19034_IRC_Supplemental Phase I Remedial Investigation Report

Supplemental Phase I
Remedial Investigation Report
Former lnternationai .Resistive Company
736 Greenway Drive
Boone, Watauga County, North Carolina
January 30, 2014
Terracon Project No. 86127103
Prepared for:
International Resistive Company, Inc.
4222 South Staples Street
Corpus Christi, Texas
Prepared by:
Terracon Consultants, Inc.
3534 Rutherford Road
TABLE OF CONTENTS
1.0 INTRODUCTION ....................................................................................................... 1
1.1 Description of Site and Surrounding Areas ....................................................... 1
1.2 Reliance ........................................................................................................... 2
1.3 Site History and Prior Assessment Activities ..................................................... 2
1.4 Objectives ........................................................................................................ 4
1.5 References ....................................................................................................... 4
2.0 GEOLOGIC AND HYDROGEOLOGIC CONDITIONS ............................................... S
2.1 Geology ............................................................................................................ 5
2.2 Hydrogeology ................................................................................................... 5
2.3 Hydrogeologic lnvestigation .............................................................................. 5
3.0 QUALITY ASSURANCE FOR SAMPLING AND ANALYSIS .................................... 6
3.1 Data Quality Objectives .................................................................................... 6
3.2 Methods for Sample Collection and Analysis .................................................... 6
3.3 Requirements for Analytical Laboratories ......................................................... 6
3.4 Qualifications for Field Staff .............................................................................. 6
3.5 Reporting Analytical Results ............................................................................. 6
3.6 Field and Laboratory Procedures ...................................................................... 7
4.0 INVESTIGATION METHODOLOGY .......................................................................... 7
4.1 Procedures for Site Characterization ................................................................ 7
4.2 Soil Assessment. .............................................................................................. 8
4.3 Groundwater Assessment .............................................................................. 1 0
4.4 Decontamination Procedures ......................................................................... 12
4.5 Investigative Derived Waste (IDW) ................................................................. 13
4.6 Surveying ....................................................................................................... 13
5.0 ASSESSMENT RESULTS AND DISCUSSION ....................................................... 13
5.1 Soil Results .................................................................................................... 13
5.2 Groundwater Results ...................................................................................... 15
6.0 CONCLUSIONS ...................................................................................................... 18
EXHIBITS
Exhibit 1 -Topographic Vicinity Map
Exhibit 2-Site Layout
Exhibit 3-Soil Boring and Monitoring Well Location Map
Exhibit 4-Geologic Cross Section A-A'
Exhibit 5-Geologic Cross Section B-B'
Exhibit 6-Geologic Cross Section C-C'
Exhibit 7-Geologic Cross Section D-D'
Exhibit 8 -Potentiometric Surface Map-Shallow Zone
Exhibit 9-Potentiometric Surface Map -Intermediate Zone
TABLES
Table 1
Table 2
Table 3
APPENDICES
APPENDIX A
APPENDIX B
Soil Analytical Data
Groundwater Analytical Data
Groundwater Elevation and Hydraulic Gradient Data
Boring Logs and Well Construction Records
Laboratory Analytical Reports and Chain of Custody Documentation
SUPPLEMENTAL PHASE I REMEDIAL INVESTIGATION REPORT
FORMER INTERNATIONAL RESISTIVE COMPANY
736 GREENWAY DRIVE
BOONE, WATAUGA COUNTY, NORTH CAROLINA
TERRACON PROJECT NO. 86127103
Report Date: January 30, 2014
1.0 INTRODUCTION
Terracon Consultants, Inc. (Terracon) has completed a Supplemental Phase I Remedial
Investigation at the former International Resistive Company (IRC) plant located at 736
Greenway Drive in Boone, Watauga County, North Carolina (Exhibit 1 ). The general layout
of the site is illustrated on Exhibit 2. Laboratory data results are summarized in Tables 1
and 2. Soil boring logs are presented in Appendix A. A copy of the laboratory analytical
data reports are provided in Appendix B.
The former IRC plant was demolished to the building floor slab in June 2013. Future
redevelopment plans for the site include removal of the slab and potential re-grading of the
site. The purpose of the sampling events described herein were twofold: 1) to assess sub-
slab soils in the vicinity of the former plant building floor drain system and 2) to assess
groundwater in the vicinity of a former hazardous materials storage building (referred to
hereafter as the "Former HazMat Storage Building") and adjacent to the aforementioned
floor drain system.
1.1 Description of Site and Surrounding Areas
The site is an approximate 17 .05-acre parcel located at 736 Greenway Drive in Boone,
Watauga County, North Carolina (Exhibit 1 ). The site is identified in Watauga County tax
records as parcel number 2910219291000 and is located at approximate north latitude 36°
11 '47.98"and west longitude -81° 40' 03.49". According to Watauga County tax records, the
current property owner is International Resistive Company, Inc. The site is currently
unoccupied and former on-site structures have been demolished. Topography at the south
of the site slopes steeply downward toward the former plant building location. Topography
across the rest of the site slopes gently to the north.
The site is located in an area occupied by single-family and multi-family residential
properties and various commercial properties.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
1.2 Reliance
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This report has been prepared for the exclusive use of International Resistive Company, Inc.
Authorization for use or reliance by any other party (except a governmental entity having
jurisdiction over the site) is prohibited without the expressed written authorization of
International Resistive Company, Inc. and Terracon. Any unauthorized distribution or reuse
is at the client's sole risk. Reliance by authorized parties will be subject to the terms,
conditions and limitations stated in the Master Services Agreement between International
Resistive Company and Terracon.
1.3 Site History and Prior Assessment Activities
The site was formerly utilized by IRC and other businesses for industrial purposes; however,
those activities have ceased and the site is currently undergoing assessment and interim
abatement measures in preparation for potential future redevelopment. In June 2013, the
plant and supporting structures were demolished. Future redevelopment plans for the site
include removal of the slabs and associated pavement parking areas and possible re-
grading of the site.
Phase I Remedial Investigation Report-Hazardous Materials Storage Area
In June 2012, S&ME, Inc. (S&ME) submitted a report titled Remedial Investigation Report -
Hazardous Materials Storage Area to IRC. Findings and conclusions presented in this
report are briefly summarized herein; it is assumed that the reader has access to this
document for further reference. The S&ME report summarized groundwater sampling
activities conducted by SynTerra in October 2011 and soil and groundwater sampling
activities conducted by S&ME in April 2012.
The above report indicated that SynTerra identified tetrachloroethylene (PCE) exceeding the
applicable groundwater standard established under 15A NCAC 2L .0202 (2L Standard) of
0. 7 micrograms per liter (IJg/L) in groundwater samples collected from two temporary
groundwater monitoring wells located in the vicinity of the Former HazMat Storage Building.
Specifically, laboratory analysis of groundwater samples identified concentrations of PCE at
210 j.Jg/L from the 16-20 foot depth interval and at 57 j.Jg/L from the 46-50 foot depth interval.
Additionally, other volatile organic compounds (VOCs) such as 1,1, 1-trichloroethane (TCA),
ethylbenzene, toluene, and xylenes were identified in these samples above their respective
laboratory detection limits. SynTerra concluded that the data collected indicated that
groundwater and potentially soil was impacted by VOCs in the vicinity of the Former HazMat
Storage Building.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
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A copy of the SynTerra report was provided to the North Carolina Department of
Environment and Natural Resources (NCDENR) Inactive Hazardous Sites Branch (IHSB).
Following its review of the above report, the NCDENR issued a Notice of Regulatory
Requirements (NORR) requiring that a Remedial Investigation be performed to assess soil
and groundwater quality in the vicinity of the Former HazMat Storage Building (Day to
Milam, December 9, 2011 ). It should be noted that both the SynTerra report and the
NCDENR NORR make reference to areas of the facility where releases of petroleum
compounds and polychlorinated biphenyls were also documented; assessment activities
performed in these other areas are documented separately and there will be no further
discussion of these areas within this document.
In response to the above NORR, IRC authorized S&ME to conduct a Phase I Remedial
Investigation (RI) of the Former HazMat Storage Building. S&ME prepared and submitted a
Remedial Investigation Work Plan (February 2012) which was reviewed and approved by
the NCDENR (Day to Milam, March 23, 2013). As part of the Phase I Rl, S&ME advanced
eleven direct push (OPT) soil borings (HMS-1 through HMS-11) in the vicinity of the Former
HazMat Storage Building. Boring depths ranged from four to 12 feet below ground surface.
A total of twenty-five soil samples were collected for laboratory analysis from the eleven soil
borings. The collected soil samples were analyzed for VOCs by EPA Method 8260B by
Shealy Environmental Services, Inc. (Shealy) in West Columbia, South Carolina (SC
Laboratory Certification Number 3201 0). PCE was the predominant constituent identified in
the soil samples; however, other compounds [including PCE daughter products
(trichloroethylene, cis-1 ,2 dichloroethylene, and vinyl chloride), 1,1 , 1 TCA, ethylbenzene,
toluene, and xylenes)] were also detected in one or more samples.
S&ME also collected 10 groundwater samples from five locations using OPT tooling.
Groundwater samples were collected from near the soil/groundwater interface and at the
presumptive top of bedrock (i.e., the depth of OPT refusal). The collected groundwater
samples were analyzed for VOCs by EPA Method 8260B by Shealy.
Based on the laboratory results from soil sampling activities, S&ME concluded that VOC-
impacted soil and groundwater was present in the area adjacent to northern and eastern
sides of the Former HazMat Storage Building. S&ME also concluded that the extent of
VOC-impacted soil (primarily from PCE) is estimated to measure at least 40 feet long by 40
feet wide with an approximate average depth of five feet amounting to an approximate
volume of 300 cubic yards of impacted soil. S&ME indicated that the extent of soils
impacted above Preliminary Soil Remediation Goals (PSRGs) established by the NCDENR
was not fully delineated.
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Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
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Laboratory data generated from groundwater sampling indicated impact from PCE and its
daughter products above the applicable 2L Standard in two of the five sampling locations.
Both the shallow and deeper samples were impacted at the above two locations. Lesser
concentrations of other organics were also detected in some of the groundwater samples.
1.4 Objectives
Following demolition of the on-site structures, IRC retained Terracon to perform additional
site investigative activities including installation of permanent groundwater monitoring wells
in the Former HazMat Building Storage area and soil sampling in selected areas of the
former plant building footprint to assess for potential impacts from past facility operations.
1.5 References
Report of Findings-Phase II Environmental Site Assessment. synTerra, November
23,2011
Phase I Remedial Investigation Report-Hazardous Materials Storage Area. S&ME,
Inc. June 2012
Watauga County, North Carolina; USDA, Natural Resources Conservation Service;
Web Soil Survey via the Internet, http://websoilsurvey.nrcs.usda.gov/app/
Geologic Map of North Carolina, dated 1985.
The Geology of the Carolinas, Carolina Geological Society Fiftieth Anniversary
Volume, edited by J. Wright Horton, Jr., and Victor A. Zullo, The University of
Tennessee Press, dated 1991.
North Carolina Department of Environment and Natural Resources, Division of
Waste Management, Superfund Section, Inactive Hazardous Sites Branch, Inactive
Hazardous Sites Program Guidelines for Assessment and Cleanup, dated April
2013.
North Carolina Department of Environment and Natural Resources, Division of
Waste Management, Superfund Section, Inactive Hazardous Sites Branch,
Registered Environmental Consultant Program -Implementation Guidance, dated
November 2012 (Edited December 12, 2012).
Topographic Map, 7.5-minute series, Boone, North Carolina Quadrangle photo-
revised 1989, published by the US Geological Survey.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
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2.0 GEOLOGIC AND HYDROGEOLOGIC CONDITIONS
2.1 Geology
Based on the Geologic Map of North Carolina, the site is located in the Blue Ridge Geologic
Province of North Carolina. Geology in the Boone area is generally comprised of biotite
granitic gneiss. Rocks are typically highly fractured and well foliated. Fractures in the rock
have contributed to an accelerated rate of weathering that has resulted in the formation of a
layer of saprolitic material at the ground surface. Based on observed soil characteristics
and a review of local site topography, some soils on the site may be alluvial deposits.
2.1.1 Depth to Bedrock
During this investigation, bedrock was encountered at depths ranging from approximately 62
feet bgs to 68 feet below ground surface (bgs). The lithology and rock surface in this area is
further described in cross section information presented in Exhibits 4 through 7.
2.2 Hydrogeology
Groundwater flow in the Blue Ridge typically m1m1cs surface topography, flowing from
topographically high areas to topographically lower areas such as stream valleys. Saprolitic
soils, such as those present on the site, typically have high porosities, but low hydraulic
conductivities, making them poor transmitters of groundwater. Additionally, saprolitic soils
may serve as a semi-confining layer. Secondary features such as joints and fractures within
the bedrock may also contribute to groundwater flow in the area.
2.3 Hydrogeologic Investigation
The USGS Topographic Map, Boone, North Carolina Quadrangle (Exhibit 1 ), indicates that
groundwater is expected to follow the topography flowing northeast across the site.
Based on the groundwater measurements from the on-site monitoring wells obtained on
November 14, 2013, the inferred groundwater flow direction in the shallow aquifer is
generally to the north and northeast. The depth to groundwater (DTW) ranged from
approximately 2.05 (HMS-MW-31) to 6.38 (HMS-MW-1S) feet bgs. Based on depth to
groundwater measurements, it appears that groundwater in the vicinity of the wells is under
artesian conditions. Groundwater contour elevations were calculated using the DTW
measurements obtained from the wells and surveyed top of casing (TOC) elevations
referenced to an established benchmark on the site. Water level data is included in Table 3.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
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The horizontal hydraulic gradient at the site was estimated to be approximately 0.37 foot per
foot. The vertical hydraulic gradient, ranges from 0.02 foot per foot (between wells HMS-
MW-4S and HMS-MW-41) to 0.09 foot per foot (between wells HMS-MW-1S and HMS-MW-
11) in an upward direction. Information concerning hydraulic gradient is included in Table 3.
3.0 QUALITY ASSURANCE FOR SAMPLING AND ANALYSIS
3.1 Data Quality Objectives
Terracon's objective was to obtain and use a level of data quality that was commensurate
with its intended use. Data reporting was performed as outlined in Appendix A, Section A.8
of the IHSB Guidelines for Assessment and Cleanup (Guidelines). In addition, Terracon
followed generally accepted standards of practice for hazardous substance site
investigations.
3.2 Methods for Sample Collection and Analysis
Terracon followed field protocols, analytical methods, and data reporting procedures
outlined in Appendix A, Sections A.6, A.7 and A.8 of the Guidelines.
3.3 Requirements for Analytical Laboratories
Analytical Laboratory: Shealy Environmental Services, Inc.
1 06 Vantage Point Drive
West Columbia, South Carolina
[phone]
3.4 Qualifications for Field Staff
Terracon personnel involved in the project are professional consulting scientists and
engineers. Terracon conducts in-house training for our field staff as part of our quality
assurance/quality control (QA/QC) program. Our field personnel have experience with
similar investigative type projects. In addition, Terracon field personnel maintain EPA
Hazardous Waste Operations and Emergency Response (HAZWOPER) certifications.
3.5 Reporting Analytical Results
As customary practice, Terracon personnel recorded the sample identification
name/number, date and time of sample collection, name/initials of field person collecting the
sample and the laboratory analytical method to be performed at the time of sample
collection in the project field book and/or on field forms. This information was also recorded
on the laboratory chain-of-custody. Chain-of-custody procedures were maintained by
Terracon personnel until the laboratory received the samples.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
3.6 Field and Laboratory Procedures
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Field procedures were conducted in general accordance with EPA Region IV, "Field
Measurement Procedures", where applicable.
Soil and groundwater samples collected during field events were submitted to Shealy
Environmental Services, Inc. (Shealy) in West Columbia, SC (NC DENR Laboratory ID No.
329). The following analytical methods were utilized during analysis of soil and groundwater
samples:
Soil
VOCs by EPA Method 82608
SVOCs by EPA Method 8270D
Lead and Nickel by EPA Method 6010C
Groundwater
VOCs by EPA Method 82608
As part of field quality control procedures, equipment rinsate blanks and trip blanks were
included on the chain-of-custody forms for analysis by the laboratory. A duplicate of sample
HMSMW-41 (designated "HMSMW-4D") was also collected and submitted for laboratory
analysis.
4.0 INVESTIGATION METHODOLOGY
4.1 Procedures for Site Characterization
The site was characterized by advancing soil borings, installing monitoring wells, and
collecting soil and groundwater samples for laboratory analysis. From July 2013 to
November 2013, Terracon conducted three sampling events on the site. These events
included two sub-slab investigations and a groundwater monitoring well installation and
sampling event. During sub-slab investigations, a total of 21 soil borings were advanced,
and 24 soil samples were collected and were analyzed for various contaminants including
VOCs, SVOCs, nickel, and lead. One groundwater screening point was also advanced, with
the resulting sample analyzed for VOCs. During the groundwater monitoring well installation
and sampling event, four shallow groundwater monitoring wells paired with four vertical
delineation groundwater monitoring wells were installed, sampled, and analyzed for VOCs in
the vicinity of the Former HazMat Storage Building.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
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The following sections outline the methodology used for collecting the environmental
samples and installing the groundwater monitoring wells at the site. The results of the
investigation are also summarized in the following sections. A Site Map depicting the
locations of the soil borings and groundwater monitoring wells is included as Exhibit 3.
4.2 Soil Assessment
4.2.1 Soil Boring Locations
During sampling events that occurred on July 15, 2013 and October 10, 2013, continuous
soil cores were collected at 21 locations on the site using a DPT rig using disposable
cellulose acetate butyrate (CAB) core barrel liners to facilitate the collection of 24 soil
samples. Soil boring logs documenting the subsurface lithology encountered during
borehole advancement were generated in the field and are included in Appendix A.
During the July 25, 2013 sampling event, ten soil borings (SSS-1 through SSS-1 0) were
advanced at the site by SAEDACCO, Inc. (SAEDACCO) of Fort Mill, South Carolina. These
soil borings were located as indicated on Exhibit 3. Borings SSS-1, SSS-2, and SSS-3
were located adjacent to the former Boiler Room. Soil boring SSS-4 was located in the
Recovery Room adjacent to a former wastewater sump. Borings SSS-5 and SSS-6 were
located in the old Plating Room adjacent to a trench drain and sump. Soil boring SSS-7 was
located in the Sludge Accumulation Area adjacent to a floor drain. Soil borings SSS-8 and
SSS-1 0 were located adjacent to trench drains in the Plating Room (Dept. 20). Soil boring
SSS-9 was located adjacent to the Tresco Warehouse in an area where a former waste
sump was reportedly maintained. Soil borings were advanced to approximate depths of 8 to
9 feet bgs. Soils in the 8 to 9 foot interval were observed to be damp, which is ind icative of
groundwater. A detailed description of this sampling event and the resulting data were
presented in a Terracon report entitled Limited Sub-Slab Investigation Report, dated
September 17, 2013; this report was submitted to the NCDENR IHSB on behalf of IRC and
it is assumed that the reader has access to this report.
On October 10, 2013, eleven soil borings (SSS-11 through SSS-21) were advanced at the
site by SAEDACCO. Soil borings SSS-11 through SSS-17 were located along the former
trench drain system with soil borings SSS-11, SSS-12, and SSS-13 located in the Plating
Room, SSS-14 located in the Solder Dip Room, SSS-15 and SSS-16 in the Sludge
Accumulation Area, and SSS-17 in the old Plating Room. Soil borings SSS-18 through
SSS-21 were located adjacent to a former wastewater sump and soil boring SSS-4 from the
July 25, 2013 sampling event.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
4.2.2 Soil Sample Collection and Field Screening
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Soil samples were collected from each boring within CAB liners. Sample characteristics
were described by the field professional and then screened with a MiniRae2000 photo-
ionization detector (PID) for the presence of organic vapors. The lithology of the soils
generally consisted of silty/sandy clay or clayey/sandy silt. Soil lithology and data from field
screening activities are presented on the boring logs included in Appendix A.
Typically, one soil sample per boring was selected for laboratory analysis based upon field
screening results, odors, staining, or other indicators of potential impact. Two soil samples
were collected from borings SSS-6, SSS-17, and SSS-20 based upon observed changes in
soil coloration and/or observed odors. Samples were collected from the 2 foot bgs interva l
at soil boring locations SSS-4, SSS-6, and SSS-14; from the 4 foot bgs interval at soil boring
locations SSS-7, SSS-18, and SSS-19; from the 6 foot bgs interval at soil boring locations
SSS-3, SSS-5, SSS-6, SSS-8, SSS-9, SSS-12, SSS-16, and SSS-17; from the 8 foot bgs
interval at soil boring locations SSS-1, SSS-2, SSS-10, SSS-11, SSS-13, SSS-15, SSS-17,
and SSS-20; and from the 10 foot bgs interval at soil boring locations SSS-20 and SSS-21 .
Prior to sample collection, non-dedicated sampling equipment was decontaminated using a
Liquinox®/water wash and scrubbing, followed by a distilled water rinse. Soil cuttings and
decontamination fluids were con tainerized in 55-gallon drums pending off-site disposal.
After samples were collected, all soil borings were abandoned and backfilled with a
bentonite grout mixture.
In order to minimize losses due to volatilization during sample collection, samples for VOC
analysis were obtained directly from the CAB liner using a laboratory supplied, disposable
sampling device and were not homogenized prior to placement within the laboratory-
prepared sample containers.
Careful handling of samples and equipment was observed throughout the sampling
procedures to avoid cross contamination. Samples were stored at approximately four
degrees centigrade (4°C) throughout the operation and during shipment to Shealy for
analysis. Chain of custody forms were maintained during the shipping and handling process
to document sample integrity. Copies of these forms are included with the laboratory
analytical reports in Appendix B.
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Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
4.2.3 Soil Laboratory Analysis
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Twenty-four combined soil samples were submitted to Shealy from the two soil sampling
events (11 from the July 2013 event and 13 from the October 2013 event). All soil samples
were analyzed for VOCs by EPA Method 82700; samples SSS-1-8, SSS-2-8, SSS3-6, and
SSS-9-6 were analyzed for SVOCs by EPA Method 82700; and samples SSS-4-2, SSS-5-6,
SSS-6-2, SSS-6-6, SSS-7-4, SSS-8-6, SSS-9-6, and SSS-10-8 were analyzed for nickel and
lead by EPA Method 6010C. Laboratory analytical reports are included in Appendix B.
4.3 Groundwater Assessment
4.3.1 Groundwater Monitoring Well Installation
Following soil sampling activities that occurred during the sampling event on October 10,
2013, the GeoProbe® rig was retooled for groundwater sampling and one groundwater
sample (SSGW-1-16) was collected utilizing a drive-point sampler with retractable sampling
screen. This groundwater screening point was installed adjacent to soil boring SSS-17 and
was advanced to an approximate depth of 16 feet bgs with a screen interval of 14-16 feet
bgs.
From October 28 to 31, 2013, SAEOACCO installed four permanent shallow groundwater
monitoring wells (HMS-MW-1S, HMS-MW-2S, HMS-MW-3S, and HMS-MW-4S) paired with
four permanent vertical delineation groundwater monitoring wells (HMS-MW-11, HMS-MW-
21, HMS-MW-31, and HMS-MW-41). These wells were installed in the vicinity of the Former
HazMat Storage Building and were intended to assess groundwater quality in this area. The
locations of the groundwater monitoring wells are depicted on Exhibit 3.
The monitoring wells were installed under the direct supervision of a North Carolina
certified well driller. The monitoring wells were installed using a Roto-Sonic drill rig
propelling 10 foot hollow-stem augers. Prior to initiating the well installation activities, a
continuous soil core was collected and field screened with a PIO for the presence of
organic vapors at each location from the ground surface until the water table was
encountered or refusal was reached. The lithology encountered at each well location was
recorded on soil boring logs, which are included in Appendix A.
The groundwater monitoring wells were constructed using two-inch diameter, Schedule 40,
polyvinyl chloride (PVC) casing fitted with a two-inch diameter, Schedule 40 PVC, factory
milled, 0.01-inch slot size, screened section. The screened sections for all wells were 10
feet in length. The screened sections in the shallow monitoring wells were placed at depths
intended to bracket the water table with the majority of the screen submerged. The
screened sections in the vertical delineation wells were placed at the maximum allowable
depth based on auger refusal. After placing the well screen and riser in the borehole, an
artificial filter pack was placed from the terminus of the borehole to approximately two feet
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above the screened section. The filter pack was followed by a bentonite plug which was a
minimum of two feet in thickness. After the bentonite plug was hydrated, the borehole was
sealed to a depth of approximately six inches below ground surface using a Portland
cement/bentonite grout to allow for the placement of a stick-up type, steel protective casing
and the completion of a concrete well pad. The groundwater monitoring wells were fitted
with a steel well tag providing the well 10, total depth, screened interval, and date installed.
As-built construction logs of the groundwater monitoring wells were generated upon
installation and are included on the soil boring logs located in Appendix A.
Shallow groundwater monitoring wells, HMS-MW-1S, HMS-MW-2S, HMS-MW-3S, and
H MS-MW -4S were installed to a depth of 17 feet bgs with a screened interval of 7-17 feet
bgs. Vertical delineation well HMS-MW-11 was installed at a depth of 67 feet bgs with a
screened interval of 57-67 feet bgs; HMS-MW-21 was installed at a depth of 68 feet bgs with
a screened interval of 58-68 feet bgs; and HMS-MW-31 and HMS-MW-41 were installed at a
depth of 63 feet bgs with a screened interval of 53-63 feet bgs. Post installation, the
monitoring wells were developed by over pumping until clear, relatively sediment-free water
was produced .
4.3.2 Groundwater Elevations
Prior to sample collection, Terracon field personnel gauged the depth to groundwater at
each groundwater monitoring well using an electronic water level meter capable of
measuring the depth to the air/liquid interface to within +/-0.01 foot.
4.3.3 Groundwater Sample Collection
During the November 14, 2013 sampling event, decontaminated, stainless-steel probe rods
with an integrated drive-point sampler were utilized to collect groundwater sample SSGW-
1-16. This groundwater screening point was installed adjacent to soil boring SSS-17. The
sampler was advanced to approximately 16 feet bgs where the sampler was retracted,
exposing approximately 2 feet of integrated well screen. The screen was exposed to
groundwater in the 14-16 foot bgs interval. Groundwater was allowed to accumulate in the
screen for approximately 10 minutes before a groundwater sample was collected with a
decontaminated, stainless-steel micro-bailer. Once the groundwater sample was collected,
the drive-point sampler was removed from the boring and the boring was backfilled using a
bentonite grout mixture.
Prior to collecting groundwater samples from the permanent monitoring wells, each well
was purged of approximately three well volumes using a peristaltic pump or submersible
pump and dedicated polyethylene tubing. Prior to purging, non-dedicated sampling
equipment was decontaminated using a Liquinox®/water wash and scrubbing, followed by a
distilled water rinse. Purge water and decontamination fluids were containerized in 55-
gallon drums pending off-site disposal.
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During purging, the groundwater field parameters temperature, pH, specific conductance
(SC) dissolved oxygen (DO), and turbidity were measured. Once the field parameters
had stabilized (i.e., less than 10% variance between three consecutive readings were
obtained for DO, SC, and temperature, and consecutive pH measurements were within ±
0.2 standard units), groundwater samples were collected using dedicated Teflon® bailers
and placed in pre-preserved, laboratory prepared, sample containers provided by Shealy.
Careful handling of the sampling equipment and containers was observed throughout the
procedure to avoid cross contamination. During sample collection, steps were taken to limit
the agitation of the groundwater samples and to prevent aeration and turbidity. Samples
were stored at approximately four degrees centigrade (4°C) throughout the sampling
activities and during shipment to Shealy for analysis. Chain of custody forms were
maintained during the shipping and handling process to document sample integrity. Copies of
these forms are included with the laboratory analytical reports in Appendix B. As part of field
quality control procedures, an equipment rinsate blank, trip blank, and a duplicate sample
were included on the chain-of-custody for analysis by the laboratory.
4.3.4 Groundwater Laboratory Analysis
Nine groundwater samples, including one duplicate sample, were submitted for analysis to
Shealy. The groundwater samples were submitted for analysis of VOCs by EPA Method
82608. Please refer to Appendix B for a copy of the laboratory analytical report and
associated chain of custody.
4.4 Decontamination Procedures
Equipment
Once removed from the sampling location, non-dedicated equipment (e.g., Geoprobe® rods,
pumps, water quality meters, etc.) were cleaned in a Liquinox® solution and then rinsed with
distilled water to reduce the potential for cross-contamination between sampling points.
Disposable items such as bailers, rope, tubing, and gloves were disposed in plastic trash
bags after each location was sampled.
The potential for cross-contamination was also reduced by sampling the least contaminated
sample locations first and progressing to the more contaminated (i.e. sources area) sample
locations, when possible.
Personnel
Terracon personnel involved in field activities are trained and currently comply with 40 CFR
1910.120, HAZWOPER training requirements. In order to further reduce the potential of
exposure and potential cross-contamination, field personnel changed gloves frequently,
such as between tasks or if the gloves became damaged.
Reliable • Responsive Resourceful 12
Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
4.5 Investigative Derived Waste (IDW)
lrerracon
AIIIDW (soil cuttings, purge water, well development water, and decontamination fluids) was
containerized in 55-gallon drums and transported off the site for disposal at a permitted
treatment and/or disposal facility.
4.6 Surveying
Each soil boring location was temporarily marked in the field using wooden stakes or
marking paint. The locations of each boring were then surveyed by Appalachian
Professional Land Surveyors & Consultants, PA of Boone, North Carolina (Licensed Land
Surveyor No. C-2398). The locations and top-of-casing elevations of each monitoring well
were also surveyed. Data obtained by the surveyor were incorporated into the site plan and
are depicted in Exhibits 3, 8, and 9.
5.0 ASSESSMENT RESULTS AND DISCUSSION
5.1 Soil Results
5.1.1 Soil Analytical Results
The soil analytical data generated during the assessment activities are provided in the
laboratory analytical reports included in Appendix B and are presented in tabular form in
Table 1. Results generated from soil sample analysis were compared to the Preliminary
Soil Remediation Goals (PSRGs) established by the NCDENR IHSB, updated July 13, 2013.
The IHSB has established health-based PSRGs for residential and industrial settings as well
as for Protection of Groundwater (PoG).
Multiple VOCs, SVOCs, and lead and nickel were observed at concentrations above the
laboratory reporting limits in one or more of the soil samples collected during the
assessment activities. The following constituents were detected at levels exceeding their
respective PSRGs:
1,1-Dichloroethane (1,1-DCA):
Concentrations of 1,1 -DCA that exceeded its respective PSRG -PoG value of 30 j..Jg/kg
were observed in samples SSS-11-8 (48 j..Jg/kg), SSS-17-6 (260 j..Jg/kg), and SSS-17-8 (450
j..Jg/kg).
Cis-1 ,2-Dichloroehtene (cis-1 ,2 -DCE):
Concentrations of cis-1 ,2 -DCE that exceeded its respective PSRG -PoG value of 360
j..Jg/kg were observed in samples SSS-1 7-6 (14,000 j..Jg/kg) and SSS-17-8 (8,800 j..Jg/kg).
Reliable • Responsive • Resourceful 13
Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
4-Methyl-2-pe nta none:
lrerracan
Concentrations of 4-methyl-2-pentanone that exceeded its respective PSRG -PoG value of
430 IJQ/kg were observed in samples SSS-17-6 (820 IJQ/kg) and SSS-17-8 (2,300 IJQ/kg).
Methylene Chloride:
Concentrations of methylene chloride that exceeded its respective PSRG -PoG value of 23
IJQ/kg were observed in samples SSS-17-6 (23,000 IJQ/kg) and SSS-17-8 (110,000 IJQ/kg).
The concentration observed in sample SSS-17-8 also exceeded its respective PSRG -
Residential value of 56,000 IJQ/kg.
Tetrachloroethylene (PCE):
Concentrations of PCE that exceeded its respective PSRG -PoG value of 5.0 IJQ/kg were
observed in samples SSS-4-2 (970 IJQ/kg), SSS-6-2 (880 IJQ/kg), SSS-7-4 (19 1-Jg/kg), SSS-
8-6 (300 1-Jg/kg), SSS-12-6 (1 00 IJQ/kg), SSS-16-6 (75 IJQ/kg), SSS-17-6 (1 ,800 IJQ/kg), SSS-
17-8 (190,000 1-Jg/kg), and SSS-19-4 (44 IJg/kg). The concentration observed in sample
SSS-17 -8 also exceeded its respective PSRG -Residential value of 17,000 IJg/kg and
PSRG -Industrial value of 82,000 1-Jg/kg.
Trichloroethylene (TCE):
Concentrations of TCE that exceeded its respective PSRG -PoG value of 18 IJg/kg were
observed in samples SSS-4-2 (20 IJg/kg), SSS-17-6 (100,000 IJg/kg), and SSS-17-8
(140,000 1-Jg/kg). Concentrations observed in samples SSS-17-6 and SSS-17-8 also
exceeded its respective PSRG -Residential value of 880 IJg/kg and PSRG -Industrial
value of 4,000 IJg/kg.
5.1.2 Laboratory Data Evaluation
In reviewing the laboratory results, several analytes are reported as detections with "J" data
qualifiers, indicating the reported value is an estimate reported within the 95% confidence
interval. A confidence interval is based on observations of a sample constructed so that
there is a specified probability that the interval contains the unknown true value of a
population parameter. It is an accepted practice to calculate confidence intervals that
have a 95 percent probability of containing the true value. These compounds were
detected above the method detection limit (MDL), but below the laboratory reporting
limit. The MDL is the lowest concentration at which an analyte can be detected in a
sample by the particular laboratory method used. "Detected" indicates that the analyte can
be distinguished from the blank with reasonable certainty. The reporting limit (also called
practical quantitation limit, or POL) is approximately five times the MDL or the lower
calibration standard, whichever is higher. Results above the POL can be distinguished from
the blank and fall within applicable standard curves. For the purposes of this assessment,
all "J" qualified data are considered analytically valid and acceptable for making site
management decisions. In addition, all quantitative data considered analytically valid and
Reliable • Responsive • Resourceful 14
Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30,2014 • Terracon Project No. 86127103
lrerracon
acceptable met all field and analytical data usability requirements. This means all quality
assurance parameters have been satisfied, including quality control and quality assessment.
This data is considered definitive and may be used for any purpose.
5.1.3 Extent of Soil Contamination
Former Trench Drain Network
Based on the laboratory analytical results for the soil samples collected by Terracon
personnel during assessment activities, historical facility operations appear to have
impacted soils in the vicinity of the former trench drain systems located near the south-
central portion of the facility; however, areas to the northeast and southwest of the identified
contaminated soils have not been sufficiently assessed such that the horizontal extent of soil
contamination has not been fully defined and further assessment is necessary. The highest
levels of soil contamination identified in this area were detected in soil boring SSS-17.
Samples from soil boring SSS-17 were collected and analyzed from the 6-foot and 8-foot
depth intervals and analyte concentrations were noted to generally increase with depth.
Further assessment in this area may be necessary in order to determine the vertical extent
of soil contamination present.
Former HazMat Storage Building
Past assessment activities conducted by S&ME identified VOC impacted soils to the north
and east of the Former HazMat Storage Building. The bulk of this impacted soil was
removed under the auspices of a NCDENR-approved Initial Abatement Plan (Terracon,
October 3, 2012) in August 2013. During implementation of the above work plan, additional
impacted soil was observed underneath the northern and eastern sides of the Former
HazMat Storage Building foundation; these soils were not removed but were left in-place to
be managed as part of the final soil remedy for the site. Further details of this action will be
presented in an Initial Abatement Report which will be submitted under separate cover.
Further assessment of this area is necessary to characterize the extent of soil impact
beneath the foundation.
Soil analytical results are summarized in Table 1. Copies of the laboratory analytical reports
are included in Appendix B.
5.2 Groundwater Results
5.2.1 Groundwater Analytical Results
The groundwater analytical data generated during the assessment activities are provided in
the laboratory analytical reports included in Appendix B and are summarized in tabular form
in Table 2. Results generated from groundwater sample analysis were compared to the
NCDENR Maximum Allowable Concentration (MAC) under 15 NCAC 2L. 0202, effective
April1, 2013.
Reliable • Responsive • Resourceful 15
Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30,2014 • Terracon Project No. 86127103
lrerracon
Multiple VOCs were observed at concentrations above the laboratory reporting limits in one
or more of the groundwater samples collected during the assessment activities. The
following compounds were found at levels exceeding their respective NCDENR MACs:
1,1-DCA:
Concentrations of 1,1 -DCA that exceeded its respective NCDENR MAC value of 6 IJg/L
were observed in sample HMS-MW-2S (42 IJg/L).
cis-1 .2 -DCE:
Concentrations of cis-1 ,2 -DCE that exceeded its respective NCDENR MAC value of 70
IJg/L were observed in sample SSGW-1-16 (130 IJg/L).
Methylene Chloride:
Concentrations of methylene chloride that exceeded its respective NCDENR MAC value of 5
IJg/L were observed in sample SSGW-1-16 (480 IJg/L).
Trichloroethylene (TCE):
Concentrations of TCE that exceeded it respective NCDENR MAC value of 3 IJg/L were
observed in sample SSGW-1-16 {320 IJg/L).
Vinyl Chloride:
Concentrations of vinyl chloride that exceeded its respective NCDENR MAC value of 0.03
IJg/L were observed in sample SSGW-1-16 {6.2 IJg/L).
5.2.2 Laboratory Data Evaluation
In reviewing the laboratory results, several analytes are reported as detections with "J" data
qualifiers, indicating the reported value is an estimate reported within the 95% confidence
interval. A confidence interval is based on observations of a sample constructed so that
there is a specified probability that the interval contains the unknown true value of a
population parameter. It is an accepted practice to calculate confidence intervals that
have a 95 percent probability of containing the true value. These compounds were
detected above the method detection limit (MDL), but below the laboratory reporting
limit. The MDL is the lowest concentration at which an analyte can be detected in a
sample by the particular laboratory method used. "Detected" indicates that the analyte can
be distinguished from the blank with reasonable certainty. The reporting limit (also called
practical quantitation limit, or PQL) is approximately five times the MDL or the lower
calibration standard, whichever is higher. Results above the PQL can be distinguished from
the blank and fall within applicable standard curves. For the purposes of this assessment,
all "J" qualified data are considered analytically valid and acceptable for making site
management decisions. In addition, all quantitative data considered analytically valid and
Reliable Responsive • Resourceful 16
Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30,2014 • Terracon Project No. 86127103
lrerracon
acceptable met all field and analytical data usability requirements. This means all quality
assurance parameters have been satisfied, including quality control and quality assessment.
This data is considered definitive and may be used for any purpose.
5.2.3 Groundwater Flow Direction
Groundwater measurements from the on-site monitoring wells obtained on November 14,
2013 indicate that artesian conditions are present along the southern portion of the site. In
three of the wells, groundwater had risen above the ground surface and into the well risers.
Evaluation of these measurements indicates groundwater flow in the saprolite aquifer is
generally to the north and northeast. As indicated in Table 3, the depth to water (DTW) in
the shallow wells, as measured from top-of-casing (TOC), ranged from approximately 3.44
feet below TOC (HMS-MW-1S) to 6.38 feet below TOC (HMS-MW-4S). The DTW in the
intermediate wells was measured as approximately 2.05 feet below TOC (HMS-MW-31) to
3.41 feet below TOC (HMS-MW-21). Potentiometric Surface Maps for both the shallow and
intermediate wells were developed using the above data and are included as Exhibits 8
and 9, respectively. As illustrated on the above Exhibits, data from the shallow wells
generally indicate a groundwater flow direction to the north while the intermediate wells
indicate groundwater flow to the northeast. Ordinarily, one would expect similar
groundwater flow directions within the same aquifer. In this case, however, it is expected
that surface features (i.e., the adjacent spring and the significant slope located immediately
to the south) are influencing the shallow groundwater flow direction in this area of the site.
5.2.4 Horizontal Delineation
Former Trench Drain Network
One sample of shallow groundwater was collected from this area using OPT tooling.
Laboratory analysis of this sample indicated that groundwater was impacted by volatile
organic compounds. Further assessment is necessary to delineate the horizontal extent of
groundwater contamination in this area.
Former HazMat Storage Building
Past assessment activities conducted by S&ME indicated that groundwater in this area was
impacted by VOCs. Data generated from sampling of groundwater monitoring wells
installed by Terracon indicate relatively low-level VOC impact in this area, predominately to
the north of the Former HazMat Storage Building (see Table 2). Based upon the more
recent data, additional assessment of the saprolite aquifer in this area is not recommended
at this time.
Reliable • Responsive • Resourceful 17
Supplemental Phase I Remedial Investigation Report
Former International Resistive Company Site • Boone, NC
January 30, 2014 • Terracon Project No. 86127103
5.2.5 Vertical Delineation
Former Trench Drain System
lrerracon
The vertical extent of groundwater impact in this area is undefined; therefore, one or more
deeper wells will be required to assess the vertical impact of VOCs.
Former HazMat Storage Building
Past assessment activities conducted by S&ME identified VOC-impacted groundwater in this
area at depths up to 44 feet bgs. Analytical results of groundwater samples collected from
intermediate (i.e., "top of rock") wells by Terracon in November 2013 indicate that
groundwater impact in the vicinity of the Former HazMat Storage Building appears to be
limited by bedrock which ranges from approximately 63 feet bgs to 68 feet bgs. Therefore,
based upon these data, further vertical delineation of groundwater in this area is not
currently recommended.
6.0 CONCLUSIONS
Based on the findings of this assessment, Terracon recommends additional soil and
groundwater assessment be conducted as indicated above in order to further assess VOC
impacts present on the site. Terracon recommends that a Phase II Remedial Investigation
Work Plan be prepared that will outline an approach to characterize the extent of soil and
groundwater impact present as a result of releases from the two areas of the site discussed
herein.
Reliable • Responsive Resourceful 18
r
EXHIBITS
TABLES
Soil Tat ......
SSS-1
SSS·2
555·3
555-.4
555-5
555-6
sss-1
555-3
555·9
ill·10
555·11
SSS·12
555·13
S5S-1o4
SSS·15
555-16
S5S-17
SSS-18
555·19
SS5-20
SSS-21
-~ PIDF1old ..... .._ .. _
(feetl .....
10
10
19.7
7.9
0.6
2.5
1.9
4.6
4.8
18.7
526
2.1
1.1
13.9
511
20.2
6.6
8.0
22.3
422
882
7.5
23.1
25.1
40.5
6.4
TABLE 1
so\\
SUPPLE14ENTAl PHASE I R.EMEDIAL INVESTIGATOIH
IA:C.PROP£R.TY
BOONE, WATAUGA COUNTY, P'fORTH CAROLINA
TERR.ACON PROJECT NO. 86127103
tt'CCIOM -I>
,,... -b..........! ....... ""'Ill' I rllllll• I M'kl' 1,1-DCA 1,1«£ ds·t,Z«f ISen2ilne benzene Acetate :z Cltlarlde' ...,...1 -·1-1:1 ............ ""'"'"'1.=-.1_..,.,.,, I,,..,.., , .. ,. .. '"'""' ""''"". ··-· PC£ '"''"' 1,t,Z·TCA 1 r.,...,.
IPIIkiJ fPIIktl
TCE
'"'""'
........ -· SSS·1·8
SSS-2-8
555·3·6
555-.4·2
555-5-6
SSS-6·2
SSS-6-6
SSS-7-4
SSS-8-6
190
•20
79
<18
16
21
130
7l
51
<14
<10
13
<'1.2
<11
<8.9
<1l
<15
<8.8
<6.8
<5.1
<5.9
<<4.6
<5.3
<<C.'!
<6.'1
<7.-<C
<-<C.-<C
<6.8
.;5.1
<5.9
19
<5.3
<-'4.<4
<6.-'4
<7.4
5.6
<5.1
<5.9
<41.6
<5.3
""'·"' <6.4
<7.-<C
<4.<fl
555-9-6 I <23 I <12 I <5.11 I <5.8 I <5.1
sss-to-a I <25 I c1l I c6.J I c6.J I <6.3
SSS-11-8 I <24 I <12 I <6.0 I 48 I 59
555·12-6 I <900 I c450 I <220 I <220 I <220
SSS-13-8 I <1,300 I <650 I <320 I <320 I .c320
sss-1+2 I 17 I -ctz I ~s.a I <5.3 I <5.8
555·15-8 I <22 I <11 I <5.5 I 1.J(JI I .c5.5
SSS-16--6 I <1,600 I <7110 I <3'10 I <390 I .,390
555-17~ I <2,400 I .. ,,200 I 2201)) I ·.260f:J) I .• 90
555-17-8 <2,500 <1,300 <630 .450(.1) <630
555·18-.4 I 61 I 9,3(Jl I <6.5 I o.98(JJ I <6.5
SSS-19-.4 I <1,200 I <590 I <290 I .c290 I .c290
SSS-20-8 I 29 I <12 I <5.11 I <5.8 I <5.8
SSS-20-10 <1,300 <670 <340 <340 <340
SSS-21·10 21(J) <14 <7.0 <7.0 <7.0
<6.8
<5.1
<5.9
19
<5.3
<4.4
<6.4
<7.4
<4.4
<6.8
<5.1
<5.9
<4.6
<5.3
"'"·"' <6.4
<7A
.......
<5.8 I <5.8
<6.1 I <6.3
1.HJ) I <6.0
<220 I <220
.c320 I ..-320
<5.8 I c5.8
<5.5 I <5.5
.c390 I .c390
, ... ::nJ I 540(J) ·~~ 420(J)
4.1(J) I <6.5
<290 I <290
.... I <5.8
<J«< <J.40
<7.0 <7.0
.;6.8
<5.1
<5.9
<U
<5.3
<4.4
<6.o4
<7.-<C
7.5
<5.8
<6.3
<6.0
<220
<320
.....
<5.5
.,.
tOO(J)
<630
<6.5
<290
<5.8
<140
<7.0
<6.8
<5.1
<5.9
co4,6
<5.3
<..C.o4
<6.4
<1 ...
<5.11
<6.3
<6.0
65(J)
<320
~s.8
<5.5
<190
340(J}
360jJ}
<6.5
lSO
<5.8
<140
<7.0
<10
<12
<'1.2
<11
<8.9
<1l
<IS
<8.8
<6.8
<5.1
<5.9
<4.6
<5.3
<4.4
<6.-4
~7.4
<-4.4
•6.8
<5.1
<5.9
970
<5,3
aao
<6.'1
19
100
<6.8
<5.1
<5.9
<4.6
<5.3
""'·" <6.4
<7.-<C
.......
<.6.6
<5.1
<5.9
... 6
<5.3
<<fl.-4
<6.-4
<7.-<C
<4.4
<6.8
<5.1
<5.9
.,
<5.3
"'"·"' <6.4
<7.--t
7.0
<6,8
<5.1
<5.9
9.0
<5.3 ....
<6.4
<7.-c
<4A
<11 I <5.8 I <5.8 I <5.8 I <5.11 I <5.1 I <5.8
<13 I c6.3 I <6.3 I <6.1 I <6.3 I <6.3 I <6.3
<12 I <6.0 I 4.1(JI I 1.9{JI I <6.0 I l.S(J) I <6.0
<450 I <220 I: 100(J) I <220 I <220 I <220 I c220
~6SO I <320 I <320 I <l20 I <320 I <320 I <320
<12 I 8.3 I .. s.a I <5.8 I ~5.8 I <5.8 I <5.8
<11 I <5.5 I <5.5 I <5.5 I .. s.s I <5.5 I <5.5
-c7ao I <390 I 7StJJ I <390 I -c390 I <390 I l40!JJ
8ZO{J) I 23,000 I 1,800 I <590 I Z60(J) 1100,000 I t,OOO
1,300 110,000 190,000 <610 ltD(JI 140,000 810
<13 I <6.5 I <6.5 I <6.5 I .c6.s I <6.5 I <6.5
9l(JJ I <290 I -44fJJ I <290 I .c290 I <290 I <290
•12 I <5.8 I 1.t{J) I <5.8 I <5.8 I .... I .. s.a
<670 <340 <340 <310 <340 <340 c)o«)
<14 .c7.0 <7.0 <7.0 <7.0 <7.0 <7.0
-1 Leod , ...... ,...,...
.... o
<J7D
660
NA
NA
NA
NA
NA
NA
<--t30
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
""
15
19
47
10
47
29
ll
20
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
PSRG·Residential 1.20E+07 I 5.60E-+<16 I 1.20E+OS I 3,300 I 48,000 I 32,000 s,400 1 2.7££+05 1 t.60E+07 1 1.10E+06 1 s.60E+O<C 1 11,000 320 I 8.20E+OS ... 1.30E+05 I 4.bOE+OS I -4.oc:E+DS
'PSRG·Industrial 1.oof~oa I 2.80f~o7 I t.20E+OS I 11,000 I 2..20E+OS I 4.0CI::+()5 I Z.70E+04 I 2.70E+OS I Z.90E•07 I 3.<40E•06 I 6.2C£+()5 I 82,000 I 1,400 I 8.20E•05 I -4,000 I 2.60E•OS I 4 . ...o£.o()6 I s.OOE+OS
PSRG·Prot«tlon of Groundwater 24,000 I 16,ooo I N.. I 30 I Z.JOO I 360 I 11,100 I t,Joo I >:.~. I 430 I 23 I s.o I 3.2 I s,soo I 18 I s,aoo I J.JOE+CIS I2.70E+05
Nates: t • Sample SSS--7-4 was originally analyzed at a 50x dihiion based on laboratory screening •rror. The sample was later re-analyzed (cLot of holding time) at a u ro dii~Aion with the rest.lts St.l'nmarized above
J ·Estimated conc1!fUalion. r•ported betwHn the Practical Quartitation Umit (POL} and lhe Method Dete<:tion Umit (MDL).
M. • No Standanllisted
NA " Not Analyzed
PCE • tetrachloroeth~~
TCE • trichloroethene
DCA· dichloroethane
DCE-dkhloroethylene
Concentn~tions in bold type Indicate exceedanc• or laboratory d!ttdlon limit
Shaded concentrattom indlcat~ ~cee<lanc~ of one or mor~ PSRGs
-lmtlktl
NA
NA
NA
8.1
9.2
14
5.8
2l
17
5.9
11
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
... ... ...
Plijje 1ol1
Groundwater
Monitoring Well
HMS-MW-1S
HMS-MW-11
HMS-MW-25
HMS-MW-21
HM5-MW-3S
HMS-MW-31
HMS-MW-4S
HMS-MW-41
HMS-MW-41
55GW-1-16
NC DENR MAC
Notes:
-
Total Well Depth ~ample
TABLE 2
SUPPLEMENTAL PHASE I REMEDIAL INVESTIGATION
IRC PROPERTY
BOONE, WATAUGA COUNTY, NORTH CAROLINA
TERRACON PROJECT NO. 86127103
_LaDoratory aetecttons
GW
Methylene
(ft bgs) ID Chloroform Chloroethane 1,1-DCA cls-1,2-DCE trans-1,2-0CE c::~e 2-:=:~e Chloride
(IJg/L) (IJg/L) (IJg/L) (1J8/L) (1J8/L) (IJg/L) (IJg/L) (IJg/L)
17 HMS-MW-15 7 <5.0 <5.0 <5.0 <5.0 <5.0 <1 0 <5.0
67 HM5-MW-11 11 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
17 HMS-MW-25 <5.0 270 42 <5.0 <5.0 <5.0 <10 <5.0
68 HM5-MW-21 12 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
17 HM5-MW-35 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
63 HM5-MW-31 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
17 HMS-MW-45 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
63 HM5-MW-41 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
63 HMS-MW-4D1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0
16 55GW-1-16 <5.0 1.6 (J) 5.5 130 4.0 (J) 0.33 (J) 3.7 (J) 480
70 3,000 6 70 100 3 NL 5
Samples collected on November 14, 2013
t -Sample HMS-MW-4D is a duplicate of sample HM5-MW-41
TCE 1, 1,1-Trichloroethane
(IJg/L) (IJg/L)
<5.0 <5.0
<5.0 <5.0
<5.0 5
<5.0 <5.0
<5.0 <5.0
<5.0 <5.0
<5.0 <5.0
<5.0 <5.0
<5.0 <5.0
320 <5.0
3 200
NC DENR MAC = North Carolina Department of Environment and Natural Resources Maximum Allowable Concentration Groundwater Standards under 15A NCAC 02L .0202 (April1, 2013)
J • Estimated concentration, reported between the Practical Quantitation Limit (POL) and the Method Detection Limit (MDL).
NL • No Standard listed
PCE -tetrachloroethene
TCE · trichloroethene
DCA -dich!oroethane
DCE -dichloroethytene
Concentrations in bold type indicate exceedance of laboratory detection limit
Shaded concentrations indicate exceedance of one or more PSRGs ----
I
Vinyl Chloride
(IJg/L)
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
6.2
0.03
Groundwater Monitoring
Well
HM8-MW-18
HMS-MW-11
HMS-MW-2S
HMS-MW-21
HM8-MW-3S
HMS-MW-31
HM8-MW-48
HMS-MW-41
Average
Notes:
Total Well Depth
(ft bgs)
17.0
67.0
17.0
68.0
17.0
63.0
17.0
63.0
TABLE 3
SUPPLEMENTAL PHASE I REMEDIAL INVESTIGATION
IRC PROPERTY
BOONE, WATAUGA COUNTY, NORTH CAROLINA
TERRACON PROJECT NO. 86127103
Top of Casing Depth to Groundwater Distance Between
Elevation Groundwater Elevation Well Pairs
(ft) (ft) (ft) (ft)
3143.09 6.38 3136.71 6.75 3143.72 2.33 3141.39
3141.13 5.82 3135.31 6.58 3141.05 3.41 3137.64
3140.96 4.21 3136.75 7.50 3141.08 2.05 3139.03
3141.55 3.44 3138.11 8.21 3141.42 2.32 3139.1
1) Depth to water level measurements were collected on November 14,2013
Horizontal Hydraulic
Gradient Between Well
Pairs
0.69
0.35
0.30
0.12
0.37
2) Top-of-Casing elevations measured in feet above mean sea level and are referenced to an onsite benchmark
-------
Vertical Hydraulic
Gradient Between Well
Pairs (Shallow to
lntennediate)
0.09
0.05
0.05
0.02
0.05
APPENDICES
APPENDIX A
Boring Logs and Well Construction Records
f-0 0
~ ~
0 cr:
C§ z ~ rJ)
> z w
~ 0.. 0
'"' 0 ;::: N ;;
"' 0 0 ~
f-er: <( ;:, rJ)
~ ~ z w ;:, z 0 cr: > z w
t;:
0 0.. w cr:
~ <( z (3 oc 0 ;:, 0 cr: u.
0 w ~ <(
0.. w (j)
!!=
0 ::J <( > f-a z
!!!
0 g
0 z oc 0 "' rJ) r f-
WELL LOG NO. HMS-MW-15 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
0 LOCATION See Exhbit A-2 INSTALLATION DETAILS ~rJ) w
0 wz o._ wcr: ~ g >Q 1: Wf-~w 0 "-"' I I ~<( w :;<:2 f-o::> --' o._ o._ wo:: o._ <(:J ~ Well Completion: w r-W :2 (J)Z 0 ~~ (.') <(
0 (f) DEPTH MATERIAL DESCRIPTION
' X ElbL-§IL TY §At::!!:! (§M), coarse grained, tan ~ i -' ,· 3.0 i -' ' -
\, FILL-SANDY SILT (MU, tan to gray -5-·~ ----
1o-=:
<"> ---. ·. 15.5 15-I IIIII 17.0 _§A!'::jDY SILT (ML), gray to tan, saprolite
._
Boring Terminated at 17 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes: Hand auger I Rotcrsonic Geoprobe
Abandonment Method:
WATER LEVEL OBSERVATIONS lrerracan Well Started: 10/29/2013 Well Completed: 10/29/2013
Depth to groundater is 6.38' below top of
casing. Drill Rig: 8140 LS Driller: RCH
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
1-0 <!)
N ;;
N
0 0:: <! 0 z ~ > z w
~ 0.. <!)
"' 0 ;::: N <0 "' <!) 0 _J
1-c:: <! :2 (/)
_J ~ z w :2 z
0 0:: > z w
~ 0 0.. w 0::
_J <! z (3 a:
0
:2 0 0:: u.
0 w ~ a: if. w (/)
!!=
0 :::; :;
1-0 z
!!l
<!) 0 -'
<!) z a: 0 "' (/) I 1-
WELL LOG NO. HMS-MW-2S Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
CJ LOCATION See Exhbit A-2 INSTALLATION DETAILS uj~ w
0 (l_ wa:: _J g >Q ~ 0 WI-_,w
I -'<! a.m I: w ::;;::;; 1-a::> -' a. a. wa:: (l_ <t::l <! Well Completion: w ,_w ::;;; UlZ 0:: 0 <trJl CJ :;:m <(
0 (/) DEPTH MATERIAL DESCRIPTION
•' ''> EILL ·SILTY !;;!,AY (!;;lc-ML), gray tan to brown I" ~ -
<.;.x -•
--
' s-= "' ' '<. 7.0 --SANDY SILT (Mll, gray tan to brown, saprolite --1~ --
17.0 1s-:::
Boring Terminated at 17 Feet
The stratification lines represent the approximate trans1t1on between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes
Hand auger I Rotc-sonic Geoprobe
Abandonment Method:
WATER LEVEL OBSERVATIONS lrerracan Well Started: 10/29/2013 Well Completed: 10/29/2013
Depth to groundater is 5. 82' below top of
casing. Drill Rig: 8140 LS Driller: RCH
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
f-0 0
N ~
0 0: <( 0 z ;"= (/) > z w
0: 0
M 0 ;:::
N ;;; "' 0 g :r <( :2 (/)
_J
;"= z w :2 z 0 0: > z w
f-0: 0 a. w 0:
;;;! z (3
it: 0
:2 0 0: lL
0 w ~ if. w (/)
!!:
0 :; ~
f-0 z
!!l
l'l 0 _J
l'l z it: 0 al
(/)
J: >-
WELL LOG NO. HMS-MW-35 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
<.9 LOCATION See Exhbit A-2 INSTALLATlON DETAILS _JUl w
0 wZ 0.
_J §: >Q ~ we::
Wf-...JW 0 I ...1<( w o.m I 1-a::> _J ::;;::;; 0. 0. we:: 0. <(:J ~ Well Completion: w t-UJ ::2; UlZ 0 <(Ul <.9 s:m <(
DEPTH 0 (f)
MATERIAL DESCRIPTION , FILL-SANDY SILT IMLl, with gravel, tan -k 3.0 •
--
., ~~-?-EILL-~ANDY ~lbi (ML}, with clay, gray tan to dark brown -5.5 5-:/1 SILTY CLAY ICL-Mll, tan to dark brown, saprolite -
8.0 --It 10.0 ~ANDY ~ILI (!!11!.), tan to dark brown, saprolite -
. l SILTY SANP (SM), with gravel, medium grained, gray to tan 1~
--j. I -' 15-I 17.0 ._
Boring Terminated at 17 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Hand auger I Rota-sonic Geoprobe
Abandonment Method:
WATER LEVEL OBSERVATIONS
lrerracan Well Started: 10/30/2013 Well Completed: 10/30/2013
Depth to groundater is 4. 21' below top of
casing. Drill Rig: 8140 LS Driller: RCH
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
f-0
G
N
0 N
0 ~ <! 0 z ;::
(f)
> z w
' 0.. G
"' 0 ;::: N
(0
<Xl
G g
f-"' <! :;;:
(/)
...J ;:: z w :;;: z 0 ~ > z UJ
l;;:
0 CL UJ ~
...J <! z 0 02 0 :;;:
~ lL
0 UJ ~ <! 0.. UJ (f)
"" 0 ::; :;
f-0 z
!!2
(.')
0 ...J
G z 02 0 "' (f)
J" f-
WELL LOG NO. HMS-MW-41 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
C9 LOCATION See Exhbit A-2 INSTALLATION DETAILS _,(f) w
0 wz a_ wO: -' g >Q ~ (.) WI-_.w
I -'<I: a.m :X: w :::;;:::;; 1-o:> _J CL a_ wo: <I;::J ~ Well Completion: w f-W a_ (f)Z 0 <I;(/) ~ C9 ~m <t: 0 (J) DEPTH MATERIAL DESCRIPTION
FILL-SILTY SAND !SMI, with gravel, tan to gray, with asphalt ~ -
3.0 ~ -
. 4. FJLL-SANDYSJLT !MLI, tan gray
-
S< 5-= SILTY SAND ISMI. medium grained, dark brown to white, saprolite -
J
-• ~ -
:::-; 1~ -• ~ -
15-= ~ 17.0 -
19_0 §IL TY §AND I§Ml. medium grained, gray to tan, with rock fragments -• ~ -'R ROCK FRAGMENT§ WITH §AND ANP §ILT, gray to tan, highly fractured ~ 2~ ~ -• ~ 23.0 -It §ANPY SILT IML), with clay, tan to dark brown zs-= -27.5 -• ~ 29.o B~I:S EBA!:aM!i:tU§ l!l!III:I §A~P A~P §ILI. gray to tan, highly fractured -">!'
30:
r:
SILTY SAND {SM). medium grained, tan, with rock fragments ~ -~ -• I~ -~ -~ 35--
38.0 ~ -• ~ -§ANDY SILT {MLI, gray tan to dark brown, with rock fragments ~ 40::: S< --• ~ -
45-=
47.0 -
METAMORPHIC BEDROCK, gray to tan, highly fractured I -• 1f.60Dril -
5~
-• JDDm -
55-= -. -• ~ -
62.0 6~ --A , gray ~ 1;1ormg 1 ermmarea ar t>;s r-eer
67.0
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Hand auger I Roto-sonic Geoprobe
Abandcnment Method:
WATER LEVEL OBSERVATIONS lrerracan Well Started: 10/31/2013 Well Completed: 10/31/2013
Depth to groundater is 2. 32' below top of
casing. Drill Rig: 8140 LS Driller. RCH
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
b (!)
N
0 N
0 cr: t5 ~ (/)
> z w ...,
0.. (.')
"' 0 ;:::
N <0 "' (!)
0 ...J
1-cr: <(
:2 (/)
...J ~ z w :2 z 0 a:: > z w
1-a:: 0 0.. w cr:
...J <( z (5
ii' 0
:2 ~ LL
0 w ~ a:: <( 0.. w (f)
~
0 ::J :;
t-o z
!!"
(!)
0 ...J
(.') z ii' 0 "' (f)
J: 1-
PROBE LOG NO. SSS-1 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
(.') LOCATION See Exhbit A-2 _,UJ w wz n. 0 € >Q 1: wa:: ....J WI-....JW (.) I ....J<( w !l.<D I 1-a::> ....J ::;;:2 n. n. wa:: n. <(:::> ~ w t-W :2 C/JZ 0 <(Ul
(.') s:ro <(
0 rJ)
DEPTH MATERIAL DESCRIPTION
'71 ~6 inches of stone -SSS-1-2 -/_,-~/ ~SIL TV CLAY ICL-MLI, orange red -
SANDY SIL TV CLAY ICL-MLI, gray brown, Old petroleum odor. -SSS-1-4 5-SSS-1-( ' -
~ 9.0 : SSS-1-8
Probe Terminated at 9 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS
lrerracon Probe Started: 7/25/2013 Probe Completed: 7/25/2013 \c
~-After Boring
Drill Rig: Driller:
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
1-0
CJ
N
0 N
0 cr: <( 0 z ;"=
(/) > z w
-, a. CJ
<'? 0 .... N
"' "' CJ s
~ <(
:2 (/)
-' ;"= z w :2 z
0 cr: 5 z w
~ 0 a. w cr:
;;! z (!j
~ 0
:2 0 cr: lL
0 w ~ if_ w (/)
!!o
0 ::; ;;
1--0 z
~
(!)
0 -' (!) z ~ 0 CD
(/)
J: 1--
PROBE LOG NO. 555-2 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
(9 LOCATION See Exhbit A-2 ...J(f) w
0 wz a.. wa:: ...J g >Q ~ WI--'w u :r: ...J<( a.rn I: w ::;;::;; 1-a::> --' a. a.. wa:: a.. <(:::> ~ w t-W ::;; (f)Z 0 <((f) (9 :;:rn <(
0 {/) DEPTH MATERIAL DESCRIPTION
I
'.5'\6 "nches of stone -SSS-2-2 SILTY SANP ISM!, with gravel, gray brown to orange, Slight petroleum odor. --
s-= SSS-2-4
II SSS-2-6 --SSS-2-8 9.0 -v
Probe Terminated at 9 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS lrerracon Probe Started: 7/25/2013 Probe Completed: 7/25/2013 ' After Boring __ \,L __
Drill Rig: Driller.
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
>--0 (.9
N ~
0 tl:
C\ ~ (/)
> z w ..,
D.. (.9
"' 0 ;::
N ;;; "' (.9
0 ...J
>-tl: <( ::;:
(j)
~ z w ::;: z 0 tl: > z LU
~
0 D.. w tl:
...J <( z Ci ii' 0 ::;:
~ u.
0 LU ~ tl: <( a. w (J)
!!o
0 ::J ~ >--0 z
~
(.9
0 ...J
(.9 z ii' 0 "' (J)
I >--
PROBE LOG NO. 555-6 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
'-' LOCATION See El<hbit A-2 ...J(j) w wz a_ 0 g >Q ~ wO: ...J W>-...JW (.) I ...J<( w a.m I 1-o:> __, ::;;::< a. 0.. wo: a_ <(::> <( w t-W ::;; (I)Z 0: 0 <((j) '-' $:m <(
nEPTH 0 (j) MATERIAL DESCRIPTION
1U ~inches of concrete -SSS-6-2 I"~ I!. -SILTY SANP ISM!, gray -4.5 -SSS-6-4 ~ CLAYEY SANP ISC), olive green to brown 5-SSS-6-6 --52 ij 8.5 -SSS-6-8
Probe Terminated at 8.5 Feet
The stratification lines represent the appra>omate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS lrerracon Probe Started: 7/25/2013 Probe Completed: 7/25/2013 'Q_ After Boring
Drill Rig: Driller.
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
..... 0 0
N c;
N
0 lY
C§ z ;":
(/)
> z w
~ Q.
0
"' 0 ;:
N ;;; 00
0 0 ....J ..... lY <( ::;; (/)
....J ;": z w ::;; z 0 lY 5 z w
..... lY 0 a. w lY
;i z ('j
"' 0 ::;; 0 lY "-
0 w ~ lY <( a. w (/)
!!,
0 ::::; ~ ..... 0 z
!!l
0 0 ....J
0 z "' 0 "' (/)
I .....
PROBE LOG NO. SSS-12 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
(!) LOCATION See Exhbit A-2 _,lfJ w w z (L 0 §: >Q ~ we:: ....J WI--....JW (.) I ....J<( w Q.al I ..... a::> -' ::;;::;; (L (L we:: (L <(::J <( w f-W ::;; lfJZ a:: 0 <((/) (!) ~al <(
inEPTH 0 (/) MATERIAL DESCRIPTION '1 ~3 inches of concrete -SSS-12--SILTY SANP ISM), gray to orange -SSS-12 -., .. 6.0 5-SSS-12--m11 s.o ~A!':jDY ~ILT (M!.l. with clay, tan -SS-12 Probe Terminated at 8 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in.,;itu these lransitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS lrerracon Probe Started: 10/10/2013 Probe Completed: 10/10/2013
No free water observed
Drill Rig: Drillec
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
1-0 <.!>
N 0 N
0 cr:
C§ z ~ > z w ..., 0.. <.!>
"' 0 ;:
N ;;; "' <::> 0 --' ~ <( ::;;
(/)
--' ~ z w ::;; z 0 cr: 5 z w
1-cr: 0 c.. w cr:
--' <( z 0 1i' 0 ::;;
0 cr: u.
0 w ~ cr: <( 0.. w (/)
~
0 ::::; ;;
1-0 z ra
<::> 0 --'
<::> z 1i' 0 w
(/) :;:
1-
PROBE LOG NO. SSS-13 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
{!) LOCATION See Exhbit A-2 -'(f) w 0 wz c.. wcr: --' §: >Q >-WI-1---'w (.) c.. co :E I --'<( w ::;;::;: 1-a::> _J c.. c.. wcr: c.. <(::> c:i w t-W (f)Z 0 <((/) :2 {!) :;:co <(
DEPTH 0 (f) MATERIAL DESCRIPTION
f-..0-5\6 inches of concrete -SS-13-SANoY SILT !Mll, gray ---SS-13 5.5 5-SS-13-SIL TV SAND ISM!. dark brown to orange --8.0 SS-13-Probe Terminated at 8 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS
lrerracan Probe Started: 10/10/2013 Probe Completed: 10/10/2013 No free water observed
Drill Rig: Driller.
3534 Rutherford Road
Taylors, South carolina Project No.: 86127103
1-0 (.!)
N ;; N
0 C! <(
0 z ~ (/)
> z w .., n. (.!)
"' 0
0::: N ;;;
"' (.!)
0 ...J :r <( ::;
(/)
...J ~ z UJ ::; z 0 C! ~ UJ
:r 0 n. w C!
...J <( z
(5
ii' 0 ::; 0 C! "-
0 w ~ it w (/)
!!o
0 ::J :;
1-0 z
'!!
(.!) g
(.!) z ii' 0 "' (/)
I' >-
PROBE LOG NO. SSS-16 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
(.9 LOCATION See Exhbit A-2 _,Ul UJ wz a._ 0 g >Q ~ wa: ...J WI-_,w (.) I ...J <( UJ a._ro J: I-n::> _J ::";:2
()._ ()._ wa: a._ <(::> <( w t-W ::;; CI)Z ex: 0 <((/) (.9 :s;ro <(
0 (/) DEPTH MATERIAL DESCRIPTION
mr ITf--.o.s'\4.inches of concrete -SS-16--3.5 ~Ati12Y ~ILI !MLl. with clay, tan -SS-16 SILTY CLAY (CL-MU, orange -5--SS-16-
' 8.0 -r SS-16-Probe Terminated at 8 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upcn
completion.
WATER LEVEL OBSERVATIONS lrerracon Probe Started: 10/10/2013 Probe Completed: 10/10/2013
No free water observed
Drill Rig: Drille~
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
1--Cl (!)
N ;; N
0 fY (:§ z i"' (/)
> z w
-, "-(!)
0') 0 ;::
N u;
<Xl
(')
0 _J
1--fY <( ::< (/)
_J i"' z w ::< z 0 fY 5 z w
t;:
0 "-w fY
_J <( z (5
ii:' 0 ::< 0 0:: lL
Cl w !:;: fY <( "-w (/)
!!=
Cl ::::; ::;
1--0 z
~
(!)
0 -'
(') z ii:' 0 "' (/) 'i' 1--
PROBE LOG NO. SSS-17 Page 1 of 1
PROJECT: IRC CLIENT: International Resistive Company, Inc.
Boone, North Carolina
SITE: 736 Greenway Drive
Boone, North Carolina
(9 LOCATION See Exhbit A-2 u::~ w
0 (l_ w<Y _J §: >Q >-WI--1-_,w u I -'<C w [L!Il I 1--rr:> -' ::;;::;; [L 0.. w<Y (l_ <(:::> <( w t-W ~ (f)Z 0:: 0 <((f) (9 5:"' <(
0 (/) DEPTH MATERIAL DESCRIPTION
IT · ~inches of concrete -~SS-17-SILTY SAND ISM!, with clay, gray --~SS-17 -5 -~SS-17-7.0 -
I I R • SANDY SILT fMU, with clay, gray -SS-17-
Probe Terminated at 8 Feet
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS lrerracon Probe Started: 10/10/2013 Probe Completed: 10/10/2013
No free water observed
Drill Rig: Driller:
3534 Rutherford Road
Taylors, South Carolina Project No.: 86127103
APPENDIX 8
Laboratory Analytical Reports
SC DHEC No: 32010
SHEALY ENVIRONMENTAL SERVICES, INC.
NELAC No: E87653
Case Narrative
Terracon Consultants, Inc.
Lot Number: OG26068
NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
GC/MS VOC
Screening results indicated matrix interferences so sample -008 was diluted SOX. All target compounds were non-detect at this dilution. A second
run was performed out of hold at no dilution. All QC passed for the out of hold run. Both runs have been reported.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 2 of78
Level 1 Report v2. 1
SHEALY ENVIRONM NTAL SERVICES, INC.
Sample Number Sample ID
001 SSS-1-8
002 SSS-2-8
003 SSS-3-6
004 SSS-4-2
005 SSS-5-6
006 SSS-6-2
007 SSS-6-6
008 SSS-7-4
009 SSS-8-6
010 SSS-9-6
011 SSS-1 0-8
(11 samples)
Shealy Environmental Services, Inc.
Sample Summary
Terracon Consultants, Inc.
Lot Number: OG26068
Matrix
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Date Sampled
07/25/2013 1040
07/25/2013 1100
07/25/2013 1130
07/25/2013 1150
07/25/2013 1215
07/25/2013 1225
07/25/2013 1230
07/25/2013 1255
07/25/2013 1305
07/25/2013 1330
07/25/2013 1355
Date Received
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
07/26/2013
Page: 3 of78
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Sample 10
001 SSS-1-8
003 SSS-3-6
003 SSS-3-6
003 SSS-3-6
004 SSS-4-2
004 SSS-4-2
004 SSS-4-2
004 SSS-4-2
004 SSS-4-2
004 SSS-4-2
004 SSS-4-2
005 SSS-5-6
005 SSS-5-6
005 SSS-5-6
006 SSS-6-2
006 SSS-6-2
006 SSS-6-2
006 SSS-6-2
007 SSS-6-6
007 SSS-6-6
007 SSS-6-6
008 SSS-7-4
008 SSS-7-4
008 SSS-7-4
008 SSS-7-4
009 SSS-8-6
009 SSS-8-6
009 SSS-8-6
009 SSS-8-6
009 SSS-8-6
009 SSS-8-6
009 SSS-8-6
010 SSS-9-6
010 SSS-9-6
011 SSS-1 0-8
011 SSS-1 0-8
(36 detections)
Shealy Environmental Services, Inc.
Executive Summary
Terracon Consultants, Inc.
Lot Number: OG26068
Matrix Parameter
Solid Acetone
Solid Acetone
Solid 2-Butanone (MEK)
Solid Fluoranthene
Solid 1, 1-Dichloroethane
Solid cis-1 ,2-Dichloroethene
Solid Tetrachloroethene
Solid Trichloroethene
Solid Xylenes (total)
Solid Lead
Solid Nickel
Solid Acetone
Solid Lead
Solid Nickel
Solid Acetone
Solid Tetrachloroethene
Solid Lead
Solid Nickel
Solid Acetone
Solid Lead
Solid Nickel
Solid Acetone
Solid Tetrachloroethene
Solid Lead
Solid Nickel
Solid Acetone
Solid 1, 1-Dichloroethane
Solid lsopropylbenzene
Solid Tetrachloroethene
Solid Trichloroethene
Solid Lead
Solid Nickel
Solid Lead
Solid Nickel
Solid Lead
Solid Nickel
Method
8260B
8260B
8260B
82700
8260B
8260B
8260B
8260B
8260B
6010C
6010C
8260B
6010C
6010C
8260B
8260B
6010C
6010C
8260B
6010C
6010C
8260B
8260B
6010C
6010C
8260B
8260B
8260B
8260B
8260B
6010C
6010C
6010C
6010C
6010C
6010C
106 Vantage Point Drive West Columbia, SC 29172 (803} 791-9700 Fax (803} 791-9111 www.shealylab.com
Result Q
190
79
13
660
19
39
970
20
9.0
15
8.3
36
19
9.2
23
880
47
14
130
10
5.8
73 H
19 H
47
23
52
5.6
7.5
300
7.0
29
17
33
5.9
20
11
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
mg/kg
mg/kg
ug/kg
mg/kg
mg/kg
ug/kg
ug/kg
mg/kg
mg/kg
ug/kg
mg/kg
mg/kg
ug/kg
ug/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Page
5
13
13
15
17
17
17
18
18
18
18
19
20
20
21
21
22
22
23
24
24
26
27
28
28
29
29
29
29
30
30
30
34
34
36
36
Page: 4 of78
Level1 Report v2.1
Client: Terracon Consultants, Inc. Laboratory ID: OG26068-001
Description: SSS-1-8 Matrix: Solid
Date Sampled:07/25/2013 1040 % Solids: 71.0 07/26/2013 2220
Date Received: 07/26/2013
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/30/2013 1435 AAC 26155 5.21
CAS Analytical
Parameter Number Method Result Q PQL Units
Acetone 67-64-1 82608 190 27 ug/kg
Benzene 71-43-2 8260B ND 6.8 ug/kg
Bromodichloromethane 75-27-4 8260B ND 6.8 ug/kg
Bromoform 75-25-2 8260B ND 6.8 ug/kg
Bromomethane (Methyl bromide) 74-83-9 8260B ND 6.8 ug/kg
2-Butanone (MEK) 78-93-3 8260B ND 14 ug/kg
Carbon disulfide 75-15-0 8260B ND 6.8 ug/kg
Carbon tetrachloride 56-23-5 8260B ND 6.8 ug/kg
Chlorobenzene 108-90-7 8260B ND 6.8 ug/kg
Chloroethane 75-00-3 8260B ND 6.8 ug/kg
Chloroform 67-66-3 8260B ND 6.8 ug/kg
Chloromethane (Methyl chloride) 74-87-3 8260B ND 6.8 ug/kg
Cyclohexane 110-82-7 8260B ND 6.8 ug/kg
1 ,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260B ND 6.8 ug/kg
Dibromochloromethane 124-48-1 8260B ND 6.8 ug/kg
1 ,2-Dibromoethane (EDB) 106-93-4 8260B ND 6.8 ug/k9
1 ,2-Dichlorobenzene 95-50-1 8260B ND 6.8 ug/kg
1 ,3-Dichlorobenzene 541-73-1 8260B ND 6.8 ug/kg
1 A-Dichlorobenzene 106-46-7 8260B ND 6.8 ug/kg
Dichlorodifluoromethane 75-71-8 8260B ND 6.8 ug/kg
1, 1-Dichloroethane 75-34-3 8260B ND 6.8 ug/kg
1 ,2-Dichloroethane 107-06-2 8260B ND 6.8 ug/kg
1, 1-Dichloroethene 75-35-4 8260B ND 6.8 ug/kg
cis-1 ,2-Dichloroethene 156-59-2 8260B ND 6.8 ug/kg
trans-1 ,2-Dichloroethene 156-60-5 8260B ND 6.8 ug/kg
1 ,2-Dichloropropane 78-87-5 8260B ND 6.8 ug/kg
cis-1 ,3-Dichloropropene 10061-01-5 8260B ND 6.8 ug/kg
trans-1 ,3-Dichloropropene 10061-02-6 8260B ND 6.8 ug/kg
Ethylbenzene 100-41-4 8260B ND 6.8 ug/kg
2-Hexanone 591-78-6 8260B ND 14 ug/kg
lsopropylbenzene 98-82-8 8260B ND 6.8 ug/kg
Methyl acetate 79-20-9 8260B ND 6.8 ug/kg
Methyl tertiary butyl ether (MTBE) 1634-04-4 8260B ND 6.8 ug/kg
4-Methyl-2-pentanone 108-10-1 8260B ND 14 ug/kg
Methylcyclohexane 108-87-2 8260B NO 6.8 ug/kg
Methylene chloride 75-09-2 8260B ND 6.8 ug/kg
Styrene 100-42-5 8260B ND 6.8 ug/kg
1,1 ,2,2-Tetrachloroethane 79-34-5 8260B ND 6.8 ug/kg
Tetrachloroethene 127-18-4 8260B ND 6.8 ug/kg
Toluene 108-88-3 8260B ND 6.8 ug/kg
POL = Practical quantitation limit 6" Detected in the method blank E "Ouantitation of compound exceeded the calibration range H "Out of holding time
ND " Not detected at or above the POL J" Estimated result< POL and:: MDL P The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Run
Page: 5 of 78
Level1 Report v2.1
Client: Terra con Consultants, Inc.
Description: SSS-1-8
Laboratory 10: OG26068-001
Matrix: Solid
Date Sampled:07/25/2013 1040
Date Received: 07/26/2013
% Solids: 71.0 07/26/2013 2220
Run Prep Method
1 5035
Parameter
Volatile Organic Compounds by GC/MS
Analytical Method
8260B
Dilution Analysis Date
1 07/30/2013 1435
Analyst
AAC
CAS Analytical
Number Method
Prep Date
Result Q
Batch
26155
PQL
Sample Wt.(g)
5.21
Units
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 8260B NO 6.8 ug/kg
1 ,2,4-Trichlorobenzene 120-82-1 8260B NO 6.8 ug/kg
1,1, 1-Trichloroethane 71-55-6 8260B NO 6.8 ug/kg
1,1 ,2-Trichloroethane 79-00-5 8260B NO 6.8 ug/kg
Trichloroethene 79-01-6 8260B NO 6.8 ug/kg
Trichlorofluoromethane 75-69-4 8260B NO 6.8 ug/kg
Vinyl chloride 75-01-4 8260B NO 6.8 ug/kg
Xylenes (total) 1330-20-7 8260B NO 6.8 ug/kg
Run 1 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 86 53-142
Bromofluorobenzene 114 47-138
Toluene-dB 99 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 82700 1 07/29/20131133 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units
Acenaphthene 83-32-9 82700 NO 460 ug/kg
Acenaphthylene 208-96-8 82700 NO 460 ug/kg
Acetophenone 98-86-2 82700 NO 460 ug/kg
Anthracene 120-12-7 82700 NO 460 ug/kg
Atrazine 1912-24-9 82700 NO 460 ug/kg
Benzaldehyde 100-52-7 82700 NO 1200 ug/kg
Benzo(a)anthracene 56-55-3 82700 NO 460 ug/kg
Benzo(a)pyrene 50-32-8 82700 NO 460 ug/kg
Benzo(b )fluoranthene 205-99-2 82700 NO 460 ug/kg
Benzo(g ,h, i)perylene 191-24-2 82700 NO 460 ug/kg
Benzo(k)fluoranthene 207-08-9 82700 NO 460 ug/kg
1,1 '-Biphenyl 92-52-4 82700 NO 460 ug/kg
4-Bromophenyl phenyl ether 101-55-3 82700 NO 460 ug/kg
Butyl benzyl phthalate 85-68-7 82700 NO 460 ug/kg
Caprolactam 105-60-2 82700 NO 1200 ug/kg
Carbazole 86-74-8 82700 NO 460 ug/kg
4-Chloro-3-methyl phenol 59-50-7 82700 NO 460 ug/kg
4-Chloroaniline 106-47-8 82700 NO 460 ug/kg
bis(2-Chloroethoxy)methane 111-91-1 82700 NO 460 ug/kg
bis(2-Chloroethyl)ether 111-44-4 82700 NO 460 ug/kg
POL ; Practical quantitation limit B ; Detected in the method blank E ; Ouantitation of compound exceeded the calibration range H ; Out of holding time
NO ; Not detected at or above the POL J ; Estimated result < POL and;: MDL P ; The RPD between two GC columns exceeds 40% N ; Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Run
Run
Page: 6 of78
Level1 Report v2.1
Client:Terracon Consultants, Inc. Laboratory ID: OG26068-001
Description: SSS-1-8 Matrix: Solid
Date Sampled:07/25/20131040 % Solids: 71.0 07/26/2013 2220
Date Received: 07/26/2013
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 07/29/2013 1133 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 460 ug/kg
2-Chloronaphthalene 91-58-7 8270D ND 460 ug/kg
2-Chlorophenol 95-57-8 8270D ND 460 ug/kg
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 460 ug/kg
Chrysene 218-01-9 8270D ND 460 ug/kg
Di-n-butyl phthalate 84-74-2 8270D ND 460 ug/kg
Di-n-octylphthalate 117-84-0 8270D ND 460 ug/kg
Dibenzo(a,h)anthracene 53-70-3 8270D ND 460 ug/kg
Dibenzofuran 132-64-9 8270D ND 460 ug/kg
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1200 ug/kg
2,4-Dichlorophenol 120-83-2 8270D ND 460 ug/kg
Diethylphthalate 84-66-2 8270D ND 460 ug/kg
Dimethyl phthalate 131-11-3 8270D ND 460 ug/kg
2,4-Dimethylphenol 105-67-9 8270D ND 460 ug/kg
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1200 ug/kg
2,4-Dinitrophenol 51-28-5 8270D NO 1200 ug/kg
2,4-0initrotoluene 121-14-2 82700 NO 460 ug/kg
2,6-0initrotoluene 606-20-2 82700 NO 460 ug/kg
bis(2-Ethylhexyl)phthalate 117-81-7 8270D NO 460 ug/kg
Fluoranthene 206-44-0 8270D NO 460 ug/kg
Fluorene 86-73-7 82700 NO 460 ug/kg
Hexachlorobenzene 118-74-1 82700 NO 460 ug/kg
Hexachlorobutadiene 87-68-3 82700 NO 460 ug/kg
Hexachlorocyclopentadiene 77-47-4 82700 NO 1200 ug/kg
Hexachloroethane 67-72-1 82700 ND 460 ug/kg
lndeno(1 ,2,3-c,d)pyrene 193-39-5 82700 ND 460 ug/kg
lsophorone 78-59-1 8270D NO 460 ug/kg
2-Methylnaphthalene 91-57-6 8270D NO 460 ug/kg
2-Methylphenol 95-48-7 82700 NO 460 ug/kg
3 & 4-Methylphenol 106-44-5 82700 NO 930 ug/kg
N-Nitrosodi-n-propylamine 621-64-7 82700 NO 460 ug/kg
N-Nitrosodiphenylam ine (Diphenylamine) 86-30-6 82700 NO 460 ug/kg
Naphthalene 91-20-3 8270D ND 460 ug/kg
2-Nitroaniline 88-74-4 8270D NO 460 ug/kg
3-Nitroaniline 99-09-2 8270D NO 460 ug/kg
4-Nitroaniline 100-01-6 8270D NO 460 ug/kg
Nitrobenzene 98-95-3 82700 NO 460 ug/kg
2-Nitrophenol 88-75-5 82700 NO 460 ug/kg
4-Nitrophenol 100-02-7 82700 NO 1200 ug/kg
Pentachlorophenol 87-86-5 82700 NO 1200 ug/kg
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result< PQL and': MDL P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, a!l soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Run
Page: 7 of78
Level 1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-1-8
Laboratory ID: OG26068-001
Matrix: Solid
Date Sampled:07/25/2013 1040
Date Received: 07/26/2013
%Solids: 71.0 07/26/2013 2220
Run Prep Method
1 3550C
Parameter
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2 ,4, 6-T richlorophenol
Surrogate
2,4,6-Tribromophenol
2-Fiuorobiphenyl
2-Fiuorophenol
Nitrobenzene-d5
Phenol-d5
T erphenyl-d 14
POL = Practical quantitation limit
Semivolatile Organic Compounds by GC/MS
Analytical Method
8270D
Q
Dilution Analysis Date
1 07/29/2013 1133
Analyst
JRG
CAS Analytical
Number Method
85-01-8 8270D
108-95-2 8270D
129-00-0 8270D
95-95-4 8270D
88-06-2 8270D
Run 1 Acceptance
%Recovery Limits
69 30-117
64 33-102
74 28-104
57 22-109
79 27-103
90 41-120
Prep Date Batch
07/27/2013 1357 25971
Result Q PQL
ND 460
ND 460
ND 460
ND 460
ND 460
B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
NO = Not detected at or above the POL J = Estimated result < POL and :': MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 {803) 791-9700 Fax [phone] www.shealylab.com
Run
Page: 8 of78
Level 1 Report v2 .1
Client: Terracon Consultants, Inc.
Description: SSS-2-8
Laboratory 10: OG26068-002
Matrix: Solid
Date Sampled:07/25/2013 1100
Date Received:07/26/2013
% Solids: 88.0 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
1 5035
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Analytical Method
8260B
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Ch lorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MT8E)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Dilution Analysis Date Analyst
AAC 1 07/30/2013 1213
CAS
Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
Analytical
Method
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
8260B
82608
8260B
82608
82608
8260B
8260B
82608
82608
8260B
8260B
Prep Date
Result Q
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Batch
26155
PQL
20
5.1
5.1
5.1
5.1
10
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
10
5.1
5.1
5.1
10
5.1
5.1
5.1
5.1
5.1
5.1
Sample Wt.(g)
5.57
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
POL :::: Practical quantitation limit B =Detected in the method blank E = Ouantitation of compound exceeded the calibration range H =Out of holding time
ND Not detected at or above the POL J = Estimated result< POL and.:: MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803} 791-9700 Fax [phone] www.shealylab.com
Run
Page: 9 of 78
Level1 Report v2.1
Client: Terra con Consultants, Inc.
Description: SSS-2-8
Laboratory ID: OG26068-002
Matrix: Solid
Date Sampled:07/25/2013 1100
Date Received: 07/26/2013
%Solids: 88.0 07/26/2013 2220
Run Prep Method
1 5035
Parameter
Volatile Organic Compounds by GC/MS
Analytical Method
8260B
Dilution Analysis Date
1 07/30/2013 1213
Analyst
AAC
CAS Analytical
Number Method
Prep Date
Result Q
Batch
26155
PQL
Sample Wt.(g)
5.57
Units
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 8260B ND 5.1 ug/kg
1 ,2,4-Trichlorobenzene 120-82-1 8260B ND 5.1 ug/kg
1,1, 1-Trichloroethane 71-55-6 8260B ND 5.1 ug/kg
1,1 ,2-Trichloroethane 79-00-5 8260B ND 5.1 ug/kg
Trichloroethene 79-01-6 8260B ND 5.1 ug/kg
Trichlorofluoromethane 75-69-4 8260B ND 5.1 ug/kg
Vinyl chloride 75-01-4 8260B ND 5.1 ug/kg
Xylenes (total) 1330-20-7 82608 ND 5.1 ug/kg
Run 1 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 83 53-142
Bromofluorobenzene 101 47-138
Toluene-d8 85 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 07/29/2013 1159 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units
Acenaphthene 83-32-9 8270D ND 370 ug/kg
Acenaphthylene 208-96-8 8270D ND 370 ug/kg
Acetophenone 98-86-2 8270D ND 370 ug/kg
Anthracene 120-12-7 8270D ND 370 ug/kg
Atrazine 1912-24-9 8270D ND 370 ug/kg
Benzaldehyde 100-52-7 8270D ND 930 ug/kg
Benzo(a)anthracene 56-55-3 8270D ND 370 ug/kg
Benzo(a)pyrene 50-32-8 8270D ND 370 ug/kg
Benzo(b )fluoranthene 205-99-2 8270D ND 370 ug/kg
Benzo(g,h,i)perylene 191-24-2 8270D ND 370 ug/kg
Benzo(k)fluoranthene 207-08-9 8270D ND 370 ug/kg
1, 1'-Biphenyl 92-52-4 8270D ND 370 ug/kg
4-Bromophenyl phenyl ether 101-55-3 8270D ND 370 ug/kg
Butyl benzyl phthalate 85-68-7 8270D ND 370 ug/kg
Caprolactam 105-60-2 8270D ND 930 ug/kg
Carbazole 86-74-8 8270D ND 370 ug/kg
4-Chloro-3-methyl phenol 59-50-7 8270D ND 370 ug/kg
4-Chloroaniline 106-47-8 8270D ND 370 ug/kg
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 370 ug/kg
bis(2-Chloroethyl)ether 111-44-4 8270D ND 370 ug/kg
POL " Practical quantitation limit B " Detected in the method blank E; Ouantitation of compound exceeded the calibration range H ; Out of holding time
ND " Not detected at or above the POL J " Estimated result < POL and z: MDL P ; The RPD between two GC columns exceeds 40% N ; Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Run
Run
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 10 of 78
Level 1 Report v2.1
Client:Terracon Consultants, Inc. Laboratory ID: OG26068-002
Description: SSS-2-8 Matrix: Solid
Date Sampled:07/25/20131100 %Solids: 88.0 07/26/2013 2220
Date Received: 07/26/2013
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 82700 1 07/29/20131159 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units Run
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 370 ug/kg
2-Chloronaphthalene 91-58-7 8270D ND 370 ug/kg
2-Chlorophenol 95-57-8 8270D ND 370 ug/kg
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 370 ug/kg
Chrysene 218-01-9 8270D NO 370 ug/kg
Di-n-butyl phthalate 84-74-2 8270D ND 370 ug/kg
Di-n-octylphthalate 117-84-0 8270D ND 370 ug/kg
Dibenzo(a,h)anthracene 53-70-3 82700 ND 370 ug/kg
Dibenzofuran 132-64-9 82700 ND 370 ug/kg
3,3'-Dichlorobenzidine 91-94-1 8270D ND 930 ug/kg
2 ,4-Dichlorophenol 120-83-2 8270D ND 370 ug/kg
Oiethylphthalate 84-66-2 8270D ND 370 ug/kg
Dimethyl phthalate 131-11-3 82700 NO 370 ug/kg
2,4-Dimethylphenol 105-67-9 8270D NO 370 ug/kg
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 930 ug/kg
2,4-0initrophenol 51-28-5 8270D ND 930 ug/kg
2 ,4-Dinitrotoluene 121-14-2 8270D ND 370 ug/kg
2,6-Dinitrotoluene 606-20-2 8270D NO 370 ug/kg
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 370 ug/kg
Fluoranthene 206-44-0 8270D ND 370 ug/kg
Fluorene 86-73-7 8270D ND 370 ug/kg
Hexachlorobenzene 118-74-1 82700 ND 370 ug/kg
Hexachlorobutadiene 87-68-3 8270D NO 370 ug/kg
Hexachlorocyclopentadiene 77-47-4 8270D NO 930 ug/kg
Hexachloroethane 67-72-1 8270D ND 370 ug/kg
lndeno(1 ,2,3-c,d)pyrene 193-39-5 8270D ND 370 ug/kg
lsophorone 78-59-1 82700 ND 370 ug/kg
2-Methylnaphthalene 91-57-6 8270D NO 370 ug/kg
2-Methylphenol 95-48-7 8270D ND 370 ug/kg
3 & 4-Methylphenol 106-44-5 8270D ND 750 ug/kg
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 370 ug/kg
N-N itrosodiphenylamine (Diphenylamine) 86-30-6 8270D NO 370 ug/kg
Naphthalene 91-20-3 8270D NO 370 ug/kg
2-Nitroaniline 88-74-4 8270D NO 370 ug/kg
3-Nitroaniline 99-09-2 8270D ND 370 ug/kg
4-N itroan iline 100-01-6 82700 ND 370 ug/kg
Nitrobenzene 98-95-3 82700 ND 370 ug/kg
2-Nitrophenol 88-75-5 8270D NO 370 ug/kg
4-N itrophenol 100-02-7 8270D NO 930 ug/kg
Pentachlorophenol 87-86-5 8270D ND 930 ug/kg
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND =Not detected at or above the POL J = Estimated result< POL and 2: MDL P ;:;;; The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 11 of 78
Level 1 Report v2.1
Client: Terra con Consultants, Inc.
Description: SSS-2·8
Laboratory ID: OG26068-002
Matrix: Solid
Date Sampled:07/25/2013 1100
Date Received: 07/26/2013
%Solids: 88.0 07/26/2013 2220
Run Prep Method
1 3550C
Parameter
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
2,4,6-Tribromophenol
2-Fiuorobiphenyl
2-Fiuorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
POL = Practical quantitation limit
Semivolatile Organic Compounds by GC/MS
Analytical Method
8270D
Q
Dilution Analysis Date
1 07/29/20131159
Analyst
JRG
CAS Analytical
Number Method
85-01-8 8270D
108-95-2 8270D
129-00-0 8270D
95-95-4 8270D
88-06-2 8270D
Run 1 Acceptance
%Recovery Limits
88 30-117
80 33-102
76 28-104
75 22-109
80 27-103
117 41-120
Prep Date Batch
07/27/2013 1357 25971
Result Q PQL
ND 370
ND 370
ND 370
ND 370
ND 370
B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
Units Run
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
NO = Not detected at or above the POL J = Estimated result< POL and ::: MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 12 of 78
Level 1 Report v2 .1
Client: Terracon Consultants, Inc.
Description: SSS-3-6
Date Sampled:07/25/2013 1130
Date Received: 07/26/2013
Laboratory ID: OG26068-003
Matrix: Solid
% Solids: 62.3 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
2 5035
Parameter
Acetone
Benzene
B rom od ich lorom ethane
Bromoform
Analytical Method
8260B
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Dilution Analysis Date Analyst
AAC 1 07/31/2013 1439
CAS
Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
Analytical
Method
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
Prep Date
Result Q
79
ND
ND
ND
ND
13
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Batch
26252
Sample Wt.(g)
6.81
PQL Units
24
5.9
5.9
5.9
5.9
12
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
12
5.9
5.9
5.9
12
5.9
5.9
5.9
5.9
5.9
5.9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Run
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
POL= Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H =Out of holding time
ND = Not detected at or above the POL J = Estimated result < POL and ;: MDL P =The RPD between two GC columns exceeds 40% N =Recovery is out of criteria
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 13 of 78
Level 1 Report v2.1
Client: Terra con Consultants, Inc.
Description: SSS-3-6
Laboratory ID: OG26068-003
Matrix: Solid
Date Sampled:07/25/2013 1130
Date Received: 07/26/2013
%Solids: 62.3 07/26/2013 2220
Run Prep Method
2 5035
Parameter
Volatile Organic Compounds by GC/MS
Analytical Method
8260B
Dilution Analysis Date
1 07/31/20131439
Analyst
AAC
CAS Analytical
Number Method
Prep Date
Result Q
Batch
26252
PQL
Sample Wt.(g)
6.81
Units
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B NO 5.9 ug/kg
1,2,4-Trichlorobenzene 120-82-1 8260B NO 5.9 ug/kg
1,1,1-Trichloroethane 71-55-6 8260B NO 5.9 ug/kg
1,1,2-Trichloroethane 79-00-5 8260B NO 5.9 ug/kg
Trichloroethene 79-01-6 8260B NO 5.9 ug/kg
Trichlorofluoromethane 75-69-4 8260B NO 5.9 ug/kg
Vinyl chloride 75-01-4 8260B NO 5.9 ug/kg
Xylenes (total) 1330-20-7 8260B NO 5.9 ug/kg
Run 2 Acceptance
Surrogate Q %Recovery Limits
1,2-Dichloroethane-d4 96 53-142
Bromofluorobenzene 88 47-138
Toluene-dB 94 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 82700 1 07/29/2013 1225 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units
Acenaphthene 83-32-9 82700 NO 530 ug/kg
Acenaphthylene 208-96-8 82700 NO 530 ug/kg
Acetophenone 98-86-2 82700 NO 530 ug/kg
Anthracene 120-12-7 82700 NO 530 ug/kg
Atrazine 1912-24-9 82700 NO 530 ug/kg
Benzaldehyde 100-52-7 82700 NO 1300 ug/kg
Benzo(a)anthracene 56-55-3 82700 NO 530 ug/kg
Benzo( a )pyrene 50-32-8 82700 NO 530 ug/kg
Benzo(b )fluoranthene 205-99-2 82700 NO 530 ug/kg
Benzo(g,h,i)perylene 191-24-2 82700 NO 530 ug/kg
Benzo(k)fluoranthene 207-08-9 82700 NO 530 ug/kg
1,1 '-Biphenyl 92-52-4 82700 NO 530 ug/kg
4-Bromophenyl phenyl ether 101-55-3 82700 NO 530 ug/kg
Butyl benzyl phthalate 85-68-7 82700 NO 530 ug/kg
Caprolactam 105-60-2 82700 NO 1300 ug/kg
Carbazole 86-74-8 82700 NO 530 ug/kg
4-Chloro-3-methyl phenol 59-50-7 82700 NO 530 ug/kg
4-Chloroaniline 106-47-8 82700 NO 530 ug/kg
bis(2-Chloroethoxy)methane 111-91-1 82700 NO 530 ug/kg
bis(2-Chloroethyl)ether 111-44-4 82700 NO 530 ug/kg
POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result< PQL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a ''W ..
Run
2
2
2
2
2
2
2
2
Run
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 14 of 78
Level 1 Report v2.1
Client:Terracon Consultants, Inc. Laboratory ID: OG26068-003
Description: SSS-3-6 Matrix: Solid
Date Sampled:07/25/2013 1130 % Solids: 62.3 07/26/2013 2220
Date Received: 07/26/2013
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 07/29/2013 1225 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units Run
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 530 ug/kg
2-Chloronaphthalene 91-58-7 8270D ND 530 ug/kg
2-Chlorophenol 95-57-8 8270D ND 530 ug/kg
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 530 ug/kg
Chrysene 218-01-9 8270D ND 530 ug/kg
Di-n-butyl phthalate 84-74-2 8270D ND 530 ug/kg
Di-n-octylphthalate 117-84-0 8270D ND 530 ug/kg
Dibenzo(a,h)anthracene 53-70-3 8270D ND 530 ug/kg
Dibenzofuran 132-64-9 8270D ND 530 ug/kg
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1300 ug/kg
2,4-Dichlorophenol 120-83-2 8270D ND 530 ug/kg
Diethylphthalate 84-66-2 8270D ND 530 ug/kg
Dimethyl phthalate 131-11-3 8270D ND 530 ug/kg
2,4-Dimethylphenol 105-67-9 8270D ND 530 ug/kg
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1300 ug/kg
2,4-Dinitrophenol 51-28-5 8270D ND 1300 ug/kg
2,4-Dinitrotoluene 121-14-2 8270D ND 530 ug/kg
2,6-Dinitrotoluene 606-20-2 8270D ND 530 ug/kg
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 530 ug/kg
Fluoranthene 206-44-0 8270D 660 530 ug/kg
Fluorene 86-73-7 8270D ND 530 ug/kg
Hexachlorobenzene 118-74-1 8270D ND 530 ug/kg
Hexachlorobutadiene 87-68-3 8270D ND 530 ug/kg
Hexachlorocyclopentadiene 77-47-4 8270D ND 1300 ug/kg
Hexachloroethane 67-72-1 8270D ND 530 ug/kg
lndeno(1 ,2,3-c,d)pyrene 193-39-5 8270D ND 530 ug/kg
lsophorone 78-59-1 8270D ND 530 ug/kg
2-Methylnaphthalene 91-57-6 8270D ND 530 ug/kg
2-Methylphenol 95-48-7 8270D ND 530 ug/kg
3 & 4-Methylphenol 106-44-5 8270D ND 1100 ug/kg
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 530 ug/kg
N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270D ND 530 ug/kg
Naphthalene 91-20-3 8270D ND 530 ug/kg
2-Nitroaniline 88-74-4 8270D ND 530 ug/kg
3-Nitroaniline 99-09-2 8270D ND 530 ug/kg
4-Nitroaniline 100-01-6 8270D ND 530 ug/kg
Nitrobenzene 98-95-3 8270D ND 530 ug/kg
2-Nitrophenol 88-75-5 8270D ND 530 ug/kg
4-Nitrophenol 100-02-7 8270D ND 1300 ug/kg
Pentachlorophenol 87-86-5 8270D ND 1300 ug/kg
POL= Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND =Not detected at or above the POL J = Estimated result< PQL and~ MDL P =The RPD between two GC columns exceeds 40% N = Recovery '1s out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 15 of78
Level 1 Report v2.1
Client:Terracon Consultants, Inc.
Description: SSS-3·6
Laboratory ID: OG26068-003
Matrix: Solid
Date Sampled:07/25/2013 1130
Date Received: 07/26/2013
%Solids: 62.3 07/26/2013 2220
Run Prep Method
1 3550C
Parameter
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
2,4,6-Tribromophenol
2-Fiuorobiphenyl
2-Fiuorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
POL = Practical quantitation limit
Semivolatile Organic Compounds by GC/MS
Analytical Method
8270D
Q
Dilution Analysis Date
1 07/29/2013 1225
Analyst
JRG
CAS Analytical
Number Method
85-01-8 8270D
108-95-2 8270D
129-00-0 8270D
95-95-4 8270D
88-06-2 8270D
Run 1 Acceptance
%Recovery Limits
82 30-117
63 33-102
75 28-104
63 22-109
78 27-103
100 41-120
Prep Date Batch
07/27/2013 1357 25971
Result Q PQL
ND 530
ND 530
ND 530
ND 530
ND 530
B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
Units Run
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND =Not detected at or above the POL J = Estimated result< POL and ~ MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 16 of 78
Level 1 Report v2.1
Client:Terracon Consultants, Inc. Laboratory ID: OG26068-004
Description: SSS-4-2 Matrix: Solid
Date Sampled:07/25/2013 1150 %Solids: 84.5 07/26/2013 2220
Date Received: 07/26/2013
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/30/2013 1300 AAC 26155 6.45
2 5035 8260B 50 07/31/20131614 AAC 26253 5.84
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 82608 ND 18 ug/kg
Benzene 71-43-2 82608 ND 4.6 ug/kg
Bromodichloromethane 75-27-4 82608 ND 4.6 ug/kg
Bromoform 75-25-2 8260B ND 4.6 ug/kg
Bromomethane (Methyl bromide) 74-83-9 82608 ND 4.6 ug/kg
2-Butanone (MEK) 78-93-3 82608 ND 9.2 ug/kg
Carbon disulfide 75-15-0 82608 ND 4.6 ug/kg
Carbon tetrachloride 56-23-5 82608 ND 4.6 ug/kg
Chlorobenzene 108-90-7 8260B ND 4.6 ug/kg
Chloroethane 75-00-3 8260B ND 4.6 ug/kg
Chloroform 67-66-3 8260B ND 4.6 ug/kg
Chloromethane (Methyl chloride) 74-87-3 82608 ND 4.6 ug/kg
Cyclohexane 110-82-7 82608 ND 4.6 ug/kg
1 ,2-Dibromo-3-chloropropane (DBCP) 96-12-8 82608 ND 4.6 ug/kg
Dibromochloromethane 124-48-1 82608 ND 4.6 ug/kg
1 ,2-Dibromoethane (ED8) 106-93-4 82608 ND 4.6 ug/kg
1 ,2-Dichlorobenzene 95-50-1 82608 ND 4.6 ug/kg
1 ,3-Dichlorobenzene 541-73-1 82608 ND 4.6 ug/kg
1 A-Dichlorobenzene 106-46-7 82608 ND 4.6 ug/kg
Dichlorodifluoromethane 75-71-8 82608 ND 4.6 ug/kg
1, 1-Dichloroethane 75-34-3 82608 19 4.6 ug/kg
1 ,2-Dichloroethane 107-06-2 8260B ND 4.6 ug/kg
1, 1-Dichloroethene 75-35-4 8260B ND 4.6 ug/kg
cis-1 ,2-Dichloroethene 156-59-2 82608 39 4.6 ug/kg
trans-1 ,2-Dichloroethene 156-60-5 82608 ND 4.6 ug/kg
1 ,2-Dichloropropane 78-87-5 82608 ND 4.6 ug/kg
cis-1 ,3-Dichloropropene 10061-01-5 82608 ND 4.6 ug/kg
trans-1 ,3-Dichloropropene 10061-02-6 82608 ND 4.6 ug/kg
Ethyl benzene 100-41-4 8260B ND 4.6 ug/kg
2-Hexanone 591-78-6 8260B ND 9.2 ug/kg
lsopropylbenzene 98-82-8 82608 ND 4.6 ug/kg
Methyl acetate 79-20-9 82608 ND 4.6 ug/kg
Methyl tertiary butyl ether (MT8E) 1634-04-4 82608 ND 4.6 ug/kg
4-Methyl-2-pentanone 108-10-1 8260B ND 9.2 ug/kg
Methylcyclohexane 108-87-2 8260B ND 4.6 ug/kg
Methylene chloride 75-09-2 8260B ND 4.6 ug/kg
Styrene 100-42-5 82608 ND 4.6 ug/kg
1,1 ,2,2-Tetrachloroethane 79-34-5 82608 ND 4.6 ug/kg
Tetrachloroethene 127-18-4 82608 970 250 ug/kg 2
POL= Practical quantitation limit B Detected in the method blank E = Ouantitation of compound exceeded the calibration range H =Out of holding time
ND = Not detected at or above the POL J = Estimated result< POL and :0: MDL P::: The RPD between two GC columns exceeds 40% N =Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 17 of 78
Level 1 Report v2.1
Client:Terracon Consultants, Inc.
Description: SSS-4-2
Laboratory ID: OG26068-004
Matrix: Solid
Date Sampled:07/25/2013 1150
Date Received: 07/26/2013
%Solids: 84.5 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
1 5035
2 5035
Parameter
Toluene
Analytical Method
82608
82608
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
1 ,2-Dichloroethane-d4
8romofluorobenzene
Toluene-d8
Run Prep Method
1 30508
Parameter
Lead
Nickel
Q
Analytical Method
6010C
Dilution Analysis Date
1 07/30/2013 1300
50 07/31/2013 1614
Analyst
AAC
AAC
CAS Analytical
Number Method
108-88-3 82608
76-13-1 82608
120-82-1 82608
71-55-6 82608
79-00-5 82608
79-01-6 8260B
75-69-4 82608
75-01-4 82608
1330-20-7 8260B
Prep Date
Result Q
ND
ND
NO
NO
NO
20
ND
ND
9.0
Run 1 Acceptance Run 2 Acceptance
%Recovery limits Q %Recovery limits
82 53-142 107 53-142
108 47-138 96 47-138
94 68-124 98 68-124
ICP-AES
Dilution Analysis Date Analyst Prep Date
1 07/31/2013 0617 CDF 07/29/20131017
CAS Analytical
Number Method Result Q
7439-92-1 6010C 15
7440-02-0 6010C 8.3
Batch
26155
26253
Sample Wt.(g)
6.45
5.84
PQL Units
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
4.6 ug/kg
Batch
25994
PQL Units
0.58 mg/kg
2.3 mg/kg
Run
1
1
Run
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result< PQL and~ MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 18 of 78
Level1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-5-6
Date Sampled:07/25/2013 1215
Date Received: 07/26/2013
Laboratory ID: OG26068-005
Matrix: Solid
% Solids: 7 4.4 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
2 5035
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Analytical Method
8260B
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (OBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-0ichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-0ichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Dilution Analysis Date
1 07/31/2013 1503
Analyst
AAC
CAS Analytical
Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
Method
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
Prep Date
Result Q
36
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
NO
NO
NO
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
Batch
26252
PQL
21
5.3
5.3
5.3
5.3
11
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
11
5.3
5.3
5.3
11
5.3
5.3
5.3
5.3
5.3
5.3
Sample Wt.(g)
6.32
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Run
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
POL::: Practical quantitation limit B =Detected in the method blank E Ouantitation of compound exceeded the calibration range H = Out of holding time
ND Not detected at or above the POL J = Estimated result< POL and.:: MDL P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 19 of 78
Level 1 Report v2.1
Client: Terra con Consultants, Inc.
Description: SSS-5-6
Laboratory ID: OG26068-005
Matrix: Solid
Date Sampled:07/25/2013 1215
Date Received: 07/26/2013
%Solids: 74.4 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 82608 1 07/31/2013 1503 AAC 26252 6.32
CAS Analytical
Parameter Number Method Result Q PQL Units Run
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 82608 NO 5.3 ug/kg 2
1 ,2,4-Trichlorobenzene 120-82-1 82608 NO 5.3 ug/kg 2
1,1, 1-Trichloroethane 71-55-6 82608 NO 5.3 ug/kg 2
1,1 ,2-Trichloroethane 79-00-5 82608 NO 5.3 ug/kg 2
Trichloroethene 79-01-6 82608 NO 5.3 ug/kg 2
Trichlorofluoromethane 75-69-4 82608 NO 5.3 ug/kg 2
Vinyl chloride 75-01-4 82608 NO 5.3 ug/kg 2
Xylenes (total) 1330-20-7 82608 NO 5.3 ug/kg 2
Run 2 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 92 53-142
8romofluorobenzene 87 47-138
Toluene-dB 99 68-124
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 30508 6010C 1 07/31/2013 0629 CDF 07/29/2013 1017 25994
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Lead 7439-92-1 6010C 19 0.63 mg/kg 1
Nickel 7440-02-0 6010C 9.2 2.5 mg/kg
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result< POL and:': MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 20 of 78
Level 1 Report v2.1
Client: Terracon Consultants, Inc. Laboratory ID: OG26068-006
Description: SSS-6-2 Matrix: Solid
Date Sampled:07/25/2013 1225 %Solids: 84.1 07/26/2013 2220
Date Received: 07/26/2013
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/30/2013 1348 AAC 26155 6.70
3 5035 8260B 50 08/05/20 13 1448 AAC 26521 6.07
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 82608 23 18 ug/kg
Benzene 71-43-2 8260B NO 4.4 ug/kg
Bromodichloromethane 75-27-4 8260B NO 4.4 ug/kg
Bromoform 75-25-2 8260B NO 4.4 ug/kg
Bromomethane (Methyl bromide) 74-83-9 8260B NO 4.4 ug/kg
2-Butanone (MEK) 78-93-3 8260B NO 8.9 ug/kg
Carbon disulfide 75-15-0 82608 NO 4.4 ug/kg
Carbon tetrachloride 56-23-5 8260B NO 4.4 ug/kg
Chlorobenzene 108-90-7 8260B NO 4.4 ug/kg
Chloroethane 75-00-3 8260B NO 4.4 ug/kg
Chloroform 67-66-3 8260B NO 4.4 ug/kg
Chloromethane (Methyl chloride) 74-87-3 8260B NO 4.4 ug/kg
Cyclohexane 110-82-7 8260B NO 4.4 ug/kg
1 ,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260B NO 4.4 ug/kg
Dibromochloromethane 124-48-1 8260B NO 4.4 ug/kg
1 ,2-Dibromoethane (EDB) 106-93-4 8260B ND 4.4 ug/kg
1 ,2-Dichlorobenzene 95-50-1 8260B NO 4.4 ug/kg
1 ,3-Dichlorobenzene 541-73-1 8260B NO 4.4 ug/kg
1 A-Dichlorobenzene 106-46-7 8260B NO 4.4 ug/kg
Dichlorodifluoromethane 75-71-8 8260B NO 4.4 ug/kg
1, 1-Dichloroethane 75-34-3 8260B NO 4.4 ug/kg
1 ,2-Dichloroethane 107-06-2 8260B NO 4.4 ug/kg
1, 1-Dichloroethene 75-35-4 8260B NO 4.4 ug/kg
cis-1 ,2-Dichloroethene 156-59-2 8260B NO 4.4 ug/kg
trans-1 ,2-Dichloroethene 156-60-5 8260B NO 4.4 ug/kg
1 ,2-Dichloropropane 78-87-5 8260B NO 4.4 ug/kg
cis-1 ,3-Dichloropropene 10061-01-5 8260B NO 4.4 ug/kg
trans-1 ,3-Dichloropropene 10061-02-6 8260B NO 4.4 ug/kg
Ethylbenzene 100-41-4 8260B NO 4.4 ug/kg
2-Hexanone 591-78-6 82608 NO 8.9 ug/kg
lsopropylbenzene 98-82-8 8260B NO 4.4 ug/kg
Methyl acetate 79-20-9 8260B NO 4.4 ug/kg
Methyl tertiary butyl ether (MTBE) 1634-04-4 82608 NO 4.4 ug/kg
4-Methyl-2-pentanone 108-10-1 8260B NO 8.9 ug/kg
Methylcyclohexane 108-87-2 8260B NO 4.4 ug/kg
Methylene chloride 75-09-2 8260B NO 4.4 ug/kg
Styrene 100-42-5 8260B NO 4.4 ug/kg
1,1 ,2,2-Tetrachloroethane 79-34-5 8260B NO 4.4 ug/kg
Tetrachloroethene 127-18-4 82608 880 240 ug/kg 3
POL= Practical quantitation limit 8 = Detected in the method blank E Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result< POL and:;: MDL P = The RPD between two GC columns exceeds 40% N ;:::; Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 21 of78
Level 1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-6-2
Laboratory 10: OG26068-006
Matrix: Solid
Date Sampled:07/25/2013 1225
Date Received: 07/26/2013
%Solids: 84.1 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 82608 1 07/30/2013 1348 AAC 26155 6.70
3 5035 82608 50 08/05/2013 1448 AAC 26521 6.07
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Toluene 108-88-3 82608 NO 4.4 ug/kg
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 82608 NO 4.4 ug/kg
1 ,2,4-Trichlorobenzene 120-82-1 82608 NO 4.4 ug/kg
1,1, 1-Trichloroethane 71-55-6 82608 NO 4.4 ug/kg
1,1 ,2-Trichloroethane 79-00-5 82608 NO 4.4 ug/kg
Trichloroethene 79-01-6 82608 NO 4.4 ug/kg
Trichlorofluoromethane 75-69-4 82608 NO 4.4 ug/kg
Vinyl chloride 75-01-4 82608 NO 4.4 ug/kg
Xylenes (total} 1330-20-7 82608 NO 4.4 ug/kg
Run 1 Acceptance Run 3 Acceptance
Surrogate Q %Recovery Limits Q %Recovery Limits
1 ,2-Dichloroethane-d4 81 53-142 108 53-142
8romofluorobenzene 101 47-138 93 47-138
Toluene-dB 89 68-124 92 68-124
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 30508 6010C 1 07/31/2013 0633 CDF 07/29/20131017 25994
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Lead 7439-92-1 6010C 47 0.55 mg/kg
Nickel 7440-02-0 6010C 14 2.2 mg/kg 1
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result< POL and~ MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 22 of 78
Level 1 Report v2 .1
Client: Terracon Consultants, Inc. Laboratory ID: OG26068-007
Description: SSS-6-6 Matrix: Solid
Date Sampled:07/25/2013 1230 % Solids: 71.2 07/26/2013 2220
Date Received: 07/26/2013
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 82608 1 07/30/2013 1411 AAC 26155 5.52
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 82608 130 25 ug/kg
Benzene 71-43-2 82608 ND 6.4 ug/kg
Bromodichloromethane 75-27-4 82608 ND 6.4 ug/kg
Bromoform 75-25-2 82608 ND 6.4 ug/kg
Bromomethane (Methyl bromide) 74-83-9 82608 ND 6.4 ug/kg
2-Butanone (MEK) 78-93-3 82608 ND 13 ug/kg
Carbon disulfide 75-15-0 82608 ND 6.4 ug/kg
Carbon tetrachloride 56-23-5 82608 ND 6.4 ug/kg
Chlorobenzene 108-90-7 82608 ND 6.4 ug/kg
Chloroethane 75-00-3 82608 ND 6.4 ug/kg
Chloroform 67-66-3 82608 ND 6.4 ug/kg
Chloromethane (Methyl chloride) 74-87-3 82608 ND 6.4 ug/kg
Cyclohexane 110-82-7 82608 ND 6.4 ug/kg
1 ,2-Dibromo-3-chloropropane (DBCP) 96-12-8 82608 ND 6.4 ug/kg
Dibromochloromethane 124-48-1 82608 ND 6.4 ug/kg
1 ,2-Dibromoethane (EDB) 106-93-4 82608 ND 6.4 ug/kg
1 ,2-Dichlorobenzene 95-50-1 82608 ND 6.4 ug/kg
1 ,3-Dichlorobenzene 541-73-1 82608 ND 6.4 ug/kg
1 A-Dichlorobenzene 106-46-7 82608 ND 6.4 ug/kg
Dichlorodifluoromethane 75-71-8 82608 ND 6.4 ug/kg
1, 1-Dichloroethane 75-34-3 82608 ND 6.4 ug/kg
1 ,2-Dichloroethane 107-06-2 82608 ND 6.4 ug/kg
1, 1-Dichloroethene 75-35-4 82608 ND 6.4 ug/kg
cis-1 ,2-Dichloroethene 156-59-2 82608 ND 6.4 ug/kg
trans-1 ,2-Dichloroethene 156-60-5 82608 ND 6.4 ug/kg
1 ,2-Dichloropropane 78-87-5 82608 ND 6.4 ug/kg
cis-1 ,3-Dichloropropene 10061-01-5 82608 ND 6.4 ug/kg
trans-1 ,3-Dichloropropene 10061-02-6 82608 ND 6.4 ug/kg
Ethylbenzene 100-41-4 82608 ND 6.4 ug/kg
2-Hexanone 591-78-6 82608 ND 13 ug/kg
lsopropylbenzene 98-82-8 82608 ND 6.4 ug/kg
Methyl acetate 79-20-9 82608 ND 6.4 ug/kg
Methyl tertiary butyl ether (MTBE) 1634-04-4 82608 ND 6.4 ug/kg
4-Methyl-2-pentanone 108-10-1 82608 ND 13 ug/kg
Methylcyclohexane 108-87-2 82608 ND 6.4 ug/kg
Methylene chloride 75-09-2 82608 ND 6.4 ug/kg
Styrene 100-42-5 82608 ND 6.4 ug/kg
1,1 ,2,2-Tetrachloroethane 79-34-5 82608 ND 6.4 ug/kg
Tetrachloroethene 127-18-4 82608 ND 6.4 ug/kg
Toluene 108-88-3 82608 ND 6.4 ug/kg
POL Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND Not detected at or above the POL J = Estimated result< POL and?. MDL P =The RPD between two GC columns exceeds 40% N ;:;;. Recovery is out of criter'1a
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 23 of 78
Level 1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-6-6
Laboratory 10: OG26068-007
Matrix: Solid
Date Sampled:07/25/2013 1230
Date Received: 07/26/2013
%Solids: 71.2 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 82608 1 07/30/2013 1411 AAC 26155 5.52
CAS Analytical
Parameter Number Method Result Q PQL Units Run
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 82608 NO 6.4 ug/kg
1 ,2,4-Trichlorobenzene 120-82-1 8260B NO 6.4 ug/kg
1,1, 1-Trichloroethane 71-55-6 82608 NO 6.4 ug/kg
1,1 ,2-Trichloroethane 79-00-5 82608 NO 6.4 ug/kg
Trichloroethene 79-01-6 82608 NO 6.4 ug/kg
Trichlorofluoromethane 75-69-4 82608 NO 6.4 ug/kg
Vinyl chloride 75-01-4 82608 NO 6.4 ug/kg
Xylenes (total) 1330-20-7 82608 NO 6.4 ug/kg
Run 1 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 82 53-142
8romofluorobenzene 116 47-138
Toluene-dB 94 68-124
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 30508 6010C 2 07/31/2013 2258 CDF 07/29/2013 1017 25994
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Lead 7439-92-1 6010C 10 1.3 mg/kg
Nickel 7440-02-0 6010C 5.8 5.3 mg/kg 1
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and::: MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless fiagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 24 of 78
Level 1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-7-4
Date Sampled:07/25/2013 1255
Date Received: 07/26/2013
Laboratory ID: OG26068-008
Matrix: Solid
% Solids: 67.6 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
1 5035
2 5035
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Analytical Method
8260B
8260B
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Dilution Analysis Date Analyst
50 07/31/2013 0458 AWM
08/30/2013 1322 JHD
CAS Analytical
Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
Method
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
82608
82608
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
Prep Date
Result Q
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Batch
26189
28442
Sample Wt.(g)
5.24
PQL
1400
350
350
350
350
710
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
350
710
350
350
350
710
350
350
350
350
350
5.00
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Run
POL Practical quantitation limit B =Detected in the method blank E = Quantitation of compound exceeded the calibration range H =Out of holding time
NO Not detected at or above the POL J = Estimated result< POL and.:: MDL P =The RPD between two GC columns exceeds 40% N :;;:; Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 25 of 78
Level 1 Report v2.1
Client:Terracon Consultants, Inc.
Description: SSS-7-4
Laboratory ID: OG26068-008
Matrix: Solid
Date Sampled:07/25/2013 1255
Date Received: 07/26/2013
%Solids: 67.6 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
1 5035
2 5035
Parameter
Toluene
Analytical Method
82608
82608
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2.4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate Q
1,2-0ichloroethane-d4
8romofluorobenzene
Toluene-d8
Dilution Analysis Date
50 07/31/2013 0458
1 08/30/20 13 1322
Analyst
AWM
JHD
Prep Date
CAS Analytical
Number Method Result Q
108-88-3 82608 NO
76-13-1 82608 NO
120-82-1 82608 NO
71-55-6 82608 NO
79-00-5 82608 NO
79-01-6 82608 NO
75-69-4 82608 NO
75-01-4 82608 NO
1330-20-7 82608 NO
Run 1 Acceptance Run 2 Acceptance
%Recovery Limits Q %Recovery Limits
107 53-142 H 92 53-142
92 47-138 H 87 47-138
96 68-124 H 88 68-124
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date
1 5035 8260B 50 07/31/2013 0458 AWM
2 5035 82608 08/30/2013 1322 JHD
CAS Analytical
Parameter Number Method Result Q
Acetone 67-64-1 8260B 73 H
Benzene 71-43-2 8260B NO H
Bromodichloromethane 75-27-4 82608 ND H
Bromoform 75-25-2 82608 ND H
8romomethane (Methyl bromide) 74-83-9 82608 NO H
2-Butanone (MEK) 78-93-3 82608 NO H
Carbon disulfide 75-15-0 82608 ND H
Carbon tetrachloride 56-23-5 82608 ND H
Chlorobenzene 108-90-7 82608 ND H
Chloroethane 75-00-3 82608 ND H
Chloroform 67-66-3 82608 NO H
Chloromethane (Methyl chloride) 74-87-3 82608 NO H
Cyclohexane 110-82-7 82608 NO H
1,2-Dibromo-3-chloropropane (08CP) 96-12-8 82608 NO H
Oibromochloromethane 124-48-1 82608 NO H
1,2-Dibromoethane (EOB) 106-93-4 82608 NO H
1,2-0ichlorobenzene 95-50-1 82608 NO H
1,3-0ichlorobenzene 541-73-1 82608 NO H
Batch
26189
28442
Sample Wt.(g)
5.24
5.00
PQL Units
350 ug/kg
350 ug/kg
350 ug/kg
350 ug/kg
350 ug/kg
350 ug/kg
350 ug/kg
350 ug/kg
350 ug/kg
Batch Sample Wt.(g)
26189 5.24
28442 5.00
PQL Units
30 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
15 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
7.4 ug/kg
Run
Run
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result< POL and 2: MDL P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 26 of 78
Level1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-7-4
Laboratory 10: OG26068-008
Matrix: Solid
Date Sampled:07/25/2013 1255
Date Received:07/26/2013
% Solids: 67.6 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
1 5035
2 5035
Analytical Method
82608
82608
Parameter
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MT8E)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1 , 1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
1 ,2-Dichloroethane-d4
8romofluorobenzene
Toluene-dB
Q
Dilution Analysis Date
50 07/31/2013 0458
08/30/2013 1322
Analyst
AWM
JHD
CAS
Number
Analytical
Method
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
Prep Date
Result Q
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
19 H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
ND H
Run 1 Acceptance Run 2 Acceptance
% Recovery Limits Q
107
92
96
53-142
47-138
68-124
H
H
H
%Recovery Limits
92
87
88
53-142
47-138
68-124
Batch
26189
28442
PQL
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
15
7.4
7.4
7.4
15
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
7.4
Sample Wt.(g)
5.24
5.00
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/k9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Run
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
PQL = Practical quantitation limit B ~Detected in the method blank E ~ Ouantitation of compound exceeded the calibration range H ~Out of holding time
ND ~ Not detected at or above the POL J Estimated result< POL and:: MDL P =The RPD between two GC columns exceeds 40% N :::: Recovery is out of criteria
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 27 of 78
Level 1 Report v2 .1
Client: Terracon Consultants, Inc.
Description: 555-7-4
Date Sampled:07/25/2013 1255
Date Received: 07/26/2013
Run Prep Method Analytical Method
1 3050B
Parameter
Lead
Nickel
6010C
ICP-AES
Dilution Analysis Date Analyst
5 07/31/2013 2302 CDF
CAS Analytical
Number Method
7439-92-1 6010C
7440-02-0 6010C
Prep Date
Laboratory ID: OG26068-008
Matrix: Solid
%Solids: 67.6 07/26/2013 2220
Batch
07/29/2013 1017 25994
Result Q PQL Units Run
47 3.4 mg/kg 1
23 14 mg/kg
POL = Practical quantitation limit B =Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J =Estimated result< POL and!': MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 28 of 78
level 1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-8-6
Date Sampled:07/25/2013 1305
Date Received:07/26/2013
Laboratory ID: OG26068-009
Matrix: Solid
%Solids: 85.6 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
2 5035
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Analytical Method
8260B
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-0ichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-0ichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-0ichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Dilution Analysis Date Analyst
AAC 1 07/31/2013 1527
CAS
Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
Analytical
Method
82608
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
8260B
82608
82608
82608
82608
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
82608
8260B
82608
8260B
8260B
8260B
8260B
8260B
82608
8260B
Prep Date
Result Q
52
ND
NO
NO
ND
ND
ND
NO
ND
ND
ND
NO
ND
NO
NO
NO
NO
ND
ND
ND
5.6
ND
ND
ND
NO
ND
ND
NO
NO
ND
7.5
ND
ND
NO
ND
ND
NO
NO
300
ND
Batch
26252
PQL
18
4.4
4.4
4.4
4.4
8.8
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
8.8
4.4
4.4
4.4
8.8
4.4
4.4
4.4
4.4
4.4
4.4
Sample Wt.(g)
6.64
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Run
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
POL= Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H =Out of holding time
ND = Not detected at or above the POL J Estimated result< POL and~ MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 29 of 78
Level 1 Report v2 .1
Client: Terra con Consultants, Inc.
Description: SSS-8-6
Laboratory ID: OG26068-009
Matrix: Solid
Date Sampled:07/25/2013 1305
Date Received: 07/26/2013
%Solids: 85.6 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 82608 1 07/31/2013 1527 AAC 26252 6.64
CAS Analytical
Parameter Number Method Result Q PQL Units Run
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 82608 ND 4.4 ug/kg 2
1 ,2,4-Trichlorobenzene 120-82-1 82608 ND 4.4 ug/kg 2
1,1, 1-Trichloroethane 71-55-6 82608 ND 4.4 ug/kg 2
1,1 ,2-Trichloroethane 79-00-5 82608 ND 4.4 ug/kg 2
Trichloroethene 79-01-6 8260B 7.0 4.4 ugfkg 2
Trichlorofluoromethane 75-69-4 82608 ND 4.4 ug/kg 2
Vinyl chloride 75-01-4 82608 ND 4.4 ug/kg 2
Xylenes (total) 1330-20-7 82608 ND 4.4 ug/kg 2
Run 2 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 98 53-142
8romofluorobenzene 74 47-138
Toluene-dB 96 68-124
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 30508 6010C 5 07/31/2013 2306 CDF 07/29/2013 1017 25994
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Lead 7439-92-1 6010C 29 2.7 mgfkg 1
Nickel 7440-02-0 6010C 17 11 mgfkg
POL = Practical quantitation limit B = Detected in tihe method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND =Not detected at or above the POL J = Estimated result< POL and~ MDL P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 30 of 78
Level 1 Report v2 .1
Client: Terracon Consultants, Inc.
Description: SSS-9·6
Date Sampled:07/25/2013 1330
Date Received: 07/26/2013
Laboratory ID: OG26068-01 0
Matrix: Solid
% Solids: 76.0 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method
2 5035
Parameter
Acetone
Benzene
B romod ich lorometha ne
Bromoform
Analytical Method
8260B
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Dilution Analysis Date
1 07/31/20131550
Analyst
AAC
CAS Analytical
Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
Method
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
Prep Date
Result Q
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Batch
26252
PQL
23
5.8
5.8
5.8
5.8
12
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
12
5.8
5.8
5.8
12
5.8
5.8
5.8
5.8
5.8
5.8
Sample Wt.(g)
5.63
Units
u9/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Run
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
POL Practical quantitation limit B = Detected in the method blank E Quantitation of compound exceeded the calibration range H = Out of holding time
ND Not detected at or above the POL J = Estimated result< POL and c:: MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 31 of 78
Level 1 Report v2 .1
Client: Terracon Consultants, Inc.
Description: SSS-9-6
Laboratory ID: OG26068-010
Matrix: Solid
Date Sampled:0712512013 1330
Date Received: 0712612013
%Solids: 76.0 0712612013 2220
Run Prep Method
2 5035
Parameter
Volatile Organic Compounds by GC/MS
Analytical Method
8260B
Dilution Analysis Date
1 07/31/20131550
Analyst
AAC
CAS Analytical
Number Method
Prep Date
Result Q
Batch
26252
PQL
Sample Wt.(g)
5.63
Units
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 8260B ND 5.8 ug/kg
1 ,2,4-Trichlorobenzene 120-82-1 8260B ND 5.8 ug/kg
1,1, 1-Trichloroethane 71-55-6 8260B ND 5.8 ug/kg
1,1 ,2-Trichloroethane 79-00-5 8260B ND 5.8 ug/kg
Trichloroethene 79-01-6 8260B ND 5.8 ug/kg
Trichlorofluoromethane 75-69-4 8260B ND 5.8 ug/kg
Vinyl chloride 75-01-4 8260B ND 5.8 ug/kg
Xylenes (total) 1330-20-7 8260B ND 5.8 ug/kg
Run 2 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 90 53-142
Bromofluorobenzene 92 47-138
Toluene-dB 94 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 07/29/2013 1252 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units
Acenaphthene 83-32-9 8270D ND 430 ug/kg
Acenaphthylene 208-96-8 8270D ND 430 ug/kg
Acetophenone 98-86-2 8270D ND 430 ug/kg
Anthracene 120-12-7 8270D ND 430 ug/kg
Atrazine 1912-24-9 8270D ND 430 ug/kg
Benzaldehyde 100-52-7 8270D ND 1100 ug/kg
Benzo(a)anthracene 56-55-3 8270D ND 430 ug/kg
Benzo(a)pyrene 50-32-8 8270D ND 430 ug/kg
Benzo(b )fluoranthene 205-99-2 8270D ND 430 ug/kg
Benzo(g,h,i)perylene 191-24-2 82700 ND 430 ug/kg
Benzo(k)fluoranthene 207-08-9 8270D ND 430 ug/kg
1,1 '-Biphenyl 92-52-4 8270D ND 430 ug/kg
4-Bromophenyl phenyl ether 101-55-3 8270D ND 430 ug/kg
Butyl benzyl phthalate 85-68-7 8270D ND 430 ug/kg
Caprolactam 105-60-2 8270D ND 1100 ug/kg
Carbazole 86-74-8 8270D ND 430 ug/kg
4-Chloro-3-methyl phenol 59-50-7 8270D ND 430 ug/kg
4-Chloroaniline 106-47-8 8270D ND 430 ug/kg
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 430 ug/kg
bis(2-Chloroethyl)ether 111-44-4 8270D ND 430 ug/kg
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and~ MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Run
2
2
2
2
2
2
2
2
Run
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 32 of 78
Level 1 Report v2.1
Client: Terracon Consultants, Inc. Laboratory ID: OG26068-010
Description: SSS-9-6 Matrix: Solid
Date Sampled:07/25/2013 1330 %Solids: 76.0 07/26/2013 2220
Date Received: 07/26/2013
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 82700 1 07/29/2013 1252 JRG 07/27/2013 1357 25971
CAS Analytical
Parameter Number Method Result Q PQL Units Run
bis(2-Chloroisopropyl)ether 108-60-1 82700 ND 430 ug/kg
2-Chloronaphthalene 91-58-7 82700 NO 430 ug/kg
2-Chlorophenol 95-57-8 82700 ND 430 ug/kg
4-Chlorophenyl phenyl ether 7005-72-3 82700 ND 430 ug/kg
Chrysene 218-01-9 82700 ND 430 ug/kg
Di-n-butyl phthalate 84-74-2 82700 ND 430 ug/kg
Di-n-octylphthalate 117-84-0 82700 ND 430 ug/kg
Dibenzo(a,h)anthracene 53-70-3 82700 NO 430 ug/kg
Dibenzofuran 132-64-9 82700 NO 430 ug/kg
3,3'-Dichlorobenzidine 91-94-1 82700 NO 1100 ug/kg
2,4-Dichlorophenol 120-83-2 82700 NO 430 ug/kg
Diethylphthalate 84-66-2 82700 NO 430 ug/kg
Dimethyl phthalate 131-11-3 82700 ND 430 ug/kg
2 ,4-Dimethylphenol 105-67-9 82700 ND 430 ug/kg
4,6-Dinitro-2-methylphenol 534-52-1 82700 ND 1100 ug/kg
2,4-Dinitrophenol 51-28-5 82700 ND 1100 ug/kg
2 ,4-Dinitrotoluene 121-14-2 82700 NO 430 ug/kg
2,6-Dinitrotoluene 606-20-2 82700 NO 430 ug/kg
bis(2-Ethylhexyl)phthalate 117-81-7 82700 ND 430 ug/kg
Fluoranthene 206-44-0 82700 ND 430 ug/kg
Fluorene 86-73-7 82700 ND 430 ug/kg
Hexachlorobenzene 118-74-1 82700 ND 430 ug/kg
Hexachlorobutadiene 87-68-3 82700 ND 430 ug/kg
Hexachlorocyclopentadiene 77-47-4 82700 ND 1100 ug/kg
Hexachloroethane 67-72-1 82700 NO 430 ug/kg
lndeno(1 ,2,3-c,d)pyrene 193-39-5 82700 ND 430 ug/kg
lsophorone 78-59-1 82700 NO 430 ug/kg
2-Methylnaphthalene 91-57-6 82700 NO 430 ug/kg
2-Methylphenol 95-48-7 82700 NO 430 ug/kg
3 & 4-Methylphenol 106-44-5 82700 ND 870 ug/kg
N-Nitrosodi-n-propylamine 621-64-7 82700 NO 430 ug/kg
N-Nitrosodiphenylam ine (Diphenylamine) 86-30-6 82700 ND 430 ug/kg
Naphthalene 91-20-3 82700 ND 430 ug/kg
2-Nitroaniline 88-74-4 82700 ND 430 ug/kg
3-Nitroaniline 99-09-2 82700 ND 430 ug/kg
4-Nitroaniline 100-01-6 82700 ND 430 ug/kg
Nitrobenzene 98-95-3 82700 NO 430 ug/kg
2-Nitrophenol 88-75-5 82700 NO 430 ug/kg
4-Nitrophenol 100-02-7 82700 NO 1100 ug/kg
Pentachlorophenol 87-86-5 82700 NO 1100 ug/kg
POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H Out of holding time
ND = Not detected at or above the POL J = Estimated result< POL and?. MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 33 of 78
Level 1 Report v2.1
Client: Terra con Consultants, Inc.
Description: SSS-9-6
Laboratory ID: OG26068-010
Matrix: Solid
Date Sampled:07/25/2013 1330
Date Received: 07/26/2013
%Solids: 76.0 07/26/2013 2220
Run Prep Method
1 3550C
Parameter
Phenanthrene
Phenol
Pyrene
2 ,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
2,4,6-Tribromophenol
2-Fiuorobiphenyl
2-Fiuorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d 14
Run Prep Method
1 30508
Parameter
Lead
Nickel
POL ; Practical quantitation limit
Semivolatile Organic Compounds by GC/MS
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 07/29/2013 1252 JRG 07/27/2013 1357 25971
CAS Analytical
Number Method Result Q PQL Units Run
85-01-8 8270D ND 430 ug/kg
108-95-2 82700 ND 430 ug/kg
129-00-0 8270D ND 430 ug/kg
95-95-4 8270D ND 430 ug/kg
88-06-2 82700 NO 430 ug/kg
Run 1 Acceptance
Q %Recovery Limits
85 30-117
65 33-102
82 28-104
69 22-109
85 27-103
103 41-120
ICP-AES
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010C 1 07/31/2013 0648 CDF 07/29/2013 1017 25994
CAS Analytical
Number Method Result Q PQL Units Run
7439-92-1 6010C 33 0.62 mg/kg
7440-02-0 6010C 5.9 2.5 mg/kg
B ; Detected in the method blank E ; Ouantitation of compound exceeded the calibration range H ; Out of holding time
ND; Not detected at or above the POL J ; Estimated result < POL and .": MDL P ; The RPD between two GC columns exceeds 40% N ; Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 34 of 78
Level1 Report v2.1
Client: Terracon Consultants, Inc. Laboratory ID: OG26068-011
Description: SSS-10-8 Matrix: Solid
Date Sampled:07/25/2013 1355 % Solids: 73.2 07/26/2013 2220
Date Received: 07/26/2013
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/30/2013 1458 AAC 26155 5.42
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 25 ug/kg
Benzene 71-43-2 8260B ND 6.3 ug/kg
Bromodichloromethane 75-27-4 8260B ND 6.3 ug/kg
Bromoform 75-25-2 8260B ND 6.3 ug/kg
Bromomethane (Methyl bromide) 74-83-9 8260B ND 6.3 ug/kg
2-Butanone (MEK) 78-93-3 8260B ND 13 ug/kg
Carbon disulfide 75-15-0 8260B ND 6.3 ug/kg
Carbon tetrachloride 56-23-5 8260B ND 6.3 ug/kg
Chlorobenzene 108-90-7 8260B ND 6.3 ug/kg
Chloroethane 75-00-3 8260B ND 6.3 ug/kg
Chloroform 67-66-3 8260B ND 6.3 ug/kg
Chloromethane (Methyl chloride) 74-87-3 8260B ND 6.3 ug/kg
Cyclohexane 110-82-7 8260B ND 6.3 ug/kg
1 ,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260B ND 6.3 ug/kg
Dibromochloromethane 124-48-1 8260B ND 6.3 ug/kg
1 ,2-Dibromoethane (EDB) 106-93-4 8260B ND 6.3 ug/kg
1 ,2-Dichlorobenzene 95-50-1 8260B ND 6.3 ug/kg
1 ,3-Dichlorobenzene 541-73-1 8260B ND 6.3 ug/kg
1 A-Dichlorobenzene 106-46-7 8260B ND 6.3 ug/kg
Dichlorodifluoromethane 75-71-8 8260B ND 6.3 ug/kg
1 , 1-Dichloroethane 75-34-3 8260B ND 6.3 ug/kg
1 ,2-Dichloroethane 107-06-2 8260B ND 6.3 ug/kg
1, 1-Dichloroethene 75-35-4 8260B ND 6.3 ug/kg
cis-1 ,2-Dichloroethene 156-59-2 8260B ND 6.3 ug/kg
trans-1 ,2-Dichloroethene 156-60-5 8260B ND 6.3 ug/kg
1 ,2-Dichloropropane 78-87-5 8260B ND 6.3 ug/kg
cis-1 ,3-Dichloropropene 10061-01-5 8260B ND 6.3 ug/kg
trans-1 ,3-Dichloropropene 10061-02-6 8260B ND 6.3 ug/kg
Ethyl benzene 100-41-4 8260B ND 6.3 ug/kg
2-Hexanone 591-78-6 8260B ND 13 ug/kg
lsopropylbenzene 98-82-8 8260B ND 6.3 ug/kg
Methyl acetate 79-20-9 8260B ND 6.3 ug/kg
Methyl tertiary butyl ether (MTBE) 1634-04-4 8260B ND 6.3 ug/kg
4-Methyl-2-pentanone 108-10-1 8260B ND 13 ug/kg
Methylcyclohexane 108-87-2 8260B ND 6.3 ug/kg
Methylene chloride 75-09-2 8260B ND 6.3 ug/kg
Styrene 100-42-5 8260B ND 6.3 ug/kg
1,1 ,2,2-Tetrachloroethane 79-34-5 8260B ND 6.3 ug/kg
Tetrachloroethene 127-18-4 8260B ND 6.3 ug/kg
Toluene 108-88-3 8260B ND 6.3 ug/kg
POL Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H =Out of holding time
ND = Not detected at or above the POL J = Estimated result< POL and ;o: MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 35 of 78
Level 1 Report v2.1
Client: Terracon Consultants, Inc.
Description: SSS-10·8
Laboratory 10: OG26068·011
Matrix: Solid
Date Sampled:07/25/2013 1355
Date Received: 07/26/2013
%Solids: 73.2 07/26/2013 2220
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 82608 1 07/30/2013 1458 AAC 26155 5.42
CAS Analytical
Parameter Number Method Result Q PQL Units Run
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 76-13-1 82608 ND 6.3 ug/kg
1 ,2,4-Trichlorobenzene 120-82-1 82608 ND 6.3 ug/kg
1,1, 1-Trichloroethane 71-55-6 82608 ND 6.3 ug/kg
1,1 ,2-Trichloroethane 79-00-5 82608 ND 6.3 ug/kg
Trichloroethene 79-01-6 82608 ND 6.3 ug/kg
Trichlorofluoromethane 75-69-4 82608 ND 6.3 ug/kg
Vinyl chloride 75-01-4 82608 ND 6.3 ug/kg
Xylenes (total) 1330-20-7 82608 ND 6.3 ug/kg
Run 1 Acceptance
Surrogate Q %Recovery Limits
1 ,2-Dichloroethane-d4 86 53-142
8romofluorobenzene 112 47-138
Toluene-dB 95 68-124
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 30508 6010C 2 07/31/2013 2310 CDF 07/29/2013 1017 25994
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Lead 7439-92-1 6010C 20 1.3 mg/kg 1
Nickel 7440-02-0 6010C 11 5.0 mg/kg 1
POL ; Practical quantitation limit 8 ; Detected in the method blank E ; Ouantitation of compound exceeded the calibration range H = Out of holding time
NO ; Not detected at or above the POL J ; Estimated result < POL and~ MDL P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 36 of 78
Level 1 Report v2.1
QC Summary
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 37 of 78
Level1 Report v2.1
Sample ID: 0026155-001
Batch: 26155
Analytical Method: 8260B
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 A-Dichlorobenzene
1 ,3-Dichlorobenzene
Dichlorodifluoromethane
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-T richlorobenzene
1,1 ,2-Trichloroethane
1,1, 1-Trichloroethane
POL ~ Practical quantitation limit
ND ~ Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Matrix: Solid
Prep Method: 5035
Result Q Oil PQL Units
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
P ~ The RPD between two GC columns exceeds 40%
J ~ Estimated result < POL and :;: MDL
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/20131134
07/30/2013 1134
07/30/2013 1134
07/30/20131134
07/30/20131134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/20131134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
Page: 38 of 78
Level 1 Report v2 .1
Sample ID: 0026155-001
Batch: 26155
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
POL= Practical quantitation limit
NO= Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Result
ND
ND
ND
ND
Q % Rec
111
84
92
Q Oil
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
POL
5.0
5.0
5.0
5.0
Units
ug/kg
ug/kg
ug/kg
ug/kg
P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
+ = RPD is out of criteria J = Estimated result< POL and ;o: MDL
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/30/20131134
07/30/2013 1134
07/30/2013 1134
07/30/2013 1134
Page: 39 of 78
Level 1 Report v2 .1
Volatile Organic Compounds by GC/MS-LCS
Sample 10: 0026155-002 Matrix: Solid
Batch: 26155 Prep Method: 5035
Analytical Method: 8260B
Spike
Amount Result %Rec
Parameter (ug/kg) (ug/kg) Q Oil % Rec Limit
Acetone 100 120 122 42-149
Benzene 50 54 108 69-123
Bromodichloromethane 50 54 107 69-121
Bromoform 50 54 108 61-119
Bromomethane (Methyl bromide) 50 54 107 10-168
2-Butanone (MEK) 100 130 126 57-148
Carbon disulfide 50 52 104 58-122
Carbon tetrachloride 50 52 103 58-136
Chlorobenzene 50 50 100 59-129
Chloroethane 50 59 118 42-163
Chloroform 50 54 107 71-125
Chloromethane (Methyl chloride) 50 49 98 34-134
Cyclohexane 50 45 89 53-139
1 ,2-Dibromo-3-chloropropane (DBCP) 50 58 115 55-125
Dibromochloromethane 50 51 101 66-119
1 ,2-Dibromoethane (EDB) 50 54 107 74-124
1 ,2-Dichlorobenzene 50 50 100 57-131
1 A-Dichlorobenzene 50 51 101 52-133
1 ,3-Dichlorobenzene 50 48 96 51-134
Dichlorodifluoromethane 50 54 109 10-157
1 ,2-Dichloroethane 50 55 110 67-129
1, 1-Dichloroethane 50 54 108 71-127
1, 1-Dichloroethene 50 53 105 69-138
cis-1 ,2-Dichloroethene 50 51 102 70-122
trans-1 ,2-Dichloroethene 50 54 107 68-131
1 ,2-Dichloropropane 50 51 103 72-124
cis-1 ,3-Dichloropropene 50 53 107 70-126
trans-1 ,3-Dichloropropene 50 49 99 70-124
Ethylbenzene 50 48 96 59-128
2-Hexanone 100 120 117 54-137
lsopropylbenzene 50 51 101 50-136
Methyl acetate 50 66 132 59-137
Methyl tertiary butyl ether (MTBE) 50 56 112 70-130
4-Methyl-2-pentanone 100 120 120 60-134
Methylcyclohexane 50 50 100 41-144
Methylene chloride 50 55 109 70-130
Styrene 50 50 100 54-136
1 , 1 ,2,2-Tetrachloroethane 50 54 107 69-132
T etrachloroethene 50 49 99 45-150
Toluene 50 51 101 61-129
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50 44 88 49-136
1 ,2,4-Trichlorobenzene 50 50 101 34-145
1,1 ,2-Trichloroethane 50 51 101 55-128
1,1, 1-Trichloroethane 50 54 109 63-128
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
P = The RPD between two GC columns exceeds 40%
J = Estimated result < PQL and :;: MDL
N ::: Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
Page: 40 of 78
Level1 Report v2.1
Sample 10: 0026155-002
Batch: 26155
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
Volatile Organic Compounds by GC/MS-LCS
Spike
Amount
(ug/kg)
50
50
50
100
0 % Rec
114
88
100
Result
(ug/kg) 0
52
53
50
100
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec
104
106
101
100
% Rec
Limit
62-126
45-138
42-132
58-128
POL = Practical quantitation limit
NO = Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and:> MDL
N Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
07/30/2013 0958
Page:41 of78
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS-LCSD
Sample ID: 0026155-003
Batch: 26155
Analytical Method: 8260B
Parameter
Spike
Amount
(ug/kg)
Acetone 100
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1 ,2-Dibromo-3-chloropropane (DBCP) 50
Dibromochloromethane 50
1 ,2-Dibromoethane (EDB) 50
1 ,2-Dichlorobenzene 50
1 A-Dichlorobenzene 50
1 ,3-Dichlorobenzene 50
Dichlorodifluoromethane 50
1 ,2-Dichloroethane 50
1, 1-Dichloroethane 50
1, 1-Dichloroethene 50
cis-1 ,2-Dichloroethene 50
trans-1 ,2-Dichloroethene 50
1 ,2-Dichloropropane 50
cis-1 ,3-Dichloropropene 50
trans-1 ,3-Dichloropropene 50
Ethylbenzene 50
2-Hexanone 100
lsopropylbenzene 50
Methyl acetate 50
Methyl tertiary butyl ether (MTBE) 50
4-Methyl-2-pentanone 100
Methylcyclohexane 50
Methylene chloride 50
Styrene 50
1,1 ,2,2-Tetrachloroethane 50
Tetrachloroethene 50
Toluene 50
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1 ,2,4-Trichlorobenzene 50
1,1 ,2-Trichloroethane 50
1,1, 1-Trichloroethane 50
Result
(ug/kg)
120
52
52
52
49
110
48
51
51
52
52
46
49
49
51
52
49
49
48
51
50
52
50
50
51
53
52
53
49
110
50
60
52
110
50
51
50
50
51
53
41
51
48
51
Q
Matrix: Solid
Prep Method: 5035
Oil %Rec %RPD
120
104
104
105
97
110
97
103
102
104
104
93
98
98
101
105
97
99
95
102
101
104
100
99
103
105
104
105
98
112
100
119
105
115
99
102
101
99
102
107
82
101
96
102
1.7
3.1
2.9
3.4
9.7
13
6.8
0.40
2.4
12
3.2
5.5
9.5
16
0.13
2.4
3.1
2.6
0.82
6.0
9.1
3.4
4.8
2.5
4.2
2.3
2.0
6.5
1.9
3.9
1.1
10
7.1
4.3
1.2
6.6
1.1
8.0
2.9
5.1
7.8
0.63
5.2
6.3
% Rec
Limit
42-149
69-123
69-121
61-119
10-168
57-148
58-122
58-136
59-129
42-163
71-125
34-134
53-139
55-125
66-119
74-124
57-131
52-133
51-134
10-157
67-129
71-127
69-138
70-122
68-131
72-124
70-126
70-124
59-128
54-137
50-136
59-137
70-130
60-134
41-144
70-130
54-136
69-132
45-150
61-129
49-136
34-145
55-128
63-128
POL = Practical quantitation limit
NO = Not detected at or above the POL
P =The RPD between two GC columns exceeds 40%
J = Estimated result < POL and :': MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
%RPD
Limit Analysis Date
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1 022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
07/30/2013 1022
Page: 42 of 78
Level 1 Report v2.1
Sample ID: 0026155-003
Batch: 26155
Analytical Method: 8260B
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
POL= Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-LCSD
Spike
Amount Result
(ug/kg) (ug/kg) Q
50 51
50 50
50 48
100 100
Q % Rec
Acceptance
Limit
114 47-138
84 53-142
97 68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec % RPD
103 1.2
100 5.5
97 4.0
101 0.95
% Rec
Limit
62-126
45-138
42-132
58-128
P =The RPD between two GC columns exceeds 40%
J = Estimated result< PQL and :0 MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
20
20
20
20
Analysis Date
07/30/2013 1022
07/30/2013 1022
07/30/20131022
07/30/2013 1022
Page: 43 of 78
Level 1 Report v2.1
Sample 10: 0026189-001
Batch: 26189
Analytical Method: 8260B
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 A-Dichlorobenzene
1 ,3-Dichlorobenzene
Dichlorodifluoromethane
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
trans-1 ,3-Dichloropropene
cis-1 ,3-Dichloropropene
Ethyl benzene
2-Hexanone
Isopropyl benzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
POL = Practical quantitation limit
NO = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Matrix: Solid
Prep Method: 5035
Result Q Oil PQL Units
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
P =The RPD between two GC columns exceeds 40%
J =Estimated result< POL and:?. MDL
1000 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
500 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
500 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
500 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
250 ug/kg
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
Page: 44 of 78
Level 1 Report v2 .1
Sample ID: 0026189-001
Batch: 26189
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
POL= Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Result Q
ND
ND
ND
ND
Q % Rec
93
116
103
Dil
50
50
50
50
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
POL
250
250
250
250
Units
ug/kg
ug/kg
ug/kg
ug/kg
P:::: The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
+ :;: RPD is out of criteria J = Estimated result< POL and:: MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
07/31/2013 0347
Page: 45 of 78
Level 1 Report v2 .1
Sample 10: 0026189-002
Batch: 26189
Analytical Method: 8260B
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 A-Dichlorobenzene
1 ,3-Dichlorobenzene
Dichlorodifluoromethane
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
trans-1 ,3-Dichloropropene
cis-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Volatile Organic Compounds by GC/MS -LCS
Spike
Amount
(ug/kg)
5000
2500
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
5000
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
Result
(ug/kg)
3700
2600
2600
2600
1400
5200
2300
2500
2600
2100
2600
2100
2500
2600
2700
2700
2600
2500
2400
2000
2600
2600
2600
2400
2600
2700
2600
2500
2500
5500
2600
3000
2700
5400
2400
2600
2600
2800
2600
2500
2100
2300
2500
2600
Q
Matrix: Solid
Prep Method: 5035
Oil % Rec
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
74
104
103
104
55
104
90
98
104
85
105
83
101
105
106
108
105
100
98
78
104
103
105
98
103
106
103
99
101
110
106
119
109
107
96
105
103
110
103
101
84
93
100
103
% Rec
Limit
42-149
69-123
69-121
61-119
10-168
57-148
58-122
58-136
59-129
42-163
71-125
34-134
53-139
55-125
66-119
74-124
57-131
52-133
51-134
10-157
67-129
71-127
69-138
70-122
68-131
72-124
70-124
70-126
59-128
54-137
50-136
59-137
70-130
60-134
41-144
70-130
54-136
69-132
45-150
61-129
49-136
34-145
63-128
55-128
POL; Practical quantitation limit
ND; Not detected at or above the POL
P ; The RPD between two GC columns exceeds 40%
J ; Estimated result < POL and": MDL
N = Recovery is out of criteria
+ ; RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless ftagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
Page: 46 of 78
Level1 Report v2.1
Sample ID: 0026189-002
Batch: 26189
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
Volatile Organic Compounds by GC/MS-LCS
Spike
Amount
(ug/kg)
2500
2500
2500
5000
Q % Rec
100
105
102
Result
(ug/kg) Q
2400
2700
2200
5200
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
Dil % Rec
50 94
50 108
50 88
50 104
% Rec
Limit
62-126
45-138
42-132
58-128
POL ;;:; Practical quantitation limit
ND " Not detected at or above the PQL
P "The RPD between two GC columns exceeds 40%
J " Estimated result< PQL and:: MDL
N Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
07/31/2013 0213
Page: 47 of 78
Level 1 Report v2.1
Sample ID: 0026189-003
Batch: 26189
Analytical Method: 8260B
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 A-Dichlorobenzene
1 ,3-Dichlorobenzene
Dichlorodifluoromethane
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
trans-1 ,3-Dichloropropene
cis-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
POL = Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-LCSD
Spike
Amount
(ug/kg)
5000
2500
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
5000
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
Result
(ug/kg)
4700
2700
2500
2500
1100
5300
2200
2500
2500
1700
2600
2200
2400
2400
2600
2800
2500
2400
2400
2100
2600
2700
2700
2500
2700
2600
2500
2600
2700
5700
2500
3100
2800
5300
2400
2700
2500
2600
2500
2600
2100
2200
2500
2600
Q
+
+
Matrix: Solid
Prep Method: 5035
Oil % Rec %RPD
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
94
106
102
101
43
105
90
99
100
70
105
87
98
95
103
110
100
96
96
83
105
106
107
101
107
103
100
103
107
115
100
126
114
105
98
106
102
105
101
103
85
88
99
106
23
2.5
1.3
3.4
24
1.3
0.95
1.4
3.4
20
0.32
4.5
2.9
10
2.9
2.2
4.7
4.6
2.0
5.8
1.5
2.6
2.0
3.0
4.1
3.1
3.2
3.5
5.5
3.7
6.1
5.6
3.9
2.1
1.7
1.4
1.7
5.2
1.5
2.8
1.2
4.9
0.68
3.1
% Rec
Limit
42-149
69-123
69-121
61-119
10-168
57-148
58-122
58-136
59-129
42-163
71-125
34-134
53-139
55-125
66-119
74-124
57-131
52-133
51-134
10-157
67-129
71-127
69-138
70-122
68-131
72-124
70-124
70-126
59-128
54-137
50-136
59-137
70-130
60-134
41-144
70-130
54-136
69-132
45-150
61-129
49-136
34-145
63-128
55-128
P = The RPD between two GC columns exceeds 40%
J = Estimated result < POL and .?: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
%RPD
Limit Analysis Date
20 07/31/2013 0237
20 07/31/2013 0237
20 07/31/2013 0237
20 07/31/2013 0237
20 07/31/2013 0237
20 07/31/2013 0237
20 07/31/2013 0237
20 07/31/2013 0237
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
Page: 48 of 78
Level 1 Report v2.1
Sample ID: 0026189-003
Batch: 26189
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
POL= Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-LCSD
Spike
Amount Result
(ug/kg) (ug/kg) 0
2500 2500
2500 2700
2500 2200
5000 5200
Q % Rec
Acceptance
Limit
104 47-138
107 53-142
100 68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec % RPD
50 99 4.5
50 107 1.6
50 88 0.76
50 104 0.47
% Rec
Limit
62-126
45-138
42-132
58-128
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and::: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
20
20
20
20
Analysis Date
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
07/31/2013 0237
Page: 49 of 78
Level 1 Report v2 .1
Sample ID: 0026252-001
Batch: 26252
Analytical Method: 8260B
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Ch lorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-0ibromo-3-chloropropane (OBCP)
Oibromochloromethane
1 ,2-0ibromoethane (EOB)
1 ,2-0ichlorobenzene
1 ,4-0ichlorobenzene
1 ,3-0ichlorobenzene
Oichlorodifluoromethane
1 ,2-0ichloroethane
1, 1-0ichloroethane
1, 1-0ichloroethene
cis-1 ,2-0ichloroethene
trans-1 ,2-0ichloroethene
1 ,2-0ichloropropane
trans-1 ,3-0ichloropropene
cis-1 ,3-0ichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
POL = Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Matrix: Solid
Prep Method: 5035
Q Oil PQL Units
20 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
10 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
1 5.0 ug/kg
1 5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
10 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
10 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and :>: MDL
N = Recovery is out of criteria
+ :::: RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 1247
07/31/2013 1247
07/31/20131247
07/31/20131247
07/31/2013 1247
07/31/20131247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/20131247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/20131247
07/31/2013 1247
07/31/2013 1247
07/31/20131247
07/31/20131247
07/31/2013 1247
07/31/20131247
07/31/2013 1247
07/31/20131247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/20131247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/2013 1247
07/31/20131247
Page: 50 of 78
Level 1 Report v2.1
Sample ID: 0026252-001
Batch: 26252
Analytical Method: 8260B
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-0ichloroethane-d4
Toluene-dB
POL Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Result
NO
NO
NO
NO
Q % Rec
98
96
97
Q Oil
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
POL
5.0
5.0
5.0
5.0
Units
ug/kg
ug/kg
ug/kg
ug/kg
P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
+ = RPD is out of criteria J = Estimated result< POL and:: MDL
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 1247
07/31/20131247
07/31/20131247
07/31/20131247
Page: 51 of 78
Level 1 Report v2 .1
Volatile Organic Compounds by GC/MS-LCS
Sample ID: 0026252-002 Matrix: Solid
Batch: 26252 Prep Method: 5035
Analytical Method: 8260B
Spike
Amount Result % Rec
Parameter (ug/kg) (ug/kg) Q Oil %Rec Limit
Acetone 100 98 98 42-149
Benzene 50 43 86 69-123
Bromodichloromethane 50 44 87 69-121
Bromoform 50 45 91 61-119
Bromomethane (Methyl bromide) 50 32 64 10-168
2-Butanone (MEK) 100 93 93 57-148
Carbon disulfide 50 38 76 58-122
Carbon tetrachloride 50 41 82 58-136
Chlorobenzene 50 44 88 59-129
Chloroethane 50 39 79 42-163
Chloroform 50 42 84 71-125
Chloromethane (Methyl chloride) 50 38 75 34-134
Cyclohexane 50 42 83 53-139
1 ,2-Dibromo-3-chloropropane (DBCP) 50 44 89 55-125
Dibromochloromethane 50 45 90 66-119
1 ,2-Dibromoethane (EDB) 50 46 91 74-124
1 ,2-Dichlorobenzene 50 43 86 57-131
1 A-Dichlorobenzene 50 44 88 52-133
1 ,3-Dichlorobenzene 50 43 86 51-134
Dichlorodifluoromethane 50 41 81 10-157
1 ,2-Dichloroethane 50 42 83 67-129
1, 1-Dichloroethane 50 43 85 71-127
1, 1-Dichloroethene 50 43 86 69-138
cis-1 ,2-Dichloroethene 50 40 81 70-122
trans-1 ,2-Dichloroethene 50 43 86 68-131
1 ,2-Dichloropropane 50 44 88 72-124
trans-1 ,3-Dichloropropene 50 44 88 70-124
cis-1 ,3-Dichloropropene 50 43 86 70-126
Ethylbenzene 50 45 89 59-128
2-Hexanone 100 100 103 54-137
lsopropylbenzene 50 45 90 50-136
Methyl acetate 50 50 99 59-137
Methyl tertiary butyl ether (MTBE) 50 46 92 70-130
4-Methyl-2-pentanone 100 95 95 60-134
Methylcyclohexane 50 42 84 41-144
Methylene chloride 50 42 84 70-130
Styrene 50 43 87 54-136
1,1 ,2,2-Tetrachloroethane 50 46 91 69-132
Tetrachloroethene 50 44 89 45-150
Toluene 50 43 85 61-129
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50 35 70 49-136
1 ,2,4-T richlorobenzene 50 44 87 34-145
1,1, 1-Trichloroethane 50 43 85 63-128
1,1 ,2-Trichloroethane 50 45 90 55-128
POL = Practical quantitation limit
ND = Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J = Estimated result < POL and:: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/20131136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/20131136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/20131136
07/31/2013 1136
07/31/20131136
07/31/20131136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/20131136
07/31/20131136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/20131136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/20131136
Page: 52 of 78
Level1 Report v2.1
Sample ID: 0026252-002
Batch: 26252
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
Volatile Organic Compounds by GC/MS -LCS
Spike
Amount
(ug/kg)
50
50
50
100
Q % Rec
102
95
99
Result
(ug/kg) Q
42
41
38
88
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
Dil % Rec
85
83
76
88
% Rec
Limit
62-126
45-138
42-132
58-128
PQL = Practical quantitation limit
ND = Not detected at or above the POL
P =The RPD between two GC columns exceeds 40%
J Estimated result< POL and:': MDL
N = Recovery is out of criteria
+ :::: RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 1136
07/31/2013 1136
07/31/2013 1136
07/31/20131136
Page: 53 of 78
Level1 Report v2.1
Volatile Organic Compounds by GC/MS · LCSD
Sample ID: 0026252-003
Batch: 26252
Analytical Method: 8260B
Parameter
Spike
Amount
(ug/kg)
Acetone 100
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1 ,2-Dibromo-3-chloropropane (DBCP) 50
Dibromochloromethane 50
1 ,2-Dibromoethane (EDB) 50
1 ,2-Dichlorobenzene 50
1 A-Dichlorobenzene 50
1 ,3-Dichlorobenzene 50
Dichlorodifluoromethane 50
1 ,2-Dichloroethane 50
1, 1-Dichloroethane 50
1, 1-Dichloroethene 50
cis-1 ,2-Dichloroethene 50
trans-1 ,2-Dichloroethene 50
1 ,2-Dichloropropane 50
trans-1 ,3-Dichloropropene 50
cis-1 ,3-Dichloropropene 50
Ethylbenzene 50
2-Hexanone 100
lsopropylbenzene 50
Methyl acetate 50
Methyl tertiary butyl ether (MTBE) 50
4-Methyl-2-pentanone 100
Methylcyclohexane 50
Methylene chloride 50
Styrene 50
1,1 ,2,2-Tetrachloroethane 50
Tetrachloroethene 50
Toluene 50
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1 ,2,4-T richlorobenzene 50
1,1, 1-Trichloroethane 50
1,1 ,2-Trichloroethane 50
Result
(ug/kg)
100
45
44
46
36
96
39
43
44
40
43
38
43
44
46
46
43
44
42
42
44
43
42
40
43
45
46
45
44
110
44
50
47
100
46
42
44
46
44
46
36
44
42
44
Q
Matrix: Solid
Prep Method: 5035
Oil % Rec %RPD
100
91
89
93
71
96
77
86
88
80
86
76
87
88
92
91
85
89
84
85
87
87
85
80
85
89
93
91
89
108
88
100
93
103
91
85
88
91
88
91
72
87
85
88
1.8
5.1
2.1
2.4
11
3.4
1.4
4.7
0.068
0.92
2.5
0.89
4.0
1.0
2.5
0.23
1.5
0.34
2.4
4.2
4.6
2.2
1.0
0.61
0.59
1.6
5.0
5.0
0.25
4.1
2.4
0.98
1.4
7.3
7.8
0.83
1.8
0.16
0.50
7.0
2.5
0.11
0.57
2.5
% Rec
Limit
42-149
69-123
69-121
61-119
10-168
57-148
58-122
58-136
59-129
42-163
71-125
34-134
53-139
55-125
66-119
74-124
57-131
52-133
51-134
10-157
67-129
71-127
69-138
70-122
68-131
72-124
70-124
70-126
59-128
54-137
50-136
59-137
70-130
60-134
41-144
70-130
54-136
69-132
45-150
61-129
49-136
34-145
63-128
55-128
POL ; Practical quantitation limit
ND; Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and? MDL
N = Recovery is out of criteria
+ ; RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit Analysis Date
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
07/31/2013 1159
07/31/20131159
07/31/20131159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/20131159
07/31/2013 1159
07/31/20131159
07/31/20131159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
Page: 54 of 78
Level 1 Report v2.1
Sample ID: 0026252-003
Batch: 26252
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
POL = Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-LCSD
Spike
Amount Result
(ug/kg) (ug/kg) Q
50 44
50 43
50 39
100 89
Q % Rec Acceptance
Limit
102 47-138
94 53-142
100 68-124
Matrix: Solid
Prep Method: 5035
Dil % Rec % RPD
88 4.2
86 3.2
78 3.1
89 0.85
% Rec
Limit
62-126
45-138
42-132
58-128
P The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
+ = RPD is out of criteria J = Estimated result < POL and ? MDL
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
20
20
20
20
Analysis Date
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
07/31/2013 1159
Page: 55 of 78
Level 1 Report v2. 1
Sample ID: 0026253-001
Batch: 26253
Analytical Method: 82608
Parameter
Tetrachloroethene
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
POL ; Practical quantitation limit
ND =Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Matrix: Solid
Prep Method: 5035
Result Q Oil PQL Units
ND
Q
50
%Rec Acceptance
Limit
93 47-138
116 53-142
103 68-124
P =The RPD between two GC columns exceeds 40%
J = Estimated result< POL and_": MDL
250 ug/kg
N == Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0347
Page: 56 of 78
Level 1 Report v2.1
Sample 10: 0026253-002
Batch: 26253
Analytical Method: 8260B
Parameter
Tetrachloroethene
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
Volatile Organic Compounds by GC/MS-LCS
Spike
Amount
(ug/kg)
2500
Q % Rec
100
105
102
Result
(ug/kg) Q
2600
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec
50 103
% Rec
Limit
45-150
POL = Practical quantitation limit
ND ; Not detected at or above the PQL
P ; The RPD between two GC columns exceeds 40%
J; Estimated result< PQL and~ MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0213
Page: 57 of 78
Level1 Report v2.1
Sample 10: 0026253-003
Batch: 26253
Analytical Method: 82608
Parameter
Tetrachloroethene
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Volatile Organic Compounds by GC/MS -LCSD
Spike
Amount Result
(ug/kg) (ug/kg) Q
2500 2500
Q % Rec Acceptance
Limit
104 47-138
107 53-142
100 68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec %RPD
50 101 1.5
% Rec
Limit
45-150
P = The RPD between two GC columns exceeds 40%
J = Estimated result < PQL and ~ MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable. all soil sample analysis are reported on a dry weight basis unless fiagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
%RPD
Limit Analysis Date
20 07/31/2013 0237
Page: 58 of 78
Level 1 Report v2.1
Sample ID: 0026521-001
Batch: 26521
Analytical Method: 8260B
Parameter
Tetrachloroethene
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
PQL = Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Matrix: Solid
Prep Method: 5035
Result Q Dil PQL Units
NO
Q
50
% Rec Acceptance
Limit
93 47-138
116 53-142
103 68-124
P = The RPD between two GC columns exceeds 40%
J = Estimated result < POL and ~ MDL
250 ug/kg
N :;:: Recovery is out of criteria
+ RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0347
Page: 59 of 78
Level 1 Report v2 .1
Sample 10: 0026521-002
Batch: 26521
Analytical Method: 82608
Parameter
T etrachloroethene
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
Volatile Organic Compounds by GC/MS -LCS
Spike
Amount
(ug/kg)
2500
Q % Rec
100
105
102
Result
(ug/kg) Q
2600
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
Oil %Rec
50 103
% Rec
Limit
45-150
POL ; Practical quantitation limit
ND ; Not detected at or above the POL
P ; The RPD between two GC columns exceeds 40%
J ; Estimated result< POL and~ MDL
N :::: Recovery is out of criteria
+ ; RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0213
Page: 60 of 78
Level 1 Report v2.1
Sample 10: 0026521-003
Batch: 26521
Analytical Method: 82608
Parameter
Tetrachloroethene
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
POL = Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS-LCSD
Spike
Amount Result
(ug/kg) (ug/kg) Q
2500 2500
Q % Rec Acceptance
Limit
104 47-138
107 53-142
100 68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec % RPD
50 101 1.5
% Rec
Limit
45-150
P =The RPD between two GC columns exceeds 40%
J = Estimated result< POL and;:: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit Analysis Date
20 07/31/2013 0237
Page: 61 of 78
Level 1 Report v2 .1
Sample ID: 0028442-001
Batch: 28442
Analytical Method: 82608
Parameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 A-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifluoromethane
1 ,2-Dichloroethane
1, 1-Dichloroethane
trans-1 ,2-Dichloroethene
cis-1 ,2-Dichloroethene
1 , 1-Dichloroethene
1 ,2-Dichloropropane
trans-1 ,3-Dichloropropene
cis-1 ,3-Dichloropropene
Ethylbenzene
2-Hexanone
I sopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane
1 ,2,4-Trichlorobenzene
1,1 ,2-Trichloroethane
1,1, 1-Trichloroethane
PQL ; Practical quantitation limit
ND ; Not detected at or above the PQL
Volatile Organic Compounds by GC/MS -MB
Matrix: Solid
Prep Method: 5035
Result Q Oil PQL Units
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
P = The RPD between two GC columns exceeds 40%
J = Estimated result < PQL and :0:: MDL
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/20 13 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
Page: 62 of78
Level1 Report v2.1
Sample ID: 0028442-001
Batch: 28442
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-0ichloroethane-d4
Toluene-dB
POL ;:; Practical quantitation limit
NO ~ Not detected at or above the POL
Volatile Organic Compounds by GC/MS-MB
Matrix: Solid
Prep Method: 5035
Result Q Dil PQL Units
NO
NO
NO
NO
Q % Rec
91
98
94
Acceptance
Limit
47-138
53-142
68-124
P ~ The RPD between two GC columns exceeds 40%
J ~ Estimated result< POL and:': MDL
5.0
5.0
5.0
5.0
ug/kg
ug/kg
ug/kg
ug/kg
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
0813012013 1235
08/30/2013 1235
08/30/2013 1235
08/30/2013 1235
Page: 63 of 78
Level 1 Report v2 .1
Volatile Organic Compounds by GC/MS-LCS
Sample 10: 0028442-002 Matrix: Solid
Batch: 28442 Prep Method: 5035
Analytical Method: 8260B
Spike
Amount Result % Rec
Parameter (ug/kg) (ug/kg) Q Oil %Rec Limit
Acetone 100 130 126 60-140
Benzene 50 43 87 69-123
Bromodichloromethane 50 44 87 69-121
Bromoform 50 44 89 61-119
Bromomethane (Methyl bromide) 50 50 100 10-168
2-Butanone (MEK) 100 100 105 57-148
Carbon disulfide 50 51 102 58-122
Carbon tetrachloride 50 45 89 58-136
Chlorobenzene 50 42 83 59-129
Chloroethane 50 49 98 42-163
Chloroform 50 44 88 71-125
Chloromethane (Methyl chloride) 50 51 103 34-134
Cyclohexane 50 43 87 53-139
1 ,2-Dibromo-3-chloropropane (DBCP) 50 42 84 55-125
Dibromochloromethane 50 43 86 66-119
1 ,2-Dibromoethane (EDB) 50 43 87 74-124
1 A-Dichlorobenzene 50 43 86 52-133
1 ,3-Dichlorobenzene 50 42 84 51-134
1 ,2-Dichlorobenzene 50 42 85 57-131
Dichlorodifluoromethane 50 42 84 10-157
1 ,2-Dichloroethane 50 46 91 67-129
1, 1-Dichloroethane 50 47 94 71-127
trans-1 ,2-Dichloroethene 50 48 95 68-131
cis-1 ,2-Dichloroethene 50 45 91 70-122
1, 1-Dichloroethene 50 43 87 69-138
1 ,2-Dichloropropane 50 44 87 72-124
trans-1 ,3-Dichloropropene 50 43 86 70-124
cis-1 ,3-Dichloropropene 50 43 86 70-126
Ethyl benzene 50 40 81 59-128
2-Hexanone 100 94 94 54-137
lsopropylbenzene 50 42 85 50-136
Methyl acetate 50 49 97 59-137
Methyl tertiary butyl ether (MTBE) 50 49 98 70-130
4-Methyl-2-pentanone 100 100 100 60-134
Methylcyclohexane 50 44 88 41-144
Methylene chloride 50 48 97 70-130
Styrene 50 43 87 54-136
1,1 ,2,2-Tetrachloroethane 50 45 89 69-132
Tetrachloroethene 50 41 81 45-150
Toluene 50 43 85 61-129
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50 46 93 49-136
1 ,2,4-T richlorobenzene 50 41 81 34-145
1,1 ,2-Trichloroethane 50 41 83 55-128
1,1, 1-Trichloroethane 50 46 93 63-128
POL = Practical quantitation limit
ND = Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J = Estimated result < POL and ": MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
08/30/2013 11 00
08/30/2013 1100
08/30/2013 11 00
08/30/2013 1100
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/20 13 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 1100
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 1100
08/30/2013 1100
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 1100
08/30/20 13 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 1100
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/20 13 11 00
08/30/20 13 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/20 13 11 00
08/30/2013 1100
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/2013 11 00
08/30/20 13 11 00
Page: 64 of 78
Level1 Report v2.1
Sample ID: 0028442-002
Batch: 28442
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-dB
Volatile Organic Compounds by GC/MS -LCS
Spike
Amount
(ug/kg)
50
50
50
100
Q % Rec
86
89
88
Result
(ug/kg) Q
42
47
59
85
Acceptance
Limit
47-138
53-142
68-124
Matrix: Solid
Prep Method: 5035
Dil % Rec
84
94
117
85
% Rec
Limit
62-126
45-138
42-132
58-128
PQL ~ Practical quantitation limit
ND Not detected at or above the POL
P :;: The RPD between two GC columns exceeds 40%
J ~ Estimated result< PQL and_:: MDL
N :;; Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
08/30/2013 1100
08/30/2013 1100
08/30/2013 1100
08/30/2013 1100
Page: 65 of 78
Level 1 Report v2 .1
Volatile Organic Compounds by GC/MS -LCSD
Sample ID: 0028442-003
Batch: 28442
Analytical Method: 8260B
Parameter
Spike
Amount
(ug/kg)
A~~~ 100
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1 ,2-Dibromo-3-chloropropane (DBCP) 50
Dibromochloromethane 50
1 ,2-Dibromoethane (EDB) 50
1 A-Dichlorobenzene 50
1 ,3-Dichlorobenzene 50
1,,2-Dichlorobenzene 50
Dichlorodifluoromethane 50
1 ,2-Dichloroethane 50
1, 1-Dichloroethane 50
trans-1 ,2-Dichloroethene 50
cis-1 ,2-Dichloroethene 50
1 , 1-Dichloroethene 50
1 ,2-Dichloropropane 50
trans-1 ,3-Dichloropropene 50
cis-1 ,3-Dichloropropene 50
Ethylbenzene 50
2-Hexanone 100
lsopropylbenzene 50
Methyl acetate 50
Methyl tertiary butyl ether (MTBE) 50
4-Methyl-2-pentanone 100
Methylcyclohexane 50
Methylene chloride 50
Styrene 50
1,1 ,2,2-Tetrachloroethane 50
Tetrachloroethene 50
Toluene 50
1,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1 ,2,4-T richlorobenzene 50
1,1 ,2-Trichloroethane 50
1,1, 1-Trichloroethane 50
Result
(ug/kg)
120
44
44
41
50
96
49
43
42
49
44
50
43
41
42
42
44
43
43
41
44
45
46
44
43
44
43
44
40
99
44
46
48
100
45
48
42
47
41
44
45
43
41
45
Q
Matrix: Solid
Prep Method: 5035
Oil % Rec %RPD
% Rec
Limit
122
87
88
83
100
96
98
85
83
98
88
100
86
82
84
84
88
85
86
82
89
90
92
88
86
88
86
88
79
99
88
92
95
103
89
97
84
93
82
89
90
86
82
91
3.3 60-140
0.51 69-123
0.73 69-121
6.6 61-119
0.31 10-168
8.9 57-148
4.1 58-122
5.0 58-136
0.26 59-129
0.045 42-163
0.44 71-125
2.5 34-134
0.57 53-139
2.7 55-125
2.6 66-119
2.6 74-124
1.7 52-133
1.1 51-134
0.80 57-131
2.7 10-157
3.2 67-129
4.5 71-127
3.1 68-131
2.6 70-122
0.79 69-138
1.0 72-124
0.57 70-124
2.7 70-126
2.2 59-128
5.1 54-137
3.5 50-136
5.4 59-137
2.8 70-130
2.4 60-134
0.96 41-144
0.24 70-130
2.6 54-136
4.8 69-132
0.58 45-150
4.0 61-129
2.7 49-136
5.9 34-145
1.5 55-128
1.8 63-128
POL = Practical quantitation limit
ND = Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J =Estimated result< POL and_:: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
%RPD
Limit Analysis Date
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
Page: 66 of 78
Level 1 Report v2.1
Sample ID: 0028442-003
Batch: 28442
Analytical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1 ,2-Dichloroethane-d4
Toluene-d8
POL= Practical quantitation limit
ND = Not detected at or above the POL
Volatile Organic Compounds by GC/MS -LCSD
Spike
Amount Result
(ug/kg) (ug/kg) Q
50 43
50 46
50 56
100 83
Q % Rec Acceptance
Limit
87 47-138
89 53-142
89 68-124
Matrix: Solid
Prep Method: 5035
Oil % Rec % RPD
86 1.5
93 1.1
112 4.4
83 2.9
% Rec
Limit
62-126
45-138
42-132
58-128
P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
+ = RPD is out of criteria J = Estimated result< POL and:: MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
20
20
20
20
Analysis Date
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
08/30/2013 1124
Page: 67 of 78
Level1 Report v2.1
Sample ID: 0025971-001
Batch: 25971
Analytical Method: 82700
Parameter
1, 1'-Biphenyl
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2 ,4-Dinitrotoluene
2 ,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
2-Nitrophenol
3 & 4-Methylphenol
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a )pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Caprolactam
Carbazole
Chrysene
Di-n-butyl phthalate
POL = Practical quantitation limit
ND =Not detected at or above the POL
Semivolatile Organic Compounds by GC/MS-MB
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Matrix: Solid
Prep Method: 3550C
Prep Date: 07/27/2013 1357
Q Oil PQL Units
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
830 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
670 ug/kg
830 ug/kg
330 ug/kg
830 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
830 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
830 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
830 ug/kg
330 ug/kg
330 ug/kg
330 ug/kg
P = The RPD between two GC columns exceeds 40%
J " Estimated result< POL and ;o: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
Page: 68 of 78
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS-MB
Sample ID: 0025971-001 Matrix: Solid
Batch: 25971 Prep Method: 3550C
Analytical Method: 82700 Prep Date: 07/27/2013 1357
Parameter Result Q Dil PQL Units
Di-n-octylphthalate NO 330 ug/kg
Dibenzo(a,h)anthracene ND 330 ug/kg
Dibenzofuran ND 330 ug/kg
Diethylphthalate NO 330 ug/kg
Dimethyl phthalate ND 330 ug/kg
Fluoranthene ND 330 ug/kg
Fluorene ND 330 ug/kg
Hexachlorobenzene ND 330 ug/kg
Hexachlorobutadiene ND 330 ug/kg
Hexachlorocyclopentadiene ND 830 ug/kg
Hexachloroethane ND 330 ug/kg
lndeno(1 ,2,3-c,d)pyrene ND 330 ug/kg
lsophorone ND 330 ug/kg
N-Nitrosodi-n-propylamine ND 330 ug/kg
N-Nitrosodiphenylamine (Diphenylamine) ND 330 ug/kg
Naphthalene ND 330 ug/kg
Nitrobenzene ND 330 ug/kg
Pentachlorophenol NO 830 ug/kg
Phenanthrene NO 330 ug/kg
Phenol ND 330 ug/kg
Pyrene ND 330 ug/kg
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 84 30-117
2-Fiuorobiphenyl 68 33-102
2-Fiuorophenol 73 28-104
Nitrobenzene-d5 67 22-109
Phenol-d5 77 27-103
Terphenyl-d14 108 41-120
POL Practical quantitation limit
ND = Not detected at or above the PQL
P The RPD between two GC columns exceeds 40%
J = Estimated result< PQL and": MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/29/2013 1040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/20131040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
07/29/2013 1040
Page: 69 of 78
Level 1 Report v2. 1
Sample 10: 0025971-002
Batch: 25971
Analytical Method: 82700
Parameter
1,1 '-Biphenyl
2,4,5-Trichlorophenol
2 ,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
2-Nitrophenol
3 & 4-Methylphenol
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo( a )anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Caprolactam
Carbazole
Chrysene
Di-n-butyl phthalate
POL ; Practical quantitation limit
ND ; Not detected at or above the POL
Semivolatile Organic Compounds by GC/MS -LCS
Matrix: Solid
Prep Method: 3550C
Prep Date: 07/27/2013 1357
Spike
Amount Result % Rec
(ug/kg) (ug/kg) Q Oil % Rec Limit
3300 2600 78 49-110
3300 2800 83 46-122
3300 2700 80 38-115
3300 3000 89 41-113
3300 3400 103 33-123
17000 17000 105 45-127
6700 6000 91 48-124
6700 6100 92 47-125
3300 2400 71 31-127
3300 2700 82 37-106
3300 2700 80 40-106
3300 3100 92 32-107
6700 5800 86 45-123
6700 5500 83 35-108
6700 5500 83 39-108
6700 6800 102 46-113
6700 5600 84 24-127
17000 18000 109 40-130
3300 2900 86 46-118
3300 3200 97 49-118
3300 3400 102 10-125
3300 2800 85 47-116
6700 7500 112 48-127
17000 20000 120 18-154
3300 2700 80 46-114
3300 3200 95 44-122
3300 2900 86 48-111
3300 2900 86 50-119
3300 2900 86 48-116
3300 2800 83 34-99
3300 2900 88 47-121
3300 3500 104 55-134
3300 3100 94 28-139
3300 3100 92 36-125
3300 2900 86 47-130
3300 2800 84 39-108
6700 4600 69 32-105
3300 2400 72 31-102
3300 3200 96 45-128
3300 3200 97 46-128
3300 3800 115 43-121
3300 3200 97 47-128
3300 2800 83 45-126
3300 3300 99 51-129
P ; The RPD between two GC columns exceeds 40%
J ; Estimated result< PQL and~ MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
07/29/20131106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/20131106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
Page: 70 of 78
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS-LCS
Sample ID: 0025971-002
Batch: 25971
Analytical Method: 8270D
Parameter
Di-n-octylphthalate
Dibenzo(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1 ,2,3-c,d)pyrene
lsophorone
Spike
Amount
(ug/kg)
3300
3300
3300
3300
3300
3300
3300
3300
3300
17000
3300
3300
3300
N-Nitrosodi-n-propylamine 3300
N-Nitrosodiphenylamine (Diphenylamine) 3300
Naphthalene 3300
Nitrobenzene 3300
Pentachlorophenol 17000
Phenanthrene 3300
Phenol 3300
Pyrene 3300
Surrogate Q % Rec
2,4,6-Tribromophenol 96
2-Fiuorobiphenyl 79
2-Fiuorophenol 84
Nitrobenzene-d5 88
Phenol-d5 85
Terphenyl-d14 116
Result
(ug/kg) Q
3100
3000
2700
3200
2900
3100
3000
3000
2700
13000
2300
3100
3000
2900
2900
2700
2700
17000
2800
2700
3200
Acceptance
Limit
30-117
33-102
28-104
22-109
27-103
41-120
Matrix: Solid
Prep Method: 3550C
Prep Date: 07/27/2013 1357
Dil % Rec
93
91
82
95
88
94
89
91
82
81
68
94
89
87
86
80
82
105
83
82
96
% Rec
Limit
49-142
45-122
45-112
49-123
48-120
50-123
48-117
44-122
33-103
18-121
30-96
45-123
41-113
32-115
53-150
36-110
33-114
27-138
49-117
36-108
47-119
POL ::: Practical quantitation limit
NO , Not detected at or above the POL
P , The RPD between two GC columns exceeds 40%
J , Estimated result< POL and .:0: MDL
N :::: Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/29/20131106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
07/29/20131106
07/29/2013 1106
07/29/2013 1106
07/29/2013 1106
Page: 71 of 78
Level 1 Report v2. 1
Semivolatile Organic Compounds by GC/MS-MS
Sample ID: OG26068-001MS
Batch: 25971
Analytical Method: 8270D
Parameter
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1 '-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo( a, h )anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Sample
Amount
(ug/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Spike
Amount
(ug/kg)
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
9400
4700
4700
4700
4700
4700
4700
4700
4700
4700
9400
4700
4700
4700
4700
23000
23000
9400
9400
4700
4700
4700
4700
4700
23000
Matrix: Solid
Prep Method: 3550C
Prep Date: 07/27/2013 1357
Result
(ug/kg)
2900
3200
2800
3200
3200
2900
3200
3700
4000
2100
3700
2700
3100
3500
1600
3500
3600
3200
2900
5100
2200
2400
3000
3100
3000
3700
3800
2200
2900
7300
3100
3300
3100
3800
19000
18000
6300
6300
3500
3500
3200
3400
2400
9000
Q Oil % Rec
62
69
59
69
69
62
69
79
85
46
78
59
67
74
34
74
77
69
62
55
48
51
65
65
65
78
82
47
62
78
67
70
66
82
81
76
67
67
75
74
68
72
52
38
P = The RPD between two GC columns exceeds 40%
J = Estimated result < PQL and": MDL
N = Recovery ls out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless fiagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% Rec
Limit Analysis Date
30-130 07/29/2013 1318
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
10-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
07/29/2013 1318
07/29/20131318
07/29/2013 1318
07/29/2013 1318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/20131318
07/29/20131318
Page: 72 of 78
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS-MS
Sample ID: OG26068-001MS Matrix: Solid
Batch: 25971 Prep Method: 3550C
Analytical Method: 82700 Prep Date: 07/27/2013 1357
Sample Spike
Amount Amount Result
Parameter (ug/kg) (ug/kg) (ug/kg) Q Dil % Rec
Hexachloroethane NO 4700 1700 35
lndeno(1 ,2,3-c,d)pyrene NO 4700 2400 50
lsophorone NO 4700 3100 65
2-Methylnaphthalene NO 4700 2700 58
2-Methylphenol NO 4700 3400 73
3 & 4-Methylphenol NO 9400 5800 62
N-Nitrosodi-n-propylamine NO 4700 2900 61
N-Nitrosodiphenylamine (Diphenylamine) NO 4700 3300 69
Naphthalene NO 4700 2500 53
2-Nitroaniline NO 9400 6100 64
3-Nitroaniline NO 9400 5700 61
4-Nitroaniline NO 9400 7900 84
Nitrobenzene NO 4700 2600 55
2-Nitrophenol NO 9400 5600 60
4-Nitrophenol NO 23000 22000 92
Pentachlorophenol NO 23000 20000 84
Phenanthrene NO 4700 3100 65
Phenol NO 4700 3200 69
Pyrene NO 4700 3400 73
2,4,5-Trichlorophenol NO 4700 3100 67
2,4,6-Trichlorophenol NO 4700 3000 63
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 76 30-117
2-Fiuorobiphenyl 58 33-102
2-Fiuorophenol 68 28-104
Nitrobenzene-d5 57 22-109
Phenol-d5 72 27-103
Terphenyl-d14 90 41-120
POL :::: Practical quantitation limit
ND" Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J " Estimated result< POL and': MDL
N ::;;: Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% Rec
Limit
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
Analysis Date
07/29/2013 1318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/2013 1318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
07/29/2013 1318
07/29/2013 1318
07/29/20131318
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07/29/2013 1318
07/29/2013 1318
07/29/20131318
07/29/20131318
07/29/20131318
Page: 73 of 78
Level 1 Report v2. 1
Semivolatile Organic Compounds by GC/MS -MSD
Sample 10: 0826068-001 MD
Batch: 25971
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 07/27/2013 1357
Sample
Amount
(ug/kg)
Spike
Amount
(ug/kg)
Result % Rec % RPD
Parameter (ug/kg) Q Oil % Rec % RPD Limit Limit Analysis Date
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1, 1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
POL = Practical quantitation limit
ND = Not detected at or above the POL
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
NO
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4700
4600
4700
4700
4700
4700
4700
4700
4700
9400
4700
4700
4700
4700
4700
4700
4700
4700
4700
9400
4700
4700
4700
4700
23000
23000
9400
9400
4700
4700
4700
4700
4700
23000
3500
3900
3400
3800
3800
3400
3800
4500
4800
2400
4400
3200
3800
4000
1800
4000
4200
3800
3300
5300
2700
2800
3200
3600
3600
4200
4600
2500
3500
8800
3600
3800
3600
4300
22000
21000
7400
7400
4000
4000
3800
4100
3000
11000
P =The RPD between two GC columns exceeds 40%
J = Estimated result < POL and.': MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
74
83
73
81
81
74
81
96
102
51
94
69
80
85
38
85
89
82
70
56
57
60
68
77
78
90
98
53
74
94
78
81
77
92
94
91
79
79
86
86
80
87
64
49
17
18
20
16
16
16
16
19
18
10
18
16
18
13
12
13
15
16
12
2.1
17
16
4.9
17
17
15
18
10
18
18
15
15
16
11
15
17
15
16
14
15
16
18
22
24
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
10-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
N = Recovery is out of criteria
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/20131344
40 07/29/20131344
40 07/29/20131344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/20131344
40 07/29/2013 1344
40 07/29/2013 1344
Page: 74 of 78
Level1 Report v2.1
Semivolatile Organic Compounds by GC/MS-MSD
Sample ID: OG26068-001MD Matrix: Solid
Batch: 25971 Prep Method: 3550C
Analytical Method: 82700 Prep Date: 07/27/2013 1357
Sample Spike
Amount Amount Result % Rec
Parameter (ug/kg) (ug/kg) (ug/kg) Q Oil % Rec % RPD Limit
Hexachloroethane ND 4700 2100 45 23 30-130
lndeno(1 ,2,3-c,d)pyrene ND 4700 2600 56 11 30-130
lsophorone ND 4700 3500 74 12 30-130
2-Methylnaphthalene ND 4700 3200 69 18 30-130
2-Methylphenol ND 4700 4000 86 17 30-130
3 & 4-Methylphenol ND 9400 7000 75 18 30-130
N-Nitrosodi-n-propylamine ND 4700 3400 73 17 30-130
N-Nitrosodiphenylamine (Diphenylamine) ND 4700 3800 82 16 30-130
Naphthalene ND 4700 3000 64 17 30-130
2-Nitroaniline ND 9400 7100 76 16 30-130
3-N itroaniline ND 9400 6700 72 16 30-130
4-Nitroaniline ND 9400 9100 97 14 30-130
Nitrobenzene ND 4700 3100 66 18 30-130
2-Nitrophenol ND 9400 6700 71 16 30-130
4-Nitrophenol ND 23000 23000 99 7.0 30-130
Pentachlorophenol ND 23000 23000 98 15 30-130
Phenanthrene ND 4700 3600 77 17 30-130
Phenol ND 4700 3600 77 11 30-130
Pyrene ND 4700 4000 85 15 30-130
2,4,5-Trichlorophenol ND 4700 3700 79 16 30-130
2 ,4,6-Trichlorophenol ND 4700 3500 74 15 30-130
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 91 30-117
2-Fiuorobiphenyl 67 33-102
2-Fiuorophenol 85 28-104
Nitrobenzene-d5 69 22-109
Phenol-d5 80 27-103
Terphenyl-d 14 105 41-120
POL~ Practical quantitation limit
ND ~ Not detected at or above the POL
P =The RPD between two GC columns exceeds 40%
J ~ Estimated result< POL and~ MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
Analysis Date
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/20131344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
07/29/2013 1344
Page: 75 of 78
Level 1 Report v2.1
Sample ID: 0025994-001
Batch: 25994
Analytical Method: 601 OC
Parameter
Lead
Nickel
Result
NO
NO
Q
ICP-AES-MB
Oil
Matrix: Solid
Prep Method: 3050B
Prep Date: 07/29/2013 1017
PQL
0.50
2.0
Units
mg/kg
mg/kg
POL = Practical quantitation limit
ND = Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and~ MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0543
07/31/2013 0543
Page: 76 of 78
Level 1 Report v2.1
Sample 10: 0025994-002
Batch: 25994
Analytical Method: 6010C
Parameter
Lead
Nickel
Spike
Amount
(mg/kg)
250
100
ICP-AES -LCS
Result
(mg/kg)
240
100
Q
Matrix: Solid
Prep Method: 30508
Prep Date: 07/29/2013 1017
Oil % Rec
98
101
% Rec
Limit
80-120
80-120
POL= Practical quantitation limit
NO = Not detected at or above the POL
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and;: MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
07/31/2013 0547
07/31/2013 0547
Page: 77 of 78
Level1 Report v2.1
Sample ID: 0025994-003
Batch: 25994
Analytical Method: 6010C
Parameter
Lead
Nickel
PQL ~ Practical quantitation limit
ND ~ Not detected at or above the PQL
Spike
Amount
(mg/kg)
250
100
ICP-AES • LCSD
Result
(mg/kg) Q
250
100
Matrix: Solid
Prep Method: 3050B
Prep Date: 07/29/2013 1017
% Rec
Oil % Rec %RPD Limit
102 4.3 80-120
103 2.2 80-120
P ~ The RPD between two GC columns exceeds 40%
J ~ Estimated result< PQL and~ MDL
N = Recovery is out of criteria
+ = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
20
20
Analysis Date
07/31/2013 0551
07/31/2013 0551
Page: 78 of 78
Level 1 Report v2.1
SHEALY
SC DHEC No: 32010
NVIRONMENTAL SERVICES INC.
NELAC No: E87653
Case Narrative
Terracon Consultants, Inc.
Lot Number: OJ12005
NC DENR 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
GC/MS VOC
Due to matrix interferences, samples -002, -003, -006, and -012 all required 50X dilutions in order to analyze. All target compounds were non-detect
at this dilution.
The LCSD associated with batch 31803 recovered MTBE below method criteria. Sample -009 was analyzed twice confirming the non-detection for
MTBE. No more vials remained to perform a third analysis. All other QC were within method criteria.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 2 of 72
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: OJ12005
Sample Number Sample ID Matrix Date Sampled
001 SSS-11-8 Solid 10/10/2013 1200
002 SSS-12-6 Solid 10/10/20131225
003 SSS-13-8 Solid 10/10/2013 1240
004 SSS-14-2 Solid 10/10/2013 1300
005 SSS-15-8 Solid 10/10/2013 1320
006 SSS-16-6 Solid 10/10/2013 1335
007 SSS-17-6 Solid 10/10/2013 1355
008 SSS-17-8 Solid 10/10/2013 1405
009 SSS-18-4 Solid 10/10120131425
010 SSS-19-4 Solid 10/10/2013 1515
011 SSS-20-8 Solid 10/1012013 1530
012 SSS-20-10 Solid 1 0/1 012013 1540
013 SSS-21-Solid 10/10/2013 1555
014 SSGW-1-16 Aqueous 10/10/2013 1605
015 TRIP Aqueous 10/10/2013
(15 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Date Received
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/11/2013
10/1112013
10/11/2013
10/11/2013
1011112013
10/11/2013
Page: 3 of72
Level 1 Report v2.1
I SHEALY ENVIRONMENTAL SERVICES, INC.
I
I
Executive Summary
Terracon Consultants, lnc.
Lot Number: OJ12005
Sample Sample lD Matrix Parameter Result O Page
I
I
t
I
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T
t
I
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I
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I
001 sss-11-8
001 sss-11-8
001 sss-11-8
001 sss-11-8
001 sss-11-8
001 sss-l1-8
002 sss-12-6
002 sss-12-6
004 sss-14-2
004 sss-14-2
005 sss-'t5-8
006 sss-16-6
006 sss-l6-6
007 sss-17-6
007 sss-l7-6
007 sss-l7-6
007 sss-17-6
007 sss-17.6
007 sss-17-6
007 sss-17-6
007 sss-I7-6
007 sss-l7-6
007 sss-17-6
007 sss-17-6
007 sss-17-6
008 sss-17-8
008 sss-17-8
008 sss-l7-8
008 sss-17-8
008 sss-l7-8
008 sss-17-8
008 sss-17-8
008 sss-17-8
008 sss-17-8
008 sss-17-8
009 sss-18-4
009 sss-I8-4
009 sss-18-4
009 sss-18-4
010 sss-19-4
010 sss-19*4
010 sss-19-4
011 SSS-20-8
011 SSS-20-8
013 SSS-21-
1 ,1-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
Tetrachloroethene
1, 1,2-Trichloroethane
Trichloroethene
Methyl acetate
Tetrachloroethene
Acetone
Methylene chloride
1 ,1 -Dichloroethane
Tetrachloroethene
Xylenes (total)
Cyclohexane
1 ,1-Dichloroethane
cis-1,2-Dichloroethene
Ethylbenzene
lsopropylbenzene
Methyl acetate
4-Methyl-2-pentanone
Methylene chloride
Tetrachloroethene
Toluene
Trichloroethene
Xylenes (total)
1 , 1-Dichloroethane
cis-1,2-Dichloroethene
Ethylbenzene
Methyl acetate
4-Methyl-2-pentanone
Methylene chloride
Tetrachloroethene
Toluene
Trichloroethene
Xylenes (total)
Acetone
2-Butanone (MEK)
1 , 1-Dichloroethane
cis-1,2-Dichloroethene
Methyl acetate
4-Methyl-2-pentanone
Tetrachloroethene
Acetone
Tetrachloroethene
Acetone
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
6
b
o
6
7
7
I
8
12
12
14
16
17
18
18
18
18
18
18
18
18
18
t9
19
19
20
20
20
20
20
20
20
2',1
21
21
22
22
22
22
24
24
24
2A
26
30
8260B
82608
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
82608
48
59
1.1
4.1
1.9
2.5
65
100
27
8.3
1.3
75
340
220
260
1 4000
540
.t00
340
820
23000
1800
260
1 00000
't000
450
8800
420
360
2300
1 1 0000
't90000
310
140000
810
68
9.3
0.98
4.1
350
93
44
29
1.'.|
2',1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uS/kg
ug/kg
ug/kg
ug/kg
usfts
ug/kg
us/kS
ug/kg
uS/kS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uO/ke
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
Sh€aly Envlronmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
Page: 4 of 72
L6vel 'l Report v2,1
T
Executive Summary (Continued)
Lot Number: OJ12005
Sample Sample lD Matrix Parameter Result O
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
014 SSGW-1-16
Aqueous Chloroethane
Aqueous Chloromethane(Methylchloride)
Aqueous 1,1-Dichloroethane
Aqueous cis-1,2-Dichloroethene
Aqueous trans-1,2-Dichloroethene
Aqueous 4-Methyl-2-pentanone
Aqueous Methylenechloride
Aqueous Trichloroethene
Aqueous Vinyl chloride
82608
82608
8260B
82608
8260B
82608
8260B
82608
82608
1.6
0.33
5.5
130
4.0
3.7
480
320
6.2
J
J
J
J
I
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t
I
I
t
I
ug/L 32
ug/L 32
ug/L 32
ug/L 32
ug/L 32
ug/L 32
ug/L 32
ug/L 33
ug/L 33
(54 detections)
I
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Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page: 5 of72
Level 1 Report v2.'l I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-001
Description: SSS.11-8 Matrix: Solid
Date Sampled:1011012013 1200 % Solids: 68.6 1011212013 1612
Date Received : 10111 12013
Volatile Orqanic Compounds by GC/MS
Batch
31 803
31 948I *rn
2
Prep Method
5035
s035
AnalyticalMethod Dilution82608 1
82608 1
Analysis Date Analyst Prep Date
10114t2013 1504 AAC
10115t2013 1205 AAC
Sample Wt.(g)
6.07
5.63
I Parameter
CAS Analytical
Number Mathad Result O
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
12
6.0
6.0
6.5
12
6.0
6.0
6.0
6.0
6.0
I
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Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T et'e, chloroethan e
Tetrachloroethene
67-64-1
71-43-2
75-27-4
7s-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75.34-3
107-06-2
7*354
1 56.59.2
1 56-60-s
78-87-5
10061-01-5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-184
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
8260B
82608
8260B
8260B
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
48
ND
59
1.1 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1-1 J
24
6.0
6.0
6.0
6.0
12
6.0
6.0
6.0
6.0
6-0
6.0
6.0
8.0
1.3
2.0
0.84
2.2
2.9
't.6
2.2
2.0
1.6
1.0
1.2
0.81
1.8
2.0
1.0
2.0
2.0
2.0
1.9
0.88
1.2
2.0
0.91
1.8
1.1
0.82
0.98
2.0
1.6
0.28
1.2
0.52
1.8
0.49
3.1
1.3
0.56
0.60
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ugI(S 1
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
udkS I
ug/kg 1
ug/kg 1
ug/kg 1
ugrkg 1ug/kg 1
usrkg 1
uglkg 1
ug/kg 1
ug/kS 1
uS/kS 1
ug/kg 1
ug/kS 1
ug/kg 'l
ug/kS 1
ug/kg 1
ug/kg 2
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
uglkg 1
I PQL = Practical quantitation limit B = Detscted in ths method blank E = Quantitation of compound exceeded the calibration range
ND = Not dstsct€d at or above the MDL J = Estimatod result < POL and: MDL P - The RPD between two GC columns excsods 400/6
Whore applicable, all soil samplo analysis ar6 reported on a dry w€ight basis unless flagged with a 'W'
H = Out of holding tims
N = Recovory is ort of critErla
Shealy Environmental Services, lnc.I 106 Vantage Point Driv6 West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.comI Page: 0 of 72
Lov6l 1 Roportv2.l
t
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-001
Description: SSS-11-8 Matrix: Solid
Date Sampled:'1011012013 1200 % Solids: 68.6 1011212013 1612
Date Received : 10111 12013
Volatile Organic Compounds by GC/MS
I
I
IRun
1
2
Prep Method
5035
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 10rt412013 1504 AAC
82608 1 10t1st2013 1205 AAC
Batch Sample Wt.(g)31803 6.07
31948 5.63
Parametel
cAs
Number
Analytical
Marhod Result O I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
'1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate % Recovery LimiG O % Recovery Limits
1 08-88-3
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 Acceptance
8260B
82608
82608
82608
82608
8260B
82608
82608
82608
ND
ND
ND
ND
1.9 J
2.5 J
ND
ND
ND
Run 2 Acceptance
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg Iug/kg 1ug/kg 1
ug/kg 1
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
2.0
0.76
2.0
1.0
0.95
2.3
1.8
1.0
3.5
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8 I
I
I
I
I
I
I
I
I
95
92
93
53-142
47-138
68-124
76
81
90
53-'.t42
47-138
68-124
POL = Practical quantilation limil B = Det*tsd in the mslhod blank E = Quantitation of @mpound sxceedsd the calibration range
ND = Not dstected at or above the MDL J = Estimatod rosult < PQL and: MDL P = The RPD betreen two GC columns excesds 40%
whore applicabl€, all soil sample anal),sis ars reported on a dry lr€ight basis unless flaggod with a "w'
H = Out of holding time
N = Recovery is out of criterla I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyhb.com
Page:7 ol72
Level 1 Report v2.1 I
I
I
T
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005.002
Description: 555-12-6 Matrix: Solid
Date Sampled:1011012013 1225 % Solids: 89.4 1011212013 1612
Date Received : 1 011 1 12013
Volatile Orqanic Compounds bv GC/MS
Run Prep MethodI 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 50 10t14t2013 1638 AAC
Batch Sample Wt.(g)31805 6.25
Parameter
cAs
Number
Analytical
Mathad Result O MDL Units Run
I
T
I
T
I
I
I
I
I
t
I
t
I
I
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
tIans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2 -T etachloroeth a ne
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-'t 5-0
s6-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-',1
1 06-46-7
75-7'.t-8
75-34-3
107-06-2
75-35-4
1 56-59-2
156-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-',t8-4
1 08-88-3
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 'l
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1uS/kS 1ugftg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg I
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
uS/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1ug/kg 1
ug/kg 'l
82608 ND 900
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 450
82608 ND 22082608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 22082608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 22082608 ND 22082608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 450
82608 ND 220
82608 65 J 220
82608 ND 220
82608 ND 450
82608 ND 220
82608 ND 220
82608 ND 220
82608 ND 22082608 r00 J 220
82608 ND 220
300
49
76
31
81
110
58
81
76
58
37
45
30
67
76
38
76
7A
76
72
33
45
76
34
a7
41
30
37
76
58
10u
18
67
18
120
49
21
22
76
PQL = Practical quantitation limit B = Detected in the msthod blank E = Quantitation of compound excoeded the calibration range H = Out of holding time
ND = Notdetected atorabove the MDL J = Estimated result< PQLand: MDL P =Ths RPD botween two GC columns exmeds 40olo N = Recovsryis outofcriteria
Where applicable, all soil sample analysis are reporied on a dry wsight basis unlsss flagged with a 'VV'
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:8 ot72
Level I Rsport v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-002
Description: 555-12-6 Matrix: Solid
Date Sampled:10r10r2013 1225 % Solids: 89.4 1011212013 1612
Date Received : 10111 12013
Volatile Orsanic Gompounds by GC/MS
t
T
IRun Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 50 1011412013 1638 AAC
Batch Sample Wt.(g)31805 6.25
Parameter
CAS Analytical
Number Method Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-1 3-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run I AcceptanceO % Recovery Limits
82608
82608
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
I
I
I
220 28 ug/kg 1
220 76 ug/kg 1
220 38 ug/kg 1
220 35 ug/kg 1
220 85 ug/kg 1
220 67 ug/kg 1
220 38 ug/kg 1
220 130 ug/kg 'l
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
I
I
I
I
I
I
I
I
I
I
90
97
84
53-142
47-138
68-124
PCIL = Practical quanftation limit B = D€tected in the mBthod blank E = Quantitation ofcompound excoeded ths calabration range
ND = Not detectod at or abov€ the MDL J = Estimated result < PQL and: MDL P = Th6 RPD botw€en lwo GC columns exceeds 407o
where applicable, all soil sample analysis are roported on a dry weight basis unless llagged with a nv'
H = Out of holdlng time
N = Recovery is out of criteria t
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 9 of 72
LEvel 1 Reportv2.l I
I
t
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-003
Description: SSS-13.8 Matrix: Solid
Date Sampled:10l1012013 1240 % Solids: 73.8 1011212013 1612
Date Received :'l 0 I 1 1 l2O1 3
Volatile Orsanic Compounds by GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 50 101',t4t2013 1702 AAC
Batch Sample Wt.(g)31805 5.22
Parameter
CAS
Number
Analytical
Method Result O MDL Units Run
I
t
I
t
I
I
t
I
I
I
I
I
I
I
I
I
t
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T et achloroetha ne
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
7s-34-3
1 07-06-2
75-35-4
156-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
1 08-88-3
1 300
320
320
320
320
650
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
320
650
320
320
320
650
320
320
320
320
320
320
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
430 ug/kg 1
71 ug/kg 1
1 10 ug/kg 1
45 ug/kg 1
120 ug/kg 1
160 ugftg 1
84 ug/kg 1
120 ug/kg 1
110 ug/kg 1
84 ug/kg 1
54 ug/kg 1
65 ug/kg 1
44 ug/kg 'l
97 ug/kg 'l
110 ug/kg 1
55 ug/kg 1
110 ug/kg 1
1 10 ug/kg 1
110 uS/kS 1
100 ug/kg 'l
47 ug/kg 1
65 ug/kg 1
110 uglkg 'l
49 ug/kg 1
97 ug/kg 1
59 ug/kg 1
44 ug/kg 1
53 ug/kg 1
1'10 uSftS 1
84 ug/kg 1
15 uS/kS 1
64 ug/kg 1
26 ug/kg 1
97 ug/kg I
27 uslkg 1
170 ug/kg 1
71 ug/kg 1
31 ug/kg 1
32 ug/kg 1
110 ug/kg 1
PQL = Practical quanti&ation,imil B = Deteclsd in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Notdotectod atorabovethe MDL J = Estimatod r€sult< PQL and: MDL P =The RPD bstween lwo GC columns excseds 40% N = Recoveryis oulofcritsria
Wh6re applicablB, all sil sample analysis are reportod on a dry weight basis unless flagged with a "W"
Shealy Environmental S€rvices, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: t0 of72
Level I Roport v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005.003
Description: SSS-13-8 Matrix: Solid
Date Sampled:'1011012013 1240 % Solids: 73.8 1011212013 1612
Date Received: 10/111201 3
Volatile Orsanic Compounds by GC/MS
I
I
IRun
1
Prep Method
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 50 101',t412013 1702 AAc
Batch Sample Wt.(g)3180s 5.22
Parameter
cAs
Number
Analytical
Mathad Result A MDL
1, 1,2-Trichloro- 1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uorometha ne
Vinyl chloride
Xylenes (total)
Surrogate
76-',13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-0',1-4
1330-20-7
Run 1 AcceptanceO 7o Recovery Limits
8260B
8260B
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
320 41 ug/kg 1
320 'l 10 ug/kg 1
32O 55 ug/kg 1
320 51 ug/kg 1
320 120 ug/kg 1
320 97 ug/kg 1
320 56 ug/kg 1
320 190 ug/kg 1
I
t
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
I
I
I
I
I
t
t
I
I
I
96
83
90
53-142
47-138
68-124
POL = Practicalquantitation limit B = Dotected in tho msthod blank E = Quantiiation ofcompound excosded the calibration range
ND = Not d6tect6d at or abova tho MDL J = Estimaled rssult < PQL and: MDL P = The RPD betreen two GC columns oxcoods 40%
where applicabls, all soil sample analysis aro roported on a dry weight basis unlsss flagged with a'\i/'
H = Out of holding tims
N = Recovsry is out of criteria T
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page:11 ot72
Lovel 1 Rsportv2.l
T
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-004
Description: SSS-14-2 Matrix: Solid
Date Sampled:10/10/2013 1300 % Solids: 81.3 '1011212013 1612
Date Received : 101'l 1 12013
Volatile Orqanic Compounds by GC/MS
Run Prep Method2 5035
Analytical Method Dilution Analysis Date Analyst82608 1 10115120131316 AAC
Prep Date Batch Sample Wt.(g)31948 5.29
Parameter
CAS
Number
Analytical
Mathad Result O PQL MDL Units Run
I
I
I
I
I
I
I
I
I
t
I
t
I
I
I
I
I
27
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.3
ND
ND
ND
ND
23
5.8
5.8
5.8
5.8
12
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
12
5.8
5.8
5.8
12
5.8
5.8
5.8
5.8
5.8
5.8
7.8
1.3
2.0
0.81
2.1
2.8
1.5
2.',|
2.0
1.5
0.96
1.2
0.78
1.7
2.0
0.99
2.0
2.0
2.0
1.9
0.85
1.2
2.O
0.88
1.7
1.1
0.79
0.95
2.0
1.5
0.27
1.1
0.46
1.7
0.48
3.0
1.3
0.55
0.58
2.O
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butranone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2 -7 elnchloroeth a n e
Tetrachloroethene
Toluene
67.64.1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
12448-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
156-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
't08-'t0-1
108-87-2
75.09-2
1 00-42-5
79-34-5
127-18-4
108-88-3
82608
8260B
82608
82608
82608
82608
8260B
82608
8260B
82608
82608
8260B
82608
82608
8260B
8260B
8260B
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
82608
82608
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2ug/kS 2ug/kS 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
uS/kS 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2ug/kg 2
ug/kg 2ug/kg 2
ug/kg 2
ug/kS 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ugkS 2
ug/kg 2
ug/kg 2
ug/kS 2
uglkg 2
ug/kg 2
uS/kS 2
ug/kg 2
ug/kS 2
PQL = Practical quantitation limit B = D€tected in th6 melhod blank E = Quantitation of compound oxca€ded tho calibration range H = Out of holding tims
NO = Notdetoctsd at orabove th6 MDL J = Estimated result< PQL and: MDL P =Th6 RPD botween iwo GC columns exceeds40%
Where applicablo, all soil sampls analysis ara reporled on a dry woight basis unless flaggsd with a "W"
N = Recovery is out of criteria
Shealy Environmental Services, lnc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
Pagez 12 ot72
Lev6l I Roport v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-004
Description: SSS-14-2 Matrix: Solid
Date Sampled:10/10/2013 1300 % Solids:8l.3 10112120131512
Date Received : 1011 1 12013
Volatile Orsanic Compounds by GC/MS
I
t
IRun
2
Prep Method
5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 I 1011512013'1316 AAC
Batch Sample Wt.(g)31948 s.29
Parameter
CAS Analytica!
Number Method Result O POL
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surogate
76-13-1
120-82-'.!
71-55-6
79-00-s
79-01-6
75-69-4
75-01-4
1 330-20-7
Run 2 AcceptanceO 7o Recovery Limits
82608
82608
8260B
82608
82608
82608
82608
8260B
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2ug/kg 2
uglkg 2ug/kg 2
ND
ND
ND
ND
ND
ND
ND
ND
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
0.73
2.0
0.99
0.92
2.2
1.7
1.0
3.4
I
I
t
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
87
80
91
53-142
47-138
68-124
I
I
T
I
I
I
t
I
I
I
PQL = Practical quantitation limil B = Dotected in tho method blank E = Quantita{on of compound exce€dod the calibration range
ND = Not dstectod at or above the MDL J = Estimated rosult < PQL and: MDL P = The RPD betwosn two GC columns oxceeds 40olo
Whore applicable, all soil sample analysis are reporled on a dry weight basis unloss flagged with a nV'
H = Out of holding tim6
N = Recovery is out of critoria t
Shealy Environm€ntal Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 (8031791-9700 Fax[phone] www.shealylab.com
Page: '13 of 72
Lewl 1 Report v2.1 I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-005
Description: SSS-15-8 Matrix: Solid
Date Sampled:1011012013 1320 % Solids: 78.9 1011212013'1612
Date Received : 1Ol'l 1 12013
Volatile Orqanic Compounds bv GC/MS
I Run Prep Method1 50352 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 1011412013 1528 AAC
82608 1 10t15t2013 1229 AAC
Batch Sample Wt.(g)31803 5.74
31948 5.15
POLIParameter
cAs
Number
Analytical
Mathod Result O MDL Units Run
t
t
t
I
t
I
I
t
I
I
I
t
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uorom ethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etr achloroethan e
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
't10-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
I 0061 -01-5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
7s-09-2
1 00-42-5
79-34-5
't27-18-4
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
8260B
8260B
82608
8260B
8260B
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
8260B
8260B
82608
8260B
82608
8260B
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg 1
ug/kg 1
ug/kg 1
ug/ks 1
ug/kg 1
ug/kg 1
ug/kS 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
usikg 1
ug/kg 1
USI(S 1
ug/kg 'l
ug/kg 'l
uS/kS 1
ugftg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 'l
ug/kg 2
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
22
5.5
5.5
5.5
5.5
11
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
11
5.5
5.5
6.2
11
5.5
5.5
5.5
5.5
5.5
7.4
1.2
1.9
0.77
2.0
2.6
1.4
2.0
1.9
1.4
0.92
1.1
0.74
1.7
1.9
0.94
1.9
1.9
1.9
1.8
0.81
1.1
1.9
0.84
1.7
1.0
0.75
0.91
1.9
1.4
0.25
1.1
0.49
1.7
0.45
2.9
1.2
0.52
0.55
t PQL = hactical quantitation limil B = Detsctsd in the msthod blank E = Quantitation of compound exceeded the calibration range
ND = Not dotectsd at or abovs the MDL J = Estimated rosult < PQL and: MDL P = The RPD b6twe6n two GC columns sxc€sds 40%
Whsre applicabls, all soil samplo analysis are roporiod on a dry waight basis unless flagged with a "W"
H = Out of hdding tim€
N = Recovory is out of criterla
Shealy Environmental Services, lnc.
I
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:11 ol72
Level I Reportv2.'l
t
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-005
Description: SSS-15-8 Matrix: Solid
Date Sampled:1011012013 1320 % Solids: 78.9 1011212013 16'12
Date Received : 1011 1 12013
Volatile Orsanic Gompounds by GC/MS
I
I
IBatch
31 803
31948
Run
1
2
Prep Method
5035
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 10rt4t2013 1528 AAC
82608 1 10t1512013 1229 AAC
Sample Wt.(g)
5.74
5.15
Parametel
CAS Analytical
Number Mathod Result O I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Run I AcceptanceO % Recovery Limits O
ND
ND
ND
ND
ND
ND
ND
ND
ND
Run 2 Acceptance
1 08-88-3
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
't 330-20-7
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
82608
82608
82608
82608
8260B
82608
82608
82608
82608
1.9
0.70
1.9
0.94
0.87
2.1
1.7
0.9s
3.2
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
I
I
I% Recovery Limlts
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
89
88
95
53-142
47-138
68-124
86
80
88
53-142
47-138
68-124 I
I
I
I
I
I
I
I
T
PCIL = Practical quantitation limit B = Dgtectod in the method blank E = Quantitation of compound exc€eded the calibration rang6
ND = Not dolscled at or above lh6 MDL J = Estimated result < PQL and: MDL P = The RPD between two GC columns exceeds 40olo
Where applicable, all soil sample analysis are reported on a dry weight basis unless f,agged wlth a nV'
H = Out of holding time
N = Recovery is out of critsria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page: 15 of72
Lovel 'l R€port v2.1 I
t
t
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-006
Description: 5S5-16-6 Matrix: Solid
Date Sampled:10/10/2013 1335 % Solids: 69.9 1011212013 16'12
Date Received: 1011112013
Volatile Organic Compounds by GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 50 10/t42013 1749 AAC
Batch Sample Wt.(g)
31805 4.57
Parameter
CAS
Number
Analytical
Meihod Result A MDL Units Run
t
I
t
I
I
I
I
I
t
I
I
I
I
t
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
tra ns- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etr achloroeth a n e
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-s
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
't00.4'r-4
591.78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
1 00-42-5
79-34-5
127-18-4
1 08-88-3
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
8260B
8260B
82608
8260B
82608
1 600
390
390
s90
390
780
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
390
780
390
390
390
780
390
390
390
390
390
390
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
75J
ND
520 ug/kg 1
86 ug/kg 1
130 ug/kg 1
55 ug/kg 1
14O ug/kg 1
190 ug/kg 'l
100 ug/kg 1140 ug/kg 1
130 ug/kg 1
100 ug/kg 1
65 uSlkS 1
78 ug/kg 1
53 ug/kg 1
120 ug/kg 1
130 ug/kg 1
67 ug/kg 1
130 ug/kg 1
130 ug/kg 1
130 ug/kg 1
130 ug/kg 1
57 ug/kg 1
78 ug/l<g 1130 udkS 1
59 ug/kg 1
120 ug/kg 1
71 ug/kg 1
53 udkg I
64 ug/kg 1
130 us/kg 1
100 ug/kg 1
18 ug/kg 1
77 ug/kg 1
31 uglkg 1
120 ug/kg 1
32 ug/kg 1
200 uS/kS 1
86 ug/kg 'l
37 uS/kS 1
39 uSftg 1
130 ug/kg 'l
PQL = Practical quanlitation limit B = D€tected in the method blank E = Quantitation of compound oxc€oded the calibration range H = Out of holding fme
ND = Notdetoctgd at orabove the MDL J = Estimated result< PQLand: MDL P = The RPD between two GC columns 6xce6ds 40% N = Recovoryis outotcritsria
Wher6 applicabls, all soil Bample analysis ar6 reported on a dry wsighl basis unlsss flaggod with a nv'
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:16of72
L6wl I Roportv2.l
Client:Terracon Gonsultants, lnc. Laboratory lD: OJ12005-006
Description: 555-16-0 Matrix: Solid
Date Sampled:10/10/2013 1335 % Solids: 69.9 1011212013 1612
Date Received : 1011 1 12013
Volatile Organic Compounds by GC/MS
I
I
IRun
1
Prep Method
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 50 1011412013 1749 AAC
Batch Sample Wt.(g)31805 4.57
Parameter
CAS Analytical
Number Marhod Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,'l -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-'13-1
120-82-1
71-55-6
79-00-5
79-01-6
7s-69-4
75-01-4
1330-20-7
Run 1 AcceptanceA % RecovGry Limits
I
I
I
82608 ND 390 49
82608 ND 390 130
82608 ND 390 67
82608 ND 390 62
82608 ND 390 150
82608 ND 390 120
82608 ND 390 67
82608 340 J 390 230
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ugrkg 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
I
I
I
I
I
I
t
I
I
I
89
77
82
53-142
47-',t38
68-124
PQL = Practical quantitation limit B = Dotected in the msthod blank E = Quaniitalion ofcompound sxceeded lhe callbration range
ND = Not det€cted at or above the MDL J = Estimated result < PQL and: MDL P = Ths RPD botw€en two GC mlumns ex€6ds 40olo
Where applieble, all soil samplo analysis are rsportsd on a dry reighl basis unless ilaggod with a w'
H = Out of holding time
N = Recovory is out ofcritoria I
Shealy Environmental Services, lnc.
106 Vantag€ Point Drive West Columbia, SC 29172 [phone] Fax [phone]'t 1 www.shealylab.com
Page:17 ot72
Lovel I Report vz.l I
I
I
I
Client:Terracon Consultants, lnc, Laboratory lD: OJ12005-007
Description: 555-17-6 Matrix: Solid
Date Sampled:10/10/2013 1355 % Solids: 82.2 1011212013 1612
Date Received : 1011 1 12013
Volatile Orqanic Gompounds bv GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 100 1011412013 1812 AAC
82608 1000 10115t20',t3 1427 AAC
Batch Sample Wt.(g)31805 5.15
31949 5.15
Parameter
cAs
Numbar
AnalyticalMarhart Result O
t
t
I
I
I
I
I
I
t
I
T
I
I
T
t
t
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-'t,2-Dichloroethene
trans- 1, 2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-'l etachloroethane
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
I 08-90-7
75-00-3
67.66-3
74.87-3
110-82-7
96-12-8
124-48-1
106"93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75.3'f-3
't07-06-2
75-35-4
't s6.59.2
1 56.60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
10041-4
591-78-6
98-82-8
79-20.9
1634-04-4
108.10-1
108-87-2
75.09-2
100-42-5
79-34-5
127-18-4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
220 J
ND
ND
ND
ND
ND
ND
ND
260 J
ND
ND
r4000
ND
ND
ND
ND
540 J
ND
100 J
340 J
ND
820 J
ND
23000
ND
ND
1800
790 ug/kg
130 ug/kg
200 ug/kg
83 ug/kg
210 ug/kS280 ug/kg150 ug/kg
210 ug/kg
200 ug/kg
150 ug/kg
98 ug/kS
120 ug/kg80 ugrkg
180 ugfl(g200 ug/kg
100 uS/kS
200 ug/kg
200 ug/kg
200 ug/kg
190 ug/kg
86 ugrkg120 ug/kg200 ug/kg
90 ugftg
180 ug/kg
110 ug/kg80 ug/kg
97 ug/kg
2OO ug/kg
150 ug/kg
27 uslkg
120 uglkg
47 ug/kg180 ug,kg
48 ug/kg
310 ug/kg
130 ug/kg56 ug/kg59 ugrkg
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
8260B
8260B
8260B
8260B
82608
82608
8260B
82608
8260B
8260B
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
2400
s90
s90
s90
s90
1 200
590
590
590
590
590
590
590
590
590
590
590
590
590
s90
590
590
s90
590
590
590
590
590
s90
1200
590
590
590
1200
590
590
590
590
590
PQL = Practical quantitation limit B = Dotected in the method blank E = Quantitation of compound excoeded the calibration rango H = Out of holding time
ND = Not detected al orabovethe MDL J = Estimated result< PQLand: MDL P = The RPD between two cC @lumns excoeds 40olo N = Recoveryisoutofcriteila
\iJher6 applicable, all soil samplo analysis are reported on a dry waight basis unless flagged with a "l /'
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 18 of72
L6wl 1 Report v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-007
Description: 555-17-6 Matrix: Solid
Date Sampled:10/1012013 1355 % Solids: 82.2 1011212013 16'12
Date Received: 1011 1 12013
Volatile Organic Compounds by GC/MS
I
I
tRun
1
2
Prep Method
5035
5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 100 1011412013 1812 MC
82608 1000 1011512013 1427 AAC
Batch Sample Wt.(g)31805 5.15
31949 5.15
Parameter
CAS Analytical
Number Mathod Result O I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 ,1 , 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyt chtoride
Xylenes (total)
Surrogate
108-88-3
76-13-',!
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1 330-20-7
Run 1 AcceptanceO % Recovery Limits
200 ug/kg
74 ug/kg
200 ug/kg100 ug/kg
93 ug/kg2200 ugrkg180 ug/kg100 ug/kg
340 ug,kg
82608
8260B
82608
82608
8260B
82608
8260B
8260B
8260B
260 J
ND
ND
ND
ND
r00000
ND
ND
1000
590
590
590
590
590
5900
590
590
590
I
1
1
1
1
2
1
1
1
I
I
IRun 2 AeceptanceO % Recovery Limits
1,2-Dichloroethane-d4
Toluene-d8
91
80
87
53-142
47-138
68-124
108
101
93
53-142
47-138
68-124 I
I
I
I
t
I
I
I
I
PQL = Practical quanlitation limit B = Delectod in the method blank E = Quantitation of compound excegded ihe calibration rangs
ND = Not dotected at or abovs the MDL J = Esilmated result < PQL and: MDL P = The RPD betwo€n two GC columns exceeds 40%
Where applicablo, all soil samplo analtEis ar€ reported on a dry welght basis unless flagged with a 1fl'
H = Out of holding time
N = Recovery is oul of criteria I
Shealy Envimnmental Services, lnc.
l06VantagePointDrive W€stColumbia,SC 29172 (8031791-9700 Fax[phone] www.shealylab.com
Page: 19 of72
Lovsl 1 Reportv2.l I
I
t
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-008
Description: SSS.17-8 Matrix: Solid
Date Sampled:'1011012013'1405 % Solids: 72.4 1011212013 1612
Date Received : 1011 1 12013
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 100 10114t20',t3 1836 AAC
82608 2000 10115120',t3 1450 AAC
Batch Sample Wt.(g)
31805 5.45
31949 5.45
Parameter
cAs
Number
Analytical
Meiho6 Result O MDL Units Run
T
I
I
I
I
I
I
I
I
T
t
T
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 ,'l -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etachloroethan e
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-1 2-8
124-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75.34.3
107-06-2
75-35-4
156-s9.2
I 56-60-5
78-87-5
1 0061 -01-5
1 0061 -02-6
1 00.t1-4
591-78-6
98-82-8
79-20-9
1634-04-4
108.10-1
108-87-2
75-09.2
100-42-5
79-34-5
127-18-4
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
8260B
8260B
8260B
82608
8260B
82608
8260B
82608
82608 110000
82608 ND
82608 ND
82608 190000
850 ug/kg 1
140 ug/kg 1
220 ug/kg 1
89 ug/kg 1
230 uS/kS 1
300 uS/kS 1160 ug/kg 1
230 ug/kg 1
22O ug/kg 1
160 ug/kg 1
110 uS/kS 1
130 ug/kg 1
85 ug/kg 1
190 ug/kg 1220 ug/kg 1
110 uS/kS 1
220 ug/kg 1220 ug/kg 1
220 ug/kg 1
2OO ug/kg 1
93 uglkg 1130 ug/kg 1
22O ug/kg 1
96 uglkg I
190 ug/kg 1
120 ug/kg 1
86 ug/kg 1
100 ug/kg 1
220 ug/kg 1
160 udkS 1
29 ug/kg 1
120 uglkg 1
51 ug/kg 1
190 uglkg 1
52 ug/kg 1
6600 ug/kg 2
140 ug/kg 160 ug/kg 1
1300 ugrkg 2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
450 J
ND
ND
8800
ND
ND
ND
ND
120 J
ND
ND
360 J
ND
2300
ND
2500
630
630
630
630
1 300
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
630
1 300
630
630
630
1300
630
1 3000
630
630
1 3000
PQL = Practical quantitatiofl limit B = Deleclad in lh6 malhod blank E = Quantitation ofcompound exc€€ded the calibration range H = Out ofholding time
ND = Nol detectsd atorabovetho MOL J = Estimated rssult< PQL and: MDL P = The RPD between two GC columns exc€eds 40% N = Recovery is outofcdtaria
Where applicable, all soil sampl€ analysis are report€d on a dry weight basis unloss flagged with a "W"
Shealy Environmental Services, lnc.
I
,* Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
I
Page:20 ot72
Level I Report v2.l
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-008
Description: SSS-17-8 Matrix: Solid
Date Sampled:1011012013 1405 % Solids: 72.4 1011212013 1612
Date Received : 10111 12013
Volatile Organic Compounds by GC/MS
I
I
IBatch
31805
31949
Run
1
2
Prep Method
5035
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 100 ',1011412013 1836 AAC
82608 2000 1011512013 1450 AAC
Sample Wt.(g)
5.45
5.45
Parameter
CAS Analytical
Number ilathod Result O I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
108-88.3
76-1 3-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-O1-4
1330-20-7
Run 1 AcceptanceA % Recovery Limits
Run 2 AcceptanceA % Recovery Limits
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
310 J
ND
ND
ND
ND
r40000
ND
ND
810
630
630
630
630
630
13000
630
630
630
220
80
220
110
100
4800
190
110
370
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 'l
ug/kg 1
uglkg 2
ug/kg 1
ug/kg 1
ugrkg 1
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
90
77
85
53-142
47-138
68-124
119
't'17
106
53-142
47-138
68-124 I
I
I
I
I
I
I
t
I
PQL = Practicalquantitation limit B = Detected in thE mothod blank E = Quantitation of compound excosded the calibration range
ND = Not detected at or above th6 MDL J = Estimated r€sult < PQL and: MDL P = The RPD botwean two GC @lumns exceeds 40%
Where applicable, all soil samplo anal!€is are rsportod on a dry wsight basis unloss nagged with a "W'
H = Out of holding time
N = Recovsry is out of crlteria I
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Pagel.2l ot72
Level 1 Report v2.1 I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-009
Description: SSS-18-4 Matrix: Solid
Date Sampled:1011012013 1425 % Solids: 67.3 1011212013 1612
Date Received : 1011 1 12013
Volatile Orqanic Compounds bv GC/MS
I Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst82608 1 10t14t2013 1551 AAC
Prep Date Batch Sample Wt.(g)31803 5.71
Parameter
cAs
Number
Analytical
Mathar{Result O MDLPOL UnitsI
I
I
I
I
I
I
I
t
I
t
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-I elnchloroeth a ne
Tetrachloroethene
Toluene
67-64-1
7',t-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
't10-82-7
96-12-8
124-48-1
106-93-4
95-50-1
54',1-73-1
106-46-7
75-71-8
75.34-3
107-06-2
75-35-4
1 56.59.2
1 56-60-5
78-87-5
1 0061 -01-5
1 0061 -02-6
100-4't-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
1 08-88-3
68
ND
ND
ND
ND
9.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.98 J
ND
ND
4.1 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg 1
ug/kg 'l
ug/kg 'l
ug/kg 'l
uS/kS 1
uglkg 1
ug/kg 1ug/kg 1
ug/kg 1
uS/kS 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ugrkg I
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uSftS 1
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
8260B
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
8260B
8260B
82608
82608
82608
82608
8260B
26
6.5
6.5
6.5
6.5
13
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
5.5
6.5
6.5
6.5
6.5
6.s
6.5
6.5
6.5
13
6.5
6.5
6.5
13
6.5
6.s
6.5
6.5
6.5
6.5
8.7
1.4
2.2
0.91
2.3
3.1
1.7
2.3
2.2
1.7
1.1
1.3
0.88
2.0
2.2
1.1
2.2
2.2
2.2
2.1
0.95
't.3
2.2
0.99
2.0
1.2
0.88
1.1
2.2
1.7
0.30
't.3
0.52
2.0
0.53
3.4
1.4
0.61
0.65
2.2
PQL = Practical quantitation limit B = Detected in th6 method blank E = Quantitation of compound exce€ded the calibration range H = Oul of holding time
ND = Notdetected at orabove tha MDL J = Estimated rssult< PQL and: MDL P =The RPD betwesn two GC columns sxcseds 40olo
Whore applicable, all soil samplo anal)6is are rsported on a dry w€ight basis unless flagged with a 'W.
N = Rocovary is out of criteria
Shealy Environmental Services, lnc.
I
106 VantaSe Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
I
Page:X2 ol72
Lovsl 1 Report v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005'009
Description: SSS-18-4 Matrix: Solid
Date Sampled:1011012013 1425 % Solids: 67.3 1011212013 1612
Date Received : 1011 1 12013
Volatile Orqanic Gompounds by GC/MS
I
t
IRun
,|
Prep Method
5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 10/1412013 1551 AAC
Batch Sample Wt.(g)31803 5.71
Parameter
CAS Analytica!
Number Method Result O PQL
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
'1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
t
I
I
0.82 ug/kg 1
2.2 ug/kg 1
1.1 ug/kg 1
1.0 ug/kg 1
2.5 ug/kg 1
2.0 ug/kg 'l
1.'l ug/kg 1
3.8 ug/kg 1
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
6.5
6.5
6.5
6.5
6.5
6.5
6.5
6.5
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
89
69
90
53-142
47-138
68-124
I
I
I
I
t
I
I
I
I
I
PQL = Practical quantitation limit B = Detect6d in lhe method blank E = Ouantitation of compound oxcoeded lhe calibration range
ND = Not dstecied at or above th€ MDL J = Estimatsd result < PQL and: MDL P = Tho RPD bEtwesn two GC columng exceeds 40%
Whsro applicable, all soil sample analysis are reporiod on a dry w€ight basis unlass flagged with a 1\l"
H = Out of holding timo
N = Recovery is out of critBria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page:23 ol72
Lsvsl 1 Reportv2.l I
I
t
t
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-010
Description: SSS.19.4 Matrix: Solid
Date Sampled:1011012013'1515 % Solids: 83.7 1011212013 1612
Date Received: 1 011 1 12013
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 50 1011412013 1859 AAC
82608 50 1011512013 1403 AAC
Batch Sample Wt.(g)31805 s.09
31949 s.09
Parameter
cAs
Number
Analytical
Merhod Result O
I
I
t
t
I
I
I
I
I
I
I
I
t
I
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 , 1-Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methy! acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T etnchloroethane
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
12448-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591 -78-6
98-82-8
79-20.9
1 634-04-4
108-10-1
108-87-2
75-09-2
100-42-s
79-34-5
127-18-4
8260B
8260B
82608
82608
82608
82608
8260B
82608
8260B
82608
82608
82608
8260B
8260B
82608
8260B
8260B
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
8260B
8260B
8260B
82608
8260B
82608
82608
ND 1200
ND 290
ND 290
ND 290
ND 290
ND 590
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 29O
ND 290
ND 290
ND 290
ND 290
ND 290
ND 290
ND 590
ND 29O
350 290
ND 29O
93 J 590
ND 29O
ND 290
ND 290
ND 290
44 J 290
390 ug/kg
65 ug/kg
100 ug/kg41 ug/kg
110 uslkg140 ug/kg76 udks110 us/kg100 ug/kg
76 ug/kg49 ug/kg
59 ug/kg
40 uS/kS
88 ug/kg100 ug/kg50 ug/kg
100 uS/kS
100 ug/kg100 ug/kg
94 uS/kS43 ug/kS59 ug/kg100 ug/kg
45 ug/kg88 ug/kg
53 ug/kg40 ug/kg
48 ug/kg100 ug/kg
76 ug/kg
13 ug/kg58 uSftS
23 ug/kg88 ugrkg
24 ug/kg150 ug/kS
65 ug/kS28 ug/kg29 ugftg
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound gxceeded the calibration range H = Out of holding lime
ND=NotdetectedatorabovelhsMDL J=Estimatedresult<PQLand:MDL P=TheRPDbetw8entwoGCcolumnsex@eds40o/o N=Recovsryisoutdcriteria
Where applicable, all soil sample anal)€is are rsported on a dry weight basis unless flagged with a nV"
Shealy Environmental Services, lnc,
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Pagez 21 ol72
Level 1 Repon v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-010
Description: SSS-19-4 Matrix: Solid
Date Sampled:10/10/2013 1515 % Solids: 83.7 1011212013 1612
Date Received : 1011 1 12013
Volatile Orsanic Compounds by GC/MS
I
T
T
Batch
31805
31949
Run
1
2
Prep Method
5035
5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 50 101',14120',t3 1859 AAC
82608 50 10115120',t31403 AAC
Sample Wt.(g)
5.09
5.09
Palameter
cAs
Number
Analytical
Method Result O Unlts I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1 330-20-7
Run I AcceptanceO % Recovery Limlts
Run 2 AcceptanceO % Recovery Limits
82608
82608
82608
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
290 100 ug/kg 1
290 37 ug/kg I290 100 ug/kg 1
290 50 uS/kS 1
290 46 ug/kg 1
290 110 ug/kg 1290 88 ug/kg 1290 50 ug/kg 1
290 170 ug/kg 1
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
97
85
91
53-142
47-138
68-124
97
86
89
53-142
47-138
68-124 I
I
I
I
I
I
I
t
I
PCIL . Practical quantitalion limit B = Detgcled in the method blank E = Quantitation of compound excesdsd the calibration range
ND=Notdstect€datorabovetheMDL J=Estimatsdresult<PQLand:MDL P=TheRPDb€tw€entwoGCcolumnsexceeds40To
wh6r€ applimbl€, all soil sample analysis ar6 reported on a dry weight basis unlss flagged with a nv"
H = Out of holding tlme
N = Recovery is oul of critoria I
Shealy Environmental Services, lnc,
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 25 ot 72
Lovol I Rsportv2.l t
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-011
Description: SSS-20-8 Matrix: Solid
Date Sampled:10/10/2013 1530 % Solids: 77.6 1011212013 1612
Date Received : 1011 1 12013
Volatile Orqanic Compounds by GC/MS
I Run Prep MethodI 5035
2 5035
AnalyticalMethod Dilution82608 1
82608 1
Analysis Date Analyst
10114t20't3 1615 AAC
10t15t2013 1252 AAC
Prep Date Batch Sample Wt.(g)31803 5.59
31 948 5.'t5
MDLIParameter
cAs
Number
AnalyticalMarhart Result O PQL Units Run
I
I
T
I
I
I
I
I
t
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBC P)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
'l ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T etnchloroetha n e
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
s6-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
't07-06-2
75-35-4
1 56-59-2
15660-5
78-87-5
10061-01-5
1 0061 -02-6
1 00-41 -4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
7S-34-5
127-18-4
8260B
82608
82608
82608
82608
82608
8260B
82608
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
8260B
82608
82608
8260B
82608
82608
8260B
82608
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
29
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.1 J
23
5.8
5.8
5.8
5.8
12
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
12
5.8
5.8
6.3
12
5.8
5.8
5.8
5.8
5.8
7.7
1.3
2.0
0.81
2.1
2.8
1.5
2.1
2.0
1.5
0.96
1.2
0.78
1.7
2.0
0.98
2.0
2.0
2.0
1.8
0.84
1.2
2.O
0.88
1.7
1.0
0.78
0.95
2.0
1.5
0.27
1.1
0.50
1.7
0.47
3.0
1.3
0.54
0.58
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1uslks 1
ug/kg 1
ug/kg 1ug/kg 1ug/kg 1
ug/lq 1
ug/kg 1
ug/kg 'l
ug/kg 1
udks 1uS/kS 1
uS/kS 1ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
udkS 1
ug/kg 2
ug/kg 1ug/kg 1
uS/kS 1
ug/kg 1ug/kg 1
ugrkg 1
I PQL = Practical quantitalion limit B = Detected in the method blank E = Quanlitation of compound excoeded the calibration range
ND = Not dstected at or abovo the MDL J = Estimated rosult < PQL and: MDL P = Ths RPD between two GC columns excesds 40%
Whore appli€ble, all soil sample anallrsis ar6 reporled on a dry reight basis unlsss flaggsd with a 'W'
H = Out of holding time
N = Recovery is out ot criteria
Shealy Environm€ntal Services, lnc.
I
106 VantaSe Point Drlve West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Pagez 26 ot 72
Level 1 Report v2.l
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-011
Description: SSS-20-8 Matrix: Solid
Date Sampled:10/10/2013 1530 % Solids: 77,6 1011212013 1612
Date Received : 1Ol1 1 12O13
Volatile Orsanic Compounds by GC/MS
I
T
IBatch
31 803
31948
Run
1
2
Prep Method
5035
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 1011412013 1615 AAC
82608 1 1011512013 1252 MC
Sample Wt.(g)
5.59
5.15
Parametel
CAS AnalyticalNumber Mathad Result O I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surogate
108-88-3
76-13-1
120-82-1
71-55-6
79-00-s
79-01-6
75-69-4
75-01-4
1 330-20-7
Run 1 AcceptanceO % Recovery Llmlts
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
Run 2 AcceptanceO % Recovery Limits
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
2.0
0.73
2.0
0.98
0.91
2.2
1.7
0.9s
3.3
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
I
t
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
91
86
s4
53-142
47-138
68-124
88
79
88
53-142
47-138
68-124 I
I
I
I
I
I
I
I
I
PCIL = Practical quantitation limit B = Dstoctod in the method blank E = Quantltation of compound exceeded the calibration range
ND = Notdetectod atorabovothe MDL J = Estimaled result< PQLand: MDL P =Th3 RPD bstw€on lwo GC columns exceods 40%
Where applicable, all soil sampl8 anal!,sis are reported on a dry weight basis unless flagged with a "w'
H = Out of holding time
N = Rocovsry is out ofcritoria t
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Pagez2T ot72
Level 1 Reportv2.l I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-012
Description: SSS-20-10 Matrix: Solid
Date Sampled:'1011012013 1540 % Solids: 80.5 1011212013 1612
Date Received : 1011 1 12013
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 50 10t14t2013',1922 AAC
Batch Sampte Wt.(g)
31805 4.62
Parameter
cAs
Number
Analytical
Marhod Result O
I
I
I
I
I
I
t
I
I
I
t
I
I
I
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,'l -Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2 -f et achloroeth a ne
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
7s-15-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-1 2-8
124-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
156-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-'t0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
82608
82608
8260B
8260B
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1 300
340
340
340
340
670
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
340
670
340
340
340
670
340
340
340
340
340
340
450
74
110
47
120
160
87
120
110
87
56
67
45
100
110
57
110
110
110
110
49
67
110
5l
100
61
46
55
110
87
15
66
27
100
28
'170
74
32
34
110
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 1
udkS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
POL = haclical quantitation limil B = Detected in the method blank E = Quantitation ofcompound exceedod th€ calibration range H = Out ofholding time
ND = Notdetocted aiorabovethe MDL J = Estimated result< POLand: MDL P = The RPD bstween lwo GC columns exc66ds 40olo N = Recov€ryis outofcritsria
Where applicable, all soil sample analysis are reported on a dry w€ight basis unless flagg€d with a "U/"
Shealy Environmental Servlces, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
Page:28 ot72
Lovol 'l Reottv2.l
Client:Terracon Gonsultants, lnc. Laboratory lD: OJ12005-012
Description: SSS-20-10 Matrix: Solid
Date Sampled:1011012013 1540 % Solids: 80.5 1011212013 1612
Date Received : 1011'l 12013
Volatile Organic Compounds by GC/MS
I
I
IRun
1
Prep Method
5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 50 1011412013 1922 AAC
Batch Sample Wt.(g)31805 4.62
Parameter
cAs
Number
Analytical
Methad Result O Units
1, 1,2-Trichloro- 1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1, 1,'l -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
ug/kg 'l
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
340
340
340
340
340
340
340
340
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
42
110
57
53
130
100
58
190
I
I
t
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
94
85
90
53-142
47-138
68-'124
t
I
I
I
t
I
t
I
I
I
PQL = Praclical quantitation limit B = Detected in the method blank E = Quantitation of compound *ceBded $e calibralion range
ND = Not detected at or abovs the MDL J = Estimated rasull < PCIL and: MDL P = The RPD botween two GC columns excaods 40olo
Where applicablg, all soil sampls analysis ars rsportod on a dry weight basis unl6s flagged with a "W.
H = Out of holding lime
N = Rscovery i6 out of critoria I
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page:29 ol72
Lev6l 1 Report v2.'l t
I
t
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-013
Description: SSS-21- Matrix: Solid
Date Sampled:10/10/2013 1555 % Solids: 73.1 1011212013 1612
Date Received : 1011 1 1201?
Volatile Orqanic Compounds bv GC/MS
Run Prep Method
2 5035
Analytical Method Dilution Analysis Date Analyst
82608 1 1011512013 1340 AAC
Prep Date Batch Sample Wt.(g)
31948 4.91
Parameter
CAS
Number
Analytical
Mathad Result O PQL Units RunMDL
I
I
I
I
T
I
T
t
I
I
28
7.0
7.0
7.O
7.0
14
7.0
7.0
7.0
7.0
7.0
7.0
7.O
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.O
7.0
7.0
7.0
7.0
7.0
7.0
14
7.0
7.O
7.0
14
7.0
7.0
7.0
7.0
7.0
7.0
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,'l -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroothene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2 -T etra chloroethan e
Tetrachloroethene
Toluene
67.6.+1
7',t-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
10,6-93-4
95-50-l
541-73-1
1 06-46-7
75-71-8
75-34-3
1 07-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591 -78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-',t8-4
1 08-88-3
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
8260B
8260B
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
82608
82608
82608
21 J
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9.3 ug/kg
1.5 ug/kg
2.4 ug/kg0.98 ug/kg
2.5 ug/kg
3.3 ug/kg1.8 ug/kg2.5 ug/kg2.4 ug/kg
1.8 ug/kg1.2 ug/kg
1.4 ug/kg
0.94 uglkg2.1 ug/kg
2.4 ug/kg1.2 uSikS2.4 uS/kS
2.4 ug/kS2.4 uglks
2.2 ug/kg
1.0 udkg1.4 uS/kS2.4 ug/kg1.1 uS/kS
2.1 ug/kg
1.3 uS/kS
0.95 ug/kg
1.1 ug/kg
2.4 ug/kg1.8 ug/kS
0.32 ug/kg1.4 ug/kg
0.56 ug/kg2.1 ug/kg
0.57 uS/kS3.6 ug/kg
1.5 ug/kg
0.65 ug/kg0.70 uS/kS
2.4 ug/kg
I
I
I
T
I POL = Pactcal quantitation limit B = Detected in the mothod blank E = Quantitation ofcompound excoeded the calibration range H = Out ofholding time
ND = Not detected at or above the MDL J = Estimated result < PQL and: MDL P = The RPD between two GC columns exceeds 40%
Where applicable, all soil sample analysis are reportod on a dry reight basis unless flagged with a "W"
N = Rocovery is out ofcriteria
Shealy Environmental Services, lnc.
I 106 Vantase Polnt Drive west Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.comI Page: 30 of 72
Level I RsDort v2.t
I
Client:Terracon Consultants, lnc. Laboratory lD: OJ{2005'013
Description: SSS-21- Matrix: Solid
Date Sampled:10/10/2013 1555 % Solids: 73.1 1011212013 1612
Date Received : 1 011 1 12013
Volatile Orqanic Compounds bv GC/MS
t
I
IRun
2
Prep Method
5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 'l 10115120131340 AAC
Batch Sample Wt.(g)31948 4.91
Parameter
CAS Analytical
Number Method Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-1 3-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 2 AcceptanceO % Recovery Limits
t
I
t
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
ug/kg 2
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
7.0
7.0
7.0
7.0
7.0
7.O
7.0
7.0
0.88
2.4
1.2
1.1
2.6
2.1
1.2
4.0
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
I
I
T
I
t
I
t
I
I
I
86
83
88
53-142
47-138
68-124
PCIL = Practical quantitalion limil B = D8l6cted in the method blank E - Ouantitation of compound sxc66dsd tho calibration rang€
ND = Not det6ct6d at or above the MDL J = Esllmatod result < PQL and: MDL P = The RPD betwe€n two GC columns excoods 40%
Where applicable, all soil sample anal),sis are reported on a dry w€ight basis unless flagged wth a nv"
H = Out of holding timB
N = Rocovery is out of criteria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l l www.shealylab.com
Page:31 of72
Level 1 Reportv2.l I
I
I
I
Client:Terracon Gonsultants, Inc. Laboratory lD: OJ12005-014
Description: SSGW-1-16 Matrix: Aqueous
Date Sampled:1 0/10/201 3 1 605
Date Received :'i011 1 12013
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 50308
5030B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch82608 1 1011512013 1342 JHD 3',1928
82608 10 10/18/2013 033'1 PMM2 32220
Parameter
cAs
Number
AnalyticalMarhad Result O MDLPQL Units
I
I
I
T
I
I
I
I
I
I
I
I
I
T
t
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfde
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methy! chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans.l,2.Dichloroethene
1 ,2-Dichloropropane
cis- 1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T elnchloroeth a ne
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75.00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75.34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108.10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
8260B
82608
82608
8260B
8260B
8260B
82608
82608
8260B
8260B
82608
82608
8260B
8260B
82608
8260B
82608
82608
8260B
8260B
8260B
8260B
8260B
82608
8260B
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.6 J
ND
0.33 J
ND
ND
ND
ND
ND
ND
ND
ND
5.5
ND
ND
130
4.0 J
ND
ND
ND
ND
ND
ND
ND
ND
3.7 J
ND
480
ND
ND
ND
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.,00
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
17
0.10
0.40
0.40
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
50
5.0
5.0
5.0
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1ug/L 1
ug/L 1
ug/L 1
ugIL 1
ug/L 1
ugIL 1
ug/L I
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ugIL 1ug/L 1
ug/L 'l
ugIL I
uglL 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L I
ugll 2
ug/L 1ug/L 1
ug/L 1
PQL = Practical quantitation limil B = Detocted in th6 method blank E = Quantitalion of compound exc€eded the calibration range H = Out of holding time
ND = Nol dst€cted at or above the MDL J = Estimated result < PQL and: MDL P = The RPD botw€en two GC columns oxceeds 40%
Where applicabls, all soilsample anal)rsls ars roportsd on a dry w€ight basis unless flagged with a'W'
N = Rocovery is out d criterla
Shealy Environmental Sorvices, lnc.
l06VantagePointDrive WestColumbia, SC 29'172 [phone] Fax[phone] www.shealylab.com
Pagez 32 ol72
Lsvel 1 ReDortv2.'l
Client:Terracon Consultants, lnc. Laboratory lD: OJ12005-014
Description: SSGW-1-16 Matrix: Aqueous
Date Sampled:1 0/1 0/201 3 1 605
Date Received : 10111 12013
Volatile Organic Compounds by GC/MS
t
I
IRun
1
2
Prep Method
50308
50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch82608 1 10t15t2013 1342 JHD 31928
82608 10 ',1011812013 0331 PMM2 32220
Parameter
cAs
Number
Analytical
Mathad Result O MDL I
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
1 08-88-3
76-13-1
120-82-1
71-55-6
79-00-5
79-01.6
75-69-4
75-01 "l
1330-20-7
Run I AcceptanceO % Recovery Lamits
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 320
82608 ND
82608 6.2
82608 ND
Run 2 AcceptanceA % Recovery Limlts
5.0 1.7
5.0 0.30
5.0 1.75.0 0.20
5.0 0.30
s0 3.05.0 0.30
2.0 0.10
5.0 1.7
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ugIL 2ug/L 1
ug/L 1
ug/L 1
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
93
96
92
70-130
70-130
70-130
93
10'l
92
70-1 30
70-130
70-1 30 I
t
I
t
I
I
I
I
I
PCIL = Praciical quantitation limlt B = Delected in the method blank E = Quantilation of compound exceedod the calibration range
ND = Not d8tscted at or above the MDL J = Estimatod result < PQL and: MDL P = Tho RPD betw€€n two GC columns exceeds 40olo
where applicable, all soil samplo analysis are reported on a dry w€ight basis unless flagged with a 'W"
H = Out of holding time
N = Recovsry is out of criteria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wu,w.shealylab.com
Page: 33 of 72
L6vel 1 Reportv2.l I
I
T
I
Client: Terracon Consultants, lnc,
Description: TRIP
Date Sampled:1011012013
Date Received : 1011 1 12013
Laboratory lD: OJ12005-015
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch82608 1 10t14t20132331 TAF 31860
Parameter
cAs
Number
Analytical
Mathod Result O MDL
I
T
I
I
I
t
I
t
I
t
I
t
I
I
I
I
t
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.s0
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
't.7
0.20
0.30
0.30
0.50
o.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-'t,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-7 etachloroethane
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-'15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
54',t-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
10061-0't-s
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
1 08-88-3
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
82608
8260B
8260B
8260B
82608
82608
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
uSlL 1
ug/L 1
ug/L 1
ug/L 1
uS/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L I
ug/L 1
uS/L Iug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound gxceedod the calibration range H = Out of holding lime
ND = Noldetected al oraboveths MDL J = Estimated result< PQLand: MDL P = The RPD batwoen two GC columns oxcsgds 40% N = Rocovsryisoutofcritetia
Whers applicable, all soil samplo analysis are rsported on a dry weighl basis unless flagged with a nV"
Shealy Environmontal Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page:4 ot72
L6vel I Reportv2.l
Client: Terracon Gonsultants, lnc.
Description: TRIP
Date Sampled:1011 012013
Date Received: 1011 1 12013
Laboratory lD: OJ12005-01 5
Matrix: Aqueous
Volatile Orsanic Compounds by GC/MS
T
t
IRun
1
Prep Method
s030B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82608 I 10/1412013 2331 TAF 31860
Parameter
cAs
Number
Analytical
Method Result O PQL MDL I1, 1,2-Trichloro-1,2,2-Trifl uoroethane
'1,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uorometha ne
Vinyl chloride
Xylenes (total)
Surrogate
76-1 3-1
120-82-1
71-55-6
79-00-5
79-01.6
75-69-4
75-01-4
1330-20-7
Run 1 Acceptancea % Recovery Limits
8260B
82608
82608
82608
82608
8260B
8260B
82608
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
0.30
1.7
0.20
0.30
0.30
0.30
0.10
1.7
I
t
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uSlL 1
ug/L 1ug/L 1
'1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
92
90
89
70-130
70-130
70-130
I
I
I
I
I
!
T
I
I
t
PQL = Practical quantitation limit B = D€tscted in the mothod blank E = Quantitation of compound Bxcoeded tho calibration range
ND = Not detectod at or above the MDL J = Estimated r8sult < PQL and: MDL P = The RPD betw€en two GC columns exceeds 400/6
Whore applicable, all soil sample analysis are report€d on a dry w€ight basis unless fagged with a'W.
H = Out of holdins timo
N = Recovery is out of criteria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 35 of 72
Level 'l Reportv2.'l I
I
QG Summary
Shealy Envircnmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'111 www.shealylab.com
Page: 36 of 72
Level 1 Report v2.1
IVolatile Organic Compounds by GC/MS - MB
Sample lD: 9631663-99'1
Batch:31803
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 I
IParameteroDit POL MDL Units Analysis Date
1,2-Dibromo-3-chloropropane(DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 , 1-Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etachloroethane
Tetrachloroethene
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
't0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
1.1
1.7
0.70
1.8
2.4
1.3
1.8
1.7
1.3
0.83
1.0
0.67
1.5
1.7
0.85
1.7
1.7
1.7
1.6
0.73
1.0
1.7
0.76
1.5
0.91
0.68
0.82
1.7
1.3
0.23
0.98
0.40
1.5
0.41
2.6
1.1
o.47
0.50
1.7
0.63
1.7
0.79
0.85
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10t14t20'13't212
1011412013 1212
10114120131212
10114120131212
10114120131212
1011412013 1212
10t14t20131212
10t1412013 1212
1011412013 1212
10t14t20131212
10114120131212
10t14t2013',1212
10114120131212
10114t2013 1212
10114t20'131212
10t't4t20'131212
10114t20131212
1011412013 1212
'10t14t20131212
10t14120131212
10t1412013 1212
10t14t20131212
10t14120't31212
10114120131212
10t14t20131212
10114t20131212
1011412013 1212
1011412013 1212
10t14t2013 1212
1011412013 1212
10t14120131212
10t14t20131212
10t14t20131212
1011412013',l212
10t14t2013't212
10114120131212
1011412013 1212
10t1412013 1212
10t14t2013 1212
10114120131212
'10114120131212
10114120131212
10t14t201312'.t2
1011412013 1212
I
I
I
I
I
I
t
I
I
I
I
I
I
1,1,2-Trichloro-1,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene ND
1, I,2-Trichloroethane
1 , I ,1 -Trichloroethane
ND
ND
PQL = Praclical quantitalion limit
ND = Not detected al or above the MDL
P = Ths RPD botwosn two GC columns exc€sds 40% N = Ro@very is out of criteria
J = Estimated rosult < PQL and i MDL + = RPD is out of critoria I
Iwhere applicable, all soil sample analysis are reportod on a dry \,\€ight basis unl€ss flagged with a "w.
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'111 www.shealylab.com
Page:37 ot72
Lovel 1 Roportv2.1
I
t Volatile Organic Compounds by GC/MS - MB
I
t"l':,:"r,oQ31803-oo1
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I Parameter Result A Dit PQL MDL Units Analysis Date
T
I
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
ND1
AcceptanceO % Rec t_ihtt
ND
ND
ND
5.0 1.9 ug/kg 1011412013 1212
5.0 1.5 ug/kg '1011412013'1212
5.0 0.86 ug/kg 10114120131212
5.0 2.9 ug/kg 1011412013 1212
Bromofluorobenzene
I i;1','",lll"**-"
I
I
t
I
I
I
I
I
I
I
90 47-138
98 53-142
99 68-124
I
I
PQL = Practi€l quantitation limit P = Th6 RPD betwoen two GC columns excseds 40% N = Re@very is out of crit€da
ND = Notdet€cted at orabove th6 MDL J = Estimatod r6sult< PQLand: MDL + = RPD is out ofcriteria
Where applicabls, all soil sample analysis ars roported on a dry wolght basis unless flagged with a nV"
Note: Galculations are performed before rounding to avoid round.off errors in calculated results
Sh6aly Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page: 38 of 72
Lovsl I Roport v2.l
I
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: OQ31803-002
Batch:31803
Analvtical Method: 82608
Matrix: Solid
Prep Method: 5035 I
SpikeAmount Result % Rec IParameter(uE/kq) (uE/ks) O oil % Rec Limit Analysis Date
Acetone 100
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1,2-Dibromo-3-chloropropane(DBCP) 50
Dibromochloromethane 50
1,2-Dibromoethane (EDB) 50
1,3-Dichlorobenzene 50
1,2-Dichlorobenzene 50
l,4-Dichlorobenzene 50
Dichlorodifiuoromethane 50
l,l-Dichloroethane 50
1,2-Dichloroethane 50
1,l-Dichloroethene 50
cis-1,2-Dichloroethene 50
trans-1,2-Dichloroethene 50
1,2-Dichloropropane 50
cis-1,3-Dichloropropene 50
trans-'t,3-Dichloropropene 50
Ethylbenzene 50
2-Hexanone 100
lsopropylbenzene 50
Methyl acetate 50
Methyl tertiary butyl ether (MTBE) 50
4-Methyl-2-pentanone 100
Methylcyclohexane 50
Methylene chloride 50
Styrene 50
1,1,2,2-Tetnchloroethane 50
Tetrachloroethene 50
Toluene 50
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1,2,4-Trichlorobenzene 50
1,1,2-Trichloroethane 50
1,1,1-Trichloroethane 50
'110
40
40
38
46
96
46
42
39
45
41
40
44
47
39
42
38
41
40
45
40
40
43
42
42
39
41
41
40
100
40
44
35
94
44
44
34
42
39
40
43
41
40
43
108
81
8'l
75
91
96
92
84
78
90
82
80
88
93
79
85
76
82
79
90
80
80
87
84
84
79
82
81
80
100
81
87
70
94
87
87
69
83
78
80
87
83
79
86
60-140
69-123
69-121
61-1 19
10-168
57-148
58-122
58-136
59-129
42-163
71-125
34-134
53-139
55-125
66-1 1 I
74-124
51-134
57-13',1
52-133
10-157
71-127
67-129
69-138
70-122
68-1 31
72-124
70-'t26
70-124
59-128
54-137
50-136
59-137
70-1 30
60-1 34
41-'144
70-130
54-136
69-132
45-150
61-129
49-1 36
34-145
55-128
63-128
10t14t20',131038
10t14t2013 1038
10/1412013 1038
1011412013 1038
10t14t20131038
10t14t20131038
10t't4t20131038
10114120't31038
1011412013 1038
10t14t20131038
10t14t2013 1038
10114120131038
1011412013 1038
10114120131038
1011412013'1038
1011412013 1038
10114t20't31038
1011412013 1038
10114t20131038
10t14120131038
10t14t2013 1038
10114t20131038
10t1412013'.t038
10114120131038
10/1412013 1038
10114120131038
10t1412013 1038
10114t20131038
10/1412013 1038
10114120131038
10114t2013',t038
10t14t2013 1038
1011412013 1038
10/1412013 1038
10t14t2013 1038
10114120131038
10t14t20131038
10t14t2013 1038
10/1412013 1038
10114120131038
10114120131038
10114120131038
1011412013 1038
10114t2013 1038
I
I
I
I
I
I
I
I
I
I
t
I
I
PQL = Practical quantitalion llmit
ND = Not deiocted at or abov€ the MDL
P = The RPD between t\,t/o GC columns oxcoeds 40% N = Recovery ls out of criteria
J = Estimatod result < PQL and 2 MDL + = RPD is out of critsria I
IWhere applicable, all soil sample analysis are reported on a dry w€ight basis unless flagged with a '\,V'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Envionmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 39 of 72
Lsvel 1 Report v2.l
I
I Volatile Organic Compounds by GC/MS'LCS
I Sample lD: oQ318o3-oo2
I Batcn:31803
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I ^tJI"", Resurt % Recr Parameter (ug/kg) (ug/kg) A Dit % Rec Limit Analysis Date
Trichloroethene
f Trichlorofluoromethane
I Vinyt chtoride
Xylenes (total)
50 41
50 47
50 44
100 78
AcceptanceO % Rec Lihit
1 82 62-126 1011412013 1038
1 93 4s-138 1011412013 1038
1 88 42-132 1011412013 1038
1 78 58-128 10114120131038
I Surrosate
Bromofluorobenzene 107 47-138
I ii;:::lr"**"- ::: z::;1
I
I
I
T
I
I
I
I
I
t
I
I
PQL = Practical quantitation limit P = Tha RPD betwo€n two GC columns exceeds 40% N = Recovsry is out of criteria
ND = Notdetectedatorabovethe MDL J = Estimated result< PQLand? MDL + = RPDisoutofcriteria
Where applicable, all soil sample analysis are reporled on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:40 ol72
L6vol I Reportv2.l
I
IVolatile Organic Compounds by GC/MS - LCSD
Sample lD: OQ31803-003
Batch:31803
Analvtical Method: 82608
Matrix: Solid
Prep Method: 5035 I
Spike
Amount
(uslks)
Result(ug/kg) O
% Rec % RPD
Dil % Rec % RPD Limit Limit Analysis Date IParameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1,2-Dibromo-3-chloropropane(DBCP) 50
Dibromochloromethane 50
1,2-Dibromoethane (EDB) 50
100
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
99
40
39
37
43
91
45
41
40
41
41
40
42
45
40
43
38
40
40
45
40
40
44
42
41
39
41
43
41
99
41
42
34
90
42
43
36
40
41
40
42
40
40
43
99
80
79
74
86
91
89
82
80
82
81
80
84
91
80
86
76
80
80
89
81
80
88
83
83
78
82
86
82
99
82
84
68
90
85
85
73
81
82
80
85
80
80
87
8.9 60-140 20 ',t011412013 1101
0.99 69-123 20 10114120131101
2.2 69-121 20 10t14t20131101
1.9 61-119 20 10114120131',t01
5.2 10-168 20 10114120131101
5.2 57-148 20 10114t20131101
2.8 58-122 20 10t14t201311012.9 58-136 20 10114t2013110',1
2.2 59-129 20 10114t2013 1101
9.1 42-163 20 10114t20131101
1.3 71-12s 20 10114120131101
0.22 34-134 20 10t14t20131101
4.0 53-139 20 10114t20131101
2.8 55-125 20 10114120131101
2.O 66-119 20 1011412013',t1011.1 74-124 20 10t14t20131101
0.18 51-134 20 '.10t14t2013',t101
1.6 57-131 20 ',t0t14t20',131101't.0 52-133 20 10t14t20131101
0.29 10-157 20 10t14120131101
0.48 71-'.t27 20 10114120131101
0.44 67-129 20 10t14t20131101
0.93 69-138 20 10114t20',t3',t101o.41 70-122 20 10114120131101
1 .0 68-131 20 10t14t2013 1101
1.3 72-124 20 10t14120131101
0.44 70-126 20 1011412013 1101
5.5 70-124 20 10t14120'.131101
2.8 59-128 20 10114120131101
0.49 54-137 20 10t14120131101
1.9 50-136 20 10t14t20'.t3 1101
3.8 59-137 20 101141201311011.8 70-130 20 10114120131101
3.9 60-134 20 1011412013110',12.9 41-144 20 10t14t20131101
2.1 70-130 20 10114t20131101
6.1 54-136 20 10t14120131101
3.2 69-132 20 1011412013 11014.9 4s-150 20 101141201311010.29 61-129 20 10114120131101
2.s 49-136 20 10114t20131101
2.8 34-145 20 10t14t20131101
1.6 55-128 20 10114t20131101
0.56 63-128 20 10t14t20',t31101
I
I
I
I
I
I
I
t
I
I
I
I
I
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane 50
1.2.4-Trichlorobenzene 50
'1,1,2-Trichloroethane
1.1. 1 -Trichloroethane
50
50
PQL = Practical quantitation limit
ND = No( detocted at or above the MDL
P = The RPD betwBn two GC columns sxcseds 40% N = Recovery ls out of critoria
J = Estimatod result < PQL and: MDL + = RPD is out of criteria I
Iwhere applicable, all soil sample analysis aro roported on a dry w€ight basis unl6s flagg€d with a "w"
Note: Calculations are performed before rounding to avoid round-off errors ln calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page:11 ot72
L6vel 1 Roport v2. l
I
I Volatile Organic Compounds by GC/MS - LCSD
I t"'l':':?:oQ31803-oo3
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I ^t#n, Resurt % Rec % RPDr Parameter (ug/kg) (ug/kg) A Dil % Rec % RPD Limit Limit Analysis Date
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
t
I
50 41
50 46
50 44
100 81
AcceptanceO % Rec Lihit
1 82 0.95 62-126 20 10t1412013 1101
1 91 2.3 45-138 20 ',t0t14t2013 1',t01
1 88 0.33 42]t32 20 10t1412013 1101
1 81 4.0 58-128 20 10114120131101
Bromofluorobenzene 94 47-138
t i;1;?flllX"**"' fi Z:::1
I
I
t
I
I
I
I
I
I
I
I
t
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Notdotected atoraboveth6 MDL J = Estimated result< PQLand: MDL + = RPD is out otcriteria
Where applicabls, all soil sample analysis are reported on a dry wsight basis unloss flagged with a nV"
Note: Calculations are performed before rounding to avoid round.off errors in calculated results
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
?age:12 ol72
Levol 1 Reportv2.l
I
IVolatile Organic Compounds by GC/MS - MB
Sample lD: 6q31695-991
Batch:31805
Analvtica! Method: 82608
Matrix: Solid
Prep Method: 5035 I
IParameteroDit POL MDL Units Analysis Date
1,2-Dibromo-3-chloropropane(DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butranone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2 -T elr achloroethan e
Tetrachloroethene
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1 000
250
250
250
250
500
250
340
55
85
35
90
120
65
90
85
65
42
50
34
75
85
43
85
85
85
80
50
37
75
38
8s
46
41
34
85
65
'12
49
20
75
21
130
55
I
I
I
I
I
I
I
I
I
I
I
I
t
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uS/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
24
25
85
32
85
40
43
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
500
250
250
250
500
250
250
250
250
250
250
250
250
250
250
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
10t1412013',t244
1011412013 1244
10t14120131244
10t14t2013 1244
10t14t20131244
1011412013 1244
1011412013 1244
10114120131244
10t14120131244
10t't4120131244
10t14t20131244
1011412013 1244
10t14t20131244
1011412013 1244
10114120131244
1011412013 1244
10t14t20131244
10t14t20131244
101't4t20131244
10t14t20131244
10114120131244
10114120131244
10t't4t20131244
10114t20131244
10t14t20131244
10114t20'.t31244
10t14t20131244
10t'14t20131244
10114120131244
10114120131244
10114120131244
10114t20131244
1011412013',t244
10114t2013 1244
10t14t2013 1244
10t14t20131244
10114120131244
1011412013 1244
1011412013 1244
10114120131244
1011412013 1244
1011412013 1244
10t14120131244
10114120131244
1,1,2-Trichloro-1,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1,1 -Trichloroethane
ND
ND
ND
PQL = Practicalquantitation limit
ND = Not detectod at or above the MDL
P = The RPD balweon two GC columns exceeds 400/6 N = Recovery is out of critoria
J = Estimated rosult < PCIL and: MDL + = RPD is out of criteria I
IWhere applicable, all soil sample analysis are reporlod on a dry w€ight basis unless flagged with a nV"
Note: Galculations are performed before rounding to avoid round-off erors in calculated results
Shealy Environm€ntal Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Pagc:43 o172
Levol I R@orl v2.1
I
I Volatile Organic Gompounds by GC/MS - MB
I sampre rD: oe318os-oo1
I Batch:3'r805
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I Parameter Result A Dil PQL MDL Units Analysis Date
Trichloroethene
I Trichlorofluoromethane
I Vinyl chloride
Xylenes (total)
ND
ND
ND
ND
50 250 95 ug/kg 1011412013 1244
50 2s0 75 ug/kg 10114120131244
50 250 43 ug/kg 10114120131244
50 250 150 ug/kg 10114120131244
I surrosate AcceptanceO % Rec Liinit
Bromofluorobenzene 105 47-138
I l;1,"#11""**"' ;l: ::::1
I
t
I
t
I
I
I
I
I
I
I
I
PQL = Practical quantitation limit P = Th3 RPD between two GC columns exceeds 40% N = Rscovery is out of criteria
ND = Not detectod at orabove the MDL J = Estimated result< PQL and: MDL + = RPD is oui ofcriteria
Where applicable, all soil sample analysis are roported on a dry weight basis unless flagged with a 'W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Pagez 4 ot72
Level I Report v2.1
t
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: OQ31805-002
Batch:31805
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 I
Spike
Amount
(us/kg)
Result
(ug/kg)
% Rec
Dil % Rec Limit Analysis Date tParametero
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-'l etrachloroeth an e
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1 ,1 , 1 -Trichloroethane
5000
2500
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2s00
2500
2500
2500
2500
2500
2500
2500
2500
5000
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
5500
2500
2s00
2100
790
5200
2500
2500
2500
2900
2400
1800
2600
2300
2400
2600
2400
2400
2500
1600
2500
2400
2s00
2500
2600
2500
2600
2600
2500
5000
2600
2700
2500
s000
2600
2500
2300
2400
2400
2500
2600
2400
2500
2500
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
109
101
99
84
32
105
102
98
100
116
97
74
103
92
95
103
96
95
99
64
99
97
99
100
106
101
103
105
100
99
103
107
101
99
105
99
91
96
98
101
102
97
102
100
60-140
69-123
69-121
61-l 1 I
1 0-168
57-148
58-122
58-1 36
59-129
42-163
71-125
34-134
53-139
55-'125
66-1 1 I
74-124
52-133
51-134
57-131
1 0-1 57
67-129
71-127
68-1 31
70-122
69-138
72-124
70-124
70-126
59-128
54-137
50-1 36
59-137
70-130
60-134
41-144
70-130
54-136
69-132
45-1 50
61-129
49-136
34-145
55-128
63-128
1011412013 1307
10t14t2013 1307
10114t20131307
'10t14t20131307
10114120'.131307
10t14t2013 1307
10t14t20131307
10t14t20131307
1011412013 1307
10t1412013',t307
10t1412013 1307
'10114120131307
10114120131307
10t14t20131307
101'1412013 1307
1011412013 1307
1011412013 1307
10t14t2013'.t307
10t1412013 1307
'10114t20131307
10114t2013 1307
10t14t20131307
1011412013 1307
10t14120131307
1011412013 1307
10t1412013 1307
10114120't31307
10t14t2013 1307
1011412013 1307
1011412013 1307
10t14t2013 1307
1011412013 1307
10t1412013 1307
1011412013',!307
1011412013 1307
1011412013 1307
10114t20131307
10t14t2013 1307
1011412013 1307
1011412013 1307
1011412013 1307
10t1412013 1307
1011412013 1307
1011412013 1307
I
I
I
I
I
I
I
I
I
t
I
t
I
PQL = Practical quantitation limit
NO = Not detscted at or above the MDL
P = Ths RPD b6twe6n trc GC columns excesds 40% N = Recovery is out of critoria
J = Estimatod rsult < PQL and : MDL r = RPD is out of critoria I
IWhsre applicable, all soil samplo anal)6is are reported on a dry weight basis unless flagged with a'Vy'
Note: Calculations are performed before roundlng to avoid round-ofr errors in calculated results
Shealy Envircnmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone]'111 www.shealylab.com
Page: tf5 of 72
Level I Roportv2.l
I
I Volatile Organic Compounds by GC/MS - LCS
I Sample lD: Oe318O5-002
I Batcn:31'os
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I ^tJ:|,"", Resurt % Rec
- Parameter (uq/kq) (uq/kq) O Dit % Rec Limit Analysis Date
t ii:1l:frl[:H*"""
Xylenes (total)
2500 2600
2500 2700
2500 2200
5000 5000
AcceptanceO % Rec Liinit
50 102 62-126 10114120131307
50 1 10 45-138 10114120',t3 1307
50 88 42-132 101',14120131307
50 101 58-128 1011412013 1307
I surrosate
Bromofluorobenzene 102 47-138
I li;::]il"**"' H ::::1
I
I
I
I
I
I
I
I
T
t
t
I
PQL = Praclical quantilation limit P = The RPD betwoen two GC columns exce€ds 40% N = Recovery is out ot criteria
ND = Notdotectod atorabovetho MDL J = Estimsted result< PQLand: MDL + = RPD is outofcriteria
Where applicabls, all soil sampla analysis are reporled on a dry woight basis unless flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 46 of 72
L6vel I Repott v2.1
t
IVolatile Organic Compounds by GC/MS - LCSD
Sample lD: Oe31805-003
Batch:31805
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 I
Spike
Amount
(ug/kg)
Result(ug/ks) O
% Rec % RPD
Dil % Rec % RPD Limit Limit Analysis Date IParametel
1,2-Dibromo-3-chloropropane(DBCP) 2500
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 , 1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,'l -Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styr6ne
1, 1,2,2 -T etrachlo roeth a n e
Tetrachloro€thene
Toluene
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1, 1-Trichloroethane
5000
2500
2500
2500
2500
5000
2500
2500
2500
2500
2500
2s00
2500
2500
2500
2500
2500
2500
2500
2500
2500
2s00
2500
2500
2500
2500
2500
2500
5000
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
6200
2500
2400
2100
490
5300
2600
2600
2400
1600
2600
'r800
2600
2300
2300
2500
2400
2400
2500
1600
2500
2600
2700
2600
2800
2500
2600
2600
2500
5000
2600
2800
2600
5200
2700
2600
2200
2300
2500
2500
2700
2400
2400
2600
50 124
50 100
50 98
50 83
50 20
50 107
50 10s50 103
50 97
50 63
50 103
50 73
50 106
50 93
50 9250 101
50 96
50 95
50 10150 64
s0 10050 102
50 107
50 104
50 111
50 100
50 102
50 10350 99
50 101
50 't02
50 111
50 104
50 103
50 107
50 105
50 86
50 94
50 9950 99
50 110
50 95
50 9650 't 05
12 60-140 20 1011412013 1330
0.81 69-123 20 10t1412013 1330
1.'t 69-121 20 10t14t2013 13301.2 61-119 20 10t14120131330
47 10-168 20 10t14120131330
2.1 57-148 20 10114t20131330
3.3 58-122 20 10114t201313304.5 58-136 20 10114t20131330
3.1 59-129 20 10t14t20131330
59 42-163 20 10114t20131330
5.1 71-125 20 10114t20131330
1.7 34-134 20 10/1412013 1330
3.0 s3-139 20 10t14t20131330
1.0 55-125 20 101',1#20131330
3.8 66-119 20 10114t201313301.3 74-124 20 10t14120131330
0.31 52-133 20 10114120131330
0.0066 51-134 20 10114120131330
1.4 57-131 20 10t14t20131330
0.17 10-1s7 20 '.t0114120131330
1.2 67-129 20 10114t2013 1330
5.7 71-127 20 10114t2013 13307.4 68-131 20 10t14t201313304.2 70-122 20 10t14120131330
s.0 69-138 20 10114t20131330
0.97 72-124 20 10114120',131330
0.96 70-124 20 10114t20131330
1.5 70-126 20 10t14120131330't.0 59-128 20 10114t20131330
1.4 54-137 20 10t1412013',t330
0.52 50-136 20 10114120'.t31330
4.1 59-137 20 10t14t20131330
3.3 70-130 20 10/t4t20131330
4.0 60-134 2A 10/14/2013 13i!01.0 41-144 20 10t14t20131330
5.9 70-130 20 10114t20131330
5.8 54-136 20 10rt4t20131330
2.0 69-132 20 1011412013 13301.2 45-150 20 10rt4t201313301.8 61-129 20 ',t011412013 1330
7.2 49-136 20 ',10114120131330
1_4 34-145 20 10/14/2013 1330
6.2 s5-128 20 10t14t201313304.9 63-128 20 1011412013 1330
I
I
I
I
I
I
I
t
I
I
I
I
I
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 2500
2500
2500
2500
PQL = Practical quantitation limit
NO = Not detected al tr abovg th6 MDL
P = Tho RPD betwe€n two GC columns exceods /too/o N = Rscovsry is out of criteria
J = Estimatod rasult < PQL and : MDL + = RPD is out of criteria t
t
Where applicable, all soil sampl€ analysis are roported on a dry woight basis unl6s flagged with a 1rJ"
Note: Calculations are performed before rounding to avoid round-ofr errors in calculated results
Sh€aly Environmental Services, lnc.
106 Vantage Point Drive west Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:17 ol72
Lsvol'l Roportv2.1
I
T Volatile Organic Compounds by GC/MS - LCSD
I t"'r':,:?,oo31'o5-oo3
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I ^tJI"", Resurt % Rec % RPD
- Parameter (ug/kg) (ug/kg) O Dil % Rec % RPD Limit Limit Analysis Date
Trichloroethene
Trichlorofl u oromethane
Vinyl chloride
Xylenes (total)
Surrogate
I
I
2500 2600 50 102 0.23 62-126 20 1011412013 1330
2500 3000 50 't20 8.5 45-138 20 1011412013 1330
2500 2200 50 88 0.46 42-132 20 10114120'.13 1330
5000 4800 50 97 3.9 58-128 20 10114120131330
AcceptanceA % Rec lihit
Bromofluorobenzene
I ii:::ff"**"'
t
I
I
t
I
I
I
I
t
I
100 47-138
106 53]142
102 68-124
I
t
PQL = Practical quantitation limit P = The RPD belwoen two GC columns exceeds 40olo N = Rscovery is out of critsria
ND = Not dotected ai or abovo the MDL J = Estimated result < PQL and: MDL + = RPD is out of critsria
Whore applicable, all soil sample analysis are roportsd on a dry weight basis unless flagg€d with a '\&'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page:4/8o172
l"6vel 1 Roport v2.'l
I
IVolatile Organic Compounds by GC/MS - MB
Sample !D: OQ31860-001
Batch:31860
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Parameter IaDit PQL MDL Units Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane(DBCP) ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
s.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
't.7
1.7
1.7
0.20
0.30
0.30
0.40
0.20
0.50
0.30
0.30
0.30
1.1
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1_7
0.20
0.30
I
I
I
I
I
I
I
I
I
I
I
I
T
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10t14t20132308
't0t14120132308
't0t14120132308
10t14t20132308
10t14t20132308
10114t20132308
10114120132308
10t14t20132308
10t14120132308
't0t14120132308
10t14120132308
10114t20132308
10114120132308
10114120132308
10114120132308
10t14t20132308
10114120132308
10t14t20132308
10t14t20132308
10t14t20132308
10t14t20132308
10114t20132308
10114120132308
10t14t20132308
10t14t20132308
10114t20'.t32308
10t14t20132308
10114120132308
10114t20132308
10114120132308
10t14t20132308
10114120132308
10114120132308
10114t20132308
10114t20132308
10114120132308
10114120132308
10t14t20132308
10114120132308
10t14120132308
't0t14t20132308
10/1412013 2308
10114t20132308
't0t14t20132308
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
trans- 1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T etrachl oroeth an e
Tetrachloroethene
Toluene
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1, 1,2-Trichloroethane
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
1
1
1
PQL = Practical quantitation limit
ND = Not detgcted ai or above tho MDL
P = The RPD betw€en two GC columns o(ceeds 40% N = Recovery is oul of criteria
J = Estimatod result < PQL and ? MDL + = RPD is out of crileda I
IWhere applicable, all soil samplo anal!6is are roported on a dry w€ight basis unless flaggod with a "W.
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmential Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Pagez 19 ot72
Lovel 1 Report v2.t
I
I Volatile Organic Compounds by GC/MS - MB
t t"*:,:?,oe31860-001
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I Parameter Result O Dil PQL MDL Units Analysis Date
Trichloroethenet l;I'r,1ff:"'"""'"
Xylenes (total)
ND
ND
ND
5.0 0.30 ug/L 1011412013 2308
5.0 0.30 ug/L 1011412013 2308
2.0 0.10 ug/L 10114120132308
5.0 1.7 ug/L '10114120132308
I Surrogate
ND1
AcceptanceO % Rec tih:t
Bromofluorobenzene
I i;1;'#11""**"'
I
I
t
T
I
T
I
I
I
I
92 70-130
94 70-130
89 70-130
I
I
PQL = Prac-tical quanttation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Notdeleclod atorabovs the MDL J = Estimated result < PQL and: MDL + = RPD is out ofcriteria
Whers applicable, all soil samplo analysis are roportod on a dry weight basis unless flagged with a "w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environm€ntial Services, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page: 50 of 72
Lowl l Roportv2.'l
I
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: OQ31860-002
Batch:31860
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Spike
Amount
(us/L)
Result(us/L)% Rec
% Rec
Limit tParametelDiloAnalysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1,2-Dichloroethane
trans- 1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T elr achloroeth a n e
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
100
50
50
50
50
100
50
50
50
50
50
50
50
s0
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
50
50
50
50
100
52
53
42
57
96
55
53
52
53
54
49
53
48
53
54
52
53
53
55
53
53
53
54
53
53
54
47
51
100
55
53
57
110
53
52
52
52
53
51
53
47
53
53
104
't04
105
84
113
96
111
107
105
105
108
99
106
97
107
107
104
107
105
1't0
107
107
106
107
106
105
107
95
103
103
109
107
113
107
106
't04
103
104
107
't02
106
94
105
105
60-140
70-130
70-130
70-130
60-140
60-140
60-140
70-130
7C,130
42-163
70-1 30
60-140
70-1 30
70-1 30
70-1 30
70-1 30
70-1 30
70-1 30
70-130
60-140
70-1 30
70-'t 30
70-1 30
70-1 30
70-130
70-130
70-130
70-130
70-130
60-140
70-130
70-130
70-130
60-140
70-130
70-130
70-130
70-130
70-130
70-130
70-1 30
70-1 30
70-1 30
70-1 30
10t14t20132134
10114120't32134
10114120132134
10t14t20132134
10114120132134
10114120132134
10t14t20132134
10t14t20132134
10t14120132134
't0t14t20132134
10t14120132134
10114120132134
10114t20132134
10114t20'132134
10t14t20132134
10t14t20't32134
10t14t20132',t34
10t14t20132134
10114120132134
10114t20132134
't0t14t20't32134
10114t20132134
10114120132134
10114t20132134
10114120132134
10114t20',t32134
10114120132134
10114120132134
10114t20132134
10114t20132134
10114120132134
10114t20132134
10114t20132134
10114t20132134
10114120132134
10t14t20132134
10114120132134
10t14120132134
10t14t20132134
10114t20132134
10t14t20132134
10t't4t20132134
10t14t20132'.134
10114t20132134
I
I
I
I
I
I
I
I
I
t
I
I
I
PQL = Practical quantitation limit
ND = Not det6cted at or above the MDL
P = The RPD bstwe€n two GC columns exceeds 40olo N = Recovery is out of critsria
J = Estimated result < PQL and: MDL + = RPD is out of criteria I
I
Where applicable, all soil sampls analysls ar6 reported on a dry w€ight basis unless flagged with a nV'
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page:51 of72
Lovol I Roportv2.'l
I
I Volatile Organic Compounds by GC/MS - LCS
I Sample lD: oe3186o-oo2
I Batcn:31860
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^tJ11"", Resurt % Rec
' Parameter (ug/L) (ug/L) O Dil % Rec Limit Analysis Date
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
1
1
1
1
T
I
50 54
50 53
50 56
100 1 10
AcceptanceA % Rec Liinit
107 70-130 10t14t20132134
106 70-130 10114120132134
112 70-130 10t14120132134
105 70-130 10t'.t412013 2134
Bromofluorobenzene
I l;1,'#ll'"**"'
I
I
T
I
I
I
t
I
t
I
90 70-130
100 70-'t 30
92 70-130
I
I
PQL = Practiml quantitation limil P = Th6 RPD b€twsen two GC columns ex@eds 40% N = Recovory is out of critsria
ND = Notdetoctod atorabovathe MDL J = Estimated result< PQL and i MDL + = RPD is out otcriteria
Where applicable, all soil samplo analysis are r6ported on a dry wsight basis unless flagged wilh a nV'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Driv6 West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:52 ol72
Lev6l 1 Roport v2.'l
I
IVolatile Organic Gompounds by GC/MS - LCSD
Sample lD: Oe31860-003
Batch:31860
Analvtica! Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
SpikeAmount Result % Rec % RPD(ug/L) (ug/L) O Dit % Rec % RPD Limit Limit Analysis Date IParametel
1,2-Dibromo-3-chloropropane(DBCP) 50
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloro€thane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
'l ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T etrachloroetha ne
Tetrachloroethen6
Toluene
100
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
100
52
52
45
54
110
55
53
52
53
53
49
53
46
54
55
51
53
52
53
53
53
52
54
53
52
54
48
52
110
54
54
56
110
52
52
52
52
54
52
53
46
53
52
103
104
105
90
't08
107
111
107
105
105
106
98
106
93
107
109
103
106
't04
106
107
106
105
107
105
104
108
96
'104
107
109
108
113
110
105
104
104
104
108
103
107
91
107
105
I
I
I
I
I
I
I
I
I
I
I
I
t
50
50
50
1.6 60-140 20 10114120132157
0.35 70-130 20 10114120132157
0.22 70-130 20 10114120132157
6.5 70-130 20 10114120132157
4.6 60-140 20 10114120132157
11 60-140 20 10t14120132157
0.14 60-140 20 10114t20132157
0.0075 70-130 20 10114120132157
0.090 70-130 20 10114t20132157
0.027 42-163 20 10114120',t32157
2.0 70-130 20 10114120132157
0.93 60-140 20 10t14t20132157
0.44 70-130 20 10t14120132157
4.3 70-130 20 10t14t20132157
0.28 70-130 20 101141201321572.1 70-130 20 10t14t20132157
1.4 70-130 20 10114t20132157
0.11 70-130 20 10t'.14t2013 2157
1.4 70-130 20 10114120132157
3.1 60-140 20 10114120132157
0.36 70-130 20 10114120132157
1.3 70-130 20 10114120132157
0.75 70-130 20 101141201321570.17 70-130 20 10114120132',t57
0.36 70-130 20 10t14t20132157
0.70 70-130 20 10114t20132157
0.95 70-130 20 10t14120',t32157
1.1 70-130 20 10114t20132157
1.4 70-130 20 10114120132157
3.9 60-140 20 10114120'.t32157
0.56 70-130 20 10114120132157
0.75 70-130 20 10t14t20132157
0.21 70-130 20 10114120132157
2.8 60-140 20 10114120132157
1.4 70-130 20 1011412013 2157
0.31 70-130 20 10114120132157
1.2 70-130 20 10114t2A82157
0.83 70-130 20 10114120132157
1 .1 70-130 20 10114t2013 21571.8 70-130 20 10114t20132157
0.64 70-130 20 10t14t20132157
2.9 70-130 20 10t14t20132157
1.3 70-130 20 10114120132157
0.42 70-130 20 10t'.14t20132157
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
'1,2,4-Trichlorobenzene
'1,1,1 -Trichloroethane
'1,1,2-Trichloroethane
PQL = Practicslquantitation limit
ND = Not det€cted at or above the MOL
P = Ths RPD between two GC columns exceeds 40% N = Recovory is out of criteria
J = Estimated result < PQL and: MDL + = RPD is out of criteda I
I
Where applicable, all soil sample analysis are repoded on a dry w€ight basis unless flaggsd with s 'W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone]'l www.shealylab.com
Page: 53 of 72
Lovsl 1 Report v2.1
I
t Volatile Organic Compounds by GC/MS - LCSD
I Sample lD: OQ31B6O-OO3
I Batcn:31E60
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^t#t,i, Resurt % Rec % RPD
- Parameter (ug/L) (us/L) O Dil % Rec % RPD Limit Limit Analysis Date
TrichloroetheneI l;T':1",1il:""*'n"""
Xylenes (total)
50 52
50 5350 55
100 100
AcceptanceO % Rec Lihtt
1 104 3.1 70-130 20 10114120132157
1 106 0.48 70-130 20 10114120132157
1 110 2.0 70-130 20 1011412013 2157
1 105 0.54 70-130 20 10114120132157
I Surrogate
Bromofluorobenzene
I l;1;?,"illl""*"'
I
I
t
I
I
t
I
I
I
I
92 70-130
98 70-130
92 70-130
I
I
PQL = Practical quantitation limit P = The RPD belweon two GC columns excseds 40% N = Recovory is out of criteria
NO = Not detected at or above tho MDL J = Estimated rosult < PQL and: MDL + = RPD is out of critoria
Whore applicable, all soil sample analysis arB reporled on a dry welght basis unless llagged with a "W'
Noter Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmsntal Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Pagez il ol72
Lov6l 1 Rsportv2.l
I
IVolatile Organic Compounds by GC/MS - MB
Sample lD: OQ31928-001
Batch:31928
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 t
Parametel IoDit PQL MDL Units Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
'1,2-Dibromo-3-chloropropane(DBCP) ND
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1,4-Dichlorobenzene
1 ,3-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 , 1-Dichloroethane
1 , 1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-'1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Styrene
1,1,2,2-T etrachloroeth ane
Tetrachloroethene
Toluene
'1,1,2-Trichloro-1,2,2-Trifluoroethane ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.40
0.20
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
0.30
I
I
I
I
I
I
I
I
T
I
I
I
I
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uS/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugll
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10t15t2013 1020
10t'15t20131020
10t1512013 1020
10/15/2013 1020
10t1512013 1020
1011st20131020
10t1512013 1020
10t15t2013 1020
10/1512013 1020
10t15t2013 1020
10t15t2013 1020
10115t20131020
10t15t2013 1020
10115t20131020
10t15t20131020
'10t15t20131020
10115t2013 1020
10115t2013 1020
10115t2013 1020
10/15/2013 1020
10t15t20131020
1011st20131020
10t',ts120131020
10t15t2013 1020
10/15/2013 1020
10t't5t20131020
't0t15t20131020
1011512013 1020
10115t2013 1020
10t1512013 1020
10115t2013 1020
10t'15t20131020
10t'15t20131020
10115t20131020
10t15t20131020
10115t20131020
10115t2013 1020
10t1512013 1020
10t15t2013 1020
10115t2013 1020
10/15/2013 1020
10115t2013 1020
101'15120131020
10t1512013',t020
ND
ND
ND
ND
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichlorofl uoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PQL = Practical quantitation limit
ND = Not detacted at or above the MDL
P = Th6 RPD betw€en two GC columns excaeds 40olo N = Rscovery is out of criteria
J = Estimated resull < PQL and : MDL + = RPO is out of crltsria I
IWh6r6 applicable, all soil sample analysis are reported on a dry weight basis unless flaggod with a 'vl/.
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Environmental Servic€s, lnc.
106 Vantage Point Drive west Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 55 of 72
Level 1 Report v2.l
I
I Volatile Organic Compounds by GC/MS - MB
I Sample lD: oe31928-oo1
I Batch:31928
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I Parameter Result O Dil POL MDL Units Analysis Date
t:i,'#,2.0 0.10 us/L 10115120131020
s.0 1.7 ug/L 1011512013 1020ND 'I
AcceptanceO % Rec Lihit
I ;:ti;t:::,ilil:, :i ll.lll
Toluene-d8 91 70-130
I
I
t
t
T
I
t
I
I
t
I
t
T
PQL = Praciical quantitation limit P = The RPD botwsen two GC columns oxcseds 40% N = Recovgry is out of criteria
ND = Not det€cted at or abovo the MOL J = Estimated result < PQL and: MDL + = RPD is out of critsia
Whsr6 appliebla, all soil sample analysis are reporled on a dry reight basis unless flagged with a 'W"
Note: Calculations are performed before rounding to avoid round.off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone]'l www.shealylab.com
Page:56of72
Lev€l 1 Roport v2.1
I
tVolatile Organic Compounds by GC/MS - LCS
Sample lD: 9q31926-992
Batch:31928
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Spike
Amount
(ug/L)
Result
(ug/L)
% Rec
Dil % Rec Limit Analysis Date IPatametera
Acetone 100
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1,2-Dibromo-3-chloropropane(DBCP) 50
Dibromochloromethane 50
1,2-Dibromoethane (EDB) 50
1,2-Dichlorobenzene 50
1,4-Dichlorobenzene 50
1,3-Dichlorobenzene 50
Dichlorodifluoromethane 50
1,2-Dichloroethane 50
1,1-Dichloroethane 50
1,1-Dichloroethene 50
trans-1,2-Dichloroethene 50
cis-1,2-Dichloroethene 50
l,2-Dichloropropane 50
cis-1,3-Dichloropropene 50
trans-1,3-Dichloropropene 50
Ethylbenzene 50
2-Hexanone 100
lsopropylbenzene 50
Methyl acetate 50
Methyl tertiary butyl ether (MTBE) 50
4-Methyl-2-pentanone 100
Methylcyclohexane 50
Styrene 50
1,1,2,2-Tetnchloroethane 50
Tetrachloroethene 50
Toluene 50
1,1,2-Trichloro-1,2,2-Trifluoroethane 50
1,2,4-Trichlorobenzene 50
1,1,1-Trichloroethane 50
1,1,2-Trichloroethane 50
Trichlorofluoromethane 50
90
49
46
50
55
100
56
48
49
55
44
53
44
49
49
49
51
50
50
54
43
53
54
49
50
48
54
52
52
92
54
47
51
97
56
54
48
51
52
50
56
46
48
46
90
98
92
99
110
103
113
96
98
109
89
107
87
97
99
98
102
100
100
108
86
106
109
98
100
96
108
103
103
92
108
95
102
97
111
108
96
102
103
100
11'l
93
96
93
60-140
70-1 30
70-1 30
70-130
60-140
60-140
60-140
70-130
70-130
42-163
70-1 30
60-140
70-1 30
70-130
70-130
70-130
70-130
70-130
7G,130
60-140
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
60-140
70-130
70-130
70-'130
60-'t40
70-130
70-130
70-130
70-130
70-'t30
70-130
70-'t30
70-1 30
70-1 30
70-130
10/15/2013 0851
1 0/1 5/201 3 0851
1 0/1 5/201 3 0851
10/1s/2013 08sl
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
1 0/1 5/201 3 0851
10/1 5/201 3 0851
10/15/2013 0851
10/15/2013 0851
10/1 5/2013 0851
10/15/2013 08s1
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/1s/2013 0851
1 0/1 s/201 3 0851
1 0/1 5/201 3 0851
10/1s/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
1 0/1 5/201 3 0851
1 0/1 5/201 3 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
10/15/2013 0851
't 0/1 s/2013 0851
1 0/1 s/201 3 0851
1 0/1 5/201 3 0851
I 0/1 5/201 3 0851
I
I
I
I
I
I
T
i
I
t
I
I
T
PQL = Practlcal quantiiation limit
ND = Not det6ct6d at or abovo the MDL
P = Thg RPD between two GC columns excseds 40% N = Rocovery is out of criteria
J = Eslimated result < PQL and: MDL + = RPD is out of criteria I
IWh6re applicabls, all soil sample analysis are reported on a dry welght basis unl€ss flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:57 ol72
l.gvol 1 ReDort v2.l
I
t Volatile Organic Compounds by GC/MS - LCS
I sampte lD: oe31928-oo2
f Batcn:3rs2'
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^tf:l"", Resurt % Recr Parameter (ug/L) (ug/L) O Dil % Rec Limit Analysis Date
I ff:i:]"il5,
Surrogate
50 58
100 'l 10
AcceotanceO % Rec Lihit
117 70-130 ',t0t15t2013 0851
106 70-130 10/15/2013 0851
I :,""::",::::,ilil:, :i ll_lll
Toluened8 94 70-130
T
I
t
t
I
I
I
I
I
t
t
T
I
PQL = Practical quantitation limit P = The RPD betwoen two GC columns oxceeds 40% N = Re@very is out of crileria
ND = Not detected at orabovethe MDL J = Estimated result< POLand: MoL + = RPD is outof critsria
Wh6r6 applicablo, all soil sample anal)rsis ara reported on a dry w€ight basis unless flagged with a'W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environm€ntal Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page: 58 of 72
Lsv6l 1 Rcpod v2.l
I
IVolatile Organic Compounds by GC/MS - LCSD
Sample lD: OQ31928-003
Batch: 3'1928
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Spike
Amount
(us/L)
Result
(ug/L)
% Rec % RPD
Dil % Rec % RPD Limit Limit Analysis Date tParametera
1,2-Dibromo-3-chloropropane(DBCP) 50
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,4-Dichlorobenzene
1 ,3.Dichlorobenzene
Dichlorodifl uoromethane
I ,2-Dichloroethane
1 ,1-Dichloroethane
1 , 1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Styrene
1,1,2,2-T etrachloroethan e
Tetrachloroethene
Toluene
100
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
84
48
45
51
50
100
51
46
49
49
44
47
45
46
51
54
51
49
49
48
43
49
49
45
47
48
53
58
51
110
51
45
48
100
53
54
48
53
52
44
53
45
55
42
84
96
90
101
101
104
101
91
97
99
88
94
89
92
101
109
103
97
99
96
87
99
98
91
93
97
106
116
102
110
102
89
95
102
105
108
96
106
103
89
106
90
109
84
5.9 60-140 20 10/15/2013 0913
2.4 70-130 20 10/15/2013 0913
2.7 70-130 20 10/15/2013 0913
1.9 70-130 20 10/15t2013 0913
9.3 60-140 20 10/15/2013 0913
0.75 60-140 20 't0/15/2013 0913
11 60-140 20 10/15/2013 09134.7 70-130 20 10/15/2013 0913
0.32 70-130 20 10/15/2013 0913
10 42-163 20 10/15/2013 0913
0.81 70-130 20 10/15/2013 0913
13 60-140 20 10/15/2013 0913
1.9 70-130 20 10115t20130913
5.5 70-130 20 10t15t20130913
2.8 70-130 20 10/1s/2013091310 70-130 20 10115t20130913
o.92 70-130 20 10t15t2013 0913
2.5 70-130 20 10/15/20130913
1.6 70-130 20 10/15/2013 0913
12 60-140 20 10t15t20130913
1.1 70-130 20 10/15/2013 0913
6.7 70-130 20 10/15/2013 0913
10 70-{30 20 10t15t201309137.6 70-130 20 't 0/1 5/2013 0913
6.6 70-130 20 10/15/2013 0913
0.59 70-130 20 10/15/20130913
2.0 70-130 20 10115120130913
11 70-130 20 't0/15/2013 0913
T
I
I
I
I
T
t
I
I
t
I
T
I
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1,2-Trichloroethane
Trich lorofl uoromethane
50
50
50
50
1.1 70-130 20 10/15/2013 0913
19 60-'t40 20 10/15/2013 0913
5.7 70-130 20 10/15/2013 0913
6.0 70-130 20 10/15/2013 0913
7 .2 70-130 20 10/15/2013 0913
5.1 60-140 20 10/15/2013 09135.4 70-130 20 10/15/2013 0913
0.72 70-130 20 10/15/2013 0913
0.56 70-130 20 10/15/2013 0913
3.2 70-130 20 10/15/2013 0913
0.021 70-130 20 10/15/2013 091312 70-130 20 10t15t20130913
4.9 70-130 20 10/15/2013 0913
3.2 70-130 20 10/1s/2013 0913
13 70-130 20 10/15/2013 0913
10 70-130 20 10/15/2013 0913
PQL = Praclicalquantilation limit
ND = Not detoctod at or abovo lhs MDL
P = The RPD betw€en two GC cdumN exceeds 40% N = Recovery is out of crit6ria
J = Estimatod rssult < PQL and i MDL + = RPD is out of critoria I
T
Whor6 applicable, all soil gample analysis are reportod on a dry weight basis unless fragged with a'w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shsaly Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sh€alylab.com
Page: 59 of 72
Level 1 Roport vz.l
I
t Volatile Organic Compounds by GC/MS - LCSD
I Sample lD: 6q3192g-9g3
I Batcn:31928
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^t#fi, Resutt % Rec % RPDr Parameter (ug/L) (ug/L) O Dil % Rec % RPD Limit Limit Analysis Date
50 54100 110
Acceotancea % Rec Lihit
Vinvl chloride
I Xybnes (total)
Surrogate
1 109 7 .2 70-130 20 10/15/2013 0913
1 106 0.28 70-130 20 10/15/2013 0913
I ?:Ti;;:::,"*"J:. :"' ;:.lll
Toluene-d8 94 70-130
I
I
I
I
I
I
I
t
t
I
T
I
I
PQL = Practical quantitatim limit P = The RPD betwoen two GC columns 6xc€ods 40olo N = Ra@very is out of criteria
ND = Notdotscted atorabovothe MDL J = Estimatad result< PQL and: MDL + = RPD is outofcriteria
Whers applic€ble, all soil sample analysis ars reporlod on a dry woight basis unless flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Envionmental SeMces, lnc.
106 Vantage Point Drive W6st Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:60 ol72
Lsvel I Report v2.l
I
IVolatile Organic Compounds by GC/MS - MB
Sample lD: 9q31946-9O't
Batch:31948
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 T
Parameter o IAnalysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
I ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethane
trans- 1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans- 1, 3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etachloroethane
Tetrachloroethene
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
1.1
1.7
0.70
1.8
2.4
1.3
1.8
1.7
1.3
0.83
1.0
0.67
1.5
1.7
0.85
1.7
1.7
1.7
't.6
1.0
0.73
1.5
0.76
1.7
0.91
0.82
0.68
1.7
1.3
0.23
0.98
0.40
1.5
0.41
2.6
1.1
0.47
0.50
1.7
0.63
1.7
0.79
0.85
I
I
I
I
I
t
t
I
I
T
t
I
T
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/k9
ug/kg
ug/kg
ug/kg
ug/kg
ug/k9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10115t20't3 't't24
10t1512013 1124
't0t15t2013 't124
10t1512013 1124
10t15120131124
10t15120131124
10t1512013 1124
10t'15120131124
10115120131124
10115120131124
10t't5120131124
10/1s/2013 1 124
10t't5t20131124
10115120131124
10115t2013 1124
10t15t20131124
1011512013',!124
10115120131'.t24
10t15120131124
10t15t2013't124
10115t20131124
1011512013'.|124
10t1512013 1124
10t1512013 1124
10115120131124
10t15rl20't31',t24
1011512013 1124
10t15120131124
10115120131',124
10115t2013 1124
10t15t20131124
10t1512013 1124
10t15120131124
10t15120131124
10t1512013 1124
10t15120',131124
10t15120131124
'10t1512013 1124
10t15t2013 1124
10t15t20131124
't0t1512013 1124
10t15120131124
10t1s120131124
10t15120131124
1,2-Dibromo-3-chloropropane(DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane ND
1.2.4-Trichlorobenzene ND
1,1,2-Trichloroethane
'l ,1 , 1-Trichloroethane
ND
ND
PQL = Practical quantitation limit
ND = Not d€tected at or above tho MDL
P = The RPD b6tws6n two Gc columns exceeds /t0% N = Racovsry is out ofcritoria
J = Estimated rosult < PQL and : MDL + = RPD is out of criteria T
I
Where applicable, all soil sample analFis aro reported on a dry weight basis unless flagged with a "vw
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Envircnmental Sorvices, lnc.
106VantagePointDrive WestColumbia,SC 29'172 [phone] Fax[phone] www.shealylab.com
Page:61 of72
Lev€l 1 Repod v2.l
I
I Volatile Organic Compounds by GC/MS - MB
t
t"."l':,:r:oQ31e48-oo1
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I Parameter Result a Dil PQL MDL Units Analysis Date
Trichloroethene
I Trichlorofluoromethane
I Vinyl chloride
Xylenes (total)
ND
ND
ND
5.0 1.9 ug/kg 1011512013 1124
5.0 1.5 ug/kg 1011512013 1124
5.0 0.86 ug/kg '10115120131124
5.0 2.9 ug/kg 10115120131124
t Surrogate
ND1
AcceptanceA 7o Rec Lihit
Bromofluorobenzene
I i;-,'"':::;"**"'
I
I
T
I
I
I
83 47-138
89 53-142
87 68-124
I
J
I
I
I
t
PQL = Practical quantitation limit P = The RPD betwean two GC columns exceeds 40% N = Recovery is out ofcriteria
ND = Not detected at or abovs the MDL J = Estimatod result < PQL and: MDL + = RPD is out of criteria
Whsre applicable, all soil sample analysis are rsported on a dry welght basis unlsss flagged with a 'W'
Note: Galculatlons are performed before rounding to avoid round-off errors in calculated resulG
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Pagel.62o172
L6vel I Report v2.l
I
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: Oe31948-002
Batch:31948
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 t
Spike
Amount(us/ks)Result(us/ks)% Rec
% Rec
Limit tParameterDitoAnalysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans- 1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-I etachloroethane
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
'1,1,1-Trichloroethane
100
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
50
50
50
50
100
40
40
39
44
95
45
40
40
42
41
40
42
45
40
44
39
39
41
43
4',1
39
42
42
43
40
42
42
42
100
43
43
40
95
43
42
36
42
41
40
42
43
41
43
104
80
80
79
89
95
89
81
80
84
82
79
84
90
80
89
79
79
83
85
82
79
85
83
87
79
83
84
85
100
86
86
80
95
86
83
72
83
82
80
83
85
82
86
60-140
69-123
69-121
61-1 19
10-168
57-',t48
58-122
58-1 36
59-129
42-163
71-125
34-'.t34
53-1 39
55-125
66-1 1 I
74-124
52-133
51-134
s7-131
10-157
67-129
71-127
68-131
70-122
69-138
72-124
70-124
70-126
59-128
54-137
50-136
59-1 37
70-1 30
60-1 34
41-144
70-1 30
54-'t36
69-1 32
45-150
61-129
49-1 36
34-145
55-128
63-128
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 09s0
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 09s0
10/15/2013 0950
10/15/2013 09s0
1011512013 0950
10/15/20't3 0950
'l 0/1 5/2013 0950
1 0/1 5/201 3 0950
1 0/1 5/201 3 0950
1 0/1 5/201 3 0950
1 0/1 5/201 3 0950
1 0/1 s/201 3 0950
1 0/1 5/201 3 0950
1 0/1 5/201 3 0950
10/15/2013 0950
10/15/2013 0950
1 0/1 5/201 3 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
10/15/2013 0950
I
I
I
I
t
I
I
I
I
I
I
I
t
PQL = Practical quantitation limil
ND = Not dotsted at or above the MDL
P = The RPO bet$/€6n two GC columns excgeds 40% N = Rocovery is out of criteria
J = Estimated rsuli < PCIL and > MDL + = RPD ls out of cribria T
IWhere applieble, all soil sample analysis ars reponed on a dry weight basis unl€ss flagged with a nW
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shoaly Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 791-S111 www.shealylab.com
Page: 63 of 72
Level 1 Reportv2.l
I
I Volatile Organic Compounds by GC/MS - LCS
I Sample lD: Oe31948-002
I Batcn:31948
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
a spikeI Amount Result % Recr Parameter (uq/ks) (uq/kq) O Dit % Rec Limit Analysis Date
t
I
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
50 42
50 45
50 44
100 82
AcceptanceO % Rec Lihit
1
1
1
1
84 62-126 10/15/2013 0950
91 45-138 10/1s/2013 0950
88 42-132 10/15/2013 0950
82 58-128 10/15/2013 0950
Bromofluorobenzene
I l;1;?illlX""*"'
I
I
I
t
I
T
86 47-138
87 53-142
89 68-124
t
t
I
I
t
I
POL = Practical quantltation limit P = Ths RPD between two GC columns oxcesds 40% N = Recovery is out of criteria
ND = Not detectod atorabove the MDL J = Estimated result < PQLand? MDL + = RPD is out ofcriteria
wh8re applicable, all soil sample analysls are reportod on a dry woight basis unless flagged with a "vV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage PointDrive WestColumbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: O1 of 72
Lsvsl 1 Rcpo.t v2.1
I
IVolatile Organic Compounds by GC/MS - LCSD
SamPle lD: OQ31948-003
Batch:31948
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 I
Spike
Amount
(ug/kg)
Result(ug/kg) O
% Rec % RPD
Dit % Rec % RPD Limit Limit Analysis Date tParameter
Acetone
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1,2-Dibromo-3-chloropropane(DBCP) 50
Dibromochloromethane 50
1,2-Dibromoethane (EDB) 50
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
1 ,2-Dichloropropane
trans- 1, 3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
Methylcyclohexane 50
Methylene chloride 50
Styrene 50
1 ,1,2,2-Tetrachloroethane 50
Tetrachloroethene 50
Toluene 50
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1,2,4-Trichlorobenzene 50
1,1,2-Trichloroethane
1 ,1 , 1-Trichloroethane
100 97
4'.!
41
39
37
92
44
42
41
41
40
39
43
46
42
43
40
39
41
45
40
39
42
41
43
39
43
42
41
95
43
41
39
96
44
41
36
42
43
41
42
43
41
42
97
81
82
79
75
92
89
83
83
81
8'r
79
86
92
83
87
80
79
81
89
80
79
84
82
85
79
86
85
83
95
86
83
77
96
87
82
73
84
85
81
83
85
83
85
7.2 60-140 20 10t15t2013 1014
1.4 69-123 20 '.10t15t20131014
3.2 69-121 20 10115t20131014
0.24 61-119 20 10t15t20131014
17 10-168 20 1011s1201310',14
4.2 57-148 20 10115120131014
0.71 58-122 20 10115120',1310142.9 58-136 20 10t15120131014
2.8 59-129 20 10/15/20131014
3.0 42-163 20 10115120131014
1.2 71-125 20 10115120131014
0.53 34-134 20 '.t0t15t20131014
1.9 53-139 20 10t15120131014
2.2 55-125 20 10115120131014
3.8 66-1 19 20 10t15t2013 10',t4
2.5 74-124 20 10115t20'.t31014
1.0 52-133 20 10t15t201310'.14
o.17 51-134 20 10t15t20131014
2.3 57-131 20 10115t20131014
5.0 10-157 20 10/15/2013 1014
1.9 67J129 20 10t15t20131014
0.028 71-127 20 10115t20131014
1.5 68-131 20 '.t0t15t201310141.9 70-122 20 10115t20131014
2.1 69-138 20 10/15/2013 1014
0.54 72-124 20 1011st2013',t014
3.7 70-124 20 10115t20',t310141.2 70-126 20 10t15t2013'.1014
2.4 59-128 20 10t'.t5t20131014
5.2 54-137 20 10t15120',131014
0.26 50-136 20 10115t20131014
3.7 59-137 20 10115t20131014
3.3 70-130 20 10115t20131014
0.61 60-134 20 10115t20131014
1.4 41-144 20 10115t20131014
1.4 70-130 20 10/15/2013 10't4
0.10 54-136 20 10t15t20131014
0.94 69-132 20 10t15120131014
3.9 45-150 20 1011512013'.10141.6 61-129 20 10t15t20131014
0.21 49-136 20 10/15/2013 1014
0.30 34-145 20 10115120131014
0.17 55-128 20 10115t20131014
1.0 63-128 20 10t15t201310'.t4
50
50
t
I
I
I
t
I
I
I
I
t
I
I
I
POL = Practicalquantitation limit
ND = Not dstected at or above the MDL
P = Th6 RPD between trc GC @lumns exceads 40% N = Recovery is out of criteria
J = Estimatsd rosult < PQL and : MDL + = RPD is out of cdteria I
tWhere applicable, all soil sample analysis ar€ reported on a dry weight basis unless flagged with a .W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 65 of 72
Levol 1 RsDortv2.l
I
I Volatile Organic Compounds by GC/MS - LCSD
I Sample lD: OQ3194B-OO3
I Batch:31948
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
t ^T:li, Resurt % Rec % RPDr Parameter (us/ks) (us/ks) O Dil % Rec % RPD Limit Limit Analysis Date
t iifi::i:,j,*:H*"."
Xylenes (total)
50 43
50 44
50 44
100 80
AcceptanceO % Rec Liinit
1 87 3.2 62-126 20 1011512013 1014
1 88 2.6 45-138 20 1011512013 1014
1 87 0.41 42-132 20 1011512013 1014
1 80 3.0 58-128 20 1011512013',|014
I Surrogate
Bromofluorobenzene
I li:::ff"**"'
t
I
I
t
I
t
I
I
t
I
89 47-138
88 53-142
93 68-124
I
t
PQL = Practical quantitation limit P = Th€ RPD between two GC columns axceeds 40% N = Rocovsry is out ofcriteria
ND = Not detocted at or above the MDL J = Estimated result < PQL and: MDL + = RPD is oul of diteria
Whers appli€ble, all soll sample analysis ars reported on a dry weight basis unl€€s 0agged with a nV"
Note: Calculations are performed before rounding to avoid round.off errors in calculated results
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Pago:6 ot72
Level 't Roport v2.1
I
IVolatile Organic Compounds by GC/MS - MB
Sample lD: 6q31949-991
Batch:31949
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 T
Parameter o IPOLAnalysis Date
Methyl acetate
Methylene chloride
Tetrachloroethene
Trichloroethene
Surrogate
I
t
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
o
50
50
50
50
AcceptanceLimlt
250
250
250
250
49
130
25
95
10114120'l'31244
10t1412013 1244
10t1412013 1244
1011412013 1244
% Rec
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
105
110
110
47-138
53-142
68-124 t
I
I
I
I
t
I
t
I
I
I
PQL = Practical quanttation limit
ND = Not detec'ted at or abova the MDL
P = The RPD batween two GC columns exceeds 40olo N E Rocovery is oul ofcritsria
J = Estimated rosult < PQL and i MDL + = RPD is out of critsria t
T
Wh€re applicable, all soil sample analysis are roportod on a dry u€ight basis unless flagged with a "vtr
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Sorvices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:67 ot72
Le\r€l I Report v2.1
t
I Volatile Organic Compounds by GC/MS - LCS
I '"'l':,:?::,ti1e4e-oo2
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I ^T;1"", Resurt % Recr Parameter (us/ks) (us/kg) O Dit % Rec Limit Analysis Date
I [#';;:"Ir"Jtr
Trichloroethene
2500 2700
2500 2500
2500 2400
2500 2600
AcceotanceO % Rec li'hit
50 107 59-137 10t1412013 1307
50 99 70-130 10t14t2013 1307
50 98 45-150 1011412013 1307
50 102 62-,t26 10t1412013 1307
t Surrosate
Bromofluorobenzene 102 47-138
I i;1-,'#ll"**"' ;:: Z:::1
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ND = Not dotected atorabove th6 MDL J. Estimated rssult< PQL and: MDL + = RPD is out ofcriteria
Wh6ro applicable, all soil sample analysis are rsported on a dry woight basis unlgss flagged with a "W"
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 68 of 72
Lovsl 'l R@ort v2.1
T
IVolatile Organic Compounds by GC/MS - LCSD
Sample lD: Oe31949-003
Batch:31949
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 I
SpikeAmount Result % Rec % RPD(us/ks) (uE/ks) O Dil % Rec % RPD Limit Limit Analysis Date IParameter
Methyl acetate
Methylene chloride
Tetrachloroethene
Trichloroethene
Surrogate
2500
2500
2500
2500
o
4.1
5.9
1.2
2800 50 111
2600 50 105
2500 50 99
2600 50 102
AcceDtance
% Rec Liinit
59-137 20 10t14t20131330
70-130 20 10114120131330
45-150 20 10114120131330
0.23 62-126 20 10t14120131330
I
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Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
100
106
102
47-138
53-142
68-124 I
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PQL = Practical quantitation limit
ND = Not detocted et or above the MDL
P = The RPD between two GC columns sxceads 40olo N = Recovery is out of criteria
J = Estimatod r€sult < PQL and: MDL + = RPD is out of crltsria I
IWhers applicable, all soil sample analysis are reported on a dry weight basis unloss flaggsd with a nV'
Note: Calculations are performed before rounding to avold round-off errors in calculated results
Shealy Environmental Services, lnc.
'f 06 Vantage Point Driv€ West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 69 of 72
Level 1 Reportv2.l
I
t Volatile Organic Compounds by GC/MS - MB
I Sampre rD: oe3222o-oo1
I Barcni3222o
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I Parameter Result a Dit PQL MDL Units Analysis Date
t Y,"Jl[ffi:l"J'*
Surrogate
5.0 1 .7 ug/L 1011712013 2146
5.0 0.30 ug/L 1011712013 2146ND1
AcceDtanceO % Rec Liinit
I Bromofluorobenzene 103 70-130
I 1,2-Dichloroethane-d4 97 70-130
Toluene-d8 93 70-130
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PQL = Praclical quantitation limit P = The RPD betwesn two GC columns exeeds 40% N = Rgcovery is out of cdteria
ND = Notdetectod atorabovelhe MDL J = Estimated result< PQL and: MOL + = RPD is outofcriteria
Wherc applicabls, all soil samplo analysis are reported on a dry wqight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental SeNices, lnc.
106VantagePointDrive WestColumbia,SC 29'172 [phone] Fax[phone] www.shealylab.com
Page: 70 of 72
Lev6l 1 Report v2.l
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: gq3222g-gg2
Balchi32220
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
SpikeAmount Result % Rec(ug/L) (ug/L) O Dit % Rec Limit Analysis Date TParametel
Methylene chloride
Trichloroethene
Surrogate
t50
50
o
51
50
AcceptanceLimit
101
99
70-130
70-130
10t17 t2013 2014
10117 t2013 2014
o[ Rec
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
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97
90
93
70-1 30
70-1 30
70-1 30
PQL = Praclical quantitation limit
ND = Not detected at or above tho MDL
P = Ths RPD between two GC columns sxceeds 40% N = Recovory is out of criteria
J = Estimated rgsult < PQL and I MDL + = RPD is out of critoria I
IWhere applicable, all soil sample analysis are roported on a dry wstght basis unkass flagged with a 1 r'
Note: Calculations are performed before rounding to avold round-off errors in calculated results
Shealy Environmental S€rvices, lnc.
106 Vantag€ Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shoalylab.com
Page:71 of72
L€vel I Roport v2.1
I
I Volatile Organic Compounds by GC/MS - LCSD
I Sample lD: 6632229-993
f Batcn:3zzzo
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^tJI"", Resutt % Rec % RPD
- Parameter (us/L) (us/L) O Dit % Rec % RPD Limit Limit Analysis Date
I :*i*j*"
50 52
50 51
AcceDtanceO % Rec t-ihit
1 103 1.9 70-130 20 ',10117120132037
1 103 3.2 70-130 20 10117120132037
I Bromofluorobenzene 100 70-130
I 1,2-Dichtoroethane-d4 94 70-130
Toluene-d8 96 70-130
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POL = Practical quantitation limit P = The RPD betweon two GC columns sxceeds 4070 N = Recovory is out of criteria
ND = Not detsctsd at or abovs the MDL J = Estimat€d result < PQL and: MDL + = RPD is out of criteria
Where applicable, all soil samplo analysis are roported on a dry weight basis unless flagged with a 'W'
Note: Calculations are performed before rounding to avoid round.off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:I2 ot72
Levol 1 Reportv2.l
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l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com Level I Reportv2.l
SHEALY ENVIRONMENTAL SERVICES. INC.
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Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
I
ILevel 1 Roport v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.I
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Report of Analysis
Terracon Consultants, lnc.
3534 Rutherford Road
Taylors, SC 29687
Attention: George Flores
Project Name:lRC
Project Number:861 27 103
Lot Number:OK15049
Date Com pl eted:l 1 121 1201 3
s*"fu
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, lnc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
aaaaaaaao
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 1 of rO
Lovel 1 Reportv2.l
SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No:32010
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NC DENR No: 329NELAC No: E87653
Case Narrative
Terracon Consultants, lnc.
Lot Number: OKl5049
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordancr with the most current approved NELAC standards, the
Shealy Environmental Services, lnc. ("Shealy') Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any excrptions to the NELAC standards, the QAMP, SOPs or policies are qualifted on the results page or discussed below.
lf you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Shealy Environmental Services, lnc.
106 Vantage Point Drive W€st Columbia, SC 29'|72 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page: 2 of40
Lav6l l Reportv2.l
T
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, lnc.
Lot Number: OK15049
Sample Number Sample lD Matrix Date Sampled Date Received
001
002
003
004
005
006
007
008
009
010
011
HMSMW.lS
HMSMW.lI
HMSMW-2S
HMSMW.2I
HMSMW-3S
HMSMW-3I
HMSMW-4S
HMSMW-4I
RINSE BLANK
HMSMW.4D
TRIP BLANK
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
't1t1412013 1830
11t14t2013',t725
11t14t2013 1810
11t14t2013 1530
11114t2013 1755
11t14t2013 1430
11114120131640
11114120131320
11114120131745
11t14t2013 1325
1111412013
11t15t2013
1111512013
11t15t2013
11t15t20'.13
11t1512013
11t1st2013
1',v1512013
11t1512013
11t1512013
11t1512013
11t1512013
(1 1 samples)
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 3 of rO
Level I Report v2.l
SHEALY ENVIRONMENTAL SERVICES, ING.
Executive Summary
Terracon Consultants, lnc.
Lot Number: OK15049
Sample Sample lD Matrix Parameter Result O
OO1 HMSMW-1S
002 HMSMW-1|
003 HMSMW-2s
003 HMSMW-2S
OO3 HMSMW-2S
OO4 HMSMW-2I
Aqueous Chloroform
Aqueous Chloroform
Aqueous Chloroethane
Aqueous 1,1-Dichloroethane
Aqueous 1,1,1-Trichloroethane
Aqueous Chloroform
8260B
82608
82608
82608
82608
8260B
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
7.0
11
270
42
5.0
12
5
7
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11
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(6 detections)
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: tl of ,O
Lev6l 'l Rgport v2.1
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Client: Terracon Consultants, lnc.
Description: HMSMW-lS
Date Sam pled : 1 1 I 1 412013 1830
Date Received : 1'l l1 512013
Laboratory lD: OK1 5049-001
Matrix: Aqueous
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11120t2013 2307 PMM2
Batch
34894
Parameter
cAs
Number
Analytical
Marhod Result a
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82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Ghloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 , 1-Dichloroethane
I ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Sgrene
1,1,2,2-T etnchloroethan e
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-2s-2
74-83-9
78-93-3
75-1 5-0
56-23-s
1 08-90-7
75-00-3
67-66-3
74-87-3
'110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
54',1-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591 -78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ugIL I
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
PQL . Practical quanlitation limit B = Doiectsd in tho method blank E = Quantitation of compound oxceeded the calibration range H = Out of holding tlmo
ND = Notdetocted at orabovs the PQL J = Estimated result< PQLand: MDL P = The RPD between two GC columns exc€sds 40% N = Recovery is outofcritsria
whero applicable, all soil sample analysis are reported on a dry r €ight basis unless flagged with a "w"
Shealy Environmental SeNices, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page:5 of tlO
Level I Report v2.1
Client: Terracon Consultants, lnc.
Description: HMSMW-1S
Date Sampled : 1 1 11 412013 1830
Date Received : 1 1 11 512013
Laboratory lD: OK1 5049-001
Matrix: Aqueous
Volatile Orsanic Compounds by GC/MS
I
I
IBatch
34894
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 ',t 1112012013 2307 PMM2
Parameter
CAS Analytical
Number Method Result O PQL
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
'l ,1 , 'l -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-'l
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run'l AcceptanceO % Recovery Limits
82608
82608
82608
82608
82608
82608
8260B
82608
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1ug/L 1
ug/L 1ug/L 1
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
107
109
101
70-1 30
70-1 30
70-130
I
I
I
I
I
I
T
I
I
I
PQL = Practical quantitation limit B = Detectsd in th6 method blank E = Quanlitation of compound exceded the calibration rang€
ND = Not dot€cted at or above tho PQL J = Eslimaled rosult < PQL and: MDL P = Ths RPD betw66n two GC columns exceods 40%
Where applicable, all soil sample analysis are reportsd on a dry w€ight basis unloss flag$d with a "Vt"
H = Out of holding time
N = Recovsry is out of critsria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79't-9111 www.shealylab.com
Page:6 of40
Le\,€l 1 Roport v2.1 I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-002
Description: HMSMW-I| Matrix: Aqueous
Date Sampled :1 1 11 412013 17 25
Date Received : 11 l1 512O13
Volatile Orqanic Compounds by GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11t2012013 2332 PMM2
Batch
34894
Parameter
cAs
Numher
Analytical
Mathar{Result O Units Run
I
I
I
I
I
I
I
I
t
I
I
I
I
I
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl ac,etate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-l etrachloroeth a ne
Tetrachloroethene
Toluene
67-64-',1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
s6-23-s
1 08-90-7
75-00-3
67.66-3
74-87-3
110-82-7
96-12-8
't24-48-1
106-93-4
95-50-1
54',1-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
10061-01-5
10061-02-6
10041-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
82608
8260B
8260B
82608
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
82608
8260B
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1ug/L 1
ug/L 1
ug/L 1
uSrL I
ug/L 1
ug/L 'l
ug/L 1
ug/L 1ug/L 'l
ug/L 1
ug/L 1
ug/L 1
uS/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uglL 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = PTactical quantitation limii B = Detected in tho msthod blank E = Quantitation of compound Excoeded th6 calibration range H = Out of holding time
ND = Not detocted at orabove the PQL J = Estimalgd result< PQL and: MDL P =The RPD botwsen two GC @lumns exceeds 40olo N = Recov€ryi6 outofctteria
Where applicable, all soil sample analysis are rsported on a dry weight basis unless flagged with a "W"
Shealy Environmental SeNices, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 7 of ,O
Lsvsl t Reportv2.l
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-002
Description: HMSMW-1| Matrix: Aqueous
Date Sampled : 1 1 11 412013 17 25
Date Received : 1 1 l1 512013
Volatile Organic Compounds by GC/MS
I
t
IRun
1
Prep Method
5030B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82608 1 11120120132332 PMM2 34894
Parameter
CAS
Number
Analytical
Method Result O Units
1,1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run I AcceptanceO % Recovery Limits
8260B
8260B
82608
82608
82608
82608
82608
8260B
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
I
I
I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
1,2-Dichloroethane-d4
Bromolluorobenzene
Toluene-d8
97
98
94
70-1 30
70-'t30
70-1 30
I
I
I
I
I
I
I
I
I
I
PQL = Practical quantitation limit B = Detected in tho method blank E = Quantitation ofcompound excoeded the oalibralion range
ND = Notdetoctod at orabovethe PQL J = Estimated result< PQLandi MDL P = The RPD betw6en two GC columns exc€eds 40olo
Wher6 applicablo, all soil sample anal!6is are reportod on a dry wdght basis unloss flaggsd with a nv'
H = Out of holding time
N = Recovery is out of criteria I
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page: 8 of40
Level 1 Reportv2.l I
I
t
I
Client: Terracon Consultants, lnc.
Description: HMSMW-2S
Date Sampled:'l 1 l1 412013 1810
Date Received :'l 1 l1 512013
Laboratory lD: OKI 5049-003
Matrixl Aqueous
Volatile Orsanic Compounds by GC/MS
Run Prep Method't 50308
2 s0308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 I 1',U20t20132355 PMM2
82608 5 11121120130831 JHD
Batch
34894
34912
Parameter
CAS
Number
AnalyticalMarhnd Result a
I
I
I
T
I
I
I
I
I
I
I
I
I
I
I
t
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
'1,1-Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-O
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-',!
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-31-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
10061-0'r -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
't634-04-4
'r08-10-1
't08-87-2
75-09-2
100-42-5
79-34-5
127-18-4
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
uglL 1
ug/L 1
ug/L 2
ug/L 1
ug/L 1
uglL 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1
ug/L 1ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
8260B
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
82608
8260B
82608
8260B
8260B
8260B
82608
82608
8260B
8260B
82608
8260B
8260B
82608
82608
82608
8260B
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
270
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5,0
5.0
25
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
PQL = ftaclical quantitation limit B = Datected in th6 method blank E = Quantitation ofcompound excoeded lhe calibration range H = Out ofholding tlme
ND = Noldetectod at or abov€ the PQL J = Estimatod result< PQL and: MDL P =The RPD between two GC columns exceeds 40% N = Recovery is outofcliteria
Where applicable, all soil sampls analysis are reportsd on a dry w€ight basis unless flagged with a'W'
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 9 of 40
Level 'l REport v2.1
Client: Terracon Consultants, lnc.
Description: HMSMW-2S
Date Sampled:1 I l1 412013 1810
Date Received : 1 1 11512013
Laboratory lD: OK1 5049-003
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
t
I
IBatch
34894
34912
Run
1
2
Prep Method
50308
5030B
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11t20t20132355 PMM2
82608 5 1112112013 0831 JHD
Parameter
cAs
Number
Analytical
Mathod Result O Units I
Toluene
1,'1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroothane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
82608 ND
82608 ND
82608 ND
82608 5.0
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
Run 2 AcceptanceA % Recovery Limits
5.0
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
101
101
96
70-1 30
70-1 30
70-'t 30
114
112
104
70-130
70-130
70-130 t
I
I
T
I
t
I
I
I
PQL = Practical quantitation limit B = Del6ct6d in the method blenk E = Quantitation of compound oxcesded tho €libration rangg
ND = Not dotocted at or above the PQL J = Estimated result < PQL and: MDL P = Ths RPD bstweon two GC columns oxceods 40%
Whero applicablo, all soil sample analysis are reported on a dry reight basis unl6s flagged with a "W'
H = Out of holding time
N = Rocovery is out of criteria I
Sh€aly Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] t www.shealylab.com
Page: 10 of40
L6vel 1 Report v2.1 I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-004
Description: HMSMW-2| Matrix: Aqueous
Date Sampled :1 1 11 4120'13 1530
Date Received : 11 l1 512013
Volatile Orqanic Gompounds bv GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11t2112013 0018 PMM2
Batch
34894
Parameter
cAs
Number
Analytical
Merhod Result O
I
I
t
T
T
T
I
I
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Ghloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1, 2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
67.66.3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
59't-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
't00-42-5
79-34-5
127-18-4
1 08-88-3
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uS/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uS/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1
uC/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1ug/L 1
ug/L 1
ug/L I
ug/L 1
ug/L I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uglL 1
ug/L 1
ug/L 1
ug/L 1
ug/L I
ug/L 1ug/L 1
ug/L 1
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
8260B
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
4-Methyl-2-pentanone
- Methvlcvclohexane
I uetnvune chlorider styrene
1, 1,2,2-T etnchloroehan e
I
Tetrachloroethene
I
PQL = Practical quantitation limil B = Oetected in the mothod blank E = Quantitation of compound excooded lhe calibration range H = Out of holding time
ND = Not d6toct6d at or abovsthe PQL J = Estimated rosult< PQL and: MDL P = The RPD between two GC columns exceeds 40olo N = Recovsry is outofcriteria
Wher6 applicable, all soil sampls analysis are raported on a dry reight basis unless flagged with a 'W"
Shealy Environmental Sorvices, lnc,
I
,* Vantage Point Driv€ West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
I
Page:11 of40
Levol 'l R@od v2.1
Client:Terracon Gonsultants, lnc. Laboratory lD: OK15049-004
Description: HMSMW-2| Matrix: Aqueous
Date Sampled :'l 1 I 1 41201 3 1 530
Date Received : 1 1 l1 5120'13
Volatile Orqanic Compounds bv GC/MS
I
I
IBatch
34894
Run
1
Prep Method
50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11t21t20130018 PMM2
Parameter
CAS Analytical
Number Meihod Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,'1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surogate
76-1 3-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
7s-01-4
1330-20-7
Run 1 AcceptanceA % Recovery Limits
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
I
t
I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
103
100
95
70-1 30
70-1 30
70-1 30
I
I
I
I
t
I
I
I
I
t
PQL = Pra6lical quantitation limit B = DotsctBd in the method blank E = Quantitation of compound exc@dod the calibration range
ND = Not dotected at or above the PQL J = Estimated result < PQL and: MDL P = Th€ RPD b6tw6en two GC columns oxceods 40ol
Where applicable, all soil sample analysis are reportsd on a dry w€ight basis unlass flagged with a -w"
H = Out of holding tims
N = Recovery is out of critgria I
Shealy Environmental Services, lnc.
106 Vantage Point Driv€ West Columbia, SC 29172 [phone] Fax [phone] wwu,.shealylab.com
Page: 12 of ,10
Lov6l 1 Roport v2.1 I
I
I
I
Client: Terracon Consultants, lnc.
Description: HMSMW-3S
Date Sampled: 1 1 11 412013'1755
Date Received : 1 1 11 512013
Laboratory lD: OKI 5049.005
Matrix: Aqueous
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch82608 ',t 11t21t2013 0040 PMM2 34894
Parameter
CAS
Number
Analytical
Method Result a
I
I
t
t
I
I
t
I
I
I
I
I
I
I
I
I
I
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
8260B
8260B
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etnchloroeth a ne
Tetrachloroethene
Toluene
67-64-',1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
s6-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
12448-1
106-S3-4
95-50-1
541-73-1
1 06-46-7
75-71-8
7s-34-3
107-06-2
75-35-4
1 56-59-2
15660-5
78-87-5
10061-01-5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
'too-42-5
79-34-5
127-18-4
1 08-88-3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uS/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
PQL = ftaclicalquantitation limit B = Det6cted in ih6 method blank E = Quantitation of compound oxceeded the calibration range H = Out of holding time
ND = Notdetected atorabovethe POL J = Estimatod result< PQLand: MDL P = Th6 RPO betreen trc GC columns ex@eds iyo N = Recovery is outof critsria
Where applicablo, all soil samplB analysis are rsported on a dry wsight basis unless flagged with a nv"
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 13 of40
Level I Reportv2.l
Client: Terracon Consultants, lnc.
Description: HMSMW-3S
Date Sampled : 1 1 11 412013 17 55
Date Received: 11115120'13
Laboratory lD: OKl 5049-005
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
t
I
tRun
1
Prep Method
5030B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82608 1 11t21t2013 0040 PMM2 34894
Parametel
CAS Analytical
Number Methar{Result O PQL
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,'1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-1 3-1
120-82-l
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
82608
82608
82608
82608
82608
82608
82608
82608
I
I
I
ug/L 'l
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
103
106
95
70-l 30
70-1 30
70-1 30
I
I
I
I
I
I
T
I
I
I
PQL = Practical quantitation limit B = Dgtscted in lhe malhod blank E = Quantitation of compound sxcoedsd the calibration range
ND = Not detected al or above the PQL J = Estimated result < FQL and: MDL P = The RPD botw*n two GC columns excseds 40%
Wh6re applicable, all soil sample analysis ar6 reporled on a dry weight basis unless flaggod with a nV"
H = Out of holding tim6
N = Rocovery is oul of critsria t
Shealy Environmental SeNices, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.sh€alylab.com
Page: 14 of ttO
Lsv6l I Reportv2.l t
T
t
t
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-006
Description: HMSMW-3| Matrix: Aqueous
Date Sampled : 1 1 I 1 412013 1 430
Date Received : 1 1 l1 5120,.3
Volatile Orqanic Compounds by GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82608 1 11t2112013 0102 PMM2 34894
Parameter
CAS
Number
Analytical
Marhart Result O POL
I
I
I
I
t
I
I
t
t
I
I
I
I
I
I
I
I
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
ug/L
ug/L
ug/L
uSlL
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
'l ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etrachloroeth a ne
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-',1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061-01-5
1 0061 -02-6
100-4't-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08.1 0-1
108-87-2
75-09-2
10042-5
79-34-5
127-18-4
108-88-3
PCIL = Practical quantitation limit B = Detectod in the method blank E = Quantitation of compound exce€ded the calibration range H = Out of holding timo
ND = Not dstected atoraboveth6 PQL J = Estimatod rosult< PQL and: MDL P. The RPD between two GC columns excseds 40% N = Rscovoryisoutofcdtotie
Where applicable, all soil samplo analysis are reportsd on a dry w€ight basis unless flagged with a 'W"
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 15 of40
Level I R6portv2.1
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-006
Description: HMSMW-3| Matrix: Aqueous
Date Sampled:11 11 412013 1430
Date Received : 11 11512013
Volatile Organic Compounds by GC/MS
t
I
tRun
1
Prep Method
50308
Analytlcal Method Dilution Analysis Date Analyst Prep Date Batch
82608 1 11121120130102 PMM2 34894
Parametel
CAS Analytical
Number iltathod Result O Run
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
7S-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
82608
82608
82608
82608
8260B
8260B
82608
82608
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
ND
ND
ND
ND
ND
ND
ND
ND
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 'l
ug/L 1ug/L 1
t
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
100
98
92
70-130
70-130
70-130
t
I
I
I
I
I
I
t
!
t
PQL = Practical quantitation limit B = Dotmtsd in the method blank E = Quanlitation of compound sxcoeded tho calibration range
ND = Not d€tected at or above the PQL J = Estimated result < PQL and: MDL P = Ths RPD betwoen lwo GC columns exceeds 40olo
Whsre applicabl€, all soil samplo analtEis are reported on a dry weight basis unloss flaggod with a nv'
H = Out of holding tims
N = Recovery is out of criteda I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page: 16 of40
L6vel 1 Report v2.1 I
T
I
I
Client: Terracon Consultants, lnc.
Description: HMSMW-4S
Date Sampled:1 1 11412013 1640
Date Received :'l 1 l1 512013
Laboratory lD: OKI 5049-007
Matrix: Aqueous
Volatile Orqanic Compounds by GC/MS
t Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch82608 1 1112112013 0125 PMM2 34894
Parameter
CAS
Number
Analytical
Mathod Result O UnitsI
I
I
I
T
8260B
82608
82608
8260B
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
't 0061-02-6
100-41-4
591 -78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
1 08-88-3
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
ug/L 1
ug/L I
ug/L 1
ug/L 1
ug/L 'l
ug/L 1
ug/L 1ug/L 1
ug/L 1
uglL 'lug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
uS/L 1ug/L 1
ug/L 1
1,2-Dibromoethane (EDB)
1 .2-Dichlorobenzene
I 1.3-Dichlorobenzene
I 1,4-Dichlorobenzene
Dichlorodifl uoromethane
I 1.1-Dichloroethane
f 1.2-Dichloroethaner 1,1-Dichloroethene
cis-1 .2-DichloroetheneI IHr:;i;?:*:ffi:I*"
cis-1,3-Dichloropropene
I iil":*#foropropene
lsooroovlbenzene
I illilllHTbuty,ether(MrBE)
4-Methyl-2-pentanone
I Methvlcvclohexane
I Mdh;b;e chtorideI styrene
'1,1,2,2-TetrachloroethaneI I:[:"J"'""'n"""
I
I POL = Practical quanttation limit B = D€lected in the method blank E = Quantilation of compound exceeded the calibration range H = Out of holding time
ND = Not det€ctod atorabovsthe POL J = Estimated rcsult< PQL and: MDL P = The RPDbetween two GC columns exeseds 40% N = Recovory is out ofcdtoria
Whero applicable, all soil samplo analysis are reportod on a dry weight basis unless flagged with a "\ /'
I
?ffi:.ilil"Jffif,l,:"'fr:'ir8:i,,bi",sc 2er72 (Bo3)7e1-e7oo Fax(803) 7s1-s'111 www.shearyrab.com
I
Page: 17 of40
Lelrel 1 Rgport v2.l
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-007
Description: HMSMW-4S Matrix: Aqueous
Date Sampled: 1 1 11 412013 1640
Date Received : 1 1 l1 512013
Volatile Orqanic Compounds bv GC/MS
I
I
IBatch
34894
Run
1
Prep Method
50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11t21t2013 0125 PMM2
Parameter
CAS Analytical
Number ltarhod Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1 330-20-7
Run I AcceptanceA 06 Recovery Limits
82608
82608
82608
82608
82608
82608
82608
8260B
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
ND
ND
ND
ND
ND
ND
ND
ND
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
I
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
ToluenedB
108
106
98
70-130
70-130
70-130
t
I
I
I
I
t
t
I
I
I
PCIL = Practical quantitatim limit B = Datected in the method blank E = Quantiiation of compound exc6eded the calibration ran96
ND = Not detocted at or above the PQL J = Estimated result < PQL and: MDL P = The RPD betw€€n two GC columns exco€ds 40%
Whoro applicabls, all soil sample analysis are reported on a dry weight basis unless f,aggod with a "w"
H = Out of holding time
N = Recovery is out of criteria I
Shealy Environmental Services, lnc.
106VantagePointDrive W€stColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 1E of40
L6rcl I Report v2.1 I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD:OK15049-008
Description: HMSMW-4I Matrix: Aqueous
Date Sampled : 11 11 412013 1320
Date Received : 11 l1 512013
Volatile Organic Compounds by GC/MSIRun Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch82608 1 ',11t21t2013 0148 PMM2 34894
Parameter
cAs
Number
Analytical
Marhod Result Ot
r Bromodichloromethane
I BromoformI Bromomethane (Methyl bromide)
2-Butanone (MEK)I :::i::ffi::t;,,."
Chlorobenzene
I :lilil:fl,"(Methy,ch,oride)
Cyclohexane
I l;i;llllffi,lilffii"pane
(DBCP)
1,2-Dibromoethane (EDB)
1 .2-Dichlorobenzene
I 1.3-Dichlorobenzene
I 1,4-Dichlorobenzene
Dichlorodifl uoromethaneI l:l3iillslllllll3r 1,1-Dichloroethene
cis-1.2-DichloroetheneI H;hi;?:I"H::,'"*
cis-1,3-Dichloropropene
t iil"l.*l+foro,ro,ene
lsooroovlbenzene
I il:HitTfi"but,ether(MrBE)
4-Methyl-2-pentanone
a Methvlcvclohexane
I uettrvtene chloriderstyrene
1, 1,2,2 -T etnchloroethan e
I
Tetrachloroethene
I
Acetone
Benzene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-s0-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
1 00-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
1 00-42-5
79-34-5
127-18-4
108-88-3
8260B
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
8260B
82608
8260B
82608
82608
8260B
82608
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ri,g/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L I
ug/L 1
ug/L 1
ug/L 'lug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ugr/L 1
uSlL 1
ug/L 1
ug/L 1
uglL 'l
ug/L 'l
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
82608
82608
8260B
82608
8260B
82608
8260B
82608
8260B
8260B
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
I PQL = Practical quantitation limit B = Dstectod in the msthod blank E = Quantitation of compound exc66ded the callbration range H = Out of holding time
ND = Notdotected atorabov6lhe PCIL J = Estimatod result< PQLand: MDL P = Ths RPD botw€en lwo GC columns excseds 40olo N = Rocoveryis outofcriteria
Where applicablo, all soil samplo analysis are roportod on a dry w€ight basis unl€ss flagged with a 'W.
Shealy Environmental Services, lnc.
f, tOO Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.comI Page: 19 of 't0Levol I Roportv2.1
I
Client:Terracon Consultants, lnc. Laboratory lD: OK15049-008
Description: HMSMW-4| Matrix: Aqueous
Date Sampled : 1 1 I 1 412013 1 320
Date Received : 11 11 512013
Volatile Organic Compounds by GC/MS
I
I
IBatch
348S4
Run
1
Prep Method
50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11121120130148 PMM2
Parameter
CAS AnalyticalNumber Method Result O Run
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 ,1 , 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-s
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
I
t
I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1ug/L 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
109
107
100
70-1 30
70-1 30
70-1 30
t
I
t
I
I
I
I
I
t
I
PQL = Praclical quantitation limit B = Detocted in ihe m€thod blank E = Quantitation of compound ilcssdod the €libration range
ND = Not det6cl6d at or above the PCIL J = Estimated result < PQL and: MDL P = The RPD b€tweon two GC columns exceeds 40%
Where applicable, all soil sample analy€is are reported on a dry w€ight basis unlsss flagged with a 'W"
H = Out of holding time
N = Rocovery is out of cdteria I
Sh6aly Environmental Sorvices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:20 of40
Lev6l 1 Report v2.1 I
t
t
I
Client: Terracon Consultants, lnc.
Description: RINSE BLANK
Date Sampled:1 1 11 412013 17 45
Date Received : 1 1 l1 512013
Laboratory lD: OK1 5049-009
Matrix: Aqueous
Volatile Orqanic Compounds bv GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82608 1 1',U20t2013 2136 PMM2 34894
Parameter
CAS
Number
Analytical
Mathnd Result O Units Run
T
T
t
I
I
I
I
I
I
I
I
I
t
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
'l ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichlorcpropane
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Sgrene
1, 1,2,2 -T elr achloroetha n e
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-s
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
't 006't -02-6
1 00-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-l
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
POL = Practical quantitation limit B = D€tgcted in tho mothod blank E = Quantitation of compound oxco€d8d $o celibration range H = Out of holding time
ND = Not d8tected al orabove tha PQL J = Estimated rosult< PQL and: MDL P = The RPD between two GC columns exceeds 40olo N = Rocovsryisoutofcliteda
Where applicable, all soil sample analysis are reported on a dry w€ight basis unless flagged with a "W"
Sh€aly Environmental S€rvices, lnc.
I
l06VantaSePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
I
Page:21 of40
Level 'l Report v2.l
Client: Terracon Gonsultants, lnc.
Description: RINSE BLANK
Date Sampled:11 11412013 17 45
Date Received : 11 11512013
Laboratory lD: OK1 5049-009
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
I
I
IBatch
34894
Run
1
Prep Method
50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 11120120132136 PMM2
Parameter
CAS Analytical
Number Mathad Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1, 1,1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (totial)
Surrogate
76-13-'l
120-82-1
71-55-6
79-00-s
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
t
I
I
ug/L 1
ug/L 1
ug/L I
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
'1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
t
I
I
I
I
I
I
I
I
I
98
106
98
70-130
70-130
70-130
PQL = Practical quantitalion limil B = Dotocted in tho mothod blank E = Quantitation of compound exc€€ded ths calibration range
ND = Not deteclod at or above the PQL J = Estimated rosult < PQL and: MDL P = The RPD betw€on two GC columns exceeds 40olo
Wh6ro applicable, all soil sample analysis are rsported on a dry wEight basis unl€ss flagged with a nV'
H = Out of holding tima
N = Recovery is out of caiteria I
Shealy Environmental Servic€s, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Paget 22 ot 40
Lovol I Roport v2.1 I
I
I
I
Client: Terracon Consultants, lnc.
Description: HMSMW-4D
Date Sampled:1 1 11 412013 1325
Date Received : 1 1 l1 512013
Laboratory lD: OK1 5049-01 0
Matrix: Aqueous
Volatile Orqanic Compounds by GC/MS
Batch
34894IRun Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 1',U2112013 0210 PMM2
Parameter
cAs
Number
Analytical
Marhart Result OI
I
I
I
I
I
I
I
I
t
t
I
I
I
T
I
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
't0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uorom ethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
'l ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,&Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Sgrene
1,1,2,2-T etrachloroethan e
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-s
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-'t2-8
124-48-1
1 06-93-4
95-50-1
54',t-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
't 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02.6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
't27-18-4
1 08-88-3
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1ug/L 1ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 'l
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L I
ug/L 1
ug/L 1ug/L 1ug/L 1
PQL - Practical quaniitation limil B = Deteted in the method blank E = Quantitation of compound exc6sd6d the calibraiion range H = Out of holding tlms
ND = Notdotected atorabovethe PQL J = Estimated result< PQLand: MDL P = The RPD between two GC columns exceeds 40olo N = Recoveryis outofcritBria
Where applicable, all soil sample analysis are reportod on a dry wtsight basis unless flagged with a nV"
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 23 of ,10
Levol I R6portv2.1
Client: Terracon Consultants, lnc.
Description: HMSMW-4D
Date Sam pled : 1 1 I 1 41201 3'1325
Date Received : 1 1 l1 512013
Laboratory lD: OK1 5049-01 0
Matrix: Aqueous
Volatile Orqanic Compounds by GC/MS
I
t
IBatch
34894
Run
1
Prep Method
50308
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 1112',1120130210 PMM2
Parameter
CAS Analytical
Numbar Mathad Result O
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 , 1 ,1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1 330-20-7
Run I AcceptanceO % Recovery Llmlts
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
I
I
I
ug/L 'l
ug/L 1
ug/L 'l
ug/L 'l
ug/L 1
ug/L 1
ug/L I
ug/L 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
106
101
97
70-130
70-1 30
70-130
I
I
I
I
I
I
I
I
I
I
PQL = Practical quantitation limit B = D€tected in the method blank E = Quantitation of compound exceeded th€ calibration rangs
ND = Not detoctod at or above the PQL J = Estimaled r€6ult < PQL and: MDL P = Ths RPD betwoen two GC columns sxceeds 40olo
Where applicable, all soil sampl€ analysis are reported on a dry woight basis unless iagged with a "W"
H = Out of holding timo
N = Rscovory is out of crltsria I
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 2'l of 40
Lewl 1 Reportvz.l I
I
I
I
Client: Terracon Consultants, Inc.
Description: TRIP BLANK
Date Sampled:1'l 11 412013
Date Received : 1 1 11 512013
Laboratory lD: OK15049-01 1
Matrix: Aqueous
Volatile Orsanic Compounds by GC/MS
Run Prep Method1 50308
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 ',t1t20t20132159 PMM2
Batch
34894
Parameter
cAs
Number
Analytical
Marhod Result O
t
T
I
I
I
t
t
t
I
I
I
I
I
I
I
I
T
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
s.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropen6
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-f elrachloroethan e
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
1',10-82-7
96-12-8
't24-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
15660-5
78-87-5
't0061-01-5
1 0061 -02-6
10041-4
591-78-6
98-82-8
79-20-9
't634-04-4
1 08-1 0-1
108-87-2
75-09-2
10042-5
79-34-5
127-18-4
1 08-88-3
82608
82608
82608
8260B
8260B
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
PQL = Practical quantitation limil B = D€tectsd in the method blank E = Quantitation of compound excseded ths calibrauon range H = Out of holding tlre
ND = Not detected atorabovs the PCIL J = Estimated rosult< PQL and: MDL P = The RPD between two GC columns exc€eds 40% N = Recoveryisoutofctiteria
Where applicable, all soil sample analysis ar6 reported on a dry w€ight basis unless flagged with a 'w"
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 25 of '00Lev6l 1 Roportv2.l
Client: Terracon Consultants, lnc.
Description: TRIP BLANK
Date Sampled:1 1 l1 412013
Date Received :'l 1 l1 512013
Laboratory lD: OKl 5049-01 1
Matrix: Aqueous
Volatile Orqanic Compounds by GG/MS
I
I
IBatch
34894
Run Prep Method't 50308
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 11120120132159 PMM2
Parameter
CAS Analytica!
Number Mathnd Result O PQL
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 , 1 , 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-s
79-01-6
75-69-4
75-014
1 330-20-7
Run I AcceptanceO % Recovery Limits
82608
82608
8260B
82608
82608
82608
8260B
82608
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
I
I
I
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1ug/L 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
101
107
98
7G130
70-130
70-130
I
I
I
I
t
I
I
I
I
I
PQL = Practical quantitation limit B = Detoctsd in lhe meihod blank E = Quantitation of compound exc€€ded tho calibralion range
NO = Not detacted at or above the PQL J = Estimated r€sull < PQL and: MDL P = Tho RPD bstwB€n two GC columns excseds ,10%
Wh6re applicablo, all soil sampls analysis are reporled on a dry w€ight basis unlsss flagged with a 'vt'
H = Out of holding time
N = Rocovery is out of critofla I
Shealy Envionmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 26 of ttO
LEvol 1 Report v2.1 I
t
QC Summary
Shealy Environmental Services, lnc. Page: ? of tO
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Lowl I Reportv2"l
IVolatile Organic Compounds by GC/MS - MB
Sample lD: OQ34894-001
Batch:34894
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Parameter tDil PQL Units Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uorom6thane
1 ,2-Dichloroethane
1 , 1-Dichloroethane
cis-1,2-Dichloroethene
1 ,1-Dichloroethene
trans-1, 2-Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-'1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etrachloroethane
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 , 1 ,1 -Trichloroethane
1, 1,2-Trichloroethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
1112012013 2112
11120120132112
11t20t20132112
11120120132'112
111201201321',!2
11120t20',t32112
11120120132'.t12
11120120132112
11120120132112
11120120132112
11120120132112
't1t20120132112
11120120132112
11t20t20132112
11120120132112
11120120132112
11t20t20132112
11120t20132112
11120t20132112
11120120132112
11120120132112
11120t201321',12
1'1120120132112
11t20120132112
11120120132112
11120t2013 2'.t'.tz
11t20120132112
11120120't32112
11120120132112
11t20t20132112
11D0t20132112
11120120132112
11120120132112
11120120132112
11t20t20132112
11120120132112
11t20t20132112
11t20t20132112
11t20t20132112
11t20t20132112
11120t20132112
11120120132112
't'U20t20132112
11t201201321',12
I
I
I
I
I
I
t
I
I
I
I
I
I
PQL = Practical quantitatim limit
ND = Not dotected at or abovo tho PQL
P = The RPD botwssn two GC columns sxGeds 40oi N = Re@very is out of crit€ria
J = Estimated result < PQL and: MDL + = RPD is out of criteria I
IWher€ applicable, all soil samplo anallsis arg reported on a dry weight basis unloss flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors ln calculated results
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 28 of 40
Level I Rsportv2.l
I
t Volatile Organic Compounds by GC/MS - MB
t
sample lD: oe348e4-oo.l
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I Parameter Result O Dil PQL Units Analysis Date
Trichloroethene
I Trichlorofluoromethane
I Vinyl chloride
Xylenes (total)
ND
ND
ND
5.0
5.0
2.O
5.0
ug/L 11120120132112
ug/L 11120120132112
ug/L 1112012013 2112
ug/L 1112012013 2112
I Surrogate
ND1
AcceptanceO % Rec Lihit
Bromofluorobenzene
I l;1;'#lI**"'
I
t
T
I
I
I
I
t
I
I
108 70-130
104 70-130
101 70-130
I
t
PQL = Practical quantitation limit P = The RPD b€twesn two GC columns exceeds 40% N = Rscovsry is out ofcriteria
ND = Notdgtsctod atorabovothe PQL J = Estimated result < PQLand > MDL + = RPD is out ofcriteria
Wh6r6 applicable, all soil sampls analysis ars reported on a dry w€ight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:29 of ,(0
L€vol 1 Report v2. l
I
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: Oe34894-002
Batch:34894
Analvtical Method: 82609
Matrix: Aqueous
Prep Method: 50308 I
Spike
Amount
(ug/L)
Result
(ug/L)
% Rec
Dil % Rec Limit Analysis Date IParametero
Acetone 100
Benzene 50
Bromodichloromethane 50
Bromoform 50
Bromomethane (Methyl bromide) 50
2-Butanone (MEK) 100
Carbon disulfide 50
Carbon tetrachloride 50
Chlorobenzene 50
Chloroethane 50
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1,2-Dibromo-3-chloropropane(DBCP) 50
Dibromochloromethane 50
'1,2-Dibromoethane (EDB) 50
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethane
cis-1,2-Dichloroethene
1 ,'l -Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T elnchloroeth a n e
Tetrachloroethene
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50Toluene 50
'1,1,2-Trichloro-1,2,2-Trifluoroethane 501,2,4-Trichlorobenzene 50
1,1, 1-Trichloroethane
'1,1,2-Trichloroethane
t
I
t
I
I
I
t
I
I
I
I
t
I
50
50
100
49
51
52
47
88
50
53
48
48
49
54
52
51
52
48
50
49
50
62
54
49
48
48
48
48
51
50
51
95
50
50
50
100
52
49
51
49
47
49
47
49
50
45
102
97
103
103
95
88
99
106
97
97
99
108
103
102
103
95
99
98
100
124
107
98
96
96
95
95
102
100
102
95
100
101
99
103
103
97
101
98
94
98
93
99
101
90
60-140
70-1 30
70-1 30
70-l 30
60-140
60-140
60-140
70-130
70-130
42-163
70-130
60-140
70-130
70-130
7G.130
70-130
70..130
70-1 30
70-1 30
60-140
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
60-140
70-130
70-130
70-130
60-140
70-1 30
70-1 30
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
1',U20t20131940
11120120131940
11t2012013 1940
11120120131940
11t20120131940
11t20120131940
11120120131940
11t2012013 1940
11120120131940
't1t20120131940
11120t2013 1940
11120120131940
11t20t20131940
11t20t20'131940
11120120131940
11120120131940
11120120131940
11t20t20131940
11120120131940
11t20t20131940
11n0t2013 1940
1112012013 1940
11120120131940
11t2012013 1940
'11t20t20131940
11120t20131940
1112012013 1940
11120t20131940
11120120't31940
11t20t20131940
11t20120't31940
11120120131940
1112012013 1940
11120t20131940
11120120131940
fin0t2013't940
11120t20131940
11t2012013'.1940
11120t20131940
11120120131940
11120t20131940
11120120131940
1'.U20t20131940
11nO12013 1940
PCIL = Practic€l quantitation limit
ND = Not datsted at or above th6 POL
P = The RPD b6twe6n two GC columns oxceeds /tO% N = Rocovery is out of caiteria
J = Estimated rosult < PQL and : MDL + = RPD is out of criteria t
IWhers applicablo, all soil sampls analysis are reported on a dry weight basis unless flagged with a "w"
Note: Calculations are performed before rounding to ayoid round.off errors in calculated resultg
Shealy Envircnmental Services, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 30 of40
L6wl 1 Roport v2.t
I
I Volatile Organic Compounds by GC/MS - LCS
I '"':':,:?:ffino-oo'
Analytical Method: 82608
Matrixi Aqueous
Prep Method: 50308
I ^tJ::",, Resurr % Rec
Parameter (us/L) (us/L) O Dil % Rec Limit Analysis Date
I llili:frli;:n*"""
Xylenes (total)
50 47
50 56
50 53
100 100
AcceptanceO % Rec Lihir
1
1
1
1
94 70-130 11t20t20131940
112 70-130 11t20t2013 1940
107 70-130 11120120131940'r03 70-130 1112012013 1940
I sr,,og"t"
Bromofluorobenzene 109 70-130
I l;1;?,"lllX"**" ',i: ;:.l::
I
t
I
I
I
I
I
I
I
I
I
t
PQL = Practical quantitatlon llmit P = The RPD b€tu€en two GC columns exceeds 40% N = Recovery is out of critsria
ND = Not deteclod at or above the PQL J = Estimated result < PQL and: MDL + = RPD is out of criteria
Where applicable, all soil sample analysis ar6 reporlod on a dty woight basis unless flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:31 of40
Levol 1 ReportY2.l
I
IVolatile Organic Compounds by GC/MS - LCSD
Sample lD: 9q34994-693
Batch:34894
Analvtical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
SpikeAmount Result % Rec % RPD(uq/L) (us/L) O Dil % Rec % RPD Limit Limit Analysis Date IParameter
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
100
50
50
50
50
100
50
50
50
50
100
47
48
51
49
96
48
52
48
49
49
51
51
51
51
48
49
48
49
61
54
49
46
45
46
46
50
48
49
100
49
51
49
100
48
50
50
48
48
47
46
47
51
47
105
95
96
101
97
96
97
104
96
97
99
102
102
102
102
97
99
96
99
121
108
98
92
90
93
92
100
96
98
101
98
102
98
102
96
101
99
96
96
95
92
95
10'l
94
2.6 60-140 20 1',U20120132002
2,8 70-130 20 11t20t20132002
6.2 70-130 20 11t20t20132002
1.9 70-130 20 11t20t20132002
2.5 60-140 20 11120t20132002
8.7 60-140 20 11120120132002
2.4 60-140 20 111201201320021.6 70-130 20 11D0t20132002
1.4 70-130 20 11120t20'.t32002
0.46 42J163 20 '.11t20t20132002
0.041 70-130 20 11t20t20132002
5.6 60-140 20 11120t201320021.5 70-130 20 11120t20132002
0.082 70-130 20 11t20t20132002
0.8s 70-130 20 11t201201320021.4 70-130 20 11t20120132002
0.39 70-130 20 11t20120132002
1.3 70-130 20 11120120132002
1.2 70-130 20 11t20120',t3 2002
2.2 60-140 20 11120t20132002
0.18 70-130 20 1',U20120132002
0.51 7G,130 20 ',t1t20t20132002
4.0 70-130 20 111201201320026.3 70-130 20 11120120132002
2.8 70-130 20 11t20120132002
3.2 70-130 20 11t20120132002
1.7 70-130 20 11t20120132002
4.1 70-130 20 11t20120132002
3.6 70-130 20 11t20t20132002
s.5 60-140 20 11120120132002
2.3 70-130 20 1'.120t201320021.1 70-130 20 11120120132002
0.96 70-130 20 11120120132002
0.70 60-140 20 11120120132002
7.0 70-130 20 11120t20132002
3.6 70-130 20 11120t20132002
1.8 70-130 20 11t20t201320021.3 70-130 20 11120120132002
2.3 70-130 20 11120120132002
3.4 70-130 20 11120t20132002
1.8 70-130 20 11t20120'.t32002
3.8 70-130 20 11120120132002
0.39 70-130 20 11120120132002
3.5 70-130 20 11120t20132002
I
t
I
I
I
T
I
I
I
I
I
I
I
Chloroform 50
Chloromethane (Methyl chloride) 50
Cyclohexane 50
1,2-Dibromo-3-chloropropane(DBCP) 50
Dibromochloromethane 50
1,2-Dibromoethane (EDB) 50
I,3-Dichlorobenzene 50
I,4-Dichlorobenzene 50
1,2-Dichlorobenzene 50
Dichlorodifluoromethane 50
l,2-Dichloroethane 50
1,'l-Dichloroethane 50
cis-1,2-Dichloroethene 50
1,1-Dichloroethene 50
trans-1,2-Dichloroethene 50
1,2-Dichloropropane 50
trans-1,3-Dichloropropene 50
cis-1,3-Dichloropropene 50
Ethylbenzene 50
2.:Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-'l elrachloroeth a ne
Tetrachloroethene
Toluene
100
50
50
50
100
50
50
50
50
50
50
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane 50
1.2.4-Trichlorobenzene 50
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
50
50
PQL = Practical quantitation limit
ND = Not dotectod at or above ths PQL
P = Ths RPD bstweon two GC columns oxceeds 40% N = Recovery is out of criteria
J = Estimated result < PQL and : MDL + = RPD is out of criteria I
Iwhare applicabla, all soil sample analysis are reported on a dry woight basis unless flagg€d with a nv"
Note: Calculations are performed before rounding to avoid round-off errors in calculated resulG
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 32 of40
Lsvel 1 Ropod v2.1 I
I Volatile Organic Compounds by GC/MS - LCSD
I Sample lD: OQ34B94-OO3
I Barcn:348e4
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^t#1"", Resutr % Rec % RPD
- Parameter (us/L) (us/L) O Dil % Rec % RPD Limit Limit Analysis Date
Trichloroethene
f Trichlorofluoromethane
I Vinyl chloride
Xylenes (total)
50 45
50 52
50 54
100 100
AcceptanceO % Rec Lihit
1 90 4.5 70-130 20 11120120132002
1 104 6.8 70-130 20 11120120132002
1 108 1.2 70-130 20 11120120132002
1 101 2.8 70-130 20 11120120132002
t Surrogate
Bromofluorobenzene
I i;.,:::lr"**"'
I
I
I
I
I
I
I
I
t
I
104 70-130
99 70-130
100 70-130
I
I
PQL = Practical quantitation limit P = The RPD between two GC columns exceods 40% N = Rocovery is out of critoria
ND = Not dotectsd at or above the POL J = Estimatod result < PQL and: MDL + = RPD is out of critoria
Whsre applicable, all soil sampls anal!6is are reported on a dry w€ight basis unless flaggsd with a 'W"
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 33 of40
Lev6l l RoDortv2.l
I
IVolatile Organic Compounds by GC/MS - Duplicate
Sample lD: OK15049-001 DU
Batch:34894
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Sample
Amount
(ug/L)
Result
(us/L)
% RPD
Dil o/o RPD Limit Analysis Date IParametero
1,2-Dibromo-3-chloropropane(DBCP) ND
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,3-Dichlorobenzene
I ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,'l -Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloioethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T etnchloroeth a n e
Tetrachloroethene
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.O
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
6.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
8.6
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
11121t2013 0431
1112112013 0431
1112112013 0431
11121t2013043'.1
1112',v2013 0431
11t21t20130431
11t21t2013 0431
11121120130431
1112112013 0431
11t21t20130431
11t21120130431
11t21t20',t30431
11121120130431
11t21t20',t3 043',1
11121120130431
11t21120130431
11121120130431
1112',120130431
11t21120130431
11t2'.U20130431
11121120130431
1112112013 0431
11n1t20130431
11t21t20130431
11121120130431
11121120130431
11t21t20'.t30431
11121120130431
11121120130431
1112112013 0431
11121120130431
11121t20130431
1112',v20130431
11121t20130431
11t2'.U20130431
'11121120130431
11t2112013043',1
11121120130431
11t21t20130431
11t21120130431
11121t20130431
11121120130431
11121120130431
11121120130431
I
I
t
I
t
I
I
I
I
I
I
t
I
1,1,2-Trichloro-1,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene
1,1,'t -Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
PCIL = Practical quantitation limit
ND = Not detectod at or above the PQL
P = ThE RPD bstwe€n two GC columns exceeds 40olo N = R6@very is out of critaria
J = Estimatod r6ult < PCIL and: MDL + = RPD is out of criteria I
IWherE applicablo, all soll sampls analysis ar6 reportod on a dry w€ight basis unless flaggsd with a "vW
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9'111 www.shealylab.com
Page: 34 of40
Lovel 1 Rooortv2,l
I
t Volatile Organic Compounds by GC/MS - Duplicate
I '"-:':,In:ffion-oo'o'
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
t iffif, Resurr % RPDParameter (uE/L) (uE/L) O Dil % RPD Limit Analysis Dater l:::li::ff[:H",,."""
I Vinyl chloride
Xylenes (total)
ND ND
ND ND
ND ND
ND ND
AcceptanceO % Rec Lihit
1
1
1
1
0.00 20 1112112013 0431
0.00 20 1112112013 0431
0.00 20 1112112013 0431
0.00 20 11121120130431
I surrosate
1 ,2-Dichloroethane-d4 1 10 70-1 30
I ::",1:::;;0"""'" g 1l-]ll
t
I
I
I
T
I
I
I
I
I
I
I
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Notdetected atoraboveth6 PQL J = Estimated result< PQLand: MDL + = RPD is outofcriteria
Where applicable, all soil samplo anal)rsis are Fported on a dry weight basis unless flagged wilh a "w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page:35 of ,10
Lovel 1 Roportv2.l
t
IVolatile Organic Compounds by GC/MS - MS
Sample lD: OK15049-002MS
Batch:34894
Analvtical Method: 82608
Matrix: Aqueous
Prep Method: 50308 I
Sample
Amount(uq/L)
Spike
Amount
(us/L)
Result
(us/L)
% Rec
Dit % Rec Limit Analysis Date IParametela
'1,2-Dibromo-3-chloropropane(DBCP) ND
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-T etr achl oroeth an e
Tetrachloroethene
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
50
50
50
50
93
51
55
53
49
90
54
64
50
51
68
64
61
47
54
48
48
50
50
74
55
64
52
50
50
50
51
52
51
110
52
53
52
't10
51
51
51
47
50
52
51
48
60
45
93
102
110
106
98
90
109
128
99
103
113
129
123
95
107
97
97
100
99
148
110
127
103
100
100
100
101
105
102
106
104
106
104
111
102
103
101
93
99
105
101
96
120
90
I
I
I
I
I
I
I
T
I
t
I
I
t
ND
ND
ND
60-140 1'.U21t20130541
70-130 11t21t20130541
71-143 11t2112013 0541
65-131 11t21t20130541
36-168 11121120130541
60-140 11121t20'.t30541
60-140 11121120130541
37-166 1112'.U2013054',1
78-129 11t21t20130541
60-140 11t21120130s41
63-123 11121120130541
20-158 11t21t20130541
70-130 11t21t20130541
70-130 1'.U21120130541
74-134 11t21t20130s41
70-130 11121120130541
70-130 1112112013 0541
70-130 11t21t20130541
70-130 11121t20130541
10-1s8 11t21120130541
69-132 11D112013 054',1
70-130 11121120130541
50-132 11121120130541
70-130 11121t20130541
70-130 11t21t2013 0541
71-126 11121t20130541
69-130 1112',U20130541
73-131 11t21120',t30541
70-130 11121120130541
60-140'.11t21t2013054'.1
70-130 11t2112013 0541
15-128 1112'.il20130541
70-130 11t2112013 0541
60-140 11121120130541
70-130 11t21t20130541
69-129 11t21t20130541
70-'t30 11t21120',130541
60-155 11121t20'.t30541
70-130 1'.U21t20130541
70-130 11121120130541
70-130 11121120130541
70-130 11121120130541
77-132 11121t2013 0541
77-132 11121120130541
1 ,1 ,2-Trichloro-1 ,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
PQL = Praclicalquantitation limil
ND = Not detEcted at or above the POL
P = The RPD betre€n two GC columns oxcsods 40olo N = Racovery is out of criteria
J = Eslimated result < PQL and 2 MDL + = RPD is out ot clitsria t
IWhoro applicable, all soil sample anal),sis ars roporlod on a dry waight basis unless flagged with a "u/'
Note: Calculations are performed before rounding to avoid round-ofr errors in calculated results
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 36 of40
Lovel I Report v2.1
I
T Volatile Organic Gompounds by GCIMS - MS
I '"':':,:?,ffi'n-oo"'
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I SamPle SPike
I Amount Amount Result % Recr Parameter (ug/L) (ug/L) (us/L) A Dit % Rec Limit Analysis Date
Trichloroethene
f Trichlorofluoromethane
I Vinyl chloride
Xylenes (total)
ND 50 51
ND 50 63
ND 50 60
ND 100 100
AcceptanceO % Rec Lihit
1 102 73-124 1112112013 0541
't 125 60-140 ',t112112013 0541
1 1',19 29-159 1112112013 0541
1 104 70-130 11121120'.130541
I Surrogate
1,2-Dichloroethane-d4
I ;:"#;::;'""'"""
I
T
I
I
t
I
T
T
T
I
1 10 70-130
106 70-130
98 70-130
t
I
PQL = Practical quantiiation limit P = The RPD betwesn two GC columns 6x@eds 40% N = Recovery is out of criteria
ND = Not detected atorabovsthe PQL J = Estimated result< PQL and: MDL + = RPD is out ofcriteria
Wh6r€ applicable, all soil samplo analysis are rsported on a dry weight basis unless flagged with a'W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Sh€aly Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803) 79'l-9111 www.shealylab.com
Page: 37 of40
Level 1 Report v2.l
I
Volatile Organic Compounds by GC/MS - MB
Sample lD: 9q34912-gg1
Batch:34912
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I
I
I
I
I
o Analysis DateUnitsParameter
Chloroethane
Surrogate
ug/L5.0ND
o
1
Acceptance
Limit
11t21t20130028
% Rec
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
111
115
101
70-130
70-l 30
70-130
I
I
I
I
I
I
I
I
I
I
t
IPQL = ftacucalquantitation limit
ND = Not d6tect6d at or abov6 the PQL
P = Ths RPD between two GC columns sxc€eds rlooi6 N . Recovory is oul of criteria
J = Estimated rosult < PQL and i MDL + = RPD is out of crit8ria
Where applicable, all soil sample analysis are roportod on a dry w€ight basis unless flagged with a "w"
Note: Calculations are performed before rounding to avold round-off errors in calculated results tShealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 38 of40
Level I Report v2.1
I
I Volatile Organic Compounds by GC/MS - LCS
I t"r':,:?:oe34e12-oo2
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308
I ^tJI"n, Resurt % RecParameter (uE/L) (uq/L) O Dit % Rec Limit Analysis Date
I ::[::""
50 53
AcceptanceO % Rec Lihit
106 42-163 11120t20132248
Bromofluorobenzene 120 70-130
I 1.2-Dichloroethane-d4 log 70-130
I Toluene-d8 105 70-130
t
I
I
I
I
t
I
I
I
I
I
I PQL = Practical quantitation limit P = Th6 RPD betw€en two GC columns exceeds 407o N = Recovery is out ofcriteria
ND = Notdetscted atorabove the PQL J = Estimaied result< PQL and: MDL + = RPD is out ofcriteria
Whers applicablo, all soil sample analysis are reported on a dry weight basis unless flagged with a 'w'
Note: Calculations are performed before rounding to ayoid round-offerrors in calculated resulGt
I
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 39 of40
Level I Rsportv2.'l
tVolatile Organic Compounds by GC/MS - LCSD
Sample lD: OQ34912-003
Batch:34912
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 T
SpikeAmount Result(uE/L) (us/L)
% Rec
% Rec % RPD Limit
% RPDLimit Analysis Date IParameter
Chloroethane
Surrogate
51
Acceotance
% Rec Li,init
4.3 42-163 11t20t20132318 I50
a
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
125
113
109
70-130
70-1 30
70-1 30 I
I
I
I
I
I
I
I
I
I
I
T
PQL = Practical quanlitation limit
ND = Not detoctod at or abovs lhe POL
P = The RPD b€twson two GC columns excaeds 40% N = Recovsry is out ofcriteria
J = Estimatod rssult < PQL and i MDL + = RPD is out of critaria t
IWher6 applicable, all soil samplo analysis ars raportod on a dry wsight basis unless flagged with a "W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 (8O3)791-9700 Fax[phone] www.shealylab.com
Page: 40 of ,00
Lsvel 1 RoDortv2.l
I
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l06 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level I Reportv2.'l
-SHEALY ENVIRONMENTAL SERVICES, INC.
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Ycr -l No il Did all corlrfutrs arrivc in 6'rnd onnditim {unbrolccn" lids oo" as.}?
Yes t2.'Was volume ar,eilablc?
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comes frrfr?
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viahi?
puumtl"'pca-siza" (l{'"oi 6mm in diarnctcrl in any }-f)A
Yes Io NA I 7. lft'crs all mdalnr(}&fi { lljltl,'nutricat samples receivcd ut a pH of ":2?Yes i No NA Were all cystridg anrfu'u rulfide samplce rcccivcd at a DH .*,12?
Ycs fl , N. []I
NAA 19. Were all applisablc )rrH3rTKNtcyanidcghcnol (.$ 2mg,/f-) 5arrTles frcc of
lsgidrrql chlorine?
Yac J No L"l I IIA t4 I
i, n i"^ n"=l
-Jtl. Wcrc mlledior tettpaa(urgr drxumcnted on thc (:OC for I:C r.tuples?
Yts fJ ll - Wcre client remar*at'rorytsts (i.e" roquc$red tlilulimc, MS,IvISD desigaationr,_ etc, ,.) corrEctly iranmr'ihed lium thc COC into the oou.meu scc{iotr iu I.IMS?
acccrrdiagly rn srrurplc rwci6tr* *r*0I?SOI,IINO:.HCI,NaO[I) n'rth t&s SR # (nrunbcri
$ample(s) -- - -. * . tttrs rc.cqiye$ rrith hubbleg ?{ '- iu di.mstcf.Sornple(s) - - -_s,cng rce.civcd q'ith TRC >0 2 mg& for Nlf3r,TK!'Iicyani4o'plenol _.*-- ..
Smrole lahels t'erified bv:Lt \,\I- narer i, " rr -r-t
Yee fl I*o tl
Lovol 1 Rooort v2.1
Shealy Environmental Services, lnc.
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