9606_WayneCountyMSWLF_GWAssessment_DIN27648_20170310

Wayne County Subtitle D Lined MSWLF
Dudley, North Carolina
March 2017
MESCO Project Number: G16016.0
Groundwater Quality Assessment Near MW-13
Prepared for
Municipal Engineering Services Company, P.A.
Garner and Boone, North Carolina
P.O. Box 97
Garner, NC 27529
License No. C-0281

Permit Number: 96-06
March 10, 2017
Ms. Jaclynne Drummond Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality
2090 US 70 Highway
Swannanoa, NC 28778
Re: Groundwater Quality Assessment Near MW-13
Wayne County Subtitle D Lined MSWLF, Phase 2
Permit No. 96-06 MESCO Project No. G16016.0

Dear Mr. Drummond,
Introduction
On behalf of Wayne County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Groundwater Quality Assessment Near MW-13 for the Wayne County Subtitle D Lined Phase 2 Municipal Solid
Waste Landfill (MSWLF). This brief report characterizes the hydrogeology, groundwater quality, landfill gas
(LFG) conditions and the corrective actions implemented in the area monitored by MW-13 which has previously
been impacted by levels of benzene above NC 2L Groundwater Standards. Most recent laboratory results indicate
that benzene is below the 2L Standard at MW-13 and at three other proximal locations within the compliance
boundary. Corrective actions in the form of LFG migration mitigation has recently been initiated to restore
groundwater quality. We respectfully request that since levels of benzene have decreased to allowable levels and
corrective actions have been implemented that no further action be required at this time. Assessment monitoring
will continue which will include landfill gas monitoring proximal to MW-13. If concentrations of contaminant(s)
are detected in MW-13 above 2L Standards in a future compliance event an assessment work plan will be
developed.
Site Background
The Wayne County Subtitle D lined MSWLF, permit #96-06, is located at 460B South Landfill Road, Dudley, North
Carolina. The site location topographic map is depicted in the attached Figure 1. The lined MSWLF is comprised
of contiguous Phase 1&2 which are inactive and an active Phase 3 which are treated as a single unit for reporting
purposes. A potentiometric map of the landfill constructed from groundwater elevation data for the uppermost
aquifer recorded during a recent event is shown on Figure 2. An annotated aerial photograph of the MW-13 area is
shown on Figure 3. An unlined closed landfill and active construction and demolition landfill, permit #96-01, is
located on the same contiguous property but is monitored separately and is not the subject of this report.

Hydrogeology
MW-13 is the well impacted by the aromatic volatile organic compound (VOC) benzene. MW-13 was installed as a
Type II well at a depth of approximately 16 feet below ground surface (bgs) that bisects the water table. An
additional two wells are in place and a hand auger boring was advanced around MW-13 to delineate the horizontal
extent of contamination. The lithology was generally consistent among the borings in the MW-13 area which
consisted of a less permeable cohesive silty clay layer in the vadose with silty sand above and below.
Hydrogeologic studies previously performed at this site determined that an unnamed coastal plain sediments overlie
the upper Cretaceous Black Creek Formation. This formation has a low permeability and is believed to act as a lower
confining layer. The confining layer was identified at approximately 112 ft amsl or approximately 19 feet below the
bottom of MW-13 and dips southwesterly in the direction of groundwater flow towards Edward's Branch. Details of
the additional assessment borings are detailed in the groundwater section below with logs and records in Appendix
A.
Based on the horizontal hydraulic gradients and the permeability of the uppermost aquifer, groundwater flow in the
uppermost aquifer is expected to follow the same general trend as the groundwater surface and in the direction
perpendicular to the groundwater contours shown on Figure 2 and Figure 4. Horizontal isotropic flow directions
beneath the liner are believed to be generally southwest towards Edward's Branch. The unnamed south flowing
ephemeral stream, bounded by wetlands, serves as a minor discharge feature with a drainage divide that is typically
located southeast or outside the waste liner limits but may potentially shift under abnormal climatic conditions and
stream level fluctuations.
Movement of groundwater through the unconfined flow system is controlled by the hydraulic properties of the
overlying regolith and the underlying confining layer. A review of the more than twenty potentiometric maps
generated of the uppermost aquifer and site conceptual models constructed during previous hydrogeologic studies
indicates that MW-13 has never been observed to be in the groundwater flow path originating from beneath the
landfill. The flow direction at MW-13 is consistently cross-gradient of the landfill with a calculated average over
the last events of S49W. Since the wetlands and drainage feature imparts localized influence on flow directions
TMW-13A is hydraulically downgradient of MW-13. Based on the potentiometric map, the average horizontal
hydraulic gradients of the groundwater surface in the MW-13 area over the last 5 events was 0.008 ft/ft. Calculated
average groundwater velocity at MW-13 ranged from 60 to 106 feet per year during the last 5 events (Table 1).
Groundwater Quality
Water quality for Phase 2 has been monitored at least on a semi-annual basis since prior to operation in May 2004
with all historical data available and reviewed in support of this report. Contaminants above regulatory Standards that
are believed to be attributed to an anthropogenic source have not been detected in any groundwater samples that
monitor any other portions of the lined landfill besides MW-13. Beginning in August 2015 samples collected from
MW-13 semi-annually contained benzene concentrations at 1.1µg/L, 1.1µg/L and 1.9µg/L which were above the NC
2L Groundwater Standard (1.0 µg/L). VOCs have never been detected in excess of the “Federal Drinking Water
Standard” (MCL). In response to the VOC exceedances in sample MW-13 all groundwater samples that monitor the
lined landfill were tested for an expansive number of constituents listed in 40CFR Appendix II in August 2016 and
only benzene levels were above regulatory Standards. In support of this assessment VOCs were recently targeted in
groundwater at MW-13 and three additional locations (P1-7, HAB-1 and TMW-13A) within 0.1 acres of MW-13.
VOCs were not detected in concentrations above regulatory Standards in any of the four locations which may indicate
the impacted area is very small, benzene levels are within allowable levels closer to the landfill and VOCs have likely
not migrated beyond the 250 foot compliance boundary. A table of all historical VOC detections in sample MW-13
is located on Table 2 and graph of all benzene detections is on Figure 5. The latest laboratory results from MW-13,
HAB-1, TMW-13A and P1-7 are enclosed in Appendix B.
2
Assessments Performed
Groundwater
Water quality evaluations were performed to determine the nature and extent of volatile organic compounds (VOCs)
in the area surrounding MW-13. A temporary monitoring well (TMW-13A) was recently installed approximately 65
feet downgradient of MW-13 at the compliance boundary (250 feet from edge of liner). TMW-13A is a type II well
installed to 9.5 feet bgs which screen bisects the water table. P1-7 is an existing observation well that is a remnant
from Hydrogeologic Design Study for Phase 1, located approximately 95 feet north of MW-13 that also bisects the
water table. HAB-1 is a boring located between the landfill and 45 feet upgradient of MW-13 which was advanced
to 12 feet which terminated 3 feet below the water table. After collecting a groundwater grab sample from open
boring HAB-1 it was abandoned with bentonite from 7-12 feet leaving a dry boring. The borehole was then re-
purposed as LFG monitoring well and renamed MP-102.
Groundwater samples were collected from three locations surrounding MW-13 in January 2017 and analyzed by Pace
Analytical (Pace) for VOCs. Benzene was detected in sample HAB-1 at 0.88 ug/L which is below the 2L Standard
(1.0 ug/L) but was not detected in samples TMW-13A and P1-7. Allowable levels of methylene chloride were
reported in samples TMW-13A and P1-7. However, the detections of methylene chloride were flagged by the
laboratory as (C9) “common laboratory contaminant” and (B) “analyte detected in associated method blank” therefore
are considered false positives. A sample collected from MW-13 during the most recent semi-annual water quality
monitoring event performed on February 16, 2017 contained levels of benzene at 0.81 ug/L which is below the 2L
Standard (1.0 ug/L).
Landfill Gas
The transport mechanism of VOCs is believed to be landfill gas (LFG) rather than liquid leachate originating from
Phase 2. Some of the many lines of evidence indicating LFG as the source include the positioning of MW-13 is
hydraulically cross-gradient of the waste, evidence of an overland flow release have not been observed, LFG has
been detected in the head-space of water and LFG wells, groundwater specific conductivity is low and dissolved
methane is elevated.
LFG has previously been detected in the head-space of MW-13, MW-16R, LFG probes MP-24, and MP-25 but levels
are inconsistent and variations are largely dependent upon barometric pressure and groundwater fluctuations. LFG
moves through the vadose primarily via convection and diffusion regardless of groundwater flow direction. It is
believed that LFG containing VOCs migrates horizontally predominately through the sand layer which is between the
cohesive clay and the capillary fringe where gas/liquid partitioning readily occurs. Scientists have proposed that
wells such as MW-13, where the well screen is above or straddles the groundwater table, migration of gas through the
vadose zone could allow LFG to accumulate in the head space (Kerfoot and Prattke, 1992) causing air/liquid phase
partitioning. This transport is often referred to as an “intrawell” pathway. Temperature and pressure changes could
then result in gas condensation on the casing wall and run down into the groundwater within the well. Illustrations of
LFG to groundwater through intrawell pathway at MW-13 in cross section view is presented as Figure 6. Direct
partioning of VOCs into groundwater through Intrawell exposure is not the only pathway that LFG may impact
groundwater. Impacts also occur outside of the well casing through LFG partitioning with soil moisture in the vadose
zone or the water table.
To evaluate LFG migration MP-101 was installed 65 feet from the liner edge perpendicular to MW-13. VOC levels
were taken with a flame ionization detector (FID) during boring excavation. VOCs were not detected until the clay
layer was penetrated at approximately 8 feet BLS. MP-101 was allowed to accumulate LFG for over 4 hours after
installation and VOC levels were very elevated (35%/vol).
KERFOOT H. B.; PRATTKE M. J. , 1992: False positive indications of leachate effects on ground water due to the use of volatile organic compounds as indicator parameters; a field study of gas migration. Ground Water Management 11: 119-132
3
Figures
Topographic Map with Site Location
01 1 MILE
FIGURE 1
Wayne County Landfill North Carolina (Dudley)
CLOSED MSW FACILITY
SUBTITLE D MSW
LANDFILL FACILITY
460 B South Landfill Rd
Dudley, NC 28333
Lat:35-17-19.1338
Long:-78-04-17.2971
Northing:561283.19
Easting:2277068.62
N
DA
T
E
DRAWING NO.SHEET NO.
SCALE:
DATE:
DRWN. BY:
CHKD. BY:
PROJECT NUMBER
BY
RE
V
.
DE
S
C
R
I
P
T
I
O
N
100500
Feet
1:360
50
LINED MSWLF PHASE LIMITS
TREE LINE (AERIAL MAPPING)
WETLANDS
COMPLIANCE BOUNDARY
EXISTING TOPOGRAPHIC CONTOURS
EXISTING PROPERTY LINE
EXISTING CREEK, STREAM, ETC.
CLOSED MSWLF, ESTIMATED EXTENT OF WASTE
POTENTIOMETRIC GROUNDWATER CONTOUR
MONITORING WELL
FIGURE 4
Wayne County Lined MSWLF, Phase 2 Page 1 of 1
Figure 5
VOC Concentrations Time Series Graph and Table
May 4, 2004 (premier event) through February 17, 2017 (most recent event)
Non-detects shown at detection limit
2L = North Carolina Groundwater Standard (Applicable Compliance Standard)
MCL = “Federal Drinking Water Standard” (Not Applicable Compliance Standard)
Well ID MW-13
VOC Benzene
2L Std 1.0
Unit
5/04/04 thru 8/29/06 ND <5
02/07/07 ND <3
8/14/07-2/12/08 ND <0.16
8/25/08-8/25/14 ND <0.25
1/21/08 thru 1/21/14 ND <0.62
02/11/15 0.67 (j)
08/20/15 1.1
03/03/16 1.1
08/22/16 1.9
02/16/17 0.81 (j)
(j) = The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL). “j-qualified”
All Historical VOC 2L Exceedances in sample MW-13
(ug/L)
0
1
2
3
4
5
6
Benzene Levels in MW-13

Benzene
Date
u g /L
Not detected prior to 2/11/15
MCL
2L
LFG to Groundwater Intrawell Pathway Cross Section View
Wayne County Lined MSWLF, Phase 2
MW-13
GCCS Pipe Annulus
Now Sealed
Lined MSWLF Ph 2
Adapted from Steve Wampler, AquAeTer, Inc. Louois Bull, Waste Management Groundwater Protection Program
2011 Presentation entitled
“LANDFILL GAS IMPACTS TO SHALLOW GROUNDWATER What is the real issue?”
N
Groundwater Flow
Figure 6
Tables
Wayne County Lined MSWLF, Phase 2 Page 1 of 1
Table 1
MW-13
(cm/sec)(%)(ft/ft)(ft/yr)
MW-13 08/25/14 2.14E-03 22.0 0.006 60 S66W 8.25 141.64 Silty Sand
MW-13 02/11/15 2.14E-03 22.0 0.008 75 S32W 7.74 142.15 Silty Sand
MW-13 08/20/15 2.14E-03 22.0 0.009 86 S50W 8.79 141.10 Silty Sand
MW-13 03/03/16 2.14E-03 22.0 0.011 106 S20W 6.78 143.11 Silty Sand
MW-13 08/22/16 2.14E-03 22.0 0.009 90 S75W 8.65 141.24 Silty Sand
Minimum 2.14E-03 22.0 0.006 60 S20W 6.78 141.10 -
Average 2.14E-03 22.0 0.008 84 S49W 8.04 141.85 -
Maximum 2.14E-03 22.0 0.011 106 S75W 8.79 143.11 -
NOTE:Values for hydraulic conductivity previously determined via slug test by MESCO.
K = hydraulic conductivity
Hydrogeologic Properties
Monitoring
Well
Sample
Date Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Average
Linear
Velocity
Rate
Flow
Direction Depth to
Groundwater
Groundwater
Potentiometric
Elevation
Screened
Interval
Lithology
(ft btoc)(ft amsl)
Hydrologic Gradient calculated from groundwater elevations recorded on their respective sample date.
Average linear velocity rate (Q) is defined by modified Darcy's equation:
ne = effective porosity
dh = head difference
dl = horizontal distance
Q=−K
ne
⋅dh
dl
Wayne County Lined MSWLF, Phase 2 Page 1 of 1
Table 2
All 28 Events (May 4, 2004 through February 16, 2017)
Result Unit
MW-13 Acetone 2/12/2008 4.10 (J)1.21 100 6000 NE
MW-13 Acetone 8/15/2011 2.5 (J)2.2 100 6000 NE
MW-13 Chloroform 2/15/2010 0.14 (J)0.14 5 70 80
MW-13 8/10/2010 0.41 (J)0.11 1 2.6 NE
MW-13 8/22/2016 0.41 (J)0.11 1 2.6 NE
MW-13 8/14/2013 1 (C9)0.97 1 4.6 5 False +
MW-13 Benzene 2/11/2015 0.67 (J)0.25 1 1 5
MW-13 Benzene 8/20/2015 1.1 0.25 1 1 5 LFG
MW-13 Benzene 3/3/2016 1.1 0.25 1 1 5 LFG
MW-13 Benzene 8/22/2016 1.9 0.25 1 1 5 LFG
MW-13 Benzene 2/16/2017 0.81 (J)0.25 1 1 5
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
(J)=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
(C9) = “Common laboratory contaminant” as flagged by the laboratory
NE = Not Established
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
VOC Detections in MW-13 above MDL
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 MCL 5 Preliminary
Cause 6
ug/l
ug/L
ug/L
Chloromethane ug/L
Chloromethane ug/L
Methylene Chloride ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains VOC constituents detected at or above MDL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 MCL = Maximum Contaminant Level aka Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
6 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L Standard.
Table 3
LFG Well ID
Sample
Tube Purge
(Seconds)
Time
Reading
Taken
Time
Pumped
(Seconds)
Initial
% LEL
Stabilized
% LEL
Stabilized
% CH4 by
Volume % O2 % CO2
Instrument
Used
Depth to
water
(FT
BLS)
Sand
Pack
Exposed
to LFG
(ft)Notes
MP-24 60 03:03 PM 60 0 0 0 nr nr FID (TVA 1000)dry 1.2
MP-101 60 02:45 PM 60 650 650 32.5 nr nr FID (TVA 1000)dry 10
MW-13 60 02:55 PM 60 0 0 0.0 nr nr FID (TVA 1000)4.93 0 Intake submerged
P1-7 60 03:35 PM 60 4 4 0.2 nr nr FID (TVA 1000)3.68 2.68
TMW-13A 60 03:14 PM 60 0 0 0.0 nr nr FID (TVA 1000)4.21 0.71
MP-101 60 not recorded 60 4 4 0.2 nr nr GEM2000 dry 10
MP-24 60 02:03 PM 60 0 0 0 nr nr FID (TVA 1000)dry 1.2
MP-101 60 03:14 PM 60 6 6 0.3 nr nr FID (TVA 1000)dry 10
MP-102 60 03:03 PM 60 2 2 0.1 nr nr FID (TVA 1000)dry 5.5
MW-13 60 02:08 PM 60 0 0 0.0 nr nr FID (TVA 1000)4.81 0 Intake submerged
P1-7 60 03:55 PM 60 0 0 0.0 nr nr FID (TVA 1000)3.57 3.81
TMW-13A 60 04:01 PM 60 0 0 0.0 nr nr FID (TVA 1000)4.18 0.68
MP-24 60 03:08 PM 60 0 0 0 17.9 3.1 GEM2000 dry 1.2
MP-25 60 03:00 PM 60 16 16 0.8 1.2 8.6 GEM2000 dry 1.4
MP-101 60 03:05 PM 60 0 0 0 20.1 0.2 GEM2000 dry 10
MP-102 60 03:10 PM 60 0 0 0 20.2 0.2 GEM2000 dry 5.5
MW-13 60 03:19 PM 60 0 0 0 20.5 0.1 GEM2000 4.81 0 Intake submerged
MW-16R 60 02:45 PM 60 0 0 0 17.1 2.9 GEM2000 5.01 0 Intake submerged
P1-7 60 03:25 PM 60 0 0 0 20.4 0.5 GEM2000 3.64 2.64
TMW-13A 60 03:12 PM 60 0 0 0 20.2 0.4 GEM2000 4.24 0.74
1/6/2017
1/18/2017
1/27/2017
2/17/2017
BASELINE BEFORE CORRECTIVE ACTION (JANUARY 6, 2017)
10 DAYS AFTER CORRECTIVE ACTION (JANUARY 27, 2017)
31 DAYS AFTER CORRECTIVE ACTION (FEBRUARY 17, 2017)
1 DAY AFTER CORRECTIVE ACTION (JANUARY 18, 2017)
Landfill Gas Monitoring Readings
32.5
0.3 0.3 0
0
5
10
15
20
25
30
35
1/
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2
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1
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1/
2
8
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2
9
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0
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Methane (%/vol) at MP-101 (130 ft from MW-13 & 65 ft from liner)

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Wayne Co Lined MSWLF, Phase 2
Appendix A
LOG OF BORING: MW-13
Wayne Co Lined MSWLF Ph. 2 Project No. G01096.0
Drilling contractor: J. Pfohl Date started: 12/3/2001 Surface elevation: 146.89 ft (MSL)
Drill rig & method: 6" O.D HSA Date ended: 12/4/2001 Top of pipe elevation: 149.89 ft (MSL)
Logged by: J. Pfohl Completion depth: 16.00 ft Depth to water (TOB): 8.00 ft
Stickup height: 3.00 ft Depth to water (24hrs): 7.56 ft
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Description of Material & Remarks
Well Diagram
5
10
15
20
SILTY SAND; Tan, organic root debris, poorly graded, moist.
SILTY CLAY; White, fine graded sand with cohesive clay, moist.
SILTY SAND; White to gray, medium to coarse grained sand, slight
cohesiveness, wet.
Boring terminated at 16.0 feet
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Municipal Engineering Services Company, P.A.
Operation/Construction Managers Civil/Sanitary Engineers Environmental Studies
PO Box 97, Garner, North Carolina 27529 [phone] PO Box 349, Boone, North Carolina 28607 [phone] Page 1 of 1
LOG OF BORING: HAB-1
Wayne Co Lined MSWLF Ph. 2 Project No. G16016.0
Drilling contractor: Date started: 1/27/2017 Surface elevation: NOT SURVEYED
Drill rig & method: Auger Date ended: 1/27/2017 Top of pipe elevation: NOT SURVEYED
Logged by: J. Pfohl Completion depth: 12.00 ft Depth to water (TOB): 9.00 ft
Stickup height: N/A Depth to water (24hrs): na
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Description of Material & Remarks
Well Diagram
5
10
Boring for grab water sample to delineate plume extent ~ 45 ft from
MW-13 towards landfill. Boring was then converted to LFG Probe
MP-102.
TOP SOIL; Dark brown, root debris, organic, dry.
SILTY SAND; Tan, trace organic root debris, poorly graded sand, moist.
SILTY CLAY; White, fine graded sand with cohesive clay, moist.
SILTY SAND; White to gray, medium to coarse grained sand, wet.
Boring terminated at 12.0 feet
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Municipal Engineering Services Company, P.A.
Operation/Construction Managers Civil/Sanitary Engineers Environmental Studies
PO Box 97, Garner, North Carolina 27529 [phone] PO Box 349, Boone, North Carolina 28607 [phone] Page 1 of 1
LOG OF BORING: MP-101
Wayne Co Lined MSWLF Ph. 2 Project No. G16016.0
Drilling contractor:Date started: 1/6/2017 Surface elevation: NOT SURVEYED
Drill rig & method: Auger Date ended: 1/6/2017 Top of pipe elevation: NOT SURVEYED
Logged by: J. Pfohl Completion depth: 12.00 ft Depth to water (TOB): dry
Stickup height: N/A Depth to water (24hrs): dry
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Description of Material & Remarks
Well Diagram
5
10
LFG monitoring well ~ 65 ft East of Waste Limit. Used for MW-13 GW
Assessment.
SILTY SAND; Tan, trace organic root debris, poorly graded sand, moist.
SILTY CLAY; White, fine graded sand with cohesive clay, moist.
SILTY SAND; White to gray, medium to coarse grained sand, dry.
Boring terminated at 12.0 feet
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Municipal Engineering Services Company, P.A.
Operation/Construction Managers Civil/Sanitary Engineers Environmental Studies
PO Box 97, Garner, North Carolina 27529 [phone] PO Box 349, Boone, North Carolina 28607 [phone] Page 1 of 1
LOG OF BORING: MP-102
Wayne Co Lined MSWLF Ph. 2 Project No. G16016.0
Drilling contractor: Date started: 1/27/2017 Surface elevation: NOT SURVEYED
Drill rig & method: Auger Date ended: 1/27/2017 Top of pipe elevation: NOT SURVEYED
Logged by: J. Pfohl Completion depth: 12.00 ft Depth to water (TOB): 9.00 ft
Stickup height: N/A Depth to water (24hrs): na
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Description of Material & Remarks
Well Diagram
5
10
LFG monitoring well ~ 45 ft NW of MW-13 which is closer to the landfill.
Converted from HAB-1 which was used for a water grab sample then
lower portion abandoned.
TOP SOIL; Dark brown, root debris, organic, dry.
SILTY SAND; Tan, trace organic root debris, poorly graded sand, moist.
SILTY CLAY; White, fine graded sand with cohesive clay, moist.
SILTY SAND; White to gray, medium to coarse grained sand, wet.
Boring terminated at 12.0 feet
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Municipal Engineering Services Company, P.A.
Operation/Construction Managers Civil/Sanitary Engineers Environmental Studies
PO Box 97, Garner, North Carolina 27529 [phone] PO Box 349, Boone, North Carolina 28607 [phone] Page 1 of 1
LOG OF BORING: TMW-13A
Wayne Co Lined MSWLF Ph. 2 Project No. G16016.0
Drilling contractor: Date started: 1/6/2017 Surface elevation: 145.14 ft (MSL)
Drill rig & method: Auger Date ended: 1/6/2017 Top of pipe elevation: 146.14 ft (MSL)
Logged by: J. Pfohl Completion depth: 9.50 ft Depth to water (TOB): 5.00 ft
Stickup height: 1.00 ft Depth to water (24hrs): 5.10 ft
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Description of Material & Remarks
Well Diagram
5
10
Temporary MW to delineate plume extent ~ 55 ft SSE of MW-13.
TOP SOIL; Dark brown, root debris, organic, dry.
SILTY SAND; Tan, trace organic root debris, poorly graded sand, moist.
SILTY CLAY; White, fine graded sand with cohesive clay, moist.
SILTY SAND; White to gray, medium to coarse grained sand, slight
cohesiveness, wet.
Boring terminated at 9.5 feet
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Municipal Engineering Services Company, P.A.
Operation/Construction Managers Civil/Sanitary Engineers Environmental Studies
PO Box 97, Garner, North Carolina 27529 [phone] PO Box 349, Boone, North Carolina 28607 [phone] Page 1 of 1
Appendix B
Laboratory Analysis Report &
Chains of Custody
#=CL#
March 07, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92330519
92330519
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Wayne Lined MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between February 17,
2017 and February 22, 2017. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 117
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 117
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92330519001 LE-1 Water 02/16/17 17:05 02/17/17 08:57
92330539001 MW-13 Water 02/16/17 10:50 02/17/17 08:52
92330539002 SW-4 Water 02/16/17 12:45 02/17/17 08:52
92330540001 MW-1 Water 02/16/17 09:10 02/17/17 08:52
92330540002 MW-3 Water 02/16/17 14:35 02/17/17 08:52
92330540003 MW-4 Water 02/16/17 14:00 02/17/17 08:52
92330540004 MW-5 Water 02/16/17 13:25 02/17/17 08:52
92330540005 MW-6 Water 02/16/17 11:50 02/17/17 08:52
92330540006 MW-7 Water 02/16/17 11:20 02/17/17 08:52
92330540007 MW-9 Water 02/16/17 09:55 02/17/17 08:52
92330540008 MW-10 Water 02/16/17 10:20 02/17/17 08:52
92330519013 MW-2 Water 02/17/17 10:19 02/22/17 08:00
92330519014 MW-8 Water 02/17/17 10:15 02/22/17 08:00
92330519015 MW-11 Water 02/17/17 13:00 02/22/17 08:00
92330519016 MW-12 Water 02/17/17 11:30 02/22/17 08:00
92330519017 MW-14 Water 02/17/17 11:40 02/22/17 08:00
92330519018 MW-15 Water 02/17/17 11:00 02/22/17 08:00
92330519019 MW-16R Water 02/17/17 15:00 02/22/17 08:00
92330519020 SW-5 Water 02/17/17 10:45 02/22/17 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 117
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92330519001 LE-1 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
SM 5210B 1 PASI-ACJH
EPA 9040 1 PASI-AKDF1
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
EPA 365.1 1 PASI-AMDW
SM 5220D 1 PASI-AMDW
92330539001 MW-13 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
92330539002 SW-4 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
92330540001 MW-1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-ASER
EPA 8270 74 PASI-CBPJ
EPA 8260 50 PASI-CZDO
SM 4500-CN-E 1 PASI-AAES2
92330540002 MW-3 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-ASER
EPA 8260 50 PASI-CZDO
92330540003 MW-4 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-ASER
EPA 8260 50 PASI-CZDO
92330540004 MW-5 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
SM 4500-CN-E 1 PASI-AAES2
92330540005 MW-6 EPA 8151 12 PASI-OLJM
EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-ASER
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 117
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 50 PASI-CZDO
SM 4500-CN-E 1 PASI-AAES2
92330540006 MW-7 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-ASER
EPA 8270 74 PASI-CBPJ
EPA 8260 50 PASI-CZDO
SM 4500-CN-E 1 PASI-AAES2
92330540007 MW-9 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-ASER
EPA 8260 50 PASI-CCAH
92330540008 MW-10 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
92330519013 MW-2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8270 74 PASI-CBPJ
EPA 8260 50 PASI-CCAH
SM 4500-CN-E 1 PASI-ADMN
92330519014 MW-8 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
SM 4500-CN-E 1 PASI-ADMN
92330519015 MW-11 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CCAH
92330519016 MW-12 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
92330519017 MW-14 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
92330519018 MW-15 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 117
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92330519019 MW-16R EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
SM 4500-CN-E 1 PASI-ADMN
92330519020 SW-5 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:LE-1 Lab ID:92330519001 Collected:02/16/17 17:05 Received:02/17/17 08:57 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 13.2 ug/L 02/24/17 06:31 7440-36-002/20/17 19:556.0 3.9 1
Arsenic 9.8J ug/L 02/24/17 06:31 7440-38-202/20/17 19:5510.0 5.0 1
Barium 187 ug/L 02/24/17 06:31 7440-39-302/20/17 19:551002.5 1
Beryllium ND ug/L 02/24/17 06:31 7440-41-702/20/17 19:551.0 0.50 1
Cadmium ND ug/L 02/24/17 06:31 7440-43-902/20/17 19:551.0 0.50 1
Chromium 32.2 ug/L 02/24/17 06:31 7440-47-302/20/17 19:5510.0 2.5 1
Cobalt 5.7J ug/L 02/24/17 06:31 7440-48-402/20/17 19:5510.0 2.5 1
Copper ND ug/L 02/24/17 06:31 7440-50-802/20/17 19:5510.0 2.5 1
Lead ND ug/L 02/24/17 06:31 7439-92-102/20/17 19:5510.0 2.5 1
Nickel 60.2 ug/L 02/24/17 06:31 7440-02-002/20/17 19:5550.0 2.5 1
Selenium ND ug/L 02/24/17 06:31 7782-49-202/20/17 19:5510.0 5.0 1
Silver ND ug/L 02/24/17 06:31 7440-22-402/20/17 19:5510.0 2.5 1
Tin 4.3J ug/L 02/24/17 06:31 7440-31-502/20/17 19:551002.5 1
Vanadium 10.8J ug/L 02/24/17 06:31 7440-62-202/20/17 19:5525.0 2.5 1
Zinc 145 ug/L 02/24/17 06:31 7440-66-602/20/17 19:5510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/23/17 18:02 7439-97-602/22/17 07:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/21/17 19:38 67-64-110010.0 1
Acetonitrile ND ug/L 02/21/17 19:38 75-05-855.0 2.2 1
Acrolein ND ug/L 02/21/17 19:38 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 02/21/17 19:38 107-13-12001.9 1
Allyl chloride ND ug/L 02/21/17 19:38 107-05-110.0 1.5 1
Benzene 4.7 ug/L 02/21/17 19:38 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/21/17 19:38 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/21/17 19:38 75-27-41.0 0.18 1
Bromoform ND ug/L 02/21/17 19:38 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/21/17 19:38 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/21/17 19:38 78-93-31000.96 1
Carbon disulfide ND ug/L 02/21/17 19:38 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/21/17 19:38 56-23-51.0 0.25 1
Chlorobenzene 6.6 ug/L 02/21/17 19:38 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/21/17 19:38 75-00-310.0 0.54 1
Chloroform ND ug/L 02/21/17 19:38 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/21/17 19:38 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/21/17 19:38 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/21/17 19:38 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/21/17 19:38 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/21/17 19:38 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/21/17 19:38 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/21/17 19:38 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/21/17 19:38 541-73-15.0 0.24 1
1,4-Dichlorobenzene 7.0 ug/L 02/21/17 19:38 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/21/17 19:38 110-57-61001.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:LE-1 Lab ID:92330519001 Collected:02/16/17 17:05 Received:02/17/17 08:57 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Dichlorodifluoromethane ND ug/L 02/21/17 19:38 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 02/21/17 19:38 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/21/17 19:38 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/21/17 19:38 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.38J ug/L 02/21/17 19:38 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/21/17 19:38 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/21/17 19:38 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/21/17 19:38 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/21/17 19:38 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 02/21/17 19:38 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/21/17 19:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/21/17 19:38 10061-02-61.0 0.26 1
Ethylbenzene 20.0 ug/L 02/21/17 19:38 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/21/17 19:38 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 02/21/17 19:38 87-68-310.0 0.71 1
2-Hexanone ND ug/L 02/21/17 19:38 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/21/17 19:38 74-88-410.0 0.32 1
Isobutanol ND ug/L 02/21/17 19:38 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/21/17 19:38 126-98-71000.93 1
Methylene Chloride ND ug/L 02/21/17 19:38 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/21/17 19:38 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)2.0J ug/L 02/21/17 19:38 108-10-11000.33 1
Naphthalene 3.4J ug/L 02/21/17 19:38 91-20-310.0 0.24 1
Propionitrile ND ug/L 02/21/17 19:38 107-12-01503.6 1
Styrene ND ug/L 02/21/17 19:38 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/21/17 19:38 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/21/17 19:38 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/21/17 19:38 127-18-41.0 0.46 1
Toluene 12.9 ug/L 02/21/17 19:38 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 02/21/17 19:38 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 02/21/17 19:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/21/17 19:38 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/21/17 19:38 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/21/17 19:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/21/17 19:38 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/21/17 19:38 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/21/17 19:38 75-01-41.0 0.62 1
Xylene (Total)62.4 ug/L 02/21/17 19:38 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %02/21/17 19:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %02/21/17 19:38 17060-07-070-130 1
Toluene-d8 (S)117 %02/21/17 19:38 2037-26-570-130 1
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 57500 ug/L 02/22/17 21:4502/18/17 02:30200020001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:LE-1 Lab ID:92330519001 Collected:02/16/17 17:05 Received:02/17/17 08:57 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 90409040 pH
pH 7.2 Std. Units 02/22/17 14:32 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 10200J ug/L 02/21/17 22:30 14808-79-8125000050005
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 11.2J ug/L 02/18/17 00:501000010.0 1
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 2080 ug/L 02/21/17 21:00 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 781000 ug/L 02/22/17 00:2225000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-13 Lab ID:92330539001 Collected:02/16/17 10:50 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/24/17 06:53 7440-36-002/20/17 19:556.0 3.9 1
Arsenic ND ug/L 02/24/17 06:53 7440-38-202/20/17 19:5510.0 5.0 1
Barium 34.7J ug/L 02/24/17 06:53 7440-39-302/20/17 19:551002.5 1
Beryllium ND ug/L 02/24/17 06:53 7440-41-702/20/17 19:551.0 0.50 1
Cadmium ND ug/L 02/24/17 06:53 7440-43-902/20/17 19:551.0 0.50 1
Chromium ND ug/L 02/24/17 06:53 7440-47-302/20/17 19:5510.0 2.5 1
Cobalt ND ug/L 02/24/17 06:53 7440-48-402/20/17 19:5510.0 2.5 1
Copper ND ug/L 02/24/17 06:53 7440-50-802/20/17 19:5510.0 2.5 1
Lead 3.6J ug/L 02/24/17 06:53 7439-92-102/20/17 19:5510.0 2.5 1
Nickel ND ug/L 02/24/17 06:53 7440-02-002/20/17 19:5550.0 2.5 1
Selenium ND ug/L 02/24/17 06:53 7782-49-202/20/17 19:5510.0 5.0 1
Silver ND ug/L 02/24/17 06:53 7440-22-402/20/17 19:5510.0 2.5 1
Vanadium 4.7J ug/L 02/24/17 06:53 7440-62-202/20/17 19:5525.0 2.5 1
Zinc ND ug/L 02/24/17 06:53 7440-66-602/20/17 19:5510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 02/24/17 18:40 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 22:33 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 22:33 107-13-12001.9 1
Benzene 0.81J ug/L 02/28/17 22:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 22:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 22:33 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 22:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 22:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 22:33 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 22:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 22:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 22:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 22:33 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 22:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 22:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 22:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 22:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 22:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 22:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 22:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 22:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 22:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 22:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 22:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 22:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/17 22:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 22:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 22:33 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-13 Lab ID:92330539001 Collected:02/16/17 10:50 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/28/17 22:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 22:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 22:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 22:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 22:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 22:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 22:33 108-10-11000.33 1
Styrene ND ug/L 02/28/17 22:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 22:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 22:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 22:33 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/17 22:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 22:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 22:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 22:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 22:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 22:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 22:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 22:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 22:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %02/28/17 22:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %02/28/17 22:33 17060-07-070-130 1
Toluene-d8 (S)101 %02/28/17 22:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:SW-4 Lab ID:92330539002 Collected:02/16/17 12:45 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:06 7440-36-002/21/17 19:256.0 3.9 1
Arsenic ND ug/L 02/28/17 05:06 7440-38-202/21/17 19:2510.0 5.0 1
Barium 190 ug/L 02/28/17 05:06 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:06 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:06 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:06 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:06 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:06 7440-50-802/21/17 19:2510.0 2.5 1
Lead ND ug/L 02/28/17 05:06 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:06 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:06 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:06 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium ND ug/L 02/28/17 05:06 7440-62-202/21/17 19:2525.0 2.5 1
Zinc 7.1J ug/L 02/28/17 05:06 7440-66-6 B02/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.032J ug/L 02/24/17 18:42 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 22:50 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 22:50 107-13-12001.9 1
Benzene ND ug/L 02/28/17 22:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 22:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 22:50 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 22:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 22:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 22:50 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 22:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 22:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 22:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 22:50 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 22:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 22:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 22:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 22:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 22:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 22:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 22:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 22:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 22:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 22:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 22:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 22:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/17 22:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 22:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 22:50 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:SW-4 Lab ID:92330539002 Collected:02/16/17 12:45 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/28/17 22:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 22:50 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 22:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 22:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 22:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 22:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 22:50 108-10-11000.33 1
Styrene ND ug/L 02/28/17 22:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 22:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 22:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 22:50 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/17 22:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 22:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 22:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 22:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 22:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 22:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 22:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 22:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 22:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)93 %02/28/17 22:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %02/28/17 22:50 17060-07-070-130 1
Toluene-d8 (S)99 %02/28/17 22:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-1 Lab ID:92330540001 Collected:02/16/17 09:10 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:15 7440-36-002/21/17 19:256.0 3.9 1
Arsenic 6.7J ug/L 02/28/17 05:15 7440-38-202/21/17 19:2510.0 5.0 1
Barium 26.8J ug/L 02/28/17 05:15 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:15 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:15 7440-43-902/21/17 19:251.0 0.50 1
Chromium 5.3J ug/L 02/28/17 05:15 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:15 7440-48-402/21/17 19:2510.0 2.5 1
Copper 2.9J ug/L 02/28/17 05:15 7440-50-802/21/17 19:2510.0 2.5 1
Lead 3.2J ug/L 02/28/17 05:15 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:15 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:15 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:15 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium 17.2J ug/L 02/28/17 05:15 7440-62-202/21/17 19:2525.0 2.5 1
Zinc 9.5J ug/L 02/28/17 05:15 7440-66-6 B02/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 02/24/17 18:44 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/24/17 02:44 7439-97-602/23/17 05:110.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 02/21/17 19:11 83-32-902/20/17 14:0810.0 0.25 1
Acenaphthylene ND ug/L 02/21/17 19:11 208-96-802/20/17 14:0810.0 0.21 1
Aniline ND ug/L 02/21/17 19:11 62-53-302/20/17 14:0810.0 1.3 1
Anthracene ND ug/L 02/21/17 19:11 120-12-702/20/17 14:0810.0 0.14 1
Benzo(a)anthracene ND ug/L 02/21/17 19:11 56-55-302/20/17 14:0810.0 0.33 1
Benzo(a)pyrene ND ug/L 02/21/17 19:11 50-32-802/20/17 14:0810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 02/21/17 19:11 205-99-202/20/17 14:0810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 02/21/17 19:11 191-24-202/20/17 14:0810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 02/21/17 19:11 207-08-902/20/17 14:0810.0 0.43 1
Benzoic Acid ND ug/L 02/21/17 19:11 65-85-002/20/17 14:0850.0 11.1 1
Benzyl alcohol ND ug/L 02/21/17 19:11 100-51-602/20/17 14:0820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 02/21/17 19:11 101-55-302/20/17 14:0810.0 1.3 1
Butylbenzylphthalate ND ug/L 02/21/17 19:11 85-68-702/20/17 14:0810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 02/21/17 19:11 59-50-702/20/17 14:0820.0 4.2 1
4-Chloroaniline ND ug/L 02/21/17 19:11 106-47-802/20/17 14:0820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 02/21/17 19:11 111-91-102/20/17 14:0810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 02/21/17 19:11 111-44-402/20/17 14:0810.0 1.5 1
2-Chloronaphthalene ND ug/L 02/21/17 19:11 91-58-702/20/17 14:0810.0 2.2 1
2-Chlorophenol ND ug/L 02/21/17 19:11 95-57-802/20/17 14:0810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 02/21/17 19:11 7005-72-302/20/17 14:0810.0 2.1 1
Chrysene ND ug/L 02/21/17 19:11 218-01-902/20/17 14:0810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 02/21/17 19:11 53-70-302/20/17 14:0810.0 0.55 1
Dibenzofuran ND ug/L 02/21/17 19:11 132-64-902/20/17 14:0810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 02/21/17 19:11 95-50-102/20/17 14:0810.0 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-1 Lab ID:92330540001 Collected:02/16/17 09:10 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1,3-Dichlorobenzene ND ug/L 02/21/17 19:11 541-73-102/20/17 14:0810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 02/21/17 19:11 106-46-702/20/17 14:0810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 02/21/17 19:11 91-94-102/20/17 14:0820.0 1.4 1
2,4-Dichlorophenol ND ug/L 02/21/17 19:11 120-83-202/20/17 14:0810.0 1.7 1
Diethylphthalate ND ug/L 02/21/17 19:11 84-66-202/20/17 14:0860001.3 1
2,4-Dimethylphenol ND ug/L 02/21/17 19:11 105-67-902/20/17 14:0810.0 2.2 1
Dimethylphthalate ND ug/L 02/21/17 19:11 131-11-302/20/17 14:0810.0 1.5 1
Di-n-butylphthalate ND ug/L 02/21/17 19:11 84-74-202/20/17 14:0810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 02/21/17 19:11 534-52-102/20/17 14:0850.0 1.7 1
2,4-Dinitrophenol ND ug/L 02/21/17 19:11 51-28-502/20/17 14:0850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 02/21/17 19:11 121-14-202/20/17 14:0810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 02/21/17 19:11 606-20-202/20/17 14:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 02/21/17 19:11 117-84-002/20/17 14:0810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 02/21/17 19:11 117-81-702/20/17 14:0815.0 0.85 1
Fluoranthene ND ug/L 02/21/17 19:11 206-44-002/20/17 14:0810.0 0.21 1
Fluorene ND ug/L 02/21/17 19:11 86-73-702/20/17 14:0810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 02/21/17 19:11 87-68-302/20/17 14:0810.0 1.8 1
Hexachlorobenzene ND ug/L 02/21/17 19:11 118-74-102/20/17 14:0810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 02/21/17 19:11 77-47-402/20/17 14:0810.0 1.8 1
Hexachloroethane ND ug/L 02/21/17 19:11 67-72-102/20/17 14:0810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/21/17 19:11 193-39-502/20/17 14:0810.0 0.29 1
Isophorone ND ug/L 02/21/17 19:11 78-59-102/20/17 14:0810.0 1.8 1
1-Methylnaphthalene ND ug/L 02/21/17 19:11 90-12-002/20/17 14:0810.0 0.32 1
2-Methylnaphthalene ND ug/L 02/21/17 19:11 91-57-602/20/17 14:0810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 02/21/17 19:11 95-48-702/20/17 14:0810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 02/21/17 19:1102/20/17 14:0810.0 1.7 1
Naphthalene ND ug/L 02/21/17 19:11 91-20-302/20/17 14:0810.0 0.34 1
2-Nitroaniline ND ug/L 02/21/17 19:11 88-74-402/20/17 14:0850.0 2.8 1
3-Nitroaniline ND ug/L 02/21/17 19:11 99-09-202/20/17 14:0850.0 2.4 1
4-Nitroaniline ND ug/L 02/21/17 19:11 100-01-602/20/17 14:0820.0 2.5 1
Nitrobenzene ND ug/L 02/21/17 19:11 98-95-302/20/17 14:0810.0 1.7 1
2-Nitrophenol ND ug/L 02/21/17 19:11 88-75-502/20/17 14:0810.0 1.7 1
4-Nitrophenol ND ug/L 02/21/17 19:11 100-02-702/20/17 14:0850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 02/21/17 19:11 62-75-902/20/17 14:0810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 02/21/17 19:11 621-64-702/20/17 14:0810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 02/21/17 19:11 86-30-602/20/17 14:0810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 02/21/17 19:11 108-60-102/20/17 14:0810.0 1.6 1
Pentachlorophenol ND ug/L 02/21/17 19:11 87-86-502/20/17 14:0825.0 2.3 1
Phenanthrene ND ug/L 02/21/17 19:11 85-01-802/20/17 14:0810.0 0.22 1
Phenol ND ug/L 02/21/17 19:1102/20/17 14:0810.0 1.7 1
Pyrene ND ug/L 02/21/17 19:11 129-00-002/20/17 14:0810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 02/21/17 19:11 120-82-102/20/17 14:0810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 02/21/17 19:11 95-95-402/20/17 14:0810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 02/21/17 19:11 88-06-202/20/17 14:0810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)66 %02/21/17 19:11 4165-60-002/20/17 14:0821-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 15 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-1 Lab ID:92330540001 Collected:02/16/17 09:10 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
2-Fluorobiphenyl (S)66 %02/21/17 19:11 321-60-802/20/17 14:0827-110 1
Terphenyl-d14 (S)73 %02/21/17 19:11 1718-51-002/20/17 14:0831-107 1
Phenol-d6 (S)21 %02/21/17 19:11 13127-88-302/20/17 14:0810-110 1
2-Fluorophenol (S)30 %02/21/17 19:11 367-12-402/20/17 14:0812-110 1
2,4,6-Tribromophenol (S)75 %02/21/17 19:11 118-79-602/20/17 14:0827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 23:07 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 23:07 107-13-12001.9 1
Benzene ND ug/L 02/28/17 23:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 23:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 23:07 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 23:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 23:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 23:07 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 23:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 23:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 23:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 23:07 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 23:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 23:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 23:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 23:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 23:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 23:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 23:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 23:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 23:07 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 23:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 23:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 23:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/17 23:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 23:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 23:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/28/17 23:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 23:07 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 23:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 23:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 23:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 23:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 23:07 108-10-11000.33 1
Styrene ND ug/L 02/28/17 23:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 23:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 23:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 23:07 127-18-41.0 0.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-1 Lab ID:92330540001 Collected:02/16/17 09:10 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Toluene ND ug/L 02/28/17 23:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 23:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 23:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 23:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 23:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 23:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 23:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 23:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 23:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)91 %02/28/17 23:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %02/28/17 23:07 17060-07-070-130 1
Toluene-d8 (S)100 %02/28/17 23:07 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 02/23/17 18:41 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-3 Lab ID:92330540002 Collected:02/16/17 14:35 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:18 7440-36-002/21/17 19:256.0 3.9 1
Arsenic 12.4 ug/L 02/28/17 05:18 7440-38-202/21/17 19:2510.0 5.0 1
Barium 26.6J ug/L 02/28/17 05:18 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:18 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:18 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:18 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:18 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:18 7440-50-802/21/17 19:2510.0 2.5 1
Lead ND ug/L 02/28/17 05:18 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:18 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:18 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:18 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium ND ug/L 02/28/17 05:18 7440-62-202/21/17 19:2525.0 2.5 1
Zinc 5.9J ug/L 02/28/17 05:18 7440-66-6 B02/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.024J ug/L 02/24/17 18:46 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/24/17 02:47 7439-97-602/23/17 05:110.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 23:24 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 23:24 107-13-12001.9 1
Benzene ND ug/L 02/28/17 23:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 23:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 23:24 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 23:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 23:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 23:24 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 23:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 23:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 23:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 23:24 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 23:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 23:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 23:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 23:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 23:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 23:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 23:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 23:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 23:24 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 23:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 23:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 23:24 75-35-45.0 0.56 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-3 Lab ID:92330540002 Collected:02/16/17 14:35 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,2-Dichloroethene ND ug/L 02/28/17 23:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 23:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 23:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/28/17 23:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 23:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 23:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 23:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 23:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 23:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 23:24 108-10-11000.33 1
Styrene ND ug/L 02/28/17 23:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 23:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 23:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 23:24 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/17 23:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 23:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 23:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 23:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 23:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 23:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 23:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 23:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 23:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %02/28/17 23:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %02/28/17 23:24 17060-07-070-130 1
Toluene-d8 (S)99 %02/28/17 23:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-4 Lab ID:92330540003 Collected:02/16/17 14:00 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:21 7440-36-002/21/17 19:256.0 3.9 1
Arsenic 5.3J ug/L 02/28/17 05:21 7440-38-202/21/17 19:2510.0 5.0 1
Barium 44.6J ug/L 02/28/17 05:21 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:21 7440-41-702/21/17 19:251.0 0.50 1
Cadmium 0.54J ug/L 02/28/17 05:21 7440-43-902/21/17 19:251.0 0.50 1
Chromium 4.8J ug/L 02/28/17 05:21 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:21 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:21 7440-50-802/21/17 19:2510.0 2.5 1
Lead ND ug/L 02/28/17 05:21 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:21 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:21 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:21 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium 7.4J ug/L 02/28/17 05:21 7440-62-202/21/17 19:2525.0 2.5 1
Zinc ND ug/L 02/28/17 05:21 7440-66-602/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.028J ug/L 02/24/17 18:48 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 1.1 ug/L 02/24/17 02:49 7439-97-602/23/17 05:110.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 23:40 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 23:40 107-13-12001.9 1
Benzene ND ug/L 02/28/17 23:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 23:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 23:40 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 23:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 23:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 23:40 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 23:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 23:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 23:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 23:40 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 23:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 23:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 23:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 23:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 23:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 23:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 23:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 23:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 23:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 23:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 23:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 23:40 75-35-45.0 0.56 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-4 Lab ID:92330540003 Collected:02/16/17 14:00 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,2-Dichloroethene ND ug/L 02/28/17 23:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 23:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 23:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/28/17 23:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 23:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 23:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 23:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 23:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 23:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 23:40 108-10-11000.33 1
Styrene ND ug/L 02/28/17 23:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 23:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 23:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 23:40 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/17 23:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 23:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 23:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 23:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 23:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 23:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 23:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 23:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 23:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %02/28/17 23:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %02/28/17 23:40 17060-07-070-130 1
Toluene-d8 (S)102 %02/28/17 23:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-5 Lab ID:92330540004 Collected:02/16/17 13:25 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:24 7440-36-002/21/17 19:256.0 3.9 1
Arsenic ND ug/L 02/28/17 05:24 7440-38-202/21/17 19:2510.0 5.0 1
Barium 46.4J ug/L 02/28/17 05:24 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:24 7440-41-702/21/17 19:251.0 0.50 1
Cadmium 1.0 ug/L 02/28/17 05:24 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:24 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:24 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:24 7440-50-802/21/17 19:2510.0 2.5 1
Lead ND ug/L 02/28/17 05:24 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:24 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:24 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:24 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium ND ug/L 02/28/17 05:24 7440-62-202/21/17 19:2525.0 2.5 1
Zinc ND ug/L 02/28/17 05:24 7440-66-602/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 02/24/17 18:50 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 23:57 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 23:57 107-13-12001.9 1
Benzene ND ug/L 02/28/17 23:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 23:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 23:57 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 23:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 23:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 23:57 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 23:57 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 23:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 23:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 23:57 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 23:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 23:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 23:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 23:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 23:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 23:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 23:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 23:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 23:57 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 23:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 23:57 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 23:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/17 23:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 23:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 23:57 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-5 Lab ID:92330540004 Collected:02/16/17 13:25 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/28/17 23:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 23:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 23:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 23:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 23:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 23:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 23:57 108-10-11000.33 1
Styrene ND ug/L 02/28/17 23:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 23:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 23:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 23:57 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/17 23:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 23:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 23:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 23:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 23:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 23:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 23:57 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 23:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 23:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %02/28/17 23:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %02/28/17 23:57 17060-07-070-130 1
Toluene-d8 (S)98 %02/28/17 23:57 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 02/23/17 18:42 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-6 Lab ID:92330540005 Collected:02/16/17 11:50 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 02/26/17 07:18 25057-89-002/22/17 16:550.090 0.045 1
2,4-D ND ug/L 02/26/17 07:18 94-75-7 L1,L302/22/17 16:550.89 0.21 1
Dalapon ND ug/L 02/26/17 07:18 75-99-0 L1,L302/22/17 16:550.87 0.41 1
2,4-DB ND ug/L 02/26/17 07:18 94-82-602/22/17 16:551.8 0.48 1
Dicamba ND ug/L 02/26/17 07:18 1918-00-902/22/17 16:550.089 0.029 1
Dichlorprop ND ug/L 02/26/17 07:18 120-36-502/22/17 16:550.62 0.18 1
Dinoseb ND ug/L 02/26/17 07:18 88-85-7 L1,L302/22/17 16:550.18 0.054 1
Pentachlorophenol ND ug/L 02/26/17 07:18 87-86-502/22/17 16:550.027 0.016 1
Picloram ND ug/L 02/26/17 07:18 1918-02-102/22/17 16:550.090 0.018 1
2,4,5-T ND ug/L 02/26/17 07:18 93-76-502/22/17 16:550.18 0.040 1
2,4,5-TP (Silvex)ND ug/L 02/26/17 07:18 93-72-102/22/17 16:550.18 0.047 1
Surrogates
2,4-DCAA (S)97 %02/26/17 07:18 19719-28-902/22/17 16:5539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:27 7440-36-002/21/17 19:256.0 3.9 1
Arsenic ND ug/L 02/28/17 05:27 7440-38-202/21/17 19:2510.0 5.0 1
Barium 50.4J ug/L 02/28/17 05:27 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:27 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:27 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:27 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:27 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:27 7440-50-802/21/17 19:2510.0 2.5 1
Lead ND ug/L 02/28/17 05:27 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:27 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:27 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:27 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium ND ug/L 02/28/17 05:27 7440-62-202/21/17 19:2525.0 2.5 1
Zinc ND ug/L 02/28/17 05:27 7440-66-602/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 02/24/17 18:52 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/24/17 02:56 7439-97-602/23/17 05:110.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/01/17 00:14 67-64-110010.0 1
Acrylonitrile ND ug/L 03/01/17 00:14 107-13-12001.9 1
Benzene ND ug/L 03/01/17 00:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/01/17 00:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/01/17 00:14 75-27-41.0 0.18 1
Bromoform ND ug/L 03/01/17 00:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/01/17 00:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/01/17 00:14 78-93-31000.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-6 Lab ID:92330540005 Collected:02/16/17 11:50 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon disulfide ND ug/L 03/01/17 00:14 75-15-01001.2 1
Carbon tetrachloride ND ug/L 03/01/17 00:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/01/17 00:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/01/17 00:14 75-00-310.0 0.54 1
Chloroform ND ug/L 03/01/17 00:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/01/17 00:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/01/17 00:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/01/17 00:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/01/17 00:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/01/17 00:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/01/17 00:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/01/17 00:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/01/17 00:14 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 03/01/17 00:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/01/17 00:14 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/01/17 00:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/01/17 00:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/01/17 00:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/01/17 00:14 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 03/01/17 00:14 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/01/17 00:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/01/17 00:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/01/17 00:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/01/17 00:14 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/01/17 00:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/01/17 00:14 108-10-11000.33 1
Styrene ND ug/L 03/01/17 00:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/01/17 00:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/01/17 00:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/01/17 00:14 127-18-41.0 0.46 1
Toluene ND ug/L 03/01/17 00:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/01/17 00:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/01/17 00:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/01/17 00:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/01/17 00:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/01/17 00:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/01/17 00:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/01/17 00:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/01/17 00:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)89 %03/01/17 00:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %03/01/17 00:14 17060-07-070-130 1
Toluene-d8 (S)106 %03/01/17 00:14 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 02/23/17 18:43 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-7 Lab ID:92330540006 Collected:02/16/17 11:20 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:40 7440-36-002/21/17 19:256.0 3.9 1
Arsenic 21.5 ug/L 02/28/17 05:40 7440-38-202/21/17 19:2510.0 5.0 1
Barium 19.7J ug/L 02/28/17 05:40 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:40 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:40 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:40 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt 8.8J ug/L 02/28/17 05:40 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:40 7440-50-802/21/17 19:2510.0 2.5 1
Lead 5.9J ug/L 02/28/17 05:40 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:40 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:40 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:40 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium 8.7J ug/L 02/28/17 05:40 7440-62-202/21/17 19:2525.0 2.5 1
Zinc ND ug/L 02/28/17 05:40 7440-66-602/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.38J ug/L 02/24/17 18:54 7440-28-002/23/17 02:205.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/24/17 02:58 7439-97-602/23/17 05:110.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 02/21/17 19:43 83-32-902/20/17 14:0810.0 0.25 1
Acenaphthylene ND ug/L 02/21/17 19:43 208-96-802/20/17 14:0810.0 0.21 1
Aniline ND ug/L 02/21/17 19:43 62-53-302/20/17 14:0810.0 1.3 1
Anthracene ND ug/L 02/21/17 19:43 120-12-702/20/17 14:0810.0 0.14 1
Benzo(a)anthracene ND ug/L 02/21/17 19:43 56-55-302/20/17 14:0810.0 0.33 1
Benzo(a)pyrene ND ug/L 02/21/17 19:43 50-32-802/20/17 14:0810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 02/21/17 19:43 205-99-202/20/17 14:0810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 02/21/17 19:43 191-24-202/20/17 14:0810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 02/21/17 19:43 207-08-902/20/17 14:0810.0 0.43 1
Benzoic Acid ND ug/L 02/21/17 19:43 65-85-002/20/17 14:0850.0 11.1 1
Benzyl alcohol ND ug/L 02/21/17 19:43 100-51-602/20/17 14:0820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 02/21/17 19:43 101-55-302/20/17 14:0810.0 1.3 1
Butylbenzylphthalate ND ug/L 02/21/17 19:43 85-68-702/20/17 14:0810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 02/21/17 19:43 59-50-702/20/17 14:0820.0 4.2 1
4-Chloroaniline ND ug/L 02/21/17 19:43 106-47-802/20/17 14:0820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 02/21/17 19:43 111-91-102/20/17 14:0810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 02/21/17 19:43 111-44-402/20/17 14:0810.0 1.5 1
2-Chloronaphthalene ND ug/L 02/21/17 19:43 91-58-702/20/17 14:0810.0 2.2 1
2-Chlorophenol ND ug/L 02/21/17 19:43 95-57-802/20/17 14:0810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 02/21/17 19:43 7005-72-302/20/17 14:0810.0 2.1 1
Chrysene ND ug/L 02/21/17 19:43 218-01-902/20/17 14:0810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 02/21/17 19:43 53-70-302/20/17 14:0810.0 0.55 1
Dibenzofuran ND ug/L 02/21/17 19:43 132-64-902/20/17 14:0810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 02/21/17 19:43 95-50-102/20/17 14:0810.0 1.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 26 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-7 Lab ID:92330540006 Collected:02/16/17 11:20 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1,3-Dichlorobenzene ND ug/L 02/21/17 19:43 541-73-102/20/17 14:0810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 02/21/17 19:43 106-46-702/20/17 14:0810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 02/21/17 19:43 91-94-102/20/17 14:0820.0 1.4 1
2,4-Dichlorophenol ND ug/L 02/21/17 19:43 120-83-202/20/17 14:0810.0 1.7 1
Diethylphthalate ND ug/L 02/21/17 19:43 84-66-202/20/17 14:0860001.3 1
2,4-Dimethylphenol ND ug/L 02/21/17 19:43 105-67-902/20/17 14:0810.0 2.2 1
Dimethylphthalate ND ug/L 02/21/17 19:43 131-11-302/20/17 14:0810.0 1.5 1
Di-n-butylphthalate ND ug/L 02/21/17 19:43 84-74-202/20/17 14:0810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 02/21/17 19:43 534-52-102/20/17 14:0850.0 1.7 1
2,4-Dinitrophenol ND ug/L 02/21/17 19:43 51-28-502/20/17 14:0850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 02/21/17 19:43 121-14-202/20/17 14:0810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 02/21/17 19:43 606-20-202/20/17 14:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 02/21/17 19:43 117-84-002/20/17 14:0810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 02/21/17 19:43 117-81-702/20/17 14:0815.0 0.85 1
Fluoranthene ND ug/L 02/21/17 19:43 206-44-002/20/17 14:0810.0 0.21 1
Fluorene ND ug/L 02/21/17 19:43 86-73-702/20/17 14:0810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 02/21/17 19:43 87-68-302/20/17 14:0810.0 1.8 1
Hexachlorobenzene ND ug/L 02/21/17 19:43 118-74-102/20/17 14:0810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 02/21/17 19:43 77-47-402/20/17 14:0810.0 1.8 1
Hexachloroethane ND ug/L 02/21/17 19:43 67-72-102/20/17 14:0810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/21/17 19:43 193-39-502/20/17 14:0810.0 0.29 1
Isophorone ND ug/L 02/21/17 19:43 78-59-102/20/17 14:0810.0 1.8 1
1-Methylnaphthalene ND ug/L 02/21/17 19:43 90-12-002/20/17 14:0810.0 0.32 1
2-Methylnaphthalene ND ug/L 02/21/17 19:43 91-57-602/20/17 14:0810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 02/21/17 19:43 95-48-702/20/17 14:0810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 02/21/17 19:4302/20/17 14:0810.0 1.7 1
Naphthalene ND ug/L 02/21/17 19:43 91-20-302/20/17 14:0810.0 0.34 1
2-Nitroaniline ND ug/L 02/21/17 19:43 88-74-402/20/17 14:0850.0 2.8 1
3-Nitroaniline ND ug/L 02/21/17 19:43 99-09-202/20/17 14:0850.0 2.4 1
4-Nitroaniline ND ug/L 02/21/17 19:43 100-01-602/20/17 14:0820.0 2.5 1
Nitrobenzene ND ug/L 02/21/17 19:43 98-95-302/20/17 14:0810.0 1.7 1
2-Nitrophenol ND ug/L 02/21/17 19:43 88-75-502/20/17 14:0810.0 1.7 1
4-Nitrophenol ND ug/L 02/21/17 19:43 100-02-702/20/17 14:0850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 02/21/17 19:43 62-75-902/20/17 14:0810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 02/21/17 19:43 621-64-702/20/17 14:0810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 02/21/17 19:43 86-30-602/20/17 14:0810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 02/21/17 19:43 108-60-102/20/17 14:0810.0 1.6 1
Pentachlorophenol ND ug/L 02/21/17 19:43 87-86-502/20/17 14:0825.0 2.3 1
Phenanthrene ND ug/L 02/21/17 19:43 85-01-802/20/17 14:0810.0 0.22 1
Phenol ND ug/L 02/21/17 19:4302/20/17 14:0810.0 1.7 1
Pyrene ND ug/L 02/21/17 19:43 129-00-002/20/17 14:0810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 02/21/17 19:43 120-82-102/20/17 14:0810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 02/21/17 19:43 95-95-402/20/17 14:0810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 02/21/17 19:43 88-06-202/20/17 14:0810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)67 %02/21/17 19:43 4165-60-002/20/17 14:0821-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-7 Lab ID:92330540006 Collected:02/16/17 11:20 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
2-Fluorobiphenyl (S)69 %02/21/17 19:43 321-60-802/20/17 14:0827-110 1
Terphenyl-d14 (S)81 %02/21/17 19:43 1718-51-002/20/17 14:0831-107 1
Phenol-d6 (S)35 %02/21/17 19:43 13127-88-302/20/17 14:0810-110 1
2-Fluorophenol (S)45 %02/21/17 19:43 367-12-402/20/17 14:0812-110 1
2,4,6-Tribromophenol (S)79 %02/21/17 19:43 118-79-602/20/17 14:0827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/01/17 00:31 67-64-110010.0 1
Acrylonitrile ND ug/L 03/01/17 00:31 107-13-12001.9 1
Benzene ND ug/L 03/01/17 00:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/01/17 00:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/01/17 00:31 75-27-41.0 0.18 1
Bromoform ND ug/L 03/01/17 00:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/01/17 00:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/01/17 00:31 78-93-31000.96 1
Carbon disulfide ND ug/L 03/01/17 00:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 03/01/17 00:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/01/17 00:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/01/17 00:31 75-00-310.0 0.54 1
Chloroform ND ug/L 03/01/17 00:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/01/17 00:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/01/17 00:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/01/17 00:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/01/17 00:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/01/17 00:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/01/17 00:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/01/17 00:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/01/17 00:31 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 03/01/17 00:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/01/17 00:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/01/17 00:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/01/17 00:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/01/17 00:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/01/17 00:31 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 03/01/17 00:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/01/17 00:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/01/17 00:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/01/17 00:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/01/17 00:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/01/17 00:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/01/17 00:31 108-10-11000.33 1
Styrene ND ug/L 03/01/17 00:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/01/17 00:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/01/17 00:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/01/17 00:31 127-18-41.0 0.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-7 Lab ID:92330540006 Collected:02/16/17 11:20 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Toluene ND ug/L 03/01/17 00:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/01/17 00:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/01/17 00:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/01/17 00:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/01/17 00:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/01/17 00:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/01/17 00:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/01/17 00:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/01/17 00:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)93 %03/01/17 00:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %03/01/17 00:31 17060-07-070-130 1
Toluene-d8 (S)108 %03/01/17 00:31 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 02/23/17 18:43 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-9 Lab ID:92330540007 Collected:02/16/17 09:55 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:43 7440-36-002/21/17 19:256.0 3.9 1
Arsenic ND ug/L 02/28/17 05:43 7440-38-202/21/17 19:2510.0 5.0 1
Barium 55.2J ug/L 02/28/17 05:43 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:43 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:43 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:43 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:43 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:43 7440-50-802/21/17 19:2510.0 2.5 1
Lead 2.7J ug/L 02/28/17 05:43 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:43 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:43 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:43 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium ND ug/L 02/28/17 05:43 7440-62-202/21/17 19:2525.0 2.5 1
Zinc ND ug/L 02/28/17 05:43 7440-66-602/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.027J ug/L 02/24/17 20:03 7440-28-002/23/17 01:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/24/17 03:01 7439-97-602/23/17 05:110.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 17:53 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 17:53 107-13-12001.9 1
Benzene ND ug/L 02/27/17 17:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 17:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 17:53 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 17:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 17:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 17:53 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 17:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 17:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 17:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 17:53 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 17:53 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 17:53 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 17:53 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 17:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 17:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 17:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 17:53 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 17:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 17:53 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 17:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 17:53 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 17:53 75-35-45.0 0.56 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-9 Lab ID:92330540007 Collected:02/16/17 09:55 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,2-Dichloroethene ND ug/L 02/27/17 17:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 17:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 17:53 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/27/17 17:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 17:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 17:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 17:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 17:53 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 17:53 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 17:53 108-10-11000.33 1
Styrene ND ug/L 02/27/17 17:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 17:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 17:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 17:53 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 17:53 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 17:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 17:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 17:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 17:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 17:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 17:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 17:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 17:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %02/27/17 17:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %02/27/17 17:53 17060-07-070-130 1
Toluene-d8 (S)93 %02/27/17 17:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-10 Lab ID:92330540008 Collected:02/16/17 10:20 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 02/28/17 05:46 7440-36-002/21/17 19:256.0 3.9 1
Arsenic ND ug/L 02/28/17 05:46 7440-38-202/21/17 19:2510.0 5.0 1
Barium 27.1J ug/L 02/28/17 05:46 7440-39-302/21/17 19:251002.5 1
Beryllium ND ug/L 02/28/17 05:46 7440-41-702/21/17 19:251.0 0.50 1
Cadmium ND ug/L 02/28/17 05:46 7440-43-902/21/17 19:251.0 0.50 1
Chromium ND ug/L 02/28/17 05:46 7440-47-302/21/17 19:2510.0 2.5 1
Cobalt ND ug/L 02/28/17 05:46 7440-48-402/21/17 19:2510.0 2.5 1
Copper ND ug/L 02/28/17 05:46 7440-50-802/21/17 19:2510.0 2.5 1
Lead 2.7J ug/L 02/28/17 05:46 7439-92-102/21/17 19:2510.0 2.5 1
Nickel ND ug/L 02/28/17 05:46 7440-02-002/21/17 19:2550.0 2.5 1
Selenium ND ug/L 02/28/17 05:46 7782-49-202/21/17 19:2510.0 5.0 1
Silver ND ug/L 02/28/17 05:46 7440-22-402/21/17 19:2510.0 2.5 1
Vanadium ND ug/L 02/28/17 05:46 7440-62-202/21/17 19:2525.0 2.5 1
Zinc ND ug/L 02/28/17 05:46 7440-66-602/21/17 19:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.032J ug/L 02/24/17 20:08 7440-28-002/23/17 01:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 18:10 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 18:10 107-13-12001.9 1
Benzene ND ug/L 02/27/17 18:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 18:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 18:10 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 18:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 18:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 18:10 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 18:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 18:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 18:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 18:10 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 18:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 18:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 18:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 18:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 18:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 18:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 18:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 18:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 18:10 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 18:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 18:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 18:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/27/17 18:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 18:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 18:10 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-10 Lab ID:92330540008 Collected:02/16/17 10:20 Received:02/17/17 08:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/27/17 18:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 18:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 18:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 18:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 18:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 18:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 18:10 108-10-11000.33 1
Styrene ND ug/L 02/27/17 18:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 18:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 18:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 18:10 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 18:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 18:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 18:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 18:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 18:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 18:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 18:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 18:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 18:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)92 %02/27/17 18:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/27/17 18:10 17060-07-070-130 1
Toluene-d8 (S)100 %02/27/17 18:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-2 Lab ID:92330519013 Collected:02/17/17 10:19 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 06:42 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 06:42 7440-38-202/23/17 19:3510.0 5.0 1
Barium 15.2J ug/L 03/03/17 06:42 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 06:42 7440-41-702/23/17 19:351.0 0.50 1
Cadmium ND ug/L 03/03/17 06:42 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 06:42 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 06:42 7440-48-402/23/17 19:3510.0 2.5 1
Copper 28.8 ug/L 03/03/17 06:42 7440-50-802/23/17 19:3510.0 2.5 1
Lead 9.4J ug/L 03/03/17 06:42 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 06:42 7440-02-002/23/17 19:3550.0 2.5 1
Selenium 16.4 ug/L 03/03/17 06:42 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 06:42 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium 4.2J ug/L 03/03/17 06:42 7440-62-202/23/17 19:3525.0 2.5 1
Zinc 9.5J ug/L 03/03/17 06:42 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.034J ug/L 02/24/17 20:22 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 02/27/17 17:06 83-32-902/23/17 13:0710.0 0.25 1
Acenaphthylene ND ug/L 02/27/17 17:06 208-96-802/23/17 13:0710.0 0.21 1
Aniline ND ug/L 02/27/17 17:06 62-53-302/23/17 13:0710.0 1.3 1
Anthracene ND ug/L 02/27/17 17:06 120-12-702/23/17 13:0710.0 0.14 1
Benzo(a)anthracene ND ug/L 02/27/17 17:06 56-55-302/23/17 13:0710.0 0.33 1
Benzo(a)pyrene ND ug/L 02/27/17 17:06 50-32-802/23/17 13:0710.0 0.30 1
Benzo(b)fluoranthene ND ug/L 02/27/17 17:06 205-99-202/23/17 13:0710.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 02/27/17 17:06 191-24-202/23/17 13:0710.0 0.38 1
Benzo(k)fluoranthene ND ug/L 02/27/17 17:06 207-08-902/23/17 13:0710.0 0.43 1
Benzoic Acid ND ug/L 02/27/17 17:06 65-85-002/23/17 13:0750.0 11.1 1
Benzyl alcohol ND ug/L 02/27/17 17:06 100-51-602/23/17 13:0720.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 02/27/17 17:06 101-55-302/23/17 13:0710.0 1.3 1
Butylbenzylphthalate ND ug/L 02/27/17 17:06 85-68-702/23/17 13:0710.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 02/27/17 17:06 59-50-702/23/17 13:0720.0 4.2 1
4-Chloroaniline ND ug/L 02/27/17 17:06 106-47-802/23/17 13:0720.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 02/27/17 17:06 111-91-102/23/17 13:0710.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 02/27/17 17:06 111-44-402/23/17 13:0710.0 1.5 1
2-Chloronaphthalene ND ug/L 02/27/17 17:06 91-58-702/23/17 13:0710.0 2.2 1
2-Chlorophenol ND ug/L 02/27/17 17:06 95-57-802/23/17 13:0710.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 02/27/17 17:06 7005-72-302/23/17 13:0710.0 2.1 1
Chrysene ND ug/L 02/27/17 17:06 218-01-902/23/17 13:0710.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 02/27/17 17:06 53-70-302/23/17 13:0710.0 0.55 1
Dibenzofuran ND ug/L 02/27/17 17:06 132-64-902/23/17 13:0710.0 1.8 1
1,2-Dichlorobenzene ND ug/L 02/27/17 17:06 95-50-102/23/17 13:0710.0 1.2 1
1,3-Dichlorobenzene ND ug/L 02/27/17 17:06 541-73-102/23/17 13:0710.0 1.1 1
1,4-Dichlorobenzene ND ug/L 02/27/17 17:06 106-46-702/23/17 13:0710.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 02/27/17 17:06 91-94-102/23/17 13:0720.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-2 Lab ID:92330519013 Collected:02/17/17 10:19 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 02/27/17 17:06 120-83-202/23/17 13:0710.0 1.7 1
Diethylphthalate ND ug/L 02/27/17 17:06 84-66-202/23/17 13:0760001.3 1
2,4-Dimethylphenol ND ug/L 02/27/17 17:06 105-67-902/23/17 13:0710.0 2.2 1
Dimethylphthalate ND ug/L 02/27/17 17:06 131-11-302/23/17 13:0710.0 1.5 1
Di-n-butylphthalate ND ug/L 02/27/17 17:06 84-74-202/23/17 13:0710.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 02/27/17 17:06 534-52-102/23/17 13:0750.0 1.7 1
2,4-Dinitrophenol ND ug/L 02/27/17 17:06 51-28-502/23/17 13:0750.0 6.5 1
2,4-Dinitrotoluene ND ug/L 02/27/17 17:06 121-14-202/23/17 13:0710.0 1.2 1
2,6-Dinitrotoluene ND ug/L 02/27/17 17:06 606-20-202/23/17 13:0710.0 1.7 1
Di-n-octylphthalate ND ug/L 02/27/17 17:06 117-84-002/23/17 13:0710.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 02/27/17 17:06 117-81-702/23/17 13:0715.0 0.85 1
Fluoranthene ND ug/L 02/27/17 17:06 206-44-002/23/17 13:0710.0 0.21 1
Fluorene ND ug/L 02/27/17 17:06 86-73-702/23/17 13:0710.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 02/27/17 17:06 87-68-302/23/17 13:0710.0 1.8 1
Hexachlorobenzene ND ug/L 02/27/17 17:06 118-74-102/23/17 13:0710.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 02/27/17 17:06 77-47-402/23/17 13:0710.0 1.8 1
Hexachloroethane ND ug/L 02/27/17 17:06 67-72-102/23/17 13:0710.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/27/17 17:06 193-39-502/23/17 13:0710.0 0.29 1
Isophorone ND ug/L 02/27/17 17:06 78-59-102/23/17 13:0710.0 1.8 1
1-Methylnaphthalene ND ug/L 02/27/17 17:06 90-12-002/23/17 13:0710.0 0.32 1
2-Methylnaphthalene ND ug/L 02/27/17 17:06 91-57-602/23/17 13:0710.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 02/27/17 17:06 95-48-702/23/17 13:0710.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 02/27/17 17:0602/23/17 13:0710.0 1.7 1
Naphthalene ND ug/L 02/27/17 17:06 91-20-302/23/17 13:0710.0 0.34 1
2-Nitroaniline ND ug/L 02/27/17 17:06 88-74-402/23/17 13:0750.0 2.8 1
3-Nitroaniline ND ug/L 02/27/17 17:06 99-09-202/23/17 13:0750.0 2.4 1
4-Nitroaniline ND ug/L 02/27/17 17:06 100-01-602/23/17 13:0720.0 2.5 1
Nitrobenzene ND ug/L 02/27/17 17:06 98-95-302/23/17 13:0710.0 1.7 1
2-Nitrophenol ND ug/L 02/27/17 17:06 88-75-502/23/17 13:0710.0 1.7 1
4-Nitrophenol ND ug/L 02/27/17 17:06 100-02-702/23/17 13:0750.0 5.8 1
N-Nitrosodimethylamine ND ug/L 02/27/17 17:06 62-75-902/23/17 13:0710.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 02/27/17 17:06 621-64-702/23/17 13:0710.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 02/27/17 17:06 86-30-602/23/17 13:0710.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 02/27/17 17:06 108-60-102/23/17 13:0710.0 1.6 1
Pentachlorophenol ND ug/L 02/27/17 17:06 87-86-502/23/17 13:0725.0 2.3 1
Phenanthrene ND ug/L 02/27/17 17:06 85-01-802/23/17 13:0710.0 0.22 1
Phenol ND ug/L 02/27/17 17:0602/23/17 13:0710.0 1.7 1
Pyrene ND ug/L 02/27/17 17:06 129-00-002/23/17 13:0710.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 02/27/17 17:06 120-82-102/23/17 13:0710.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 02/27/17 17:06 95-95-402/23/17 13:0710.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 02/27/17 17:06 88-06-202/23/17 13:0710.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)71 %02/27/17 17:06 4165-60-002/23/17 13:0721-110 1
2-Fluorobiphenyl (S)76 %02/27/17 17:06 321-60-802/23/17 13:0727-110 1
Terphenyl-d14 (S)79 %02/27/17 17:06 1718-51-002/23/17 13:0731-107 1
Phenol-d6 (S)21 %02/27/17 17:06 13127-88-302/23/17 13:0710-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-2 Lab ID:92330519013 Collected:02/17/17 10:19 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
2-Fluorophenol (S)32 %02/27/17 17:06 367-12-402/23/17 13:0712-110 1
2,4,6-Tribromophenol (S)84 %02/27/17 17:06 118-79-602/23/17 13:0727-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 22:06 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 22:06 107-13-12001.9 1
Benzene ND ug/L 02/27/17 22:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 22:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 22:06 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 22:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 22:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 22:06 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 22:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 22:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 22:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 22:06 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 22:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 22:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 22:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 22:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 22:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 22:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 22:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 22:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 22:06 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 22:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 22:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 22:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.20J ug/L 02/27/17 22:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 22:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 22:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/27/17 22:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 22:06 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 22:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 22:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 22:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 22:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 22:06 108-10-11000.33 1
Styrene ND ug/L 02/27/17 22:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 22:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 22:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 22:06 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 22:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 22:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 22:06 79-00-51.0 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-2 Lab ID:92330519013 Collected:02/17/17 10:19 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Trichloroethene ND ug/L 02/27/17 22:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 22:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 22:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 22:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 22:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 22:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/27/17 22:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/27/17 22:06 17060-07-070-130 1
Toluene-d8 (S)93 %02/27/17 22:06 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 03/01/17 13:43 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-8 Lab ID:92330519014 Collected:02/17/17 10:15 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 06:45 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 06:45 7440-38-202/23/17 19:3510.0 5.0 1
Barium 12.1J ug/L 03/03/17 06:45 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 06:45 7440-41-702/23/17 19:351.0 0.50 1
Cadmium ND ug/L 03/03/17 06:45 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 06:45 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 06:45 7440-48-402/23/17 19:3510.0 2.5 1
Copper ND ug/L 03/03/17 06:45 7440-50-802/23/17 19:3510.0 2.5 1
Lead ND ug/L 03/03/17 06:45 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 06:45 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 06:45 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 06:45 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium ND ug/L 03/03/17 06:45 7440-62-202/23/17 19:3525.0 2.5 1
Zinc ND ug/L 03/03/17 06:45 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.055J ug/L 02/24/17 20:28 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 22:23 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 22:23 107-13-12001.9 1
Benzene ND ug/L 02/27/17 22:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 22:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 22:23 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 22:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 22:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 22:23 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 22:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 22:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 22:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 22:23 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 22:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 22:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 22:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 22:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 22:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 22:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 22:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 22:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 22:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 22:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 22:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 22:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/27/17 22:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 22:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 22:23 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-8 Lab ID:92330519014 Collected:02/17/17 10:15 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/27/17 22:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 22:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 22:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 22:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 22:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 22:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 22:23 108-10-11000.33 1
Styrene ND ug/L 02/27/17 22:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 22:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 22:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 22:23 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 22:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 22:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 22:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 22:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 22:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 22:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 22:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 22:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 22:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/17 22:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %02/27/17 22:23 17060-07-070-130 1
Toluene-d8 (S)108 %02/27/17 22:23 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 03/01/17 13:44 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-11 Lab ID:92330519015 Collected:02/17/17 13:00 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 06:48 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 06:48 7440-38-202/23/17 19:3510.0 5.0 1
Barium 22.4J ug/L 03/03/17 06:48 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 06:48 7440-41-702/23/17 19:351.0 0.50 1
Cadmium 1.2 ug/L 03/03/17 06:48 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 06:48 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 06:48 7440-48-402/23/17 19:3510.0 2.5 1
Copper ND ug/L 03/03/17 06:48 7440-50-802/23/17 19:3510.0 2.5 1
Lead ND ug/L 03/03/17 06:48 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 06:48 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 06:48 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 06:48 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium ND ug/L 03/03/17 06:48 7440-62-202/23/17 19:3525.0 2.5 1
Zinc ND ug/L 03/03/17 06:48 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.042J ug/L 02/24/17 20:29 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.22 ug/L 03/03/17 16:39 7439-97-603/01/17 07:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 22:40 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 22:40 107-13-12001.9 1
Benzene ND ug/L 02/27/17 22:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 22:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 22:40 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 22:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 22:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 22:40 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 22:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 22:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 22:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 22:40 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 22:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 22:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 22:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 22:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 22:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 22:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 22:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 22:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 22:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 22:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 22:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 22:40 75-35-45.0 0.56 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-11 Lab ID:92330519015 Collected:02/17/17 13:00 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,2-Dichloroethene ND ug/L 02/27/17 22:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 22:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 22:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/27/17 22:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 22:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 22:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 22:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 22:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 22:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 22:40 108-10-11000.33 1
Styrene ND ug/L 02/27/17 22:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 22:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 22:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 22:40 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 22:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 22:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 22:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 22:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 22:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 22:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 22:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 22:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 22:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/17 22:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %02/27/17 22:40 17060-07-070-130 1
Toluene-d8 (S)107 %02/27/17 22:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-12 Lab ID:92330519016 Collected:02/17/17 11:30 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 07:00 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 07:00 7440-38-202/23/17 19:3510.0 5.0 1
Barium 94.5J ug/L 03/03/17 07:00 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 07:00 7440-41-702/23/17 19:351.0 0.50 1
Cadmium ND ug/L 03/03/17 07:00 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 07:00 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt 29.2 ug/L 03/03/17 07:00 7440-48-402/23/17 19:3510.0 2.5 1
Copper ND ug/L 03/03/17 07:00 7440-50-802/23/17 19:3510.0 2.5 1
Lead ND ug/L 03/03/17 07:00 7439-92-102/23/17 19:3510.0 2.5 1
Nickel 2.6J ug/L 03/03/17 07:00 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 07:00 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 07:00 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium ND ug/L 03/03/17 07:00 7440-62-202/23/17 19:3525.0 2.5 1
Zinc 22.2 ug/L 03/03/17 07:00 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.18J ug/L 02/24/17 20:31 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 22:56 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 22:56 107-13-12001.9 1
Benzene 0.30J ug/L 02/27/17 22:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 22:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 22:56 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 22:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 22:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 22:56 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 22:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 22:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 22:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 22:56 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 22:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 22:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 22:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 22:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 22:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 22:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 22:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 22:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 22:56 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 22:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 22:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 22:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/27/17 22:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 22:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 22:56 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-12 Lab ID:92330519016 Collected:02/17/17 11:30 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/27/17 22:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 22:56 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 22:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 22:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 22:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 22:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 22:56 108-10-11000.33 1
Styrene ND ug/L 02/27/17 22:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 22:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 22:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 22:56 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 22:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 22:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 22:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 22:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 22:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 22:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 22:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 22:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 22:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)83 %02/27/17 22:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/27/17 22:56 17060-07-070-130 1
Toluene-d8 (S)96 %02/27/17 22:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-14 Lab ID:92330519017 Collected:02/17/17 11:40 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 07:03 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 07:03 7440-38-202/23/17 19:3510.0 5.0 1
Barium 48.1J ug/L 03/03/17 07:03 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 07:03 7440-41-702/23/17 19:351.0 0.50 1
Cadmium ND ug/L 03/03/17 07:03 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 07:03 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 07:03 7440-48-402/23/17 19:3510.0 2.5 1
Copper ND ug/L 03/03/17 07:03 7440-50-802/23/17 19:3510.0 2.5 1
Lead ND ug/L 03/03/17 07:03 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 07:03 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 07:03 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 07:03 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium ND ug/L 03/03/17 07:03 7440-62-202/23/17 19:3525.0 2.5 1
Zinc ND ug/L 03/03/17 07:03 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 02/24/17 20:33 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 23:13 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 23:13 107-13-12001.9 1
Benzene ND ug/L 02/27/17 23:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 23:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 23:13 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 23:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 23:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 23:13 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 23:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 23:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 23:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 23:13 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 23:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 23:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 23:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 23:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 23:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 23:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 23:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 23:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 23:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 23:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 23:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 23:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/27/17 23:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 23:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 23:13 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-14 Lab ID:92330519017 Collected:02/17/17 11:40 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/27/17 23:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 23:13 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 23:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 23:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 23:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 23:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 23:13 108-10-11000.33 1
Styrene ND ug/L 02/27/17 23:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 23:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 23:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 23:13 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 23:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 23:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 23:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 23:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 23:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 23:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 23:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 23:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 23:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %02/27/17 23:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %02/27/17 23:13 17060-07-070-130 1
Toluene-d8 (S)116 %02/27/17 23:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-15 Lab ID:92330519018 Collected:02/17/17 11:00 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 07:06 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 07:06 7440-38-202/23/17 19:3510.0 5.0 1
Barium ND ug/L 03/03/17 07:06 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 07:06 7440-41-702/23/17 19:351.0 0.50 1
Cadmium 8.0 ug/L 03/03/17 07:06 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 07:06 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 07:06 7440-48-402/23/17 19:3510.0 2.5 1
Copper ND ug/L 03/03/17 07:06 7440-50-802/23/17 19:3510.0 2.5 1
Lead ND ug/L 03/03/17 07:06 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 07:06 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 07:06 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 07:06 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium ND ug/L 03/03/17 07:06 7440-62-202/23/17 19:3525.0 2.5 1
Zinc ND ug/L 03/03/17 07:06 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 02/24/17 20:35 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/27/17 23:30 67-64-110010.0 1
Acrylonitrile ND ug/L 02/27/17 23:30 107-13-12001.9 1
Benzene ND ug/L 02/27/17 23:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/27/17 23:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/27/17 23:30 75-27-41.0 0.18 1
Bromoform ND ug/L 02/27/17 23:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/27/17 23:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/27/17 23:30 78-93-31000.96 1
Carbon disulfide ND ug/L 02/27/17 23:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/27/17 23:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/27/17 23:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/27/17 23:30 75-00-310.0 0.54 1
Chloroform ND ug/L 02/27/17 23:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/27/17 23:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/17 23:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/27/17 23:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/17 23:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/27/17 23:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/27/17 23:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/27/17 23:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/27/17 23:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/27/17 23:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/27/17 23:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/27/17 23:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/27/17 23:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/27/17 23:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/27/17 23:30 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-15 Lab ID:92330519018 Collected:02/17/17 11:00 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/27/17 23:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/27/17 23:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/27/17 23:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/27/17 23:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/27/17 23:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/27/17 23:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/17 23:30 108-10-11000.33 1
Styrene ND ug/L 02/27/17 23:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/17 23:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/17 23:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/27/17 23:30 127-18-41.0 0.46 1
Toluene ND ug/L 02/27/17 23:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/27/17 23:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/27/17 23:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/27/17 23:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/27/17 23:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/27/17 23:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/27/17 23:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/27/17 23:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/27/17 23:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %02/27/17 23:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/27/17 23:30 17060-07-070-130 1
Toluene-d8 (S)106 %02/27/17 23:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-16R Lab ID:92330519019 Collected:02/17/17 15:00 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 07:09 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 07:09 7440-38-202/23/17 19:3510.0 5.0 1
Barium 35.4J ug/L 03/03/17 07:09 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 07:09 7440-41-702/23/17 19:351.0 0.50 1
Cadmium 0.52J ug/L 03/03/17 07:09 7440-43-902/23/17 19:351.0 0.50 1
Chromium 9.8J ug/L 03/03/17 07:09 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 07:09 7440-48-402/23/17 19:3510.0 2.5 1
Copper 12.3 ug/L 03/03/17 07:09 7440-50-802/23/17 19:3510.0 2.5 1
Lead 5.8J ug/L 03/03/17 07:09 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 07:09 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 07:09 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 07:09 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium 14.6J ug/L 03/03/17 07:09 7440-62-202/23/17 19:3525.0 2.5 1
Zinc 11.6 ug/L 03/03/17 07:09 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.022J ug/L 02/24/17 20:37 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 02:19 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 02:19 107-13-12001.9 1
Benzene ND ug/L 02/28/17 02:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 02:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 02:19 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 02:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 02:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 02:19 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 02:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 02:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 02:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 02:19 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 02:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 02:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 02:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 02:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 02:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 02:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 02:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 02:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 02:19 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 02:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 02:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 02:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/17 02:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 02:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 02:19 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:MW-16R Lab ID:92330519019 Collected:02/17/17 15:00 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/28/17 02:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 02:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 02:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 02:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 02:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 02:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 02:19 108-10-11000.33 1
Styrene ND ug/L 02/28/17 02:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 02:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 02:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 02:19 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/17 02:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 02:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 02:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 02:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 02:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 02:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 02:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 02:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 02:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)89 %02/28/17 02:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %02/28/17 02:19 17060-07-070-130 1
Toluene-d8 (S)94 %02/28/17 02:19 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 03/01/17 13:45 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 117
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:SW-5 Lab ID:92330519020 Collected:02/17/17 10:45 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 03/03/17 07:12 7440-36-002/23/17 19:356.0 3.9 1
Arsenic ND ug/L 03/03/17 07:12 7440-38-202/23/17 19:3510.0 5.0 1
Barium 187 ug/L 03/03/17 07:12 7440-39-302/23/17 19:351002.5 1
Beryllium ND ug/L 03/03/17 07:12 7440-41-702/23/17 19:351.0 0.50 1
Cadmium 0.65J ug/L 03/03/17 07:12 7440-43-902/23/17 19:351.0 0.50 1
Chromium ND ug/L 03/03/17 07:12 7440-47-302/23/17 19:3510.0 2.5 1
Cobalt ND ug/L 03/03/17 07:12 7440-48-402/23/17 19:3510.0 2.5 1
Copper ND ug/L 03/03/17 07:12 7440-50-802/23/17 19:3510.0 2.5 1
Lead ND ug/L 03/03/17 07:12 7439-92-102/23/17 19:3510.0 2.5 1
Nickel ND ug/L 03/03/17 07:12 7440-02-002/23/17 19:3550.0 2.5 1
Selenium ND ug/L 03/03/17 07:12 7782-49-202/23/17 19:3510.0 5.0 1
Silver ND ug/L 03/03/17 07:12 7440-22-402/23/17 19:3510.0 2.5 1
Vanadium ND ug/L 03/03/17 07:12 7440-62-202/23/17 19:3525.0 2.5 1
Zinc 8.7J ug/L 03/03/17 07:12 7440-66-602/23/17 19:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.029J ug/L 02/24/17 20:45 7440-28-002/24/17 02:155.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/28/17 02:36 67-64-110010.0 1
Acrylonitrile ND ug/L 02/28/17 02:36 107-13-12001.9 1
Benzene ND ug/L 02/28/17 02:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/17 02:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/28/17 02:36 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/17 02:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/28/17 02:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/17 02:36 78-93-31000.96 1
Carbon disulfide ND ug/L 02/28/17 02:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/28/17 02:36 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/17 02:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/28/17 02:36 75-00-310.0 0.54 1
Chloroform ND ug/L 02/28/17 02:36 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/28/17 02:36 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/17 02:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/28/17 02:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/17 02:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/17 02:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/17 02:36 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/28/17 02:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/17 02:36 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/28/17 02:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/17 02:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/28/17 02:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/17 02:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/17 02:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/17 02:36 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Sample:SW-5 Lab ID:92330519020 Collected:02/17/17 10:45 Received:02/22/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 02/28/17 02:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/17 02:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/17 02:36 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/28/17 02:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/28/17 02:36 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/28/17 02:36 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/17 02:36 108-10-11000.33 1
Styrene ND ug/L 02/28/17 02:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/17 02:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/17 02:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/28/17 02:36 127-18-41.0 0.46 1
Toluene 0.26J ug/L 02/28/17 02:36 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/17 02:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/17 02:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/17 02:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/17 02:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/17 02:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/17 02:36 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/28/17 02:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/17 02:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/28/17 02:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %02/28/17 02:36 17060-07-070-130 1
Toluene-d8 (S)101 %02/28/17 02:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Huntersville, NC 28078
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Page 51 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349177
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936998
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 02/23/17 17:030.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936999LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937000MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330396004
1937001
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 93 75-12591 1 252.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349477
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92330540001, 92330540002, 92330540003, 92330540005, 92330540006, 92330540007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1938932
Associated Lab Samples:92330540001, 92330540002, 92330540003, 92330540005, 92330540006, 92330540007
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 02/24/17 02:060.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1938933LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1938934MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330674021
1938935
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-12597 3 252.5ND 2.5 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350064
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92330519015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941842
Associated Lab Samples:92330519015
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 03/03/17 15:390.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941843LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1941844MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330875004
1941845
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 96 75-12599 2 252.5ND 2.4 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
348994
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92330519001, 92330539001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936214
Associated Lab Samples:92330519001, 92330539001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 02/24/17 05:123.9
Arsenic ug/L ND 10.0 02/24/17 05:125.0
Barium ug/L ND 5.0 02/24/17 05:122.5
Beryllium ug/L ND 1.0 02/24/17 05:120.50
Cadmium ug/L ND 1.0 02/24/17 05:120.50
Chromium ug/L ND 5.0 02/24/17 05:122.5
Cobalt ug/L ND 5.0 02/24/17 05:122.5
Copper ug/L ND 5.0 02/24/17 05:122.5
Lead ug/L ND 5.0 02/24/17 05:122.5
Nickel ug/L ND 5.0 02/24/17 05:122.5
Selenium ug/L ND 10.0 02/24/17 05:125.0
Silver ug/L ND 5.0 02/24/17 05:122.5
Tin ug/L ND 5.0 02/24/17 05:122.5
Vanadium ug/L ND 5.0 02/24/17 05:122.5
Zinc ug/L ND 10.0 02/24/17 05:155.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936215LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 479500 96 80-120
Arsenic ug/L 469500 94 80-120
Barium ug/L 493500 99 80-120
Beryllium ug/L 491500 98 80-120
Cadmium ug/L 479500 96 80-120
Chromium ug/L 496500 99 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 487500 97 80-120
Lead ug/L 470500 94 80-120
Nickel ug/L 481500 96 80-120
Selenium ug/L 467500 93 80-120
Silver ug/L 239250 96 80-120
Tin ug/L 483500 97 80-120
Vanadium ug/L 482500 96 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1936216MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330396001
1936217
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12596 2 20500ND489478
Arsenic ug/L 500 97 75-12595 2 20500ND483473
Barium ug/L 500 96 75-12595 1 205007.2 488 481
Beryllium ug/L 500 97 75-12595 1 20500ND483477
Cadmium ug/L 500 96 75-12594 3 20500ND482470
Chromium ug/L 500 98 75-12595 3 20500ND488476
Cobalt ug/L 500 96 75-12593 2 20500ND478466
Copper ug/L 500 98 75-12595 2 20500ND488477
Lead ug/L 500 93 75-12591 2 20500ND467457
Nickel ug/L 500 96 75-12593 3 20500ND478466
Selenium ug/L 500 94 75-12592 2 20500ND471462
Silver ug/L 250 96 75-12593 3 20250ND240234
Tin ug/L 500 98 75-12596 2 20500ND490479
Vanadium ug/L 500 99 75-12595 3 20500ND493476
Zinc ug/L 500 96 75-12594 3 20500ND482470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349100
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005, 92330540006,
92330540007, 92330540008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936657
Associated Lab Samples:92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005, 92330540006,
92330540007, 92330540008
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 02/28/17 05:003.9
Arsenic ug/L ND 10.0 02/28/17 05:005.0
Barium ug/L ND 5.0 02/28/17 05:002.5
Beryllium ug/L ND 1.0 02/28/17 05:000.50
Cadmium ug/L ND 1.0 02/28/17 05:000.50
Chromium ug/L ND 5.0 02/28/17 05:002.5
Cobalt ug/L ND 5.0 02/28/17 05:002.5
Copper ug/L ND 5.0 02/28/17 05:002.5
Lead ug/L ND 5.0 02/28/17 05:002.5
Nickel ug/L ND 5.0 02/28/17 05:002.5
Selenium ug/L ND 10.0 02/28/17 05:005.0
Silver ug/L ND 5.0 02/28/17 05:002.5
Vanadium ug/L ND 5.0 02/28/17 05:002.5
Zinc ug/L 5.1J 10.0 02/28/17 05:005.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936658LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 481500 96 80-120
Arsenic ug/L 456500 91 80-120
Barium ug/L 496500 99 80-120
Beryllium ug/L 477500 95 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 490500 98 80-120
Cobalt ug/L 482500 96 80-120
Copper ug/L 471500 94 80-120
Lead ug/L 475500 95 80-120
Nickel ug/L 488500 98 80-120
Selenium ug/L 469500 94 80-120
Silver ug/L 236250 94 80-120
Vanadium ug/L 476500 95 80-120
Zinc ug/L 483500 97 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1936659MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330577007
1936660
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12595 2 20500ND472479
Arsenic ug/L 500 91 75-12592 1 20500ND455460
Barium ug/L 500 96 75-12597 1 20500116597602
Beryllium ug/L 500 94 75-12596 2 20500ND470481
Cadmium ug/L 500 95 75-12595 0 20500103577579
Chromium ug/L 500 94 75-12597 3 20500ND473486
Cobalt ug/L 500 92 75-12593 1 20500ND460466
Copper ug/L 500 92 75-12595 3 205004.7J 464 479
Lead ug/L 500 92 75-12593 2 20500ND459466
Nickel ug/L 500 93 75-12593 0 20500186651649
Selenium ug/L 500 90 75-12593 3 20500ND453466
Silver ug/L 250 93 75-12595 3 20250ND232238
Vanadium ug/L 500 94 75-12596 3 20500ND470483
Zinc ug/L 500 98 75-12589 3 2050089013801340
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349553
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330519019,
92330519020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1939173
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330519019,
92330519020
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 03/03/17 06:243.9
Arsenic ug/L ND 10.0 03/03/17 06:245.0
Barium ug/L ND 5.0 03/03/17 06:242.5
Beryllium ug/L ND 1.0 03/03/17 06:240.50
Cadmium ug/L ND 1.0 03/03/17 06:240.50
Chromium ug/L ND 5.0 03/03/17 06:242.5
Cobalt ug/L ND 5.0 03/03/17 06:242.5
Copper ug/L ND 5.0 03/03/17 06:242.5
Lead ug/L ND 5.0 03/03/17 06:242.5
Nickel ug/L ND 5.0 03/03/17 06:242.5
Selenium ug/L ND 10.0 03/03/17 06:245.0
Silver ug/L ND 5.0 03/03/17 06:242.5
Vanadium ug/L ND 5.0 03/03/17 06:242.5
Zinc ug/L ND 10.0 03/03/17 06:275.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1939174LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 482500 96 80-120
Arsenic ug/L 461500 92 80-120
Barium ug/L 461500 92 80-120
Beryllium ug/L 475500 95 80-120
Cadmium ug/L 464500 93 80-120
Chromium ug/L 466500 93 80-120
Cobalt ug/L 467500 93 80-120
Copper ug/L 485500 97 80-120
Lead ug/L 460500 92 80-120
Nickel ug/L 460500 92 80-120
Selenium ug/L 463500 93 80-120
Silver ug/L 244250 97 80-120
Vanadium ug/L 472500 94 80-120
Zinc ug/L 460500 92 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1939175MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92331034001
1939176
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 3 20500ND480492
Arsenic ug/L 500 92 75-12594 2 20500ND459469
Barium ug/L 500 91 75-12593 2 20500ND456465
Beryllium ug/L 500 94 75-12596 2 20500ND469480
Cadmium ug/L 500 92 75-12594 2 20500ND462469
Chromium ug/L 500 93 75-12595 2 20500ND466474
Cobalt ug/L 500 93 75-12595 2 20500ND466475
Copper ug/L 500 97 75-12598 1 20500ND487491
Lead ug/L 500 91 75-12594 2 20500ND457468
Nickel ug/L 500 92 75-12593 2 20500ND458467
Selenium ug/L 500 92 75-12594 2 20500ND462471
Silver ug/L 250 97 75-12598 2 20250ND242246
Vanadium ug/L 500 95 75-12596 1 20500ND475482
Zinc ug/L 500 91 75-12593 2 20500ND456465
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349257
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92330539001, 92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005,
92330540006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1937708
Associated Lab Samples:92330539001, 92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005,
92330540006
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 02/24/17 18:000.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1937709LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 94.7100 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937710MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330674021
1937711
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 97 75-12595 2 20100ND97.5 95.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349258
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92330540007, 92330540008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1937712
Associated Lab Samples:92330540007, 92330540008
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 02/24/17 19:590.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1937713LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 92.3100 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937714MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330540007
1937715
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 95 75-12596 1 201000.027J 95.2 96.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349668
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330519019,
92330519020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1939942
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330519019,
92330519020
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 02/24/17 20:120.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1939943LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 94.6100 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1939980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330519013
1939981
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 90 75-12595 6 201000.034J 90.2 95.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349193
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1937163
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/21/17 11:120.33
1,1,1-Trichloroethane ug/L ND 1.0 02/21/17 11:120.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/21/17 11:120.40
1,1,2-Trichloroethane ug/L ND 1.0 02/21/17 11:120.29
1,1-Dichloroethane ug/L ND 5.0 02/21/17 11:120.32
1,1-Dichloroethene ug/L ND 5.0 02/21/17 11:120.56
1,1-Dichloropropene ug/L ND 5.0 02/21/17 11:120.49
1,2,3-Trichloropropane ug/L ND 1.0 02/21/17 11:120.41
1,2,4-Trichlorobenzene ug/L ND 10.0 02/21/17 11:120.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/21/17 11:122.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/21/17 11:120.27
1,2-Dichlorobenzene ug/L ND 5.0 02/21/17 11:120.30
1,2-Dichloroethane ug/L ND 1.0 02/21/17 11:120.24
1,2-Dichloropropane ug/L ND 1.0 02/21/17 11:120.27
1,3-Dichlorobenzene ug/L ND 5.0 02/21/17 11:120.24
1,3-Dichloropropane ug/L ND 1.0 02/21/17 11:120.28
1,4-Dichlorobenzene ug/L ND 1.0 02/21/17 11:120.33
2,2-Dichloropropane ug/L ND 15.0 02/21/17 11:120.13
2-Butanone (MEK)ug/L ND 100 02/21/17 11:120.96
2-Hexanone ug/L ND 50.0 02/21/17 11:120.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/21/17 11:120.33
Acetone ug/L ND 100 02/21/17 11:1210.0
Acetonitrile ug/L ND 55.0 02/21/17 11:122.2
Acrolein ug/L ND 53.0 02/21/17 11:121.6
Acrylonitrile ug/L ND 200 02/21/17 11:121.9
Allyl chloride ug/L ND 10.0 02/21/17 11:121.5
Benzene ug/L ND 1.0 02/21/17 11:120.25
Bromochloromethane ug/L ND 3.0 02/21/17 11:120.17
Bromodichloromethane ug/L ND 1.0 02/21/17 11:120.18
Bromoform ug/L ND 3.0 02/21/17 11:120.26
Bromomethane ug/L ND 10.0 02/21/17 11:120.29
Carbon disulfide ug/L ND 100 02/21/17 11:121.2
Carbon tetrachloride ug/L ND 1.0 02/21/17 11:120.25
Chlorobenzene ug/L ND 3.0 02/21/17 11:120.23
Chloroethane ug/L ND 10.0 02/21/17 11:120.54
Chloroform ug/L ND 5.0 02/21/17 11:120.14
Chloromethane ug/L ND 1.0 02/21/17 11:120.11
Chloroprene ug/L ND 20.0 02/21/17 11:120.27
cis-1,2-Dichloroethene ug/L ND 5.0 02/21/17 11:120.19
cis-1,3-Dichloropropene ug/L ND 1.0 02/21/17 11:120.13
Dibromochloromethane ug/L ND 3.0 02/21/17 11:120.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1937163
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 02/21/17 11:120.21
Dichlorodifluoromethane ug/L ND 5.0 02/21/17 11:120.21
Ethyl methacrylate ug/L ND 10.0 02/21/17 11:120.20
Ethylbenzene ug/L ND 1.0 02/21/17 11:120.30
Hexachloro-1,3-butadiene ug/L ND 10.0 02/21/17 11:120.71
Iodomethane ug/L ND 10.0 02/21/17 11:120.32
Isobutanol ug/L ND 100 02/21/17 11:1235.0
Methacrylonitrile ug/L ND 100 02/21/17 11:120.93
Methyl methacrylate ug/L ND 30.0 02/21/17 11:122.0
Methylene Chloride ug/L ND 1.0 02/21/17 11:120.97
Naphthalene ug/L ND 10.0 02/21/17 11:120.24
Propionitrile ug/L ND 150 02/21/17 11:123.6
Styrene ug/L ND 1.0 02/21/17 11:120.26
Tetrachloroethene ug/L ND 1.0 02/21/17 11:120.46
Toluene ug/L ND 1.0 02/21/17 11:120.26
trans-1,2-Dichloroethene ug/L ND 5.0 02/21/17 11:120.49
trans-1,3-Dichloropropene ug/L ND 1.0 02/21/17 11:120.26
trans-1,4-Dichloro-2-butene ug/L ND 100 02/21/17 11:121.0
Trichloroethene ug/L ND 1.0 02/21/17 11:120.47
Trichlorofluoromethane ug/L ND 1.0 02/21/17 11:120.20
Vinyl acetate ug/L ND 50.0 02/21/17 11:120.35
Vinyl chloride ug/L ND 1.0 02/21/17 11:120.62
Xylene (Total)ug/L ND 5.0 02/21/17 11:120.66
1,2-Dichloroethane-d4 (S)%108 70-130 02/21/17 11:12
4-Bromofluorobenzene (S)%99 70-130 02/21/17 11:12
Toluene-d8 (S)%113 70-130 02/21/17 11:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1937164LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.250 98 80-125
1,1,1-Trichloroethane ug/L 46.050 92 71-129
1,1,2,2-Tetrachloroethane ug/L 50.250 100 79-124
1,1,2-Trichloroethane ug/L 54.150 108 85-125
1,1-Dichloroethane ug/L 48.650 97 73-126
1,1-Dichloroethene ug/L 48.150 96 66-135
1,1-Dichloropropene ug/L 51.050 102 74-135
1,2,3-Trichloropropane ug/L 53.850 108 75-130
1,2,4-Trichlorobenzene ug/L 52.050 104 75-134
1,2-Dibromo-3-chloropropane ug/L 49.450 99 71-133
1,2-Dibromoethane (EDB)ug/L 53.250 106 83-124
1,2-Dichlorobenzene ug/L 51.950 104 80-133
1,2-Dichloroethane ug/L 43.650 87 67-128
1,2-Dichloropropane ug/L 51.950 104 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1937164LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 50.350 101 77-130
1,3-Dichloropropane ug/L 55.850 112 76-131
1,4-Dichlorobenzene ug/L 48.950 98 78-130
2,2-Dichloropropane ug/L 44.850 90 40-160
2-Butanone (MEK)ug/L 90.1J100 90 61-144
2-Hexanone ug/L 89.6100 90 68-143
4-Methyl-2-pentanone (MIBK)ug/L 87.7J100 88 72-135
Acetone ug/L 86.3J100 86 48-146
Acetonitrile ug/L 414500 83 62-150
Acrolein ug/L 184250 74 24-160
Acrylonitrile ug/L 219250 88 40-160
Allyl chloride ug/L 47.850 96 66-137
Benzene ug/L 52.050 104 80-125
Bromochloromethane ug/L 51.250 102 71-125
Bromodichloromethane ug/L 49.750 99 78-124
Bromoform ug/L 45.050 90 71-128
Bromomethane ug/L 52.150 104 40-160
Carbon disulfide ug/L 49.7J50 99 50-160
Carbon tetrachloride ug/L 49.350 99 69-131
Chlorobenzene ug/L 51.850 104 81-122
Chloroethane ug/L 57.950 116 39-148
Chloroform ug/L 49.650 99 73-127
Chloromethane ug/L 62.650 125 44-146
Chloroprene ug/L 54.750 109 75-145
cis-1,2-Dichloroethene ug/L 50.750 101 74-124
cis-1,3-Dichloropropene ug/L 54.750 109 72-132
Dibromochloromethane ug/L 49.050 98 78-125
Dibromomethane ug/L 47.950 96 82-120
Dichlorodifluoromethane ug/L 50.050 100 34-157
Ethyl methacrylate ug/L 48.650 97 82-121
Ethylbenzene ug/L 50.750 101 79-121
Hexachloro-1,3-butadiene ug/L 55.150 110 72-131
Iodomethane ug/L 113100 113 39-154
Isobutanol ug/L 8141000 81 34-160
Methacrylonitrile ug/L 471500 94 74-134
Methyl methacrylate ug/L 48.350 97 84-124
Methylene Chloride ug/L 47.050 94 64-133
Naphthalene ug/L 50.550 101 73-133
Propionitrile ug/L 400500 80 73-140
Styrene ug/L 52.150 104 84-126
Tetrachloroethene ug/L 51.250 102 78-122
Toluene ug/L 53.050 106 80-121
trans-1,2-Dichloroethene ug/L 50.150 100 71-127
trans-1,3-Dichloropropene ug/L 54.150 108 69-141
trans-1,4-Dichloro-2-butene ug/L 51.9J50 104 40-160
Trichloroethene ug/L 55.350 111 78-122
Trichlorofluoromethane ug/L 55.850 112 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1937164LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 97.8100 98 40-160
Vinyl chloride ug/L 43.750 87 58-137
Xylene (Total)ug/L 150150 100 81-126
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%92 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937165MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330577007
1937166
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 87 70-13093 7 3020ND17.4 18.6
1,1,1-Trichloroethane ug/L 20 124 70-130122 1 3020ND24.7 24.5
1,1,2,2-Tetrachloroethane ug/L 20 100 70-130103 3 3020ND20.0 20.6
1,1,2-Trichloroethane ug/L 20 105 70-130111 6 3020ND21.0 22.3
1,1-Dichloroethane ug/L M12016770-130157 6 3020ND33.6 31.8
1,1-Dichloroethene ug/L M12016870-166154 9 3020ND33.7 30.8
1,1-Dichloropropene ug/L 20 125 70-130123 2 3020ND25.0 24.5
1,2,3-Trichloropropane ug/L 20 96 70-130104 9 3020ND19.2 20.9
1,2,4-Trichlorobenzene ug/L 20 99 70-13098 2 3020ND19.9 19.5
1,2-Dibromo-3-
chloropropane ug/L 20 86 70-13096 11 3020ND17.1 19.2
1,2-Dibromoethane (EDB)ug/L 20 90 70-13099 10 3020ND17.9 19.8
1,2-Dichlorobenzene ug/L 20 105 70-130105 1 3020ND21.1 21.0
1,2-Dichloroethane ug/L 20 122 70-130123 1 3020ND24.4 24.7
1,2-Dichloropropane ug/L 20 113 70-130117 3 3020ND22.6 23.3
1,3-Dichlorobenzene ug/L 20 101 70-13097 3 3020ND20.1 19.5
1,3-Dichloropropane ug/L 20 105 70-130110 5 3020ND21.1 22.1
1,4-Dichlorobenzene ug/L 20 109 70-130104 5 3020ND22.2 21.1
2,2-Dichloropropane ug/L 20 117 70-130111 5 3020ND23.5 22.3
2-Butanone (MEK)ug/L 40 85 70-13097 13 3040ND34.2J 38.9J
2-Hexanone ug/L 40 91 70-130106 15 3040ND36.2J 42.2J
4-Methyl-2-pentanone
(MIBK)ug/L 40 95 70-130112 16 3040ND38.1J 44.7J
Acetone ug/L 40 82 70-13095 15 3040ND32.9J 38.2J
Acetonitrile ug/L 200 92 70-130118 25 30200ND183236
Acrolein ug/L 100 70 70-13077 8 30100ND70.5 76.6
Acrylonitrile ug/L 100 101 70-130118 15 30100ND101J118J
Allyl chloride ug/L M12016170-130134 18 3020ND32.2 26.8
Benzene ug/L 20 120 70-148121 1 30200.44J 24.4 24.6
Bromochloromethane ug/L M12013670-130132 4 3020ND27.3 26.3
Bromodichloromethane ug/L 20 116 70-130115 1 3020ND23.1 23.0
Bromoform ug/L 20 78 70-13087 11 3020ND15.5 17.4
Bromomethane ug/L M12014070-130134 4 3020ND27.9 26.8
Carbon disulfide ug/L M12016070-130157 1 3020ND31.9J 31.5J
Carbon tetrachloride ug/L 20 113 70-130111 2 3020ND22.7 22.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937165MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330577007
1937166
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chlorobenzene ug/L 20 113 70-146115 2 3020ND22.6 23.0
Chloroethane ug/L M12020570-130202 1 30200.69J 41.6 41.1
Chloroform ug/L M12013970-130132 5 3020ND27.8 26.4
Chloromethane ug/L M12015870-130149 6 3020ND31.6 29.7
Chloroprene ug/L M12013270-130132 0 3020ND26.4 26.4
cis-1,2-Dichloroethene ug/L M12016070-130160 0 3020ND32.0 32.0
cis-1,3-Dichloropropene ug/L 20 105 70-130109 3 3020ND21.1 21.7
Dibromochloromethane ug/L 20 81 70-13089 9 3020ND16.2 17.7
Dibromomethane ug/L 20 110 70-130113 3 3020ND21.9 22.6
Dichlorodifluoromethane ug/L M12014270-130137 4 3020ND28.3 27.4
Ethyl methacrylate ug/L 20 115 70-130124 7 3020ND23.1 24.8
Ethylbenzene ug/L 20 117 70-130118 0 3020ND23.4 23.5
Hexachloro-1,3-butadiene ug/L 20 102 70-130105 3 3020ND20.4 20.9
Iodomethane ug/L M14016170-130180 11 3040ND64.2 72.0
Isobutanol ug/L M1,R14003570-13050 34 30400ND141200
Methacrylonitrile ug/L 200 103 70-130120 16 30200ND205241
Methyl methacrylate ug/L 20 99 70-130103 3 3020ND19.9J 20.6J
Methylene Chloride ug/L M12015770-130150 5 3020ND31.3 29.9
Naphthalene ug/L 20 93 70-13096 3 3020ND18.6 19.2
Propionitrile ug/L 200 83 70-130102 21 30200ND166204
Styrene ug/L 20 116 70-130118 2 3020ND23.1 23.7
Tetrachloroethene ug/L 20 97 70-130106 9 3020ND19.4 21.3
Toluene ug/L 20 133 70-155131 1 3020ND26.6 26.2
trans-1,2-Dichloroethene ug/L M12014370-130140 2 3020ND28.6 27.9
trans-1,3-Dichloropropene ug/L 20 102 70-130108 6 3020ND20.4 21.7
trans-1,4-Dichloro-2-butene ug/L M1206770-13087 26 3020ND13.3J 17.4J
Trichloroethene ug/L 20 105 69-151107 2 3020ND21.0 21.5
Trichlorofluoromethane ug/L M12020070-130189 5 3020ND39.9 37.8
Vinyl acetate ug/L 40 83 70-13090 8 3040ND33.2J 36.0J
Vinyl chloride ug/L M12015870-130141 11 3020ND31.5 28.3
1,2-Dichloroethane-d4 (S)%115 70-130117
4-Bromofluorobenzene (S)%99 70-130103
Toluene-d8 (S)%107 70-130104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349990
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92330539001, 92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005,
92330540006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941517
Associated Lab Samples:92330539001, 92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005,
92330540006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/28/17 19:280.33
1,1,1-Trichloroethane ug/L ND 1.0 02/28/17 19:280.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/28/17 19:280.40
1,1,2-Trichloroethane ug/L ND 1.0 02/28/17 19:280.29
1,1-Dichloroethane ug/L ND 5.0 02/28/17 19:280.32
1,1-Dichloroethene ug/L ND 5.0 02/28/17 19:280.56
1,2,3-Trichloropropane ug/L ND 1.0 02/28/17 19:280.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/28/17 19:282.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/28/17 19:280.27
1,2-Dichlorobenzene ug/L ND 5.0 02/28/17 19:280.30
1,2-Dichloroethane ug/L ND 1.0 02/28/17 19:280.24
1,2-Dichloropropane ug/L ND 1.0 02/28/17 19:280.27
1,4-Dichlorobenzene ug/L ND 1.0 02/28/17 19:280.33
2-Butanone (MEK)ug/L ND 100 02/28/17 19:280.96
2-Hexanone ug/L ND 50.0 02/28/17 19:280.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/28/17 19:280.33
Acetone ug/L ND 100 02/28/17 19:2810.0
Acrylonitrile ug/L ND 200 02/28/17 19:281.9
Benzene ug/L ND 1.0 02/28/17 19:280.25
Bromochloromethane ug/L ND 3.0 02/28/17 19:280.17
Bromodichloromethane ug/L ND 1.0 02/28/17 19:280.18
Bromoform ug/L ND 3.0 02/28/17 19:280.26
Bromomethane ug/L ND 10.0 02/28/17 19:280.29
Carbon disulfide ug/L ND 100 02/28/17 19:281.2
Carbon tetrachloride ug/L ND 1.0 02/28/17 19:280.25
Chlorobenzene ug/L ND 3.0 02/28/17 19:280.23
Chloroethane ug/L ND 10.0 02/28/17 19:280.54
Chloroform ug/L ND 5.0 02/28/17 19:280.14
Chloromethane ug/L ND 1.0 02/28/17 19:280.11
cis-1,2-Dichloroethene ug/L ND 5.0 02/28/17 19:280.19
cis-1,3-Dichloropropene ug/L ND 1.0 02/28/17 19:280.13
Dibromochloromethane ug/L ND 3.0 02/28/17 19:280.21
Dibromomethane ug/L ND 10.0 02/28/17 19:280.21
Ethylbenzene ug/L ND 1.0 02/28/17 19:280.30
Iodomethane ug/L ND 10.0 02/28/17 19:280.32
Methylene Chloride ug/L ND 1.0 02/28/17 19:280.97
Styrene ug/L ND 1.0 02/28/17 19:280.26
Tetrachloroethene ug/L ND 1.0 02/28/17 19:280.46
Toluene ug/L ND 1.0 02/28/17 19:280.26
trans-1,2-Dichloroethene ug/L ND 5.0 02/28/17 19:280.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 69 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941517
Associated Lab Samples:92330539001, 92330539002, 92330540001, 92330540002, 92330540003, 92330540004, 92330540005,
92330540006
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 02/28/17 19:280.26
trans-1,4-Dichloro-2-butene ug/L ND 100 02/28/17 19:281.0
Trichloroethene ug/L ND 1.0 02/28/17 19:280.47
Trichlorofluoromethane ug/L ND 1.0 02/28/17 19:280.20
Vinyl acetate ug/L ND 50.0 02/28/17 19:280.35
Vinyl chloride ug/L ND 1.0 02/28/17 19:280.62
Xylene (Total)ug/L ND 5.0 02/28/17 19:280.66
1,2-Dichloroethane-d4 (S)%96 70-130 02/28/17 19:28
4-Bromofluorobenzene (S)%92 70-130 02/28/17 19:28
Toluene-d8 (S)%97 70-130 02/28/17 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941518LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.450 101 80-125
1,1,1-Trichloroethane ug/L 49.950 100 71-129
1,1,2,2-Tetrachloroethane ug/L 48.750 97 79-124
1,1,2-Trichloroethane ug/L 52.750 105 85-125
1,1-Dichloroethane ug/L 48.750 97 73-126
1,1-Dichloroethene ug/L 52.350 105 66-135
1,2,3-Trichloropropane ug/L 48.250 96 75-130
1,2-Dibromo-3-chloropropane ug/L 48.450 97 71-133
1,2-Dibromoethane (EDB)ug/L 49.150 98 83-124
1,2-Dichlorobenzene ug/L 50.650 101 80-133
1,2-Dichloroethane ug/L 49.550 99 67-128
1,2-Dichloropropane ug/L 51.750 103 75-132
1,4-Dichlorobenzene ug/L 49.350 99 78-130
2-Butanone (MEK)ug/L 105100 105 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 72-135
Acetone ug/L 110100 110 48-146
Acrylonitrile ug/L 265250 106 40-160
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 50.850 102 71-125
Bromodichloromethane ug/L 54.050 108 78-124
Bromoform ug/L 48.550 97 71-128
Bromomethane ug/L 50.150 100 40-160
Carbon disulfide ug/L 47.6J50 95 50-160
Carbon tetrachloride ug/L 50.850 102 69-131
Chlorobenzene ug/L 51.450 103 81-122
Chloroethane ug/L 52.150 104 39-148
Chloroform ug/L 49.650 99 73-127
Chloromethane ug/L 48.350 97 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941518LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.050 100 74-124
cis-1,3-Dichloropropene ug/L 52.650 105 72-132
Dibromochloromethane ug/L 52.050 104 78-125
Dibromomethane ug/L 53.150 106 82-120
Ethylbenzene ug/L 49.650 99 79-121
Iodomethane ug/L 111100 111 39-154
Methylene Chloride ug/L 52.350 105 64-133
Styrene ug/L 50.550 101 84-126
Tetrachloroethene ug/L 48.550 97 78-122
Toluene ug/L 52.250 104 80-121
trans-1,2-Dichloroethene ug/L 50.850 102 71-127
trans-1,3-Dichloropropene ug/L 53.750 107 69-141
trans-1,4-Dichloro-2-butene ug/L 47.6J50 95 40-160
Trichloroethene ug/L 50.350 101 78-122
Trichlorofluoromethane ug/L 53.950 108 53-137
Vinyl acetate ug/L 109100 109 40-160
Vinyl chloride ug/L 43.050 86 58-137
Xylene (Total)ug/L 150150 100 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1942951MATRIX SPIKE SAMPLE:
MSSpike
Result
92330523002
1,1,1,2-Tetrachloroethane ug/L 20.120 100 70-130ND
1,1,1-Trichloroethane ug/L 21.620 108 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,2-Trichloroethane ug/L 19.920 99 70-130ND
1,1-Dichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethene ug/L 21.920 110 70-166ND
1,2,3-Trichloropropane ug/L 20.420 102 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.420 97 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.720 103 70-130ND
1,2-Dichlorobenzene ug/L 20.720 102 70-1300.38J
1,2-Dichloroethane ug/L 18.720 93 70-130ND
1,2-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 23.620 101 70-1303.5
2-Butanone (MEK)ug/L 37.7J40 94 70-130ND
2-Hexanone ug/L 38.9J40 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.6J40 102 70-130ND
Acetone ug/L 39.3J40 82 70-130ND
Acrylonitrile ug/L 101J100 101 70-130ND
Benzene ug/L 21.920 105 70-1480.90J
Bromochloromethane ug/L 19.820 99 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1942951MATRIX SPIKE SAMPLE:
MSSpike
Result
92330523002
Bromodichloromethane ug/L 20.920 105 70-130ND
Bromoform ug/L 18.820 94 70-130ND
Bromomethane ug/L 15.820 79 70-130ND
Carbon disulfide ug/L 18.6J20 93 70-130ND
Carbon tetrachloride ug/L 21.720 109 70-130ND
Chlorobenzene ug/L 34.920 122 70-14610.5
Chloroethane ug/L 20.020 100 70-130ND
Chloroform ug/L 19.920 99 70-130ND
Chloromethane ug/L 16.420 82 70-130ND
cis-1,2-Dichloroethene ug/L 19.820 99 70-130ND
cis-1,3-Dichloropropene ug/L 20.320 102 70-130ND
Dibromochloromethane ug/L 20.220 101 70-130ND
Dibromomethane ug/L 18.620 93 70-130ND
Ethylbenzene ug/L 20.820 104 70-130ND
Iodomethane ug/L 29.640 74 70-130ND
Methylene Chloride ug/L 18.520 92 70-130ND
Styrene ug/L 20.420 102 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 20.120 100 70-155ND
trans-1,2-Dichloroethene ug/L 21.220 106 70-130ND
trans-1,3-Dichloropropene ug/L 19.120 96 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.7J20 88 70-130ND
Trichloroethene ug/L 20.620 103 69-151ND
Trichlorofluoromethane ug/L 22.320 112 70-130ND
Vinyl acetate ug/L 37.0J40 92 70-130ND
Vinyl chloride ug/L 16.420 82 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330523001
1942950SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330523001
1942950SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L 0.33J 300.42J
Chloromethane ug/L 0.21J 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%89 22111
4-Bromofluorobenzene (S)%97 196
Toluene-d8 (S)%105 699
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350034
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330540007,
92330540008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941758
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330540007,
92330540008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/27/17 16:450.33
1,1,1-Trichloroethane ug/L ND 1.0 02/27/17 16:450.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/27/17 16:450.40
1,1,2-Trichloroethane ug/L ND 1.0 02/27/17 16:450.29
1,1-Dichloroethane ug/L ND 5.0 02/27/17 16:450.32
1,1-Dichloroethene ug/L ND 5.0 02/27/17 16:450.56
1,2,3-Trichloropropane ug/L ND 1.0 02/27/17 16:450.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/27/17 16:452.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/27/17 16:450.27
1,2-Dichlorobenzene ug/L ND 5.0 02/27/17 16:450.30
1,2-Dichloroethane ug/L ND 1.0 02/27/17 16:450.24
1,2-Dichloropropane ug/L ND 1.0 02/27/17 16:450.27
1,4-Dichlorobenzene ug/L ND 1.0 02/27/17 16:450.33
2-Butanone (MEK)ug/L ND 100 02/27/17 16:450.96
2-Hexanone ug/L ND 50.0 02/27/17 16:450.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/27/17 16:450.33
Acetone ug/L ND 100 02/27/17 16:4510.0
Acrylonitrile ug/L ND 200 02/27/17 16:451.9
Benzene ug/L ND 1.0 02/27/17 16:450.25
Bromochloromethane ug/L ND 3.0 02/27/17 16:450.17
Bromodichloromethane ug/L ND 1.0 02/27/17 16:450.18
Bromoform ug/L ND 3.0 02/27/17 16:450.26
Bromomethane ug/L ND 10.0 02/27/17 16:450.29
Carbon disulfide ug/L ND 100 02/27/17 16:451.2
Carbon tetrachloride ug/L ND 1.0 02/27/17 16:450.25
Chlorobenzene ug/L ND 3.0 02/27/17 16:450.23
Chloroethane ug/L ND 10.0 02/27/17 16:450.54
Chloroform ug/L ND 5.0 02/27/17 16:450.14
Chloromethane ug/L ND 1.0 02/27/17 16:450.11
cis-1,2-Dichloroethene ug/L ND 5.0 02/27/17 16:450.19
cis-1,3-Dichloropropene ug/L ND 1.0 02/27/17 16:450.13
Dibromochloromethane ug/L ND 3.0 02/27/17 16:450.21
Dibromomethane ug/L ND 10.0 02/27/17 16:450.21
Ethylbenzene ug/L ND 1.0 02/27/17 16:450.30
Iodomethane ug/L ND 10.0 02/27/17 16:450.32
Methylene Chloride ug/L ND 1.0 02/27/17 16:450.97
Styrene ug/L ND 1.0 02/27/17 16:450.26
Tetrachloroethene ug/L ND 1.0 02/27/17 16:450.46
Toluene ug/L ND 1.0 02/27/17 16:450.26
trans-1,2-Dichloroethene ug/L ND 5.0 02/27/17 16:450.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941758
Associated Lab Samples:92330519013, 92330519014, 92330519015, 92330519016, 92330519017, 92330519018, 92330540007,
92330540008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 02/27/17 16:450.26
trans-1,4-Dichloro-2-butene ug/L ND 100 02/27/17 16:451.0
Trichloroethene ug/L ND 1.0 02/27/17 16:450.47
Trichlorofluoromethane ug/L ND 1.0 02/27/17 16:450.20
Vinyl acetate ug/L ND 50.0 02/27/17 16:450.35
Vinyl chloride ug/L ND 1.0 02/27/17 16:450.62
Xylene (Total)ug/L ND 5.0 02/27/17 16:450.66
1,2-Dichloroethane-d4 (S)%98 70-130 02/27/17 16:45
4-Bromofluorobenzene (S)%97 70-130 02/27/17 16:45
Toluene-d8 (S)%93 70-130 02/27/17 16:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941759LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.250 96 80-125
1,1,1-Trichloroethane ug/L 47.150 94 71-129
1,1,2,2-Tetrachloroethane ug/L 47.350 95 79-124
1,1,2-Trichloroethane ug/L 49.450 99 85-125
1,1-Dichloroethane ug/L 45.250 90 73-126
1,1-Dichloroethene ug/L 51.250 102 66-135
1,2,3-Trichloropropane ug/L 46.550 93 75-130
1,2-Dibromo-3-chloropropane ug/L 48.350 97 71-133
1,2-Dibromoethane (EDB)ug/L 47.350 95 83-124
1,2-Dichlorobenzene ug/L 47.750 95 80-133
1,2-Dichloroethane ug/L 42.850 86 67-128
1,2-Dichloropropane ug/L 47.250 94 75-132
1,4-Dichlorobenzene ug/L 45.550 91 78-130
2-Butanone (MEK)ug/L 95.0J100 95 61-144
2-Hexanone ug/L 96.6100 97 68-143
4-Methyl-2-pentanone (MIBK)ug/L 97.2J100 97 72-135
Acetone ug/L 103100 103 48-146
Acrylonitrile ug/L 239250 96 40-160
Benzene ug/L 48.750 97 80-125
Bromochloromethane ug/L 46.350 93 71-125
Bromodichloromethane ug/L 50.250 100 78-124
Bromoform ug/L 47.950 96 71-128
Bromomethane ug/L 49.150 98 40-160
Carbon disulfide ug/L 49.1J50 98 50-160
Carbon tetrachloride ug/L 48.550 97 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 52.150 104 39-148
Chloroform ug/L 44.250 88 73-127
Chloromethane ug/L 48.850 98 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941759LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 44.750 89 74-124
cis-1,3-Dichloropropene ug/L 50.150 100 72-132
Dibromochloromethane ug/L 49.250 98 78-125
Dibromomethane ug/L 48.950 98 82-120
Ethylbenzene ug/L 48.050 96 79-121
Iodomethane ug/L 96.4100 96 39-154
Methylene Chloride ug/L 48.050 96 64-133
Styrene ug/L 48.250 96 84-126
Tetrachloroethene ug/L 48.250 96 78-122
Toluene ug/L 47.650 95 80-121
trans-1,2-Dichloroethene ug/L 47.750 95 71-127
trans-1,3-Dichloropropene ug/L 48.750 97 69-141
trans-1,4-Dichloro-2-butene ug/L 44.3J50 89 40-160
Trichloroethene ug/L 48.550 97 78-122
Trichlorofluoromethane ug/L 58.950 118 53-137
Vinyl acetate ug/L 96.8100 97 40-160
Vinyl chloride ug/L 44.050 88 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1941760MATRIX SPIKE SAMPLE:
MSSpike
Result
92330540007
1,1,1,2-Tetrachloroethane ug/L 21.620 108 70-130ND
1,1,1-Trichloroethane ug/L 22.520 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.920 115 70-130ND
1,1,2-Trichloroethane ug/L 23.220 116 70-130ND
1,1-Dichloroethane ug/L 21.920 109 70-130ND
1,1-Dichloroethene ug/L 23.620 118 70-166ND
1,2,3-Trichloropropane ug/L 22.520 113 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.620 98 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.420 112 70-130ND
1,2-Dichlorobenzene ug/L 22.420 112 70-130ND
1,2-Dichloroethane ug/L 20.620 102 70-130ND
1,2-Dichloropropane ug/L 22.420 112 70-130ND
1,4-Dichlorobenzene ug/L 21.520 108 70-130ND
2-Butanone (MEK)ug/L 43.0J40 107 70-130ND
2-Hexanone ug/L 45.5J40 114 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 45.1J40 113 70-130ND
Acetone ug/L 43.1J40 105 70-130ND
Acrylonitrile ug/L 104J100 104 70-130ND
Benzene ug/L 24.420 122 70-148ND
Bromochloromethane ug/L 21.520 107 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Page 76 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1941760MATRIX SPIKE SAMPLE:
MSSpike
Result
92330540007
Bromodichloromethane ug/L 23.820 119 70-130ND
Bromoform ug/L 19.720 98 70-130ND
Bromomethane ug/L 20.820 104 70-130ND
Carbon disulfide ug/L 21.2J20 106 70-130ND
Carbon tetrachloride ug/L 24.120 121 70-130ND
Chlorobenzene ug/L 22.720 113 70-146ND
Chloroethane ug/L 23.320 117 70-130ND
Chloroform ug/L 21.820 109 70-130ND
Chloromethane ug/L 23.720 118 70-130ND
cis-1,2-Dichloroethene ug/L 21.920 110 70-130ND
cis-1,3-Dichloropropene ug/L 22.720 113 70-130ND
Dibromochloromethane ug/L 24.120 121 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Ethylbenzene ug/L 23.220 116 70-130ND
Iodomethane ug/L 43.140 108 70-130ND
Methylene Chloride ug/L 21.920 109 70-130ND
Styrene ug/L 22.520 112 70-130ND
Tetrachloroethene ug/L 24.720 124 70-130ND
Toluene ug/L 23.920 120 70-155ND
trans-1,2-Dichloroethene ug/L 22.820 114 70-130ND
trans-1,3-Dichloropropene ug/L 22.420 112 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.3J20 96 70-130ND
Trichloroethene ug/L 24.120 121 69-151ND
Trichlorofluoromethane ug/L 25.020 125 70-130ND
Vinyl acetate ug/L 39.2J40 98 70-130ND
Vinyl chloride ug/L 19.520 98 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%107 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330540008
1941761SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Page 77 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330540008
1941761SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%100 298
4-Bromofluorobenzene (S)%94 392
Toluene-d8 (S)%97 3100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350035
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92330519019, 92330519020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941762
Associated Lab Samples:92330519019, 92330519020
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/28/17 02:020.33
1,1,1-Trichloroethane ug/L ND 1.0 02/28/17 02:020.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/28/17 02:020.40
1,1,2-Trichloroethane ug/L ND 1.0 02/28/17 02:020.29
1,1-Dichloroethane ug/L ND 5.0 02/28/17 02:020.32
1,1-Dichloroethene ug/L ND 5.0 02/28/17 02:020.56
1,2,3-Trichloropropane ug/L ND 1.0 02/28/17 02:020.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/28/17 02:022.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/28/17 02:020.27
1,2-Dichlorobenzene ug/L ND 5.0 02/28/17 02:020.30
1,2-Dichloroethane ug/L ND 1.0 02/28/17 02:020.24
1,2-Dichloropropane ug/L ND 1.0 02/28/17 02:020.27
1,4-Dichlorobenzene ug/L ND 1.0 02/28/17 02:020.33
2-Butanone (MEK)ug/L ND 100 02/28/17 02:020.96
2-Hexanone ug/L ND 50.0 02/28/17 02:020.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/28/17 02:020.33
Acetone ug/L ND 100 02/28/17 02:0210.0
Acrylonitrile ug/L ND 200 02/28/17 02:021.9
Benzene ug/L ND 1.0 02/28/17 02:020.25
Bromochloromethane ug/L ND 3.0 02/28/17 02:020.17
Bromodichloromethane ug/L ND 1.0 02/28/17 02:020.18
Bromoform ug/L ND 3.0 02/28/17 02:020.26
Bromomethane ug/L ND 10.0 02/28/17 02:020.29
Carbon disulfide ug/L ND 100 02/28/17 02:021.2
Carbon tetrachloride ug/L ND 1.0 02/28/17 02:020.25
Chlorobenzene ug/L ND 3.0 02/28/17 02:020.23
Chloroethane ug/L ND 10.0 02/28/17 02:020.54
Chloroform ug/L ND 5.0 02/28/17 02:020.14
Chloromethane ug/L ND 1.0 02/28/17 02:020.11
cis-1,2-Dichloroethene ug/L ND 5.0 02/28/17 02:020.19
cis-1,3-Dichloropropene ug/L ND 1.0 02/28/17 02:020.13
Dibromochloromethane ug/L ND 3.0 02/28/17 02:020.21
Dibromomethane ug/L ND 10.0 02/28/17 02:020.21
Ethylbenzene ug/L ND 1.0 02/28/17 02:020.30
Iodomethane ug/L ND 10.0 02/28/17 02:020.32
Methylene Chloride ug/L ND 1.0 02/28/17 02:020.97
Styrene ug/L ND 1.0 02/28/17 02:020.26
Tetrachloroethene ug/L ND 1.0 02/28/17 02:020.46
Toluene ug/L ND 1.0 02/28/17 02:020.26
trans-1,2-Dichloroethene ug/L ND 5.0 02/28/17 02:020.49
trans-1,3-Dichloropropene ug/L ND 1.0 02/28/17 02:020.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1941762
Associated Lab Samples:92330519019, 92330519020
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 02/28/17 02:021.0
Trichloroethene ug/L ND 1.0 02/28/17 02:020.47
Trichlorofluoromethane ug/L ND 1.0 02/28/17 02:020.20
Vinyl acetate ug/L ND 50.0 02/28/17 02:020.35
Vinyl chloride ug/L ND 1.0 02/28/17 02:020.62
Xylene (Total)ug/L ND 5.0 02/28/17 02:020.66
1,2-Dichloroethane-d4 (S)%96 70-130 02/28/17 02:02
4-Bromofluorobenzene (S)%94 70-130 02/28/17 02:02
Toluene-d8 (S)%92 70-130 02/28/17 02:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941763LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.550 97 80-125
1,1,1-Trichloroethane ug/L 46.150 92 71-129
1,1,2,2-Tetrachloroethane ug/L 47.550 95 79-124
1,1,2-Trichloroethane ug/L 48.450 97 85-125
1,1-Dichloroethane ug/L 45.350 91 73-126
1,1-Dichloroethene ug/L 47.550 95 66-135
1,2,3-Trichloropropane ug/L 44.950 90 75-130
1,2-Dibromo-3-chloropropane ug/L 46.550 93 71-133
1,2-Dibromoethane (EDB)ug/L 47.650 95 83-124
1,2-Dichlorobenzene ug/L 49.050 98 80-133
1,2-Dichloroethane ug/L 44.050 88 67-128
1,2-Dichloropropane ug/L 47.150 94 75-132
1,4-Dichlorobenzene ug/L 46.650 93 78-130
2-Butanone (MEK)ug/L 98.4J100 98 61-144
2-Hexanone ug/L 97.5100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 97.2J100 97 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 247250 99 40-160
Benzene ug/L 49.250 98 80-125
Bromochloromethane ug/L 47.850 96 71-125
Bromodichloromethane ug/L 50.250 100 78-124
Bromoform ug/L 46.650 93 71-128
Bromomethane ug/L 47.350 95 40-160
Carbon disulfide ug/L 44.0J50 88 50-160
Carbon tetrachloride ug/L 47.350 95 69-131
Chlorobenzene ug/L 49.450 99 81-122
Chloroethane ug/L 50.550 101 39-148
Chloroform ug/L 45.250 90 73-127
Chloromethane ug/L 48.250 96 44-146
cis-1,2-Dichloroethene ug/L 45.950 92 74-124
cis-1,3-Dichloropropene ug/L 47.150 94 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1941763LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 50.150 100 78-125
Dibromomethane ug/L 47.950 96 82-120
Ethylbenzene ug/L 47.350 95 79-121
Iodomethane ug/L 99.6100 100 39-154
Methylene Chloride ug/L 47.850 96 64-133
Styrene ug/L 48.450 97 84-126
Tetrachloroethene ug/L 42.550 85 78-122
Toluene ug/L 46.350 93 80-121
trans-1,2-Dichloroethene ug/L 46.550 93 71-127
trans-1,3-Dichloropropene ug/L 48.250 96 69-141
trans-1,4-Dichloro-2-butene ug/L 40.6J50 81 40-160
Trichloroethene ug/L 48.650 97 78-122
Trichlorofluoromethane ug/L 49.850 100 53-137
Vinyl acetate ug/L 100100 100 40-160
Vinyl chloride ug/L 39.950 80 58-137
Xylene (Total)ug/L 142150 95 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1941764MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330712012
1941765
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 103 70-130105 2 3020ND20.7 21.0
1,1,1-Trichloroethane ug/L 20 111 70-130113 1 3020ND22.6 22.9
1,1,2,2-Tetrachloroethane ug/L 20 103 70-130102 1 3020ND20.5 20.4
1,1,2-Trichloroethane ug/L 20 100 70-130107 7 3020ND20.0 21.4
1,1-Dichloroethane ug/L 20 102 70-130109 6 30200.62J 21.1 22.5
1,1-Dichloroethene ug/L 20 115 70-166115 0 30200.56J 23.6 23.5
1,2,3-Trichloropropane ug/L 20 99 70-13099 0 3020ND19.8 19.8
1,2-Dibromo-3-chloropropane ug/L 20 100 70-13097 3 3020ND19.9 19.4
1,2-Dibromoethane (EDB)ug/L 20 101 70-130101 1 3020ND20.1 20.2
1,2-Dichlorobenzene ug/L 20 104 70-130107 3 3020ND20.7 21.3
1,2-Dichloroethane ug/L 20 98 70-130102 4 3020ND19.8 20.7
1,2-Dichloropropane ug/L 20 102 70-130107 5 3020ND20.4 21.4
1,4-Dichlorobenzene ug/L 20 101 70-130105 4 3020ND20.1 21.0
2-Butanone (MEK)ug/L 40 106 70-130106 1 30401.8J 44.3J 44.1J
2-Hexanone ug/L 40 108 70-130105 2 3040ND43.3J 42.4J
4-Methyl-2-pentanone(MIBK)ug/L 40 105 70-130110 4 3040ND42.2J 43.8J
Acetone ug/L 40 106 70-130107 1 3040ND50.3J 50.6J
Acrylonitrile ug/L 100 111 70-130110 1 30100ND111J110J
Benzene ug/L 20 107 70-148114 6 3020ND21.4 22.8
Bromochloromethane ug/L 20 101 70-130105 4 3020ND20.2 21.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1941764MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330712012
1941765
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 20 104 70-130112 8 3020ND20.8 22.4
Bromoform ug/L 20 92 70-13095 3 3020ND18.4 19.0
Bromomethane ug/L 20 99 70-130106 6 3020ND19.8 21.1
Carbon disulfide ug/L 20 100 70-130105 5 3020ND20.0J 21.1J
Carbon tetrachloride ug/L 20 110 70-130111 1 3020ND21.9 22.2
Chlorobenzene ug/L 20 110 70-146111 1 3020ND21.9 22.2
Chloroethane ug/L 20 117 70-130120 3 3020ND23.5 24.1
Chloroform ug/L 20 104 70-130107 3 3020ND20.7 21.3
Chloromethane ug/L 20 116 70-130114 1 30200.26J 23.4 23.1
cis-1,2-Dichloroethene ug/L 20 90 70-130109 6 302040.7 58.6 62.5
cis-1,3-Dichloropropene ug/L 20 97 70-130105 8 3020ND19.5 21.1
Dibromochloromethane ug/L 20 103 70-130103 1 3020ND20.6 20.7
Dibromomethane ug/L 20 103 70-130109 5 3020ND20.6 21.7
Ethylbenzene ug/L 20 109 70-130111 2 3020ND21.8 22.2
Iodomethane ug/L 40 104 70-130119 13 3040ND41.8 47.7
Methylene Chloride ug/L 20 104 70-130109 5 3020ND20.8 21.8
Styrene ug/L 20 104 70-130107 3 3020ND20.7 21.4
Tetrachloroethene ug/L 20 108 70-130102 6 3020ND21.8 20.6
Toluene ug/L 20 105 70-155106 1 3020ND21.0 21.3
trans-1,2-Dichloroethene ug/L 20 110 70-130112 3 3020ND22.1 22.7
trans-1,3-Dichloropropene ug/L 20 96 70-130101 5 3020ND19.1 20.2
trans-1,4-Dichloro-2-butene ug/L 20 83 70-13083 0 3020ND16.6J 16.7J
Trichloroethene ug/L 20 89 69-15199 3 302039.1 56.9 58.8
Trichlorofluoromethane ug/L M12013170-130121 8 3020ND26.2 24.3
Vinyl acetate ug/L 40 89 70-13095 7 3040ND35.7J 38.2J
Vinyl chloride ug/L 20 99 70-130100 1 3020ND19.8 20.0
1,2-Dichloroethane-d4 (S)%97 70-130101
4-Bromofluorobenzene (S)%97 70-13097
Toluene-d8 (S)%99 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
352340
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92330540005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1893894
Associated Lab Samples:92330540005
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 02/26/17 03:480.042
2,4,5-TP (Silvex)ug/L ND 0.19 02/26/17 03:480.049
2,4-D ug/L ND 0.94 02/26/17 03:480.22
2,4-DB ug/L ND 1.9 02/26/17 03:480.51
Bentazon ug/L ND 0.094 02/26/17 03:480.047
Dalapon ug/L ND 0.91 02/26/17 03:480.43
Dicamba ug/L ND 0.094 02/26/17 03:480.030
Dichlorprop ug/L ND 0.65 02/26/17 03:480.19
Dinoseb ug/L ND 0.19 02/26/17 03:480.057
Pentachlorophenol ug/L ND 0.028 02/26/17 03:480.017
Picloram ug/L ND 0.094 02/26/17 03:480.019
2,4-DCAA (S)%100 39-139 02/26/17 03:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1893895LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.61.2 133 37-133
2,4,5-TP (Silvex)ug/L 1.31.2 105 53-134
2,4-D ug/L 7.7 L1612835-124
2,4-DB ug/L 13.212 110 31-132
Bentazon ug/L 0.31.6 52 51-125
Dalapon ug/L 7.5 L1612410-122
Dicamba ug/L 0.68.6 113 44-125
Dichlorprop ug/L 5.24.2 123 70-130
Dinoseb ug/L 1.5 L11.2 121 13-116
Pentachlorophenol ug/L 0.25.18 138 39-170
Picloram ug/L 0.42.6 71 10-127
2,4-DCAA (S)%111 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1893917MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330577007
1893918
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 126 37-133125 0 401.2ND 1.5 1.5
2,4,5-TP (Silvex)ug/L 1.2 104 53-13498 5 401.2ND 1.3 1.2
2,4-D ug/L M06.1 128 35-124124 3 406.1ND 7.7 7.5
2,4-DB ug/L 12.1 106 31-132107 1 4012.2ND 12.9 13.0
Bentazon ug/L M1.61 18 51-12523 21 40.61ND 0.11 0.14
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1893917MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330577007
1893918
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dalapon ug/L M06.1 116 10-122123 6 406.1ND 7.1 7.5
Dicamba ug/L M1.61 121 44-125129 7 40.61ND 0.73 0.78
Dichlorprop ug/L 4.2 115 70-130110 4 404.3ND 4.9 4.7
Dinoseb ug/L M01.2 122 13-116118 3 401.2ND 1.5 1.4
Pentachlorophenol ug/L M1,R1.18 56 39-17034 48 40.18ND 0.10 0.063
Picloram ug/L .61 73 10-12773 1 40.61ND 0.44 0.45
2,4-DCAA (S)%107 39-139112 40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349028
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92330540001, 92330540006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936347
Associated Lab Samples:92330540001, 92330540006
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 02/21/17 13:351.9
1,2-Dichlorobenzene ug/L ND 10.0 02/21/17 13:351.2
1,3-Dichlorobenzene ug/L ND 10.0 02/21/17 13:351.1
1,4-Dichlorobenzene ug/L ND 10.0 02/21/17 13:351.2
1-Methylnaphthalene ug/L ND 10.0 02/21/17 13:350.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 02/21/17 13:351.6
2,4,5-Trichlorophenol ug/L ND 10.0 02/21/17 13:352.2
2,4,6-Trichlorophenol ug/L ND 10.0 02/21/17 13:351.9
2,4-Dichlorophenol ug/L ND 10.0 02/21/17 13:351.7
2,4-Dimethylphenol ug/L ND 10.0 02/21/17 13:352.2
2,4-Dinitrophenol ug/L ND 50.0 02/21/17 13:356.5
2,4-Dinitrotoluene ug/L ND 10.0 02/21/17 13:351.2
2,6-Dinitrotoluene ug/L ND 10.0 02/21/17 13:351.7
2-Chloronaphthalene ug/L ND 10.0 02/21/17 13:352.2
2-Chlorophenol ug/L ND 10.0 02/21/17 13:351.5
2-Methylnaphthalene ug/L ND 10.0 02/21/17 13:350.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 02/21/17 13:351.7
2-Nitroaniline ug/L ND 50.0 02/21/17 13:352.8
2-Nitrophenol ug/L ND 10.0 02/21/17 13:351.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 02/21/17 13:351.7
3,3'-Dichlorobenzidine ug/L ND 20.0 02/21/17 13:351.4
3-Nitroaniline ug/L ND 50.0 02/21/17 13:352.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 02/21/17 13:351.7
4-Bromophenylphenyl ether ug/L ND 10.0 02/21/17 13:351.3
4-Chloro-3-methylphenol ug/L ND 20.0 02/21/17 13:354.2
4-Chloroaniline ug/L ND 20.0 02/21/17 13:353.4
4-Chlorophenylphenyl ether ug/L ND 10.0 02/21/17 13:352.1
4-Nitroaniline ug/L ND 20.0 02/21/17 13:352.5
4-Nitrophenol ug/L ND 50.0 02/21/17 13:355.8
Acenaphthene ug/L ND 10.0 02/21/17 13:350.25
Acenaphthylene ug/L ND 10.0 02/21/17 13:350.21
Aniline ug/L ND 10.0 02/21/17 13:351.3
Anthracene ug/L ND 10.0 02/21/17 13:350.14
Benzo(a)anthracene ug/L ND 10.0 02/21/17 13:350.33
Benzo(a)pyrene ug/L ND 10.0 02/21/17 13:350.30
Benzo(b)fluoranthene ug/L ND 10.0 02/21/17 13:350.28
Benzo(g,h,i)perylene ug/L ND 10.0 02/21/17 13:350.38
Benzo(k)fluoranthene ug/L ND 10.0 02/21/17 13:350.43
Benzoic Acid ug/L ND 50.0 02/21/17 13:3511.1
Benzyl alcohol ug/L ND 20.0 02/21/17 13:353.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 02/21/17 13:351.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 85 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936347
Associated Lab Samples:92330540001, 92330540006
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 02/21/17 13:351.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 02/21/17 13:350.85
Butylbenzylphthalate ug/L ND 10.0 02/21/17 13:350.75
Chrysene ug/L ND 10.0 02/21/17 13:350.21
Di-n-butylphthalate ug/L ND 10.0 02/21/17 13:351.1
Di-n-octylphthalate ug/L ND 10.0 02/21/17 13:350.86
Dibenz(a,h)anthracene ug/L ND 10.0 02/21/17 13:350.55
Dibenzofuran ug/L ND 10.0 02/21/17 13:351.8
Diethylphthalate ug/L ND 6000 02/21/17 13:351.3
Dimethylphthalate ug/L ND 10.0 02/21/17 13:351.5
Fluoranthene ug/L ND 10.0 02/21/17 13:350.21
Fluorene ug/L ND 10.0 02/21/17 13:350.21
Hexachloro-1,3-butadiene ug/L ND 10.0 02/21/17 13:351.8
Hexachlorobenzene ug/L ND 10.0 02/21/17 13:351.1
Hexachlorocyclopentadiene ug/L ND 10.0 02/21/17 13:351.8
Hexachloroethane ug/L ND 10.0 02/21/17 13:351.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 02/21/17 13:350.29
Isophorone ug/L ND 10.0 02/21/17 13:351.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 02/21/17 13:352.1
N-Nitrosodimethylamine ug/L ND 10.0 02/21/17 13:351.3
N-Nitrosodiphenylamine ug/L ND 10.0 02/21/17 13:351.3
Naphthalene ug/L ND 10.0 02/21/17 13:350.34
Nitrobenzene ug/L ND 10.0 02/21/17 13:351.7
Pentachlorophenol ug/L ND 25.0 02/21/17 13:352.3
Phenanthrene ug/L ND 10.0 02/21/17 13:350.22
Phenol ug/L ND 10.0 02/21/17 13:351.7
Pyrene ug/L ND 10.0 02/21/17 13:350.19
2,4,6-Tribromophenol (S)%68 27-110 02/21/17 13:35
2-Fluorobiphenyl (S)%64 27-110 02/21/17 13:35
2-Fluorophenol (S)%33 12-110 02/21/17 13:35
Nitrobenzene-d5 (S)%67 21-110 02/21/17 13:35
Phenol-d6 (S)%20 10-110 02/21/17 13:35
Terphenyl-d14 (S)%84 31-107 02/21/17 13:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936348LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 29.650 59 31-120
1,2-Dichlorobenzene ug/L 26.950 54 38-120
1,3-Dichlorobenzene ug/L 25.750 51 30-122
1,4-Dichlorobenzene ug/L 25.650 51 37-120
1-Methylnaphthalene ug/L 34.350 69 34-113
2,2'-Oxybis(1-chloropropane)ug/L 32.550 65 18-120
2,4,5-Trichlorophenol ug/L 36.350 73 43-113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936348LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 42.750 85 42-120
2,4-Dichlorophenol ug/L 35.050 70 30-120
2,4-Dimethylphenol ug/L 36.750 73 29-111
2,4-Dinitrophenol ug/L 276250 110 19-132
2,4-Dinitrotoluene ug/L 51.250 102 58-128
2,6-Dinitrotoluene ug/L 52.950 106 54-129
2-Chloronaphthalene ug/L 44.350 89 43-117
2-Chlorophenol ug/L 29.750 59 37-120
2-Methylnaphthalene ug/L 35.150 70 33-120
2-Methylphenol(o-Cresol)ug/L 24.550 49 31-120
2-Nitroaniline ug/L 85.3100 85 48-121
2-Nitrophenol ug/L 37.150 74 25-116
3&4-Methylphenol(m&p Cresol)ug/L 22.150 44 23-120
3,3'-Dichlorobenzidine ug/L 81.2100 81 10-154
3-Nitroaniline ug/L 85.7100 86 43-115
4,6-Dinitro-2-methylphenol ug/L 98.8100 99 44-124
4-Bromophenylphenyl ether ug/L 36.650 73 34-113
4-Chloro-3-methylphenol ug/L 74.2100 74 31-110
4-Chloroaniline ug/L 69.1100 69 20-120
4-Chlorophenylphenyl ether ug/L 38.450 77 34-116
4-Nitroaniline ug/L 89.6100 90 46-128
4-Nitrophenol ug/L 90.6250 36 11-120
Acenaphthene ug/L 38.750 77 48-114
Acenaphthylene ug/L 39.250 78 48-112
Aniline ug/L 24.750 49 26-120
Anthracene ug/L 40.650 81 57-118
Benzo(a)anthracene ug/L 43.250 86 56-121
Benzo(a)pyrene ug/L 38.450 77 55-127
Benzo(b)fluoranthene ug/L 42.350 85 53-128
Benzo(g,h,i)perylene ug/L 37.550 75 54-125
Benzo(k)fluoranthene ug/L 39.450 79 51-123
Benzoic Acid ug/L 79.4250 32 10-120
Benzyl alcohol ug/L 56.1100 56 27-120
bis(2-Chloroethoxy)methane ug/L 34.450 69 32-120
bis(2-Chloroethyl) ether ug/L 32.850 66 33-111
bis(2-Ethylhexyl)phthalate ug/L 53.950 108 50-145
Butylbenzylphthalate ug/L 55.550 111 54-138
Chrysene ug/L 43.150 86 58-127
Di-n-butylphthalate ug/L 47.250 94 56-125
Di-n-octylphthalate ug/L 49.450 99 50-134
Dibenz(a,h)anthracene ug/L 39.550 79 53-129
Dibenzofuran ug/L 38.850 78 45-120
Diethylphthalate ug/L 47.7J50 95 53-120
Dimethylphthalate ug/L 43.850 88 55-116
Fluoranthene ug/L 41.250 82 57-125
Fluorene ug/L 40.950 82 53-118
Hexachloro-1,3-butadiene ug/L 27.450 55 23-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936348LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 38.650 77 49-116
Hexachlorocyclopentadiene ug/L 36.450 73 26-158
Hexachloroethane ug/L 24.950 50 30-114
Indeno(1,2,3-cd)pyrene ug/L 39.050 78 55-128
Isophorone ug/L 41.350 83 31-118
N-Nitroso-di-n-propylamine ug/L 35.850 72 32-119
N-Nitrosodimethylamine ug/L 22.250 44 13-120
N-Nitrosodiphenylamine ug/L 39.250 78 43-120
Naphthalene ug/L 32.850 66 32-120
Nitrobenzene ug/L 39.350 79 33-110
Pentachlorophenol ug/L 105100 105 10-137
Phenanthrene ug/L 40.350 81 57-117
Phenol ug/L 14.450 29 10-120
Pyrene ug/L 42.550 85 55-122
2,4,6-Tribromophenol (S)%89 27-110
2-Fluorobiphenyl (S)%73 27-110
2-Fluorophenol (S)%36 12-110
Nitrobenzene-d5 (S)%69 21-110
Phenol-d6 (S)%26 10-110
Terphenyl-d14 (S)%91 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349579
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92330519013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1939411
Associated Lab Samples:92330519013
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 02/24/17 10:151.9
1,2-Dichlorobenzene ug/L ND 10.0 02/24/17 10:151.2
1,3-Dichlorobenzene ug/L ND 10.0 02/24/17 10:151.1
1,4-Dichlorobenzene ug/L ND 10.0 02/24/17 10:151.2
1-Methylnaphthalene ug/L ND 10.0 02/24/17 10:150.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 02/24/17 10:151.6
2,4,5-Trichlorophenol ug/L ND 10.0 02/24/17 10:152.2
2,4,6-Trichlorophenol ug/L ND 10.0 02/24/17 10:151.9
2,4-Dichlorophenol ug/L ND 10.0 02/24/17 10:151.7
2,4-Dimethylphenol ug/L ND 10.0 02/24/17 10:152.2
2,4-Dinitrophenol ug/L ND 50.0 02/24/17 10:156.5
2,4-Dinitrotoluene ug/L ND 10.0 02/24/17 10:151.2
2,6-Dinitrotoluene ug/L ND 10.0 02/24/17 10:151.7
2-Chloronaphthalene ug/L ND 10.0 02/24/17 10:152.2
2-Chlorophenol ug/L ND 10.0 02/24/17 10:151.5
2-Methylnaphthalene ug/L ND 10.0 02/24/17 10:150.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 02/24/17 10:151.7
2-Nitroaniline ug/L ND 50.0 02/24/17 10:152.8
2-Nitrophenol ug/L ND 10.0 02/24/17 10:151.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 02/24/17 10:151.7
3,3'-Dichlorobenzidine ug/L ND 20.0 02/24/17 10:151.4
3-Nitroaniline ug/L ND 50.0 02/24/17 10:152.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 02/24/17 10:151.7
4-Bromophenylphenyl ether ug/L ND 10.0 02/24/17 10:151.3
4-Chloro-3-methylphenol ug/L ND 20.0 02/24/17 10:154.2
4-Chloroaniline ug/L ND 20.0 02/24/17 10:153.4
4-Chlorophenylphenyl ether ug/L ND 10.0 02/24/17 10:152.1
4-Nitroaniline ug/L ND 20.0 02/24/17 10:152.5
4-Nitrophenol ug/L ND 50.0 02/24/17 10:155.8
Acenaphthene ug/L ND 10.0 02/24/17 10:150.25
Acenaphthylene ug/L ND 10.0 02/24/17 10:150.21
Aniline ug/L ND 10.0 02/24/17 10:151.3
Anthracene ug/L ND 10.0 02/24/17 10:150.14
Benzo(a)anthracene ug/L ND 10.0 02/24/17 10:150.33
Benzo(a)pyrene ug/L ND 10.0 02/24/17 10:150.30
Benzo(b)fluoranthene ug/L ND 10.0 02/24/17 10:150.28
Benzo(g,h,i)perylene ug/L ND 10.0 02/24/17 10:150.38
Benzo(k)fluoranthene ug/L ND 10.0 02/24/17 10:150.43
Benzoic Acid ug/L ND 50.0 02/24/17 10:1511.1
Benzyl alcohol ug/L ND 20.0 02/24/17 10:153.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 02/24/17 10:151.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1939411
Associated Lab Samples:92330519013
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 02/24/17 10:151.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 02/24/17 10:150.85
Butylbenzylphthalate ug/L ND 10.0 02/24/17 10:150.75
Chrysene ug/L ND 10.0 02/24/17 10:150.21
Di-n-butylphthalate ug/L ND 10.0 02/24/17 10:151.1
Di-n-octylphthalate ug/L ND 10.0 02/24/17 10:150.86
Dibenz(a,h)anthracene ug/L ND 10.0 02/24/17 10:150.55
Dibenzofuran ug/L ND 10.0 02/24/17 10:151.8
Diethylphthalate ug/L ND 6000 02/24/17 10:151.3
Dimethylphthalate ug/L ND 10.0 02/24/17 10:151.5
Fluoranthene ug/L ND 10.0 02/24/17 10:150.21
Fluorene ug/L ND 10.0 02/24/17 10:150.21
Hexachloro-1,3-butadiene ug/L ND 10.0 02/24/17 10:151.8
Hexachlorobenzene ug/L ND 10.0 02/24/17 10:151.1
Hexachlorocyclopentadiene ug/L ND 10.0 02/24/17 10:151.8
Hexachloroethane ug/L ND 10.0 02/24/17 10:151.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 02/24/17 10:150.29
Isophorone ug/L ND 10.0 02/24/17 10:151.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 02/24/17 10:152.1
N-Nitrosodimethylamine ug/L ND 10.0 02/24/17 10:151.3
N-Nitrosodiphenylamine ug/L ND 10.0 02/24/17 10:151.3
Naphthalene ug/L ND 10.0 02/24/17 10:150.34
Nitrobenzene ug/L ND 10.0 02/24/17 10:151.7
Pentachlorophenol ug/L ND 25.0 02/24/17 10:152.3
Phenanthrene ug/L ND 10.0 02/24/17 10:150.22
Phenol ug/L ND 10.0 02/24/17 10:151.7
Pyrene ug/L ND 10.0 02/24/17 10:150.19
2,4,6-Tribromophenol (S)%84 27-110 02/24/17 10:15
2-Fluorobiphenyl (S)%76 27-110 02/24/17 10:15
2-Fluorophenol (S)%41 12-110 02/24/17 10:15
Nitrobenzene-d5 (S)%99 21-110 02/24/17 10:15
Phenol-d6 (S)%27 10-110 02/24/17 10:15
Terphenyl-d14 (S)%98 31-107 02/24/17 10:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1939412LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 38.450 77 31-120
1,2-Dichlorobenzene ug/L 31.750 63 38-120
1,3-Dichlorobenzene ug/L 29.050 58 30-122
1,4-Dichlorobenzene ug/L 29.750 59 37-120
1-Methylnaphthalene ug/L 39.550 79 34-113
2,2'-Oxybis(1-chloropropane)ug/L 32.950 66 18-120
2,4,5-Trichlorophenol ug/L 40.650 81 43-113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1939412LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 49.950 100 42-120
2,4-Dichlorophenol ug/L 44.950 90 30-120
2,4-Dimethylphenol ug/L 43.650 87 29-111
2,4-Dinitrophenol ug/L 245250 98 19-132
2,4-Dinitrotoluene ug/L 53.350 107 58-128
2,6-Dinitrotoluene ug/L 51.750 103 54-129
2-Chloronaphthalene ug/L 50.450 101 43-117
2-Chlorophenol ug/L 34.650 69 37-120
2-Methylnaphthalene ug/L 41.150 82 33-120
2-Methylphenol(o-Cresol)ug/L 27.950 56 31-120
2-Nitroaniline ug/L 93.6100 94 48-121
2-Nitrophenol ug/L 42.050 84 25-116
3&4-Methylphenol(m&p Cresol)ug/L 20.750 41 23-120
3,3'-Dichlorobenzidine ug/L 93.6100 94 10-154
3-Nitroaniline ug/L 87.5100 88 43-115
4,6-Dinitro-2-methylphenol ug/L 91.6100 92 44-124
4-Bromophenylphenyl ether ug/L 45.950 92 34-113
4-Chloro-3-methylphenol ug/L 86.4100 86 31-110
4-Chloroaniline ug/L 83.1100 83 20-120
4-Chlorophenylphenyl ether ug/L 44.650 89 34-116
4-Nitroaniline ug/L 89.8100 90 46-128
4-Nitrophenol ug/L 136250 55 11-120
Acenaphthene ug/L 44.250 88 48-114
Acenaphthylene ug/L 44.450 89 48-112
Aniline ug/L 26.550 53 26-120
Anthracene ug/L 46.350 93 57-118
Benzo(a)anthracene ug/L 49.250 98 56-121
Benzo(a)pyrene ug/L 54.950 110 55-127
Benzo(b)fluoranthene ug/L 58.050 116 53-128
Benzo(g,h,i)perylene ug/L 51.250 102 54-125
Benzo(k)fluoranthene ug/L 55.050 110 51-123
Benzoic Acid ug/L 84.8250 34 10-120
Benzyl alcohol ug/L 65.0100 65 27-120
bis(2-Chloroethoxy)methane ug/L 40.950 82 32-120
bis(2-Chloroethyl) ether ug/L 36.050 72 33-111
bis(2-Ethylhexyl)phthalate ug/L 57.250 114 50-145
Butylbenzylphthalate ug/L 57.150 114 54-138
Chrysene ug/L 46.350 93 58-127
Di-n-butylphthalate ug/L 53.950 108 56-125
Di-n-octylphthalate ug/L 59.250 118 50-134
Dibenz(a,h)anthracene ug/L 54.250 108 53-129
Dibenzofuran ug/L 44.350 89 45-120
Diethylphthalate ug/L 49.5J50 99 53-120
Dimethylphthalate ug/L 48.450 97 55-116
Fluoranthene ug/L 48.950 98 57-125
Fluorene ug/L 45.850 92 53-118
Hexachloro-1,3-butadiene ug/L 37.350 75 23-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Page 91 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1939412LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 42.350 85 49-116
Hexachlorocyclopentadiene ug/L 46.250 92 26-158
Hexachloroethane ug/L 31.550 63 30-114
Indeno(1,2,3-cd)pyrene ug/L 54.750 109 55-128
Isophorone ug/L 52.150 104 31-118
N-Nitroso-di-n-propylamine ug/L 42.250 84 32-119
N-Nitrosodimethylamine ug/L 25.550 51 13-120
N-Nitrosodiphenylamine ug/L 44.150 88 43-120
Naphthalene ug/L 39.350 79 32-120
Nitrobenzene ug/L 51.850 104 33-110
Pentachlorophenol ug/L 101100 101 10-137
Phenanthrene ug/L 45.850 92 57-117
Phenol ug/L 17.450 35 10-120
Pyrene ug/L 49.050 98 55-122
2,4,6-Tribromophenol (S)%97 27-110
2-Fluorobiphenyl (S)%85 27-110
2-Fluorophenol (S)%45 12-110
Nitrobenzene-d5 (S)%96 21-110
Phenol-d6 (S)%32 10-110
Terphenyl-d14 (S)%100 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
348843
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1935680
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 02/22/17 21:452000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1935681LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 181000198000 91 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330523001
1935682SAMPLE DUPLICATE:
BOD, 5 day ug/L ND B210ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Huntersville, NC 28078
[phone]
Page 93 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349339
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92330519001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330519001
1938038SAMPLE DUPLICATE:
pH Std. Units 7.3 H6197.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349158
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936889
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 02/21/17 20:321000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936890LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19400J20000 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1936891MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330376001
1936892
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M1200009090-11088 0 102000047100J65000J64800J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
348846
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1935691
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 02/18/17 00:3110.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1935692LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 25102500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1935693MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330435003
1935694
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 95 90-11095 0 1025000.041
mg/L 2420 2420
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349069
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936554
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
Phosphorus ug/L ND 50.0 02/21/17 20:4625.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936555LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 25902500 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1936556MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92329937006
1936557
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 95 90-11096 1 1025000.058
mg/L 2440 2450
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1936558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330308001
1936559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 99 90-11098 1 1025000.45 mg/L 2930 2910
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349537
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92330540001, 92330540004, 92330540005, 92330540006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1939086
Associated Lab Samples:92330540001, 92330540004, 92330540005, 92330540006
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 02/23/17 18:214.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1939087LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 113100 113 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1939088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330384002
1939089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11008080-12070 8 101000.063
mg/L 143 132
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1939090MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330577007
1939091
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 88 80-12087 1 10100ND87.5 87.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
350196
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92330519013, 92330519014, 92330519019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1942543
Associated Lab Samples:92330519013, 92330519014, 92330519019
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 03/01/17 13:284.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1942544LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 94.6100 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1942545MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92331094001
1942546
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 87 80-12088 1 10100ND89.3 90.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1942547MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92331074003
1942548
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11006780-12070 3 101000.0094
mg/L 76.8 79.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 117
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349235
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92330519001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1937618
Associated Lab Samples:92330519001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 02/22/17 00:2212500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1937619LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 747000750000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937620MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330190006
1937621
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 105 90-110104 1 375000050.0 mg/L 835000 830000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937622MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330433001
1937623
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 99 90-110101 1 3750000345 mg/L 1080000 1100000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Huntersville, NC 28078
[phone]
Page 100 of 117
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculatedfor the dilution using the most amount of sample.B2
Analysis initiated outside of the 15 minute EPA required holding time.H6
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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Huntersville, NC 28078
[phone]
Page 101 of 117
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92330540005 352340 353027MW-6 EPA 8151 EPA 8151
92330519001 348994 349091LE-1 EPA 3010A EPA 6010
92330539001 348994 349091MW-13 EPA 3010A EPA 6010
92330539002 349100 349267SW-4 EPA 3010A EPA 6010
92330540001 349100 349267MW-1 EPA 3010A EPA 6010
92330540002 349100 349267MW-3 EPA 3010A EPA 6010
92330540003 349100 349267MW-4 EPA 3010A EPA 6010
92330540004 349100 349267MW-5 EPA 3010A EPA 6010
92330540005 349100 349267MW-6 EPA 3010A EPA 6010
92330540006 349100 349267MW-7 EPA 3010A EPA 6010
92330540007 349100 349267MW-9 EPA 3010A EPA 6010
92330540008 349100 349267MW-10 EPA 3010A EPA 6010
92330519013 349553 349687MW-2 EPA 3010A EPA 6010
92330519014 349553 349687MW-8 EPA 3010A EPA 6010
92330519015 349553 349687MW-11 EPA 3010A EPA 6010
92330519016 349553 349687MW-12 EPA 3010A EPA 6010
92330519017 349553 349687MW-14 EPA 3010A EPA 6010
92330519018 349553 349687MW-15 EPA 3010A EPA 6010
92330519019 349553 349687MW-16R EPA 3010A EPA 6010
92330519020 349553 349687SW-5 EPA 3010A EPA 6010
92330539001 349257 349497MW-13 EPA 3010A EPA 6020B
92330539002 349257 349497SW-4 EPA 3010A EPA 6020B
92330540001 349257 349497MW-1 EPA 3010A EPA 6020B
92330540002 349257 349497MW-3 EPA 3010A EPA 6020B
92330540003 349257 349497MW-4 EPA 3010A EPA 6020B
92330540004 349257 349497MW-5 EPA 3010A EPA 6020B
92330540005 349257 349497MW-6 EPA 3010A EPA 6020B
92330540006 349257 349497MW-7 EPA 3010A EPA 6020B
92330540007 349258 349499MW-9 EPA 3010A EPA 6020B
92330540008 349258 349499MW-10 EPA 3010A EPA 6020B
92330519013 349668 349712MW-2 EPA 3010A EPA 6020B
92330519014 349668 349712MW-8 EPA 3010A EPA 6020B
92330519015 349668 349712MW-11 EPA 3010A EPA 6020B
92330519016 349668 349712MW-12 EPA 3010A EPA 6020B
92330519017 349668 349712MW-14 EPA 3010A EPA 6020B
92330519018 349668 349712MW-15 EPA 3010A EPA 6020B
92330519019 349668 349712MW-16R EPA 3010A EPA 6020B
92330519020 349668 349712SW-5 EPA 3010A EPA 6020B
92330519001 349177 349284LE-1 EPA 7470 EPA 7470
92330540001 349477 349493MW-1 EPA 7470 EPA 7470
92330540002 349477 349493MW-3 EPA 7470 EPA 7470
92330540003 349477 349493MW-4 EPA 7470 EPA 7470
92330540005 349477 349493MW-6 EPA 7470 EPA 7470
92330540006 349477 349493MW-7 EPA 7470 EPA 7470
92330540007 349477 349493MW-9 EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
Pace Analytical Services, LLC
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[phone]
Page 102 of 117
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92330519
Wayne Lined MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92330519015 350064 350267MW-11 EPA 7470 EPA 7470
92330540001 349028 349164MW-1 EPA 3510 EPA 8270
92330540006 349028 349164MW-7 EPA 3510 EPA 8270
92330519013 349579 349794MW-2 EPA 3510 EPA 8270
92330519001 349193LE-1 EPA 8260
92330539001 349990MW-13 EPA 8260
92330539002 349990SW-4 EPA 8260
92330540001 349990MW-1 EPA 8260
92330540002 349990MW-3 EPA 8260
92330540003 349990MW-4 EPA 8260
92330540004 349990MW-5 EPA 8260
92330540005 349990MW-6 EPA 8260
92330540006 349990MW-7 EPA 8260
92330540007 350034MW-9 EPA 8260
92330540008 350034MW-10 EPA 8260
92330519013 350034MW-2 EPA 8260
92330519014 350034MW-8 EPA 8260
92330519015 350034MW-11 EPA 8260
92330519016 350034MW-12 EPA 8260
92330519017 350034MW-14 EPA 8260
92330519018 350034MW-15 EPA 8260
92330519019 350035MW-16R EPA 8260
92330519020 350035SW-5 EPA 8260
92330519001 348843 348850LE-1 SM 5210B SM 5210B
92330519001 349339LE-1 EPA 9040
92330519001 349158LE-1 EPA 300.0
92330519001 348846LE-1 EPA 353.2
92330519001 349069LE-1 EPA 365.1
92330540001 349537MW-1 SM 4500-CN-E
92330540004 349537MW-5 SM 4500-CN-E
92330540005 349537MW-6 SM 4500-CN-E
92330540006 349537MW-7 SM 4500-CN-E
92330519013 350196MW-2 SM 4500-CN-E
92330519014 350196MW-8 SM 4500-CN-E
92330519019 350196MW-16R SM 4500-CN-E
92330519001 349235LE-1 SM 5220D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2017 06:06 PM
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9800 Kincey Ave. Suite 100
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[phone]
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#=CL#
February 09, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92328155
92328155
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE LINED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 31, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92328155001 HAB-1 Water 01/27/17 16:00 01/31/17 08:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92328155001 HAB-1 EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Sample:HAB-1 Lab ID:92328155001 Collected:01/27/17 16:00 Received:01/31/17 08:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 16.3J ug/L 02/07/17 17:01 67-64-1 C810010.0 1
Acrylonitrile ND ug/L 02/07/17 17:01 107-13-12001.9 1
Benzene 0.87J ug/L 02/07/17 17:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/07/17 17:01 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/07/17 17:01 75-27-41.0 0.18 1
Bromoform ND ug/L 02/07/17 17:01 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/07/17 17:01 74-83-910.0 0.29 1
2-Butanone (MEK)7.7J ug/L 02/07/17 17:01 78-93-3 C81000.96 1
Carbon disulfide ND ug/L 02/07/17 17:01 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/07/17 17:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/07/17 17:01 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/07/17 17:01 75-00-310.0 0.54 1
Chloroform ND ug/L 02/07/17 17:01 67-66-35.0 0.14 1
Chloromethane 0.20J ug/L 02/07/17 17:01 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/07/17 17:01 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/07/17 17:01 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/07/17 17:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/07/17 17:01 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/07/17 17:01 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/07/17 17:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/07/17 17:01 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/07/17 17:01 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/07/17 17:01 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 02/07/17 17:01 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/07/17 17:01 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/07/17 17:01 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/07/17 17:01 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 02/07/17 17:01 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/07/17 17:01 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/07/17 17:01 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/07/17 17:01 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/07/17 17:01 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/07/17 17:01 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/07/17 17:01 108-10-11000.33 1
Styrene ND ug/L 02/07/17 17:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/07/17 17:01 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/07/17 17:01 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/07/17 17:01 127-18-41.0 0.46 1
Toluene ND ug/L 02/07/17 17:01 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/07/17 17:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/07/17 17:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/07/17 17:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/07/17 17:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/07/17 17:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/07/17 17:01 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/07/17 17:01 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 5 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Sample:HAB-1 Lab ID:92328155001 Collected:01/27/17 16:00 Received:01/31/17 08:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 02/07/17 17:01 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %02/07/17 17:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/07/17 17:01 17060-07-070-130 1
Toluene-d8 (S)101 %02/07/17 17:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
347216
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92328155001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1925970
Associated Lab Samples:92328155001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/07/17 12:470.33
1,1,1-Trichloroethane ug/L ND 1.0 02/07/17 12:470.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/07/17 12:470.40
1,1,2-Trichloroethane ug/L ND 1.0 02/07/17 12:470.29
1,1-Dichloroethane ug/L ND 5.0 02/07/17 12:470.32
1,1-Dichloroethene ug/L ND 5.0 02/07/17 12:470.56
1,2,3-Trichloropropane ug/L ND 1.0 02/07/17 12:470.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/07/17 12:472.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/07/17 12:470.27
1,2-Dichlorobenzene ug/L ND 5.0 02/07/17 12:470.30
1,2-Dichloroethane ug/L ND 1.0 02/07/17 12:470.24
1,2-Dichloropropane ug/L ND 1.0 02/07/17 12:470.27
1,4-Dichlorobenzene ug/L ND 1.0 02/07/17 12:470.33
2-Butanone (MEK)ug/L ND 100 02/07/17 12:470.96
2-Hexanone ug/L ND 50.0 02/07/17 12:470.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/07/17 12:470.33
Acetone ug/L ND 100 02/07/17 12:4710.0
Acrylonitrile ug/L ND 200 02/07/17 12:471.9
Benzene ug/L ND 1.0 02/07/17 12:470.25
Bromochloromethane ug/L ND 3.0 02/07/17 12:470.17
Bromodichloromethane ug/L ND 1.0 02/07/17 12:470.18
Bromoform ug/L ND 3.0 02/07/17 12:470.26
Bromomethane ug/L ND 10.0 02/07/17 12:470.29
Carbon disulfide ug/L ND 100 02/07/17 12:471.2
Carbon tetrachloride ug/L ND 1.0 02/07/17 12:470.25
Chlorobenzene ug/L ND 3.0 02/07/17 12:470.23
Chloroethane ug/L ND 10.0 02/07/17 12:470.54
Chloroform ug/L ND 5.0 02/07/17 12:470.14
Chloromethane ug/L ND 1.0 02/07/17 12:470.11
cis-1,2-Dichloroethene ug/L ND 5.0 02/07/17 12:470.19
cis-1,3-Dichloropropene ug/L ND 1.0 02/07/17 12:470.13
Dibromochloromethane ug/L ND 3.0 02/07/17 12:470.21
Dibromomethane ug/L ND 10.0 02/07/17 12:470.21
Ethylbenzene ug/L ND 1.0 02/07/17 12:470.30
Iodomethane ug/L ND 10.0 02/07/17 12:470.32
Methylene Chloride ug/L ND 1.0 02/07/17 12:470.97
Styrene ug/L ND 1.0 02/07/17 12:470.26
Tetrachloroethene ug/L ND 1.0 02/07/17 12:470.46
Toluene ug/L ND 1.0 02/07/17 12:470.26
trans-1,2-Dichloroethene ug/L ND 5.0 02/07/17 12:470.49
trans-1,3-Dichloropropene ug/L ND 1.0 02/07/17 12:470.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1925970
Associated Lab Samples:92328155001
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 02/07/17 12:471.0
Trichloroethene ug/L ND 1.0 02/07/17 12:470.47
Trichlorofluoromethane ug/L ND 1.0 02/07/17 12:470.20
Vinyl acetate ug/L ND 50.0 02/07/17 12:470.35
Vinyl chloride ug/L ND 1.0 02/07/17 12:470.62
Xylene (Total)ug/L ND 5.0 02/07/17 12:470.66
1,2-Dichloroethane-d4 (S)%101 70-130 02/07/17 12:47
4-Bromofluorobenzene (S)%98 70-130 02/07/17 12:47
Toluene-d8 (S)%102 70-130 02/07/17 12:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1925971LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.250 90 80-125
1,1,1-Trichloroethane ug/L 49.350 99 71-129
1,1,2,2-Tetrachloroethane ug/L 46.450 93 79-124
1,1,2-Trichloroethane ug/L 48.950 98 85-125
1,1-Dichloroethane ug/L 47.750 95 73-126
1,1-Dichloroethene ug/L 52.050 104 66-135
1,2,3-Trichloropropane ug/L 48.250 96 75-130
1,2-Dibromo-3-chloropropane ug/L 43.650 87 71-133
1,2-Dibromoethane (EDB)ug/L 46.450 93 83-124
1,2-Dichlorobenzene ug/L 46.650 93 80-133
1,2-Dichloroethane ug/L 49.050 98 67-128
1,2-Dichloropropane ug/L 46.950 94 75-132
1,4-Dichlorobenzene ug/L 45.150 90 78-130
2-Butanone (MEK)ug/L 98.0J100 98 61-144
2-Hexanone ug/L 94.5100 95 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 99.2J100 99 48-146
Acrylonitrile ug/L 252250 101 40-160
Benzene ug/L 48.950 98 80-125
Bromochloromethane ug/L 51.250 102 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 42.150 84 71-128
Bromomethane ug/L 50.850 102 40-160
Carbon disulfide ug/L 52.1J50 104 50-160
Carbon tetrachloride ug/L 45.950 92 69-131
Chlorobenzene ug/L 47.050 94 81-122
Chloroethane ug/L 52.950 106 39-148
Chloroform ug/L 48.450 97 73-127
Chloromethane ug/L 54.250 108 44-146
cis-1,2-Dichloroethene ug/L 48.750 97 74-124
cis-1,3-Dichloropropene ug/L 49.050 98 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1925971LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 46.850 94 78-125
Dibromomethane ug/L 48.850 98 82-120
Ethylbenzene ug/L 45.950 92 79-121
Iodomethane ug/L 99.8100 100 39-154
Methylene Chloride ug/L 51.950 104 64-133
Styrene ug/L 47.050 94 84-126
Tetrachloroethene ug/L 44.550 89 78-122
Toluene ug/L 48.150 96 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 48.150 96 69-141
trans-1,4-Dichloro-2-butene ug/L 46.7J50 93 40-160
Trichloroethene ug/L 47.750 95 78-122
Trichlorofluoromethane ug/L 56.750 113 53-137
Vinyl acetate ug/L 102100 102 40-160
Vinyl chloride ug/L 44.950 90 58-137
Xylene (Total)ug/L 139150 92 81-126
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1925972MATRIX SPIKE SAMPLE:
MSSpike
Result
92327840012
1,1,1,2-Tetrachloroethane ug/L 38.940 97 70-130ND
1,1,1-Trichloroethane ug/L 43.840 110 70-130ND
1,1,2,2-Tetrachloroethane ug/L 40.640 102 70-130ND
1,1,2-Trichloroethane ug/L 42.440 106 70-130ND
1,1-Dichloroethane ug/L 42.240 105 70-130ND
1,1-Dichloroethene ug/L 47.140 118 70-166ND
1,2,3-Trichloropropane ug/L 43.640 109 70-130ND
1,2-Dibromo-3-chloropropane ug/L 40.140 100 70-130ND
1,2-Dibromoethane (EDB)ug/L 39.640 99 70-130ND
1,2-Dichlorobenzene ug/L 41.440 104 70-130ND
1,2-Dichloroethane ug/L 41.640 102 70-1300.77J
1,2-Dichloropropane ug/L 41.640 104 70-130ND
1,4-Dichlorobenzene ug/L 41.940 101 70-1301.6J
2-Butanone (MEK)ug/L 1440 E,M18031670-1301190
2-Hexanone ug/L 92.8J80 111 70-1304.1J
4-Methyl-2-pentanone (MIBK)ug/L 121J80 116 70-13027.9J
Acetone ug/L 1450 E,M18030170-1301210
Acrylonitrile ug/L 226J200 113 70-130ND
Benzene ug/L 49.540 109 70-1485.7
Bromochloromethane ug/L 43.440 108 70-130ND
Bromodichloromethane ug/L 41.840 105 70-130ND
Bromoform ug/L 33.140 83 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1925972MATRIX SPIKE SAMPLE:
MSSpike
Result
92327840012
Bromomethane ug/L 46.640 117 70-130ND
Carbon disulfide ug/L 45.6J40 114 70-130ND
Carbon tetrachloride ug/L 40.640 101 70-130ND
Chlorobenzene ug/L 43.240 105 70-1461.1J
Chloroethane ug/L 46.840 117 70-130ND
Chloroform ug/L 43.140 108 70-130ND
Chloromethane ug/L 48.240 121 70-130ND
cis-1,2-Dichloroethene ug/L 43.240 107 70-1300.39J
cis-1,3-Dichloropropene ug/L 40.140 100 70-130ND
Dibromochloromethane ug/L 38.740 97 70-130ND
Dibromomethane ug/L 42.240 105 70-130ND
Ethylbenzene ug/L 56.240 104 70-13014.7
Iodomethane ug/L 83.380 104 70-130ND
Methylene Chloride ug/L 51.140 108 70-1307.8
Styrene ug/L 42.040 104 70-130ND
Tetrachloroethene ug/L 40.240 101 70-130ND
Toluene ug/L 47.740 109 70-1554.0
trans-1,2-Dichloroethene ug/L 45.440 113 70-130ND
trans-1,3-Dichloropropene ug/L 39.040 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 35.1J40 88 70-130ND
Trichloroethene ug/L 44.140 110 69-151ND
Trichlorofluoromethane ug/L 50.240 126 70-130ND
Vinyl acetate ug/L 83.5J80 104 70-130ND
Vinyl chloride ug/L 39.540 98 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92328155001
1925973SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 307.7J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92328155001
1925973SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 3016.3J
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.92J 300.87J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.18J 300.20J
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 298
4-Bromofluorobenzene (S)%97 097
Toluene-d8 (S)%100 1101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
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Page 11 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Result may be biased high due to carryover from previously analyzed sample.C8
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
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Page 12 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92328155
WAYNE LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92328155001 347216HAB-1 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2017 12:44 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 13 of 16
Page 14 of 16
Page 15 of 16
Page 16 of 16
#=CL#
January 17, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92325857
92325857
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE P1-7
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 11, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325857
WAYNE P1-7
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 16
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325857
WAYNE P1-7
Lab ID Sample ID Matrix Date Collected Date Received
92325857001 P1-7 Water 01/06/17 16:00 01/11/17 08:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325857
WAYNE P1-7
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325857001 P1-7 EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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Page 4 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325857
WAYNE P1-7
Sample:P1-7 Lab ID:92325857001 Collected:01/06/17 16:00 Received:01/11/17 08:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/13/17 17:23 67-64-110010.0 1
Acrylonitrile ND ug/L 01/13/17 17:23 107-13-12001.9 1
Benzene ND ug/L 01/13/17 17:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/13/17 17:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/13/17 17:23 75-27-41.0 0.18 1
Bromoform ND ug/L 01/13/17 17:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/13/17 17:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/13/17 17:23 78-93-31000.96 1
Carbon disulfide ND ug/L 01/13/17 17:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/13/17 17:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/13/17 17:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/13/17 17:23 75-00-310.0 0.54 1
Chloroform ND ug/L 01/13/17 17:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/13/17 17:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/13/17 17:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/13/17 17:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/13/17 17:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/13/17 17:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/13/17 17:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/13/17 17:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/13/17 17:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/13/17 17:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/13/17 17:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/13/17 17:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/13/17 17:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/13/17 17:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/13/17 17:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/13/17 17:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/13/17 17:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/13/17 17:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/13/17 17:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/13/17 17:23 74-88-410.0 0.32 1
Methylene Chloride 2.7 ug/L 01/13/17 17:23 75-09-2 B,C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/13/17 17:23 108-10-11000.33 1
Styrene ND ug/L 01/13/17 17:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/13/17 17:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/13/17 17:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/13/17 17:23 127-18-41.0 0.46 1
Toluene ND ug/L 01/13/17 17:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/13/17 17:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/13/17 17:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/13/17 17:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/13/17 17:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/13/17 17:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/13/17 17:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/13/17 17:23 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 5 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325857
WAYNE P1-7
Sample:P1-7 Lab ID:92325857001 Collected:01/06/17 16:00 Received:01/11/17 08:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 01/13/17 17:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %01/13/17 17:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %01/13/17 17:23 17060-07-070-130 1
Toluene-d8 (S)103 %01/13/17 17:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 6 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325857
WAYNE P1-7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344130
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325857001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1909054
Associated Lab Samples:92325857001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/13/17 11:530.33
1,1,1-Trichloroethane ug/L ND 1.0 01/13/17 11:530.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/13/17 11:530.40
1,1,2-Trichloroethane ug/L ND 1.0 01/13/17 11:530.29
1,1-Dichloroethane ug/L ND 5.0 01/13/17 11:530.32
1,1-Dichloroethene ug/L ND 5.0 01/13/17 11:530.56
1,2,3-Trichloropropane ug/L ND 1.0 01/13/17 11:530.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/13/17 11:532.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/13/17 11:530.27
1,2-Dichlorobenzene ug/L ND 5.0 01/13/17 11:530.30
1,2-Dichloroethane ug/L ND 1.0 01/13/17 11:530.24
1,2-Dichloropropane ug/L ND 1.0 01/13/17 11:530.27
1,4-Dichlorobenzene ug/L ND 1.0 01/13/17 11:530.33
2-Butanone (MEK)ug/L ND 100 01/13/17 11:530.96
2-Hexanone ug/L ND 50.0 01/13/17 11:530.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/13/17 11:530.33
Acetone ug/L ND 100 01/13/17 11:5310.0
Acrylonitrile ug/L ND 200 01/13/17 11:531.9
Benzene ug/L ND 1.0 01/13/17 11:530.25
Bromochloromethane ug/L ND 3.0 01/13/17 11:530.17
Bromodichloromethane ug/L ND 1.0 01/13/17 11:530.18
Bromoform ug/L ND 3.0 01/13/17 11:530.26
Bromomethane ug/L ND 10.0 01/13/17 11:530.29
Carbon disulfide ug/L ND 100 01/13/17 11:531.2
Carbon tetrachloride ug/L ND 1.0 01/13/17 11:530.25
Chlorobenzene ug/L ND 3.0 01/13/17 11:530.23
Chloroethane ug/L ND 10.0 01/13/17 11:530.54
Chloroform ug/L ND 5.0 01/13/17 11:530.14
Chloromethane ug/L ND 1.0 01/13/17 11:530.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/13/17 11:530.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/13/17 11:530.13
Dibromochloromethane ug/L ND 3.0 01/13/17 11:530.21
Dibromomethane ug/L ND 10.0 01/13/17 11:530.21
Ethylbenzene ug/L ND 1.0 01/13/17 11:530.30
Iodomethane ug/L ND 10.0 01/13/17 11:530.32
Methylene Chloride ug/L 2.0 1.0 C901/13/17 11:530.97
Styrene ug/L ND 1.0 01/13/17 11:530.26
Tetrachloroethene ug/L ND 1.0 01/13/17 11:530.46
Toluene ug/L ND 1.0 01/13/17 11:530.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/13/17 11:530.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/13/17 11:530.26
REPORT OF LABORATORY ANALYSIS
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Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325857
WAYNE P1-7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1909054
Associated Lab Samples:92325857001
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/13/17 11:531.0
Trichloroethene ug/L ND 1.0 01/13/17 11:530.47
Trichlorofluoromethane ug/L ND 1.0 01/13/17 11:530.20
Vinyl acetate ug/L ND 50.0 01/13/17 11:530.35
Vinyl chloride ug/L ND 1.0 01/13/17 11:530.62
Xylene (Total)ug/L ND 5.0 01/13/17 11:530.66
1,2-Dichloroethane-d4 (S)%93 70-130 01/13/17 11:53
4-Bromofluorobenzene (S)%104 70-130 01/13/17 11:53
Toluene-d8 (S)%104 70-130 01/13/17 11:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909055LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 80-125
1,1,1-Trichloroethane ug/L 50.550 101 71-129
1,1,2,2-Tetrachloroethane ug/L 46.150 92 79-124
1,1,2-Trichloroethane ug/L 46.950 94 85-125
1,1-Dichloroethane ug/L 46.850 94 73-126
1,1-Dichloroethene ug/L 52.350 105 66-135
1,2,3-Trichloropropane ug/L 47.150 94 75-130
1,2-Dibromo-3-chloropropane ug/L 44.550 89 71-133
1,2-Dibromoethane (EDB)ug/L 47.550 95 83-124
1,2-Dichlorobenzene ug/L 47.750 95 80-133
1,2-Dichloroethane ug/L 45.850 92 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,4-Dichlorobenzene ug/L 46.350 93 78-130
2-Butanone (MEK)ug/L 82.4J100 82 61-144
2-Hexanone ug/L 83.0100 83 68-143
4-Methyl-2-pentanone (MIBK)ug/L 84.8J100 85 72-135
Acetone ug/L 82.1J100 82 48-146
Acrylonitrile ug/L 213250 85 40-160
Benzene ug/L 49.150 98 80-125
Bromochloromethane ug/L 45.950 92 71-125
Bromodichloromethane ug/L 46.550 93 78-124
Bromoform ug/L 49.050 98 71-128
Bromomethane ug/L 31.050 62 40-160
Carbon disulfide ug/L 46.7J50 93 50-160
Carbon tetrachloride ug/L 53.750 107 69-131
Chlorobenzene ug/L 49.950 100 81-122
Chloroethane ug/L 48.650 97 39-148
Chloroform ug/L 46.150 92 73-127
Chloromethane ug/L 44.250 88 44-146
cis-1,2-Dichloroethene ug/L 45.450 91 74-124
cis-1,3-Dichloropropene ug/L 49.550 99 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325857
WAYNE P1-7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909055LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 50.350 101 78-125
Dibromomethane ug/L 47.450 95 82-120
Ethylbenzene ug/L 49.050 98 79-121
Iodomethane ug/L 72.2100 72 39-154
Methylene Chloride ug/L 50.050 100 64-133
Styrene ug/L 49.150 98 84-126
Tetrachloroethene ug/L 48.750 97 78-122
Toluene ug/L 46.750 93 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 49.150 98 69-141
trans-1,4-Dichloro-2-butene ug/L 39.6J50 79 40-160
Trichloroethene ug/L 51.050 102 78-122
Trichlorofluoromethane ug/L 54.350 109 53-137
Vinyl acetate ug/L 92.1100 92 40-160
Vinyl chloride ug/L 40.950 82 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909056MATRIX SPIKE SAMPLE:
MSSpike
Result
92325855001
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,2-Trichloroethane ug/L 20.720 103 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 24.020 120 70-166ND
1,2,3-Trichloropropane ug/L 18.920 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.320 87 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 20.620 103 70-130ND
1,2-Dichloroethane ug/L 20.720 103 70-130ND
1,2-Dichloropropane ug/L 20.720 104 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 33.3J40 83 70-130ND
2-Hexanone ug/L 33.4J40 83 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.1J40 88 70-130ND
Acetone ug/L 33.0J40 83 70-130ND
Acrylonitrile ug/L 90.5J100 90 70-130ND
Benzene ug/L 22.820 114 70-148ND
Bromochloromethane ug/L 20.820 104 70-130ND
Bromodichloromethane ug/L 21.020 105 70-130ND
Bromoform ug/L 16.220 81 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325857
WAYNE P1-7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909056MATRIX SPIKE SAMPLE:
MSSpike
Result
92325855001
Bromomethane ug/L 20.220 101 70-130ND
Carbon disulfide ug/L 21.4J20 107 70-130ND
Carbon tetrachloride ug/L 23.620 118 70-130ND
Chlorobenzene ug/L 21.920 109 70-146ND
Chloroethane ug/L 22.020 110 70-130ND
Chloroform ug/L 21.120 106 70-130ND
Chloromethane ug/L 22.320 111 70-130ND
cis-1,2-Dichloroethene ug/L 21.320 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.120 105 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 21.420 107 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 27.1 M1406870-130ND
Methylene Chloride ug/L 23.920 109 70-1302.1
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 20.720 104 70-130ND
Toluene ug/L 21.820 109 70-155ND
trans-1,2-Dichloroethene ug/L 22.320 111 70-130ND
trans-1,3-Dichloropropene ug/L 20.720 104 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.0J20 70 70-130ND
Trichloroethene ug/L 22.820 114 69-151ND
Trichlorofluoromethane ug/L 25.620 128 70-130ND
Vinyl acetate ug/L 33.1J40 83 70-130ND
Vinyl chloride ug/L 19.320 97 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325855002
1909057SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325857
WAYNE P1-7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325855002
1909057SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L 2.2 C97302.1
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%94 195
4-Bromofluorobenzene (S)%103 2101
Toluene-d8 (S)%107 2105
REPORT OF LABORATORY ANALYSIS
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Page 11 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325857
WAYNE P1-7
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 12 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325857
WAYNE P1-7
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325857001 344130P1-7 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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[phone]
Page 13 of 16
Page 14 of 16
Page 15 of 16
Page 16 of 16
#=CL#
January 17, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92325858
92325858
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE-TMW-13A
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 11, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 16
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Lab ID Sample ID Matrix Date Collected Date Received
92325858001 TMW-13A Water 01/06/17 15:30 01/11/17 08:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325858001 TMW-13A EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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Page 4 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Sample:TMW-13A Lab ID:92325858001 Collected:01/06/17 15:30 Received:01/11/17 08:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/13/17 17:41 67-64-110010.0 1
Acrylonitrile ND ug/L 01/13/17 17:41 107-13-12001.9 1
Benzene ND ug/L 01/13/17 17:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/13/17 17:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/13/17 17:41 75-27-41.0 0.18 1
Bromoform ND ug/L 01/13/17 17:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/13/17 17:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/13/17 17:41 78-93-31000.96 1
Carbon disulfide ND ug/L 01/13/17 17:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/13/17 17:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/13/17 17:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/13/17 17:41 75-00-310.0 0.54 1
Chloroform ND ug/L 01/13/17 17:41 67-66-35.0 0.14 1
Chloromethane 0.39J ug/L 01/13/17 17:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/13/17 17:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/13/17 17:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/13/17 17:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/13/17 17:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/13/17 17:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/13/17 17:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/13/17 17:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/13/17 17:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/13/17 17:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/13/17 17:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/13/17 17:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/13/17 17:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/13/17 17:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/13/17 17:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/13/17 17:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/13/17 17:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/13/17 17:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/13/17 17:41 74-88-410.0 0.32 1
Methylene Chloride 2.5 ug/L 01/13/17 17:41 75-09-2 B,C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/13/17 17:41 108-10-11000.33 1
Styrene ND ug/L 01/13/17 17:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/13/17 17:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/13/17 17:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/13/17 17:41 127-18-41.0 0.46 1
Toluene ND ug/L 01/13/17 17:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/13/17 17:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/13/17 17:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/13/17 17:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/13/17 17:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/13/17 17:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/13/17 17:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/13/17 17:41 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 5 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Sample:TMW-13A Lab ID:92325858001 Collected:01/06/17 15:30 Received:01/11/17 08:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 01/13/17 17:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/13/17 17:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %01/13/17 17:41 17060-07-070-130 1
Toluene-d8 (S)106 %01/13/17 17:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344130
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325858001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1909054
Associated Lab Samples:92325858001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/13/17 11:530.33
1,1,1-Trichloroethane ug/L ND 1.0 01/13/17 11:530.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/13/17 11:530.40
1,1,2-Trichloroethane ug/L ND 1.0 01/13/17 11:530.29
1,1-Dichloroethane ug/L ND 5.0 01/13/17 11:530.32
1,1-Dichloroethene ug/L ND 5.0 01/13/17 11:530.56
1,2,3-Trichloropropane ug/L ND 1.0 01/13/17 11:530.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/13/17 11:532.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/13/17 11:530.27
1,2-Dichlorobenzene ug/L ND 5.0 01/13/17 11:530.30
1,2-Dichloroethane ug/L ND 1.0 01/13/17 11:530.24
1,2-Dichloropropane ug/L ND 1.0 01/13/17 11:530.27
1,4-Dichlorobenzene ug/L ND 1.0 01/13/17 11:530.33
2-Butanone (MEK)ug/L ND 100 01/13/17 11:530.96
2-Hexanone ug/L ND 50.0 01/13/17 11:530.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/13/17 11:530.33
Acetone ug/L ND 100 01/13/17 11:5310.0
Acrylonitrile ug/L ND 200 01/13/17 11:531.9
Benzene ug/L ND 1.0 01/13/17 11:530.25
Bromochloromethane ug/L ND 3.0 01/13/17 11:530.17
Bromodichloromethane ug/L ND 1.0 01/13/17 11:530.18
Bromoform ug/L ND 3.0 01/13/17 11:530.26
Bromomethane ug/L ND 10.0 01/13/17 11:530.29
Carbon disulfide ug/L ND 100 01/13/17 11:531.2
Carbon tetrachloride ug/L ND 1.0 01/13/17 11:530.25
Chlorobenzene ug/L ND 3.0 01/13/17 11:530.23
Chloroethane ug/L ND 10.0 01/13/17 11:530.54
Chloroform ug/L ND 5.0 01/13/17 11:530.14
Chloromethane ug/L ND 1.0 01/13/17 11:530.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/13/17 11:530.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/13/17 11:530.13
Dibromochloromethane ug/L ND 3.0 01/13/17 11:530.21
Dibromomethane ug/L ND 10.0 01/13/17 11:530.21
Ethylbenzene ug/L ND 1.0 01/13/17 11:530.30
Iodomethane ug/L ND 10.0 01/13/17 11:530.32
Methylene Chloride ug/L 2.0 1.0 C901/13/17 11:530.97
Styrene ug/L ND 1.0 01/13/17 11:530.26
Tetrachloroethene ug/L ND 1.0 01/13/17 11:530.46
Toluene ug/L ND 1.0 01/13/17 11:530.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/13/17 11:530.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/13/17 11:530.26
REPORT OF LABORATORY ANALYSIS
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Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1909054
Associated Lab Samples:92325858001
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/13/17 11:531.0
Trichloroethene ug/L ND 1.0 01/13/17 11:530.47
Trichlorofluoromethane ug/L ND 1.0 01/13/17 11:530.20
Vinyl acetate ug/L ND 50.0 01/13/17 11:530.35
Vinyl chloride ug/L ND 1.0 01/13/17 11:530.62
Xylene (Total)ug/L ND 5.0 01/13/17 11:530.66
1,2-Dichloroethane-d4 (S)%93 70-130 01/13/17 11:53
4-Bromofluorobenzene (S)%104 70-130 01/13/17 11:53
Toluene-d8 (S)%104 70-130 01/13/17 11:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909055LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 80-125
1,1,1-Trichloroethane ug/L 50.550 101 71-129
1,1,2,2-Tetrachloroethane ug/L 46.150 92 79-124
1,1,2-Trichloroethane ug/L 46.950 94 85-125
1,1-Dichloroethane ug/L 46.850 94 73-126
1,1-Dichloroethene ug/L 52.350 105 66-135
1,2,3-Trichloropropane ug/L 47.150 94 75-130
1,2-Dibromo-3-chloropropane ug/L 44.550 89 71-133
1,2-Dibromoethane (EDB)ug/L 47.550 95 83-124
1,2-Dichlorobenzene ug/L 47.750 95 80-133
1,2-Dichloroethane ug/L 45.850 92 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,4-Dichlorobenzene ug/L 46.350 93 78-130
2-Butanone (MEK)ug/L 82.4J100 82 61-144
2-Hexanone ug/L 83.0100 83 68-143
4-Methyl-2-pentanone (MIBK)ug/L 84.8J100 85 72-135
Acetone ug/L 82.1J100 82 48-146
Acrylonitrile ug/L 213250 85 40-160
Benzene ug/L 49.150 98 80-125
Bromochloromethane ug/L 45.950 92 71-125
Bromodichloromethane ug/L 46.550 93 78-124
Bromoform ug/L 49.050 98 71-128
Bromomethane ug/L 31.050 62 40-160
Carbon disulfide ug/L 46.7J50 93 50-160
Carbon tetrachloride ug/L 53.750 107 69-131
Chlorobenzene ug/L 49.950 100 81-122
Chloroethane ug/L 48.650 97 39-148
Chloroform ug/L 46.150 92 73-127
Chloromethane ug/L 44.250 88 44-146
cis-1,2-Dichloroethene ug/L 45.450 91 74-124
cis-1,3-Dichloropropene ug/L 49.550 99 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
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Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1909055LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 50.350 101 78-125
Dibromomethane ug/L 47.450 95 82-120
Ethylbenzene ug/L 49.050 98 79-121
Iodomethane ug/L 72.2100 72 39-154
Methylene Chloride ug/L 50.050 100 64-133
Styrene ug/L 49.150 98 84-126
Tetrachloroethene ug/L 48.750 97 78-122
Toluene ug/L 46.750 93 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 49.150 98 69-141
trans-1,4-Dichloro-2-butene ug/L 39.6J50 79 40-160
Trichloroethene ug/L 51.050 102 78-122
Trichlorofluoromethane ug/L 54.350 109 53-137
Vinyl acetate ug/L 92.1100 92 40-160
Vinyl chloride ug/L 40.950 82 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909056MATRIX SPIKE SAMPLE:
MSSpike
Result
92325855001
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,2-Trichloroethane ug/L 20.720 103 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 24.020 120 70-166ND
1,2,3-Trichloropropane ug/L 18.920 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.320 87 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 20.620 103 70-130ND
1,2-Dichloroethane ug/L 20.720 103 70-130ND
1,2-Dichloropropane ug/L 20.720 104 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 33.3J40 83 70-130ND
2-Hexanone ug/L 33.4J40 83 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.1J40 88 70-130ND
Acetone ug/L 33.0J40 83 70-130ND
Acrylonitrile ug/L 90.5J100 90 70-130ND
Benzene ug/L 22.820 114 70-148ND
Bromochloromethane ug/L 20.820 104 70-130ND
Bromodichloromethane ug/L 21.020 105 70-130ND
Bromoform ug/L 16.220 81 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1909056MATRIX SPIKE SAMPLE:
MSSpike
Result
92325855001
Bromomethane ug/L 20.220 101 70-130ND
Carbon disulfide ug/L 21.4J20 107 70-130ND
Carbon tetrachloride ug/L 23.620 118 70-130ND
Chlorobenzene ug/L 21.920 109 70-146ND
Chloroethane ug/L 22.020 110 70-130ND
Chloroform ug/L 21.120 106 70-130ND
Chloromethane ug/L 22.320 111 70-130ND
cis-1,2-Dichloroethene ug/L 21.320 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.120 105 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 21.420 107 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 27.1 M1406870-130ND
Methylene Chloride ug/L 23.920 109 70-1302.1
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 20.720 104 70-130ND
Toluene ug/L 21.820 109 70-155ND
trans-1,2-Dichloroethene ug/L 22.320 111 70-130ND
trans-1,3-Dichloropropene ug/L 20.720 104 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.0J20 70 70-130ND
Trichloroethene ug/L 22.820 114 69-151ND
Trichlorofluoromethane ug/L 25.620 128 70-130ND
Vinyl acetate ug/L 33.1J40 83 70-130ND
Vinyl chloride ug/L 19.320 97 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325855002
1909057SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325855002
1909057SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L 2.2 C97302.1
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%94 195
4-Bromofluorobenzene (S)%103 2101
Toluene-d8 (S)%107 2105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325858
WAYNE-TMW-13A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325858001 344130TMW-13A EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/17/2017 06:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 16
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