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Home My WebLink About21018_E Craighead Storage_Phase II ESA-Test Pit Excavations_2015Via Email July 8, 2015 Crescent Communities, LLC 227 W. Trade Street, Suite 1000 Charlotte, NC 28203 Attention: Mr. Creighton Call Re: Phase II ESA Test Pit Excavations NoDa Greenway E. Craighead Road / Philemon Avenue Charlotte, North Carolina H&H Job No. CRE-001 Dear Creighton: Hart & Hickman, PC (H&H) has conducted Phase II Environmental Site Assessment (ESA) test pit activities at the NoDa Greenway property (site) located along E. Craighead Road and Philemon Avenue in Charlotte, Mecklenburg County, North Carolina. In order to assess the areas of reported dumping and filling activities and to evaluate the nature of fill materials, H&H excavated 13 test pits and collected soil samples. Because the property south of Philemon Ave is covered by an existing Brownfields Agreement with the North Carolina Department of Environment and Natural Resources (DENR) Brownfields Program, H&H provided the work plan for that portion of the site to Ms. Carolyn Minnich of DENR to review. As noted in Carolyn’s attached email response approving this work, prior metal detections at the site are considered to be naturally occurring. Per your request, H&H will not complete a Phase II ESA report at this time. Rather, we are providing the attached data for your files. We will be glad to complete environmental reports for this work at your request. Please find enclosed the following documentation of the test pit activities: •a figure depicting the test pit and associated sample locations; •a tabular summary of the analytical results in comparison to potential regulatory screening levels; •copies of test pit logs; •laboratory analytical reports; and •Email to DENR Brownfields Program with response. Mr. Creighton Call July 8, 2015 Page 2 S:\AAA-Master Projects\Crescent Communities (CRE)\CRE-001 NoDa Greenway\Report\Test Pit Package Cover Letter.doc Should you have any questions or need further information, please do not hesitate to contact me at (704) 586-0007. Sincerely, Hart & Hickman, PC Matt Bramblett, PE Principal Attachments ATTACHMENT 1 SITE MAP RALEIGH ST R E E T RAILROAD TRACK S N. TRYON ST R E E T PHILEM O N A V E N U E TP-1 GRAVEL STORAGE YARD CHURCH TRX TRAILER TRAILER GRADING MATERIAL PILES& SCREENING MACHINE CRUSHED CONCRETE E . C R A I G H E A D R O A D PINE NEEDLE STORAGE VACANT RESIDENCE TP-2 TP-3 TP-4 TP-13 TP-12 TP-11 TP-10 TP-9 TP-8 TP-7 TP-6 TP-5 TP-12 REFUSED TP-9 REFUSED TP-5 REFUSED (2.5) (9) (10.5) (4.5) (>4) (14) (11.5) (11.5) (12) (12) (13) (8) (11)METROMONT CONCRETE TP-12 REFUSED TP-12 REFUSED 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) License # C-1269 / #C-245 Geology JOB NO. CRE-001 REVISION NO. 0DATE: 06-25-15 FIGURE NO. 2 MULTIPLE PARCELS - NODA GREENWAY E. CRAIGHEAD ROAD / PHILEMON AVENUE CHARLOTTE, NORTH CAROLINA SITE MAP NOTES: 1. AERIAL PHOTOGRAPH (2013) & PARCEL LAYERSOBTAINED FROM MECKLENBURG COUNTY GIS. 2. TEST PITS WERE INSTALLED ON JUNE 22 & 23, 2015.3. TP-5 WAS UNABLE TO REACH BOTTOM OF FILL/ DEBRIS. LEGEND SITE PROPERTY BOUNDARY LITTLE SUGAR CREEK &ASSOCIATED TRIBUTARIES TEST PIT REFUSED TEST PIT FILL/ DEBRIS DEPTH (FT.)(13) ATTACHMENT 2 SUMMARY OF TEST PIT SOIL ANALYTICAL DATA Table 1 (Page 1 of 1) Summary of Test Pit Soil Analytical DataNoDa Greenway Charlotte, North Carolina H&H Job No. CRE-001 S:\AAA-Master Projects\Crescent Communities (CRE)\CRE-001 NoDa Greenway\Tables\Test Pit_Analytical Data Tables7/8/2015 Table 1 (Page 1 of 1)Hart & Hickman, PC Sample ID TP-1 TP-3 TP-4 TP-5 TP-7 TP-9 TP-12 Depth (ft bgs)0-2 2-4 4-6 4-6 0-2 0-2 0-2 8-10 0-2 0-2 8-10 8-10 0-2 6-13 0-2 0-2 10-11 Sample Date 6/23/2015 6/23/2015 6/23/2015 6/23/2015 6/23/2015 6/22/2015 6/22/2015 6/22/2015 6/22/2015 6/22/2015 6/22/2015 6/22/2015 6/22/2015 6/22/2015 6/23/2015 6/23/2015 6/23/2015 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg VOCs (8260B) Acetone 24 12,000 100,000 ----0.152 0.0666 0.0801 <0.0417 <0.0428 0.196 0.0470 <0.0461 <0.0522 <0.0583 <0.0529 <0.0527 <0.0460 NA 0.0568 <0.0461 0.359 Carbon disulfide 3.8 150 700 ----<0.00483 <0.00488 <0.00773 <0.00417 0.00788 <0.00625 0.00454 <0.00461 <0.00522 <0.00583 <0.00529 0.0516 <0.00460 NA <0.00507 <0.00461 <0.00620 Dichlorodifluoromethane 29 17 74 ----<0.00193 <0.00195 <0.00309 <0.00167 <0.00171 <0.00250 <0.00162 <0.00185 <0.00209 <0.00233 <0.00212 <0.00211 0.00191 NA <0.00203 <0.00184 <0.00248 SVOCs (8270C) Acenaphthene 8.4 700 9,000 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 <0.0667 <0.334 <0.0668 1.29 40.3 <0.335 <0.0666 <0.329 NA <0.333 <0.335 <0.331 Anthracene 660 3,400 46,000 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.112 <0.334 0.0814 2.38 64.5 <0.335 <0.0666 <0.329 NA <0.333 <0.335 <0.331 Benzo[a]anthracene 0.18 0.15 2.9 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.326 <0.334 0.282 7.21 139 0.570 0.190 <0.329 NA <0.333 0.446 0.512 Benzo[a]pyrene 0.059 0.015 0.29 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.278 <0.334 0.259 6.51 124 0.493 0.155 <0.329 NA <0.333 0.419 0.460 Benzo[b]fluoranthene 0.60 0.15 2.9 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.343 0.385 0.349 8.72 175 0.668 0.190 <0.329 NA <0.333 0.602 0.624 Benzo[g,h,i]perylene 7,800 NS NS ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.162 <0.334 0.149 3.51 80.7 0.362 0.0892 <0.329 NA <0.333 <0.335 <0.331 Benzo[k]fluoranthene 5.9 1.5 29 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.182 <0.334 0.122 3.31 69.6 0.337 0.105 <0.329 NA <0.333 <0.335 0.331 Bis(2-ehtylhexyl) phthalate NS 38 160 ----<0.332 <1.65 <0.332 <1.66 <0.326 <0.332 <1.66 <0.332 <1.66 <66.1 <1.66 <0.331 <1.63 NA <1.65 <1.66 8.00 Chrysene 18 15 290 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.301 <0.334 0.282 6.81 136 0.567 0.177 <0.329 NA <0.333 0.487 0.517 Fluoranthene 330 460 6,000 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.707 0.355 0.593 14.8 331 1.18 0.354 0.535 NA <0.333 0.873 1.09 Fluorene 56 460 6,000 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 <0.0667 <0.334 <0.0668 0.672 35.1 <0.335 <0.0666 <0.329 NA <0.333 <0.335 <0.331 Indeno[1,2,3-cd]pyrene 3.5 0.15 2.9 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.142 <0.334 0.132 3.12 67.3 <0.335 0.0736 <0.329 NA <0.333 <0.335 <0.331 Naphthalene 0.21 3.8 17 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 <0.0667 <0.334 <0.0668 <0.334 15.7 <0.335 <0.0666 <0.329 NA <0.333 <0.335 <0.331 Phenanthrene 68 NS NS ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.392 <0.334 0.354 7.69 236 0.656 0.210 0.338 NA <0.333 0.529 0.760 Pyrene 220 340 4,600 ----<0.0669 <0.333 <0.0668 <0.333 <0.0656 0.626 <0.334 0.527 12.6 230 0.973 0.314 0.439 NA <0.333 0.733 0.902 HSL Metals** (6010B/7471A4) Arsenic 5.8 0.67 3.0 1.0 - 18 4.8 <2.33 <2.30 3.62 2.77 7.07 <2.42 40.3 3.25 3.63 8.93 2.79 3.61 3.72 NA 2.60 3.54 3.59 Chromium 360,000 24,000 100,000 7.0 - 300 65 15.7 13.6 19.7 12.0 20.5 18.2 17.2 27.8 38.7 26.6 19.0 22.9 34.7 NA 17.8 30.5 38.1 Copper 700 620 9,400 3 - 100 34 5.46 19.3 16.4 15.0 23.1 17.9 19.2 35.2 31.1 29.9 38.3 22.4 25.6 NA 35.6 21.3 20.6 Lead 270 400 800 ND - 50 16 13.0 27.3 33.5 51.7 25.2 7.09 26.3 89.0 29.9 64.4 69.9 143 59.3 NA 12.6 32.4 32.1 Manganese 65 360 5,200 <2.0 - 7,000*640 860 158 322 413 780 189 203 165 582 318 493 339 571 NA 323 875 336 Mercury 1.0 1.9 8.0 0.03 - 0.52 0.121 <0.116 <0.113 <0.129 <0.113 <0.125 <0.122 0.155 0.190 <0.120 0.338 0.167 <0.130 <0.112 NA <0.127 <0.113 <0.121 Nickel 130 300 4,400 ND - 150 23 2.43 6.71 6.71 11.2 11.2 8.06 7.46 8.41 14.5 13.1 8.09 8.01 8.00 NA 7.95 10.1 6.89 Zinc 1,200 4,600 70,000 25 - 124 56 <11.7 26.1 49.8 67.4 37.7 55.1 55.9 78.6 78.9 162 134 172 59.9 NA 71.0 104 95.4 Hexavalent Chromium (7196)3.8 0.3 6.3 ----<5.74 <5.85 <6.58 <5.52 <6.07 <6.01 <5.61 <6.19 <6.16 <5.76 <6.26 <6.40 <5.48 NA <6.31 <5.65 <5.95 pH (9045D)----------NA NA 11.5 NA NA NA NA NA NA NA NA NA NA 13.0 NA NA NA Notes:1) NC Department of Environment and Natural Resources (DENR) Inactive Hazardous Sites Branch (IHSB) Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs) - March 2015 2) DENR IHSB Preliminary Residential Soil Remediation Goal - March 20153) DENR IHSB Preliminary Industrial Soil Remediation Goal - March 20154) Mercury analyzed by EPA Method 7471A5)Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.* = Range and mean values of background metals for Southeastern USA soilsOnly those compounds detected in at least one sample shown above Gray font indicates a non-detect value Italic indicates an exceedance of the industrial PSRG values. Bold indicates an exceedance of the residential PSRG values. Underlined indicates an exceedance of the Protection of Groundwater PSRG values. ** = In the case of metals, concentrations in exceedance of PSRG values are only considered to be impacts if also above 2 times the background mean value. EPA Method number follows parameter in parenthesis VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds HSL = Hazardous Substance ListNS = screening criteria not specified; NA = not analyzed; -- = Not applicablemg/kg = milligrams per kilogram mg/kg TP-11TP-8 mg/kg mg/kg mg/kg TP-2 South of Philemon Ave TP-6Protection of Groundwater PSRGs 1 Residential PSRGs 2 Industrial PSRGs 3 Range Mean Screening Criteria Regional Background Metals in Soil 5 North of Philemon Ave TP-13 ATTACHMENT 3 TEST PIT LOGS GB Dry, soft, pale tan, SILT (~20% bricks and concrete rubble and ~80% soil) Slightly moist, soft, brown, silty CLAY (~5% bicks and concrete rubble and ~95% soil) Slightly moist, soft, dark grey, silty CLAY Alluvium without roots or woody debris Bottom of test pit at 2.5 feet. 2.4 2.5 0 0 DRAWN BY:DLS BORING COMPLETED:6/23/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgsFill depth 0 to 2.5 ft bgs BORING STARTED:6/23/15 LOGGED BY:DLS TOTAL DEPTH: 2.5 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-1 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0 1 2 3 0 1 2 3 GB GB Slightly moist, slightly stiff, brown and grey, silty CLAY(~40% coarse gravel, ~10% asphalt debris, ~50% soil) Staining beginning at 2 ft bgsPetroleum-like odor beginning at 3 ft bgs Slightly moist, loose to dense, white and tan, coarse sand.No stainning present Suspected lime material Saturated, loose to dense, white and tan, coarse sand. (~50% bricks, ~50% soil) Saturated, loose to dense, white and tan, coarse sand.(~35% concrete rubble, ~5% timbers, ~60% soil) Saturated, soft, dark grey, CLAYAlluvium with numerous roots and woody debris Bottom of test pit at 9.0 feet. 5 5.5 6.2 5.8 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/23/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Samples collected from 2 to 4 ft bgsand 4 to 6 ft bgsFill depth 0 to 9 ft bgs BORING STARTED:6/23/15 LOGGED BY:DLS TOTAL DEPTH: 9 ft. TOP OF CASING ELEV: DEPTH TO WATER: 5 ft. DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-2 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 0.0 2.5 5.0 7.5 10.0 GB Dry, soft, black and grey, sandy SILT(~60% concrete rubble, ~15% asphalt debris, ~25% soil) Dry, soft, black and grey, sandy SILT(~80% asphalt debris and asphalt gravel, ~20% soil) Saturated, soft, black, clayey SILT(~20% asphalt debris, ~80% soil) Saturated, soft, dark grey, silty CLAYAlluvium with numerous roots and woody debris Bottom of test pit at 10.5 feet. 3.5 7.4 2.1 1.1 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/23/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 4 to 6 ft bgsFill depth 0 to 10.5 ft bgs BORING STARTED:6/23/15 LOGGED BY:DLS TOTAL DEPTH: 10.5 ft. TOP OF CASING ELEV: DEPTH TO WATER: 6 ft. DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-3 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 0.0 2.5 5.0 7.5 10.0 GB Concrete Dry, soft, brown and grey, silty CLAY(~30% gravel, ~5% wood debris, ~65% soil) Moist, soft, dark grey, silty CLAYAlluvium with numerous roots and woody debris Bottom of test pit at 4.5 feet. 0 0.7 0.6 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/23/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgsFill depth 0 to 4.5 ft bgs BORING STARTED:6/23/15 LOGGED BY:DLS TOTAL DEPTH: 4.5 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-4 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0 1 2 3 4 5 6 0 1 2 3 4 5 6 GB Concrete Dry, soft, brown, SILT (~25% concrete rubble, ~25% rock, ~1% rebar, ~49% soil) Bottom of test pit at 4.0 feet. 2.4 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgsFill depth 0 to >4 ft bgs. Excavator wasunable to break through a layer of concrete BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 4 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-5 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0 1 2 3 4 5 0 1 2 3 4 5 GB GB Coarse gravel Dry, soft, orange brown, sandy SILT(~25% bricks, ~40% concrete rubble, ~5% asphalt, ~1% rebar, ~29% soil) Slightly moist, stiff, black and grey, silty CLAY(~7% wood, ~1% rock, ~1% concrete rubble, ~1% metal,~90% soil) Slightly moist, stiff, black and grey, silty CLAY(~7.5% rock, ~7.5% concrete rubble, ~5% rebar and metal, ~80% soil) Slightly moist, stiff, black and grey, silty CLAY(~12.5% concrete rubble, ~12.5% brick, ~5% rebar andmetal, ~3% wood, ~67% soil) Saturated, stiff, black and grey, silty CLAY(~12.5% concrete rubble, ~12.5% brick, ~5% rebar and metal, ~3% wood, ~67% soil) Slightly moist, soft, dark grey, silty CLAY Alluvium with numerous roots and woody debris Bottom of test pit at 14.0 feet. 4 0 1.7 0 0 0 0 0 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Samples collected from 0 to 2 ft bgs and 8 to 10 ft bgsFill depth 0 to 14 ft bgs BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 14 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-6 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 15.0 0.0 2.5 5.0 7.5 10.0 12.5 15.0 GB Coarse gravel Slightly moist, stiff, brown and grey, silty CLAY (~50% brick, ~15% concrete, ~35% soil) Slightly moist, stiff, dark grey, silty CLAY(~10% brick, ~1% rebar and metal, ~89% soil) Slightly moist, slightly soft, dark grey, silty CLAY(~40% brick, ~5% wood, ~55% soil) Saturated, soft, dark grey, silty CLAYAlluvium with numerous roots and woody debris Bottom of test pit at 11.5 feet. 0 0 0.2 0 0 2 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgsFill depth 0 to 11.5 ft bgs BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 11.5 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-7 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 0.0 2.5 5.0 7.5 10.0 12.5 Dry, soft, dark brown, clayey sandy SILT(~30% concrete rubble, ~20% brick, ~50% soil) Dry, soft, dark brown, clayey sandy SILT(~20% concrete rubble, ~5% brick, ~75% soil) Dry, soft, dark brown, clayey sandy SILT (~20% concrete rubble, ~5% brick, ~1% rebar and metal,~74% soil) Slightly moist, soft, dark brown, clayey sandy SILT(~30% concrete rubble, ~1% rebar and metal, ~69% soil) Slightly moist, soft, dark brown, clayey sandy SILT(~30% concrete rubble, ~5% wood, ~1% rebar and metal, ~64% soil) Moist, soft, dark brown, clayey sandy SILT (~30% concrete rubble, ~5% wood, ~1% rebar and metal,~64% soil) Saturated, soft, dark grey, CLAYAlluvium with numerous roots and woody debris Bottom of test pit at 12.0 feet. 0.5 0.4 1.4 0.9 2.5 1.4 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgs and8 to 10 ft bgsFill depth 0 to 12 ft bgs BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 12 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-8 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 0.0 2.5 5.0 7.5 10.0 12.5 GB Concrete Slightly moist, slightly stiff, dark orange brown, silty CLAY (~10% gravel, ~2% rebar and metal, ~1% wood, ~87% soil) Slightly moist, slightly stiff, dark brown and black, silty CLAY (~20% brick, ~15% concrete rubble, ~1% wood, ~64% soil) Slightly moist, slightly stiff, dark brown and black, siltyCLAY (~10% wood, ~5% brick, ~1% plastic, ~84% soil) Saturated, soft, dark grey, CLAYAlluvium with numerous roots and woody debris Bottom of test pit at 11.5 feet. 0.2 0 0 1.5 0 0 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 8 to 10 ft bgsFill depth 0 to 11.5 ft bgs BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 11.5 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-9 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 0.0 2.5 5.0 7.5 10.0 12.5 Concrete Slightly moist, soft, orange brown, clayey sandy SILT. (~50% concrete rubble, ~1% metal, ~49% soil) Slightly moist, soft, brown, silty CLAY(~40% concrete rubble, ~60% soil) Moist, soft, brown, silty CLAY (~15% concrete rubble, ~10% asphalt debris, ~75% soil) Saturated, soft, dark grey, silty CLAY Alluvium with numerous roots and woody debris Bottom of test pit at 12.0 feet. 1 0 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab No sample collectedFill depth 0 to 12 ft bgs BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 12 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-10 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 0.0 2.5 5.0 7.5 10.0 12.5 GB GB Concrete Slightly moist, soft, red brown, silty CLAY(~25% concrete rubble, ~10% bricks, ~65% soil) Weak concrete Moist, very hard, white, silty SAND Suspected lime material Saturated, soft, dark grey, silty CLAY Alluvium with numerous roots and woody debris Bottom of test pit at 13.0 feet. 3.2 0 0 0 0 0 0 0 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/22/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgs and6 to 13 ft bgs (pH only)Fill depth 0 to 13 ft bgs BORING STARTED:6/22/15 LOGGED BY:DLS TOTAL DEPTH: 13 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-11 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 0.0 2.5 5.0 7.5 10.0 12.5 GB Slightly moist, soft, dark brown, silty CLAY(~25% rocky debris, ~75% organic rich top soil) Slightly moist, soft, dark brown, silty CLAY(~15% wood, ~10% concrete, ~75% soil) Saturated, soft, dark grey, silty CLAY Alluvium with numerous roots and woody debris Bottom of test pit at 8.0 feet. 0.9 1.1 0.6 0 0.8 1 0.7 0 DRAWN BY:DLS BORING COMPLETED:6/23/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Sample collected from 0 to 2 ft bgsFill depth 0 to 8 ft bgs BORING STARTED:6/23/15 LOGGED BY:DLS TOTAL DEPTH: 8 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-12 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 0.0 2.5 5.0 7.5 GB GB Slightly moist, slightly soft, orange brown, CLAY(~75% bricks, ~25% soil) Slightly moist, slightly soft, orange brown, CLAY (~40% bricks, ~30% concrete, ~5% metal, ~25% soil) Slightly moist, slightly soft, orange brown, CLAY(~50% concrete rubble, ~20% bricks and clay tiles, ~5%metal, ~25% soil) Saturated, soft, dark grey, silty CLAY Alluvium with numerous roots and woody debris Bottom of test pit at 11.0 feet. 13.1 5.8 1.2 0 0 0 0 0 0 0 0 0 DRAWN BY:DLS BORING COMPLETED:6/23/15 DRILLING CONTRACTOR:EVO Remarks: DRILL RIG/ METHOD:John Deere 230C / Excavation SAMPLING METHOD:Grab Samples collected from 0 to 2 ft bgsand 10 to 11 ft bgsFill depth 0 to 11 ft bgs BORING STARTED:6/23/15 LOGGED BY:DLS TOTAL DEPTH: 11 ft. TOP OF CASING ELEV: DEPTH TO WATER: DE P T H (f t ) DE P T H (f t ) RE C O V E R Y ( % ) SA M P L E T Y P E NU M B E R MATERIAL DESCRIPTION LI T H O L O G Y SA M P . BK G . BL O W CO U N T S (N V A L U E ) WELL DIAGRAM OV A ( p p m ) Sheet 1 of 1 TEST PIT NUMBER TP-13 PROJECT:NODA Greenway JOB NUMBER:CRE-001 LOCATION:Charlotte, North Carolina WE L L L O G - H A R T H I C K M A N . G D T - 6 / 2 5 / 1 5 1 1 : 1 2 - S : \ A A A - M A S T E R G I N T P R O J E C T S \ C R E - 0 0 1 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 7.5 10.0 12.5 0.0 2.5 5.0 7.5 10.0 12.5 ATTACHMENT 4 LABORATORY ANALYTICAL REPORTS ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-81218-1 TestAmerica Sample Delivery Group: CRE-001 Client Project/Site: NODA Greenway/Charlotte, NC For: Hart & Hickman, PC 2923 S Tryon Street Suite 100 Charlotte, North Carolina 28203 Attn: Brett Lawrence Authorized for release by: 7/2/2015 9:26:55 AM Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 12 13 Table of Contents Client: Hart & Hickman, PC Project/Site: NODA Greenway/Charlotte, NC TestAmerica Job ID: 490-81218-1 SDG: CRE-001 Page 2 of 50 TestAmerica Nashville7/2/2015 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50 1 2 3 4 5 6 7 8 9 10 11 12 13 Sample Summary TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID Client Sample ID ReceivedCollectedMatrix 490-81218-1 TP-1 (0-2)Soil 06/23/15 11:40 06/24/15 08:30 490-81218-2 TP-2 (2-4)Soil 06/23/15 12:15 06/24/15 08:30 490-81218-3 TP-2 (4-6)Soil 06/23/15 12:20 06/24/15 08:30 490-81218-4 TP-3 (4-6)Soil 06/23/15 12:50 06/24/15 08:30 490-81218-5 TP-4 (0-2)Soil 06/23/15 13:10 06/24/15 08:30 TestAmerica Nashville Page 3 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Case Narrative Client: Hart & Hickman, PC TestAmerica Job ID: 490-81218-1 Project/Site: NODA Greenway/Charlotte, NC SDG: CRE-001 Job ID: 490-81218-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-81218-1 Comments No additional comments. Receipt The samples were received on 6/24/2015 8:30 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 3.4º C. GC/MS VOA Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with analytical batch 490-259533. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC/MS Semi VOA Method(s) 8270D: Surrogate recovery for the following sample was outside control limits: TP-2 (4-6) (490-81218-3). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. Method(s) 8270D: The following samples were diluted due to the nature of the sample matrix: TP-2 (2-4) (490-81218-2) and TP-3 (4-6) (490-81218-4). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. General Chemistry Method(s) 7196A: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch 490-260615 recovered outside control limits for the following analytes: Hexavalent Chromium. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica NashvillePage 4 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Definitions/Glossary TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Qualifiers GC/MS Semi VOA Qualifier Description X Surrogate is outside control limits Qualifier Metals Qualifier Description F1 MS and/or MSD Recovery is outside acceptance limits. Qualifier General Chemistry Qualifier Description *RPD of the LCS and LCSD exceeds the control limits Qualifier F1 MS and/or MSD Recovery is outside acceptance limits. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 5 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-1Client Sample ID: TP-1 (0-2) Matrix: SoilDate Collected: 06/23/15 11:40 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 84 0.10 %06/24/15 14:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 6 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-1Client Sample ID: TP-1 (0-2) Matrix: SoilDate Collected: 06/23/15 11:40 Percent Solids: 83.6Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.152 0.0483 mg/Kg ☼06/23/15 11:40 06/26/15 02:05 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Benzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Bromobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Bromochloromethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Bromodichloromethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Bromoform ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Bromomethane ND 0.0483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼2-Butanone (MEK)ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Carbon disulfide ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Carbon tetrachloride ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Chlorobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Chlorodibromomethane ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Chloroethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Chloroform ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Chloromethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼2-Chlorotoluene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼4-Chlorotoluene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼cis-1,2-Dichloroethene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼cis-1,3-Dichloropropene ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2-Dibromo-3-Chloropropane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2-Dibromoethane (EDB)ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Dibromomethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2-Dichlorobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,3-Dichlorobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,4-Dichlorobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Dichlorodifluoromethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,1-Dichloroethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2-Dichloroethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,1-Dichloroethene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2-Dichloroethene, Total ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2-Dichloropropane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,3-Dichloropropane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼2,2-Dichloropropane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,1-Dichloropropene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Diisopropyl ether ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Ethylbenzene ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Hexachlorobutadiene ND 0.0483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼2-Hexanone ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Isopropylbenzene ND 0.00966 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Methylene Chloride ND 0.0483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼4-Methyl-2-pentanone (MIBK)ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Methyl tert-butyl ether ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Naphthalene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼n-Butylbenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼N-Propylbenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼p-Isopropyltoluene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼sec-Butylbenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Styrene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼tert-Butylbenzene ND TestAmerica Nashville Page 7 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-1Client Sample ID: TP-1 (0-2) Matrix: SoilDate Collected: 06/23/15 11:40 Percent Solids: 83.6Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00193 mg/Kg ☼06/23/15 11:40 06/26/15 02:05 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,1,2,2-Tetrachloroethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Tetrachloroethene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Toluene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼trans-1,2-Dichloroethene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼trans-1,3-Dichloropropene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2,3-Trichlorobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2,4-Trichlorobenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,1,1-Trichloroethane ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,1,2-Trichloroethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Trichloroethene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Trichlorofluoromethane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2,3-Trichloropropane ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,2,4-Trimethylbenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼1,3,5-Trimethylbenzene ND 0.00193 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Vinyl chloride ND 0.00483 mg/Kg 06/23/15 11:40 06/26/15 02:05 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)96 70-130 06/23/15 11:40 06/26/15 02:05 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)99 06/23/15 11:40 06/26/15 02:05 170-130 1,2-Dichloroethane-d4 (Surr)103 06/23/15 11:40 06/26/15 02:05 170-130 Toluene-d8 (Surr)99 06/23/15 11:40 06/26/15 02:05 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0669 mg/Kg ☼06/26/15 09:17 06/28/15 16:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Acenaphthylene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Anthracene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Benzo[a]anthracene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Benzo[a]pyrene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Benzo[b]fluoranthene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Benzo[g,h,i]perylene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Benzo[k]fluoranthene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Bis(2-chloroethoxy)methane ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Bis(2-chloroethyl)ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼bis (2-chloroisopropyl) ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Bis(2-ethylhexyl) phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4-Bromophenyl phenyl ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Butyl benzyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Carbazole ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4-Chloroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4-Chloro-3-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2-Chloronaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2-Chlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4-Chlorophenyl phenyl ether ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Chrysene ND 0.665 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Cresols ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Dibenz(a,h)anthracene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Dibenzofuran ND TestAmerica Nashville Page 8 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-1Client Sample ID: TP-1 (0-2) Matrix: SoilDate Collected: 06/23/15 11:40 Percent Solids: 83.6Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 0.332 mg/Kg ☼06/26/15 09:17 06/28/15 16:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼1,3-Dichlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼1,4-Dichlorobenzene ND 0.666 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼3,3'-Dichlorobenzidine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,4-Dichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Diethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,4-Dimethylphenol ND 1.67 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Dimethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Di-n-butyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4,6-Dinitro-2-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,4-Dinitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,4-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,6-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Di-n-octyl phthalate ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Fluoranthene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Fluorene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Hexachlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Hexachlorobutadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Hexachlorocyclopentadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Hexachloroethane ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Indeno[1,2,3-cd]pyrene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Isophorone ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼1-Methylnaphthalene ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2-Methylnaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2-Methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼3 & 4 Methylphenol ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Naphthalene ND 0.832 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2-Nitroaniline ND 0.832 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼3-Nitroaniline ND 0.832 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4-Nitroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Nitrobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼4-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼N-Nitrosodi-n-propylamine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.832 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Pentachlorophenol ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Phenanthrene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Phenol ND 0.0669 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼Pyrene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼1,2,4-Trichlorobenzene ND 0.832 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,4,5-Trichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:09 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)76 29-120 06/26/15 09:17 06/28/15 16:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)79 06/26/15 09:17 06/28/15 16:09 110-120 Nitrobenzene-d5 (Surr)72 06/26/15 09:17 06/28/15 16:09 127-120 Phenol-d5 (Surr)82 06/26/15 09:17 06/28/15 16:09 110-120 Terphenyl-d14 (Surr)87 06/26/15 09:17 06/28/15 16:09 113-120 TestAmerica Nashville Page 9 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-1Client Sample ID: TP-1 (0-2) Matrix: SoilDate Collected: 06/23/15 11:40 Percent Solids: 83.6Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)77 10-120 06/26/15 09:17 06/28/15 16:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.7 mg/Kg ☼06/25/15 08:59 06/25/15 16:22 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.33 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Arsenic ND 1.17 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Beryllium ND 1.17 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Cadmium ND 1.17 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Chromium 15.7 2.33 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Copper 5.46 1.17 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Lead 13.0 3.50 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Manganese 860 2.33 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Nickel 2.43 2.33 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Selenium ND 1.17 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Silver ND 2.33 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Thallium ND 11.7 mg/Kg 06/25/15 08:59 06/25/15 16:22 1☼Zinc ND Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.116 mg/Kg ☼06/24/15 16:44 06/26/15 00:10 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND * F1 5.74 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 10 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-2Client Sample ID: TP-2 (2-4) Matrix: SoilDate Collected: 06/23/15 12:15 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 85 0.10 %06/24/15 14:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 11 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-2Client Sample ID: TP-2 (2-4) Matrix: SoilDate Collected: 06/23/15 12:15 Percent Solids: 85.1Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.0666 0.0488 mg/Kg ☼06/23/15 12:15 06/26/15 02:36 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Benzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Bromobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Bromochloromethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Bromodichloromethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Bromoform ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Bromomethane ND 0.0488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼2-Butanone (MEK)ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Carbon disulfide ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Carbon tetrachloride ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Chlorobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Chlorodibromomethane ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Chloroethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Chloroform ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Chloromethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼2-Chlorotoluene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼4-Chlorotoluene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼cis-1,2-Dichloroethene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼cis-1,3-Dichloropropene ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2-Dibromo-3-Chloropropane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2-Dibromoethane (EDB)ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Dibromomethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2-Dichlorobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,3-Dichlorobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,4-Dichlorobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Dichlorodifluoromethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,1-Dichloroethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2-Dichloroethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,1-Dichloroethene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2-Dichloroethene, Total ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2-Dichloropropane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,3-Dichloropropane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼2,2-Dichloropropane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,1-Dichloropropene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Diisopropyl ether ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Ethylbenzene ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Hexachlorobutadiene ND 0.0488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼2-Hexanone ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Isopropylbenzene ND 0.00977 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Methylene Chloride ND 0.0488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼4-Methyl-2-pentanone (MIBK)ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Methyl tert-butyl ether ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Naphthalene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼n-Butylbenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼N-Propylbenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼p-Isopropyltoluene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼sec-Butylbenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Styrene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼tert-Butylbenzene ND TestAmerica Nashville Page 12 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-2Client Sample ID: TP-2 (2-4) Matrix: SoilDate Collected: 06/23/15 12:15 Percent Solids: 85.1Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00195 mg/Kg ☼06/23/15 12:15 06/26/15 02:36 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,1,2,2-Tetrachloroethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Tetrachloroethene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Toluene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼trans-1,2-Dichloroethene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼trans-1,3-Dichloropropene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2,3-Trichlorobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2,4-Trichlorobenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,1,1-Trichloroethane ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,1,2-Trichloroethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Trichloroethene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Trichlorofluoromethane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2,3-Trichloropropane ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,2,4-Trimethylbenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼1,3,5-Trimethylbenzene ND 0.00195 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Vinyl chloride ND 0.00488 mg/Kg 06/23/15 12:15 06/26/15 02:36 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)104 70-130 06/23/15 12:15 06/26/15 02:36 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 06/23/15 12:15 06/26/15 02:36 170-130 1,2-Dichloroethane-d4 (Surr)106 06/23/15 12:15 06/26/15 02:36 170-130 Toluene-d8 (Surr)107 06/23/15 12:15 06/26/15 02:36 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.333 mg/Kg ☼06/26/15 09:17 06/28/15 16:32 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Acenaphthylene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Benzo[a]anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Benzo[a]pyrene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Benzo[b]fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Benzo[g,h,i]perylene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Benzo[k]fluoranthene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Bis(2-chloroethoxy)methane ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Bis(2-chloroethyl)ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼bis (2-chloroisopropyl) ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Bis(2-ethylhexyl) phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4-Bromophenyl phenyl ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Butyl benzyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Carbazole ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4-Chloroaniline ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4-Chloro-3-methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2-Chloronaphthalene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2-Chlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4-Chlorophenyl phenyl ether ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Chrysene ND 3.31 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Cresols ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Dibenz(a,h)anthracene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Dibenzofuran ND TestAmerica Nashville Page 13 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-2Client Sample ID: TP-2 (2-4) Matrix: SoilDate Collected: 06/23/15 12:15 Percent Solids: 85.1Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.65 mg/Kg ☼06/26/15 09:17 06/28/15 16:32 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼1,3-Dichlorobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼1,4-Dichlorobenzene ND 3.31 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼3,3'-Dichlorobenzidine ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,4-Dichlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Diethyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,4-Dimethylphenol ND 8.29 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Dimethyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Di-n-butyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4,6-Dinitro-2-methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,4-Dinitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,4-Dinitrotoluene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,6-Dinitrotoluene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Di-n-octyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Fluorene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Hexachlorobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Hexachlorobutadiene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Hexachlorocyclopentadiene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Hexachloroethane ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Indeno[1,2,3-cd]pyrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Isophorone ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼1-Methylnaphthalene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2-Methylnaphthalene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2-Methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼3 & 4 Methylphenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Naphthalene ND 4.13 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2-Nitroaniline ND 4.13 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼3-Nitroaniline ND 4.13 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4-Nitroaniline ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Nitrobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2-Nitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼4-Nitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼N-Nitrosodi-n-propylamine ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.13 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Pentachlorophenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Phenanthrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Phenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼Pyrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼1,2,4-Trichlorobenzene ND 4.13 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,4,5-Trichlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 16:32 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)82 29-120 06/26/15 09:17 06/28/15 16:32 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)82 06/26/15 09:17 06/28/15 16:32 510-120 Nitrobenzene-d5 (Surr)72 06/26/15 09:17 06/28/15 16:32 527-120 Phenol-d5 (Surr)86 06/26/15 09:17 06/28/15 16:32 510-120 Terphenyl-d14 (Surr)94 06/26/15 09:17 06/28/15 16:32 513-120 TestAmerica Nashville Page 14 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-2Client Sample ID: TP-2 (2-4) Matrix: SoilDate Collected: 06/23/15 12:15 Percent Solids: 85.1Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)89 10-120 06/26/15 09:17 06/28/15 16:32 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.5 mg/Kg ☼06/25/15 08:59 06/25/15 16:26 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.30 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Arsenic ND 1.15 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Beryllium ND 1.15 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Cadmium ND 1.15 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Chromium 13.6 2.30 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Copper 19.3 1.15 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Lead 27.3 3.45 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Manganese 158 2.30 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Nickel 6.71 2.30 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Selenium ND 1.15 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Silver ND 2.30 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Thallium ND 11.5 mg/Kg 06/25/15 08:59 06/25/15 16:26 1☼Zinc 26.1 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.113 mg/Kg ☼06/24/15 16:44 06/26/15 00:13 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.85 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 15 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-3Client Sample ID: TP-2 (4-6) Matrix: SoilDate Collected: 06/23/15 12:20 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 75 0.10 %06/24/15 14:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry - Soluble RL RL pH 11.5 0.100 SU 06/27/15 10:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.100 Degrees C 06/27/15 10:08 1Temperature21.7 TestAmerica Nashville Page 16 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-3Client Sample ID: TP-2 (4-6) Matrix: SoilDate Collected: 06/23/15 12:20 Percent Solids: 74.8Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.0801 0.0773 mg/Kg ☼06/23/15 12:20 06/26/15 03:07 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Benzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Bromobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Bromochloromethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Bromodichloromethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Bromoform ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Bromomethane ND 0.0773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼2-Butanone (MEK)ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Carbon disulfide ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Carbon tetrachloride ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Chlorobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Chlorodibromomethane ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Chloroethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Chloroform ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Chloromethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼2-Chlorotoluene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼4-Chlorotoluene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼cis-1,2-Dichloroethene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼cis-1,3-Dichloropropene ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2-Dibromo-3-Chloropropane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2-Dibromoethane (EDB)ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Dibromomethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2-Dichlorobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,3-Dichlorobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,4-Dichlorobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Dichlorodifluoromethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,1-Dichloroethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2-Dichloroethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,1-Dichloroethene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2-Dichloroethene, Total ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2-Dichloropropane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,3-Dichloropropane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼2,2-Dichloropropane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,1-Dichloropropene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Diisopropyl ether ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Ethylbenzene ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Hexachlorobutadiene ND 0.0773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼2-Hexanone ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Isopropylbenzene ND 0.0155 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Methylene Chloride ND 0.0773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼4-Methyl-2-pentanone (MIBK)ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Methyl tert-butyl ether ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Naphthalene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼n-Butylbenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼N-Propylbenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼p-Isopropyltoluene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼sec-Butylbenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Styrene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼tert-Butylbenzene ND TestAmerica Nashville Page 17 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-3Client Sample ID: TP-2 (4-6) Matrix: SoilDate Collected: 06/23/15 12:20 Percent Solids: 74.8Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00309 mg/Kg ☼06/23/15 12:20 06/26/15 03:07 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,1,2,2-Tetrachloroethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Tetrachloroethene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Toluene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼trans-1,2-Dichloroethene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼trans-1,3-Dichloropropene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2,3-Trichlorobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2,4-Trichlorobenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,1,1-Trichloroethane ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,1,2-Trichloroethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Trichloroethene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Trichlorofluoromethane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2,3-Trichloropropane ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,2,4-Trimethylbenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼1,3,5-Trimethylbenzene ND 0.00309 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Vinyl chloride ND 0.00773 mg/Kg 06/23/15 12:20 06/26/15 03:07 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)101 70-130 06/23/15 12:20 06/26/15 03:07 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)103 06/23/15 12:20 06/26/15 03:07 170-130 1,2-Dichloroethane-d4 (Surr)102 06/23/15 12:20 06/26/15 03:07 170-130 Toluene-d8 (Surr)107 06/23/15 12:20 06/26/15 03:07 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0668 mg/Kg ☼06/26/15 09:17 06/28/15 16:56 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Acenaphthylene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Anthracene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Benzo[a]anthracene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Benzo[a]pyrene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Benzo[b]fluoranthene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Benzo[g,h,i]perylene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Benzo[k]fluoranthene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Bis(2-chloroethoxy)methane ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Bis(2-chloroethyl)ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼bis (2-chloroisopropyl) ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Bis(2-ethylhexyl) phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4-Bromophenyl phenyl ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Butyl benzyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Carbazole ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4-Chloroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4-Chloro-3-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2-Chloronaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2-Chlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4-Chlorophenyl phenyl ether ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Chrysene ND 0.664 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Cresols ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Dibenz(a,h)anthracene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Dibenzofuran ND TestAmerica Nashville Page 18 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-3Client Sample ID: TP-2 (4-6) Matrix: SoilDate Collected: 06/23/15 12:20 Percent Solids: 74.8Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 0.332 mg/Kg ☼06/26/15 09:17 06/28/15 16:56 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼1,3-Dichlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼1,4-Dichlorobenzene ND 0.665 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼3,3'-Dichlorobenzidine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,4-Dichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Diethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,4-Dimethylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Dimethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Di-n-butyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4,6-Dinitro-2-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,4-Dinitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,4-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,6-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Di-n-octyl phthalate ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Fluoranthene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Fluorene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Hexachlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Hexachlorobutadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Hexachlorocyclopentadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Hexachloroethane ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Indeno[1,2,3-cd]pyrene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Isophorone ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼1-Methylnaphthalene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2-Methylnaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2-Methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼3 & 4 Methylphenol ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Naphthalene ND 0.830 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2-Nitroaniline ND 0.830 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼3-Nitroaniline ND 0.830 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4-Nitroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Nitrobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼4-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼N-Nitrosodi-n-propylamine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.830 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Pentachlorophenol ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Phenanthrene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Phenol ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼Pyrene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼1,2,4-Trichlorobenzene ND 0.830 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,4,5-Trichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 16:56 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)77 29-120 06/26/15 09:17 06/28/15 16:56 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)1 X 06/26/15 09:17 06/28/15 16:56 110-120 Nitrobenzene-d5 (Surr)71 06/26/15 09:17 06/28/15 16:56 127-120 Phenol-d5 (Surr)8 X 06/26/15 09:17 06/28/15 16:56 110-120 Terphenyl-d14 (Surr)90 06/26/15 09:17 06/28/15 16:56 113-120 TestAmerica Nashville Page 19 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-3Client Sample ID: TP-2 (4-6) Matrix: SoilDate Collected: 06/23/15 12:20 Percent Solids: 74.8Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)5 X 10-120 06/26/15 09:17 06/28/15 16:56 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 13.3 mg/Kg ☼06/25/15 08:59 06/25/15 16:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.66 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Arsenic 3.62 1.33 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Beryllium ND 1.33 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Cadmium ND 1.33 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Chromium 19.7 2.66 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Copper 16.4 1.33 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Lead 33.5 4.00 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Manganese 322 2.66 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Nickel 6.71 2.66 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Selenium ND 1.33 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Silver ND 2.66 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Thallium ND 13.3 mg/Kg 06/25/15 08:59 06/25/15 16:39 1☼Zinc 49.8 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.129 mg/Kg ☼06/24/15 16:44 06/26/15 00:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.58 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 20 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-4Client Sample ID: TP-3 (4-6) Matrix: SoilDate Collected: 06/23/15 12:50 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 89 0.10 %06/24/15 14:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 21 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-4Client Sample ID: TP-3 (4-6) Matrix: SoilDate Collected: 06/23/15 12:50 Percent Solids: 88.6Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0417 mg/Kg ☼06/23/15 12:50 06/26/15 03:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Benzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Bromobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Bromochloromethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Bromodichloromethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Bromoform ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Bromomethane ND 0.0417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼2-Butanone (MEK)ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Carbon disulfide ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Carbon tetrachloride ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Chlorobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Chlorodibromomethane ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Chloroethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Chloroform ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Chloromethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼2-Chlorotoluene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼4-Chlorotoluene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼cis-1,2-Dichloroethene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼cis-1,3-Dichloropropene ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2-Dibromo-3-Chloropropane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2-Dibromoethane (EDB)ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Dibromomethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2-Dichlorobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,3-Dichlorobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,4-Dichlorobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Dichlorodifluoromethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,1-Dichloroethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2-Dichloroethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,1-Dichloroethene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2-Dichloroethene, Total ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2-Dichloropropane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,3-Dichloropropane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼2,2-Dichloropropane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,1-Dichloropropene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Diisopropyl ether ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Ethylbenzene ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Hexachlorobutadiene ND 0.0417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼2-Hexanone ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Isopropylbenzene ND 0.00835 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Methylene Chloride ND 0.0417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼4-Methyl-2-pentanone (MIBK)ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Methyl tert-butyl ether ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Naphthalene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼n-Butylbenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼N-Propylbenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼p-Isopropyltoluene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼sec-Butylbenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Styrene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼tert-Butylbenzene ND TestAmerica Nashville Page 22 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-4Client Sample ID: TP-3 (4-6) Matrix: SoilDate Collected: 06/23/15 12:50 Percent Solids: 88.6Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00167 mg/Kg ☼06/23/15 12:50 06/26/15 03:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,1,2,2-Tetrachloroethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Tetrachloroethene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Toluene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼trans-1,2-Dichloroethene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼trans-1,3-Dichloropropene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2,3-Trichlorobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2,4-Trichlorobenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,1,1-Trichloroethane ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,1,2-Trichloroethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Trichloroethene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Trichlorofluoromethane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2,3-Trichloropropane ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,2,4-Trimethylbenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼1,3,5-Trimethylbenzene ND 0.00167 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Vinyl chloride ND 0.00417 mg/Kg 06/23/15 12:50 06/26/15 03:37 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)100 70-130 06/23/15 12:50 06/26/15 03:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 06/23/15 12:50 06/26/15 03:37 170-130 1,2-Dichloroethane-d4 (Surr)107 06/23/15 12:50 06/26/15 03:37 170-130 Toluene-d8 (Surr)104 06/23/15 12:50 06/26/15 03:37 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.333 mg/Kg ☼06/26/15 09:17 06/28/15 17:20 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Acenaphthylene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Benzo[a]anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Benzo[a]pyrene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Benzo[b]fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Benzo[g,h,i]perylene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Benzo[k]fluoranthene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Bis(2-chloroethoxy)methane ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Bis(2-chloroethyl)ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼bis (2-chloroisopropyl) ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Bis(2-ethylhexyl) phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4-Bromophenyl phenyl ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Butyl benzyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Carbazole ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4-Chloroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4-Chloro-3-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2-Chloronaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2-Chlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4-Chlorophenyl phenyl ether ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Chrysene ND 3.31 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Cresols ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Dibenz(a,h)anthracene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Dibenzofuran ND TestAmerica Nashville Page 23 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-4Client Sample ID: TP-3 (4-6) Matrix: SoilDate Collected: 06/23/15 12:50 Percent Solids: 88.6Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.66 mg/Kg ☼06/26/15 09:17 06/28/15 17:20 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼1,3-Dichlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼1,4-Dichlorobenzene ND 3.32 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼3,3'-Dichlorobenzidine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,4-Dichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Diethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,4-Dimethylphenol ND 8.31 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Dimethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Di-n-butyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4,6-Dinitro-2-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,4-Dinitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,4-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,6-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Di-n-octyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Fluorene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Hexachlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Hexachlorobutadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Hexachlorocyclopentadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Hexachloroethane ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Indeno[1,2,3-cd]pyrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Isophorone ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼1-Methylnaphthalene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2-Methylnaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2-Methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼3 & 4 Methylphenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Naphthalene ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2-Nitroaniline ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼3-Nitroaniline ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4-Nitroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Nitrobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼4-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼N-Nitrosodi-n-propylamine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Pentachlorophenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Phenanthrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Phenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼Pyrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼1,2,4-Trichlorobenzene ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,4,5-Trichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 17:20 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)65 29-120 06/26/15 09:17 06/28/15 17:20 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)69 06/26/15 09:17 06/28/15 17:20 510-120 Nitrobenzene-d5 (Surr)61 06/26/15 09:17 06/28/15 17:20 527-120 Phenol-d5 (Surr)67 06/26/15 09:17 06/28/15 17:20 510-120 Terphenyl-d14 (Surr)78 06/26/15 09:17 06/28/15 17:20 513-120 TestAmerica Nashville Page 24 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-4Client Sample ID: TP-3 (4-6) Matrix: SoilDate Collected: 06/23/15 12:50 Percent Solids: 88.6Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)80 10-120 06/26/15 09:17 06/28/15 17:20 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.1 mg/Kg ☼06/25/15 08:59 06/25/15 16:44 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.21 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Arsenic 2.77 1.11 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Beryllium ND 1.11 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Cadmium ND 1.11 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Chromium 12.0 2.21 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Copper 15.0 1.11 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Lead 51.7 3.32 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Manganese 413 2.21 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Nickel 11.2 2.21 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Selenium ND 1.11 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Silver ND 2.21 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Thallium ND 11.1 mg/Kg 06/25/15 08:59 06/25/15 16:44 1☼Zinc 67.4 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.113 mg/Kg ☼06/24/15 16:44 06/26/15 00:17 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.52 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 25 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-5Client Sample ID: TP-4 (0-2) Matrix: SoilDate Collected: 06/23/15 13:10 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 81 0.10 %06/24/15 14:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 26 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-5Client Sample ID: TP-4 (0-2) Matrix: SoilDate Collected: 06/23/15 13:10 Percent Solids: 80.8Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0428 mg/Kg ☼06/23/15 13:10 06/26/15 04:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Benzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Bromobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Bromochloromethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Bromodichloromethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Bromoform ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Bromomethane ND 0.0428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼2-Butanone (MEK)ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Carbon disulfide 0.00788 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Carbon tetrachloride ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Chlorobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Chlorodibromomethane ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Chloroethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Chloroform ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Chloromethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼2-Chlorotoluene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼4-Chlorotoluene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼cis-1,2-Dichloroethene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼cis-1,3-Dichloropropene ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2-Dibromo-3-Chloropropane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2-Dibromoethane (EDB)ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Dibromomethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2-Dichlorobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,3-Dichlorobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,4-Dichlorobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Dichlorodifluoromethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,1-Dichloroethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2-Dichloroethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,1-Dichloroethene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2-Dichloroethene, Total ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2-Dichloropropane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,3-Dichloropropane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼2,2-Dichloropropane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,1-Dichloropropene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Diisopropyl ether ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Ethylbenzene ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Hexachlorobutadiene ND 0.0428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼2-Hexanone ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Isopropylbenzene ND 0.00856 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Methylene Chloride ND 0.0428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼4-Methyl-2-pentanone (MIBK)ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Methyl tert-butyl ether ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Naphthalene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼n-Butylbenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼N-Propylbenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼p-Isopropyltoluene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼sec-Butylbenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Styrene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼tert-Butylbenzene ND TestAmerica Nashville Page 27 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-5Client Sample ID: TP-4 (0-2) Matrix: SoilDate Collected: 06/23/15 13:10 Percent Solids: 80.8Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00171 mg/Kg ☼06/23/15 13:10 06/26/15 04:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,1,2,2-Tetrachloroethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Tetrachloroethene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Toluene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼trans-1,2-Dichloroethene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼trans-1,3-Dichloropropene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2,3-Trichlorobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2,4-Trichlorobenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,1,1-Trichloroethane ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,1,2-Trichloroethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Trichloroethene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Trichlorofluoromethane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2,3-Trichloropropane ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,2,4-Trimethylbenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼1,3,5-Trimethylbenzene ND 0.00171 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Vinyl chloride ND 0.00428 mg/Kg 06/23/15 13:10 06/26/15 04:08 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)95 70-130 06/23/15 13:10 06/26/15 04:08 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)104 06/23/15 13:10 06/26/15 04:08 170-130 1,2-Dichloroethane-d4 (Surr)112 06/23/15 13:10 06/26/15 04:08 170-130 Toluene-d8 (Surr)100 06/23/15 13:10 06/26/15 04:08 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0656 mg/Kg ☼06/26/15 09:17 06/28/15 17:44 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Acenaphthylene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Anthracene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Benzo[a]anthracene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Benzo[a]pyrene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Benzo[b]fluoranthene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Benzo[g,h,i]perylene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Benzo[k]fluoranthene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Bis(2-chloroethoxy)methane ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Bis(2-chloroethyl)ether ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼bis (2-chloroisopropyl) ether ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Bis(2-ethylhexyl) phthalate ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4-Bromophenyl phenyl ether ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Butyl benzyl phthalate ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Carbazole ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4-Chloroaniline ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4-Chloro-3-methylphenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2-Chloronaphthalene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2-Chlorophenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4-Chlorophenyl phenyl ether ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Chrysene ND 0.652 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Cresols ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Dibenz(a,h)anthracene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Dibenzofuran ND TestAmerica Nashville Page 28 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-5Client Sample ID: TP-4 (0-2) Matrix: SoilDate Collected: 06/23/15 13:10 Percent Solids: 80.8Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 0.326 mg/Kg ☼06/26/15 09:17 06/28/15 17:44 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼1,3-Dichlorobenzene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼1,4-Dichlorobenzene ND 0.653 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼3,3'-Dichlorobenzidine ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,4-Dichlorophenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Diethyl phthalate ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,4-Dimethylphenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Dimethyl phthalate ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Di-n-butyl phthalate ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4,6-Dinitro-2-methylphenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,4-Dinitrophenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,4-Dinitrotoluene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,6-Dinitrotoluene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Di-n-octyl phthalate ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Fluoranthene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Fluorene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Hexachlorobenzene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Hexachlorobutadiene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Hexachlorocyclopentadiene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Hexachloroethane ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Indeno[1,2,3-cd]pyrene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Isophorone ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼1-Methylnaphthalene ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2-Methylnaphthalene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2-Methylphenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼3 & 4 Methylphenol ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Naphthalene ND 0.816 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2-Nitroaniline ND 0.816 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼3-Nitroaniline ND 0.816 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4-Nitroaniline ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Nitrobenzene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2-Nitrophenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼4-Nitrophenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼N-Nitrosodi-n-propylamine ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.816 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Pentachlorophenol ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Phenanthrene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Phenol ND 0.0656 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼Pyrene ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼1,2,4-Trichlorobenzene ND 0.816 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,4,5-Trichlorophenol ND 0.326 mg/Kg 06/26/15 09:17 06/28/15 17:44 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)78 29-120 06/26/15 09:17 06/28/15 17:44 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)80 06/26/15 09:17 06/28/15 17:44 110-120 Nitrobenzene-d5 (Surr)75 06/26/15 09:17 06/28/15 17:44 127-120 Phenol-d5 (Surr)84 06/26/15 09:17 06/28/15 17:44 110-120 Terphenyl-d14 (Surr)92 06/26/15 09:17 06/28/15 17:44 113-120 TestAmerica Nashville Page 29 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Lab Sample ID: 490-81218-5Client Sample ID: TP-4 (0-2) Matrix: SoilDate Collected: 06/23/15 13:10 Percent Solids: 80.8Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)82 10-120 06/26/15 09:17 06/28/15 17:44 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.2 mg/Kg ☼06/25/15 08:59 06/25/15 16:48 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.45 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Arsenic 7.07 1.22 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Beryllium ND 1.22 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Cadmium ND 1.22 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Chromium 20.5 2.45 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Copper 23.1 1.22 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Lead 25.2 3.67 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Manganese 780 2.45 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Nickel 11.2 2.45 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Selenium ND 1.22 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Silver ND 2.45 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Thallium ND 12.2 mg/Kg 06/25/15 08:59 06/25/15 16:48 1☼Zinc 37.7 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.125 mg/Kg ☼06/24/15 16:44 06/26/15 00:20 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.07 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 30 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 8260B - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-259533/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 RL MDL Acetone ND 0.0500 mg/Kg 06/26/15 01:36 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00200 mg/Kg 06/26/15 01:36 1Benzene ND 0.00200 mg/Kg 06/26/15 01:36 1Bromobenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Bromochloromethane ND 0.00200 mg/Kg 06/26/15 01:36 1Bromodichloromethane ND 0.00200 mg/Kg 06/26/15 01:36 1Bromoform ND 0.00200 mg/Kg 06/26/15 01:36 1Bromomethane ND 0.0500 mg/Kg 06/26/15 01:36 12-Butanone (MEK) ND 0.00500 mg/Kg 06/26/15 01:36 1Carbon disulfide ND 0.00200 mg/Kg 06/26/15 01:36 1Carbon tetrachloride ND 0.00200 mg/Kg 06/26/15 01:36 1Chlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Chlorodibromomethane ND 0.00500 mg/Kg 06/26/15 01:36 1Chloroethane ND 0.00200 mg/Kg 06/26/15 01:36 1Chloroform ND 0.00200 mg/Kg 06/26/15 01:36 1Chloromethane ND 0.00200 mg/Kg 06/26/15 01:36 12-Chlorotoluene ND 0.00200 mg/Kg 06/26/15 01:36 14-Chlorotoluene ND 0.00200 mg/Kg 06/26/15 01:36 1cis-1,2-Dichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1cis-1,3-Dichloropropene ND 0.00500 mg/Kg 06/26/15 01:36 11,2-Dibromo-3-Chloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 06/26/15 01:36 1Dibromomethane ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,3-Dichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,4-Dichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Dichlorodifluoromethane ND 0.00200 mg/Kg 06/26/15 01:36 11,1-Dichloroethane ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichloroethane ND 0.00200 mg/Kg 06/26/15 01:36 11,1-Dichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichloroethene, Total ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,3-Dichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 12,2-Dichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,1-Dichloropropene ND 0.00200 mg/Kg 06/26/15 01:36 1Diisopropyl ether ND 0.00200 mg/Kg 06/26/15 01:36 1Ethylbenzene ND 0.00500 mg/Kg 06/26/15 01:36 1Hexachlorobutadiene ND 0.0500 mg/Kg 06/26/15 01:36 12-Hexanone ND 0.00200 mg/Kg 06/26/15 01:36 1Isopropylbenzene ND 0.0100 mg/Kg 06/26/15 01:36 1Methylene Chloride ND 0.0500 mg/Kg 06/26/15 01:36 14-Methyl-2-pentanone (MIBK) ND 0.00200 mg/Kg 06/26/15 01:36 1Methyl tert-butyl ether ND 0.00500 mg/Kg 06/26/15 01:36 1Naphthalene ND 0.00200 mg/Kg 06/26/15 01:36 1n-Butylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1N-Propylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1p-Isopropyltoluene ND 0.00200 mg/Kg 06/26/15 01:36 1sec-Butylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Styrene TestAmerica Nashville Page 31 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-259533/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 RL MDL tert-Butylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00200 mg/Kg 06/26/15 01:36 11,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 06/26/15 01:36 11,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 06/26/15 01:36 1Tetrachloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1Toluene ND 0.00200 mg/Kg 06/26/15 01:36 1trans-1,2-Dichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1trans-1,3-Dichloropropene ND 0.00200 mg/Kg 06/26/15 01:36 11,2,3-Trichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,2,4-Trichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,1,1-Trichloroethane ND 0.00500 mg/Kg 06/26/15 01:36 11,1,2-Trichloroethane ND 0.00200 mg/Kg 06/26/15 01:36 1Trichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1Trichlorofluoromethane ND 0.00200 mg/Kg 06/26/15 01:36 11,2,3-Trichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,2,4-Trimethylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,3,5-Trimethylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Vinyl chloride ND 0.00500 mg/Kg 06/26/15 01:36 1Xylenes, Total 4-Bromofluorobenzene (Surr)96 70-130 06/26/15 01:36 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 100 06/26/15 01:36 1Dibromofluoromethane (Surr)70-130 98 06/26/15 01:36 11,2-Dichloroethane-d4 (Surr)70-130 104 06/26/15 01:36 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259533/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 Acetone 0.250 0.2518 mg/Kg 101 51-149 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Benzene 0.0500 0.05122 mg/Kg 102 75-127 Bromobenzene 0.0500 0.04974 mg/Kg 99 75-130 Bromochloromethane 0.0500 0.04870 mg/Kg 97 70-132 Bromodichloromethane 0.0500 0.04687 mg/Kg 94 68-135 Bromoform 0.0500 0.04196 mg/Kg 84 36-150 Bromomethane 0.0500 0.04917 mg/Kg 98 43-142 2-Butanone (MEK)0.250 0.2497 mg/Kg 100 61-132 Carbon disulfide 0.0500 0.05509 mg/Kg 110 74-135 Carbon tetrachloride 0.0500 0.04942 mg/Kg 99 70-141 Chlorobenzene 0.0500 0.05075 mg/Kg 101 84-125 Chlorodibromomethane 0.0500 0.04209 mg/Kg 84 66-134 Chloroethane 0.0500 0.05416 mg/Kg 108 53-144 Chloroform 0.0500 0.04736 mg/Kg 95 76-130 Chloromethane 0.0500 0.05009 mg/Kg 100 23-150 2-Chlorotoluene 0.0500 0.04932 mg/Kg 99 78-132 4-Chlorotoluene 0.0500 0.04894 mg/Kg 98 77-138 cis-1,2-Dichloroethene 0.0500 0.05157 mg/Kg 103 75-125 TestAmerica Nashville Page 32 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259533/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 cis-1,3-Dichloropropene 0.0500 0.05069 mg/Kg 101 73-148 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits 1,2-Dibromo-3-Chloropropane 0.0500 0.04046 mg/Kg 81 49-142 1,2-Dibromoethane (EDB)0.0500 0.04914 mg/Kg 98 80-135 Dibromomethane 0.0500 0.05175 mg/Kg 103 71-130 1,2-Dichlorobenzene 0.0500 0.04914 mg/Kg 98 80-134 1,3-Dichlorobenzene 0.0500 0.04865 mg/Kg 97 79-137 1,4-Dichlorobenzene 0.0500 0.04587 mg/Kg 92 77-139 Dichlorodifluoromethane 0.0500 0.04349 mg/Kg 87 12-144 1,1-Dichloroethane 0.0500 0.05002 mg/Kg 100 75-124 1,2-Dichloroethane 0.0500 0.04856 mg/Kg 97 65-134 1,1-Dichloroethene 0.0500 0.05036 mg/Kg 101 75-131 1,2-Dichloroethene, Total 0.100 0.1029 mg/Kg 103 75-128 1,2-Dichloropropane 0.0500 0.05375 mg/Kg 107 69-120 1,3-Dichloropropane 0.0500 0.05101 mg/Kg 102 78-126 2,2-Dichloropropane 0.0500 0.05311 mg/Kg 106 68-145 1,1-Dichloropropene 0.0500 0.05115 mg/Kg 102 79-127 Diisopropyl ether 0.0500 0.05087 mg/Kg 102 68-124 Ethylbenzene 0.0500 0.05284 mg/Kg 106 80-134 Hexachlorobutadiene 0.0500 0.04884 mg/Kg 98 65-148 2-Hexanone 0.250 0.2645 mg/Kg 106 57-148 Isopropylbenzene 0.0500 0.05318 mg/Kg 106 80-150 Methylene Chloride 0.0500 0.05083 mg/Kg 102 68-144 4-Methyl-2-pentanone (MIBK)0.250 0.2685 mg/Kg 107 59-138 Methyl tert-butyl ether 0.0500 0.04824 mg/Kg 96 70-136 Naphthalene 0.0500 0.05379 mg/Kg 108 69-150 n-Butylbenzene 0.0500 0.04755 mg/Kg 95 72-152 N-Propylbenzene 0.0500 0.05067 mg/Kg 101 75-137 p-Isopropyltoluene 0.0500 0.04869 mg/Kg 97 77-141 sec-Butylbenzene 0.0500 0.05091 mg/Kg 102 79-141 Styrene 0.0500 0.05408 mg/Kg 108 74-131 tert-Butylbenzene 0.0500 0.05027 mg/Kg 101 80-132 1,1,1,2-Tetrachloroethane 0.0500 0.04780 mg/Kg 96 80-136 1,1,2,2-Tetrachloroethane 0.0500 0.04858 mg/Kg 97 66-134 Tetrachloroethene 0.0500 0.05083 mg/Kg 102 78-140 Toluene 0.0500 0.05436 mg/Kg 109 80-132 trans-1,2-Dichloroethene 0.0500 0.05133 mg/Kg 103 76-128 trans-1,3-Dichloropropene 0.0500 0.04166 mg/Kg 83 62-139 1,2,3-Trichlorobenzene 0.0500 0.04839 mg/Kg 97 70-150 1,2,4-Trichlorobenzene 0.0500 0.04753 mg/Kg 95 62-150 1,1,1-Trichloroethane 0.0500 0.05164 mg/Kg 103 72-140 1,1,2-Trichloroethane 0.0500 0.04981 mg/Kg 100 78-128 Trichloroethene 0.0500 0.05308 mg/Kg 106 77-127 Trichlorofluoromethane 0.0500 0.04776 mg/Kg 96 50-140 1,2,3-Trichloropropane 0.0500 0.04856 mg/Kg 97 65-139 1,2,4-Trimethylbenzene 0.0500 0.04807 mg/Kg 96 77-139 1,3,5-Trimethylbenzene 0.0500 0.05041 mg/Kg 101 78-138 Vinyl chloride 0.0500 0.05091 mg/Kg 102 47-136 Xylenes, Total 0.100 0.1021 mg/Kg 102 80-137 TestAmerica Nashville Page 33 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259533/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 4-Bromofluorobenzene (Surr)70 -130 Surrogate 96 LCS LCS Qualifier Limits%Recovery 100Dibromofluoromethane (Surr)70 -130 961,2-Dichloroethane-d4 (Surr)70 -130 105Toluene-d8 (Surr)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-259533/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 Acetone 0.250 0.2298 mg/Kg 92 51-149 9 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Benzene 0.0500 0.05170 mg/Kg 103 75-127 1 50 Bromobenzene 0.0500 0.04942 mg/Kg 99 75-130 1 50 Bromochloromethane 0.0500 0.04859 mg/Kg 97 70-132 0 50 Bromodichloromethane 0.0500 0.04706 mg/Kg 94 68-135 0 50 Bromoform 0.0500 0.04146 mg/Kg 83 36-150 1 50 Bromomethane 0.0500 0.05378 mg/Kg 108 43-142 9 50 2-Butanone (MEK)0.250 0.2231 mg/Kg 89 61-132 11 50 Carbon disulfide 0.0500 0.05844 mg/Kg 117 74-135 6 50 Carbon tetrachloride 0.0500 0.04997 mg/Kg 100 70-141 1 50 Chlorobenzene 0.0500 0.05114 mg/Kg 102 84-125 1 50 Chlorodibromomethane 0.0500 0.04269 mg/Kg 85 66-134 1 50 Chloroethane 0.0500 0.05447 mg/Kg 109 53-144 1 50 Chloroform 0.0500 0.04753 mg/Kg 95 76-130 0 49 Chloromethane 0.0500 0.05024 mg/Kg 100 23-150 0 50 2-Chlorotoluene 0.0500 0.04984 mg/Kg 100 78-132 1 50 4-Chlorotoluene 0.0500 0.04941 mg/Kg 99 77-138 1 50 cis-1,2-Dichloroethene 0.0500 0.05191 mg/Kg 104 75-125 1 50 cis-1,3-Dichloropropene 0.0500 0.05005 mg/Kg 100 73-148 1 50 1,2-Dibromo-3-Chloropropane 0.0500 0.03941 mg/Kg 79 49-142 3 50 1,2-Dibromoethane (EDB)0.0500 0.04841 mg/Kg 97 80-135 2 50 Dibromomethane 0.0500 0.05057 mg/Kg 101 71-130 2 50 1,2-Dichlorobenzene 0.0500 0.04954 mg/Kg 99 80-134 1 50 1,3-Dichlorobenzene 0.0500 0.04836 mg/Kg 97 79-137 1 50 1,4-Dichlorobenzene 0.0500 0.04609 mg/Kg 92 77-139 0 50 Dichlorodifluoromethane 0.0500 0.04490 mg/Kg 90 12-144 3 50 1,1-Dichloroethane 0.0500 0.05107 mg/Kg 102 75-124 2 50 1,2-Dichloroethane 0.0500 0.04807 mg/Kg 96 65-134 1 50 1,1-Dichloroethene 0.0500 0.05219 mg/Kg 104 75-131 4 50 1,2-Dichloroethene, Total 0.100 0.1034 mg/Kg 103 75-128 0 41 1,2-Dichloropropane 0.0500 0.05311 mg/Kg 106 69-120 1 50 1,3-Dichloropropane 0.0500 0.05083 mg/Kg 102 78-126 0 42 2,2-Dichloropropane 0.0500 0.05452 mg/Kg 109 68-145 3 50 1,1-Dichloropropene 0.0500 0.05184 mg/Kg 104 79-127 1 50 Diisopropyl ether 0.0500 0.05114 mg/Kg 102 68-124 1 45 Ethylbenzene 0.0500 0.05366 mg/Kg 107 80-134 2 50 Hexachlorobutadiene 0.0500 0.05028 mg/Kg 101 65-148 3 50 2-Hexanone 0.250 0.2553 mg/Kg 102 57-148 4 50 TestAmerica Nashville Page 34 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-259533/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 Isopropylbenzene 0.0500 0.05394 mg/Kg 108 80-150 1 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Methylene Chloride 0.0500 0.05083 mg/Kg 102 68-144 0 50 4-Methyl-2-pentanone (MIBK)0.250 0.2586 mg/Kg 103 59-138 4 50 Methyl tert-butyl ether 0.0500 0.04819 mg/Kg 96 70-136 0 50 Naphthalene 0.0500 0.05095 mg/Kg 102 69-150 5 50 n-Butylbenzene 0.0500 0.04893 mg/Kg 98 72-152 3 50 N-Propylbenzene 0.0500 0.05191 mg/Kg 104 75-137 2 50 p-Isopropyltoluene 0.0500 0.04985 mg/Kg 100 77-141 2 50 sec-Butylbenzene 0.0500 0.05216 mg/Kg 104 79-141 2 50 Styrene 0.0500 0.05374 mg/Kg 107 74-131 1 50 tert-Butylbenzene 0.0500 0.05128 mg/Kg 103 80-132 2 50 1,1,1,2-Tetrachloroethane 0.0500 0.04870 mg/Kg 97 80-136 2 50 1,1,2,2-Tetrachloroethane 0.0500 0.05028 mg/Kg 101 66-134 3 50 Tetrachloroethene 0.0500 0.05272 mg/Kg 105 78-140 4 50 Toluene 0.0500 0.05429 mg/Kg 109 80-132 0 50 trans-1,2-Dichloroethene 0.0500 0.05144 mg/Kg 103 76-128 0 50 trans-1,3-Dichloropropene 0.0500 0.04398 mg/Kg 88 62-139 5 50 1,2,3-Trichlorobenzene 0.0500 0.04745 mg/Kg 95 70-150 2 50 1,2,4-Trichlorobenzene 0.0500 0.04658 mg/Kg 93 62-150 2 50 1,1,1-Trichloroethane 0.0500 0.05278 mg/Kg 106 72-140 2 50 1,1,2-Trichloroethane 0.0500 0.04997 mg/Kg 100 78-128 0 50 Trichloroethene 0.0500 0.05368 mg/Kg 107 77-127 1 50 Trichlorofluoromethane 0.0500 0.05044 mg/Kg 101 50-140 5 50 1,2,3-Trichloropropane 0.0500 0.04781 mg/Kg 96 65-139 2 50 1,2,4-Trimethylbenzene 0.0500 0.04875 mg/Kg 97 77-139 1 50 1,3,5-Trimethylbenzene 0.0500 0.05027 mg/Kg 101 78-138 0 50 Vinyl chloride 0.0500 0.05233 mg/Kg 105 47-136 3 50 Xylenes, Total 0.100 0.1035 mg/Kg 103 80-137 1 50 4-Bromofluorobenzene (Surr)70 -130 Surrogate 97 LCSD LCSD Qualifier Limits%Recovery 99Dibromofluoromethane (Surr)70 -130 941,2-Dichloroethane-d4 (Surr)70 -130 105Toluene-d8 (Surr)70 -130 Method: 6010C - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 490-259251/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 RL MDL Antimony ND 9.98 mg/Kg 06/25/15 08:59 06/25/15 14:56 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Arsenic ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Beryllium ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Cadmium ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Chromium ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Copper TestAmerica Nashville Page 35 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-259251/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 RL MDL Lead ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 2.99 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Manganese ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Nickel ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Selenium ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Silver ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Thallium ND 9.98 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Zinc Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259251/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Antimony 40.0 38.74 mg/Kg 97 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Arsenic 20.0 19.84 mg/Kg 99 80-120 Beryllium 20.0 20.54 mg/Kg 103 80-120 Cadmium 20.0 19.86 mg/Kg 99 80-120 Chromium 80.0 82.60 mg/Kg 103 80-120 Copper 100 102.0 mg/Kg 102 80-120 Lead 20.0 19.88 mg/Kg 99 80-120 Manganese 200 204.4 mg/Kg 102 80-120 Nickel 200 202.6 mg/Kg 101 80-120 Selenium 20.0 19.46 mg/Kg 97 80-120 Silver 20.0 18.08 mg/Kg 90 80-120 Thallium 120 121.4 mg/Kg 101 80-120 Zinc 200 193.9 mg/Kg 97 80-120 Client Sample ID: Matrix SpikeLab Sample ID: 490-81215-D-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Antimony ND 47.3 47.53 mg/Kg 96 75-125☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Arsenic 8.93 23.6 33.30 mg/Kg 103 75-125☼ Beryllium ND 23.6 23.89 mg/Kg 101 75-125☼ Cadmium ND 23.6 22.88 mg/Kg 94 75-125☼ Chromium 26.6 94.5 126.1 mg/Kg 105 75-125☼ Copper 29.9 118 143.0 mg/Kg 96 75-125☼ Lead 64.4 F1 23.6 102.5 F1 mg/Kg 162 75-125☼ Manganese 318 236 517.1 mg/Kg 84 75-125☼ Nickel 13.1 236 240.1 mg/Kg 96 75-125☼ Selenium ND 23.6 20.96 mg/Kg 89 75-125☼ Silver ND 23.6 21.10 mg/Kg 89 75-125☼ Thallium ND 142 131.7 mg/Kg 93 75-125☼ Zinc 162 236 385.7 mg/Kg 95 75-125☼ TestAmerica Nashville Page 36 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-81215-D-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Antimony ND 46.3 44.18 mg/Kg 91 75-125 7 20☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Arsenic 8.93 23.1 35.95 mg/Kg 117 75-125 8 20☼ Beryllium ND 23.1 23.55 mg/Kg 102 75-125 1 20☼ Cadmium ND 23.1 22.62 mg/Kg 95 75-125 1 20☼ Chromium 26.6 92.5 122.5 mg/Kg 104 75-125 3 20☼ Copper 29.9 116 147.8 mg/Kg 102 75-125 3 20☼ Lead 64.4 F1 23.1 124.0 F1 mg/Kg 258 75-125 19 20☼ Manganese 318 231 554.7 mg/Kg 103 75-125 7 20☼ Nickel 13.1 231 237.6 mg/Kg 97 75-125 1 20☼ Selenium ND 23.1 20.89 mg/Kg 90 75-125 0 20☼ Silver ND 23.1 21.51 mg/Kg 93 75-125 2 20☼ Thallium ND 139 129.9 mg/Kg 94 75-125 1 20☼ Zinc 162 231 366.4 mg/Kg 88 75-125 5 20☼ Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Client Sample ID: Method BlankLab Sample ID: MB 490-259128/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 RL MDL Mercury ND 0.0998 mg/Kg 06/24/15 16:44 06/26/15 10:35 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259128/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 Mercury 0.162 0.1819 mg/Kg 112 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Matrix SpikeLab Sample ID: 490-80975-G-6-C MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 Mercury ND F1 0.196 0.2523 F1 mg/Kg 129 80-120☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-80975-G-6-D MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 Mercury ND F1 0.193 0.2589 F1 mg/Kg 134 80-120 3 20☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD TestAmerica Nashville Page 37 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 7196A - Chromium, Hexavalent Client Sample ID: Method BlankLab Sample ID: MB 490-260615/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 RL MDL Chromium, hex ND 4.95 mg/Kg 06/29/15 16:57 07/01/15 18:21 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCSI 490-260615/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex 64.1 67.82 mg/Kg 106 80-120 Analyte LCSI LCSI DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control SampleLab Sample ID: LCSS 490-260615/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex 39.9 43.07 mg/Kg 108 80-120 Analyte LCSS LCSS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSSD 490-260615/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex 39.7 34.31 *mg/Kg 87 80-120 23 20 Analyte LCSSD LCSSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: TP-1 (0-2)Lab Sample ID: 490-81218-1 MSI Matrix: Soil Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex ND * F1 76.8 61.60 mg/Kg 80 75-125☼ Analyte MSI MSI DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: TP-1 (0-2)Lab Sample ID: 490-81218-1 MSS Matrix: Soil Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex ND * F1 47.3 40.69 mg/Kg 86 75-125☼ Analyte MSS MSS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: TP-1 (0-2)Lab Sample ID: 490-81218-1 DU Matrix: Soil Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex ND * F1 ND mg/Kg NC 20☼ Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD TestAmerica Nashville Page 38 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method: 9045D - pH Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259987/12 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259987 pH 7.00 7.020 SU 100 95-105 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: DuplicateLab Sample ID: 490-81306-A-1-C DU Matrix: Solid Prep Type: Soluble Analysis Batch: 259987 pH 5.49 5.490 SU 0 20 Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD Temperature 21.7 21.70 Degrees C 0 20 Method: Moisture - Percent Moisture Client Sample ID: DuplicateLab Sample ID: 490-81215-E-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 258926 Percent Solids 83 85 %2 20 Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD TestAmerica Nashville Page 39 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC GC/MS VOA Prep Batch: 259059 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 5035490-81218-1 TP-1 (0-2)Total/NA Soil 5035490-81218-2 TP-2 (2-4)Total/NA Soil 5035490-81218-3 TP-2 (4-6)Total/NA Soil 5035490-81218-4 TP-3 (4-6)Total/NA Soil 5035490-81218-5 TP-4 (0-2)Total/NA Analysis Batch: 259533 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 8260B 259059490-81218-1 TP-1 (0-2)Total/NA Soil 8260B 259059490-81218-2 TP-2 (2-4)Total/NA Soil 8260B 259059490-81218-3 TP-2 (4-6)Total/NA Soil 8260B 259059490-81218-4 TP-3 (4-6)Total/NA Soil 8260B 259059490-81218-5 TP-4 (0-2)Total/NA Solid 8260BLCS 490-259533/4 Lab Control Sample Total/NA Solid 8260BLCSD 490-259533/5 Lab Control Sample Dup Total/NA Solid 8260BMB 490-259533/7 Method Blank Total/NA GC/MS Semi VOA Prep Batch: 259662 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 3550C490-81218-1 TP-1 (0-2)Total/NA Soil 3550C490-81218-2 TP-2 (2-4)Total/NA Soil 3550C490-81218-3 TP-2 (4-6)Total/NA Soil 3550C490-81218-4 TP-3 (4-6)Total/NA Soil 3550C490-81218-5 TP-4 (0-2)Total/NA Analysis Batch: 260226 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 8270D 259662490-81218-1 TP-1 (0-2)Total/NA Soil 8270D 259662490-81218-2 TP-2 (2-4)Total/NA Soil 8270D 259662490-81218-3 TP-2 (4-6)Total/NA Soil 8270D 259662490-81218-4 TP-3 (4-6)Total/NA Soil 8270D 259662490-81218-5 TP-4 (0-2)Total/NA Metals Prep Batch: 259128 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B490-80975-G-6-C MS Matrix Spike Total/NA Solid 7471B490-80975-G-6-D MSD Matrix Spike Duplicate Total/NA Soil 7471B490-81218-1 TP-1 (0-2)Total/NA Soil 7471B490-81218-2 TP-2 (2-4)Total/NA Soil 7471B490-81218-3 TP-2 (4-6)Total/NA Soil 7471B490-81218-4 TP-3 (4-6)Total/NA Soil 7471B490-81218-5 TP-4 (0-2)Total/NA Solid 7471BLCS 490-259128/2-A Lab Control Sample Total/NA Solid 7471BMB 490-259128/1-A Method Blank Total/NA TestAmerica Nashville Page 40 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Metals (Continued) Prep Batch: 259251 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3051A490-81215-D-1-B MS Matrix Spike Total/NA Solid 3051A490-81215-D-1-C MSD Matrix Spike Duplicate Total/NA Soil 3051A490-81218-1 TP-1 (0-2)Total/NA Soil 3051A490-81218-2 TP-2 (2-4)Total/NA Soil 3051A490-81218-3 TP-2 (4-6)Total/NA Soil 3051A490-81218-4 TP-3 (4-6)Total/NA Soil 3051A490-81218-5 TP-4 (0-2)Total/NA Solid 3051ALCS 490-259251/2-A Lab Control Sample Total/NA Solid 3051AMB 490-259251/1-A Method Blank Total/NA Analysis Batch: 259614 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010C 259251490-81215-D-1-B MS Matrix Spike Total/NA Solid 6010C 259251490-81215-D-1-C MSD Matrix Spike Duplicate Total/NA Soil 6010C 259251490-81218-1 TP-1 (0-2)Total/NA Soil 6010C 259251490-81218-2 TP-2 (2-4)Total/NA Soil 6010C 259251490-81218-3 TP-2 (4-6)Total/NA Soil 6010C 259251490-81218-4 TP-3 (4-6)Total/NA Soil 6010C 259251490-81218-5 TP-4 (0-2)Total/NA Solid 6010C 259251LCS 490-259251/2-A Lab Control Sample Total/NA Solid 6010C 259251MB 490-259251/1-A Method Blank Total/NA Analysis Batch: 259797 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 259128490-80975-G-6-C MS Matrix Spike Total/NA Solid 7471B 259128490-80975-G-6-D MSD Matrix Spike Duplicate Total/NA Soil 7471B 259128490-81218-1 TP-1 (0-2)Total/NA Soil 7471B 259128490-81218-2 TP-2 (2-4)Total/NA Soil 7471B 259128490-81218-3 TP-2 (4-6)Total/NA Soil 7471B 259128490-81218-4 TP-3 (4-6)Total/NA Soil 7471B 259128490-81218-5 TP-4 (0-2)Total/NA Solid 7471B 259128LCS 490-259128/2-A Lab Control Sample Total/NA Solid 7471B 259128MB 490-259128/1-A Method Blank Total/NA General Chemistry Analysis Batch: 258926 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture490-81189-A-1 MS Matrix Spike Total/NA Solid Moisture490-81189-A-1 MSD Matrix Spike Duplicate Total/NA Solid Moisture490-81215-E-1 DU Duplicate Total/NA Soil Moisture490-81218-1 TP-1 (0-2)Total/NA Soil Moisture490-81218-2 TP-2 (2-4)Total/NA Soil Moisture490-81218-3 TP-2 (4-6)Total/NA Soil Moisture490-81218-4 TP-3 (4-6)Total/NA Soil Moisture490-81218-5 TP-4 (0-2)Total/NA Leach Batch: 259766 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil DI Leach490-81218-3 TP-2 (4-6)Soluble TestAmerica Nashville Page 41 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC General Chemistry (Continued) Leach Batch: 259766 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid DI Leach490-81306-A-1-C DU Duplicate Soluble Analysis Batch: 259987 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 9045D 259766490-81218-3 TP-2 (4-6)Soluble Solid 9045D 259766490-81306-A-1-C DU Duplicate Soluble Solid 9045DLCS 490-259987/12 Lab Control Sample Total/NA Prep Batch: 260615 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 3060A490-81218-1 TP-1 (0-2)Total/NA Soil 3060A490-81218-1 DU TP-1 (0-2)Total/NA Soil 3060A490-81218-1 MSI TP-1 (0-2)Total/NA Soil 3060A490-81218-1 MSS TP-1 (0-2)Total/NA Soil 3060A490-81218-2 TP-2 (2-4)Total/NA Soil 3060A490-81218-3 TP-2 (4-6)Total/NA Soil 3060A490-81218-4 TP-3 (4-6)Total/NA Soil 3060A490-81218-5 TP-4 (0-2)Total/NA Solid 3060ALCSI 490-260615/4-A Lab Control Sample Total/NA Solid 3060ALCSS 490-260615/2-A Lab Control Sample Total/NA Solid 3060ALCSSD 490-260615/3-A Lab Control Sample Dup Total/NA Solid 3060AMB 490-260615/1-A Method Blank Total/NA Analysis Batch: 261360 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 7196A 260615490-81218-1 TP-1 (0-2)Total/NA Soil 7196A 260615490-81218-1 DU TP-1 (0-2)Total/NA Soil 7196A 260615490-81218-1 MSI TP-1 (0-2)Total/NA Soil 7196A 260615490-81218-1 MSS TP-1 (0-2)Total/NA Soil 7196A 260615490-81218-2 TP-2 (2-4)Total/NA Soil 7196A 260615490-81218-3 TP-2 (4-6)Total/NA Soil 7196A 260615490-81218-4 TP-3 (4-6)Total/NA Soil 7196A 260615490-81218-5 TP-4 (0-2)Total/NA Solid 7196A 260615LCSI 490-260615/4-A Lab Control Sample Total/NA Solid 7196A 260615LCSS 490-260615/2-A Lab Control Sample Total/NA Solid 7196A 260615LCSSD 490-260615/3-A Lab Control Sample Dup Total/NA Solid 7196A 260615MB 490-260615/1-A Method Blank Total/NA TestAmerica Nashville Page 42 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81218-1 Project/Site: NODA Greenway/Charlotte, NC SDG: CRE-001 Client Sample ID: TP-1 (0-2)Lab Sample ID: 490-81218-1 Matrix: SoilDate Collected: 06/23/15 11:40 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 14:041 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-1 (0-2)Lab Sample ID: 490-81218-1 Matrix: SoilDate Collected: 06/23/15 11:40 Percent Solids: 83.6Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 11:40 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.195 g 5.0 mL Analysis 8260B 1 259533 06/26/15 02:05 KKK TAL NSHTotal/NA 6.195 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 35.96 g 1 mL Analysis 8270D 1 260226 06/28/15 16:09 SNR TAL NSHTotal/NA 35.96 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.513 g 100 mL Analysis 6010C 1 259614 06/25/15 16:22 LEG TAL NSHTotal/NA 0.513 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.619 g 100 mL Analysis 7471B 1 259797 06/26/15 00:10 CME TAL NSHTotal/NA 0.619 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.6057 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.6057 g 500 mL Client Sample ID: TP-2 (2-4)Lab Sample ID: 490-81218-2 Matrix: SoilDate Collected: 06/23/15 12:15 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 14:041 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-2 (2-4)Lab Sample ID: 490-81218-2 Matrix: SoilDate Collected: 06/23/15 12:15 Percent Solids: 85.1Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 12:15 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.013 g 5.0 mL Analysis 8260B 1 259533 06/26/15 02:36 KKK TAL NSHTotal/NA 6.013 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 35.51 g 1 mL Analysis 8270D 5 260226 06/28/15 16:32 SNR TAL NSHTotal/NA 35.51 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.511 g 100 mL Analysis 6010C 1 259614 06/25/15 16:26 LEG TAL NSHTotal/NA 0.511 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.622 g 100 mL Analysis 7471B 1 259797 06/26/15 00:13 CME TAL NSHTotal/NA 0.622 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5104 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5104 g 500 mL TestAmerica Nashville Page 43 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81218-1 Project/Site: NODA Greenway/Charlotte, NC SDG: CRE-001 Client Sample ID: TP-2 (4-6)Lab Sample ID: 490-81218-3 Matrix: SoilDate Collected: 06/23/15 12:20 Date Received: 06/24/15 08:30 Leach DI Leach SJM06/26/15 12:37 TAL NSH259766 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Soluble 20 g 20 mL Analysis 9045D 1 259987 06/27/15 10:08 SJM TAL NSHSoluble20 g 20 mL Analysis Moisture 1 258926 06/24/15 14:04 MAA TAL NSHTotal/NA Client Sample ID: TP-2 (4-6)Lab Sample ID: 490-81218-3 Matrix: SoilDate Collected: 06/23/15 12:20 Percent Solids: 74.8Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 12:20 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 4.325 g 5.0 mL Analysis 8260B 1 259533 06/26/15 03:07 KKK TAL NSHTotal/NA 4.325 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 40.24 g 1 mL Analysis 8270D 1 260226 06/28/15 16:56 SNR TAL NSHTotal/NA 40.24 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.502 g 100 mL Analysis 6010C 1 259614 06/25/15 16:39 LEG TAL NSHTotal/NA 0.502 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.621 g 100 mL Analysis 7471B 1 259797 06/26/15 00:15 CME TAL NSHTotal/NA 0.621 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5385 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5385 g 500 mL Client Sample ID: TP-3 (4-6)Lab Sample ID: 490-81218-4 Matrix: SoilDate Collected: 06/23/15 12:50 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 14:041 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-3 (4-6)Lab Sample ID: 490-81218-4 Matrix: SoilDate Collected: 06/23/15 12:50 Percent Solids: 88.6Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 12:50 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.758 g 5.0 mL Analysis 8260B 1 259533 06/26/15 03:37 KKK TAL NSHTotal/NA 6.758 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 34.03 g 1 mL Analysis 8270D 5 260226 06/28/15 17:20 SNR TAL NSHTotal/NA 34.03 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.510 g 100 mL Analysis 6010C 1 259614 06/25/15 16:44 LEG TAL NSHTotal/NA 0.510 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.597 g 100 mL Analysis 7471B 1 259797 06/26/15 00:17 CME TAL NSHTotal/NA 0.597 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5539 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5539 g 500 mL TestAmerica Nashville Page 44 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81218-1 Project/Site: NODA Greenway/Charlotte, NC SDG: CRE-001 Client Sample ID: TP-4 (0-2)Lab Sample ID: 490-81218-5 Matrix: SoilDate Collected: 06/23/15 13:10 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 14:041 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-4 (0-2)Lab Sample ID: 490-81218-5 Matrix: SoilDate Collected: 06/23/15 13:10 Percent Solids: 80.8Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 13:10 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 7.232 g 5.0 mL Analysis 8260B 1 259533 06/26/15 04:08 KKK TAL NSHTotal/NA 7.232 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 37.92 g 1 mL Analysis 8270D 1 260226 06/28/15 17:44 SNR TAL NSHTotal/NA 37.92 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.506 g 100 mL Analysis 6010C 1 259614 06/25/15 16:48 LEG TAL NSHTotal/NA 0.506 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.595 g 100 mL Analysis 7471B 1 259797 06/26/15 00:20 CME TAL NSHTotal/NA 0.595 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5479 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5479 g 500 mL Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 45 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Method Summary TestAmerica Job ID: 490-81218-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway/Charlotte, NC Method Method Description LaboratoryProtocol SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH SW8466010CMetals (ICP)TAL NSH SW8467471BMercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)TAL NSH SW8467196AChromium, Hexavalent TAL NSH SW8469045DpH TAL NSH EPAMoisturePercent Moisture TAL NSH Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 46 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Certification Summary Client: Hart & Hickman, PC TestAmerica Job ID: 490-81218-1 Project/Site: NODA Greenway/Charlotte, NC SDG: CRE-001 Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification ID Expiration Date North Carolina (WW/SW)3874State Program 12-31-15 Analysis Method Prep Method Matrix Analyte The following analytes are included in this report, but certification is not offered by the governing authority: 9045D Soil Temperature Moisture Soil Percent Solids TestAmerica Nashville Page 47 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 48 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 49 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Login Sample Receipt Checklist Client: Hart & Hickman, PC Job Number: 490-81218-1 SDG Number: CRE-001 Login Number: 81218 Question Answer Comment Creator: McBride, Mike List Source: TestAmerica Nashville List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.3.4 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time. TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. TestAmerica Nashville Page 50 of 50 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-81215-1 TestAmerica Sample Delivery Group: CRE-001 Client Project/Site: NODA Greenway, Charlotte NC For: Hart & Hickman, PC 2923 S Tryon Street Suite 100 Charlotte, North Carolina 28203 Attn: Brett Lawrence Authorized for release by: 7/2/2015 11:38:20 AM Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 12 13 Table of Contents Client: Hart & Hickman, PC Project/Site: NODA Greenway, Charlotte NC TestAmerica Job ID: 490-81215-1 SDG: CRE-001 Page 2 of 95 TestAmerica Nashville7/2/2015 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .62 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .79 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .84 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .90 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .92 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95 1 2 3 4 5 6 7 8 9 10 11 12 13 Sample Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID Client Sample ID ReceivedCollectedMatrix 490-81215-1 TP-8 (0-2)Soil 06/22/15 10:10 06/24/15 08:30 490-81215-2 TP-8 (8-10)Soil 06/22/15 10:15 06/24/15 08:30 490-81215-3 TP-11 (0-2)Soil 06/22/15 12:15 06/24/15 08:30 490-81215-4 TP-5 (0-2)Soil 06/22/15 14:20 06/24/15 08:30 490-81215-5 TP-6 (0-2)Soil 06/22/15 15:10 06/24/15 08:30 490-81215-6 TP-6 (8-10)Soil 06/22/15 15:15 06/24/15 08:30 490-81215-7 TP-7 (0-2)Soil 06/22/15 15:45 06/24/15 08:30 490-81215-8 TP-9 (8-10)Soil 06/22/15 16:25 06/24/15 08:30 490-81215-9 TP-11 (6-13)Soil 06/22/15 16:45 06/24/15 08:30 490-81215-10 TP-12 (0-2)Soil 06/23/15 09:30 06/24/15 08:30 490-81215-11 TP-13 (0-2)Soil 06/23/15 10:15 06/24/15 08:30 490-81215-12 TP-13 (10-11)Soil 06/23/15 10:20 06/24/15 08:30 TestAmerica Nashville Page 3 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Case Narrative Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Job ID: 490-81215-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-81215-1 Comments No additional comments. Receipt The samples were received on 6/24/2015 8:30 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 1.6º C. GC/MS VOA Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with analytical batch 490-259533. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC/MS Semi VOA Method(s) 8270D: The following sample required a dilution due to the nature of the sample matrix: TP-8 (0-2) (490-81215-1). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information. Method(s) 8270D: The following samples were diluted due to the nature of the sample matrix: TP-8 (0-2) (490-81215-1), TP-8 (8-10) (490-81215-2), TP-11 (0-2) (490-81215-3), TP-6 (0-2) (490-81215-5), TP-7 (0-2) (490-81215-7), TP-12 (0-2) (490-81215-10), TP-13 (0-2) (490-81215-11) and TP-13 (10-11) (490-81215-12). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. General Chemistry Method(s) 7196A: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch 490-260615 recovered outside control limits for the following analytes: Hexavalent Chromium. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica NashvillePage 4 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Definitions/Glossary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Qualifiers GC/MS Semi VOA Qualifier Description F1 MS and/or MSD Recovery is outside acceptance limits. Qualifier F2 MS/MSD RPD exceeds control limits X Surrogate is outside control limits J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Metals Qualifier Description F1 MS and/or MSD Recovery is outside acceptance limits. Qualifier General Chemistry Qualifier Description *RPD of the LCS and LCSD exceeds the control limits Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 5 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-1Client Sample ID: TP-8 (0-2) Matrix: SoilDate Collected: 06/22/15 10:10 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 83 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 6 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-1Client Sample ID: TP-8 (0-2) Matrix: SoilDate Collected: 06/22/15 10:10 Percent Solids: 83.5Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0583 mg/Kg ☼06/22/15 10:10 06/26/15 04:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Benzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Bromobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Bromochloromethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Bromodichloromethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Bromoform ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Bromomethane ND 0.0583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼2-Butanone (MEK)ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Carbon disulfide ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Carbon tetrachloride ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Chlorobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Chlorodibromomethane ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Chloroethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Chloroform ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Chloromethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼2-Chlorotoluene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼4-Chlorotoluene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼cis-1,2-Dichloroethene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼cis-1,3-Dichloropropene ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2-Dibromo-3-Chloropropane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2-Dibromoethane (EDB)ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Dibromomethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2-Dichlorobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,3-Dichlorobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,4-Dichlorobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Dichlorodifluoromethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,1-Dichloroethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2-Dichloroethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,1-Dichloroethene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2-Dichloroethene, Total ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2-Dichloropropane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,3-Dichloropropane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼2,2-Dichloropropane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,1-Dichloropropene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Diisopropyl ether ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Ethylbenzene ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Hexachlorobutadiene ND 0.0583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼2-Hexanone ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Isopropylbenzene ND 0.0117 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Methylene Chloride ND 0.0583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼4-Methyl-2-pentanone (MIBK)ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Methyl tert-butyl ether ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Naphthalene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼n-Butylbenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼N-Propylbenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼p-Isopropyltoluene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼sec-Butylbenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Styrene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼tert-Butylbenzene ND TestAmerica Nashville Page 7 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-1Client Sample ID: TP-8 (0-2) Matrix: SoilDate Collected: 06/22/15 10:10 Percent Solids: 83.5Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00233 mg/Kg ☼06/22/15 10:10 06/26/15 04:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,1,2,2-Tetrachloroethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Tetrachloroethene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Toluene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼trans-1,2-Dichloroethene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼trans-1,3-Dichloropropene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2,3-Trichlorobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2,4-Trichlorobenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,1,1-Trichloroethane ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,1,2-Trichloroethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Trichloroethene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Trichlorofluoromethane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2,3-Trichloropropane ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,2,4-Trimethylbenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼1,3,5-Trimethylbenzene ND 0.00233 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Vinyl chloride ND 0.00583 mg/Kg 06/22/15 10:10 06/26/15 04:39 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)96 70-130 06/22/15 10:10 06/26/15 04:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)103 06/22/15 10:10 06/26/15 04:39 170-130 1,2-Dichloroethane-d4 (Surr)108 06/22/15 10:10 06/26/15 04:39 170-130 Toluene-d8 (Surr)104 06/22/15 10:10 06/26/15 04:39 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene 40.3 13.3 mg/Kg ☼06/26/15 09:17 06/28/15 11:45 200 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Acenaphthylene ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Anthracene 64.5 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Benzo[a]anthracene 139 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Benzo[a]pyrene 124 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Benzo[b]fluoranthene 175 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Benzo[g,h,i]perylene 80.7 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Benzo[k]fluoranthene 69.6 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Bis(2-chloroethoxy)methane ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Bis(2-chloroethyl)ether ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼bis (2-chloroisopropyl) ether ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Bis(2-ethylhexyl) phthalate ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4-Bromophenyl phenyl ether ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Butyl benzyl phthalate ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Carbazole ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4-Chloroaniline ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4-Chloro-3-methylphenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2-Chloronaphthalene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2-Chlorophenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4-Chlorophenyl phenyl ether ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Chrysene 136 132 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Cresols ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Dibenz(a,h)anthracene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Dibenzofuran ND TestAmerica Nashville Page 8 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-1Client Sample ID: TP-8 (0-2) Matrix: SoilDate Collected: 06/22/15 10:10 Percent Solids: 83.5Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 66.1 mg/Kg ☼06/26/15 09:17 06/28/15 11:45 200 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼1,3-Dichlorobenzene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼1,4-Dichlorobenzene ND 132 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼3,3'-Dichlorobenzidine ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,4-Dichlorophenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Diethyl phthalate ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,4-Dimethylphenol ND 332 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Dimethyl phthalate ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Di-n-butyl phthalate ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4,6-Dinitro-2-methylphenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,4-Dinitrophenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,4-Dinitrotoluene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,6-Dinitrotoluene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Di-n-octyl phthalate ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Fluoranthene 331 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Fluorene 35.1 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Hexachlorobenzene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Hexachlorobutadiene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Hexachlorocyclopentadiene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Hexachloroethane ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Indeno[1,2,3-cd]pyrene 67.3 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Isophorone ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼1-Methylnaphthalene ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2-Methylnaphthalene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2-Methylphenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼3 & 4 Methylphenol ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Naphthalene 15.7 165 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2-Nitroaniline ND 165 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼3-Nitroaniline ND 165 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4-Nitroaniline ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Nitrobenzene ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2-Nitrophenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼4-Nitrophenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼N-Nitrosodi-n-propylamine ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼n-Nitrosodiphenylamine(as diphenylamine) ND 165 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Pentachlorophenol ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Phenanthrene 236 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Phenol ND 13.3 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼Pyrene 230 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼1,2,4-Trichlorobenzene ND 165 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,4,5-Trichlorophenol ND 66.1 mg/Kg 06/26/15 09:17 06/28/15 11:45 200☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)0 X 29-120 06/26/15 09:17 06/28/15 11:45 200 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)0 X 06/26/15 09:17 06/28/15 11:45 20010-120 Nitrobenzene-d5 (Surr)0 X 06/26/15 09:17 06/28/15 11:45 20027-120 Phenol-d5 (Surr)0 X 06/26/15 09:17 06/28/15 11:45 20010-120 Terphenyl-d14 (Surr)0 X 06/26/15 09:17 06/28/15 11:45 20013-120 TestAmerica Nashville Page 9 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-1Client Sample ID: TP-8 (0-2) Matrix: SoilDate Collected: 06/22/15 10:10 Percent Solids: 83.5Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)0 X 10-120 06/26/15 09:17 06/28/15 11:45 200 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.6 mg/Kg ☼06/25/15 08:59 06/25/15 15:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.31 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Arsenic 8.93 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Beryllium ND 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Cadmium ND 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Chromium 26.6 2.31 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Copper 29.9 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Lead 64.4 F1 3.47 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Manganese 318 2.31 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Nickel 13.1 2.31 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Selenium ND 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Silver ND 2.31 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Thallium ND 11.6 mg/Kg 06/25/15 08:59 06/25/15 15:09 1☼Zinc 162 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury 0.338 0.117 mg/Kg ☼06/24/15 16:44 06/26/15 10:54 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.76 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 10 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-2Client Sample ID: TP-8 (8-10) Matrix: SoilDate Collected: 06/22/15 10:15 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 78 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 11 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-2Client Sample ID: TP-8 (8-10) Matrix: SoilDate Collected: 06/22/15 10:15 Percent Solids: 77.8Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0529 mg/Kg ☼06/22/15 10:15 06/26/15 05:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Benzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Bromobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Bromochloromethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Bromodichloromethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Bromoform ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Bromomethane ND 0.0529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼2-Butanone (MEK)ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Carbon disulfide ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Carbon tetrachloride ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Chlorobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Chlorodibromomethane ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Chloroethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Chloroform ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Chloromethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼2-Chlorotoluene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼4-Chlorotoluene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼cis-1,2-Dichloroethene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼cis-1,3-Dichloropropene ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2-Dibromo-3-Chloropropane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2-Dibromoethane (EDB)ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Dibromomethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2-Dichlorobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,3-Dichlorobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,4-Dichlorobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Dichlorodifluoromethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,1-Dichloroethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2-Dichloroethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,1-Dichloroethene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2-Dichloroethene, Total ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2-Dichloropropane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,3-Dichloropropane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼2,2-Dichloropropane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,1-Dichloropropene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Diisopropyl ether ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Ethylbenzene ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Hexachlorobutadiene ND 0.0529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼2-Hexanone ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Isopropylbenzene ND 0.0106 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Methylene Chloride ND 0.0529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼4-Methyl-2-pentanone (MIBK)ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Methyl tert-butyl ether ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Naphthalene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼n-Butylbenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼N-Propylbenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼p-Isopropyltoluene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼sec-Butylbenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Styrene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼tert-Butylbenzene ND TestAmerica Nashville Page 12 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-2Client Sample ID: TP-8 (8-10) Matrix: SoilDate Collected: 06/22/15 10:15 Percent Solids: 77.8Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00212 mg/Kg ☼06/22/15 10:15 06/26/15 05:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,1,2,2-Tetrachloroethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Tetrachloroethene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Toluene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼trans-1,2-Dichloroethene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼trans-1,3-Dichloropropene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2,3-Trichlorobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2,4-Trichlorobenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,1,1-Trichloroethane ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,1,2-Trichloroethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Trichloroethene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Trichlorofluoromethane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2,3-Trichloropropane ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,2,4-Trimethylbenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼1,3,5-Trimethylbenzene ND 0.00212 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Vinyl chloride ND 0.00529 mg/Kg 06/22/15 10:15 06/26/15 05:09 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)94 70-130 06/22/15 10:15 06/26/15 05:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 06/22/15 10:15 06/26/15 05:09 170-130 1,2-Dichloroethane-d4 (Surr)111 06/22/15 10:15 06/26/15 05:09 170-130 Toluene-d8 (Surr)100 06/22/15 10:15 06/26/15 05:09 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.335 mg/Kg ☼06/26/15 09:17 06/28/15 12:09 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Acenaphthylene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Anthracene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Benzo[a]anthracene 0.570 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Benzo[a]pyrene 0.493 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Benzo[b]fluoranthene 0.668 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Benzo[g,h,i]perylene 0.362 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Benzo[k]fluoranthene 0.337 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Bis(2-chloroethoxy)methane ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Bis(2-chloroethyl)ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼bis (2-chloroisopropyl) ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Bis(2-ethylhexyl) phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4-Bromophenyl phenyl ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Butyl benzyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Carbazole ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4-Chloroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4-Chloro-3-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2-Chloronaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2-Chlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4-Chlorophenyl phenyl ether ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Chrysene 0.567 3.33 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Cresols ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Dibenz(a,h)anthracene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Dibenzofuran ND TestAmerica Nashville Page 13 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-2Client Sample ID: TP-8 (8-10) Matrix: SoilDate Collected: 06/22/15 10:15 Percent Solids: 77.8Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.66 mg/Kg ☼06/26/15 09:17 06/28/15 12:09 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼1,3-Dichlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼1,4-Dichlorobenzene ND 3.33 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼3,3'-Dichlorobenzidine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,4-Dichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Diethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,4-Dimethylphenol ND 8.34 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Dimethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Di-n-butyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4,6-Dinitro-2-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,4-Dinitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,4-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,6-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Di-n-octyl phthalate ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Fluoranthene 1.18 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Fluorene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Hexachlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Hexachlorobutadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Hexachlorocyclopentadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Hexachloroethane ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Indeno[1,2,3-cd]pyrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Isophorone ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼1-Methylnaphthalene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2-Methylnaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2-Methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼3 & 4 Methylphenol ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Naphthalene ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2-Nitroaniline ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼3-Nitroaniline ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4-Nitroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Nitrobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼4-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼N-Nitrosodi-n-propylamine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Pentachlorophenol ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Phenanthrene 0.656 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Phenol ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼Pyrene 0.973 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼1,2,4-Trichlorobenzene ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,4,5-Trichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:09 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)85 29-120 06/26/15 09:17 06/28/15 12:09 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)85 06/26/15 09:17 06/28/15 12:09 510-120 Nitrobenzene-d5 (Surr)78 06/26/15 09:17 06/28/15 12:09 527-120 Phenol-d5 (Surr)88 06/26/15 09:17 06/28/15 12:09 510-120 Terphenyl-d14 (Surr)94 06/26/15 09:17 06/28/15 12:09 513-120 TestAmerica Nashville Page 14 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-2Client Sample ID: TP-8 (8-10) Matrix: SoilDate Collected: 06/22/15 10:15 Percent Solids: 77.8Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)92 10-120 06/26/15 09:17 06/28/15 12:09 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.8 mg/Kg ☼06/25/15 08:59 06/25/15 15:30 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Arsenic 2.79 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Beryllium ND 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Cadmium ND 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Chromium 19.0 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Copper 38.3 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Lead 69.9 3.84 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Manganese 493 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Nickel 8.09 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Selenium ND 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Silver ND 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Thallium ND 12.8 mg/Kg 06/25/15 08:59 06/25/15 15:30 1☼Zinc 134 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury 0.167 0.126 mg/Kg ☼06/24/15 16:44 06/26/15 10:56 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.26 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 15 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-3Client Sample ID: TP-11 (0-2) Matrix: SoilDate Collected: 06/22/15 12:15 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 88 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 16 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-3Client Sample ID: TP-11 (0-2) Matrix: SoilDate Collected: 06/22/15 12:15 Percent Solids: 87.9Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0460 mg/Kg ☼06/22/15 12:15 06/26/15 05:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Benzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Bromobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Bromochloromethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Bromodichloromethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Bromoform ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Bromomethane ND 0.0460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼2-Butanone (MEK)ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Carbon disulfide ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Carbon tetrachloride ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Chlorobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Chlorodibromomethane ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Chloroethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Chloroform ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Chloromethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼2-Chlorotoluene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼4-Chlorotoluene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼cis-1,2-Dichloroethene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼cis-1,3-Dichloropropene ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2-Dibromo-3-Chloropropane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2-Dibromoethane (EDB)ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Dibromomethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2-Dichlorobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,3-Dichlorobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,4-Dichlorobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Dichlorodifluoromethane 0.00191 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,1-Dichloroethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2-Dichloroethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,1-Dichloroethene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2-Dichloroethene, Total ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2-Dichloropropane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,3-Dichloropropane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼2,2-Dichloropropane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,1-Dichloropropene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Diisopropyl ether ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Ethylbenzene ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Hexachlorobutadiene ND 0.0460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼2-Hexanone ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Isopropylbenzene ND 0.00920 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Methylene Chloride ND 0.0460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼4-Methyl-2-pentanone (MIBK)ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Methyl tert-butyl ether ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Naphthalene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼n-Butylbenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼N-Propylbenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼p-Isopropyltoluene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼sec-Butylbenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Styrene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼tert-Butylbenzene ND TestAmerica Nashville Page 17 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-3Client Sample ID: TP-11 (0-2) Matrix: SoilDate Collected: 06/22/15 12:15 Percent Solids: 87.9Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00184 mg/Kg ☼06/22/15 12:15 06/26/15 05:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,1,2,2-Tetrachloroethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Tetrachloroethene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Toluene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼trans-1,2-Dichloroethene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼trans-1,3-Dichloropropene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2,3-Trichlorobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2,4-Trichlorobenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,1,1-Trichloroethane ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,1,2-Trichloroethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Trichloroethene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Trichlorofluoromethane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2,3-Trichloropropane ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,2,4-Trimethylbenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼1,3,5-Trimethylbenzene ND 0.00184 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Vinyl chloride ND 0.00460 mg/Kg 06/22/15 12:15 06/26/15 05:39 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)97 70-130 06/22/15 12:15 06/26/15 05:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)105 06/22/15 12:15 06/26/15 05:39 170-130 1,2-Dichloroethane-d4 (Surr)111 06/22/15 12:15 06/26/15 05:39 170-130 Toluene-d8 (Surr)104 06/22/15 12:15 06/26/15 05:39 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.329 mg/Kg ☼06/26/15 09:17 06/28/15 12:33 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Acenaphthylene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Anthracene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Benzo[a]anthracene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Benzo[a]pyrene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Benzo[b]fluoranthene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Benzo[g,h,i]perylene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Benzo[k]fluoranthene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Bis(2-chloroethoxy)methane ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Bis(2-chloroethyl)ether ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼bis (2-chloroisopropyl) ether ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Bis(2-ethylhexyl) phthalate ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4-Bromophenyl phenyl ether ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Butyl benzyl phthalate ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Carbazole ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4-Chloroaniline ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4-Chloro-3-methylphenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2-Chloronaphthalene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2-Chlorophenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4-Chlorophenyl phenyl ether ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Chrysene ND 3.27 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Cresols ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Dibenz(a,h)anthracene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Dibenzofuran ND TestAmerica Nashville Page 18 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-3Client Sample ID: TP-11 (0-2) Matrix: SoilDate Collected: 06/22/15 12:15 Percent Solids: 87.9Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.63 mg/Kg ☼06/26/15 09:17 06/28/15 12:33 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼1,3-Dichlorobenzene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼1,4-Dichlorobenzene ND 3.27 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼3,3'-Dichlorobenzidine ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,4-Dichlorophenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Diethyl phthalate ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,4-Dimethylphenol ND 8.20 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Dimethyl phthalate ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Di-n-butyl phthalate ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4,6-Dinitro-2-methylphenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,4-Dinitrophenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,4-Dinitrotoluene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,6-Dinitrotoluene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Di-n-octyl phthalate ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Fluoranthene 0.535 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Fluorene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Hexachlorobenzene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Hexachlorobutadiene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Hexachlorocyclopentadiene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Hexachloroethane ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Indeno[1,2,3-cd]pyrene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Isophorone ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼1-Methylnaphthalene ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2-Methylnaphthalene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2-Methylphenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼3 & 4 Methylphenol ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Naphthalene ND 4.09 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2-Nitroaniline ND 4.09 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼3-Nitroaniline ND 4.09 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4-Nitroaniline ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Nitrobenzene ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2-Nitrophenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼4-Nitrophenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼N-Nitrosodi-n-propylamine ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.09 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Pentachlorophenol ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Phenanthrene 0.338 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Phenol ND 0.329 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼Pyrene 0.439 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼1,2,4-Trichlorobenzene ND 4.09 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,4,5-Trichlorophenol ND 1.63 mg/Kg 06/26/15 09:17 06/28/15 12:33 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)86 29-120 06/26/15 09:17 06/28/15 12:33 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)84 06/26/15 09:17 06/28/15 12:33 510-120 Nitrobenzene-d5 (Surr)78 06/26/15 09:17 06/28/15 12:33 527-120 Phenol-d5 (Surr)89 06/26/15 09:17 06/28/15 12:33 510-120 Terphenyl-d14 (Surr)99 06/26/15 09:17 06/28/15 12:33 513-120 TestAmerica Nashville Page 19 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-3Client Sample ID: TP-11 (0-2) Matrix: SoilDate Collected: 06/22/15 12:15 Percent Solids: 87.9Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)95 10-120 06/26/15 09:17 06/28/15 12:33 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.4 mg/Kg ☼06/25/15 08:59 06/25/15 15:34 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.28 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Arsenic 3.72 1.14 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Beryllium ND 1.14 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Cadmium ND 1.14 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Chromium 34.7 2.28 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Copper 25.6 1.14 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Lead 59.3 3.43 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Manganese 571 2.28 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Nickel 8.00 2.28 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Selenium ND 1.14 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Silver ND 2.28 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Thallium ND 11.4 mg/Kg 06/25/15 08:59 06/25/15 15:34 1☼Zinc 59.9 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.112 mg/Kg ☼06/24/15 16:44 06/26/15 11:03 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.48 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 20 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-4Client Sample ID: TP-5 (0-2) Matrix: SoilDate Collected: 06/22/15 14:20 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 82 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 21 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-4Client Sample ID: TP-5 (0-2) Matrix: SoilDate Collected: 06/22/15 14:20 Percent Solids: 81.6Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.196 0.0625 mg/Kg ☼06/22/15 14:20 06/26/15 06:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Benzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Bromobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Bromochloromethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Bromodichloromethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Bromoform ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Bromomethane ND 0.0625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼2-Butanone (MEK)ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Carbon disulfide ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Carbon tetrachloride ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Chlorobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Chlorodibromomethane ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Chloroethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Chloroform ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Chloromethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼2-Chlorotoluene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼4-Chlorotoluene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼cis-1,2-Dichloroethene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼cis-1,3-Dichloropropene ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2-Dibromo-3-Chloropropane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2-Dibromoethane (EDB)ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Dibromomethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2-Dichlorobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,3-Dichlorobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,4-Dichlorobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Dichlorodifluoromethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,1-Dichloroethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2-Dichloroethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,1-Dichloroethene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2-Dichloroethene, Total ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2-Dichloropropane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,3-Dichloropropane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼2,2-Dichloropropane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,1-Dichloropropene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Diisopropyl ether ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Ethylbenzene ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Hexachlorobutadiene ND 0.0625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼2-Hexanone ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Isopropylbenzene ND 0.0125 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Methylene Chloride ND 0.0625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼4-Methyl-2-pentanone (MIBK)ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Methyl tert-butyl ether ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Naphthalene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼n-Butylbenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼N-Propylbenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼p-Isopropyltoluene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼sec-Butylbenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Styrene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼tert-Butylbenzene ND TestAmerica Nashville Page 22 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-4Client Sample ID: TP-5 (0-2) Matrix: SoilDate Collected: 06/22/15 14:20 Percent Solids: 81.6Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00250 mg/Kg ☼06/22/15 14:20 06/26/15 06:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,1,2,2-Tetrachloroethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Tetrachloroethene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Toluene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼trans-1,2-Dichloroethene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼trans-1,3-Dichloropropene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2,3-Trichlorobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2,4-Trichlorobenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,1,1-Trichloroethane ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,1,2-Trichloroethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Trichloroethene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Trichlorofluoromethane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2,3-Trichloropropane ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,2,4-Trimethylbenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼1,3,5-Trimethylbenzene ND 0.00250 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Vinyl chloride ND 0.00625 mg/Kg 06/22/15 14:20 06/26/15 06:09 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)96 70-130 06/22/15 14:20 06/26/15 06:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)106 06/22/15 14:20 06/26/15 06:09 170-130 1,2-Dichloroethane-d4 (Surr)115 06/22/15 14:20 06/26/15 06:09 170-130 Toluene-d8 (Surr)101 06/22/15 14:20 06/26/15 06:09 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0667 mg/Kg ☼06/26/15 09:17 06/28/15 12:57 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Acenaphthylene ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Anthracene 0.112 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Benzo[a]anthracene 0.326 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Benzo[a]pyrene 0.278 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Benzo[b]fluoranthene 0.343 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Benzo[g,h,i]perylene 0.162 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Benzo[k]fluoranthene 0.182 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Bis(2-chloroethoxy)methane ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Bis(2-chloroethyl)ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼bis (2-chloroisopropyl) ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Bis(2-ethylhexyl) phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4-Bromophenyl phenyl ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Butyl benzyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Carbazole ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4-Chloroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4-Chloro-3-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2-Chloronaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2-Chlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4-Chlorophenyl phenyl ether ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Chrysene 0.301 0.663 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Cresols ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Dibenz(a,h)anthracene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Dibenzofuran ND TestAmerica Nashville Page 23 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-4Client Sample ID: TP-5 (0-2) Matrix: SoilDate Collected: 06/22/15 14:20 Percent Solids: 81.6Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 0.332 mg/Kg ☼06/26/15 09:17 06/28/15 12:57 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼1,3-Dichlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼1,4-Dichlorobenzene ND 0.664 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼3,3'-Dichlorobenzidine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,4-Dichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Diethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,4-Dimethylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Dimethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Di-n-butyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4,6-Dinitro-2-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,4-Dinitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,4-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,6-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Di-n-octyl phthalate ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Fluoranthene 0.707 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Fluorene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Hexachlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Hexachlorobutadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Hexachlorocyclopentadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Hexachloroethane ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Indeno[1,2,3-cd]pyrene 0.142 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Isophorone ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼1-Methylnaphthalene ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2-Methylnaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2-Methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼3 & 4 Methylphenol ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Naphthalene ND 0.829 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2-Nitroaniline ND 0.829 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼3-Nitroaniline ND 0.829 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4-Nitroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Nitrobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼4-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼N-Nitrosodi-n-propylamine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.829 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Pentachlorophenol ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Phenanthrene 0.392 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Phenol ND 0.0667 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼Pyrene 0.626 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼1,2,4-Trichlorobenzene ND 0.829 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,4,5-Trichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 12:57 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)67 29-120 06/26/15 09:17 06/28/15 12:57 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)57 06/26/15 09:17 06/28/15 12:57 110-120 Nitrobenzene-d5 (Surr)60 06/26/15 09:17 06/28/15 12:57 127-120 Phenol-d5 (Surr)69 06/26/15 09:17 06/28/15 12:57 110-120 Terphenyl-d14 (Surr)82 06/26/15 09:17 06/28/15 12:57 113-120 TestAmerica Nashville Page 24 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-4Client Sample ID: TP-5 (0-2) Matrix: SoilDate Collected: 06/22/15 14:20 Percent Solids: 81.6Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)60 10-120 06/26/15 09:17 06/28/15 12:57 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.1 mg/Kg ☼06/25/15 08:59 06/25/15 15:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.42 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Arsenic ND 1.21 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Beryllium ND 1.21 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Cadmium ND 1.21 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Chromium 18.2 2.42 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Copper 17.9 1.21 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Lead 7.09 3.63 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Manganese 189 2.42 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Nickel 8.06 2.42 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Selenium ND 1.21 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Silver ND 2.42 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Thallium ND 12.1 mg/Kg 06/25/15 08:59 06/25/15 15:47 1☼Zinc 55.1 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.122 mg/Kg ☼06/24/15 16:44 06/26/15 11:05 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.01 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 25 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-5Client Sample ID: TP-6 (0-2) Matrix: SoilDate Collected: 06/22/15 15:10 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 86 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 26 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-5Client Sample ID: TP-6 (0-2) Matrix: SoilDate Collected: 06/22/15 15:10 Percent Solids: 86.1Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.0470 0.0405 mg/Kg ☼06/22/15 15:10 06/26/15 06:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Benzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Bromobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Bromochloromethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Bromodichloromethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Bromoform ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Bromomethane ND 0.0405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼2-Butanone (MEK)ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Carbon disulfide 0.00454 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Carbon tetrachloride ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Chlorobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Chlorodibromomethane ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Chloroethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Chloroform ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Chloromethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼2-Chlorotoluene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼4-Chlorotoluene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼cis-1,2-Dichloroethene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼cis-1,3-Dichloropropene ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2-Dibromo-3-Chloropropane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2-Dibromoethane (EDB)ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Dibromomethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2-Dichlorobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,3-Dichlorobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,4-Dichlorobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Dichlorodifluoromethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,1-Dichloroethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2-Dichloroethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,1-Dichloroethene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2-Dichloroethene, Total ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2-Dichloropropane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,3-Dichloropropane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼2,2-Dichloropropane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,1-Dichloropropene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Diisopropyl ether ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Ethylbenzene ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Hexachlorobutadiene ND 0.0405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼2-Hexanone ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Isopropylbenzene ND 0.00810 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Methylene Chloride ND 0.0405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼4-Methyl-2-pentanone (MIBK)ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Methyl tert-butyl ether ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Naphthalene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼n-Butylbenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼N-Propylbenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼p-Isopropyltoluene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼sec-Butylbenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Styrene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼tert-Butylbenzene ND TestAmerica Nashville Page 27 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-5Client Sample ID: TP-6 (0-2) Matrix: SoilDate Collected: 06/22/15 15:10 Percent Solids: 86.1Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00162 mg/Kg ☼06/22/15 15:10 06/26/15 06:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,1,2,2-Tetrachloroethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Tetrachloroethene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Toluene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼trans-1,2-Dichloroethene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼trans-1,3-Dichloropropene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2,3-Trichlorobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2,4-Trichlorobenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,1,1-Trichloroethane ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,1,2-Trichloroethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Trichloroethene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Trichlorofluoromethane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2,3-Trichloropropane ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,2,4-Trimethylbenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼1,3,5-Trimethylbenzene ND 0.00162 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Vinyl chloride ND 0.00405 mg/Kg 06/22/15 15:10 06/26/15 06:39 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)96 70-130 06/22/15 15:10 06/26/15 06:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 06/22/15 15:10 06/26/15 06:39 170-130 1,2-Dichloroethane-d4 (Surr)111 06/22/15 15:10 06/26/15 06:39 170-130 Toluene-d8 (Surr)101 06/22/15 15:10 06/26/15 06:39 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.334 mg/Kg ☼06/26/15 09:17 06/28/15 13:21 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Acenaphthylene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Anthracene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Benzo[a]anthracene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Benzo[a]pyrene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Benzo[b]fluoranthene 0.385 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Benzo[g,h,i]perylene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Benzo[k]fluoranthene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Bis(2-chloroethoxy)methane ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Bis(2-chloroethyl)ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼bis (2-chloroisopropyl) ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Bis(2-ethylhexyl) phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4-Bromophenyl phenyl ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Butyl benzyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Carbazole ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4-Chloroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4-Chloro-3-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2-Chloronaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2-Chlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4-Chlorophenyl phenyl ether ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Chrysene ND 3.32 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Cresols ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Dibenz(a,h)anthracene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Dibenzofuran ND TestAmerica Nashville Page 28 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-5Client Sample ID: TP-6 (0-2) Matrix: SoilDate Collected: 06/22/15 15:10 Percent Solids: 86.1Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.66 mg/Kg ☼06/26/15 09:17 06/28/15 13:21 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼1,3-Dichlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼1,4-Dichlorobenzene ND 3.32 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼3,3'-Dichlorobenzidine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,4-Dichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Diethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,4-Dimethylphenol ND 8.32 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Dimethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Di-n-butyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4,6-Dinitro-2-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,4-Dinitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,4-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,6-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Di-n-octyl phthalate ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Fluoranthene 0.355 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Fluorene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Hexachlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Hexachlorobutadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Hexachlorocyclopentadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Hexachloroethane ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Indeno[1,2,3-cd]pyrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Isophorone ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼1-Methylnaphthalene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2-Methylnaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2-Methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼3 & 4 Methylphenol ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Naphthalene ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2-Nitroaniline ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼3-Nitroaniline ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4-Nitroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Nitrobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼4-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼N-Nitrosodi-n-propylamine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Pentachlorophenol ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Phenanthrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Phenol ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼Pyrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼1,2,4-Trichlorobenzene ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,4,5-Trichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 13:21 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)91 29-120 06/26/15 09:17 06/28/15 13:21 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)95 06/26/15 09:17 06/28/15 13:21 510-120 Nitrobenzene-d5 (Surr)84 06/26/15 09:17 06/28/15 13:21 527-120 Phenol-d5 (Surr)100 06/26/15 09:17 06/28/15 13:21 510-120 Terphenyl-d14 (Surr)106 06/26/15 09:17 06/28/15 13:21 513-120 TestAmerica Nashville Page 29 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-5Client Sample ID: TP-6 (0-2) Matrix: SoilDate Collected: 06/22/15 15:10 Percent Solids: 86.1Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)103 10-120 06/26/15 09:17 06/28/15 13:21 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.6 mg/Kg ☼06/25/15 08:59 06/25/15 15:52 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.32 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Arsenic 40.3 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Beryllium ND 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Cadmium ND 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Chromium 17.2 2.32 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Copper 19.2 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Lead 26.3 3.48 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Manganese 203 2.32 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Nickel 7.46 2.32 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Selenium ND 1.16 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Silver ND 2.32 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Thallium ND 11.6 mg/Kg 06/25/15 08:59 06/25/15 15:52 1☼Zinc 55.9 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury 0.155 0.114 mg/Kg ☼06/24/15 16:44 06/26/15 11:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.61 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 30 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-6Client Sample ID: TP-6 (8-10) Matrix: SoilDate Collected: 06/22/15 15:15 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 79 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 31 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-6Client Sample ID: TP-6 (8-10) Matrix: SoilDate Collected: 06/22/15 15:15 Percent Solids: 79.2Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0461 mg/Kg ☼06/22/15 15:15 06/26/15 07:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Benzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Bromobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Bromochloromethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Bromodichloromethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Bromoform ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Bromomethane ND 0.0461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼2-Butanone (MEK)ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Carbon disulfide ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Carbon tetrachloride ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Chlorobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Chlorodibromomethane ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Chloroethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Chloroform ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Chloromethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼2-Chlorotoluene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼4-Chlorotoluene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼cis-1,2-Dichloroethene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼cis-1,3-Dichloropropene ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2-Dibromo-3-Chloropropane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2-Dibromoethane (EDB)ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Dibromomethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2-Dichlorobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,3-Dichlorobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,4-Dichlorobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Dichlorodifluoromethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,1-Dichloroethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2-Dichloroethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,1-Dichloroethene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2-Dichloroethene, Total ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2-Dichloropropane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,3-Dichloropropane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼2,2-Dichloropropane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,1-Dichloropropene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Diisopropyl ether ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Ethylbenzene ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Hexachlorobutadiene ND 0.0461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼2-Hexanone ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Isopropylbenzene ND 0.00923 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Methylene Chloride ND 0.0461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼4-Methyl-2-pentanone (MIBK)ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Methyl tert-butyl ether ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Naphthalene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼n-Butylbenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼N-Propylbenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼p-Isopropyltoluene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼sec-Butylbenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Styrene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼tert-Butylbenzene ND TestAmerica Nashville Page 32 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-6Client Sample ID: TP-6 (8-10) Matrix: SoilDate Collected: 06/22/15 15:15 Percent Solids: 79.2Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00185 mg/Kg ☼06/22/15 15:15 06/26/15 07:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,1,2,2-Tetrachloroethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Tetrachloroethene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Toluene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼trans-1,2-Dichloroethene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼trans-1,3-Dichloropropene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2,3-Trichlorobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2,4-Trichlorobenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,1,1-Trichloroethane ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,1,2-Trichloroethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Trichloroethene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Trichlorofluoromethane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2,3-Trichloropropane ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,2,4-Trimethylbenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼1,3,5-Trimethylbenzene ND 0.00185 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Vinyl chloride ND 0.00461 mg/Kg 06/22/15 15:15 06/26/15 07:08 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)97 70-130 06/22/15 15:15 06/26/15 07:08 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)106 06/22/15 15:15 06/26/15 07:08 170-130 1,2-Dichloroethane-d4 (Surr)114 06/22/15 15:15 06/26/15 07:08 170-130 Toluene-d8 (Surr)99 06/22/15 15:15 06/26/15 07:08 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0668 mg/Kg ☼06/26/15 09:17 06/28/15 13:45 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Acenaphthylene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Anthracene 0.0814 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Benzo[a]anthracene 0.282 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Benzo[a]pyrene 0.259 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Benzo[b]fluoranthene 0.349 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Benzo[g,h,i]perylene 0.149 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Benzo[k]fluoranthene 0.122 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Bis(2-chloroethoxy)methane ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Bis(2-chloroethyl)ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼bis (2-chloroisopropyl) ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Bis(2-ethylhexyl) phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4-Bromophenyl phenyl ether ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Butyl benzyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Carbazole ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4-Chloroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4-Chloro-3-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2-Chloronaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2-Chlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4-Chlorophenyl phenyl ether ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Chrysene 0.282 0.664 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Cresols ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Dibenz(a,h)anthracene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Dibenzofuran ND TestAmerica Nashville Page 33 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-6Client Sample ID: TP-6 (8-10) Matrix: SoilDate Collected: 06/22/15 15:15 Percent Solids: 79.2Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 0.332 mg/Kg ☼06/26/15 09:17 06/28/15 13:45 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼1,3-Dichlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼1,4-Dichlorobenzene ND 0.665 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼3,3'-Dichlorobenzidine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,4-Dichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Diethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,4-Dimethylphenol ND 1.67 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Dimethyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Di-n-butyl phthalate ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4,6-Dinitro-2-methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,4-Dinitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,4-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,6-Dinitrotoluene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Di-n-octyl phthalate ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Fluoranthene 0.593 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Fluorene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Hexachlorobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Hexachlorobutadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Hexachlorocyclopentadiene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Hexachloroethane ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Indeno[1,2,3-cd]pyrene 0.132 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Isophorone ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼1-Methylnaphthalene ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2-Methylnaphthalene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2-Methylphenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼3 & 4 Methylphenol ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Naphthalene ND 0.831 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2-Nitroaniline ND 0.831 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼3-Nitroaniline ND 0.831 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4-Nitroaniline ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Nitrobenzene ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼4-Nitrophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼N-Nitrosodi-n-propylamine ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.831 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Pentachlorophenol ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Phenanthrene 0.354 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Phenol ND 0.0668 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼Pyrene 0.527 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼1,2,4-Trichlorobenzene ND 0.831 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,4,5-Trichlorophenol ND 0.332 mg/Kg 06/26/15 09:17 06/28/15 13:45 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)72 29-120 06/26/15 09:17 06/28/15 13:45 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)74 06/26/15 09:17 06/28/15 13:45 110-120 Nitrobenzene-d5 (Surr)67 06/26/15 09:17 06/28/15 13:45 127-120 Phenol-d5 (Surr)78 06/26/15 09:17 06/28/15 13:45 110-120 Terphenyl-d14 (Surr)82 06/26/15 09:17 06/28/15 13:45 113-120 TestAmerica Nashville Page 34 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-6Client Sample ID: TP-6 (8-10) Matrix: SoilDate Collected: 06/22/15 15:15 Percent Solids: 79.2Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)72 10-120 06/26/15 09:17 06/28/15 13:45 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.8 mg/Kg ☼06/25/15 08:59 06/25/15 15:56 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Arsenic 3.25 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Beryllium ND 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Cadmium ND 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Chromium 27.8 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Copper 35.2 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Lead 89.0 3.84 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Manganese 165 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Nickel 8.41 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Selenium ND 1.28 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Silver ND 2.56 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Thallium ND 12.8 mg/Kg 06/25/15 08:59 06/25/15 15:56 1☼Zinc 78.6 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury 0.190 0.123 mg/Kg ☼06/24/15 16:44 06/26/15 11:10 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.19 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 35 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-7Client Sample ID: TP-7 (0-2) Matrix: SoilDate Collected: 06/22/15 15:45 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 81 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 36 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-7Client Sample ID: TP-7 (0-2) Matrix: SoilDate Collected: 06/22/15 15:45 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0522 mg/Kg ☼06/22/15 15:45 06/26/15 07:38 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Benzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Bromobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Bromochloromethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Bromodichloromethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Bromoform ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Bromomethane ND 0.0522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼2-Butanone (MEK)ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Carbon disulfide ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Carbon tetrachloride ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Chlorobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Chlorodibromomethane ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Chloroethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Chloroform ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Chloromethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼2-Chlorotoluene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼4-Chlorotoluene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼cis-1,2-Dichloroethene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼cis-1,3-Dichloropropene ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2-Dibromo-3-Chloropropane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2-Dibromoethane (EDB)ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Dibromomethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2-Dichlorobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,3-Dichlorobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,4-Dichlorobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Dichlorodifluoromethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,1-Dichloroethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2-Dichloroethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,1-Dichloroethene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2-Dichloroethene, Total ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2-Dichloropropane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,3-Dichloropropane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼2,2-Dichloropropane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,1-Dichloropropene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Diisopropyl ether ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Ethylbenzene ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Hexachlorobutadiene ND 0.0522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼2-Hexanone ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Isopropylbenzene ND 0.0104 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Methylene Chloride ND 0.0522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼4-Methyl-2-pentanone (MIBK)ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Methyl tert-butyl ether ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Naphthalene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼n-Butylbenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼N-Propylbenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼p-Isopropyltoluene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼sec-Butylbenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Styrene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼tert-Butylbenzene ND TestAmerica Nashville Page 37 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-7Client Sample ID: TP-7 (0-2) Matrix: SoilDate Collected: 06/22/15 15:45 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00209 mg/Kg ☼06/22/15 15:45 06/26/15 07:38 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,1,2,2-Tetrachloroethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Tetrachloroethene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Toluene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼trans-1,2-Dichloroethene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼trans-1,3-Dichloropropene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2,3-Trichlorobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2,4-Trichlorobenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,1,1-Trichloroethane ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,1,2-Trichloroethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Trichloroethene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Trichlorofluoromethane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2,3-Trichloropropane ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,2,4-Trimethylbenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼1,3,5-Trimethylbenzene ND 0.00209 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Vinyl chloride ND 0.00522 mg/Kg 06/22/15 15:45 06/26/15 07:38 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)96 70-130 06/22/15 15:45 06/26/15 07:38 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)107 06/22/15 15:45 06/26/15 07:38 170-130 1,2-Dichloroethane-d4 (Surr)113 06/22/15 15:45 06/26/15 07:38 170-130 Toluene-d8 (Surr)99 06/22/15 15:45 06/26/15 07:38 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene 1.29 0.334 mg/Kg ☼06/26/15 09:17 06/28/15 14:09 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Acenaphthylene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Anthracene 2.38 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Benzo[a]anthracene 7.21 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Benzo[a]pyrene 6.51 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Benzo[b]fluoranthene 8.72 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Benzo[g,h,i]perylene 3.51 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Benzo[k]fluoranthene 3.31 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Bis(2-chloroethoxy)methane ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Bis(2-chloroethyl)ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼bis (2-chloroisopropyl) ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Bis(2-ethylhexyl) phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4-Bromophenyl phenyl ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Butyl benzyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Carbazole ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4-Chloroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4-Chloro-3-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2-Chloronaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2-Chlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4-Chlorophenyl phenyl ether ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Chrysene 6.81 3.32 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Cresols ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Dibenz(a,h)anthracene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Dibenzofuran ND TestAmerica Nashville Page 38 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-7Client Sample ID: TP-7 (0-2) Matrix: SoilDate Collected: 06/22/15 15:45 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.66 mg/Kg ☼06/26/15 09:17 06/28/15 14:09 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼1,3-Dichlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼1,4-Dichlorobenzene ND 3.32 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼3,3'-Dichlorobenzidine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,4-Dichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Diethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,4-Dimethylphenol ND 8.32 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Dimethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Di-n-butyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4,6-Dinitro-2-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,4-Dinitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,4-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,6-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Di-n-octyl phthalate ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Fluoranthene 14.8 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Fluorene 0.672 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Hexachlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Hexachlorobutadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Hexachlorocyclopentadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Hexachloroethane ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Indeno[1,2,3-cd]pyrene 3.12 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Isophorone ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼1-Methylnaphthalene ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2-Methylnaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2-Methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼3 & 4 Methylphenol ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Naphthalene ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2-Nitroaniline ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼3-Nitroaniline ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4-Nitroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Nitrobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼4-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼N-Nitrosodi-n-propylamine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Pentachlorophenol ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Phenanthrene 7.69 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Phenol ND 0.334 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼Pyrene 12.6 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼1,2,4-Trichlorobenzene ND 4.15 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,4,5-Trichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:09 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)84 29-120 06/26/15 09:17 06/28/15 14:09 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)81 06/26/15 09:17 06/28/15 14:09 510-120 Nitrobenzene-d5 (Surr)76 06/26/15 09:17 06/28/15 14:09 527-120 Phenol-d5 (Surr)86 06/26/15 09:17 06/28/15 14:09 510-120 Terphenyl-d14 (Surr)95 06/26/15 09:17 06/28/15 14:09 513-120 TestAmerica Nashville Page 39 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-7Client Sample ID: TP-7 (0-2) Matrix: SoilDate Collected: 06/22/15 15:45 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)90 10-120 06/26/15 09:17 06/28/15 14:09 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.8 mg/Kg ☼06/25/15 08:59 06/25/15 16:00 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.36 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Arsenic 3.63 1.18 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Beryllium ND 1.18 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Cadmium ND 1.18 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Chromium 38.7 2.36 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Copper 31.1 1.18 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Lead 29.9 3.53 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Manganese 582 2.36 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Nickel 14.5 2.36 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Selenium ND 1.18 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Silver ND 2.36 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Thallium ND 11.8 mg/Kg 06/25/15 08:59 06/25/15 16:00 1☼Zinc 78.9 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.120 mg/Kg ☼06/24/15 16:44 06/26/15 11:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.16 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 40 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-8Client Sample ID: TP-9 (8-10) Matrix: SoilDate Collected: 06/22/15 16:25 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 76 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 41 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-8Client Sample ID: TP-9 (8-10) Matrix: SoilDate Collected: 06/22/15 16:25 Percent Solids: 76.0Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0527 mg/Kg ☼06/22/15 16:25 06/26/15 08:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Benzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Bromobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Bromochloromethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Bromodichloromethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Bromoform ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Bromomethane ND 0.0527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼2-Butanone (MEK)ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Carbon disulfide 0.0516 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Carbon tetrachloride ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Chlorobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Chlorodibromomethane ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Chloroethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Chloroform ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Chloromethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼2-Chlorotoluene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼4-Chlorotoluene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼cis-1,2-Dichloroethene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼cis-1,3-Dichloropropene ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2-Dibromo-3-Chloropropane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2-Dibromoethane (EDB)ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Dibromomethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2-Dichlorobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,3-Dichlorobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,4-Dichlorobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Dichlorodifluoromethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,1-Dichloroethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2-Dichloroethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,1-Dichloroethene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2-Dichloroethene, Total ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2-Dichloropropane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,3-Dichloropropane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼2,2-Dichloropropane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,1-Dichloropropene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Diisopropyl ether ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Ethylbenzene ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Hexachlorobutadiene ND 0.0527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼2-Hexanone ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Isopropylbenzene ND 0.0105 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Methylene Chloride ND 0.0527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼4-Methyl-2-pentanone (MIBK)ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Methyl tert-butyl ether ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Naphthalene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼n-Butylbenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼N-Propylbenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼p-Isopropyltoluene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼sec-Butylbenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Styrene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼tert-Butylbenzene ND TestAmerica Nashville Page 42 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-8Client Sample ID: TP-9 (8-10) Matrix: SoilDate Collected: 06/22/15 16:25 Percent Solids: 76.0Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00211 mg/Kg ☼06/22/15 16:25 06/26/15 08:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,1,2,2-Tetrachloroethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Tetrachloroethene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Toluene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼trans-1,2-Dichloroethene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼trans-1,3-Dichloropropene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2,3-Trichlorobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2,4-Trichlorobenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,1,1-Trichloroethane ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,1,2-Trichloroethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Trichloroethene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Trichlorofluoromethane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2,3-Trichloropropane ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,2,4-Trimethylbenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼1,3,5-Trimethylbenzene ND 0.00211 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Vinyl chloride ND 0.00527 mg/Kg 06/22/15 16:25 06/26/15 08:09 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)92 70-130 06/22/15 16:25 06/26/15 08:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)109 06/22/15 16:25 06/26/15 08:09 170-130 1,2-Dichloroethane-d4 (Surr)112 06/22/15 16:25 06/26/15 08:09 170-130 Toluene-d8 (Surr)100 06/22/15 16:25 06/26/15 08:09 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0666 mg/Kg ☼06/26/15 09:17 06/28/15 14:33 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Acenaphthylene ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Anthracene ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Benzo[a]anthracene 0.190 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Benzo[a]pyrene 0.155 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Benzo[b]fluoranthene 0.190 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Benzo[g,h,i]perylene 0.0892 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Benzo[k]fluoranthene 0.105 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Bis(2-chloroethoxy)methane ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Bis(2-chloroethyl)ether ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼bis (2-chloroisopropyl) ether ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Bis(2-ethylhexyl) phthalate ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4-Bromophenyl phenyl ether ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Butyl benzyl phthalate ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Carbazole ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4-Chloroaniline ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4-Chloro-3-methylphenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2-Chloronaphthalene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2-Chlorophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4-Chlorophenyl phenyl ether ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Chrysene 0.177 0.662 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Cresols ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Dibenz(a,h)anthracene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Dibenzofuran ND TestAmerica Nashville Page 43 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-8Client Sample ID: TP-9 (8-10) Matrix: SoilDate Collected: 06/22/15 16:25 Percent Solids: 76.0Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 0.331 mg/Kg ☼06/26/15 09:17 06/28/15 14:33 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼1,3-Dichlorobenzene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼1,4-Dichlorobenzene ND 0.663 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼3,3'-Dichlorobenzidine ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,4-Dichlorophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Diethyl phthalate ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,4-Dimethylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Dimethyl phthalate ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Di-n-butyl phthalate ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4,6-Dinitro-2-methylphenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,4-Dinitrophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,4-Dinitrotoluene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,6-Dinitrotoluene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Di-n-octyl phthalate ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Fluoranthene 0.354 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Fluorene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Hexachlorobenzene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Hexachlorobutadiene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Hexachlorocyclopentadiene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Hexachloroethane ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Indeno[1,2,3-cd]pyrene 0.0736 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Isophorone ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼1-Methylnaphthalene ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2-Methylnaphthalene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2-Methylphenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼3 & 4 Methylphenol ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Naphthalene ND 0.828 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2-Nitroaniline ND 0.828 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼3-Nitroaniline ND 0.828 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4-Nitroaniline ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Nitrobenzene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2-Nitrophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼4-Nitrophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼N-Nitrosodi-n-propylamine ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.828 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Pentachlorophenol ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Phenanthrene 0.210 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Phenol ND 0.0666 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼Pyrene 0.314 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼1,2,4-Trichlorobenzene ND 0.828 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,4,5-Trichlorophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 14:33 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)79 29-120 06/26/15 09:17 06/28/15 14:33 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)83 06/26/15 09:17 06/28/15 14:33 110-120 Nitrobenzene-d5 (Surr)76 06/26/15 09:17 06/28/15 14:33 127-120 Phenol-d5 (Surr)89 06/26/15 09:17 06/28/15 14:33 110-120 Terphenyl-d14 (Surr)92 06/26/15 09:17 06/28/15 14:33 113-120 TestAmerica Nashville Page 44 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-8Client Sample ID: TP-9 (8-10) Matrix: SoilDate Collected: 06/22/15 16:25 Percent Solids: 76.0Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)83 10-120 06/26/15 09:17 06/28/15 14:33 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 13.1 mg/Kg ☼06/25/15 08:59 06/25/15 16:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.62 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Arsenic 3.61 1.31 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Beryllium ND 1.31 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Cadmium ND 1.31 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Chromium 22.9 2.62 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Copper 22.4 1.31 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Lead 143 3.93 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Manganese 339 2.62 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Nickel 8.01 2.62 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Selenium ND 1.31 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Silver ND 2.62 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Thallium ND 13.1 mg/Kg 06/25/15 08:59 06/25/15 16:04 1☼Zinc 172 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.130 mg/Kg ☼06/24/15 16:44 06/26/15 11:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.40 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 45 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-9Client Sample ID: TP-11 (6-13) Matrix: SoilDate Collected: 06/22/15 16:45 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 69 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry - Soluble RL RL pH 13.0 0.100 SU 06/27/15 10:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.100 Degrees C 06/27/15 10:08 1Temperature21.7 TestAmerica Nashville Page 46 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-10Client Sample ID: TP-12 (0-2) Matrix: SoilDate Collected: 06/23/15 09:30 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 78 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 47 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-10Client Sample ID: TP-12 (0-2) Matrix: SoilDate Collected: 06/23/15 09:30 Percent Solids: 78.0Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.0568 0.0507 mg/Kg ☼06/23/15 09:30 06/26/15 08:40 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Benzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Bromobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Bromochloromethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Bromodichloromethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Bromoform ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Bromomethane ND 0.0507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼2-Butanone (MEK)ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Carbon disulfide ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Carbon tetrachloride ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Chlorobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Chlorodibromomethane ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Chloroethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Chloroform ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Chloromethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼2-Chlorotoluene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼4-Chlorotoluene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼cis-1,2-Dichloroethene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼cis-1,3-Dichloropropene ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2-Dibromo-3-Chloropropane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2-Dibromoethane (EDB)ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Dibromomethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2-Dichlorobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,3-Dichlorobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,4-Dichlorobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Dichlorodifluoromethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,1-Dichloroethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2-Dichloroethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,1-Dichloroethene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2-Dichloroethene, Total ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2-Dichloropropane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,3-Dichloropropane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼2,2-Dichloropropane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,1-Dichloropropene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Diisopropyl ether ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Ethylbenzene ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Hexachlorobutadiene ND 0.0507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼2-Hexanone ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Isopropylbenzene ND 0.0101 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Methylene Chloride ND 0.0507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼4-Methyl-2-pentanone (MIBK)ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Methyl tert-butyl ether ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Naphthalene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼n-Butylbenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼N-Propylbenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼p-Isopropyltoluene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼sec-Butylbenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Styrene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼tert-Butylbenzene ND TestAmerica Nashville Page 48 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-10Client Sample ID: TP-12 (0-2) Matrix: SoilDate Collected: 06/23/15 09:30 Percent Solids: 78.0Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00203 mg/Kg ☼06/23/15 09:30 06/26/15 08:40 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,1,2,2-Tetrachloroethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Tetrachloroethene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Toluene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼trans-1,2-Dichloroethene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼trans-1,3-Dichloropropene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2,3-Trichlorobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2,4-Trichlorobenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,1,1-Trichloroethane ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,1,2-Trichloroethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Trichloroethene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Trichlorofluoromethane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2,3-Trichloropropane ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,2,4-Trimethylbenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼1,3,5-Trimethylbenzene ND 0.00203 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Vinyl chloride ND 0.00507 mg/Kg 06/23/15 09:30 06/26/15 08:40 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)98 70-130 06/23/15 09:30 06/26/15 08:40 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)110 06/23/15 09:30 06/26/15 08:40 170-130 1,2-Dichloroethane-d4 (Surr)112 06/23/15 09:30 06/26/15 08:40 170-130 Toluene-d8 (Surr)101 06/23/15 09:30 06/26/15 08:40 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.333 mg/Kg ☼06/26/15 09:17 06/28/15 14:57 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Acenaphthylene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Benzo[a]anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Benzo[a]pyrene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Benzo[b]fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Benzo[g,h,i]perylene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Benzo[k]fluoranthene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Bis(2-chloroethoxy)methane ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Bis(2-chloroethyl)ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼bis (2-chloroisopropyl) ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Bis(2-ethylhexyl) phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4-Bromophenyl phenyl ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Butyl benzyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Carbazole ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4-Chloroaniline ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4-Chloro-3-methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2-Chloronaphthalene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2-Chlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4-Chlorophenyl phenyl ether ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Chrysene ND 3.31 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Cresols ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Dibenz(a,h)anthracene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Dibenzofuran ND TestAmerica Nashville Page 49 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-10Client Sample ID: TP-12 (0-2) Matrix: SoilDate Collected: 06/23/15 09:30 Percent Solids: 78.0Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.65 mg/Kg ☼06/26/15 09:17 06/28/15 14:57 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼1,3-Dichlorobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼1,4-Dichlorobenzene ND 3.31 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼3,3'-Dichlorobenzidine ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,4-Dichlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Diethyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,4-Dimethylphenol ND 8.29 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Dimethyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Di-n-butyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4,6-Dinitro-2-methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,4-Dinitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,4-Dinitrotoluene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,6-Dinitrotoluene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Di-n-octyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Fluorene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Hexachlorobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Hexachlorobutadiene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Hexachlorocyclopentadiene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Hexachloroethane ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Indeno[1,2,3-cd]pyrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Isophorone ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼1-Methylnaphthalene ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2-Methylnaphthalene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2-Methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼3 & 4 Methylphenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Naphthalene ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2-Nitroaniline ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼3-Nitroaniline ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4-Nitroaniline ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Nitrobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2-Nitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼4-Nitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼N-Nitrosodi-n-propylamine ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Pentachlorophenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Phenanthrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Phenol ND 0.333 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼Pyrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼1,2,4-Trichlorobenzene ND 4.14 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,4,5-Trichlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 14:57 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)93 29-120 06/26/15 09:17 06/28/15 14:57 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)92 06/26/15 09:17 06/28/15 14:57 510-120 Nitrobenzene-d5 (Surr)83 06/26/15 09:17 06/28/15 14:57 527-120 Phenol-d5 (Surr)96 06/26/15 09:17 06/28/15 14:57 510-120 Terphenyl-d14 (Surr)108 06/26/15 09:17 06/28/15 14:57 513-120 TestAmerica Nashville Page 50 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-10Client Sample ID: TP-12 (0-2) Matrix: SoilDate Collected: 06/23/15 09:30 Percent Solids: 78.0Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)103 10-120 06/26/15 09:17 06/28/15 14:57 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.9 mg/Kg ☼06/25/15 08:59 06/25/15 16:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.57 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Arsenic 2.60 1.29 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Beryllium ND 1.29 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Cadmium ND 1.29 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Chromium 17.8 2.57 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Copper 35.6 1.29 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Lead 12.6 3.86 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Manganese 323 2.57 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Nickel 7.95 2.57 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Selenium ND 1.29 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Silver ND 2.57 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Thallium ND 12.9 mg/Kg 06/25/15 08:59 06/25/15 16:09 1☼Zinc 71.0 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.127 mg/Kg ☼06/24/15 16:44 06/26/15 11:17 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *6.31 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 51 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-11Client Sample ID: TP-13 (0-2) Matrix: SoilDate Collected: 06/23/15 10:15 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 87 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 52 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-11Client Sample ID: TP-13 (0-2) Matrix: SoilDate Collected: 06/23/15 10:15 Percent Solids: 87.1Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0461 mg/Kg ☼06/23/15 10:15 06/26/15 09:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Benzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Bromobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Bromochloromethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Bromodichloromethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Bromoform ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Bromomethane ND 0.0461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼2-Butanone (MEK)ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Carbon disulfide ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Carbon tetrachloride ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Chlorobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Chlorodibromomethane ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Chloroethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Chloroform ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Chloromethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼2-Chlorotoluene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼4-Chlorotoluene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼cis-1,2-Dichloroethene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼cis-1,3-Dichloropropene ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2-Dibromo-3-Chloropropane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2-Dibromoethane (EDB)ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Dibromomethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2-Dichlorobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,3-Dichlorobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,4-Dichlorobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Dichlorodifluoromethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,1-Dichloroethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2-Dichloroethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,1-Dichloroethene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2-Dichloroethene, Total ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2-Dichloropropane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,3-Dichloropropane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼2,2-Dichloropropane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,1-Dichloropropene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Diisopropyl ether ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Ethylbenzene ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Hexachlorobutadiene ND 0.0461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼2-Hexanone ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Isopropylbenzene ND 0.00921 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Methylene Chloride ND 0.0461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼4-Methyl-2-pentanone (MIBK)ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Methyl tert-butyl ether ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Naphthalene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼n-Butylbenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼N-Propylbenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼p-Isopropyltoluene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼sec-Butylbenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Styrene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼tert-Butylbenzene ND TestAmerica Nashville Page 53 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-11Client Sample ID: TP-13 (0-2) Matrix: SoilDate Collected: 06/23/15 10:15 Percent Solids: 87.1Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00184 mg/Kg ☼06/23/15 10:15 06/26/15 09:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,1,2,2-Tetrachloroethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Tetrachloroethene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Toluene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼trans-1,2-Dichloroethene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼trans-1,3-Dichloropropene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2,3-Trichlorobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2,4-Trichlorobenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,1,1-Trichloroethane ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,1,2-Trichloroethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Trichloroethene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Trichlorofluoromethane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2,3-Trichloropropane ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,2,4-Trimethylbenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼1,3,5-Trimethylbenzene ND 0.00184 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Vinyl chloride ND 0.00461 mg/Kg 06/23/15 10:15 06/26/15 09:09 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)94 70-130 06/23/15 10:15 06/26/15 09:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)106 06/23/15 10:15 06/26/15 09:09 170-130 1,2-Dichloroethane-d4 (Surr)115 06/23/15 10:15 06/26/15 09:09 170-130 Toluene-d8 (Surr)104 06/23/15 10:15 06/26/15 09:09 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.335 mg/Kg ☼06/26/15 09:17 06/28/15 15:21 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Acenaphthylene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Anthracene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Benzo[a]anthracene 0.446 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Benzo[a]pyrene 0.419 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Benzo[b]fluoranthene 0.602 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Benzo[g,h,i]perylene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Benzo[k]fluoranthene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Bis(2-chloroethoxy)methane ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Bis(2-chloroethyl)ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼bis (2-chloroisopropyl) ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Bis(2-ethylhexyl) phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4-Bromophenyl phenyl ether ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Butyl benzyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Carbazole ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4-Chloroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4-Chloro-3-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2-Chloronaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2-Chlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4-Chlorophenyl phenyl ether ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Chrysene 0.487 3.33 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Cresols ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Dibenz(a,h)anthracene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Dibenzofuran ND TestAmerica Nashville Page 54 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-11Client Sample ID: TP-13 (0-2) Matrix: SoilDate Collected: 06/23/15 10:15 Percent Solids: 87.1Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.66 mg/Kg ☼06/26/15 09:17 06/28/15 15:21 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼1,3-Dichlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼1,4-Dichlorobenzene ND 3.33 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼3,3'-Dichlorobenzidine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,4-Dichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Diethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,4-Dimethylphenol ND 8.34 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Dimethyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Di-n-butyl phthalate ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4,6-Dinitro-2-methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,4-Dinitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,4-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,6-Dinitrotoluene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Di-n-octyl phthalate ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Fluoranthene 0.873 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Fluorene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Hexachlorobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Hexachlorobutadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Hexachlorocyclopentadiene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Hexachloroethane ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Indeno[1,2,3-cd]pyrene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Isophorone ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼1-Methylnaphthalene ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2-Methylnaphthalene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2-Methylphenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼3 & 4 Methylphenol ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Naphthalene ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2-Nitroaniline ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼3-Nitroaniline ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4-Nitroaniline ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Nitrobenzene ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼4-Nitrophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼N-Nitrosodi-n-propylamine ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Pentachlorophenol ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Phenanthrene 0.529 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Phenol ND 0.335 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼Pyrene 0.733 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼1,2,4-Trichlorobenzene ND 4.16 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,4,5-Trichlorophenol ND 1.66 mg/Kg 06/26/15 09:17 06/28/15 15:21 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)68 29-120 06/26/15 09:17 06/28/15 15:21 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)62 06/26/15 09:17 06/28/15 15:21 510-120 Nitrobenzene-d5 (Surr)63 06/26/15 09:17 06/28/15 15:21 527-120 Phenol-d5 (Surr)68 06/26/15 09:17 06/28/15 15:21 510-120 Terphenyl-d14 (Surr)78 06/26/15 09:17 06/28/15 15:21 513-120 TestAmerica Nashville Page 55 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-11Client Sample ID: TP-13 (0-2) Matrix: SoilDate Collected: 06/23/15 10:15 Percent Solids: 87.1Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)73 10-120 06/26/15 09:17 06/28/15 15:21 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.4 mg/Kg ☼06/25/15 08:59 06/25/15 16:13 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.29 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Arsenic 3.54 1.14 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Beryllium ND 1.14 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Cadmium ND 1.14 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Chromium 30.5 2.29 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Copper 21.3 1.14 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Lead 32.4 3.43 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Manganese 875 2.29 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Nickel 10.1 2.29 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Selenium ND 1.14 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Silver ND 2.29 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Thallium ND 11.4 mg/Kg 06/25/15 08:59 06/25/15 16:13 1☼Zinc 104 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.113 mg/Kg ☼06/24/15 16:44 06/26/15 00:06 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.65 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 56 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-12Client Sample ID: TP-13 (10-11) Matrix: SoilDate Collected: 06/23/15 10:20 Date Received: 06/24/15 08:30 General Chemistry RL RL Percent Solids 81 0.10 %06/24/15 09:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 57 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-12Client Sample ID: TP-13 (10-11) Matrix: SoilDate Collected: 06/23/15 10:20 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.359 0.0620 mg/Kg ☼06/23/15 10:20 06/26/15 09:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Benzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Bromobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Bromochloromethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Bromodichloromethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Bromoform ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Bromomethane ND 0.0620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼2-Butanone (MEK)ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Carbon disulfide ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Carbon tetrachloride ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Chlorobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Chlorodibromomethane ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Chloroethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Chloroform ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Chloromethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼2-Chlorotoluene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼4-Chlorotoluene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼cis-1,2-Dichloroethene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼cis-1,3-Dichloropropene ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2-Dibromo-3-Chloropropane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2-Dibromoethane (EDB)ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Dibromomethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2-Dichlorobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,3-Dichlorobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,4-Dichlorobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Dichlorodifluoromethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,1-Dichloroethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2-Dichloroethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,1-Dichloroethene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2-Dichloroethene, Total ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2-Dichloropropane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,3-Dichloropropane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼2,2-Dichloropropane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,1-Dichloropropene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Diisopropyl ether ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Ethylbenzene ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Hexachlorobutadiene ND 0.0620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼2-Hexanone ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Isopropylbenzene ND 0.0124 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Methylene Chloride ND 0.0620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼4-Methyl-2-pentanone (MIBK)ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Methyl tert-butyl ether ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Naphthalene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼n-Butylbenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼N-Propylbenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼p-Isopropyltoluene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼sec-Butylbenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Styrene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼tert-Butylbenzene ND TestAmerica Nashville Page 58 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-12Client Sample ID: TP-13 (10-11) Matrix: SoilDate Collected: 06/23/15 10:20 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00248 mg/Kg ☼06/23/15 10:20 06/26/15 09:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,1,2,2-Tetrachloroethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Tetrachloroethene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Toluene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼trans-1,2-Dichloroethene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼trans-1,3-Dichloropropene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2,3-Trichlorobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2,4-Trichlorobenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,1,1-Trichloroethane ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,1,2-Trichloroethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Trichloroethene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Trichlorofluoromethane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2,3-Trichloropropane ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,2,4-Trimethylbenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼1,3,5-Trimethylbenzene ND 0.00248 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Vinyl chloride ND 0.00620 mg/Kg 06/23/15 10:20 06/26/15 09:39 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)98 70-130 06/23/15 10:20 06/26/15 09:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)109 06/23/15 10:20 06/26/15 09:39 170-130 1,2-Dichloroethane-d4 (Surr)115 06/23/15 10:20 06/26/15 09:39 170-130 Toluene-d8 (Surr)104 06/23/15 10:20 06/26/15 09:39 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.331 mg/Kg ☼06/26/15 09:17 06/28/15 15:44 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Acenaphthylene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Anthracene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Benzo[a]anthracene 0.512 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Benzo[a]pyrene 0.460 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Benzo[b]fluoranthene 0.624 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Benzo[g,h,i]perylene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Benzo[k]fluoranthene 0.331 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Bis(2-chloroethoxy)methane ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Bis(2-chloroethyl)ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼bis (2-chloroisopropyl) ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Bis(2-ethylhexyl) phthalate 8.00 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4-Bromophenyl phenyl ether ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Butyl benzyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Carbazole ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4-Chloroaniline ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4-Chloro-3-methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2-Chloronaphthalene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2-Chlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4-Chlorophenyl phenyl ether ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Chrysene 0.517 3.29 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Cresols ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Dibenz(a,h)anthracene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Dibenzofuran ND TestAmerica Nashville Page 59 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-12Client Sample ID: TP-13 (10-11) Matrix: SoilDate Collected: 06/23/15 10:20 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 1.65 mg/Kg ☼06/26/15 09:17 06/28/15 15:44 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼1,3-Dichlorobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼1,4-Dichlorobenzene ND 3.30 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼3,3'-Dichlorobenzidine ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,4-Dichlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Diethyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,4-Dimethylphenol ND 8.25 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Dimethyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Di-n-butyl phthalate ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4,6-Dinitro-2-methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,4-Dinitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,4-Dinitrotoluene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,6-Dinitrotoluene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Di-n-octyl phthalate ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Fluoranthene 1.09 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Fluorene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Hexachlorobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Hexachlorobutadiene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Hexachlorocyclopentadiene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Hexachloroethane ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Indeno[1,2,3-cd]pyrene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Isophorone ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼1-Methylnaphthalene ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2-Methylnaphthalene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2-Methylphenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼3 & 4 Methylphenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Naphthalene ND 4.12 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2-Nitroaniline ND 4.12 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼3-Nitroaniline ND 4.12 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4-Nitroaniline ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Nitrobenzene ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2-Nitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼4-Nitrophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼N-Nitrosodi-n-propylamine ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼n-Nitrosodiphenylamine(as diphenylamine) ND 4.12 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Pentachlorophenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Phenanthrene 0.760 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Phenol ND 0.331 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼Pyrene 0.902 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼1,2,4-Trichlorobenzene ND 4.12 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,4,5-Trichlorophenol ND 1.65 mg/Kg 06/26/15 09:17 06/28/15 15:44 5☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)97 29-120 06/26/15 09:17 06/28/15 15:44 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)92 06/26/15 09:17 06/28/15 15:44 510-120 Nitrobenzene-d5 (Surr)88 06/26/15 09:17 06/28/15 15:44 527-120 Phenol-d5 (Surr)98 06/26/15 09:17 06/28/15 15:44 510-120 Terphenyl-d14 (Surr)109 06/26/15 09:17 06/28/15 15:44 513-120 TestAmerica Nashville Page 60 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Lab Sample ID: 490-81215-12Client Sample ID: TP-13 (10-11) Matrix: SoilDate Collected: 06/23/15 10:20 Percent Solids: 80.9Date Received: 06/24/15 08:30 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)110 10-120 06/26/15 09:17 06/28/15 15:44 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 11.9 mg/Kg ☼06/25/15 08:59 06/25/15 16:17 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.38 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Arsenic 3.59 1.19 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Beryllium ND 1.19 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Cadmium ND 1.19 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Chromium 38.1 2.38 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Copper 20.6 1.19 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Lead 32.1 3.56 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Manganese 336 2.38 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Nickel 6.89 2.38 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Selenium ND 1.19 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Silver ND 2.38 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Thallium ND 11.9 mg/Kg 06/25/15 08:59 06/25/15 16:17 1☼Zinc 95.4 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.121 mg/Kg ☼06/24/15 16:44 06/26/15 00:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier General Chemistry RL MDL Chromium, hex ND *5.95 mg/Kg ☼06/29/15 16:57 07/01/15 18:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 61 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8260B - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-259533/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 RL MDL Acetone ND 0.0500 mg/Kg 06/26/15 01:36 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00200 mg/Kg 06/26/15 01:36 1Benzene ND 0.00200 mg/Kg 06/26/15 01:36 1Bromobenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Bromochloromethane ND 0.00200 mg/Kg 06/26/15 01:36 1Bromodichloromethane ND 0.00200 mg/Kg 06/26/15 01:36 1Bromoform ND 0.00200 mg/Kg 06/26/15 01:36 1Bromomethane ND 0.0500 mg/Kg 06/26/15 01:36 12-Butanone (MEK) ND 0.00500 mg/Kg 06/26/15 01:36 1Carbon disulfide ND 0.00200 mg/Kg 06/26/15 01:36 1Carbon tetrachloride ND 0.00200 mg/Kg 06/26/15 01:36 1Chlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Chlorodibromomethane ND 0.00500 mg/Kg 06/26/15 01:36 1Chloroethane ND 0.00200 mg/Kg 06/26/15 01:36 1Chloroform ND 0.00200 mg/Kg 06/26/15 01:36 1Chloromethane ND 0.00200 mg/Kg 06/26/15 01:36 12-Chlorotoluene ND 0.00200 mg/Kg 06/26/15 01:36 14-Chlorotoluene ND 0.00200 mg/Kg 06/26/15 01:36 1cis-1,2-Dichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1cis-1,3-Dichloropropene ND 0.00500 mg/Kg 06/26/15 01:36 11,2-Dibromo-3-Chloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 06/26/15 01:36 1Dibromomethane ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,3-Dichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,4-Dichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Dichlorodifluoromethane ND 0.00200 mg/Kg 06/26/15 01:36 11,1-Dichloroethane ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichloroethane ND 0.00200 mg/Kg 06/26/15 01:36 11,1-Dichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichloroethene, Total ND 0.00200 mg/Kg 06/26/15 01:36 11,2-Dichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,3-Dichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 12,2-Dichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,1-Dichloropropene ND 0.00200 mg/Kg 06/26/15 01:36 1Diisopropyl ether ND 0.00200 mg/Kg 06/26/15 01:36 1Ethylbenzene ND 0.00500 mg/Kg 06/26/15 01:36 1Hexachlorobutadiene ND 0.0500 mg/Kg 06/26/15 01:36 12-Hexanone ND 0.00200 mg/Kg 06/26/15 01:36 1Isopropylbenzene ND 0.0100 mg/Kg 06/26/15 01:36 1Methylene Chloride ND 0.0500 mg/Kg 06/26/15 01:36 14-Methyl-2-pentanone (MIBK) ND 0.00200 mg/Kg 06/26/15 01:36 1Methyl tert-butyl ether ND 0.00500 mg/Kg 06/26/15 01:36 1Naphthalene ND 0.00200 mg/Kg 06/26/15 01:36 1n-Butylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1N-Propylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1p-Isopropyltoluene ND 0.00200 mg/Kg 06/26/15 01:36 1sec-Butylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Styrene TestAmerica Nashville Page 62 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-259533/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 RL MDL tert-Butylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00200 mg/Kg 06/26/15 01:36 11,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 06/26/15 01:36 11,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 06/26/15 01:36 1Tetrachloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1Toluene ND 0.00200 mg/Kg 06/26/15 01:36 1trans-1,2-Dichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1trans-1,3-Dichloropropene ND 0.00200 mg/Kg 06/26/15 01:36 11,2,3-Trichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,2,4-Trichlorobenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,1,1-Trichloroethane ND 0.00500 mg/Kg 06/26/15 01:36 11,1,2-Trichloroethane ND 0.00200 mg/Kg 06/26/15 01:36 1Trichloroethene ND 0.00200 mg/Kg 06/26/15 01:36 1Trichlorofluoromethane ND 0.00200 mg/Kg 06/26/15 01:36 11,2,3-Trichloropropane ND 0.00200 mg/Kg 06/26/15 01:36 11,2,4-Trimethylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 11,3,5-Trimethylbenzene ND 0.00200 mg/Kg 06/26/15 01:36 1Vinyl chloride ND 0.00500 mg/Kg 06/26/15 01:36 1Xylenes, Total 4-Bromofluorobenzene (Surr)96 70-130 06/26/15 01:36 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 100 06/26/15 01:36 1Dibromofluoromethane (Surr)70-130 98 06/26/15 01:36 11,2-Dichloroethane-d4 (Surr)70-130 104 06/26/15 01:36 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259533/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 Acetone 0.250 0.2518 mg/Kg 101 51-149 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Benzene 0.0500 0.05122 mg/Kg 102 75-127 Bromobenzene 0.0500 0.04974 mg/Kg 99 75-130 Bromochloromethane 0.0500 0.04870 mg/Kg 97 70-132 Bromodichloromethane 0.0500 0.04687 mg/Kg 94 68-135 Bromoform 0.0500 0.04196 mg/Kg 84 36-150 Bromomethane 0.0500 0.04917 mg/Kg 98 43-142 2-Butanone (MEK)0.250 0.2497 mg/Kg 100 61-132 Carbon disulfide 0.0500 0.05509 mg/Kg 110 74-135 Carbon tetrachloride 0.0500 0.04942 mg/Kg 99 70-141 Chlorobenzene 0.0500 0.05075 mg/Kg 101 84-125 Chlorodibromomethane 0.0500 0.04209 mg/Kg 84 66-134 Chloroethane 0.0500 0.05416 mg/Kg 108 53-144 Chloroform 0.0500 0.04736 mg/Kg 95 76-130 Chloromethane 0.0500 0.05009 mg/Kg 100 23-150 2-Chlorotoluene 0.0500 0.04932 mg/Kg 99 78-132 4-Chlorotoluene 0.0500 0.04894 mg/Kg 98 77-138 cis-1,2-Dichloroethene 0.0500 0.05157 mg/Kg 103 75-125 TestAmerica Nashville Page 63 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259533/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 cis-1,3-Dichloropropene 0.0500 0.05069 mg/Kg 101 73-148 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits 1,2-Dibromo-3-Chloropropane 0.0500 0.04046 mg/Kg 81 49-142 1,2-Dibromoethane (EDB)0.0500 0.04914 mg/Kg 98 80-135 Dibromomethane 0.0500 0.05175 mg/Kg 103 71-130 1,2-Dichlorobenzene 0.0500 0.04914 mg/Kg 98 80-134 1,3-Dichlorobenzene 0.0500 0.04865 mg/Kg 97 79-137 1,4-Dichlorobenzene 0.0500 0.04587 mg/Kg 92 77-139 Dichlorodifluoromethane 0.0500 0.04349 mg/Kg 87 12-144 1,1-Dichloroethane 0.0500 0.05002 mg/Kg 100 75-124 1,2-Dichloroethane 0.0500 0.04856 mg/Kg 97 65-134 1,1-Dichloroethene 0.0500 0.05036 mg/Kg 101 75-131 1,2-Dichloroethene, Total 0.100 0.1029 mg/Kg 103 75-128 1,2-Dichloropropane 0.0500 0.05375 mg/Kg 107 69-120 1,3-Dichloropropane 0.0500 0.05101 mg/Kg 102 78-126 2,2-Dichloropropane 0.0500 0.05311 mg/Kg 106 68-145 1,1-Dichloropropene 0.0500 0.05115 mg/Kg 102 79-127 Diisopropyl ether 0.0500 0.05087 mg/Kg 102 68-124 Ethylbenzene 0.0500 0.05284 mg/Kg 106 80-134 Hexachlorobutadiene 0.0500 0.04884 mg/Kg 98 65-148 2-Hexanone 0.250 0.2645 mg/Kg 106 57-148 Isopropylbenzene 0.0500 0.05318 mg/Kg 106 80-150 Methylene Chloride 0.0500 0.05083 mg/Kg 102 68-144 4-Methyl-2-pentanone (MIBK)0.250 0.2685 mg/Kg 107 59-138 Methyl tert-butyl ether 0.0500 0.04824 mg/Kg 96 70-136 Naphthalene 0.0500 0.05379 mg/Kg 108 69-150 n-Butylbenzene 0.0500 0.04755 mg/Kg 95 72-152 N-Propylbenzene 0.0500 0.05067 mg/Kg 101 75-137 p-Isopropyltoluene 0.0500 0.04869 mg/Kg 97 77-141 sec-Butylbenzene 0.0500 0.05091 mg/Kg 102 79-141 Styrene 0.0500 0.05408 mg/Kg 108 74-131 tert-Butylbenzene 0.0500 0.05027 mg/Kg 101 80-132 1,1,1,2-Tetrachloroethane 0.0500 0.04780 mg/Kg 96 80-136 1,1,2,2-Tetrachloroethane 0.0500 0.04858 mg/Kg 97 66-134 Tetrachloroethene 0.0500 0.05083 mg/Kg 102 78-140 Toluene 0.0500 0.05436 mg/Kg 109 80-132 trans-1,2-Dichloroethene 0.0500 0.05133 mg/Kg 103 76-128 trans-1,3-Dichloropropene 0.0500 0.04166 mg/Kg 83 62-139 1,2,3-Trichlorobenzene 0.0500 0.04839 mg/Kg 97 70-150 1,2,4-Trichlorobenzene 0.0500 0.04753 mg/Kg 95 62-150 1,1,1-Trichloroethane 0.0500 0.05164 mg/Kg 103 72-140 1,1,2-Trichloroethane 0.0500 0.04981 mg/Kg 100 78-128 Trichloroethene 0.0500 0.05308 mg/Kg 106 77-127 Trichlorofluoromethane 0.0500 0.04776 mg/Kg 96 50-140 1,2,3-Trichloropropane 0.0500 0.04856 mg/Kg 97 65-139 1,2,4-Trimethylbenzene 0.0500 0.04807 mg/Kg 96 77-139 1,3,5-Trimethylbenzene 0.0500 0.05041 mg/Kg 101 78-138 Vinyl chloride 0.0500 0.05091 mg/Kg 102 47-136 Xylenes, Total 0.100 0.1021 mg/Kg 102 80-137 TestAmerica Nashville Page 64 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259533/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 4-Bromofluorobenzene (Surr)70 -130 Surrogate 96 LCS LCS Qualifier Limits%Recovery 100Dibromofluoromethane (Surr)70 -130 961,2-Dichloroethane-d4 (Surr)70 -130 105Toluene-d8 (Surr)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-259533/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 Acetone 0.250 0.2298 mg/Kg 92 51-149 9 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Benzene 0.0500 0.05170 mg/Kg 103 75-127 1 50 Bromobenzene 0.0500 0.04942 mg/Kg 99 75-130 1 50 Bromochloromethane 0.0500 0.04859 mg/Kg 97 70-132 0 50 Bromodichloromethane 0.0500 0.04706 mg/Kg 94 68-135 0 50 Bromoform 0.0500 0.04146 mg/Kg 83 36-150 1 50 Bromomethane 0.0500 0.05378 mg/Kg 108 43-142 9 50 2-Butanone (MEK)0.250 0.2231 mg/Kg 89 61-132 11 50 Carbon disulfide 0.0500 0.05844 mg/Kg 117 74-135 6 50 Carbon tetrachloride 0.0500 0.04997 mg/Kg 100 70-141 1 50 Chlorobenzene 0.0500 0.05114 mg/Kg 102 84-125 1 50 Chlorodibromomethane 0.0500 0.04269 mg/Kg 85 66-134 1 50 Chloroethane 0.0500 0.05447 mg/Kg 109 53-144 1 50 Chloroform 0.0500 0.04753 mg/Kg 95 76-130 0 49 Chloromethane 0.0500 0.05024 mg/Kg 100 23-150 0 50 2-Chlorotoluene 0.0500 0.04984 mg/Kg 100 78-132 1 50 4-Chlorotoluene 0.0500 0.04941 mg/Kg 99 77-138 1 50 cis-1,2-Dichloroethene 0.0500 0.05191 mg/Kg 104 75-125 1 50 cis-1,3-Dichloropropene 0.0500 0.05005 mg/Kg 100 73-148 1 50 1,2-Dibromo-3-Chloropropane 0.0500 0.03941 mg/Kg 79 49-142 3 50 1,2-Dibromoethane (EDB)0.0500 0.04841 mg/Kg 97 80-135 2 50 Dibromomethane 0.0500 0.05057 mg/Kg 101 71-130 2 50 1,2-Dichlorobenzene 0.0500 0.04954 mg/Kg 99 80-134 1 50 1,3-Dichlorobenzene 0.0500 0.04836 mg/Kg 97 79-137 1 50 1,4-Dichlorobenzene 0.0500 0.04609 mg/Kg 92 77-139 0 50 Dichlorodifluoromethane 0.0500 0.04490 mg/Kg 90 12-144 3 50 1,1-Dichloroethane 0.0500 0.05107 mg/Kg 102 75-124 2 50 1,2-Dichloroethane 0.0500 0.04807 mg/Kg 96 65-134 1 50 1,1-Dichloroethene 0.0500 0.05219 mg/Kg 104 75-131 4 50 1,2-Dichloroethene, Total 0.100 0.1034 mg/Kg 103 75-128 0 41 1,2-Dichloropropane 0.0500 0.05311 mg/Kg 106 69-120 1 50 1,3-Dichloropropane 0.0500 0.05083 mg/Kg 102 78-126 0 42 2,2-Dichloropropane 0.0500 0.05452 mg/Kg 109 68-145 3 50 1,1-Dichloropropene 0.0500 0.05184 mg/Kg 104 79-127 1 50 Diisopropyl ether 0.0500 0.05114 mg/Kg 102 68-124 1 45 Ethylbenzene 0.0500 0.05366 mg/Kg 107 80-134 2 50 Hexachlorobutadiene 0.0500 0.05028 mg/Kg 101 65-148 3 50 2-Hexanone 0.250 0.2553 mg/Kg 102 57-148 4 50 TestAmerica Nashville Page 65 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-259533/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259533 Isopropylbenzene 0.0500 0.05394 mg/Kg 108 80-150 1 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Methylene Chloride 0.0500 0.05083 mg/Kg 102 68-144 0 50 4-Methyl-2-pentanone (MIBK)0.250 0.2586 mg/Kg 103 59-138 4 50 Methyl tert-butyl ether 0.0500 0.04819 mg/Kg 96 70-136 0 50 Naphthalene 0.0500 0.05095 mg/Kg 102 69-150 5 50 n-Butylbenzene 0.0500 0.04893 mg/Kg 98 72-152 3 50 N-Propylbenzene 0.0500 0.05191 mg/Kg 104 75-137 2 50 p-Isopropyltoluene 0.0500 0.04985 mg/Kg 100 77-141 2 50 sec-Butylbenzene 0.0500 0.05216 mg/Kg 104 79-141 2 50 Styrene 0.0500 0.05374 mg/Kg 107 74-131 1 50 tert-Butylbenzene 0.0500 0.05128 mg/Kg 103 80-132 2 50 1,1,1,2-Tetrachloroethane 0.0500 0.04870 mg/Kg 97 80-136 2 50 1,1,2,2-Tetrachloroethane 0.0500 0.05028 mg/Kg 101 66-134 3 50 Tetrachloroethene 0.0500 0.05272 mg/Kg 105 78-140 4 50 Toluene 0.0500 0.05429 mg/Kg 109 80-132 0 50 trans-1,2-Dichloroethene 0.0500 0.05144 mg/Kg 103 76-128 0 50 trans-1,3-Dichloropropene 0.0500 0.04398 mg/Kg 88 62-139 5 50 1,2,3-Trichlorobenzene 0.0500 0.04745 mg/Kg 95 70-150 2 50 1,2,4-Trichlorobenzene 0.0500 0.04658 mg/Kg 93 62-150 2 50 1,1,1-Trichloroethane 0.0500 0.05278 mg/Kg 106 72-140 2 50 1,1,2-Trichloroethane 0.0500 0.04997 mg/Kg 100 78-128 0 50 Trichloroethene 0.0500 0.05368 mg/Kg 107 77-127 1 50 Trichlorofluoromethane 0.0500 0.05044 mg/Kg 101 50-140 5 50 1,2,3-Trichloropropane 0.0500 0.04781 mg/Kg 96 65-139 2 50 1,2,4-Trimethylbenzene 0.0500 0.04875 mg/Kg 97 77-139 1 50 1,3,5-Trimethylbenzene 0.0500 0.05027 mg/Kg 101 78-138 0 50 Vinyl chloride 0.0500 0.05233 mg/Kg 105 47-136 3 50 Xylenes, Total 0.100 0.1035 mg/Kg 103 80-137 1 50 4-Bromofluorobenzene (Surr)70 -130 Surrogate 97 LCSD LCSD Qualifier Limits%Recovery 99Dibromofluoromethane (Surr)70 -130 941,2-Dichloroethane-d4 (Surr)70 -130 105Toluene-d8 (Surr)70 -130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-259662/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 RL MDL Acenaphthene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Acenaphthylene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Anthracene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Benzo[a]anthracene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Benzo[a]pyrene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Benzo[b]fluoranthene TestAmerica Nashville Page 66 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-259662/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 RL MDL Benzo[g,h,i]perylene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Benzo[k]fluoranthene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Bis(2-chloroethoxy)methane ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Bis(2-chloroethyl)ether ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1bis (2-chloroisopropyl) ether ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Bis(2-ethylhexyl) phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 14-Bromophenyl phenyl ether ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Butyl benzyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Carbazole ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 14-Chloroaniline ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 14-Chloro-3-methylphenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12-Chloronaphthalene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12-Chlorophenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 14-Chlorophenyl phenyl ether ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Chrysene ND 0.666 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Cresols ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Dibenz(a,h)anthracene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Dibenzofuran ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 11,2-Dichlorobenzene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 11,3-Dichlorobenzene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 11,4-Dichlorobenzene ND 0.667 mg/Kg 06/26/15 09:17 06/27/15 14:57 13,3'-Dichlorobenzidine ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,4-Dichlorophenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Diethyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,4-Dimethylphenol ND 1.67 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Dimethyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Di-n-butyl phthalate ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 14,6-Dinitro-2-methylphenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,4-Dinitrophenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,4-Dinitrotoluene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,6-Dinitrotoluene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Di-n-octyl phthalate ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Fluoranthene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Fluorene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Hexachlorobenzene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Hexachlorobutadiene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Hexachlorocyclopentadiene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Hexachloroethane ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Indeno[1,2,3-cd]pyrene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Isophorone ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 11-Methylnaphthalene ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 12-Methylnaphthalene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12-Methylphenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 13 & 4 Methylphenol ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Naphthalene ND 0.833 mg/Kg 06/26/15 09:17 06/27/15 14:57 12-Nitroaniline ND 0.833 mg/Kg 06/26/15 09:17 06/27/15 14:57 13-Nitroaniline ND 0.833 mg/Kg 06/26/15 09:17 06/27/15 14:57 14-Nitroaniline TestAmerica Nashville Page 67 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-259662/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 RL MDL Nitrobenzene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12-Nitrophenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 14-Nitrophenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1N-Nitrosodi-n-propylamine ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1n-Nitrosodiphenylamine(as diphenylamine) ND 0.833 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Pentachlorophenol ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Phenanthrene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Phenol ND 0.0670 mg/Kg 06/26/15 09:17 06/27/15 14:57 1Pyrene ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 11,2,4-Trichlorobenzene ND 0.833 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,4,5-Trichlorophenol ND 0.333 mg/Kg 06/26/15 09:17 06/27/15 14:57 12,4,6-Trichlorophenol 2-Fluorobiphenyl (Surr)81 29-120 06/27/15 14:57 1 MB MB Surrogate 06/26/15 09:17 Dil FacPreparedAnalyzedQualifierLimits%Recovery 70 06/26/15 09:17 06/27/15 14:57 12-Fluorophenol (Surr)10-120 76 06/26/15 09:17 06/27/15 14:57 1Nitrobenzene-d5 (Surr)27-120 73 06/26/15 09:17 06/27/15 14:57 1Phenol-d5 (Surr)10-120 89 06/26/15 09:17 06/27/15 14:57 1Terphenyl-d14 (Surr)13-120 50 06/26/15 09:17 06/27/15 14:57 12,4,6-Tribromophenol (Surr)10-120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259662/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 Acenaphthene 1.67 1.434 mg/Kg 86 36-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Acenaphthylene 1.67 1.419 mg/Kg 85 38-120 Anthracene 1.67 1.487 mg/Kg 89 46-124 Benzo[a]anthracene 1.67 1.477 mg/Kg 89 45-120 Benzo[a]pyrene 1.67 1.510 mg/Kg 91 45-120 Benzo[b]fluoranthene 1.67 1.465 mg/Kg 88 42-120 Benzo[g,h,i]perylene 1.67 1.655 mg/Kg 99 38-120 Benzo[k]fluoranthene 1.67 1.495 mg/Kg 90 42-120 Bis(2-chloroethoxy)methane 1.67 1.406 mg/Kg 84 32-120 Bis(2-chloroethyl)ether 1.67 1.300 mg/Kg 78 31-120 bis (2-chloroisopropyl) ether 1.67 1.368 mg/Kg 82 32-120 Bis(2-ethylhexyl) phthalate 1.67 1.596 mg/Kg 96 43-120 4-Bromophenyl phenyl ether 1.67 1.368 mg/Kg 82 40-120 Butyl benzyl phthalate 1.67 1.562 mg/Kg 94 43-133 Carbazole 1.67 1.457 mg/Kg 87 44-120 4-Chloroaniline 1.67 1.160 mg/Kg 70 35-120 4-Chloro-3-methylphenol 1.67 1.556 mg/Kg 93 38-120 2-Chloronaphthalene 1.67 1.499 mg/Kg 90 34-120 2-Chlorophenol 1.67 1.381 mg/Kg 83 32-120 4-Chlorophenyl phenyl ether 1.67 1.352 mg/Kg 81 42-120 Chrysene 1.67 1.462 mg/Kg 88 43-120 TestAmerica Nashville Page 68 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259662/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 Cresols 3.33 2.933 mg/Kg 88 36-129 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Dibenz(a,h)anthracene 1.67 1.666 mg/Kg 100 32-128 Dibenzofuran 1.67 1.389 mg/Kg 83 41-120 1,2-Dichlorobenzene 1.67 1.287 mg/Kg 77 33-120 1,3-Dichlorobenzene 1.67 1.289 mg/Kg 77 32-120 1,4-Dichlorobenzene 1.67 1.305 mg/Kg 78 32-120 3,3'-Dichlorobenzidine 1.67 1.614 mg/Kg 97 39-120 2,4-Dichlorophenol 1.67 1.454 mg/Kg 87 32-120 Diethyl phthalate 1.67 1.423 mg/Kg 85 41-122 2,4-Dimethylphenol 1.67 1.411 mg/Kg 85 32-120 Dimethyl phthalate 1.67 1.449 J mg/Kg 87 55-120 Di-n-butyl phthalate 1.67 1.586 mg/Kg 95 46-127 4,6-Dinitro-2-methylphenol 3.33 2.776 mg/Kg 83 27-134 2,4-Dinitrophenol 3.33 2.007 mg/Kg 60 10-142 2,4-Dinitrotoluene 1.67 1.520 mg/Kg 91 43-120 2,6-Dinitrotoluene 1.67 1.502 mg/Kg 90 43-120 Di-n-octyl phthalate 1.67 1.588 mg/Kg 95 40-130 Fluoranthene 1.67 1.474 mg/Kg 88 46-120 Fluorene 1.67 1.393 mg/Kg 84 42-120 Hexachlorobenzene 1.67 1.382 mg/Kg 83 44-120 Hexachlorobutadiene 1.67 1.277 mg/Kg 77 31-120 Hexachlorocyclopentadiene 1.67 1.248 mg/Kg 75 24-120 Hexachloroethane 1.67 1.281 mg/Kg 77 33-120 Indeno[1,2,3-cd]pyrene 1.67 1.600 mg/Kg 96 41-121 Isophorone 1.67 1.497 mg/Kg 90 33-120 1-Methylnaphthalene 1.67 1.451 mg/Kg 87 32-120 2-Methylnaphthalene 1.67 1.348 mg/Kg 81 28-120 2-Methylphenol 1.67 1.437 mg/Kg 86 36-120 3 & 4 Methylphenol 1.67 1.496 mg/Kg 90 37-120 Naphthalene 1.67 1.356 mg/Kg 81 32-120 2-Nitroaniline 1.67 1.694 mg/Kg 102 40-120 3-Nitroaniline 1.67 1.479 mg/Kg 89 42-120 4-Nitroaniline 1.67 1.429 mg/Kg 86 43-120 Nitrobenzene 1.67 1.419 mg/Kg 85 26-120 2-Nitrophenol 1.67 1.440 mg/Kg 86 29-120 4-Nitrophenol 3.33 3.164 mg/Kg 95 32-136 N-Nitrosodi-n-propylamine 1.67 1.543 mg/Kg 93 35-120 n-Nitrosodiphenylamine(as diphenylamine) 3.33 3.006 mg/Kg 90 52-140 Pentachlorophenol 3.33 2.301 mg/Kg 69 44-134 Phenanthrene 1.67 1.395 mg/Kg 84 45-120 Phenol 1.67 1.442 mg/Kg 87 30-120 Pyrene 1.67 1.510 mg/Kg 91 43-120 1,2,4-Trichlorobenzene 1.67 1.280 mg/Kg 77 29-120 2,4,5-Trichlorophenol 1.67 1.553 mg/Kg 93 39-120 2,4,6-Trichlorophenol 1.67 1.630 mg/Kg 98 39-120 TestAmerica Nashville Page 69 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259662/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 2-Fluorobiphenyl (Surr)29 -120 Surrogate 87 LCS LCS Qualifier Limits%Recovery 812-Fluorophenol (Surr)10 -120 82Nitrobenzene-d5 (Surr)27 -120 84Phenol-d5 (Surr)10 -120 87Terphenyl-d14 (Surr)13 -120 822,4,6-Tribromophenol (Surr)10 -120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-259662/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 Acenaphthene 1.67 1.561 mg/Kg 94 36-120 8 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Acenaphthylene 1.67 1.540 mg/Kg 92 38-120 8 50 Anthracene 1.67 1.615 mg/Kg 97 46-124 8 49 Benzo[a]anthracene 1.67 1.615 mg/Kg 97 45-120 9 50 Benzo[a]pyrene 1.67 1.643 mg/Kg 99 45-120 8 50 Benzo[b]fluoranthene 1.67 1.622 mg/Kg 97 42-120 10 50 Benzo[g,h,i]perylene 1.67 1.803 mg/Kg 108 38-120 9 50 Benzo[k]fluoranthene 1.67 1.604 mg/Kg 96 42-120 7 45 Bis(2-chloroethoxy)methane 1.67 1.540 mg/Kg 92 32-120 9 50 Bis(2-chloroethyl)ether 1.67 1.425 mg/Kg 85 31-120 9 50 bis (2-chloroisopropyl) ether 1.67 1.570 mg/Kg 94 32-120 14 50 Bis(2-ethylhexyl) phthalate 1.67 1.766 mg/Kg 106 43-120 10 50 4-Bromophenyl phenyl ether 1.67 1.507 mg/Kg 90 40-120 10 37 Butyl benzyl phthalate 1.67 1.675 mg/Kg 100 43-133 7 50 Carbazole 1.67 1.590 mg/Kg 95 44-120 9 46 4-Chloroaniline 1.67 1.253 mg/Kg 75 35-120 8 50 4-Chloro-3-methylphenol 1.67 1.646 mg/Kg 99 38-120 6 49 2-Chloronaphthalene 1.67 1.609 mg/Kg 97 34-120 7 50 2-Chlorophenol 1.67 1.550 mg/Kg 93 32-120 12 50 4-Chlorophenyl phenyl ether 1.67 1.462 mg/Kg 88 42-120 8 50 Chrysene 1.67 1.588 mg/Kg 95 43-120 8 49 Cresols 3.33 3.269 mg/Kg 98 36-129 11 50 Dibenz(a,h)anthracene 1.67 1.779 mg/Kg 107 32-128 7 50 Dibenzofuran 1.67 1.516 mg/Kg 91 41-120 9 50 1,2-Dichlorobenzene 1.67 1.459 mg/Kg 88 33-120 13 50 1,3-Dichlorobenzene 1.67 1.472 mg/Kg 88 32-120 13 50 1,4-Dichlorobenzene 1.67 1.505 mg/Kg 90 32-120 14 50 3,3'-Dichlorobenzidine 1.67 1.772 mg/Kg 106 39-120 9 50 2,4-Dichlorophenol 1.67 1.551 mg/Kg 93 32-120 6 50 Diethyl phthalate 1.67 1.527 mg/Kg 92 41-122 7 45 2,4-Dimethylphenol 1.67 1.532 mg/Kg 92 32-120 8 50 Dimethyl phthalate 1.67 1.580 J mg/Kg 95 55-120 9 46 Di-n-butyl phthalate 1.67 1.714 mg/Kg 103 46-127 8 49 4,6-Dinitro-2-methylphenol 3.33 2.959 mg/Kg 89 27-134 6 50 2,4-Dinitrophenol 3.33 2.280 mg/Kg 68 10-142 13 50 2,4-Dinitrotoluene 1.67 1.639 mg/Kg 98 43-120 8 50 TestAmerica Nashville Page 70 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-259662/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 2,6-Dinitrotoluene 1.67 1.619 mg/Kg 97 43-120 8 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Di-n-octyl phthalate 1.67 1.750 mg/Kg 105 40-130 10 50 Fluoranthene 1.67 1.603 mg/Kg 96 46-120 8 50 Fluorene 1.67 1.526 mg/Kg 92 42-120 9 50 Hexachlorobenzene 1.67 1.488 mg/Kg 89 44-120 7 50 Hexachlorobutadiene 1.67 1.390 mg/Kg 83 31-120 8 50 Hexachlorocyclopentadiene 1.67 1.389 mg/Kg 83 24-120 11 50 Hexachloroethane 1.67 1.503 mg/Kg 90 33-120 16 50 Indeno[1,2,3-cd]pyrene 1.67 1.746 mg/Kg 105 41-121 9 50 Isophorone 1.67 1.625 mg/Kg 97 33-120 8 50 1-Methylnaphthalene 1.67 1.573 mg/Kg 94 32-120 8 50 2-Methylnaphthalene 1.67 1.483 mg/Kg 89 28-120 9 50 2-Methylphenol 1.67 1.620 mg/Kg 97 36-120 12 50 3 & 4 Methylphenol 1.67 1.649 mg/Kg 99 37-120 10 50 Naphthalene 1.67 1.492 mg/Kg 89 32-120 10 50 2-Nitroaniline 1.67 1.861 mg/Kg 112 40-120 9 50 3-Nitroaniline 1.67 1.620 mg/Kg 97 42-120 9 49 4-Nitroaniline 1.67 1.527 mg/Kg 92 43-120 7 49 Nitrobenzene 1.67 1.575 mg/Kg 95 26-120 10 50 2-Nitrophenol 1.67 1.563 mg/Kg 94 29-120 8 50 4-Nitrophenol 3.33 3.459 mg/Kg 104 32-136 9 45 N-Nitrosodi-n-propylamine 1.67 1.685 mg/Kg 101 35-120 9 50 n-Nitrosodiphenylamine(as diphenylamine) 3.33 3.257 mg/Kg 98 52-140 8 50 Pentachlorophenol 3.33 2.367 mg/Kg 71 44-134 3 50 Phenanthrene 1.67 1.519 mg/Kg 91 45-120 9 50 Phenol 1.67 1.600 mg/Kg 96 30-120 10 50 Pyrene 1.67 1.638 mg/Kg 98 43-120 8 50 1,2,4-Trichlorobenzene 1.67 1.440 mg/Kg 86 29-120 12 50 2,4,5-Trichlorophenol 1.67 1.715 mg/Kg 103 39-120 10 50 2,4,6-Trichlorophenol 1.67 1.838 mg/Kg 110 39-120 12 50 2-Fluorobiphenyl (Surr)29 -120 Surrogate 96 LCSD LCSD Qualifier Limits%Recovery 932-Fluorophenol (Surr)10 -120 92Nitrobenzene-d5 (Surr)27 -120 96Phenol-d5 (Surr)10 -120 96Terphenyl-d14 (Surr)13 -120 892,4,6-Tribromophenol (Surr)10 -120 Client Sample ID: Matrix SpikeLab Sample ID: 490-80471-A-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 Acenaphthene ND 1.74 1.379 mg/Kg 79 19-120☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Acenaphthylene ND 1.74 1.412 mg/Kg 81 25-120☼ Anthracene ND 1.74 1.421 mg/Kg 82 28-125☼ TestAmerica Nashville Page 71 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-80471-A-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 Benzo[a]anthracene ND 1.74 1.415 mg/Kg 81 23-120☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Benzo[a]pyrene ND 1.74 1.432 mg/Kg 82 15-128☼ Benzo[b]fluoranthene ND 1.74 1.397 mg/Kg 80 12-133☼ Benzo[g,h,i]perylene ND 1.74 1.535 mg/Kg 88 22-120☼ Benzo[k]fluoranthene ND 1.74 1.411 mg/Kg 81 28-120☼ Bis(2-chloroethoxy)methane ND 1.74 1.442 mg/Kg 83 24-120☼ Bis(2-chloroethyl)ether ND 1.74 1.399 mg/Kg 80 22-120☼ bis (2-chloroisopropyl) ether ND 1.74 1.449 mg/Kg 83 20-120☼ Bis(2-ethylhexyl) phthalate 0.427 1.74 1.796 mg/Kg 79 26-120☼ 4-Bromophenyl phenyl ether ND 1.74 1.329 mg/Kg 76 31-120☼ Butyl benzyl phthalate ND 1.74 1.493 mg/Kg 86 24-133☼ Carbazole ND 1.74 1.414 mg/Kg 81 25-123☼ 4-Chloroaniline ND 1.74 1.362 mg/Kg 78 26-120☼ 4-Chloro-3-methylphenol ND 1.74 1.548 mg/Kg 89 21-120☼ 2-Chloronaphthalene ND 1.74 1.468 mg/Kg 84 24-120☼ 2-Chlorophenol ND 1.74 1.435 mg/Kg 82 25-120☼ 4-Chlorophenyl phenyl ether ND 1.74 1.309 mg/Kg 75 26-120☼ Chrysene ND 1.74 1.383 mg/Kg 79 20-120☼ Cresols ND 3.48 3.041 mg/Kg 87 10-200☼ Dibenz(a,h)anthracene ND 1.74 1.540 mg/Kg 88 12-128☼ Dibenzofuran ND 1.74 1.383 mg/Kg 79 21-120☼ 1,2-Dichlorobenzene ND 1.74 1.342 mg/Kg 77 10-120☼ 1,3-Dichlorobenzene ND 1.74 1.374 mg/Kg 79 10-120☼ 1,4-Dichlorobenzene ND 1.74 1.364 mg/Kg 78 10-120☼ 3,3'-Dichlorobenzidine ND 1.74 1.596 mg/Kg 92 10-120☼ 2,4-Dichlorophenol ND 1.74 1.386 mg/Kg 80 17-120☼ Diethyl phthalate ND 1.74 1.368 mg/Kg 79 29-122☼ 2,4-Dimethylphenol ND 1.74 1.392 mg/Kg 80 17-120☼ Dimethyl phthalate ND 1.74 ND mg/Kg 82 30-120☼ Di-n-butyl phthalate ND 1.74 1.564 mg/Kg 90 29-126☼ 4,6-Dinitro-2-methylphenol ND 3.48 2.713 mg/Kg 78 10-134☼ 2,4-Dinitrophenol ND 3.48 2.116 mg/Kg 61 10-150☼ 2,4-Dinitrotoluene ND 1.74 1.417 mg/Kg 81 24-121☼ 2,6-Dinitrotoluene ND 1.74 1.449 mg/Kg 83 24-120☼ Di-n-octyl phthalate ND F1 F2 1.74 ND F1 mg/Kg 2 27-130☼ Fluoranthene ND 1.74 1.422 mg/Kg 82 10-143☼ Fluorene ND 1.74 1.366 mg/Kg 78 20-120☼ Hexachlorobenzene ND 1.74 1.325 mg/Kg 76 25-120☼ Hexachlorobutadiene ND 1.74 1.323 mg/Kg 76 10-120☼ Hexachlorocyclopentadiene ND 1.74 1.307 mg/Kg 75 10-120☼ Hexachloroethane ND 1.74 1.406 mg/Kg 81 10-120☼ Indeno[1,2,3-cd]pyrene ND 1.74 1.488 mg/Kg 85 22-121☼ Isophorone ND 1.74 1.523 mg/Kg 87 24-120☼ 1-Methylnaphthalene ND 1.74 1.451 mg/Kg 83 10-120☼ 2-Methylnaphthalene ND 1.74 1.359 mg/Kg 78 13-120☼ 2-Methylphenol ND 1.74 1.531 mg/Kg 88 23-120☼ 3 & 4 Methylphenol ND 1.74 1.510 mg/Kg 87 19-120☼ Naphthalene ND 1.74 1.367 mg/Kg 79 10-120☼ TestAmerica Nashville Page 72 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-80471-A-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 2-Nitroaniline ND 1.74 1.700 mg/Kg 98 31-120☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits 3-Nitroaniline ND 1.74 1.425 mg/Kg 82 31-120☼ 4-Nitroaniline ND 1.74 1.367 mg/Kg 79 28-120☼ Nitrobenzene ND 1.74 1.413 mg/Kg 81 19-120☼ 2-Nitrophenol ND 1.74 1.474 mg/Kg 85 23-120☼ 4-Nitrophenol ND 3.48 3.055 mg/Kg 88 16-139☼ N-Nitrosodi-n-propylamine ND 1.74 1.595 mg/Kg 92 24-120☼ n-Nitrosodiphenylamine(as diphenylamine) ND 3.48 2.899 mg/Kg 83 26-150☼ Pentachlorophenol ND 3.48 2.560 mg/Kg 74 19-145☼ Phenanthrene ND 1.74 1.342 mg/Kg 77 21-122☼ Phenol ND 1.74 1.479 mg/Kg 85 15-120☼ Pyrene ND 1.74 1.443 mg/Kg 83 20-123☼ 1,2,4-Trichlorobenzene ND 1.74 1.292 mg/Kg 74 14-120☼ 2,4,5-Trichlorophenol ND 1.74 1.553 mg/Kg 89 27-120☼ 2,4,6-Trichlorophenol ND 1.74 1.613 mg/Kg 93 24-122☼ 2-Fluorobiphenyl (Surr)29 -120 Surrogate 82 MS MS Qualifier Limits%Recovery 822-Fluorophenol (Surr)10 -120 80Nitrobenzene-d5 (Surr)27 -120 82Phenol-d5 (Surr)10 -120 81Terphenyl-d14 (Surr)13 -120 742,4,6-Tribromophenol (Surr)10 -120 Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-80471-A-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 Acenaphthene ND 1.72 1.429 mg/Kg 83 19-120 4 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Acenaphthylene ND 1.72 1.499 mg/Kg 87 25-120 6 50☼ Anthracene ND 1.72 1.518 mg/Kg 88 28-125 7 49☼ Benzo[a]anthracene ND 1.72 1.501 mg/Kg 87 23-120 6 50☼ Benzo[a]pyrene ND 1.72 1.510 mg/Kg 88 15-128 5 50☼ Benzo[b]fluoranthene ND 1.72 1.514 mg/Kg 88 12-133 8 50☼ Benzo[g,h,i]perylene ND 1.72 1.625 mg/Kg 94 22-120 6 50☼ Benzo[k]fluoranthene ND 1.72 1.435 mg/Kg 83 28-120 2 45☼ Bis(2-chloroethoxy)methane ND 1.72 1.460 mg/Kg 85 24-120 1 50☼ Bis(2-chloroethyl)ether ND 1.72 1.388 mg/Kg 81 22-120 1 50☼ bis (2-chloroisopropyl) ether ND 1.72 1.434 mg/Kg 83 20-120 1 50☼ Bis(2-ethylhexyl) phthalate 0.427 1.72 1.828 mg/Kg 81 26-120 2 50☼ 4-Bromophenyl phenyl ether ND 1.72 1.425 mg/Kg 83 31-120 7 37☼ Butyl benzyl phthalate ND 1.72 1.561 mg/Kg 91 24-133 4 50☼ Carbazole ND 1.72 1.506 mg/Kg 88 25-123 6 46☼ 4-Chloroaniline ND 1.72 1.400 mg/Kg 81 26-120 3 50☼ 4-Chloro-3-methylphenol ND 1.72 1.561 mg/Kg 91 21-120 1 49☼ 2-Chloronaphthalene ND 1.72 1.492 mg/Kg 87 24-120 2 50☼ TestAmerica Nashville Page 73 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-80471-A-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 2-Chlorophenol ND 1.72 1.416 mg/Kg 82 25-120 1 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD 4-Chlorophenyl phenyl ether ND 1.72 1.390 mg/Kg 81 26-120 6 50☼ Chrysene ND 1.72 1.443 mg/Kg 84 20-120 4 49☼ Cresols ND 3.44 3.090 mg/Kg 90 10-200 2 50☼ Dibenz(a,h)anthracene ND 1.72 1.601 mg/Kg 93 12-128 4 50☼ Dibenzofuran ND 1.72 1.415 mg/Kg 82 21-120 2 50☼ 1,2-Dichlorobenzene ND 1.72 1.347 mg/Kg 78 10-120 0 50☼ 1,3-Dichlorobenzene ND 1.72 1.339 mg/Kg 78 10-120 3 50☼ 1,4-Dichlorobenzene ND 1.72 1.357 mg/Kg 79 10-120 1 50☼ 3,3'-Dichlorobenzidine ND 1.72 1.688 mg/Kg 98 10-120 6 50☼ 2,4-Dichlorophenol ND 1.72 1.438 mg/Kg 84 17-120 4 50☼ Diethyl phthalate ND 1.72 1.406 mg/Kg 82 29-122 3 45☼ 2,4-Dimethylphenol ND 1.72 1.431 mg/Kg 83 17-120 3 50☼ Dimethyl phthalate ND 1.72 ND mg/Kg 86 30-120 3 46☼ Di-n-butyl phthalate ND 1.72 1.624 mg/Kg 94 29-126 4 49☼ 4,6-Dinitro-2-methylphenol ND 3.44 2.819 mg/Kg 82 10-134 4 50☼ 2,4-Dinitrophenol ND 3.44 2.074 mg/Kg 60 10-150 2 50☼ 2,4-Dinitrotoluene ND 1.72 1.484 mg/Kg 86 24-121 5 50☼ 2,6-Dinitrotoluene ND 1.72 1.518 mg/Kg 88 24-120 5 50☼ Di-n-octyl phthalate ND F1 F2 1.72 1.621 F2 mg/Kg 94 27-130 190 50☼ Fluoranthene ND 1.72 1.508 mg/Kg 88 10-143 6 50☼ Fluorene ND 1.72 1.409 mg/Kg 82 20-120 3 50☼ Hexachlorobenzene ND 1.72 1.393 mg/Kg 81 25-120 5 50☼ Hexachlorobutadiene ND 1.72 1.325 mg/Kg 77 10-120 0 50☼ Hexachlorocyclopentadiene ND 1.72 1.300 mg/Kg 76 10-120 1 50☼ Hexachloroethane ND 1.72 1.381 mg/Kg 80 10-120 2 50☼ Indeno[1,2,3-cd]pyrene ND 1.72 1.555 mg/Kg 90 22-121 4 50☼ Isophorone ND 1.72 1.516 mg/Kg 88 24-120 0 50☼ 1-Methylnaphthalene ND 1.72 1.489 mg/Kg 87 10-120 3 50☼ 2-Methylnaphthalene ND 1.72 1.375 mg/Kg 80 13-120 1 50☼ 2-Methylphenol ND 1.72 1.536 mg/Kg 89 23-120 0 50☼ 3 & 4 Methylphenol ND 1.72 1.554 mg/Kg 90 19-120 3 50☼ Naphthalene ND 1.72 1.413 mg/Kg 82 10-120 3 50☼ 2-Nitroaniline ND 1.72 1.807 mg/Kg 105 31-120 6 50☼ 3-Nitroaniline ND 1.72 1.439 mg/Kg 84 31-120 1 49☼ 4-Nitroaniline ND 1.72 1.410 mg/Kg 82 28-120 3 49☼ Nitrobenzene ND 1.72 1.422 mg/Kg 83 19-120 1 50☼ 2-Nitrophenol ND 1.72 1.495 mg/Kg 87 23-120 1 50☼ 4-Nitrophenol ND 3.44 3.170 mg/Kg 92 16-139 4 45☼ N-Nitrosodi-n-propylamine ND 1.72 1.618 mg/Kg 94 24-120 1 50☼ n-Nitrosodiphenylamine(as diphenylamine) ND 3.44 3.059 mg/Kg 89 26-150 5 50☼ Pentachlorophenol ND 3.44 2.659 mg/Kg 77 19-145 4 50☼ Phenanthrene ND 1.72 1.426 mg/Kg 83 21-122 6 50☼ Phenol ND 1.72 1.476 mg/Kg 86 15-120 0 50☼ Pyrene ND 1.72 1.501 mg/Kg 87 20-123 4 50☼ 1,2,4-Trichlorobenzene ND 1.72 1.327 mg/Kg 77 14-120 3 50☼ 2,4,5-Trichlorophenol ND 1.72 1.621 mg/Kg 94 27-120 4 50☼ TestAmerica Nashville Page 74 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-80471-A-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 260013 Prep Batch: 259662 2,4,6-Trichlorophenol ND 1.72 1.661 mg/Kg 97 24-122 3 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD 2-Fluorobiphenyl (Surr)29 -120 Surrogate 87 MSD MSD Qualifier Limits%Recovery 772-Fluorophenol (Surr)10 -120 81Nitrobenzene-d5 (Surr)27 -120 84Phenol-d5 (Surr)10 -120 85Terphenyl-d14 (Surr)13 -120 822,4,6-Tribromophenol (Surr)10 -120 Method: 6010C - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 490-259251/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 RL MDL Antimony ND 9.98 mg/Kg 06/25/15 08:59 06/25/15 14:56 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Arsenic ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Beryllium ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Cadmium ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Chromium ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Copper ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Lead ND 2.99 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Manganese ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Nickel ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Selenium ND 0.998 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Silver ND 2.00 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Thallium ND 9.98 mg/Kg 06/25/15 08:59 06/25/15 14:56 1Zinc Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259251/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Antimony 40.0 38.74 mg/Kg 97 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Arsenic 20.0 19.84 mg/Kg 99 80-120 Beryllium 20.0 20.54 mg/Kg 103 80-120 Cadmium 20.0 19.86 mg/Kg 99 80-120 Chromium 80.0 82.60 mg/Kg 103 80-120 Copper 100 102.0 mg/Kg 102 80-120 Lead 20.0 19.88 mg/Kg 99 80-120 Manganese 200 204.4 mg/Kg 102 80-120 Nickel 200 202.6 mg/Kg 101 80-120 Selenium 20.0 19.46 mg/Kg 97 80-120 Silver 20.0 18.08 mg/Kg 90 80-120 Thallium 120 121.4 mg/Kg 101 80-120 TestAmerica Nashville Page 75 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259251/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Zinc 200 193.9 mg/Kg 97 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: TP-8 (0-2)Lab Sample ID: 490-81215-1 MS Matrix: Soil Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Antimony ND 47.3 47.53 mg/Kg 96 75-125☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Arsenic 8.93 23.6 33.30 mg/Kg 103 75-125☼ Beryllium ND 23.6 23.89 mg/Kg 101 75-125☼ Cadmium ND 23.6 22.88 mg/Kg 94 75-125☼ Chromium 26.6 94.5 126.1 mg/Kg 105 75-125☼ Copper 29.9 118 143.0 mg/Kg 96 75-125☼ Lead 64.4 F1 23.6 102.5 F1 mg/Kg 162 75-125☼ Manganese 318 236 517.1 mg/Kg 84 75-125☼ Nickel 13.1 236 240.1 mg/Kg 96 75-125☼ Selenium ND 23.6 20.96 mg/Kg 89 75-125☼ Silver ND 23.6 21.10 mg/Kg 89 75-125☼ Thallium ND 142 131.7 mg/Kg 93 75-125☼ Zinc 162 236 385.7 mg/Kg 95 75-125☼ Client Sample ID: TP-8 (0-2)Lab Sample ID: 490-81215-1 MSD Matrix: Soil Prep Type: Total/NA Analysis Batch: 259614 Prep Batch: 259251 Antimony ND 46.3 44.18 mg/Kg 91 75-125 7 20☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Arsenic 8.93 23.1 35.95 mg/Kg 117 75-125 8 20☼ Beryllium ND 23.1 23.55 mg/Kg 102 75-125 1 20☼ Cadmium ND 23.1 22.62 mg/Kg 95 75-125 1 20☼ Chromium 26.6 92.5 122.5 mg/Kg 104 75-125 3 20☼ Copper 29.9 116 147.8 mg/Kg 102 75-125 3 20☼ Lead 64.4 F1 23.1 124.0 F1 mg/Kg 258 75-125 19 20☼ Manganese 318 231 554.7 mg/Kg 103 75-125 7 20☼ Nickel 13.1 231 237.6 mg/Kg 97 75-125 1 20☼ Selenium ND 23.1 20.89 mg/Kg 90 75-125 0 20☼ Silver ND 23.1 21.51 mg/Kg 93 75-125 2 20☼ Thallium ND 139 129.9 mg/Kg 94 75-125 1 20☼ Zinc 162 231 366.4 mg/Kg 88 75-125 5 20☼ Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Client Sample ID: Method BlankLab Sample ID: MB 490-259128/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 RL MDL Mercury ND 0.0998 mg/Kg 06/24/15 16:44 06/26/15 10:35 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier TestAmerica Nashville Page 76 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259128/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 Mercury 0.162 0.1819 mg/Kg 112 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Matrix SpikeLab Sample ID: 490-80975-G-6-C MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 Mercury ND F1 0.196 0.2523 F1 mg/Kg 129 80-120☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-80975-G-6-D MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 259797 Prep Batch: 259128 Mercury ND F1 0.193 0.2589 F1 mg/Kg 134 80-120 3 20☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: 7196A - Chromium, Hexavalent Client Sample ID: Method BlankLab Sample ID: MB 490-260615/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 RL MDL Chromium, hex ND 4.95 mg/Kg 06/29/15 16:57 07/01/15 18:21 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCSI 490-260615/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex 64.1 67.82 mg/Kg 106 80-120 Analyte LCSI LCSI DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control SampleLab Sample ID: LCSS 490-260615/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex 39.9 43.07 mg/Kg 108 80-120 Analyte LCSS LCSS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSSD 490-260615/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex 39.7 34.31 *mg/Kg 87 80-120 23 20 Analyte LCSSD LCSSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD TestAmerica Nashville Page 77 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method: 7196A - Chromium, Hexavalent (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-81218-D-1-D MSI Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex ND *76.8 61.60 mg/Kg 80 75-125☼ Analyte MSI MSI DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix SpikeLab Sample ID: 490-81218-D-1-E MSS Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex ND *47.3 40.69 mg/Kg 86 75-125☼ Analyte MSS MSS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: DuplicateLab Sample ID: 490-81218-D-1-C DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 261360 Prep Batch: 260615 Chromium, hex ND *ND mg/Kg NC 20☼ Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD Method: 9045D - pH Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-259987/12 Matrix: Solid Prep Type: Total/NA Analysis Batch: 259987 pH 7.00 7.020 SU 100 95-105 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: DuplicateLab Sample ID: 490-81306-A-1-C DU Matrix: Solid Prep Type: Soluble Analysis Batch: 259987 pH 5.49 5.490 SU 0 20 Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD Temperature 21.7 21.70 Degrees C 0 20 Method: Moisture - Percent Moisture Client Sample ID: TP-8 (0-2)Lab Sample ID: 490-81215-1 DU Matrix: Soil Prep Type: Total/NA Analysis Batch: 258926 Percent Solids 83 85 %2 20 Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD TestAmerica Nashville Page 78 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC GC/MS VOA Prep Batch: 259059 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 5035490-81215-1 TP-8 (0-2)Total/NA Soil 5035490-81215-2 TP-8 (8-10)Total/NA Soil 5035490-81215-3 TP-11 (0-2)Total/NA Soil 5035490-81215-4 TP-5 (0-2)Total/NA Soil 5035490-81215-5 TP-6 (0-2)Total/NA Soil 5035490-81215-6 TP-6 (8-10)Total/NA Soil 5035490-81215-7 TP-7 (0-2)Total/NA Soil 5035490-81215-8 TP-9 (8-10)Total/NA Soil 5035490-81215-10 TP-12 (0-2)Total/NA Soil 5035490-81215-11 TP-13 (0-2)Total/NA Soil 5035490-81215-12 TP-13 (10-11)Total/NA Analysis Batch: 259533 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 8260B 259059490-81215-1 TP-8 (0-2)Total/NA Soil 8260B 259059490-81215-2 TP-8 (8-10)Total/NA Soil 8260B 259059490-81215-3 TP-11 (0-2)Total/NA Soil 8260B 259059490-81215-4 TP-5 (0-2)Total/NA Soil 8260B 259059490-81215-5 TP-6 (0-2)Total/NA Soil 8260B 259059490-81215-6 TP-6 (8-10)Total/NA Soil 8260B 259059490-81215-7 TP-7 (0-2)Total/NA Soil 8260B 259059490-81215-8 TP-9 (8-10)Total/NA Soil 8260B 259059490-81215-10 TP-12 (0-2)Total/NA Soil 8260B 259059490-81215-11 TP-13 (0-2)Total/NA Soil 8260B 259059490-81215-12 TP-13 (10-11)Total/NA Solid 8260BLCS 490-259533/4 Lab Control Sample Total/NA Solid 8260BLCSD 490-259533/5 Lab Control Sample Dup Total/NA Solid 8260BMB 490-259533/7 Method Blank Total/NA GC/MS Semi VOA Prep Batch: 259662 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3550C490-80471-A-1-B MS Matrix Spike Total/NA Solid 3550C490-80471-A-1-C MSD Matrix Spike Duplicate Total/NA Soil 3550C490-81215-1 TP-8 (0-2)Total/NA Soil 3550C490-81215-2 TP-8 (8-10)Total/NA Soil 3550C490-81215-3 TP-11 (0-2)Total/NA Soil 3550C490-81215-4 TP-5 (0-2)Total/NA Soil 3550C490-81215-5 TP-6 (0-2)Total/NA Soil 3550C490-81215-6 TP-6 (8-10)Total/NA Soil 3550C490-81215-7 TP-7 (0-2)Total/NA Soil 3550C490-81215-8 TP-9 (8-10)Total/NA Soil 3550C490-81215-10 TP-12 (0-2)Total/NA Soil 3550C490-81215-11 TP-13 (0-2)Total/NA Soil 3550C490-81215-12 TP-13 (10-11)Total/NA Solid 3550CLCS 490-259662/2-A Lab Control Sample Total/NA Solid 3550CLCSD 490-259662/3-A Lab Control Sample Dup Total/NA Solid 3550CMB 490-259662/1-A Method Blank Total/NA TestAmerica Nashville Page 79 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC GC/MS Semi VOA (Continued) Analysis Batch: 260013 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270D 259662490-80471-A-1-B MS Matrix Spike Total/NA Solid 8270D 259662490-80471-A-1-C MSD Matrix Spike Duplicate Total/NA Solid 8270D 259662LCS 490-259662/2-A Lab Control Sample Total/NA Solid 8270D 259662LCSD 490-259662/3-A Lab Control Sample Dup Total/NA Solid 8270D 259662MB 490-259662/1-A Method Blank Total/NA Analysis Batch: 260226 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 8270D 259662490-81215-1 TP-8 (0-2)Total/NA Soil 8270D 259662490-81215-2 TP-8 (8-10)Total/NA Soil 8270D 259662490-81215-3 TP-11 (0-2)Total/NA Soil 8270D 259662490-81215-4 TP-5 (0-2)Total/NA Soil 8270D 259662490-81215-5 TP-6 (0-2)Total/NA Soil 8270D 259662490-81215-6 TP-6 (8-10)Total/NA Soil 8270D 259662490-81215-7 TP-7 (0-2)Total/NA Soil 8270D 259662490-81215-8 TP-9 (8-10)Total/NA Soil 8270D 259662490-81215-10 TP-12 (0-2)Total/NA Soil 8270D 259662490-81215-11 TP-13 (0-2)Total/NA Soil 8270D 259662490-81215-12 TP-13 (10-11)Total/NA Metals Prep Batch: 259128 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B490-80975-G-6-C MS Matrix Spike Total/NA Solid 7471B490-80975-G-6-D MSD Matrix Spike Duplicate Total/NA Soil 7471B490-81215-1 TP-8 (0-2)Total/NA Soil 7471B490-81215-2 TP-8 (8-10)Total/NA Soil 7471B490-81215-3 TP-11 (0-2)Total/NA Soil 7471B490-81215-4 TP-5 (0-2)Total/NA Soil 7471B490-81215-5 TP-6 (0-2)Total/NA Soil 7471B490-81215-6 TP-6 (8-10)Total/NA Soil 7471B490-81215-7 TP-7 (0-2)Total/NA Soil 7471B490-81215-8 TP-9 (8-10)Total/NA Soil 7471B490-81215-10 TP-12 (0-2)Total/NA Soil 7471B490-81215-11 TP-13 (0-2)Total/NA Soil 7471B490-81215-12 TP-13 (10-11)Total/NA Solid 7471BLCS 490-259128/2-A Lab Control Sample Total/NA Solid 7471BMB 490-259128/1-A Method Blank Total/NA Prep Batch: 259251 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 3051A490-81215-1 TP-8 (0-2)Total/NA Soil 3051A490-81215-1 MS TP-8 (0-2)Total/NA Soil 3051A490-81215-1 MSD TP-8 (0-2)Total/NA Soil 3051A490-81215-2 TP-8 (8-10)Total/NA Soil 3051A490-81215-3 TP-11 (0-2)Total/NA Soil 3051A490-81215-4 TP-5 (0-2)Total/NA Soil 3051A490-81215-5 TP-6 (0-2)Total/NA Soil 3051A490-81215-6 TP-6 (8-10)Total/NA TestAmerica Nashville Page 80 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Metals (Continued) Prep Batch: 259251 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 3051A490-81215-7 TP-7 (0-2)Total/NA Soil 3051A490-81215-8 TP-9 (8-10)Total/NA Soil 3051A490-81215-10 TP-12 (0-2)Total/NA Soil 3051A490-81215-11 TP-13 (0-2)Total/NA Soil 3051A490-81215-12 TP-13 (10-11)Total/NA Solid 3051ALCS 490-259251/2-A Lab Control Sample Total/NA Solid 3051AMB 490-259251/1-A Method Blank Total/NA Analysis Batch: 259614 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 6010C 259251490-81215-1 TP-8 (0-2)Total/NA Soil 6010C 259251490-81215-1 MS TP-8 (0-2)Total/NA Soil 6010C 259251490-81215-1 MSD TP-8 (0-2)Total/NA Soil 6010C 259251490-81215-2 TP-8 (8-10)Total/NA Soil 6010C 259251490-81215-3 TP-11 (0-2)Total/NA Soil 6010C 259251490-81215-4 TP-5 (0-2)Total/NA Soil 6010C 259251490-81215-5 TP-6 (0-2)Total/NA Soil 6010C 259251490-81215-6 TP-6 (8-10)Total/NA Soil 6010C 259251490-81215-7 TP-7 (0-2)Total/NA Soil 6010C 259251490-81215-8 TP-9 (8-10)Total/NA Soil 6010C 259251490-81215-10 TP-12 (0-2)Total/NA Soil 6010C 259251490-81215-11 TP-13 (0-2)Total/NA Soil 6010C 259251490-81215-12 TP-13 (10-11)Total/NA Solid 6010C 259251LCS 490-259251/2-A Lab Control Sample Total/NA Solid 6010C 259251MB 490-259251/1-A Method Blank Total/NA Analysis Batch: 259797 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 259128490-80975-G-6-C MS Matrix Spike Total/NA Solid 7471B 259128490-80975-G-6-D MSD Matrix Spike Duplicate Total/NA Soil 7471B 259128490-81215-1 TP-8 (0-2)Total/NA Soil 7471B 259128490-81215-2 TP-8 (8-10)Total/NA Soil 7471B 259128490-81215-3 TP-11 (0-2)Total/NA Soil 7471B 259128490-81215-4 TP-5 (0-2)Total/NA Soil 7471B 259128490-81215-5 TP-6 (0-2)Total/NA Soil 7471B 259128490-81215-6 TP-6 (8-10)Total/NA Soil 7471B 259128490-81215-7 TP-7 (0-2)Total/NA Soil 7471B 259128490-81215-8 TP-9 (8-10)Total/NA Soil 7471B 259128490-81215-10 TP-12 (0-2)Total/NA Soil 7471B 259128490-81215-11 TP-13 (0-2)Total/NA Soil 7471B 259128490-81215-12 TP-13 (10-11)Total/NA Solid 7471B 259128LCS 490-259128/2-A Lab Control Sample Total/NA Solid 7471B 259128MB 490-259128/1-A Method Blank Total/NA General Chemistry Analysis Batch: 258926 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture490-81189-A-1 MS Matrix Spike Total/NA Solid Moisture490-81189-A-1 MSD Matrix Spike Duplicate Total/NA TestAmerica Nashville Page 81 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC General Chemistry (Continued) Analysis Batch: 258926 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil Moisture490-81215-1 TP-8 (0-2)Total/NA Soil Moisture490-81215-1 DU TP-8 (0-2)Total/NA Soil Moisture490-81215-2 TP-8 (8-10)Total/NA Soil Moisture490-81215-3 TP-11 (0-2)Total/NA Soil Moisture490-81215-4 TP-5 (0-2)Total/NA Soil Moisture490-81215-5 TP-6 (0-2)Total/NA Soil Moisture490-81215-6 TP-6 (8-10)Total/NA Soil Moisture490-81215-7 TP-7 (0-2)Total/NA Soil Moisture490-81215-8 TP-9 (8-10)Total/NA Soil Moisture490-81215-9 TP-11 (6-13)Total/NA Soil Moisture490-81215-10 TP-12 (0-2)Total/NA Soil Moisture490-81215-11 TP-13 (0-2)Total/NA Soil Moisture490-81215-12 TP-13 (10-11)Total/NA Leach Batch: 259766 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil DI Leach490-81215-9 TP-11 (6-13)Soluble Solid DI Leach490-81306-A-1-C DU Duplicate Soluble Analysis Batch: 259987 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 9045D 259766490-81215-9 TP-11 (6-13)Soluble Solid 9045D 259766490-81306-A-1-C DU Duplicate Soluble Solid 9045DLCS 490-259987/12 Lab Control Sample Total/NA Prep Batch: 260615 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 3060A490-81215-1 TP-8 (0-2)Total/NA Soil 3060A490-81215-2 TP-8 (8-10)Total/NA Soil 3060A490-81215-3 TP-11 (0-2)Total/NA Soil 3060A490-81215-4 TP-5 (0-2)Total/NA Soil 3060A490-81215-5 TP-6 (0-2)Total/NA Soil 3060A490-81215-6 TP-6 (8-10)Total/NA Soil 3060A490-81215-7 TP-7 (0-2)Total/NA Soil 3060A490-81215-8 TP-9 (8-10)Total/NA Soil 3060A490-81215-10 TP-12 (0-2)Total/NA Soil 3060A490-81215-11 TP-13 (0-2)Total/NA Soil 3060A490-81215-12 TP-13 (10-11)Total/NA Solid 3060A490-81218-D-1-C DU Duplicate Total/NA Solid 3060A490-81218-D-1-D MSI Matrix Spike Total/NA Solid 3060A490-81218-D-1-E MSS Matrix Spike Total/NA Solid 3060ALCSI 490-260615/4-A Lab Control Sample Total/NA Solid 3060ALCSS 490-260615/2-A Lab Control Sample Total/NA Solid 3060ALCSSD 490-260615/3-A Lab Control Sample Dup Total/NA Solid 3060AMB 490-260615/1-A Method Blank Total/NA Analysis Batch: 261360 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 7196A 260615490-81215-1 TP-8 (0-2)Total/NA Soil 7196A 260615490-81215-2 TP-8 (8-10)Total/NA Soil 7196A 260615490-81215-3 TP-11 (0-2)Total/NA TestAmerica Nashville Page 82 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC General Chemistry (Continued) Analysis Batch: 261360 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Soil 7196A 260615490-81215-4 TP-5 (0-2)Total/NA Soil 7196A 260615490-81215-5 TP-6 (0-2)Total/NA Soil 7196A 260615490-81215-6 TP-6 (8-10)Total/NA Soil 7196A 260615490-81215-7 TP-7 (0-2)Total/NA Soil 7196A 260615490-81215-8 TP-9 (8-10)Total/NA Soil 7196A 260615490-81215-10 TP-12 (0-2)Total/NA Soil 7196A 260615490-81215-11 TP-13 (0-2)Total/NA Soil 7196A 260615490-81215-12 TP-13 (10-11)Total/NA Solid 7196A 260615490-81218-D-1-C DU Duplicate Total/NA Solid 7196A 260615490-81218-D-1-D MSI Matrix Spike Total/NA Solid 7196A 260615490-81218-D-1-E MSS Matrix Spike Total/NA Solid 7196A 260615LCSI 490-260615/4-A Lab Control Sample Total/NA Solid 7196A 260615LCSS 490-260615/2-A Lab Control Sample Total/NA Solid 7196A 260615LCSSD 490-260615/3-A Lab Control Sample Dup Total/NA Solid 7196A 260615MB 490-260615/1-A Method Blank Total/NA TestAmerica Nashville Page 83 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Client Sample ID: TP-8 (0-2)Lab Sample ID: 490-81215-1 Matrix: SoilDate Collected: 06/22/15 10:10 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-8 (0-2)Lab Sample ID: 490-81215-1 Matrix: SoilDate Collected: 06/22/15 10:10 Percent Solids: 83.5Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 10:10 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.139 g 5.0 mL Analysis 8260B 1 259533 06/26/15 04:39 KKK TAL NSHTotal/NA 5.139 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 36.21 g 1 mL Analysis 8270D 200 260226 06/28/15 11:45 SNR TAL NSHTotal/NA 36.21 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.518 g 100 mL Analysis 6010C 1 259614 06/25/15 15:09 LEG TAL NSHTotal/NA 0.518 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.614 g 100 mL Analysis 7471B 1 259797 06/26/15 10:54 CME TAL NSHTotal/NA 0.614 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.6015 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.6015 g 500 mL Client Sample ID: TP-8 (8-10)Lab Sample ID: 490-81215-2 Matrix: SoilDate Collected: 06/22/15 10:15 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-8 (8-10)Lab Sample ID: 490-81215-2 Matrix: SoilDate Collected: 06/22/15 10:15 Percent Solids: 77.8Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 10:15 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.068 g 5.0 mL Analysis 8260B 1 259533 06/26/15 05:09 KKK TAL NSHTotal/NA 6.068 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 38.59 g 1 mL Analysis 8270D 5 260226 06/28/15 12:09 SNR TAL NSHTotal/NA 38.59 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.502 g 100 mL Analysis 6010C 1 259614 06/25/15 15:30 LEG TAL NSHTotal/NA 0.502 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.610 g 100 mL Analysis 7471B 1 259797 06/26/15 10:56 CME TAL NSHTotal/NA 0.610 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5657 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5657 g 500 mL TestAmerica Nashville Page 84 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Client Sample ID: TP-11 (0-2)Lab Sample ID: 490-81215-3 Matrix: SoilDate Collected: 06/22/15 12:15 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-11 (0-2)Lab Sample ID: 490-81215-3 Matrix: SoilDate Collected: 06/22/15 12:15 Percent Solids: 87.9Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 12:15 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.183 g 5.0 mL Analysis 8260B 1 259533 06/26/15 05:39 KKK TAL NSHTotal/NA 6.183 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 34.77 g 1 mL Analysis 8270D 5 260226 06/28/15 12:33 SNR TAL NSHTotal/NA 34.77 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.498 g 100 mL Analysis 6010C 1 259614 06/25/15 15:34 LEG TAL NSHTotal/NA 0.498 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.609 g 100 mL Analysis 7471B 1 259797 06/26/15 11:03 CME TAL NSHTotal/NA 0.609 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5940 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5940 g 500 mL Client Sample ID: TP-5 (0-2)Lab Sample ID: 490-81215-4 Matrix: SoilDate Collected: 06/22/15 14:20 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-5 (0-2)Lab Sample ID: 490-81215-4 Matrix: SoilDate Collected: 06/22/15 14:20 Percent Solids: 81.6Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 14:20 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 4.9 g 5.0 mL Analysis 8260B 1 259533 06/26/15 06:09 KKK TAL NSHTotal/NA 4.9 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 36.91 g 1 mL Analysis 8270D 1 260226 06/28/15 12:57 SNR TAL NSHTotal/NA 36.91 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.506 g 100 mL Analysis 6010C 1 259614 06/25/15 15:47 LEG TAL NSHTotal/NA 0.506 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.602 g 100 mL Analysis 7471B 1 259797 06/26/15 11:05 CME TAL NSHTotal/NA 0.602 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5460 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5460 g 500 mL TestAmerica Nashville Page 85 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Client Sample ID: TP-6 (0-2)Lab Sample ID: 490-81215-5 Matrix: SoilDate Collected: 06/22/15 15:10 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-6 (0-2)Lab Sample ID: 490-81215-5 Matrix: SoilDate Collected: 06/22/15 15:10 Percent Solids: 86.1Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 15:10 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 7.168 g 5.0 mL Analysis 8260B 1 259533 06/26/15 06:39 KKK TAL NSHTotal/NA 7.168 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 34.96 g 1 mL Analysis 8270D 5 260226 06/28/15 13:21 SNR TAL NSHTotal/NA 34.96 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.500 g 100 mL Analysis 6010C 1 259614 06/25/15 15:52 LEG TAL NSHTotal/NA 0.500 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.610 g 100 mL Analysis 7471B 1 259797 06/26/15 11:08 CME TAL NSHTotal/NA 0.610 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5876 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5876 g 500 mL Client Sample ID: TP-6 (8-10)Lab Sample ID: 490-81215-6 Matrix: SoilDate Collected: 06/22/15 15:15 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-6 (8-10)Lab Sample ID: 490-81215-6 Matrix: SoilDate Collected: 06/22/15 15:15 Percent Solids: 79.2Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 15:15 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.845 g 5.0 mL Analysis 8260B 1 259533 06/26/15 07:08 KKK TAL NSHTotal/NA 6.845 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 38.00 g 1 mL Analysis 8270D 1 260226 06/28/15 13:45 SNR TAL NSHTotal/NA 38.00 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.494 g 100 mL Analysis 6010C 1 259614 06/25/15 15:56 LEG TAL NSHTotal/NA 0.494 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.617 g 100 mL Analysis 7471B 1 259797 06/26/15 11:10 CME TAL NSHTotal/NA 0.617 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5520 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5520 g 500 mL TestAmerica Nashville Page 86 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Client Sample ID: TP-7 (0-2)Lab Sample ID: 490-81215-7 Matrix: SoilDate Collected: 06/22/15 15:45 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-7 (0-2)Lab Sample ID: 490-81215-7 Matrix: SoilDate Collected: 06/22/15 15:45 Percent Solids: 80.9Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 15:45 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.926 g 5.0 mL Analysis 8260B 1 259533 06/26/15 07:38 KKK TAL NSHTotal/NA 5.926 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 37.25 g 1 mL Analysis 8270D 5 260226 06/28/15 14:09 SNR TAL NSHTotal/NA 37.25 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.525 g 100 mL Analysis 6010C 1 259614 06/25/15 16:00 LEG TAL NSHTotal/NA 0.525 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.618 g 100 mL Analysis 7471B 1 259797 06/26/15 11:12 CME TAL NSHTotal/NA 0.618 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5100 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5100 g 500 mL Client Sample ID: TP-9 (8-10)Lab Sample ID: 490-81215-8 Matrix: SoilDate Collected: 06/22/15 16:25 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-9 (8-10)Lab Sample ID: 490-81215-8 Matrix: SoilDate Collected: 06/22/15 16:25 Percent Solids: 76.0Date Received: 06/24/15 08:30 Prep 5035 JLP06/22/15 16:25 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.242 g 5.0 mL Analysis 8260B 1 259533 06/26/15 08:09 KKK TAL NSHTotal/NA 6.242 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 39.75 g 1 mL Analysis 8270D 1 260226 06/28/15 14:33 SNR TAL NSHTotal/NA 39.75 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.503 g 100 mL Analysis 6010C 1 259614 06/25/15 16:04 LEG TAL NSHTotal/NA 0.503 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.608 g 100 mL Analysis 7471B 1 259797 06/26/15 11:15 CME TAL NSHTotal/NA 0.608 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5709 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5709 g 500 mL TestAmerica Nashville Page 87 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Client Sample ID: TP-11 (6-13)Lab Sample ID: 490-81215-9 Matrix: SoilDate Collected: 06/22/15 16:45 Date Received: 06/24/15 08:30 Leach DI Leach SJM06/26/15 12:37 TAL NSH259766 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Soluble 20 g 20 mL Analysis 9045D 1 259987 06/27/15 10:08 SJM TAL NSHSoluble20 g 20 mL Analysis Moisture 1 258926 06/24/15 09:47 MAA TAL NSHTotal/NA Client Sample ID: TP-12 (0-2)Lab Sample ID: 490-81215-10 Matrix: SoilDate Collected: 06/23/15 09:30 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-12 (0-2)Lab Sample ID: 490-81215-10 Matrix: SoilDate Collected: 06/23/15 09:30 Percent Solids: 78.0Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 09:30 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.325 g 5.0 mL Analysis 8260B 1 259533 06/26/15 08:40 KKK TAL NSHTotal/NA 6.325 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 38.72 g 1 mL Analysis 8270D 5 260226 06/28/15 14:57 SNR TAL NSHTotal/NA 38.72 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.498 g 100 mL Analysis 6010C 1 259614 06/25/15 16:09 LEG TAL NSHTotal/NA 0.498 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.607 g 100 mL Analysis 7471B 1 259797 06/26/15 11:17 CME TAL NSHTotal/NA 0.607 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5403 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5403 g 500 mL Client Sample ID: TP-13 (0-2)Lab Sample ID: 490-81215-11 Matrix: SoilDate Collected: 06/23/15 10:15 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-13 (0-2)Lab Sample ID: 490-81215-11 Matrix: SoilDate Collected: 06/23/15 10:15 Percent Solids: 87.1Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 10:15 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.23 g 5.0 mL Analysis 8260B 1 259533 06/26/15 09:09 KKK TAL NSHTotal/NA 6.23 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 34.48 g 1 mL Analysis 8270D 5 260226 06/28/15 15:21 SNR TAL NSHTotal/NA 34.48 g 1 mL TestAmerica Nashville Page 88 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Prep 3051A ZLN06/25/15 08:59 TAL NSH259251 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 0.502 g 100 mL Analysis 6010C 1 259614 06/25/15 16:13 LEG TAL NSHTotal/NA 0.502 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.611 g 100 mL Analysis 7471B 1 259797 06/26/15 00:06 CME TAL NSHTotal/NA 0.611 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5392 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5392 g 500 mL Client Sample ID: TP-13 (10-11)Lab Sample ID: 490-81215-12 Matrix: SoilDate Collected: 06/23/15 10:20 Date Received: 06/24/15 08:30 Analysis Moisture MAA06/24/15 09:471 TAL NSH258926 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: TP-13 (10-11)Lab Sample ID: 490-81215-12 Matrix: SoilDate Collected: 06/23/15 10:20 Percent Solids: 80.9Date Received: 06/24/15 08:30 Prep 5035 JLP06/23/15 10:20 TAL NSH259059 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 4.982 g 5.0 mL Analysis 8260B 1 259533 06/26/15 09:39 KKK TAL NSHTotal/NA 4.982 g 5.0 mL Prep 3550C 259662 06/26/15 09:17 LDC TAL NSHTotal/NA 37.50 g 1 mL Analysis 8270D 5 260226 06/28/15 15:44 SNR TAL NSHTotal/NA 37.50 g 1 mL Prep 3051A 259251 06/25/15 08:59 ZLN TAL NSHTotal/NA 0.520 g 100 mL Analysis 6010C 1 259614 06/25/15 16:17 LEG TAL NSHTotal/NA 0.520 g 100 mL Prep 7471B 259128 06/24/15 16:44 RDF TAL NSHTotal/NA 0.612 g 100 mL Analysis 7471B 1 259797 06/26/15 00:08 CME TAL NSHTotal/NA 0.612 g 100 mL Prep 3060A 260615 06/29/15 16:57 BLM TAL NSHTotal/NA 2.5953 g 500 mL Analysis 7196A 1 261360 07/01/15 18:21 BLM TAL NSHTotal/NA 2.5953 g 500 mL Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 89 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Method Summary TestAmerica Job ID: 490-81215-1Client: Hart & Hickman, PC SDG: CRE-001Project/Site: NODA Greenway, Charlotte NC Method Method Description LaboratoryProtocol SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH SW8466010CMetals (ICP)TAL NSH SW8467471BMercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)TAL NSH SW8467196AChromium, Hexavalent TAL NSH SW8469045DpH TAL NSH EPAMoisturePercent Moisture TAL NSH Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 90 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Certification Summary Client: Hart & Hickman, PC TestAmerica Job ID: 490-81215-1 Project/Site: NODA Greenway, Charlotte NC SDG: CRE-001 Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification ID Expiration Date North Carolina (WW/SW)3874State Program 12-31-15 Analysis Method Prep Method Matrix Analyte The following analytes are included in this report, but certification is not offered by the governing authority: 9045D Soil Temperature Moisture Soil Percent Solids TestAmerica Nashville Page 91 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 92 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 93 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 94 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Login Sample Receipt Checklist Client: Hart & Hickman, PC Job Number: 490-81215-1 SDG Number: CRE-001 Login Number: 81215 Question Answer Comment Creator: McBride, Mike List Source: TestAmerica Nashville List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.1.6 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time. TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. TestAmerica Nashville Page 95 of 95 7/2/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 ATTACHMENT 5 DENR BROWNFIELDS EMAIL CORRESPONDANCE From: Minnich, Carolyn [mailto:carolyn.minnich@ncdenr.gov] Sent: Friday, June 19, 2015 9:06 AM To: Matt Bramblett Cc: Brett Lawrence; Joselyn Harriger Subject: RE: Abernethy Brownfields Site Test Pits Thank you for following up with me today. The scope of work is acceptable and approved. In the previous soil sampling, we had agreed the metals were likely naturally occurring. This included arsenic, manganese, & thallium. Please follow up with me a needed if new contamination is discovered on the brownfields property during redevelopment. Thank you. CFM Carolyn Minnich, Brownfields Project Manager www.ncbrownfields.org 704/661-0330 _____________________________________________________________________________________________________________________________________________________________________________________________________________ Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the content is exempt by statute or other regulation. From: Matt Bramblett [mailto:MBramblett@harthickman.com] Sent: Monday, June 15, 2015 3:14 PM To: Minnich, Carolyn Cc: Brett Lawrence; Joselyn Harriger Subject: Abernethy Brownfields Site Test Pits Hi Carolyn, Joselyn is on maternity leave, and I am filling in on the Abernethy Brownfields project (#18015-14- 060). During some recent geotechnical borings, extensive fill was found on and near this site. In order to further assess the areas of fill and to evaluate the nature of fill, H&H proposes to excavate 4 test pits and collect soil samples (see attached location map). The test pits will be logged for lithology, including types of fill material observed, and photographed to document subsurface conditions. H&H will use a trackhoe capable of excavation to depths near 20 ft to attempt to find the base of the fill materials. Soils from the test pits will be screened in the field for the presence of odors, staining, and/or elevated photoionization detector (PID) readings. Based on field screening and materials encountered during excavation activities, a total of approximately 3 to 4 soil samples will be collected from the test pits and submitted to a North Carolina certified laboratory for analysis of volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs), and hazardous substance list (HSL) metals plus hexavalent chromium by 6010/7470/7196. Approximately 2 of these soil samples will be taken from a surficial (0 to 2 ft) interval. The test pits will be backfilled utilizing the removed materials. I think that you and Joselyn had conferred on previous metal detections on the west side of the Abernethy Brownfields site and agreed that the metal detections were likely naturally occurring. Therefore, in addition to helping to characterize the fill, the proposed soil samples will be useful in further evaluating metal concentrations as naturally occurring. We are going to conduct the test pits on June 22 and 23. Because this is supplemental information, which post-dates the Brownfields Agreement, we are planning to move forward with this work. However, if you have time to consider and approve this work soon, that would be super. Thanks, Matt Matt Bramblett, PE, Principal Hart & Hickman, PC | 2923 South Tryon Street, Suite 100 | Charlotte, NC 28203 Direct 704-887-4620 | Mobile 704-560-8009 | Main 704-586-0007 www.harthickman.com