9606_WayneCountySubtitleD_August2017GW_DIN27582_201612

Wayne County Subtitle D Lined MSWLF
Dudley, North Carolina
August 2016
MESCO Project Number: G16016.0
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.
Garner and Boone, North Carolina
P.O. Box 97
Garner, NC 27529
License No. C-0281

Permit Number: 96-06
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Above Standards Page 2
Surface Water Samples Above Standards Page 3
Leachate Samples Page 3
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 4
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer Figure 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections in Water Samples Above SWSL, GWP, 2L, 2B or MCL (Appendix 1) Table 5
Detections in Water Samples Above MDL (Appendix II) Table 6
Detections in Leachate Samples above SWSL, GWP or 2L Table 7
Hydrologic Properties at Monitoring Well Locations Table 8
Total Metal Concentrations Evaluation Table Table 9
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
December 26, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Wayne County Subtitle D Lined MSWLF
Permit No. 96-06
MESCO Project No. G16016.0
Event Date(s): August 22, 30-September 1, 2016
Dear Ms. Drummond,
Introduction
On behalf of Wayne County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the summer 2016 event performed at the Wayne County Subtitle D Lined
Municipal Solid Waste Landfill (MSWLF). NCDENR Solid Waste Rules 15A NCAC 13B.1632 require that Wayne
County provide this report to the NC SWS on a semi-annual basis. This report documents the quality of the
groundwater, surface waters and leachate during the monitoring event performed on August 22, 30-September 1,
2016.
During this event assessment monitoring was initiated which entailed analysis of all groundwater samples for the
Appendix II constituents listed in 40 CFR 258 in response to detections of benzene in samples collected from MW-
13. Inorganic parameters were detected in most of the groundwater samples. Metals were detected in excess of
their respective groundwater Standard six times including the background well. Total cadmium was detected above
the surface water Standard in samples collected upstream and downstream of the landfill. The preliminary source
assigned to the metal detections is erosion of natural deposits. Benzene was detected above the 2L Standard in
sample MW-13 for the third consecutive event. The preliminary source of benzene is likely anthropogenic.
Contaminants in the untreated leachate samples remain low relative to Standards and published values.
Background
The Wayne County Subtitle D lined MSWLF, permit #96-06 (Phases 1-3), is located at 460-B South Landfill Road,
Dudley, Wayne County, North Carolina. The lined MSWLF is comprised of contiguous Phases 1, 2 & 3 which
are treated as a single unit in this report. Phase 3 was granted a Permit to Operate (PTO) on June 11, 2013 and at the
time of this event waste had been placed upon most of the liner except for the west sump.
The lined landfill is located west and beyond a perennial local discharge feature from a C&D landfill operating upon
an unlined landfill which is monitored separately under Permit #96-01. The site location topographic map is
depicted in the attached Figure 1.
Water quality at this facility has been monitored at least semi-annually including several pre-operation baseline
events with complete historical data available since prior to operation of Phase 1 in 1997. This event was performed
in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the
permit to operate.

As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Well construction summary table, field observations table, field parameter data table, sampling
and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates table,
potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed herein.
Sampling Procedure
Samples were collected in accordance with the Ground and Surface Water Sampling & Analysis Plan (SAP) [DIN
13717] dated April 25, 2011 and approved by the SWS on May 19, 2011 [DIN 13957]. The site specific SAP
includes water sample collection and analysis from twelve downgradient monitoring wells (MW-2 through MW-
16R), one background well (MW-1), four surface water locations (SW-2, SW-3, SW-4 and SW-5) and a leachate
sample (LE-1). Surface water point SW-1, located downstream of SW-3, monitors the unnamed tributary of
Edward's Branch as part of the separate SAP for the adjacent Active C&D and Closed MSWLF. Results of SW-1
are also presented in this report due to the shared discharge features. Quality control measures, which included
analysis of equipment blank samples (EB), field blank samples (FB), and trip blank samples (TB) were also
reported. Monitoring locations are depicted on the potentiometric map of the uppermost aquifer, Figure 2.
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated with deficiencies rectified as documented on Table 2.
The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low-flow pumping methodology or bailing was used to adequately purge the wells to a minimum of three times the
volume of standing water in the well or until dry. Surface water samples were dipped from the surface at previously
designated locations. During well purging and surface water sample collection the required field parameters were
recorded. The samples were then placed into laboratory-prepared, pre-preserved containers via a new disposable
polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-certified laboratory under proper
chain of custody (C-O-C) protocols and analyzed within the proper hold-times.
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature and
visual turbidity. A summary of the field parameter data is presented in Table 3 and the field sampling data sheet is
enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the laboratory analysis.
Groundwater samples were analyzed for the constituents listed in 40 CFR 258 Appendix II. Surface water samples
were tested for parameters listed in listed in 40 CFR 258 Appendix I. Leachate samples (LE-1) were analyzed for a
leachate specific list that includes Appendix I parameters, nitrate, phosphorus, chemical oxygen demand (COD),
biological oxygen demand (BOD), sulfate, and pH. A sampling and analysis table summarizing the locations,
constituents, and methods is presented on Table 4.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards
(GWP), North Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B)
for a class C waterbody, and Federally established Maximum Contaminant Levels (MCL) also known as “Primary
Drinking Water Standards”. MCL Standards are not applicable for regulatory compliance at this facility rather to
underscore the fact that 2L Standards are more stringent than MCL Standard for 37 constituents. Table 6 shows the
Appendix II exclusive (defined in this report as not also listed in Appendix I) constituents detected above the MDL.
Laboratory results and C-O-Cs are presented in Appendix A.
2
Quality Control Samples
Total tin was the only constituent detected in the quality control blanks (FB and EB). Since the Appendix II
exclusive parameter tin was also only detected in MW-3 at a very low “j-qualified” concentration any potential
artifact contamination is largely non-consequential.
Groundwater Samples Above Standards
Total cadmium was detected in samples MW-8 (3.5 µg/L), MW-14 (4.0 µg/L) above the 2L Standard (2.0 µg/L).
Dissolved cadmium was found in sample MW-11 (4.0 µg/L) but not detected in the total form (<2.5 µg/L) which
may indicate false positive or high bias attributed to lab filtration. Total vanadium was detected in sample MW-16R
(5.5j µg/L) and background well MW-1 (46.3 µg/L) above the GWP (3.5 µg/L). Further analysis indicated that
dissolved (lab filtered) vanadium was not detected in MW-16R. Total thallium was detected in sample MW-2 (5.2j
µg/L) above the GWP (0.28 µg/L) and MCL (2.0 µg/L) but below the SWSL (5.5 µg/L) thus “j-qualified”.
Benzene was detected in sample MW-13 (1.9 µg/L) slightly above the 2L Standard (1.0 µg/L).
Supplemental samples (chloride and dissolved methane) were collected from MW-13 and background well MW-1 in
an effort to determine whether the source is leachate or LFG. MW-13 had chloride levels 9 mg/L (> 3 times) and
methane levels 4.34 mg/L (868 times) compared to background levels.
Surface Water Samples Above Standards
Total cadmium was detected in downstream sample SW-4 (2.3 µg/L) and upstream sample SW-5 (4.3 µg/L) above
the 2B Standard (2.0 µg/L).
Leachate Samples
Leachate sample LE-1 contained quantifiable concentrations of four metals and five VOCs as presented in Table 7.
Cadmium, the most common metal detected in ground and surface water samples, has never been detected in any of
the more than 150 leachate samples collected over the last 19 years. Contaminant levels in the untreated leachate
samples are low compared to typical published values which is consistent with historical results.
Groundwater and Surface Water Characterization
MESCO prepared a potentiometric map using groundwater elevation data from the uppermost aquifer measured
during this event (Figure 2). Groundwater velocity rates and directions were calculated and are included on Table
8. Consistent with historical observations groundwater flows from the southwest towards Edward's Branch, which
serves as the local discharge feature. Groundwater velocity rates ranged from 2 feet/year (MW-15) to 90 feet/year
(MW-13) averaging approximately 25 feet/year which is also consistent with historical calculations. Streams
located within the facility boundaries were visually observed at low seasonal flow, low volume and low turbidity.
Findings
The inorganic detections are not believed to have originated from anthropogenic sources rather a product of erosion
of natural deposits. All metal concentrations that were above a Standard were below the all time highest observed
levels in the background well or upstream surface water point and above the all time highest observed level in the
leachate after applying a 20:1 dilution (Table 9). An Alternative Source Demonstration (ASD) addressing the
inorganic detections is planned to be submitted prior to the February 6, 2017 deadline.
Benzene was detected in excess of the 2L Standard during this and the previous two events. MW-13 is located
cross-gradient and within the lined Phase 2 relevant compliance boundary. Landfill gas (LFG) has been detected in
the vadose near MW-13. The preliminary source of benzene detected in MW-13 is likely anthropogenic with a
transport mechanism of either leachate and/or LFG. The elevated chloride levels observed in sample MW-13
typically indicates a leachate source. However; the highly-elevated dissolved methane levels as found in MW-13
may indicate LFG as the source or indicative of microbial degradation of hydrocarbons. Since the supplemental
results may be considered contradictory a definitive source is undetermined at this time. The area will be further
3
assessed to determine the most probable source and corrective actions are planned to be implemented as necessary.
Closing
Wayne County will continue semi-annual water quality monitoring with the next event scheduled for February 2017.
If you have any questions or comments regarding this report, please contact us at [phone] or by email at
[e-mail] .
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
Jonathan Pfohl Steven R. Gandy, Ph.D, P.E.
Senior Environmental Specialist Senior Project Manager
Enclosures
cc: Mr. Tim Rogers
Wayne County

Ms. Christine Ritter
Solid Waste Section
4
Figures
Topographic Map with Site Location
01 1 MILE
FIGURE 1
Wayne County Landfill North Carolina (Dudley)
CLOSED MSW FACILITY
SUBTITLE D MSW
LANDFILL FACILITY
460 B South Landfill Rd
Dudley, NC 28333
Lat:35-17-19.1338
Long:-78-04-17.2971
Northing:561283.19
Easting:2277068.62
N
Tables
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
August 30-31, 2016
Latitude Longitude
(inches)(ft)
MW-1 12/5/97 2 22.50 7.50 15 soil 164.51 161.95 149.35 15.16 35.2980417 78.0666750
MW-2 12/5/97 2 20.00 5.00 15 soil 147.27 144.63 137.11 10.16 35.2946417 78.0699806
MW-3 12/4/97 2 20.00 5.00 15 soil 141.13 136.40 132.82 8.31 35.2940694 78.0725889
MW-4 12/3/97 2 25.00 10.00 15 soil 139.80 137.80 123.45 16.35 35.2934694 78.0756444
MW-5 12/3/97 2 23.00 8.00 15 soil 140.15 137.35 124.14 16.01 35.2941972 78.0757333
MW-6 12/3/97 2 25.00 10.00 15 soil 146.58 144.42 130.43 16.15 35.2946000 78.0741306
MW-7 12/4/97 2 20.00 5.00 15 soil 135.89 133.57 129.86 6.03 35.2878278 78.0740694
MW-8 12/18/97 2 20.00 5.00 15 soil 135.25 132.79 127.97 7.28 35.2973056 78.0733889
MW-9 12/4/97 2 23.00 8.00 15 soil 141.31 139.13 129.06 12.25 35.2939444 78.0739453
MW-10 12/4/97 2 23.00 8.00 15 soil 141.43 139.19 128.05 13.38 35.2937472 78.0747222
MW-11 4/15/04 2 15.49 5.49 10 soil 134.76 131.76 130.61 4.15 35.2980861 78.0729639
MW-12 4/15/04 2 16.45 6.45 10 soil 135.19 132.19 130.17 5.02 35.2991889 78.0727111
MW-13 4/15/04 2 15.85 5.85 10 soil 149.89 146.89 141.24 8.65 35.2952722 78.0687417
MW-14 9/21/06 2 21.24 6.24 15 soil 137.51 134.68 130.46 7.05 35.2998500 78.0728806
MW-15 9/26/06 2 16.17 6.17 10 soil 131.74 129.01 127.61 4.13 35.3006028 78.0727778
MW-16R 6/4/13 2 22.00 7.00 15 Soil sand 160.39 157.39 145.26 15.13 35.2962278 78.0673861
P-5 1/11/96 2 19.00 11.00 8 soil 159.42 156.25 144.66 14.76 35.3002167 78.0688833
P3-15S 9/21/06 2 16.53 6.53 10 soil 152.23 149.14 141.61 10.62 35.3005639 78.0700639
Monitoring Well Date Installed
Well
Diameter
Total
Well
Depth
Top of Screen
Depth
Screen
Length Geology of Screened Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of PVC well casing
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
August 30-31, 2016
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes Faint organic odor. Metal case lid repaired by County
MW-3 Yes Yes Yes Yes Yes Yes See comments below
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Yes ID tag re-installed
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes Tree across path
MW-8 Yes Yes Yes Yes Yes ?Pad covered with soil, reducing odor
MW-9 Yes Yes Yes Yes No Yes ID tag missing.
MW-10 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes ?Pad covered with soil, could hear water cascade
MW-12 Yes Yes Yes Yes Yes ?Pad covered with soil
MW-13 Yes Yes Yes Yes Yes ?Pad covered with soil
MW-14 Yes Yes Yes Yes Yes Yes
MW-15 Yes Yes Yes Yes Yes Yes
MW-16R Yes Yes Yes Yes Yes Yes
LE-1 Yes -----
SW-1 Yes -----Shared Downstream of SW-3
SW-3 No -----Shared Upstream furthest east Dry
SW-4 Yes -----
SW-5 Yes -----Upstream of facility
SW-6 Yes -----
Any unusual field conditions, observations, or events:
Phase 3 now in operation with waste covering the footprint except for far west sump.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Assumed
Effective
Ph 3 well. Bubbles in purge water (LFG?)
Ph 3 well
Ph 3 well. CH4 0% which is not typical
Leachate lagoon sample. Equal composite from 3 inverts
Downstream of Ph 1 on Edward's Branch
Adjoiner west of Edwards Branch across from Ph 2 & 3 has cleared forest since 9/12. Adjoiner may potentially impact wetlands.
County replaced pad and case around MW-3 in August 2013. Riser extended 2.63' so top of casing now 141.13 ft amsl.
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
August 30-31, 2016
Parameter Temp.ORP DO pH TDS Turbidity
Units C mg/L SU visual %/vol
MW-1 15.16 149.35 164.51 17.4 NR NR 4.1 24 NR Slight NR
MW-2 10.16 137.11 147.27 19.9 NR NR 5.9 554 NR Clear NR
MW-3 8.31 132.82 141.13 20.6 NR NR 5.6 356 NR Clear NR
MW-4 16.35 123.45 139.80 17.6 NR NR 4.1 33 NR Clear NR
MW-5 16.01 124.14 140.15 20.5 NR NR 5.0 23 NR Clear NR
MW-6 16.15 130.43 146.58 16.1 NR NR 5.1 19 NR Clear NR
MW-7 6.03 129.86 135.89 20.7 NR NR 5.7 203 NR Slight NR
MW-8 7.28 127.97 135.25 18.8 NR NR 4.7 43 NR Clear NR
MW-9 12.25 129.06 141.31 20.9 NR NR 4.5 54 NR Slight NR
MW-10 13.38 128.05 141.43 19.5 NR NR 4.3 49 NR Slight NR
MW-11 4.15 130.61 134.76 20.7 NR NR 4.8 32 NR Clear NR
MW-12 5.02 130.17 135.19 18.9 NR NR 4.9 134 NR Clear NR
MW-13 8.65 141.24 149.89 19.3 NR NR 3.9 85 NR Clear NR
MW-14 7.05 130.46 137.51 21.6 NR NR 4.2 70 NR Slight NR
MW-15 4.13 127.61 131.74 19.0 NR NR 5.1 51 NR Clear NR
MW-16R 15.13 145.26 160.39 18.4 NR NR 3.6 35 NR Clear Exists
Minimum 4.13 123.45 131.74 16.1 NR NR 3.6 19 NR Clear NR
Average 10.33 132.35 142.68 19.4 NR NR 4.7 110 NR Slight NR
Maximum 16.35 149.35 164.51 21.6 NR NR 5.9 554 NR Slight Exists
SW-1 ---22.1 NR NR 6.9 998 NR Slight NR
SW-2 ---NR NR NR NR NR NR NR NR
SW-3 ---NR NR NR NR NR NR NR NR
SW-4 ---25.3 NR NR 5.8 247 NR Clear NR
SW-5 ---25.6 NR NR 5.9 258 NR Clear NR
Minimum ---22.1 NR NR 5.8 247 NR Clear NR
Average ---24.3 NR NR 6.2 501 NR Clear NR
Maximum ---25.6 NR NR 6.9 998 NR Slight NR
NR = No Reading Attempted and not required
Exist = Visually observed LFG vapors (waves) from MW-16R
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane Gas
in Well
Headspace
ft (btoc)ft (amsl)ft (amsl)mV цs/cm ppb
Wayne County Subtitle D Lined MSWLF (Dudley)Page 1 of 1
Table 4
Sampling and Analysis Summary
August 22, 30-September 1, 2016
App. I CDLF Field Parameter App. II
T o t a l M e t a l s
D i s s o l v e d O x y g e n (D O )
O x i d a t i o n R e d u c t i o n P o t e n t i a l (O R P )
T e m p e r a t u r e
C o n d u c t i v i t y
T o t a l D i s s o l v e d S o l i d s (T D S )
p H T u r b i d i t y
T o t a l M e t a l s
D i s s o l v e d M e t a l s
P e s t i c i d e s
H e r b i c i d e s -C h l o r i n a t e d
T o t a l C y a n i d e
S u l f i d e
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 8 2 6 0 B
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
V i s u a l
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 8 0 8 1 B
L a b S W 8 1 5 1 A
L a b E P A 8 0 8 2 A
L a b E P A 8 2 7 0 D
L a b E P A 9 0 1 4
L a b S M 1 8 4 5 0 0 -S D
MW-1 x x x x x x x x x x x x
MW-2 x x x x x x x x x x x x
MW-3 x x x x x x x x x x x x x
MW-4 x x x x x x x x x x x x x
MW-5 x x x x x x x x x x x x
MW-6 x x x x x x x x x x x x
MW-7 x x x x x x x x x x x x
MW-8 x x x x x x x x x x x x
MW-9 x x x x x x x x x x x x x
MW-10 x x x x x x x x x x x x
MW-11 x x x x x x x x x x x x x
MW-12 x x x x x x x x x x x x x
MW-13 x x x x x x x x x x x x
MW-14 x x x x x x x x x x x x
MW-15 x x x x x x x x x x x x
MW-16R x x x x x x x x x x x x x
SW-1 x x x x x x x x x
SW-4 x x
SW-5 x x
SW-6 x x x x x x x
EB x x x
FB x x x
TB x x
App I & II = Appendix I & II List from current 40 CFR 258
V O C s
T e t r a h y d r o f u r a n
V O C s
P o l y c h l o r i n a t e d b i p h e n y l (P C B )
S e m i v o l a t i l e O r g a n i c s (S V O C s )
Wayne County Subtitle D MSWLF, Phases 1-3 Page 1 of 1
Table 5
August 22, 30-31, 2016
Result Unit
MW-1 Chromium, total 8/30/2016 19.8 2.5 10 10 100 N (is BG)
MW-1 Vanadium, total 8/30/2016 46.3 2.5 25 3.5 NE N (is BG)
MW-1 Zinc, total 8/30/2016 16.8 5 10 1000 NE
MW-2 Thallium, total 8/30/2016 5.2j 5 5.5 0.28 2 N (<BG>L)
MW-2 Zinc, total 8/30/2016 10.3 5 10 1000 NE
MW-5 Barium, total 8/30/2016 135 2.5 100 700 2000
MW-6 Cadmium, total 8/30/2016 1.1 0.5 1 2 5
MW-8 Cadmium, total 8/31/2016 3.5 0.5 1 2 5 N (<BG>L)
MW-9 Cadmium, total 8/31/2016 ND<2.5 0.5 1 2 5
MW-9 Cadmium, Dissolved 8/31/2016 1.3 0.5 1 2 5
MW-11 Cadmium, total 8/31/2016 ND<2.5 0.5 1 2 5
MW-11 Cadmium, Dissolved 8/31/2016 4 0.5 1 2 5 B (Lab)
MW-13 Benzene 8/22/2016 1.9 0.25 1 1 5 LFG
MW-14 Cadmium, total 8/31/2016 4 0.5 1 2 5 N (<BG>L)
MW-16R Vanadium, total 8/30/2016 5.5j 2.5 25 3.5 NE N (<BG>L)
MW-16R Vanadium, dissolved 8/30/2016 ND<2.5 2.5 25 3.5 NE
SW-4 Barium, total 8/31/2016 415 2.5 100 200000 2000
SW-4 Cadmium, total 8/31/2016 2.3 0.5 1 2 5 N
SW-5 Barium, total 8/31/2016 448 2.5 100 200000 2000
SW-5 Cadmium, total 8/31/2016 4.3 0.5 1 2 5 N (is BG)
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
(Lab) = Believed introduced in the lab (false positive). Specifically the filter as dissolved phase higher than total phase.
<BG = Below the highest level ever observed in the background well (MW-A).
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
Detections in Water Samples above SWSL, GWP, 2L, 2B or MCL (Appendix I)
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, 2B or MCL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Maximum Contaminant Level aka Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
B = Background as detected upgradient/upstream of facility
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
>L = Above the highest ever observed in leachate after a 20:1 dilution factor.
L = Leachate
Wayne County Subtitle D MSWLF, Phases 1-3 Page 1 of 1
Table 6
August 22, 30-September 1, 2016
Sample ID Result Unit
MW-1 Cyanide 8/30/2016 6.6j 4 10 70 200
MW-1 8/30/2016 23.5j 2.8 20 NE NE NE
MW-2 Cyanide 8/30/2016 4.3j 4 10 70 200
MW-2 8/30/2016 7j 0.84 20 NE NE NE
MW-3 Tin, Dissolved 8/31/2016 2.6j 2.5 100 NE NE NE
MW-3 Mercury, Dissolved 8/31/2016 0.23 0.09 0.2 1 2
MW-4 Mercury, Dissolved 8/31/2016 1.6 0.09 0.2 1 2
MW-4 Mercury, total 8/31/2016 1.2 0.1 0.2 1 2
MW-5 Cyanide 8/30/2016 6.1j 4 10 70 200
MW-6 Cyanide 8/30/2016 4j 4 10 70 200
MW-6 Mercury, total 8/30/2016 0.35 0.1 0.2 1 2
MW-6 8/30/2016 0.022j 0.02 25 NE NE NE
MW-7 Cyanide 8/30/2016 5.4j 4 10 70 200
MW-7 Mercury, total 8/30/2016 0.27 0.1 0.2 1 2
MW-7 8/30/2016 7j 0.84 20 NE NE NE
MW-9 Mercury, Dissolved 8/31/2016 0.23 0.09 0.2 1 2
MW-9 Mercury, total 8/31/2016 0.17j 0.1 0.2 1 2
MW-11 Mercury, Dissolved 8/31/2016 0.14j 0.09 0.2 1 2
MW-11 Mercury, total 8/31/2016 0.1j 0.1 0.2 1 2
MW-16R Cyanide 8/30/2016 6.7j 4 10 70 200
EB Tin, total 9/1/2016 2.9j 2.5 100 NE NE NE
FB Tin, total 9/1/2016 3.6j 2.5 100 NE NE NE
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
Detections in Water Samples Above MDL (Appendix II Exclusive)
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
2-Acetylaminofluorene ug/L
ug/L
2-Acetylaminofluorene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Pentachlorophenol ug/L
ug/L
ug/L
2-Acetylaminofluorene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains Appendix II exclusive constituents (not also listed on Appendix I) detected at or above MDL.
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Maximum Contaminant Level aka Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Wayne County Subtitle D MSWLF Page 1 of 1
Table 7
August 30, 2016
Result Unit
LE1 8/30/16 8.9 4.8 1 4.6
LE1 Benzene 8/30/16 1.6 1.2 1 1 5 221
LE1 Toluene 8/30/16 57.3 1.3 1 600 1016
LE1 8/30/16 1050 4.8 100 4200 4151
LE1 Acetone 8/30/16 604 50 100 6000 2163
LE1 Antimony, total 8/30/16 9.2 3.8 6 1.4 6 4520
LE1 Chromium, total 8/30/16 37.8 2.5 10 10 100
LE1 Vanadium, total 8/30/16 15.4j 2.5 25 3.5 NE 179
LE1 Zinc, total 8/30/16 1120 5 10 1000 NE 8320
LE1 Sulfate 8/30/16 41800j 5000 250000 250000 244000
LE1 pH 8/30/16 7.9 Std. Units 0.1 NE
LE1 Phosphorus 8/30/16 1020 25 NE
LE1 BOD, 5 day 8/30/16 392000 2000 NE 3837000
LE1 COD 8/30/16 1390000 12500 NE 4773000
j=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable.
NE = Not Established
BOLD =
Detections in Leachate Sample Above SWSL, 2L, GWP or MCL
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 GWP 5 MCL 6 “Average
Leachate” 7
Methylene Chloride ug/L
ug/L
ug/L
2-Butanone (MEK)ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains only constituents detected at or above SWSL, GWP, 2L, or MCL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit (Current as of Sampling Event)
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard (Current as of Sampling Event)
5 GWP = Groundwater Protection Standard (Current as of Sampling Event)
6 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
7 Average concentration of leachate from a comparable “Dry Tomb” Landfill published in 1988 by EPA document Summary of Data on MSWLF Leachate Characteristics
Concentration > 2L, GWP, MCL or “Average Leachate”
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 8
August 30-31, 2016
Flow Rate
(cm/sec)(%)(ft/ft)(ft/yr)
MW-1 3.21E-04 31 0.0113 12 S73E 15.16 149.35
MW-2 1.37E-03 31 0.0100 46 S66W 10.16 137.11
MW-3 9.72E-04 31 0.0079 26 S88W 8.31 132.82
MW-4 2.33E-04 9 0.0157 42 S74W 16.35 123.45
MW-5 1.45E-04 9 0.0157 26 S74W 16.01 124.14
MW-6 8.38E-05 31 0.0106 3 S89W 16.15 130.43
MW-7 6.84E-05 9 0.0038 3 N56W 6.03 129.86
MW-8 1.68E-04 9 0.0126 24 S71W 7.28 127.97
MW-9 6.37E-04 31 0.0143 30 S67W 12.25 129.06
MW-10 4.74E-04 31 0.0158 25 S75W 13.38 128.05
MW-11 1.46E-04 22 0.0125 9 S70W 4.15 130.61
MW-12 1.63E-04 22 0.0145 11 N84W 5.02 130.17
MW-13 2.14E-03 22 0.0090 90 S75W 8.65 141.24
MW-14 2.63E-04 22 0.0212 26 N54W 7.05 130.46
MW-15 1.82E-05 22 0.0208 2 N61W 4.13 127.61
MW-16R 22 0.0088 S38W 15.13 145.26
Minimum 1.82E-05 9 0.0038 2 -4.13 123.45
Average 4.80E-04 22 0.0128 25 -10.33 132.35
Maximum 2.14E-03 31 0.0212 90 -16.35 149.35
NOTE:
Hydraulic Conductivity values from slug tests performed on each monitoring well.
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation
(ft btoc)(ft amsl)
na na
Effective porosity values from Design Hydrogeologic Studies for Wayne County.
Hydrologic gradient calculated from groundwater elevations recorded on August 30-31, 2016.
Average Linear Velocity rate (Q) is defined by modified Darcy's equation:
K= hydraulic conductivity
ne= effective porosity
dh= head difference
dl= horizontal distance
Q=−K
ne
⋅dh
dl
Table 9
Total Metal Concentrations
Wayne Co. Subtitle D Lined MSWLF, Phases 1, 2 & 3
Total Metal An
t
i
m
o
n
y
Ar
s
e
n
i
c
Ba
r
i
u
m
Be
r
y
l
l
i
u
m
Ca
d
m
i
u
m
Ch
r
o
m
i
u
m
Co
b
a
l
t
Co
p
p
e
r
Le
a
d
Ni
c
k
e
l
Se
l
e
n
i
u
m
Si
l
v
e
r
Th
a
l
l
i
u
m
Va
n
a
d
i
u
m
Zi
n
c
SWSL 6 10 100 1 1 10 10 10 10 50 10 10 5.5 25 10
2L/GWP STANDARD
SAMPLE ID
Screened
Lithology Data Period
MW-1 (BG Well)Regolith All Time High <5 29.2 113 1.6 9.7 129 18 19.5 76 0.9 0.7 0.1 9.1 310 148.
MW-2 Regolith Max Baseline <30 <10 <500 4.91 <1 <10 <200 144.108 <50 <20 <10 <10 241 90.
MW-3 Regolith Max Baseline <30 <10 <500 <2 <1 <10 <200 25 22 <50 <20 <10 <10 <40 <50
MW-4 Regolith Max Baseline <30 143 <500 2.3 42 <200 105.43 <50 <20 <10 <10 177 145.
MW-5 Regolith Max Baseline <30 73 <500 <2 1.1 26 88 <10 32 <50 <20 <10 <10 172 94.
MW-6 Regolith Max Baseline <30 <10 <500 <2 <1 <10 <200 21.12 <50 <20 <10 <10 53 <50
MW-7 Regolith Max Baseline <30 35 <500 6.5 <1 10.<200 40.32 <50 <20 <10 <10 67 162.
MW-8 Regolith Max Baseline <30 39 <500 4.7 2.33 51 27.59 <50 <20 <10 <10 75 599.
MW-9 Regolith Max Baseline <30 <10 <500 <2 <1 <10 <200 35.25 <50 <20 <10 <10 <40 <50
MW-10 Regolith Max Baseline <30 <10 <500 <2 <1 <10 <200 28.25 <50 <20 <10 <10 <40 75.
MW-11 Regolith Max Baseline <30 <10 <500 <2 2.19 <10 <10 11 <50 <20 <10 <10 <40 <50
MW-12 Regolith Max Baseline <30 <10 967 3 <1 79 14 <200 <10 <50 <20 <10 <10 104 <50
MW-13 Regolith Max Baseline <30 14 <500 <2 <1 <10 <10 <200 49 <50 <20 <10 <10 <40 177
MW-14 Regolith Max Baseline <5 6.4 37.5 <1 <1 <5 <5 <5 <5 <5 6.6 <5 <10 <5 <10
MW-15 Regolith Max Baseline <5 5.6 60.1 1.5 6.9 42.7 5.7 6.5 6.9 7.7.7 38.3 <10 <5 46.8
MW-16/MW-16R Regolith Max Baseline <5 5.9 80.2 <1 <1 <5 <5 <5 <5 <5 <5.5 <5 <10 <5 <10
LAGOON -All Time High 13.9 56 489 1.6 <.5 59.6 56 1770 188 102 18 3.0 9.7 21.7 964
LAGOON Diluted -All Time High D 0.7 2.8 24.5 0.08 <0.02
5
2.98 2.8 88.5 9.4 5.1 0.9 0.15 0.485 1.09 48.2
Table contains concentrations of Appendix I metals
All Time High = Highest ever recorded at either the upgradient backgound well or untreated leachate sample. Samples consistantly collected on a semi-annual basis.
Diluted D = Extrapolated concentration when untreated leachate is mixed with groundwater. A 20:1 dilution ratio (dividing by 20) is the EPA's default dilution attenuation factor (DAF) and the SLSP Method basis
When two wells shown together indicates wells that have been replaced so data used for both wells
BOLD =
20 201.4 10 700 4 2 10 0.28 3.5 1000
UPGRADIENT BACKGROUND WELL PHASES 1,2 & 3
PHASE & LAGOON (PHASE 1 BASELINE 1997)
PHASE 2 (PHASE 2 BASELINE 2004)
1 1000 15 100
GWP = Groundwater Protection Standard (Current as of 10/6/16)
(BG Well) = Background Well Located hydraulically upgradient of Waste Unit
Concentration > 2L or GWP Standard
PHASE 3 (PHASE 3 BASELINE 2012)
UNTREATED LEACHATE (EFFECTIVELY A COMPOSITE OF PHASES 1, 2 & 3) RESULTS FROM 1997 - 2016
Max Baseline = Maximum concentration detected during the first four events performed within 6 months of commencement of landfill operations including at least 1 before opening. Considered
natural intrawell background levels.
< = Not Detected with Detection Limit Indicated
SWSL = Solid Waste Section Reporting Limit
2L = North Carolina 15A NCAC 2L Groundwater Quality Standard (Current as of 10/6/16)
Wayne Co. Subtitle D Landfill Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
February 21, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92310738
92310738
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE LINED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between August 31,
2016 and September 02, 2016. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
Report revised on 2.21.17 to change a sample ID per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 200
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 200
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92310738001 MW-1 Water 08/30/16 10:30 08/31/16 08:41
92310738002 MW-2 Water 08/30/16 16:00 08/31/16 08:41
92310738003 MW-5 Water 08/30/16 11:00 08/31/16 08:41
92310738004 MW-6 Water 08/30/16 13:40 08/31/16 08:41
92310738005 MW-7 Water 08/30/16 14:30 08/31/16 08:41
92310738006 MW-16R Water 08/30/16 15:10 08/31/16 08:41
92310738007 LE-1 Water 08/30/16 15:10 08/31/16 08:41
92310738009 MW-4 Water 08/31/16 14:00 09/02/16 08:50
92310738010 MW-8 Water 08/31/16 11:35 09/02/16 08:50
92310738011 MW-9 Water 08/31/16 13:00 09/02/16 08:50
92310738012 MW-10 Water 08/31/16 14:00 09/02/16 08:50
92310738013 MW-11 Water 08/31/16 14:45 09/02/16 08:50
92310738014 MW-12 Water 08/31/16 15:20 09/02/16 08:50
92310738015 MW-3 Water 08/31/16 10:00 09/02/16 08:50
92310738016 MW-14 Water 08/31/16 16:00 09/02/16 08:50
92310738017 MW-15 Water 08/31/16 16:40 09/02/16 08:50
92310738018 SW-4 Water 08/31/16 11:00 09/02/16 08:50
92310738019 SW-5 Water 08/31/16 16:55 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 200
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92310738001 MW-1 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
RSK 175 Modified 3 PASI-CWDV
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92310738002 MW-2 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92310738003 MW-5 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738004 MW-6 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 200
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738005 MW-7 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738006 MW-16R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 4500-CN-E 1 PASI-ASER
92310738007 LE-1 EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
SM 5210B 1 PASI-AALC
EPA 9040 1 PASI-AKDF1
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
EPA 365.1 1 PASI-ASER
SM 5220D 1 PASI-AMDW
92310738009 MW-4 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 7470 1 PASI-AWAB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 200
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738010 MW-8 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738011 MW-9 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738012 MW-10 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738013 MW-11 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 200
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738014 MW-12 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738015 MW-3 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738016 MW-14 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 200
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738017 MW-15 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92310738018 SW-4 EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92310738019 SW-5 EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-1 Lab ID:92310738001 Collected:08/30/16 10:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/02/16 15:21 309-00-209/01/16 12:000.25 0.25 1
alpha-BHC ND ug/L 09/02/16 15:21 319-84-609/01/16 12:000.25 0.25 1
beta-BHC ND ug/L 09/02/16 15:21 319-85-709/01/16 12:000.25 0.25 1
delta-BHC ND ug/L 09/02/16 15:21 319-86-809/01/16 12:000.25 0.25 1
gamma-BHC (Lindane)ND ug/L 09/02/16 15:21 58-89-909/01/16 12:000.25 0.25 1
Chlordane (Technical)ND ug/L 09/02/16 15:21 57-74-909/01/16 12:002.5 1.0 1
4,4'-DDD ND ug/L 09/02/16 15:21 72-54-809/01/16 12:000.50 0.25 1
4,4'-DDE ND ug/L 09/02/16 15:21 72-55-909/01/16 12:000.50 0.25 1
4,4'-DDT ND ug/L 09/02/16 15:21 50-29-309/01/16 12:000.50 0.25 1
Dieldrin ND ug/L 09/02/16 15:21 60-57-109/01/16 12:000.38 0.25 1
Endosulfan I ND ug/L 09/02/16 15:21 959-98-809/01/16 12:000.50 0.25 1
Endosulfan II ND ug/L 09/02/16 15:21 33213-65-909/01/16 12:000.50 0.25 1
Endosulfan sulfate ND ug/L 09/02/16 15:21 1031-07-809/01/16 12:000.50 0.25 1
Endrin ND ug/L 09/02/16 15:21 72-20-809/01/16 12:000.50 0.25 1
Endrin aldehyde ND ug/L 09/02/16 15:21 7421-93-409/01/16 12:000.50 0.25 1
Heptachlor ND ug/L 09/02/16 15:21 76-44-809/01/16 12:000.25 0.25 1
Heptachlor epoxide ND ug/L 09/02/16 15:21 1024-57-309/01/16 12:000.38 0.25 1
Methoxychlor ND ug/L 09/02/16 15:21 72-43-509/01/16 12:005.0 0.75 1
Toxaphene ND ug/L 09/02/16 15:21 8001-35-209/01/16 12:007.5 1.0 1
Surrogates
Tetrachloro-m-xylene (S)85 %09/02/16 15:21 877-09-809/01/16 12:0020-130 1
Decachlorobiphenyl (S)51 %09/02/16 15:21 2051-24-309/01/16 12:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/02/16 19:57 12674-11-209/01/16 12:002.5 2.5 1
PCB-1221 (Aroclor 1221)ND ug/L 09/02/16 19:57 11104-28-209/01/16 12:002.5 2.5 1
PCB-1232 (Aroclor 1232)ND ug/L 09/02/16 19:57 11141-16-509/01/16 12:002.5 2.5 1
PCB-1242 (Aroclor 1242)ND ug/L 09/02/16 19:57 53469-21-909/01/16 12:002.5 2.5 1
PCB-1248 (Aroclor 1248)ND ug/L 09/02/16 19:57 12672-29-609/01/16 12:002.5 2.5 1
PCB-1254 (Aroclor 1254)ND ug/L 09/02/16 19:57 11097-69-109/01/16 12:002.5 2.5 1
PCB-1260 (Aroclor 1260)ND ug/L 09/02/16 19:57 11096-82-509/01/16 12:002.5 2.5 1
Surrogates
Decachlorobiphenyl (S)47 %09/02/16 19:57 2051-24-309/01/16 12:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/03/16 00:47 25057-89-009/02/16 08:250.095 0.047 1
2,4-D ND ug/L 09/03/16 00:47 94-75-709/02/16 08:250.95 0.23 1
Dalapon ND ug/L 09/03/16 00:47 75-99-009/02/16 08:250.92 0.43 1
2,4-DB ND ug/L 09/03/16 00:47 94-82-609/02/16 08:251.9 0.51 1
Dicamba ND ug/L 09/03/16 00:47 1918-00-909/02/16 08:250.095 0.030 1
Dichlorprop ND ug/L 09/03/16 00:47 120-36-509/02/16 08:250.66 0.19 1
Dinoseb ND ug/L 09/03/16 00:47 88-85-709/02/16 08:250.19 0.057 1
Pentachlorophenol ND ug/L 09/03/16 00:47 87-86-509/02/16 08:250.029 0.017 1
Picloram ND ug/L 09/03/16 00:47 1918-02-109/02/16 08:250.095 0.019 1
2,4,5-T ND ug/L 09/03/16 00:47 93-76-509/02/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/03/16 00:47 93-72-109/02/16 08:250.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-1 Lab ID:92310738001 Collected:08/30/16 10:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)77 %09/03/16 00:47 19719-28-909/02/16 08:2539-139 1
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Ethane ND ug/L 09/02/16 14:18 74-84-0 N210.0 10.0 1
Ethene ND ug/L 09/02/16 14:18 74-85-1 N210.0 10.0 1
Methane ND ug/L 09/02/16 14:18 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/02/16 18:59 7440-36-009/01/16 19:306.0 3.8 1
Arsenic 9.8J ug/L 09/02/16 18:59 7440-38-2 B09/01/16 19:3010.0 2.5 1
Barium 41.5J ug/L 09/02/16 18:59 7440-39-309/01/16 19:301002.5 1
Beryllium 0.59J ug/L 09/02/16 18:59 7440-41-709/01/16 19:301.0 0.50 1
Cadmium ND ug/L 09/02/16 18:59 7440-43-909/01/16 19:301.0 0.50 1
Chromium 19.8 ug/L 09/02/16 18:59 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt ND ug/L 09/02/16 18:59 7440-48-409/01/16 19:3010.0 2.5 1
Copper 7.0J ug/L 09/02/16 18:59 7440-50-809/01/16 19:3010.0 2.5 1
Lead 9.3J ug/L 09/02/16 18:59 7439-92-109/01/16 19:3010.0 2.5 1
Nickel ND ug/L 09/02/16 18:59 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 18:59 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 18:59 7440-22-409/01/16 19:3010.0 2.5 1
Thallium ND ug/L 09/03/16 14:20 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 18:59 7440-31-509/01/16 19:301002.5 1
Vanadium 46.3 ug/L 09/02/16 18:59 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 16.8 ug/L 09/02/16 18:59 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/01/16 09:05 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 10:02 83-32-909/02/16 11:0233.3 0.83 1
Acenaphthylene ND ug/L 09/15/16 10:02 208-96-809/02/16 11:0233.3 0.70 1
Acetophenone ND ug/L 09/15/16 10:02 98-86-2 L309/02/16 11:0233.3 6.5 1
2-Acetylaminofluorene 23.5J ug/L 09/14/16 19:26 53-96-3 B09/02/16 11:0266.7 2.8 1
4-Aminobiphenyl ND ug/L 09/14/16 19:26 92-67-109/02/16 11:0266.7 3.1 1
Anthracene ND ug/L 09/15/16 10:02 120-12-709/02/16 11:0233.3 0.47 1
Benzo(a)anthracene ND ug/L 09/15/16 10:02 56-55-309/02/16 11:0233.3 1.1 1
Benzo(a)pyrene ND ug/L 09/15/16 10:02 50-32-809/02/16 11:0233.3 1.0 1
Benzo(b)fluoranthene ND ug/L 09/15/16 10:02 205-99-209/02/16 11:0233.3 0.93 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 10:02 191-24-209/02/16 11:0233.3 1.3 1
Benzo(k)fluoranthene ND ug/L 09/15/16 10:02 207-08-909/02/16 11:0233.3 1.4 1
Benzyl alcohol ND ug/L 09/15/16 10:02 100-51-609/02/16 11:0266.7 11.3 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 10:02 101-55-309/02/16 11:0233.3 4.4 1
Butylbenzylphthalate ND ug/L 09/15/16 10:02 85-68-709/02/16 11:0233.3 2.5 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 10:02 59-50-709/02/16 11:0266.7 13.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-1 Lab ID:92310738001 Collected:08/30/16 10:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chloroaniline ND ug/L 09/15/16 10:02 106-47-809/02/16 11:0266.7 11.3 1
Chlorobenzilate ND ug/L 09/14/16 19:26 510-15-609/02/16 11:0233.3 2.4 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 10:02 111-91-109/02/16 11:0233.3 5.6 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 10:02 111-44-409/02/16 11:0233.3 4.9 1
2-Chloronaphthalene ND ug/L 09/15/16 10:02 91-58-709/02/16 11:0233.3 7.4 1
2-Chlorophenol ND ug/L 09/15/16 10:02 95-57-809/02/16 11:0233.3 4.9 1
4-Chlorophenylphenyl ether ND ug/L 09/15/16 10:02 7005-72-309/02/16 11:0233.3 7.0 1
Chrysene ND ug/L 09/15/16 10:02 218-01-909/02/16 11:0233.3 0.70 1
Diallate ND ug/L 09/14/16 19:26 2303-16-409/02/16 11:0233.3 4.3 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 10:02 53-70-309/02/16 11:0233.3 1.8 1
Dibenzofuran ND ug/L 09/15/16 10:02 132-64-909/02/16 11:0233.3 5.9 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 10:02 91-94-109/02/16 11:0266.7 4.7 1
2,4-Dichlorophenol ND ug/L 09/15/16 10:02 120-83-209/02/16 11:0233.3 5.5 1
2,6-Dichlorophenol ND ug/L 09/14/16 19:26 87-65-009/02/16 11:0233.3 6.1 1
Diethylphthalate ND ug/L 09/15/16 10:02 84-66-209/02/16 11:02200004.4 1
Dimethoate ND ug/L 09/14/16 19:26 60-51-509/02/16 11:0266.7 3.0 1
P-Dimethylaminoazobenzene ND ug/L 09/14/16 19:26 60-11-709/02/16 11:0233.3 1.2 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/14/16 19:26 57-97-609/02/16 11:0233.3 2.6 1
3,3'-Dimethylbenzidine ND ug/L 09/14/16 19:26 119-93-709/02/16 11:0233.3 7.1 1
2,4-Dimethylphenol ND ug/L 09/15/16 10:02 105-67-909/02/16 11:0233.3 7.3 1
Dimethylphthalate ND ug/L 09/15/16 10:02 131-11-309/02/16 11:0233.3 4.9 1
Di-n-butylphthalate ND ug/L 09/15/16 10:02 84-74-209/02/16 11:0233.3 3.5 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 10:02 534-52-109/02/16 11:021675.5 1
1,3-Dinitrobenzene ND ug/L 09/14/16 19:26 99-65-009/02/16 11:0266.7 5.0 1
2,4-Dinitrophenol ND ug/L 09/15/16 10:02 51-28-509/02/16 11:0216721.8 1
2,4-Dinitrotoluene ND ug/L 09/15/16 10:02 121-14-209/02/16 11:0233.3 4.0 1
2,6-Dinitrotoluene ND ug/L 09/15/16 10:02 606-20-209/02/16 11:0233.3 5.6 1
Di-n-octylphthalate ND ug/L 09/15/16 10:02 117-84-009/02/16 11:0233.3 2.9 1
Diphenylamine ND ug/L 09/15/16 10:02 122-39-409/02/16 11:0233.3 4.4 1
Disulfoton ND ug/L 09/14/16 19:26 298-04-409/02/16 11:0233.3 4.7 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 10:02 117-81-709/02/16 11:0250.0 2.8 1
Ethyl methanesulfonate ND ug/L 09/14/16 19:26 62-50-009/02/16 11:0266.7 6.0 1
Famphur ND ug/L 09/14/16 19:26 52-85-709/02/16 11:0266.7 5.8 1
Fluoranthene ND ug/L 09/15/16 10:02 206-44-009/02/16 11:0233.3 0.70 1
Fluorene ND ug/L 09/15/16 10:02 86-73-709/02/16 11:0233.3 0.70 1
Hexachlorobenzene ND ug/L 09/15/16 10:02 118-74-109/02/16 11:0233.3 3.8 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 10:02 77-47-409/02/16 11:0233.3 5.8 1
Hexachloroethane ND ug/L 09/15/16 10:02 67-72-109/02/16 11:0233.3 4.9 1
Hexachloropropene ND ug/L 09/14/16 19:26 1888-71-709/02/16 11:0233.3 5.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 10:02 193-39-509/02/16 11:0233.3 0.97 1
Isodrin ND ug/L 09/14/16 19:26 465-73-609/02/16 11:0266.7 6.8 1
Isophorone ND ug/L 09/15/16 10:02 78-59-109/02/16 11:0233.3 5.9 1
Isosafrole ND ug/L 09/14/16 19:26 120-58-109/02/16 11:0233.3 6.0 1
Kepone ND ug/L 09/14/16 19:26 143-50-009/02/16 11:0266.7 10.5 1
Methapyrilene ND ug/L 09/14/16 19:26 91-80-509/02/16 11:023339.2 1
3-Methylcholanthrene ND ug/L 09/14/16 19:26 56-49-509/02/16 11:0233.3 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-1 Lab ID:92310738001 Collected:08/30/16 10:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Methyl methanesulfonate ND ug/L 09/14/16 19:26 66-27-309/02/16 11:0233.3 4.2 1
2-Methylnaphthalene ND ug/L 09/15/16 10:02 91-57-609/02/16 11:0233.3 0.93 1
Methyl parathion ND ug/L 09/14/16 19:26 298-00-009/02/16 11:0233.3 3.6 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 10:02 95-48-709/02/16 11:0233.3 5.8 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 10:0209/02/16 11:0233.3 5.7 1
1-Naphthalenamine ND ug/L 09/14/16 19:26 134-32-709/02/16 11:0233.3 3.2 1
2-Naphthalenamine ND ug/L 09/14/16 19:26 91-59-809/02/16 11:0233.3 3.3 1
1,4-Naphthoquinone ND ug/L 09/14/16 19:26 130-15-409/02/16 11:0233.3 5.9 1
2-Nitroaniline ND ug/L 09/15/16 10:02 88-74-409/02/16 11:021679.4 1
3-Nitroaniline ND ug/L 09/15/16 10:02 99-09-209/02/16 11:021678.1 1
4-Nitroaniline ND ug/L 09/15/16 10:02 100-01-609/02/16 11:0266.7 8.5 1
Nitrobenzene ND ug/L 09/15/16 10:02 98-95-309/02/16 11:0233.3 5.5 1
2-Nitrophenol ND ug/L 09/15/16 10:02 88-75-509/02/16 11:0233.3 5.5 1
4-Nitrophenol ND ug/L 09/15/16 10:02 100-02-709/02/16 11:0216719.3 1
5-Nitro-o-toluidine ND ug/L 09/14/16 19:26 99-55-809/02/16 11:0233.3 4.1 1
N-Nitrosodiethylamine ND ug/L 09/14/16 19:26 55-18-5 L309/02/16 11:0266.7 6.0 1
N-Nitrosodimethylamine ND ug/L 09/15/16 10:02 62-75-909/02/16 11:0233.3 4.2 1
N-Nitroso-di-n-butylamine ND ug/L 09/14/16 19:26 924-16-309/02/16 11:0233.3 7.4 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 10:02 621-64-7 L309/02/16 11:0233.3 6.9 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 10:02 86-30-609/02/16 11:0233.3 4.4 1
N-Nitrosomethylethylamine ND ug/L 09/14/16 19:26 10595-95-609/02/16 11:0233.3 6.1 1
N-Nitrosopiperidine ND ug/L 09/14/16 19:26 100-75-409/02/16 11:0266.7 6.2 1
N-Nitrosopyrrolidine ND ug/L 09/14/16 19:26 930-55-2 L309/02/16 11:0233.3 8.3 1
O,O,O-Triethylphosphorothioate ND ug/L 09/14/16 19:26 126-68-109/02/16 11:0233.3 6.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 10:02 108-60-109/02/16 11:0233.3 5.4 1
Parathion (Ethyl parathion)ND ug/L 09/14/16 19:26 56-38-209/02/16 11:0233.3 3.5 1
Pentachlorobenzene ND ug/L 09/14/16 19:26 608-93-509/02/16 11:0233.3 6.7 1
Pentachloronitrobenzene ND ug/L 09/14/16 19:26 82-68-809/02/16 11:0266.7 3.4 1
Pentachlorophenol ND ug/L 09/15/16 10:02 87-86-509/02/16 11:0283.3 7.7 1
Phenacetin ND ug/L 09/14/16 19:26 62-44-209/02/16 11:0266.7 3.2 1
Phenanthrene ND ug/L 09/15/16 10:02 85-01-809/02/16 11:0233.3 0.73 1
Phenol ND ug/L 09/15/16 10:0209/02/16 11:0233.3 5.6 1
p-Phenylenediamine ND ug/L 09/14/16 19:26 106-50-309/02/16 11:0233.3 3.2 1
Phorate ND ug/L 09/14/16 19:26 298-02-209/02/16 11:0233.3 3.5 1
Pronamide ND ug/L 09/14/16 19:26 23950-58-509/02/16 11:0233.3 3.2 1
Pyrene ND ug/L 09/15/16 10:02 129-00-009/02/16 11:0233.3 0.63 1
Safrole ND ug/L 09/14/16 19:26 94-59-709/02/16 11:0233.3 5.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/14/16 19:26 95-94-309/02/16 11:0233.3 5.6 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 10:02 58-90-209/02/16 11:0233.3 7.5 1
Thionazin ND ug/L 09/14/16 19:26 297-97-209/02/16 11:0266.7 4.1 1
O-Toluidine ND ug/L 09/14/16 19:26 95-53-409/02/16 11:0233.3 5.5 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 10:02 95-95-409/02/16 11:0233.3 7.5 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 10:02 88-06-209/02/16 11:0233.3 6.3 1
1,3,5-Trinitrobenzene ND ug/L 09/14/16 19:26 99-35-409/02/16 11:0233.3 3.6 1
Surrogates
Nitrobenzene-d5 (S)75 %09/15/16 10:02 4165-60-009/02/16 11:0221-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-1 Lab ID:92310738001 Collected:08/30/16 10:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
2-Fluorobiphenyl (S)78 %09/15/16 10:02 321-60-809/02/16 11:0227-110 1
Terphenyl-d14 (S)69 %09/15/16 10:02 1718-51-009/02/16 11:0231-107 1
Phenol-d6 (S)52 %09/15/16 10:02 13127-88-309/02/16 11:0210-110 1
2-Fluorophenol (S)61 %09/15/16 10:02 367-12-409/02/16 11:0212-110 1
2,4,6-Tribromophenol (S)102 %09/15/16 10:02 118-79-609/02/16 11:0227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/02/16 13:59 67-64-110010.0 1
Acetonitrile ND ug/L 09/02/16 13:59 75-05-855.0 2.2 1
Acrolein ND ug/L 09/02/16 13:59 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/02/16 13:59 107-13-12001.9 1
Allyl chloride ND ug/L 09/02/16 13:59 107-05-110.0 1.5 1
Benzene ND ug/L 09/02/16 13:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/02/16 13:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/02/16 13:59 75-27-41.0 0.18 1
Bromoform ND ug/L 09/02/16 13:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/02/16 13:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/02/16 13:59 78-93-31000.96 1
Carbon disulfide ND ug/L 09/02/16 13:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/02/16 13:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/02/16 13:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/02/16 13:59 75-00-310.0 0.54 1
Chloroform 0.26J ug/L 09/02/16 13:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/02/16 13:59 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/02/16 13:59 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/02/16 13:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/02/16 13:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/02/16 13:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/02/16 13:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/02/16 13:59 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/02/16 13:59 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/02/16 13:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/02/16 13:59 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 09/02/16 13:59 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/02/16 13:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/02/16 13:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/02/16 13:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/02/16 13:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/02/16 13:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/02/16 13:59 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/02/16 13:59 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/02/16 13:59 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/02/16 13:59 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/02/16 13:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/02/16 13:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 13 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-1 Lab ID:92310738001 Collected:08/30/16 10:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/02/16 13:59 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/02/16 13:59 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/02/16 13:59 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/02/16 13:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/02/16 13:59 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/02/16 13:59 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/02/16 13:59 126-98-71000.93 1
Methylene Chloride ND ug/L 09/02/16 13:59 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/02/16 13:59 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/02/16 13:59 108-10-11000.33 1
Naphthalene ND ug/L 09/02/16 13:59 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/02/16 13:59 107-12-01503.6 1
Styrene ND ug/L 09/02/16 13:59 100-42-5 B1.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/02/16 13:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/02/16 13:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/02/16 13:59 127-18-41.0 0.46 1
Toluene ND ug/L 09/02/16 13:59 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/02/16 13:59 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/02/16 13:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/02/16 13:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/02/16 13:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/02/16 13:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/02/16 13:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/02/16 13:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/02/16 13:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/02/16 13:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %09/02/16 13:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/02/16 13:59 17060-07-070-130 1
Toluene-d8 (S)104 %09/02/16 13:59 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 21:16 18496-25-8 M110001001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3750 ug/L 09/08/16 17:25 16887-00-610005001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 6.6J ug/L 09/12/16 23:53 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-2 Lab ID:92310738002 Collected:08/30/16 16:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/02/16 15:38 309-00-209/01/16 12:000.050 0.050 1
alpha-BHC ND ug/L 09/02/16 15:38 319-84-609/01/16 12:000.050 0.050 1
beta-BHC ND ug/L 09/02/16 15:38 319-85-709/01/16 12:000.050 0.050 1
delta-BHC ND ug/L 09/02/16 15:38 319-86-809/01/16 12:000.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/02/16 15:38 58-89-909/01/16 12:000.050 0.050 1
Chlordane (Technical)ND ug/L 09/02/16 15:38 57-74-909/01/16 12:000.50 0.20 1
4,4'-DDD ND ug/L 09/02/16 15:38 72-54-809/01/16 12:000.10 0.050 1
4,4'-DDE ND ug/L 09/02/16 15:38 72-55-909/01/16 12:000.10 0.050 1
4,4'-DDT ND ug/L 09/02/16 15:38 50-29-309/01/16 12:000.10 0.050 1
Dieldrin ND ug/L 09/02/16 15:38 60-57-109/01/16 12:000.075 0.050 1
Endosulfan I ND ug/L 09/02/16 15:38 959-98-809/01/16 12:000.10 0.050 1
Endosulfan II ND ug/L 09/02/16 15:38 33213-65-909/01/16 12:000.10 0.050 1
Endosulfan sulfate ND ug/L 09/02/16 15:38 1031-07-809/01/16 12:000.10 0.050 1
Endrin ND ug/L 09/02/16 15:38 72-20-809/01/16 12:000.10 0.050 1
Endrin aldehyde ND ug/L 09/02/16 15:38 7421-93-409/01/16 12:000.10 0.050 1
Heptachlor ND ug/L 09/02/16 15:38 76-44-809/01/16 12:000.050 0.050 1
Heptachlor epoxide ND ug/L 09/02/16 15:38 1024-57-309/01/16 12:000.075 0.050 1
Methoxychlor ND ug/L 09/02/16 15:38 72-43-509/01/16 12:001.0 0.15 1
Toxaphene ND ug/L 09/02/16 15:38 8001-35-209/01/16 12:001.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)60 %09/02/16 15:38 877-09-809/01/16 12:0020-130 1
Decachlorobiphenyl (S)43 %09/02/16 15:38 2051-24-309/01/16 12:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/02/16 20:18 12674-11-209/01/16 12:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/02/16 20:18 11104-28-209/01/16 12:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/02/16 20:18 11141-16-509/01/16 12:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/02/16 20:18 53469-21-909/01/16 12:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/02/16 20:18 12672-29-609/01/16 12:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/02/16 20:18 11097-69-109/01/16 12:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/02/16 20:18 11096-82-509/01/16 12:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)39 %09/02/16 20:18 2051-24-309/01/16 12:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/03/16 01:17 25057-89-009/02/16 08:250.096 0.048 1
2,4-D ND ug/L 09/03/16 01:17 94-75-709/02/16 08:250.95 0.23 1
Dalapon ND ug/L 09/03/16 01:17 75-99-009/02/16 08:250.92 0.44 1
2,4-DB ND ug/L 09/03/16 01:17 94-82-609/02/16 08:251.9 0.52 1
Dicamba ND ug/L 09/03/16 01:17 1918-00-909/02/16 08:250.095 0.030 1
Dichlorprop ND ug/L 09/03/16 01:17 120-36-509/02/16 08:250.66 0.19 1
Dinoseb ND ug/L 09/03/16 01:17 88-85-7 M109/02/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 09/03/16 01:17 87-86-509/02/16 08:250.029 0.017 1
Picloram ND ug/L 09/03/16 01:17 1918-02-109/02/16 08:250.096 0.019 1
2,4,5-T ND ug/L 09/03/16 01:17 93-76-509/02/16 08:250.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/03/16 01:17 93-72-109/02/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-2 Lab ID:92310738002 Collected:08/30/16 16:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)67 %09/03/16 01:17 19719-28-909/02/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/02/16 19:08 7440-36-009/01/16 19:306.0 3.8 1
Arsenic 10.6 ug/L 09/02/16 19:08 7440-38-2 B09/01/16 19:3010.0 2.5 1
Barium 26.7J ug/L 09/02/16 19:08 7440-39-309/01/16 19:301002.5 1
Beryllium ND ug/L 09/02/16 19:08 7440-41-709/01/16 19:301.0 0.50 1
Cadmium ND ug/L 09/02/16 19:08 7440-43-909/01/16 19:301.0 0.50 1
Chromium ND ug/L 09/02/16 19:08 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt 4.6J ug/L 09/02/16 19:08 7440-48-409/01/16 19:3010.0 2.5 1
Copper ND ug/L 09/02/16 19:08 7440-50-809/01/16 19:3010.0 2.5 1
Lead 5.5J ug/L 09/02/16 19:08 7439-92-109/01/16 19:3010.0 2.5 1
Nickel ND ug/L 09/02/16 19:08 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 19:08 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 19:08 7440-22-409/01/16 19:3010.0 2.5 1
Thallium 5.2J ug/L 09/03/16 14:29 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 19:08 7440-31-509/01/16 19:301002.5 1
Vanadium 2.8J ug/L 09/02/16 19:08 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 10.3 ug/L 09/02/16 19:08 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/01/16 09:08 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 13:14 83-32-909/02/16 11:0210.0 0.25 1
Acenaphthylene ND ug/L 09/15/16 13:14 208-96-809/02/16 11:0210.0 0.21 1
Acetophenone ND ug/L 09/15/16 13:14 98-86-2 L309/02/16 11:0210.0 2.0 1
2-Acetylaminofluorene 7.0J ug/L 09/15/16 13:14 53-96-3 B09/02/16 11:0220.0 0.84 1
4-Aminobiphenyl ND ug/L 09/15/16 13:14 92-67-109/02/16 11:0220.0 0.92 1
Anthracene ND ug/L 09/15/16 13:14 120-12-709/02/16 11:0210.0 0.14 1
Benzo(a)anthracene ND ug/L 09/15/16 13:14 56-55-309/02/16 11:0210.0 0.33 1
Benzo(a)pyrene ND ug/L 09/15/16 13:14 50-32-809/02/16 11:0210.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/15/16 13:14 205-99-209/02/16 11:0210.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 13:14 191-24-209/02/16 11:0210.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/15/16 13:14 207-08-909/02/16 11:0210.0 0.43 1
Benzyl alcohol ND ug/L 09/15/16 13:14 100-51-609/02/16 11:0220.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 13:14 101-55-309/02/16 11:0210.0 1.3 1
Butylbenzylphthalate ND ug/L 09/15/16 13:14 85-68-709/02/16 11:0210.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 13:14 59-50-709/02/16 11:0220.0 4.2 1
4-Chloroaniline ND ug/L 09/15/16 13:14 106-47-809/02/16 11:0220.0 3.4 1
Chlorobenzilate ND ug/L 09/15/16 13:14 510-15-609/02/16 11:0210.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 13:14 111-91-109/02/16 11:0210.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 13:14 111-44-409/02/16 11:0210.0 1.5 1
2-Chloronaphthalene ND ug/L 09/15/16 13:14 91-58-709/02/16 11:0210.0 2.2 1
2-Chlorophenol ND ug/L 09/15/16 13:14 95-57-809/02/16 11:0210.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-2 Lab ID:92310738002 Collected:08/30/16 16:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/15/16 13:14 7005-72-309/02/16 11:0210.0 2.1 1
Chrysene ND ug/L 09/15/16 13:14 218-01-909/02/16 11:0210.0 0.21 1
Diallate ND ug/L 09/15/16 13:14 2303-16-409/02/16 11:0210.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 13:14 53-70-309/02/16 11:0210.0 0.55 1
Dibenzofuran ND ug/L 09/15/16 13:14 132-64-909/02/16 11:0210.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 13:14 91-94-109/02/16 11:0220.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/15/16 13:14 120-83-209/02/16 11:0210.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/15/16 13:14 87-65-009/02/16 11:0210.0 1.8 1
Diethylphthalate ND ug/L 09/15/16 13:14 84-66-209/02/16 11:0260001.3 1
Dimethoate ND ug/L 09/15/16 13:14 60-51-509/02/16 11:0220.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/15/16 13:14 60-11-709/02/16 11:0210.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/15/16 13:14 57-97-609/02/16 11:0210.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/15/16 13:14 119-93-709/02/16 11:0210.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/15/16 13:14 105-67-909/02/16 11:0210.0 2.2 1
Dimethylphthalate ND ug/L 09/15/16 13:14 131-11-309/02/16 11:0210.0 1.5 1
Di-n-butylphthalate ND ug/L 09/15/16 13:14 84-74-209/02/16 11:0210.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 13:14 534-52-109/02/16 11:0250.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/15/16 13:14 99-65-009/02/16 11:0220.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/15/16 13:14 51-28-509/02/16 11:0250.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/15/16 13:14 121-14-209/02/16 11:0210.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/15/16 13:14 606-20-209/02/16 11:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 09/15/16 13:14 117-84-009/02/16 11:0210.0 0.86 1
Diphenylamine ND ug/L 09/15/16 13:14 122-39-409/02/16 11:0210.0 1.3 1
Disulfoton ND ug/L 09/15/16 13:14 298-04-409/02/16 11:0210.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 13:14 117-81-709/02/16 11:0215.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/15/16 13:14 62-50-009/02/16 11:0220.0 1.8 1
Famphur ND ug/L 09/15/16 13:14 52-85-709/02/16 11:0220.0 1.7 1
Fluoranthene ND ug/L 09/15/16 13:14 206-44-009/02/16 11:0210.0 0.21 1
Fluorene ND ug/L 09/15/16 13:14 86-73-709/02/16 11:0210.0 0.21 1
Hexachlorobenzene ND ug/L 09/15/16 13:14 118-74-109/02/16 11:0210.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 13:14 77-47-409/02/16 11:0210.0 1.8 1
Hexachloroethane ND ug/L 09/15/16 13:14 67-72-109/02/16 11:0210.0 1.5 1
Hexachloropropene ND ug/L 09/15/16 13:14 1888-71-709/02/16 11:0210.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 13:14 193-39-509/02/16 11:0210.0 0.29 1
Isodrin ND ug/L 09/15/16 13:14 465-73-609/02/16 11:0220.0 2.0 1
Isophorone ND ug/L 09/15/16 13:14 78-59-109/02/16 11:0210.0 1.8 1
Isosafrole ND ug/L 09/15/16 13:14 120-58-109/02/16 11:0210.0 1.8 1
Kepone ND ug/L 09/15/16 13:14 143-50-009/02/16 11:0220.0 3.1 1
Methapyrilene ND ug/L 09/15/16 13:14 91-80-509/02/16 11:021002.7 1
3-Methylcholanthrene ND ug/L 09/15/16 13:14 56-49-509/02/16 11:0210.0 0.82 1
Methyl methanesulfonate ND ug/L 09/15/16 13:14 66-27-309/02/16 11:0210.0 1.3 1
2-Methylnaphthalene ND ug/L 09/15/16 13:14 91-57-609/02/16 11:0210.0 0.28 1
Methyl parathion ND ug/L 09/15/16 13:14 298-00-009/02/16 11:0210.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 13:14 95-48-709/02/16 11:0210.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 13:1409/02/16 11:0210.0 1.7 1
1-Naphthalenamine ND ug/L 09/15/16 13:14 134-32-709/02/16 11:0210.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-2 Lab ID:92310738002 Collected:08/30/16 16:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/15/16 13:14 91-59-809/02/16 11:0210.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/15/16 13:14 130-15-409/02/16 11:0210.0 1.8 1
2-Nitroaniline ND ug/L 09/15/16 13:14 88-74-409/02/16 11:0250.0 2.8 1
3-Nitroaniline ND ug/L 09/15/16 13:14 99-09-209/02/16 11:0250.0 2.4 1
4-Nitroaniline ND ug/L 09/15/16 13:14 100-01-609/02/16 11:0220.0 2.5 1
Nitrobenzene ND ug/L 09/15/16 13:14 98-95-309/02/16 11:0210.0 1.7 1
2-Nitrophenol ND ug/L 09/15/16 13:14 88-75-509/02/16 11:0210.0 1.7 1
4-Nitrophenol ND ug/L 09/15/16 13:14 100-02-709/02/16 11:0250.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/15/16 13:14 99-55-809/02/16 11:0210.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/15/16 13:14 55-18-5 L309/02/16 11:0220.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/15/16 13:14 62-75-909/02/16 11:0210.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/15/16 13:14 924-16-309/02/16 11:0210.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 13:14 621-64-7 L309/02/16 11:0210.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 13:14 86-30-609/02/16 11:0210.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/15/16 13:14 10595-95-609/02/16 11:0210.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/15/16 13:14 100-75-409/02/16 11:0220.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/15/16 13:14 930-55-2 L309/02/16 11:0210.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/15/16 13:14 126-68-109/02/16 11:0210.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 13:14 108-60-109/02/16 11:0210.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/15/16 13:14 56-38-209/02/16 11:0210.0 1.1 1
Pentachlorobenzene ND ug/L 09/15/16 13:14 608-93-509/02/16 11:0210.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/15/16 13:14 82-68-809/02/16 11:0220.0 1.0 1
Pentachlorophenol ND ug/L 09/15/16 13:14 87-86-509/02/16 11:0225.0 2.3 1
Phenacetin ND ug/L 09/15/16 13:14 62-44-209/02/16 11:0220.0 0.97 1
Phenanthrene ND ug/L 09/15/16 13:14 85-01-809/02/16 11:0210.0 0.22 1
Phenol ND ug/L 09/15/16 13:1409/02/16 11:0210.0 1.7 1
p-Phenylenediamine ND ug/L 09/15/16 13:14 106-50-309/02/16 11:0210.0 0.96 1
Phorate ND ug/L 09/15/16 13:14 298-02-209/02/16 11:0210.0 1.1 1
Pronamide ND ug/L 09/15/16 13:14 23950-58-509/02/16 11:0210.0 0.97 1
Pyrene ND ug/L 09/15/16 13:14 129-00-009/02/16 11:0210.0 0.19 1
Safrole ND ug/L 09/15/16 13:14 94-59-709/02/16 11:0210.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/15/16 13:14 95-94-309/02/16 11:0210.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 13:14 58-90-209/02/16 11:0210.0 2.3 1
Thionazin ND ug/L 09/15/16 13:14 297-97-209/02/16 11:0220.0 1.2 1
O-Toluidine ND ug/L 09/15/16 13:14 95-53-409/02/16 11:0210.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 13:14 95-95-409/02/16 11:0210.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 13:14 88-06-209/02/16 11:0210.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/15/16 13:14 99-35-409/02/16 11:0210.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)78 %09/15/16 13:14 4165-60-009/02/16 11:0221-110 1
2-Fluorobiphenyl (S)81 %09/15/16 13:14 321-60-809/02/16 11:0227-110 1
Terphenyl-d14 (S)72 %09/15/16 13:14 1718-51-009/02/16 11:0231-107 1
Phenol-d6 (S)31 %09/15/16 13:14 13127-88-309/02/16 11:0210-110 1
2-Fluorophenol (S)43 %09/15/16 13:14 367-12-409/02/16 11:0212-110 1
2,4,6-Tribromophenol (S)92 %09/15/16 13:14 118-79-609/02/16 11:0227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 18 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-2 Lab ID:92310738002 Collected:08/30/16 16:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/02/16 14:16 67-64-110010.0 1
Acetonitrile ND ug/L 09/02/16 14:16 75-05-855.0 2.2 1
Acrolein ND ug/L 09/02/16 14:16 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/02/16 14:16 107-13-12001.9 1
Allyl chloride ND ug/L 09/02/16 14:16 107-05-110.0 1.5 1
Benzene ND ug/L 09/02/16 14:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/02/16 14:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/02/16 14:16 75-27-41.0 0.18 1
Bromoform ND ug/L 09/02/16 14:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/02/16 14:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/02/16 14:16 78-93-31000.96 1
Carbon disulfide ND ug/L 09/02/16 14:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/02/16 14:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/02/16 14:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/02/16 14:16 75-00-310.0 0.54 1
Chloroform ND ug/L 09/02/16 14:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/02/16 14:16 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/02/16 14:16 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/02/16 14:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/02/16 14:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/02/16 14:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/02/16 14:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/02/16 14:16 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/02/16 14:16 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/02/16 14:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/02/16 14:16 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 09/02/16 14:16 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/02/16 14:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/02/16 14:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/02/16 14:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/02/16 14:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/02/16 14:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/02/16 14:16 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/02/16 14:16 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/02/16 14:16 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/02/16 14:16 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/02/16 14:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/02/16 14:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/02/16 14:16 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/02/16 14:16 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/02/16 14:16 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/02/16 14:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/02/16 14:16 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/02/16 14:16 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/02/16 14:16 126-98-71000.93 1
Methylene Chloride ND ug/L 09/02/16 14:16 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-2 Lab ID:92310738002 Collected:08/30/16 16:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/02/16 14:16 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/02/16 14:16 108-10-11000.33 1
Naphthalene ND ug/L 09/02/16 14:16 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/02/16 14:16 107-12-01503.6 1
Styrene ND ug/L 09/02/16 14:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/02/16 14:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/02/16 14:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/02/16 14:16 127-18-41.0 0.46 1
Toluene ND ug/L 09/02/16 14:16 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/02/16 14:16 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/02/16 14:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/02/16 14:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/02/16 14:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/02/16 14:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/02/16 14:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/02/16 14:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/02/16 14:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/02/16 14:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %09/02/16 14:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/02/16 14:16 17060-07-070-130 1
Toluene-d8 (S)102 %09/02/16 14:16 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 21:16 18496-25-810001001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 26500 ug/L 09/08/16 17:26 16887-00-6500025005
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.3J ug/L 09/12/16 23:54 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-5 Lab ID:92310738003 Collected:08/30/16 11:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/02/16 15:56 309-00-209/01/16 12:000.12 0.12 1
alpha-BHC ND ug/L 09/02/16 15:56 319-84-609/01/16 12:000.12 0.12 1
beta-BHC ND ug/L 09/02/16 15:56 319-85-709/01/16 12:000.12 0.12 1
delta-BHC ND ug/L 09/02/16 15:56 319-86-809/01/16 12:000.12 0.12 1
gamma-BHC (Lindane)ND ug/L 09/02/16 15:56 58-89-909/01/16 12:000.12 0.12 1
Chlordane (Technical)ND ug/L 09/02/16 15:56 57-74-909/01/16 12:001.2 0.50 1
4,4'-DDD ND ug/L 09/02/16 15:56 72-54-809/01/16 12:000.25 0.12 1
4,4'-DDE ND ug/L 09/02/16 15:56 72-55-909/01/16 12:000.25 0.12 1
4,4'-DDT ND ug/L 09/02/16 15:56 50-29-309/01/16 12:000.25 0.12 1
Dieldrin ND ug/L 09/02/16 15:56 60-57-109/01/16 12:000.19 0.12 1
Endosulfan I ND ug/L 09/02/16 15:56 959-98-809/01/16 12:000.25 0.12 1
Endosulfan II ND ug/L 09/02/16 15:56 33213-65-909/01/16 12:000.25 0.12 1
Endosulfan sulfate ND ug/L 09/02/16 15:56 1031-07-809/01/16 12:000.25 0.12 1
Endrin ND ug/L 09/02/16 15:56 72-20-809/01/16 12:000.25 0.12 1
Endrin aldehyde ND ug/L 09/02/16 15:56 7421-93-409/01/16 12:000.25 0.12 1
Heptachlor ND ug/L 09/02/16 15:56 76-44-809/01/16 12:000.12 0.12 1
Heptachlor epoxide ND ug/L 09/02/16 15:56 1024-57-309/01/16 12:000.19 0.12 1
Methoxychlor ND ug/L 09/02/16 15:56 72-43-509/01/16 12:002.5 0.38 1
Toxaphene ND ug/L 09/02/16 15:56 8001-35-209/01/16 12:003.8 0.50 1
Surrogates
Tetrachloro-m-xylene (S)72 %09/02/16 15:56 877-09-809/01/16 12:0020-130 1
Decachlorobiphenyl (S)36 %09/02/16 15:56 2051-24-309/01/16 12:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/02/16 20:39 12674-11-209/01/16 12:001.2 1.2 1
PCB-1221 (Aroclor 1221)ND ug/L 09/02/16 20:39 11104-28-209/01/16 12:001.2 1.2 1
PCB-1232 (Aroclor 1232)ND ug/L 09/02/16 20:39 11141-16-509/01/16 12:001.2 1.2 1
PCB-1242 (Aroclor 1242)ND ug/L 09/02/16 20:39 53469-21-909/01/16 12:001.2 1.2 1
PCB-1248 (Aroclor 1248)ND ug/L 09/02/16 20:39 12672-29-609/01/16 12:001.2 1.2 1
PCB-1254 (Aroclor 1254)ND ug/L 09/02/16 20:39 11097-69-109/01/16 12:001.2 1.2 1
PCB-1260 (Aroclor 1260)ND ug/L 09/02/16 20:39 11096-82-509/01/16 12:001.2 1.2 1
Surrogates
Decachlorobiphenyl (S)36 %09/02/16 20:39 2051-24-309/01/16 12:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/03/16 02:47 25057-89-009/02/16 08:250.095 0.047 1
2,4-D ND ug/L 09/03/16 02:47 94-75-709/02/16 08:250.95 0.23 1
Dalapon ND ug/L 09/03/16 02:47 75-99-009/02/16 08:250.92 0.43 1
2,4-DB ND ug/L 09/03/16 02:47 94-82-609/02/16 08:251.9 0.51 1
Dicamba ND ug/L 09/03/16 02:47 1918-00-909/02/16 08:250.095 0.030 1
Dichlorprop ND ug/L 09/03/16 02:47 120-36-509/02/16 08:250.66 0.19 1
Dinoseb ND ug/L 09/03/16 02:47 88-85-709/02/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 09/03/16 02:47 87-86-509/02/16 08:250.029 0.017 1
Picloram ND ug/L 09/03/16 02:47 1918-02-109/02/16 08:250.095 0.019 1
2,4,5-T ND ug/L 09/03/16 02:47 93-76-509/02/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/03/16 02:47 93-72-109/02/16 08:250.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-5 Lab ID:92310738003 Collected:08/30/16 11:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)79 %09/03/16 02:47 19719-28-909/02/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/02/16 19:12 7440-36-009/01/16 19:306.0 3.8 1
Arsenic ND ug/L 09/02/16 19:12 7440-38-2 B09/01/16 19:3010.0 2.5 1
Barium 135 ug/L 09/02/16 19:12 7440-39-309/01/16 19:301002.5 1
Beryllium ND ug/L 09/02/16 19:12 7440-41-709/01/16 19:301.0 0.50 1
Cadmium 0.53J ug/L 09/02/16 19:12 7440-43-909/01/16 19:301.0 0.50 1
Chromium ND ug/L 09/02/16 19:12 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt ND ug/L 09/02/16 19:12 7440-48-409/01/16 19:3010.0 2.5 1
Copper ND ug/L 09/02/16 19:12 7440-50-809/01/16 19:3010.0 2.5 1
Lead ND ug/L 09/02/16 19:12 7439-92-109/01/16 19:3010.0 2.5 1
Nickel ND ug/L 09/02/16 19:12 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 19:12 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 19:12 7440-22-409/01/16 19:3010.0 2.5 1
Thallium ND ug/L 09/03/16 14:32 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 19:12 7440-31-509/01/16 19:301002.5 1
Vanadium ND ug/L 09/02/16 19:12 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 5.1J ug/L 09/02/16 19:12 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/01/16 09:10 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 11:20 83-32-909/02/16 11:0220.0 0.50 1
Acenaphthylene ND ug/L 09/19/16 11:20 208-96-809/02/16 11:0220.0 0.42 1
Acetophenone ND ug/L 09/19/16 11:20 98-86-2 L309/02/16 11:0220.0 3.9 1
2-Acetylaminofluorene ND ug/L 09/19/16 11:20 53-96-309/02/16 11:0240.0 1.7 1
4-Aminobiphenyl ND ug/L 09/19/16 11:20 92-67-109/02/16 11:0240.0 1.8 1
Anthracene ND ug/L 09/19/16 11:20 120-12-709/02/16 11:0220.0 0.28 1
Benzo(a)anthracene ND ug/L 09/19/16 11:20 56-55-309/02/16 11:0220.0 0.66 1
Benzo(a)pyrene ND ug/L 09/19/16 11:20 50-32-809/02/16 11:0220.0 0.60 1
Benzo(b)fluoranthene ND ug/L 09/19/16 11:20 205-99-209/02/16 11:0220.0 0.56 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 11:20 191-24-209/02/16 11:0220.0 0.76 1
Benzo(k)fluoranthene ND ug/L 09/19/16 11:20 207-08-909/02/16 11:0220.0 0.86 1
Benzyl alcohol ND ug/L 09/19/16 11:20 100-51-609/02/16 11:0240.0 6.8 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 11:20 101-55-309/02/16 11:0220.0 2.6 1
Butylbenzylphthalate ND ug/L 09/19/16 11:20 85-68-709/02/16 11:0220.0 1.5 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 11:20 59-50-709/02/16 11:0240.0 8.3 1
4-Chloroaniline ND ug/L 09/19/16 11:20 106-47-809/02/16 11:0240.0 6.8 1
Chlorobenzilate ND ug/L 09/19/16 11:20 510-15-609/02/16 11:0220.0 1.4 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 11:20 111-91-109/02/16 11:0220.0 3.4 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 11:20 111-44-409/02/16 11:0220.0 2.9 1
2-Chloronaphthalene ND ug/L 09/19/16 11:20 91-58-709/02/16 11:0220.0 4.4 1
2-Chlorophenol ND ug/L 09/19/16 11:20 95-57-809/02/16 11:0220.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 22 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-5 Lab ID:92310738003 Collected:08/30/16 11:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 11:20 7005-72-309/02/16 11:0220.0 4.2 1
Chrysene ND ug/L 09/19/16 11:20 218-01-909/02/16 11:0220.0 0.42 1
Diallate ND ug/L 09/19/16 11:20 2303-16-409/02/16 11:0220.0 2.6 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 11:20 53-70-309/02/16 11:0220.0 1.1 1
Dibenzofuran ND ug/L 09/19/16 11:20 132-64-909/02/16 11:0220.0 3.5 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 11:20 91-94-109/02/16 11:0240.0 2.8 1
2,4-Dichlorophenol ND ug/L 09/19/16 11:20 120-83-209/02/16 11:0220.0 3.3 1
2,6-Dichlorophenol ND ug/L 09/19/16 11:20 87-65-009/02/16 11:0220.0 3.6 1
Diethylphthalate ND ug/L 09/19/16 11:20 84-66-209/02/16 11:02120002.7 1
Dimethoate ND ug/L 09/19/16 11:20 60-51-509/02/16 11:0240.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 11:20 60-11-709/02/16 11:0220.0 0.70 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 11:20 57-97-609/02/16 11:0220.0 1.5 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 11:20 119-93-709/02/16 11:0220.0 4.3 1
2,4-Dimethylphenol ND ug/L 09/19/16 11:20 105-67-909/02/16 11:0220.0 4.4 1
Dimethylphthalate ND ug/L 09/19/16 11:20 131-11-309/02/16 11:0220.0 3.0 1
Di-n-butylphthalate ND ug/L 09/19/16 11:20 84-74-209/02/16 11:0220.0 2.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 11:20 534-52-109/02/16 11:021003.3 1
1,3-Dinitrobenzene ND ug/L 09/19/16 11:20 99-65-009/02/16 11:0240.0 3.0 1
2,4-Dinitrophenol ND ug/L 09/19/16 11:20 51-28-509/02/16 11:0210013.1 1
2,4-Dinitrotoluene ND ug/L 09/19/16 11:20 121-14-209/02/16 11:0220.0 2.4 1
2,6-Dinitrotoluene ND ug/L 09/19/16 11:20 606-20-209/02/16 11:0220.0 3.4 1
Di-n-octylphthalate ND ug/L 09/19/16 11:20 117-84-009/02/16 11:0220.0 1.7 1
Diphenylamine ND ug/L 09/19/16 11:20 122-39-409/02/16 11:0220.0 2.6 1
Disulfoton ND ug/L 09/19/16 11:20 298-04-409/02/16 11:0220.0 2.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 11:20 117-81-709/02/16 11:0230.0 1.7 1
Ethyl methanesulfonate ND ug/L 09/19/16 11:20 62-50-009/02/16 11:0240.0 3.6 1
Famphur ND ug/L 09/19/16 11:20 52-85-709/02/16 11:0240.0 3.5 1
Fluoranthene ND ug/L 09/19/16 11:20 206-44-009/02/16 11:0220.0 0.42 1
Fluorene ND ug/L 09/19/16 11:20 86-73-709/02/16 11:0220.0 0.42 1
Hexachlorobenzene ND ug/L 09/19/16 11:20 118-74-109/02/16 11:0220.0 2.3 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 11:20 77-47-409/02/16 11:0220.0 3.5 1
Hexachloroethane ND ug/L 09/19/16 11:20 67-72-109/02/16 11:0220.0 2.9 1
Hexachloropropene ND ug/L 09/19/16 11:20 1888-71-709/02/16 11:0220.0 3.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 11:20 193-39-509/02/16 11:0220.0 0.58 1
Isodrin ND ug/L 09/19/16 11:20 465-73-609/02/16 11:0240.0 4.1 1
Isophorone ND ug/L 09/19/16 11:20 78-59-109/02/16 11:0220.0 3.5 1
Isosafrole ND ug/L 09/19/16 11:20 120-58-109/02/16 11:0220.0 3.6 1
Kepone ND ug/L 09/19/16 11:20 143-50-009/02/16 11:0240.0 6.3 1
Methapyrilene ND ug/L 09/19/16 11:20 91-80-509/02/16 11:022005.5 1
3-Methylcholanthrene ND ug/L 09/19/16 11:20 56-49-509/02/16 11:0220.0 1.6 1
Methyl methanesulfonate ND ug/L 09/19/16 11:20 66-27-309/02/16 11:0220.0 2.5 1
2-Methylnaphthalene ND ug/L 09/19/16 11:20 91-57-609/02/16 11:0220.0 0.56 1
Methyl parathion ND ug/L 09/19/16 11:20 298-00-009/02/16 11:0220.0 2.2 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 11:20 95-48-709/02/16 11:0220.0 3.5 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 11:2009/02/16 11:0220.0 3.4 1
1-Naphthalenamine ND ug/L 09/19/16 11:20 134-32-709/02/16 11:0220.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-5 Lab ID:92310738003 Collected:08/30/16 11:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 11:20 91-59-809/02/16 11:0220.0 2.0 1
1,4-Naphthoquinone ND ug/L 09/19/16 11:20 130-15-409/02/16 11:0220.0 3.6 1
2-Nitroaniline ND ug/L 09/19/16 11:20 88-74-409/02/16 11:021005.6 1
3-Nitroaniline ND ug/L 09/19/16 11:20 99-09-209/02/16 11:021004.8 1
4-Nitroaniline ND ug/L 09/19/16 11:20 100-01-609/02/16 11:0240.0 5.1 1
Nitrobenzene ND ug/L 09/19/16 11:20 98-95-309/02/16 11:0220.0 3.3 1
2-Nitrophenol ND ug/L 09/19/16 11:20 88-75-509/02/16 11:0220.0 3.3 1
4-Nitrophenol ND ug/L 09/19/16 11:20 100-02-709/02/16 11:0210011.6 1
5-Nitro-o-toluidine ND ug/L 09/19/16 11:20 99-55-809/02/16 11:0220.0 2.4 1
N-Nitrosodiethylamine ND ug/L 09/19/16 11:20 55-18-5 L309/02/16 11:0240.0 3.6 1
N-Nitrosodimethylamine ND ug/L 09/19/16 11:20 62-75-909/02/16 11:0220.0 2.5 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 11:20 924-16-309/02/16 11:0220.0 4.4 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 11:20 621-64-7 L309/02/16 11:0220.0 4.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 11:20 86-30-609/02/16 11:0220.0 2.6 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 11:20 10595-95-609/02/16 11:0220.0 3.6 1
N-Nitrosopiperidine ND ug/L 09/19/16 11:20 100-75-409/02/16 11:0240.0 3.7 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 11:20 930-55-2 L309/02/16 11:0220.0 5.0 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 11:20 126-68-109/02/16 11:0220.0 3.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 11:20 108-60-109/02/16 11:0220.0 3.2 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 11:20 56-38-209/02/16 11:0220.0 2.1 1
Pentachlorobenzene ND ug/L 09/19/16 11:20 608-93-509/02/16 11:0220.0 4.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 11:20 82-68-809/02/16 11:0240.0 2.0 1
Pentachlorophenol ND ug/L 09/19/16 11:20 87-86-509/02/16 11:0250.0 4.6 1
Phenacetin ND ug/L 09/19/16 11:20 62-44-209/02/16 11:0240.0 1.9 1
Phenanthrene ND ug/L 09/19/16 11:20 85-01-809/02/16 11:0220.0 0.44 1
Phenol ND ug/L 09/19/16 11:2009/02/16 11:0220.0 3.4 1
p-Phenylenediamine ND ug/L 09/19/16 11:20 106-50-309/02/16 11:0220.0 1.9 1
Phorate ND ug/L 09/19/16 11:20 298-02-209/02/16 11:0220.0 2.1 1
Pronamide ND ug/L 09/19/16 11:20 23950-58-509/02/16 11:0220.0 1.9 1
Pyrene ND ug/L 09/19/16 11:20 129-00-009/02/16 11:0220.0 0.38 1
Safrole ND ug/L 09/19/16 11:20 94-59-709/02/16 11:0220.0 3.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 11:20 95-94-309/02/16 11:0220.0 3.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 11:20 58-90-209/02/16 11:0220.0 4.5 1
Thionazin ND ug/L 09/19/16 11:20 297-97-209/02/16 11:0240.0 2.4 1
O-Toluidine ND ug/L 09/19/16 11:20 95-53-409/02/16 11:0220.0 3.3 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 11:20 95-95-409/02/16 11:0220.0 4.5 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 11:20 88-06-209/02/16 11:0220.0 3.8 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 11:20 99-35-409/02/16 11:0220.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)72 %09/19/16 11:20 4165-60-009/02/16 11:0221-110 1
2-Fluorobiphenyl (S)79 %09/19/16 11:20 321-60-809/02/16 11:0227-110 1
Terphenyl-d14 (S)77 %09/19/16 11:20 1718-51-009/02/16 11:0231-107 1
Phenol-d6 (S)33 %09/19/16 11:20 13127-88-309/02/16 11:0210-110 1
2-Fluorophenol (S)40 %09/19/16 11:20 367-12-409/02/16 11:0212-110 1
2,4,6-Tribromophenol (S)70 %09/19/16 11:20 118-79-609/02/16 11:0227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-5 Lab ID:92310738003 Collected:08/30/16 11:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/02/16 14:34 67-64-110010.0 1
Acetonitrile ND ug/L 09/02/16 14:34 75-05-855.0 2.2 1
Acrolein ND ug/L 09/02/16 14:34 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/02/16 14:34 107-13-12001.9 1
Allyl chloride ND ug/L 09/02/16 14:34 107-05-110.0 1.5 1
Benzene ND ug/L 09/02/16 14:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/02/16 14:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/02/16 14:34 75-27-41.0 0.18 1
Bromoform ND ug/L 09/02/16 14:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/02/16 14:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/02/16 14:34 78-93-31000.96 1
Carbon disulfide ND ug/L 09/02/16 14:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/02/16 14:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/02/16 14:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/02/16 14:34 75-00-310.0 0.54 1
Chloroform ND ug/L 09/02/16 14:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/02/16 14:34 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/02/16 14:34 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/02/16 14:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/02/16 14:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/02/16 14:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/02/16 14:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/02/16 14:34 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/02/16 14:34 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/02/16 14:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/02/16 14:34 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 09/02/16 14:34 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/02/16 14:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/02/16 14:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/02/16 14:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/02/16 14:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/02/16 14:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/02/16 14:34 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/02/16 14:34 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/02/16 14:34 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/02/16 14:34 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/02/16 14:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/02/16 14:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/02/16 14:34 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/02/16 14:34 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/02/16 14:34 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/02/16 14:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/02/16 14:34 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/02/16 14:34 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/02/16 14:34 126-98-71000.93 1
Methylene Chloride ND ug/L 09/02/16 14:34 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-5 Lab ID:92310738003 Collected:08/30/16 11:00 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/02/16 14:34 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/02/16 14:34 108-10-11000.33 1
Naphthalene ND ug/L 09/02/16 14:34 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/02/16 14:34 107-12-01503.6 1
Styrene ND ug/L 09/02/16 14:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/02/16 14:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/02/16 14:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/02/16 14:34 127-18-41.0 0.46 1
Toluene ND ug/L 09/02/16 14:34 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/02/16 14:34 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/02/16 14:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/02/16 14:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/02/16 14:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/02/16 14:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/02/16 14:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/02/16 14:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/02/16 14:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/02/16 14:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %09/02/16 14:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %09/02/16 14:34 17060-07-070-130 1
Toluene-d8 (S)102 %09/02/16 14:34 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 21:16 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 6.1J ug/L 09/12/16 23:54 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-6 Lab ID:92310738004 Collected:08/30/16 13:40 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/02/16 16:14 309-00-209/01/16 12:000.050 0.050 1
alpha-BHC ND ug/L 09/02/16 16:14 319-84-609/01/16 12:000.050 0.050 1
beta-BHC ND ug/L 09/02/16 16:14 319-85-709/01/16 12:000.050 0.050 1
delta-BHC ND ug/L 09/02/16 16:14 319-86-809/01/16 12:000.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/02/16 16:14 58-89-909/01/16 12:000.050 0.050 1
Chlordane (Technical)ND ug/L 09/02/16 16:14 57-74-909/01/16 12:000.50 0.20 1
4,4'-DDD ND ug/L 09/02/16 16:14 72-54-809/01/16 12:000.10 0.050 1
4,4'-DDE ND ug/L 09/02/16 16:14 72-55-909/01/16 12:000.10 0.050 1
4,4'-DDT ND ug/L 09/02/16 16:14 50-29-3 M109/01/16 12:000.10 0.050 1
Dieldrin ND ug/L 09/02/16 16:14 60-57-109/01/16 12:000.075 0.050 1
Endosulfan I ND ug/L 09/02/16 16:14 959-98-809/01/16 12:000.10 0.050 1
Endosulfan II ND ug/L 09/02/16 16:14 33213-65-909/01/16 12:000.10 0.050 1
Endosulfan sulfate ND ug/L 09/02/16 16:14 1031-07-809/01/16 12:000.10 0.050 1
Endrin ND ug/L 09/02/16 16:14 72-20-809/01/16 12:000.10 0.050 1
Endrin aldehyde ND ug/L 09/02/16 16:14 7421-93-4 M109/01/16 12:000.10 0.050 1
Heptachlor ND ug/L 09/02/16 16:14 76-44-809/01/16 12:000.050 0.050 1
Heptachlor epoxide ND ug/L 09/02/16 16:14 1024-57-309/01/16 12:000.075 0.050 1
Methoxychlor ND ug/L 09/02/16 16:14 72-43-5 M109/01/16 12:001.0 0.15 1
Toxaphene ND ug/L 09/02/16 16:14 8001-35-209/01/16 12:001.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)77 %09/02/16 16:14 877-09-809/01/16 12:0020-130 1
Decachlorobiphenyl (S)62 %09/02/16 16:14 2051-24-309/01/16 12:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/02/16 21:00 12674-11-209/01/16 12:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/02/16 21:00 11104-28-209/01/16 12:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/02/16 21:00 11141-16-509/01/16 12:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/02/16 21:00 53469-21-909/01/16 12:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/02/16 21:00 12672-29-609/01/16 12:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/02/16 21:00 11097-69-109/01/16 12:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/02/16 21:00 11096-82-509/01/16 12:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)59 %09/02/16 21:00 2051-24-309/01/16 12:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/03/16 03:17 25057-89-009/02/16 08:250.095 0.047 1
2,4-D ND ug/L 09/03/16 03:17 94-75-709/02/16 08:250.95 0.23 1
Dalapon ND ug/L 09/03/16 03:17 75-99-009/02/16 08:250.92 0.43 1
2,4-DB ND ug/L 09/03/16 03:17 94-82-609/02/16 08:251.9 0.51 1
Dicamba ND ug/L 09/03/16 03:17 1918-00-909/02/16 08:250.095 0.030 1
Dichlorprop ND ug/L 09/03/16 03:17 120-36-509/02/16 08:250.66 0.19 1
Dinoseb ND ug/L 09/03/16 03:17 88-85-709/02/16 08:250.19 0.057 1
Pentachlorophenol 0.022J ug/L 09/03/16 03:17 87-86-509/02/16 08:250.029 0.017 1
Picloram ND ug/L 09/03/16 03:17 1918-02-109/02/16 08:250.095 0.019 1
2,4,5-T ND ug/L 09/03/16 03:17 93-76-509/02/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/03/16 03:17 93-72-109/02/16 08:250.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 27 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-6 Lab ID:92310738004 Collected:08/30/16 13:40 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)70 %09/03/16 03:17 19719-28-909/02/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/02/16 19:15 7440-36-009/01/16 19:306.0 3.8 1
Arsenic 4.5J ug/L 09/02/16 19:15 7440-38-2 B09/01/16 19:3010.0 2.5 1
Barium 45.9J ug/L 09/02/16 19:15 7440-39-309/01/16 19:301002.5 1
Beryllium ND ug/L 09/02/16 19:15 7440-41-709/01/16 19:301.0 0.50 1
Cadmium 1.1 ug/L 09/02/16 19:15 7440-43-909/01/16 19:301.0 0.50 1
Chromium ND ug/L 09/02/16 19:15 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt ND ug/L 09/02/16 19:15 7440-48-409/01/16 19:3010.0 2.5 1
Copper ND ug/L 09/02/16 19:15 7440-50-809/01/16 19:3010.0 2.5 1
Lead ND ug/L 09/02/16 19:15 7439-92-109/01/16 19:3010.0 2.5 1
Nickel ND ug/L 09/02/16 19:15 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 19:15 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 19:15 7440-22-409/01/16 19:3010.0 2.5 1
Thallium ND ug/L 09/03/16 14:36 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 19:15 7440-31-509/01/16 19:301002.5 1
Vanadium ND ug/L 09/02/16 19:15 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 7.5J ug/L 09/02/16 19:15 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.35 ug/L 09/01/16 09:12 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 18:00 83-32-9 H209/13/16 10:2110.0 0.25 1
Acenaphthylene ND ug/L 09/15/16 18:00 208-96-8 H209/13/16 10:2110.0 0.21 1
Acetophenone ND ug/L 09/15/16 18:00 98-86-2 H209/13/16 10:2110.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/15/16 18:00 53-96-3 H209/13/16 10:2120.0 0.84 1
4-Aminobiphenyl ND ug/L 09/15/16 18:00 92-67-1 H209/13/16 10:2120.0 0.92 1
Anthracene ND ug/L 09/15/16 18:00 120-12-7 H209/13/16 10:2110.0 0.14 1
Benzo(a)anthracene ND ug/L 09/15/16 18:00 56-55-3 H209/13/16 10:2110.0 0.33 1
Benzo(a)pyrene ND ug/L 09/15/16 18:00 50-32-8 H209/13/16 10:2110.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/15/16 18:00 205-99-2 H209/13/16 10:2110.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 18:00 191-24-2 H209/13/16 10:2110.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/15/16 18:00 207-08-9 H209/13/16 10:2110.0 0.43 1
Benzyl alcohol ND ug/L 09/15/16 18:00 100-51-6 H209/13/16 10:2120.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 18:00 101-55-3 H209/13/16 10:2110.0 1.3 1
Butylbenzylphthalate ND ug/L 09/15/16 18:00 85-68-7 H209/13/16 10:2110.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 18:00 59-50-7 H209/13/16 10:2120.0 4.2 1
4-Chloroaniline ND ug/L 09/15/16 18:00 106-47-8 H209/13/16 10:2120.0 3.4 1
Chlorobenzilate ND ug/L 09/15/16 18:00 510-15-6 H209/13/16 10:2110.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 18:00 111-91-1 H209/13/16 10:2110.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 18:00 111-44-4 H209/13/16 10:2110.0 1.5 1
2-Chloronaphthalene ND ug/L 09/15/16 18:00 91-58-7 H209/13/16 10:2110.0 2.2 1
2-Chlorophenol ND ug/L 09/15/16 18:00 95-57-8 H209/13/16 10:2110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-6 Lab ID:92310738004 Collected:08/30/16 13:40 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/15/16 18:00 7005-72-3 H209/13/16 10:2110.0 2.1 1
Chrysene ND ug/L 09/15/16 18:00 218-01-9 H209/13/16 10:2110.0 0.21 1
Diallate ND ug/L 09/15/16 18:00 2303-16-4 H209/13/16 10:2110.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 18:00 53-70-3 H209/13/16 10:2110.0 0.55 1
Dibenzofuran ND ug/L 09/15/16 18:00 132-64-9 H209/13/16 10:2110.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 18:00 91-94-1 H209/13/16 10:2120.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/15/16 18:00 120-83-2 H209/13/16 10:2110.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/15/16 18:00 87-65-0 H209/13/16 10:2110.0 1.8 1
Diethylphthalate ND ug/L 09/15/16 18:00 84-66-2 H209/13/16 10:2160001.3 1
Dimethoate ND ug/L 09/15/16 18:00 60-51-5 H209/13/16 10:2120.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/15/16 18:00 60-11-7 H209/13/16 10:2110.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/15/16 18:00 57-97-6 H209/13/16 10:2110.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/15/16 18:00 119-93-7 H209/13/16 10:2110.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/15/16 18:00 105-67-9 H209/13/16 10:2110.0 2.2 1
Dimethylphthalate ND ug/L 09/15/16 18:00 131-11-3 H209/13/16 10:2110.0 1.5 1
Di-n-butylphthalate ND ug/L 09/15/16 18:00 84-74-2 H209/13/16 10:2110.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 18:00 534-52-1 H209/13/16 10:2150.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/15/16 18:00 99-65-0 H209/13/16 10:2120.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/15/16 18:00 51-28-5 H209/13/16 10:2150.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/15/16 18:00 121-14-2 H209/13/16 10:2110.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/15/16 18:00 606-20-2 H209/13/16 10:2110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/15/16 18:00 117-84-0 H209/13/16 10:2110.0 0.86 1
Diphenylamine ND ug/L 09/15/16 18:00 122-39-4 H209/13/16 10:2110.0 1.3 1
Disulfoton ND ug/L 09/15/16 18:00 298-04-4 H209/13/16 10:2110.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 18:00 117-81-7 H209/13/16 10:2115.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/15/16 18:00 62-50-0 H209/13/16 10:2120.0 1.8 1
Famphur ND ug/L 09/15/16 18:00 52-85-7 H209/13/16 10:2120.0 1.7 1
Fluoranthene ND ug/L 09/15/16 18:00 206-44-0 H209/13/16 10:2110.0 0.21 1
Fluorene ND ug/L 09/15/16 18:00 86-73-7 H209/13/16 10:2110.0 0.21 1
Hexachlorobenzene ND ug/L 09/15/16 18:00 118-74-1 H209/13/16 10:2110.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 18:00 77-47-4 H209/13/16 10:2110.0 1.8 1
Hexachloroethane ND ug/L 09/15/16 18:00 67-72-1 H209/13/16 10:2110.0 1.5 1
Hexachloropropene ND ug/L 09/15/16 18:00 1888-71-7 H209/13/16 10:2110.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 18:00 193-39-5 H209/13/16 10:2110.0 0.29 1
Isodrin ND ug/L 09/15/16 18:00 465-73-6 H209/13/16 10:2120.0 2.0 1
Isophorone ND ug/L 09/15/16 18:00 78-59-1 H209/13/16 10:2110.0 1.8 1
Isosafrole ND ug/L 09/15/16 18:00 120-58-1 H209/13/16 10:2110.0 1.8 1
Kepone ND ug/L 09/15/16 18:00 143-50-0 H209/13/16 10:2120.0 3.1 1
Methapyrilene ND ug/L 09/15/16 18:00 91-80-5 H209/13/16 10:211002.7 1
3-Methylcholanthrene ND ug/L 09/15/16 18:00 56-49-5 H209/13/16 10:2110.0 0.82 1
Methyl methanesulfonate ND ug/L 09/15/16 18:00 66-27-3 H209/13/16 10:2110.0 1.3 1
2-Methylnaphthalene ND ug/L 09/15/16 18:00 91-57-6 H209/13/16 10:2110.0 0.28 1
Methyl parathion ND ug/L 09/15/16 18:00 298-00-0 H209/13/16 10:2110.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 18:00 95-48-7 H209/13/16 10:2110.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 18:00 H209/13/16 10:2110.0 1.7 1
1-Naphthalenamine ND ug/L 09/15/16 18:00 134-32-7 H209/13/16 10:2110.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-6 Lab ID:92310738004 Collected:08/30/16 13:40 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/15/16 18:00 91-59-8 H209/13/16 10:2110.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/15/16 18:00 130-15-4 H209/13/16 10:2110.0 1.8 1
2-Nitroaniline ND ug/L 09/15/16 18:00 88-74-4 H209/13/16 10:2150.0 2.8 1
3-Nitroaniline ND ug/L 09/15/16 18:00 99-09-2 H209/13/16 10:2150.0 2.4 1
4-Nitroaniline ND ug/L 09/15/16 18:00 100-01-6 H209/13/16 10:2120.0 2.5 1
Nitrobenzene ND ug/L 09/15/16 18:00 98-95-3 H209/13/16 10:2110.0 1.7 1
2-Nitrophenol ND ug/L 09/15/16 18:00 88-75-5 H209/13/16 10:2110.0 1.7 1
4-Nitrophenol ND ug/L 09/15/16 18:00 100-02-7 H209/13/16 10:2150.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/15/16 18:00 99-55-8 H209/13/16 10:2110.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/15/16 18:00 55-18-5 H209/13/16 10:2120.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/15/16 18:00 62-75-9 H209/13/16 10:2110.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/15/16 18:00 924-16-3 H209/13/16 10:2110.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 18:00 621-64-7 H209/13/16 10:2110.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 18:00 86-30-6 H209/13/16 10:2110.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/15/16 18:00 10595-95-6 H209/13/16 10:2110.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/15/16 18:00 100-75-4 H209/13/16 10:2120.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/15/16 18:00 930-55-2 H209/13/16 10:2110.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/15/16 18:00 126-68-1 H209/13/16 10:2110.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 18:00 108-60-1 H209/13/16 10:2110.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/15/16 18:00 56-38-2 H209/13/16 10:2110.0 1.1 1
Pentachlorobenzene ND ug/L 09/15/16 18:00 608-93-5 H209/13/16 10:2110.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/15/16 18:00 82-68-8 H209/13/16 10:2120.0 1.0 1
Pentachlorophenol ND ug/L 09/15/16 18:00 87-86-5 H209/13/16 10:2125.0 2.3 1
Phenacetin ND ug/L 09/15/16 18:00 62-44-2 H209/13/16 10:2120.0 0.97 1
Phenanthrene ND ug/L 09/15/16 18:00 85-01-8 H209/13/16 10:2110.0 0.22 1
Phenol ND ug/L 09/15/16 18:00 H209/13/16 10:2110.0 1.7 1
p-Phenylenediamine ND ug/L 09/15/16 18:00 106-50-3 H209/13/16 10:2110.0 0.96 1
Phorate ND ug/L 09/15/16 18:00 298-02-2 H209/13/16 10:2110.0 1.1 1
Pronamide ND ug/L 09/15/16 18:00 23950-58-5 H209/13/16 10:2110.0 0.97 1
Pyrene ND ug/L 09/15/16 18:00 129-00-0 H209/13/16 10:2110.0 0.19 1
Safrole ND ug/L 09/15/16 18:00 94-59-7 H209/13/16 10:2110.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/15/16 18:00 95-94-3 H209/13/16 10:2110.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 18:00 58-90-2 H209/13/16 10:2110.0 2.3 1
Thionazin ND ug/L 09/15/16 18:00 297-97-2 H209/13/16 10:2120.0 1.2 1
O-Toluidine ND ug/L 09/15/16 18:00 95-53-4 H209/13/16 10:2110.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 18:00 95-95-4 H209/13/16 10:2110.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 18:00 88-06-2 H209/13/16 10:2110.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/15/16 18:00 99-35-4 H209/13/16 10:2110.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)72 %09/15/16 18:00 4165-60-009/13/16 10:2121-110 1
2-Fluorobiphenyl (S)72 %09/15/16 18:00 321-60-809/13/16 10:2127-110 1
Terphenyl-d14 (S)87 %09/15/16 18:00 1718-51-009/13/16 10:2131-107 1
Phenol-d6 (S)31 %09/15/16 18:00 13127-88-309/13/16 10:2110-110 1
2-Fluorophenol (S)38 %09/15/16 18:00 367-12-409/13/16 10:2112-110 1
2,4,6-Tribromophenol (S)71 %09/15/16 18:00 118-79-609/13/16 10:2127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-6 Lab ID:92310738004 Collected:08/30/16 13:40 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/02/16 14:51 67-64-110010.0 1
Acetonitrile ND ug/L 09/02/16 14:51 75-05-855.0 2.2 1
Acrolein ND ug/L 09/02/16 14:51 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/02/16 14:51 107-13-12001.9 1
Allyl chloride ND ug/L 09/02/16 14:51 107-05-110.0 1.5 1
Benzene ND ug/L 09/02/16 14:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/02/16 14:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/02/16 14:51 75-27-41.0 0.18 1
Bromoform ND ug/L 09/02/16 14:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/02/16 14:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/02/16 14:51 78-93-31000.96 1
Carbon disulfide ND ug/L 09/02/16 14:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/02/16 14:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/02/16 14:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/02/16 14:51 75-00-310.0 0.54 1
Chloroform ND ug/L 09/02/16 14:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/02/16 14:51 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/02/16 14:51 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/02/16 14:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/02/16 14:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/02/16 14:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/02/16 14:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/02/16 14:51 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/02/16 14:51 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/02/16 14:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/02/16 14:51 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 09/02/16 14:51 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/02/16 14:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/02/16 14:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/02/16 14:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/02/16 14:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/02/16 14:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/02/16 14:51 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/02/16 14:51 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/02/16 14:51 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/02/16 14:51 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/02/16 14:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/02/16 14:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/02/16 14:51 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/02/16 14:51 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/02/16 14:51 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/02/16 14:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/02/16 14:51 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/02/16 14:51 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/02/16 14:51 126-98-71000.93 1
Methylene Chloride ND ug/L 09/02/16 14:51 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-6 Lab ID:92310738004 Collected:08/30/16 13:40 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/02/16 14:51 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/02/16 14:51 108-10-11000.33 1
Naphthalene ND ug/L 09/02/16 14:51 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/02/16 14:51 107-12-01503.6 1
Styrene ND ug/L 09/02/16 14:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/02/16 14:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/02/16 14:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/02/16 14:51 127-18-41.0 0.46 1
Toluene ND ug/L 09/02/16 14:51 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/02/16 14:51 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/02/16 14:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/02/16 14:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/02/16 14:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/02/16 14:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/02/16 14:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/02/16 14:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/02/16 14:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/02/16 14:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %09/02/16 14:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/02/16 14:51 17060-07-070-130 1
Toluene-d8 (S)104 %09/02/16 14:51 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 21:16 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.0J ug/L 09/12/16 23:59 57-12-5 M1,R110.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-7 Lab ID:92310738005 Collected:08/30/16 14:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/02/16 16:49 309-00-209/01/16 12:000.050 0.050 1
alpha-BHC ND ug/L 09/02/16 16:49 319-84-609/01/16 12:000.050 0.050 1
beta-BHC ND ug/L 09/02/16 16:49 319-85-709/01/16 12:000.050 0.050 1
delta-BHC ND ug/L 09/02/16 16:49 319-86-809/01/16 12:000.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/02/16 16:49 58-89-909/01/16 12:000.050 0.050 1
Chlordane (Technical)ND ug/L 09/02/16 16:49 57-74-909/01/16 12:000.50 0.20 1
4,4'-DDD ND ug/L 09/02/16 16:49 72-54-809/01/16 12:000.10 0.050 1
4,4'-DDE ND ug/L 09/02/16 16:49 72-55-909/01/16 12:000.10 0.050 1
4,4'-DDT ND ug/L 09/02/16 16:49 50-29-309/01/16 12:000.10 0.050 1
Dieldrin ND ug/L 09/02/16 16:49 60-57-109/01/16 12:000.075 0.050 1
Endosulfan I ND ug/L 09/02/16 16:49 959-98-809/01/16 12:000.10 0.050 1
Endosulfan II ND ug/L 09/02/16 16:49 33213-65-909/01/16 12:000.10 0.050 1
Endosulfan sulfate ND ug/L 09/02/16 16:49 1031-07-809/01/16 12:000.10 0.050 1
Endrin ND ug/L 09/02/16 16:49 72-20-809/01/16 12:000.10 0.050 1
Endrin aldehyde ND ug/L 09/02/16 16:49 7421-93-409/01/16 12:000.10 0.050 1
Heptachlor ND ug/L 09/02/16 16:49 76-44-809/01/16 12:000.050 0.050 1
Heptachlor epoxide ND ug/L 09/02/16 16:49 1024-57-309/01/16 12:000.075 0.050 1
Methoxychlor ND ug/L 09/02/16 16:49 72-43-509/01/16 12:001.0 0.15 1
Toxaphene ND ug/L 09/02/16 16:49 8001-35-209/01/16 12:001.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)89 %09/02/16 16:49 877-09-809/01/16 12:0020-130 1
Decachlorobiphenyl (S)63 %09/02/16 16:49 2051-24-309/01/16 12:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/02/16 21:42 12674-11-209/01/16 12:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/02/16 21:42 11104-28-209/01/16 12:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/02/16 21:42 11141-16-509/01/16 12:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/02/16 21:42 53469-21-909/01/16 12:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/02/16 21:42 12672-29-609/01/16 12:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/02/16 21:42 11097-69-109/01/16 12:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/02/16 21:42 11096-82-509/01/16 12:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)59 %09/02/16 21:42 2051-24-309/01/16 12:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/03/16 03:47 25057-89-009/02/16 08:250.095 0.047 1
2,4-D ND ug/L 09/03/16 03:47 94-75-709/02/16 08:250.95 0.23 1
Dalapon ND ug/L 09/03/16 03:47 75-99-009/02/16 08:250.92 0.43 1
2,4-DB ND ug/L 09/03/16 03:47 94-82-609/02/16 08:251.9 0.51 1
Dicamba ND ug/L 09/03/16 03:47 1918-00-909/02/16 08:250.095 0.030 1
Dichlorprop ND ug/L 09/03/16 03:47 120-36-509/02/16 08:250.66 0.19 1
Dinoseb ND ug/L 09/03/16 03:47 88-85-709/02/16 08:250.19 0.058 1
Pentachlorophenol ND ug/L 09/03/16 03:47 87-86-509/02/16 08:250.029 0.017 1
Picloram ND ug/L 09/03/16 03:47 1918-02-109/02/16 08:250.095 0.019 1
2,4,5-T ND ug/L 09/03/16 03:47 93-76-509/02/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/03/16 03:47 93-72-109/02/16 08:250.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-7 Lab ID:92310738005 Collected:08/30/16 14:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)82 %09/03/16 03:47 19719-28-909/02/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/02/16 19:18 7440-36-009/01/16 19:306.0 3.8 1
Arsenic ND ug/L 09/02/16 19:18 7440-38-209/01/16 19:3010.0 2.5 1
Barium 45.5J ug/L 09/02/16 19:18 7440-39-309/01/16 19:301002.5 1
Beryllium ND ug/L 09/02/16 19:18 7440-41-709/01/16 19:301.0 0.50 1
Cadmium ND ug/L 09/02/16 19:18 7440-43-909/01/16 19:301.0 0.50 1
Chromium ND ug/L 09/02/16 19:18 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt ND ug/L 09/02/16 19:18 7440-48-409/01/16 19:3010.0 2.5 1
Copper 4.3J ug/L 09/02/16 19:18 7440-50-809/01/16 19:3010.0 2.5 1
Lead ND ug/L 09/02/16 19:18 7439-92-109/01/16 19:3010.0 2.5 1
Nickel ND ug/L 09/02/16 19:18 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 19:18 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 19:18 7440-22-409/01/16 19:3010.0 2.5 1
Thallium ND ug/L 09/03/16 14:39 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 19:18 7440-31-509/01/16 19:301002.5 1
Vanadium ND ug/L 09/02/16 19:18 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 7.2J ug/L 09/02/16 19:18 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.27 ug/L 09/01/16 09:15 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 18:29 83-32-9 H209/13/16 10:2110.0 0.25 1
Acenaphthylene ND ug/L 09/15/16 18:29 208-96-8 H209/13/16 10:2110.0 0.21 1
Acetophenone ND ug/L 09/15/16 18:29 98-86-2 H209/13/16 10:2110.0 2.0 1
2-Acetylaminofluorene 7.0J ug/L 09/15/16 18:29 53-96-3 H209/13/16 10:2120.0 0.84 1
4-Aminobiphenyl ND ug/L 09/15/16 18:29 92-67-1 H209/13/16 10:2120.0 0.92 1
Anthracene ND ug/L 09/15/16 18:29 120-12-7 H209/13/16 10:2110.0 0.14 1
Benzo(a)anthracene ND ug/L 09/15/16 18:29 56-55-3 H209/13/16 10:2110.0 0.33 1
Benzo(a)pyrene ND ug/L 09/15/16 18:29 50-32-8 H209/13/16 10:2110.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/15/16 18:29 205-99-2 H209/13/16 10:2110.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 18:29 191-24-2 H209/13/16 10:2110.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/15/16 18:29 207-08-9 H209/13/16 10:2110.0 0.43 1
Benzyl alcohol ND ug/L 09/15/16 18:29 100-51-6 H209/13/16 10:2120.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 18:29 101-55-3 H209/13/16 10:2110.0 1.3 1
Butylbenzylphthalate ND ug/L 09/15/16 18:29 85-68-7 H209/13/16 10:2110.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 18:29 59-50-7 H209/13/16 10:2120.0 4.2 1
4-Chloroaniline ND ug/L 09/15/16 18:29 106-47-8 H209/13/16 10:2120.0 3.4 1
Chlorobenzilate ND ug/L 09/15/16 18:29 510-15-6 H209/13/16 10:2110.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 18:29 111-91-1 H209/13/16 10:2110.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 18:29 111-44-4 H209/13/16 10:2110.0 1.5 1
2-Chloronaphthalene ND ug/L 09/15/16 18:29 91-58-7 H209/13/16 10:2110.0 2.2 1
2-Chlorophenol ND ug/L 09/15/16 18:29 95-57-8 H209/13/16 10:2110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-7 Lab ID:92310738005 Collected:08/30/16 14:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/15/16 18:29 7005-72-3 H209/13/16 10:2110.0 2.1 1
Chrysene ND ug/L 09/15/16 18:29 218-01-9 H209/13/16 10:2110.0 0.21 1
Diallate ND ug/L 09/15/16 18:29 2303-16-4 H209/13/16 10:2110.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 18:29 53-70-3 H209/13/16 10:2110.0 0.55 1
Dibenzofuran ND ug/L 09/15/16 18:29 132-64-9 H209/13/16 10:2110.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 18:29 91-94-1 H209/13/16 10:2120.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/15/16 18:29 120-83-2 H209/13/16 10:2110.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/15/16 18:29 87-65-0 H209/13/16 10:2110.0 1.8 1
Diethylphthalate ND ug/L 09/15/16 18:29 84-66-2 H209/13/16 10:2160001.3 1
Dimethoate ND ug/L 09/15/16 18:29 60-51-5 H209/13/16 10:2120.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/15/16 18:29 60-11-7 H209/13/16 10:2110.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/15/16 18:29 57-97-6 H209/13/16 10:2110.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/15/16 18:29 119-93-7 H209/13/16 10:2110.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/15/16 18:29 105-67-9 H209/13/16 10:2110.0 2.2 1
Dimethylphthalate ND ug/L 09/15/16 18:29 131-11-3 H209/13/16 10:2110.0 1.5 1
Di-n-butylphthalate ND ug/L 09/15/16 18:29 84-74-2 H209/13/16 10:2110.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 18:29 534-52-1 H209/13/16 10:2150.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/15/16 18:29 99-65-0 H209/13/16 10:2120.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/15/16 18:29 51-28-5 H209/13/16 10:2150.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/15/16 18:29 121-14-2 H209/13/16 10:2110.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/15/16 18:29 606-20-2 H209/13/16 10:2110.0 1.7 1
Di-n-octylphthalate ND ug/L 09/15/16 18:29 117-84-0 H209/13/16 10:2110.0 0.86 1
Diphenylamine ND ug/L 09/15/16 18:29 122-39-4 H209/13/16 10:2110.0 1.3 1
Disulfoton ND ug/L 09/15/16 18:29 298-04-4 H209/13/16 10:2110.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 18:29 117-81-7 H209/13/16 10:2115.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/15/16 18:29 62-50-0 H209/13/16 10:2120.0 1.8 1
Famphur ND ug/L 09/15/16 18:29 52-85-7 H209/13/16 10:2120.0 1.7 1
Fluoranthene ND ug/L 09/15/16 18:29 206-44-0 H209/13/16 10:2110.0 0.21 1
Fluorene ND ug/L 09/15/16 18:29 86-73-7 H209/13/16 10:2110.0 0.21 1
Hexachlorobenzene ND ug/L 09/15/16 18:29 118-74-1 H209/13/16 10:2110.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 18:29 77-47-4 H209/13/16 10:2110.0 1.8 1
Hexachloroethane ND ug/L 09/15/16 18:29 67-72-1 H209/13/16 10:2110.0 1.5 1
Hexachloropropene ND ug/L 09/15/16 18:29 1888-71-7 H209/13/16 10:2110.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 18:29 193-39-5 H209/13/16 10:2110.0 0.29 1
Isodrin ND ug/L 09/15/16 18:29 465-73-6 H209/13/16 10:2120.0 2.0 1
Isophorone ND ug/L 09/15/16 18:29 78-59-1 H209/13/16 10:2110.0 1.8 1
Isosafrole ND ug/L 09/15/16 18:29 120-58-1 H209/13/16 10:2110.0 1.8 1
Kepone ND ug/L 09/15/16 18:29 143-50-0 H209/13/16 10:2120.0 3.1 1
Methapyrilene ND ug/L 09/15/16 18:29 91-80-5 H209/13/16 10:211002.7 1
3-Methylcholanthrene ND ug/L 09/15/16 18:29 56-49-5 H209/13/16 10:2110.0 0.82 1
Methyl methanesulfonate ND ug/L 09/15/16 18:29 66-27-3 H209/13/16 10:2110.0 1.3 1
2-Methylnaphthalene ND ug/L 09/15/16 18:29 91-57-6 H209/13/16 10:2110.0 0.28 1
Methyl parathion ND ug/L 09/15/16 18:29 298-00-0 H209/13/16 10:2110.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 18:29 95-48-7 H209/13/16 10:2110.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 18:29 H209/13/16 10:2110.0 1.7 1
1-Naphthalenamine ND ug/L 09/15/16 18:29 134-32-7 H209/13/16 10:2110.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-7 Lab ID:92310738005 Collected:08/30/16 14:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/15/16 18:29 91-59-8 H209/13/16 10:2110.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/15/16 18:29 130-15-4 H209/13/16 10:2110.0 1.8 1
2-Nitroaniline ND ug/L 09/15/16 18:29 88-74-4 H209/13/16 10:2150.0 2.8 1
3-Nitroaniline ND ug/L 09/15/16 18:29 99-09-2 H209/13/16 10:2150.0 2.4 1
4-Nitroaniline ND ug/L 09/15/16 18:29 100-01-6 H209/13/16 10:2120.0 2.5 1
Nitrobenzene ND ug/L 09/15/16 18:29 98-95-3 H209/13/16 10:2110.0 1.7 1
2-Nitrophenol ND ug/L 09/15/16 18:29 88-75-5 H209/13/16 10:2110.0 1.7 1
4-Nitrophenol ND ug/L 09/15/16 18:29 100-02-7 H209/13/16 10:2150.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/15/16 18:29 99-55-8 H209/13/16 10:2110.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/15/16 18:29 55-18-5 H209/13/16 10:2120.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/15/16 18:29 62-75-9 H209/13/16 10:2110.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/15/16 18:29 924-16-3 H209/13/16 10:2110.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 18:29 621-64-7 H209/13/16 10:2110.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 18:29 86-30-6 H209/13/16 10:2110.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/15/16 18:29 10595-95-6 H209/13/16 10:2110.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/15/16 18:29 100-75-4 H209/13/16 10:2120.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/15/16 18:29 930-55-2 H209/13/16 10:2110.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/15/16 18:29 126-68-1 H209/13/16 10:2110.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 18:29 108-60-1 H209/13/16 10:2110.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/15/16 18:29 56-38-2 H209/13/16 10:2110.0 1.1 1
Pentachlorobenzene ND ug/L 09/15/16 18:29 608-93-5 H209/13/16 10:2110.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/15/16 18:29 82-68-8 H209/13/16 10:2120.0 1.0 1
Pentachlorophenol ND ug/L 09/15/16 18:29 87-86-5 H209/13/16 10:2125.0 2.3 1
Phenacetin ND ug/L 09/15/16 18:29 62-44-2 H209/13/16 10:2120.0 0.97 1
Phenanthrene ND ug/L 09/15/16 18:29 85-01-8 H209/13/16 10:2110.0 0.22 1
Phenol ND ug/L 09/15/16 18:29 H209/13/16 10:2110.0 1.7 1
p-Phenylenediamine ND ug/L 09/15/16 18:29 106-50-3 H209/13/16 10:2110.0 0.96 1
Phorate ND ug/L 09/15/16 18:29 298-02-2 H209/13/16 10:2110.0 1.1 1
Pronamide ND ug/L 09/15/16 18:29 23950-58-5 H209/13/16 10:2110.0 0.97 1
Pyrene ND ug/L 09/15/16 18:29 129-00-0 H209/13/16 10:2110.0 0.19 1
Safrole ND ug/L 09/15/16 18:29 94-59-7 H209/13/16 10:2110.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/15/16 18:29 95-94-3 H209/13/16 10:2110.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 18:29 58-90-2 H209/13/16 10:2110.0 2.3 1
Thionazin ND ug/L 09/15/16 18:29 297-97-2 H209/13/16 10:2120.0 1.2 1
O-Toluidine ND ug/L 09/15/16 18:29 95-53-4 H209/13/16 10:2110.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 18:29 95-95-4 H209/13/16 10:2110.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 18:29 88-06-2 H209/13/16 10:2110.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/15/16 18:29 99-35-4 H209/13/16 10:2110.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)72 %09/15/16 18:29 4165-60-009/13/16 10:2121-110 1
2-Fluorobiphenyl (S)73 %09/15/16 18:29 321-60-809/13/16 10:2127-110 1
Terphenyl-d14 (S)80 %09/15/16 18:29 1718-51-009/13/16 10:2131-107 1
Phenol-d6 (S)31 %09/15/16 18:29 13127-88-309/13/16 10:2110-110 1
2-Fluorophenol (S)41 %09/15/16 18:29 367-12-409/13/16 10:2112-110 1
2,4,6-Tribromophenol (S)83 %09/15/16 18:29 118-79-609/13/16 10:2127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 36 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-7 Lab ID:92310738005 Collected:08/30/16 14:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/02/16 15:08 67-64-110010.0 1
Acetonitrile ND ug/L 09/02/16 15:08 75-05-855.0 2.2 1
Acrolein ND ug/L 09/02/16 15:08 107-02-8 M153.0 1.6 1
Acrylonitrile ND ug/L 09/02/16 15:08 107-13-12001.9 1
Allyl chloride ND ug/L 09/02/16 15:08 107-05-110.0 1.5 1
Benzene ND ug/L 09/02/16 15:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/02/16 15:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/02/16 15:08 75-27-41.0 0.18 1
Bromoform ND ug/L 09/02/16 15:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/02/16 15:08 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 09/02/16 15:08 78-93-31000.96 1
Carbon disulfide ND ug/L 09/02/16 15:08 75-15-0 M11001.2 1
Carbon tetrachloride ND ug/L 09/02/16 15:08 56-23-5 M11.0 0.25 1
Chlorobenzene ND ug/L 09/02/16 15:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/02/16 15:08 75-00-310.0 0.54 1
Chloroform ND ug/L 09/02/16 15:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/02/16 15:08 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/02/16 15:08 126-99-8 M120.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/02/16 15:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/02/16 15:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/02/16 15:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/02/16 15:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/02/16 15:08 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/02/16 15:08 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/02/16 15:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/02/16 15:08 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 09/02/16 15:08 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/02/16 15:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/02/16 15:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/02/16 15:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/02/16 15:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/02/16 15:08 156-60-5 M15.0 0.49 1
1,2-Dichloropropane ND ug/L 09/02/16 15:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/02/16 15:08 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/02/16 15:08 594-20-7 M115.0 0.13 1
1,1-Dichloropropene ND ug/L 09/02/16 15:08 563-58-6 M15.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/02/16 15:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/02/16 15:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/02/16 15:08 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/02/16 15:08 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/02/16 15:08 87-68-3 M110.0 0.71 1
2-Hexanone ND ug/L 09/02/16 15:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/02/16 15:08 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/02/16 15:08 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/02/16 15:08 126-98-71000.93 1
Methylene Chloride ND ug/L 09/02/16 15:08 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 37 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-7 Lab ID:92310738005 Collected:08/30/16 14:30 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/02/16 15:08 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/02/16 15:08 108-10-11000.33 1
Naphthalene ND ug/L 09/02/16 15:08 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/02/16 15:08 107-12-01503.6 1
Styrene ND ug/L 09/02/16 15:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/02/16 15:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/02/16 15:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/02/16 15:08 127-18-41.0 0.46 1
Toluene ND ug/L 09/02/16 15:08 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/02/16 15:08 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/02/16 15:08 71-55-6 M11.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/02/16 15:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/02/16 15:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/02/16 15:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/02/16 15:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/02/16 15:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/02/16 15:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/02/16 15:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %09/02/16 15:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %09/02/16 15:08 17060-07-070-130 1
Toluene-d8 (S)104 %09/02/16 15:08 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 21:16 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.4J ug/L 09/13/16 00:02 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-16R Lab ID:92310738006 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/02/16 17:24 309-00-209/01/16 12:000.10 0.10 1
alpha-BHC ND ug/L 09/02/16 17:24 319-84-609/01/16 12:000.10 0.10 1
beta-BHC ND ug/L 09/02/16 17:24 319-85-709/01/16 12:000.10 0.10 1
delta-BHC ND ug/L 09/02/16 17:24 319-86-809/01/16 12:000.10 0.10 1
gamma-BHC (Lindane)ND ug/L 09/02/16 17:24 58-89-909/01/16 12:000.10 0.10 1
Chlordane (Technical)ND ug/L 09/02/16 17:24 57-74-909/01/16 12:001.0 0.40 1
4,4'-DDD ND ug/L 09/02/16 17:24 72-54-809/01/16 12:000.20 0.10 1
4,4'-DDE ND ug/L 09/02/16 17:24 72-55-909/01/16 12:000.20 0.10 1
4,4'-DDT ND ug/L 09/02/16 17:24 50-29-309/01/16 12:000.20 0.10 1
Dieldrin ND ug/L 09/02/16 17:24 60-57-109/01/16 12:000.15 0.10 1
Endosulfan I ND ug/L 09/02/16 17:24 959-98-809/01/16 12:000.20 0.10 1
Endosulfan II ND ug/L 09/02/16 17:24 33213-65-909/01/16 12:000.20 0.10 1
Endosulfan sulfate ND ug/L 09/02/16 17:24 1031-07-809/01/16 12:000.20 0.10 1
Endrin ND ug/L 09/02/16 17:24 72-20-809/01/16 12:000.20 0.10 1
Endrin aldehyde ND ug/L 09/02/16 17:24 7421-93-409/01/16 12:000.20 0.10 1
Heptachlor ND ug/L 09/02/16 17:24 76-44-809/01/16 12:000.10 0.10 1
Heptachlor epoxide ND ug/L 09/02/16 17:24 1024-57-309/01/16 12:000.15 0.10 1
Methoxychlor ND ug/L 09/02/16 17:24 72-43-509/01/16 12:002.0 0.30 1
Toxaphene ND ug/L 09/02/16 17:24 8001-35-209/01/16 12:003.0 0.40 1
Surrogates
Tetrachloro-m-xylene (S)85 %09/02/16 17:24 877-09-809/01/16 12:0020-130 1
Decachlorobiphenyl (S)46 %09/02/16 17:24 2051-24-309/01/16 12:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/02/16 22:24 12674-11-209/01/16 12:001.0 1.0 1
PCB-1221 (Aroclor 1221)ND ug/L 09/02/16 22:24 11104-28-209/01/16 12:001.0 1.0 1
PCB-1232 (Aroclor 1232)ND ug/L 09/02/16 22:24 11141-16-509/01/16 12:001.0 1.0 1
PCB-1242 (Aroclor 1242)ND ug/L 09/02/16 22:24 53469-21-909/01/16 12:001.0 1.0 1
PCB-1248 (Aroclor 1248)ND ug/L 09/02/16 22:24 12672-29-609/01/16 12:001.0 1.0 1
PCB-1254 (Aroclor 1254)ND ug/L 09/02/16 22:24 11097-69-109/01/16 12:001.0 1.0 1
PCB-1260 (Aroclor 1260)ND ug/L 09/02/16 22:24 11096-82-509/01/16 12:001.0 1.0 1
Surrogates
Decachlorobiphenyl (S)43 %09/02/16 22:24 2051-24-309/01/16 12:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/03/16 04:17 25057-89-009/02/16 08:250.095 0.047 1
2,4-D ND ug/L 09/03/16 04:17 94-75-709/02/16 08:250.95 0.23 1
Dalapon ND ug/L 09/03/16 04:17 75-99-009/02/16 08:250.92 0.43 1
2,4-DB ND ug/L 09/03/16 04:17 94-82-609/02/16 08:251.9 0.51 1
Dicamba ND ug/L 09/03/16 04:17 1918-00-909/02/16 08:250.095 0.030 1
Dichlorprop ND ug/L 09/03/16 04:17 120-36-509/02/16 08:250.66 0.19 1
Dinoseb ND ug/L 09/03/16 04:17 88-85-709/02/16 08:250.19 0.057 1
Pentachlorophenol ND ug/L 09/03/16 04:17 87-86-509/02/16 08:250.029 0.017 1
Picloram ND ug/L 09/03/16 04:17 1918-02-109/02/16 08:250.095 0.019 1
2,4,5-T ND ug/L 09/03/16 04:17 93-76-509/02/16 08:250.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/03/16 04:17 93-72-109/02/16 08:250.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-16R Lab ID:92310738006 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)78 %09/03/16 04:17 19719-28-909/02/16 08:2539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/02/16 19:21 7440-36-009/01/16 19:306.0 3.8 1
Arsenic ND ug/L 09/02/16 19:21 7440-38-209/01/16 19:3010.0 2.5 1
Barium 32.2J ug/L 09/02/16 19:21 7440-39-309/01/16 19:301002.5 1
Beryllium ND ug/L 09/02/16 19:21 7440-41-709/01/16 19:301.0 0.50 1
Cadmium ND ug/L 09/02/16 19:21 7440-43-909/01/16 19:301.0 0.50 1
Chromium 3.8J ug/L 09/02/16 19:21 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt ND ug/L 09/02/16 19:21 7440-48-409/01/16 19:3010.0 2.5 1
Copper 3.4J ug/L 09/02/16 19:21 7440-50-809/01/16 19:3010.0 2.5 1
Lead ND ug/L 09/02/16 19:21 7439-92-109/01/16 19:3010.0 2.5 1
Nickel ND ug/L 09/02/16 19:21 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 19:21 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 19:21 7440-22-409/01/16 19:3010.0 2.5 1
Thallium ND ug/L 09/03/16 14:42 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 19:21 7440-31-509/01/16 19:301002.5 1
Vanadium 5.5J ug/L 09/02/16 19:21 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 5.2J ug/L 09/02/16 19:21 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/01/16 09:17 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 14:10 83-32-909/02/16 11:0220.0 0.50 1
Acenaphthylene ND ug/L 09/15/16 14:10 208-96-809/02/16 11:0220.0 0.42 1
Acetophenone ND ug/L 09/15/16 14:10 98-86-2 L309/02/16 11:0220.0 3.9 1
2-Acetylaminofluorene ND ug/L 09/15/16 14:10 53-96-309/02/16 11:0240.0 1.7 1
4-Aminobiphenyl ND ug/L 09/15/16 14:10 92-67-109/02/16 11:0240.0 1.8 1
Anthracene ND ug/L 09/15/16 14:10 120-12-709/02/16 11:0220.0 0.28 1
Benzo(a)anthracene ND ug/L 09/15/16 14:10 56-55-309/02/16 11:0220.0 0.66 1
Benzo(a)pyrene ND ug/L 09/15/16 14:10 50-32-809/02/16 11:0220.0 0.60 1
Benzo(b)fluoranthene ND ug/L 09/15/16 14:10 205-99-209/02/16 11:0220.0 0.56 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 14:10 191-24-209/02/16 11:0220.0 0.76 1
Benzo(k)fluoranthene ND ug/L 09/15/16 14:10 207-08-909/02/16 11:0220.0 0.86 1
Benzyl alcohol ND ug/L 09/15/16 14:10 100-51-609/02/16 11:0240.0 6.8 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 14:10 101-55-309/02/16 11:0220.0 2.6 1
Butylbenzylphthalate ND ug/L 09/15/16 14:10 85-68-709/02/16 11:0220.0 1.5 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 14:10 59-50-709/02/16 11:0240.0 8.3 1
4-Chloroaniline ND ug/L 09/15/16 14:10 106-47-809/02/16 11:0240.0 6.8 1
Chlorobenzilate ND ug/L 09/15/16 14:10 510-15-609/02/16 11:0220.0 1.4 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 14:10 111-91-109/02/16 11:0220.0 3.4 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 14:10 111-44-409/02/16 11:0220.0 2.9 1
2-Chloronaphthalene ND ug/L 09/15/16 14:10 91-58-709/02/16 11:0220.0 4.4 1
2-Chlorophenol ND ug/L 09/15/16 14:10 95-57-809/02/16 11:0220.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-16R Lab ID:92310738006 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/15/16 14:10 7005-72-309/02/16 11:0220.0 4.2 1
Chrysene ND ug/L 09/15/16 14:10 218-01-909/02/16 11:0220.0 0.42 1
Diallate ND ug/L 09/15/16 14:10 2303-16-409/02/16 11:0220.0 2.6 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 14:10 53-70-309/02/16 11:0220.0 1.1 1
Dibenzofuran ND ug/L 09/15/16 14:10 132-64-909/02/16 11:0220.0 3.5 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 14:10 91-94-109/02/16 11:0240.0 2.8 1
2,4-Dichlorophenol ND ug/L 09/15/16 14:10 120-83-209/02/16 11:0220.0 3.3 1
2,6-Dichlorophenol ND ug/L 09/15/16 14:10 87-65-009/02/16 11:0220.0 3.6 1
Diethylphthalate ND ug/L 09/15/16 14:10 84-66-209/02/16 11:02120002.7 1
Dimethoate ND ug/L 09/15/16 14:10 60-51-509/02/16 11:0240.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 09/15/16 14:10 60-11-709/02/16 11:0220.0 0.70 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/15/16 14:10 57-97-609/02/16 11:0220.0 1.5 1
3,3'-Dimethylbenzidine ND ug/L 09/15/16 14:10 119-93-709/02/16 11:0220.0 4.3 1
2,4-Dimethylphenol ND ug/L 09/15/16 14:10 105-67-909/02/16 11:0220.0 4.4 1
Dimethylphthalate ND ug/L 09/15/16 14:10 131-11-309/02/16 11:0220.0 3.0 1
Di-n-butylphthalate ND ug/L 09/15/16 14:10 84-74-209/02/16 11:0220.0 2.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 14:10 534-52-109/02/16 11:021003.3 1
1,3-Dinitrobenzene ND ug/L 09/15/16 14:10 99-65-009/02/16 11:0240.0 3.0 1
2,4-Dinitrophenol ND ug/L 09/15/16 14:10 51-28-509/02/16 11:0210013.1 1
2,4-Dinitrotoluene ND ug/L 09/15/16 14:10 121-14-209/02/16 11:0220.0 2.4 1
2,6-Dinitrotoluene ND ug/L 09/15/16 14:10 606-20-209/02/16 11:0220.0 3.4 1
Di-n-octylphthalate ND ug/L 09/15/16 14:10 117-84-009/02/16 11:0220.0 1.7 1
Diphenylamine ND ug/L 09/15/16 14:10 122-39-409/02/16 11:0220.0 2.6 1
Disulfoton ND ug/L 09/15/16 14:10 298-04-409/02/16 11:0220.0 2.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 14:10 117-81-709/02/16 11:0230.0 1.7 1
Ethyl methanesulfonate ND ug/L 09/15/16 14:10 62-50-009/02/16 11:0240.0 3.6 1
Famphur ND ug/L 09/15/16 14:10 52-85-709/02/16 11:0240.0 3.5 1
Fluoranthene ND ug/L 09/15/16 14:10 206-44-009/02/16 11:0220.0 0.42 1
Fluorene ND ug/L 09/15/16 14:10 86-73-709/02/16 11:0220.0 0.42 1
Hexachlorobenzene ND ug/L 09/15/16 14:10 118-74-109/02/16 11:0220.0 2.3 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 14:10 77-47-409/02/16 11:0220.0 3.5 1
Hexachloroethane ND ug/L 09/15/16 14:10 67-72-109/02/16 11:0220.0 2.9 1
Hexachloropropene ND ug/L 09/15/16 14:10 1888-71-709/02/16 11:0220.0 3.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 14:10 193-39-509/02/16 11:0220.0 0.58 1
Isodrin ND ug/L 09/15/16 14:10 465-73-609/02/16 11:0240.0 4.1 1
Isophorone ND ug/L 09/15/16 14:10 78-59-109/02/16 11:0220.0 3.5 1
Isosafrole ND ug/L 09/15/16 14:10 120-58-109/02/16 11:0220.0 3.6 1
Kepone ND ug/L 09/15/16 14:10 143-50-009/02/16 11:0240.0 6.3 1
Methapyrilene ND ug/L 09/15/16 14:10 91-80-509/02/16 11:022005.5 1
3-Methylcholanthrene ND ug/L 09/15/16 14:10 56-49-509/02/16 11:0220.0 1.6 1
Methyl methanesulfonate ND ug/L 09/15/16 14:10 66-27-309/02/16 11:0220.0 2.5 1
2-Methylnaphthalene ND ug/L 09/15/16 14:10 91-57-609/02/16 11:0220.0 0.56 1
Methyl parathion ND ug/L 09/15/16 14:10 298-00-009/02/16 11:0220.0 2.2 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 14:10 95-48-709/02/16 11:0220.0 3.5 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 14:1009/02/16 11:0220.0 3.4 1
1-Naphthalenamine ND ug/L 09/15/16 14:10 134-32-709/02/16 11:0220.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 41 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-16R Lab ID:92310738006 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/15/16 14:10 91-59-809/02/16 11:0220.0 2.0 1
1,4-Naphthoquinone ND ug/L 09/15/16 14:10 130-15-409/02/16 11:0220.0 3.6 1
2-Nitroaniline ND ug/L 09/15/16 14:10 88-74-409/02/16 11:021005.6 1
3-Nitroaniline ND ug/L 09/15/16 14:10 99-09-209/02/16 11:021004.8 1
4-Nitroaniline ND ug/L 09/15/16 14:10 100-01-609/02/16 11:0240.0 5.1 1
Nitrobenzene ND ug/L 09/15/16 14:10 98-95-309/02/16 11:0220.0 3.3 1
2-Nitrophenol ND ug/L 09/15/16 14:10 88-75-509/02/16 11:0220.0 3.3 1
4-Nitrophenol ND ug/L 09/15/16 14:10 100-02-709/02/16 11:0210011.6 1
5-Nitro-o-toluidine ND ug/L 09/15/16 14:10 99-55-809/02/16 11:0220.0 2.4 1
N-Nitrosodiethylamine ND ug/L 09/15/16 14:10 55-18-5 L309/02/16 11:0240.0 3.6 1
N-Nitrosodimethylamine ND ug/L 09/15/16 14:10 62-75-909/02/16 11:0220.0 2.5 1
N-Nitroso-di-n-butylamine ND ug/L 09/15/16 14:10 924-16-309/02/16 11:0220.0 4.4 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 14:10 621-64-7 L309/02/16 11:0220.0 4.1 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 14:10 86-30-609/02/16 11:0220.0 2.6 1
N-Nitrosomethylethylamine ND ug/L 09/15/16 14:10 10595-95-609/02/16 11:0220.0 3.6 1
N-Nitrosopiperidine ND ug/L 09/15/16 14:10 100-75-409/02/16 11:0240.0 3.7 1
N-Nitrosopyrrolidine ND ug/L 09/15/16 14:10 930-55-2 L309/02/16 11:0220.0 5.0 1
O,O,O-Triethylphosphorothioate ND ug/L 09/15/16 14:10 126-68-109/02/16 11:0220.0 3.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 14:10 108-60-109/02/16 11:0220.0 3.2 1
Parathion (Ethyl parathion)ND ug/L 09/15/16 14:10 56-38-209/02/16 11:0220.0 2.1 1
Pentachlorobenzene ND ug/L 09/15/16 14:10 608-93-509/02/16 11:0220.0 4.0 1
Pentachloronitrobenzene ND ug/L 09/15/16 14:10 82-68-809/02/16 11:0240.0 2.0 1
Pentachlorophenol ND ug/L 09/15/16 14:10 87-86-509/02/16 11:0250.0 4.6 1
Phenacetin ND ug/L 09/15/16 14:10 62-44-209/02/16 11:0240.0 1.9 1
Phenanthrene ND ug/L 09/15/16 14:10 85-01-809/02/16 11:0220.0 0.44 1
Phenol ND ug/L 09/15/16 14:1009/02/16 11:0220.0 3.4 1
p-Phenylenediamine ND ug/L 09/15/16 14:10 106-50-309/02/16 11:0220.0 1.9 1
Phorate ND ug/L 09/15/16 14:10 298-02-209/02/16 11:0220.0 2.1 1
Pronamide ND ug/L 09/15/16 14:10 23950-58-509/02/16 11:0220.0 1.9 1
Pyrene ND ug/L 09/15/16 14:10 129-00-009/02/16 11:0220.0 0.38 1
Safrole ND ug/L 09/15/16 14:10 94-59-709/02/16 11:0220.0 3.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/15/16 14:10 95-94-309/02/16 11:0220.0 3.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 14:10 58-90-209/02/16 11:0220.0 4.5 1
Thionazin ND ug/L 09/15/16 14:10 297-97-209/02/16 11:0240.0 2.4 1
O-Toluidine ND ug/L 09/15/16 14:10 95-53-409/02/16 11:0220.0 3.3 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 14:10 95-95-409/02/16 11:0220.0 4.5 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 14:10 88-06-209/02/16 11:0220.0 3.8 1
1,3,5-Trinitrobenzene ND ug/L 09/15/16 14:10 99-35-409/02/16 11:0220.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)73 %09/15/16 14:10 4165-60-009/02/16 11:0221-110 1
2-Fluorobiphenyl (S)74 %09/15/16 14:10 321-60-809/02/16 11:0227-110 1
Terphenyl-d14 (S)84 %09/15/16 14:10 1718-51-009/02/16 11:0231-107 1
Phenol-d6 (S)43 %09/15/16 14:10 13127-88-309/02/16 11:0210-110 1
2-Fluorophenol (S)51 %09/15/16 14:10 367-12-409/02/16 11:0212-110 1
2,4,6-Tribromophenol (S)86 %09/15/16 14:10 118-79-609/02/16 11:0227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-16R Lab ID:92310738006 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 28.7J ug/L 09/02/16 15:25 67-64-1 B10010.0 1
Acetonitrile ND ug/L 09/02/16 15:25 75-05-855.0 2.2 1
Acrolein ND ug/L 09/02/16 15:25 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/02/16 15:25 107-13-12001.9 1
Allyl chloride ND ug/L 09/02/16 15:25 107-05-110.0 1.5 1
Benzene ND ug/L 09/02/16 15:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/02/16 15:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/02/16 15:25 75-27-41.0 0.18 1
Bromoform ND ug/L 09/02/16 15:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/02/16 15:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/02/16 15:25 78-93-31000.96 1
Carbon disulfide ND ug/L 09/02/16 15:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/02/16 15:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/02/16 15:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/02/16 15:25 75-00-310.0 0.54 1
Chloroform ND ug/L 09/02/16 15:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/02/16 15:25 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/02/16 15:25 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/02/16 15:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/02/16 15:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/02/16 15:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/02/16 15:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/02/16 15:25 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/02/16 15:25 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/02/16 15:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/02/16 15:25 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 09/02/16 15:25 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/02/16 15:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/02/16 15:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/02/16 15:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/02/16 15:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/02/16 15:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/02/16 15:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/02/16 15:25 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/02/16 15:25 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/02/16 15:25 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/02/16 15:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/02/16 15:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/02/16 15:25 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/02/16 15:25 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/02/16 15:25 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/02/16 15:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/02/16 15:25 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/02/16 15:25 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/02/16 15:25 126-98-71000.93 1
Methylene Chloride ND ug/L 09/02/16 15:25 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-16R Lab ID:92310738006 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/02/16 15:25 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/02/16 15:25 108-10-11000.33 1
Naphthalene ND ug/L 09/02/16 15:25 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/02/16 15:25 107-12-01503.6 1
Styrene ND ug/L 09/02/16 15:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/02/16 15:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/02/16 15:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/02/16 15:25 127-18-41.0 0.46 1
Toluene ND ug/L 09/02/16 15:25 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/02/16 15:25 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/02/16 15:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/02/16 15:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/02/16 15:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/02/16 15:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/02/16 15:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/02/16 15:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/02/16 15:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/02/16 15:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/02/16 15:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/02/16 15:25 17060-07-070-130 1
Toluene-d8 (S)100 %09/02/16 15:25 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 21:16 18496-25-810001001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4470 ug/L 09/08/16 17:27 16887-00-610005001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 6.7J ug/L 09/13/16 00:02 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:LE-1 Lab ID:92310738007 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 9.2 ug/L 09/02/16 19:24 7440-36-009/01/16 19:306.0 3.8 1
Arsenic 13.3 ug/L 09/02/16 19:24 7440-38-2 B09/01/16 19:3010.0 2.5 1
Barium 76.1J ug/L 09/02/16 19:24 7440-39-309/01/16 19:301002.5 1
Beryllium ND ug/L 09/02/16 19:24 7440-41-709/01/16 19:301.0 0.50 1
Cadmium ND ug/L 09/02/16 19:24 7440-43-909/01/16 19:301.0 0.50 1
Chromium 37.8 ug/L 09/02/16 19:24 7440-47-309/01/16 19:3010.0 2.5 1
Cobalt ND ug/L 09/02/16 19:24 7440-48-409/01/16 19:3010.0 2.5 1
Copper ND ug/L 09/02/16 19:24 7440-50-809/01/16 19:3010.0 2.5 1
Lead 2.8J ug/L 09/02/16 19:24 7439-92-109/01/16 19:3010.0 2.5 1
Nickel 44.0J ug/L 09/02/16 19:24 7440-02-009/01/16 19:3050.0 2.5 1
Selenium ND ug/L 09/02/16 19:24 7782-49-209/01/16 19:3010.0 5.0 1
Silver ND ug/L 09/02/16 19:24 7440-22-409/01/16 19:3010.0 2.5 1
Thallium ND ug/L 09/03/16 14:45 7440-28-009/01/16 19:305.5 5.0 1
Tin ND ug/L 09/02/16 19:24 7440-31-509/01/16 19:301002.5 1
Vanadium 15.4J ug/L 09/02/16 19:24 7440-62-209/01/16 19:3025.0 2.5 1
Zinc 1120 ug/L 09/02/16 19:24 7440-66-609/01/16 19:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/01/16 09:27 7439-97-609/01/16 04:050.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 604 ug/L 09/08/16 00:36 67-64-1 L150050.0 5
Acetonitrile ND ug/L 09/08/16 00:36 75-05-827511.0 5
Acrolein ND ug/L 09/08/16 00:36 107-02-82658.0 5
Acrylonitrile ND ug/L 09/08/16 00:36 107-13-110009.4 5
Allyl chloride ND ug/L 09/08/16 00:36 107-05-150.0 7.7 5
Benzene 1.6J ug/L 09/08/16 00:36 71-43-25.0 1.2 5
Bromochloromethane ND ug/L 09/08/16 00:36 74-97-515.0 0.85 5
Bromodichloromethane ND ug/L 09/08/16 00:36 75-27-45.0 0.90 5
Bromoform ND ug/L 09/08/16 00:36 75-25-215.0 1.3 5
Bromomethane ND ug/L 09/08/16 00:36 74-83-950.0 1.4 5
2-Butanone (MEK)1050 ug/L 09/08/16 00:36 78-93-35004.8 5
Carbon disulfide ND ug/L 09/08/16 00:36 75-15-05005.8 5
Carbon tetrachloride ND ug/L 09/08/16 00:36 56-23-55.0 1.2 5
Chlorobenzene ND ug/L 09/08/16 00:36 108-90-715.0 1.2 5
Chloroethane ND ug/L 09/08/16 00:36 75-00-350.0 2.7 5
Chloroform ND ug/L 09/08/16 00:36 67-66-325.0 0.70 5
Chloromethane ND ug/L 09/08/16 00:36 74-87-35.0 0.55 5
Chloroprene ND ug/L 09/08/16 00:36 126-99-81001.4 5
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 00:36 96-12-865.0 10.0 5
Dibromochloromethane ND ug/L 09/08/16 00:36 124-48-115.0 1.0 5
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 00:36 106-93-45.0 1.4 5
Dibromomethane ND ug/L 09/08/16 00:36 74-95-350.0 1.0 5
1,2-Dichlorobenzene ND ug/L 09/08/16 00:36 95-50-125.0 1.5 5
1,3-Dichlorobenzene ND ug/L 09/08/16 00:36 541-73-125.0 1.2 5
1,4-Dichlorobenzene ND ug/L 09/08/16 00:36 106-46-75.0 1.6 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:LE-1 Lab ID:92310738007 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 00:36 110-57-6 L35005.0 5
Dichlorodifluoromethane ND ug/L 09/08/16 00:36 75-71-825.0 1.0 5
1,1-Dichloroethane ND ug/L 09/08/16 00:36 75-34-325.0 1.6 5
1,2-Dichloroethane ND ug/L 09/08/16 00:36 107-06-25.0 1.2 5
1,1-Dichloroethene ND ug/L 09/08/16 00:36 75-35-425.0 2.8 5
cis-1,2-Dichloroethene ND ug/L 09/08/16 00:36 156-59-225.0 0.95 5
trans-1,2-Dichloroethene ND ug/L 09/08/16 00:36 156-60-525.0 2.4 5
1,2-Dichloropropane ND ug/L 09/08/16 00:36 78-87-55.0 1.4 5
1,3-Dichloropropane ND ug/L 09/08/16 00:36 142-28-95.0 1.4 5
2,2-Dichloropropane ND ug/L 09/08/16 00:36 594-20-775.0 0.65 5
1,1-Dichloropropene ND ug/L 09/08/16 00:36 563-58-625.0 2.4 5
cis-1,3-Dichloropropene ND ug/L 09/08/16 00:36 10061-01-55.0 0.65 5
trans-1,3-Dichloropropene ND ug/L 09/08/16 00:36 10061-02-65.0 1.3 5
Ethylbenzene ND ug/L 09/08/16 00:36 100-41-45.0 1.5 5
Ethyl methacrylate ND ug/L 09/08/16 00:36 97-63-250.0 1.0 5
Hexachloro-1,3-butadiene ND ug/L 09/08/16 00:36 87-68-350.0 3.6 5
2-Hexanone 3.4J ug/L 09/08/16 00:36 591-78-62502.3 5
Iodomethane ND ug/L 09/08/16 00:36 74-88-450.0 1.6 5
Isobutanol ND ug/L 09/08/16 00:36 78-83-15001755
Methacrylonitrile ND ug/L 09/08/16 00:36 126-98-75004.6 5
Methylene Chloride 8.9 ug/L 09/08/16 00:36 75-09-2 C95.0 4.8 5
Methyl methacrylate ND ug/L 09/08/16 00:36 80-62-61509.8 5
4-Methyl-2-pentanone (MIBK)17.0J ug/L 09/08/16 00:36 108-10-15001.6 5
Naphthalene ND ug/L 09/08/16 00:36 91-20-350.0 1.2 5
Propionitrile ND ug/L 09/08/16 00:36 107-12-075018.2 5
Styrene ND ug/L 09/08/16 00:36 100-42-55.0 1.3 5
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 00:36 630-20-625.0 1.6 5
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 00:36 79-34-515.0 2.0 5
Tetrachloroethene ND ug/L 09/08/16 00:36 127-18-45.0 2.3 5
Toluene 57.3 ug/L 09/08/16 00:36 108-88-35.0 1.3 5
1,2,4-Trichlorobenzene ND ug/L 09/08/16 00:36 120-82-150.0 1.8 5
1,1,1-Trichloroethane ND ug/L 09/08/16 00:36 71-55-65.0 2.4 5
1,1,2-Trichloroethane ND ug/L 09/08/16 00:36 79-00-55.0 1.4 5
Trichloroethene ND ug/L 09/08/16 00:36 79-01-65.0 2.4 5
Trichlorofluoromethane ND ug/L 09/08/16 00:36 75-69-45.0 1.0 5
1,2,3-Trichloropropane ND ug/L 09/08/16 00:36 96-18-45.0 2.0 5
Vinyl acetate ND ug/L 09/08/16 00:36 108-05-42501.8 5
Vinyl chloride ND ug/L 09/08/16 00:36 75-01-45.0 3.1 5
Xylene (Total)ND ug/L 09/08/16 00:36 1330-20-725.0 3.3 5
Surrogates
4-Bromofluorobenzene (S)96 %09/08/16 00:36 460-00-470-130 5
1,2-Dichloroethane-d4 (S)103 %09/08/16 00:36 17060-07-070-130 5
Toluene-d8 (S)100 %09/08/16 00:36 2037-26-570-130 5
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 392000 ug/L 09/06/16 09:0909/01/16 05:00200020001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 46 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:LE-1 Lab ID:92310738007 Collected:08/30/16 15:10 Received:08/31/16 08:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 90409040 pH
pH 7.9 Std. Units 09/06/16 10:39 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 41800J ug/L 09/02/16 18:57 14808-79-8125000050005
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 09/01/16 01:161000010.0 1
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 1020 ug/L 09/09/16 05:52 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 1390000 ug/L 09/14/16 16:5725000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 16:32 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 16:32 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 16:32 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 16:32 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 16:32 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 16:32 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 16:32 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 16:32 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 16:32 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 16:32 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 16:32 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 16:32 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 16:32 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 16:32 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 16:32 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 16:32 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 16:32 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 16:32 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 16:32 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)24 %09/07/16 16:32 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)32 %09/07/16 16:32 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 18:50 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 18:50 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 18:50 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 18:50 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 18:50 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 18:50 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 18:50 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)35 %09/07/16 18:50 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 07:57 25057-89-009/06/16 09:200.095 0.047 1
2,4-D ND ug/L 09/08/16 07:57 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 07:57 75-99-0 L309/06/16 09:200.92 0.43 1
2,4-DB ND ug/L 09/08/16 07:57 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 07:57 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 07:57 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 07:57 88-85-709/06/16 09:200.19 0.057 1
Pentachlorophenol ND ug/L 09/08/16 07:57 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 07:57 1918-02-109/06/16 09:200.095 0.019 1
2,4,5-T ND ug/L 09/08/16 07:57 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 07:57 93-72-109/06/16 09:200.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)81 %09/08/16 07:57 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:47 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:47 7440-38-209/06/16 21:0010.0 2.5 1
Barium 38.8J ug/L 09/07/16 23:47 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:47 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:47 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:47 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:47 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:47 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:47 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:47 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:47 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:47 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:47 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:47 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:47 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:47 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Antimony, Dissolved ND ug/L 09/20/16 14:57 7440-36-009/07/16 02:115.0 3.8 1
Arsenic, Dissolved ND ug/L 09/20/16 14:57 7440-38-209/07/16 02:1110.0 5.0 1
Barium, Dissolved 33.5 ug/L 09/20/16 14:57 7440-39-309/07/16 02:115.0 2.5 1
Beryllium, Dissolved 0.18J ug/L 09/20/16 14:57 7440-41-709/07/16 02:111.0 0.050 1
Cadmium, Dissolved ND ug/L 09/20/16 14:57 7440-43-909/07/16 02:111.0 0.50 1
Chromium, Dissolved ND ug/L 09/20/16 14:57 7440-47-309/07/16 02:115.0 2.5 1
Cobalt, Dissolved ND ug/L 09/20/16 14:57 7440-48-409/07/16 02:115.0 2.5 1
Copper, Dissolved ND ug/L 09/20/16 14:57 7440-50-809/07/16 02:115.0 2.5 1
Lead, Dissolved ND ug/L 09/20/16 14:57 7439-92-109/07/16 02:115.0 2.5 1
Nickel, Dissolved ND ug/L 09/20/16 14:57 7440-02-009/07/16 02:115.0 2.5 1
Selenium, Dissolved ND ug/L 09/20/16 14:57 7782-49-209/07/16 02:1110.0 5.0 1
Silver, Dissolved ND ug/L 09/20/16 14:57 7440-22-409/07/16 02:115.0 2.5 1
Thallium, Dissolved ND ug/L 09/20/16 14:57 7440-28-009/07/16 02:1110.0 5.0 1
Tin, Dissolved ND ug/L 09/20/16 14:57 7440-31-509/07/16 02:115.0 2.5 1
Vanadium, Dissolved ND ug/L 09/20/16 14:57 7440-62-209/07/16 02:115.0 2.5 1
Zinc, Dissolved 2.7J ug/L 09/20/16 14:57 7440-66-609/07/16 02:1110.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 1.2 ug/L 09/08/16 13:09 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved 1.6 ug/L 09/20/16 01:28 7439-97-609/18/16 21:350.20 0.090 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 19:53 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/15/16 19:53 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/15/16 19:53 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/15/16 19:53 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/15/16 19:53 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/15/16 19:53 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/15/16 19:53 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/15/16 19:53 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/15/16 19:53 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 19:53 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/15/16 19:53 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/15/16 19:53 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 19:53 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/15/16 19:53 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 19:53 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/15/16 19:53 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/15/16 19:53 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 19:53 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 19:53 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/15/16 19:53 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/15/16 19:53 95-57-809/06/16 13:4010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 09/15/16 19:53 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/15/16 19:53 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/15/16 19:53 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 19:53 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/15/16 19:53 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 19:53 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/15/16 19:53 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/15/16 19:53 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/15/16 19:53 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/15/16 19:53 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/15/16 19:53 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/15/16 19:53 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/15/16 19:53 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/15/16 19:53 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/15/16 19:53 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/15/16 19:53 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 19:53 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/15/16 19:53 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/15/16 19:53 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/15/16 19:53 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/15/16 19:53 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/15/16 19:53 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/15/16 19:53 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/15/16 19:53 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 19:53 117-81-709/06/16 13:4015.0 0.85 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Ethyl methanesulfonate ND ug/L 09/15/16 19:53 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/15/16 19:53 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/15/16 19:53 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/15/16 19:53 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/15/16 19:53 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 19:53 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/15/16 19:53 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/15/16 19:53 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 19:53 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/15/16 19:53 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/15/16 19:53 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/15/16 19:53 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/15/16 19:53 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/15/16 19:53 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/15/16 19:53 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/15/16 19:53 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/15/16 19:53 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/15/16 19:53 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 19:53 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 19:5309/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/15/16 19:53 134-32-709/06/16 13:4010.0 0.96 1
2-Naphthalenamine ND ug/L 09/15/16 19:53 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/15/16 19:53 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/15/16 19:53 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/15/16 19:53 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/15/16 19:53 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/15/16 19:53 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/15/16 19:53 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/15/16 19:53 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/15/16 19:53 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/15/16 19:53 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/15/16 19:53 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/15/16 19:53 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 19:53 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 19:53 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/15/16 19:53 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/15/16 19:53 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/15/16 19:53 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/15/16 19:53 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 19:53 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/15/16 19:53 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/15/16 19:53 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/15/16 19:53 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/15/16 19:53 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/15/16 19:53 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/15/16 19:53 85-01-809/06/16 13:4010.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 51 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenol ND ug/L 09/15/16 19:5309/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/15/16 19:53 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/15/16 19:53 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/15/16 19:53 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/15/16 19:53 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/15/16 19:53 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/15/16 19:53 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 19:53 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/15/16 19:53 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/15/16 19:53 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 19:53 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 19:53 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/15/16 19:53 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)63 %09/15/16 19:53 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)66 %09/15/16 19:53 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)69 %09/15/16 19:53 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)25 %09/15/16 19:53 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)34 %09/15/16 19:53 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)73 %09/15/16 19:53 118-79-609/06/16 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 01:10 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 01:10 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 01:10 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 01:10 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 01:10 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 01:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 01:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 01:10 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 01:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 01:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 01:10 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 01:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 01:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 01:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 01:10 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 01:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 01:10 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 01:10 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 01:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 01:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 01:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 01:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 01:10 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 01:10 541-73-15.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 09/08/16 01:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 01:10 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 01:10 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 01:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 01:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 01:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 01:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 01:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 01:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 01:10 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 01:10 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 01:10 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 01:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 01:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 01:10 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 01:10 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 01:10 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 01:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 01:10 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 01:10 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 01:10 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 01:10 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 01:10 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 01:10 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 01:10 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 01:10 107-12-01503.6 1
Styrene ND ug/L 09/08/16 01:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 01:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 01:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 01:10 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 01:10 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 01:10 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 01:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 01:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 01:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 01:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 01:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 01:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 01:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 01:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %09/08/16 01:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 01:10 17060-07-070-130 1
Toluene-d8 (S)100 %09/08/16 01:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-4 Lab ID:92310738009 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:13 57-12-5 R110.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-8 Lab ID:92310738010 Collected:08/31/16 11:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 16:50 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 16:50 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 16:50 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 16:50 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 16:50 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 16:50 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 16:50 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 16:50 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 16:50 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 16:50 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 16:50 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 16:50 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 16:50 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 16:50 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 16:50 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 16:50 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 16:50 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 16:50 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 16:50 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)77 %09/07/16 16:50 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)61 %09/07/16 16:50 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 19:10 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 19:10 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 19:10 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 19:10 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 19:10 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 19:10 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 19:10 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)61 %09/07/16 19:10 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 08:27 25057-89-009/06/16 09:200.095 0.048 1
2,4-D ND ug/L 09/08/16 08:27 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 08:27 75-99-0 L3,M009/06/16 09:200.92 0.43 1
2,4-DB ND ug/L 09/08/16 08:27 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 08:27 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 08:27 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 08:27 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 08:27 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 08:27 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 08:27 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 08:27 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-8 Lab ID:92310738010 Collected:08/31/16 11:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)76 %09/08/16 08:27 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:50 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:50 7440-38-209/06/16 21:0010.0 2.5 1
Barium 14.9J ug/L 09/07/16 23:50 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:50 7440-41-709/06/16 21:001.0 0.50 1
Cadmium 3.5 ug/L 09/07/16 23:50 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:50 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:50 7440-48-409/06/16 21:0010.0 2.5 1
Copper 4.2J ug/L 09/07/16 23:50 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:50 7439-92-109/06/16 21:0010.0 2.5 1
Nickel 4.1J ug/L 09/07/16 23:50 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:50 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:50 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:50 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:50 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:50 7440-62-209/06/16 21:0025.0 2.5 1
Zinc 6.7J ug/L 09/07/16 23:50 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:11 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/15/16 20:21 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/15/16 20:21 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/15/16 20:21 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/15/16 20:21 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/15/16 20:21 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/15/16 20:21 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/15/16 20:21 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/15/16 20:21 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/15/16 20:21 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/15/16 20:21 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/15/16 20:21 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/15/16 20:21 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/15/16 20:21 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/15/16 20:21 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/15/16 20:21 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/15/16 20:21 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/15/16 20:21 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/15/16 20:21 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/15/16 20:21 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/15/16 20:21 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/15/16 20:21 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-8 Lab ID:92310738010 Collected:08/31/16 11:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/15/16 20:21 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/15/16 20:21 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/15/16 20:21 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/15/16 20:21 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/15/16 20:21 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/15/16 20:21 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/15/16 20:21 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/15/16 20:21 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/15/16 20:21 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/15/16 20:21 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/15/16 20:21 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/15/16 20:21 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/15/16 20:21 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/15/16 20:21 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/15/16 20:21 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/15/16 20:21 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/15/16 20:21 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/15/16 20:21 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/15/16 20:21 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/15/16 20:21 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/15/16 20:21 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/15/16 20:21 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/15/16 20:21 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/15/16 20:21 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/15/16 20:21 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/15/16 20:21 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/15/16 20:21 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/15/16 20:21 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/15/16 20:21 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/15/16 20:21 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/15/16 20:21 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/15/16 20:21 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/15/16 20:21 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/15/16 20:21 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/15/16 20:21 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/15/16 20:21 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/15/16 20:21 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/15/16 20:21 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/15/16 20:21 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/15/16 20:21 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/15/16 20:21 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/15/16 20:21 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/15/16 20:21 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/15/16 20:21 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/15/16 20:2109/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/15/16 20:21 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 57 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-8 Lab ID:92310738010 Collected:08/31/16 11:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/15/16 20:21 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/15/16 20:21 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/15/16 20:21 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/15/16 20:21 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/15/16 20:21 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/15/16 20:21 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/15/16 20:21 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/15/16 20:21 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/15/16 20:21 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/15/16 20:21 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/15/16 20:21 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/15/16 20:21 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/15/16 20:21 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/15/16 20:21 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/15/16 20:21 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/15/16 20:21 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/15/16 20:21 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/15/16 20:21 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/15/16 20:21 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/15/16 20:21 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/15/16 20:21 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/15/16 20:21 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/15/16 20:21 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/15/16 20:21 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/15/16 20:21 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/15/16 20:2109/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/15/16 20:21 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/15/16 20:21 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/15/16 20:21 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/15/16 20:21 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/15/16 20:21 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/15/16 20:21 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/15/16 20:21 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/15/16 20:21 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/15/16 20:21 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/15/16 20:21 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/15/16 20:21 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/15/16 20:21 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)81 %09/15/16 20:21 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)82 %09/15/16 20:21 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)102 %09/15/16 20:21 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)31 %09/15/16 20:21 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)45 %09/15/16 20:21 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)89 %09/15/16 20:21 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-8 Lab ID:92310738010 Collected:08/31/16 11:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 01:27 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 01:27 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 01:27 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 01:27 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 01:27 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 01:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 01:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 01:27 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 01:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 01:27 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 01:27 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 01:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 01:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 01:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 01:27 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 01:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 01:27 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 01:27 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 01:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 01:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 01:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 01:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 01:27 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 01:27 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 01:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 01:27 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 01:27 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 01:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 01:27 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 01:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 01:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 01:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 01:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 01:27 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 01:27 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 01:27 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 01:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 01:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 01:27 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 01:27 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 01:27 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 01:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 01:27 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 01:27 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 01:27 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 01:27 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-8 Lab ID:92310738010 Collected:08/31/16 11:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 01:27 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 01:27 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 01:27 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 01:27 107-12-01503.6 1
Styrene ND ug/L 09/08/16 01:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 01:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 01:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 01:27 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 01:27 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 01:27 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 01:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 01:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 01:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 01:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 01:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 01:27 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 01:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 01:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 01:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/08/16 01:27 17060-07-070-130 1
Toluene-d8 (S)102 %09/08/16 01:27 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:15 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 17:25 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 17:25 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 17:25 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 17:25 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 17:25 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 17:25 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 17:25 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 17:25 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 17:25 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 17:25 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 17:25 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 17:25 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 17:25 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 17:25 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 17:25 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 17:25 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 17:25 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 17:25 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 17:25 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)75 %09/07/16 17:25 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)61 %09/07/16 17:25 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 19:30 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 19:30 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 19:30 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 19:30 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 19:30 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 19:30 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 19:30 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)63 %09/07/16 19:30 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 09:57 25057-89-009/06/16 09:200.096 0.048 1
2,4-D ND ug/L 09/08/16 09:57 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 09:57 75-99-0 L309/06/16 09:200.92 0.44 1
2,4-DB ND ug/L 09/08/16 09:57 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 09:57 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 09:57 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 09:57 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 09:57 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 09:57 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 09:57 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 09:57 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 61 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)89 %09/08/16 09:57 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:53 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:53 7440-38-209/06/16 21:0010.0 2.5 1
Barium 76.7J ug/L 09/07/16 23:53 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:53 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:53 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:53 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:53 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:53 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:53 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:53 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:53 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:53 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:53 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:53 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:53 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:53 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Antimony, Dissolved ND ug/L 10/12/16 15:30 7440-36-009/07/16 02:115.0 3.8 1
Arsenic, Dissolved ND ug/L 10/12/16 15:30 7440-38-209/07/16 02:1110.0 5.0 1
Barium, Dissolved 72.5 ug/L 10/12/16 15:30 7440-39-309/07/16 02:115.0 2.5 1
Beryllium, Dissolved 0.14J ug/L 10/12/16 15:30 7440-41-709/07/16 02:111.0 0.050 1
Cadmium, Dissolved 1.3 ug/L 10/12/16 15:30 7440-43-909/07/16 02:111.0 0.50 1
Chromium, Dissolved ND ug/L 10/12/16 15:30 7440-47-309/07/16 02:115.0 2.5 1
Cobalt, Dissolved ND ug/L 10/12/16 15:30 7440-48-409/07/16 02:115.0 2.5 1
Copper, Dissolved ND ug/L 10/12/16 15:30 7440-50-809/07/16 02:115.0 2.5 1
Lead, Dissolved 3.2J ug/L 10/12/16 15:30 7439-92-109/07/16 02:115.0 2.5 1
Nickel, Dissolved ND ug/L 10/12/16 15:30 7440-02-009/07/16 02:115.0 2.5 1
Selenium, Dissolved ND ug/L 10/12/16 15:30 7782-49-209/07/16 02:1110.0 5.0 1
Silver, Dissolved ND ug/L 10/12/16 15:30 7440-22-409/07/16 02:115.0 2.5 1
Thallium, Dissolved ND ug/L 10/12/16 15:30 7440-28-009/07/16 02:1110.0 5.0 1
Tin, Dissolved ND ug/L 10/12/16 15:30 7440-31-509/07/16 02:115.0 2.5 1
Vanadium, Dissolved ND ug/L 10/12/16 15:30 7440-62-209/07/16 02:115.0 2.5 1
Zinc, Dissolved ND ug/L 10/12/16 15:30 7440-66-609/07/16 02:1110.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.17J ug/L 09/08/16 13:14 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved 0.23 ug/L 09/28/16 11:54 7439-97-609/28/16 04:200.20 0.090 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/16/16 15:57 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/16/16 15:57 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/16/16 15:57 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/16/16 15:57 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/16/16 15:57 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/16/16 15:57 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/16/16 15:57 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/16/16 15:57 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/16/16 15:57 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/16/16 15:57 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/16/16 15:57 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/16/16 15:57 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/16/16 15:57 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/16/16 15:57 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/16/16 15:57 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/16/16 15:57 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/16/16 15:57 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/16/16 15:57 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/16/16 15:57 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/16/16 15:57 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/16/16 15:57 95-57-809/06/16 13:4010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 09/16/16 15:57 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/16/16 15:57 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/16/16 15:57 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/16/16 15:57 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/16/16 15:57 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/16/16 15:57 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/16/16 15:57 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/16/16 15:57 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/16/16 15:57 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/16/16 15:57 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/16/16 15:57 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/16/16 15:57 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/16/16 15:57 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/16/16 15:57 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/16/16 15:57 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/16/16 15:57 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/16/16 15:57 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/16/16 15:57 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/16/16 15:57 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/16/16 15:57 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/16/16 15:57 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/16/16 15:57 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/16/16 15:57 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/16/16 15:57 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/16/16 15:57 117-81-709/06/16 13:4015.0 0.85 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Ethyl methanesulfonate ND ug/L 09/16/16 15:57 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/16/16 15:57 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/16/16 15:57 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/16/16 15:57 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/16/16 15:57 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/16/16 15:57 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/16/16 15:57 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/16/16 15:57 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/16/16 15:57 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/16/16 15:57 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/16/16 15:57 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/16/16 15:57 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/16/16 15:57 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/16/16 15:57 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/16/16 15:57 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/16/16 15:57 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/16/16 15:57 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/16/16 15:57 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/16/16 15:57 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/16/16 15:5709/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/16/16 15:57 134-32-709/06/16 13:4010.0 0.96 1
2-Naphthalenamine ND ug/L 09/16/16 15:57 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/16/16 15:57 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/16/16 15:57 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/16/16 15:57 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/16/16 15:57 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/16/16 15:57 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/16/16 15:57 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/16/16 15:57 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/16/16 15:57 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/16/16 15:57 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/16/16 15:57 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/16/16 15:57 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/16/16 15:57 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/16/16 15:57 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/16/16 15:57 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/16/16 15:57 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/16/16 15:57 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/16/16 15:57 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/16/16 15:57 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/16/16 15:57 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/16/16 15:57 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/16/16 15:57 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/16/16 15:57 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/16/16 15:57 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/16/16 15:57 85-01-809/06/16 13:4010.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenol ND ug/L 09/16/16 15:5709/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/16/16 15:57 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/16/16 15:57 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/16/16 15:57 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/16/16 15:57 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/16/16 15:57 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/16/16 15:57 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/16/16 15:57 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/16/16 15:57 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/16/16 15:57 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/16/16 15:57 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/16/16 15:57 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/16/16 15:57 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)77 %09/16/16 15:57 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)81 %09/16/16 15:57 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)90 %09/16/16 15:57 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)32 %09/16/16 15:57 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)43 %09/16/16 15:57 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)82 %09/16/16 15:57 118-79-609/06/16 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 01:44 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 01:44 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 01:44 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 01:44 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 01:44 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 01:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 01:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 01:44 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 01:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 01:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 01:44 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 01:44 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 01:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 01:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 01:44 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 01:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 01:44 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 01:44 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 01:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 01:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 01:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 01:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 01:44 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 01:44 541-73-15.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 09/08/16 01:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 01:44 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 01:44 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 01:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 01:44 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 01:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 01:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 01:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 01:44 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 01:44 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 01:44 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 01:44 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 01:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 01:44 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 01:44 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 01:44 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 01:44 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 01:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 01:44 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 01:44 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 01:44 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 01:44 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 01:44 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 01:44 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 01:44 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 01:44 107-12-01503.6 1
Styrene ND ug/L 09/08/16 01:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 01:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 01:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 01:44 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 01:44 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 01:44 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 01:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 01:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 01:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 01:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 01:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 01:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 01:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 01:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %09/08/16 01:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 01:44 17060-07-070-130 1
Toluene-d8 (S)103 %09/08/16 01:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 66 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-9 Lab ID:92310738011 Collected:08/31/16 13:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:16 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 67 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 18:00 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 18:00 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 18:00 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 18:00 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 18:00 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 18:00 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 18:00 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 18:00 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 18:00 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 18:00 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 18:00 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 18:00 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 18:00 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 18:00 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 18:00 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 18:00 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 18:00 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 18:00 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 18:00 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)66 %09/07/16 18:00 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)33 %09/07/16 18:00 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 19:50 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 19:50 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 19:50 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 19:50 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 19:50 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 19:50 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 19:50 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)34 %09/07/16 19:50 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 10:58 25057-89-009/06/16 09:200.095 0.047 1
2,4-D ND ug/L 09/08/16 10:58 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 10:58 75-99-0 L309/06/16 09:200.92 0.43 1
2,4-DB ND ug/L 09/08/16 10:58 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 10:58 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 10:58 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 10:58 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 10:58 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 10:58 1918-02-109/06/16 09:200.095 0.019 1
2,4,5-T ND ug/L 09/08/16 10:58 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 10:58 93-72-109/06/16 09:200.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)80 %09/08/16 10:58 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:57 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 2.8J ug/L 09/07/16 23:57 7440-38-209/06/16 21:0010.0 2.5 1
Barium 42.4J ug/L 09/07/16 23:57 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:57 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:57 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:57 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:57 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:57 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:57 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:57 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:57 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:57 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:57 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:57 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:57 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:57 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Antimony, Dissolved ND ug/L 09/20/16 15:06 7440-36-009/07/16 02:115.0 3.8 1
Arsenic, Dissolved ND ug/L 09/20/16 15:06 7440-38-209/07/16 02:1110.0 5.0 1
Barium, Dissolved 21.7 ug/L 09/20/16 15:06 7440-39-309/07/16 02:115.0 2.5 1
Beryllium, Dissolved ND ug/L 09/20/16 15:06 7440-41-709/07/16 02:111.0 0.050 1
Cadmium, Dissolved ND ug/L 09/20/16 15:06 7440-43-909/07/16 02:111.0 0.50 1
Chromium, Dissolved ND ug/L 09/20/16 15:06 7440-47-309/07/16 02:115.0 2.5 1
Cobalt, Dissolved ND ug/L 09/20/16 15:06 7440-48-409/07/16 02:115.0 2.5 1
Copper, Dissolved ND ug/L 09/20/16 15:06 7440-50-809/07/16 02:115.0 2.5 1
Lead, Dissolved ND ug/L 09/20/16 15:06 7439-92-109/07/16 02:115.0 2.5 1
Nickel, Dissolved ND ug/L 09/20/16 15:06 7440-02-009/07/16 02:115.0 2.5 1
Selenium, Dissolved ND ug/L 09/20/16 15:06 7782-49-209/07/16 02:1110.0 5.0 1
Silver, Dissolved ND ug/L 09/20/16 15:06 7440-22-409/07/16 02:115.0 2.5 1
Thallium, Dissolved ND ug/L 09/20/16 15:06 7440-28-009/07/16 02:1110.0 5.0 1
Tin, Dissolved ND ug/L 09/20/16 15:06 7440-31-509/07/16 02:115.0 2.5 1
Vanadium, Dissolved ND ug/L 09/20/16 15:06 7440-62-209/07/16 02:115.0 2.5 1
Zinc, Dissolved 3.1J ug/L 09/20/16 15:06 7440-66-609/07/16 02:1110.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:16 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved ND ug/L 09/20/16 01:30 7439-97-609/18/16 21:350.20 0.090 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/16/16 16:25 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/16/16 16:25 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/16/16 16:25 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/16/16 16:25 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/16/16 16:25 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/16/16 16:25 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/16/16 16:25 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/16/16 16:25 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/16/16 16:25 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/16/16 16:25 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/16/16 16:25 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/16/16 16:25 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/16/16 16:25 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/16/16 16:25 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/16/16 16:25 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/16/16 16:25 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/16/16 16:25 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/16/16 16:25 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/16/16 16:25 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/16/16 16:25 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/16/16 16:25 95-57-809/06/16 13:4010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 09/16/16 16:25 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/16/16 16:25 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/16/16 16:25 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/16/16 16:25 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/16/16 16:25 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/16/16 16:25 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/16/16 16:25 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/16/16 16:25 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/16/16 16:25 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/16/16 16:25 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/16/16 16:25 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/16/16 16:25 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/16/16 16:25 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/16/16 16:25 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/16/16 16:25 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/16/16 16:25 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/16/16 16:25 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/16/16 16:25 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/16/16 16:25 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/16/16 16:25 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/16/16 16:25 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/16/16 16:25 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/16/16 16:25 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/16/16 16:25 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/16/16 16:25 117-81-709/06/16 13:4015.0 0.85 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Ethyl methanesulfonate ND ug/L 09/16/16 16:25 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/16/16 16:25 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/16/16 16:25 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/16/16 16:25 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/16/16 16:25 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/16/16 16:25 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/16/16 16:25 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/16/16 16:25 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/16/16 16:25 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/16/16 16:25 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/16/16 16:25 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/16/16 16:25 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/16/16 16:25 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/16/16 16:25 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/16/16 16:25 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/16/16 16:25 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/16/16 16:25 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/16/16 16:25 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/16/16 16:25 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/16/16 16:2509/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/16/16 16:25 134-32-709/06/16 13:4010.0 0.96 1
2-Naphthalenamine ND ug/L 09/16/16 16:25 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/16/16 16:25 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/16/16 16:25 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/16/16 16:25 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/16/16 16:25 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/16/16 16:25 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/16/16 16:25 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/16/16 16:25 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/16/16 16:25 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/16/16 16:25 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/16/16 16:25 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/16/16 16:25 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/16/16 16:25 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/16/16 16:25 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/16/16 16:25 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/16/16 16:25 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/16/16 16:25 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/16/16 16:25 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/16/16 16:25 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/16/16 16:25 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/16/16 16:25 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/16/16 16:25 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/16/16 16:25 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/16/16 16:25 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/16/16 16:25 85-01-809/06/16 13:4010.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 71 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenol ND ug/L 09/16/16 16:2509/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/16/16 16:25 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/16/16 16:25 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/16/16 16:25 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/16/16 16:25 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/16/16 16:25 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/16/16 16:25 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/16/16 16:25 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/16/16 16:25 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/16/16 16:25 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/16/16 16:25 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/16/16 16:25 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/16/16 16:25 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)54 %09/16/16 16:25 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)59 %09/16/16 16:25 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)51 %09/16/16 16:25 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)26 %09/16/16 16:25 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)31 %09/16/16 16:25 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)56 %09/16/16 16:25 118-79-609/06/16 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 02:01 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 02:01 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 02:01 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 02:01 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 02:01 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 02:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 02:01 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 02:01 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 02:01 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 02:01 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 02:01 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 02:01 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 02:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 02:01 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 02:01 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 02:01 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 02:01 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 02:01 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 02:01 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 02:01 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 02:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 02:01 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 02:01 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 02:01 541-73-15.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 72 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 09/08/16 02:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 02:01 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 02:01 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 02:01 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 02:01 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 02:01 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 02:01 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 02:01 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 02:01 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 02:01 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 02:01 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 02:01 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 02:01 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 02:01 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 02:01 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 02:01 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 02:01 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 02:01 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 02:01 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 02:01 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 02:01 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 02:01 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 02:01 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 02:01 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 02:01 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 02:01 107-12-01503.6 1
Styrene ND ug/L 09/08/16 02:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 02:01 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 02:01 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 02:01 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 02:01 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 02:01 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 02:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 02:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 02:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 02:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 02:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 02:01 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 02:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 02:01 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %09/08/16 02:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %09/08/16 02:01 17060-07-070-130 1
Toluene-d8 (S)101 %09/08/16 02:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-10 Lab ID:92310738012 Collected:08/31/16 14:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:17 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 18:18 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 18:18 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 18:18 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 18:18 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 18:18 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 18:18 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 18:18 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 18:18 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 18:18 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 18:18 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 18:18 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 18:18 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 18:18 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 18:18 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 18:18 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 18:18 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 18:18 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 18:18 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 18:18 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)77 %09/07/16 18:18 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)65 %09/07/16 18:18 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 20:10 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 20:10 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 20:10 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 20:10 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 20:10 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 20:10 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 20:10 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)66 %09/07/16 20:10 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 11:28 25057-89-009/06/16 09:200.095 0.047 1
2,4-D ND ug/L 09/08/16 11:28 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 11:28 75-99-0 L309/06/16 09:200.92 0.43 1
2,4-DB ND ug/L 09/08/16 11:28 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 11:28 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 11:28 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 11:28 88-85-709/06/16 09:200.19 0.057 1
Pentachlorophenol ND ug/L 09/08/16 11:28 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 11:28 1918-02-109/06/16 09:200.095 0.019 1
2,4,5-T ND ug/L 09/08/16 11:28 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 11:28 93-72-109/06/16 09:200.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)90 %09/08/16 11:28 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/08/16 00:09 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 3.1J ug/L 09/08/16 00:09 7440-38-209/06/16 21:0010.0 2.5 1
Barium 24.6J ug/L 09/08/16 00:09 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/08/16 00:09 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/08/16 00:09 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/08/16 00:09 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/08/16 00:09 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/08/16 00:09 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/08/16 00:09 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/08/16 00:09 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/08/16 00:09 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/08/16 00:09 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/08/16 00:09 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/08/16 00:09 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/08/16 00:09 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/08/16 00:09 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Antimony, Dissolved ND ug/L 09/20/16 15:10 7440-36-009/07/16 02:115.0 3.8 1
Arsenic, Dissolved ND ug/L 09/20/16 15:10 7440-38-209/07/16 02:1110.0 5.0 1
Barium, Dissolved 22.7 ug/L 09/20/16 15:10 7440-39-309/07/16 02:115.0 2.5 1
Beryllium, Dissolved ND ug/L 09/20/16 15:10 7440-41-709/07/16 02:111.0 0.050 1
Cadmium, Dissolved 4.0 ug/L 09/20/16 15:10 7440-43-909/07/16 02:111.0 0.50 1
Chromium, Dissolved ND ug/L 09/20/16 15:10 7440-47-309/07/16 02:115.0 2.5 1
Cobalt, Dissolved ND ug/L 09/20/16 15:10 7440-48-409/07/16 02:115.0 2.5 1
Copper, Dissolved ND ug/L 09/20/16 15:10 7440-50-809/07/16 02:115.0 2.5 1
Lead, Dissolved ND ug/L 09/20/16 15:10 7439-92-109/07/16 02:115.0 2.5 1
Nickel, Dissolved ND ug/L 09/20/16 15:10 7440-02-009/07/16 02:115.0 2.5 1
Selenium, Dissolved ND ug/L 09/20/16 15:10 7782-49-209/07/16 02:1110.0 5.0 1
Silver, Dissolved ND ug/L 09/20/16 15:10 7440-22-409/07/16 02:115.0 2.5 1
Thallium, Dissolved ND ug/L 09/20/16 15:10 7440-28-009/07/16 02:1110.0 5.0 1
Tin, Dissolved ND ug/L 09/20/16 15:10 7440-31-509/07/16 02:115.0 2.5 1
Vanadium, Dissolved ND ug/L 09/20/16 15:10 7440-62-209/07/16 02:115.0 2.5 1
Zinc, Dissolved 5.0J ug/L 09/20/16 15:10 7440-66-609/07/16 02:1110.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10J ug/L 09/08/16 13:19 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved 0.14J ug/L 09/20/16 01:32 7439-97-609/18/16 21:350.20 0.090 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 11:48 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 11:48 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 11:48 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 11:48 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 11:48 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 11:48 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 11:48 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 11:48 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 11:48 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 11:48 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 11:48 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 11:48 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 11:48 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 11:48 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 11:48 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 11:48 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 11:48 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 11:48 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 11:48 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 11:48 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 11:48 95-57-809/06/16 13:4010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 09/19/16 11:48 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 11:48 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 11:48 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 11:48 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 11:48 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 11:48 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 11:48 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 11:48 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 11:48 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 11:48 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 11:48 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 11:48 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 11:48 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 11:48 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 11:48 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 11:48 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 11:48 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 11:48 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 11:48 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 11:48 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 11:48 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 11:48 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 11:48 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 11:48 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 11:48 117-81-709/06/16 13:4015.0 0.85 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Page 77 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Ethyl methanesulfonate ND ug/L 09/19/16 11:48 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 11:48 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 11:48 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 11:48 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 11:48 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 11:48 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 11:48 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 11:48 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 11:48 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 11:48 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 11:48 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 11:48 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 11:48 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 11:48 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 11:48 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 11:48 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 11:48 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 11:48 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 11:48 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 11:4809/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 11:48 134-32-709/06/16 13:4010.0 0.96 1
2-Naphthalenamine ND ug/L 09/19/16 11:48 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 11:48 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 11:48 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 11:48 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 11:48 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 11:48 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 11:48 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 11:48 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 11:48 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 11:48 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 11:48 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 11:48 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 11:48 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 11:48 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 11:48 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 11:48 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 11:48 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 11:48 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 11:48 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 11:48 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 11:48 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 11:48 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 11:48 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 11:48 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 11:48 85-01-809/06/16 13:4010.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenol ND ug/L 09/19/16 11:4809/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 11:48 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 11:48 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 11:48 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 11:48 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 11:48 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 11:48 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 11:48 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 11:48 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 11:48 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 11:48 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 11:48 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 11:48 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)81 %09/19/16 11:48 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)83 %09/19/16 11:48 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)102 %09/19/16 11:48 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)31 %09/19/16 11:48 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)44 %09/19/16 11:48 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)86 %09/19/16 11:48 118-79-609/06/16 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 02:19 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 02:19 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 02:19 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 02:19 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 02:19 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 02:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 02:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 02:19 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 02:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 02:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 02:19 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 02:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 02:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 02:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 02:19 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 02:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 02:19 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 02:19 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 02:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 02:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 02:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 02:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 02:19 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 02:19 541-73-15.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 09/08/16 02:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 02:19 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 02:19 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 02:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 02:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 02:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 02:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 02:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 02:19 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 02:19 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 02:19 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 02:19 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 02:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 02:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 02:19 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 02:19 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 02:19 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 02:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 02:19 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 02:19 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 02:19 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 02:19 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 02:19 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 02:19 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 02:19 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 02:19 107-12-01503.6 1
Styrene ND ug/L 09/08/16 02:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 02:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 02:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 02:19 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 02:19 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 02:19 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 02:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 02:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 02:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 02:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 02:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 02:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 02:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 02:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 02:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/08/16 02:19 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 02:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-11 Lab ID:92310738013 Collected:08/31/16 14:45 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:18 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 18:35 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 18:35 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 18:35 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 18:35 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 18:35 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 18:35 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 18:35 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 18:35 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 18:35 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 18:35 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 18:35 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 18:35 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 18:35 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 18:35 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 18:35 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 18:35 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 18:35 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 18:35 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 18:35 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)72 %09/07/16 18:35 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)60 %09/07/16 18:35 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 20:30 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 20:30 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 20:30 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 20:30 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 20:30 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 20:30 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 20:30 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)63 %09/07/16 20:30 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 11:58 25057-89-009/06/16 09:200.097 0.049 1
2,4-D ND ug/L 09/08/16 11:58 94-75-709/06/16 09:200.97 0.23 1
Dalapon ND ug/L 09/08/16 11:58 75-99-0 L309/06/16 09:200.94 0.44 1
2,4-DB ND ug/L 09/08/16 11:58 94-82-609/06/16 09:202.0 0.53 1
Dicamba ND ug/L 09/08/16 11:58 1918-00-909/06/16 09:200.097 0.031 1
Dichlorprop ND ug/L 09/08/16 11:58 120-36-509/06/16 09:200.67 0.20 1
Dinoseb ND ug/L 09/08/16 11:58 88-85-709/06/16 09:200.20 0.059 1
Pentachlorophenol ND ug/L 09/08/16 11:58 87-86-509/06/16 09:200.029 0.018 1
Picloram ND ug/L 09/08/16 11:58 1918-02-109/06/16 09:200.098 0.020 1
2,4,5-T ND ug/L 09/08/16 11:58 93-76-509/06/16 09:200.20 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 11:58 93-72-109/06/16 09:200.20 0.051 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)89 %09/08/16 11:58 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/08/16 00:12 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/08/16 00:12 7440-38-209/06/16 21:0010.0 2.5 1
Barium 34.3J ug/L 09/08/16 00:12 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/08/16 00:12 7440-41-709/06/16 21:001.0 0.50 1
Cadmium 0.72J ug/L 09/08/16 00:12 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/08/16 00:12 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt 7.8J ug/L 09/08/16 00:12 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/08/16 00:12 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/08/16 00:12 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/08/16 00:12 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/08/16 00:12 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/08/16 00:12 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/08/16 00:12 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/08/16 00:12 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/08/16 00:12 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/08/16 00:12 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Antimony, Dissolved ND ug/L 09/20/16 15:13 7440-36-009/07/16 02:115.0 3.8 1
Arsenic, Dissolved ND ug/L 09/20/16 15:13 7440-38-209/07/16 02:1110.0 5.0 1
Barium, Dissolved 41.6 ug/L 09/20/16 15:13 7440-39-309/07/16 02:115.0 2.5 1
Beryllium, Dissolved ND ug/L 09/20/16 15:13 7440-41-709/07/16 02:111.0 0.050 1
Cadmium, Dissolved ND ug/L 09/20/16 15:13 7440-43-909/07/16 02:111.0 0.50 1
Chromium, Dissolved ND ug/L 09/20/16 15:13 7440-47-309/07/16 02:115.0 2.5 1
Cobalt, Dissolved 9.8 ug/L 09/20/16 15:13 7440-48-409/07/16 02:115.0 2.5 1
Copper, Dissolved ND ug/L 09/20/16 15:13 7440-50-809/07/16 02:115.0 2.5 1
Lead, Dissolved ND ug/L 09/20/16 15:13 7439-92-109/07/16 02:115.0 2.5 1
Nickel, Dissolved ND ug/L 09/20/16 15:13 7440-02-009/07/16 02:115.0 2.5 1
Selenium, Dissolved ND ug/L 09/20/16 15:13 7782-49-209/07/16 02:1110.0 5.0 1
Silver, Dissolved ND ug/L 09/20/16 15:13 7440-22-409/07/16 02:115.0 2.5 1
Thallium, Dissolved ND ug/L 09/20/16 15:13 7440-28-009/07/16 02:1110.0 5.0 1
Tin, Dissolved ND ug/L 09/20/16 15:13 7440-31-509/07/16 02:115.0 2.5 1
Vanadium, Dissolved ND ug/L 09/20/16 15:13 7440-62-209/07/16 02:115.0 2.5 1
Zinc, Dissolved 8.3J ug/L 09/20/16 15:13 7440-66-609/07/16 02:1110.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:21 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved ND ug/L 09/20/16 01:35 7439-97-609/18/16 21:350.20 0.090 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/16/16 17:21 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/16/16 17:21 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/16/16 17:21 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/16/16 17:21 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/16/16 17:21 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/16/16 17:21 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/16/16 17:21 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/16/16 17:21 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/16/16 17:21 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/16/16 17:21 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/16/16 17:21 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/16/16 17:21 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/16/16 17:21 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/16/16 17:21 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/16/16 17:21 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/16/16 17:21 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/16/16 17:21 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/16/16 17:21 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/16/16 17:21 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/16/16 17:21 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/16/16 17:21 95-57-809/06/16 13:4010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 09/16/16 17:21 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/16/16 17:21 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/16/16 17:21 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/16/16 17:21 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/16/16 17:21 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/16/16 17:21 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/16/16 17:21 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/16/16 17:21 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/16/16 17:21 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/16/16 17:21 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/16/16 17:21 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/16/16 17:21 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/16/16 17:21 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/16/16 17:21 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/16/16 17:21 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/16/16 17:21 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/16/16 17:21 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/16/16 17:21 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/16/16 17:21 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/16/16 17:21 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/16/16 17:21 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/16/16 17:21 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/16/16 17:21 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/16/16 17:21 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/16/16 17:21 117-81-709/06/16 13:4015.0 0.85 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Ethyl methanesulfonate ND ug/L 09/16/16 17:21 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/16/16 17:21 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/16/16 17:21 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/16/16 17:21 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/16/16 17:21 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/16/16 17:21 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/16/16 17:21 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/16/16 17:21 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/16/16 17:21 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/16/16 17:21 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/16/16 17:21 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/16/16 17:21 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/16/16 17:21 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/16/16 17:21 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/16/16 17:21 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/16/16 17:21 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/16/16 17:21 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/16/16 17:21 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/16/16 17:21 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/16/16 17:2109/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/16/16 17:21 134-32-709/06/16 13:4010.0 0.96 1
2-Naphthalenamine ND ug/L 09/16/16 17:21 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/16/16 17:21 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/16/16 17:21 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/16/16 17:21 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/16/16 17:21 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/16/16 17:21 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/16/16 17:21 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/16/16 17:21 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/16/16 17:21 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/16/16 17:21 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/16/16 17:21 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/16/16 17:21 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/16/16 17:21 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/16/16 17:21 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/16/16 17:21 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/16/16 17:21 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/16/16 17:21 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/16/16 17:21 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/16/16 17:21 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/16/16 17:21 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/16/16 17:21 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/16/16 17:21 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/16/16 17:21 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/16/16 17:21 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/16/16 17:21 85-01-809/06/16 13:4010.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenol ND ug/L 09/16/16 17:2109/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/16/16 17:21 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/16/16 17:21 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/16/16 17:21 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/16/16 17:21 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/16/16 17:21 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/16/16 17:21 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/16/16 17:21 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/16/16 17:21 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/16/16 17:21 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/16/16 17:21 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/16/16 17:21 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/16/16 17:21 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)78 %09/16/16 17:21 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)80 %09/16/16 17:21 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)86 %09/16/16 17:21 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)31 %09/16/16 17:21 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)42 %09/16/16 17:21 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)84 %09/16/16 17:21 118-79-609/06/16 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 02:36 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 02:36 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 02:36 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 02:36 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 02:36 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 02:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 02:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 02:36 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 02:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 02:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 02:36 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 02:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 02:36 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 02:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 02:36 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 02:36 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 02:36 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 02:36 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 02:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 02:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 02:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 02:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 02:36 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 02:36 541-73-15.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 86 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 09/08/16 02:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 02:36 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 02:36 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 02:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 02:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 02:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 02:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 02:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 02:36 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 02:36 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 02:36 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 02:36 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 02:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 02:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 02:36 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 02:36 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 02:36 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 02:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 02:36 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 02:36 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 02:36 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 02:36 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 02:36 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 02:36 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 02:36 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 02:36 107-12-01503.6 1
Styrene ND ug/L 09/08/16 02:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 02:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 02:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 02:36 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 02:36 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 02:36 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 02:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 02:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 02:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 02:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 02:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 02:36 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 02:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 02:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %09/08/16 02:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/08/16 02:36 17060-07-070-130 1
Toluene-d8 (S)102 %09/08/16 02:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-12 Lab ID:92310738014 Collected:08/31/16 15:20 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:19 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 88 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 18:53 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 18:53 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 18:53 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 18:53 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 18:53 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 18:53 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 18:53 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 18:53 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 18:53 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 18:53 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 18:53 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 18:53 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 18:53 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 18:53 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 18:53 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 18:53 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 18:53 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 18:53 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 18:53 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %09/07/16 18:53 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)52 %09/07/16 18:53 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 20:50 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 20:50 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 20:50 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 20:50 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 20:50 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 20:50 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 20:50 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)54 %09/07/16 20:50 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 12:28 25057-89-009/06/16 09:200.096 0.048 1
2,4-D ND ug/L 09/08/16 12:28 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 12:28 75-99-0 L309/06/16 09:200.92 0.44 1
2,4-DB ND ug/L 09/08/16 12:28 94-82-609/06/16 09:201.9 0.52 1
Dicamba ND ug/L 09/08/16 12:28 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 12:28 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 12:28 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 12:28 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 12:28 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 12:28 93-76-509/06/16 09:200.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 12:28 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)81 %09/08/16 12:28 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/08/16 00:15 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/08/16 00:15 7440-38-209/06/16 21:0010.0 2.5 1
Barium 31.8J ug/L 09/08/16 00:15 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/08/16 00:15 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/08/16 00:15 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/08/16 00:15 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/08/16 00:15 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/08/16 00:15 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/08/16 00:15 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/08/16 00:15 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/08/16 00:15 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/08/16 00:15 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/08/16 00:15 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/08/16 00:15 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/08/16 00:15 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/08/16 00:15 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Antimony, Dissolved ND ug/L 10/12/16 15:34 7440-36-009/07/16 02:115.0 3.8 1
Arsenic, Dissolved ND ug/L 10/12/16 15:34 7440-38-209/07/16 02:1110.0 5.0 1
Barium, Dissolved 27.4 ug/L 10/12/16 15:34 7440-39-309/07/16 02:115.0 2.5 1
Beryllium, Dissolved ND ug/L 10/12/16 15:34 7440-41-709/07/16 02:111.0 0.050 1
Cadmium, Dissolved ND ug/L 10/12/16 15:34 7440-43-909/07/16 02:111.0 0.50 1
Chromium, Dissolved ND ug/L 10/12/16 15:34 7440-47-309/07/16 02:115.0 2.5 1
Cobalt, Dissolved ND ug/L 10/12/16 15:34 7440-48-409/07/16 02:115.0 2.5 1
Copper, Dissolved ND ug/L 10/12/16 15:34 7440-50-809/07/16 02:115.0 2.5 1
Lead, Dissolved ND ug/L 10/12/16 15:34 7439-92-109/07/16 02:115.0 2.5 1
Nickel, Dissolved ND ug/L 10/12/16 15:34 7440-02-009/07/16 02:115.0 2.5 1
Selenium, Dissolved ND ug/L 10/12/16 15:34 7782-49-209/07/16 02:1110.0 5.0 1
Silver, Dissolved ND ug/L 10/12/16 15:34 7440-22-409/07/16 02:115.0 2.5 1
Thallium, Dissolved ND ug/L 10/12/16 15:34 7440-28-009/07/16 02:1110.0 5.0 1
Tin, Dissolved 2.6J ug/L 10/12/16 15:34 7440-31-509/07/16 02:115.0 2.5 1
Vanadium, Dissolved ND ug/L 10/12/16 15:34 7440-62-209/07/16 02:115.0 2.5 1
Zinc, Dissolved ND ug/L 10/12/16 15:34 7440-66-609/07/16 02:1110.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 14:21 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved 0.23 ug/L 09/28/16 11:56 7439-97-609/28/16 04:200.20 0.090 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 16:01 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 16:01 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 16:01 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 16:01 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 16:01 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 16:01 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 16:01 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 16:01 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 16:01 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 16:01 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 16:01 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 16:01 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 16:01 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 16:01 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 16:01 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 16:01 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 16:01 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 16:01 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 16:01 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 16:01 91-58-7 M109/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 16:01 95-57-809/06/16 13:4010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 09/19/16 16:01 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 16:01 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 16:01 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 16:01 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 16:01 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 16:01 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 16:01 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 16:01 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 16:01 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 16:01 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 16:01 60-11-7 M109/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 16:01 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 16:01 119-93-7 M109/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 16:01 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 16:01 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 16:01 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 16:01 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 16:01 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 16:01 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 16:01 121-14-2 M109/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 16:01 606-20-2 M109/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 16:01 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 16:01 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 16:01 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 16:01 117-81-709/06/16 13:4015.0 0.85 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 91 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Ethyl methanesulfonate ND ug/L 09/19/16 16:01 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 16:01 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 16:01 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 16:01 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 16:01 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 16:01 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 16:01 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 16:01 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 16:01 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 16:01 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 16:01 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 16:01 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 16:01 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 16:01 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 16:01 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 16:01 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 16:01 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 16:01 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 16:01 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 16:0109/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 16:01 134-32-709/06/16 13:4010.0 0.96 1
2-Naphthalenamine ND ug/L 09/19/16 16:01 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 16:01 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 16:01 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 16:01 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 16:01 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 16:01 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 16:01 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 16:01 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 16:01 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 16:01 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 16:01 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 16:01 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 16:01 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 16:01 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 16:01 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 16:01 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 16:01 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 16:01 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 16:01 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 16:01 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 16:01 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 16:01 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 16:01 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 16:01 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 16:01 85-01-809/06/16 13:4010.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenol ND ug/L 09/19/16 16:0109/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 16:01 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 16:01 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 16:01 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 16:01 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 16:01 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 16:01 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 16:01 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 16:01 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 16:01 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 16:01 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 16:01 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 16:01 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)78 %09/19/16 16:01 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)77 %09/19/16 16:01 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)86 %09/19/16 16:01 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)31 %09/19/16 16:01 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)44 %09/19/16 16:01 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)86 %09/19/16 16:01 118-79-609/06/16 13:4027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 02:53 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 02:53 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 02:53 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 02:53 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 02:53 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 02:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 02:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 02:53 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 02:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 02:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 02:53 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 02:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 02:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 02:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 02:53 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 02:53 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 02:53 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 02:53 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 02:53 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 02:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 02:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 02:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 02:53 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 02:53 541-73-15.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 09/08/16 02:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 02:53 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 02:53 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 02:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 02:53 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 02:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 02:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 02:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 02:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 02:53 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 02:53 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 02:53 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 02:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 02:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 02:53 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 02:53 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 02:53 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 02:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 02:53 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 02:53 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 02:53 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 02:53 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 02:53 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 02:53 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 02:53 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 02:53 107-12-01503.6 1
Styrene ND ug/L 09/08/16 02:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 02:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 02:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 02:53 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 02:53 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 02:53 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 02:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 02:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 02:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 02:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 02:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 02:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 02:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 02:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %09/08/16 02:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 02:53 17060-07-070-130 1
Toluene-d8 (S)103 %09/08/16 02:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-3 Lab ID:92310738015 Collected:08/31/16 10:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:22 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-14 Lab ID:92310738016 Collected:08/31/16 16:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 19:10 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 19:10 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 19:10 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 19:10 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 19:10 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 19:10 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 19:10 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 19:10 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 19:10 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 19:10 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 19:10 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 19:10 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 19:10 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 19:10 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 19:10 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 19:10 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 19:10 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 19:10 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 19:10 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)89 %09/07/16 19:10 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)60 %09/07/16 19:10 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 21:10 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 21:10 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 21:10 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 21:10 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 21:10 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 21:10 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 21:10 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)64 %09/07/16 21:10 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 12:58 25057-89-009/06/16 09:200.097 0.049 1
2,4-D ND ug/L 09/08/16 12:58 94-75-709/06/16 09:200.97 0.23 1
Dalapon ND ug/L 09/08/16 12:58 75-99-0 L309/06/16 09:200.94 0.44 1
2,4-DB ND ug/L 09/08/16 12:58 94-82-609/06/16 09:202.0 0.53 1
Dicamba ND ug/L 09/08/16 12:58 1918-00-909/06/16 09:200.097 0.031 1
Dichlorprop ND ug/L 09/08/16 12:58 120-36-509/06/16 09:200.67 0.20 1
Dinoseb ND ug/L 09/08/16 12:58 88-85-709/06/16 09:200.20 0.059 1
Pentachlorophenol ND ug/L 09/08/16 12:58 87-86-509/06/16 09:200.029 0.018 1
Picloram ND ug/L 09/08/16 12:58 1918-02-109/06/16 09:200.098 0.020 1
2,4,5-T ND ug/L 09/08/16 12:58 93-76-509/06/16 09:200.20 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 12:58 93-72-109/06/16 09:200.20 0.051 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-14 Lab ID:92310738016 Collected:08/31/16 16:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)89 %09/08/16 12:58 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/08/16 00:19 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/08/16 00:19 7440-38-209/06/16 21:0010.0 2.5 1
Barium 15.3J ug/L 09/08/16 00:19 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/08/16 00:19 7440-41-709/06/16 21:001.0 0.50 1
Cadmium 4.0 ug/L 09/08/16 00:19 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/08/16 00:19 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/08/16 00:19 7440-48-409/06/16 21:0010.0 2.5 1
Copper 4.3J ug/L 09/08/16 00:19 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/08/16 00:19 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/08/16 00:19 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/08/16 00:19 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/08/16 00:19 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/08/16 00:19 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/08/16 00:19 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/08/16 00:19 7440-62-209/06/16 21:0025.0 2.5 1
Zinc 5.8J ug/L 09/08/16 00:19 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 14:24 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 12:16 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 12:16 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 12:16 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 12:16 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 12:16 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 12:16 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 12:16 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 12:16 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 12:16 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 12:16 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 12:16 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 12:16 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 12:16 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 12:16 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 12:16 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 12:16 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 12:16 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 12:16 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 12:16 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 12:16 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 12:16 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 97 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-14 Lab ID:92310738016 Collected:08/31/16 16:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 12:16 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 12:16 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 12:16 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 12:16 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 12:16 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 12:16 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 12:16 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 12:16 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 12:16 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 12:16 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 12:16 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 12:16 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 12:16 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 12:16 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 12:16 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 12:16 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 12:16 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 12:16 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 12:16 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 12:16 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 12:16 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 12:16 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 12:16 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 12:16 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 12:16 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 12:16 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 12:16 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 12:16 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 12:16 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 12:16 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 12:16 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 12:16 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 12:16 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 12:16 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 12:16 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 12:16 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 12:16 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 12:16 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 12:16 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 12:16 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 12:16 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 12:16 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 12:16 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 12:16 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 12:1609/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 12:16 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-14 Lab ID:92310738016 Collected:08/31/16 16:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 12:16 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 12:16 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 12:16 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 12:16 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 12:16 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 12:16 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 12:16 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 12:16 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 12:16 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 12:16 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 12:16 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 12:16 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 12:16 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 12:16 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 12:16 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 12:16 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 12:16 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 12:16 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 12:16 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 12:16 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 12:16 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 12:16 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 12:16 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 12:16 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 12:16 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 12:1609/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 12:16 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 12:16 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 12:16 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 12:16 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 12:16 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 12:16 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 12:16 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 12:16 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 12:16 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 12:16 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 12:16 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 12:16 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)78 %09/19/16 12:16 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)80 %09/19/16 12:16 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)91 %09/19/16 12:16 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)33 %09/19/16 12:16 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)44 %09/19/16 12:16 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)88 %09/19/16 12:16 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-14 Lab ID:92310738016 Collected:08/31/16 16:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 03:10 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 03:10 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 03:10 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 03:10 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 03:10 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 03:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 03:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 03:10 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 03:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 03:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 03:10 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 03:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 03:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 03:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 03:10 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 03:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 03:10 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 03:10 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 03:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 03:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 03:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 03:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 03:10 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 03:10 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 03:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 03:10 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 03:10 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 03:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 03:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 03:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 03:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 03:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 03:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 03:10 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 03:10 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 03:10 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 03:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 03:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 03:10 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 03:10 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 03:10 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 03:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 03:10 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 03:10 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 03:10 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 03:10 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-14 Lab ID:92310738016 Collected:08/31/16 16:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 03:10 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 03:10 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 03:10 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 03:10 107-12-01503.6 1
Styrene ND ug/L 09/08/16 03:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 03:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 03:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 03:10 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 03:10 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 03:10 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 03:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 03:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 03:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 03:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 03:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 03:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 03:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 03:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 03:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 03:10 17060-07-070-130 1
Toluene-d8 (S)106 %09/08/16 03:10 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:22 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-15 Lab ID:92310738017 Collected:08/31/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 19:28 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 19:28 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 19:28 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 19:28 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 19:28 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 19:28 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 19:28 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 19:28 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 19:28 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 19:28 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 19:28 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 19:28 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 19:28 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 19:28 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 19:28 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 19:28 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 19:28 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 19:28 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 19:28 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)74 %09/07/16 19:28 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)69 %09/07/16 19:28 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 21:50 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 21:50 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 21:50 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 21:50 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 21:50 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 21:50 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 21:50 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)68 %09/07/16 21:50 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 13:28 25057-89-009/06/16 09:200.096 0.048 1
2,4-D ND ug/L 09/08/16 13:28 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 13:28 75-99-0 L309/06/16 09:200.93 0.44 1
2,4-DB ND ug/L 09/08/16 13:28 94-82-609/06/16 09:201.9 0.52 1
Dicamba ND ug/L 09/08/16 13:28 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 13:28 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 13:28 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 13:28 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 13:28 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 13:28 93-76-509/06/16 09:200.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 13:28 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 102 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-15 Lab ID:92310738017 Collected:08/31/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)86 %09/08/16 13:28 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/08/16 00:22 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/08/16 00:22 7440-38-209/06/16 21:0010.0 2.5 1
Barium ND ug/L 09/08/16 00:22 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/08/16 00:22 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/08/16 00:22 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/08/16 00:22 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/08/16 00:22 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/08/16 00:22 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/08/16 00:22 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/08/16 00:22 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/08/16 00:22 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/08/16 00:22 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/08/16 00:22 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/08/16 00:22 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/08/16 00:22 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/08/16 00:22 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 14:26 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 12:44 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 12:44 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 12:44 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 12:44 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 12:44 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 12:44 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 12:44 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 12:44 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 12:44 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 12:44 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 12:44 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 12:44 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 12:44 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 12:44 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 12:44 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 12:44 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 12:44 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 12:44 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 12:44 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 12:44 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 12:44 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-15 Lab ID:92310738017 Collected:08/31/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 12:44 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 12:44 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 12:44 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 12:44 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 12:44 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 12:44 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 12:44 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 12:44 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 12:44 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 12:44 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 12:44 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 12:44 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 12:44 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 12:44 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 12:44 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 12:44 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 12:44 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 12:44 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 12:44 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 12:44 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 12:44 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 12:44 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 12:44 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 12:44 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 12:44 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 12:44 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 12:44 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 12:44 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 12:44 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 12:44 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 12:44 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 12:44 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 12:44 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 12:44 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 12:44 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 12:44 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 12:44 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 12:44 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 12:44 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 12:44 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 12:44 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 12:44 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 12:44 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 12:44 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 12:4409/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 12:44 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-15 Lab ID:92310738017 Collected:08/31/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 12:44 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 12:44 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 12:44 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 12:44 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 12:44 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 12:44 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 12:44 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 12:44 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 12:44 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 12:44 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 12:44 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 12:44 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 12:44 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 12:44 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 12:44 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 12:44 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 12:44 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 12:44 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 12:44 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 12:44 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 12:44 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 12:44 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 12:44 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 12:44 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 12:44 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 12:4409/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 12:44 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 12:44 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 12:44 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 12:44 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 12:44 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 12:44 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 12:44 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 12:44 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 12:44 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 12:44 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 12:44 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 12:44 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)76 %09/19/16 12:44 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)75 %09/19/16 12:44 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)95 %09/19/16 12:44 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)30 %09/19/16 12:44 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)41 %09/19/16 12:44 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)82 %09/19/16 12:44 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-15 Lab ID:92310738017 Collected:08/31/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 03:27 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 03:27 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 03:27 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 03:27 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 03:27 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 03:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 03:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 03:27 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 03:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 03:27 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 03:27 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 03:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 03:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 03:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 03:27 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 03:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 03:27 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 03:27 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 03:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 03:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 03:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 03:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 03:27 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 03:27 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 03:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 03:27 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 03:27 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 03:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 03:27 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 03:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 03:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 03:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 03:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 03:27 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 03:27 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 03:27 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 03:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 03:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 03:27 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 03:27 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 03:27 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 03:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 03:27 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 03:27 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 03:27 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 03:27 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 106 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:MW-15 Lab ID:92310738017 Collected:08/31/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 03:27 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 03:27 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 03:27 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 03:27 107-12-01503.6 1
Styrene ND ug/L 09/08/16 03:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 03:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 03:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 03:27 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 03:27 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 03:27 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 03:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 03:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 03:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 03:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 03:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 03:27 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 03:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 03:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 03:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 03:27 17060-07-070-130 1
Toluene-d8 (S)105 %09/08/16 03:27 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/06/16 23:36 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:23 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 107 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:SW-4 Lab ID:92310738018 Collected:08/31/16 11:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/11/16 00:09 7440-36-009/09/16 19:206.0 3.8 1
Arsenic ND ug/L 09/11/16 00:09 7440-38-209/09/16 19:2010.0 2.5 1
Barium 415 ug/L 09/11/16 00:09 7440-39-309/09/16 19:201002.5 1
Beryllium ND ug/L 09/11/16 00:09 7440-41-709/09/16 19:201.0 0.50 1
Cadmium 2.3 ug/L 09/11/16 00:09 7440-43-909/09/16 19:201.0 0.50 1
Chromium ND ug/L 09/11/16 00:09 7440-47-309/09/16 19:2010.0 2.5 1
Cobalt ND ug/L 09/11/16 00:09 7440-48-409/09/16 19:2010.0 2.5 1
Copper ND ug/L 09/11/16 00:09 7440-50-809/09/16 19:2010.0 2.5 1
Lead ND ug/L 09/11/16 00:09 7439-92-109/09/16 19:2010.0 2.5 1
Nickel ND ug/L 09/11/16 00:09 7440-02-009/09/16 19:2050.0 2.5 1
Selenium ND ug/L 09/11/16 00:09 7782-49-209/09/16 19:2010.0 5.0 1
Silver ND ug/L 09/11/16 00:09 7440-22-409/09/16 19:2010.0 2.5 1
Thallium ND ug/L 09/11/16 00:09 7440-28-009/09/16 19:205.5 5.0 1
Vanadium ND ug/L 09/11/16 00:09 7440-62-209/09/16 19:2025.0 2.5 1
Zinc 18.5 ug/L 09/11/16 00:09 7440-66-6 B09/09/16 19:2010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 03:45 67-64-1 L310010.0 1
Acrylonitrile ND ug/L 09/08/16 03:45 107-13-12001.9 1
Benzene ND ug/L 09/08/16 03:45 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 03:45 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 03:45 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 03:45 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 03:45 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 03:45 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 03:45 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 03:45 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 03:45 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 03:45 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 03:45 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 03:45 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 03:45 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 03:45 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 03:45 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 03:45 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 03:45 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/08/16 03:45 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 03:45 110-57-6 L31001.0 1
1,1-Dichloroethane ND ug/L 09/08/16 03:45 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 03:45 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 03:45 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 03:45 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 03:45 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 03:45 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 03:45 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 03:45 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 108 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:SW-4 Lab ID:92310738018 Collected:08/31/16 11:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/08/16 03:45 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/08/16 03:45 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 03:45 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 09/08/16 03:45 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 03:45 108-10-11000.33 1
Styrene ND ug/L 09/08/16 03:45 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 03:45 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 03:45 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 03:45 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 03:45 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/08/16 03:45 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 03:45 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 03:45 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 03:45 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 03:45 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 03:45 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 03:45 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 03:45 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %09/08/16 03:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %09/08/16 03:45 17060-07-070-130 1
Toluene-d8 (S)109 %09/08/16 03:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 109 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:SW-5 Lab ID:92310738019 Collected:08/31/16 16:55 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/11/16 00:28 7440-36-009/09/16 19:206.0 3.8 1
Arsenic 3.7J ug/L 09/11/16 00:28 7440-38-2 B09/09/16 19:2010.0 2.5 1
Barium 448 ug/L 09/11/16 00:28 7440-39-309/09/16 19:201002.5 1
Beryllium ND ug/L 09/11/16 00:28 7440-41-709/09/16 19:201.0 0.50 1
Cadmium 4.3 ug/L 09/11/16 00:28 7440-43-909/09/16 19:201.0 0.50 1
Chromium ND ug/L 09/11/16 00:28 7440-47-309/09/16 19:2010.0 2.5 1
Cobalt 3.0J ug/L 09/11/16 00:28 7440-48-409/09/16 19:2010.0 2.5 1
Copper 5.0J ug/L 09/11/16 00:28 7440-50-809/09/16 19:2010.0 2.5 1
Lead 5.3J ug/L 09/11/16 00:28 7439-92-109/09/16 19:2010.0 2.5 1
Nickel 4.1J ug/L 09/11/16 00:28 7440-02-009/09/16 19:2050.0 2.5 1
Selenium ND ug/L 09/11/16 00:28 7782-49-209/09/16 19:2010.0 5.0 1
Silver ND ug/L 09/11/16 00:28 7440-22-409/09/16 19:2010.0 2.5 1
Thallium ND ug/L 09/11/16 00:28 7440-28-009/09/16 19:205.5 5.0 1
Vanadium 2.9J ug/L 09/11/16 00:28 7440-62-209/09/16 19:2025.0 2.5 1
Zinc 20.9 ug/L 09/11/16 00:28 7440-66-6 B09/09/16 19:2010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 04:02 67-64-1 L310010.0 1
Acrylonitrile ND ug/L 09/08/16 04:02 107-13-12001.9 1
Benzene ND ug/L 09/08/16 04:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 04:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 04:02 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 04:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 04:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 04:02 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 04:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 04:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 04:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 04:02 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 04:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 04:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 04:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 04:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 04:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 04:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 04:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/08/16 04:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 04:02 110-57-6 L31001.0 1
1,1-Dichloroethane ND ug/L 09/08/16 04:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 04:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 04:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 04:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 04:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 04:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 04:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 04:02 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 200
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Sample:SW-5 Lab ID:92310738019 Collected:08/31/16 16:55 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/08/16 04:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/08/16 04:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 04:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 09/08/16 04:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 04:02 108-10-11000.33 1
Styrene ND ug/L 09/08/16 04:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 04:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 04:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 04:02 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 04:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/08/16 04:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 04:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 04:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 04:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 04:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 04:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 04:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 04:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %09/08/16 04:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %09/08/16 04:02 17060-07-070-130 1
Toluene-d8 (S)105 %09/08/16 04:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 111 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327243
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Associated Lab Samples:92310738001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813258
Associated Lab Samples:92310738001
Matrix:Water
AnalyzedMDL
Ethane ug/L ND 10.0 N209/02/16 10:2910.0
Ethene ug/L ND 10.0 N209/02/16 10:2910.0
Methane ug/L ND 10.0 N209/02/16 10:2910.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813259LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1813260
Ethane ug/L 622 N26589570-13097639 3 20
Ethene ug/L 1010 N211209070-13089997 1 20
Methane ug/L 338 N23968570-13094370 9 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 112 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327037
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006, 92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1812112
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006, 92310738007
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 09/01/16 08:440.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812113LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1812114MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310771011
1812115
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 59 75-12544 15 252.51.1 2.6 2.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327371
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814119
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 09/08/16 12:340.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814120LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814121MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311072001
1814122
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-125104 3 252.5ND 2.5 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328823
EPA 7470
EPA 7470
7470 Mercury Dissolved
Associated Lab Samples:92310738009, 92310738012, 92310738013, 92310738014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1822533
Associated Lab Samples:92310738009, 92310738012, 92310738013, 92310738014
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 09/20/16 01:040.090
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1822534LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.52.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1822535MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92312581008
1822536
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 84 75-12583 0 252.5ND 2.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
330655
EPA 7470
EPA 7470
7470 Mercury Dissolved
Associated Lab Samples:92310738011, 92310738015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1832063
Associated Lab Samples:92310738011, 92310738015
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 09/28/16 10:570.090
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1832064LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1832065MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738015
1832066
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 77 75-12576 2 252.50.23 2.2 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327130
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006, 92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1812571
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006, 92310738007
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/02/16 18:443.8
Arsenic ug/L 3.7J 10.0 09/02/16 18:442.5
Barium ug/L ND 100 09/02/16 18:442.5
Beryllium ug/L ND 1.0 09/02/16 18:440.50
Cadmium ug/L ND 1.0 09/02/16 18:440.50
Chromium ug/L ND 10.0 09/02/16 18:442.5
Cobalt ug/L ND 10.0 09/02/16 18:442.5
Copper ug/L ND 10.0 09/02/16 18:442.5
Lead ug/L ND 10.0 09/02/16 18:442.5
Nickel ug/L ND 50.0 09/02/16 18:442.5
Selenium ug/L ND 10.0 09/02/16 18:445.0
Silver ug/L ND 10.0 09/02/16 18:442.5
Thallium ug/L ND 5.5 09/03/16 14:055.0
Tin ug/L ND 100 09/02/16 18:442.5
Vanadium ug/L ND 25.0 09/02/16 18:442.5
Zinc ug/L ND 10.0 09/02/16 18:445.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812572LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 500500 100 80-120
Arsenic ug/L 489500 98 80-120
Barium ug/L 460500 92 80-120
Beryllium ug/L 460500 92 80-120
Cadmium ug/L 487500 97 80-120
Chromium ug/L 468500 94 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 495500 99 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 506500 101 80-120
Silver ug/L 244250 97 80-120
Thallium ug/L 473500 95 80-120
Tin ug/L 498500 100 80-120
Vanadium ug/L 474500 95 80-120
Zinc ug/L 502500 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1812573MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738001
1812574
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 77 75-12578 2 25500ND386392
Arsenic ug/L 500 98 75-12598 1 255009.8J 499 502
Barium ug/L 500 92 75-12592 0 2550041.5J 503 504
Beryllium ug/L 500 92 75-12593 0 255000.59J 463 464
Cadmium ug/L 500 98 75-12598 1 25500ND488490
Chromium ug/L 500 96 75-12597 0 2550019.8 501 503
Cobalt ug/L 500 100 75-125100 0 25500ND500500
Copper ug/L 500 102 75-125102 0 255007.0J 516 515
Lead ug/L 500 96 75-12597 1 255009.3J 491 496
Nickel ug/L 500 95 75-12595 0 25500ND478480
Selenium ug/L 500 100 75-12599 0 25500ND500498
Silver ug/L 250 98 75-12598 0 25250ND244245
Thallium ug/L 500 90 75-12592 1 25500ND453460
Tin ug/L 500 98 75-12599 1 25500ND491494
Vanadium ug/L 500 98 75-12598 0 2550046.3 535 536
Zinc ug/L 500 102 75-125103 1 2550016.8 526 530
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327495
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814776
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/07/16 22:513.8
Arsenic ug/L ND 10.0 09/07/16 22:512.5
Barium ug/L ND 100 09/07/16 22:512.5
Beryllium ug/L ND 1.0 09/07/16 22:510.50
Cadmium ug/L ND 1.0 09/07/16 22:510.50
Chromium ug/L ND 10.0 09/07/16 22:512.5
Cobalt ug/L ND 10.0 09/07/16 22:512.5
Copper ug/L ND 10.0 09/07/16 22:512.5
Lead ug/L ND 10.0 09/07/16 22:512.5
Nickel ug/L ND 50.0 09/07/16 22:512.5
Selenium ug/L ND 10.0 09/07/16 22:515.0
Silver ug/L ND 10.0 09/07/16 22:512.5
Thallium ug/L ND 5.5 09/07/16 22:515.0
Tin ug/L ND 100 09/07/16 22:512.5
Vanadium ug/L ND 25.0 09/07/16 22:512.5
Zinc ug/L ND 10.0 09/07/16 22:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814777LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 463500 93 80-120
Arsenic ug/L 449500 90 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 502500 100 80-120
Lead ug/L 471500 94 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 478500 96 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 460500 92 80-120
Tin ug/L 476500 95 80-120
Vanadium ug/L 490500 98 80-120
Zinc ug/L 474500 95 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814778MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311078001
1814779
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 85 75-12586 0 25500ND428430
Arsenic ug/L 500 87 75-12588 1 255005.8J 443 446
Barium ug/L 500 104 75-125104 1 2550020.2J 539 542
Beryllium ug/L 500 100 75-125101 1 25500ND499503
Cadmium ug/L 500 97 75-12597 0 25500ND484485
Chromium ug/L 500 104 75-125106 2 2550020.1 541 550
Cobalt ug/L 500 95 75-12595 0 25500ND475475
Copper ug/L 500 102 75-125103 0 255003.1J 514 516
Lead ug/L 500 93 75-12593 0 255004.4J 469 469
Nickel ug/L 500 95 75-12596 1 25500ND476481
Selenium ug/L 500 92 75-12592 1 25500ND462466
Silver ug/L 250 98 75-12598 0 25250ND245245
Thallium ug/L 500 90 75-12591 1 25500ND451456
Tin ug/L 500 94 75-12594 0 25500ND471471
Vanadium ug/L 500 99 75-125100 1 2550028.4 524 527
Zinc ug/L 500 96 75-12596 0 25500ND482485
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327945
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92310738018, 92310738019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1817217
Associated Lab Samples:92310738018, 92310738019
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/11/16 00:033.8
Arsenic ug/L 6.5J 10.0 09/11/16 00:032.5
Barium ug/L ND 100 09/11/16 00:032.5
Beryllium ug/L ND 1.0 09/11/16 00:030.50
Cadmium ug/L ND 1.0 09/11/16 00:030.50
Chromium ug/L ND 10.0 09/11/16 00:032.5
Cobalt ug/L ND 10.0 09/11/16 00:032.5
Copper ug/L ND 10.0 09/11/16 00:032.5
Lead ug/L ND 10.0 09/11/16 00:032.5
Nickel ug/L ND 50.0 09/11/16 00:032.5
Selenium ug/L ND 10.0 09/11/16 00:035.0
Silver ug/L ND 10.0 09/11/16 00:032.5
Thallium ug/L ND 5.5 09/11/16 00:035.0
Vanadium ug/L ND 25.0 09/11/16 00:032.5
Zinc ug/L 6.2J 10.0 09/11/16 00:035.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1817218LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 502500 100 80-120
Arsenic ug/L 497500 99 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 520500 104 80-120
Cadmium ug/L 508500 102 80-120
Chromium ug/L 519500 104 80-120
Cobalt ug/L 518500 104 80-120
Copper ug/L 522500 104 80-120
Lead ug/L 510500 102 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 255250 102 80-120
Thallium ug/L 512500 102 80-120
Vanadium ug/L 510500 102 80-120
Zinc ug/L 530500 106 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1817219MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738018
1817220
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12597 0 25500ND486484
Arsenic ug/L 500 98 75-12598 0 25500ND491492
Barium ug/L 500 97 75-12598 1 25500415899905
Beryllium ug/L 500 100 75-125101 0 25500ND502504
Cadmium ug/L 500 98 75-12598 0 255002.3 493 494
Chromium ug/L 500 99 75-125100 0 25500ND497498
Cobalt ug/L 500 99 75-12599 0 25500ND499499
Copper ug/L 500 101 75-125101 0 25500ND509510
Lead ug/L 500 98 75-12597 0 25500ND490489
Nickel ug/L 500 97 75-12597 0 25500ND486486
Selenium ug/L 500 100 75-125100 0 25500ND500502
Silver ug/L 250 98 75-12599 1 25250ND246247
Thallium ug/L 500 97 75-12597 0 25500ND487487
Vanadium ug/L 500 99 75-12599 0 25500ND495497
Zinc ug/L 500 101 75-125101 0 2550018.5 524 524
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327533
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92310738009, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814923
Associated Lab Samples:92310738009, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015
Matrix:Water
AnalyzedMDL
Antimony, Dissolved ug/L ND 5.0 09/20/16 14:513.8
Arsenic, Dissolved ug/L ND 10.0 09/20/16 14:515.0
Barium, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Beryllium, Dissolved ug/L ND 1.0 09/20/16 14:510.050
Cadmium, Dissolved ug/L ND 1.0 09/20/16 14:510.50
Chromium, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Cobalt, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Copper, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Lead, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Nickel, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Selenium, Dissolved ug/L ND 10.0 09/20/16 14:515.0
Silver, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Thallium, Dissolved ug/L ND 10.0 09/20/16 14:515.0
Tin, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Vanadium, Dissolved ug/L ND 5.0 09/20/16 14:512.5
Zinc, Dissolved ug/L ND 10.0 09/20/16 14:512.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814924LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 462500 92 80-120
Arsenic, Dissolved ug/L 447500 89 80-120
Barium, Dissolved ug/L 509500 102 80-120
Beryllium, Dissolved ug/L 486500 97 80-120
Cadmium, Dissolved ug/L 475500 95 80-120
Chromium, Dissolved ug/L 500500 100 80-120
Cobalt, Dissolved ug/L 476500 95 80-120
Copper, Dissolved ug/L 487500 97 80-120
Lead, Dissolved ug/L 467500 93 80-120
Nickel, Dissolved ug/L 474500 95 80-120
Selenium, Dissolved ug/L 463500 93 80-120
Silver, Dissolved ug/L 240250 96 80-120
Thallium, Dissolved ug/L 507500 101 80-120
Tin, Dissolved ug/L 477500 95 80-120
Vanadium, Dissolved ug/L 484500 97 80-120
Zinc, Dissolved ug/L 474500 95 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814927MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738009
1814928
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 500 85 75-12583 2 20500ND427420
Arsenic, Dissolved ug/L 500 81 75-12580 2 20500ND411404
Barium, Dissolved ug/L 500 94 75-12593 1 2050033.5 504 498
Beryllium, Dissolved ug/L 500 89 75-12588 1 205000.18J 443 438
Cadmium, Dissolved ug/L 500 87 75-12586 1 20500ND437433
Chromium, Dissolved ug/L 500 91 75-12591 0 20500ND457457
Cobalt, Dissolved ug/L 500 87 75-12585 1 20500ND434427
Copper, Dissolved ug/L 500 90 75-12589 1 20500ND449444
Lead, Dissolved ug/L 500 84 75-12584 1 20500ND422420
Nickel, Dissolved ug/L 500 87 75-12586 1 20500ND436431
Selenium, Dissolved ug/L 500 86 75-12585 1 20500ND428426
Silver, Dissolved ug/L 250 88 75-12588 1 20250ND221220
Thallium, Dissolved ug/L 500 82 75-12581 2 20500ND413406
Tin, Dissolved ug/L 500 86 75-12586 1 20500ND433429
Vanadium, Dissolved ug/L 500 88 75-12588 1 20500ND443439
Zinc, Dissolved ug/L 500 86 75-12586 1 205002.7J 434 431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327295
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813520
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/02/16 13:250.33
1,1,1-Trichloroethane ug/L ND 1.0 09/02/16 13:250.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/02/16 13:250.40
1,1,2-Trichloroethane ug/L ND 1.0 09/02/16 13:250.29
1,1-Dichloroethane ug/L ND 5.0 09/02/16 13:250.32
1,1-Dichloroethene ug/L ND 5.0 09/02/16 13:250.56
1,1-Dichloropropene ug/L ND 5.0 09/02/16 13:250.49
1,2,3-Trichloropropane ug/L ND 1.0 09/02/16 13:250.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/02/16 13:250.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/02/16 13:252.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/02/16 13:250.27
1,2-Dichlorobenzene ug/L ND 5.0 09/02/16 13:250.30
1,2-Dichloroethane ug/L ND 1.0 09/02/16 13:250.24
1,2-Dichloropropane ug/L ND 1.0 09/02/16 13:250.27
1,3-Dichlorobenzene ug/L ND 5.0 09/02/16 13:250.24
1,3-Dichloropropane ug/L ND 1.0 09/02/16 13:250.28
1,4-Dichlorobenzene ug/L ND 1.0 09/02/16 13:250.33
2,2-Dichloropropane ug/L ND 15.0 09/02/16 13:250.13
2-Butanone (MEK)ug/L ND 100 09/02/16 13:250.96
2-Hexanone ug/L ND 50.0 09/02/16 13:250.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/02/16 13:250.33
Acetone ug/L 24.2J 100 09/02/16 13:2510.0
Acetonitrile ug/L ND 55.0 09/02/16 13:252.2
Acrolein ug/L ND 53.0 09/02/16 13:251.6
Acrylonitrile ug/L ND 200 09/02/16 13:251.9
Allyl chloride ug/L ND 10.0 09/02/16 13:251.5
Benzene ug/L ND 1.0 09/02/16 13:250.25
Bromochloromethane ug/L ND 3.0 09/02/16 13:250.17
Bromodichloromethane ug/L ND 1.0 09/02/16 13:250.18
Bromoform ug/L ND 3.0 09/02/16 13:250.26
Bromomethane ug/L ND 10.0 09/02/16 13:250.29
Carbon disulfide ug/L ND 100 09/02/16 13:251.2
Carbon tetrachloride ug/L ND 1.0 09/02/16 13:250.25
Chlorobenzene ug/L ND 3.0 09/02/16 13:250.23
Chloroethane ug/L ND 10.0 09/02/16 13:250.54
Chloroform ug/L ND 5.0 09/02/16 13:250.14
Chloromethane ug/L ND 1.0 09/02/16 13:250.11
Chloroprene ug/L ND 20.0 09/02/16 13:250.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/02/16 13:250.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/02/16 13:250.13
Dibromochloromethane ug/L ND 3.0 09/02/16 13:250.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 125 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813520
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 09/02/16 13:250.21
Dichlorodifluoromethane ug/L ND 5.0 09/02/16 13:250.21
Ethyl methacrylate ug/L ND 10.0 09/02/16 13:250.20
Ethylbenzene ug/L ND 1.0 09/02/16 13:250.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/02/16 13:250.71
Iodomethane ug/L ND 10.0 09/02/16 13:250.32
Isobutanol ug/L ND 100 09/02/16 13:2535.0
Methacrylonitrile ug/L ND 100 09/02/16 13:250.93
Methyl methacrylate ug/L ND 30.0 09/02/16 13:252.0
Methylene Chloride ug/L ND 1.0 09/02/16 13:250.97
Naphthalene ug/L ND 10.0 09/02/16 13:250.24
Propionitrile ug/L ND 150 09/02/16 13:253.6
Styrene ug/L 0.60J 1.0 09/02/16 13:250.26
Tetrachloroethene ug/L ND 1.0 09/02/16 13:250.46
Toluene ug/L ND 1.0 09/02/16 13:250.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/02/16 13:250.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/02/16 13:250.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/02/16 13:251.0
Trichloroethene ug/L ND 1.0 09/02/16 13:250.47
Trichlorofluoromethane ug/L ND 1.0 09/02/16 13:250.20
Vinyl acetate ug/L ND 50.0 09/02/16 13:250.35
Vinyl chloride ug/L ND 1.0 09/02/16 13:250.62
Xylene (Total)ug/L ND 5.0 09/02/16 13:250.66
1,2-Dichloroethane-d4 (S)%94 70-130 09/02/16 13:25
4-Bromofluorobenzene (S)%107 70-130 09/02/16 13:25
Toluene-d8 (S)%106 70-130 09/02/16 13:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813521LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.450 99 80-125
1,1,1-Trichloroethane ug/L 48.050 96 71-129
1,1,2,2-Tetrachloroethane ug/L 46.050 92 79-124
1,1,2-Trichloroethane ug/L 49.350 99 85-125
1,1-Dichloroethane ug/L 47.550 95 73-126
1,1-Dichloroethene ug/L 47.650 95 66-135
1,1-Dichloropropene ug/L 47.950 96 74-135
1,2,3-Trichloropropane ug/L 44.550 89 75-130
1,2,4-Trichlorobenzene ug/L 49.950 100 75-134
1,2-Dibromo-3-chloropropane ug/L 46.350 93 71-133
1,2-Dibromoethane (EDB)ug/L 51.750 103 83-124
1,2-Dichlorobenzene ug/L 49.650 99 80-133
1,2-Dichloroethane ug/L 48.950 98 67-128
1,2-Dichloropropane ug/L 49.250 98 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813521LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.250 98 77-130
1,3-Dichloropropane ug/L 49.150 98 76-131
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2,2-Dichloropropane ug/L 49.550 99 40-160
2-Butanone (MEK)ug/L 104100 104 61-144
2-Hexanone ug/L 94.0100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 72-135
Acetone ug/L 94.4J100 94 48-146
Acetonitrile ug/L 353500 71 62-150
Acrolein ug/L 178250 71 24-160
Acrylonitrile ug/L 238250 95 40-160
Allyl chloride ug/L 41.750 83 66-137
Benzene ug/L 49.950 100 80-125
Bromochloromethane ug/L 49.950 100 71-125
Bromodichloromethane ug/L 47.650 95 78-124
Bromoform ug/L 45.750 91 71-128
Bromomethane ug/L 44.550 89 40-160
Carbon disulfide ug/L 46.1J50 92 50-160
Carbon tetrachloride ug/L 48.550 97 69-131
Chlorobenzene ug/L 48.350 97 81-122
Chloroethane ug/L 51.750 103 39-148
Chloroform ug/L 46.350 93 73-127
Chloromethane ug/L 44.850 90 44-146
Chloroprene ug/L 51.150 102 75-145
cis-1,2-Dichloroethene ug/L 49.350 99 74-124
cis-1,3-Dichloropropene ug/L 49.850 100 72-132
Dibromochloromethane ug/L 49.950 100 78-125
Dibromomethane ug/L 49.850 100 82-120
Dichlorodifluoromethane ug/L 42.450 85 34-157
Ethyl methacrylate ug/L 49.650 99 82-121
Ethylbenzene ug/L 47.450 95 79-121
Hexachloro-1,3-butadiene ug/L 49.050 98 72-131
Iodomethane ug/L 72.6100 73 39-154
Isobutanol ug/L 8211000 82 34-160
Methacrylonitrile ug/L 515500 103 74-134
Methyl methacrylate ug/L 51.750 103 84-124
Methylene Chloride ug/L 48.550 97 64-133
Naphthalene ug/L 46.350 93 73-133
Propionitrile ug/L 434500 87 73-140
Styrene ug/L 49.150 98 84-126
Tetrachloroethene ug/L 45.750 91 78-122
Toluene ug/L 49.050 98 80-121
trans-1,2-Dichloroethene ug/L 49.350 99 71-127
trans-1,3-Dichloropropene ug/L 47.550 95 69-141
trans-1,4-Dichloro-2-butene ug/L 66.3J50 133 40-160
Trichloroethene ug/L 52.150 104 78-122
Trichlorofluoromethane ug/L 46.050 92 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813521LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 101100 101 40-160
Vinyl chloride ug/L 45.250 90 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815215MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738005
1,1,1,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,1-Trichloroethane ug/L 27.2 M12013670-130ND
1,1,2,2-Tetrachloroethane ug/L 20.920 104 70-130ND
1,1,2-Trichloroethane ug/L 20.720 103 70-130ND
1,1-Dichloroethane ug/L 24.320 122 70-130ND
1,1-Dichloroethene ug/L 28.220 141 70-166ND
1,1-Dichloropropene ug/L 27.3 M12013770-130ND
1,2,3-Trichloropropane ug/L 20.620 103 70-130ND
1,2,4-Trichlorobenzene ug/L 24.720 123 70-130ND
1,2-Dibromo-3-chloropropane ug/L 23.620 118 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.320 117 70-130ND
1,2-Dichlorobenzene ug/L 23.820 119 70-130ND
1,2-Dichloroethane ug/L 22.820 113 70-130ND
1,2-Dichloropropane ug/L 23.420 117 70-130ND
1,3-Dichlorobenzene ug/L 25.120 126 70-130ND
1,3-Dichloropropane ug/L 21.520 108 70-130ND
1,4-Dichlorobenzene ug/L 23.620 118 70-130ND
2,2-Dichloropropane ug/L 27.4 M12013770-130ND
2-Butanone (MEK)ug/L 41.1J40 103 70-130ND
2-Hexanone ug/L 42.9J40 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.7J40 107 70-130ND
Acetone ug/L 43.8J40 106 70-130ND
Acetonitrile ug/L 216200 108 70-130ND
Acrolein ug/L 187 M110018770-130ND
Acrylonitrile ug/L 117J100 117 70-130ND
Allyl chloride ug/L 23.820 119 70-130ND
Benzene ug/L 25.020 125 70-148ND
Bromochloromethane ug/L 25.220 126 70-130ND
Bromodichloromethane ug/L 23.820 119 70-130ND
Bromoform ug/L 21.020 105 70-130ND
Bromomethane ug/L 30.4 M12015270-130ND
Carbon disulfide ug/L 36.3J M12017870-130ND
Carbon tetrachloride ug/L 26.6 M12013370-130ND
Chlorobenzene ug/L 23.120 115 70-146ND
Chloroethane ug/L 25.820 129 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815215MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738005
Chloroform ug/L 24.220 121 70-130ND
Chloromethane ug/L 22.920 115 70-130ND
Chloroprene ug/L 27.9 M12014070-130ND
cis-1,2-Dichloroethene ug/L 25.220 126 70-130ND
cis-1,3-Dichloropropene ug/L 23.920 120 70-130ND
Dibromochloromethane ug/L 22.720 114 70-130ND
Dibromomethane ug/L 21.920 110 70-130ND
Dichlorodifluoromethane ug/L 19.720 99 70-130ND
Ethyl methacrylate ug/L 22.120 110 70-130ND
Ethylbenzene ug/L 23.820 119 70-130ND
Hexachloro-1,3-butadiene ug/L 29.9 M12015070-130ND
Iodomethane ug/L 43.240 108 70-130ND
Isobutanol ug/L 370400 92 70-130ND
Methacrylonitrile ug/L 218200 109 70-130ND
Methyl methacrylate ug/L 21.4J20 107 70-130ND
Methylene Chloride ug/L 25.020 125 70-130ND
Naphthalene ug/L 22.920 114 70-130ND
Propionitrile ug/L 212200 106 70-130ND
Styrene ug/L 23.720 118 70-130ND
Tetrachloroethene ug/L 23.820 119 70-130ND
Toluene ug/L 24.320 121 70-155ND
trans-1,2-Dichloroethene ug/L 26.2 M12013170-130ND
trans-1,3-Dichloropropene ug/L 21.920 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 24.720 124 69-151ND
Trichlorofluoromethane ug/L 25.720 128 70-130ND
Vinyl acetate ug/L 47.1J40 118 70-130ND
Vinyl chloride ug/L 23.920 120 70-130ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738006
1813522SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738006
1813522SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 27.1J 6 3028.7J
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Huntersville, NC 28078
[phone]
Page 130 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738006
1813522SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%96 096
4-Bromofluorobenzene (S)%104 3101
Toluene-d8 (S)%105 5100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327683
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92310738007, 92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014,
92310738015, 92310738016, 92310738017, 92310738018, 92310738019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815879
Associated Lab Samples:92310738007, 92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014,
92310738015, 92310738016, 92310738017, 92310738018, 92310738019
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/07/16 23:440.33
1,1,1-Trichloroethane ug/L ND 1.0 09/07/16 23:440.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/07/16 23:440.40
1,1,2-Trichloroethane ug/L ND 1.0 09/07/16 23:440.29
1,1-Dichloroethane ug/L ND 5.0 09/07/16 23:440.32
1,1-Dichloroethene ug/L ND 5.0 09/07/16 23:440.56
1,1-Dichloropropene ug/L ND 5.0 09/07/16 23:440.49
1,2,3-Trichloropropane ug/L ND 1.0 09/07/16 23:440.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/07/16 23:440.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/07/16 23:442.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/07/16 23:440.27
1,2-Dichlorobenzene ug/L ND 5.0 09/07/16 23:440.30
1,2-Dichloroethane ug/L ND 1.0 09/07/16 23:440.24
1,2-Dichloropropane ug/L ND 1.0 09/07/16 23:440.27
1,3-Dichlorobenzene ug/L ND 5.0 09/07/16 23:440.24
1,3-Dichloropropane ug/L ND 1.0 09/07/16 23:440.28
1,4-Dichlorobenzene ug/L ND 1.0 09/07/16 23:440.33
2,2-Dichloropropane ug/L ND 15.0 09/07/16 23:440.13
2-Butanone (MEK)ug/L ND 100 09/07/16 23:440.96
2-Hexanone ug/L ND 50.0 09/07/16 23:440.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/07/16 23:440.33
Acetone ug/L ND 100 09/07/16 23:4410.0
Acetonitrile ug/L ND 55.0 09/07/16 23:442.2
Acrolein ug/L ND 53.0 09/07/16 23:441.6
Acrylonitrile ug/L ND 200 09/07/16 23:441.9
Allyl chloride ug/L ND 10.0 09/07/16 23:441.5
Benzene ug/L ND 1.0 09/07/16 23:440.25
Bromochloromethane ug/L ND 3.0 09/07/16 23:440.17
Bromodichloromethane ug/L ND 1.0 09/07/16 23:440.18
Bromoform ug/L ND 3.0 09/07/16 23:440.26
Bromomethane ug/L ND 10.0 09/07/16 23:440.29
Carbon disulfide ug/L ND 100 09/07/16 23:441.2
Carbon tetrachloride ug/L ND 1.0 09/07/16 23:440.25
Chlorobenzene ug/L ND 3.0 09/07/16 23:440.23
Chloroethane ug/L ND 10.0 09/07/16 23:440.54
Chloroform ug/L ND 5.0 09/07/16 23:440.14
Chloromethane ug/L ND 1.0 09/07/16 23:440.11
Chloroprene ug/L ND 20.0 09/07/16 23:440.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/07/16 23:440.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/07/16 23:440.13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Page 132 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815879
Associated Lab Samples:92310738007, 92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014,
92310738015, 92310738016, 92310738017, 92310738018, 92310738019
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 3.0 09/07/16 23:440.21
Dibromomethane ug/L ND 10.0 09/07/16 23:440.21
Dichlorodifluoromethane ug/L ND 5.0 09/07/16 23:440.21
Ethyl methacrylate ug/L ND 10.0 09/07/16 23:440.20
Ethylbenzene ug/L ND 1.0 09/07/16 23:440.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/07/16 23:440.71
Iodomethane ug/L ND 10.0 09/07/16 23:440.32
Isobutanol ug/L ND 100 09/07/16 23:4435.0
Methacrylonitrile ug/L ND 100 09/07/16 23:440.93
Methyl methacrylate ug/L ND 30.0 09/07/16 23:442.0
Methylene Chloride ug/L ND 1.0 09/07/16 23:440.97
Naphthalene ug/L ND 10.0 09/07/16 23:440.24
Propionitrile ug/L ND 150 09/07/16 23:443.6
Styrene ug/L ND 1.0 09/07/16 23:440.26
Tetrachloroethene ug/L ND 1.0 09/07/16 23:440.46
Toluene ug/L ND 1.0 09/07/16 23:440.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/07/16 23:440.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/07/16 23:440.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/07/16 23:441.0
Trichloroethene ug/L ND 1.0 09/07/16 23:440.47
Trichlorofluoromethane ug/L ND 1.0 09/07/16 23:440.20
Vinyl acetate ug/L ND 50.0 09/07/16 23:440.35
Vinyl chloride ug/L ND 1.0 09/07/16 23:440.62
Xylene (Total)ug/L ND 5.0 09/07/16 23:440.66
1,2-Dichloroethane-d4 (S)%105 70-130 09/07/16 23:44
4-Bromofluorobenzene (S)%101 70-130 09/07/16 23:44
Toluene-d8 (S)%101 70-130 09/07/16 23:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815880LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.050 110 80-125
1,1,1-Trichloroethane ug/L 51.850 104 71-129
1,1,2,2-Tetrachloroethane ug/L 56.350 113 79-124
1,1,2-Trichloroethane ug/L 52.150 104 85-125
1,1-Dichloroethane ug/L 50.850 102 73-126
1,1-Dichloroethene ug/L 54.350 109 66-135
1,1-Dichloropropene ug/L 52.350 105 74-135
1,2,3-Trichloropropane ug/L 53.550 107 75-130
1,2,4-Trichlorobenzene ug/L 56.350 113 75-134
1,2-Dibromo-3-chloropropane ug/L 52.850 106 71-133
1,2-Dibromoethane (EDB)ug/L 60.450 121 83-124
1,2-Dichlorobenzene ug/L 56.350 113 80-133
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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[phone]
Page 133 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815880LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 50.450 101 67-128
1,2-Dichloropropane ug/L 51.350 103 75-132
1,3-Dichlorobenzene ug/L 56.650 113 77-130
1,3-Dichloropropane ug/L 54.150 108 76-131
1,4-Dichlorobenzene ug/L 54.550 109 78-130
2,2-Dichloropropane ug/L 49.050 98 40-160
2-Butanone (MEK)ug/L 127100 127 61-144
2-Hexanone ug/L 125100 125 68-143
4-Methyl-2-pentanone (MIBK)ug/L 115100 115 72-135
Acetone ug/L 155 L010015548-146
Acetonitrile ug/L 593500 119 62-150
Acrolein ug/L 289 F325011624-160
Acrylonitrile ug/L 288250 115 40-160
Allyl chloride ug/L 51.650 103 66-137
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 54.250 108 71-125
Bromodichloromethane ug/L 53.150 106 78-124
Bromoform ug/L 47.550 95 71-128
Bromomethane ug/L 49.7 F3509940-160
Carbon disulfide ug/L 67.7J F35013550-160
Carbon tetrachloride ug/L 52.750 105 69-131
Chlorobenzene ug/L 53.550 107 81-122
Chloroethane ug/L 49.950 100 39-148
Chloroform ug/L 49.350 99 73-127
Chloromethane ug/L 47.250 94 44-146
Chloroprene ug/L 53.850 108 75-145
cis-1,2-Dichloroethene ug/L 51.350 103 74-124
cis-1,3-Dichloropropene ug/L 54.750 109 72-132
Dibromochloromethane ug/L 57.350 115 78-125
Dibromomethane ug/L 51.150 102 82-120
Dichlorodifluoromethane ug/L 47.050 94 34-157
Ethyl methacrylate ug/L 56.150 112 82-121
Ethylbenzene ug/L 52.250 104 79-121
Hexachloro-1,3-butadiene ug/L 52.550 105 72-131
Iodomethane ug/L 113100 113 39-154
Isobutanol ug/L 15601000 156 34-160
Methacrylonitrile ug/L 595500 119 74-134
Methyl methacrylate ug/L 57.150 114 84-124
Methylene Chloride ug/L 54.950 110 64-133
Naphthalene ug/L 54.650 109 73-133
Propionitrile ug/L 616500 123 73-140
Styrene ug/L 54.250 108 84-126
Tetrachloroethene ug/L 52.350 105 78-122
Toluene ug/L 51.650 103 80-121
trans-1,2-Dichloroethene ug/L 51.150 102 71-127
trans-1,3-Dichloropropene ug/L 53.050 106 69-141
trans-1,4-Dichloro-2-butene ug/L 92.4J F3,L05018540-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815880LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 52.250 104 78-122
Trichlorofluoromethane ug/L 49.750 99 53-137
Vinyl acetate ug/L 119100 119 40-160
Vinyl chloride ug/L 46.850 94 58-137
Xylene (Total)ug/L 155150 103 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815882MATRIX SPIKE SAMPLE:
MSSpike
Result
92311078007
1,1,1,2-Tetrachloroethane ug/L 21.320 107 70-130ND
1,1,1-Trichloroethane ug/L 23.520 118 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,2-Trichloroethane ug/L 20.920 104 70-130ND
1,1-Dichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethene ug/L 23.120 115 70-166ND
1,1-Dichloropropene ug/L 22.920 115 70-130ND
1,2,3-Trichloropropane ug/L 21.820 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.720 114 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.020 105 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.620 118 70-130ND
1,2-Dichlorobenzene ug/L 23.020 115 70-130ND
1,2-Dichloroethane ug/L 21.320 106 70-130ND
1,2-Dichloropropane ug/L 22.520 112 70-130ND
1,3-Dichlorobenzene ug/L 22.820 114 70-130ND
1,3-Dichloropropane ug/L 22.320 111 70-130ND
1,4-Dichlorobenzene ug/L 21.620 108 70-130ND
2,2-Dichloropropane ug/L 24.320 122 70-130ND
2-Butanone (MEK)ug/L 39.2J40 98 70-130ND
2-Hexanone ug/L 40.5J40 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.2J40 98 70-130ND
Acetone ug/L 34.5J40 86 70-130ND
Acetonitrile ug/L 180200 90 70-130ND
Acrolein ug/L 114100 114 70-130ND
Acrylonitrile ug/L 104J100 104 70-130ND
Allyl chloride ug/L 21.320 106 70-130ND
Benzene ug/L 22.520 113 70-148ND
Bromochloromethane ug/L 23.020 115 70-130ND
Bromodichloromethane ug/L 22.620 113 70-130ND
Bromoform ug/L 20.720 103 70-130ND
Bromomethane ug/L 20.220 101 70-130ND
Carbon disulfide ug/L 23.1J20 116 70-130ND
Carbon tetrachloride ug/L 22.920 114 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815882MATRIX SPIKE SAMPLE:
MSSpike
Result
92311078007
Chlorobenzene ug/L 23.520 118 70-146ND
Chloroethane ug/L 21.020 105 70-130ND
Chloroform ug/L 22.120 110 70-130ND
Chloromethane ug/L 18.220 91 70-130ND
Chloroprene ug/L 23.320 117 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 22.820 114 70-130ND
Dibromochloromethane ug/L 21.120 105 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Dichlorodifluoromethane ug/L 13.3 M1206670-130ND
Ethyl methacrylate ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 22.820 114 70-130ND
Hexachloro-1,3-butadiene ug/L 24.620 123 70-130ND
Iodomethane ug/L 43.440 108 70-130ND
Isobutanol ug/L 366400 91 70-130ND
Methacrylonitrile ug/L 216200 108 70-130ND
Methyl methacrylate ug/L 21.1J20 105 70-130ND
Methylene Chloride ug/L 19.820 99 70-130ND
Naphthalene ug/L 20.420 102 70-130ND
Propionitrile ug/L 200200 100 70-130ND
Styrene ug/L 25.020 125 70-130ND
Tetrachloroethene ug/L 21.820 109 70-130ND
Toluene ug/L 21.920 109 70-155ND
trans-1,2-Dichloroethene ug/L 23.320 116 70-130ND
trans-1,3-Dichloropropene ug/L 21.720 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.6J20 98 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 22.320 111 70-130ND
Vinyl acetate ug/L 42.8J40 107 70-130ND
Vinyl chloride ug/L 19.420 97 70-130ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078006
1815881SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078006
1815881SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.24J 300.34J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L 0.28J 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078006
1815881SAMPLE DUPLICATE:
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 4102
4-Bromofluorobenzene (S)%103 2101
Toluene-d8 (S)%109 5103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327101
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1812393
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 09/02/16 17:420.050
4,4'-DDE ug/L ND 0.10 09/02/16 17:420.050
4,4'-DDT ug/L ND 0.10 09/02/16 17:420.050
Aldrin ug/L ND 0.050 09/02/16 17:420.050
alpha-BHC ug/L ND 0.050 09/02/16 17:420.050
beta-BHC ug/L ND 0.050 09/02/16 17:420.050
Chlordane (Technical)ug/L ND 0.50 09/02/16 17:420.20
delta-BHC ug/L ND 0.050 09/02/16 17:420.050
Dieldrin ug/L ND 0.075 09/02/16 17:420.050
Endosulfan I ug/L ND 0.10 09/02/16 17:420.050
Endosulfan II ug/L ND 0.10 09/02/16 17:420.050
Endosulfan sulfate ug/L ND 0.10 09/02/16 17:420.050
Endrin ug/L ND 0.10 09/02/16 17:420.050
Endrin aldehyde ug/L ND 0.10 09/02/16 17:420.050
gamma-BHC (Lindane)ug/L ND 0.050 09/02/16 17:420.050
Heptachlor ug/L ND 0.050 09/02/16 17:420.050
Heptachlor epoxide ug/L ND 0.075 09/02/16 17:420.050
Methoxychlor ug/L ND 1.0 09/02/16 17:420.15
Toxaphene ug/L ND 1.5 09/02/16 17:420.20
Decachlorobiphenyl (S)%70 20-130 09/02/16 17:42
Tetrachloro-m-xylene (S)%81 20-130 09/02/16 17:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812394LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.23.25 93 20-150
4,4'-DDE ug/L 0.21.25 86 20-150
4,4'-DDT ug/L 0.23.25 95 20-150
Aldrin ug/L 0.18.25 71 20-150
alpha-BHC ug/L 0.21.25 86 20-150
beta-BHC ug/L 0.22.25 90 20-150
delta-BHC ug/L 0.23.25 92 20-150
Dieldrin ug/L 0.22.25 89 20-150
Endosulfan I ug/L 0.23.25 92 20-150
Endosulfan II ug/L 0.24.25 96 20-150
Endosulfan sulfate ug/L 0.23.25 95 20-150
Endrin ug/L 0.25.25 99 20-150
Endrin aldehyde ug/L 0.21.25 84 20-150
gamma-BHC (Lindane)ug/L 0.22.25 89 20-150
Heptachlor ug/L 0.21.25 86 20-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 139 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812394LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.22.25 91 20-150
Methoxychlor ug/L 0.81J.74 110 20-150
Decachlorobiphenyl (S)%49 20-130
Tetrachloro-m-xylene (S)%82 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1812395MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738004
4,4'-DDD ug/L 0.29.25 117 20-150ND
4,4'-DDE ug/L 0.18.25 73 20-150ND
4,4'-DDT ug/L 0.49 M3.25 199 20-150ND
Aldrin ug/L 0.18.25 72 20-150ND
alpha-BHC ug/L 0.20.25 81 20-150ND
beta-BHC ug/L 0.23.25 94 20-150ND
delta-BHC ug/L 0.18.25 72 20-150ND
Dieldrin ug/L 0.21.25 83 20-150ND
Endosulfan I ug/L 0.18.25 74 20-150ND
Endosulfan II ug/L 0.37.25 149 20-150ND
Endosulfan sulfate ug/L 0.98 M3.25 395 20-150ND
Endrin ug/L 0.28.25 115 20-150ND
Endrin aldehyde ug/L 0.53 M3.25 214 20-150ND
gamma-BHC (Lindane)ug/L 0.20.25 81 20-150ND
Heptachlor ug/L 0.18.25 71 20-150ND
Heptachlor epoxide ug/L 0.19.25 77 20-150ND
Methoxychlor ug/L 1.5 M3.74 208 20-150ND
Decachlorobiphenyl (S)%S5193020-130
Tetrachloro-m-xylene (S)%87 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738005
1812396SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738005
1812396SAMPLE DUPLICATE:
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%60 563
Tetrachloro-m-xylene (S)%61 3889
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327585
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815055
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 09/07/16 21:310.050
4,4'-DDE ug/L ND 0.10 09/07/16 21:310.050
4,4'-DDT ug/L ND 0.10 09/07/16 21:310.050
Aldrin ug/L ND 0.050 09/07/16 21:310.050
alpha-BHC ug/L ND 0.050 09/07/16 21:310.050
beta-BHC ug/L ND 0.050 09/07/16 21:310.050
Chlordane (Technical)ug/L ND 0.50 09/07/16 21:310.20
delta-BHC ug/L ND 0.050 09/07/16 21:310.050
Dieldrin ug/L ND 0.075 09/07/16 21:310.050
Endosulfan I ug/L ND 0.10 09/07/16 21:310.050
Endosulfan II ug/L ND 0.10 09/07/16 21:310.050
Endosulfan sulfate ug/L ND 0.10 09/07/16 21:310.050
Endrin ug/L ND 0.10 09/07/16 21:310.050
Endrin aldehyde ug/L ND 0.10 09/07/16 21:310.050
gamma-BHC (Lindane)ug/L ND 0.050 09/07/16 21:310.050
Heptachlor ug/L ND 0.050 09/07/16 21:310.050
Heptachlor epoxide ug/L ND 0.075 09/07/16 21:310.050
Methoxychlor ug/L ND 1.0 09/07/16 21:310.15
Toxaphene ug/L ND 1.5 09/07/16 21:310.20
Decachlorobiphenyl (S)%67 20-130 09/07/16 21:31
Tetrachloro-m-xylene (S)%63 20-130 09/07/16 21:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815056LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.19.25 77 20-150
4,4'-DDE ug/L 0.18.25 72 20-150
4,4'-DDT ug/L 0.20.25 80 20-150
Aldrin ug/L 0.14.25 55 20-150
alpha-BHC ug/L 0.17.25 70 20-150
beta-BHC ug/L 0.18.25 74 20-150
delta-BHC ug/L 0.18.25 75 20-150
Dieldrin ug/L 0.17.25 69 20-150
Endosulfan I ug/L 0.18.25 75 20-150
Endosulfan II ug/L 0.20.25 81 20-150
Endosulfan sulfate ug/L 0.20.25 82 20-150
Endrin ug/L 0.18.25 72 20-150
Endrin aldehyde ug/L 0.18.25 74 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815056LABORATORY CONTROL SAMPLE:
LCSSpike
gamma-BHC (Lindane)ug/L 0.18.25 72 20-150
Heptachlor ug/L 0.16.25 66 20-150
Heptachlor epoxide ug/L 0.18.25 72 20-150
Methoxychlor ug/L 0.73J.74 98 20-150
Decachlorobiphenyl (S)%61 20-130
Tetrachloro-m-xylene (S)%68 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815057MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738010
4,4'-DDD ug/L 0.15.25 59 20-150ND
4,4'-DDE ug/L 0.15.25 61 20-150ND
4,4'-DDT ug/L 0.15.25 60 20-150ND
Aldrin ug/L 0.14.25 57 20-150ND
alpha-BHC ug/L 0.17.25 68 20-150ND
beta-BHC ug/L 0.18.25 71 20-150ND
delta-BHC ug/L 0.18.25 73 20-150ND
Dieldrin ug/L 0.16.25 63 20-150ND
Endosulfan I ug/L 0.17.25 70 20-150ND
Endosulfan II ug/L 0.17.25 69 20-150ND
Endosulfan sulfate ug/L 0.17.25 68 20-150ND
Endrin ug/L 0.18.25 73 20-150ND
Endrin aldehyde ug/L 0.15.25 61 20-150ND
gamma-BHC (Lindane)ug/L 0.18.25 71 20-150ND
Heptachlor ug/L 0.18.25 73 20-150ND
Heptachlor epoxide ug/L 0.18.25 74 20-150ND
Methoxychlor ug/L 0.57J.74 77 20-150ND
Decachlorobiphenyl (S)%37 20-130
Tetrachloro-m-xylene (S)%69 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738011
1815058SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738011
1815058SAMPLE DUPLICATE:
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%62 261
Tetrachloro-m-xylene (S)%70 675
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327100
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1812389
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 09/02/16 18:540.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 09/02/16 18:540.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 09/02/16 18:540.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 09/02/16 18:540.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 09/02/16 18:540.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 09/02/16 18:540.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 09/02/16 18:540.50
Decachlorobiphenyl (S)%66 10-132 09/02/16 18:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812390LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 3.05 61 50-150
PCB-1260 (Aroclor 1260)ug/L 3.35 66 50-150
Decachlorobiphenyl (S)%41 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1812391MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738004
PCB-1016 (Aroclor 1016)ug/L 3.25 64 50-150ND
PCB-1260 (Aroclor 1260)ug/L 3.65 72 50-150ND
Decachlorobiphenyl (S)%70 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738005
1812392SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%57 459
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327587
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815061
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 09/07/16 22:500.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 09/07/16 22:500.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 09/07/16 22:500.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 09/07/16 22:500.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 09/07/16 22:500.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 09/07/16 22:500.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 09/07/16 22:500.50
Decachlorobiphenyl (S)%64 10-132 09/07/16 22:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815062LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 4.55 89 50-150
PCB-1260 (Aroclor 1260)ug/L 5.15 102 50-150
Decachlorobiphenyl (S)%65 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815063MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738016
PCB-1016 (Aroclor 1016)ug/L 5.05 99 50-150ND
PCB-1260 (Aroclor 1260)ug/L 4.85 95 50-150ND
Decachlorobiphenyl (S)%84 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738017
1815064SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%71 568
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
318664
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1693396
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 09/02/16 23:470.042
2,4,5-TP (Silvex)ug/L ND 0.19 09/02/16 23:470.049
2,4-D ug/L ND 0.94 09/02/16 23:470.22
2,4-DB ug/L ND 1.9 09/02/16 23:470.51
Bentazon ug/L ND 0.094 09/02/16 23:470.047
Dalapon ug/L ND 0.91 09/02/16 23:470.43
Dicamba ug/L ND 0.094 09/02/16 23:470.030
Dichlorprop ug/L ND 0.65 09/02/16 23:470.19
Dinoseb ug/L ND 0.19 09/02/16 23:470.057
Pentachlorophenol ug/L ND 0.028 09/02/16 23:470.017
Picloram ug/L ND 0.094 09/02/16 23:470.019
2,4-DCAA (S)%84 39-139 09/02/16 23:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1693397LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.11.2 90 37-133
2,4,5-TP (Silvex)ug/L 1.01.2 87 53-134
2,4-D ug/L 5.16 85 35-124
2,4-DB ug/L 11.012 92 31-132
Bentazon ug/L 0.62.6 103 51-125
Dalapon ug/L 5.26 87 10-122
Dicamba ug/L 0.52.6 86 44-125
Dichlorprop ug/L 3.64.2 87 70-130
Dinoseb ug/L 0.971.2 81 13-116
Pentachlorophenol ug/L 0.17.18 94 39-170
Picloram ug/L 0.58.6 97 10-127
2,4-DCAA (S)%81 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1693720MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738002
1693721
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 2.4 81 37-13391 12 402.4ND 1.9 2.2
2,4,5-TP (Silvex)ug/L 2.4 78 53-13488 12 402.4ND 1.9 2.1
2,4-D ug/L 12 77 35-12487 12 4012ND9.3 10.5
2,4-DB ug/L 24 80 31-13291 13 4024ND19.3 21.9
Bentazon ug/L 1.2 87 51-12597 11 401.2ND 1.0 1.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1693720MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738002
1693721
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dalapon ug/L 12 94 10-12298 4 4012ND11.2 11.7
Dicamba ug/L 1.2 78 44-12588 11 401.2ND 0.94 1.1
Dichlorprop ug/L 8.4 81 70-13090 11 408.4ND 6.8 7.6
Dinoseb ug/L M12.4 0 13-1160 402.4ND ND ND
Pentachlorophenol ug/L .36 75 39-17082 9 40.36ND 0.27 0.30
Picloram ug/L 1.2 87 10-127101 15 401.2ND 1.0 1.2
2,4-DCAA (S)%76 39-13986 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
318978
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1695159
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 09/08/16 06:570.042
2,4,5-TP (Silvex)ug/L ND 0.19 09/08/16 06:570.049
2,4-D ug/L ND 0.94 09/08/16 06:570.22
2,4-DB ug/L ND 1.9 09/08/16 06:570.51
Bentazon ug/L ND 0.094 09/08/16 06:570.047
Dalapon ug/L ND 0.91 09/08/16 06:570.43
Dicamba ug/L ND 0.094 09/08/16 06:570.030
Dichlorprop ug/L ND 0.65 09/08/16 06:570.19
Dinoseb ug/L ND 0.19 09/08/16 06:570.057
Pentachlorophenol ug/L ND 0.028 09/08/16 06:570.017
Picloram ug/L ND 0.094 09/08/16 06:570.019
2,4-DCAA (S)%79 39-139 09/08/16 06:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1695160LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.21.2 103 37-133
2,4,5-TP (Silvex)ug/L 1.11.2 94 53-134
2,4-D ug/L 5.46 91 35-124
2,4-DB ug/L 13.512 112 31-132
Bentazon ug/L 0.50.6 83 51-125
Dalapon ug/L 7.7 L0612910-122
Dicamba ug/L 0.55.6 92 44-125
Dichlorprop ug/L 4.04.2 96 70-130
Dinoseb ug/L 0.871.2 73 13-116
Pentachlorophenol ug/L 0.18.18 101 39-170
Picloram ug/L 0.60.6 100 10-127
2,4-DCAA (S)%89 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1695291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738010
1695292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 2.4 106 37-13399 6 402.4ND 2.5 2.4
2,4,5-TP (Silvex)ug/L 2.4 97 53-13492 5 402.4ND 2.3 2.2
2,4-D ug/L 12 93 35-12489 4 4012ND11.2 10.7
2,4-DB ug/L 24 104 31-13296 8 4024ND25.0 23.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1695291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738010
1695292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bentazon ug/L 1.2 82 51-12579 3 401.2ND 0.98 0.95
Dalapon ug/L M01212310-122129 4 4012ND14.8 15.4
Dicamba ug/L 1.2 93 44-12589 4 401.2ND 1.1 1.1
Dichlorprop ug/L 8.4 95 70-13092 3 408.4ND 8.0 7.7
Dinoseb ug/L 2.4 53 13-11672 30 402.4ND 1.3 1.7
Pentachlorophenol ug/L .36 96 39-17096 0 40.36ND 0.34 0.34
Picloram ug/L 1.2 105 10-12793 12 401.2ND 1.3 1.1
2,4-DCAA (S)%93 39-13987 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327270
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813342
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738006
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 09/14/16 15:581.7
1,3,5-Trinitrobenzene ug/L ND 10.0 09/14/16 15:581.1
1,3-Dinitrobenzene ug/L ND 20.0 09/14/16 15:581.5
1,4-Naphthoquinone ug/L ND 10.0 09/14/16 15:581.8
1-Naphthalenamine ug/L ND 10.0 09/14/16 15:580.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/14/16 15:581.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 09/14/16 15:582.3
2,4,5-Trichlorophenol ug/L ND 10.0 09/14/16 15:582.2
2,4,6-Trichlorophenol ug/L ND 10.0 09/14/16 15:581.9
2,4-Dichlorophenol ug/L ND 10.0 09/14/16 15:581.7
2,4-Dimethylphenol ug/L ND 10.0 09/14/16 15:582.2
2,4-Dinitrophenol ug/L ND 50.0 09/14/16 15:586.5
2,4-Dinitrotoluene ug/L ND 10.0 09/14/16 15:581.2
2,6-Dichlorophenol ug/L ND 10.0 09/14/16 15:581.8
2,6-Dinitrotoluene ug/L ND 10.0 09/14/16 15:581.7
2-Acetylaminofluorene ug/L 7.1J 20.0 09/14/16 15:580.84
2-Chloronaphthalene ug/L ND 10.0 09/14/16 15:582.2
2-Chlorophenol ug/L ND 10.0 09/14/16 15:581.5
2-Methylnaphthalene ug/L ND 10.0 09/14/16 15:580.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/14/16 15:581.7
2-Naphthalenamine ug/L ND 10.0 09/14/16 15:580.98
2-Nitroaniline ug/L ND 50.0 09/14/16 15:582.8
2-Nitrophenol ug/L ND 10.0 09/14/16 15:581.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/14/16 15:581.7
3,3'-Dichlorobenzidine ug/L ND 20.0 09/14/16 15:581.4
3,3'-Dimethylbenzidine ug/L ND 10.0 09/14/16 15:582.1
3-Methylcholanthrene ug/L ND 10.0 09/14/16 15:580.82
3-Nitroaniline ug/L ND 50.0 09/14/16 15:582.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 09/14/16 15:581.7
4-Aminobiphenyl ug/L ND 20.0 09/14/16 15:580.92
4-Bromophenylphenyl ether ug/L ND 10.0 09/14/16 15:581.3
4-Chloro-3-methylphenol ug/L ND 20.0 09/14/16 15:584.2
4-Chloroaniline ug/L ND 20.0 09/14/16 15:583.4
4-Chlorophenylphenyl ether ug/L ND 10.0 09/14/16 15:582.1
4-Nitroaniline ug/L ND 20.0 09/14/16 15:582.5
4-Nitrophenol ug/L ND 50.0 09/14/16 15:585.8
5-Nitro-o-toluidine ug/L ND 10.0 09/14/16 15:581.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 09/14/16 15:580.77
Acenaphthene ug/L ND 10.0 09/14/16 15:580.25
Acenaphthylene ug/L ND 10.0 09/14/16 15:580.21
Acetophenone ug/L ND 10.0 09/14/16 15:582.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813342
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738006
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 09/14/16 15:580.14
Benzo(a)anthracene ug/L ND 10.0 09/14/16 15:580.33
Benzo(a)pyrene ug/L ND 10.0 09/14/16 15:580.30
Benzo(b)fluoranthene ug/L ND 10.0 09/14/16 15:580.28
Benzo(g,h,i)perylene ug/L ND 10.0 09/14/16 15:580.38
Benzo(k)fluoranthene ug/L ND 10.0 09/14/16 15:580.43
Benzyl alcohol ug/L ND 20.0 09/14/16 15:583.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/14/16 15:581.7
bis(2-Chloroethyl) ether ug/L ND 10.0 09/14/16 15:581.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 09/14/16 15:580.85
Butylbenzylphthalate ug/L ND 10.0 09/14/16 15:580.75
Chlorobenzilate ug/L ND 10.0 09/14/16 15:580.72
Chrysene ug/L ND 10.0 09/14/16 15:580.21
Di-n-butylphthalate ug/L ND 10.0 09/14/16 15:581.1
Di-n-octylphthalate ug/L ND 10.0 09/14/16 15:580.86
Diallate ug/L ND 10.0 09/14/16 15:581.3
Dibenz(a,h)anthracene ug/L ND 10.0 09/14/16 15:580.55
Dibenzofuran ug/L ND 10.0 09/14/16 15:581.8
Diethylphthalate ug/L ND 6000 09/14/16 15:581.3
Dimethoate ug/L ND 20.0 09/14/16 15:580.92
Dimethylphthalate ug/L ND 10.0 09/14/16 15:581.5
Diphenylamine ug/L ND 10.0 09/14/16 15:581.3
Disulfoton ug/L ND 10.0 09/14/16 15:581.4
Ethyl methanesulfonate ug/L ND 20.0 09/14/16 15:581.8
Famphur ug/L ND 20.0 09/14/16 15:581.7
Fluoranthene ug/L ND 10.0 09/14/16 15:580.21
Fluorene ug/L ND 10.0 09/14/16 15:580.21
Hexachlorobenzene ug/L ND 10.0 09/14/16 15:581.1
Hexachlorocyclopentadiene ug/L ND 10.0 09/14/16 15:581.8
Hexachloroethane ug/L ND 10.0 09/14/16 15:581.5
Hexachloropropene ug/L ND 10.0 09/14/16 15:581.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/14/16 15:580.29
Isodrin ug/L ND 20.0 09/14/16 15:582.0
Isophorone ug/L ND 10.0 09/14/16 15:581.8
Isosafrole ug/L ND 10.0 09/14/16 15:581.8
Kepone ug/L ND 20.0 09/14/16 15:583.1
Methapyrilene ug/L ND 100 09/14/16 15:582.7
Methyl methanesulfonate ug/L ND 10.0 09/14/16 15:581.3
Methyl parathion ug/L ND 10.0 09/14/16 15:581.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 09/14/16 15:582.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/14/16 15:582.1
N-Nitrosodiethylamine ug/L ND 20.0 09/14/16 15:581.8
N-Nitrosodimethylamine ug/L ND 10.0 09/14/16 15:581.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/14/16 15:581.3
N-Nitrosomethylethylamine ug/L ND 10.0 09/14/16 15:581.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813342
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738006
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 09/14/16 15:581.9
N-Nitrosopyrrolidine ug/L ND 10.0 09/14/16 15:582.5
Nitrobenzene ug/L ND 10.0 09/14/16 15:581.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 09/14/16 15:581.8
O-Toluidine ug/L ND 10.0 09/14/16 15:581.6
P-Dimethylaminoazobenzene ug/L ND 10.0 09/14/16 15:580.35
p-Phenylenediamine ug/L ND 10.0 09/14/16 15:580.96
Parathion (Ethyl parathion)ug/L ND 10.0 09/14/16 15:581.1
Pentachlorobenzene ug/L ND 10.0 09/14/16 15:582.0
Pentachloronitrobenzene ug/L ND 20.0 09/14/16 15:581.0
Pentachlorophenol ug/L ND 25.0 09/14/16 15:582.3
Phenacetin ug/L ND 20.0 09/14/16 15:580.97
Phenanthrene ug/L ND 10.0 09/14/16 15:580.22
Phenol ug/L ND 10.0 09/14/16 15:581.7
Phorate ug/L ND 10.0 09/14/16 15:581.1
Pronamide ug/L ND 10.0 09/14/16 15:580.97
Pyrene ug/L ND 10.0 09/14/16 15:580.19
Safrole ug/L ND 10.0 09/14/16 15:581.5
Thionazin ug/L ND 20.0 09/14/16 15:581.2
2,4,6-Tribromophenol (S)%89 27-110 09/14/16 15:58
2-Fluorobiphenyl (S)%73 27-110 09/14/16 15:58
2-Fluorophenol (S)%47 12-110 09/14/16 15:58
Nitrobenzene-d5 (S)%79 21-110 09/14/16 15:58
Phenol-d6 (S)%33 10-110 09/14/16 15:58
Terphenyl-d14 (S)%92 31-107 09/14/16 15:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813343LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 37.150 74 16-129
1,3,5-Trinitrobenzene ug/L 52.450 105 55-125
1,3-Dinitrobenzene ug/L 49.650 99 30-122
1,4-Naphthoquinone ug/L 45.750 91 31-120
1-Naphthalenamine ug/L 39.750 79 37-126
2,2'-Oxybis(1-chloropropane)ug/L 53.350 107 18-120
2,3,4,6-Tetrachlorophenol ug/L 63.950 128 54-276
2,4,5-Trichlorophenol ug/L 48.450 97 43-113
2,4,6-Trichlorophenol ug/L 49.550 99 42-120
2,4-Dichlorophenol ug/L 49.450 99 30-120
2,4-Dimethylphenol ug/L 55.150 110 29-111
2,4-Dinitrophenol ug/L 192250 77 19-132
2,4-Dinitrotoluene ug/L 58.650 117 58-128
2,6-Dichlorophenol ug/L 41.750 83 54-128
2,6-Dinitrotoluene ug/L 56.950 114 54-129
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 153 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813343LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 58.050 116 81-160
2-Chloronaphthalene ug/L 48.850 98 43-117
2-Chlorophenol ug/L 54.550 109 37-120
2-Methylnaphthalene ug/L 48.250 96 33-120
2-Methylphenol(o-Cresol)ug/L 58.250 116 31-120
2-Naphthalenamine ug/L 51.650 103 41-136
2-Nitroaniline ug/L 88.6100 89 48-121
2-Nitrophenol ug/L 49.950 100 25-116
3&4-Methylphenol(m&p Cresol)ug/L 53.650 107 23-120
3,3'-Dichlorobenzidine ug/L 98.2250 39 10-154
3,3'-Dimethylbenzidine ug/L 42.9100 43 10-157
3-Methylcholanthrene ug/L 47.750 95 65-130
3-Nitroaniline ug/L 95.7100 96 43-115
4,6-Dinitro-2-methylphenol ug/L 91.8100 92 44-124
4-Aminobiphenyl ug/L 37.650 75 21-125
4-Bromophenylphenyl ether ug/L 41.650 83 34-113
4-Chloro-3-methylphenol ug/L 102100 102 31-110
4-Chloroaniline ug/L 88.7100 89 20-120
4-Chlorophenylphenyl ether ug/L 48.050 96 34-116
4-Nitroaniline ug/L 108100 108 46-128
4-Nitrophenol ug/L 131250 52 11-120
5-Nitro-o-toluidine ug/L 64.050 128 78-160
7,12-Dimethylbenz(a)anthracene ug/L 42.550 85 47-124
Acenaphthene ug/L 45.250 90 48-114
Acenaphthylene ug/L 45.850 92 48-112
Acetophenone ug/L 62.0 L05012424-120
Anthracene ug/L 44.250 88 57-118
Benzo(a)anthracene ug/L 45.150 90 56-121
Benzo(a)pyrene ug/L 44.050 88 55-127
Benzo(b)fluoranthene ug/L 45.450 91 53-128
Benzo(g,h,i)perylene ug/L 49.150 98 54-125
Benzo(k)fluoranthene ug/L 41.750 83 51-123
Benzyl alcohol ug/L 111100 111 27-120
bis(2-Chloroethoxy)methane ug/L 47.150 94 32-120
bis(2-Chloroethyl) ether ug/L 51.150 102 33-111
bis(2-Ethylhexyl)phthalate ug/L 47.750 95 50-145
Butylbenzylphthalate ug/L 49.350 99 54-138
Chlorobenzilate ug/L 45.650 91 65-132
Chrysene ug/L 42.950 86 58-127
Di-n-butylphthalate ug/L 48.450 97 56-125
Di-n-octylphthalate ug/L 50.850 102 50-134
Diallate ug/L 42.150 84 47-123
Dibenz(a,h)anthracene ug/L 48.450 97 53-129
Dibenzofuran ug/L 44.050 88 45-120
Diethylphthalate ug/L 48.9J50 98 53-120
Dimethoate ug/L 51.550 103 57-139
Dimethylphthalate ug/L 44.950 90 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 154 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813343LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 37.150 74 42-120
Disulfoton ug/L 41.750 83 49-156
Ethyl methanesulfonate ug/L 52.450 105 43-120
Famphur ug/L 110100 110 40-160
Fluoranthene ug/L 52.650 105 57-125
Fluorene ug/L 49.350 99 53-118
Hexachlorobenzene ug/L 42.550 85 49-116
Hexachlorocyclopentadiene ug/L 36.750 73 26-158
Hexachloroethane ug/L 34.550 69 30-114
Hexachloropropene ug/L 30.950 62 13-137
Indeno(1,2,3-cd)pyrene ug/L 48.250 96 55-128
Isodrin ug/L 43.950 88 68-129
Isophorone ug/L 50.750 101 31-118
Isosafrole ug/L 39.950 80 48-107
Kepone ug/L 90.0100 90 10-124
Methapyrilene ug/L 35.2J50 70 40-160
Methyl methanesulfonate ug/L 36.350 73 25-114
Methyl parathion ug/L 52.550 105 58-137
N-Nitroso-di-n-butylamine ug/L 46.250 92 36-115
N-Nitroso-di-n-propylamine ug/L 67.3 L05013532-119
N-Nitrosodiethylamine ug/L 58.2 L05011647-115
N-Nitrosodimethylamine ug/L 18.450 37 13-120
N-Nitrosodiphenylamine ug/L 37.150 74 43-120
N-Nitrosomethylethylamine ug/L 43.950 88 39-120
N-Nitrosopiperidine ug/L 48.050 96 43-113
N-Nitrosopyrrolidine ug/L 73.9 L05014832-110
Nitrobenzene ug/L 45.550 91 33-110
O,O,O-Triethylphosphorothioate ug/L 41.150 82 51-127
O-Toluidine ug/L 59.950 120 27-120
P-Dimethylaminoazobenzene ug/L 23.0100 23 10-120
p-Phenylenediamine ug/L 64.350 129 72-143
Parathion (Ethyl parathion)ug/L 52.350 105 56-140
Pentachlorobenzene ug/L 40.550 81 30-137
Pentachloronitrobenzene ug/L 50.350 101 70-124
Pentachlorophenol ug/L 112250 45 10-137
Phenacetin ug/L 51.450 103 60-130
Phenanthrene ug/L 44.050 88 57-117
Phenol ug/L 27.350 55 10-120
Phorate ug/L 43.950 88 55-126
Pronamide ug/L 44.350 89 75-124
Pyrene ug/L 40.850 82 55-122
Safrole ug/L 42.150 84 41-120
Thionazin ug/L 48.650 97 63-137
2,4,6-Tribromophenol (S)%93 27-110
2-Fluorobiphenyl (S)%78 27-110
2-Fluorophenol (S)%56 12-110
Nitrobenzene-d5 (S)%82 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 155 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813343LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%52 10-110
Terphenyl-d14 (S)%80 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1813344MATRIX SPIKE SAMPLE:
MSSpike
Result
92310856002
1,2,4,5-Tetrachlorobenzene ug/L 39.550 79 50-150ND
1,3,5-Trinitrobenzene ug/L 55.250 110 50-150ND
1,3-Dinitrobenzene ug/L 53.650 107 50-150ND
1,4-Naphthoquinone ug/L 48.750 97 50-150ND
1-Naphthalenamine ug/L 42.550 85 50-150ND
2,2'-Oxybis(1-chloropropane)ug/L 52.050 104 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 64.450 129 50-150ND
2,4,5-Trichlorophenol ug/L 51.050 102 19-105ND
2,4,6-Trichlorophenol ug/L 52.950 106 13-108ND
2,4-Dichlorophenol ug/L 50.450 101 29-111ND
2,4-Dimethylphenol ug/L 56.5 M15011321-103ND
2,4-Dinitrophenol ug/L 182250 73 10-109ND
2,4-Dinitrotoluene ug/L 58.4 M15011727-104ND
2,6-Dichlorophenol ug/L 43.050 86 50-150ND
2,6-Dinitrotoluene ug/L 58.9 M15011828-101ND
2-Acetylaminofluorene ug/L 60.850 107 50-1507.1J
2-Chloronaphthalene ug/L 50.850 102 14-102ND
2-Chlorophenol ug/L 50.750 101 16-110ND
2-Methylnaphthalene ug/L 48.950 98 13-110ND
2-Methylphenol(o-Cresol)ug/L 54.150 108 19-110ND
2-Naphthalenamine ug/L 53.650 107 50-150ND
2-Nitroaniline ug/L 91.8100 92 26-103ND
2-Nitrophenol ug/L 52.150 104 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 50.450 101 20-110ND
3,3'-Dichlorobenzidine ug/L 103250 41 25-112ND
3,3'-Dimethylbenzidine ug/L 83.6100 84 50-150ND
3-Methylcholanthrene ug/L 50.650 101 50-150ND
3-Nitroaniline ug/L 96.7100 97 29-110ND
4,6-Dinitro-2-methylphenol ug/L 99.5100 100 10-117ND
4-Aminobiphenyl ug/L 48.250 96 50-150ND
4-Bromophenylphenyl ether ug/L 46.050 92 20-105ND
4-Chloro-3-methylphenol ug/L 107100 107 22-110ND
4-Chloroaniline ug/L 92.7100 93 20-100ND
4-Chlorophenylphenyl ether ug/L 49.350 99 19-102ND
4-Nitroaniline ug/L 106100 106 29-110ND
4-Nitrophenol ug/L 130250 52 10-110ND
5-Nitro-o-toluidine ug/L 65.450 131 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 45.550 91 50-150ND
Acenaphthene ug/L 46.750 93 17-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 156 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1813344MATRIX SPIKE SAMPLE:
MSSpike
Result
92310856002
Acenaphthylene ug/L 47.550 95 21-100ND
Acetophenone ug/L 57.350 115 50-150ND
Anthracene ug/L 46.550 93 24-109ND
Benzo(a)anthracene ug/L 46.350 93 22-117ND
Benzo(a)pyrene ug/L 46.350 93 23-104ND
Benzo(b)fluoranthene ug/L 48.750 97 23-103ND
Benzo(g,h,i)perylene ug/L 50.250 100 18-111ND
Benzo(k)fluoranthene ug/L 43.550 87 22-113ND
Benzyl alcohol ug/L 103 M110010319-101ND
bis(2-Chloroethoxy)methane ug/L 48.150 96 22-110ND
bis(2-Chloroethyl) ether ug/L 48.350 97 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 49.550 99 23-102ND
Butylbenzylphthalate ug/L 51.250 102 25-110ND
Chlorobenzilate ug/L 48.150 96 50-150ND
Chrysene ug/L 44.850 90 23-115ND
Di-n-butylphthalate ug/L 50.150 100 26-110ND
Di-n-octylphthalate ug/L 52.050 104 22-110ND
Diallate ug/L 47.350 95 50-150ND
Dibenz(a,h)anthracene ug/L 50.250 100 21-112ND
Dibenzofuran ug/L 44.750 89 19-102ND
Diethylphthalate ug/L 49.2J50 98 29-110ND
Dimethoate ug/L 54.850 110 50-150ND
Dimethylphthalate ug/L 46.450 93 27-110ND
Diphenylamine ug/L 41.150 82 50-150ND
Disulfoton ug/L 44.950 90 50-150ND
Ethyl methanesulfonate ug/L 50.850 102 50-150ND
Famphur ug/L 81.6100 82 50-150ND
Fluoranthene ug/L 53.050 106 23-112ND
Fluorene ug/L 50.150 100 22-104ND
Hexachlorobenzene ug/L 47.250 94 21-116ND
Hexachlorocyclopentadiene ug/L 41.350 83 10-110ND
Hexachloroethane ug/L 37.650 75 10-110ND
Hexachloropropene ug/L 33.650 67 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 49.850 100 20-113ND
Isodrin ug/L 46.950 94 50-150ND
Isophorone ug/L 52.350 105 50-150ND
Isosafrole ug/L 42.950 86 50-150ND
Kepone ug/L 127100 127 50-150ND
Methapyrilene ug/L 56.1J50 112 50-150ND
Methyl methanesulfonate ug/L 35.250 70 50-150ND
Methyl parathion ug/L 54.550 109 50-150ND
N-Nitroso-di-n-butylamine ug/L 52.150 104 50-150ND
N-Nitroso-di-n-propylamine ug/L 62.3 M05012521-105ND
N-Nitrosodiethylamine ug/L 55.050 110 50-150ND
N-Nitrosodimethylamine ug/L 18.650 37 10-110ND
N-Nitrosodiphenylamine ug/L 41.150 82 23-107ND
N-Nitrosomethylethylamine ug/L 43.450 87 50-150ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 157 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1813344MATRIX SPIKE SAMPLE:
MSSpike
Result
92310856002
N-Nitrosopiperidine ug/L 51.350 103 50-150ND
N-Nitrosopyrrolidine ug/L 72.850 146 50-150ND
Nitrobenzene ug/L 46.950 94 20-110ND
O,O,O-Triethylphosphorothioate ug/L 41.950 84 50-150ND
O-Toluidine ug/L 55.650 111 50-150ND
P-Dimethylaminoazobenzene ug/L 24.6 M11002550-150ND
p-Phenylenediamine ug/L 62.750 125 50-150ND
Parathion (Ethyl parathion)ug/L 52.950 106 50-150ND
Pentachlorobenzene ug/L 42.650 85 50-150ND
Pentachloronitrobenzene ug/L 54.550 109 50-150ND
Pentachlorophenol ug/L 118250 47 10-118ND
Phenacetin ug/L 55.050 110 50-150ND
Phenanthrene ug/L 46.550 93 24-106ND
Phenol ug/L 25.550 51 12-110ND
Phorate ug/L 48.350 97 50-150ND
Pronamide ug/L 46.450 93 50-150ND
Pyrene ug/L 43.450 87 24-114ND
Safrole ug/L 43.850 88 50-150ND
Thionazin ug/L 49.650 99 50-150ND
2,4,6-Tribromophenol (S)%101 27-110
2-Fluorobiphenyl (S)%82 27-110
2-Fluorophenol (S)%53 12-110
Nitrobenzene-d5 (S)%86 21-110
Phenol-d6 (S)%48 10-110
Terphenyl-d14 (S)%86 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310856003
1813345SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 307.1J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Huntersville, NC 28078
[phone]
Page 158 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310856003
1813345SAMPLE DUPLICATE:
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 159 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310856003
1813345SAMPLE DUPLICATE:
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%87 14100
2-Fluorobiphenyl (S)%78 884
2-Fluorophenol (S)%43 1550
Nitrobenzene-d5 (S)%76 1387
Phenol-d6 (S)%33 735
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 160 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310856003
1813345SAMPLE DUPLICATE:
Terphenyl-d14 (S)%86 288
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 161 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327459
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814546
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 09/14/16 16:261.7
1,3,5-Trinitrobenzene ug/L ND 10.0 09/14/16 16:261.1
1,3-Dinitrobenzene ug/L ND 20.0 09/14/16 16:261.5
1,4-Naphthoquinone ug/L ND 10.0 09/14/16 16:261.8
1-Naphthalenamine ug/L ND 10.0 09/14/16 16:260.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/14/16 16:261.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 09/14/16 16:262.3
2,4,5-Trichlorophenol ug/L ND 10.0 09/14/16 16:262.2
2,4,6-Trichlorophenol ug/L ND 10.0 09/14/16 16:261.9
2,4-Dichlorophenol ug/L ND 10.0 09/14/16 16:261.7
2,4-Dimethylphenol ug/L ND 10.0 09/14/16 16:262.2
2,4-Dinitrophenol ug/L ND 50.0 09/14/16 16:266.5
2,4-Dinitrotoluene ug/L ND 10.0 09/14/16 16:261.2
2,6-Dichlorophenol ug/L ND 10.0 09/14/16 16:261.8
2,6-Dinitrotoluene ug/L ND 10.0 09/14/16 16:261.7
2-Acetylaminofluorene ug/L 7.1J 20.0 09/14/16 16:260.84
2-Chloronaphthalene ug/L ND 10.0 09/14/16 16:262.2
2-Chlorophenol ug/L ND 10.0 09/14/16 16:261.5
2-Methylnaphthalene ug/L ND 10.0 09/14/16 16:260.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/14/16 16:261.7
2-Naphthalenamine ug/L ND 10.0 09/14/16 16:260.98
2-Nitroaniline ug/L ND 50.0 09/14/16 16:262.8
2-Nitrophenol ug/L ND 10.0 09/14/16 16:261.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/14/16 16:261.7
3,3'-Dichlorobenzidine ug/L ND 20.0 09/14/16 16:261.4
3,3'-Dimethylbenzidine ug/L ND 10.0 09/14/16 16:262.1
3-Methylcholanthrene ug/L ND 10.0 09/14/16 16:260.82
3-Nitroaniline ug/L ND 50.0 09/14/16 16:262.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 09/14/16 16:261.7
4-Aminobiphenyl ug/L ND 20.0 09/14/16 16:260.92
4-Bromophenylphenyl ether ug/L ND 10.0 09/14/16 16:261.3
4-Chloro-3-methylphenol ug/L ND 20.0 09/14/16 16:264.2
4-Chloroaniline ug/L ND 20.0 09/14/16 16:263.4
4-Chlorophenylphenyl ether ug/L ND 10.0 09/14/16 16:262.1
4-Nitroaniline ug/L ND 20.0 09/14/16 16:262.5
4-Nitrophenol ug/L ND 50.0 09/14/16 16:265.8
5-Nitro-o-toluidine ug/L ND 10.0 09/14/16 16:261.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 09/14/16 16:260.77
Acenaphthene ug/L ND 10.0 09/14/16 16:260.25
Acenaphthylene ug/L ND 10.0 09/14/16 16:260.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 162 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814546
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
Acetophenone ug/L ND 10.0 09/14/16 16:262.0
Anthracene ug/L ND 10.0 09/14/16 16:260.14
Benzo(a)anthracene ug/L ND 10.0 09/14/16 16:260.33
Benzo(a)pyrene ug/L ND 10.0 09/14/16 16:260.30
Benzo(b)fluoranthene ug/L ND 10.0 09/14/16 16:260.28
Benzo(g,h,i)perylene ug/L ND 10.0 09/14/16 16:260.38
Benzo(k)fluoranthene ug/L ND 10.0 09/14/16 16:260.43
Benzyl alcohol ug/L ND 20.0 09/14/16 16:263.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/14/16 16:261.7
bis(2-Chloroethyl) ether ug/L ND 10.0 09/14/16 16:261.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 09/14/16 16:260.85
Butylbenzylphthalate ug/L ND 10.0 09/14/16 16:260.75
Chlorobenzilate ug/L ND 10.0 09/14/16 16:260.72
Chrysene ug/L ND 10.0 09/14/16 16:260.21
Di-n-butylphthalate ug/L ND 10.0 09/14/16 16:261.1
Di-n-octylphthalate ug/L ND 10.0 09/14/16 16:260.86
Diallate ug/L ND 10.0 09/14/16 16:261.3
Dibenz(a,h)anthracene ug/L ND 10.0 09/14/16 16:260.55
Dibenzofuran ug/L ND 10.0 09/14/16 16:261.8
Diethylphthalate ug/L ND 6000 09/14/16 16:261.3
Dimethoate ug/L ND 20.0 09/14/16 16:260.92
Dimethylphthalate ug/L ND 10.0 09/14/16 16:261.5
Diphenylamine ug/L ND 10.0 09/14/16 16:261.3
Disulfoton ug/L ND 10.0 09/14/16 16:261.4
Ethyl methanesulfonate ug/L ND 20.0 09/14/16 16:261.8
Famphur ug/L ND 20.0 09/14/16 16:261.7
Fluoranthene ug/L ND 10.0 09/14/16 16:260.21
Fluorene ug/L ND 10.0 09/14/16 16:260.21
Hexachlorobenzene ug/L ND 10.0 09/14/16 16:261.1
Hexachlorocyclopentadiene ug/L ND 10.0 09/14/16 16:261.8
Hexachloroethane ug/L ND 10.0 09/14/16 16:261.5
Hexachloropropene ug/L ND 10.0 09/14/16 16:261.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/14/16 16:260.29
Isodrin ug/L ND 20.0 09/14/16 16:262.0
Isophorone ug/L ND 10.0 09/14/16 16:261.8
Isosafrole ug/L ND 10.0 09/14/16 16:261.8
Kepone ug/L ND 20.0 09/14/16 16:263.1
Methapyrilene ug/L ND 100 09/14/16 16:262.7
Methyl methanesulfonate ug/L ND 10.0 09/14/16 16:261.3
Methyl parathion ug/L ND 10.0 09/14/16 16:261.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 09/14/16 16:262.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/14/16 16:262.1
N-Nitrosodiethylamine ug/L ND 20.0 09/14/16 16:261.8
N-Nitrosodimethylamine ug/L ND 10.0 09/14/16 16:261.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/14/16 16:261.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 163 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814546
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
N-Nitrosomethylethylamine ug/L ND 10.0 09/14/16 16:261.8
N-Nitrosopiperidine ug/L ND 20.0 09/14/16 16:261.9
N-Nitrosopyrrolidine ug/L ND 10.0 09/14/16 16:262.5
Nitrobenzene ug/L ND 10.0 09/14/16 16:261.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 09/14/16 16:261.8
O-Toluidine ug/L ND 10.0 09/14/16 16:261.6
P-Dimethylaminoazobenzene ug/L ND 10.0 09/14/16 16:260.35
p-Phenylenediamine ug/L ND 10.0 09/14/16 16:260.96
Parathion (Ethyl parathion)ug/L ND 10.0 09/14/16 16:261.1
Pentachlorobenzene ug/L ND 10.0 09/14/16 16:262.0
Pentachloronitrobenzene ug/L ND 20.0 09/14/16 16:261.0
Pentachlorophenol ug/L ND 25.0 09/14/16 16:262.3
Phenacetin ug/L ND 20.0 09/14/16 16:260.97
Phenanthrene ug/L ND 10.0 09/14/16 16:260.22
Phenol ug/L ND 10.0 09/14/16 16:261.7
Phorate ug/L ND 10.0 09/14/16 16:261.1
Pronamide ug/L ND 10.0 09/14/16 16:260.97
Pyrene ug/L ND 10.0 09/14/16 16:260.19
Safrole ug/L ND 10.0 09/14/16 16:261.5
Thionazin ug/L ND 20.0 09/14/16 16:261.2
2,4,6-Tribromophenol (S)%88 27-110 09/14/16 16:26
2-Fluorobiphenyl (S)%70 27-110 09/14/16 16:26
2-Fluorophenol (S)%45 12-110 09/14/16 16:26
Nitrobenzene-d5 (S)%77 21-110 09/14/16 16:26
Phenol-d6 (S)%33 10-110 09/14/16 16:26
Terphenyl-d14 (S)%89 31-107 09/14/16 16:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 38.650 77 16-129
1,3,5-Trinitrobenzene ug/L 53.950 108 55-125
1,3-Dinitrobenzene ug/L 54.250 108 30-122
1,4-Naphthoquinone ug/L 49.050 98 31-120
1-Naphthalenamine ug/L 43.450 87 37-126
2,2'-Oxybis(1-chloropropane)ug/L 38.450 77 18-120
2,3,4,6-Tetrachlorophenol ug/L 11850 237 54-276
2,4,5-Trichlorophenol ug/L 47.950 96 43-113
2,4,6-Trichlorophenol ug/L 48.450 97 42-120
2,4-Dichlorophenol ug/L 48.850 98 30-120
2,4-Dimethylphenol ug/L 44.550 89 29-111
2,4-Dinitrophenol ug/L 193250 77 19-132
2,4-Dinitrotoluene ug/L 59.750 119 58-128
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 164 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dichlorophenol ug/L 44.950 90 54-128
2,6-Dinitrotoluene ug/L 60.550 121 54-129
2-Acetylaminofluorene ug/L 61.850 124 81-160
2-Chloronaphthalene ug/L 50.150 100 43-117
2-Chlorophenol ug/L 38.450 77 37-120
2-Methylnaphthalene ug/L 46.750 93 33-120
2-Methylphenol(o-Cresol)ug/L 34.650 69 31-120
2-Naphthalenamine ug/L 55.350 111 41-136
2-Nitroaniline ug/L 73.1100 73 48-121
2-Nitrophenol ug/L 47.950 96 25-116
3&4-Methylphenol(m&p Cresol)ug/L 30.050 60 23-120
3,3'-Dichlorobenzidine ug/L 97.0250 39 10-154
3,3'-Dimethylbenzidine ug/L 96.6100 97 10-157
3-Methylcholanthrene ug/L 52.450 105 65-130
3-Nitroaniline ug/L 89.3100 89 43-115
4,6-Dinitro-2-methylphenol ug/L 96.1100 96 44-124
4-Aminobiphenyl ug/L 49.350 99 21-125
4-Bromophenylphenyl ether ug/L 49.050 98 34-113
4-Chloro-3-methylphenol ug/L 98.8100 99 31-110
4-Chloroaniline ug/L 91.2100 91 20-120
4-Chlorophenylphenyl ether ug/L 53.750 107 34-116
4-Nitroaniline ug/L 94.0100 94 46-128
4-Nitrophenol ug/L 108250 43 11-120
5-Nitro-o-toluidine ug/L 65.550 131 78-160
7,12-Dimethylbenz(a)anthracene ug/L 46.550 93 47-124
Acenaphthene ug/L 42.150 84 48-114
Acenaphthylene ug/L 44.050 88 48-112
Acetophenone ug/L 39.950 80 24-120
Anthracene ug/L 43.450 87 57-118
Benzo(a)anthracene ug/L 48.150 96 56-121
Benzo(a)pyrene ug/L 48.450 97 55-127
Benzo(b)fluoranthene ug/L 51.850 104 53-128
Benzo(g,h,i)perylene ug/L 54.250 108 54-125
Benzo(k)fluoranthene ug/L 50.450 101 51-123
Benzyl alcohol ug/L 66.7100 67 27-120
bis(2-Chloroethoxy)methane ug/L 43.850 88 32-120
bis(2-Chloroethyl) ether ug/L 39.950 80 33-111
bis(2-Ethylhexyl)phthalate ug/L 40.850 82 50-145
Butylbenzylphthalate ug/L 42.450 85 54-138
Chlorobenzilate ug/L 49.050 98 65-132
Chrysene ug/L 48.450 97 58-127
Di-n-butylphthalate ug/L 43.050 86 56-125
Di-n-octylphthalate ug/L 37.550 75 50-134
Diallate ug/L 48.850 98 47-123
Dibenz(a,h)anthracene ug/L 54.350 109 53-129
Dibenzofuran ug/L 44.150 88 45-120
Diethylphthalate ug/L 50.8J50 102 53-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 165 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethoate ug/L 52.750 105 57-139
Dimethylphthalate ug/L 49.050 98 55-116
Diphenylamine ug/L 37.750 75 42-120
Disulfoton ug/L 46.650 93 49-156
Ethyl methanesulfonate ug/L 51.950 104 43-120
Famphur ug/L 87.6100 88 40-160
Fluoranthene ug/L 49.350 99 57-125
Fluorene ug/L 49.850 100 53-118
Hexachlorobenzene ug/L 52.650 105 49-116
Hexachlorocyclopentadiene ug/L 31.350 63 26-158
Hexachloroethane ug/L 27.250 54 30-114
Hexachloropropene ug/L 26.750 53 13-137
Indeno(1,2,3-cd)pyrene ug/L 51.650 103 55-128
Isodrin ug/L 47.250 94 68-129
Isophorone ug/L 46.050 92 31-118
Isosafrole ug/L 42.650 85 48-107
Kepone ug/L 91.5100 92 10-124
Methapyrilene ug/L 58.1J50 116 40-160
Methyl methanesulfonate ug/L 34.050 68 25-114
Methyl parathion ug/L 53.850 108 58-137
N-Nitroso-di-n-butylamine ug/L 53.050 106 36-115
N-Nitroso-di-n-propylamine ug/L 35.650 71 32-119
N-Nitrosodiethylamine ug/L 56.550 113 47-115
N-Nitrosodimethylamine ug/L 22.650 45 13-120
N-Nitrosodiphenylamine ug/L 37.750 75 43-120
N-Nitrosomethylethylamine ug/L 46.750 93 39-120
N-Nitrosopiperidine ug/L 54.550 109 43-113
N-Nitrosopyrrolidine ug/L 79.2 L05015832-110
Nitrobenzene ug/L 42.850 86 33-110
O,O,O-Triethylphosphorothioate ug/L 43.350 87 51-127
O-Toluidine ug/L 61.3 L05012327-120
P-Dimethylaminoazobenzene ug/L 25.2100 25 10-120
p-Phenylenediamine ug/L 63.450 127 72-143
Parathion (Ethyl parathion)ug/L 52.450 105 56-140
Pentachlorobenzene ug/L 43.050 86 30-137
Pentachloronitrobenzene ug/L 53.250 106 70-124
Pentachlorophenol ug/L 105250 42 10-137
Phenacetin ug/L 55.050 110 60-130
Phenanthrene ug/L 44.150 88 57-117
Phenol ug/L 19.850 40 10-120
Phorate ug/L 49.150 98 55-126
Pronamide ug/L 47.550 95 75-124
Pyrene ug/L 45.050 90 55-122
Safrole ug/L 44.250 88 41-120
Thionazin ug/L 52.050 104 63-137
2,4,6-Tribromophenol (S)%106 27-110
2-Fluorobiphenyl (S)%76 27-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 166 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
2-Fluorophenol (S)%47 12-110
Nitrobenzene-d5 (S)%78 21-110
Phenol-d6 (S)%32 10-110
Terphenyl-d14 (S)%96 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1814548MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738015
1,2,4,5-Tetrachlorobenzene ug/L 39.850 80 50-150ND
1,3,5-Trinitrobenzene ug/L 52.750 105 50-150ND
1,3-Dinitrobenzene ug/L 51.050 102 50-150ND
1,4-Naphthoquinone ug/L 47.050 94 50-150ND
1-Naphthalenamine ug/L 37.250 74 50-150ND
2,2'-Oxybis(1-chloropropane)ug/L 45.150 90 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 68.350 137 50-150ND
2,4,5-Trichlorophenol ug/L 50.950 102 19-105ND
2,4,6-Trichlorophenol ug/L 50.750 101 13-108ND
2,4-Dichlorophenol ug/L 46.550 93 29-111ND
2,4-Dimethylphenol ug/L 51.650 103 21-103ND
2,4-Dinitrophenol ug/L 194250 78 10-109ND
2,4-Dinitrotoluene ug/L 55.0 M15011027-104ND
2,6-Dichlorophenol ug/L 41.550 83 50-150ND
2,6-Dinitrotoluene ug/L 56.9 M15011428-101ND
2-Acetylaminofluorene ug/L 57.750 115 50-150ND
2-Chloronaphthalene ug/L 54.5 M15010914-102ND
2-Chlorophenol ug/L 43.050 86 16-110ND
2-Methylnaphthalene ug/L 45.050 90 13-110ND
2-Methylphenol(o-Cresol)ug/L 43.150 86 19-110ND
2-Naphthalenamine ug/L 48.850 98 50-150ND
2-Nitroaniline ug/L 85.7100 86 26-103ND
2-Nitrophenol ug/L 51.350 103 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 37.650 75 20-110ND
3,3'-Dichlorobenzidine ug/L 93.7250 37 25-112ND
3,3'-Dimethylbenzidine ug/L 46.7 M11004750-150ND
3-Methylcholanthrene ug/L 49.750 99 50-150ND
3-Nitroaniline ug/L 86.9100 87 29-110ND
4,6-Dinitro-2-methylphenol ug/L 100100 100 10-117ND
4-Aminobiphenyl ug/L 41.650 83 50-150ND
4-Bromophenylphenyl ether ug/L 46.650 93 20-105ND
4-Chloro-3-methylphenol ug/L 96.3100 96 22-110ND
4-Chloroaniline ug/L 83.8100 84 20-100ND
4-Chlorophenylphenyl ether ug/L 47.750 95 19-102ND
4-Nitroaniline ug/L 94.2100 94 29-110ND
4-Nitrophenol ug/L 113250 45 10-110ND
5-Nitro-o-toluidine ug/L 60.450 121 50-150ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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[phone]
Page 167 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1814548MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738015
7,12-Dimethylbenz(a)anthracene ug/L 47.350 95 50-150ND
Acenaphthene ug/L 45.450 91 17-100ND
Acenaphthylene ug/L 46.450 93 21-100ND
Acetophenone ug/L 46.550 93 50-150ND
Anthracene ug/L 46.650 93 24-109ND
Benzo(a)anthracene ug/L 45.950 92 22-117ND
Benzo(a)pyrene ug/L 45.750 91 23-104ND
Benzo(b)fluoranthene ug/L 47.750 95 23-103ND
Benzo(g,h,i)perylene ug/L 48.150 96 18-111ND
Benzo(k)fluoranthene ug/L 45.950 92 22-113ND
Benzyl alcohol ug/L 81.4100 81 19-101ND
bis(2-Chloroethoxy)methane ug/L 46.350 93 22-110ND
bis(2-Chloroethyl) ether ug/L 45.950 92 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 51.050 102 23-102ND
Butylbenzylphthalate ug/L 53.050 106 25-110ND
Chlorobenzilate ug/L 52.850 106 50-150ND
Chrysene ug/L 45.350 91 23-115ND
Di-n-butylphthalate ug/L 49.050 98 26-110ND
Di-n-octylphthalate ug/L 50.550 101 22-110ND
Diallate ug/L 49.650 99 50-150ND
Dibenz(a,h)anthracene ug/L 46.350 93 21-112ND
Dibenzofuran ug/L 43.650 87 19-102ND
Diethylphthalate ug/L 47.6J50 95 29-110ND
Dimethoate ug/L 51.350 103 50-150ND
Dimethylphthalate ug/L 44.950 90 27-110ND
Diphenylamine ug/L 42.050 84 50-150ND
Disulfoton ug/L 47.850 96 50-150ND
Ethyl methanesulfonate ug/L 43.350 87 50-150ND
Famphur ug/L 101100 101 50-150ND
Fluoranthene ug/L 49.950 100 23-112ND
Fluorene ug/L 48.050 96 22-104ND
Hexachlorobenzene ug/L 46.750 93 21-116ND
Hexachlorocyclopentadiene ug/L 42.450 85 10-110ND
Hexachloroethane ug/L 34.350 69 10-110ND
Hexachloropropene ug/L 31.550 63 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 47.450 95 20-113ND
Isodrin ug/L 46.650 93 50-150ND
Isophorone ug/L 48.550 97 50-150ND
Isosafrole ug/L 42.950 86 50-150ND
Kepone ug/L 61.5100 62 50-150ND
Methapyrilene ug/L 37.6J50 75 50-150ND
Methyl methanesulfonate ug/L 33.050 66 50-150ND
Methyl parathion ug/L 53.350 107 50-150ND
N-Nitroso-di-n-butylamine ug/L 41.450 83 50-150ND
N-Nitroso-di-n-propylamine ug/L 46.350 93 21-105ND
N-Nitrosodiethylamine ug/L 51.050 102 50-150ND
N-Nitrosodimethylamine ug/L 22.650 45 10-110ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Huntersville, NC 28078
[phone]
Page 168 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1814548MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738015
N-Nitrosodiphenylamine ug/L 42.050 84 23-107ND
N-Nitrosomethylethylamine ug/L 44.550 89 50-150ND
N-Nitrosopiperidine ug/L 48.450 97 50-150ND
N-Nitrosopyrrolidine ug/L 53.050 106 50-150ND
Nitrobenzene ug/L 46.050 92 20-110ND
O,O,O-Triethylphosphorothioate ug/L 41.450 83 50-150ND
O-Toluidine ug/L 44.950 90 50-150ND
P-Dimethylaminoazobenzene ug/L 26.3 M11002650-150ND
p-Phenylenediamine ug/L 51.950 104 50-150ND
Parathion (Ethyl parathion)ug/L 52.950 106 50-150ND
Pentachlorobenzene ug/L 42.550 85 50-150ND
Pentachloronitrobenzene ug/L 55.250 110 50-150ND
Pentachlorophenol ug/L 112250 45 10-118ND
Phenacetin ug/L 52.650 105 50-150ND
Phenanthrene ug/L 46.050 92 24-106ND
Phenol ug/L 20.350 41 12-110ND
Phorate ug/L 50.550 101 50-150ND
Pronamide ug/L 47.650 95 50-150ND
Pyrene ug/L 45.850 92 24-114ND
Safrole ug/L 41.150 82 50-150ND
Thionazin ug/L 49.750 99 50-150ND
2,4,6-Tribromophenol (S)%102 27-110
2-Fluorobiphenyl (S)%83 27-110
2-Fluorophenol (S)%51 12-110
Nitrobenzene-d5 (S)%85 21-110
Phenol-d6 (S)%40 10-110
Terphenyl-d14 (S)%85 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078003
1814549SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 169 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078003
1814549SAMPLE DUPLICATE:
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 170 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078003
1814549SAMPLE DUPLICATE:
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%92 2671
2-Fluorobiphenyl (S)%77 7336
2-Fluorophenol (S)%45 1398
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Huntersville, NC 28078
[phone]
Page 171 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078003
1814549SAMPLE DUPLICATE:
Nitrobenzene-d5 (S)%80 14114
Phenol-d6 (S)%31 9911
Terphenyl-d14 (S)%82 1868
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 172 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328263
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92310738004, 92310738005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1819074
Associated Lab Samples:92310738004, 92310738005
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 09/15/16 14:391.7
1,3,5-Trinitrobenzene ug/L ND 10.0 09/15/16 14:391.1
1,3-Dinitrobenzene ug/L ND 20.0 09/15/16 14:391.5
1,4-Naphthoquinone ug/L ND 10.0 09/15/16 14:391.8
1-Naphthalenamine ug/L ND 10.0 09/15/16 14:390.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/15/16 14:391.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 09/15/16 14:392.3
2,4,5-Trichlorophenol ug/L ND 10.0 09/15/16 14:392.2
2,4,6-Trichlorophenol ug/L ND 10.0 09/15/16 14:391.9
2,4-Dichlorophenol ug/L ND 10.0 09/15/16 14:391.7
2,4-Dimethylphenol ug/L ND 10.0 09/15/16 14:392.2
2,4-Dinitrophenol ug/L ND 50.0 09/15/16 14:396.5
2,4-Dinitrotoluene ug/L ND 10.0 09/15/16 14:391.2
2,6-Dichlorophenol ug/L ND 10.0 09/15/16 14:391.8
2,6-Dinitrotoluene ug/L ND 10.0 09/15/16 14:391.7
2-Acetylaminofluorene ug/L ND 20.0 09/15/16 14:390.84
2-Chloronaphthalene ug/L ND 10.0 09/15/16 14:392.2
2-Chlorophenol ug/L ND 10.0 09/15/16 14:391.5
2-Methylnaphthalene ug/L ND 10.0 09/15/16 14:390.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/15/16 14:391.7
2-Naphthalenamine ug/L ND 10.0 09/15/16 14:390.98
2-Nitroaniline ug/L ND 50.0 09/15/16 14:392.8
2-Nitrophenol ug/L ND 10.0 09/15/16 14:391.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/15/16 14:391.7
3,3'-Dichlorobenzidine ug/L ND 20.0 09/15/16 14:391.4
3,3'-Dimethylbenzidine ug/L ND 10.0 09/15/16 14:392.1
3-Methylcholanthrene ug/L ND 10.0 09/15/16 14:390.82
3-Nitroaniline ug/L ND 50.0 09/15/16 14:392.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 09/15/16 14:391.7
4-Aminobiphenyl ug/L ND 20.0 09/15/16 14:390.92
4-Bromophenylphenyl ether ug/L ND 10.0 09/15/16 14:391.3
4-Chloro-3-methylphenol ug/L ND 20.0 09/15/16 14:394.2
4-Chloroaniline ug/L ND 20.0 09/15/16 14:393.4
4-Chlorophenylphenyl ether ug/L ND 10.0 09/15/16 14:392.1
4-Nitroaniline ug/L ND 20.0 09/15/16 14:392.5
4-Nitrophenol ug/L ND 50.0 09/15/16 14:395.8
5-Nitro-o-toluidine ug/L ND 10.0 09/15/16 14:391.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 09/15/16 14:390.77
Acenaphthene ug/L ND 10.0 09/15/16 14:390.25
Acenaphthylene ug/L ND 10.0 09/15/16 14:390.21
Acetophenone ug/L ND 10.0 09/15/16 14:392.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Huntersville, NC 28078
[phone]
Page 173 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1819074
Associated Lab Samples:92310738004, 92310738005
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 09/15/16 14:390.14
Benzo(a)anthracene ug/L ND 10.0 09/15/16 14:390.33
Benzo(a)pyrene ug/L ND 10.0 09/15/16 14:390.30
Benzo(b)fluoranthene ug/L ND 10.0 09/15/16 14:390.28
Benzo(g,h,i)perylene ug/L ND 10.0 09/15/16 14:390.38
Benzo(k)fluoranthene ug/L ND 10.0 09/15/16 14:390.43
Benzyl alcohol ug/L ND 20.0 09/15/16 14:393.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/15/16 14:391.7
bis(2-Chloroethyl) ether ug/L ND 10.0 09/15/16 14:391.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 09/15/16 14:390.85
Butylbenzylphthalate ug/L ND 10.0 09/15/16 14:390.75
Chlorobenzilate ug/L ND 10.0 09/15/16 14:390.72
Chrysene ug/L ND 10.0 09/15/16 14:390.21
Di-n-butylphthalate ug/L ND 10.0 09/15/16 14:391.1
Di-n-octylphthalate ug/L ND 10.0 09/15/16 14:390.86
Diallate ug/L ND 10.0 09/15/16 14:391.3
Dibenz(a,h)anthracene ug/L ND 10.0 09/15/16 14:390.55
Dibenzofuran ug/L ND 10.0 09/15/16 14:391.8
Diethylphthalate ug/L ND 6000 09/15/16 14:391.3
Dimethoate ug/L ND 20.0 09/15/16 14:390.92
Dimethylphthalate ug/L ND 10.0 09/15/16 14:391.5
Diphenylamine ug/L ND 10.0 09/15/16 14:391.3
Disulfoton ug/L ND 10.0 09/15/16 14:391.4
Ethyl methanesulfonate ug/L ND 20.0 09/15/16 14:391.8
Famphur ug/L ND 20.0 09/15/16 14:391.7
Fluoranthene ug/L ND 10.0 09/15/16 14:390.21
Fluorene ug/L ND 10.0 09/15/16 14:390.21
Hexachlorobenzene ug/L ND 10.0 09/15/16 14:391.1
Hexachlorocyclopentadiene ug/L ND 10.0 09/15/16 14:391.8
Hexachloroethane ug/L ND 10.0 09/15/16 14:391.5
Hexachloropropene ug/L ND 10.0 09/15/16 14:391.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/15/16 14:390.29
Isodrin ug/L ND 20.0 09/15/16 14:392.0
Isophorone ug/L ND 10.0 09/15/16 14:391.8
Isosafrole ug/L ND 10.0 09/15/16 14:391.8
Kepone ug/L ND 20.0 09/15/16 14:393.1
Methapyrilene ug/L ND 100 09/15/16 14:392.7
Methyl methanesulfonate ug/L ND 10.0 09/15/16 14:391.3
Methyl parathion ug/L ND 10.0 09/15/16 14:391.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 09/15/16 14:392.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/15/16 14:392.1
N-Nitrosodiethylamine ug/L ND 20.0 09/15/16 14:391.8
N-Nitrosodimethylamine ug/L ND 10.0 09/15/16 14:391.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/15/16 14:391.3
N-Nitrosomethylethylamine ug/L ND 10.0 09/15/16 14:391.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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[phone]
Page 174 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1819074
Associated Lab Samples:92310738004, 92310738005
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 09/15/16 14:391.9
N-Nitrosopyrrolidine ug/L ND 10.0 09/15/16 14:392.5
Nitrobenzene ug/L ND 10.0 09/15/16 14:391.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 09/15/16 14:391.8
O-Toluidine ug/L ND 10.0 09/15/16 14:391.6
P-Dimethylaminoazobenzene ug/L ND 10.0 09/15/16 14:390.35
p-Phenylenediamine ug/L ND 10.0 09/15/16 14:390.96
Parathion (Ethyl parathion)ug/L ND 10.0 09/15/16 14:391.1
Pentachlorobenzene ug/L ND 10.0 09/15/16 14:392.0
Pentachloronitrobenzene ug/L ND 20.0 09/15/16 14:391.0
Pentachlorophenol ug/L ND 25.0 09/15/16 14:392.3
Phenacetin ug/L ND 20.0 09/15/16 14:390.97
Phenanthrene ug/L ND 10.0 09/15/16 14:390.22
Phenol ug/L ND 10.0 09/15/16 14:391.7
Phorate ug/L ND 10.0 09/15/16 14:391.1
Pronamide ug/L ND 10.0 09/15/16 14:390.97
Pyrene ug/L ND 10.0 09/15/16 14:390.19
Safrole ug/L ND 10.0 09/15/16 14:391.5
Thionazin ug/L ND 20.0 09/15/16 14:391.2
2,4,6-Tribromophenol (S)%74 27-110 09/15/16 14:39
2-Fluorobiphenyl (S)%69 27-110 09/15/16 14:39
2-Fluorophenol (S)%40 12-110 09/15/16 14:39
Nitrobenzene-d5 (S)%72 21-110 09/15/16 14:39
Phenol-d6 (S)%30 10-110 09/15/16 14:39
Terphenyl-d14 (S)%83 31-107 09/15/16 14:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1819075LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1819076
1,2,4,5-Tetrachlorobenzene ug/L 34.850 70 16-1297638.0 9 30
1,3,5-Trinitrobenzene ug/L 50.050 100 55-12510150.7 1 30
1,3-Dinitrobenzene ug/L 46.850 94 30-1229848.9 4 30
1,4-Naphthoquinone ug/L 41.950 84 31-1208642.8 2 30
1-Naphthalenamine ug/L 34.450 69 37-1267135.5 3 30
2,2'-Oxybis(1-chloropropane)ug/L 42.850 86 18-1208140.4 6 30
2,3,4,6-Tetrachlorophenol ug/L 61.950 124 54-27611657.8 7 30
2,4,5-Trichlorophenol ug/L 45.150 90 43-1139446.9 4 30
2,4,6-Trichlorophenol ug/L 46.150 92 42-1209547.4 3 30
2,4-Dichlorophenol ug/L 44.350 89 30-1209044.9 2 30
2,4-Dimethylphenol ug/L 48.350 97 29-1119748.5 0 30
2,4-Dinitrophenol ug/L 177250 71 19-13272179 1 30
2,4-Dinitrotoluene ug/L 50.450 101 58-12810351.6 2 30
2,6-Dichlorophenol ug/L 38.750 77 54-1287939.6 2 30
2,6-Dinitrotoluene ug/L 51.450 103 54-12910552.6 2 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Huntersville, NC 28078
[phone]
Page 175 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1819075LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1819076
2-Acetylaminofluorene ug/L 55.250 110 81-16011456.9 3 30
2-Chloronaphthalene ug/L 44.250 88 43-1179446.9 6 30
2-Chlorophenol ug/L 42.150 84 37-1208039.8 6 30
2-Methylnaphthalene ug/L 41.750 83 33-1208241.1 2 30
2-Methylphenol(o-Cresol)ug/L 41.650 83 31-1207939.6 5 30
2-Naphthalenamine ug/L 46.050 92 41-1369647.9 4 30
2-Nitroaniline ug/L 77.9100 78 48-1218079.6 2 30
2-Nitrophenol ug/L 46.850 94 25-1169648.2 3 30
3&4-Methylphenol(m&p Cresol)ug/L 37.850 76 23-1207135.5 6 30
3,3'-Dichlorobenzidine ug/L 90.6250 36 10-1543793.6 3 30
3,3'-Dimethylbenzidine ug/L 54.7 R11005510-1577877.8 35 30
3-Methylcholanthrene ug/L 46.550 93 65-1309647.8 3 30
3-Nitroaniline ug/L 81.1100 81 43-1158382.6 2 30
4,6-Dinitro-2-methylphenol ug/L 89.8100 90 44-1249392.7 3 30
4-Aminobiphenyl ug/L 39.150 78 21-1258944.5 13 30
4-Bromophenylphenyl ether ug/L 42.150 84 34-1138542.4 1 30
4-Chloro-3-methylphenol ug/L 90.8100 91 31-1108888.4 3 30
4-Chloroaniline ug/L 78.0100 78 20-1207877.7 0 30
4-Chlorophenylphenyl ether ug/L 43.550 87 34-1168843.9 1 30
4-Nitroaniline ug/L 87.5100 87 46-1289191.2 4 30
4-Nitrophenol ug/L 117250 47 11-12044109 7 30
5-Nitro-o-toluidine ug/L 55.750 111 78-16011457.0 2 30
7,12-Dimethylbenz(a)anthracene ug/L 42.450 85 47-1248944.3 4 30
Acenaphthene ug/L 40.650 81 48-1148241.1 1 30
Acenaphthylene ug/L 41.750 83 48-1128442.1 1 30
Acetophenone ug/L 44.950 90 24-1208542.3 6 30
Anthracene ug/L 41.850 84 57-1188542.4 1 30
Benzo(a)anthracene ug/L 43.050 86 56-1218743.6 1 30
Benzo(a)pyrene ug/L 42.250 84 55-1278743.7 3 30
Benzo(b)fluoranthene ug/L 44.350 89 53-1289346.5 5 30
Benzo(g,h,i)perylene ug/L 44.750 89 54-1259045.2 1 30
Benzo(k)fluoranthene ug/L 40.850 82 51-1238642.9 5 30
Benzyl alcohol ug/L 78.5100 78 27-1207574.7 5 30
bis(2-Chloroethoxy)methane ug/L 42.450 85 32-1208643.2 2 30
bis(2-Chloroethyl) ether ug/L 44.050 88 33-1118341.4 6 30
bis(2-Ethylhexyl)phthalate ug/L 46.550 93 50-1459246.1 1 30
Butylbenzylphthalate ug/L 48.150 96 54-1389748.6 1 30
Chlorobenzilate ug/L 48.350 97 65-1329748.3 0 30
Chrysene ug/L 41.350 83 58-1278643.2 4 30
Di-n-butylphthalate ug/L 45.150 90 56-1259246.0 2 30
Di-n-octylphthalate ug/L 47.650 95 50-1349446.8 2 30
Diallate ug/L 43.850 88 47-1238844.1 1 30
Dibenz(a,h)anthracene ug/L 44.950 90 53-1299245.8 2 30
Dibenzofuran ug/L 39.450 79 45-1208039.9 1 30
Diethylphthalate ug/L 43.8J50 88 53-1208743.3J 1 30
Dimethoate ug/L 44.650 89 57-1399346.4 4 30
Dimethylphthalate ug/L 41.250 82 55-1168240.9 1 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 176 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1819075LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1819076
Diphenylamine ug/L 37.150 74 42-1207638.0 3 30
Disulfoton ug/L 41.350 83 49-1568542.4 3 30
Ethyl methanesulfonate ug/L 40.050 80 43-1207537.6 6 30
Famphur ug/L 75.4100 75 40-1606767.1 12 30
Fluoranthene ug/L 45.750 91 57-1259648.1 5 30
Fluorene ug/L 43.850 88 53-1188844.1 1 30
Hexachlorobenzene ug/L 42.650 85 49-1168642.8 0 30
Hexachlorocyclopentadiene ug/L 38.550 77 26-1588039.8 3 30
Hexachloroethane ug/L 33.750 67 30-1146331.7 6 30
Hexachloropropene ug/L 28.050 56 13-1375929.6 5 30
Indeno(1,2,3-cd)pyrene ug/L 44.750 89 55-1289145.6 2 30
Isodrin ug/L 43.650 87 68-1298843.9 1 30
Isophorone ug/L 44.650 89 31-1188844.2 1 30
Isosafrole ug/L 38.350 77 48-1078039.8 4 30
Kepone ug/L 88.1100 88 10-124104104 17 30
Methapyrilene ug/L 32.7J50 65 40-1609447.2J 30
Methyl methanesulfonate ug/L 31.050 62 25-1145929.7 4 30
Methyl parathion ug/L 49.050 98 58-13710050.1 2 30
N-Nitroso-di-n-butylamine ug/L 39.150 78 36-1158241.1 5 30
N-Nitroso-di-n-propylamine ug/L 45.150 90 32-1198241.1 9 30
N-Nitrosodiethylamine ug/L 47.950 96 47-1159145.5 5 30
N-Nitrosodimethylamine ug/L 20.350 41 13-1204321.4 5 30
N-Nitrosodiphenylamine ug/L 37.150 74 43-1207638.0 3 30
N-Nitrosomethylethylamine ug/L 41.450 83 39-1208241.0 1 30
N-Nitrosopiperidine ug/L 44.350 89 43-1139045.0 2 30
N-Nitrosopyrrolidine ug/L 48.450 97 32-1108643.0 12 30
Nitrobenzene ug/L 42.250 84 33-1108642.9 2 30
O,O,O-Triethylphosphorothioate ug/L 39.450 79 51-1277939.5 0 30
O-Toluidine ug/L 43.150 86 27-1208140.3 7 30
P-Dimethylaminoazobenzene ug/L 24.1100 24 10-1202423.8 1 30
p-Phenylenediamine ug/L 50.950 102 72-14310251.2 1 30
Parathion (Ethyl parathion)ug/L 49.050 98 56-14010150.3 3 30
Pentachlorobenzene ug/L 39.050 78 30-1378140.3 3 30
Pentachloronitrobenzene ug/L 50.750 101 70-12410451.9 2 30
Pentachlorophenol ug/L 104250 41 10-13743108 4 30
Phenacetin ug/L 47.350 95 60-13010150.7 7 30
Phenanthrene ug/L 41.350 83 57-1178442.0 2 30
Phenol ug/L 20.250 40 10-1203919.7 2 30
Phorate ug/L 44.350 89 55-1268944.6 1 30
Pronamide ug/L 42.650 85 75-1248844.2 4 30
Pyrene ug/L 41.650 83 55-1228341.3 1 30
Safrole ug/L 38.150 76 41-1207738.7 2 30
Thionazin ug/L 46.150 92 63-1379246.2 0 30
2,4,6-Tribromophenol (S)%92 27-11093
2-Fluorobiphenyl (S)%73 27-11077
2-Fluorophenol (S)%51 12-11050
Nitrobenzene-d5 (S)%78 21-11080
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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[phone]
Page 177 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1819075LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1819076
Phenol-d6 (S)%40 10-11037
Terphenyl-d14 (S)%84 31-10784
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 178 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327519
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814862
Associated Lab Samples:92310738001, 92310738002, 92310738003, 92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 09/06/16 21:16100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814863LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 548J500 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814864MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738001
1814865
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15002480-1200 10500ND120JND
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814866MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310969006
1814867
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15006180-12061 0 10500ND329J330J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 179 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327527
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814887
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 09/06/16 23:36100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814888LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 542J500 108 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814889MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310969022
1814890
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 93 80-12092 1 10500ND491J488J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814891MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738014
1814892
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 87 80-12086 0 10500ND438J436J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 180 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327038
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1812116
Associated Lab Samples:92310738007
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 09/06/16 09:092000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812117LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 203000198000 103 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310743001
1812118SAMPLE DUPLICATE:
BOD, 5 day ug/L 460000 B2,D65610260 mg/L
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 181 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327407
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92310738007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310609002
1814193SAMPLE DUPLICATE:
pH Std. Units 8.1 H6098.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 182 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327242
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1813254
Associated Lab Samples:92310738007
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 09/02/16 16:431000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1813255LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19300J20000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1813256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310541003
1813257
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M6200004790-11084 1 1020000596 mg/L 606000J 613000J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 183 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327040
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1812125
Associated Lab Samples:92310738007
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 09/01/16 00:5310.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1812126LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24302500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1812127MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310743075
1812128
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 92 90-110108 8 1025002.7 mg/L 4960 5360
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1812129MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310743077
1812130
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 100 90-11099 0 1025001.7 mg/L 4230 4230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 184 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327710
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815993
Associated Lab Samples:92310738007
Matrix:Water
AnalyzedMDL
Phosphorus ug/L ND 50.0 09/09/16 05:2325.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815994LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 23402500 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1815995MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310621001
1815996
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L M625008090-110-39 2 102500163 mg/L 165000 162000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1815997MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311332006
1815998
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 98 90-11099 0 1025002.4 mg/L 4840 4850
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 185 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327852
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92310738001, 92310738002, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1816733
Associated Lab Samples:92310738001, 92310738002, 92310738006
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 09/08/16 17:20500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1816734LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2050020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1816735MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311072004
1816736
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000024990-110249 0 101000033.7 mg/L 58600 58600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1816737MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311106003
1816738
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M1100008490-11084 0 101000028.3 mg/L 36700 36700
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 186 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328108
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92310738001, 92310738002, 92310738003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1818147
Associated Lab Samples:92310738001, 92310738002, 92310738003
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 09/12/16 23:384.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1818148LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 95.6100 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818149MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310743006
1818150
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 97 75-12590 6 101000.027
mg/L 124 117
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818151MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310546002
1818152
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1,R1100675-1255 12 10100ND11.6 10.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 187 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328112
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92310738004, 92310738005, 92310738006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1818161
Associated Lab Samples:92310738004, 92310738005, 92310738006
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 09/13/16 00:104.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1818162LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 100100 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738004
1818164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11001475-12566 118 101004.0J 18.1 70.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 188 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328197
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1818832
Associated Lab Samples:92310738009, 92310738010, 92310738011, 92310738012, 92310738013, 92310738014, 92310738015,
92310738016, 92310738017
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 09/13/16 03:114.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1818833LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 98.4100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818834MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738009
1818835
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L R11007975-12590 13 10100ND81.9 93.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818836MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311268001
1818837
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 106 75-125108 2 10100ND110112
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 189 of 200
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328057
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92310738007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1818041
Associated Lab Samples:92310738007
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 09/14/16 16:5712500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1818042LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 748000750000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818043MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311482002
1818044
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M6750000-208 90-110-181 1 375000026300
mg/L
2480000
0
2500000
0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818045MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311539001
1818046
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 98 90-11098 0 3750000ND753000753000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 190 of 200
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
Common Laboratory Contaminant.C9
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Extraction or preparation conducted outside EPA method holding time.H2
Analysis initiated outside of the 15 minute EPA required holding time.H6
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 191 of 200
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 192 of 200
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92310738001 327101 327266MW-1 EPA 3510 EPA 8081
92310738002 327101 327266MW-2 EPA 3510 EPA 8081
92310738003 327101 327266MW-5 EPA 3510 EPA 8081
92310738004 327101 327266MW-6 EPA 3510 EPA 8081
92310738005 327101 327266MW-7 EPA 3510 EPA 8081
92310738006 327101 327266MW-16R EPA 3510 EPA 8081
92310738009 327585 327743MW-4 EPA 3510 EPA 8081
92310738010 327585 327743MW-8 EPA 3510 EPA 8081
92310738011 327585 327743MW-9 EPA 3510 EPA 8081
92310738012 327585 327743MW-10 EPA 3510 EPA 8081
92310738013 327585 327743MW-11 EPA 3510 EPA 8081
92310738014 327585 327743MW-12 EPA 3510 EPA 8081
92310738015 327585 327743MW-3 EPA 3510 EPA 8081
92310738016 327585 327743MW-14 EPA 3510 EPA 8081
92310738017 327585 327743MW-15 EPA 3510 EPA 8081
92310738001 327100 327265MW-1 EPA 3510 EPA 8082
92310738002 327100 327265MW-2 EPA 3510 EPA 8082
92310738003 327100 327265MW-5 EPA 3510 EPA 8082
92310738004 327100 327265MW-6 EPA 3510 EPA 8082
92310738005 327100 327265MW-7 EPA 3510 EPA 8082
92310738006 327100 327265MW-16R EPA 3510 EPA 8082
92310738009 327587 327745MW-4 EPA 3510 EPA 8082
92310738010 327587 327745MW-8 EPA 3510 EPA 8082
92310738011 327587 327745MW-9 EPA 3510 EPA 8082
92310738012 327587 327745MW-10 EPA 3510 EPA 8082
92310738013 327587 327745MW-11 EPA 3510 EPA 8082
92310738014 327587 327745MW-12 EPA 3510 EPA 8082
92310738015 327587 327745MW-3 EPA 3510 EPA 8082
92310738016 327587 327745MW-14 EPA 3510 EPA 8082
92310738017 327587 327745MW-15 EPA 3510 EPA 8082
92310738001 318664 318868MW-1 EPA 8151 EPA 8151
92310738002 318664 318868MW-2 EPA 8151 EPA 8151
92310738003 318664 318868MW-5 EPA 8151 EPA 8151
92310738004 318664 318868MW-6 EPA 8151 EPA 8151
92310738005 318664 318868MW-7 EPA 8151 EPA 8151
92310738006 318664 318868MW-16R EPA 8151 EPA 8151
92310738009 318978 319386MW-4 EPA 8151 EPA 8151
92310738010 318978 319386MW-8 EPA 8151 EPA 8151
92310738011 318978 319386MW-9 EPA 8151 EPA 8151
92310738012 318978 319386MW-10 EPA 8151 EPA 8151
92310738013 318978 319386MW-11 EPA 8151 EPA 8151
92310738014 318978 319386MW-12 EPA 8151 EPA 8151
92310738015 318978 319386MW-3 EPA 8151 EPA 8151
92310738016 318978 319386MW-14 EPA 8151 EPA 8151
92310738017 318978 319386MW-15 EPA 8151 EPA 8151
92310738001 327243MW-1 RSK 175 Modified
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 193 of 200
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92310738001 327130 327207MW-1 EPA 3010A EPA 6010
92310738002 327130 327207MW-2 EPA 3010A EPA 6010
92310738003 327130 327207MW-5 EPA 3010A EPA 6010
92310738004 327130 327207MW-6 EPA 3010A EPA 6010
92310738005 327130 327207MW-7 EPA 3010A EPA 6010
92310738006 327130 327207MW-16R EPA 3010A EPA 6010
92310738007 327130 327207LE-1 EPA 3010A EPA 6010
92310738009 327495 327550MW-4 EPA 3010A EPA 6010
92310738010 327495 327550MW-8 EPA 3010A EPA 6010
92310738011 327495 327550MW-9 EPA 3010A EPA 6010
92310738012 327495 327550MW-10 EPA 3010A EPA 6010
92310738013 327495 327550MW-11 EPA 3010A EPA 6010
92310738014 327495 327550MW-12 EPA 3010A EPA 6010
92310738015 327495 327550MW-3 EPA 3010A EPA 6010
92310738016 327495 327550MW-14 EPA 3010A EPA 6010
92310738017 327495 327550MW-15 EPA 3010A EPA 6010
92310738018 327945 328067SW-4 EPA 3010A EPA 6010
92310738019 327945 328067SW-5 EPA 3010A EPA 6010
92310738009 327533 327552MW-4 EPA 3010 EPA 6010
92310738011 327533 327552MW-9 EPA 3010 EPA 6010
92310738012 327533 327552MW-10 EPA 3010 EPA 6010
92310738013 327533 327552MW-11 EPA 3010 EPA 6010
92310738014 327533 327552MW-12 EPA 3010 EPA 6010
92310738015 327533 327552MW-3 EPA 3010 EPA 6010
92310738001 327037 327051MW-1 EPA 7470 EPA 7470
92310738002 327037 327051MW-2 EPA 7470 EPA 7470
92310738003 327037 327051MW-5 EPA 7470 EPA 7470
92310738004 327037 327051MW-6 EPA 7470 EPA 7470
92310738005 327037 327051MW-7 EPA 7470 EPA 7470
92310738006 327037 327051MW-16R EPA 7470 EPA 7470
92310738007 327037 327051LE-1 EPA 7470 EPA 7470
92310738009 327371 327378MW-4 EPA 7470 EPA 7470
92310738010 327371 327378MW-8 EPA 7470 EPA 7470
92310738011 327371 327378MW-9 EPA 7470 EPA 7470
92310738012 327371 327378MW-10 EPA 7470 EPA 7470
92310738013 327371 327378MW-11 EPA 7470 EPA 7470
92310738014 327371 327378MW-12 EPA 7470 EPA 7470
92310738015 327371 327378MW-3 EPA 7470 EPA 7470
92310738016 327371 327378MW-14 EPA 7470 EPA 7470
92310738017 327371 327378MW-15 EPA 7470 EPA 7470
92310738009 328823 329096MW-4 EPA 7470 EPA 7470
92310738011 330655 330669MW-9 EPA 7470 EPA 7470
92310738012 328823 329096MW-10 EPA 7470 EPA 7470
92310738013 328823 329096MW-11 EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 194 of 200
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92310738014 328823 329096MW-12 EPA 7470 EPA 7470
92310738015 330655 330669MW-3 EPA 7470 EPA 7470
92310738001 327270 327461MW-1 EPA 3510 EPA 8270
92310738002 327270 327461MW-2 EPA 3510 EPA 8270
92310738003 327270 327461MW-5 EPA 3510 EPA 8270
92310738004 328263 328375MW-6 EPA 3510 EPA 8270
92310738005 328263 328375MW-7 EPA 3510 EPA 8270
92310738006 327270 327461MW-16R EPA 3510 EPA 8270
92310738009 327459 327627MW-4 EPA 3510 EPA 8270
92310738010 327459 327627MW-8 EPA 3510 EPA 8270
92310738011 327459 327627MW-9 EPA 3510 EPA 8270
92310738012 327459 327627MW-10 EPA 3510 EPA 8270
92310738013 327459 327627MW-11 EPA 3510 EPA 8270
92310738014 327459 327627MW-12 EPA 3510 EPA 8270
92310738015 327459 327627MW-3 EPA 3510 EPA 8270
92310738016 327459 327627MW-14 EPA 3510 EPA 8270
92310738017 327459 327627MW-15 EPA 3510 EPA 8270
92310738001 327295MW-1 EPA 8260
92310738002 327295MW-2 EPA 8260
92310738003 327295MW-5 EPA 8260
92310738004 327295MW-6 EPA 8260
92310738005 327295MW-7 EPA 8260
92310738006 327295MW-16R EPA 8260
92310738007 327683LE-1 EPA 8260
92310738009 327683MW-4 EPA 8260
92310738010 327683MW-8 EPA 8260
92310738011 327683MW-9 EPA 8260
92310738012 327683MW-10 EPA 8260
92310738013 327683MW-11 EPA 8260
92310738014 327683MW-12 EPA 8260
92310738015 327683MW-3 EPA 8260
92310738016 327683MW-14 EPA 8260
92310738017 327683MW-15 EPA 8260
92310738018 327683SW-4 EPA 8260
92310738019 327683SW-5 EPA 8260
92310738001 327519MW-1 SM 4500-S2D
92310738002 327519MW-2 SM 4500-S2D
92310738003 327519MW-5 SM 4500-S2D
92310738004 327519MW-6 SM 4500-S2D
92310738005 327519MW-7 SM 4500-S2D
92310738006 327519MW-16R SM 4500-S2D
92310738009 327527MW-4 SM 4500-S2D
92310738010 327527MW-8 SM 4500-S2D
92310738011 327527MW-9 SM 4500-S2D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 195 of 200
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92310738
WAYNE LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92310738012 327527MW-10 SM 4500-S2D
92310738013 327527MW-11 SM 4500-S2D
92310738014 327527MW-12 SM 4500-S2D
92310738015 327527MW-3 SM 4500-S2D
92310738016 327527MW-14 SM 4500-S2D
92310738017 327527MW-15 SM 4500-S2D
92310738007 327038 327047LE-1 SM 5210B SM 5210B
92310738007 327407LE-1 EPA 9040
92310738007 327242LE-1 EPA 300.0
92310738007 327040LE-1 EPA 353.2
92310738007 327710LE-1 EPA 365.1
92310738001 327852MW-1 SM 4500-Cl-E
92310738002 327852MW-2 SM 4500-Cl-E
92310738006 327852MW-16R SM 4500-Cl-E
92310738001 328108MW-1 SM 4500-CN-E
92310738002 328108MW-2 SM 4500-CN-E
92310738003 328108MW-5 SM 4500-CN-E
92310738004 328112MW-6 SM 4500-CN-E
92310738005 328112MW-7 SM 4500-CN-E
92310738006 328112MW-16R SM 4500-CN-E
92310738009 328197MW-4 SM 4500-CN-E
92310738010 328197MW-8 SM 4500-CN-E
92310738011 328197MW-9 SM 4500-CN-E
92310738012 328197MW-10 SM 4500-CN-E
92310738013 328197MW-11 SM 4500-CN-E
92310738014 328197MW-12 SM 4500-CN-E
92310738015 328197MW-3 SM 4500-CN-E
92310738016 328197MW-14 SM 4500-CN-E
92310738017 328197MW-15 SM 4500-CN-E
92310738007 328057LE-1 SM 5220D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2017 03:38 PM
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Page 197 of 200
Page 198 of 200
Page 199 of 200
Page 200 of 200
#=CL#
September 13, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311096
92311096
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE MSWLF BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92311096001 EB Water 09/01/16 17:00 09/02/16 08:50
92311096002 FB Water 09/01/16 17:15 09/02/16 08:50
92311096003 TB Water 09/01/16 00:00 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311096001 EB EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AWAB
EPA 8260 68 PASI-CGAW
92311096002 FB EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AWAB
EPA 8260 68 PASI-CGAW
92311096003 TB EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:EB Lab ID:92311096001 Collected:09/01/16 17:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/11/16 00:31 7440-36-009/09/16 19:206.0 3.8 1
Arsenic ND ug/L 09/11/16 00:31 7440-38-209/09/16 19:2010.0 2.5 1
Barium ND ug/L 09/11/16 00:31 7440-39-309/09/16 19:201002.5 1
Beryllium ND ug/L 09/11/16 00:31 7440-41-709/09/16 19:201.0 0.50 1
Cadmium ND ug/L 09/11/16 00:31 7440-43-909/09/16 19:201.0 0.50 1
Chromium ND ug/L 09/11/16 00:31 7440-47-309/09/16 19:2010.0 2.5 1
Cobalt ND ug/L 09/11/16 00:31 7440-48-409/09/16 19:2010.0 2.5 1
Copper ND ug/L 09/11/16 00:31 7440-50-809/09/16 19:2010.0 2.5 1
Lead ND ug/L 09/11/16 00:31 7439-92-109/09/16 19:2010.0 2.5 1
Nickel ND ug/L 09/11/16 00:31 7440-02-009/09/16 19:2050.0 2.5 1
Selenium ND ug/L 09/11/16 00:31 7782-49-209/09/16 19:2010.0 5.0 1
Silver ND ug/L 09/11/16 00:31 7440-22-409/09/16 19:2010.0 2.5 1
Thallium ND ug/L 09/11/16 00:31 7440-28-009/09/16 19:205.5 5.0 1
Tin 2.9J ug/L 09/11/16 00:31 7440-31-509/09/16 19:201002.5 1
Vanadium ND ug/L 09/11/16 00:31 7440-62-209/09/16 19:2025.0 2.5 1
Zinc 6.1J ug/L 09/11/16 00:31 7440-66-6 B09/09/16 19:2010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/09/16 12:49 7439-97-609/09/16 02:450.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 06:37 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 06:37 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 06:37 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 06:37 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 06:37 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 06:37 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 06:37 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 06:37 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 06:37 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 06:37 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 06:37 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 06:37 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 06:37 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 06:37 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 06:37 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 06:37 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 06:37 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 06:37 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 06:37 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 06:37 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 06:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 06:37 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 06:37 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 06:37 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 06:37 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:EB Lab ID:92311096001 Collected:09/01/16 17:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 06:37 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 06:37 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 06:37 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 06:37 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 06:37 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 06:37 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 06:37 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 06:37 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 06:37 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 06:37 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 06:37 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 06:37 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 06:37 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 06:37 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 06:37 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 06:37 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 06:37 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 06:37 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 06:37 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 06:37 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 06:37 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 06:37 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 06:37 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 06:37 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 06:37 107-12-01503.6 1
Styrene ND ug/L 09/08/16 06:37 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 06:37 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 06:37 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 06:37 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 06:37 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 06:37 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 06:37 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 06:37 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 06:37 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 06:37 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 06:37 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 06:37 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 06:37 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 06:37 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 06:37 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 06:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 06:37 17060-07-070-130 1
Toluene-d8 (S)101 %09/08/16 06:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:FB Lab ID:92311096002 Collected:09/01/16 17:15 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/11/16 00:34 7440-36-009/09/16 19:206.0 3.8 1
Arsenic ND ug/L 09/11/16 00:34 7440-38-209/09/16 19:2010.0 2.5 1
Barium ND ug/L 09/11/16 00:34 7440-39-309/09/16 19:201002.5 1
Beryllium ND ug/L 09/11/16 00:34 7440-41-709/09/16 19:201.0 0.50 1
Cadmium ND ug/L 09/11/16 00:34 7440-43-909/09/16 19:201.0 0.50 1
Chromium ND ug/L 09/11/16 00:34 7440-47-309/09/16 19:2010.0 2.5 1
Cobalt ND ug/L 09/11/16 00:34 7440-48-409/09/16 19:2010.0 2.5 1
Copper ND ug/L 09/11/16 00:34 7440-50-809/09/16 19:2010.0 2.5 1
Lead ND ug/L 09/11/16 00:34 7439-92-109/09/16 19:2010.0 2.5 1
Nickel ND ug/L 09/11/16 00:34 7440-02-009/09/16 19:2050.0 2.5 1
Selenium ND ug/L 09/11/16 00:34 7782-49-209/09/16 19:2010.0 5.0 1
Silver ND ug/L 09/11/16 00:34 7440-22-409/09/16 19:2010.0 2.5 1
Thallium ND ug/L 09/11/16 00:34 7440-28-009/09/16 19:205.5 5.0 1
Tin 3.6J ug/L 09/11/16 00:34 7440-31-509/09/16 19:201002.5 1
Vanadium ND ug/L 09/11/16 00:34 7440-62-209/09/16 19:2025.0 2.5 1
Zinc 7.3J ug/L 09/11/16 00:34 7440-66-6 B09/09/16 19:2010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/09/16 13:01 7439-97-609/09/16 02:450.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 06:54 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 06:54 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 06:54 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 06:54 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 06:54 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 06:54 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 06:54 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 06:54 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 06:54 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 06:54 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 06:54 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 06:54 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 06:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 06:54 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 06:54 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 06:54 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 06:54 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 06:54 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 06:54 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 06:54 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 06:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 06:54 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 06:54 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 06:54 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 06:54 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:FB Lab ID:92311096002 Collected:09/01/16 17:15 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 06:54 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 06:54 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 06:54 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 06:54 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 06:54 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 06:54 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 06:54 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 06:54 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 06:54 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 06:54 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 06:54 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 06:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 06:54 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 06:54 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 06:54 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 06:54 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 06:54 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 06:54 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 06:54 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 06:54 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 06:54 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 06:54 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 06:54 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 06:54 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 06:54 107-12-01503.6 1
Styrene ND ug/L 09/08/16 06:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 06:54 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 06:54 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 06:54 127-18-41.0 0.46 1
Tetrahydrofuran 3.7J ug/L 09/08/16 06:54 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 06:54 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 06:54 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 06:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 06:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 06:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 06:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 06:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 06:54 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 06:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 06:54 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 06:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %09/08/16 06:54 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 06:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:TB Lab ID:92311096003 Collected:09/01/16 00:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 07:11 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 07:11 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 07:11 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 07:11 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 07:11 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 07:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 07:11 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 07:11 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 07:11 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 07:11 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 07:11 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 07:11 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 07:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 07:11 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 07:11 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 07:11 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 07:11 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 07:11 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 07:11 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 07:11 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 07:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 07:11 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 07:11 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 07:11 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 07:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 07:11 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 07:11 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 07:11 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 07:11 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 07:11 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 07:11 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 07:11 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 07:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 07:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 07:11 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 07:11 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 07:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 07:11 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 07:11 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 07:11 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 07:11 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 07:11 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 07:11 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 07:11 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 07:11 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 07:11 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
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Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:TB Lab ID:92311096003 Collected:09/01/16 00:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 07:11 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 07:11 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 07:11 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 07:11 107-12-01503.6 1
Styrene ND ug/L 09/08/16 07:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 07:11 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 07:11 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 07:11 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 07:11 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 07:11 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 07:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 07:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 07:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 07:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 07:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 07:11 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 07:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 07:11 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 07:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 07:11 17060-07-070-130 1
Toluene-d8 (S)105 %09/08/16 07:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327540
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92311096001, 92311096002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814951
Associated Lab Samples:92311096001, 92311096002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 09/09/16 12:280.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814952LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814953MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311075001
1814954
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 48 75-12596 66 252.5ND 1.2 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327945
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92311096001, 92311096002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1817217
Associated Lab Samples:92311096001, 92311096002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/11/16 00:033.8
Arsenic ug/L 6.5J 10.0 09/11/16 00:032.5
Barium ug/L ND 100 09/11/16 00:032.5
Beryllium ug/L ND 1.0 09/11/16 00:030.50
Cadmium ug/L ND 1.0 09/11/16 00:030.50
Chromium ug/L ND 10.0 09/11/16 00:032.5
Cobalt ug/L ND 10.0 09/11/16 00:032.5
Copper ug/L ND 10.0 09/11/16 00:032.5
Lead ug/L ND 10.0 09/11/16 00:032.5
Nickel ug/L ND 50.0 09/11/16 00:032.5
Selenium ug/L ND 10.0 09/11/16 00:035.0
Silver ug/L ND 10.0 09/11/16 00:032.5
Thallium ug/L ND 5.5 09/11/16 00:035.0
Tin ug/L ND 100 09/11/16 00:032.5
Vanadium ug/L ND 25.0 09/11/16 00:032.5
Zinc ug/L 6.2J 10.0 09/11/16 00:035.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1817218LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 502500 100 80-120
Arsenic ug/L 497500 99 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 520500 104 80-120
Cadmium ug/L 508500 102 80-120
Chromium ug/L 519500 104 80-120
Cobalt ug/L 518500 104 80-120
Copper ug/L 522500 104 80-120
Lead ug/L 510500 102 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 255250 102 80-120
Thallium ug/L 512500 102 80-120
Tin ug/L 513500 103 80-120
Vanadium ug/L 510500 102 80-120
Zinc ug/L 530500 106 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1817219MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738018
1817220
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12597 0 25500ND486484
Arsenic ug/L 500 98 75-12598 0 25500ND491492
Barium ug/L 500 97 75-12598 1 25500415899905
Beryllium ug/L 500 100 75-125101 0 25500ND502504
Cadmium ug/L 500 98 75-12598 0 255002.3 493 494
Chromium ug/L 500 99 75-125100 0 25500ND497498
Cobalt ug/L 500 99 75-12599 0 25500ND499499
Copper ug/L 500 101 75-125101 0 25500ND509510
Lead ug/L 500 98 75-12597 0 25500ND490489
Nickel ug/L 500 97 75-12597 0 25500ND486486
Selenium ug/L 500 100 75-125100 0 25500ND500502
Silver ug/L 250 98 75-12599 1 25250ND246247
Thallium ug/L 500 97 75-12597 0 25500ND487487
Tin ug/L 500 98 75-12598 0 25500ND494494
Vanadium ug/L 500 99 75-12599 0 25500ND495497
Zinc ug/L 500 101 75-125101 0 2550018.5 524 524
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311096001, 92311096002, 92311096003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311096001, 92311096002, 92311096003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/08/16 00:010.33
1,1,1-Trichloroethane ug/L ND 1.0 09/08/16 00:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/08/16 00:010.40
1,1,2-Trichloroethane ug/L ND 1.0 09/08/16 00:010.29
1,1-Dichloroethane ug/L ND 5.0 09/08/16 00:010.32
1,1-Dichloroethene ug/L ND 5.0 09/08/16 00:010.56
1,1-Dichloropropene ug/L ND 5.0 09/08/16 00:010.49
1,2,3-Trichloropropane ug/L ND 1.0 09/08/16 00:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/08/16 00:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/08/16 00:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/16 00:010.27
1,2-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.30
1,2-Dichloroethane ug/L ND 1.0 09/08/16 00:010.24
1,2-Dichloropropane ug/L ND 1.0 09/08/16 00:010.27
1,3-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.24
1,3-Dichloropropane ug/L ND 1.0 09/08/16 00:010.28
1,4-Dichlorobenzene ug/L ND 1.0 09/08/16 00:010.33
2,2-Dichloropropane ug/L ND 15.0 09/08/16 00:010.13
2-Butanone (MEK)ug/L ND 100 09/08/16 00:010.96
2-Hexanone ug/L ND 50.0 09/08/16 00:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/08/16 00:010.33
Acetone ug/L ND 100 09/08/16 00:0110.0
Acetonitrile ug/L ND 55.0 09/08/16 00:012.2
Acrolein ug/L ND 53.0 09/08/16 00:011.6
Acrylonitrile ug/L ND 200 09/08/16 00:011.9
Allyl chloride ug/L ND 10.0 09/08/16 00:011.5
Benzene ug/L ND 1.0 09/08/16 00:010.25
Bromochloromethane ug/L ND 3.0 09/08/16 00:010.17
Bromodichloromethane ug/L ND 1.0 09/08/16 00:010.18
Bromoform ug/L ND 3.0 09/08/16 00:010.26
Bromomethane ug/L ND 10.0 09/08/16 00:010.29
Carbon disulfide ug/L ND 100 09/08/16 00:011.2
Carbon tetrachloride ug/L ND 1.0 09/08/16 00:010.25
Chlorobenzene ug/L ND 3.0 09/08/16 00:010.23
Chloroethane ug/L ND 10.0 09/08/16 00:010.54
Chloroform ug/L ND 5.0 09/08/16 00:010.14
Chloromethane ug/L ND 1.0 09/08/16 00:010.11
Chloroprene ug/L ND 20.0 09/08/16 00:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.13
Dibromochloromethane ug/L ND 3.0 09/08/16 00:010.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311096001, 92311096002, 92311096003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 09/08/16 00:010.21
Dichlorodifluoromethane ug/L ND 5.0 09/08/16 00:010.21
Ethyl methacrylate ug/L ND 10.0 09/08/16 00:010.20
Ethylbenzene ug/L ND 1.0 09/08/16 00:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/08/16 00:010.71
Iodomethane ug/L ND 10.0 09/08/16 00:010.32
Isobutanol ug/L ND 100 09/08/16 00:0135.0
Methacrylonitrile ug/L ND 100 09/08/16 00:010.93
Methyl methacrylate ug/L ND 30.0 09/08/16 00:012.0
Methylene Chloride ug/L ND 1.0 09/08/16 00:010.97
Naphthalene ug/L ND 10.0 09/08/16 00:010.24
Propionitrile ug/L ND 150 09/08/16 00:013.6
Styrene ug/L ND 1.0 09/08/16 00:010.26
Tetrachloroethene ug/L ND 1.0 09/08/16 00:010.46
Tetrahydrofuran ug/L ND 10.0 09/08/16 00:013.1
Toluene ug/L ND 1.0 09/08/16 00:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/08/16 00:011.0
Trichloroethene ug/L ND 1.0 09/08/16 00:010.47
Trichlorofluoromethane ug/L ND 1.0 09/08/16 00:010.20
Vinyl acetate ug/L ND 50.0 09/08/16 00:010.35
Vinyl chloride ug/L ND 1.0 09/08/16 00:010.62
Xylene (Total)ug/L ND 5.0 09/08/16 00:010.66
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/16 00:01
4-Bromofluorobenzene (S)%101 70-130 09/08/16 00:01
Toluene-d8 (S)%103 70-130 09/08/16 00:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 80-125
1,1,1-Trichloroethane ug/L 54.750 109 71-129
1,1,2,2-Tetrachloroethane ug/L 53.850 108 79-124
1,1,2-Trichloroethane ug/L 53.150 106 85-125
1,1-Dichloroethane ug/L 54.750 109 73-126
1,1-Dichloroethene ug/L 59.450 119 66-135
1,1-Dichloropropene ug/L 56.350 113 74-135
1,2,3-Trichloropropane ug/L 54.150 108 75-130
1,2,4-Trichlorobenzene ug/L 56.550 113 75-134
1,2-Dibromo-3-chloropropane ug/L 52.050 104 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 57.850 116 80-133
1,2-Dichloroethane ug/L 54.050 108 67-128
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 53.150 106 75-132
1,3-Dichlorobenzene ug/L 57.650 115 77-130
1,3-Dichloropropane ug/L 54.250 108 76-131
1,4-Dichlorobenzene ug/L 55.150 110 78-130
2,2-Dichloropropane ug/L 53.350 107 40-160
2-Butanone (MEK)ug/L 133100 133 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 158 L010015848-146
Acetonitrile ug/L 623500 125 62-150
Acrolein ug/L 307 F325012324-160
Acrylonitrile ug/L 297250 119 40-160
Allyl chloride ug/L 55.550 111 66-137
Benzene ug/L 55.650 111 80-125
Bromochloromethane ug/L 59.350 119 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 53.7 F35010740-160
Carbon disulfide ug/L 74.3J F35014950-160
Carbon tetrachloride ug/L 58.250 116 69-131
Chlorobenzene ug/L 55.950 112 81-122
Chloroethane ug/L 55.850 112 39-148
Chloroform ug/L 53.150 106 73-127
Chloromethane ug/L 52.150 104 44-146
Chloroprene ug/L 57.250 114 75-145
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
cis-1,3-Dichloropropene ug/L 57.450 115 72-132
Dibromochloromethane ug/L 57.550 115 78-125
Dibromomethane ug/L 52.150 104 82-120
Dichlorodifluoromethane ug/L 51.750 103 34-157
Ethyl methacrylate ug/L 56.750 113 82-121
Ethylbenzene ug/L 54.250 108 79-121
Hexachloro-1,3-butadiene ug/L 57.750 115 72-131
Iodomethane ug/L 124100 124 39-154
Isobutanol ug/L 15401000 154 34-160
Methacrylonitrile ug/L 606500 121 74-134
Methyl methacrylate ug/L 57.650 115 84-124
Methylene Chloride ug/L 58.550 117 64-133
Naphthalene ug/L 55.150 110 73-133
Propionitrile ug/L 620500 124 73-140
Styrene ug/L 56.350 113 84-126
Tetrachloroethene ug/L 54.450 109 78-122
Tetrahydrofuran ug/L 609500 122 69-148
Toluene ug/L 54.550 109 80-121
trans-1,2-Dichloroethene ug/L 55.850 112 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
trans-1,4-Dichloro-2-butene ug/L 92.9J F3,L05018640-160
REPORT OF LABORATORY ANALYSIS
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Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 55.550 111 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 123100 123 40-160
Vinyl chloride ug/L 52.350 105 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,1-Dichloropropene ug/L 21.620 108 70-130ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.820 114 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 19.720 99 70-130ND
1,2-Dichloropropane ug/L 21.120 106 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,3-Dichloropropane ug/L 20.320 101 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2,2-Dichloropropane ug/L 22.820 114 70-130ND
2-Butanone (MEK)ug/L 39.8J40 99 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.1J40 98 70-130ND
Acetone ug/L 37.7J40 73 70-130ND
Acetonitrile ug/L 186200 93 70-130ND
Acrolein ug/L 115100 115 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 20.720 104 70-130ND
Benzene ug/L 21.920 109 70-148ND
Bromochloromethane ug/L 21.120 105 70-130ND
Bromodichloromethane ug/L 20.920 104 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
Chloroprene ug/L 22.020 110 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 108 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 20.320 101 70-130ND
Dichlorodifluoromethane ug/L 13.5 M1206870-130ND
Ethyl methacrylate ug/L 20.620 103 70-130ND
Ethylbenzene ug/L 21.120 106 70-130ND
Hexachloro-1,3-butadiene ug/L 24.220 121 70-130ND
Iodomethane ug/L 40.040 100 70-130ND
Isobutanol ug/L 423400 106 70-130ND
Methacrylonitrile ug/L 205200 102 70-130ND
Methyl methacrylate ug/L 21.0J20 105 70-130ND
Methylene Chloride ug/L 18.620 93 70-130ND
Naphthalene ug/L 20.620 103 70-130ND
Propionitrile ug/L 205200 103 70-130ND
Styrene ug/L 21.820 109 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Tetrahydrofuran ug/L 205200 101 70-130ND
Toluene ug/L 21.420 103 70-1550.76J
trans-1,2-Dichloroethene ug/L 21.520 107 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 22.620 113 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 39.8J40 100 70-130ND
Vinyl chloride ug/L 18.220 91 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 19 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L 0.66J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 7105
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%108 6102
REPORT OF LABORATORY ANALYSIS
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Page 20 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 21 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311096001 327945 328067EBEPA 3010A EPA 6010
92311096002 327945 328067FBEPA 3010A EPA 6010
92311096001 327540 327557EBEPA 7470 EPA 7470
92311096002 327540 327557FBEPA 7470 EPA 7470
92311096001 327693EBEPA 8260
92311096002 327693FBEPA 8260
92311096003 327693TBEPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 22 of 24
Page 23 of 24
Page 24 of 24
#=CL#
September 01, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92309797
92309797
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE LINED (MW-13)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on August 23, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 37
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Lab ID Sample ID Matrix Date Collected Date Received
92309797001 MW-13 Water 08/22/16 14:50 08/23/16 08:28
REPORT OF LABORATORY ANALYSIS
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Page 3 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92309797001 MW-13 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AEWS
SM 4500-CN-E 1 PASI-ADMN
REPORT OF LABORATORY ANALYSIS
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Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Sample:MW-13 Lab ID:92309797001 Collected:08/22/16 14:50 Received:08/23/16 08:28 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 08/24/16 12:03 309-00-208/23/16 12:270.050 0.050 1
alpha-BHC ND ug/L 08/24/16 12:03 319-84-608/23/16 12:270.050 0.050 1
beta-BHC ND ug/L 08/24/16 12:03 319-85-708/23/16 12:270.050 0.050 1
delta-BHC ND ug/L 08/24/16 12:03 319-86-808/23/16 12:270.050 0.050 1
gamma-BHC (Lindane)ND ug/L 08/24/16 12:03 58-89-908/23/16 12:270.050 0.050 1
Chlordane (Technical)ND ug/L 08/24/16 12:03 57-74-908/23/16 12:270.50 0.20 1
4,4'-DDD ND ug/L 08/24/16 12:03 72-54-808/23/16 12:270.10 0.050 1
4,4'-DDE ND ug/L 08/24/16 12:03 72-55-908/23/16 12:270.10 0.050 1
4,4'-DDT ND ug/L 08/24/16 12:03 50-29-308/23/16 12:270.10 0.050 1
Dieldrin ND ug/L 08/24/16 12:03 60-57-108/23/16 12:270.075 0.050 1
Endosulfan I ND ug/L 08/24/16 12:03 959-98-808/23/16 12:270.10 0.050 1
Endosulfan II ND ug/L 08/24/16 12:03 33213-65-908/23/16 12:270.10 0.050 1
Endosulfan sulfate ND ug/L 08/24/16 12:03 1031-07-808/23/16 12:270.10 0.050 1
Endrin ND ug/L 08/24/16 12:03 72-20-808/23/16 12:270.10 0.050 1
Endrin aldehyde ND ug/L 08/24/16 12:03 7421-93-408/23/16 12:270.10 0.050 1
Heptachlor ND ug/L 08/24/16 12:03 76-44-808/23/16 12:270.050 0.050 1
Heptachlor epoxide ND ug/L 08/24/16 12:03 1024-57-308/23/16 12:270.075 0.050 1
Methoxychlor ND ug/L 08/24/16 12:03 72-43-508/23/16 12:271.0 0.15 1
Toxaphene ND ug/L 08/24/16 12:03 8001-35-208/23/16 12:271.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)66 %08/24/16 12:03 877-09-808/23/16 12:2720-130 1
Decachlorobiphenyl (S)52 %08/24/16 12:03 2051-24-308/23/16 12:2720-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 08/24/16 14:29 12674-11-208/23/16 15:240.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 08/24/16 14:29 11104-28-208/23/16 15:240.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 08/24/16 14:29 11141-16-508/23/16 15:240.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 08/24/16 14:29 53469-21-908/23/16 15:240.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 08/24/16 14:29 12672-29-608/23/16 15:240.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 08/24/16 14:29 11097-69-108/23/16 15:240.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 08/24/16 14:29 11096-82-508/23/16 15:240.50 0.50 1
Surrogates
Decachlorobiphenyl (S)50 %08/24/16 14:29 2051-24-308/23/16 15:2410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 08/31/16 08:18 25057-89-008/26/16 08:550.096 0.048 1
2,4-D ND ug/L 08/31/16 08:18 94-75-708/26/16 08:550.95 0.23 1
Dalapon ND ug/L 08/31/16 08:18 75-99-008/26/16 08:550.92 0.44 1
2,4-DB ND ug/L 08/31/16 08:18 94-82-608/26/16 08:551.9 0.52 1
Dicamba ND ug/L 08/31/16 08:18 1918-00-908/26/16 08:550.095 0.030 1
Dichlorprop ND ug/L 08/31/16 08:18 120-36-508/26/16 08:550.66 0.19 1
Dinoseb ND ug/L 08/31/16 08:18 88-85-708/26/16 08:550.19 0.058 1
Pentachlorophenol ND ug/L 08/31/16 08:18 87-86-508/26/16 08:550.029 0.017 1
Picloram ND ug/L 08/31/16 08:18 1918-02-108/26/16 08:550.096 0.019 1
2,4,5-T ND ug/L 08/31/16 08:18 93-76-508/26/16 08:550.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 08/31/16 08:18 93-72-108/26/16 08:550.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
Pace Analytical Services, Inc.
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Page 5 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Sample:MW-13 Lab ID:92309797001 Collected:08/22/16 14:50 Received:08/23/16 08:28 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)95 %08/31/16 08:18 19719-28-908/26/16 08:5539-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 08/25/16 19:36 7440-36-008/24/16 18:506.0 3.8 1
Arsenic ND ug/L 08/25/16 19:36 7440-38-208/24/16 18:5010.0 2.5 1
Barium 31.7J ug/L 08/25/16 19:36 7440-39-308/24/16 18:501002.5 1
Beryllium ND ug/L 08/25/16 19:36 7440-41-708/24/16 18:501.0 0.50 1
Cadmium ND ug/L 08/25/16 19:36 7440-43-908/24/16 18:501.0 0.50 1
Chromium ND ug/L 08/25/16 19:36 7440-47-308/24/16 18:5010.0 2.5 1
Cobalt ND ug/L 08/25/16 19:36 7440-48-408/24/16 18:5010.0 2.5 1
Copper 3.2J ug/L 08/25/16 19:36 7440-50-808/24/16 18:5010.0 2.5 1
Lead ND ug/L 08/25/16 19:36 7439-92-108/24/16 18:5010.0 2.5 1
Nickel ND ug/L 08/25/16 19:36 7440-02-008/24/16 18:5050.0 2.5 1
Selenium ND ug/L 08/25/16 19:36 7782-49-208/24/16 18:5010.0 5.0 1
Silver ND ug/L 08/25/16 19:36 7440-22-408/24/16 18:5010.0 2.5 1
Thallium ND ug/L 08/25/16 19:36 7440-28-008/24/16 18:505.5 5.0 1
Tin ND ug/L 08/25/16 19:36 7440-31-508/24/16 18:501002.5 1
Vanadium ND ug/L 08/25/16 19:36 7440-62-208/24/16 18:5025.0 2.5 1
Zinc ND ug/L 08/25/16 19:36 7440-66-608/24/16 18:5010.0 5.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 08/24/16 17:17 83-32-908/23/16 12:0010.0 0.25 1
Acenaphthylene ND ug/L 08/24/16 17:17 208-96-808/23/16 12:0010.0 0.21 1
Acetophenone ND ug/L 08/24/16 17:17 98-86-208/23/16 12:0010.0 2.0 1
2-Acetylaminofluorene ND ug/L 08/24/16 17:17 53-96-308/23/16 12:0020.0 0.84 1
4-Aminobiphenyl ND ug/L 08/24/16 17:17 92-67-108/23/16 12:0020.0 0.92 1
Anthracene ND ug/L 08/24/16 17:17 120-12-708/23/16 12:0010.0 0.14 1
Benzo(a)anthracene ND ug/L 08/24/16 17:17 56-55-308/23/16 12:0010.0 0.33 1
Benzo(a)pyrene ND ug/L 08/24/16 17:17 50-32-808/23/16 12:0010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 08/24/16 17:17 205-99-208/23/16 12:0010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 08/24/16 17:17 191-24-208/23/16 12:0010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 08/24/16 17:17 207-08-908/23/16 12:0010.0 0.43 1
Benzyl alcohol ND ug/L 08/24/16 17:17 100-51-608/23/16 12:0020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 08/24/16 17:17 101-55-308/23/16 12:0010.0 1.3 1
Butylbenzylphthalate ND ug/L 08/24/16 17:17 85-68-708/23/16 12:0010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 08/24/16 17:17 59-50-708/23/16 12:0020.0 4.2 1
4-Chloroaniline ND ug/L 08/24/16 17:17 106-47-808/23/16 12:0020.0 3.4 1
Chlorobenzilate ND ug/L 08/24/16 17:17 510-15-608/23/16 12:0010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/16 17:17 111-91-108/23/16 12:0010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 08/24/16 17:17 111-44-408/23/16 12:0010.0 1.5 1
2-Chloronaphthalene ND ug/L 08/24/16 17:17 91-58-708/23/16 12:0010.0 2.2 1
2-Chlorophenol ND ug/L 08/24/16 17:17 95-57-808/23/16 12:0010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 08/24/16 17:17 7005-72-308/23/16 12:0010.0 2.1 1
Chrysene ND ug/L 08/24/16 17:17 218-01-908/23/16 12:0010.0 0.21 1
Diallate ND ug/L 08/24/16 17:17 2303-16-408/23/16 12:0010.0 1.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Sample:MW-13 Lab ID:92309797001 Collected:08/22/16 14:50 Received:08/23/16 08:28 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenz(a,h)anthracene ND ug/L 08/24/16 17:17 53-70-308/23/16 12:0010.0 0.55 1
Dibenzofuran ND ug/L 08/24/16 17:17 132-64-908/23/16 12:0010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 08/24/16 17:17 91-94-108/23/16 12:0020.0 1.4 1
2,4-Dichlorophenol ND ug/L 08/24/16 17:17 120-83-208/23/16 12:0010.0 1.7 1
2,6-Dichlorophenol ND ug/L 08/24/16 17:17 87-65-008/23/16 12:0010.0 1.8 1
Diethylphthalate ND ug/L 08/24/16 17:17 84-66-208/23/16 12:0060001.3 1
Dimethoate ND ug/L 08/24/16 17:17 60-51-508/23/16 12:0020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 08/24/16 17:17 60-11-708/23/16 12:0010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 08/24/16 17:17 57-97-608/23/16 12:0010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 08/24/16 17:17 119-93-708/23/16 12:0010.0 2.1 1
2,4-Dimethylphenol ND ug/L 08/24/16 17:17 105-67-908/23/16 12:0010.0 2.2 1
Dimethylphthalate ND ug/L 08/24/16 17:17 131-11-308/23/16 12:0010.0 1.5 1
Di-n-butylphthalate ND ug/L 08/24/16 17:17 84-74-208/23/16 12:0010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/16 17:17 534-52-108/23/16 12:0050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 08/24/16 17:17 99-65-008/23/16 12:0020.0 1.5 1
2,4-Dinitrophenol ND ug/L 08/24/16 17:17 51-28-508/23/16 12:0050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 08/24/16 17:17 121-14-208/23/16 12:0010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/24/16 17:17 606-20-208/23/16 12:0010.0 1.7 1
Di-n-octylphthalate ND ug/L 08/24/16 17:17 117-84-008/23/16 12:0010.0 0.86 1
Diphenylamine ND ug/L 08/24/16 17:17 122-39-408/23/16 12:0010.0 1.3 1
Disulfoton ND ug/L 08/24/16 17:17 298-04-408/23/16 12:0010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/16 17:17 117-81-708/23/16 12:0015.0 0.85 1
Ethyl methanesulfonate ND ug/L 08/24/16 17:17 62-50-008/23/16 12:0020.0 1.8 1
Famphur ND ug/L 08/24/16 17:17 52-85-708/23/16 12:0020.0 1.7 1
Fluoranthene ND ug/L 08/24/16 17:17 206-44-008/23/16 12:0010.0 0.21 1
Fluorene ND ug/L 08/24/16 17:17 86-73-708/23/16 12:0010.0 0.21 1
Hexachlorobenzene ND ug/L 08/24/16 17:17 118-74-108/23/16 12:0010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 08/24/16 17:17 77-47-408/23/16 12:0010.0 1.8 1
Hexachloroethane ND ug/L 08/24/16 17:17 67-72-108/23/16 12:0010.0 1.5 1
Hexachloropropene ND ug/L 08/24/16 17:17 1888-71-708/23/16 12:0010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/16 17:17 193-39-508/23/16 12:0010.0 0.29 1
Isodrin ND ug/L 08/24/16 17:17 465-73-608/23/16 12:0020.0 2.0 1
Isophorone ND ug/L 08/24/16 17:17 78-59-108/23/16 12:0010.0 1.8 1
Isosafrole ND ug/L 08/24/16 17:17 120-58-108/23/16 12:0010.0 1.8 1
Kepone ND ug/L 08/24/16 17:17 143-50-008/23/16 12:0020.0 3.1 1
Methapyrilene ND ug/L 08/24/16 17:17 91-80-508/23/16 12:001002.7 1
3-Methylcholanthrene ND ug/L 08/24/16 17:17 56-49-508/23/16 12:0010.0 0.82 1
Methyl methanesulfonate ND ug/L 08/24/16 17:17 66-27-308/23/16 12:0010.0 1.3 1
2-Methylnaphthalene ND ug/L 08/24/16 17:17 91-57-608/23/16 12:0010.0 0.28 1
Methyl parathion ND ug/L 08/24/16 17:17 298-00-008/23/16 12:0010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/16 17:17 95-48-708/23/16 12:0010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/16 17:1708/23/16 12:0010.0 1.7 1
1-Naphthalenamine ND ug/L 08/24/16 17:17 134-32-708/23/16 12:0010.0 0.96 1
2-Naphthalenamine ND ug/L 08/24/16 17:17 91-59-808/23/16 12:0010.0 0.98 1
1,4-Naphthoquinone ND ug/L 08/24/16 17:17 130-15-408/23/16 12:0010.0 1.8 1
2-Nitroaniline ND ug/L 08/24/16 17:17 88-74-408/23/16 12:0050.0 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Sample:MW-13 Lab ID:92309797001 Collected:08/22/16 14:50 Received:08/23/16 08:28 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
3-Nitroaniline ND ug/L 08/24/16 17:17 99-09-208/23/16 12:0050.0 2.4 1
4-Nitroaniline ND ug/L 08/24/16 17:17 100-01-608/23/16 12:0020.0 2.5 1
Nitrobenzene ND ug/L 08/24/16 17:17 98-95-308/23/16 12:0010.0 1.7 1
2-Nitrophenol ND ug/L 08/24/16 17:17 88-75-508/23/16 12:0010.0 1.7 1
4-Nitrophenol ND ug/L 08/24/16 17:17 100-02-708/23/16 12:0050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 08/24/16 17:17 99-55-808/23/16 12:0010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 08/24/16 17:17 55-18-508/23/16 12:0020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 08/24/16 17:17 62-75-908/23/16 12:0010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 08/24/16 17:17 924-16-308/23/16 12:0010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/16 17:17 621-64-708/23/16 12:0010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 08/24/16 17:17 86-30-608/23/16 12:0010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 08/24/16 17:17 10595-95-608/23/16 12:0010.0 1.8 1
N-Nitrosopiperidine ND ug/L 08/24/16 17:17 100-75-408/23/16 12:0020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 08/24/16 17:17 930-55-208/23/16 12:0010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 08/24/16 17:17 126-68-108/23/16 12:0010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/16 17:17 108-60-108/23/16 12:0010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 08/24/16 17:17 56-38-208/23/16 12:0010.0 1.1 1
Pentachlorobenzene ND ug/L 08/24/16 17:17 608-93-508/23/16 12:0010.0 2.0 1
Pentachloronitrobenzene ND ug/L 08/24/16 17:17 82-68-808/23/16 12:0020.0 1.0 1
Pentachlorophenol ND ug/L 08/24/16 17:17 87-86-508/23/16 12:0025.0 2.3 1
Phenacetin ND ug/L 08/24/16 17:17 62-44-208/23/16 12:0020.0 0.97 1
Phenanthrene ND ug/L 08/24/16 17:17 85-01-808/23/16 12:0010.0 0.22 1
Phenol ND ug/L 08/24/16 17:1708/23/16 12:0010.0 1.7 1
p-Phenylenediamine ND ug/L 08/24/16 17:17 106-50-308/23/16 12:0010.0 0.96 1
Phorate ND ug/L 08/24/16 17:17 298-02-208/23/16 12:0010.0 1.1 1
Pronamide ND ug/L 08/24/16 17:17 23950-58-508/23/16 12:0010.0 0.97 1
Pyrene ND ug/L 08/24/16 17:17 129-00-008/23/16 12:0010.0 0.19 1
Safrole ND ug/L 08/24/16 17:17 94-59-708/23/16 12:0010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 08/24/16 17:17 95-94-308/23/16 12:0010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 08/24/16 17:17 58-90-208/23/16 12:0010.0 2.3 1
Thionazin ND ug/L 08/24/16 17:17 297-97-208/23/16 12:0020.0 1.2 1
O-Toluidine ND ug/L 08/24/16 17:17 95-53-408/23/16 12:0010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 08/24/16 17:17 95-95-408/23/16 12:0010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 08/24/16 17:17 88-06-208/23/16 12:0010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 08/24/16 17:17 99-35-4 L308/23/16 12:0010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)70 %08/24/16 17:17 4165-60-008/23/16 12:0021-110 1
2-Fluorobiphenyl (S)71 %08/24/16 17:17 321-60-808/23/16 12:0027-110 1
Terphenyl-d14 (S)92 %08/24/16 17:17 1718-51-008/23/16 12:0031-107 1
Phenol-d6 (S)27 %08/24/16 17:17 13127-88-308/23/16 12:0010-110 1
2-Fluorophenol (S)38 %08/24/16 17:17 367-12-408/23/16 12:0012-110 1
2,4,6-Tribromophenol (S)71 %08/24/16 17:17 118-79-608/23/16 12:0027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 08/23/16 21:18 67-64-110010.0 1
Acetonitrile ND ug/L 08/23/16 21:18 75-05-855.0 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Sample:MW-13 Lab ID:92309797001 Collected:08/22/16 14:50 Received:08/23/16 08:28 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrolein ND ug/L 08/23/16 21:18 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 08/23/16 21:18 107-13-12001.9 1
Allyl chloride ND ug/L 08/23/16 21:18 107-05-110.0 1.5 1
Benzene 1.9 ug/L 08/23/16 21:18 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 08/23/16 21:18 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 08/23/16 21:18 75-27-41.0 0.18 1
Bromoform ND ug/L 08/23/16 21:18 75-25-23.0 0.26 1
Bromomethane ND ug/L 08/23/16 21:18 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 08/23/16 21:18 78-93-31000.96 1
Carbon disulfide ND ug/L 08/23/16 21:18 75-15-01001.2 1
Carbon tetrachloride ND ug/L 08/23/16 21:18 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 08/23/16 21:18 108-90-73.0 0.23 1
Chloroethane ND ug/L 08/23/16 21:18 75-00-310.0 0.54 1
Chloroform ND ug/L 08/23/16 21:18 67-66-35.0 0.14 1
Chloromethane 0.41J ug/L 08/23/16 21:18 74-87-31.0 0.11 1
Chloroprene ND ug/L 08/23/16 21:18 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 08/23/16 21:18 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 08/23/16 21:18 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 08/23/16 21:18 106-93-4 L31.0 0.27 1
Dibromomethane ND ug/L 08/23/16 21:18 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 08/23/16 21:18 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 08/23/16 21:18 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 08/23/16 21:18 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 08/23/16 21:18 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 08/23/16 21:18 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 08/23/16 21:18 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 08/23/16 21:18 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 08/23/16 21:18 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 08/23/16 21:18 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 08/23/16 21:18 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 08/23/16 21:18 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 08/23/16 21:18 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/23/16 21:18 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 08/23/16 21:18 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 08/23/16 21:18 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 08/23/16 21:18 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 08/23/16 21:18 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 08/23/16 21:18 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 08/23/16 21:18 87-68-3 L310.0 0.71 1
2-Hexanone ND ug/L 08/23/16 21:18 591-78-650.0 0.46 1
Iodomethane ND ug/L 08/23/16 21:18 74-88-410.0 0.32 1
Isobutanol ND ug/L 08/23/16 21:18 78-83-110035.0 1
Methacrylonitrile ND ug/L 08/23/16 21:18 126-98-71000.93 1
Methylene Chloride ND ug/L 08/23/16 21:18 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 08/23/16 21:18 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/23/16 21:18 108-10-11000.33 1
REPORT OF LABORATORY ANALYSIS
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Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Sample:MW-13 Lab ID:92309797001 Collected:08/22/16 14:50 Received:08/23/16 08:28 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl-tert-butyl ether ND ug/L 08/23/16 21:18 1634-04-41.0 0.21 1
Naphthalene ND ug/L 08/23/16 21:18 91-20-310.0 0.24 1
Propionitrile ND ug/L 08/23/16 21:18 107-12-01503.6 1
Styrene ND ug/L 08/23/16 21:18 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 08/23/16 21:18 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 08/23/16 21:18 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 08/23/16 21:18 127-18-41.0 0.46 1
Toluene ND ug/L 08/23/16 21:18 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 08/23/16 21:18 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 08/23/16 21:18 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 08/23/16 21:18 79-00-51.0 0.29 1
Trichloroethene ND ug/L 08/23/16 21:18 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 08/23/16 21:18 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 08/23/16 21:18 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 08/23/16 21:18 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 08/23/16 21:18 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 08/23/16 21:18 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %08/23/16 21:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/23/16 21:18 17060-07-070-130 1
Toluene-d8 (S)98 %08/23/16 21:18 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 08/24/16 17:30 18496-25-8 M110001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 08/30/16 14:26 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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Page 10 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
326184
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1807111
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 08/25/16 19:203.8
Arsenic ug/L ND 10.0 08/25/16 19:202.5
Barium ug/L ND 100 08/25/16 19:202.5
Beryllium ug/L ND 1.0 08/25/16 19:200.50
Cadmium ug/L ND 1.0 08/25/16 19:200.50
Chromium ug/L ND 10.0 08/25/16 19:202.5
Cobalt ug/L ND 10.0 08/25/16 19:202.5
Copper ug/L ND 10.0 08/25/16 19:202.5
Lead ug/L ND 10.0 08/25/16 19:202.5
Nickel ug/L ND 50.0 08/25/16 19:202.5
Selenium ug/L ND 10.0 08/25/16 19:205.0
Silver ug/L ND 10.0 08/25/16 19:202.5
Thallium ug/L ND 5.5 08/25/16 19:205.0
Tin ug/L ND 100 08/25/16 19:202.5
Vanadium ug/L ND 25.0 08/25/16 19:202.5
Zinc ug/L ND 10.0 08/25/16 19:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1807112LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 490500 98 80-120
Arsenic ug/L 473500 95 80-120
Barium ug/L 510500 102 80-120
Beryllium ug/L 499500 100 80-120
Cadmium ug/L 494500 99 80-120
Chromium ug/L 493500 99 80-120
Cobalt ug/L 493500 99 80-120
Copper ug/L 509500 102 80-120
Lead ug/L 488500 98 80-120
Nickel ug/L 484500 97 80-120
Selenium ug/L 491500 98 80-120
Silver ug/L 249250 99 80-120
Thallium ug/L 473500 95 80-120
Tin ug/L 492500 98 80-120
Vanadium ug/L 489500 98 80-120
Zinc ug/L 489500 98 80-120
REPORT OF LABORATORY ANALYSIS
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Page 11 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1807113MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92309797001
1807114
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12599 1 25500ND491498
Arsenic ug/L 500 96 75-12596 1 25500ND478482
Barium ug/L 500 103 75-125103 0 2550031.7J 546 546
Beryllium ug/L 500 101 75-125101 0 25500ND503505
Cadmium ug/L 500 100 75-125100 1 25500ND499502
Chromium ug/L 500 100 75-125100 1 25500ND498501
Cobalt ug/L 500 99 75-125100 1 25500ND496500
Copper ug/L 500 103 75-125103 0 255003.2J 517 519
Lead ug/L 500 98 75-12598 1 25500ND489493
Nickel ug/L 500 98 75-12599 1 25500ND489493
Selenium ug/L 500 99 75-12599 0 25500ND496498
Silver ug/L 250 100 75-125100 0 25250ND250250
Thallium ug/L 500 95 75-12597 1 25500ND479486
Tin ug/L 500 99 75-125100 1 25500ND494501
Vanadium ug/L 500 99 75-125100 0 25500ND496498
Zinc ug/L 500 99 75-12599 1 25500ND497500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 12 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
326005
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806088
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 08/23/16 12:000.33
1,1,1-Trichloroethane ug/L ND 1.0 08/23/16 12:000.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 08/23/16 12:000.40
1,1,2-Trichloroethane ug/L ND 1.0 08/23/16 12:000.29
1,1-Dichloroethane ug/L ND 5.0 08/23/16 12:000.32
1,1-Dichloroethene ug/L ND 5.0 08/23/16 12:000.56
1,1-Dichloropropene ug/L ND 5.0 08/23/16 12:000.49
1,2,3-Trichloropropane ug/L ND 1.0 08/23/16 12:000.41
1,2,4-Trichlorobenzene ug/L ND 10.0 08/23/16 12:000.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 08/23/16 12:002.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/23/16 12:000.27
1,2-Dichlorobenzene ug/L ND 5.0 08/23/16 12:000.30
1,2-Dichloroethane ug/L ND 1.0 08/23/16 12:000.24
1,2-Dichloropropane ug/L ND 1.0 08/23/16 12:000.27
1,3-Dichlorobenzene ug/L ND 5.0 08/23/16 12:000.24
1,3-Dichloropropane ug/L ND 1.0 08/23/16 12:000.28
1,4-Dichlorobenzene ug/L ND 1.0 08/23/16 12:000.33
2,2-Dichloropropane ug/L ND 15.0 08/23/16 12:000.13
2-Butanone (MEK)ug/L ND 100 08/23/16 12:000.96
2-Hexanone ug/L ND 50.0 08/23/16 12:000.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 08/23/16 12:000.33
Acetone ug/L ND 100 08/23/16 12:0010.0
Acetonitrile ug/L ND 55.0 08/23/16 12:002.2
Acrolein ug/L ND 53.0 08/23/16 12:001.6
Acrylonitrile ug/L ND 200 08/23/16 12:001.9
Allyl chloride ug/L ND 10.0 08/23/16 12:001.5
Benzene ug/L ND 1.0 08/23/16 12:000.25
Bromochloromethane ug/L ND 3.0 08/23/16 12:000.17
Bromodichloromethane ug/L ND 1.0 08/23/16 12:000.18
Bromoform ug/L ND 3.0 08/23/16 12:000.26
Bromomethane ug/L ND 10.0 08/23/16 12:000.29
Carbon disulfide ug/L ND 100 08/23/16 12:001.2
Carbon tetrachloride ug/L ND 1.0 08/23/16 12:000.25
Chlorobenzene ug/L ND 3.0 08/23/16 12:000.23
Chloroethane ug/L ND 10.0 08/23/16 12:000.54
Chloroform ug/L ND 5.0 08/23/16 12:000.14
Chloromethane ug/L ND 1.0 08/23/16 12:000.11
Chloroprene ug/L ND 20.0 08/23/16 12:000.27
cis-1,2-Dichloroethene ug/L ND 5.0 08/23/16 12:000.19
cis-1,3-Dichloropropene ug/L ND 1.0 08/23/16 12:000.13
Dibromochloromethane ug/L ND 3.0 08/23/16 12:000.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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[phone]
Page 13 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806088
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 08/23/16 12:000.21
Dichlorodifluoromethane ug/L ND 5.0 08/23/16 12:000.21
Ethyl methacrylate ug/L ND 10.0 08/23/16 12:000.20
Ethylbenzene ug/L ND 1.0 08/23/16 12:000.30
Hexachloro-1,3-butadiene ug/L ND 10.0 08/23/16 12:000.71
Iodomethane ug/L ND 10.0 08/23/16 12:000.32
Isobutanol ug/L ND 100 08/23/16 12:0035.0
Methacrylonitrile ug/L ND 100 08/23/16 12:000.93
Methyl methacrylate ug/L ND 30.0 08/23/16 12:002.0
Methylene Chloride ug/L ND 1.0 08/23/16 12:000.97
Naphthalene ug/L ND 10.0 08/23/16 12:000.24
Propionitrile ug/L ND 150 08/23/16 12:003.6
Styrene ug/L ND 1.0 08/23/16 12:000.26
Tetrachloroethene ug/L ND 1.0 08/23/16 12:000.46
Toluene ug/L ND 1.0 08/23/16 12:000.26
trans-1,2-Dichloroethene ug/L ND 5.0 08/23/16 12:000.49
trans-1,3-Dichloropropene ug/L ND 1.0 08/23/16 12:000.26
trans-1,4-Dichloro-2-butene ug/L ND 100 08/23/16 12:001.0
Trichloroethene ug/L ND 1.0 08/23/16 12:000.47
Trichlorofluoromethane ug/L ND 1.0 08/23/16 12:000.20
Vinyl acetate ug/L ND 50.0 08/23/16 12:000.35
Vinyl chloride ug/L ND 1.0 08/23/16 12:000.62
Xylene (Total)ug/L ND 5.0 08/23/16 12:000.66
1,2-Dichloroethane-d4 (S)%101 70-130 08/23/16 12:00
4-Bromofluorobenzene (S)%98 70-130 08/23/16 12:00
Toluene-d8 (S)%100 70-130 08/23/16 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806089LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.550 121 80-125
1,1,1-Trichloroethane ug/L 55.850 112 71-129
1,1,2,2-Tetrachloroethane ug/L 56.050 112 79-124
1,1,2-Trichloroethane ug/L 52.250 104 85-125
1,1-Dichloroethane ug/L 53.050 106 73-126
1,1-Dichloroethene ug/L 55.050 110 66-135
1,1-Dichloropropene ug/L 51.950 104 74-135
1,2,3-Trichloropropane ug/L 52.450 105 75-130
1,2,4-Trichlorobenzene ug/L 63.550 127 75-134
1,2-Dibromo-3-chloropropane ug/L 65.050 130 71-133
1,2-Dibromoethane (EDB)ug/L 63.3 L05012783-124
1,2-Dichlorobenzene ug/L 61.350 123 80-133
1,2-Dichloroethane ug/L 49.450 99 67-128
1,2-Dichloropropane ug/L 50.950 102 75-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 14 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806089LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 60.150 120 77-130
1,3-Dichloropropane ug/L 55.650 111 76-131
1,4-Dichlorobenzene ug/L 59.150 118 78-130
2,2-Dichloropropane ug/L 58.050 116 40-160
2-Butanone (MEK)ug/L 117100 117 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 72-135
Acetone ug/L 123100 123 48-146
Acetonitrile ug/L 556500 111 62-150
Acrolein ug/L 292250 117 24-160
Acrylonitrile ug/L 268250 107 40-160
Allyl chloride ug/L 53.150 106 66-137
Benzene ug/L 54.650 109 80-125
Bromochloromethane ug/L 52.150 104 71-125
Bromodichloromethane ug/L 53.750 107 78-124
Bromoform ug/L 51.150 102 71-128
Bromomethane ug/L 53.350 107 40-160
Carbon disulfide ug/L 53.1J50 106 50-160
Carbon tetrachloride ug/L 54.950 110 69-131
Chlorobenzene ug/L 59.850 120 81-122
Chloroethane ug/L 46.850 94 39-148
Chloroform ug/L 52.350 105 73-127
Chloromethane ug/L 58.050 116 44-146
Chloroprene ug/L 56.050 112 75-145
cis-1,2-Dichloroethene ug/L 52.750 105 74-124
cis-1,3-Dichloropropene ug/L 54.750 109 72-132
Dibromochloromethane ug/L 52.650 105 78-125
Dibromomethane ug/L 52.850 106 82-120
Dichlorodifluoromethane ug/L 50.350 101 34-157
Ethyl methacrylate ug/L 60.150 120 82-121
Ethylbenzene ug/L 57.550 115 79-121
Hexachloro-1,3-butadiene ug/L 70.0 L05014072-131
Iodomethane ug/L 123100 123 39-154
Isobutanol ug/L 13101000 131 34-160
Methacrylonitrile ug/L 561500 112 74-134
Methyl methacrylate ug/L 52.950 106 84-124
Methylene Chloride ug/L 51.950 104 64-133
Naphthalene ug/L 62.050 124 73-133
Propionitrile ug/L 538500 108 73-140
Styrene ug/L 60.550 121 84-126
Tetrachloroethene ug/L 57.150 114 78-122
Toluene ug/L 52.750 105 80-121
trans-1,2-Dichloroethene ug/L 53.050 106 71-127
trans-1,3-Dichloropropene ug/L 51.750 103 69-141
trans-1,4-Dichloro-2-butene ug/L 133 L05026640-160
Trichloroethene ug/L 53.850 108 78-122
Trichlorofluoromethane ug/L 51.550 103 53-137
REPORT OF LABORATORY ANALYSIS
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Page 15 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806089LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 105100 105 40-160
Vinyl chloride ug/L 52.050 104 58-137
Xylene (Total)ug/L 170150 113 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1806091MATRIX SPIKE SAMPLE:
MSSpike
Result
92309264008
1,1,1,2-Tetrachloroethane ug/L 22.820 114 70-130ND
1,1,1-Trichloroethane ug/L 62.520 123 70-13037.8
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,2-Trichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethane ug/L 43.020 109 70-13021.3
1,1-Dichloroethene ug/L 37.320 124 70-16612.6
1,1-Dichloropropene ug/L 22.720 113 70-130ND
1,2,3-Trichloropropane ug/L 21.920 109 70-130ND
1,2,4-Trichlorobenzene ug/L 25.620 128 70-130ND
1,2-Dibromo-3-chloropropane ug/L 25.820 129 70-130ND
1,2-Dibromoethane (EDB)ug/L 24.420 122 70-130ND
1,2-Dichlorobenzene ug/L 24.520 123 70-130ND
1,2-Dichloroethane ug/L 20.820 104 70-130ND
1,2-Dichloropropane ug/L 21.720 109 70-130ND
1,3-Dichlorobenzene ug/L 24.720 124 70-130ND
1,3-Dichloropropane ug/L 22.020 110 70-130ND
1,4-Dichlorobenzene ug/L 24.720 123 70-130ND
2,2-Dichloropropane ug/L 24.320 122 70-130ND
2-Butanone (MEK)ug/L 44.4J40 111 70-130ND
2-Hexanone ug/L 50.0J40 125 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.1J40 110 70-130ND
Acetone ug/L 44.6J40 111 70-130ND
Acetonitrile ug/L 241200 120 70-130ND
Acrolein ug/L 129100 129 70-130ND
Acrylonitrile ug/L 108J100 108 70-130ND
Allyl chloride ug/L 25.920 130 70-130ND
Benzene ug/L 23.720 119 70-148ND
Bromochloromethane ug/L 23.420 117 70-130ND
Bromodichloromethane ug/L 22.620 113 70-130ND
Bromoform ug/L 21.820 109 70-130ND
Bromomethane ug/L 22.120 111 70-130ND
Carbon disulfide ug/L 24.6J20 123 70-130ND
Carbon tetrachloride ug/L 25.820 129 70-130ND
Chlorobenzene ug/L 24.620 123 70-146ND
Chloroethane ug/L 24.020 120 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 16 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1806091MATRIX SPIKE SAMPLE:
MSSpike
Result
92309264008
Chloroform ug/L 21.620 108 70-130ND
Chloromethane ug/L 25.020 125 70-130ND
Chloroprene ug/L 25.120 126 70-130ND
cis-1,2-Dichloroethene ug/L 25.220 111 70-1303.1
cis-1,3-Dichloropropene ug/L 22.220 111 70-130ND
Dibromochloromethane ug/L 22.120 110 70-130ND
Dibromomethane ug/L 22.420 112 70-130ND
Dichlorodifluoromethane ug/L 20.720 103 70-130ND
Ethyl methacrylate ug/L 24.020 120 70-130ND
Ethylbenzene ug/L 24.520 123 70-130ND
Hexachloro-1,3-butadiene ug/L 30.3 M02015170-130ND
Iodomethane ug/L 45.340 113 70-130ND
Isobutanol ug/L 517400 129 70-130ND
Methacrylonitrile ug/L 219200 110 70-130ND
Methyl methacrylate ug/L 21.5J20 108 70-130ND
Methylene Chloride ug/L 21.820 106 70-130ND
Naphthalene ug/L 22.720 113 70-130ND
Propionitrile ug/L 220200 110 70-130ND
Styrene ug/L 24.820 124 70-130ND
Tetrachloroethene ug/L 24.920 120 70-1300.86J
Toluene ug/L 23.020 115 70-155ND
trans-1,2-Dichloroethene ug/L 23.620 118 70-130ND
trans-1,3-Dichloropropene ug/L 21.120 105 70-130ND
trans-1,4-Dichloro-2-butene ug/L 28.8J M02014470-130ND
Trichloroethene ug/L 25.720 120 69-1511.7
Trichlorofluoromethane ug/L 23.820 119 70-130ND
Vinyl acetate ug/L 42.4J40 106 70-130ND
Vinyl chloride ug/L 23.720 119 70-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92309264007
1806090SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 34.1 2 3033.5
1,1-Dichloroethene ug/L 1.6J 5 301.5
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 17 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92309264007
1806090SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.99J 300.97J
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 2.2 3 302.1
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L 0.56J 300.57J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 1.1J 10 301.0
Chloroethane ug/L 3.0J 1 302.9
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 4.7J 5 304.4
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 0.54J 300.50J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 18 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92309264007
1806090SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 300.86J
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 2.1 1 302.1
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%104 4100
4-Bromofluorobenzene (S)%95 499
Toluene-d8 (S)%100 2103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 19 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
325982
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1805867
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 08/24/16 12:210.050
4,4'-DDE ug/L ND 0.10 08/24/16 12:210.050
4,4'-DDT ug/L ND 0.10 08/24/16 12:210.050
Aldrin ug/L ND 0.050 08/24/16 12:210.050
alpha-BHC ug/L ND 0.050 08/24/16 12:210.050
beta-BHC ug/L ND 0.050 08/24/16 12:210.050
Chlordane (Technical)ug/L ND 0.50 08/24/16 12:210.20
delta-BHC ug/L ND 0.050 08/24/16 12:210.050
Dieldrin ug/L ND 0.075 08/24/16 12:210.050
Endosulfan I ug/L ND 0.10 08/24/16 12:210.050
Endosulfan II ug/L ND 0.10 08/24/16 12:210.050
Endosulfan sulfate ug/L ND 0.10 08/24/16 12:210.050
Endrin ug/L ND 0.10 08/24/16 12:210.050
Endrin aldehyde ug/L ND 0.10 08/24/16 12:210.050
gamma-BHC (Lindane)ug/L ND 0.050 08/24/16 12:210.050
Heptachlor ug/L ND 0.050 08/24/16 12:210.050
Heptachlor epoxide ug/L ND 0.075 08/24/16 12:210.050
Methoxychlor ug/L ND 1.0 08/24/16 12:210.15
Toxaphene ug/L ND 1.5 08/24/16 12:210.20
Decachlorobiphenyl (S)%52 20-130 08/24/16 12:21
Tetrachloro-m-xylene (S)%68 20-130 08/24/16 12:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1805868LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.21.25 85 20-150
4,4'-DDE ug/L 0.20.25 81 20-150
4,4'-DDT ug/L 0.23.25 91 20-150
Aldrin ug/L 0.18.25 72 20-150
alpha-BHC ug/L 0.18.25 74 20-150
beta-BHC ug/L 0.21.25 86 20-150
delta-BHC ug/L 0.22.25 87 20-150
Dieldrin ug/L 0.20.25 79 20-150
Endosulfan I ug/L 0.21.25 85 20-150
Endosulfan II ug/L 0.23.25 92 20-150
Endosulfan sulfate ug/L 0.23.25 94 20-150
Endrin ug/L 0.23.25 91 20-150
Endrin aldehyde ug/L 0.20.25 81 20-150
gamma-BHC (Lindane)ug/L 0.20.25 79 20-150
Heptachlor ug/L 0.20.25 82 20-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 20 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1805868LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.21.25 83 20-150
Methoxychlor ug/L 0.82J.74 111 20-150
Decachlorobiphenyl (S)%39 20-130
Tetrachloro-m-xylene (S)%71 20-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1805869MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92309612003
1805870
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4,4'-DDD ug/L .5 88 20-15079 11 30.5ND 0.44 0.39
4,4'-DDE ug/L .5 84 20-15075 11 30.5ND 0.41 0.37
4,4'-DDT ug/L .5 96 20-15085 12 30.5ND 0.48 0.42
Aldrin ug/L .5 74 20-15067 9 30.5ND 0.37 0.33
alpha-BHC ug/L .5 75 20-15069 9 30.5ND 0.37 0.34
beta-BHC ug/L .5 90 20-15082 9 30.5ND 0.44 0.40
delta-BHC ug/L .5 89 20-15082 8 30.5ND 0.44 0.40
Dieldrin ug/L .5 82 20-15075 8 30.5ND 0.41 0.37
Endosulfan I ug/L .5 88 20-15079 10 30.5ND 0.44 0.39
Endosulfan II ug/L .5 97 20-15087 11 30.5ND 0.48 0.43
Endosulfan sulfate ug/L .5 100 20-15089 11 30.5ND 0.49 0.44
Endrin ug/L .5 96 20-15087 9 30.5ND 0.47 0.43
Endrin aldehyde ug/L .5 85 20-15077 10 30.5ND 0.42 0.38
gamma-BHC (Lindane)ug/L .5 81 20-15074 9 30.5ND 0.40 0.37
Heptachlor ug/L .5 85 20-15078 8 30.5ND 0.42 0.39
Heptachlor epoxide ug/L .5 86 20-15078 9 30.5ND 0.42 0.39
Methoxychlor ug/L 1.5 116 20-150105 10 301.5ND 1.7J 1.6J
Decachlorobiphenyl (S)%74 20-13057
Tetrachloro-m-xylene (S)%75 20-13071
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 21 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
326095
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806444
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 08/24/16 14:500.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 08/24/16 14:500.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 08/24/16 14:500.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 08/24/16 14:500.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 08/24/16 14:500.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 08/24/16 14:500.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 08/24/16 14:500.50
Decachlorobiphenyl (S)%49 10-132 08/24/16 14:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806445LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1806446
PCB-1016 (Aroclor 1016)ug/L 3.15 62 50-150673.3 7 30
PCB-1260 (Aroclor 1260)ug/L 3.95 78 50-150783.9 0 30
Decachlorobiphenyl (S)%73 10-13250
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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[phone]
Page 22 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
317247
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1685821
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 08/31/16 04:180.042
2,4,5-TP (Silvex)ug/L ND 0.19 08/31/16 04:180.049
2,4-D ug/L ND 0.94 08/31/16 04:180.22
2,4-DB ug/L ND 1.9 08/31/16 04:180.51
Bentazon ug/L ND 0.094 08/31/16 04:180.047
Dalapon ug/L ND 0.91 08/31/16 04:180.43
Dicamba ug/L ND 0.094 08/31/16 04:180.030
Dichlorprop ug/L ND 0.65 08/31/16 04:180.19
Dinoseb ug/L ND 0.19 08/31/16 04:180.057
Pentachlorophenol ug/L ND 0.028 08/31/16 04:180.017
Picloram ug/L ND 0.094 08/31/16 04:180.019
2,4-DCAA (S)%86 39-139 08/31/16 04:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1685822LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1686120
2,4,5-T ug/L 1.21.2 101 37-133971.2 4 40
2,4,5-TP (Silvex)ug/L 1.21.2 98 53-134931.1 5 40
2,4-D ug/L 5.86 96 35-124905.4 6 40
2,4-DB ug/L 12.412 103 31-13210212.3 1 40
Bentazon ug/L 0.64.6 107 51-125990.59 8 40
Dalapon ug/L 5.86 97 10-122975.8 0 40
Dicamba ug/L 0.57.6 95 44-125920.55 3 40
Dichlorprop ug/L 4.14.2 97 70-130933.9 4 40
Dinoseb ug/L 0.671.2 56 13-116550.66 2 40
Pentachlorophenol ug/L 0.18.18 99 39-170980.18 1 40
Picloram ug/L 0.63.6 105 10-127990.60 6 40
2,4-DCAA (S)%90 39-13986 40
REPORT OF LABORATORY ANALYSIS
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Page 23 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
326024
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806191
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 08/24/16 16:441.7
1,3,5-Trinitrobenzene ug/L ND 10.0 08/24/16 16:441.1
1,3-Dinitrobenzene ug/L ND 20.0 08/24/16 16:441.5
1,4-Naphthoquinone ug/L ND 10.0 08/24/16 16:441.8
1-Naphthalenamine ug/L ND 10.0 08/24/16 16:440.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 08/24/16 16:441.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 08/24/16 16:442.3
2,4,5-Trichlorophenol ug/L ND 10.0 08/24/16 16:442.2
2,4,6-Trichlorophenol ug/L ND 10.0 08/24/16 16:441.9
2,4-Dichlorophenol ug/L ND 10.0 08/24/16 16:441.7
2,4-Dimethylphenol ug/L ND 10.0 08/24/16 16:442.2
2,4-Dinitrophenol ug/L ND 50.0 08/24/16 16:446.5
2,4-Dinitrotoluene ug/L ND 10.0 08/24/16 16:441.2
2,6-Dichlorophenol ug/L ND 10.0 08/24/16 16:441.8
2,6-Dinitrotoluene ug/L ND 10.0 08/24/16 16:441.7
2-Acetylaminofluorene ug/L ND 20.0 08/24/16 16:440.84
2-Chloronaphthalene ug/L ND 10.0 08/24/16 16:442.2
2-Chlorophenol ug/L ND 10.0 08/24/16 16:441.5
2-Methylnaphthalene ug/L ND 10.0 08/24/16 16:440.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/24/16 16:441.7
2-Naphthalenamine ug/L ND 10.0 08/24/16 16:440.98
2-Nitroaniline ug/L ND 50.0 08/24/16 16:442.8
2-Nitrophenol ug/L ND 10.0 08/24/16 16:441.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/24/16 16:441.7
3,3'-Dichlorobenzidine ug/L ND 20.0 08/24/16 16:441.4
3,3'-Dimethylbenzidine ug/L ND 10.0 08/24/16 16:442.1
3-Methylcholanthrene ug/L ND 10.0 08/24/16 16:440.82
3-Nitroaniline ug/L ND 50.0 08/24/16 16:442.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 08/24/16 16:441.7
4-Aminobiphenyl ug/L ND 20.0 08/24/16 16:440.92
4-Bromophenylphenyl ether ug/L ND 10.0 08/24/16 16:441.3
4-Chloro-3-methylphenol ug/L ND 20.0 08/24/16 16:444.2
4-Chloroaniline ug/L ND 20.0 08/24/16 16:443.4
4-Chlorophenylphenyl ether ug/L ND 10.0 08/24/16 16:442.1
4-Nitroaniline ug/L ND 20.0 08/24/16 16:442.5
4-Nitrophenol ug/L ND 50.0 08/24/16 16:445.8
5-Nitro-o-toluidine ug/L ND 10.0 08/24/16 16:441.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 08/24/16 16:440.77
Acenaphthene ug/L ND 10.0 08/24/16 16:440.25
Acenaphthylene ug/L ND 10.0 08/24/16 16:440.21
Acetophenone ug/L ND 10.0 08/24/16 16:442.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 24 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806191
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 08/24/16 16:440.14
Benzo(a)anthracene ug/L ND 10.0 08/24/16 16:440.33
Benzo(a)pyrene ug/L ND 10.0 08/24/16 16:440.30
Benzo(b)fluoranthene ug/L ND 10.0 08/24/16 16:440.28
Benzo(g,h,i)perylene ug/L ND 10.0 08/24/16 16:440.38
Benzo(k)fluoranthene ug/L ND 10.0 08/24/16 16:440.43
Benzyl alcohol ug/L ND 20.0 08/24/16 16:443.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/24/16 16:441.7
bis(2-Chloroethyl) ether ug/L ND 10.0 08/24/16 16:441.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 08/24/16 16:440.85
Butylbenzylphthalate ug/L ND 10.0 08/24/16 16:440.75
Chlorobenzilate ug/L ND 10.0 08/24/16 16:440.72
Chrysene ug/L ND 10.0 08/24/16 16:440.21
Di-n-butylphthalate ug/L ND 10.0 08/24/16 16:441.1
Di-n-octylphthalate ug/L ND 10.0 08/24/16 16:440.86
Diallate ug/L ND 10.0 08/24/16 16:441.3
Dibenz(a,h)anthracene ug/L ND 10.0 08/24/16 16:440.55
Dibenzofuran ug/L ND 10.0 08/24/16 16:441.8
Diethylphthalate ug/L ND 6000 08/24/16 16:441.3
Dimethoate ug/L ND 20.0 08/24/16 16:440.92
Dimethylphthalate ug/L ND 10.0 08/24/16 16:441.5
Diphenylamine ug/L ND 10.0 08/24/16 16:441.3
Disulfoton ug/L ND 10.0 08/24/16 16:441.4
Ethyl methanesulfonate ug/L ND 20.0 08/24/16 16:441.8
Famphur ug/L ND 20.0 08/24/16 16:441.7
Fluoranthene ug/L ND 10.0 08/24/16 16:440.21
Fluorene ug/L ND 10.0 08/24/16 16:440.21
Hexachlorobenzene ug/L ND 10.0 08/24/16 16:441.1
Hexachlorocyclopentadiene ug/L ND 10.0 08/24/16 16:441.8
Hexachloroethane ug/L ND 10.0 08/24/16 16:441.5
Hexachloropropene ug/L ND 10.0 08/24/16 16:441.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/24/16 16:440.29
Isodrin ug/L ND 20.0 08/24/16 16:442.0
Isophorone ug/L ND 10.0 08/24/16 16:441.8
Isosafrole ug/L ND 10.0 08/24/16 16:441.8
Kepone ug/L ND 20.0 08/24/16 16:443.1
Methapyrilene ug/L ND 100 08/24/16 16:442.7
Methyl methanesulfonate ug/L ND 10.0 08/24/16 16:441.3
Methyl parathion ug/L ND 10.0 08/24/16 16:441.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 08/24/16 16:442.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/24/16 16:442.1
N-Nitrosodiethylamine ug/L ND 20.0 08/24/16 16:441.8
N-Nitrosodimethylamine ug/L ND 10.0 08/24/16 16:441.3
N-Nitrosodiphenylamine ug/L ND 10.0 08/24/16 16:441.3
N-Nitrosomethylethylamine ug/L ND 10.0 08/24/16 16:441.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 25 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806191
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 08/24/16 16:441.9
N-Nitrosopyrrolidine ug/L ND 10.0 08/24/16 16:442.5
Nitrobenzene ug/L ND 10.0 08/24/16 16:441.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 08/24/16 16:441.8
O-Toluidine ug/L ND 10.0 08/24/16 16:441.6
P-Dimethylaminoazobenzene ug/L ND 10.0 08/24/16 16:440.35
p-Phenylenediamine ug/L ND 10.0 08/24/16 16:440.96
Parathion (Ethyl parathion)ug/L ND 10.0 08/24/16 16:441.1
Pentachlorobenzene ug/L ND 10.0 08/24/16 16:442.0
Pentachloronitrobenzene ug/L ND 20.0 08/24/16 16:441.0
Pentachlorophenol ug/L ND 25.0 08/24/16 16:442.3
Phenacetin ug/L ND 20.0 08/24/16 16:440.97
Phenanthrene ug/L ND 10.0 08/24/16 16:440.22
Phenol ug/L ND 10.0 08/24/16 16:441.7
Phorate ug/L ND 10.0 08/24/16 16:441.1
Pronamide ug/L ND 10.0 08/24/16 16:440.97
Pyrene ug/L ND 10.0 08/24/16 16:440.19
Safrole ug/L ND 10.0 08/24/16 16:441.5
Thionazin ug/L ND 20.0 08/24/16 16:441.2
2,4,6-Tribromophenol (S)%72 27-110 08/24/16 16:44
2-Fluorobiphenyl (S)%73 27-110 08/24/16 16:44
2-Fluorophenol (S)%42 12-110 08/24/16 16:44
Nitrobenzene-d5 (S)%75 21-110 08/24/16 16:44
Phenol-d6 (S)%30 10-110 08/24/16 16:44
Terphenyl-d14 (S)%99 31-107 08/24/16 16:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806192LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1806193
1,2,4,5-Tetrachlorobenzene ug/L 39.950 80 16-1297437.1 7 30
1,3,5-Trinitrobenzene ug/L 173 L05034555-125324162 6 30
1,3-Dinitrobenzene ug/L 45.750 91 30-1228140.7 12 30
1,4-Naphthoquinone ug/L 47.350 95 31-1208441.9 12 30
1-Naphthalenamine ug/L 38.450 77 37-1268040.1 4 30
2,2'-Oxybis(1-chloropropane)ug/L 40.350 81 18-1207436.9 9 30
2,3,4,6-Tetrachlorophenol ug/L 88.750 177 54-27617989.6 1 30
2,4,5-Trichlorophenol ug/L 46.850 94 43-1138944.7 5 30
2,4,6-Trichlorophenol ug/L 46.850 94 42-1208743.3 8 30
2,4-Dichlorophenol ug/L 45.650 91 30-1207939.5 14 30
2,4-Dimethylphenol ug/L 47.050 94 29-1118240.9 14 30
2,4-Dinitrophenol ug/L 161250 64 19-13256139 14 30
2,4-Dinitrotoluene ug/L 50.050 100 58-12810351.4 3 30
2,6-Dichlorophenol ug/L 38.650 77 54-1286934.5 11 30
2,6-Dinitrotoluene ug/L 55.750 111 54-1299748.7 13 30
REPORT OF LABORATORY ANALYSIS
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Page 26 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806192LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1806193
2-Acetylaminofluorene ug/L 56.150 112 81-16010150.3 11 30
2-Chloronaphthalene ug/L 46.450 93 43-1178843.8 6 30
2-Chlorophenol ug/L 39.750 79 37-1206331.5 23 30
2-Methylnaphthalene ug/L 41.850 84 33-1207135.7 16 30
2-Methylphenol(o-Cresol)ug/L 36.950 74 31-1206632.8 12 30
2-Naphthalenamine ug/L 48.050 96 41-13610251.0 6 30
2-Nitroaniline ug/L 87.5100 87 48-1217473.6 17 30
2-Nitrophenol ug/L 44.850 90 25-1168743.3 3 30
3&4-Methylphenol(m&p Cresol)ug/L 32.450 65 23-1205527.6 16 30
3,3'-Dichlorobenzidine ug/L 92.8250 37 10-1543690.9 2 30
3,3'-Dimethylbenzidine ug/L 70.4100 70 10-1577372.8 3 30
3-Methylcholanthrene ug/L 41.450 83 65-1307939.5 5 30
3-Nitroaniline ug/L 83.5100 84 43-1157877.7 7 30
4,6-Dinitro-2-methylphenol ug/L 103100 103 44-1249393.0 10 30
4-Aminobiphenyl ug/L 41.050 82 21-1258743.3 5 30
4-Bromophenylphenyl ether ug/L 47.450 95 34-1138944.5 6 30
4-Chloro-3-methylphenol ug/L 98.5100 99 31-1108180.8 20 30
4-Chloroaniline ug/L 78.2100 78 20-1207170.9 10 30
4-Chlorophenylphenyl ether ug/L 49.050 98 34-1168844.0 11 30
4-Nitroaniline ug/L 89.8100 90 46-1287877.8 14 30
4-Nitrophenol ug/L 107250 43 11-1203997.6 9 30
5-Nitro-o-toluidine ug/L 61.050 122 78-16010753.6 13 30
7,12-Dimethylbenz(a)anthracene ug/L 44.450 89 47-1248944.6 0 30
Acenaphthene ug/L 41.850 84 48-1147939.5 6 30
Acenaphthylene ug/L 45.050 90 48-1128341.7 7 30
Acetophenone ug/L 42.650 85 24-1207638.1 11 30
Anthracene ug/L 44.550 89 57-1188040.0 11 30
Benzo(a)anthracene ug/L 43.250 86 56-1218642.9 1 30
Benzo(a)pyrene ug/L 44.150 88 55-1278743.5 2 30
Benzo(b)fluoranthene ug/L 44.350 89 53-1288944.3 0 30
Benzo(g,h,i)perylene ug/L 40.650 81 54-1258040.1 1 30
Benzo(k)fluoranthene ug/L 45.450 91 51-1239045.2 0 30
Benzyl alcohol ug/L 74.0100 74 27-1206565.2 13 30
bis(2-Chloroethoxy)methane ug/L 43.150 86 32-1208240.9 5 30
bis(2-Chloroethyl) ether ug/L 42.250 84 33-1116733.4 23 30
bis(2-Ethylhexyl)phthalate ug/L 50.550 101 50-1459949.5 2 30
Butylbenzylphthalate ug/L 51.650 103 54-1389447.1 9 30
Chlorobenzilate ug/L 51.950 104 65-1329145.3 13 30
Chrysene ug/L 45.550 91 58-1278341.5 9 30
Di-n-butylphthalate ug/L 47.150 94 56-1259246.1 2 30
Di-n-octylphthalate ug/L 50.650 101 50-1348944.3 13 30
Diallate ug/L 45.750 91 47-1238542.4 8 30
Dibenz(a,h)anthracene ug/L 38.450 77 53-1297738.3 0 30
Dibenzofuran ug/L 40.550 81 45-1208341.4 2 30
Diethylphthalate ug/L 46.1J50 92 53-1209346.5J 1 30
Dimethoate ug/L 39.050 78 57-1397637.9 3 30
Dimethylphthalate ug/L 46.650 93 55-1168240.8 13 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806192LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1806193
Diphenylamine ug/L 51.550 103 42-1209145.3 13 30
Disulfoton ug/L 43.050 86 49-1568140.6 6 30
Ethyl methanesulfonate ug/L 42.2 R1508443-1205929.7 35 30
Famphur ug/L 47.9100 48 40-1604242.2 13 30
Fluoranthene ug/L 42.850 86 57-1259045.0 5 30
Fluorene ug/L 49.050 98 53-1188743.6 12 30
Hexachlorobenzene ug/L 45.350 91 49-1168743.3 4 30
Hexachlorocyclopentadiene ug/L 34.750 69 26-1586432.0 8 30
Hexachloroethane ug/L 34.550 69 30-1145929.7 15 30
Hexachloropropene ug/L 33.250 66 13-1376230.8 7 30
Indeno(1,2,3-cd)pyrene ug/L 40.150 80 55-1288040.2 0 30
Isodrin ug/L 47.050 94 68-1298442.2 11 30
Isophorone ug/L 47.450 95 31-1189346.4 2 30
Isosafrole ug/L 44.650 89 48-1078542.5 5 30
Kepone ug/L 56.4100 56 10-1245050.5 11 30
Methapyrilene ug/L 45.5J50 91 40-1608944.6J 30
Methyl methanesulfonate ug/L 31.750 63 25-1145025.1 23 30
Methyl parathion ug/L 45.250 90 58-1379547.7 6 30
N-Nitroso-di-n-butylamine ug/L 44.950 90 36-1157336.3 21 30
N-Nitroso-di-n-propylamine ug/L 50.450 101 32-1198844.0 13 30
N-Nitrosodiethylamine ug/L 49.650 99 47-1157738.6 25 30
N-Nitrosodimethylamine ug/L 23.350 47 13-1203819.2 19 30
N-Nitrosodiphenylamine ug/L 51.550 103 43-1209145.3 13 30
N-Nitrosomethylethylamine ug/L 43.950 88 39-1207135.4 21 30
N-Nitrosopiperidine ug/L 47.850 96 43-1139145.5 5 30
N-Nitrosopyrrolidine ug/L 41.350 83 32-1107738.3 8 30
Nitrobenzene ug/L 43.250 86 33-1108643.0 1 30
O,O,O-Triethylphosphorothioate ug/L 41.050 82 51-1277638.0 8 30
O-Toluidine ug/L 39.850 80 27-1207235.8 11 30
P-Dimethylaminoazobenzene ug/L 27.4100 27 10-1202423.8 14 30
p-Phenylenediamine ug/L 44.350 89 72-1438743.5 2 30
Parathion (Ethyl parathion)ug/L 55.550 111 56-1409647.8 15 30
Pentachlorobenzene ug/L 42.250 84 30-1378039.9 6 30
Pentachloronitrobenzene ug/L 54.550 109 70-12410251.1 6 30
Pentachlorophenol ug/L 91.4250 37 10-1373688.8 3 30
Phenacetin ug/L 45.250 90 60-1309547.3 5 30
Phenanthrene ug/L 41.750 83 57-1178039.8 5 30
Phenol ug/L 22.650 45 10-1203416.8 29 30
Phorate ug/L 62.750 125 55-12611858.9 6 30
Pronamide ug/L 42.850 86 75-1248542.4 1 30
Pyrene ug/L 48.350 97 55-1228140.7 17 30
Safrole ug/L 44.850 90 41-1207437.1 19 30
Thionazin ug/L 53.150 106 63-1379346.7 13 30
2,4,6-Tribromophenol (S)%99 27-11094
2-Fluorobiphenyl (S)%78 27-11073
2-Fluorophenol (S)%49 12-11040
Nitrobenzene-d5 (S)%82 21-11083
REPORT OF LABORATORY ANALYSIS
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Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806192LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1806193
Phenol-d6 (S)%37 10-11028
Terphenyl-d14 (S)%99 31-10791
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1806708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35261375003
1806709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4,5-Tetrachlorobenzene ug/L 7 301.7U 36.8 34.3
1,3,5-Trinitrobenzene ug/L R134301.1U 355 252
1,3-Dinitrobenzene ug/L R134301.5U 85.9 61.2
1,4-Naphthoquinone ug/L R137301.8U 69.3 47.5
1-Naphthalenamine ug/L R131300.96U 31.1 22.7
2,2'-Oxybis(1-chloropropane)ug/L 15 301.6U 38.5 33.3
2,3,4,6-Tetrachlorophenol ug/L R135302.3U 202 142
2,4,5-Trichlorophenol ug/L 25 302.2U 75.4 58.5
2,4,6-Trichlorophenol ug/L 8 301.9U 63.1 58.1
2,4-Dichlorophenol ug/L 9 301.7U 35.1 38.3
2,4-Dimethylphenol ug/L 6 302.2U 36.4 38.8
2,4-Dinitrophenol ug/L R133306.5U 367 264
2,4-Dinitrotoluene ug/L R150301.2U 120 71.7
2,6-Dichlorophenol ug/L 2 301.8U 32.6 33.2
2,6-Dinitrotoluene ug/L R138301.7U 103 70.1
2-Acetylaminofluorene ug/L R146300.84U 121 75.9
2-Chloronaphthalene ug/L 8 302.2U 49.0 45.4
2-Chlorophenol ug/L 28 301.5U 39.6 29.8
2-Methylnaphthalene ug/L 2 300.28U 34.8 35.7
2-Methylphenol(o-Cresol)ug/L 18 301.7U 37.2 31.2
2-Naphthalenamine ug/L R131300.98U 42.5 31.2
2-Nitroaniline ug/L 26 302.8U 145 112
2-Nitrophenol ug/L 5 301.7U 34.9 36.7
3&4-Methylphenol(m&p
Cresol)ug/L 28 301.7U 50.0 37.8
3,3'-Dichlorobenzidine ug/L R137301.4U 183 125
3,3'-Dimethylbenzidine ug/L 302.1U 14.0J 18.3J
3-Methylcholanthrene ug/L R145300.82U 95.7 60.7
3-Nitroaniline ug/L 302.4U 100 70.9J
4,6-Dinitro-2-methylphenol ug/L R137301.7U 211 146
4-Aminobiphenyl ug/L 9 300.92U 53.4 48.9
4-Bromophenylphenyl ether ug/L R134301.3U 87.9 62.6
4-Chloro-3-methylphenol ug/L 10 304.2U 129 117
4-Chloroaniline ug/L 303.4U 17.3J 18.3J
4-Chlorophenylphenyl ether ug/L 30 302.1U 81.8 60.3
4-Nitroaniline ug/L R149302.5U 187 114
4-Nitrophenol ug/L 28 305.8U 313 235
5-Nitro-o-toluidine ug/L R142301.2U 115 74.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1806708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35261375003
1806709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
7,12-
Dimethylbenz(a)anthracene ug/L R140300.77U 103 68.4
Acenaphthene ug/L 15 300.25U 55.6 47.9
Acenaphthylene ug/L 16 300.21U 58.6 49.8
Acetophenone ug/L R132302.0U 44.7 32.4
Anthracene ug/L R138300.14U 90.9 61.7
Benzo(a)anthracene ug/L R137300.33U 102 69.6
Benzo(a)pyrene ug/L R144300.30U 101 65.2
Benzo(b)fluoranthene ug/L R138300.28U 105 71.6
Benzo(g,h,i)perylene ug/L R137300.38U 95.9 65.9
Benzo(k)fluoranthene ug/L R141300.43U 102 67.4
Benzyl alcohol ug/L 26 303.4U 64.7 49.6
bis(2-Chloroethoxy)methane ug/L 10 301.7U 32.5 35.8
bis(2-Chloroethyl) ether ug/L 22 301.5U 38.9 31.3
bis(2-Ethylhexyl)phthalate ug/L R163300.85U 120 62.9
Butylbenzylphthalate ug/L R165300.75U 124 63.0
Chlorobenzilate ug/L R1423011373.7
Chrysene ug/L R138300.21U 97.2 66.0
Di-n-butylphthalate ug/L R152301.1U 104 61.3
Di-n-octylphthalate ug/L R166300.86U 108 54.2
Diallate ug/L R137301.3U 92.4 63.4
Dibenz(a,h)anthracene ug/L R141300.55U 92.1 60.9
Dibenzofuran ug/L 28 301.8U 69.3 52.4
Diethylphthalate ug/L R155301.3U 111J 63.0J
Dimethoate ug/L R1323089.3 64.5
Dimethylphthalate ug/L R142301.5U 93.4 61.1
Diphenylamine ug/L R143301.3U 97.8 62.9
Disulfoton ug/L R1343090.6 64.4
Ethyl methanesulfonate ug/L 301.8U 32.2J 27.6J
Famphur ug/L 18 30182151
Fluoranthene ug/L 28 300.21U 90.3 67.8
Fluorene ug/L R134300.21U 86.3 61.3
Hexachlorobenzene ug/L R132301.1U 86.8 62.8
Hexachlorocyclopentadiene ug/L 5 301.8U 27.8 26.4
Hexachloroethane ug/L 19 301.5U 31.5 25.9
Hexachloropropene ug/L 12 301.6U 28.0 24.7
Indeno(1,2,3-cd)pyrene ug/L R141300.29U 96.0 63.5
Isodrin ug/L R135302.0U 80.7 56.5
Isophorone ug/L 7 301.8U 40.1 43.2
Isosafrole ug/L 9 301.8U 49.1 45.0
Kepone ug/L 3 303.1U 95.6 92.4
Methapyrilene ug/L 302.7U 12.8J 15.0J
Methyl methanesulfonate ug/L 21 301.3U 27.1 22.1
Methyl parathion ug/L R1353098.8 69.1
N-Nitroso-di-n-butylamine ug/L 9 302.2U 42.1 46.1
N-Nitroso-di-n-propylamine ug/L R132302.1U 50.2 36.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1806708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35261375003
1806709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodiethylamine ug/L 301.8U 46.3 34.9J
N-Nitrosodimethylamine ug/L 301.3U 20.1 19.1J
N-Nitrosodiphenylamine ug/L R143301.3U 97.8 62.9
N-Nitrosomethylethylamine ug/L 17 301.8U 37.1 31.3
N-Nitrosopiperidine ug/L 301.9U 37.6J 39.8J
N-Nitrosopyrrolidine ug/L 17 302.5U 43.5 36.7
Nitrobenzene ug/L 8 301.7U 36.8 39.7
O,O,O-
Triethylphosphorothioate ug/L 1 301.8U 30.2 30.3
O-Toluidine ug/L 301.6U 10J 7.5J
P-
Dimethylaminoazobenzene ug/L R141300.35U 58.6 38.7
p-Phenylenediamine ug/L R133300.96U 92.3 66.5
Parathion (Ethyl parathion)ug/L R1343010976.8
Pentachlorobenzene ug/L 26 302.0U 64.8 50.0
Pentachloronitrobenzene ug/L R1373011176.4
Pentachlorophenol ug/L 28 30191145
Phenacetin ug/L R132300.97U 93.3 67.5
Phenanthrene ug/L R133300.22U 87.9 63.2
Phenol ug/L 8 301.7U 22.3 20.5
Phorate ug/L R1343012991.5
Pronamide ug/L R133300.97U 91.1 65.6
Pyrene ug/L R148300.19U 108 66.2
Safrole ug/L 4 301.5U 36.6 35.1
Thionazin ug/L R150301.2U 111 66.7
2,4,6-Tribromophenol (S)%94 27-11070
2-Fluorobiphenyl (S)%38 27-11037
2-Fluorophenol (S)%26 12-11021
Nitrobenzene-d5 (S)%33 21-11036
Phenol-d6 (S)%21 10-11019
Terphenyl-d14 (S)%97 31-10760
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 31 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
326142
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1806738
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 08/24/16 17:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1806739LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 509J500 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1806740MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92309797001
1806741
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M3500080-1200 10500NDNDND
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1806742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92309269003
1806743
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 103 80-120102 0 10500ND513J511J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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Page 32 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
326641
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92309797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1809570
Associated Lab Samples:92309797001
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 08/30/16 14:104.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1809571LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 98.4100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1809572MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92309530001
1809573
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 102 75-125100 2 10100ND103102
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1809574MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92309797001
1809575
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 99 75-12597 2 10100ND10199.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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[phone]
Page 33 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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[phone]
Page 34 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92309797
WAYNE LINED (MW-13)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92309797001 325982 326151MW-13 EPA 3510 EPA 8081
92309797001 326095 326152MW-13 EPA 3510 EPA 8082
92309797001 317247 317862MW-13 EPA 8151 EPA 8151
92309797001 326184 326229MW-13 EPA 3010A EPA 6010
92309797001 326024 326194MW-13 EPA 3510 EPA 8270
92309797001 326005MW-13 EPA 8260
92309797001 326142MW-13 SM 4500-S2D
92309797001 326641MW-13 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/01/2016 11:52 AM
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[phone]
Page 35 of 37
Page 36 of 37
Page 37 of 37
#=CL#
September 09, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311076
92311076
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE LINED MSWLF-MW-13
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Huntersville, NC 28078
[phone]
Page 2 of 11
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Lab ID Sample ID Matrix Date Collected Date Received
92311076001 MW-13 Water 09/01/16 08:30 09/02/16 11:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311076001 MW-13 RSK 175 Modified 3 PASI-CWDV
SM 4500-Cl-E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Sample:MW-13 Lab ID:92311076001 Collected:09/01/16 08:30 Received:09/02/16 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Ethane ND ug/L 09/07/16 13:47 74-84-0 N210.0 10.0 1
Ethene ND ug/L 09/07/16 13:47 74-85-1 N210.0 10.0 1
Methane 4340 ug/L 09/07/16 13:47 74-82-8 N210.0 10.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 12800 ug/L 09/08/16 17:28 16887-00-610005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327617
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Associated Lab Samples:92311076001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815307
Associated Lab Samples:92311076001
Matrix:Water
AnalyzedMDL
Ethane ug/L ND 10.0 N209/07/16 10:1310.0
Ethene ug/L ND 10.0 N209/07/16 10:1310.0
Methane ug/L ND 10.0 N209/07/16 10:1310.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815308LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1815309
Ethane ug/L 601 N26589170-13094618 3 20
Ethene ug/L 1090 N211209770-13087969 11 20
Methane ug/L 395 N239610070-13089354 11 20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327852
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92311076001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1816733
Associated Lab Samples:92311076001
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 09/08/16 17:20500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1816734LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2050020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1816735MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311072004
1816736
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000024990-110249 0 101000033.7 mg/L 58600 58600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1816737MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311106003
1816738
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M1100008490-11084 0 101000028.3 mg/L 36700 36700
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 04:24 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 04:24 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311076
WAYNE LINED MSWLF-MW-13
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311076001 327617MW-13 RSK 175 Modified
92311076001 327852MW-13 SM 4500-Cl-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 04:24 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 11
Page 10 of 11
Page 11 of 11
#=CL#
September 09, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311079
92311079
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Wayne MSWLF-SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Lab ID Sample ID Matrix Date Collected Date Received
92311079001 SW-1 Water 09/01/16 16:40 09/02/16 08:50
92311079002 SW-6 Water 09/01/16 16:55 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311079001 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92311079002 SW-6 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92311079001 Collected:09/01/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:34 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:34 7440-38-209/06/16 21:0010.0 2.5 1
Barium 175 ug/L 09/07/16 23:34 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:34 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:34 7440-43-909/06/16 21:001.0 0.50 1
Chromium 3.5J ug/L 09/07/16 23:34 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:34 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:34 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:34 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:34 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:34 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:34 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:34 7440-28-009/06/16 21:005.5 5.0 1
Vanadium ND ug/L 09/07/16 23:34 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:34 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 08:03 67-64-1 L310010.0 1
Acrylonitrile ND ug/L 09/08/16 08:03 107-13-12001.9 1
Benzene ND ug/L 09/08/16 08:03 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 08:03 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 08:03 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 08:03 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 08:03 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 08:03 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 08:03 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 08:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 08:03 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 08:03 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 08:03 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 08:03 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 08:03 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 08:03 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 08:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 08:03 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 08:03 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/08/16 08:03 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 08:03 110-57-6 L31001.0 1
1,1-Dichloroethane ND ug/L 09/08/16 08:03 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 08:03 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 08:03 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 08:03 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 08:03 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 08:03 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 08:03 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 08:03 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92311079001 Collected:09/01/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/08/16 08:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/08/16 08:03 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 08:03 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 09/08/16 08:03 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 08:03 108-10-11000.33 1
Styrene ND ug/L 09/08/16 08:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 08:03 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 08:03 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 08:03 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 08:03 109-99-910.0 3.1 1
Toluene 0.42J ug/L 09/08/16 08:03 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/08/16 08:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 08:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 08:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 08:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 08:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 08:03 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 08:03 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 08:03 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 08:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 08:03 17060-07-070-130 1
Toluene-d8 (S)102 %09/08/16 08:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-6 Lab ID:92311079002 Collected:09/01/16 16:55 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:41 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:41 7440-38-209/06/16 21:0010.0 2.5 1
Barium 166 ug/L 09/07/16 23:41 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:41 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:41 7440-43-909/06/16 21:001.0 0.50 1
Chromium 3.0J ug/L 09/07/16 23:41 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:41 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:41 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:41 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:41 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:41 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:41 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:41 7440-28-009/06/16 21:005.5 5.0 1
Vanadium ND ug/L 09/07/16 23:41 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:41 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 08:20 67-64-1 L310010.0 1
Acrylonitrile ND ug/L 09/08/16 08:20 107-13-12001.9 1
Benzene ND ug/L 09/08/16 08:20 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 08:20 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 08:20 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 08:20 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 08:20 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 08:20 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 08:20 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 08:20 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 08:20 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 08:20 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 08:20 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 08:20 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 08:20 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 08:20 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 08:20 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 08:20 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 08:20 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/08/16 08:20 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 08:20 110-57-6 L31001.0 1
1,1-Dichloroethane ND ug/L 09/08/16 08:20 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 08:20 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 08:20 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 08:20 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 08:20 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 08:20 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 08:20 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 08:20 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-6 Lab ID:92311079002 Collected:09/01/16 16:55 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/08/16 08:20 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/08/16 08:20 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 08:20 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 09/08/16 08:20 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 08:20 108-10-11000.33 1
Styrene ND ug/L 09/08/16 08:20 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 08:20 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 08:20 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 08:20 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 08:20 109-99-910.0 3.1 1
Toluene 0.76J ug/L 09/08/16 08:20 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/08/16 08:20 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 08:20 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 08:20 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 08:20 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 08:20 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 08:20 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 08:20 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 08:20 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 08:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/08/16 08:20 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 08:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327495
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92311079001, 92311079002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814776
Associated Lab Samples:92311079001, 92311079002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/07/16 22:513.8
Arsenic ug/L ND 10.0 09/07/16 22:512.5
Barium ug/L ND 100 09/07/16 22:512.5
Beryllium ug/L ND 1.0 09/07/16 22:510.50
Cadmium ug/L ND 1.0 09/07/16 22:510.50
Chromium ug/L ND 10.0 09/07/16 22:512.5
Cobalt ug/L ND 10.0 09/07/16 22:512.5
Copper ug/L ND 10.0 09/07/16 22:512.5
Lead ug/L ND 10.0 09/07/16 22:512.5
Nickel ug/L ND 50.0 09/07/16 22:512.5
Selenium ug/L ND 10.0 09/07/16 22:515.0
Silver ug/L ND 10.0 09/07/16 22:512.5
Thallium ug/L ND 5.5 09/07/16 22:515.0
Vanadium ug/L ND 25.0 09/07/16 22:512.5
Zinc ug/L ND 10.0 09/07/16 22:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814777LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 463500 93 80-120
Arsenic ug/L 449500 90 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 502500 100 80-120
Lead ug/L 471500 94 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 478500 96 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 460500 92 80-120
Vanadium ug/L 490500 98 80-120
Zinc ug/L 474500 95 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814778MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311078001
1814779
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 85 75-12586 0 25500ND428430
Arsenic ug/L 500 87 75-12588 1 255005.8J 443 446
Barium ug/L 500 104 75-125104 1 2550020.2J 539 542
Beryllium ug/L 500 100 75-125101 1 25500ND499503
Cadmium ug/L 500 97 75-12597 0 25500ND484485
Chromium ug/L 500 104 75-125106 2 2550020.1 541 550
Cobalt ug/L 500 95 75-12595 0 25500ND475475
Copper ug/L 500 102 75-125103 0 255003.1J 514 516
Lead ug/L 500 93 75-12593 0 255004.4J 469 469
Nickel ug/L 500 95 75-12596 1 25500ND476481
Selenium ug/L 500 92 75-12592 1 25500ND462466
Silver ug/L 250 98 75-12598 0 25250ND245245
Thallium ug/L 500 90 75-12591 1 25500ND451456
Vanadium ug/L 500 99 75-125100 1 2550028.4 524 527
Zinc ug/L 500 96 75-12596 0 25500ND482485
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311079001, 92311079002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311079001, 92311079002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/08/16 00:010.33
1,1,1-Trichloroethane ug/L ND 1.0 09/08/16 00:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/08/16 00:010.40
1,1,2-Trichloroethane ug/L ND 1.0 09/08/16 00:010.29
1,1-Dichloroethane ug/L ND 5.0 09/08/16 00:010.32
1,1-Dichloroethene ug/L ND 5.0 09/08/16 00:010.56
1,2,3-Trichloropropane ug/L ND 1.0 09/08/16 00:010.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/08/16 00:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/16 00:010.27
1,2-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.30
1,2-Dichloroethane ug/L ND 1.0 09/08/16 00:010.24
1,2-Dichloropropane ug/L ND 1.0 09/08/16 00:010.27
1,4-Dichlorobenzene ug/L ND 1.0 09/08/16 00:010.33
2-Butanone (MEK)ug/L ND 100 09/08/16 00:010.96
2-Hexanone ug/L ND 50.0 09/08/16 00:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/08/16 00:010.33
Acetone ug/L ND 100 09/08/16 00:0110.0
Acrylonitrile ug/L ND 200 09/08/16 00:011.9
Benzene ug/L ND 1.0 09/08/16 00:010.25
Bromochloromethane ug/L ND 3.0 09/08/16 00:010.17
Bromodichloromethane ug/L ND 1.0 09/08/16 00:010.18
Bromoform ug/L ND 3.0 09/08/16 00:010.26
Bromomethane ug/L ND 10.0 09/08/16 00:010.29
Carbon disulfide ug/L ND 100 09/08/16 00:011.2
Carbon tetrachloride ug/L ND 1.0 09/08/16 00:010.25
Chlorobenzene ug/L ND 3.0 09/08/16 00:010.23
Chloroethane ug/L ND 10.0 09/08/16 00:010.54
Chloroform ug/L ND 5.0 09/08/16 00:010.14
Chloromethane ug/L ND 1.0 09/08/16 00:010.11
cis-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.13
Dibromochloromethane ug/L ND 3.0 09/08/16 00:010.21
Dibromomethane ug/L ND 10.0 09/08/16 00:010.21
Ethylbenzene ug/L ND 1.0 09/08/16 00:010.30
Iodomethane ug/L ND 10.0 09/08/16 00:010.32
Methylene Chloride ug/L ND 1.0 09/08/16 00:010.97
Styrene ug/L ND 1.0 09/08/16 00:010.26
Tetrachloroethene ug/L ND 1.0 09/08/16 00:010.46
Tetrahydrofuran ug/L ND 10.0 09/08/16 00:013.1
Toluene ug/L ND 1.0 09/08/16 00:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311079001, 92311079002
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/08/16 00:011.0
Trichloroethene ug/L ND 1.0 09/08/16 00:010.47
Trichlorofluoromethane ug/L ND 1.0 09/08/16 00:010.20
Vinyl acetate ug/L ND 50.0 09/08/16 00:010.35
Vinyl chloride ug/L ND 1.0 09/08/16 00:010.62
Xylene (Total)ug/L ND 5.0 09/08/16 00:010.66
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/16 00:01
4-Bromofluorobenzene (S)%101 70-130 09/08/16 00:01
Toluene-d8 (S)%103 70-130 09/08/16 00:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 80-125
1,1,1-Trichloroethane ug/L 54.750 109 71-129
1,1,2,2-Tetrachloroethane ug/L 53.850 108 79-124
1,1,2-Trichloroethane ug/L 53.150 106 85-125
1,1-Dichloroethane ug/L 54.750 109 73-126
1,1-Dichloroethene ug/L 59.450 119 66-135
1,2,3-Trichloropropane ug/L 54.150 108 75-130
1,2-Dibromo-3-chloropropane ug/L 52.050 104 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 57.850 116 80-133
1,2-Dichloroethane ug/L 54.050 108 67-128
1,2-Dichloropropane ug/L 53.150 106 75-132
1,4-Dichlorobenzene ug/L 55.150 110 78-130
2-Butanone (MEK)ug/L 133100 133 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 158 L010015848-146
Acrylonitrile ug/L 297250 119 40-160
Benzene ug/L 55.650 111 80-125
Bromochloromethane ug/L 59.350 119 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 53.7 F35010740-160
Carbon disulfide ug/L 74.3J F35014950-160
Carbon tetrachloride ug/L 58.250 116 69-131
Chlorobenzene ug/L 55.950 112 81-122
Chloroethane ug/L 55.850 112 39-148
Chloroform ug/L 53.150 106 73-127
Chloromethane ug/L 52.150 104 44-146
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,3-Dichloropropene ug/L 57.450 115 72-132
Dibromochloromethane ug/L 57.550 115 78-125
Dibromomethane ug/L 52.150 104 82-120
Ethylbenzene ug/L 54.250 108 79-121
Iodomethane ug/L 124100 124 39-154
Methylene Chloride ug/L 58.550 117 64-133
Styrene ug/L 56.350 113 84-126
Tetrachloroethene ug/L 54.450 109 78-122
Tetrahydrofuran ug/L 609500 122 69-148
Toluene ug/L 54.550 109 80-121
trans-1,2-Dichloroethene ug/L 55.850 112 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
trans-1,4-Dichloro-2-butene ug/L 92.9J F3,L05018640-160
Trichloroethene ug/L 55.550 111 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 123100 123 40-160
Vinyl chloride ug/L 52.350 105 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 19.720 99 70-130ND
1,2-Dichloropropane ug/L 21.120 106 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2-Butanone (MEK)ug/L 39.8J40 99 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.1J40 98 70-130ND
Acetone ug/L 37.7J40 73 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Benzene ug/L 21.920 109 70-148ND
Bromochloromethane ug/L 21.120 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
Bromodichloromethane ug/L 20.920 104 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 108 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 20.320 101 70-130ND
Ethylbenzene ug/L 21.120 106 70-130ND
Iodomethane ug/L 40.040 100 70-130ND
Methylene Chloride ug/L 18.620 93 70-130ND
Styrene ug/L 21.820 109 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Tetrahydrofuran ug/L 205200 101 70-130ND
Toluene ug/L 21.420 103 70-1550.76J
trans-1,2-Dichloroethene ug/L 21.520 107 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 22.620 113 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 39.8J40 100 70-130ND
Vinyl chloride ug/L 18.220 91 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L 0.66J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 7105
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%108 6102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311079001 327495 327550SW-1 EPA 3010A EPA 6010
92311079002 327495 327550SW-6 EPA 3010A EPA 6010
92311079001 327693SW-1 EPA 8260
92311079002 327693SW-6 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 19
Page 18 of 19
Page 19 of 19
Appendix B
Field Sampling Parameter Data Sheet(s)