16017_Carolina_Medical_IA_Quality_Study_Results_20120516

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): C205450
Raleigh, NC 27616
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Carolina Medical
Attn: Kirk Pollard
Mineral Springs Environmental (MI017)
4600 Mineral Springs Lane
Bill Scott
Project Manager
Wednesday, May 16, 2012
RE: Laboratory Results for
Dear Kirk Pollard,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, May 11, 2012.
The total number of pages in this report, including this page is 23.
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SAMPLE SUMMARY/LABORATORY CHRONICLE
JS-089 C205450-01RE1 Sampled:05/10/12 17:15 Received:05/11/12 10:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
TO-15 06/09/12 05/15/12 11:00 5/15/2012 13:29
JS-055 C205450-02RE1 Sampled:05/10/12 17:15 Received:05/11/12 10:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
TO-15 06/09/12 05/15/12 11:00 5/15/2012 15:20
JS-024 C205450-03RE1 Sampled:05/10/12 17:15 Received:05/11/12 10:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
TO-15 06/09/12 05/15/12 11:00 5/15/2012 16:34
JS-043 C205450-04RE1 Sampled:05/10/12 17:15 Received:05/11/12 10:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
TO-15 06/09/12 05/15/12 11:00 5/15/2012 17:11
JS-039 C205450-05RE1 Sampled:05/10/12 17:15 Received:05/11/12 10:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
TO-15 06/09/12 05/15/12 11:00 5/15/2012 17:49
JS-096 C205450-06RE1 Sampled:05/10/12 17:15 Received:05/11/12 10:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
TO-15 06/09/12 05/15/12 11:00 5/15/2012 18:26
Page 2 of 23
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SAMPLE DETECTION SUMMARY
Lab ID:Client ID:JS-089 C205450-01RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.7 2.5 ppbv TO-15J 1,3-Butadiene 1.5
2.0 2.5 ppbv TO-15J 2-Butanone 0.77
5.6 2.5 ppbv TO-15 2-Propanol 0.83
11 2.5 ppbv TO-15 4-Ethyltoluene 0.98
7.3 2.5 ppbv TO-15 Acetone 0.66
4.4 2.5 ppbv TO-15 Benzene 0.39
2.0 2.5 ppbv TO-15J Ethylbenzene 0.49
1.3 2.5 ppbv TO-15J Heptane 0.98
1.6 2.5 ppbv TO-15JB J-01Methylene chloride 0.78
5.5 2.5 ppbv TO-15 Propene 1.6
1.5 2.5 ppbv TO-15J Styrene 0.63
4.1 2.5 ppbv TO-15 Toluene 0.45
5.8 2.5 ppbv TO-15 Xylenes (Total)1.0
Lab ID:Client ID:JS-055 C205450-02RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
3.3 2.5 ppbv TO-15 1,3-Butadiene 1.5
3.0 2.5 ppbv TO-15 2-Butanone 0.77
3.1 2.5 ppbv TO-15 2-Propanol 0.83
24 2.5 ppbv TO-15 4-Ethyltoluene 0.98
12 2.5 ppbv TO-15 Acetone 0.66
7.9 2.5 ppbv TO-15 Benzene 0.39
3.9 2.5 ppbv TO-15 Ethylbenzene 0.49
1.2 2.5 ppbv TO-15J Heptane 0.98
3.3 2.5 ppbv TO-15B J-01Methylene chloride 0.78
0.98 2.5 ppbv TO-15J n-Hexane 0.82
11 2.5 ppbv TO-15 Propene 1.6
2.7 2.5 ppbv TO-15 Styrene 0.63
7.9 2.5 ppbv TO-15 Toluene 0.45
280 240 ppbv TO-15 Total Light Petroleum Hydrocarbons 240
12 2.5 ppbv TO-15 JXylenes (Total)1.0
Lab ID:Client ID:JS-024 C205450-03RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.2 2.5 ppbv TO-15J 2,2,4-Trimethylpentane 0.74
1.5 2.5 ppbv TO-15J 2-Butanone 0.77
1.5 2.5 ppbv TO-15J 2-Propanol 0.83
2.4 2.5 ppbv TO-15J 4-Ethyltoluene 0.98
9.4 2.5 ppbv TO-15 Acetone 0.66
2.2 2.5 ppbv TO-15J Benzene 0.39
0.50 2.5 ppbv TO-15J Ethylbenzene 0.49
1.2 2.5 ppbv TO-15JB J-01Methylene chloride 0.78
2.5 2.5 ppbv TO-15 Propene 1.6
0.82 2.5 ppbv TO-15J Tetrachloroethene 0.56
1.3 2.5 ppbv TO-15J Toluene 0.45
1.4 2.5 ppbv TO-15J Xylenes (Total)1.0
Lab ID:Client ID:JS-043 C205450-04RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
Page 3 of 23
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Lab ID:Client ID:JS-043 C205450-04RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.6 2.5 ppbv TO-15J 1,3-Butadiene 1.5
1.7 2.5 ppbv TO-15J 2-Butanone 0.77
2.4 2.5 ppbv TO-15J 2-Propanol 0.83
10 2.5 ppbv TO-15 4-Ethyltoluene 0.98
10 2.5 ppbv TO-15 Acetone 0.66
3.9 2.5 ppbv TO-15 Benzene 0.39
1.7 2.5 ppbv TO-15J Ethylbenzene 0.49
3.7 2.5 ppbv TO-15B J-01Methylene chloride 0.78
2.3 2.5 ppbv TO-15J n-Hexane 0.82
5.2 2.5 ppbv TO-15 Propene 1.6
1.1 2.5 ppbv TO-15J Styrene 0.63
0.87 2.5 ppbv TO-15J Tetrachloroethene 0.56
4.0 2.5 ppbv TO-15 Toluene 0.45
5.0 2.5 ppbv TO-15 Xylenes (Total)1.0
Lab ID:Client ID:JS-039 C205450-05RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.6 2.5 ppbv TO-15J 2-Butanone 0.77
1.5 2.5 ppbv TO-15J 2-Propanol 0.83
5.9 2.5 ppbv TO-15 4-Ethyltoluene 0.98
10 2.5 ppbv TO-15 Acetone 0.66
2.3 2.5 ppbv TO-15J Benzene 0.39
1.0 2.5 ppbv TO-15J Ethylbenzene 0.49
5.7 2.5 ppbv TO-15B J-01Methylene chloride 0.78
1.0 2.5 ppbv TO-15J n-Hexane 0.82
3.1 2.5 ppbv TO-15 Propene 1.6
0.66 2.5 ppbv TO-15J Styrene 0.63
2.4 2.5 ppbv TO-15J Toluene 0.45
3.0 2.5 ppbv TO-15 JXylenes (Total)1.0
Lab ID:Client ID:JS-096 C205450-06RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.0 2.5 ppbv TO-15J 2-Butanone 0.77
1.1 2.5 ppbv TO-15J 2-Propanol 0.83
5.5 2.5 ppbv TO-15 Acetone 0.66
2.3 2.5 ppbv TO-15JB J-01Methylene chloride 0.78
0.74 2.5 ppbv TO-15J Toluene 0.45
Page 4 of 23
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ANALYTICAL RESULTS
JS-089Description:Lab Sample ID:C205450-01 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 13:291,1,1-Trichloroethane [71-55-6]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,1,2,2-Tetrachloroethane [79-34-5]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,1,2-Trichloroethane [79-00-5]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,1-Dichloroethane [75-34-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,1-Dichloroethene [75-35-4]1 0.94 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,2,4-Trichlorobenzene [120-82-1]1 0.67 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,2,4-Trimethylbenzene [95-63-6]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,2-Dibromoethane [106-93-4]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,2-Dichlorobenzene [95-50-1]1 1.8 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,2-Dichloroethane [107-06-2]1 0.51 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,2-Dichloropropane [78-87-5]1 0.47 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,3,5-Trimethylbenzene [108-67-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,3-Butadiene [106-99-0]1 1.5 GMB2E150092.51.7 J
ppbv TO-15 05/15/12 13:291,3-Dichlorobenzene [541-73-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,4-Dichlorobenzene [106-46-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:291,4-Dioxane [123-91-1]1 0.57 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:292,2,4-Trimethylpentane [540-84-1]1 0.74 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:292-Butanone [78-93-3]1 0.77 GMB2E150092.52.0 J
ppbv TO-15 05/15/12 13:292-Hexanone [591-78-6]1 0.85 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:292-Propanol [67-63-0]1 0.83 GMB2E150092.55.6
ppbv TO-15 05/15/12 13:293-Chloropropene [107-05-1]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:294-Ethyltoluene [622-96-8]1 0.98 GMB2E150092.511
ppbv TO-15 05/15/12 13:294-Methyl-2-pentanone [108-10-1]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Acetone [67-64-1]1 0.66 GMB2E150092.57.3
ppbv TO-15 05/15/12 13:29Benzene [71-43-2]1 0.39 GMB2E150092.54.4
ppbv TO-15 05/15/12 13:29Benzyl chloride [100-44-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Bromodichloromethane [75-27-4]1 0.43 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Bromoethene [593-60-2]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Bromoform [75-25-2]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Bromomethane [74-83-9]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Carbon disulfide [75-15-0]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Carbon tetrachloride [56-23-5]1 0.60 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Chlorobenzene [108-90-7]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Chloroethane [75-00-3]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Chloroform [67-66-3]1 0.65 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Chloromethane [74-87-3]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29cis-1,2-Dichloroethene [156-59-2]1 0.64 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29cis-1,3-Dichloropropene [10061-01-5]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Cyclohexane [110-82-7]1 0.92 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Dibromochloromethane [124-48-1]1 0.32 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Dichlorodifluoromethane [75-71-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Ethyl Acetate [141-78-6]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Ethylbenzene [100-41-4]1 0.49 GMB2E150092.52.0 J
ppbv TO-15 05/15/12 13:29Freon 113 [76-13-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Freon 114 [76-14-2]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Heptane [142-82-5]1 0.98 GMB2E150092.51.3 J
ppbv TO-15 05/15/12 13:29Hexachlorobutadiene [87-68-3]1 0.96 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Methylene chloride [75-09-2]1 0.78 GMB2E150092.51.6 JB J-01
Page 5 of 23
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JS-089Description:Lab Sample ID:C205450-01 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 13:29Methyl-tert-butyl ether [1634-04-4]1 0.54 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29n-Hexane [110-54-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Propene [115-07-1]1 1.6 GMB2E150092.55.5
ppbv TO-15 05/15/12 13:29Styrene [100-42-5]1 0.63 GMB2E150092.51.5 J
ppbv TO-15 05/15/12 13:29Tetrachloroethene [127-18-4]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Tetrahydrofuran [109-99-9]1 0.84 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Toluene [108-88-3]1 0.45 GMB2E150092.54.1
ppbv TO-15 05/15/12 13:29Total Light Petroleum Hydrocarbons
[ECL-0163]
1 240 GMB2E15009240ND
ppbv TO-15 05/15/12 13:29trans-1,2-Dichloroethene [156-60-5]1 0.93 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29trans-1,3-Dichloropropene [10061-02-6]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Trichloroethene [79-01-6]1 0.52 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Trichlorofluoromethane [75-69-4]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Vinyl acetate [108-05-4]1 0.78 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Vinyl chloride [75-01-4]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 13:29Xylenes (Total) [1330-20-7]1 1.0 GMB2E150092.55.8
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-12493.8 %GMBTO-15 05/15/12 13:292E150092931.2 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 6 of 23
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JS-055Description:Lab Sample ID:C205450-02 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 15:201,1,1-Trichloroethane [71-55-6]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,1,2,2-Tetrachloroethane [79-34-5]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,1,2-Trichloroethane [79-00-5]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,1-Dichloroethane [75-34-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,1-Dichloroethene [75-35-4]1 0.94 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,2,4-Trichlorobenzene [120-82-1]1 0.67 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,2,4-Trimethylbenzene [95-63-6]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,2-Dibromoethane [106-93-4]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,2-Dichlorobenzene [95-50-1]1 1.8 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,2-Dichloroethane [107-06-2]1 0.51 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,2-Dichloropropane [78-87-5]1 0.47 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,3,5-Trimethylbenzene [108-67-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,3-Butadiene [106-99-0]1 1.5 GMB2E150092.53.3
ppbv TO-15 05/15/12 15:201,3-Dichlorobenzene [541-73-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,4-Dichlorobenzene [106-46-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:201,4-Dioxane [123-91-1]1 0.57 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:202,2,4-Trimethylpentane [540-84-1]1 0.74 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:202-Butanone [78-93-3]1 0.77 GMB2E150092.53.0
ppbv TO-15 05/15/12 15:202-Hexanone [591-78-6]1 0.85 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:202-Propanol [67-63-0]1 0.83 GMB2E150092.53.1
ppbv TO-15 05/15/12 15:203-Chloropropene [107-05-1]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:204-Ethyltoluene [622-96-8]1 0.98 GMB2E150092.524
ppbv TO-15 05/15/12 15:204-Methyl-2-pentanone [108-10-1]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Acetone [67-64-1]1 0.66 GMB2E150092.512
ppbv TO-15 05/15/12 15:20Benzene [71-43-2]1 0.39 GMB2E150092.57.9
ppbv TO-15 05/15/12 15:20Benzyl chloride [100-44-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Bromodichloromethane [75-27-4]1 0.43 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Bromoethene [593-60-2]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Bromoform [75-25-2]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Bromomethane [74-83-9]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Carbon disulfide [75-15-0]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Carbon tetrachloride [56-23-5]1 0.60 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Chlorobenzene [108-90-7]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Chloroethane [75-00-3]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Chloroform [67-66-3]1 0.65 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Chloromethane [74-87-3]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20cis-1,2-Dichloroethene [156-59-2]1 0.64 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20cis-1,3-Dichloropropene [10061-01-5]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Cyclohexane [110-82-7]1 0.92 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Dibromochloromethane [124-48-1]1 0.32 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Dichlorodifluoromethane [75-71-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Ethyl Acetate [141-78-6]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Ethylbenzene [100-41-4]1 0.49 GMB2E150092.53.9
ppbv TO-15 05/15/12 15:20Freon 113 [76-13-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Freon 114 [76-14-2]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Heptane [142-82-5]1 0.98 GMB2E150092.51.2 J
ppbv TO-15 05/15/12 15:20Hexachlorobutadiene [87-68-3]1 0.96 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Methylene chloride [75-09-2]1 0.78 GMB2E150092.53.3 B J-01
ppbv TO-15 05/15/12 15:20Methyl-tert-butyl ether [1634-04-4]1 0.54 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20n-Hexane [110-54-3]1 0.82 GMB2E150092.50.98 J
ppbv TO-15 05/15/12 15:20Propene [115-07-1]1 1.6 GMB2E150092.511
Page 7 of 23
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JS-055Description:Lab Sample ID:C205450-02 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 15:20Styrene [100-42-5]1 0.63 GMB2E150092.52.7
ppbv TO-15 05/15/12 15:20Tetrachloroethene [127-18-4]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Tetrahydrofuran [109-99-9]1 0.84 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Toluene [108-88-3]1 0.45 GMB2E150092.57.9
ppbv TO-15 05/15/12 15:20Total Light Petroleum Hydrocarbons
[ECL-0163]
1 240 GMB2E15009240280
ppbv TO-15 05/15/12 15:20trans-1,2-Dichloroethene [156-60-5]1 0.93 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20trans-1,3-Dichloropropene [10061-02-6]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Trichloroethene [79-01-6]1 0.52 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Trichlorofluoromethane [75-69-4]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Vinyl acetate [108-05-4]1 0.78 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Vinyl chloride [75-01-4]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 15:20Xylenes (Total) [1330-20-7]1 1.0 GMB2E150092.512 J
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-12489.7 %GMBTO-15 05/15/12 15:202E150092831.2 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 23
www.encolabs.com
JS-024Description:Lab Sample ID:C205450-03 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 16:341,1,1-Trichloroethane [71-55-6]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,1,2,2-Tetrachloroethane [79-34-5]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,1,2-Trichloroethane [79-00-5]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,1-Dichloroethane [75-34-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,1-Dichloroethene [75-35-4]1 0.94 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,2,4-Trichlorobenzene [120-82-1]1 0.67 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,2,4-Trimethylbenzene [95-63-6]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,2-Dibromoethane [106-93-4]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,2-Dichlorobenzene [95-50-1]1 1.8 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,2-Dichloroethane [107-06-2]1 0.51 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,2-Dichloropropane [78-87-5]1 0.47 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,3,5-Trimethylbenzene [108-67-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,3-Butadiene [106-99-0]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,3-Dichlorobenzene [541-73-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,4-Dichlorobenzene [106-46-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:341,4-Dioxane [123-91-1]1 0.57 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:342,2,4-Trimethylpentane [540-84-1]1 0.74 GMB2E150092.51.2 J
ppbv TO-15 05/15/12 16:342-Butanone [78-93-3]1 0.77 GMB2E150092.51.5 J
ppbv TO-15 05/15/12 16:342-Hexanone [591-78-6]1 0.85 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:342-Propanol [67-63-0]1 0.83 GMB2E150092.51.5 J
ppbv TO-15 05/15/12 16:343-Chloropropene [107-05-1]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:344-Ethyltoluene [622-96-8]1 0.98 GMB2E150092.52.4 J
ppbv TO-15 05/15/12 16:344-Methyl-2-pentanone [108-10-1]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Acetone [67-64-1]1 0.66 GMB2E150092.59.4
ppbv TO-15 05/15/12 16:34Benzene [71-43-2]1 0.39 GMB2E150092.52.2 J
ppbv TO-15 05/15/12 16:34Benzyl chloride [100-44-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Bromodichloromethane [75-27-4]1 0.43 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Bromoethene [593-60-2]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Bromoform [75-25-2]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Bromomethane [74-83-9]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Carbon disulfide [75-15-0]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Carbon tetrachloride [56-23-5]1 0.60 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Chlorobenzene [108-90-7]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Chloroethane [75-00-3]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Chloroform [67-66-3]1 0.65 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Chloromethane [74-87-3]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34cis-1,2-Dichloroethene [156-59-2]1 0.64 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34cis-1,3-Dichloropropene [10061-01-5]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Cyclohexane [110-82-7]1 0.92 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Dibromochloromethane [124-48-1]1 0.32 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Dichlorodifluoromethane [75-71-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Ethyl Acetate [141-78-6]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Ethylbenzene [100-41-4]1 0.49 GMB2E150092.50.50 J
ppbv TO-15 05/15/12 16:34Freon 113 [76-13-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Freon 114 [76-14-2]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Heptane [142-82-5]1 0.98 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Hexachlorobutadiene [87-68-3]1 0.96 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Methylene chloride [75-09-2]1 0.78 GMB2E150092.51.2 JB J-01
ppbv TO-15 05/15/12 16:34Methyl-tert-butyl ether [1634-04-4]1 0.54 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34n-Hexane [110-54-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Propene [115-07-1]1 1.6 GMB2E150092.52.5
Page 9 of 23
www.encolabs.com
JS-024Description:Lab Sample ID:C205450-03 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 16:34Styrene [100-42-5]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Tetrachloroethene [127-18-4]1 0.56 GMB2E150092.50.82 J
ppbv TO-15 05/15/12 16:34Tetrahydrofuran [109-99-9]1 0.84 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Toluene [108-88-3]1 0.45 GMB2E150092.51.3 J
ppbv TO-15 05/15/12 16:34Total Light Petroleum Hydrocarbons
[ECL-0163]
1 240 GMB2E15009240ND
ppbv TO-15 05/15/12 16:34trans-1,2-Dichloroethene [156-60-5]1 0.93 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34trans-1,3-Dichloropropene [10061-02-6]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Trichloroethene [79-01-6]1 0.52 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Trichlorofluoromethane [75-69-4]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Vinyl acetate [108-05-4]1 0.78 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Vinyl chloride [75-01-4]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 16:34Xylenes (Total) [1330-20-7]1 1.0 GMB2E150092.51.4 J
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-12496.5 %GMBTO-15 05/15/12 16:342E150093031.2 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 10 of 23
www.encolabs.com
JS-043Description:Lab Sample ID:C205450-04 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 17:111,1,1-Trichloroethane [71-55-6]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,1,2,2-Tetrachloroethane [79-34-5]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,1,2-Trichloroethane [79-00-5]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,1-Dichloroethane [75-34-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,1-Dichloroethene [75-35-4]1 0.94 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,2,4-Trichlorobenzene [120-82-1]1 0.67 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,2,4-Trimethylbenzene [95-63-6]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,2-Dibromoethane [106-93-4]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,2-Dichlorobenzene [95-50-1]1 1.8 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,2-Dichloroethane [107-06-2]1 0.51 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,2-Dichloropropane [78-87-5]1 0.47 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,3,5-Trimethylbenzene [108-67-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,3-Butadiene [106-99-0]1 1.5 GMB2E150092.51.6 J
ppbv TO-15 05/15/12 17:111,3-Dichlorobenzene [541-73-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,4-Dichlorobenzene [106-46-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:111,4-Dioxane [123-91-1]1 0.57 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:112,2,4-Trimethylpentane [540-84-1]1 0.74 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:112-Butanone [78-93-3]1 0.77 GMB2E150092.51.7 J
ppbv TO-15 05/15/12 17:112-Hexanone [591-78-6]1 0.85 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:112-Propanol [67-63-0]1 0.83 GMB2E150092.52.4 J
ppbv TO-15 05/15/12 17:113-Chloropropene [107-05-1]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:114-Ethyltoluene [622-96-8]1 0.98 GMB2E150092.510
ppbv TO-15 05/15/12 17:114-Methyl-2-pentanone [108-10-1]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Acetone [67-64-1]1 0.66 GMB2E150092.510
ppbv TO-15 05/15/12 17:11Benzene [71-43-2]1 0.39 GMB2E150092.53.9
ppbv TO-15 05/15/12 17:11Benzyl chloride [100-44-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Bromodichloromethane [75-27-4]1 0.43 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Bromoethene [593-60-2]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Bromoform [75-25-2]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Bromomethane [74-83-9]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Carbon disulfide [75-15-0]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Carbon tetrachloride [56-23-5]1 0.60 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Chlorobenzene [108-90-7]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Chloroethane [75-00-3]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Chloroform [67-66-3]1 0.65 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Chloromethane [74-87-3]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11cis-1,2-Dichloroethene [156-59-2]1 0.64 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11cis-1,3-Dichloropropene [10061-01-5]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Cyclohexane [110-82-7]1 0.92 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Dibromochloromethane [124-48-1]1 0.32 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Dichlorodifluoromethane [75-71-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Ethyl Acetate [141-78-6]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Ethylbenzene [100-41-4]1 0.49 GMB2E150092.51.7 J
ppbv TO-15 05/15/12 17:11Freon 113 [76-13-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Freon 114 [76-14-2]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Heptane [142-82-5]1 0.98 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Hexachlorobutadiene [87-68-3]1 0.96 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Methylene chloride [75-09-2]1 0.78 GMB2E150092.53.7 B J-01
ppbv TO-15 05/15/12 17:11Methyl-tert-butyl ether [1634-04-4]1 0.54 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11n-Hexane [110-54-3]1 0.82 GMB2E150092.52.3 J
ppbv TO-15 05/15/12 17:11Propene [115-07-1]1 1.6 GMB2E150092.55.2
Page 11 of 23
www.encolabs.com
JS-043Description:Lab Sample ID:C205450-04 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 17:11Styrene [100-42-5]1 0.63 GMB2E150092.51.1 J
ppbv TO-15 05/15/12 17:11Tetrachloroethene [127-18-4]1 0.56 GMB2E150092.50.87 J
ppbv TO-15 05/15/12 17:11Tetrahydrofuran [109-99-9]1 0.84 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Toluene [108-88-3]1 0.45 GMB2E150092.54.0
ppbv TO-15 05/15/12 17:11Total Light Petroleum Hydrocarbons
[ECL-0163]
1 240 GMB2E15009240ND
ppbv TO-15 05/15/12 17:11trans-1,2-Dichloroethene [156-60-5]1 0.93 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11trans-1,3-Dichloropropene [10061-02-6]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Trichloroethene [79-01-6]1 0.52 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Trichlorofluoromethane [75-69-4]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Vinyl acetate [108-05-4]1 0.78 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Vinyl chloride [75-01-4]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:11Xylenes (Total) [1330-20-7]1 1.0 GMB2E150092.55.0
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-12496.8 %GMBTO-15 05/15/12 17:112E150093031.2 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 12 of 23
www.encolabs.com
JS-039Description:Lab Sample ID:C205450-05 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 17:491,1,1-Trichloroethane [71-55-6]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,1,2,2-Tetrachloroethane [79-34-5]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,1,2-Trichloroethane [79-00-5]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,1-Dichloroethane [75-34-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,1-Dichloroethene [75-35-4]1 0.94 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,2,4-Trichlorobenzene [120-82-1]1 0.67 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,2,4-Trimethylbenzene [95-63-6]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,2-Dibromoethane [106-93-4]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,2-Dichlorobenzene [95-50-1]1 1.8 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,2-Dichloroethane [107-06-2]1 0.51 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,2-Dichloropropane [78-87-5]1 0.47 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,3,5-Trimethylbenzene [108-67-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,3-Butadiene [106-99-0]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,3-Dichlorobenzene [541-73-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,4-Dichlorobenzene [106-46-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:491,4-Dioxane [123-91-1]1 0.57 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:492,2,4-Trimethylpentane [540-84-1]1 0.74 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:492-Butanone [78-93-3]1 0.77 GMB2E150092.51.6 J
ppbv TO-15 05/15/12 17:492-Hexanone [591-78-6]1 0.85 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:492-Propanol [67-63-0]1 0.83 GMB2E150092.51.5 J
ppbv TO-15 05/15/12 17:493-Chloropropene [107-05-1]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:494-Ethyltoluene [622-96-8]1 0.98 GMB2E150092.55.9
ppbv TO-15 05/15/12 17:494-Methyl-2-pentanone [108-10-1]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Acetone [67-64-1]1 0.66 GMB2E150092.510
ppbv TO-15 05/15/12 17:49Benzene [71-43-2]1 0.39 GMB2E150092.52.3 J
ppbv TO-15 05/15/12 17:49Benzyl chloride [100-44-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Bromodichloromethane [75-27-4]1 0.43 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Bromoethene [593-60-2]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Bromoform [75-25-2]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Bromomethane [74-83-9]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Carbon disulfide [75-15-0]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Carbon tetrachloride [56-23-5]1 0.60 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Chlorobenzene [108-90-7]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Chloroethane [75-00-3]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Chloroform [67-66-3]1 0.65 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Chloromethane [74-87-3]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49cis-1,2-Dichloroethene [156-59-2]1 0.64 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49cis-1,3-Dichloropropene [10061-01-5]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Cyclohexane [110-82-7]1 0.92 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Dibromochloromethane [124-48-1]1 0.32 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Dichlorodifluoromethane [75-71-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Ethyl Acetate [141-78-6]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Ethylbenzene [100-41-4]1 0.49 GMB2E150092.51.0 J
ppbv TO-15 05/15/12 17:49Freon 113 [76-13-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Freon 114 [76-14-2]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Heptane [142-82-5]1 0.98 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Hexachlorobutadiene [87-68-3]1 0.96 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Methylene chloride [75-09-2]1 0.78 GMB2E150092.55.7 B J-01
ppbv TO-15 05/15/12 17:49Methyl-tert-butyl ether [1634-04-4]1 0.54 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49n-Hexane [110-54-3]1 0.82 GMB2E150092.51.0 J
ppbv TO-15 05/15/12 17:49Propene [115-07-1]1 1.6 GMB2E150092.53.1
Page 13 of 23
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JS-039Description:Lab Sample ID:C205450-05 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 17:49Styrene [100-42-5]1 0.63 GMB2E150092.50.66 J
ppbv TO-15 05/15/12 17:49Tetrachloroethene [127-18-4]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Tetrahydrofuran [109-99-9]1 0.84 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Toluene [108-88-3]1 0.45 GMB2E150092.52.4 J
ppbv TO-15 05/15/12 17:49Total Light Petroleum Hydrocarbons
[ECL-0163]
1 240 GMB2E15009240ND
ppbv TO-15 05/15/12 17:49trans-1,2-Dichloroethene [156-60-5]1 0.93 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49trans-1,3-Dichloropropene [10061-02-6]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Trichloroethene [79-01-6]1 0.52 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Trichlorofluoromethane [75-69-4]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Vinyl acetate [108-05-4]1 0.78 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Vinyl chloride [75-01-4]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 17:49Xylenes (Total) [1330-20-7]1 1.0 GMB2E150092.53.0 J
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-12498.5 %GMBTO-15 05/15/12 17:492E150093131.2 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 14 of 23
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JS-096Description:Lab Sample ID:C205450-06 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 18:261,1,1-Trichloroethane [71-55-6]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,1,2,2-Tetrachloroethane [79-34-5]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,1,2-Trichloroethane [79-00-5]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,1-Dichloroethane [75-34-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,1-Dichloroethene [75-35-4]1 0.94 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,2,4-Trichlorobenzene [120-82-1]1 0.67 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,2,4-Trimethylbenzene [95-63-6]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,2-Dibromoethane [106-93-4]1 0.41 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,2-Dichlorobenzene [95-50-1]1 1.8 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,2-Dichloroethane [107-06-2]1 0.51 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,2-Dichloropropane [78-87-5]1 0.47 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,3,5-Trimethylbenzene [108-67-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,3-Butadiene [106-99-0]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,3-Dichlorobenzene [541-73-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,4-Dichlorobenzene [106-46-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:261,4-Dioxane [123-91-1]1 0.57 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:262,2,4-Trimethylpentane [540-84-1]1 0.74 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:262-Butanone [78-93-3]1 0.77 GMB2E150092.51.0 J
ppbv TO-15 05/15/12 18:262-Hexanone [591-78-6]1 0.85 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:262-Propanol [67-63-0]1 0.83 GMB2E150092.51.1 J
ppbv TO-15 05/15/12 18:263-Chloropropene [107-05-1]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:264-Ethyltoluene [622-96-8]1 0.98 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:264-Methyl-2-pentanone [108-10-1]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Acetone [67-64-1]1 0.66 GMB2E150092.55.5
ppbv TO-15 05/15/12 18:26Benzene [71-43-2]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Benzyl chloride [100-44-7]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Bromodichloromethane [75-27-4]1 0.43 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Bromoethene [593-60-2]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Bromoform [75-25-2]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Bromomethane [74-83-9]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Carbon disulfide [75-15-0]1 0.66 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Carbon tetrachloride [56-23-5]1 0.60 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Chlorobenzene [108-90-7]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Chloroethane [75-00-3]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Chloroform [67-66-3]1 0.65 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Chloromethane [74-87-3]1 1.5 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26cis-1,2-Dichloroethene [156-59-2]1 0.64 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26cis-1,3-Dichloropropene [10061-01-5]1 0.39 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Cyclohexane [110-82-7]1 0.92 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Dibromochloromethane [124-48-1]1 0.32 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Dichlorodifluoromethane [75-71-8]1 1.3 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Ethyl Acetate [141-78-6]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Ethylbenzene [100-41-4]1 0.49 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Freon 113 [76-13-1]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Freon 114 [76-14-2]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Heptane [142-82-5]1 0.98 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Hexachlorobutadiene [87-68-3]1 0.96 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Methylene chloride [75-09-2]1 0.78 GMB2E150092.52.3 JB J-01
ppbv TO-15 05/15/12 18:26Methyl-tert-butyl ether [1634-04-4]1 0.54 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26n-Hexane [110-54-3]1 0.82 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Propene [115-07-1]1 1.6 GMB2E150092.5ND
Page 15 of 23
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JS-096Description:Lab Sample ID:C205450-06 05/11/12 10:15Received:
Matrix:Air Sampled:05/10/12 17:15 Work Order:C205450
Carolina MedicalProject:Sampled By:Jimmy Hair % Solids:
Volatile Organic Compounds by GCMS
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByBatchMRLFlag Notes
ppbv TO-15 05/15/12 18:26Styrene [100-42-5]1 0.63 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Tetrachloroethene [127-18-4]1 0.56 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Tetrahydrofuran [109-99-9]1 0.84 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Toluene [108-88-3]1 0.45 GMB2E150092.50.74 J
ppbv TO-15 05/15/12 18:26Total Light Petroleum Hydrocarbons
[ECL-0163]
1 240 GMB2E15009240ND
ppbv TO-15 05/15/12 18:26trans-1,2-Dichloroethene [156-60-5]1 0.93 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26trans-1,3-Dichloropropene [10061-02-6]1 0.46 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Trichloroethene [79-01-6]1 0.52 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Trichlorofluoromethane [75-69-4]1 1.1 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Vinyl acetate [108-05-4]1 0.78 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Vinyl chloride [75-01-4]1 1.4 GMB2E150092.5ND
ppbv TO-15 05/15/12 18:26Xylenes (Total) [1330-20-7]1 1.0 GMB2E150092.5ND
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-124101 %GMBTO-15 05/15/12 18:262E150093131.2 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 16 of 23
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 2E12001 - Same
Prepared: 05/12/2012 15:04 Analyzed: 05/12/2012 15:17Blank (2E12001-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.50.66 U 1,1,1-Trichloroethane
ppbv2.51.1 U 1,1,2,2-Tetrachloroethane
ppbv2.50.41 U 1,1,2-Trichloroethane
ppbv2.50.82 U 1,1-Dichloroethane
ppbv2.50.94 U 1,1-Dichloroethene
ppbv2.50.68 J 1,2,4-Trichlorobenzene
ppbv2.51.5 U 1,2,4-Trimethylbenzene
ppbv2.50.41 U 1,2-Dibromoethane
ppbv2.51.8 U 1,2-Dichlorobenzene
ppbv2.50.51 U 1,2-Dichloroethane
ppbv2.50.47 U 1,2-Dichloropropane
ppbv2.51.3 U 1,3,5-Trimethylbenzene
ppbv2.51.5 U 1,3-Butadiene
ppbv2.51.4 U 1,3-Dichlorobenzene
ppbv2.51.4 U 1,4-Dichlorobenzene
ppbv2.50.57 U 1,4-Dioxane
ppbv2.50.74 U 2,2,4-Trimethylpentane
ppbv2.50.77 U 2-Butanone
ppbv2.50.85 U 2-Hexanone
ppbv2.50.83 U 2-Propanol
ppbv2.51.1 U 3-Chloropropene
ppbv2.50.98 U 4-Ethyltoluene
ppbv2.50.63 U 4-Methyl-2-pentanone
ppbv2.50.66 U Acetone
ppbv2.50.39 U Benzene
ppbv2.51.4 U Benzyl chloride
ppbv2.50.43 U Bromodichloromethane
ppbv2.51.3 U Bromoethene
ppbv2.50.56 U Bromoform
ppbv2.51.1 U Bromomethane
ppbv2.50.66 U Carbon disulfide
ppbv2.50.60 U Carbon tetrachloride
ppbv2.50.46 U Chlorobenzene
ppbv2.51.3 U Chloroethane
ppbv2.50.65 U Chloroform
ppbv2.51.5 U Chloromethane
ppbv2.50.64 U cis-1,2-Dichloroethene
ppbv2.50.39 U cis-1,3-Dichloropropene
ppbv2.50.92 U Cyclohexane
ppbv2.50.32 U Dibromochloromethane
ppbv2.51.3 U Dichlorodifluoromethane
ppbv2.50.82 U Ethyl Acetate
ppbv2.50.49 U Ethylbenzene
ppbv2.51.4 U Freon 113
ppbv2.51.1 U Freon 114
ppbv2.50.98 U Heptane
ppbv2.50.96 U Hexachlorobutadiene
ppbv2.50.78 U Methylene chloride
ppbv2.50.54 U Methyl-tert-butyl ether
Page 17 of 23
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 2E12001 - Same
Prepared: 05/12/2012 15:04 Analyzed: 05/12/2012 15:17Blank (2E12001-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.50.82 U n-Hexane
ppbv2.51.6 U Propene
ppbv2.50.63 U Styrene
ppbv2.50.56 U Tetrachloroethene
ppbv2.50.84 U Tetrahydrofuran
ppbv2.50.45 U Toluene
ppbv240240U Total Light Petroleum Hydrocarbons
ppbv2.50.93 U trans-1,2-Dichloroethene
ppbv2.50.46 U trans-1,3-Dichloropropene
ppbv2.50.52 U Trichloroethene
ppbv2.51.1 U Trichlorofluoromethane
ppbv2.50.78 U Vinyl acetate
ppbv2.51.4 U Vinyl chloride
ppbv2.51.0 U Xylenes (Total)
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 93.529
Prepared: 05/12/2012 15:04 Analyzed: 05/12/2012 15:54LCS (2E12001-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.5 10.0 53-17511211 1,1-Dichloroethene
ppbv2.5 10.0 65-13310611 Benzene
ppbv2.5 10.0 56-15812312 Chlorobenzene
ppbv2.5 10.0 55-13810711 Toluene
ppbv2.5 10.0 59-13311612 Trichloroethene
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 86.827
Prepared: 05/12/2012 15:04 Analyzed: 05/12/2012 22:17Matrix Spike (2E12001-MS1)
Source: B202397-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv40 160 53-17512915 U210 1,1-Dichloroethene
ppbv40 160 65-13311234210 Benzene
ppbv40 160 56-1581407.4 U220 Chlorobenzene
ppbv40 160 55-138160250500 QM-07Toluene
ppbv40 160 59-1331338.3 U210 Trichloroethene
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 91.328
Prepared: 05/12/2012 15:04 Analyzed: 05/12/2012 22:53Matrix Spike Dup (2E12001-MSD1)
Source: B202397-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv40 160 4353-175124 4.1215 U200 1,1-Dichloroethene
ppbv40 160 3565-133118 4.8534220 Benzene
ppbv40 160 2056-158157 11.77.4 U250 Chlorobenzene
ppbv40 160 2555-138202 12.3250570 QM-07Toluene
ppbv40 160 1459-133146 9.248.3 U230 QM-07Trichloroethene
Page 18 of 23
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 2E12001 - Same
Prepared: 05/12/2012 15:04 Analyzed: 05/12/2012 22:53Matrix Spike Dup (2E12001-MSD1) Continued
Source: B202397-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 91.829
Batch 2E15009 - Same
Prepared: 05/15/2012 11:00 Analyzed: 05/15/2012 12:15Blank (2E15009-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.50.66 U 1,1,1-Trichloroethane
ppbv2.51.1 U 1,1,2,2-Tetrachloroethane
ppbv2.50.41 U 1,1,2-Trichloroethane
ppbv2.50.82 U 1,1-Dichloroethane
ppbv2.50.94 U 1,1-Dichloroethene
ppbv2.50.67 U 1,2,4-Trichlorobenzene
ppbv2.51.5 U 1,2,4-Trimethylbenzene
ppbv2.50.41 U 1,2-Dibromoethane
ppbv2.51.8 U 1,2-Dichlorobenzene
ppbv2.50.51 U 1,2-Dichloroethane
ppbv2.50.47 U 1,2-Dichloropropane
ppbv2.51.3 U 1,3,5-Trimethylbenzene
ppbv2.51.5 U 1,3-Butadiene
ppbv2.51.4 U 1,3-Dichlorobenzene
ppbv2.51.4 U 1,4-Dichlorobenzene
ppbv2.50.57 U 1,4-Dioxane
ppbv2.50.74 U 2,2,4-Trimethylpentane
ppbv2.50.77 U 2-Butanone
ppbv2.50.85 U 2-Hexanone
ppbv2.50.83 U 2-Propanol
ppbv2.51.1 U 3-Chloropropene
ppbv2.50.98 U 4-Ethyltoluene
ppbv2.50.63 U 4-Methyl-2-pentanone
ppbv2.50.66 U Acetone
ppbv2.50.39 U Benzene
ppbv2.51.4 U Benzyl chloride
ppbv2.50.43 U Bromodichloromethane
ppbv2.51.3 U Bromoethene
ppbv2.50.56 U Bromoform
ppbv2.51.1 U Bromomethane
ppbv2.50.66 U Carbon disulfide
ppbv2.50.60 U Carbon tetrachloride
ppbv2.50.46 U Chlorobenzene
ppbv2.51.3 U Chloroethane
ppbv2.50.65 U Chloroform
ppbv2.51.5 U Chloromethane
ppbv2.50.64 U cis-1,2-Dichloroethene
ppbv2.50.39 U cis-1,3-Dichloropropene
ppbv2.50.92 U Cyclohexane
ppbv2.50.32 U Dibromochloromethane
Page 19 of 23
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 2E15009 - Same
Prepared: 05/15/2012 11:00 Analyzed: 05/15/2012 12:15Blank (2E15009-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.51.3 U Dichlorodifluoromethane
ppbv2.50.82 U Ethyl Acetate
ppbv2.50.49 U Ethylbenzene
ppbv2.51.4 U Freon 113
ppbv2.51.1 U Freon 114
ppbv2.50.98 U Heptane
ppbv2.50.96 U Hexachlorobutadiene
ppbv2.50.81 J O-01Methylene chloride
ppbv2.50.54 U Methyl-tert-butyl ether
ppbv2.50.82 U n-Hexane
ppbv2.51.6 U Propene
ppbv2.50.63 U Styrene
ppbv2.50.56 U Tetrachloroethene
ppbv2.50.84 U Tetrahydrofuran
ppbv2.50.45 U Toluene
ppbv240240U Total Light Petroleum Hydrocarbons
ppbv2.50.93 U trans-1,2-Dichloroethene
ppbv2.50.46 U trans-1,3-Dichloropropene
ppbv2.50.52 U Trichloroethene
ppbv2.51.1 U Trichlorofluoromethane
ppbv2.50.78 U Vinyl acetate
ppbv2.51.4 U Vinyl chloride
ppbv2.51.0 U Xylenes (Total)
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 10132
Prepared: 05/15/2012 11:00 Analyzed: 05/15/2012 12:51LCS (2E15009-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.5 10.0 53-17511211 1,1-Dichloroethene
ppbv2.5 10.0 65-13310210 Benzene
ppbv2.5 10.0 56-15893.39.3 Chlorobenzene
ppbv2.5 10.0 55-13882.58.2 Toluene
ppbv2.5 10.0 59-13373.27.3 Trichloroethene
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 91.729
Prepared: 05/15/2012 11:00 Analyzed: 05/15/2012 19:07Matrix Spike (2E15009-MS1)
Source: C205450-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.5 10.0 53-1751250.94 U13 1,1-Dichloroethene
ppbv2.5 10.0 65-1331204.416 Benzene
ppbv2.5 10.0 56-15892.90.46 U9.3 Chlorobenzene
ppbv2.5 10.0 55-13897.44.114 Toluene
ppbv2.5 10.0 59-13367.20.52 U6.7 Trichloroethene
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 99.931
Prepared: 05/15/2012 11:00 Analyzed: 05/15/2012 19:47Matrix Spike Dup (2E15009-MSD1)
Page 20 of 23
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 2E15009 - Same
Prepared: 05/15/2012 11:00 Analyzed: 05/15/2012 19:47Matrix Spike Dup (2E15009-MSD1) Continued
Source: C205450-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ppbv2.5 10.0 4353-175122 2.830.94 U12 1,1-Dichloroethene
ppbv2.5 10.0 3565-133109 6.574.415 Benzene
ppbv2.5 10.0 2056-15892.4 0.5400.46 U9.2 Chlorobenzene
ppbv2.5 10.0 2555-13893.4 2.924.113 Toluene
ppbv2.5 10.0 1459-13373.8 9.360.52 U7.4 Trichloroethene
ppbv 31.2 64-124Surrogate: 4-Bromofluorobenzene 96.130
Page 21 of 23
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
ND The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
Result is estimated due to positive results in the associated method blank.J-01
This compound is a common laboratory contaminant.O-01
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
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