/17 13:1374.0
N-Nitroso-di-n-propylamine ug/kg ND 330 01/13/17 13:1363.0
N-Nitrosodimethylamine ug/kg ND 330 01/13/17 13:13107
N-Nitrosodiphenylamine ug/kg ND 330 01/13/17 13:1398.0
Naphthalene ug/kg ND 330 01/13/17 13:1381.0
Nitrobenzene ug/kg ND 330 01/13/17 13:1390.0
Pentachlorophenol ug/kg ND 1650 01/13/17 13:1360.0
Phenanthrene ug/kg ND 330 01/13/17 13:1355.0
Phenol ug/kg ND 330 01/13/17 13:1399.0
Pyrene ug/kg ND 330 01/13/17 13:1356.0
2,4,6-Tribromophenol (S)%72 27-110 01/13/17 13:13
2-Fluorobiphenyl (S)%69 30-110 01/13/17 13:13
2-Fluorophenol (S)%79 13-110 01/13/17 13:13
Nitrobenzene-d5 (S)%68 23-110 01/13/17 13:13
Phenol-d6 (S)%77 22-110 01/13/17 13:13
Terphenyl-d14 (S)%81 28-110 01/13/17 13:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908843LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 8791670 53 36-120
1,2-Dichlorobenzene ug/kg 9341670 56 41-120
1,3-Dichlorobenzene ug/kg 938 L0167056 66-120
1,4-Dichlorobenzene ug/kg 9031670 54 42-120
1-Methylnaphthalene ug/kg 8381670 50 40-120
2,2'-Oxybis(1-chloropropane)ug/kg 9171670 55 17-120
2,4,5-Trichlorophenol ug/kg 8951670 54 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908843LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 11101670 67 40-120
2,4-Dichlorophenol ug/kg 9201670 55 33-120
2,4-Dimethylphenol ug/kg 9821670 59 36-120
2,4-Dinitrophenol ug/kg 48908330 59 22-121
2,4-Dinitrotoluene ug/kg 12701670 76 60-120
2,6-Dinitrotoluene ug/kg 12101670 73 54-120
2-Chloronaphthalene ug/kg 8651670 52 41-120
2-Chlorophenol ug/kg 10101670 61 39-120
2-Methylnaphthalene ug/kg 8811670 53 26-120
2-Methylphenol(o-Cresol)ug/kg 7921670 48 41-120
2-Nitroaniline ug/kg 24703330 74 45-120
2-Nitrophenol ug/kg 9081670 54 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 8281670 50 35-120
3,3'-Dichlorobenzidine ug/kg 24203330 73 16-125
3-Nitroaniline ug/kg 26103330 78 45-120
4,6-Dinitro-2-methylphenol ug/kg 29903330 90 46-120
4-Bromophenylphenyl ether ug/kg 11401670 68 36-120
4-Chloro-3-methylphenol ug/kg 23003330 69 37-120
4-Chloroaniline ug/kg 17803330 53 35-120
4-Chlorophenylphenyl ether ug/kg 10401670 62 30-120
4-Nitroaniline ug/kg 28203330 85 48-120
4-Nitrophenol ug/kg 76508330 92 43-120
Acenaphthene ug/kg 9661670 58 46-120
Acenaphthylene ug/kg 9781670 59 46-120
Aniline ug/kg 7591670 46 33-120
Anthracene ug/kg 12101670 72 63-120
Benzo(a)anthracene ug/kg 12901670 77 61-120
Benzo(a)pyrene ug/kg 12001670 72 59-120
Benzo(b)fluoranthene ug/kg 12501670 75 55-120
Benzo(g,h,i)perylene ug/kg 11901670 71 57-120
Benzo(k)fluoranthene ug/kg 11901670 71 56-120
Benzoic Acid ug/kg 43608330 52 13-120
Benzyl alcohol ug/kg 18903330 57 34-120
bis(2-Chloroethoxy)methane ug/kg 8321670 50 21-120
bis(2-Chloroethyl) ether ug/kg 9181670 55 25-120
bis(2-Ethylhexyl)phthalate ug/kg 15401670 92 56-123
Butylbenzylphthalate ug/kg 14901670 90 57-120
Chrysene ug/kg 12501670 75 64-120
Di-n-butylphthalate ug/kg 14401670 87 58-120
Di-n-octylphthalate ug/kg 16001670 96 47-121
Dibenz(a,h)anthracene ug/kg 12601670 76 56-120
Dibenzofuran ug/kg 10001670 60 43-120
Diethylphthalate ug/kg 14001670 84 55-120
Dimethylphthalate ug/kg 13201670 79 54-120
Fluoranthene ug/kg 12901670 78 61-120
Fluorene ug/kg 11201670 67 51-120
Hexachloro-1,3-butadiene ug/kg 8641670 52 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1908843LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 11801670 71 53-120
Hexachlorocyclopentadiene ug/kg 9061670 54 18-150
Hexachloroethane ug/kg 9331670 56 39-120
Indeno(1,2,3-cd)pyrene ug/kg 12401670 74 58-120
Isophorone ug/kg 9481670 57 38-120
N-Nitroso-di-n-propylamine ug/kg 9381670 56 30-120
N-Nitrosodimethylamine ug/kg 9311670 56 32-120
N-Nitrosodiphenylamine ug/kg 11601670 70 50-120
Naphthalene ug/kg 8691670 52 38-120
Nitrobenzene ug/kg 9001670 54 37-120
Pentachlorophenol ug/kg 33703330 101 10-120
Phenanthrene ug/kg 12401670 74 62-120
Phenol ug/kg 8701670 52 37-120
Pyrene ug/kg 12401670 74 63-120
2,4,6-Tribromophenol (S)%76 27-110
2-Fluorobiphenyl (S)%50 30-110
2-Fluorophenol (S)%60 13-110
Nitrobenzene-d5 (S)%53 23-110
Phenol-d6 (S)%56 22-110
Terphenyl-d14 (S)%79 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1908844MATRIX SPIKE SAMPLE:
MSSpike
Result
92325933001
1,2,4-Trichlorobenzene ug/kg 6362000 32 18-119ND
1,2-Dichlorobenzene ug/kg 686 M1200034 50-110ND
1,3-Dichlorobenzene ug/kg 6512000 33 27-110ND
1,4-Dichlorobenzene ug/kg 6562000 33 28-110ND
1-Methylnaphthalene ug/kg 6732000 34 24-116ND
2,2'-Oxybis(1-chloropropane)ug/kg 709 M1200036 50-150ND
2,4,5-Trichlorophenol ug/kg 8312000 42 28-110ND
2,4,6-Trichlorophenol ug/kg 9652000 48 17-117ND
2,4-Dichlorophenol ug/kg 7402000 37 21-128ND
2,4-Dimethylphenol ug/kg 7122000 36 10-120ND
2,4-Dinitrophenol ug/kg ND M199800 10-107ND
2,4-Dinitrotoluene ug/kg 10402000 52 36-109ND
2,6-Dinitrotoluene ug/kg 10002000 50 32-110ND
2-Chloronaphthalene ug/kg 6962000 35 30-107ND
2-Chlorophenol ug/kg 7422000 37 14-106ND
2-Methylnaphthalene ug/kg 6882000 34 10-135ND
2-Methylphenol(o-Cresol)ug/kg 6502000 33 10-124ND
2-Nitroaniline ug/kg 20903990 52 26-116ND
2-Nitrophenol ug/kg 5962000 30 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 6062000 30 10-109ND
3,3'-Dichlorobenzidine ug/kg 1970J3990 49 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1908844MATRIX SPIKE SAMPLE:
MSSpike
Result
92325933001
3-Nitroaniline ug/kg 21503990 54 22-110ND
4,6-Dinitro-2-methylphenol ug/kg 9993990 25 13-121ND
4-Bromophenylphenyl ether ug/kg 9662000 48 31-109ND
4-Chloro-3-methylphenol ug/kg 22603990 57 13-128ND
4-Chloroaniline ug/kg 1140J3990 29 18-102ND
4-Chlorophenylphenyl ether ug/kg 9592000 48 29-112ND
4-Nitroaniline ug/kg 22303990 56 16-111ND
4-Nitrophenol ug/kg 49009980 49 14-135ND
Acenaphthene ug/kg 8422000 42 26-114ND
Acenaphthylene ug/kg 8292000 42 32-108ND
Aniline ug/kg 377J2000 19 10-107ND
Anthracene ug/kg 10402000 52 32-111ND
Benzo(a)anthracene ug/kg 11002000 55 25-117ND
Benzo(a)pyrene ug/kg 10602000 53 25-106ND
Benzo(b)fluoranthene ug/kg 11102000 56 24-110ND
Benzo(g,h,i)perylene ug/kg 9602000 48 19-112ND
Benzo(k)fluoranthene ug/kg 9992000 50 24-114ND
Benzoic Acid ug/kg 1040J9980 10 10-110ND
Benzyl alcohol ug/kg 13803990 34 24-106ND
bis(2-Chloroethoxy)methane ug/kg 5932000 30 13-119ND
bis(2-Chloroethyl) ether ug/kg 7172000 36 10-134ND
bis(2-Ethylhexyl)phthalate ug/kg 11302000 57 10-125ND
Butylbenzylphthalate ug/kg 10602000 53 18-110ND
Chrysene ug/kg 11102000 56 30-110ND
Di-n-butylphthalate ug/kg 11802000 59 19-112ND
Di-n-octylphthalate ug/kg 12602000 63 17-105ND
Dibenz(a,h)anthracene ug/kg 10202000 51 23-111ND
Dibenzofuran ug/kg 8912000 45 35-103ND
Diethylphthalate ug/kg 12002000 60 27-113ND
Dimethylphthalate ug/kg 11502000 57 26-111ND
Fluoranthene ug/kg 11702000 58 33-109ND
Fluorene ug/kg 10102000 50 32-113ND
Hexachloro-1,3-butadiene ug/kg 5892000 29 16-116ND
Hexachlorobenzene ug/kg 10402000 52 27-120ND
Hexachlorocyclopentadiene ug/kg 296J2000 15 10-108ND
Hexachloroethane ug/kg 6272000 31 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 9802000 49 10-122ND
Isophorone ug/kg 6872000 34 28-114ND
N-Nitroso-di-n-propylamine ug/kg 7222000 36 27-113ND
N-Nitrosodimethylamine ug/kg 6302000 32 10-109ND
N-Nitrosodiphenylamine ug/kg 10202000 51 10-128ND
Naphthalene ug/kg 6582000 33 25-110ND
Nitrobenzene ug/kg 6612000 33 18-114ND
Pentachlorophenol ug/kg 20503990 51 10-122ND
Phenanthrene ug/kg 11102000 56 30-114ND
Phenol ug/kg 6272000 31 11-102ND
Pyrene ug/kg 9652000 48 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1908844MATRIX SPIKE SAMPLE:
MSSpike
Result
92325933001
2,4,6-Tribromophenol (S)%54 27-110
2-Fluorobiphenyl (S)%S029 30-110
2-Fluorophenol (S)%33 13-110
Nitrobenzene-d5 (S)%31 23-110
Phenol-d6 (S)%37 22-110
Terphenyl-d14 (S)%44 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325933005
1908845SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325933005
1908845SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 3073.7J
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%22 S09361
2-Fluorobiphenyl (S)%47 2337
2-Fluorophenol (S)%29 4144
Nitrobenzene-d5 (S)%44 2335
Phenol-d6 (S)%33 2844
Terphenyl-d14 (S)%60 261
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344127
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92325933001, 92325933002, 92325933003, 92325933004, 92325933005, 92325933006, 92325933007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325877001
1908995SAMPLE DUPLICATE:
Percent Moisture %16.0 2 2516.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92326012004
1908996SAMPLE DUPLICATE:
Percent Moisture %17.4 0 2517.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344662
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92325933008, 92325933009
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325933008
1912181SAMPLE DUPLICATE:
Percent Moisture %12.2 2 2512.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 57
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325933
71167563 CAROLINA FOUNDRY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325933001 344177 344207S-11 EPA 3050 EPA 6010
92325933002 344177 344207S-12 EPA 3050 EPA 6010
92325933003 344177 344207S-13 EPA 3050 EPA 6010
92325933004 344177 344207S-14 EPA 3050 EPA 6010
92325933005 344177 344207S-15 EPA 3050 EPA 6010
92325933006 344177 344207S-16 EPA 3050 EPA 6010
92325933007 344177 344207DUP-01-011017 EPA 3050 EPA 6010
92325933008 344177 344207BG-01 EPA 3050 EPA 6010
92325933009 344177 344207BG-02 EPA 3050 EPA 6010
92325933001 344075 344151S-11 EPA 7471 EPA 7471
92325933002 344075 344151S-12 EPA 7471 EPA 7471
92325933003 344075 344151S-13 EPA 7471 EPA 7471
92325933004 344075 344151S-14 EPA 7471 EPA 7471
92325933005 344075 344151S-15 EPA 7471 EPA 7471
92325933006 344075 344151S-16 EPA 7471 EPA 7471
92325933007 344075 344151DUP-01-011017 EPA 7471 EPA 7471
92325933008 344075 344151BG-01 EPA 7471 EPA 7471
92325933009 344075 344151BG-02 EPA 7471 EPA 7471
92325933001 344099 344292S-11 EPA 3546 EPA 8270
92325933002 344099 344292S-12 EPA 3546 EPA 8270
92325933003 344099 344292S-13 EPA 3546 EPA 8270
92325933004 344099 344292S-14 EPA 3546 EPA 8270
92325933005 344099 344292S-15 EPA 3546 EPA 8270
92325933006 344099 344292S-16 EPA 3546 EPA 8270
92325933007 344099 344292DUP-01-011017 EPA 3546 EPA 8270
92325933001 344113S-11 EPA 8260
92325933002 344113S-12 EPA 8260
92325933003 344113S-13 EPA 8260
92325933004 344113S-14 EPA 8260
92325933005 344113S-15 EPA 8260
92325933006 344113S-16 EPA 8260
92325933007 344113DUP-01-011017 EPA 8260
92325933001 344127S-11 ASTM D2974-87
92325933002 344127S-12 ASTM D2974-87
92325933003 344127S-13 ASTM D2974-87
92325933004 344127S-14 ASTM D2974-87
92325933005 344127S-15 ASTM D2974-87
92325933006 344127S-16 ASTM D2974-87
92325933007 344127DUP-01-011017 ASTM D2974-87
92325933008 344662BG-01 ASTM D2974-87
92325933009 344662BG-02 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2017 09:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 57
Page 55 of 57
Page 56 of 57
Page 57 of 57
4/5/2017
Ms. Haley Hindes
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte NC 28206
Project Name: Carolina Foundry
Project #: 71167563
Dear Ms. Haley Hindes
The following report includes the data for the above referenced project for sample(s)
received on 1/13/2017 at Air Toxics Ltd.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contact the Project Manager: Ausha Scott at 916-985-1000 if you have any questions
regarding the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1701155AR1
Page 1 of 51
Ms. Haley Hindes
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
WORK ORDER #:1701155AR1
CLIENT:BILL TO:
PHONE:
Accounts Payable
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
704-509-1777
704-509-1888
01/13/2017
DATE COMPLETED:01/20/2017
P.O. #
PROJECT #71167563 Carolina Foundry
Work Order Summary
FAX:
DATE RECEIVED:
DATE REISSUED:04/03/2017
CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SV-01 TO-15 6.0 "Hg 15 psi
02A SV-02 TO-15 7.0 "Hg 15 psi
03A SV-03 TO-15 5.0 "Hg 15 psi
04A SV-04 TO-15 4.5 "Hg 15 psi
05A SV-05 TO-15 4.5 "Hg 15 psi
06A SV-06 TO-15 6.0 "Hg 15 psi
07A SV-07 TO-15 4.5 "Hg 15 psi
08A DUP-1-10-17 TO-15 3.5 "Hg 15.4 psi
09A Lab Blank TO-15 NA NA
09B Lab Blank TO-15 NA NA
10A CCV TO-15 NA NA
10B CCV TO-15 NA NA
11A LCS TO-15 NA NA
11AA LCSD TO-15 NA NA
11B LCS TO-15 NA NA
11BB LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2016, Expiration date: 10/17/2017.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
04/04/17
Page 2 of 51
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704434-16-11, UT NELAP CA0093332016-7, VA NELAP - 8113, WA NELAP - C935
LABORATORY NARRATIVEEPA Method TO-15Terracon Consulting EngineersWorkorder# 1701155AR1
Eight 1 Liter Summa Canister samples were received on January 13, 2017. The laboratory performed
analysis via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic
driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant
project quality control requirements and verification of all quantified amounts.
There were no receiving discrepancies.
Receiving Notes
The workorder was reissued on 4/3/17 for the following reasons:
1)To report estimated values for target compound hits that are below the reporting limit but greater than
the method detection limit. Concentrations that are below the level at which the canister was certified (0.2
ppbv for compounds reported at 0.5 ppbv and 0.8 ppbv for compounds reported at 2.0 ppbv) may be false
positives.
2)To report the data using a different format.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:24 PM
2.52
msdp.i / p011617R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-01A
1/10/17 06:12 PM
1 Liter Summa Canister
Carolina Foundry
SV-01
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.91.2 Not Detected2.8
1,1,2,2-Tetrachloroethane 79-34-5 8.61.2 Not Detected3.5
1,1,2-Trichloroethane 79-00-5 6.91.4 Not Detected2.8
1,1-Dichloroethane 75-34-3 5.10.37 Not Detected2.0
1,1-Dichloroethene 75-35-4 5.01.1 Not Detected2.0
1,2,4-Trichlorobenzene 120-82-1 373.6 Not Detected18
1,2,4-Trimethylbenzene 95-63-6 6.21.9 2.4 J2.5
1,2-Dibromoethane (EDB)106-93-4 9.70.88 Not Detected3.9
1,2-Dichlorobenzene 95-50-1 7.61.0 Not Detected3.0
1,2-Dichloroethane 107-06-2 5.11.0 3.4 J2.0
1,2-Dichloropropane 78-87-5 5.81.0 7.22.3
1,3,5-Trimethylbenzene 108-67-8 6.21.3 Not Detected2.5
1,3-Butadiene 106-99-0 2.80.58 Not Detected1.1
1,3-Dichlorobenzene 541-73-1 7.60.48 Not Detected3.0
1,4-Dichlorobenzene 106-46-7 7.60.87 Not Detected3.0
1,4-Dioxane 123-91-1 182.7 Not Detected8.5
2,2,4-Trimethylpentane 540-84-1 5.90.53 0.70 J2.4
2-Butanone (Methyl Ethyl Ketone)78-93-3 152.1 Not Detected7.0
2-Hexanone 591-78-6 210.91 Not Detected9.7
2-Propanol 67-63-0 120.90 Not Detected5.8
3-Chloropropene 107-05-1 162.6 Not Detected7.4
4-Ethyltoluene 622-96-8 6.21.4 Not Detected2.5
4-Methyl-2-pentanone 108-10-1 5.21.4 Not Detected2.1
Acetone 67-64-1 302.6 18 J5.6
Page 4 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:24 PM
2.52
msdp.i / p011617R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-01A
1/10/17 06:12 PM
1 Liter Summa Canister
Carolina Foundry
SV-01
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.51.3 Not Detected2.6
Benzene 71-43-2 4.00.37 Not Detected1.6
Bromodichloromethane 75-27-4 8.41.4 Not Detected3.4
Bromoform 75-25-2 131.6 Not Detected5.2
Bromomethane 74-83-9 494.1 Not Detected9.2
Carbon Disulfide 75-15-0 160.92 1.3 J7.4
Carbon Tetrachloride 56-23-5 7.94.6 Not Detected4.6
Chlorobenzene 108-90-7 5.80.75 Not Detected2.3
Chloroethane 75-00-3 131.9 Not Detected6.2
Chloroform 67-66-3 6.21.1 Not Detected2.5
Chloromethane 74-87-3 264.2 Not Detected4.9
cis-1,2-Dichloroethene 156-59-2 5.01.5 Not Detected2.0
cis-1,3-Dichloropropene 10061-01-5 5.71.1 Not Detected2.3
Cumene 98-82-8 6.20.72 Not Detected2.5
Cyclohexane 110-82-7 4.30.77 Not Detected1.7
Dibromochloromethane 124-48-1 111.3 Not Detected4.3
Ethanol 64-17-5 9.51.3 394.5
Ethyl Benzene 100-41-4 5.50.66 Not Detected2.2
Freon 11 75-69-4 7.11.3 162.8
Freon 113 76-13-1 9.62.0 Not Detected3.9
Freon 114 76-14-2 8.81.2 Not Detected3.5
Freon 12 75-71-8 6.21.3 1.6 J2.5
Heptane 142-82-5 5.20.99 1.5 J2.1
Hexachlorobutadiene 87-68-3 544.6 Not Detected25
Page 5 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:24 PM
2.52
msdp.i / p011617R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-01A
1/10/17 06:12 PM
1 Liter Summa Canister
Carolina Foundry
SV-01
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.40.30 Not Detected1.8
m,p-Xylene 108-38-3 5.50.82 1.3 J2.2
Methyl tert-butyl ether 1634-04-4 181.2 Not Detected1.8
Methylene Chloride 75-09-2 441.9 Not Detected8.2
o-Xylene 95-47-6 5.50.66 Not Detected2.2
Propylbenzene 103-65-1 6.20.70 Not Detected2.5
Styrene 100-42-5 5.41.2 2.6 J2.1
Tetrachloroethene 127-18-4 8.51.2 6.9 J3.4
Tetrahydrofuran 109-99-9 3.70.77 Not Detected1.5
Toluene 108-88-3 4.70.58 9.31.9
trans-1,2-Dichloroethene 156-60-5 5.01.8 Not Detected2.0
trans-1,3-Dichloropropene 10061-02-6 5.70.60 Not Detected2.3
Trichloroethene 79-01-6 6.81.5 Not Detected2.7
Vinyl Chloride 75-01-4 3.20.29 Not Detected1.3
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 93
4-Bromofluorobenzene 460-00-4 70-130 98
Toluene-d8 2037-26-5 70-130 104
Page 6 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:50 PM
2.64
msdp.i / p011618R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-02A
1/10/17 02:14 PM
1 Liter Summa Canister
Carolina Foundry
SV-02
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 7.21.2 Not Detected2.9
1,1,2,2-Tetrachloroethane 79-34-5 9.11.2 Not Detected3.6
1,1,2-Trichloroethane 79-00-5 7.21.4 Not Detected2.9
1,1-Dichloroethane 75-34-3 5.30.39 Not Detected2.1
1,1-Dichloroethene 75-35-4 5.21.1 Not Detected2.1
1,2,4-Trichlorobenzene 120-82-1 393.7 Not Detected18
1,2,4-Trimethylbenzene 95-63-6 6.52.0 Not Detected2.6
1,2-Dibromoethane (EDB)106-93-4 100.92 Not Detected4.0
1,2-Dichlorobenzene 95-50-1 7.91.0 Not Detected3.2
1,2-Dichloroethane 107-06-2 5.31.1 Not Detected2.1
1,2-Dichloropropane 78-87-5 6.11.1 Not Detected2.4
1,3,5-Trimethylbenzene 108-67-8 6.51.4 Not Detected2.6
1,3-Butadiene 106-99-0 2.90.61 Not Detected1.2
1,3-Dichlorobenzene 541-73-1 7.90.50 Not Detected3.2
1,4-Dichlorobenzene 106-46-7 7.90.91 Not Detected3.2
1,4-Dioxane 123-91-1 192.8 Not Detected8.9
2,2,4-Trimethylpentane 540-84-1 6.20.56 Not Detected2.5
2-Butanone (Methyl Ethyl Ketone)78-93-3 162.2 5.8 J7.3
2-Hexanone 591-78-6 220.95 Not Detected10
2-Propanol 67-63-0 130.95 7.0 J6.1
3-Chloropropene 107-05-1 162.7 Not Detected7.8
4-Ethyltoluene 622-96-8 6.51.5 Not Detected2.6
4-Methyl-2-pentanone 108-10-1 5.41.4 Not Detected2.2
Acetone 67-64-1 312.8 715.9
Page 7 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:50 PM
2.64
msdp.i / p011618R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-02A
1/10/17 02:14 PM
1 Liter Summa Canister
Carolina Foundry
SV-02
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.81.4 Not Detected2.7
Benzene 71-43-2 4.20.39 Not Detected1.7
Bromodichloromethane 75-27-4 8.81.5 Not Detected3.5
Bromoform 75-25-2 141.7 Not Detected5.4
Bromomethane 74-83-9 514.3 Not Detected9.6
Carbon Disulfide 75-15-0 160.96 2.2 J7.7
Carbon Tetrachloride 56-23-5 8.34.9 Not Detected4.9
Chlorobenzene 108-90-7 6.10.78 Not Detected2.4
Chloroethane 75-00-3 142.0 Not Detected6.5
Chloroform 67-66-3 6.41.1 Not Detected2.6
Chloromethane 74-87-3 274.4 Not Detected5.1
cis-1,2-Dichloroethene 156-59-2 5.21.6 Not Detected2.1
cis-1,3-Dichloropropene 10061-01-5 6.01.2 Not Detected2.4
Cumene 98-82-8 6.50.75 Not Detected2.6
Cyclohexane 110-82-7 4.50.80 Not Detected1.8
Dibromochloromethane 124-48-1 111.4 Not Detected4.5
Ethanol 64-17-5 9.91.4 224.7
Ethyl Benzene 100-41-4 5.70.69 Not Detected2.3
Freon 11 75-69-4 7.41.4 Not Detected3.0
Freon 113 76-13-1 102.2 Not Detected4.0
Freon 114 76-14-2 9.21.3 Not Detected3.7
Freon 12 75-71-8 6.51.3 2.0 J2.6
Heptane 142-82-5 5.41.0 Not Detected2.2
Hexachlorobutadiene 87-68-3 564.8 Not Detected26
Page 8 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:50 PM
2.64
msdp.i / p011618R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-02A
1/10/17 02:14 PM
1 Liter Summa Canister
Carolina Foundry
SV-02
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.60.31 Not Detected1.9
m,p-Xylene 108-38-3 5.70.86 Not Detected2.3
Methyl tert-butyl ether 1634-04-4 191.2 Not Detected1.9
Methylene Chloride 75-09-2 462.0 Not Detected8.6
o-Xylene 95-47-6 5.70.69 Not Detected2.3
Propylbenzene 103-65-1 6.50.74 Not Detected2.6
Styrene 100-42-5 5.61.2 Not Detected2.2
Tetrachloroethene 127-18-4 9.01.2 2.5 J3.6
Tetrahydrofuran 109-99-9 3.90.81 Not Detected1.6
Toluene 108-88-3 5.00.60 0.87 J2.0
trans-1,2-Dichloroethene 156-60-5 5.21.9 Not Detected2.1
trans-1,3-Dichloropropene 10061-02-6 6.00.63 Not Detected2.4
Trichloroethene 79-01-6 7.11.6 Not Detected2.8
Vinyl Chloride 75-01-4 3.40.30 Not Detected1.3
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 94
4-Bromofluorobenzene 460-00-4 70-130 98
Toluene-d8 2037-26-5 70-130 102
Page 9 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:20 PM
2.42
msdp.i / p011619R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-03A
1/10/17 04:36 PM
1 Liter Summa Canister
Carolina Foundry
SV-03
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.61.1 Not Detected2.6
1,1,2,2-Tetrachloroethane 79-34-5 8.31.1 Not Detected3.3
1,1,2-Trichloroethane 79-00-5 6.61.3 Not Detected2.6
1,1-Dichloroethane 75-34-3 4.90.36 Not Detected2.0
1,1-Dichloroethene 75-35-4 4.81.0 Not Detected1.9
1,2,4-Trichlorobenzene 120-82-1 363.4 Not Detected17
1,2,4-Trimethylbenzene 95-63-6 5.91.8 2.2 J2.4
1,2-Dibromoethane (EDB)106-93-4 9.30.84 Not Detected3.7
1,2-Dichlorobenzene 95-50-1 7.30.96 Not Detected2.9
1,2-Dichloroethane 107-06-2 4.90.98 Not Detected2.0
1,2-Dichloropropane 78-87-5 5.60.98 Not Detected2.2
1,3,5-Trimethylbenzene 108-67-8 5.91.2 Not Detected2.4
1,3-Butadiene 106-99-0 2.70.56 Not Detected1.1
1,3-Dichlorobenzene 541-73-1 7.30.46 Not Detected2.9
1,4-Dichlorobenzene 106-46-7 7.30.83 Not Detected2.9
1,4-Dioxane 123-91-1 172.6 Not Detected8.2
2,2,4-Trimethylpentane 540-84-1 5.60.51 1.7 J2.3
2-Butanone (Methyl Ethyl Ketone)78-93-3 142.0 2.6 J6.7
2-Hexanone 591-78-6 200.87 Not Detected9.3
2-Propanol 67-63-0 120.87 Not Detected5.6
3-Chloropropene 107-05-1 152.5 Not Detected7.1
4-Ethyltoluene 622-96-8 5.91.4 Not Detected2.4
4-Methyl-2-pentanone 108-10-1 5.01.3 Not Detected2.0
Acetone 67-64-1 292.5 16 J5.4
Page 10 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:20 PM
2.42
msdp.i / p011619R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-03A
1/10/17 04:36 PM
1 Liter Summa Canister
Carolina Foundry
SV-03
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.31.3 Not Detected2.5
Benzene 71-43-2 3.90.36 2.6 J1.5
Bromodichloromethane 75-27-4 8.11.4 Not Detected3.2
Bromoform 75-25-2 121.6 Not Detected5.0
Bromomethane 74-83-9 473.9 Not Detected8.8
Carbon Disulfide 75-15-0 150.88 2.2 J7.1
Carbon Tetrachloride 56-23-5 7.64.5 Not Detected4.5
Chlorobenzene 108-90-7 5.60.72 Not Detected2.2
Chloroethane 75-00-3 131.8 Not Detected6.0
Chloroform 67-66-3 5.91.0 Not Detected2.4
Chloromethane 74-87-3 254.0 Not Detected4.7
cis-1,2-Dichloroethene 156-59-2 4.81.5 Not Detected1.9
cis-1,3-Dichloropropene 10061-01-5 5.51.1 Not Detected2.2
Cumene 98-82-8 5.90.69 Not Detected2.4
Cyclohexane 110-82-7 4.20.74 Not Detected1.7
Dibromochloromethane 124-48-1 101.3 Not Detected4.1
Ethanol 64-17-5 9.11.3 5.0 J4.3
Ethyl Benzene 100-41-4 5.20.63 Not Detected2.1
Freon 11 75-69-4 6.81.2 Not Detected2.7
Freon 113 76-13-1 9.32.0 Not Detected3.7
Freon 114 76-14-2 8.41.2 Not Detected3.4
Freon 12 75-71-8 6.01.2 2.3 J2.4
Heptane 142-82-5 5.00.95 Not Detected2.0
Hexachlorobutadiene 87-68-3 524.4 Not Detected24
Page 11 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:20 PM
2.42
msdp.i / p011619R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-03A
1/10/17 04:36 PM
1 Liter Summa Canister
Carolina Foundry
SV-03
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.30.29 Not Detected1.7
m,p-Xylene 108-38-3 5.20.79 1.5 J2.1
Methyl tert-butyl ether 1634-04-4 171.1 Not Detected1.7
Methylene Chloride 75-09-2 421.8 Not Detected7.9
o-Xylene 95-47-6 5.20.64 0.67 J2.1
Propylbenzene 103-65-1 5.90.67 Not Detected2.4
Styrene 100-42-5 5.21.2 1.7 J2.1
Tetrachloroethene 127-18-4 8.21.1 Not Detected3.3
Tetrahydrofuran 109-99-9 3.60.74 Not Detected1.4
Toluene 108-88-3 4.60.55 3.7 J1.8
trans-1,2-Dichloroethene 156-60-5 4.81.8 Not Detected1.9
trans-1,3-Dichloropropene 10061-02-6 5.50.58 Not Detected2.2
Trichloroethene 79-01-6 6.51.5 Not Detected2.6
Vinyl Chloride 75-01-4 3.10.28 Not Detected1.2
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 93
4-Bromofluorobenzene 460-00-4 70-130 96
Toluene-d8 2037-26-5 70-130 102
Page 12 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:46 PM
2.38
msdp.i / p011620R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-04A
1/10/17 01:24 PM
1 Liter Summa Canister
Carolina Foundry
SV-04
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.51.1 Not Detected2.6
1,1,2,2-Tetrachloroethane 79-34-5 8.21.1 Not Detected3.3
1,1,2-Trichloroethane 79-00-5 6.51.3 Not Detected2.6
1,1-Dichloroethane 75-34-3 4.80.35 Not Detected1.9
1,1-Dichloroethene 75-35-4 4.71.0 Not Detected1.9
1,2,4-Trichlorobenzene 120-82-1 353.4 Not Detected17
1,2,4-Trimethylbenzene 95-63-6 5.81.8 402.3
1,2-Dibromoethane (EDB)106-93-4 9.10.83 Not Detected3.6
1,2-Dichlorobenzene 95-50-1 7.20.94 Not Detected2.9
1,2-Dichloroethane 107-06-2 4.80.97 Not Detected1.9
1,2-Dichloropropane 78-87-5 5.50.97 Not Detected2.2
1,3,5-Trimethylbenzene 108-67-8 5.81.2 142.3
1,3-Butadiene 106-99-0 2.60.55 Not Detected1.0
1,3-Dichlorobenzene 541-73-1 7.20.46 Not Detected2.9
1,4-Dichlorobenzene 106-46-7 7.20.82 Not Detected2.9
1,4-Dioxane 123-91-1 172.5 Not Detected8.1
2,2,4-Trimethylpentane 540-84-1 5.60.50 2.6 J2.2
2-Butanone (Methyl Ethyl Ketone)78-93-3 142.0 2806.6
2-Hexanone 591-78-6 190.86 499.2
2-Propanol 67-63-0 120.85 255.5
3-Chloropropene 107-05-1 152.4 Not Detected7.0
4-Ethyltoluene 622-96-8 5.81.4 542.3
4-Methyl-2-pentanone 108-10-1 4.91.3 321.9
Acetone 67-64-1 282.5 1200 E5.3
Page 13 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:46 PM
2.38
msdp.i / p011620R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-04A
1/10/17 01:24 PM
1 Liter Summa Canister
Carolina Foundry
SV-04
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.21.2 Not Detected2.5
Benzene 71-43-2 3.80.35 831.5
Bromodichloromethane 75-27-4 8.01.4 Not Detected3.2
Bromoform 75-25-2 121.5 Not Detected4.9
Bromomethane 74-83-9 463.9 Not Detected8.7
Carbon Disulfide 75-15-0 150.87 1007.0
Carbon Tetrachloride 56-23-5 7.54.4 Not Detected4.4
Chlorobenzene 108-90-7 5.50.70 Not Detected2.2
Chloroethane 75-00-3 121.8 Not Detected5.9
Chloroform 67-66-3 5.81.0 Not Detected2.3
Chloromethane 74-87-3 244.0 Not Detected4.6
cis-1,2-Dichloroethene 156-59-2 4.71.4 Not Detected1.9
cis-1,3-Dichloropropene 10061-01-5 5.41.1 Not Detected2.2
Cumene 98-82-8 5.80.68 4.0 J2.3
Cyclohexane 110-82-7 4.10.72 6.81.6
Dibromochloromethane 124-48-1 101.3 Not Detected4.0
Ethanol 64-17-5 9.01.2 524.2
Ethyl Benzene 100-41-4 5.20.62 452.1
Freon 11 75-69-4 6.71.2 Not Detected2.7
Freon 113 76-13-1 9.11.9 Not Detected3.6
Freon 114 76-14-2 8.31.2 Not Detected3.3
Freon 12 75-71-8 5.91.2 2.0 J2.4
Heptane 142-82-5 4.90.94 552.0
Hexachlorobutadiene 87-68-3 514.4 Not Detected24
Page 14 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:46 PM
2.38
msdp.i / p011620R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-04A
1/10/17 01:24 PM
1 Liter Summa Canister
Carolina Foundry
SV-04
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.20.28 531.7
m,p-Xylene 108-38-3 5.20.78 1102.1
Methyl tert-butyl ether 1634-04-4 171.1 Not Detected1.7
Methylene Chloride 75-09-2 411.8 Not Detected7.8
o-Xylene 95-47-6 5.20.63 542.1
Propylbenzene 103-65-1 5.80.66 112.3
Styrene 100-42-5 5.11.1 9.12.0
Tetrachloroethene 127-18-4 8.11.1 3.9 J3.2
Tetrahydrofuran 109-99-9 3.50.73 Not Detected1.4
Toluene 108-88-3 4.50.54 1801.8
trans-1,2-Dichloroethene 156-60-5 4.71.7 Not Detected1.9
trans-1,3-Dichloropropene 10061-02-6 5.40.57 Not Detected2.2
Trichloroethene 79-01-6 6.41.5 Not Detected2.6
Vinyl Chloride 75-01-4 3.00.27 Not Detected1.2
J = Estimated value.
E = Exceeds instrument calibration range.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 92
4-Bromofluorobenzene 460-00-4 70-130 100
Toluene-d8 2037-26-5 70-130 104
Page 15 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 11:13 PM
2.38
msdp.i / p011621R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-05A
1/10/17 12:12 PM
1 Liter Summa Canister
Carolina Foundry
SV-05
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.51.1 Not Detected2.6
1,1,2,2-Tetrachloroethane 79-34-5 8.21.1 Not Detected3.3
1,1,2-Trichloroethane 79-00-5 6.51.3 Not Detected2.6
1,1-Dichloroethane 75-34-3 4.80.35 Not Detected1.9
1,1-Dichloroethene 75-35-4 4.71.0 Not Detected1.9
1,2,4-Trichlorobenzene 120-82-1 353.4 Not Detected17
1,2,4-Trimethylbenzene 95-63-6 5.81.8 2.1 J2.3
1,2-Dibromoethane (EDB)106-93-4 9.10.83 Not Detected3.6
1,2-Dichlorobenzene 95-50-1 7.20.94 Not Detected2.9
1,2-Dichloroethane 107-06-2 4.80.97 Not Detected1.9
1,2-Dichloropropane 78-87-5 5.50.97 Not Detected2.2
1,3,5-Trimethylbenzene 108-67-8 5.81.2 Not Detected2.3
1,3-Butadiene 106-99-0 2.60.55 Not Detected1.0
1,3-Dichlorobenzene 541-73-1 7.20.46 Not Detected2.9
1,4-Dichlorobenzene 106-46-7 7.20.82 Not Detected2.9
1,4-Dioxane 123-91-1 172.5 Not Detected8.1
2,2,4-Trimethylpentane 540-84-1 5.60.50 Not Detected2.2
2-Butanone (Methyl Ethyl Ketone)78-93-3 142.0 Not Detected6.6
2-Hexanone 591-78-6 190.86 Not Detected9.2
2-Propanol 67-63-0 120.85 Not Detected5.5
3-Chloropropene 107-05-1 152.4 Not Detected7.0
4-Ethyltoluene 622-96-8 5.81.4 Not Detected2.3
4-Methyl-2-pentanone 108-10-1 4.91.3 Not Detected1.9
Acetone 67-64-1 282.5 28 J5.3
Page 16 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 11:13 PM
2.38
msdp.i / p011621R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-05A
1/10/17 12:12 PM
1 Liter Summa Canister
Carolina Foundry
SV-05
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.21.2 Not Detected2.5
Benzene 71-43-2 3.80.35 Not Detected1.5
Bromodichloromethane 75-27-4 8.01.4 Not Detected3.2
Bromoform 75-25-2 121.5 Not Detected4.9
Bromomethane 74-83-9 463.9 Not Detected8.7
Carbon Disulfide 75-15-0 150.87 2.7 J7.0
Carbon Tetrachloride 56-23-5 7.54.4 Not Detected4.4
Chlorobenzene 108-90-7 5.50.70 Not Detected2.2
Chloroethane 75-00-3 121.8 Not Detected5.9
Chloroform 67-66-3 5.81.0 Not Detected2.3
Chloromethane 74-87-3 244.0 Not Detected4.6
cis-1,2-Dichloroethene 156-59-2 4.71.4 Not Detected1.9
cis-1,3-Dichloropropene 10061-01-5 5.41.1 Not Detected2.2
Cumene 98-82-8 5.80.68 Not Detected2.3
Cyclohexane 110-82-7 4.10.72 Not Detected1.6
Dibromochloromethane 124-48-1 101.3 Not Detected4.0
Ethanol 64-17-5 9.01.2 134.2
Ethyl Benzene 100-41-4 5.20.62 Not Detected2.1
Freon 11 75-69-4 6.71.2 Not Detected2.7
Freon 113 76-13-1 9.11.9 Not Detected3.6
Freon 114 76-14-2 8.31.2 Not Detected3.3
Freon 12 75-71-8 5.91.2 Not Detected2.4
Heptane 142-82-5 4.90.94 Not Detected2.0
Hexachlorobutadiene 87-68-3 514.4 Not Detected24
Page 17 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 11:13 PM
2.38
msdp.i / p011621R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-05A
1/10/17 12:12 PM
1 Liter Summa Canister
Carolina Foundry
SV-05
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.20.28 Not Detected1.7
m,p-Xylene 108-38-3 5.20.78 Not Detected2.1
Methyl tert-butyl ether 1634-04-4 171.1 Not Detected1.7
Methylene Chloride 75-09-2 411.8 Not Detected7.8
o-Xylene 95-47-6 5.20.63 Not Detected2.1
Propylbenzene 103-65-1 5.80.66 Not Detected2.3
Styrene 100-42-5 5.11.1 1.8 J2.0
Tetrachloroethene 127-18-4 8.11.1 6.6 J3.2
Tetrahydrofuran 109-99-9 3.50.73 Not Detected1.4
Toluene 108-88-3 4.50.54 1.2 J1.8
trans-1,2-Dichloroethene 156-60-5 4.71.7 Not Detected1.9
trans-1,3-Dichloropropene 10061-02-6 5.40.57 Not Detected2.2
Trichloroethene 79-01-6 6.41.5 Not Detected2.6
Vinyl Chloride 75-01-4 3.00.27 Not Detected1.2
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 94
4-Bromofluorobenzene 460-00-4 70-130 97
Toluene-d8 2037-26-5 70-130 104
Page 18 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 04:20 PM
2.52
msdp.i / p011710R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-06A
1/10/17 03:30 PM
1 Liter Summa Canister
Carolina Foundry
SV-06
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.91.2 Not Detected2.8
1,1,2,2-Tetrachloroethane 79-34-5 8.61.2 Not Detected3.5
1,1,2-Trichloroethane 79-00-5 6.91.4 Not Detected2.8
1,1-Dichloroethane 75-34-3 5.10.37 Not Detected2.0
1,1-Dichloroethene 75-35-4 5.01.1 Not Detected2.0
1,2,4-Trichlorobenzene 120-82-1 373.6 Not Detected18
1,2,4-Trimethylbenzene 95-63-6 6.21.9 802.5
1,2-Dibromoethane (EDB)106-93-4 9.70.88 Not Detected3.9
1,2-Dichlorobenzene 95-50-1 7.61.0 Not Detected3.0
1,2-Dichloroethane 107-06-2 5.11.0 1.9 J2.0
1,2-Dichloropropane 78-87-5 5.81.0 4.2 J2.3
1,3,5-Trimethylbenzene 108-67-8 6.21.3 202.5
1,3-Butadiene 106-99-0 2.80.58 Not Detected1.1
1,3-Dichlorobenzene 541-73-1 7.60.48 Not Detected3.0
1,4-Dichlorobenzene 106-46-7 7.60.87 Not Detected3.0
1,4-Dioxane 123-91-1 182.7 Not Detected8.5
2,2,4-Trimethylpentane 540-84-1 5.90.53 Not Detected2.4
2-Butanone (Methyl Ethyl Ketone)78-93-3 152.1 11 J7.0
2-Hexanone 591-78-6 210.91 Not Detected9.7
2-Propanol 67-63-0 120.90 Not Detected5.8
3-Chloropropene 107-05-1 162.6 Not Detected7.4
4-Ethyltoluene 622-96-8 6.21.4 322.5
4-Methyl-2-pentanone 108-10-1 5.21.4 Not Detected2.1
Acetone 67-64-1 302.6 555.6
Page 19 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 04:20 PM
2.52
msdp.i / p011710R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-06A
1/10/17 03:30 PM
1 Liter Summa Canister
Carolina Foundry
SV-06
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.51.3 Not Detected2.6
Benzene 71-43-2 4.00.37 Not Detected1.6
Bromodichloromethane 75-27-4 8.41.4 Not Detected3.4
Bromoform 75-25-2 131.6 Not Detected5.2
Bromomethane 74-83-9 494.1 Not Detected9.2
Carbon Disulfide 75-15-0 160.92 6.6 J7.4
Carbon Tetrachloride 56-23-5 7.94.6 Not Detected4.6
Chlorobenzene 108-90-7 5.80.75 Not Detected2.3
Chloroethane 75-00-3 131.9 Not Detected6.2
Chloroform 67-66-3 6.21.1 Not Detected2.5
Chloromethane 74-87-3 264.2 Not Detected4.9
cis-1,2-Dichloroethene 156-59-2 5.01.5 Not Detected2.0
cis-1,3-Dichloropropene 10061-01-5 5.71.1 Not Detected2.3
Cumene 98-82-8 6.20.72 1.6 J2.5
Cyclohexane 110-82-7 4.30.77 Not Detected1.7
Dibromochloromethane 124-48-1 111.3 Not Detected4.3
Ethanol 64-17-5 9.51.3 144.5
Ethyl Benzene 100-41-4 5.50.66 Not Detected2.2
Freon 11 75-69-4 7.11.3 1.4 J2.8
Freon 113 76-13-1 9.62.0 Not Detected3.9
Freon 114 76-14-2 8.81.2 Not Detected3.5
Freon 12 75-71-8 6.21.3 2.1 J2.5
Heptane 142-82-5 5.20.99 1.5 J2.1
Hexachlorobutadiene 87-68-3 544.6 Not Detected25
Page 20 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 04:20 PM
2.52
msdp.i / p011710R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-06A
1/10/17 03:30 PM
1 Liter Summa Canister
Carolina Foundry
SV-06
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.40.30 3.2 J1.8
m,p-Xylene 108-38-3 5.50.82 3.3 J2.2
Methyl tert-butyl ether 1634-04-4 181.2 Not Detected1.8
Methylene Chloride 75-09-2 441.9 Not Detected8.2
o-Xylene 95-47-6 5.50.66 2.5 J2.2
Propylbenzene 103-65-1 6.20.70 4.9 J2.5
Styrene 100-42-5 5.41.2 Not Detected2.1
Tetrachloroethene 127-18-4 8.51.2 6.6 J3.4
Tetrahydrofuran 109-99-9 3.70.77 Not Detected1.5
Toluene 108-88-3 4.70.58 6.91.9
trans-1,2-Dichloroethene 156-60-5 5.01.8 Not Detected2.0
trans-1,3-Dichloropropene 10061-02-6 5.70.60 Not Detected2.3
Trichloroethene 79-01-6 6.81.5 Not Detected2.7
Vinyl Chloride 75-01-4 3.20.29 Not Detected1.3
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 92
4-Bromofluorobenzene 460-00-4 70-130 105
Toluene-d8 2037-26-5 70-130 102
Page 21 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:30 AM
2.38
msdp.i / p011624R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-07A
1/10/17 06:52 PM
1 Liter Summa Canister
Carolina Foundry
SV-07
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.51.1 Not Detected2.6
1,1,2,2-Tetrachloroethane 79-34-5 8.21.1 Not Detected3.3
1,1,2-Trichloroethane 79-00-5 6.51.3 Not Detected2.6
1,1-Dichloroethane 75-34-3 4.80.35 Not Detected1.9
1,1-Dichloroethene 75-35-4 4.71.0 Not Detected1.9
1,2,4-Trichlorobenzene 120-82-1 353.4 Not Detected17
1,2,4-Trimethylbenzene 95-63-6 5.81.8 9.42.3
1,2-Dibromoethane (EDB)106-93-4 9.10.83 Not Detected3.6
1,2-Dichlorobenzene 95-50-1 7.20.94 Not Detected2.9
1,2-Dichloroethane 107-06-2 4.80.97 Not Detected1.9
1,2-Dichloropropane 78-87-5 5.50.97 Not Detected2.2
1,3,5-Trimethylbenzene 108-67-8 5.81.2 4.5 J2.3
1,3-Butadiene 106-99-0 2.60.55 Not Detected1.0
1,3-Dichlorobenzene 541-73-1 7.20.46 Not Detected2.9
1,4-Dichlorobenzene 106-46-7 7.20.82 Not Detected2.9
1,4-Dioxane 123-91-1 172.5 Not Detected8.1
2,2,4-Trimethylpentane 540-84-1 5.60.50 1.7 J2.2
2-Butanone (Methyl Ethyl Ketone)78-93-3 142.0 4.9 J6.6
2-Hexanone 591-78-6 190.86 Not Detected9.2
2-Propanol 67-63-0 120.85 Not Detected5.5
3-Chloropropene 107-05-1 152.4 Not Detected7.0
4-Ethyltoluene 622-96-8 5.81.4 112.3
4-Methyl-2-pentanone 108-10-1 4.91.3 Not Detected1.9
Acetone 67-64-1 282.5 1005.3
Page 22 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:30 AM
2.38
msdp.i / p011624R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-07A
1/10/17 06:52 PM
1 Liter Summa Canister
Carolina Foundry
SV-07
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.21.2 Not Detected2.5
Benzene 71-43-2 3.80.35 1.3 J1.5
Bromodichloromethane 75-27-4 8.01.4 Not Detected3.2
Bromoform 75-25-2 121.5 Not Detected4.9
Bromomethane 74-83-9 463.9 Not Detected8.7
Carbon Disulfide 75-15-0 150.87 1.7 J7.0
Carbon Tetrachloride 56-23-5 7.54.4 Not Detected4.4
Chlorobenzene 108-90-7 5.50.70 Not Detected2.2
Chloroethane 75-00-3 121.8 Not Detected5.9
Chloroform 67-66-3 5.81.0 Not Detected2.3
Chloromethane 74-87-3 244.0 Not Detected4.6
cis-1,2-Dichloroethene 156-59-2 4.71.4 Not Detected1.9
cis-1,3-Dichloropropene 10061-01-5 5.41.1 Not Detected2.2
Cumene 98-82-8 5.80.68 Not Detected2.3
Cyclohexane 110-82-7 4.10.72 Not Detected1.6
Dibromochloromethane 124-48-1 101.3 Not Detected4.0
Ethanol 64-17-5 9.01.2 264.2
Ethyl Benzene 100-41-4 5.20.62 1.2 J2.1
Freon 11 75-69-4 6.71.2 312.7
Freon 113 76-13-1 9.11.9 Not Detected3.6
Freon 114 76-14-2 8.31.2 Not Detected3.3
Freon 12 75-71-8 5.91.2 2.0 J2.4
Heptane 142-82-5 4.90.94 1.8 J2.0
Hexachlorobutadiene 87-68-3 514.4 Not Detected24
Page 23 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:30 AM
2.38
msdp.i / p011624R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-07A
1/10/17 06:52 PM
1 Liter Summa Canister
Carolina Foundry
SV-07
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.20.28 6.51.7
m,p-Xylene 108-38-3 5.20.78 5.82.1
Methyl tert-butyl ether 1634-04-4 171.1 Not Detected1.7
Methylene Chloride 75-09-2 411.8 Not Detected7.8
o-Xylene 95-47-6 5.20.63 2.2 J2.1
Propylbenzene 103-65-1 5.80.66 2.4 J2.3
Styrene 100-42-5 5.11.1 3.8 J2.0
Tetrachloroethene 127-18-4 8.11.1 3.2 J3.2
Tetrahydrofuran 109-99-9 3.50.73 Not Detected1.4
Toluene 108-88-3 4.50.54 131.8
trans-1,2-Dichloroethene 156-60-5 4.71.7 Not Detected1.9
trans-1,3-Dichloropropene 10061-02-6 5.40.57 Not Detected2.2
Trichloroethene 79-01-6 6.41.5 Not Detected2.6
Vinyl Chloride 75-01-4 3.00.27 Not Detected1.2
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 92
4-Bromofluorobenzene 460-00-4 70-130 99
Toluene-d8 2037-26-5 70-130 104
Page 24 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:04 AM
2.32
msdp.i / p011623R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-08A
1/10/17 12:00 AM
1 Liter Summa Canister
Carolina Foundry
DUP-1-10-17
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 6.31.1 Not Detected2.5
1,1,2,2-Tetrachloroethane 79-34-5 8.01.1 Not Detected3.2
1,1,2-Trichloroethane 79-00-5 6.31.2 Not Detected2.5
1,1-Dichloroethane 75-34-3 4.70.34 Not Detected1.9
1,1-Dichloroethene 75-35-4 4.61.0 Not Detected1.8
1,2,4-Trichlorobenzene 120-82-1 343.3 Not Detected16
1,2,4-Trimethylbenzene 95-63-6 5.71.7 402.3
1,2-Dibromoethane (EDB)106-93-4 8.90.81 Not Detected3.6
1,2-Dichlorobenzene 95-50-1 7.00.92 Not Detected2.8
1,2-Dichloroethane 107-06-2 4.70.94 Not Detected1.9
1,2-Dichloropropane 78-87-5 5.40.94 Not Detected2.1
1,3,5-Trimethylbenzene 108-67-8 5.71.2 132.3
1,3-Butadiene 106-99-0 2.60.54 Not Detected1.0
1,3-Dichlorobenzene 541-73-1 7.00.44 Not Detected2.8
1,4-Dichlorobenzene 106-46-7 7.00.80 Not Detected2.8
1,4-Dioxane 123-91-1 172.5 Not Detected7.8
2,2,4-Trimethylpentane 540-84-1 5.40.49 2.5 J2.2
2-Butanone (Methyl Ethyl Ketone)78-93-3 141.9 2706.4
2-Hexanone 591-78-6 190.84 478.9
2-Propanol 67-63-0 110.83 235.4
3-Chloropropene 107-05-1 142.4 Not Detected6.8
4-Ethyltoluene 622-96-8 5.71.3 512.3
4-Methyl-2-pentanone 108-10-1 4.81.3 311.9
Acetone 67-64-1 282.4 1100 E5.2
Page 25 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:04 AM
2.32
msdp.i / p011623R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-08A
1/10/17 12:00 AM
1 Liter Summa Canister
Carolina Foundry
DUP-1-10-17
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 6.01.2 Not Detected2.4
Benzene 71-43-2 3.70.34 781.5
Bromodichloromethane 75-27-4 7.81.3 Not Detected3.1
Bromoform 75-25-2 121.5 Not Detected4.8
Bromomethane 74-83-9 453.8 Not Detected8.5
Carbon Disulfide 75-15-0 140.85 1006.8
Carbon Tetrachloride 56-23-5 7.34.3 Not Detected4.3
Chlorobenzene 108-90-7 5.30.69 Not Detected2.1
Chloroethane 75-00-3 121.7 Not Detected5.8
Chloroform 67-66-3 5.70.98 Not Detected2.3
Chloromethane 74-87-3 243.9 Not Detected4.5
cis-1,2-Dichloroethene 156-59-2 4.61.4 Not Detected1.8
cis-1,3-Dichloropropene 10061-01-5 5.31.0 Not Detected2.1
Cumene 98-82-8 5.70.66 4.0 J2.3
Cyclohexane 110-82-7 4.00.70 5.71.6
Dibromochloromethane 124-48-1 9.91.2 Not Detected4.0
Ethanol 64-17-5 8.71.2 514.1
Ethyl Benzene 100-41-4 5.00.61 432.0
Freon 11 75-69-4 6.51.2 Not Detected2.6
Freon 113 76-13-1 8.91.9 Not Detected3.6
Freon 114 76-14-2 8.11.1 Not Detected3.2
Freon 12 75-71-8 5.71.2 1.7 J2.3
Heptane 142-82-5 4.80.91 541.9
Hexachlorobutadiene 87-68-3 494.2 Not Detected23
Page 26 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:04 AM
2.32
msdp.i / p011623R1
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-08A
1/10/17 12:00 AM
1 Liter Summa Canister
Carolina Foundry
DUP-1-10-17
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 4.10.27 531.6
m,p-Xylene 108-38-3 5.00.76 1002.0
Methyl tert-butyl ether 1634-04-4 171.1 Not Detected1.7
Methylene Chloride 75-09-2 401.7 Not Detected7.6
o-Xylene 95-47-6 5.00.61 512.0
Propylbenzene 103-65-1 5.70.65 112.3
Styrene 100-42-5 4.91.1 7.92.0
Tetrachloroethene 127-18-4 7.91.1 3.4 J3.1
Tetrahydrofuran 109-99-9 3.40.71 Not Detected1.4
Toluene 108-88-3 4.40.53 1701.7
trans-1,2-Dichloroethene 156-60-5 4.61.7 Not Detected1.8
trans-1,3-Dichloropropene 10061-02-6 5.30.56 Not Detected2.1
Trichloroethene 79-01-6 6.21.4 Not Detected2.5
Vinyl Chloride 75-01-4 3.00.26 Not Detected1.2
J = Estimated value.
E = Exceeds instrument calibration range.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 93
4-Bromofluorobenzene 460-00-4 70-130 99
Toluene-d8 2037-26-5 70-130 102
Page 27 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 06:01 PM
1.00
msdp.i / p011615a
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-09A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 2.70.47 Not Detected1.1
1,1,2,2-Tetrachloroethane 79-34-5 3.40.46 Not Detected1.4
1,1,2-Trichloroethane 79-00-5 2.70.54 Not Detected1.1
1,1-Dichloroethane 75-34-3 2.00.15 Not Detected0.81
1,1-Dichloroethene 75-35-4 2.00.43 Not Detected0.79
1,2,4-Trichlorobenzene 120-82-1 151.4 Not Detected7.0
1,2,4-Trimethylbenzene 95-63-6 2.40.75 Not Detected0.98
1,2-Dibromoethane (EDB)106-93-4 3.80.35 Not Detected1.5
1,2-Dichlorobenzene 95-50-1 3.00.40 Not Detected1.2
1,2-Dichloroethane 107-06-2 2.00.41 Not Detected0.81
1,2-Dichloropropane 78-87-5 2.30.41 Not Detected0.92
1,3,5-Trimethylbenzene 108-67-8 2.40.52 Not Detected0.98
1,3-Butadiene 106-99-0 1.10.23 Not Detected0.44
1,3-Dichlorobenzene 541-73-1 3.00.19 Not Detected1.2
1,4-Dichlorobenzene 106-46-7 3.00.34 Not Detected1.2
1,4-Dioxane 123-91-1 7.21.1 Not Detected3.4
2,2,4-Trimethylpentane 540-84-1 2.30.21 Not Detected0.93
2-Butanone (Methyl Ethyl Ketone)78-93-3 5.90.83 Not Detected2.8
2-Hexanone 591-78-6 8.20.36 Not Detected3.8
2-Propanol 67-63-0 4.90.36 Not Detected2.3
3-Chloropropene 107-05-1 6.31.0 Not Detected2.9
4-Ethyltoluene 622-96-8 2.40.57 Not Detected0.98
4-Methyl-2-pentanone 108-10-1 2.00.55 Not Detected0.82
Acetone 67-64-1 121.0 Not Detected2.2
Page 28 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 06:01 PM
1.00
msdp.i / p011615a
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-09A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 2.60.53 Not Detected1.0
Benzene 71-43-2 1.60.15 Not Detected0.64
Bromodichloromethane 75-27-4 3.40.57 Not Detected1.3
Bromoform 75-25-2 5.20.64 Not Detected2.1
Bromomethane 74-83-9 191.6 Not Detected3.6
Carbon Disulfide 75-15-0 6.20.36 0.38 J2.9
Carbon Tetrachloride 56-23-5 3.11.8 Not Detected1.8
Chlorobenzene 108-90-7 2.30.30 Not Detected0.92
Chloroethane 75-00-3 5.30.75 Not Detected2.5
Chloroform 67-66-3 2.40.42 Not Detected0.98
Chloromethane 74-87-3 101.7 Not Detected1.9
cis-1,2-Dichloroethene 156-59-2 2.00.61 Not Detected0.79
cis-1,3-Dichloropropene 10061-01-5 2.30.45 Not Detected0.91
Cumene 98-82-8 2.40.28 Not Detected0.98
Cyclohexane 110-82-7 1.70.30 Not Detected0.69
Dibromochloromethane 124-48-1 4.20.54 Not Detected1.7
Ethanol 64-17-5 3.80.52 Not Detected1.8
Ethyl Benzene 100-41-4 2.20.26 Not Detected0.87
Freon 11 75-69-4 2.80.52 Not Detected1.1
Freon 113 76-13-1 3.80.82 Not Detected1.5
Freon 114 76-14-2 3.50.48 Not Detected1.4
Freon 12 75-71-8 2.50.50 Not Detected0.99
Heptane 142-82-5 2.00.39 Not Detected0.82
Hexachlorobutadiene 87-68-3 211.8 Not Detected10
Page 29 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 06:01 PM
1.00
msdp.i / p011615a
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-09A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 1.80.12 Not Detected0.70
m,p-Xylene 108-38-3 2.20.33 Not Detected0.87
Methyl tert-butyl ether 1634-04-4 7.20.47 Not Detected0.72
Methylene Chloride 75-09-2 170.74 Not Detected3.3
o-Xylene 95-47-6 2.20.26 Not Detected0.87
Propylbenzene 103-65-1 2.40.28 Not Detected0.98
Styrene 100-42-5 2.10.48 Not Detected0.85
Tetrachloroethene 127-18-4 3.40.47 Not Detected1.4
Tetrahydrofuran 109-99-9 1.50.31 Not Detected0.59
Toluene 108-88-3 1.90.23 Not Detected0.75
trans-1,2-Dichloroethene 156-60-5 2.00.73 Not Detected0.79
trans-1,3-Dichloropropene 10061-02-6 2.30.24 Not Detected0.91
Trichloroethene 79-01-6 2.70.61 Not Detected1.1
Vinyl Chloride 75-01-4 1.30.11 Not Detected0.51
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 92
4-Bromofluorobenzene 460-00-4 70-130 96
Toluene-d8 2037-26-5 70-130 105
Page 30 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:56 PM
1.00
msdp.i / p011705c
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-09B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
1,1,1-Trichloroethane 71-55-6 2.70.47 Not Detected1.1
1,1,2,2-Tetrachloroethane 79-34-5 3.40.46 Not Detected1.4
1,1,2-Trichloroethane 79-00-5 2.70.54 Not Detected1.1
1,1-Dichloroethane 75-34-3 2.00.15 Not Detected0.81
1,1-Dichloroethene 75-35-4 2.00.43 Not Detected0.79
1,2,4-Trichlorobenzene 120-82-1 151.4 Not Detected7.0
1,2,4-Trimethylbenzene 95-63-6 2.40.75 Not Detected0.98
1,2-Dibromoethane (EDB)106-93-4 3.80.35 Not Detected1.5
1,2-Dichlorobenzene 95-50-1 3.00.40 Not Detected1.2
1,2-Dichloroethane 107-06-2 2.00.41 Not Detected0.81
1,2-Dichloropropane 78-87-5 2.30.41 Not Detected0.92
1,3,5-Trimethylbenzene 108-67-8 2.40.52 0.71 J0.98
1,3-Butadiene 106-99-0 1.10.23 Not Detected0.44
1,3-Dichlorobenzene 541-73-1 3.00.19 0.23 J1.2
1,4-Dichlorobenzene 106-46-7 3.00.34 Not Detected1.2
1,4-Dioxane 123-91-1 7.21.1 Not Detected3.4
2,2,4-Trimethylpentane 540-84-1 2.30.21 0.28 J0.93
2-Butanone (Methyl Ethyl Ketone)78-93-3 5.90.83 Not Detected2.8
2-Hexanone 591-78-6 8.20.36 Not Detected3.8
2-Propanol 67-63-0 4.90.36 Not Detected2.3
3-Chloropropene 107-05-1 6.31.0 Not Detected2.9
4-Ethyltoluene 622-96-8 2.40.57 Not Detected0.98
4-Methyl-2-pentanone 108-10-1 2.00.55 Not Detected0.82
Acetone 67-64-1 121.0 Not Detected2.2
Page 31 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:56 PM
1.00
msdp.i / p011705c
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-09B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
alpha-Chlorotoluene 100-44-7 2.60.53 Not Detected1.0
Benzene 71-43-2 1.60.15 Not Detected0.64
Bromodichloromethane 75-27-4 3.40.57 Not Detected1.3
Bromoform 75-25-2 5.20.64 Not Detected2.1
Bromomethane 74-83-9 191.6 Not Detected3.6
Carbon Disulfide 75-15-0 6.20.36 0.67 J2.9
Carbon Tetrachloride 56-23-5 3.11.8 Not Detected1.8
Chlorobenzene 108-90-7 2.30.30 Not Detected0.92
Chloroethane 75-00-3 5.30.75 Not Detected2.5
Chloroform 67-66-3 2.40.42 Not Detected0.98
Chloromethane 74-87-3 101.7 Not Detected1.9
cis-1,2-Dichloroethene 156-59-2 2.00.61 Not Detected0.79
cis-1,3-Dichloropropene 10061-01-5 2.30.45 Not Detected0.91
Cumene 98-82-8 2.40.28 Not Detected0.98
Cyclohexane 110-82-7 1.70.30 Not Detected0.69
Dibromochloromethane 124-48-1 4.20.54 Not Detected1.7
Ethanol 64-17-5 3.80.52 1.6 J1.8
Ethyl Benzene 100-41-4 2.20.26 Not Detected0.87
Freon 11 75-69-4 2.80.52 Not Detected1.1
Freon 113 76-13-1 3.80.82 Not Detected1.5
Freon 114 76-14-2 3.50.48 Not Detected1.4
Freon 12 75-71-8 2.50.50 Not Detected0.99
Heptane 142-82-5 2.00.39 Not Detected0.82
Hexachlorobutadiene 87-68-3 211.8 Not Detected10
Page 32 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 12:56 PM
1.00
msdp.i / p011705c
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-09B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
(ug/m3)CAS#
LOD
Compound (ug/m3)
MDL Rpt. Limit
(ug/m3)
Amount
(ug/m3)
Hexane 110-54-3 1.80.12 Not Detected0.70
m,p-Xylene 108-38-3 2.20.33 Not Detected0.87
Methyl tert-butyl ether 1634-04-4 7.20.47 Not Detected0.72
Methylene Chloride 75-09-2 170.74 Not Detected3.3
o-Xylene 95-47-6 2.20.26 Not Detected0.87
Propylbenzene 103-65-1 2.40.28 Not Detected0.98
Styrene 100-42-5 2.10.48 Not Detected0.85
Tetrachloroethene 127-18-4 3.40.47 Not Detected1.4
Tetrahydrofuran 109-99-9 1.50.31 Not Detected0.59
Toluene 108-88-3 1.90.23 Not Detected0.75
trans-1,2-Dichloroethene 156-60-5 2.00.73 Not Detected0.79
trans-1,3-Dichloropropene 10061-02-6 2.30.24 Not Detected0.91
Trichloroethene 79-01-6 2.70.61 Not Detected1.1
Vinyl Chloride 75-01-4 1.30.11 Not Detected0.51
J = Estimated value.
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 96
4-Bromofluorobenzene 460-00-4 70-130 98
Toluene-d8 2037-26-5 70-130 103
Page 33 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:58 AM
1.00
msdp.i / p011602
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-10A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
CCV
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
1,1,1-Trichloroethane 71-55-6 100
1,1,2,2-Tetrachloroethane 79-34-5 108
1,1,2-Trichloroethane 79-00-5 111
1,1-Dichloroethane 75-34-3 104
1,1-Dichloroethene 75-35-4 104
1,2,4-Trichlorobenzene 120-82-1 104
1,2,4-Trimethylbenzene 95-63-6 111
1,2-Dibromoethane (EDB)106-93-4 108
1,2-Dichlorobenzene 95-50-1 109
1,2-Dichloroethane 107-06-2 102
1,2-Dichloropropane 78-87-5 107
1,3,5-Trimethylbenzene 108-67-8 113
1,3-Butadiene 106-99-0 125
1,3-Dichlorobenzene 541-73-1 109
1,4-Dichlorobenzene 106-46-7 110
1,4-Dioxane 123-91-1 105
2,2,4-Trimethylpentane 540-84-1 106
2-Butanone (Methyl Ethyl Ketone)78-93-3 102
2-Hexanone 591-78-6 103
2-Propanol 67-63-0 95
3-Chloropropene 107-05-1 96
4-Ethyltoluene 622-96-8 110
4-Methyl-2-pentanone 108-10-1 108
Acetone 67-64-1 107
Page 34 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:58 AM
1.00
msdp.i / p011602
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-10A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
CCV
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
alpha-Chlorotoluene 100-44-7 107
Benzene 71-43-2 108
Bromodichloromethane 75-27-4 106
Bromoform 75-25-2 108
Bromomethane 74-83-9 105
Carbon Disulfide 75-15-0 100
Carbon Tetrachloride 56-23-5 103
Chlorobenzene 108-90-7 107
Chloroethane 75-00-3 102
Chloroform 67-66-3 106
Chloromethane 74-87-3 104
cis-1,2-Dichloroethene 156-59-2 105
cis-1,3-Dichloropropene 10061-01-5 107
Cumene 98-82-8 111
Cyclohexane 110-82-7 107
Dibromochloromethane 124-48-1 107
Ethanol 64-17-5 93
Ethyl Benzene 100-41-4 114
Freon 11 75-69-4 102
Freon 113 76-13-1 102
Freon 114 76-14-2 108
Freon 12 75-71-8 106
Heptane 142-82-5 109
Hexachlorobutadiene 87-68-3 107
Page 35 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 09:58 AM
1.00
msdp.i / p011602
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-10A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
CCV
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
Hexane 110-54-3 108
m,p-Xylene 108-38-3 116
Methyl tert-butyl ether 1634-04-4 93
Methylene Chloride 75-09-2 105
o-Xylene 95-47-6 114
Propylbenzene 103-65-1 108
Styrene 100-42-5 114
Tetrachloroethene 127-18-4 109
Tetrahydrofuran 109-99-9 106
Toluene 108-88-3 107
trans-1,2-Dichloroethene 156-60-5 109
trans-1,3-Dichloropropene 10061-02-6 105
Trichloroethene 79-01-6 108
Vinyl Chloride 75-01-4 115
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 93
4-Bromofluorobenzene 460-00-4 70-130 104
Toluene-d8 2037-26-5 70-130 104
Page 36 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 09:22 AM
1.00
msdp.i / p011702
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-10B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
CCV
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
1,1,1-Trichloroethane 71-55-6 101
1,1,2,2-Tetrachloroethane 79-34-5 106
1,1,2-Trichloroethane 79-00-5 109
1,1-Dichloroethane 75-34-3 106
1,1-Dichloroethene 75-35-4 106
1,2,4-Trichlorobenzene 120-82-1 104
1,2,4-Trimethylbenzene 95-63-6 114
1,2-Dibromoethane (EDB)106-93-4 109
1,2-Dichlorobenzene 95-50-1 107
1,2-Dichloroethane 107-06-2 102
1,2-Dichloropropane 78-87-5 106
1,3,5-Trimethylbenzene 108-67-8 116
1,3-Butadiene 106-99-0 122
1,3-Dichlorobenzene 541-73-1 108
1,4-Dichlorobenzene 106-46-7 108
1,4-Dioxane 123-91-1 106
2,2,4-Trimethylpentane 540-84-1 109
2-Butanone (Methyl Ethyl Ketone)78-93-3 104
2-Hexanone 591-78-6 105
2-Propanol 67-63-0 99
3-Chloropropene 107-05-1 102
4-Ethyltoluene 622-96-8 107
4-Methyl-2-pentanone 108-10-1 109
Acetone 67-64-1 109
Page 37 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 09:22 AM
1.00
msdp.i / p011702
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-10B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
CCV
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
alpha-Chlorotoluene 100-44-7 107
Benzene 71-43-2 107
Bromodichloromethane 75-27-4 106
Bromoform 75-25-2 106
Bromomethane 74-83-9 116
Carbon Disulfide 75-15-0 100
Carbon Tetrachloride 56-23-5 106
Chlorobenzene 108-90-7 107
Chloroethane 75-00-3 102
Chloroform 67-66-3 107
Chloromethane 74-87-3 102
cis-1,2-Dichloroethene 156-59-2 109
cis-1,3-Dichloropropene 10061-01-5 109
Cumene 98-82-8 113
Cyclohexane 110-82-7 109
Dibromochloromethane 124-48-1 107
Ethanol 64-17-5 98
Ethyl Benzene 100-41-4 114
Freon 11 75-69-4 102
Freon 113 76-13-1 101
Freon 114 76-14-2 108
Freon 12 75-71-8 107
Heptane 142-82-5 109
Hexachlorobutadiene 87-68-3 103
Page 38 of 51
Dilution Factor:
Instrument/Filename:
1/17/17 09:22 AM
1.00
msdp.i / p011702
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-10B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
CCV
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
Hexane 110-54-3 112
m,p-Xylene 108-38-3 114
Methyl tert-butyl ether 1634-04-4 98
Methylene Chloride 75-09-2 104
o-Xylene 95-47-6 115
Propylbenzene 103-65-1 108
Styrene 100-42-5 113
Tetrachloroethene 127-18-4 109
Tetrahydrofuran 109-99-9 110
Toluene 108-88-3 107
trans-1,2-Dichloroethene 156-60-5 111
trans-1,3-Dichloropropene 10061-02-6 106
Trichloroethene 79-01-6 107
Vinyl Chloride 75-01-4 107
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 95
4-Bromofluorobenzene 460-00-4 70-130 103
Toluene-d8 2037-26-5 70-130 104
Page 39 of 51
Dilution Factor:
Instrument/Filename:
1/16/17 10:44 AM
1.00
msdp.i / p011603
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
1,1,1-Trichloroethane 71-55-6 95
1,1,2,2-Tetrachloroethane 79-34-5 104
1,1,2-Trichloroethane 79-00-5 105
1,1-Dichloroethane 75-34-3 93
1,1-Dichloroethene 75-35-4 95
1,2,4-Trichlorobenzene 120-82-1 87
1,2,4-Trimethylbenzene 95-63-6 114
1,2-Dibromoethane (EDB)106-93-4 101
1,2-Dichlorobenzene 95-50-1 105
1,2-Dichloroethane 107-06-2 92
1,2-Dichloropropane 78-87-5 99
1,3,5-Trimethylbenzene 108-67-8 115
1,3-Butadiene 106-99-0 114
1,3-Dichlorobenzene 541-73-1 105
1,4-Dichlorobenzene 106-46-7 107
1,4-Dioxane 123-91-1 102
2,2,4-Trimethylpentane 540-84-1 104
2-Butanone (Methyl Ethyl Ketone)78-93-3 94
2-Hexanone 591-78-6 110
2-Propanol 67-63-0 91
3-Chloropropene 107-05-1 93
4-Ethyltoluene 622-96-8 113
4-Methyl-2-pentanone 108-10-1 109
Acetone 67-64-1 98
Page 40 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/16/17 10:44 AM
1.00
msdp.i / p011603
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
alpha-Chlorotoluene 100-44-7 109
Benzene 71-43-2 98
Bromodichloromethane 75-27-4 99
Bromoform 75-25-2 106
Bromomethane 74-83-9 106
Carbon Disulfide 75-15-0 93
Carbon Tetrachloride 56-23-5 101
Chlorobenzene 108-90-7 101
Chloroethane 75-00-3 95
Chloroform 67-66-3 95
Chloromethane 74-87-3 92
cis-1,2-Dichloroethene 156-59-2 89
cis-1,3-Dichloropropene 10061-01-5 105
Cumene 98-82-8 110
Cyclohexane 110-82-7 103
Dibromochloromethane 124-48-1 102
Ethanol 64-17-5 83
Ethyl Benzene 100-41-4 112
Freon 11 75-69-4 91
Freon 113 76-13-1 93
Freon 114 76-14-2 95
Freon 12 75-71-8 97
Heptane 142-82-5 106
Hexachlorobutadiene 87-68-3 89
Page 41 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/16/17 10:44 AM
1.00
msdp.i / p011603
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
Hexane 110-54-3 104
m,p-Xylene 108-38-3 112
Methyl tert-butyl ether 1634-04-4 90
Methylene Chloride 75-09-2 93
o-Xylene 95-47-6 113
Propylbenzene 103-65-1 108
Styrene 100-42-5 119
Tetrachloroethene 127-18-4 102
Tetrahydrofuran 109-99-9 100
Toluene 108-88-3 100
trans-1,2-Dichloroethene 156-60-5 107
trans-1,3-Dichloropropene 10061-02-6 98
Trichloroethene 79-01-6 99
Vinyl Chloride 75-01-4 109
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 93
4-Bromofluorobenzene 460-00-4 70-130 104
Toluene-d8 2037-26-5 70-130 103
Page 42 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/16/17 11:10 AM
1.00
msdp.i / p011604
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11AA
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
1,1,1-Trichloroethane 71-55-6 95
1,1,2,2-Tetrachloroethane 79-34-5 104
1,1,2-Trichloroethane 79-00-5 104
1,1-Dichloroethane 75-34-3 94
1,1-Dichloroethene 75-35-4 94
1,2,4-Trichlorobenzene 120-82-1 102
1,2,4-Trimethylbenzene 95-63-6 114
1,2-Dibromoethane (EDB)106-93-4 102
1,2-Dichlorobenzene 95-50-1 106
1,2-Dichloroethane 107-06-2 91
1,2-Dichloropropane 78-87-5 98
1,3,5-Trimethylbenzene 108-67-8 115
1,3-Butadiene 106-99-0 114
1,3-Dichlorobenzene 541-73-1 106
1,4-Dichlorobenzene 106-46-7 108
1,4-Dioxane 123-91-1 101
2,2,4-Trimethylpentane 540-84-1 105
2-Butanone (Methyl Ethyl Ketone)78-93-3 95
2-Hexanone 591-78-6 111
2-Propanol 67-63-0 92
3-Chloropropene 107-05-1 94
4-Ethyltoluene 622-96-8 114
4-Methyl-2-pentanone 108-10-1 109
Acetone 67-64-1 96
Page 43 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/16/17 11:10 AM
1.00
msdp.i / p011604
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11AA
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
alpha-Chlorotoluene 100-44-7 111
Benzene 71-43-2 98
Bromodichloromethane 75-27-4 98
Bromoform 75-25-2 105
Bromomethane 74-83-9 107
Carbon Disulfide 75-15-0 92
Carbon Tetrachloride 56-23-5 101
Chlorobenzene 108-90-7 101
Chloroethane 75-00-3 96
Chloroform 67-66-3 95
Chloromethane 74-87-3 93
cis-1,2-Dichloroethene 156-59-2 91
cis-1,3-Dichloropropene 10061-01-5 105
Cumene 98-82-8 110
Cyclohexane 110-82-7 104
Dibromochloromethane 124-48-1 101
Ethanol 64-17-5 82
Ethyl Benzene 100-41-4 111
Freon 11 75-69-4 91
Freon 113 76-13-1 94
Freon 114 76-14-2 96
Freon 12 75-71-8 95
Heptane 142-82-5 108
Hexachlorobutadiene 87-68-3 102
Page 44 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/16/17 11:10 AM
1.00
msdp.i / p011604
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11AA
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
Hexane 110-54-3 103
m,p-Xylene 108-38-3 113
Methyl tert-butyl ether 1634-04-4 92
Methylene Chloride 75-09-2 94
o-Xylene 95-47-6 113
Propylbenzene 103-65-1 108
Styrene 100-42-5 118
Tetrachloroethene 127-18-4 100
Tetrahydrofuran 109-99-9 100
Toluene 108-88-3 100
trans-1,2-Dichloroethene 156-60-5 111
trans-1,3-Dichloropropene 10061-02-6 98
Trichloroethene 79-01-6 99
Vinyl Chloride 75-01-4 103
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 95
4-Bromofluorobenzene 460-00-4 70-130 104
Toluene-d8 2037-26-5 70-130 102
Page 45 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/17/17 09:47 AM
1.00
msdp.i / p011703
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
1,1,1-Trichloroethane 71-55-6 96
1,1,2,2-Tetrachloroethane 79-34-5 102
1,1,2-Trichloroethane 79-00-5 103
1,1-Dichloroethane 75-34-3 95
1,1-Dichloroethene 75-35-4 95
1,2,4-Trichlorobenzene 120-82-1 102
1,2,4-Trimethylbenzene 95-63-6 113
1,2-Dibromoethane (EDB)106-93-4 101
1,2-Dichlorobenzene 95-50-1 104
1,2-Dichloroethane 107-06-2 91
1,2-Dichloropropane 78-87-5 97
1,3,5-Trimethylbenzene 108-67-8 116
1,3-Butadiene 106-99-0 116
1,3-Dichlorobenzene 541-73-1 105
1,4-Dichlorobenzene 106-46-7 107
1,4-Dioxane 123-91-1 100
2,2,4-Trimethylpentane 540-84-1 107
2-Butanone (Methyl Ethyl Ketone)78-93-3 97
2-Hexanone 591-78-6 109
2-Propanol 67-63-0 93
3-Chloropropene 107-05-1 96
4-Ethyltoluene 622-96-8 108
4-Methyl-2-pentanone 108-10-1 108
Acetone 67-64-1 96
Page 46 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/17/17 09:47 AM
1.00
msdp.i / p011703
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
alpha-Chlorotoluene 100-44-7 109
Benzene 71-43-2 95
Bromodichloromethane 75-27-4 97
Bromoform 75-25-2 104
Bromomethane 74-83-9 106
Carbon Disulfide 75-15-0 94
Carbon Tetrachloride 56-23-5 101
Chlorobenzene 108-90-7 100
Chloroethane 75-00-3 96
Chloroform 67-66-3 96
Chloromethane 74-87-3 93
cis-1,2-Dichloroethene 156-59-2 92
cis-1,3-Dichloropropene 10061-01-5 105
Cumene 98-82-8 109
Cyclohexane 110-82-7 106
Dibromochloromethane 124-48-1 101
Ethanol 64-17-5 85
Ethyl Benzene 100-41-4 111
Freon 11 75-69-4 93
Freon 113 76-13-1 93
Freon 114 76-14-2 97
Freon 12 75-71-8 98
Heptane 142-82-5 105
Hexachlorobutadiene 87-68-3 101
Page 47 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/17/17 09:47 AM
1.00
msdp.i / p011703
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11B
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
Hexane 110-54-3 105
m,p-Xylene 108-38-3 112
Methyl tert-butyl ether 1634-04-4 93
Methylene Chloride 75-09-2 94
o-Xylene 95-47-6 112
Propylbenzene 103-65-1 106
Styrene 100-42-5 116
Tetrachloroethene 127-18-4 101
Tetrahydrofuran 109-99-9 103
Toluene 108-88-3 98
trans-1,2-Dichloroethene 156-60-5 109
trans-1,3-Dichloropropene 10061-02-6 99
Trichloroethene 79-01-6 100
Vinyl Chloride 75-01-4 107
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 94
4-Bromofluorobenzene 460-00-4 70-130 104
Toluene-d8 2037-26-5 70-130 101
Page 48 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/17/17 10:11 AM
1.00
msdp.i / p011704
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11BB
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
1,1,1-Trichloroethane 71-55-6 96
1,1,2,2-Tetrachloroethane 79-34-5 103
1,1,2-Trichloroethane 79-00-5 103
1,1-Dichloroethane 75-34-3 96
1,1-Dichloroethene 75-35-4 98
1,2,4-Trichlorobenzene 120-82-1 106
1,2,4-Trimethylbenzene 95-63-6 116
1,2-Dibromoethane (EDB)106-93-4 102
1,2-Dichlorobenzene 95-50-1 106
1,2-Dichloroethane 107-06-2 90
1,2-Dichloropropane 78-87-5 97
1,3,5-Trimethylbenzene 108-67-8 114
1,3-Butadiene 106-99-0 114
1,3-Dichlorobenzene 541-73-1 106
1,4-Dichlorobenzene 106-46-7 108
1,4-Dioxane 123-91-1 100
2,2,4-Trimethylpentane 540-84-1 108
2-Butanone (Methyl Ethyl Ketone)78-93-3 98
2-Hexanone 591-78-6 110
2-Propanol 67-63-0 95
3-Chloropropene 107-05-1 99
4-Ethyltoluene 622-96-8 113
4-Methyl-2-pentanone 108-10-1 108
Acetone 67-64-1 98
Page 49 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/17/17 10:11 AM
1.00
msdp.i / p011704
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11BB
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
alpha-Chlorotoluene 100-44-7 110
Benzene 71-43-2 95
Bromodichloromethane 75-27-4 97
Bromoform 75-25-2 105
Bromomethane 74-83-9 108
Carbon Disulfide 75-15-0 94
Carbon Tetrachloride 56-23-5 102
Chlorobenzene 108-90-7 101
Chloroethane 75-00-3 96
Chloroform 67-66-3 97
Chloromethane 74-87-3 95
cis-1,2-Dichloroethene 156-59-2 94
cis-1,3-Dichloropropene 10061-01-5 106
Cumene 98-82-8 110
Cyclohexane 110-82-7 106
Dibromochloromethane 124-48-1 101
Ethanol 64-17-5 85
Ethyl Benzene 100-41-4 112
Freon 11 75-69-4 93
Freon 113 76-13-1 94
Freon 114 76-14-2 98
Freon 12 75-71-8 97
Heptane 142-82-5 106
Hexachlorobutadiene 87-68-3 105
Page 50 of 51
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/17/17 10:11 AM
1.00
msdp.i / p011704
EPA METHOD TO-15 GC/MS FULL SCAN
1701155AR1-11BB
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collected:
Media:
CAS#Compound %Recovery
Hexane 110-54-3 108
m,p-Xylene 108-38-3 113
Methyl tert-butyl ether 1634-04-4 95
Methylene Chloride 75-09-2 95
o-Xylene 95-47-6 114
Propylbenzene 103-65-1 107
Styrene 100-42-5 118
Tetrachloroethene 127-18-4 102
Tetrahydrofuran 109-99-9 104
Toluene 108-88-3 98
trans-1,2-Dichloroethene 156-60-5 112
trans-1,3-Dichloropropene 10061-02-6 99
Trichloroethene 79-01-6 98
Vinyl Chloride 75-01-4 112
D: Analyte not within the DoD scope of accreditation.
CAS#Surrogates Limits %Recovery
1,2-Dichloroethane-d4 17060-07-0 70-130 94
4-Bromofluorobenzene 460-00-4 70-130 102
Toluene-d8 2037-26-5 70-130 101
Page 51 of 51
* % Recovery is calculated using unrounded analytical results.
4/3/2017
Ms. Haley Hindes
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte NC 28206
Project Name: Carolina Foundry
Project #: 71167563
Dear Ms. Haley Hindes
The following report includes the data for the above referenced project for sample(s)
received on 1/13/2017 at Air Toxics Ltd.
The data and associated QC analyzed by Modified ASTM D-1946 are compliant with
the project requirements or laboratory criteria with the exception of the deviations
noted in the attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contact the Project Manager: Ausha Scott at 916-985-1000 if you have any questions
regarding the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1701155BR1
Page 1 of 8
Ms. Haley Hindes
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
WORK ORDER #:1701155BR1
CLIENT:BILL TO:
PHONE:
Accounts Payable
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
704-509-1777
704-509-1888
01/13/2017
DATE COMPLETED:01/24/2017
P.O. #
PROJECT #71167563 Carolina Foundry
Work Order Summary
FAX:
DATE RECEIVED:
DATE REISSUED:04/03/2017
CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
07A SV-07 Modified ASTM D-1946 4.5 "Hg 15 psi
08A Lab Blank Modified ASTM D-1946 NA NA
09A LCS Modified ASTM D-1946 NA NA
09AA LCSD Modified ASTM D-1946 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2016, Expiration date: 10/17/2017.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
04/03/17
Page 2 of 8
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704434-16-11, UT NELAP CA0093332016-7, VA NELAP - 8113, WA NELAP - C935
LABORATORY NARRATIVEModified ASTM D-1946Terracon Consulting EngineersWorkorder# 1701155BR1
One 1 Liter Summa Canister sample was received on January 13, 2017. The laboratory performed
analysis via Modified ASTM Method D-1946 for Helium in air using GC/TCD. The method involves
direct injection of 1.0 mL of sample.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsASTM D-1946
Calibration A single point
calibration is
performed using a
reference standard
closely matching the
composition of the
unknown.
A minimum of 5-point calibration curve is performed.
Quantitation is based on average Response Factor.
Reference Standard The composition of any
reference standard
must be known to
within 0.01 mol % for
any component.
The standards used by ATL are blended to a >/= 95%
accuracy.
Sample Injection Volume Components whose
concentrations are in
excess of 5 % should
not be analyzed by
using sample volumes
greater than 0.5 mL.
The sample container is connected directly to a fixed
volume sample loop of 1.0 mL on the GC. Linear range
is defined by the calibration curve. Bags are loaded by
vacuum.
Normalization Normalize the mole
percent values by
multiplying each value
by 100 and dividing by
the sum of the original
values. The sum of the
original values should
not differ from 100%
by more than 1.0%.
Results are not normalized. The sum of the reported
values can differ from 100% by as much as 15%, either
due to analytical variability or an unusual sample matrix.
Precision Precision requirements
established at each
concentration level.
Duplicates should agree within 25% RPD for detections
> 5 X's the RL.
Receiving Notes
There were no receiving discrepancies.
There were no analytical discrepancies.
Analytical Notes
Page 3 of 8
Per client request, the workorder was reissued on 4/3/2017 to report estimated values for target
compound hits that are below the reporting limit but greater than the method detection limit.
Seven qualifiers may have been used on the data analysis sheets and indicate as follows:
B - Compound present in laboratory blank greater than reporting limit.
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the detection limit.
M - Reported value may be biased due to apparent matrix interferences.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 4 of 8
Dilution Factor:
Instrument/Filename:
1/16/17 12:02 PM
2.38
gc10.i / 10011606c
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
1701155BR1-07A
1/10/17 06:52 PM
1 Liter Summa Canister
Carolina Foundry
SV-07
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collecte
Media:
(%)CAS#
LOD
Compound (%)
MDL Rpt. Limit
(%)
Amount
(%)
Helium 7440-59-7 0.120 0.370.012
Page 5 of 8
Dilution Factor:
Instrument/Filename:
1/16/17 08:51 AM
1.00
gc10.i / 10011603c
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
1701155BR1-08A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
Lab Blank
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collecte
Media:
(%)CAS#
LOD
Compound (%)
MDL Rpt. Limit
(%)
Amount
(%)
Helium 7440-59-7 0.0500 Not Detected0.0050
Page 6 of 8
Dilution Factor:
Instrument/Filename:
1/16/17 07:36 AM
1.00
gc10.i / 10011602c
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
1701155BR1-09A
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCS
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collecte
Media:
CAS#Compound %Recovery
Helium 7440-59-7 101
Page 7 of 8
* % Recovery is calculated using unrounded analytical results.
Dilution Factor:
Instrument/Filename:
1/16/17 02:06 PM
1.00
gc10.i / 10011611c
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
1701155BR1-09AA
NA - Not Applicable
NA - Not Applicable
Carolina Foundry
LCSD
Date/Time Analyzed:
Client ID:
Lab ID:
Date/Time Collecte
Media:
CAS#Compound %Recovery
Helium 7440-59-7 102
Page 8 of 8
* % Recovery is calculated using unrounded analytical results.
APPENDIX C – BROWNFIELDS RISK CALCULATORS
Brownfields Soil Risk Calculators (Residential)
Brownfields Groundwater Concentration to Indoor Air Risk Calculator (Residential)
Brownfields Soil Vapor Concentration to Indoor Air Concentration Risk Calculator
(Residential)
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+05 Acetone 67-64-1 1.22E+04 N 1.51E-02 --2.48E-07
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0568 9.96E-10 1.62E-04
~Methylnaphthalene, 2-91-57-6 4.80E+01 N 0.164 --6.83E-04
~Naphthalene 91-20-3 3.80E+00 C 0.0121 3.18E-09 9.31E-05
2.2E+02 Trimethylbenzene, 1,2,4-95-63-6 1.16E+01 N 0.0056 --9.66E-05
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
4.2E-09 1.0E-03
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: SS-1
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+02 Butylbenzene, n-104-51-8 7.80E+02 N 0.139 --3.56E-05
1.5E+02 Butylbenzene, sec-135-98-8 1.56E+03 N 0.0927 --1.19E-05
~Fluorene 86-73-7 4.80E+02 N 0.202 --8.42E-05
3.9E+02 ~Methylnaphthalene, 1-90-12-0 1.80E+01 C 0.616 3.42E-08 1.47E-04
~Methylnaphthalene, 2-91-57-6 4.80E+01 N 0.727 --3.03E-03
~Naphthalene 91-20-3 3.80E+00 C 0.456 1.20E-07 3.51E-03
~Pyrene 129-00-0 3.60E+02 N 0.132 --7.33E-05
2.6E+02 Propyl benzene 103-65-1 7.60E+02 N 0.0646 --1.70E-05
2.2E+02 Trimethylbenzene, 1,2,4-95-63-6 1.16E+01 N 0.635 --1.09E-02
1.8E+02 Trimethylbenzene, 1,3,5-108-67-8 1.56E+02 N 0.169 --2.17E-04
2.6E+02 Xylenes 1330-20-7 1.16E+02 N 0.0641 --1.11E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
1.5E-07 1.8E-02
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: SS-2
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Arsenic, Inorganic 7440-38-2 6.80E-01 C 5.1 7.50E-06 1.46E-01
Barium 7440-39-3 3.00E+03 N 74 --4.93E-03
Chromium, Total 7440-47-3 -- N 31 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 65 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.9 --8.18E-02
~Benz[a]anthracene 56-55-3 1.60E-01 C,M 0.3 1.88E-06 --
~Benzo[a]pyrene 50-32-8 1.60E-02 C,M 0.33 2.06E-05 --
~Benzo[b]fluoranthene 205-99-2 1.60E-01 C,M 0.41 2.56E-06 --
~Benzo[k]fluoranthene 207-08-9 1.60E+00 C,M 0.2 1.25E-07 --
~Chrysene 218-01-9 1.60E+01 C,M 0.31 1.94E-08 --
~Fluoranthene 206-44-0 4.80E+02 N 0.59 --2.46E-04
~Indeno[1,2,3-cd]pyrene 193-39-5 1.60E-01 C,M 0.21 1.31E-06 --
~Pyrene 129-00-0 3.60E+02 N 0.54 --3.00E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
3.4E-05 2.3E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-1
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+05 Acetone 67-64-1 1.22E+04 N 1.20E-01 --1.97E-06
Arsenic, Inorganic 7440-38-2 6.80E-01 C 5.7 8.38E-06 1.63E-01
Barium 7440-39-3 3.00E+03 N 94 --6.27E-03
Cadmium (Water)7440-43-9 -- N 0.3 ----
Chromium, Total 7440-47-3 -- N 69 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 120 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.41 --3.73E-02
~Acenaphthene 83-32-9 7.20E+02 N 0.23 --6.39E-05
~Anthracene 120-12-7 3.60E+03 N 0.23 --1.28E-05
~Benz[a]anthracene 56-55-3 1.60E-01 C,M 0.65 4.06E-06 --
~Benzo[a]pyrene 50-32-8 1.60E-02 C,M 0.71 4.44E-05 --
~Benzo[b]fluoranthene 205-99-2 1.60E-01 C,M 0.89 5.56E-06 --
~Benzo[k]fluoranthene 207-08-9 1.60E+00 C,M 0.45 2.81E-07 --
~Chrysene 218-01-9 1.60E+01 C,M 0.67 4.19E-08 --
~Fluoranthene 206-44-0 4.80E+02 N 1.2 --5.00E-04
~Indeno[1,2,3-cd]pyrene 193-39-5 1.60E-01 C,M 0.44 2.75E-06 --
~Pyrene 129-00-0 3.60E+02 N 1.2 --6.67E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
6.5E-05 2.1E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-2
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Arsenic, Inorganic 7440-38-2 6.80E-01 C 1.9 2.79E-06 5.43E-02
Barium 7440-39-3 3.00E+03 N 49 --3.27E-03
1.1E+02 Butylbenzene, n-104-51-8 7.80E+02 N 0.16 --4.10E-05
1.5E+02 Butylbenzene, sec-135-98-8 1.56E+03 N 0.13 --1.67E-05
Chromium, Total 7440-47-3 -- N 32 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 4.7 --NA
~Fluorene 86-73-7 4.80E+02 N 0.35 --1.46E-04
3.9E+02 ~Methylnaphthalene, 1-90-12-0 1.80E+01 C 1.9 1.06E-07 4.52E-04
~Methylnaphthalene, 2-91-57-6 4.80E+01 N 2.7 --1.13E-02
~Naphthalene 91-20-3 3.80E+00 C 0.54 1.42E-07 4.15E-03
~Pyrene 129-00-0 3.60E+02 N 0.16 --8.89E-05
2.2E+02 Trimethylbenzene, 1,2,4-95-63-6 1.16E+01 N 0.85 --1.47E-02
1.8E+02 Trimethylbenzene, 1,3,5-108-67-8 1.56E+02 N 0.29 --3.72E-04
4.3E+02 Xylene, o-95-47-6 1.30E+02 N 0.091 --1.40E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
3.0E-06 8.9E-02
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-4
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Arsenic, Inorganic 7440-38-2 6.80E-01 C 2.1 3.09E-06 6.00E-02
Barium 7440-39-3 3.00E+03 N 49 --3.27E-03
1.5E+02 Butylbenzene, sec-135-98-8 1.56E+03 N 0.012 --1.54E-06
Chromium, Total 7440-47-3 -- N 30 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 11 --NA
3.9E+02 ~Methylnaphthalene, 1-90-12-0 1.80E+01 C 0.37 2.06E-08 8.81E-05
~Pyrene 129-00-0 3.60E+02 N 0.13 --7.22E-05
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
3.1E-06 6.3E-02
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-5
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.1 4.56E-06 8.86E-02
Barium 7440-39-3 3.00E+03 N 100 --6.67E-03
1.5E+02 Butylbenzene, sec-135-98-8 1.56E+03 N 0.13 --1.67E-05
Chromium, Total 7440-47-3 -- N 46 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 15 --NA
3.9E+02 ~Methylnaphthalene, 1-90-12-0 1.80E+01 C 0.61 3.39E-08 1.45E-04
~Methylnaphthalene, 2-91-57-6 4.80E+01 N 0.86 --3.58E-03
~Naphthalene 91-20-3 3.80E+00 C 0.5 1.32E-07 3.85E-03
2.6E+02 Propyl benzene 103-65-1 7.60E+02 N 0.097 --2.55E-05
2.2E+02 Trimethylbenzene, 1,2,4-95-63-6 1.16E+01 N 0.6 --1.03E-02
1.8E+02 Trimethylbenzene, 1,3,5-108-67-8 1.56E+02 N 0.2 --2.56E-04
4.3E+02 Xylene, o-95-47-6 1.30E+02 N 0.089 --1.37E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
4.7E-06 1.1E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-5A
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Arsenic, Inorganic 7440-38-2 6.80E-01 C 2.3 3.38E-06 6.57E-02
Barium 7440-39-3 3.00E+03 N 24 --1.60E-03
Chromium, Total 7440-47-3 -- N 31 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 11 --NA
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
3.4E-06 6.7E-02
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-6
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Arsenic, Inorganic 7440-38-2 6.80E-01 C 2.4 3.53E-06 6.86E-02
Barium 7440-39-3 3.00E+03 N 40 --2.67E-03
Chromium, Total 7440-47-3 -- N 38 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 9.7 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.037 --3.36E-03
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
3.5E-06 7.5E-02
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-7
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+05 Acetone 67-64-1 1.22E+04 N 1.50E-01 --2.46E-06
Arsenic, Inorganic 7440-38-2 6.80E-01 C 4.9 7.21E-06 1.40E-01
Barium 7440-39-3 3.00E+03 N 150 --1.00E-02
Chromium, Total 7440-47-3 -- N 41 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 17 --NA
2.8E+04 Methyl Ethyl Ketone (2-Butanone)78-93-3 5.40E+03 N 0.017 --6.30E-07
~Naphthalene 91-20-3 3.80E+00 C 0.0039 1.03E-09 3.00E-05
Zinc and Compounds 7440-66-6 4.60E+03 N 67.3 --2.93E-03
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
7.2E-06 1.5E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-9
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+05 Acetone 67-64-1 1.22E+04 N 5.30E-02 --8.69E-07
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.3 4.85E-06 9.43E-02
Barium 7440-39-3 3.00E+03 N 47 --3.13E-03
Chromium, Total 7440-47-3 -- N 38 ----
~Lead and Compounds 7439-92-1 4.00E+02 N 11 --NA
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
4.9E-06 9.7E-02
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-10
Page 1 of 1
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+05 Acetone 67-64-1 1.22E+04 N 6.30E-03 --1.03E-07
Aluminum 7429-90-5 1.54E+04 N 11000 --1.43E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.9 5.74E-06 1.11E-01
Barium 7440-39-3 3.00E+03 N 44.1 --2.94E-03
Chromium, Total 7440-47-3 -- N 23.2 ----
Copper 7440-50-8 6.20E+02 N 69.6 --2.25E-02
~Lead and Compounds 7439-92-1 4.00E+02 N 15.9 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.044 --4.00E-03
~Naphthalene 91-20-3 3.80E+00 C 0.0039 1.03E-09 3.00E-05Zinc and Compounds 7440-66-6 4.60E+03 N 67.3 --2.93E-03
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
5.7E-06 2.9E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-11
Page 1 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 11000 --1.43E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 4.6 6.76E-06 1.31E-01
Barium 7440-39-3 3.00E+03 N 72.9 --4.86E-03
Cadmium (Water)7440-43-9 -- N 0.069 ----
Chromium, Total 7440-47-3 -- N 26.2 ----
Copper 7440-50-8 6.20E+02 N 57.1 --1.84E-02
~Lead and Compounds 7439-92-1 4.00E+02 N 81.8 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.063 --5.73E-03
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0043 7.54E-11 1.23E-05
~Benz[a]anthracene 56-55-3 1.60E-01 C,M 0.172 1.08E-06 --
~Benzo[a]pyrene 50-32-8 1.60E-02 C,M 0.179 1.12E-05 --
~Benzo[b]fluoranthene 205-99-2 1.60E-01 C,M 0.239 1.49E-06 --
~Benzo[k]fluoranthene 207-08-9 1.60E+00 C,M 0.106 6.63E-08 --
~Chrysene 218-01-9 1.60E+01 C,M 0.172 1.08E-08 --
~Fluoranthene 206-44-0 4.80E+02 N 0.354 --1.48E-04
~Indeno[1,2,3-cd]pyrene 193-39-5 1.60E-01 C,M 0.112 7.00E-07 --
~Pyrene 129-00-0 3.60E+02 N 0.278 --1.54E-04
Silver 7440-22-4 7.80E+01 N 0.26 --6.67E-04Zinc and Compounds 7440-66-6 4.60E+03 N 74.2 --3.23E-03
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
2.1E-05 3.1E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-12
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 15300 --1.99E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 2.9 4.26E-06 8.29E-02
Barium 7440-39-3 3.00E+03 N 59.9 --3.99E-03
Chromium, Total 7440-47-3 -- N 24.1 ----
Copper 7440-50-8 6.20E+02 N 12.3 --3.97E-03
~Lead and Compounds 7439-92-1 4.00E+02 N 11.5 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.011 --1.00E-03
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0063 1.11E-10 1.80E-05Zinc and Compounds 7440-66-6 4.60E+03 N 8.4 --3.65E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
4.3E-06 2.9E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-13
Page 3 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 10500 --1.36E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.6 5.29E-06 1.03E-01
Barium 7440-39-3 3.00E+03 N 17.5 --1.17E-03
Chromium, Total 7440-47-3 -- N 35.7 ----
Copper 7440-50-8 6.20E+02 N 19 --6.13E-03
~Lead and Compounds 7439-92-1 4.00E+02 N 11.3 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.1 --9.09E-03
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0063 1.11E-10 1.80E-05Zinc and Compounds 7440-66-6 4.60E+03 N 14.3 --6.22E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
5.3E-06 2.6E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-14
Page 4 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 9880 --1.28E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.6 5.29E-06 1.03E-01
Barium 7440-39-3 3.00E+03 N 22.9 --1.53E-03
Chromium, Total 7440-47-3 -- N 25.2 ----
Copper 7440-50-8 6.20E+02 N 18.1 --5.84E-03
~Lead and Compounds 7439-92-1 4.00E+02 N 21.8 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.065 --5.91E-03
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0057 1.00E-10 1.63E-05
~Fluoranthene 206-44-0 4.80E+02 N 0.0737 --3.07E-05Zinc and Compounds 7440-66-6 4.60E+03 N 13.7 --5.96E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
5.3E-06 2.5E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-15
Page 5 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
1.1E+05 Acetone 67-64-1 1.22E+04 N 1.10E-02 --1.80E-07
Aluminum 7429-90-5 1.54E+04 N 14300 --1.86E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.3 4.85E-06 9.43E-02
Barium 7440-39-3 3.00E+03 N 24.1 --1.61E-03
Cadmium (Water)7440-43-9 -- N 0.088 ----
Chromium, Total 7440-47-3 -- N 30.8 ----
Copper 7440-50-8 6.20E+02 N 21 --6.77E-03
~Lead and Compounds 7439-92-1 4.00E+02 N 15.6 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.051 --4.64E-03
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0114 2.00E-10 3.26E-05
Silver 7440-22-4 7.80E+01 N 0.47 --1.21E-03
Zinc and Compounds 7440-66-6 4.60E+03 N 12.2 --5.30E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
4.9E-06 2.9E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: S-16
Page 6 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 10500 --1.36E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 3.6 5.29E-06 1.03E-01
Barium 7440-39-3 3.00E+03 N 17.5 --1.17E-03
Chromium, Total 7440-47-3 -- N 35.7 ----
Copper 7440-50-8 6.20E+02 N 19 --6.13E-03
~Lead and Compounds 7439-92-1 4.00E+02 N 11.3 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.1 --9.09E-03
3.3E+03 Methylene Chloride 75-09-2 5.70E+01 C,M 0.0063 1.11E-10 1.80E-05Zinc and Compounds 7440-66-6 4.60E+03 N 14.3 --6.22E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
5.3E-06 2.6E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: DUP-01-011117
Page 7 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 7650 --9.94E-02
Arsenic, Inorganic 7440-38-2 6.80E-01 C 4.2 6.18E-06 1.20E-01
Barium 7440-39-3 3.00E+03 N 88 --5.87E-03
Cadmium (Water)7440-43-9 -- N 0.74 ----
Chromium, Total 7440-47-3 -- N 32.5 ----
Copper 7440-50-8 6.20E+02 N 1270 --4.10E-01
~Lead and Compounds 7439-92-1 4.00E+02 N 201 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.12 --1.09E-02
Silver 7440-22-4 7.80E+01 N 0.59 --1.51E-03Zinc and Compounds 7440-66-6 4.60E+03 N 586 --2.55E-02
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
6.2E-06 6.7E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: BG-01
Page 8 of 21
IHSB-BROWNFIELDS Residential Soil Risk Calculator (November 2015 RSL)
Csat
(mg/kg)
Contaminant CAS No.Preliminary Residential
Health Based Soil
Remediation Goal (PSRG)
(mg/kg)
Basis Site Soil
Concentration
(mg/kg)
Cancer Risk Non -Cancer
HQ
Sample Location
Aluminum 7429-90-5 1.54E+04 N 8900 --1.16E-01
Arsenic, Inorganic 7440-38-2 6.80E-01 C 4.4 6.47E-06 1.26E-01
Barium 7440-39-3 3.00E+03 N 16.7 --1.11E-03
Chromium, Total 7440-47-3 -- N 32.7 ----
Copper 7440-50-8 6.20E+02 N 17 --5.48E-03
~Lead and Compounds 7439-92-1 4.00E+02 N 8.5 --NA
3.1E+00 ~Mercury (elemental)7439-97-6 2.20E+00 N 0.071 --6.45E-03
Zinc and Compounds 7440-66-6 4.60E+03 N 9 --3.91E-04
The concentration in the PSRG Column must be
compared to the Csat and the lower of the two is
the final health-based PSRG. N= Non-Carcinogenic
Effect; C=Carcinogenic Effect; M = Mutagenic
Effect. Cancer risk greater than 1.0E+02 is outside
model predictive range.
Sum of
Risk/Hazard
Quotient
6.5E-06 2.5E-01
Carolina Foundry, Charlotte, NC Terracon Project No. 71167563 Sample ID: BG-02
Page 9 of 21
xx Groundwater Concentration to Indoor Air Concentration (GWC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value Instructions
x Exposure Scenario Scenario Residential Select residential or commercial scenario from pull down list
x Target Risk for Carcinogens TCR 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ 0.2
Average Groundwater Temperature (oC)Tgw 25 Enter average of the stabilized groundwater temperature to correct Henry's Law Constant for groundwater target concentrations
x
x
Site
Groundwater
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Cgw Cia IUR RfC
x CAS Chemical Name (ug/L)(ug/m3)(ug/m3)-1 (mg/m3)i
75-09-2 Methylene Chloride 2.0E+00 2.66E-01 2.6E-09 4.2E-04 9.42E+02 1.00E-08 I 6.00E-01 I Mut100-42-5 Styrene 3.0E-01 3.37E-02 No IUR 3.2E-05 1.86E+03 1.00E+00 ICumulative2.6E-09 4.57E-04
Risk/Cumulative
HQ
Notes:_______________
(1)Inhalation Pathway Exposure Parameters (RME):______________
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_GW 70 ATc_C_GW 70 ATc_GW 70
Averaging time for non-carcinogens (yrs)ATnc_R_GW 26 ATnc_C_GW 25 Atnc_GW 26
Exposure duration (yrs)ED_R_GW 26 ED_C_GW 25 ED_GW 26
Exposure frequency (days/yr)EF_R_GW 350 EF_C_GW 250 EF_GW 350
Exposure time (hr/day)ET_R_GW 24 ET_C_GW 8 ET_GW 24
(2)Generic Attenuation Factors:
Source Medium of Vapors Symbol Value Symbol Value Symbol Value
Groundwater ( - )AFgw_R_GW 0.001 AFgw_C_GW 0.001 AFgw_GW 0.001
Sub-Slab and Exterior Soil Gas ( - )AFss_R_GW 0.03 AFss_C_GW 0.01 AFss_GW 0.03
(3)Formulas
Cia, target = MIN( Cia,c; Cia,nc)
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_GW 1.00E-06 mIURTCE_C_GW 0.00E+00 mIURTCE_GW 1.00E-06
IURTCE_R_GW 3.10E-06 IURTCE_C_GW 4.10E-06 IURTCE_GW 3.10E-06
Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:
0 - 2 years 22 - 6 years 46 - 16 years 10
16 - 26 years 10
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.aspH = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtmlS = See RSL User Guide, Section 5X = PPRTV AppendixMut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
3
1
72
Residential Commercial Selected (based onscenario)
Note: This section applies to trichloroethylene and other mutagenic
chemicals, but not to vinyl chloride.
Age Cohort ExposureDuration Age-dependent adjustmentfactor10
3
HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based onscenario)
Residential Commercial Selected (based onscenario)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563GW-02
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
GroundwaterScreeningLevel (ug/l)
IURSource*RFCSource*
Mutagenic
Indicator
CR
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
xx Groundwater Concentration to Indoor Air Concentration (GWC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value Instructions
x Exposure Scenario Scenario Residential Select residential or commercial scenario from pull down list
x Target Risk for Carcinogens TCR 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ 0.2
Average Groundwater Temperature (oC)Tgw 25 Enter average of the stabilized groundwater temperature to correct Henry's Law Constant for groundwater target concentrations
x
x
Site
Groundwater
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Cgw Cia IUR RfC
x CAS Chemical Name (ug/L)(ug/m3)(ug/m3)-1 (mg/m3)i
75-09-2 Methylene Chloride 1.9E+00 2.52E-01 2.5E-09 4.0E-04 9.42E+02 1.00E-08 I 6.00E-01 I MutCumulative2.5E-09 4.03E-04
Risk/Cumulative
HQ
Notes:_______________
(1)Inhalation Pathway Exposure Parameters (RME):______________
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_GW 70 ATc_C_GW 70 ATc_GW 70
Averaging time for non-carcinogens (yrs)ATnc_R_GW 26 ATnc_C_GW 25 Atnc_GW 26
Exposure duration (yrs)ED_R_GW 26 ED_C_GW 25 ED_GW 26Exposure frequency (days/yr)EF_R_GW 350 EF_C_GW 250 EF_GW 350
Exposure time (hr/day)ET_R_GW 24 ET_C_GW 8 ET_GW 24
(2)Generic Attenuation Factors:
Source Medium of Vapors Symbol Value Symbol Value Symbol Value
Groundwater ( - )AFgw_R_GW 0.001 AFgw_C_GW 0.001 AFgw_GW 0.001
Sub-Slab and Exterior Soil Gas ( - )AFss_R_GW 0.03 AFss_C_GW 0.01 AFss_GW 0.03
(3)Formulas
Cia, target = MIN( Cia,c; Cia,nc)
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)
Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_GW 1.00E-06 mIURTCE_C_GW 0.00E+00 mIURTCE_GW 1.00E-06
IURTCE_R_GW 3.10E-06 IURTCE_C_GW 4.10E-06 IURTCE_GW 3.10E-06
Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:
0 - 2 years 22 - 6 years 46 - 16 years 1016 - 26 years 10
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.asp
H = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtmlS = See RSL User Guide, Section 5X = PPRTV AppendixMut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.
Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
3
1
72
Residential Commercial Selected (based onscenario)
Note: This section applies to trichloroethylene and other mutagenicchemicals, but not to vinyl chloride.
Age Cohort ExposureDuration Age-dependent adjustment
factor103
HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based onscenario)
Residential Commercial Selected (based on
scenario)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563GW-03
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
GroundwaterScreeningLevel (ug/l)
IURSource*RFCSource*
Mutagenic
Indicator
CR
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
xx Groundwater Concentration to Indoor Air Concentration (GWC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value Instructions
x Exposure Scenario Scenario Residential Select residential or commercial scenario from pull down list
x Target Risk for Carcinogens TCR 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ 0.2
Average Groundwater Temperature (oC)Tgw 25 Enter average of the stabilized groundwater temperature to correct Henry's Law Constant for groundwater target concentrations
x
x
Site
Groundwater
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Cgw Cia IUR RfC
x CAS Chemical Name (ug/L)(ug/m3)(ug/m3)-1 (mg/m3)i
75-09-2 Methylene Chloride 2.0E+00 2.66E-01 2.6E-09 4.2E-04 9.42E+02 1.00E-08 I 6.00E-01 I Mut100-42-5 Styrene 3.9E-01 4.38E-02 No IUR 4.2E-05 1.86E+03 1.00E+00 ICumulative2.6E-09 4.67E-04
Risk/Cumulative
HQ
Notes:_______________
(1)Inhalation Pathway Exposure Parameters (RME):______________
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_GW 70 ATc_C_GW 70 ATc_GW 70
Averaging time for non-carcinogens (yrs)ATnc_R_GW 26 ATnc_C_GW 25 Atnc_GW 26
Exposure duration (yrs)ED_R_GW 26 ED_C_GW 25 ED_GW 26
Exposure frequency (days/yr)EF_R_GW 350 EF_C_GW 250 EF_GW 350
Exposure time (hr/day)ET_R_GW 24 ET_C_GW 8 ET_GW 24
(2)Generic Attenuation Factors:
Source Medium of Vapors Symbol Value Symbol Value Symbol Value
Groundwater ( - )AFgw_R_GW 0.001 AFgw_C_GW 0.001 AFgw_GW 0.001
Sub-Slab and Exterior Soil Gas ( - )AFss_R_GW 0.03 AFss_C_GW 0.01 AFss_GW 0.03
(3)Formulas
Cia, target = MIN( Cia,c; Cia,nc)
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_GW 1.00E-06 mIURTCE_C_GW 0.00E+00 mIURTCE_GW 1.00E-06
IURTCE_R_GW 3.10E-06 IURTCE_C_GW 4.10E-06 IURTCE_GW 3.10E-06
Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:
0 - 2 years 22 - 6 years 46 - 16 years 10
16 - 26 years 10
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.aspH = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtmlS = See RSL User Guide, Section 5X = PPRTV AppendixMut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
3
1
72
Residential Commercial Selected (based onscenario)
Note: This section applies to trichloroethylene and other mutagenic
chemicals, but not to vinyl chloride.
Age Cohort ExposureDuration Age-dependent adjustmentfactor10
3
HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based onscenario)
Residential Commercial Selected (based onscenario)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563DUP-02-011117
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
GroundwaterScreeningLevel (ug/l)
IURSource*RFCSource*
Mutagenic
Indicator
CR
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
78-87-5 Dichloropropane, 1,2-7.2E+00 2.16E-01 7.7E-07 5.2E-02 2.78E+01 1.00E-05 CA 4.00E-03 I108-88-3 Toluene 9.3E+00 2.79E-01 No IUR 5.4E-05 3.48E+04 5.00E+00 I
Risk/Cumulative HQ 7.7E-07 5.18E-02
Risk/Cumulative HQ
(1)Inhalation Pathway Exposure Parameters (RME):
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_SG 70 ATc_C_SG 70 ATc_SG 70Averaging time for non-carcinogens (yrs)ATnc_R_SG 26 ATnc_C_SG 25 ATnc_SG 26
Exposure duration (yrs)ED_R_SG 26 ED_C_SG 25 ED_SG 26
Exposure frequency (days/yr)EF_R_SG 350 EF_C_SG 250 EF_SG 350Exposure time (hr/day)ET_R_SG 24 ET_C_SG 8 ET_SG 24
(2)Generic Attenuation Factors:
Source Medium of Vapors .Symbol Value Symbol Value Symbol Value
Groundwater ( - )AFgw_R_SG 0.001 AFgw_C_SG 0.001 AFgw_SG 0.001
Sub-Slab and Exterior Soil Gas ( - )AFss_R_SG 0.03 AFss_C_SG 0.01 AFss_SG 0.03
(3)Formulas .
Cia, target = MIN( Cia,c; Cia,nc).Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)
Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_SG 1.00E-06 mIURTCE_C_SG 0.00E+00 mIURTCE_SG 1.00E-06IURTCE_R_SG 3.10E-06 IURTCE_C_SG 4.10E-06 IURTCE_SG 3.10E-06
.Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:
.
0 - 2 years 2
2 - 6 years 4
.6 - 16 years 10
16 - 26 years 10
.Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
.
Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:.
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtmlA = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.asp
H = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtml
S = See RSL User Guide, Section 5
X = PPRTV AppendixMut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.
Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.
Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
SV-01
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0Unacceptable
Residential Commercial Selected (based on
scenario)
Residential Commercial Selected (based on
scenario)
Selected (based on
scenario)
Note: This section applies to trichloroethylene and other mutagenic
chemicals, but not to vinyl chloride.
Age Cohort Exposure
Duration
Age-dependent adjustment
factor10
33
1
72
Residential Commercial
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
67-64-1 Acetone 7.1E+01 2.13E+00 No IUR 6.6E-05 2.16E+05 3.10E+01 ARisk/Cumulative HQ 0.0E+00 6.59E-05
Risk/Cumulative HQ
(1)Inhalation Pathway Exposure Parameters (RME):
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_SG 70 ATc_C_SG 70 ATc_SG 70
Averaging time for non-carcinogens (yrs)ATnc_R_SG 26 ATnc_C_SG 25 ATnc_SG 26Exposure duration (yrs)ED_R_SG 26 ED_C_SG 25 ED_SG 26Exposure frequency (days/yr)EF_R_SG 350 EF_C_SG 250 EF_SG 350
Exposure time (hr/day)ET_R_SG 24 ET_C_SG 8 ET_SG 24
(2)Generic Attenuation Factors:
Source Medium of Vapors .Symbol Value Symbol Value Symbol ValueGroundwater( - )AFgw_R_SG 0.001 AFgw_C_SG 0.001 AFgw_SG 0.001Sub-Slab and Exterior Soil Gas ( - )AFss_R_SG 0.03 AFss_C_SG 0.01 AFss_SG 0.03
(3)Formulas .
Cia, target = MIN( Cia,c; Cia,nc).
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_SG 1.00E-06 mIURTCE_C_SG 0.00E+00 mIURTCE_SG 1.00E-06
IURTCE_R_SG 3.10E-06 IURTCE_C_SG 4.10E-06 IURTCE_SG 3.10E-06
.
Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:.
0 - 2 years 22 - 6 years 4
.6 - 16 years 1016 - 26 years 10
.
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
.Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:.
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.htmlCA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.asp
H = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtml
S = See RSL User Guide, Section 5
X = PPRTV Appendix
Mut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.
Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.
Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
SV-02
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based on
scenario)
Residential Commercial Selected (based on
scenario)
Selected (based on
scenario)
Note: This section applies to trichloroethylene and other mutagenicchemicals, but not to vinyl chloride.
Age Cohort Exposure
Duration
Age-dependent adjustment
factor
10
3
31
72
Residential Commercial
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
67-64-1 Acetone 1.2E+03 3.60E+01 No IUR 1.1E-03 2.16E+05 3.10E+01 A71-43-2 Benzene 8.3E+01 2.49E+00 6.9E-06 8.0E-02 1.20E+02 7.80E-06 I 3.00E-02 I
75-15-0 Carbon Disulfide 1.0E+02 3.00E+00 No IUR 4.1E-03 4.87E+03 7.00E-01 I110-82-7 Cyclohexane 6.8E+00 2.04E-01 No IUR 3.3E-05 4.17E+04 6.00E+00 I
100-41-4 Ethylbenzene 4.5E+01 1.35E+00 1.2E-06 1.3E-03 3.74E+02 2.50E-06 CA 1.00E+00 I
110-54-3 Hexane, N-5.3E+01 1.59E+00 No IUR 2.2E-03 4.87E+03 7.00E-01 I591-78-6 Hexanone, 2-4.9E+01 1.47E+00 No IUR 4.7E-02 2.09E+02 3.00E-02 I
67-63-0 Isopropanol 2.5E+01 7.50E-01 No IUR 3.6E-03 1.39E+03 2.00E-01 P78-93-3 Methyl Ethyl Ketone (2-Butanone)2.8E+02 8.40E+00 No IUR 1.6E-03 3.48E+04 5.00E+00 I
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)3.2E+01 9.60E-01 No IUR 3.1E-04 2.09E+04 3.00E+00 I
103-65-1 Propyl benzene 1.1E+01 3.30E-01 No IUR 3.2E-04 6.95E+03 1.00E+00 X100-42-5 Styrene 9.1E+00 2.73E-01 No IUR 2.6E-04 6.95E+03 1.00E+00 I
108-88-3 Toluene 1.8E+02 5.40E+00 No IUR 1.0E-03 3.48E+04 5.00E+00 I95-63-6 Trimethylbenzene, 1,2,4-4.0E+01 1.20E+00 No IUR 1.6E-01 4.87E+01 7.00E-03 P
95-47-6 Xylene, o-5.4E+01 1.62E+00 No IUR 1.6E-02 6.95E+02 1.00E-01 S
1330-20-7 Xylenes 1.1E+02 3.30E+00 No IUR 3.2E-02 6.95E+02 1.00E-01 IRisk/Cumulative HQ 8.1E-06 3.54E-01
Risk/Cumulative HQ
(1)Inhalation Pathway Exposure Parameters (RME):
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_SG 70 ATc_C_SG 70 ATc_SG 70
Averaging time for non-carcinogens (yrs)ATnc_R_SG 26 ATnc_C_SG 25 ATnc_SG 26Exposure duration (yrs)ED_R_SG 26 ED_C_SG 25 ED_SG 26Exposure frequency (days/yr)EF_R_SG 350 EF_C_SG 250 EF_SG 350
Exposure time (hr/day)ET_R_SG 24 ET_C_SG 8 ET_SG 24
(2)Generic Attenuation Factors:
Source Medium of Vapors .Symbol Value Symbol Value Symbol ValueGroundwater( - )AFgw_R_SG 0.001 AFgw_C_SG 0.001 AFgw_SG 0.001Sub-Slab and Exterior Soil Gas ( - )AFss_R_SG 0.03 AFss_C_SG 0.01 AFss_SG 0.03
(3)Formulas .
Cia, target = MIN( Cia,c; Cia,nc).
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_SG 1.00E-06 mIURTCE_C_SG 0.00E+00 mIURTCE_SG 1.00E-06
IURTCE_R_SG 3.10E-06 IURTCE_C_SG 4.10E-06 IURTCE_SG 3.10E-06
.
Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:.
0 - 2 years 22 - 6 years 4
.6 - 16 years 1016 - 26 years 10
.
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
.Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:.
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
SV-04
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based on
scenario)
Residential Commercial Selected (based on
scenario)
Selected (based on
scenario)
Note: This section applies to trichloroethylene and other mutagenicchemicals, but not to vinyl chloride.
Age Cohort Exposure
Duration
Age-dependent adjustment
factor
10
3
31
72
Residential Commercial
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 2
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
SV-04
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.aspH = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtml
S = See RSL User Guide, Section 5
X = PPRTV Appendix
Mut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.
Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
VISL Calculator Version 3.4.5, November 2015 RSLs Page 2 of 2
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
67-64-1 Acetone 5.5E+01 1.65E+00 No IUR 5.1E-05 2.16E+05 3.10E+01 A108-88-3 Toluene 6.9E+00 2.07E-01 No IUR 4.0E-05 3.48E+04 5.00E+00 I
95-63-6 Trimethylbenzene, 1,2,4-8.0E+01 2.40E+00 No IUR 3.3E-01 4.87E+01 7.00E-03 PRisk/Cumulative HQ 0.0E+00 3.29E-01
Risk/Cumulative HQ
(1)Inhalation Pathway Exposure Parameters (RME):
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_SG 70 ATc_C_SG 70 ATc_SG 70
Averaging time for non-carcinogens (yrs)ATnc_R_SG 26 ATnc_C_SG 25 ATnc_SG 26
Exposure duration (yrs)ED_R_SG 26 ED_C_SG 25 ED_SG 26Exposure frequency (days/yr)EF_R_SG 350 EF_C_SG 250 EF_SG 350
Exposure time (hr/day)ET_R_SG 24 ET_C_SG 8 ET_SG 24
(2)Generic Attenuation Factors:
Source Medium of Vapors .Symbol Value Symbol Value Symbol Value
Groundwater ( - )AFgw_R_SG 0.001 AFgw_C_SG 0.001 AFgw_SG 0.001Sub-Slab and Exterior Soil Gas ( - )AFss_R_SG 0.03 AFss_C_SG 0.01 AFss_SG 0.03
(3)Formulas .Cia, target = MIN( Cia,c; Cia,nc).Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)
Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_SG 1.00E-06 mIURTCE_C_SG 0.00E+00 mIURTCE_SG 1.00E-06
IURTCE_R_SG 3.10E-06 IURTCE_C_SG 4.10E-06 IURTCE_SG 3.10E-06
.Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:
.
0 - 2 years 22 - 6 years 4
.6 - 16 years 10
16 - 26 years 10.
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
.Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:.
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.asp
H = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtml
S = See RSL User Guide, Section 5X = PPRTV Appendix
Mut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.
Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
SV-06
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based on
scenario)
Residential Commercial Selected (based on
scenario)
Selected (based on
scenario)
Note: This section applies to trichloroethylene and other mutagenicchemicals, but not to vinyl chloride.
Age Cohort Exposure
Duration
Age-dependent adjustment
factor
103
3
1
72
Residential Commercial
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
xx Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario Residential
x Target Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
67-64-1 Acetone 1.0E+02 3.00E+00 No IUR 9.3E-05 2.16E+05 3.10E+01 A110-54-3 Hexane, N-6.5E+00 1.95E-01 No IUR 2.7E-04 4.87E+03 7.00E-01 I
108-88-3 Toluene 1.3E+01 3.90E-01 No IUR 7.5E-05 3.48E+04 5.00E+00 I
95-63-6 Trimethylbenzene, 1,2,4-9.4E+00 2.82E-01 No IUR 3.9E-02 4.87E+01 7.00E-03 P
1330-20-7 Xylenes 5.8E+00 1.74E-01 No IUR 1.7E-03 6.95E+02 1.00E-01 I
Risk/Cumulative 0.0E+00 4.07E-02
Risk/Cumulative HQ
(1)Inhalation Pathway Exposure Parameters (RME):
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_SG 70 ATc_C_SG 70 ATc_SG 70Averaging time for non-carcinogens (yrs)ATnc_R_SG 26 ATnc_C_SG 25 ATnc_SG 26
Exposure duration (yrs)ED_R_SG 26 ED_C_SG 25 ED_SG 26Exposure frequency (days/yr)EF_R_SG 350 EF_C_SG 250 EF_SG 350Exposure time (hr/day)ET_R_SG 24 ET_C_SG 8 ET_SG 24
(2)Generic Attenuation Factors:
Source Medium of Vapors .Symbol Value Symbol Value Symbol Value
Groundwater ( - )AFgw_R_SG 0.001 AFgw_C_SG 0.001 AFgw_SG 0.001Sub-Slab and Exterior Soil Gas ( - )AFss_R_SG 0.03 AFss_C_SG 0.01 AFss_SG 0.03
(3)Formulas .
Cia, target = MIN( Cia,c; Cia,nc).
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)
Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_SG 1.00E-06 mIURTCE_C_SG 0.00E+00 mIURTCE_SG 1.00E-06
IURTCE_R_SG 3.10E-06 IURTCE_C_SG 4.10E-06 IURTCE_SG 3.10E-06
.Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:.
0 - 2 years 22 - 6 years 4
.6 - 16 years 10
16 - 26 years 10
.
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
.
Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:.
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.htmlCA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.aspH = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtmlS = See RSL User Guide, Section 5X = PPRTV Appendix
Mut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).
TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: MecklenburgSV-07
Instructions
Select residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil GasScreeningLevel (ug/m3)
IURSource*RFCSource*
MutagenicIndicator
CR HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based onscenario)
Residential Commercial Selected (based on
scenario)
Selected (based on
scenario)
Note: This section applies to trichloroethylene and other mutagenic
chemicals, but not to vinyl chloride.
Age Cohort Exposure
Duration Age-dependent adjustmentfactor10
3
3
1
72
Residential Commercial
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 1
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
67-64-1 Acetone 1.1E+03 3.30E+01 No IUR 1.0E-03 2.16E+05 3.10E+01 A71-43-2 Benzene 7.8E+01 2.34E+00 6.5E-06 7.5E-02 1.20E+02 7.80E-06 I 3.00E-02 I
75-15-0 Carbon Disulfide 1.0E+02 3.00E+00 No IUR 4.1E-03 4.87E+03 7.00E-01 I110-82-7 Cyclohexane 5.7E+00 1.71E-01 No IUR 2.7E-05 4.17E+04 6.00E+00 I
100-41-4 Ethylbenzene 4.3E+01 1.29E+00 1.1E-06 1.2E-03 3.74E+02 2.50E-06 CA 1.00E+00 I
110-54-3 Hexane, N-5.3E+01 1.59E+00 No IUR 2.2E-03 4.87E+03 7.00E-01 I591-78-6 Hexanone, 2-4.7E+01 1.41E+00 No IUR 4.5E-02 2.09E+02 3.00E-02 I
67-63-0 Isopropanol 2.3E+01 6.90E-01 No IUR 3.3E-03 1.39E+03 2.00E-01 P78-93-3 Methyl Ethyl Ketone (2-Butanone)2.7E+02 8.10E+00 No IUR 1.6E-03 3.48E+04 5.00E+00 I
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)3.1E+01 9.30E-01 No IUR 3.0E-04 2.09E+04 3.00E+00 I
103-65-1 Propyl benzene 1.1E+01 3.30E-01 No IUR 3.2E-04 6.95E+03 1.00E+00 X100-42-5 Styrene 7.9E+00 2.37E-01 No IUR 2.3E-04 6.95E+03 1.00E+00 I
108-88-3 Toluene 1.7E+02 5.10E+00 No IUR 9.8E-04 3.48E+04 5.00E+00 I95-63-6 Trimethylbenzene, 1,2,4-4.0E+01 1.20E+00 No IUR 1.6E-01 4.87E+01 7.00E-03 P
95-47-6 Xylene, o-5.1E+01 1.53E+00 No IUR 1.5E-02 6.95E+02 1.00E-01 S
1330-20-7 Xylenes 1.0E+02 3.00E+00 No IUR 2.9E-02 6.95E+02 1.00E-01 IRisk/Cumulative HQ 7.6E-06 3.43E-01
Risk/Cumulative HQ
(1)Inhalation Pathway Exposure Parameters (RME):
Exposure Scenario Units Symbol Value Symbol Value Symbol Value
Averaging time for carcinogens (yrs)ATc_R_SG 70 ATc_C_SG 70 ATc_SG 70
Averaging time for non-carcinogens (yrs)ATnc_R_SG 26 ATnc_C_SG 25 ATnc_SG 26Exposure duration (yrs)ED_R_SG 26 ED_C_SG 25 ED_SG 26Exposure frequency (days/yr)EF_R_SG 350 EF_C_SG 250 EF_SG 350
Exposure time (hr/day)ET_R_SG 24 ET_C_SG 8 ET_SG 24
(2)Generic Attenuation Factors:
Source Medium of Vapors .Symbol Value Symbol Value Symbol ValueGroundwater( - )AFgw_R_SG 0.001 AFgw_C_SG 0.001 AFgw_SG 0.001Sub-Slab and Exterior Soil Gas ( - )AFss_R_SG 0.03 AFss_C_SG 0.01 AFss_SG 0.03
(3)Formulas .
Cia, target = MIN( Cia,c; Cia,nc).
Cia,c (ug/m3) = TCR x ATc x (365 days/yr) x (24 hrs/day) / (ED x EF x ET x IUR)Cia,nc (ug/m3) = THQ x ATnc x (365 days/yr) x (24 hrs/day) x RfC x (1000 ug/mg) / (ED x EF x ET)
(4)Special Case Chemicals
Trichloroethylene Symbol Value Symbol Value Symbol Value
mIURTCE_R_SG 1.00E-06 mIURTCE_C_SG 0.00E+00 mIURTCE_SG 1.00E-06
IURTCE_R_SG 3.10E-06 IURTCE_C_SG 4.10E-06 IURTCE_SG 3.10E-06
.
Mutagenic Chemicals The exposure durations and age-dependent adjustment factors for mutagenic-mode-of-action are listed in the table below:.
0 - 2 years 22 - 6 years 4
.6 - 16 years 1016 - 26 years 10
.
Mutagenic-mode-of-action (MMOA) adjustment factor This factor is used in the equations for mutagenic chemicals.
.Vinyl Chloride See the Navigation Guide equation for Cia,c for vinyl chloride.
Notation:.
I = IRIS: EPA Integrated Risk Information System (IRIS). Available online at: http://www.epa.gov/iris/subst/index.html
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
DUP-1-10-17
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
If cumulative risk >1.0E-04 or cumulative HQ>1.0
Unacceptable
Residential Commercial Selected (based on
scenario)
Residential Commercial Selected (based on
scenario)
Selected (based on
scenario)
Note: This section applies to trichloroethylene and other mutagenicchemicals, but not to vinyl chloride.
Age Cohort Exposure
Duration
Age-dependent adjustment
factor
10
3
31
72
Residential Commercial
VISL Calculator Version 3.4.5, November 2015 RSLs Page 1 of 2
x
x Sub-slab or Exterior Soil Gas Concentration to Indoor Air Concentration (SGC-IAC) Calculator Version 3.45, November 2015 RSLs
x
x Parameter Symbol Value
x Exposure Scenario Scenario ResidentialxTarget Risk for Carcinogens TCR_SG 1.00E-05
x Target Hazard Quotient for Non-Carcinogens THQ_SG 0.2
x
x
Site Sub-slab or
Exterior Soil Gas
Concentration
Calculated
Indoor Air
Concentration
VI
Carcinogenic
Risk
VI Hazard Inhalation Unit
Risk
Reference
Concentration
x Csg Cia IUR RfC
x CAS Chemical Name (ug/m3)(ug/m3)(ug/m3)-1 (mg/m3)i
Enter target risk for carcinogens (for comparison to the calculated VI carcinogenic risk in column F)
IHSB -Brownfields Vapor Intrusion Calculator - Based on OSWER VAPOR INTRUSION ASSESSMENT Site Name: Carolina Foundry Site ID: 71167563 City: Charlotte County: Mecklenburg
DUP-1-10-17
InstructionsSelect residential or commercial scenario from pull down list
Enter target hazard quotient for non-carcinogens (for comparison to the calculated VI hazard in column G)
Soil Gas
Screening
Level (ug/m3)
IURSource*RFCSource*
Mutagenic
Indicator
CR HQ
P = PPRTV. EPA Provisional Peer Reviewed Toxicity Values (PPRTVs). Available online at:http://hhpprtv.ornl.gov/pprtv.shtml
A = Agency for Toxic Substances and Disease Registry (ATSDR) Minimum Risk Levels (MRLs). Available online at:http://www.atsdr.cdc.gov/mrls/index.html
CA = California Environmental Protection Agency/Office of Environmental Health Hazard Assessment assessments. Available online at:http://www.oehha.ca.gov/risk/ChemicalDB/index.aspH = HEAST. EPA Superfund Health Effects Assessment Summary Tables (HEAST) database. Available online at:http://epa-heast.ornl.gov/heast.shtml
S = See RSL User Guide, Section 5
X = PPRTV Appendix
Mut = Chemical acts according to the mutagenic-mode-of-action, special exposure parameters apply (see footnote (4) above).
VC = Special exposure equation for vinyl chloride applies (see Navigation Guide for equation).TCE = Special mutagenic and non-mutagenic IURs for trichloroethylene apply (see footnote (4) above).
Yellow highlighting indicates site-specific parameters that may be edited by the user.Blue highlighting indicates exposure factors that are based on Risk Assessment Guidance for Superfund (RAGS) or EPA vapor intrusion guidance, which generally should not be changed.
Pink highlighting indicates VI carcinogenic risk greater than the target risk for carcinogens (TCR) or VI Hazard greater than or equal to the target hazard quotient for non-carcinogens (THQ).
VISL Calculator Version 3.4.5, November 2015 RSLs Page 2 of 2