19057_Pepsi_Bottiling_2016_Annual_Redevelopement_Update_Rpt_2017_02_01

S:\AAA-Master Projects\Lennar (LEN)\LEN-001\Annual Report\Report\Pepsi Bottiling Facility (BFProj# 19057-15-060)_Annual Report.doc
Via Email

February 1, 2017

LMC New Bern Holdings, LP
201 S. Tryon St., Ste. 1000
Charlotte, NC 28202

Attn: Mr. Chris Helsabeck

Re: 2016 Annual Redevelopment Update Report
Pepsi Bottling Facility
2764 and 2820 South Blvd.
Charlotte, North Carolina
Brownfields Project# 19057-15-060
H&H Job No. LEN-001

Dear Chris:

1.0 Introduction

H&H has prepared this annual redevelopment update report to document environmental related
activities occurring in 2016 at the former Pepsi Bottling facility (BF Project# 19057-15-060)
located at 2734 and 2820 South Boulevard in Charlotte, North Carolina (Site or subject Site). A
Site location map is provided as Figure 1. This report has been prepared in accordance with
Land Use Restriction (LUR) 3 in the executed Brownfields Agreement for the Site.

In 2016, Pepsi Bottling ceased operations at the Site, and the former bottling facility was razed in
September/October 2016. Asbestos containing building materials were removed and properly
disposed prior to demolition of the Pepsi Buildings. In 2016, surface grading to remove organic
rich surficial soils at the Brownfields property was conducted upon completion of demolition
activities. In addition, during demolition of the facility, the General Contractor (GC) discovered
a below ground oil-water separator (OWS). A brief discussion of Site activities associated with
Mr. Chris Helsabeck
February 1, 2017
Page 2
S:\AAA-Master Projects\Lennar (LEN)\LEN-001\Annual Report\Report\Pepsi Bottiling Facility (BFProj# 19057-15-060)_Annual Report.doc

the surface grubbing and OWS is provided in the following sections.

2.0 Surface Soil Assessment Activities

To evaluate the potential for impacts in organic rich shallow soil to be removed from the Site
during proposed surface grubbing activities, H&H collected soil samples in northern, central,
eastern, southern, and western portions of the Brownfields property on September 27, 2016 in
accordance with the plan approved by The North Carolina Department of Environmental Quality
(DEQ) Brownfields Program. Aliquot soil sample locations are depicted on Figure 2.

Shallow soil borings were advanced with a decontaminated stainless steel hand auger in areas at
the Site where surface grubbing was to be performed and aliquot soil samples were collected
from the center of the hand auger bucket at each boring location. Aliquot soil samples from each
area were then combined and homogenized to form composite soil samples representative of
each of the five portions of the Site where surface soil would be removed.

The five composite soil samples, labeled SS-N (from the northern portions of the site), SS-E
(from the eastern portions of the Site), SS-S (from the southern portions of the Site), SS-W (from
the western portions of the Site), and SS-C (from the central portions of the Site), were placed
directly into laboratory-supplied sample containers, labeled with the sample identification, date,
time, and requested analyses. The sample containers were then placed in a laboratory-supplied
cooler and iced. The sample cooler was delivered to Contest Analytical Laboratory under
standard chain of custody protocols for laboratory analysis of semi-volatile organic compounds
(SVOCs) by EPA Method 8270D, and Priority Pollutant List (PPL) metals plus hexavalent
chromium by EPA Methods 6020A/7471B/7196A. Additionally, H&H collected a grab sample
from one aliquot sample location in each of the five areas for laboratory analysis of volatile
organic compounds (VOCs) by EPA Method 8260B.

Mr. Chris Helsabeck
February 1, 2017
Page 3
S:\AAA-Master Projects\Lennar (LEN)\LEN-001\Annual Report\Report\Pepsi Bottiling Facility (BFProj# 19057-15-060)_Annual Report.doc

Laboratory analytical results are summarized in Table 1. As indicated in Table 1, low levels of
the polynuclear aromatic hydrocarbon (PAH) benzo(a)pyrene were detected at concentrations
exceeding the Inactive Hazardous Sites Branch (IHSB) Protection of Groundwater and
Residential Preliminary Soil Remediation Goal (PSRGs) in composite soil samples SS-N, SS-C,
and SS-S. Additionally, the PAH benzo(a)anthracene was detected above the Protection of
Groundwater and Residential PSRG in soil sample SS-C. No compound concentrations
exceeded their Industrial PSRGs. No other compound concentrations were detected above
PSRGs in any other samples collected at the Site during the surface soil assessment.

Because PAHs were detected at concentrations exceeding PSRGs in three of the soil samples at
the Site, in November 2016 approximately 315.78 tons of soil generated during surface grubbing
activities was transported to the Republic Services Landfill in Concord, NC for disposal.
Disposal documents are provided in Appendix B.

3.0 Oil Water Separator Activities

A sub-grade OWS located near the former mechanic bay along New Bern Street was discovered
by the GC during Pepsi Bottling facility demolition activities. The approximate location of the
OWS is shown on Figure 2. Additionally, a single man-hole settling chamber collecting water
discharge from the OWS prior to discharge to the municipal sanitary sewer system was
discovered near the OWS along New Bern Street (Figure 2).

On October 26, 2016, H&H personnel inspected the OWS and settling chamber. A sample of the
residual material in the OWS chamber was collected for disposal characterization purposes. At
the request of the disposal contractor, the OWS sample was submitted for laboratory analysis of
VOCs by EPA Method 8260B, SVOCs by EPA Method 8270D, and Toxicity Characteristic
Leaching Procedure (TCLP) metals by EPA Method 6010D.

Mr. Chris Helsabeck
February 1, 2017
Page 4
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Laboratory analytical results for the residual OWS material indicated that the VOC ethylbenzene
(0.063 mg/kg) and the SVOC bis(2-ethylhexyl)phthalate (32 mg/kg) were detected in the sample.
The TCLP metals analysis indicated the presence of cadmium (0.062 mg/L) and lead (0.28
mg/L) but at concentrations below EPA regulatory levels for characteristically hazardous
material. The laboratory analytical report is provided in Appendix A.

On November 1, 2016, H&H personnel mobilized to the Site to provide oversight during
removal of approximately 1,250-gallons of water and sludge from the oil-water separator and
nearby single man-hole settling chamber. The water and sludge were removed via vac truck and
transported off-site to EVO’s permitted facility located near Winton-Salem for disposal as non-
hazardous waste. A certificate of disposal for the water and sludge removed from the OWS
system is provided in Appendix B.

On November 2, 2016, H&H mobilized to the Site to provide oversight during removal of the
OWS. The concrete OWS was removed using a track-mounted excavator and staged on plastic
prior to being transported to the Republic Services landfill. Upon removal of the separator,
H&H observed minor staining on the sidewalls of the OWS basin near the influent and effluent
plumbing. Five soil samples were collected from the OWS basin and field screened for evidence
of staining, odors, and organic vapors using a calibrated photoionization detector (PID). Based
on field screening results and per the approved Environmental Management Plan (EMP), one
soil sample (OWS-E) was collected from the eastern sidewall of the OWS basin from an area of
obvious staining located approximately 5 feet below the ground surface (ft bgs). The staining
and potential impacts in the OWS basin were observed below the final redevelopment grade in
this area of the Site.

The soil sample was collected from soil not in direct contact with the excavator bucket and
placed directly into laboratory-supplied glassware, labeled with the sample identification, date,
time, and requested analyses. The sample was then placed on ice in a laboratory-supplied cooler
Mr. Chris Helsabeck
February 1, 2017
Page 5
S:\AAA-Master Projects\Lennar (LEN)\LEN-001\Annual Report\Report\Pepsi Bottiling Facility (BFProj# 19057-15-060)_Annual Report.doc

and delivered to TestAmerica Laboratories, Inc. under standard chain of custody protocols for
analysis of VOCs by EPA Method 8260B, SVOCs by EPA Method 8270D, and PPL metals plus
hexavalent chromium by EPA Methods 6010D/7471B/7196A to document the potential presence
of residual soil impacts in this area.

Laboratory analytical results for the OWS basin sample are summarized in Table 1 and indicate
that no VOC or SVOC compounds were detected above laboratory reporting limits. Several
metals including trivalent chromium (20.5 mg/kg), copper (11.1 mg/kg), lead (19.4 mg/kg),
manganese (78.5 mg/kg), nickel (4.54 mg/kg), and zinc (14.7 mg/kg) were detected above
laboratory reporting limits, but below IHSB PSRGs. Upon completion of the sampling
activities, the OWS basin was backfilled with clean soil and compacted for planned grading
activities.

4.0 Summary

In September 2016, H&H conducted surface soil assessment activities at the Site to evaluate the
potential for impacts in areas where proposed surface grubbing activities were needed for
redevelopment. Results of the surface soil assessment indicated that PAH compounds were
detected above IHSB PSRGs in several areas. Therefore, approximately 315.78 tons of soil
generated during surface grubbing were transported off-site to the Republic Services landfill in
Concord, NC for disposal.

During demolition of the former Pepsi Bottling facility, the GC discovered a sub-grade oil-water
separator near the former mechanic bay on the southern portion of the Site near New Bern Street.
Additionally, a single man-hole settling chamber that collected water discharge from the oil-
water separator system was discovered near New Bern Street. H&H provided oversight during
the removal of residual material from the oil-water separator and the settling chamber for off-site
disposal and during removal of the oil-water separator. Minor staining on the sidewalls of the
Mr. Chris Helsabeck
February 1, 2017
Page 6
S:\AAA-Master Projects\Lennar (LEN)\LEN-001\Annual Report\Report\Pepsi Bottiling Facility (BFProj# 19057-15-060)_Annual Report.doc

OWS basin near the influent and effluent plumbing was observed at a depth of approximately 5
ft bgs and below the final redevelopment grade in this portion of the Site. A soil sample was
collected for laboratory analysis from stained soil located on the eastern sidewall of the basin.
Laboratory analytical results did not identify significant impacts in OWS basin soil. Upon
completion of the OWS removal and sampling activities, the basin was backfilled with clean soil
and compacted for planned grading activities.

Redevelopment activities at the Brownfields property are ongoing and are being conducted in
accordance with the approved Environmental Management Plan.

We appreciate the opportunity to assist with this project. Should you have any questions or need
additional information, please do not hesitate to call us at [phone].

Very truly yours,

Hart & Hickman, PC
Ralph McGee, PG Steven C. Hart, PG
Project Geologist Principal

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Table 1 (Page 1 of 1)Hart & Hickman, PC
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA, 1991
TITLE
PROJECT
SITE LOCATION MAP
PEPSI BOTTLING OF CHARLOTTE
2734 & 2820 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
01-31-2017 0
1LEN-001
SO
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NEW BERN STREET
OWS-E
LEGEND
SITE PROPERTY BOUNDARY
SS-N ALIQUOT SOIL SAMPLE
LOCATION
SS-E ALIQUOT SOIL SAMPLE
LOCATION
SS-W ALIQUOT SOIL SAMPLE
LOCATION
SS-C ALIQUOT SOIL SAMPLE
LOCATION
SS-S ALIQUOT SOIL SAMPLE
LOCATION
NON-IMPACTED AREA
IMPACTED
OWS-E SAMPLE LOCATION
OIL/WATER SEPARATOR
MAN-HOLE SETTLING CHAMBER
JOB NO. LEN-001
REVISION NO. 0DATE: 2-1-17
FIGURE NO. 2
PEPSI BOTTLING OF CHARLOTTE
2734 & 2820 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2014).
2.ALIQUOT SOIL SAMPLES COLLECTED FROM EACH
AREA WERE HOMOGENIZED AND ONE COMPOSITE
SOIL SAMPLE REPRESENTATIVE OF EACH AREA
WAS COLLECTED FOR LABORATORY ANALYSIS.
3.SOIL ASSESSMENT ACTIVITIES WERE CONDUCTED
BY H&H ON 9/27/16.
OWS-E
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Appendix A

Laboratory Analytical Results
Page 1 of 60
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 8
16I1188-01 8
16I1188-02 14
16I1188-03 20
16I1188-04 26
16I1188-05 32
Sample Preparation Information 38
QC Data 40
Volatile Organic Compounds by GC/MS 40
B159499 40
Semivolatile Organic Compounds by GC/MS 45
B159422 45
Metals Analyses (Total) 50
B159329 50
B159436 51
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 52
B159654 52
Flag/Qualifier Summary 53
Certifications 54
Chain of Custody/Sample Receipt 58
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Table of Contents
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
10/31/2016
Hart & Hickman (Charlotte)
Ralph McGee
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: LEN-001
Lab Submittal Date: 10/26/2016
Prism Work Order: 6100472
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
L Parameter reported with possible low bias. LCS recovery below the QC limit.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
RL Increased RL because of the sample matrix.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 20
Sample Receipt Summary
10/31/2016
Prism Work Order: 6100472
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6100472-01 10/26/16OWS 10/26/16Solid
Samples were received in good condition at 1.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 20
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6100472
10/31/2016
Summary of Detections
General Method
32 mg/kg dry6100472-01 OWS Bis(2-Ethylhexyl)phthalate *8270DSemivolatile Organic Compounds by GC/MS
0.062 mg/L6100472-01 OWS Cadmium *6010DTCLP Metals
0.28 mg/L6100472-01 OWS Lead *6010DTCLP Metals
0.063 mg/kg dry6100472-01 OWS Ethylbenzene *8260BVolatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 20
Laboratory Report
10/31/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: OWS
Prism Sample ID: 6100472-01
Prism Work Order: 6100472
Time Collected: 10/26/16 08:40
Time Submitted: 10/26/16 09:20
General Chemistry Parameters
64.4 *SM2540 G P6J054610.100 10/28/16 15:54 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS RL
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.401,2,4-Trichlorobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.391,2-Dichlorobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.361,3-Dichlorobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.371,4-Dichlorobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.491-Methylnaphthalene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.482,4,6-Trichlorophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.492,4-Dichlorophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.392,4-Dimethylphenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.362,4-Dinitrophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.312,4-Dinitrotoluene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.342,6-Dinitrotoluene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.372-Chloronaphthalene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.362-Chlorophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.412-Methylnaphthalene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.332-Methylphenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.472-Nitrophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.513,3'-Dichlorobenzidine
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.323/4-Methylphenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.384,6-Dinitro-2-methylphenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.444-Bromophenyl phenyl ether
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.364-Chloro-3-methylphenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.314-Chloroaniline
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.334-Chlorophenyl phenyl ether
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.394-Nitrophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.35Acenaphthene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.37Acenaphthylene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.41Anthracene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.34Azobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.34Benzo(a)anthracene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.28Benzo(a)pyrene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.30Benzo(b)fluoranthene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.28Benzo(g,h,i)perylene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.34Benzo(k)fluoranthene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.22Benzoic Acid
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.34Benzyl alcohol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.44bis(2-Chloroethoxy)methane
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.36Bis(2-Chloroethyl)ether
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.44Bis(2-chloroisopropyl)ether
32 *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.38Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 20
Laboratory Report
10/31/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: OWS
Prism Sample ID: 6100472-01
Prism Work Order: 6100472
Time Collected: 10/26/16 08:40
Time Submitted: 10/26/16 09:20
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.36Butyl benzyl phthalate
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.32Chrysene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.31Dibenzo(a,h)anthracene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.39Dibenzofuran
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.35Diethyl phthalate
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.34Dimethyl phthalate
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.36Di-n-butyl phthalate
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.31Di-n-octyl phthalate
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.33Fluoranthene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.37Fluorene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.41Hexachlorobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.46Hexachlorobutadiene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.46Hexachlorocyclopentadiene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.43Hexachloroethane
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.29Indeno(1,2,3-cd)pyrene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.35Isophorone
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.41Naphthalene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.36Nitrobenzene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.40N-Nitroso-di-n-propylamine
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.39N-Nitrosodiphenylamine
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.30Pentachlorophenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.33Phenanthrene
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.38Phenol
BRL *8270D P6J050652.6 10/31/16 10:23 JMVmg/kg dry 0.34Pyrene
Surrogate Recovery Control Limits
39-13263 %2,4,6-Tribromophenol
44-11574 %2-Fluorobiphenyl
35-11566 %2-Fluorophenol
37-12250 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12758 %Terphenyl-d14
TCLP Extraction by EPA 1311
Complete *1311 P6J0521110/28/16 7:00 JABN/ATCLP Extraction
TCLP Metals
BRL *6010D P6J052210.050 10/28/16 20:04 bgmmg/L 0.012Arsenic
BRL *6010D P6J052215.0 10/28/16 20:04 bgmmg/L 0.0065Barium
0.062 *6010D P6J052210.025 10/28/16 20:04 bgmmg/L 0.00065Cadmium
BRL *6010D P6J052210.25 10/28/16 20:04 bgmmg/L 0.0038Chromium
0.28 *6010D P6J052210.050 10/28/16 20:04 bgmmg/L 0.0080Lead
BRL *6010D P6J052210.10 10/28/16 20:04 bgmmg/L 0.022Selenium
BRL *6010D P6J052210.25 10/28/16 20:04 bgmmg/L 0.00050Silver
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 20
Laboratory Report
10/31/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: OWS
Prism Sample ID: 6100472-01
Prism Work Order: 6100472
Time Collected: 10/26/16 08:40
Time Submitted: 10/26/16 09:20
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000641,1,1,2-Tetrachloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000381,1,1-Trichloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000531,1,2,2-Tetrachloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000691,1,2-Trichloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000221,1-Dichloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000341,1-Dichloroethylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000431,1-Dichloropropylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000441,2,3-Trichlorobenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000991,2,3-Trichloropropane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000581,2,4-Trichlorobenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000591,2,4-Trimethylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000311,2-Dibromoethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000371,2-Dichlorobenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000461,2-Dichloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000481,2-Dichloropropane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000591,3,5-Trimethylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000511,3-Dichlorobenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000391,3-Dichloropropane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000311,4-Dichlorobenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000372,2-Dichloropropane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000402-Chlorotoluene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000464-Chlorotoluene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.000374-Isopropyltoluene
BRL *8260B P6J054810.078 10/31/16 13:12 ANGmg/kg dry 0.0019Acetone
BRL *8260B P6J054810.0047 10/31/16 13:12 ANGmg/kg dry 0.00045Benzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00065Bromobenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00043Bromochloromethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00043Bromodichloromethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00088Bromoform
BRL *8260B P6J054810.016 10/31/16 13:12 ANGmg/kg dry 0.00096Bromomethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00039Carbon Tetrachloride
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00041Chlorobenzene
BRL *8260B P6J054810.016 10/31/16 13:12 ANGmg/kg dry 0.00065Chloroethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00056Chloroform
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00052Chloromethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00033cis-1,2-Dichloroethylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00026cis-1,3-Dichloropropylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00032Dibromochloromethane
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00035Dichlorodifluoromethane
0.063 *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00030Ethylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00032Isopropyl Ether
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00046Isopropylbenzene (Cumene)
BRL *8260B P6J054810.016 10/31/16 13:12 ANGmg/kg dry 0.00072m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 20
Laboratory Report
10/31/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: OWS
Prism Sample ID: 6100472-01
Prism Work Order: 6100472
Time Collected: 10/26/16 08:40
Time Submitted: 10/26/16 09:20
BRL *8260B P6J054810.078 10/31/16 13:12 ANGmg/kg dry 0.00070Methyl Butyl Ketone (2-Hexanone)
BRL *8260B P6J054810.16 10/31/16 13:12 ANGmg/kg dry 0.00070Methyl Ethyl Ketone (2-Butanone)
BRL *8260B P6J054810.078 10/31/16 13:12 ANGmg/kg dry 0.00066Methyl Isobutyl Ketone
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00044Methylene Chloride
BRL *8260B P6J054810.016 10/31/16 13:12 ANGmg/kg dry 0.00025Methyl-tert-Butyl Ether
BRL *8260B P6J054810.016 10/31/16 13:12 ANGmg/kg dry 0.00025Naphthalene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00040n-Butylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00046n-Propylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00032o-Xylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00038sec-Butylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00047Styrene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00026tert-Butylbenzene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00037Tetrachloroethylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00045Toluene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00046trans-1,2-Dichloroethylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00041trans-1,3-Dichloropropylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00050Trichloroethylene
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00050Trichlorofluoromethane
BRL *8260B P6J054810.039 10/31/16 13:12 ANGmg/kg dry 0.0011Vinyl acetate
BRL *8260B P6J054810.0078 10/31/16 13:12 ANGmg/kg dry 0.00038Vinyl chloride
BRL *8260B P6J054810.023 10/31/16 13:12 ANGmg/kg dry 0.0015Xylenes, total
Surrogate Recovery Control Limits
70-130128 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-12991 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0548 - 5035
Blank (P6J0548-BLK1)Prepared & Analyzed: 10/31/16
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0548 - 5035
Blank (P6J0548-BLK1)Prepared & Analyzed: 10/31/16
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9446.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 76-129Surrogate: Toluene-d8 8743.4
LCS (P6J0548-BS1)Prepared & Analyzed: 10/31/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0456 0.0050 0.05000 72-11591
1,1,1-Trichloroethane mg/kg wet0.0504 0.0050 0.05000 67-131101
1,1,2,2-Tetrachloroethane mg/kg wet0.0406 0.0050 0.05000 56-12681
1,1,2-Trichloroethane mg/kg wet0.0417 0.0050 0.05000 70-13383
1,1-Dichloroethane mg/kg wet0.0502 0.0050 0.05000 74-127100
1,1-Dichloroethylene mg/kg wet0.0464 0.0050 0.05000 67-14993
1,1-Dichloropropylene mg/kg wet0.0477 0.0050 0.05000 71-13095
1,2,3-Trichlorobenzene mg/kg wet0.0428 0.0050 0.05000 68-13086
1,2,3-Trichloropropane mg/kg wet0.0399 0.0050 0.05000 60-13780
1,2,4-Trichlorobenzene mg/kg wet0.0421 0.0050 0.05000 66-12584
1,2,4-Trimethylbenzene mg/kg wet0.0447 0.0050 0.05000 69-12989
1,2-Dibromoethane mg/kg wet0.0484 0.0050 0.05000 70-13297
1,2-Dichlorobenzene mg/kg wet0.0440 0.0050 0.05000 72-12388
1,2-Dichloroethane mg/kg wet0.0461 0.0050 0.05000 68-12892
1,2-Dichloropropane mg/kg wet0.0479 0.0050 0.05000 73-13096
1,3,5-Trimethylbenzene mg/kg wet0.0456 0.0050 0.05000 69-12891
1,3-Dichlorobenzene mg/kg wet0.0426 0.0050 0.05000 71-12085
1,3-Dichloropropane mg/kg wet0.0408 0.0050 0.05000 75-12482
1,4-Dichlorobenzene mg/kg wet0.0428 0.0050 0.05000 71-12386
2,2-Dichloropropane mg/kg wet0.0494 0.0050 0.05000 50-14299
2-Chlorotoluene mg/kg wet0.0441 0.0050 0.05000 67-12488
4-Chlorotoluene mg/kg wet0.0435 0.0050 0.05000 71-12687
4-Isopropyltoluene mg/kg wet0.0451 0.0050 0.05000 68-12990
Acetone mg/kg wet0.152 0.050 0.1000 29-198152
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0548 - 5035
LCS (P6J0548-BS1)Prepared & Analyzed: 10/31/16
Benzene mg/kg wet0.0506 0.0030 0.05000 74-127101
Bromobenzene mg/kg wet0.0422 0.0050 0.05000 73-12584
Bromochloromethane mg/kg wet0.0482 0.0050 0.05000 72-13496
Bromodichloromethane mg/kg wet0.0499 0.0050 0.05000 75-122100
Bromoform mg/kg wet0.0453 0.0050 0.05000 66-13591
Bromomethane mg/kg wet0.0247 0.010 0.05000 20-18049
Carbon Tetrachloride mg/kg wet0.0504 0.0050 0.05000 64-143101
Chlorobenzene mg/kg wet0.0460 0.0050 0.05000 74-11892
Chloroethane mg/kg wet0.0255 0.010 0.05000 33-14951
Chloroform mg/kg wet0.0495 0.0050 0.05000 73-12799
Chloromethane mg/kg wet0.00520 0.0050 0.05000 L45-14310
cis-1,2-Dichloroethylene mg/kg wet0.0499 0.0050 0.05000 76-134100
cis-1,3-Dichloropropylene mg/kg wet0.0508 0.0050 0.05000 71-125102
Dibromochloromethane mg/kg wet0.0440 0.0050 0.05000 73-12288
Dichlorodifluoromethane mg/kg wetBRL0.0050 0.05000 L26-146
Ethylbenzene mg/kg wet0.0452 0.0050 0.05000 74-12890
Isopropyl Ether mg/kg wet0.0479 0.0050 0.05000 59-15996
Isopropylbenzene (Cumene)mg/kg wet0.0446 0.0050 0.05000 68-12689
m,p-Xylenes mg/kg wet0.0900 0.010 0.1000 75-12490
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0456 0.050 0.05000 61-15791
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0602 0.10 0.05000 63-149120
Methyl Isobutyl Ketone mg/kg wet0.0500 0.050 0.05000 57-162100
Methylene Chloride mg/kg wet0.0455 0.0050 0.05000 74-12991
Methyl-tert-Butyl Ether mg/kg wet0.0491 0.010 0.05000 70-13098
Naphthalene mg/kg wet0.0420 0.010 0.05000 57-15784
n-Butylbenzene mg/kg wet0.0451 0.0050 0.05000 65-13590
n-Propylbenzene mg/kg wet0.0430 0.0050 0.05000 67-13086
o-Xylene mg/kg wet0.0445 0.0050 0.05000 74-12689
sec-Butylbenzene mg/kg wet0.0438 0.0050 0.05000 66-13188
Styrene mg/kg wet0.0477 0.0050 0.05000 77-12195
tert-Butylbenzene mg/kg wet0.0425 0.0050 0.05000 67-13285
Tetrachloroethylene mg/kg wet0.0493 0.0050 0.05000 68-13099
Toluene mg/kg wet0.0500 0.0050 0.05000 71-129100
trans-1,2-Dichloroethylene mg/kg wet0.0496 0.0050 0.05000 73-13299
trans-1,3-Dichloropropylene mg/kg wet0.0488 0.0050 0.05000 68-12398
Trichloroethylene mg/kg wet0.0530 0.0050 0.05000 75-133106
Trichlorofluoromethane mg/kg wet0.0291 0.0050 0.05000 44-14658
Vinyl acetate mg/kg wet0.0507 0.025 0.05000 85-161101
Vinyl chloride mg/kg wet0.00846 0.0050 0.05000 L48-14717
Xylenes, total mg/kg wet0.134 0.015 0.1500 74-12690
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9648.1
ug/L 50.00 76-129Surrogate: Toluene-d8 8643.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0548 - 5035
LCS Dup (P6J0548-BSD1)Prepared & Analyzed: 10/31/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0433 0.0050 0.05000 2072-11587 5
1,1,1-Trichloroethane mg/kg wet0.0466 0.0050 0.05000 2067-13193 8
1,1,2,2-Tetrachloroethane mg/kg wet0.0400 0.0050 0.05000 2056-12680 1
1,1,2-Trichloroethane mg/kg wet0.0422 0.0050 0.05000 2070-13384 1
1,1-Dichloroethane mg/kg wet0.0471 0.0050 0.05000 2074-12794 6
1,1-Dichloroethylene mg/kg wet0.0447 0.0050 0.05000 2067-14989 4
1,1-Dichloropropylene mg/kg wet0.0448 0.0050 0.05000 2071-13090 6
1,2,3-Trichlorobenzene mg/kg wet0.0430 0.0050 0.05000 2068-13086 0.5
1,2,3-Trichloropropane mg/kg wet0.0405 0.0050 0.05000 2060-13781 1
1,2,4-Trichlorobenzene mg/kg wet0.0421 0.0050 0.05000 2066-12584 0.07
1,2,4-Trimethylbenzene mg/kg wet0.0430 0.0050 0.05000 2069-12986 4
1,2-Dibromoethane mg/kg wet0.0472 0.0050 0.05000 2070-13294 3
1,2-Dichlorobenzene mg/kg wet0.0424 0.0050 0.05000 2072-12385 4
1,2-Dichloroethane mg/kg wet0.0454 0.0050 0.05000 2068-12891 2
1,2-Dichloropropane mg/kg wet0.0472 0.0050 0.05000 2073-13094 1
1,3,5-Trimethylbenzene mg/kg wet0.0428 0.0050 0.05000 2069-12886 7
1,3-Dichlorobenzene mg/kg wet0.0411 0.0050 0.05000 2071-12082 4
1,3-Dichloropropane mg/kg wet0.0404 0.0050 0.05000 2075-12481 0.9
1,4-Dichlorobenzene mg/kg wet0.0408 0.0050 0.05000 2071-12382 5
2,2-Dichloropropane mg/kg wet0.0484 0.0050 0.05000 2050-14297 2
2-Chlorotoluene mg/kg wet0.0424 0.0050 0.05000 2067-12485 4
4-Chlorotoluene mg/kg wet0.0412 0.0050 0.05000 2071-12682 5
4-Isopropyltoluene mg/kg wet0.0426 0.0050 0.05000 2068-12985 6
Acetone mg/kg wet0.136 0.050 0.1000 2029-198136 11
Benzene mg/kg wet0.0484 0.0030 0.05000 2074-12797 4
Bromobenzene mg/kg wet0.0408 0.0050 0.05000 2073-12582 3
Bromochloromethane mg/kg wet0.0485 0.0050 0.05000 2072-13497 0.7
Bromodichloromethane mg/kg wet0.0489 0.0050 0.05000 2075-12298 2
Bromoform mg/kg wet0.0448 0.0050 0.05000 2066-13590 1
Bromomethane mg/kg wet0.0203 0.010 0.05000 2020-18041 20
Carbon Tetrachloride mg/kg wet0.0482 0.0050 0.05000 2064-14396 5
Chlorobenzene mg/kg wet0.0445 0.0050 0.05000 2074-11889 3
Chloroethane mg/kg wet0.0223 0.010 0.05000 2033-14945 13
Chloroform mg/kg wet0.0472 0.0050 0.05000 2073-12794 5
Chloromethane mg/kg wet0.00458 0.0050 0.05000 20 L45-1439 13
cis-1,2-Dichloroethylene mg/kg wet0.0484 0.0050 0.05000 2076-13497 3
cis-1,3-Dichloropropylene mg/kg wet0.0497 0.0050 0.05000 2071-12599 2
Dibromochloromethane mg/kg wet0.0450 0.0050 0.05000 2073-12290 2
Dichlorodifluoromethane mg/kg wetBRL0.0050 0.05000 20 L26-146
Ethylbenzene mg/kg wet0.0438 0.0050 0.05000 2074-12888 3
Isopropyl Ether mg/kg wet0.0470 0.0050 0.05000 2059-15994 2
Isopropylbenzene (Cumene)mg/kg wet0.0416 0.0050 0.05000 2068-12683 7
m,p-Xylenes mg/kg wet0.0880 0.010 0.1000 2075-12488 2
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0460 0.050 0.05000 2061-15792 0.9
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0556 0.10 0.05000 2063-149111 8
Methyl Isobutyl Ketone mg/kg wet0.0504 0.050 0.05000 2057-162101 0.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0548 - 5035
LCS Dup (P6J0548-BSD1)Prepared & Analyzed: 10/31/16
Methylene Chloride mg/kg wet0.0451 0.0050 0.05000 2074-12990 0.9
Methyl-tert-Butyl Ether mg/kg wet0.0483 0.010 0.05000 2070-13097 2
Naphthalene mg/kg wet0.0424 0.010 0.05000 2057-15785 0.9
n-Butylbenzene mg/kg wet0.0424 0.0050 0.05000 2065-13585 6
n-Propylbenzene mg/kg wet0.0415 0.0050 0.05000 2067-13083 4
o-Xylene mg/kg wet0.0428 0.0050 0.05000 2074-12686 4
sec-Butylbenzene mg/kg wet0.0408 0.0050 0.05000 2066-13182 7
Styrene mg/kg wet0.0464 0.0050 0.05000 2077-12193 3
tert-Butylbenzene mg/kg wet0.0402 0.0050 0.05000 2067-13280 6
Tetrachloroethylene mg/kg wet0.0456 0.0050 0.05000 2068-13091 8
Toluene mg/kg wet0.0482 0.0050 0.05000 2071-12996 4
trans-1,2-Dichloroethylene mg/kg wet0.0480 0.0050 0.05000 2073-13296 3
trans-1,3-Dichloropropylene mg/kg wet0.0477 0.0050 0.05000 2068-12395 2
Trichloroethylene mg/kg wet0.0506 0.0050 0.05000 2075-133101 5
Trichlorofluoromethane mg/kg wet0.0251 0.0050 0.05000 2044-14650 15
Vinyl acetate mg/kg wet0.0474 0.025 0.05000 2085-16195 7
Vinyl chloride mg/kg wet0.00713 0.0050 0.05000 20 L48-14714 17
Xylenes, total mg/kg wet0.131 0.015 0.1500 2074-12687 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9849.0
ug/L 50.00 76-129Surrogate: Toluene-d8 8844.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0506 - 3546
Blank (P6J0506-BLK1)Prepared: 10/27/16 Analyzed: 10/28/16
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0506 - 3546
Blank (P6J0506-BLK1)Prepared: 10/27/16 Analyzed: 10/28/16
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.332 39-132Surrogate: 2,4,6-Tribromophenol 852.82
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 881.47
mg/kg wet 3.332 35-115Surrogate: 2-Fluorophenol 852.84
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 821.37
mg/kg wet 3.332 34-121Surrogate: Phenol-d5 842.81
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 931.55
LCS (P6J0506-BS1)Prepared: 10/27/16 Analyzed: 10/28/16
1,2,4-Trichlorobenzene mg/kg wet1.31 0.33 1.661 34-11879
1,2-Dichlorobenzene mg/kg wet1.21 0.33 1.661 33-11773
1,3-Dichlorobenzene mg/kg wet1.16 0.33 1.661 30-11570
1,4-Dichlorobenzene mg/kg wet1.19 0.33 1.661 31-11572
1-Methylnaphthalene mg/kg wet1.32 0.33 1.661 40-11979
2,4,6-Trichlorophenol mg/kg wet1.52 0.33 1.661 39-12692
2,4-Dichlorophenol mg/kg wet1.44 0.33 1.661 40-12287
2,4-Dimethylphenol mg/kg wet1.64 0.33 1.661 30-12799
2,4-Dinitrophenol mg/kg wet0.649 0.33 1.661 27-12939
2,4-Dinitrotoluene mg/kg wet1.49 0.33 1.661 48-12690
2,6-Dinitrotoluene mg/kg wet1.46 0.33 1.661 46-12488
2-Chloronaphthalene mg/kg wet2.81 0.33 1.661 LH41-114169
2-Chlorophenol mg/kg wet1.41 0.33 1.661 34-12185
2-Methylnaphthalene mg/kg wet1.31 0.33 1.661 38-12279
2-Methylphenol mg/kg wet1.37 0.33 1.661 32-12283
2-Nitrophenol mg/kg wet1.42 0.33 1.661 36-12385
3,3'-Dichlorobenzidine mg/kg wet1.20 0.33 1.661 22-12172
3/4-Methylphenol mg/kg wet1.39 0.33 1.661 34-11984
4,6-Dinitro-2-methylphenol mg/kg wet1.31 0.33 1.661 29-13279
4-Bromophenyl phenyl ether mg/kg wet1.42 0.33 1.661 46-12485
4-Chloro-3-methylphenol mg/kg wet1.55 0.33 1.661 45-12293
4-Chloroaniline mg/kg wet0.885 0.33 1.661 17-10653
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0506 - 3546
LCS (P6J0506-BS1)Prepared: 10/27/16 Analyzed: 10/28/16
4-Chlorophenyl phenyl ether mg/kg wet1.40 0.33 1.661 45-12184
4-Nitrophenol mg/kg wet1.62 0.33 1.661 30-13297
Acenaphthene mg/kg wet1.39 0.33 1.661 40-12384
Acenaphthylene mg/kg wet1.45 0.33 1.661 32-13287
Anthracene mg/kg wet1.54 0.33 1.661 47-12393
Azobenzene mg/kg wet1.53 0.33 1.661 39-12592
Benzo(a)anthracene mg/kg wet1.61 0.33 1.661 49-12697
Benzo(a)pyrene mg/kg wet1.43 0.33 1.661 45-12986
Benzo(b)fluoranthene mg/kg wet1.39 0.33 1.661 45-13284
Benzo(g,h,i)perylene mg/kg wet1.41 0.33 1.661 43-13485
Benzo(k)fluoranthene mg/kg wet1.53 0.33 1.661 47-13292
Benzoic Acid mg/kg wet0.485 0.33 1.661 10-8329
Benzyl alcohol mg/kg wet1.33 0.33 1.661 29-12280
bis(2-Chloroethoxy)methane mg/kg wet1.27 0.33 1.661 36-12177
Bis(2-Chloroethyl)ether mg/kg wet1.17 0.33 1.661 31-12071
Bis(2-chloroisopropyl)ether mg/kg wet1.19 0.33 1.661 33-13172
Bis(2-Ethylhexyl)phthalate mg/kg wet1.70 0.33 1.661 51-133103
Butyl benzyl phthalate mg/kg wet1.64 0.33 1.661 48-13299
Chrysene mg/kg wet1.68 0.33 1.661 50-124101
Dibenzo(a,h)anthracene mg/kg wet1.43 0.33 1.661 45-13486
Dibenzofuran mg/kg wet1.48 0.33 1.661 44-12089
Diethyl phthalate mg/kg wet1.56 0.33 1.661 50-12494
Dimethyl phthalate mg/kg wet1.50 0.33 1.661 48-12490
Di-n-butyl phthalate mg/kg wet1.66 0.33 1.661 51-128100
Di-n-octyl phthalate mg/kg wet1.58 0.33 1.661 45-14095
Fluoranthene mg/kg wet1.57 0.33 1.661 50-12794
Fluorene mg/kg wet1.45 0.33 1.661 43-12587
Hexachlorobenzene mg/kg wet1.53 0.33 1.661 45-12292
Hexachlorobutadiene mg/kg wet1.29 0.33 1.661 32-12378
Hexachlorocyclopentadiene mg/kg wet1.28 0.33 1.661 32-11777
Hexachloroethane mg/kg wet1.17 0.33 1.661 28-11770
Indeno(1,2,3-cd)pyrene mg/kg wet1.38 0.33 1.661 45-13383
Isophorone mg/kg wet1.33 0.33 1.661 30-12280
Naphthalene mg/kg wet1.34 0.33 1.661 35-12381
Nitrobenzene mg/kg wet1.30 0.33 1.661 34-12278
N-Nitroso-di-n-propylamine mg/kg wet1.18 0.33 1.661 36-12071
N-Nitrosodiphenylamine mg/kg wet1.53 0.33 1.661 38-12792
Pentachlorophenol mg/kg wet1.53 0.33 1.661 25-13392
Phenanthrene mg/kg wet1.55 0.33 1.661 50-12193
Phenol mg/kg wet1.38 0.33 1.661 34-12183
Pyrene mg/kg wet1.61 0.33 1.661 47-12797
mg/kg wet 3.322 39-132Surrogate: 2,4,6-Tribromophenol 902.98
mg/kg wet 1.661 44-115Surrogate: 2-Fluorobiphenyl 861.42
mg/kg wet 3.322 35-115Surrogate: 2-Fluorophenol 832.76
mg/kg wet 1.661 37-122Surrogate: Nitrobenzene-d5 781.30
mg/kg wet 3.322 34-121Surrogate: Phenol-d5 812.69
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0506 - 3546
LCS (P6J0506-BS1)Prepared: 10/27/16 Analyzed: 10/28/16
mg/kg wet 1.661 54-127Surrogate: Terphenyl-d14 891.48
LCS Dup (P6J0506-BSD1)Prepared: 10/27/16 Analyzed: 10/28/16
1,2,4-Trichlorobenzene mg/kg wet1.36 0.33 1.660 2034-11882 4
1,2-Dichlorobenzene mg/kg wet1.25 0.33 1.660 2033-11775 3
1,3-Dichlorobenzene mg/kg wet1.19 0.33 1.660 2030-11572 3
1,4-Dichlorobenzene mg/kg wet1.21 0.33 1.660 2031-11573 1
1-Methylnaphthalene mg/kg wet1.34 0.33 1.660 2040-11981 2
2,4,6-Trichlorophenol mg/kg wet1.53 0.33 1.660 2039-12692 0.5
2,4-Dichlorophenol mg/kg wet1.50 0.33 1.660 2040-12290 4
2,4-Dimethylphenol mg/kg wet1.66 0.33 1.660 2030-127100 1
2,4-Dinitrophenol mg/kg wet0.991 0.33 1.660 20 D27-12960 42
2,4-Dinitrotoluene mg/kg wet1.52 0.33 1.660 2048-12691 2
2,6-Dinitrotoluene mg/kg wet1.49 0.33 1.660 2046-12490 2
2-Chloronaphthalene mg/kg wet2.88 0.33 1.660 20 LH41-114174 3
2-Chlorophenol mg/kg wet1.45 0.33 1.660 2034-12187 3
2-Methylnaphthalene mg/kg wet1.34 0.33 1.660 2038-12281 3
2-Methylphenol mg/kg wet1.39 0.33 1.660 2032-12284 2
2-Nitrophenol mg/kg wet1.46 0.33 1.660 2036-12388 3
3,3'-Dichlorobenzidine mg/kg wet1.50 0.33 1.660 20 D22-12190 22
3/4-Methylphenol mg/kg wet1.43 0.33 1.660 2034-11986 3
4,6-Dinitro-2-methylphenol mg/kg wet1.58 0.33 1.660 2029-13295 19
4-Bromophenyl phenyl ether mg/kg wet1.43 0.33 1.660 2046-12486 0.8
4-Chloro-3-methylphenol mg/kg wet1.58 0.33 1.660 2045-12295 2
4-Chloroaniline mg/kg wet1.23 0.33 1.660 20 D17-10674 32
4-Chlorophenyl phenyl ether mg/kg wet1.42 0.33 1.660 2045-12186 2
4-Nitrophenol mg/kg wet1.63 0.33 1.660 2030-13298 0.5
Acenaphthene mg/kg wet1.42 0.33 1.660 2040-12386 2
Acenaphthylene mg/kg wet1.48 0.33 1.660 2032-13289 2
Anthracene mg/kg wet1.58 0.33 1.660 2047-12395 3
Azobenzene mg/kg wet1.55 0.33 1.660 2039-12594 2
Benzo(a)anthracene mg/kg wet1.64 0.33 1.660 2049-12698 2
Benzo(a)pyrene mg/kg wet1.46 0.33 1.660 2045-12988 2
Benzo(b)fluoranthene mg/kg wet1.41 0.33 1.660 2045-13285 1
Benzo(g,h,i)perylene mg/kg wet1.41 0.33 1.660 2043-13485 0.3
Benzo(k)fluoranthene mg/kg wet1.54 0.33 1.660 2047-13293 0.3
Benzoic Acid mg/kg wet0.601 0.33 1.660 20 D10-8336 21
Benzyl alcohol mg/kg wet1.38 0.33 1.660 2029-12283 4
bis(2-Chloroethoxy)methane mg/kg wet1.30 0.33 1.660 2036-12179 2
Bis(2-Chloroethyl)ether mg/kg wet1.22 0.33 1.660 2031-12074 4
Bis(2-chloroisopropyl)ether mg/kg wet1.22 0.33 1.660 2033-13173 2
Bis(2-Ethylhexyl)phthalate mg/kg wet1.72 0.33 1.660 2051-133104 1
Butyl benzyl phthalate mg/kg wet1.67 0.33 1.660 2048-132101 2
Chrysene mg/kg wet1.69 0.33 1.660 2050-124102 0.9
Dibenzo(a,h)anthracene mg/kg wet1.43 0.33 1.660 2045-13486 0.07
Dibenzofuran mg/kg wet1.53 0.33 1.660 2044-12092 3
Diethyl phthalate mg/kg wet1.56 0.33 1.660 2050-12494 0.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0506 - 3546
LCS Dup (P6J0506-BSD1)Prepared: 10/27/16 Analyzed: 10/28/16
Dimethyl phthalate mg/kg wet1.53 0.33 1.660 2048-12492 2
Di-n-butyl phthalate mg/kg wet1.68 0.33 1.660 2051-128101 1
Di-n-octyl phthalate mg/kg wet1.58 0.33 1.660 2045-14095 0.4
Fluoranthene mg/kg wet1.59 0.33 1.660 2050-12796 2
Fluorene mg/kg wet1.48 0.33 1.660 2043-12589 2
Hexachlorobenzene mg/kg wet1.56 0.33 1.660 2045-12294 2
Hexachlorobutadiene mg/kg wet1.33 0.33 1.660 2032-12380 3
Hexachlorocyclopentadiene mg/kg wet1.31 0.33 1.660 2032-11779 2
Hexachloroethane mg/kg wet1.20 0.33 1.660 2028-11772 3
Indeno(1,2,3-cd)pyrene mg/kg wet1.39 0.33 1.660 2045-13384 0.9
Isophorone mg/kg wet1.36 0.33 1.660 2030-12282 2
Naphthalene mg/kg wet1.37 0.33 1.660 2035-12382 2
Nitrobenzene mg/kg wet1.33 0.33 1.660 2034-12280 2
N-Nitroso-di-n-propylamine mg/kg wet1.23 0.33 1.660 2036-12074 4
N-Nitrosodiphenylamine mg/kg wet1.57 0.33 1.660 2038-12794 2
Pentachlorophenol mg/kg wet1.63 0.33 1.660 2025-13398 6
Phenanthrene mg/kg wet1.57 0.33 1.660 2050-12194 1
Phenol mg/kg wet1.44 0.33 1.660 2034-12187 5
Pyrene mg/kg wet1.62 0.33 1.660 2047-12798 0.6
mg/kg wet 3.320 39-132Surrogate: 2,4,6-Tribromophenol 913.02
mg/kg wet 1.660 44-115Surrogate: 2-Fluorobiphenyl 881.46
mg/kg wet 3.320 35-115Surrogate: 2-Fluorophenol 852.81
mg/kg wet 1.660 37-122Surrogate: Nitrobenzene-d5 801.32
mg/kg wet 3.320 34-121Surrogate: Phenol-d5 832.75
mg/kg wet 1.660 54-127Surrogate: Terphenyl-d14 901.49
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP Metals - Quality Control
Batch P6J0522 - 3010A
Blank (P6J0522-BLK1)Prepared & Analyzed: 10/28/16
Arsenic mg/LBRL0.050
Barium mg/LBRL5.0
Cadmium mg/LBRL0.025
Chromium mg/LBRL0.25
Lead mg/LBRL0.050
Selenium mg/LBRL0.10
Silver mg/LBRL0.25
LCS (P6J0522-BS1)Prepared & Analyzed: 10/28/16
Arsenic mg/L1.26 0.050 1.250 80-120101
Barium mg/L1.25 5.0 1.250 80-120100
Cadmium mg/L1.26 0.025 1.250 80-120101
Chromium mg/L1.23 0.25 1.250 80-12099
Lead mg/L1.22 0.050 1.250 80-12097
Selenium mg/L1.29 0.10 1.250 80-120103
Silver mg/L0.491 0.25 0.5000 80-12098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 20
10/31/16
Level II QC Report
2923 South Tryon St. Ste 100
Project: LEN-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6100472
Time Submitted: 10/26/2016 9:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P6J0546 - Solids, Dry Weight
Duplicate (P6J0546-DUP4)Prepared & Analyzed: 10/28/16 Source: 6100472-01
% Solids % by Weight63.2 0.100 64.4 202
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P6J05466100472-01 10/28/16 15:5430 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6J05066100472-01 10/27/16 14:3030.05 1g mL
Prep Method: 1311
Lab Number Batch Date/TimeInitialFinal
P6J05216100472-01 10/27/16 14:201002000gmL
Prep Method: 3010A
Lab Number Batch Date/TimeInitialFinal
P6J05226100472-01 10/28/16 11:3010 50mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6J05486100472-01 10/31/16 8:525 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 20
Page 20 of 20
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-115387-1
TestAmerica Sample Delivery Group: LEN-001
Client Project/Site: LEN-001
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Ralph McGee
Authorized for release by:
11/16/2016 1:51:20 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: LEN-001
TestAmerica Job ID: 490-115387-1
SDG: LEN-001
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
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Sample Summary
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-115387-1 OWS-E Soil 11/02/16 10:00 11/03/16 09:05
TestAmerica Nashville
Page 3 of 34 11/16/2016
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-115387-1
Project/Site: LEN-001 SDG: LEN-001
Job ID: 490-115387-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-115387-1
Comments
No additional comments.
Receipt
The sample was received on 11/3/2016 9:05 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 5.1º C.
GC/MS VOA
Method 8260B: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for analytical batch
490-385041 recovered outside control limits for the following analytes: 1,1,2,2-Tetrachloroethane and 1,2,3-Trichloropropane.
Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-385041.
Method 8260B: Internal standard responses were outside of acceptance limits for the following sample: OWS-E (490-115387-1). The
sample(s) shows evidence of matrix interference.
Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-385160.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: The continuing calibration verification (CCV) for analytical batch 490-384673 was outside the method criteria for
hexachlorocyclopentadiene . A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable; therefore, the data is reported. (CCVIS 490-384673/3)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 7196A: The matrix spike soluble (MSS) recovery for preparation batch 490-385105 and analytical batch 490-385350 was outside
control limits due to sample matrix. The associated laboratory control soluble sample (LCSS), laboratory control insoluble sample (LCSI),
and post digestion spike (PDS) recoveries met acceptance criteria.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 34 11/16/2016
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Definitions/Glossary
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Qualifiers
GC/MS VOA
Qualifier Description
*RPD of the LCS and LCSD exceeds the control limits
Qualifier
*ISTD response or retention time outside acceptable limits
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
General Chemistry
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Lab Sample ID: 490-115387-1Client Sample ID: OWS-E
Matrix: SoilDate Collected: 11/02/16 10:00
Date Received: 11/03/16 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0475 mg/Kg ☼11/02/16 09:00 11/09/16 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Benzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼Bromobenzene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Bromochloromethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Bromodichloromethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Bromoform ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Bromomethane ND
0.0475 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼2-Butanone (MEK)ND
0.00475 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Carbon disulfide ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Carbon tetrachloride ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Chlorobenzene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Chlorodibromomethane ND
0.00475 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Chloroethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Chloroform ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Chloromethane ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼2-Chlorotoluene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼4-Chlorotoluene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼cis-1,2-Dichloroethene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼cis-1,3-Dichloropropene ND
0.00489 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,2-Dibromo-3-Chloropropane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,2-Dibromoethane (EDB)ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Dibromomethane ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,2-Dichlorobenzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,3-Dichlorobenzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,4-Dichlorobenzene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Dichlorodifluoromethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,1-Dichloroethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,2-Dichloroethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,1-Dichloroethene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,2-Dichloroethene, Total ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,2-Dichloropropane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,3-Dichloropropane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼2,2-Dichloropropane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,1-Dichloropropene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Diisopropyl ether ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Ethylbenzene ND
0.00489 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼Hexachlorobutadiene ND
0.0475 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼2-Hexanone ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Isopropylbenzene ND
0.00951 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Methylene Chloride ND
0.0475 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼4-Methyl-2-pentanone (MIBK)ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Methyl tert-butyl ether ND
0.00489 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼Naphthalene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼n-Butylbenzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼N-Propylbenzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼p-Isopropyltoluene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼sec-Butylbenzene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Styrene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Lab Sample ID: 490-115387-1Client Sample ID: OWS-E
Matrix: SoilDate Collected: 11/02/16 10:00
Date Received: 11/03/16 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00190 mg/Kg ☼11/02/16 09:00 11/09/16 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,1,2,2-Tetrachloroethane ND *
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Tetrachloroethene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Toluene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼trans-1,2-Dichloroethene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼trans-1,3-Dichloropropene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,2,3-Trichlorobenzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,2,4-Trichlorobenzene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,1,1-Trichloroethane ND
0.00475 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼1,1,2-Trichloroethane ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Trichloroethene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Trichlorofluoromethane ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,2,3-Trichloropropane ND *
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,2,4-Trimethylbenzene ND
0.00196 mg/Kg 11/02/16 09:00 11/09/16 01:18 1☼1,3,5-Trimethylbenzene ND
0.00190 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Vinyl chloride ND
0.00570 mg/Kg 11/02/16 09:00 11/09/16 16:20 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)109 70-130 11/02/16 09:00 11/09/16 01:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)99 *11/02/16 09:00 11/09/16 16:20 170-130
Dibromofluoromethane (Surr)106 11/02/16 09:00 11/09/16 01:18 170-130
Dibromofluoromethane (Surr)112 11/02/16 09:00 11/09/16 16:20 170-130
1,2-Dichloroethane-d4 (Surr)106 11/02/16 09:00 11/09/16 01:18 170-130
1,2-Dichloroethane-d4 (Surr)113 11/02/16 09:00 11/09/16 16:20 170-130
Toluene-d8 (Surr)103 11/02/16 09:00 11/09/16 01:18 170-130
Toluene-d8 (Surr)100 11/02/16 09:00 11/09/16 16:20 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0665 mg/Kg ☼11/05/16 11:09 11/08/16 00:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Acenaphthylene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Anthracene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Benzo[a]anthracene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Benzo[a]pyrene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Benzo[b]fluoranthene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Benzo[g,h,i]perylene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Benzo[k]fluoranthene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Bis(2-chloroethoxy)methane ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Bis(2-chloroethyl)ether ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼bis (2-chloroisopropyl) ether ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Bis(2-ethylhexyl) phthalate ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4-Bromophenyl phenyl ether ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Butyl benzyl phthalate ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Carbazole ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4-Chloroaniline ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4-Chloro-3-methylphenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2-Chloronaphthalene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2-Chlorophenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4-Chlorophenyl phenyl ether ND
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Client Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Lab Sample ID: 490-115387-1Client Sample ID: OWS-E
Matrix: SoilDate Collected: 11/02/16 10:00
Date Received: 11/03/16 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Chrysene ND 0.0665 mg/Kg ☼11/05/16 11:09 11/08/16 00:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.661 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Cresols ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Dibenz(a,h)anthracene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Dibenzofuran ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼1,2-Dichlorobenzene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼1,3-Dichlorobenzene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼1,4-Dichlorobenzene ND
0.665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼3,3'-Dichlorobenzidine ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,4-Dichlorophenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Diethyl phthalate ND
0.665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,4-Dimethylphenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Dimethyl phthalate ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Di-n-butyl phthalate ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4,6-Dinitro-2-methylphenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,4-Dinitrophenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,4-Dinitrotoluene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,6-Dinitrotoluene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Di-n-octyl phthalate ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Fluoranthene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Fluorene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Hexachlorobenzene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Hexachlorobutadiene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Hexachlorocyclopentadiene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Hexachloroethane ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Indeno[1,2,3-cd]pyrene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Isophorone ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼1-Methylnaphthalene ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2-Methylnaphthalene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2-Methylphenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼3 & 4 Methylphenol ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Naphthalene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2-Nitroaniline ND
0.665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼3-Nitroaniline ND
0.665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4-Nitroaniline ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Nitrobenzene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2-Nitrophenol ND
0.665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼4-Nitrophenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼N-Nitrosodi-n-propylamine ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Pentachlorophenol ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Phenanthrene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Phenol ND
0.0665 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼Pyrene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼1,2,4-Trichlorobenzene ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,4,5-Trichlorophenol ND
0.331 mg/Kg 11/05/16 11:09 11/08/16 00:59 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)63 29-120 11/05/16 11:09 11/08/16 00:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Lab Sample ID: 490-115387-1Client Sample ID: OWS-E
Matrix: SoilDate Collected: 11/02/16 10:00
Date Received: 11/03/16 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2-Fluorophenol (Surr)56 10-120 11/05/16 11:09 11/08/16 00:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)53 11/05/16 11:09 11/08/16 00:59 127-120
Phenol-d5 (Surr)61 11/05/16 11:09 11/08/16 00:59 110-120
Terphenyl-d14 (Surr)74 11/05/16 11:09 11/08/16 00:59 113-120
2,4,6-Tribromophenol (Surr)85 11/05/16 11:09 11/08/16 00:59 110-120
Method: 6010D - Metals (ICP)
RL MDL
Antimony ND 12.7 mg/Kg ☼11/06/16 12:48 11/11/16 19:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.53 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Arsenic ND
1.27 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Beryllium ND
1.27 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Cadmium ND
1.27 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Chromium 20.5
2.53 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Copper 11.1
1.27 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Lead 19.4
3.80 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Manganese 78.5
2.53 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Nickel 4.54
2.53 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Selenium ND
1.27 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Silver ND
2.53 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Thallium ND
12.7 mg/Kg 11/06/16 12:48 11/11/16 19:04 1☼Zinc 14.7
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.129 mg/Kg ☼11/10/16 09:42 11/10/16 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.44 mg/Kg ☼11/09/16 08:47 11/09/16 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 77.5 0.1 %11/04/16 11:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-385041/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
RL MDL
Acetone ND 0.0500 mg/Kg 11/08/16 22:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 11/08/16 22:06 1Benzene
ND 0.00200 mg/Kg 11/08/16 22:06 1Bromobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1Bromochloromethane
ND 0.00200 mg/Kg 11/08/16 22:06 1Bromodichloromethane
ND 0.00200 mg/Kg 11/08/16 22:06 1Bromoform
ND 0.00200 mg/Kg 11/08/16 22:06 1Bromomethane
ND 0.0500 mg/Kg 11/08/16 22:06 12-Butanone (MEK)
ND 0.00500 mg/Kg 11/08/16 22:06 1Carbon disulfide
ND 0.00200 mg/Kg 11/08/16 22:06 1Carbon tetrachloride
ND 0.00200 mg/Kg 11/08/16 22:06 1Chlorobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1Chlorodibromomethane
ND 0.00500 mg/Kg 11/08/16 22:06 1Chloroethane
ND 0.00200 mg/Kg 11/08/16 22:06 1Chloroform
ND 0.00200 mg/Kg 11/08/16 22:06 1Chloromethane
ND 0.00200 mg/Kg 11/08/16 22:06 12-Chlorotoluene
ND 0.00200 mg/Kg 11/08/16 22:06 14-Chlorotoluene
ND 0.00200 mg/Kg 11/08/16 22:06 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 11/08/16 22:06 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 11/08/16 22:06 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 11/08/16 22:06 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 11/08/16 22:06 1Dibromomethane
ND 0.00200 mg/Kg 11/08/16 22:06 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 11/08/16 22:06 11,1-Dichloroethane
ND 0.00200 mg/Kg 11/08/16 22:06 11,2-Dichloroethane
ND 0.00200 mg/Kg 11/08/16 22:06 11,1-Dichloroethene
ND 0.00200 mg/Kg 11/08/16 22:06 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 11/08/16 22:06 11,2-Dichloropropane
ND 0.00200 mg/Kg 11/08/16 22:06 11,3-Dichloropropane
ND 0.00200 mg/Kg 11/08/16 22:06 12,2-Dichloropropane
ND 0.00200 mg/Kg 11/08/16 22:06 11,1-Dichloropropene
ND 0.00200 mg/Kg 11/08/16 22:06 1Diisopropyl ether
ND 0.00200 mg/Kg 11/08/16 22:06 1Ethylbenzene
ND 0.00500 mg/Kg 11/08/16 22:06 1Hexachlorobutadiene
ND 0.0500 mg/Kg 11/08/16 22:06 12-Hexanone
ND 0.00200 mg/Kg 11/08/16 22:06 1Isopropylbenzene
ND 0.0100 mg/Kg 11/08/16 22:06 1Methylene Chloride
ND 0.0500 mg/Kg 11/08/16 22:06 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 11/08/16 22:06 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 11/08/16 22:06 1Naphthalene
ND 0.00200 mg/Kg 11/08/16 22:06 1n-Butylbenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1N-Propylbenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1p-Isopropyltoluene
ND 0.00200 mg/Kg 11/08/16 22:06 1sec-Butylbenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1Styrene
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-385041/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
RL MDL
tert-Butylbenzene ND 0.00200 mg/Kg 11/08/16 22:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 11/08/16 22:06 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 11/08/16 22:06 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 11/08/16 22:06 1Tetrachloroethene
ND 0.00200 mg/Kg 11/08/16 22:06 1Toluene
ND 0.00200 mg/Kg 11/08/16 22:06 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 11/08/16 22:06 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 11/08/16 22:06 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 11/08/16 22:06 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 11/08/16 22:06 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 11/08/16 22:06 1Trichloroethene
ND 0.00200 mg/Kg 11/08/16 22:06 1Trichlorofluoromethane
ND 0.00200 mg/Kg 11/08/16 22:06 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 11/08/16 22:06 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 11/08/16 22:06 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 11/08/16 22:06 1Vinyl chloride
ND 0.00600 mg/Kg 11/08/16 22:06 1Xylenes, Total
4-Bromofluorobenzene (Surr)97 70-130 11/08/16 22:06 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
114 11/08/16 22:06 1Dibromofluoromethane (Surr)70-130
122 11/08/16 22:06 11,2-Dichloroethane-d4 (Surr)70-130
99 11/08/16 22:06 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-385041/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
Acetone 0.250 0.2357 mg/Kg 94 45-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05005 mg/Kg 100 70-130
Bromobenzene 0.0500 0.04377 mg/Kg 88 67-130
Bromochloromethane 0.0500 0.05843 mg/Kg 117 70-133
Bromodichloromethane 0.0500 0.05260 mg/Kg 105 70-130
Bromoform 0.0500 0.04846 mg/Kg 97 59-137
Bromomethane 0.0500 0.06112 mg/Kg 122 32-150
2-Butanone (MEK)0.250 0.2307 mg/Kg 92 50-149
Carbon disulfide 0.0500 0.04575 mg/Kg 92 66-138
Carbon tetrachloride 0.0500 0.06077 mg/Kg 122 70-131
Chlorobenzene 0.0500 0.04916 mg/Kg 98 70-130
Chlorodibromomethane 0.0500 0.05047 mg/Kg 101 70-130
Chloroethane 0.0500 0.05245 mg/Kg 105 37-150
Chloroform 0.0500 0.06046 mg/Kg 121 70-130
Chloromethane 0.0500 0.03443 mg/Kg 69 53-150
2-Chlorotoluene 0.0500 0.04863 mg/Kg 97 70-132
4-Chlorotoluene 0.0500 0.04912 mg/Kg 98 67-135
cis-1,2-Dichloroethene 0.0500 0.05579 mg/Kg 112 70-132
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-385041/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
cis-1,3-Dichloropropene 0.0500 0.04848 mg/Kg 97 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.03543 mg/Kg 71 47-144
1,2-Dibromoethane (EDB)0.0500 0.04833 mg/Kg 97 69-130
Dibromomethane 0.0500 0.05768 mg/Kg 115 70-130
1,2-Dichlorobenzene 0.0500 0.04944 mg/Kg 99 70-134
1,3-Dichlorobenzene 0.0500 0.04855 mg/Kg 97 69-137
1,4-Dichlorobenzene 0.0500 0.04925 mg/Kg 99 66-134
Dichlorodifluoromethane 0.0500 0.04664 mg/Kg 93 32-150
1,1-Dichloroethane 0.0500 0.04948 mg/Kg 99 70-130
1,2-Dichloroethane 0.0500 0.06071 mg/Kg 121 65-134
1,1-Dichloroethene 0.0500 0.05172 mg/Kg 103 70-131
1,2-Dichloroethene, Total 0.100 0.1097 mg/Kg 110 70-130
1,2-Dichloropropane 0.0500 0.04944 mg/Kg 99 70-130
1,3-Dichloropropane 0.0500 0.04688 mg/Kg 94 70-130
2,2-Dichloropropane 0.0500 0.05631 mg/Kg 113 57-150
1,1-Dichloropropene 0.0500 0.05188 mg/Kg 104 70-130
Diisopropyl ether 0.0500 0.05155 mg/Kg 103 68-134
Ethylbenzene 0.0500 0.04983 mg/Kg 100 70-130
Hexachlorobutadiene 0.0500 0.04133 mg/Kg 83 64-137
2-Hexanone 0.250 0.2096 mg/Kg 84 47-148
Isopropylbenzene 0.0500 0.05075 mg/Kg 101 70-130
Methylene Chloride 0.0500 0.05021 mg/Kg 100 69-130
4-Methyl-2-pentanone (MIBK)0.250 0.2175 mg/Kg 87 48-150
Methyl tert-butyl ether 0.0500 0.05336 mg/Kg 107 54-145
Naphthalene 0.0500 0.03876 mg/Kg 78 55-149
n-Butylbenzene 0.0500 0.04890 mg/Kg 98 57-150
N-Propylbenzene 0.0500 0.04821 mg/Kg 96 62-150
p-Isopropyltoluene 0.0500 0.04825 mg/Kg 97 66-147
sec-Butylbenzene 0.0500 0.04906 mg/Kg 98 68-147
Styrene 0.0500 0.04957 mg/Kg 99 70-131
tert-Butylbenzene 0.0500 0.04836 mg/Kg 97 70-138
1,1,1,2-Tetrachloroethane 0.0500 0.04960 mg/Kg 99 70-130
1,1,2,2-Tetrachloroethane 0.0500 0.04259 mg/Kg 85 61-134
Tetrachloroethene 0.0500 0.05211 mg/Kg 104 70-130
Toluene 0.0500 0.05068 mg/Kg 101 70-130
trans-1,2-Dichloroethene 0.0500 0.05387 mg/Kg 108 70-130
trans-1,3-Dichloropropene 0.0500 0.04941 mg/Kg 99 67-130
1,2,3-Trichlorobenzene 0.0500 0.04002 mg/Kg 80 57-146
1,2,4-Trichlorobenzene 0.0500 0.04031 mg/Kg 81 47-150
1,1,1-Trichloroethane 0.0500 0.06142 mg/Kg 123 70-130
1,1,2-Trichloroethane 0.0500 0.04762 mg/Kg 95 70-130
Trichloroethene 0.0500 0.05412 mg/Kg 108 70-130
Trichlorofluoromethane 0.0500 0.05848 mg/Kg 117 53-150
1,2,3-Trichloropropane 0.0500 0.04521 mg/Kg 90 60-139
1,2,4-Trimethylbenzene 0.0500 0.04808 mg/Kg 96 70-140
1,3,5-Trimethylbenzene 0.0500 0.04877 mg/Kg 98 69-141
Vinyl chloride 0.0500 0.04351 mg/Kg 87 63-150
Xylenes, Total 0.100 0.09811 mg/Kg 98 70-130
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-385041/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
4-Bromofluorobenzene (Surr)70 -130
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
116Dibromofluoromethane (Surr)70 -130
1221,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-385041/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
Acetone 0.250 0.2326 mg/Kg 93 45-145 1 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05065 mg/Kg 101 70-130 1 37
Bromobenzene 0.0500 0.05351 mg/Kg 107 67-130 20 40
Bromochloromethane 0.0500 0.05769 mg/Kg 115 70-133 1 15
Bromodichloromethane 0.0500 0.05283 mg/Kg 106 70-130 0 20
Bromoform 0.0500 0.04877 mg/Kg 98 59-137 1 17
Bromomethane 0.0500 0.06089 mg/Kg 122 32-150 0 45
2-Butanone (MEK)0.250 0.2276 mg/Kg 91 50-149 1 39
Carbon disulfide 0.0500 0.04591 mg/Kg 92 66-138 0 41
Carbon tetrachloride 0.0500 0.06184 mg/Kg 124 70-131 2 41
Chlorobenzene 0.0500 0.05017 mg/Kg 100 70-130 2 40
Chlorodibromomethane 0.0500 0.04992 mg/Kg 100 70-130 1 14
Chloroethane 0.0500 0.05154 mg/Kg 103 37-150 2 50
Chloroform 0.0500 0.05960 mg/Kg 119 70-130 1 15
Chloromethane 0.0500 0.03443 mg/Kg 69 53-150 0 47
2-Chlorotoluene 0.0500 0.05863 mg/Kg 117 70-132 19 41
4-Chlorotoluene 0.0500 0.05978 mg/Kg 120 67-135 20 41
cis-1,2-Dichloroethene 0.0500 0.05538 mg/Kg 111 70-132 1 18
cis-1,3-Dichloropropene 0.0500 0.04831 mg/Kg 97 70-130 0 42
1,2-Dibromo-3-Chloropropane 0.0500 0.04309 mg/Kg 86 47-144 20 38
1,2-Dibromoethane (EDB)0.0500 0.04926 mg/Kg 99 69-130 2 17
Dibromomethane 0.0500 0.05644 mg/Kg 113 70-130 2 19
1,2-Dichlorobenzene 0.0500 0.05261 mg/Kg 105 70-134 6 40
1,3-Dichlorobenzene 0.0500 0.05022 mg/Kg 100 69-137 3 41
1,4-Dichlorobenzene 0.0500 0.05154 mg/Kg 103 66-134 5 41
Dichlorodifluoromethane 0.0500 0.04638 mg/Kg 93 32-150 1 50
1,1-Dichloroethane 0.0500 0.04981 mg/Kg 100 70-130 1 42
1,2-Dichloroethane 0.0500 0.06010 mg/Kg 120 65-134 1 16
1,1-Dichloroethene 0.0500 0.05045 mg/Kg 101 70-131 2 43
1,2-Dichloroethene, Total 0.100 0.1074 mg/Kg 107 70-130 2 41
1,2-Dichloropropane 0.0500 0.04836 mg/Kg 97 70-130 2 15
1,3-Dichloropropane 0.0500 0.04761 mg/Kg 95 70-130 2 15
2,2-Dichloropropane 0.0500 0.05588 mg/Kg 112 57-150 1 42
1,1-Dichloropropene 0.0500 0.05300 mg/Kg 106 70-130 2 41
Diisopropyl ether 0.0500 0.05156 mg/Kg 103 68-134 0 36
Ethylbenzene 0.0500 0.05096 mg/Kg 102 70-130 2 38
Hexachlorobutadiene 0.0500 0.04996 mg/Kg 100 64-137 19 44
2-Hexanone 0.250 0.2104 mg/Kg 84 47-148 0 38
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-385041/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385041
Isopropylbenzene 0.0500 0.05228 mg/Kg 105 70-130 3 39
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.05099 mg/Kg 102 69-130 2 19
4-Methyl-2-pentanone (MIBK)0.250 0.2183 mg/Kg 87 48-150 0 41
Methyl tert-butyl ether 0.0500 0.05268 mg/Kg 105 54-145 1 36
Naphthalene 0.0500 0.04512 mg/Kg 90 55-149 15 37
n-Butylbenzene 0.0500 0.05092 mg/Kg 102 57-150 4 39
N-Propylbenzene 0.0500 0.05747 mg/Kg 115 62-150 18 38
p-Isopropyltoluene 0.0500 0.05034 mg/Kg 101 66-147 4 38
sec-Butylbenzene 0.0500 0.05782 mg/Kg 116 68-147 16 38
Styrene 0.0500 0.04955 mg/Kg 99 70-131 0 40
tert-Butylbenzene 0.0500 0.05894 mg/Kg 118 70-138 20 38
1,1,1,2-Tetrachloroethane 0.0500 0.05137 mg/Kg 103 70-130 3 41
1,1,2,2-Tetrachloroethane 0.0500 0.05062 *mg/Kg 101 61-134 17 16
Tetrachloroethene 0.0500 0.05283 mg/Kg 106 70-130 1 41
Toluene 0.0500 0.05129 mg/Kg 103 70-130 1 40
trans-1,2-Dichloroethene 0.0500 0.05203 mg/Kg 104 70-130 3 41
trans-1,3-Dichloropropene 0.0500 0.04988 mg/Kg 100 67-130 1 41
1,2,3-Trichlorobenzene 0.0500 0.04754 mg/Kg 95 57-146 17 42
1,2,4-Trichlorobenzene 0.0500 0.04761 mg/Kg 95 47-150 17 43
1,1,1-Trichloroethane 0.0500 0.06125 mg/Kg 123 70-130 0 41
1,1,2-Trichloroethane 0.0500 0.04764 mg/Kg 95 70-130 0 17
Trichloroethene 0.0500 0.05460 mg/Kg 109 70-130 1 41
Trichlorofluoromethane 0.0500 0.05850 mg/Kg 117 53-150 0 49
1,2,3-Trichloropropane 0.0500 0.05404 *mg/Kg 108 60-139 18 16
1,2,4-Trimethylbenzene 0.0500 0.05852 mg/Kg 117 70-140 20 38
1,3,5-Trimethylbenzene 0.0500 0.05891 mg/Kg 118 69-141 19 38
Vinyl chloride 0.0500 0.04213 mg/Kg 84 63-150 3 46
Xylenes, Total 0.100 0.09932 mg/Kg 99 70-130 1 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
110
LCSD LCSD
Qualifier Limits%Recovery
115Dibromofluoromethane (Surr)70 -130
1221,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-385160/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
RL MDL
Acetone ND 0.0500 mg/Kg 11/09/16 13:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 11/09/16 13:25 1Benzene
ND 0.00200 mg/Kg 11/09/16 13:25 1Bromobenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1Bromochloromethane
ND 0.00200 mg/Kg 11/09/16 13:25 1Bromodichloromethane
ND 0.00200 mg/Kg 11/09/16 13:25 1Bromoform
ND 0.00200 mg/Kg 11/09/16 13:25 1Bromomethane
ND 0.0500 mg/Kg 11/09/16 13:25 12-Butanone (MEK)
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-385160/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
RL MDL
Carbon disulfide ND 0.00500 mg/Kg 11/09/16 13:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 11/09/16 13:25 1Carbon tetrachloride
ND 0.00200 mg/Kg 11/09/16 13:25 1Chlorobenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1Chlorodibromomethane
ND 0.00500 mg/Kg 11/09/16 13:25 1Chloroethane
ND 0.00200 mg/Kg 11/09/16 13:25 1Chloroform
ND 0.00200 mg/Kg 11/09/16 13:25 1Chloromethane
ND 0.00200 mg/Kg 11/09/16 13:25 12-Chlorotoluene
ND 0.00200 mg/Kg 11/09/16 13:25 14-Chlorotoluene
ND 0.00200 mg/Kg 11/09/16 13:25 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 11/09/16 13:25 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 11/09/16 13:25 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 11/09/16 13:25 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 11/09/16 13:25 1Dibromomethane
ND 0.00200 mg/Kg 11/09/16 13:25 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 11/09/16 13:25 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 11/09/16 13:25 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 11/09/16 13:25 11,1-Dichloroethane
ND 0.00200 mg/Kg 11/09/16 13:25 11,2-Dichloroethane
ND 0.00200 mg/Kg 11/09/16 13:25 11,1-Dichloroethene
ND 0.00200 mg/Kg 11/09/16 13:25 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 11/09/16 13:25 11,2-Dichloropropane
ND 0.00200 mg/Kg 11/09/16 13:25 11,3-Dichloropropane
ND 0.00200 mg/Kg 11/09/16 13:25 12,2-Dichloropropane
ND 0.00200 mg/Kg 11/09/16 13:25 11,1-Dichloropropene
ND 0.00200 mg/Kg 11/09/16 13:25 1Diisopropyl ether
ND 0.00200 mg/Kg 11/09/16 13:25 1Ethylbenzene
ND 0.00500 mg/Kg 11/09/16 13:25 1Hexachlorobutadiene
ND 0.0500 mg/Kg 11/09/16 13:25 12-Hexanone
ND 0.00200 mg/Kg 11/09/16 13:25 1Isopropylbenzene
ND 0.0100 mg/Kg 11/09/16 13:25 1Methylene Chloride
ND 0.0500 mg/Kg 11/09/16 13:25 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 11/09/16 13:25 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 11/09/16 13:25 1Naphthalene
ND 0.00200 mg/Kg 11/09/16 13:25 1n-Butylbenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1N-Propylbenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1p-Isopropyltoluene
ND 0.00200 mg/Kg 11/09/16 13:25 1sec-Butylbenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1Styrene
ND 0.00200 mg/Kg 11/09/16 13:25 1tert-Butylbenzene
ND 0.00200 mg/Kg 11/09/16 13:25 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 11/09/16 13:25 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 11/09/16 13:25 1Tetrachloroethene
ND 0.00200 mg/Kg 11/09/16 13:25 1Toluene
ND 0.00200 mg/Kg 11/09/16 13:25 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 11/09/16 13:25 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 11/09/16 13:25 11,2,3-Trichlorobenzene
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-385160/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
RL MDL
1,2,4-Trichlorobenzene ND 0.00200 mg/Kg 11/09/16 13:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 11/09/16 13:25 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 11/09/16 13:25 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 11/09/16 13:25 1Trichloroethene
ND 0.00200 mg/Kg 11/09/16 13:25 1Trichlorofluoromethane
ND 0.00200 mg/Kg 11/09/16 13:25 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 11/09/16 13:25 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 11/09/16 13:25 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 11/09/16 13:25 1Vinyl chloride
ND 0.00600 mg/Kg 11/09/16 13:25 1Xylenes, Total
4-Bromofluorobenzene (Surr)106 70-130 11/09/16 13:25 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
112 11/09/16 13:25 1Dibromofluoromethane (Surr)70-130
117 11/09/16 13:25 11,2-Dichloroethane-d4 (Surr)70-130
99 11/09/16 13:25 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-385160/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
Acetone 0.250 0.2134 mg/Kg 85 45-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05253 mg/Kg 105 70-130
Bromobenzene 0.0500 0.04749 mg/Kg 95 67-130
Bromochloromethane 0.0500 0.05424 mg/Kg 108 70-133
Bromodichloromethane 0.0500 0.05273 mg/Kg 105 70-130
Bromoform 0.0500 0.04569 mg/Kg 91 59-137
Bromomethane 0.0500 0.05372 mg/Kg 107 32-150
2-Butanone (MEK)0.250 0.2053 mg/Kg 82 50-149
Carbon disulfide 0.0500 0.05055 mg/Kg 101 66-138
Carbon tetrachloride 0.0500 0.06138 mg/Kg 123 70-131
Chlorobenzene 0.0500 0.05152 mg/Kg 103 70-130
Chlorodibromomethane 0.0500 0.04874 mg/Kg 97 70-130
Chloroethane 0.0500 0.05100 mg/Kg 102 37-150
Chloroform 0.0500 0.05724 mg/Kg 114 70-130
Chloromethane 0.0500 0.04268 mg/Kg 85 53-150
2-Chlorotoluene 0.0500 0.05244 mg/Kg 105 70-132
4-Chlorotoluene 0.0500 0.05314 mg/Kg 106 67-135
cis-1,2-Dichloroethene 0.0500 0.05798 mg/Kg 116 70-132
cis-1,3-Dichloropropene 0.0500 0.04922 mg/Kg 98 70-130
1,2-Dibromo-3-Chloropropane 0.0500 0.03837 mg/Kg 77 47-144
1,2-Dibromoethane (EDB)0.0500 0.04679 mg/Kg 94 69-130
Dibromomethane 0.0500 0.05310 mg/Kg 106 70-130
1,2-Dichlorobenzene 0.0500 0.05257 mg/Kg 105 70-134
1,3-Dichlorobenzene 0.0500 0.05364 mg/Kg 107 69-137
1,4-Dichlorobenzene 0.0500 0.05324 mg/Kg 106 66-134
Dichlorodifluoromethane 0.0500 0.05053 mg/Kg 101 32-150
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-385160/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
1,1-Dichloroethane 0.0500 0.05310 mg/Kg 106 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 0.0500 0.05699 mg/Kg 114 65-134
1,1-Dichloroethene 0.0500 0.05250 mg/Kg 105 70-131
1,2-Dichloroethene, Total 0.100 0.1142 mg/Kg 114 70-130
1,2-Dichloropropane 0.0500 0.05166 mg/Kg 103 70-130
1,3-Dichloropropane 0.0500 0.04727 mg/Kg 95 70-130
2,2-Dichloropropane 0.0500 0.05747 mg/Kg 115 57-150
1,1-Dichloropropene 0.0500 0.05386 mg/Kg 108 70-130
Diisopropyl ether 0.0500 0.05403 mg/Kg 108 68-134
Ethylbenzene 0.0500 0.05170 mg/Kg 103 70-130
Hexachlorobutadiene 0.0500 0.05618 mg/Kg 112 64-137
2-Hexanone 0.250 0.1910 mg/Kg 76 47-148
Isopropylbenzene 0.0500 0.05289 mg/Kg 106 70-130
Methylene Chloride 0.0500 0.05203 mg/Kg 104 69-130
4-Methyl-2-pentanone (MIBK)0.250 0.1972 mg/Kg 79 48-150
Methyl tert-butyl ether 0.0500 0.04986 mg/Kg 100 54-145
Naphthalene 0.0500 0.04349 mg/Kg 87 55-149
n-Butylbenzene 0.0500 0.05299 mg/Kg 106 57-150
N-Propylbenzene 0.0500 0.05272 mg/Kg 105 62-150
p-Isopropyltoluene 0.0500 0.05248 mg/Kg 105 66-147
sec-Butylbenzene 0.0500 0.05349 mg/Kg 107 68-147
Styrene 0.0500 0.05126 mg/Kg 103 70-131
tert-Butylbenzene 0.0500 0.05187 mg/Kg 104 70-138
1,1,1,2-Tetrachloroethane 0.0500 0.05102 mg/Kg 102 70-130
1,1,2,2-Tetrachloroethane 0.0500 0.04367 mg/Kg 87 61-134
Tetrachloroethene 0.0500 0.05509 mg/Kg 110 70-130
Toluene 0.0500 0.05230 mg/Kg 105 70-130
trans-1,2-Dichloroethene 0.0500 0.05626 mg/Kg 113 70-130
trans-1,3-Dichloropropene 0.0500 0.04912 mg/Kg 98 67-130
1,2,3-Trichlorobenzene 0.0500 0.05103 mg/Kg 102 57-146
1,2,4-Trichlorobenzene 0.0500 0.05203 mg/Kg 104 47-150
1,1,1-Trichloroethane 0.0500 0.06028 mg/Kg 121 70-130
1,1,2-Trichloroethane 0.0500 0.04677 mg/Kg 94 70-130
Trichloroethene 0.0500 0.05510 mg/Kg 110 70-130
Trichlorofluoromethane 0.0500 0.05606 mg/Kg 112 53-150
1,2,3-Trichloropropane 0.0500 0.04404 mg/Kg 88 60-139
1,2,4-Trimethylbenzene 0.0500 0.05293 mg/Kg 106 70-140
1,3,5-Trimethylbenzene 0.0500 0.05217 mg/Kg 104 69-141
Vinyl chloride 0.0500 0.04501 mg/Kg 90 63-150
Xylenes, Total 0.100 0.1029 mg/Kg 103 70-130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
108Dibromofluoromethane (Surr)70 -130
1091,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-385160/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
Acetone 0.250 0.2360 mg/Kg 94 45-145 10 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05270 mg/Kg 105 70-130 0 37
Bromobenzene 0.0500 0.04752 mg/Kg 95 67-130 0 40
Bromochloromethane 0.0500 0.05556 mg/Kg 111 70-133 2 15
Bromodichloromethane 0.0500 0.05392 mg/Kg 108 70-130 2 20
Bromoform 0.0500 0.04782 mg/Kg 96 59-137 5 17
Bromomethane 0.0500 0.05316 mg/Kg 106 32-150 1 45
2-Butanone (MEK)0.250 0.2255 mg/Kg 90 50-149 9 39
Carbon disulfide 0.0500 0.05000 mg/Kg 100 66-138 1 41
Carbon tetrachloride 0.0500 0.06167 mg/Kg 123 70-131 0 41
Chlorobenzene 0.0500 0.05136 mg/Kg 103 70-130 0 40
Chlorodibromomethane 0.0500 0.04918 mg/Kg 98 70-130 1 14
Chloroethane 0.0500 0.05043 mg/Kg 101 37-150 1 50
Chloroform 0.0500 0.05830 mg/Kg 117 70-130 2 15
Chloromethane 0.0500 0.04539 mg/Kg 91 53-150 6 47
2-Chlorotoluene 0.0500 0.05193 mg/Kg 104 70-132 1 41
4-Chlorotoluene 0.0500 0.05244 mg/Kg 105 67-135 1 41
cis-1,2-Dichloroethene 0.0500 0.05846 mg/Kg 117 70-132 1 18
cis-1,3-Dichloropropene 0.0500 0.04992 mg/Kg 100 70-130 1 42
1,2-Dibromo-3-Chloropropane 0.0500 0.04330 mg/Kg 87 47-144 12 38
1,2-Dibromoethane (EDB)0.0500 0.04960 mg/Kg 99 69-130 6 17
Dibromomethane 0.0500 0.05521 mg/Kg 110 70-130 4 19
1,2-Dichlorobenzene 0.0500 0.05366 mg/Kg 107 70-134 2 40
1,3-Dichlorobenzene 0.0500 0.05256 mg/Kg 105 69-137 2 41
1,4-Dichlorobenzene 0.0500 0.05269 mg/Kg 105 66-134 1 41
Dichlorodifluoromethane 0.0500 0.05228 mg/Kg 105 32-150 3 50
1,1-Dichloroethane 0.0500 0.05342 mg/Kg 107 70-130 1 42
1,2-Dichloroethane 0.0500 0.05893 mg/Kg 118 65-134 3 16
1,1-Dichloroethene 0.0500 0.05262 mg/Kg 105 70-131 0 43
1,2-Dichloroethene, Total 0.100 0.1145 mg/Kg 115 70-130 0 41
1,2-Dichloropropane 0.0500 0.05292 mg/Kg 106 70-130 2 15
1,3-Dichloropropane 0.0500 0.04940 mg/Kg 99 70-130 4 15
2,2-Dichloropropane 0.0500 0.05706 mg/Kg 114 57-150 1 42
1,1-Dichloropropene 0.0500 0.05460 mg/Kg 109 70-130 1 41
Diisopropyl ether 0.0500 0.05498 mg/Kg 110 68-134 2 36
Ethylbenzene 0.0500 0.05178 mg/Kg 104 70-130 0 38
Hexachlorobutadiene 0.0500 0.05662 mg/Kg 113 64-137 1 44
2-Hexanone 0.250 0.2103 mg/Kg 84 47-148 10 38
Isopropylbenzene 0.0500 0.05295 mg/Kg 106 70-130 0 39
Methylene Chloride 0.0500 0.05239 mg/Kg 105 69-130 1 19
4-Methyl-2-pentanone (MIBK)0.250 0.2176 mg/Kg 87 48-150 10 41
Methyl tert-butyl ether 0.0500 0.05169 mg/Kg 103 54-145 4 36
Naphthalene 0.0500 0.04719 mg/Kg 94 55-149 8 37
n-Butylbenzene 0.0500 0.05348 mg/Kg 107 57-150 1 39
N-Propylbenzene 0.0500 0.05210 mg/Kg 104 62-150 1 38
p-Isopropyltoluene 0.0500 0.05119 mg/Kg 102 66-147 3 38
sec-Butylbenzene 0.0500 0.05096 mg/Kg 102 68-147 5 38
Styrene 0.0500 0.05110 mg/Kg 102 70-131 0 40
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-385160/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385160
tert-Butylbenzene 0.0500 0.05178 mg/Kg 104 70-138 0 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1,2-Tetrachloroethane 0.0500 0.05128 mg/Kg 103 70-130 1 41
1,1,2,2-Tetrachloroethane 0.0500 0.04639 mg/Kg 93 61-134 6 16
Tetrachloroethene 0.0500 0.05427 mg/Kg 109 70-130 2 41
Toluene 0.0500 0.05163 mg/Kg 103 70-130 1 40
trans-1,2-Dichloroethene 0.0500 0.05606 mg/Kg 112 70-130 0 41
trans-1,3-Dichloropropene 0.0500 0.05029 mg/Kg 101 67-130 2 41
1,2,3-Trichlorobenzene 0.0500 0.05317 mg/Kg 106 57-146 4 42
1,2,4-Trichlorobenzene 0.0500 0.05377 mg/Kg 108 47-150 3 43
1,1,1-Trichloroethane 0.0500 0.06011 mg/Kg 120 70-130 0 41
1,1,2-Trichloroethane 0.0500 0.04874 mg/Kg 97 70-130 4 17
Trichloroethene 0.0500 0.05630 mg/Kg 113 70-130 2 41
Trichlorofluoromethane 0.0500 0.05444 mg/Kg 109 53-150 3 49
1,2,3-Trichloropropane 0.0500 0.04648 mg/Kg 93 60-139 5 16
1,2,4-Trimethylbenzene 0.0500 0.05252 mg/Kg 105 70-140 1 38
1,3,5-Trimethylbenzene 0.0500 0.05268 mg/Kg 105 69-141 1 38
Vinyl chloride 0.0500 0.04919 mg/Kg 98 63-150 9 46
Xylenes, Total 0.100 0.1025 mg/Kg 103 70-130 0 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
112Dibromofluoromethane (Surr)70 -130
1131,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-384397/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
RL MDL
Acenaphthene ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Acenaphthylene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Anthracene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Benzo[a]anthracene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Benzo[a]pyrene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Benzo[b]fluoranthene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Benzo[g,h,i]perylene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Benzo[k]fluoranthene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Bis(2-chloroethoxy)methane
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Bis(2-chloroethyl)ether
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1bis (2-chloroisopropyl) ether
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Bis(2-ethylhexyl) phthalate
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 14-Bromophenyl phenyl ether
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Butyl benzyl phthalate
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Carbazole
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 14-Chloroaniline
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-384397/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
RL MDL
4-Chloro-3-methylphenol ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12-Chloronaphthalene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12-Chlorophenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 14-Chlorophenyl phenyl ether
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Chrysene
ND 0.666 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Cresols
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Dibenz(a,h)anthracene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Dibenzofuran
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 11,2-Dichlorobenzene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 11,3-Dichlorobenzene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 11,4-Dichlorobenzene
ND 0.670 mg/Kg 11/05/16 11:09 11/07/16 20:27 13,3'-Dichlorobenzidine
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,4-Dichlorophenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Diethyl phthalate
ND 0.670 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,4-Dimethylphenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Dimethyl phthalate
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Di-n-butyl phthalate
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 14,6-Dinitro-2-methylphenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,4-Dinitrophenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,4-Dinitrotoluene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,6-Dinitrotoluene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Di-n-octyl phthalate
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Fluoranthene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Fluorene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Hexachlorobenzene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Hexachlorobutadiene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Hexachlorocyclopentadiene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Hexachloroethane
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Indeno[1,2,3-cd]pyrene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Isophorone
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 11-Methylnaphthalene
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 12-Methylnaphthalene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12-Methylphenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 13 & 4 Methylphenol
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Naphthalene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12-Nitroaniline
ND 0.670 mg/Kg 11/05/16 11:09 11/07/16 20:27 13-Nitroaniline
ND 0.670 mg/Kg 11/05/16 11:09 11/07/16 20:27 14-Nitroaniline
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Nitrobenzene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12-Nitrophenol
ND 0.670 mg/Kg 11/05/16 11:09 11/07/16 20:27 14-Nitrophenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1N-Nitrosodi-n-propylamine
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Pentachlorophenol
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Phenanthrene
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Phenol
ND 0.0670 mg/Kg 11/05/16 11:09 11/07/16 20:27 1Pyrene
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-384397/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
RL MDL
1,2,4-Trichlorobenzene ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,4,5-Trichlorophenol
ND 0.333 mg/Kg 11/05/16 11:09 11/07/16 20:27 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)90 29-120 11/07/16 20:27 1
MB MB
Surrogate
11/05/16 11:09
Dil FacPreparedAnalyzedQualifierLimits%Recovery
54 11/05/16 11:09 11/07/16 20:27 12-Fluorophenol (Surr)10-120
83 11/05/16 11:09 11/07/16 20:27 1Nitrobenzene-d5 (Surr)27-120
64 11/05/16 11:09 11/07/16 20:27 1Phenol-d5 (Surr)10-120
104 11/05/16 11:09 11/07/16 20:27 1Terphenyl-d14 (Surr)13-120
46 11/05/16 11:09 11/07/16 20:27 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-384397/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
Acenaphthene 1.67 1.335 mg/Kg 80 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.322 mg/Kg 79 38-120
Anthracene 1.67 1.373 mg/Kg 82 46-124
Benzo[a]anthracene 1.67 1.443 mg/Kg 87 45-120
Benzo[a]pyrene 1.67 1.447 mg/Kg 87 45-120
Benzo[b]fluoranthene 1.67 1.427 mg/Kg 86 42-120
Benzo[g,h,i]perylene 1.67 1.611 mg/Kg 97 38-120
Benzo[k]fluoranthene 1.67 1.612 mg/Kg 97 42-120
Bis(2-chloroethoxy)methane 1.67 1.232 mg/Kg 74 32-120
Bis(2-chloroethyl)ether 1.67 1.195 mg/Kg 72 31-120
bis (2-chloroisopropyl) ether 1.67 1.216 mg/Kg 73 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.524 mg/Kg 91 43-120
4-Bromophenyl phenyl ether 1.67 1.390 mg/Kg 83 40-120
Butyl benzyl phthalate 1.67 1.487 mg/Kg 89 43-133
Carbazole 1.67 1.393 mg/Kg 84 44-120
4-Chloroaniline 1.67 1.417 mg/Kg 85 35-120
4-Chloro-3-methylphenol 1.67 1.592 mg/Kg 96 38-120
2-Chloronaphthalene 1.67 1.308 mg/Kg 78 34-120
2-Chlorophenol 1.67 1.270 mg/Kg 76 32-120
4-Chlorophenyl phenyl ether 1.67 1.364 mg/Kg 82 42-120
Chrysene 1.67 1.437 mg/Kg 86 43-120
Cresols 3.33 2.805 mg/Kg 84 36-129
Dibenz(a,h)anthracene 1.67 1.529 mg/Kg 92 32-128
Dibenzofuran 1.67 1.335 mg/Kg 80 41-120
1,2-Dichlorobenzene 1.67 1.281 mg/Kg 77 33-120
1,3-Dichlorobenzene 1.67 1.282 mg/Kg 77 32-120
1,4-Dichlorobenzene 1.67 1.247 mg/Kg 75 32-120
3,3'-Dichlorobenzidine 1.67 1.207 mg/Kg 72 39-120
2,4-Dichlorophenol 1.67 1.436 mg/Kg 86 32-120
Diethyl phthalate 1.67 1.517 mg/Kg 91 41-122
2,4-Dimethylphenol 1.67 1.535 mg/Kg 92 32-120
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-384397/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
Dimethyl phthalate 1.67 1.441 mg/Kg 86 55-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Di-n-butyl phthalate 1.67 1.526 mg/Kg 92 46-127
4,6-Dinitro-2-methylphenol 3.33 2.313 mg/Kg 69 27-134
2,4-Dinitrophenol 3.33 1.984 mg/Kg 60 10-142
2,4-Dinitrotoluene 1.67 1.444 mg/Kg 87 43-120
2,6-Dinitrotoluene 1.67 1.354 mg/Kg 81 43-120
Di-n-octyl phthalate 1.67 1.577 mg/Kg 95 40-130
Fluoranthene 1.67 1.415 mg/Kg 85 46-120
Fluorene 1.67 1.347 mg/Kg 81 42-120
Hexachlorobenzene 1.67 1.455 mg/Kg 87 44-120
Hexachlorobutadiene 1.67 1.391 mg/Kg 83 31-120
Hexachlorocyclopentadiene 1.67 0.7469 mg/Kg 45 24-120
Hexachloroethane 1.67 1.421 mg/Kg 85 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.544 mg/Kg 93 41-121
Isophorone 1.67 1.219 mg/Kg 73 33-120
1-Methylnaphthalene 1.67 1.296 mg/Kg 78 32-120
2-Methylnaphthalene 1.67 1.305 mg/Kg 78 28-120
2-Methylphenol 1.67 1.426 mg/Kg 86 36-120
3 & 4 Methylphenol 1.67 1.379 mg/Kg 83 37-120
Naphthalene 1.67 1.276 mg/Kg 77 32-120
2-Nitroaniline 1.67 1.194 mg/Kg 72 40-120
3-Nitroaniline 1.67 1.304 mg/Kg 78 42-120
4-Nitroaniline 1.67 1.258 mg/Kg 75 43-120
Nitrobenzene 1.67 1.124 mg/Kg 67 26-120
2-Nitrophenol 1.67 1.283 mg/Kg 77 29-120
4-Nitrophenol 3.33 2.471 mg/Kg 74 32-136
N-Nitrosodi-n-propylamine 1.67 1.074 mg/Kg 64 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.368 mg/Kg 97 52-140
Pentachlorophenol 3.33 2.304 mg/Kg 69 44-134
Phenanthrene 1.67 1.368 mg/Kg 82 45-120
Phenol 1.67 1.199 mg/Kg 72 30-120
Pyrene 1.67 1.395 mg/Kg 84 43-120
1,2,4-Trichlorobenzene 1.67 1.251 mg/Kg 75 29-120
2,4,5-Trichlorophenol 1.67 1.503 mg/Kg 90 39-120
2,4,6-Trichlorophenol 1.67 1.408 mg/Kg 84 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
81
LCS LCS
Qualifier Limits%Recovery
752-Fluorophenol (Surr)10 -120
74Nitrobenzene-d5 (Surr)27 -120
78Phenol-d5 (Surr)10 -120
89Terphenyl-d14 (Surr)13 -120
1012,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-384397/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
Acenaphthene 1.67 1.436 mg/Kg 86 36-120 7 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 1.67 1.418 mg/Kg 85 38-120 7 50
Anthracene 1.67 1.432 mg/Kg 86 46-124 4 49
Benzo[a]anthracene 1.67 1.524 mg/Kg 91 45-120 5 50
Benzo[a]pyrene 1.67 1.519 mg/Kg 91 45-120 5 50
Benzo[b]fluoranthene 1.67 1.497 mg/Kg 90 42-120 5 50
Benzo[g,h,i]perylene 1.67 1.715 mg/Kg 103 38-120 6 50
Benzo[k]fluoranthene 1.67 1.605 mg/Kg 96 42-120 0 45
Bis(2-chloroethoxy)methane 1.67 1.335 mg/Kg 80 32-120 8 50
Bis(2-chloroethyl)ether 1.67 1.348 mg/Kg 81 31-120 12 50
bis (2-chloroisopropyl) ether 1.67 1.406 mg/Kg 84 32-120 15 50
Bis(2-ethylhexyl) phthalate 1.67 1.593 mg/Kg 96 43-120 4 50
4-Bromophenyl phenyl ether 1.67 1.481 mg/Kg 89 40-120 6 37
Butyl benzyl phthalate 1.67 1.513 mg/Kg 91 43-133 2 50
Carbazole 1.67 1.481 mg/Kg 89 44-120 6 46
4-Chloroaniline 1.67 1.552 mg/Kg 93 35-120 9 50
4-Chloro-3-methylphenol 1.67 1.729 mg/Kg 104 38-120 8 49
2-Chloronaphthalene 1.67 1.437 mg/Kg 86 34-120 9 50
2-Chlorophenol 1.67 1.429 mg/Kg 86 32-120 12 50
4-Chlorophenyl phenyl ether 1.67 1.457 mg/Kg 87 42-120 7 50
Chrysene 1.67 1.495 mg/Kg 90 43-120 4 49
Cresols 3.33 3.035 mg/Kg 91 36-129 8 50
Dibenz(a,h)anthracene 1.67 1.601 mg/Kg 96 32-128 5 50
Dibenzofuran 1.67 1.424 mg/Kg 85 41-120 7 50
1,2-Dichlorobenzene 1.67 1.433 mg/Kg 86 33-120 11 50
1,3-Dichlorobenzene 1.67 1.426 mg/Kg 86 32-120 11 50
1,4-Dichlorobenzene 1.67 1.394 mg/Kg 84 32-120 11 50
3,3'-Dichlorobenzidine 1.67 1.252 mg/Kg 75 39-120 4 50
2,4-Dichlorophenol 1.67 1.591 mg/Kg 95 32-120 10 50
Diethyl phthalate 1.67 1.618 mg/Kg 97 41-122 6 45
2,4-Dimethylphenol 1.67 1.605 mg/Kg 96 32-120 4 50
Dimethyl phthalate 1.67 1.518 mg/Kg 91 55-120 5 46
Di-n-butyl phthalate 1.67 1.609 mg/Kg 97 46-127 5 49
4,6-Dinitro-2-methylphenol 3.33 2.489 mg/Kg 75 27-134 7 50
2,4-Dinitrophenol 3.33 2.128 mg/Kg 64 10-142 7 50
2,4-Dinitrotoluene 1.67 1.562 mg/Kg 94 43-120 8 50
2,6-Dinitrotoluene 1.67 1.419 mg/Kg 85 43-120 5 50
Di-n-octyl phthalate 1.67 1.609 mg/Kg 97 40-130 2 50
Fluoranthene 1.67 1.499 mg/Kg 90 46-120 6 50
Fluorene 1.67 1.462 mg/Kg 88 42-120 8 50
Hexachlorobenzene 1.67 1.546 mg/Kg 93 44-120 6 50
Hexachlorobutadiene 1.67 1.500 mg/Kg 90 31-120 7 50
Hexachlorocyclopentadiene 1.67 0.7896 mg/Kg 47 24-120 6 50
Hexachloroethane 1.67 1.574 mg/Kg 94 33-120 10 50
Indeno[1,2,3-cd]pyrene 1.67 1.606 mg/Kg 96 41-121 4 50
Isophorone 1.67 1.321 mg/Kg 79 33-120 8 50
1-Methylnaphthalene 1.67 1.434 mg/Kg 86 32-120 10 50
2-Methylnaphthalene 1.67 1.409 mg/Kg 85 28-120 8 50
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-384397/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 384673 Prep Batch: 384397
2-Methylphenol 1.67 1.560 mg/Kg 94 36-120 9 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
3 & 4 Methylphenol 1.67 1.475 mg/Kg 88 37-120 7 50
Naphthalene 1.67 1.405 mg/Kg 84 32-120 10 50
2-Nitroaniline 1.67 1.291 mg/Kg 77 40-120 8 50
3-Nitroaniline 1.67 1.411 mg/Kg 85 42-120 8 49
4-Nitroaniline 1.67 1.369 mg/Kg 82 43-120 8 49
Nitrobenzene 1.67 1.210 mg/Kg 73 26-120 7 50
2-Nitrophenol 1.67 1.431 mg/Kg 86 29-120 11 50
4-Nitrophenol 3.33 2.752 mg/Kg 83 32-136 11 45
N-Nitrosodi-n-propylamine 1.67 1.249 mg/Kg 75 35-120 15 50
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.436 mg/Kg 101 52-140 5 50
Pentachlorophenol 3.33 2.456 mg/Kg 74 44-134 6 50
Phenanthrene 1.67 1.448 mg/Kg 87 45-120 6 50
Phenol 1.67 1.346 mg/Kg 81 30-120 12 50
Pyrene 1.67 1.452 mg/Kg 87 43-120 4 50
1,2,4-Trichlorobenzene 1.67 1.386 mg/Kg 83 29-120 10 50
2,4,5-Trichlorophenol 1.67 1.678 mg/Kg 101 39-120 11 50
2,4,6-Trichlorophenol 1.67 1.488 mg/Kg 89 39-120 6 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
86
LCSD LCSD
Qualifier Limits%Recovery
812-Fluorophenol (Surr)10 -120
79Nitrobenzene-d5 (Surr)27 -120
86Phenol-d5 (Surr)10 -120
96Terphenyl-d14 (Surr)13 -120
1062,4,6-Tribromophenol (Surr)10 -120
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-385520/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385701 Prep Batch: 385520
RL MDL
Mercury ND 0.0960 mg/Kg 11/10/16 09:42 11/10/16 12:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-385520/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385701 Prep Batch: 385520
Mercury 0.168 0.1523 mg/Kg 91 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 7471B - Mercury (CVAA) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-115389-E-1-D MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385701 Prep Batch: 385520
Mercury 0.268 F1 0.227 0.4374 F1 mg/Kg 75 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-115389-E-1-E MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385701 Prep Batch: 385520
Mercury 0.268 F1 0.227 0.4261 F1 mg/Kg 70 80-120 3 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 490-385105/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385350 Prep Batch: 385105
RL MDL
Chromium, hex ND 4.89 mg/Kg 11/09/16 08:47 11/09/16 16:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 490-385105/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385350 Prep Batch: 385105
Chromium, hex 63.4 51.48 mg/Kg 81 80-120
Analyte
LCSI LCSI
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 490-385105/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385350 Prep Batch: 385105
Chromium, hex 39.0 35.91 mg/Kg 92 80-120
Analyte
LCSS LCSS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 680-131744-G-21-A MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385350 Prep Batch: 385105
Chromium, hex ND F1 45.5 17.50 F1 mg/Kg 38 75-125☼
Analyte
MSS MSS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 680-131744-G-21-B MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385350 Prep Batch: 385105
Chromium, hex ND F1 75.0 65.23 mg/Kg 87 75-125☼
Analyte
MSI MSI
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method: 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: DuplicateLab Sample ID: 680-131744-G-21-D DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 385350 Prep Batch: 385105
Chromium, hex ND F1 ND mg/Kg NC 20☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: Moisture - Percent Moisture
Client Sample ID: OWS-ELab Sample ID: 490-115387-1 DU
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 384183
Percent Solids 77.5 78.5 %1 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
GC/MS VOA
Prep Batch: 384068
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035490-115387-1 OWS-E Total/NA
Soil 5035490-115387-1 OWS-E Total/NA
Analysis Batch: 385041
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 384068490-115387-1 OWS-E Total/NA
Solid 8260BMB 490-385041/7 Method Blank Total/NA
Solid 8260BLCS 490-385041/4 Lab Control Sample Total/NA
Solid 8260BLCSD 490-385041/5 Lab Control Sample Dup Total/NA
Analysis Batch: 385160
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 384068490-115387-1 OWS-E Total/NA
Solid 8260BMB 490-385160/6 Method Blank Total/NA
Solid 8260BLCS 490-385160/3 Lab Control Sample Total/NA
Solid 8260BLCSD 490-385160/4 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 384397
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3550C490-115387-1 OWS-E Total/NA
Solid 3550CMB 490-384397/1-A Method Blank Total/NA
Solid 3550CLCS 490-384397/2-A Lab Control Sample Total/NA
Solid 3550CLCSD 490-384397/4-A Lab Control Sample Dup Total/NA
Analysis Batch: 384673
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270D 384397490-115387-1 OWS-E Total/NA
Solid 8270D 384397MB 490-384397/1-A Method Blank Total/NA
Solid 8270D 384397LCS 490-384397/2-A Lab Control Sample Total/NA
Solid 8270D 384397LCSD 490-384397/4-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 384486
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3051A490-115387-1 OWS-E Total/NA
Prep Batch: 385520
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-115387-1 OWS-E Total/NA
Solid 7471BMB 490-385520/1-A Method Blank Total/NA
Solid 7471BLCS 490-385520/2-A Lab Control Sample Total/NA
Solid 7471B490-115389-E-1-D MS Matrix Spike Total/NA
Solid 7471B490-115389-E-1-E MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 385701
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 385520490-115387-1 OWS-E Total/NA
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Metals (Continued)
Analysis Batch: 385701 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 385520MB 490-385520/1-A Method Blank Total/NA
Solid 7471B 385520LCS 490-385520/2-A Lab Control Sample Total/NA
Solid 7471B 385520490-115389-E-1-D MS Matrix Spike Total/NA
Solid 7471B 385520490-115389-E-1-E MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 386253
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 384486490-115387-1 OWS-E Total/NA
General Chemistry
Analysis Batch: 384183
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture490-115387-1 OWS-E Total/NA
Soil Moisture490-115387-1 DU OWS-E Total/NA
Prep Batch: 385105
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3060A490-115387-1 OWS-E Total/NA
Solid 3060AMB 490-385105/1-A Method Blank Total/NA
Solid 3060ALCSI 490-385105/3-A Lab Control Sample Total/NA
Solid 3060ALCSS 490-385105/2-A Lab Control Sample Total/NA
Solid 3060A680-131744-G-21-A MSS Matrix Spike Total/NA
Solid 3060A680-131744-G-21-B MSI Matrix Spike Total/NA
Solid 3060A680-131744-G-21-D DU Duplicate Total/NA
Analysis Batch: 385350
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7196A 385105490-115387-1 OWS-E Total/NA
Solid 7196A 385105MB 490-385105/1-A Method Blank Total/NA
Solid 7196A 385105LCSI 490-385105/3-A Lab Control Sample Total/NA
Solid 7196A 385105LCSS 490-385105/2-A Lab Control Sample Total/NA
Solid 7196A 385105680-131744-G-21-A MSS Matrix Spike Total/NA
Solid 7196A 385105680-131744-G-21-B MSI Matrix Spike Total/NA
Solid 7196A 385105680-131744-G-21-D DU Duplicate Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-115387-1
Project/Site: LEN-001 SDG: LEN-001
Client Sample ID: OWS-E Lab Sample ID: 490-115387-1
Matrix: SoilDate Collected: 11/02/16 10:00
Date Received: 11/03/16 09:05
Prep 5035 JLP11/02/16 09:00 TAL NSH384068
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.588 g 5.0 mL
Analysis 8260B 1 385041 11/09/16 01:18 EML TAL NSHTotal/NA 5 g 5 mL
Prep 5035 384068 11/02/16 09:00 JLP TAL NSHTotal/NA 6.783 g 5.0 mL
Analysis 8260B 1 385160 11/09/16 16:20 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 384397 11/05/16 11:09 LOJ TAL NSHTotal/NA 38.97 g 1.00 mL
Analysis 8270D 1 384673 11/08/16 00:59 T1C TAL NSHTotal/NA
Prep 3051A 384486 11/06/16 12:48 PG1 TAL NSHTotal/NA 0.509 g 100 mL
Analysis 6010D 1 386253 11/11/16 19:04 TSC TAL NSHTotal/NA
Prep 7471B 385520 11/10/16 09:42 LCS TAL NSHTotal/NA 0.600 g 100 mL
Analysis 7471B 1 385701 11/10/16 13:21 LCS TAL NSHTotal/NA
Prep 3060A 385105 11/09/16 08:47 DJP TAL NSHTotal/NA 2.5022 g 500 mL
Analysis 7196A 1 385350 11/09/16 16:13 BLM TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 384183 11/04/16 11:42 AAB TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-115387-1Client: Hart & Hickman, PC
SDG: LEN-001Project/Site: LEN-001
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
SW8467196AChromium, Hexavalent TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-115387-1
Project/Site: LEN-001 SDG: LEN-001
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Moisture Soil Percent Solids
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-115387-1
SDG Number: LEN-001
Login Number: 115387
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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Appendix B

Disposal Documents