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HomeMy WebLinkAbout5504_LakeNormanCDLF_Fall2016GW_DIN27442_20161122  10 Quiet Brook Court 314-496-4654 St. Charles, MO 63303 www.jettenviro.com January 24, 2017 Submitted via Electronic Mail Ms. Jackie Drummond North Carolina Department of Environmental Quality Division of Waste Management - Solid Waste Section Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778 Dear Ms. Drummond: Re: Submittal of Groundwater and Surface Water Monitoring Results Second Semi-Annual 2016 Event Lake Norman Construction & Demolition Landfill North Carolina, Permit # 55-04 On behalf of BFI Lake Norman Landfill, Inc., Jett Environmental Consulting is providing a water quality summary for the Second Semi-Annual 2016 sampling event for the Lake Norman Construction & Demolition Landfill. Groundwater and surface water sampling was performed by Pace Analytical Services, Inc. (Pace) and analytical testing was performed by Pace. The groundwater and surface water samples were analyzed for the Detection Monitoring parameters listed in 15A North Carolina Administrative Code (NCAC) 13B .0544(b)(1)(D), which included the constituents listed in Appendix I of 40 CFR Part 258 (15 heavy metals and 47 organics), mercury, chloride, manganese, sulfate, iron, specific conductance, pH, temperature, alkalinity, and total dissolved solids. In accordance with a North Carolina Department of Environmental Quality (NCDEQ) memorandum for C&D landfills dated June 25, 2010, tetrahydrofuran was also monitored for each of the samples collected. Included in Attachment A is a copy of the laboratory analytical report and field information forms. Assessment Monitoring Program A Groundwater Assessment Monitoring Work Plan was compiled in accordance with 15A NCAC 13B .0545, due to confirmed methylene chloride detections at MW-4 above the North Carolina 15A NCAC 2L Water Quality Standard of 5 ug/L during the Second Semi-Annual 2014 event. The Groundwater Monitoring Assessment Work Plan was submitted on March 9, 2015 by Jett Environmental Consulting and approved by NCDEQ in correspondence dated March 16, 2015. Well MW-5 was installed downgradient of MW-4 on March 25, 2015. The sampling activities associated with the Work Plan were completed during the May 2015 event. A summary of the May 2015 event data was provided to NCDEQ in correspondence dated July 27, 2015. No volatile organic compounds (VOCs) have been confirmed detected above NC Solid Waste Section Limits (SWSLs) or NC 2L Standards at MW-5. Per a March 8, 2016 NCDEQ letter, MW-4 was approved for abandonment and replaced with MW-5 in the groundwater monitoring program. The NCDEQ letter requested the site continue in Assessment Monitoring for the time being. Well MW-4 was abandoned on July 25, 2016, as documented in a Well Abandonment Report submitted to NCDEQ on August 12, 2016 by SCS Engineers. Groundwater Flow Rate & Direction The attached Figure 1 provides a potentiometric surface map utilizing water level data from the Second Semi- Annual 2016 event. Groundwater flow direction for the Second Semi-Annual 2016 event was generally to the northwest, consistent with past reports. 2      To calculate the average linear groundwater velocity, the hydraulic gradients were measured from the potentiometric surface map. The groundwater velocities are then calculated from the following equation: v = [ Ki/n ] * 365 where: v = groundwater flow velocity (ft/year) K = hydraulic conductivity (ft/day) i = hydraulic gradient (ft/ft) n = effective porosity (dimensionless) Based on information provided in the “Construction Plan Application” by S&ME, Inc. dated February 20, 1998, hydraulic conductivity measurements average 1.13 ft/day and the effective porosity measurements average 33%. During the Second Semi-Annual 2016 event, the hydraulic gradient from the southeast to northwest portion of the site was estimated at 0.0238 ft/ft. Using the hydraulic conductivity of 1.13 ft/day, the effective porosity of 0.33, and a hydraulic gradient of 0.0238 ft/ft, the calculated groundwater velocity was 0.081 ft/day (30 ft/yr) for the Second Semi-Annual 2016 event. Effectiveness of the Monitoring Systems The groundwater monitoring well network is designed to detect potential effects on groundwater from the facility. The designated upgradient monitoring well, MW-1, is positioned to monitor background groundwater quality for the facility. The remaining three wells (MW-2, MW-3, and MW-5) are positioned in the downgradient position around the base of the landfill footprint. Each of the wells was sampled during the Second Semi-Annual 2016 event. The surface water monitoring network is designed to detect potential effects on surface water from the facility. The designated upgradient point, SW-1, is positioned to monitor background surface water quality for the facility. The designated downgradient point, SW-2, is positioned to monitor surface water quality downgradient from the landfill. Both surface water monitoring points were sampled during the Second Semi-Annual 2016 event. Based on a review of well and surface water locations, groundwater flow directions, flow gradients, flow rates, and sampling availability, the present monitoring program is considered sufficient to monitor groundwater and surface water quality surrounding the facility. Monitoring Summary A summary of the inorganic results and organic detections for the Second Semi-Annual 2016 event is available on Table 1. The following is a brief summary of the monitoring data from the Second Semi-Annual 2016 event: Groundwater  The NC SWSL is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the concentration below which reported analytical results must be qualified as estimated. No VOCs were detected at or above an SWSL during the Second Semi-Annual 2016 event.  Two inorganic constituents were reported above the NC 2L Standards: total iron at MW-2, MW-3, and MW-5; and total manganese at MW-2, MW-3, and MW-5. 3      Total Iron and Manganese at MW-2, MW-3, and MW-5 The Second Semi-Annual 2016 total iron concentrations at MW-2 (452 ug/L), MW-3 (1,620 ug/L), and MW-5 (1,050 ug/L) are consistent with the historical total iron concentrations at MW-2 (72.8 to 968 ug/L), MW-3 (84.2 to 10,500 ug/L), and MW-5 (214 to 4,140 ug/L), respectively. The Second Semi-Annual 2016 total manganese concentrations at MW-2 (74.2 ug/L), MW-3 (435 ug/L), and MW-5 (921 ug/L) are consistent with the historical total manganese concentrations at MW-2 (5.2 to 113 ug/L), MW-3 (17.3 to 989 ug/L), and MW-5 (763 to 1,080 ug/L), respectively. The total iron and total manganese concentrations in groundwater wells MW-2, MW-3, and MW-5 are not a change from historic results and appear to be attributable to naturally occurring conditions at the site and not related to the landfill. Surface Water  No VOCs were detected at or above an SWSL in surface water samples.  One inorganic constituent was reported above the NC 2B Standards: total iron at SW-1. Total Iron at SW-1 SW-1 is located upgradient to the facility. The Second Semi-Annual 2016 concentration of total iron at SW-1 (1,570 ug/L) is consistent with historical total iron concentrations at upgradient surface water point SW-1 (474 to 2,920 ug/L). The total iron concentrations in upgradient surface water point SW-1 appear to be attributable to naturally occurring conditions at the site and not related to the landfill. Assessment Activities Summary In order to delineate the extent of methylene chloride in the vicinity of MW-4, one additional well (MW-5) was installed downgradient of MW-4 in March 2015 (see Figure 1). Delineation well MW-5 allowed collection of groundwater samples in the direction of any potential migration. The only organic compounds that had been confirmed detected above SWSLs at MW-4 were methylene chloride, tetrahydrofuran, and trichlorofluoromethane. Methylene chloride and trichlorofluoromethane are commonly found in landfill gas (LFG). Since new downgradient well MW-5 indicated no confirmed VOCs at or above applicable NC SWSLs or NC 2L Standards (May and November 2015 events), then the extent of VOC impact had been considered defined on the landfill property by MW-5. Per a March 8, 2016 NCDEQ letter, MW- 4 was approved for abandonment and replaced with MW-5 in the groundwater monitoring program. Downgradient well MW-5 continued to indicate no confirmed VOCs at or above applicable NC SWSLs or NC 2L Standards during the two events in 2016. Recommendations Since no VOCs have been detected above an SWSL or 2L Standard at the groundwater monitoring wells or surface water samples for at least the last two years (both semi-annual events in 2015 and 2016) and no inorganic constituent concentrations appear landfill related, the site requests returning to a Detection Monitoring program. The next semi-annual sampling event is tentatively scheduled for May 2017. 4      Should you have any questions or concerns, please contact Mr. Mike Gurley at (704) 262-6019 or Steve Jett at (314) 496-4654. Sincerely, Steve Jett, LG #1825 Owner Jett Environmental Consulting, PLLC (C-517) Attachment: Figure 1 – Potentiometric Surface Map Table 1 – Data Compared to NC Standards, Second Semi-Annual 2016 Event Attachment A - Laboratory Analytical Report & Field Information Forms cc: Mike Gurley, Republic Services, Inc. (PDF via Email) Lake Norman Landfill (1 Hardcopy) Figure Well Gradient Status Top of PVC Casing Elevation (fmsl)1 Depth to Water (ft)2 Groundwater Elevation (fmsl) MW-1 Upgradient 745.77 39.50 706.27 MW-2 Downgradient 680.37 13.30 667.07 MW-3 Downgradient 679.60 13.05 666.55 MW-5 Downgradient 680.24 14.21 666.03 Note 1: Top of PVC Casing Elevations from correspondence dated 5/10/02 by S&ME, Inc. with the exception of MW-5, which was provided by Lawrence Associates on 6/22/15. Note 2: Depth to water measured by Pace Analytical Services, Inc. on 11/22/16. Groundwater Elevation Summary Table Lake Norman Landfill Table Constituent Units MDL SWSL NC 2L Std MW-1 MW-2 MW-3 MW-5 Alkalinity as CaCO3 ug/L 1000 1000 NE 80000 25000 25000 60000 Antimony, Total ug/L 0.85 6 NE J 1.19 <6 <6 <6 Arsenic, Total ug/L 1.64 10 10 <10 <10 <10 <10 Barium, Total ug/L 0.44 100 700 J 77.8 128 J 53.2 J 21.3 Beryllium, Total ug/L 0.08 1 NE <1 <1 <1 <1 Cadmium, Total ug/L 0.07 1 2 <1 <1 <1 <1 Chloride ug/L 1000 1000 250,000 3500 8600 21000 5200 Chromium, Total ug/L 0.94 10 10 <10 <10 J 1.36 <10 Cobalt, Total ug/L 0.52 10 NE <10 J 3.15 J 7.28 J 0.85 Copper, Total ug/L 0.54 10 1,000 J 2.31 J 1.34 J 4.46 J 0.6 Iron, Total ug/L 9.54 40 300 J 11.4 452 1620 1050 Lead, Total ug/L 0.12 10 15 <10 J 0.16 J 0.44 J 0.2 Manganese, Total ug/L 1.02 10 50 J 4.03 74.2 435 921 Mercury, Total ug/L 0.041 0.2 1 <0.2 <0.2 <0.2 J 0.109 Nickel, Total ug/L 0.55 50 100 <50 J 4.25 J 2.48 <50 pH (Field)su NE NE NE 5.62 5.27 5.11 6.02 Selenium, Total ug/L 1 10 20 <10 <10 <10 <10 Silver, Total ug/L 0.48 10 20 <10 <10 <10 <10 Specific Conductance (Field)umhos/cm 1 1 NE 222 233 169 191 Sulfate as SO4 ug/L 5000 5000 250,000 5900 56000 11000 <5000 Temperature (Field)Deg-C NE NE NE 15.3 16.7 16.1 15.1 Thallium, Total ug/L 0.21 5.5 NE <5.5 <5.5 <5.5 <5.5 Total Dissolved Solids (TDS)ug/L 10000 10000 500,000 149000 148000 131000 137000 Turbidity (Field)NTU NE NE NE 0.64 2.99 2.11 6.17 Vanadium, Total ug/L 7.14 25 NE <25 <25 <25 <25 Zinc, Total ug/L 2.1 10 1,000 J B 3.07 J B 2.45 J B 3.45 J B 4.3 Acetone ug/L 4.9 100 6,000 J B 5 J B 5 J B 7.2 J B 5.4 Chloromethane ug/L 0.4 1 3 <1 <1 J 0.5 <1 Toluene ug/L 0.3 1 600 J 0.3 <1 <1 <1 Trichlorofluoromethane ug/L 0.5 1 2,000 <1 <1 J 0.5 <1 Constituent (ug/L) Units MDL SWSL NC 2B Std SW-1 SW-2 Alkalinity as CaCO3 ug/L 1000 1000 NE 51500 80000 Antimony, Total ug/L 0.85 6 NE <6 <6 Arsenic, Total ug/L 1.64 10 10 <10 <10 Barium, Total ug/L 0.44 100 1,000 J 39.9 101 Beryllium, Total ug/L 0.08 1 6.5 <1 <1 Cadmium, Total ug/L 0.07 1 2 <1 <1 Chloride ug/L 1000 1000 230,000 6000 12000 Chromium, Total ug/L 0.94 10 20 <10 <10 Cobalt, Total ug/L 0.52 10 NE <10 <10 Copper, Total ug/L 0.54 10 3 J 0.55 J 1.32 Dissolved Oxygen (Field)ug/L NE NE NE 3950 3760 Iron, Total ug/L 9.54 40 1,000 1570 541 Lead, Total ug/L 0.12 10 25 J 0.15 J 0.34 Manganese, Total ug/L 1.02 10 200 180 139 Mercury, Total ug/L 0.041 0.2 0.012 <0.2 <0.2 Nickel, Total ug/L 0.55 50 8.3 <50 <50 pH (Field)su NE NE NE 5.42 5.72 Selenium, Total ug/L 1 10 5 J B 1.27 <10 Silver, Total ug/L 0.48 10 0.06 <10 <10 Specific Conductance (Field)umhos/cm 1 1 NE 135 256 Sulfate as SO4 ug/L 5000 5000 NE <5000 11000 Temperature (Field)Deg-C NE NE NE 5.46 6.12 Thallium, Total ug/L 0.21 5.5 NE <5.5 <5.5 Total Dissolved Solids (TDS)ug/L 10000 10000 NE 108000 173000 Turbidity (Field)NTU NE NE NE 3.08 7.73 Vanadium, Total ug/L 7.14 25 NE <25 <25 Zinc, Total ug/L 2.1 10 50 J B 9.45 B 14.8Acetoneug/L 4.9 100 2,000 J B 6.6 J B 5 NE: Denotes a NC 2L or 2B Standard is not established. Only the VOCs detected during this event are displayed on the table. J: Denotes Sample result above the MDL but below the SWSL; estimated value; value may not be accurate. B: Denotes parameter also detected in a field blank, equipment blank, trip blank, and or laboratory method blank at similar level. Denotes result above an SWSL is also above the NC 2L or 2B Standard: For NC 2B Standard, lowest value utilized from the classifications from the 2B Table published May 15, 2013. TABLE 1 SECOND SEMI-ANNUAL 2016 EVENT DATA COMPARED TO NC STANDARDS LAKE NORMAN C&D LANDFILL GROUNDWATER SAMPLES SURFACE WATER SAMPLES Attachment A Laboratory Analytical Report & Field Information Forms P AC E AN A L YT I C A L S E R VI C E S , L L C . En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C Pr o j e c t : L a k e N o r m a n C & D L a n d f i l l Co n c o r d , N C 2 8 0 2 7 51 0 5 M o r e h e a d R d . M r . M i k e G u r l e y W e a p p r e c i a t e t h e o p p o r t u n i t y t o p r o v i d e t h e a n a l y t i c a l s u p p o r t f o r y o u r p r o j e c t . T h e a n a l y t i c a l r e s u l t s i n t h i s r e p o r t a r e b a s e d u p o n i n f o r m a t i o n s u p p l i e d b y y o u , t h e cl i e n t , a n d a r e f o r y o u r e x c l u s i v e u s e . I f y o u h a v e a n y q u e s t i o n s r e g a r d i n g t h i s d a t a p a c k a g e , p l e a s e d o n o t h e s i t a t e t o c a l l . Pa c e An a l y t i c a l S e r v i c e s , LLC. certifies that th e f o l l o w i n g a n a l y t i c a l r e s u l t s m e e t a l l r e q u i r e m e n t s o f t h e N a t i o n a l E n v i r o n m e n t a l L a b o r a t o r y Ac c r e d i t a t i o n C o n f e r e n c e (N E L A C ) . A l l t e s t r e s u l t s r e l a t e o n l y t o t h e sa m p l e s a n a l y z e d . La b o r a t o r y R e p o r t Pr o j e c t # : [ n o n e ] Pr e p a r e d F o r : At t e n t i o n : De c e m b e r 1 2 , 2 0 1 6 Re p o r t N u m b e r : AZ K 0 7 6 4 Ap p r o v e d : Th i s r e p o r t m a y n o t b e r e p r o d u c e d , e x c e p t i n f u l l , wi t h o u t w r i t t e n a p p r o v a l f r o m P a c e An a l y t i c a l S e r v i c e s , L L C . Page 1 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Sa m p l e I D La b o r a t o r y I D Ma t r i x Da t e S a m p l e d AN A L YT I C A L R E P O R T F O R S A M P L E S Date Received 55 0 4 - M W 1 AZ K 0 7 6 4 - 0 1 1 1/ 2 2 / 1 6 1 7 : 1 8 1 1/23/16 1 1:25 Gr o u n d W at e r 55 0 4 - M W 2 AZ K 0 7 6 4 - 0 2 1 1/ 2 2 / 1 6 1 6 : 3 5 1 1/23/16 1 1:25 Gr o u n d W at e r 55 0 4 - M W 3 AZ K 0 7 6 4 - 0 3 1 1/ 2 2 / 1 6 1 6 : 0 3 1 1/23/16 1 1:25 Gr o u n d W at e r 55 0 4 - M W 5 AZ K 0 7 6 4 - 0 4 1 1/ 2 2 / 1 6 1 5 : 2 4 1 1/23/16 1 1:25 Gr o u n d W at e r 55 0 4 - D u p l i c a t e AZ K 0 7 6 4 - 0 5 1 1/ 2 2 / 1 6 0 0 : 0 0 1 1/23/16 1 1:25 Gr o u n d W at e r 55 0 4 - E q u i p m e n t B l a n k AZ K 0 7 6 4 - 0 6 1 1/ 2 3 / 1 6 1 1: 0 0 1 1/23/16 1 1:25 W at e r 55 0 4 - F i e l d B l a n k AZ K 0 7 6 4 - 0 7 1 1/ 2 2 / 1 6 1 6 : 0 8 1 1/23/16 1 1:25 W at e r 55 0 4 - T rip B l a n k AZ K 0 7 6 4 - 0 8 1 1/ 2 2 / 1 6 0 0 : 0 0 1 1/23/16 1 1:25 W at e r 55 0 4 - S W 1 AZ K 0 7 6 4 - 0 9 1 1/ 2 2 / 1 6 1 3 : 2 4 1 1/23/16 1 1:25 Su r f a c e W at e r 55 0 4 - S W 2 AZ K 0 7 6 4 - 1 0 1 1/ 2 2 / 1 6 1 6 : 5 0 1 1/23/16 1 1:25 Su r f a c e W at e r Page 2 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 1 Gr o u n d W at e r AZ K 0 7 6 4 - 0 1 AZK0764 1 1/ 2 2 / 1 6 1 7 : 1 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 On S i t e EP A 9 0 5 0 A 22 2 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10687 NA 1 CO N D 1 1/22/16 17:18 1 1/ 2 2 / 1 6 1 7 : 1 8 EP A 9 0 4 0 C 5. 6 2 pH U n i t s 1 Fi e l d - p H 61 10687 NA PH 1 1/22/16 17:18 1 1/ 2 2 / 1 6 1 7 : 1 8 SM 2 5 5 0 B 15 . 3 °C 1 Fi e l d - T em p e r a t u r e 61 10687 NA TE M P 1 1/22/16 17:18 1 1/ 2 2 / 1 6 1 7 : 1 8 EP A 1 8 0 . 1 0. 6 4 NT U 1 Fi e l d - T ur b i d i t y 61 10687 NA TU R B 1 1/22/16 17:18 1 1/ 2 2 / 1 6 1 7 : 1 8 NA 39 . 5 0 fe e t 1 Fi e l d - W at e r L e v e l 61 10687 NA WL 1 1/22/16 17:18 1 1/ 2 2 / 1 6 1 7 : 1 8 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 80 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 14 9 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 35 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 05:36 1 1/ 2 8 / 1 6 1 1:00 EP A 9 0 5 6 A 59 0 0 ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 05:36 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l EP A 6 0 2 0 B 1. 1 9 ug / L 1 An t i m o n y 6. 0 0 J 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 77 . 8 ug / L 1 Ba r i u m 10 0 J 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 Page 3 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 1 Gr o u n d W at e r AZ K 0 7 6 4 - 0 1 AZK0764 1 1/ 2 2 / 1 6 1 7 : 1 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 2. 3 1 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 3. 0 7 ug / L 1 Zi n c 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 1 1. 4 ug / L 1 Ir o n 40 . 0 J 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 4. 0 3 ug / L 1 Ma n g a n e s e 10 . 0 J 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 22:18 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:02 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 5. 0 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 4 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 1 Gr o u n d W at e r AZ K 0 7 6 4 - 0 1 AZK0764 1 1/ 2 2 / 1 6 1 7 : 1 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 5 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 1 Gr o u n d W at e r AZ K 0 7 6 4 - 0 1 AZK0764 1 1/ 2 2 / 1 6 1 7 : 1 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 3 ug / L 1 T olu e n e 1. 0 J 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 12 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 98 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 15:39 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 6 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 2 Gr o u n d W at e r AZ K 0 7 6 4 - 0 2 AZK0764 1 1/ 2 2 / 1 6 1 6 : 3 5 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 On S i t e EP A 9 0 5 0 A 23 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10687 NA 1 CO N D 1 1/22/16 16:35 1 1/ 2 2 / 1 6 1 6 : 3 5 EP A 9 0 4 0 C 5. 2 7 pH U n i t s 1 Fi e l d - p H 61 10687 NA PH 1 1/22/16 16:35 1 1/ 2 2 / 1 6 1 6 : 3 5 SM 2 5 5 0 B 16 . 7 °C 1 Fi e l d - T em p e r a t u r e 61 10687 NA TE M P 1 1/22/16 16:35 1 1/ 2 2 / 1 6 1 6 : 3 5 EP A 1 8 0 . 1 2. 9 9 NT U 1 Fi e l d - T ur b i d i t y 61 10687 NA TU R B 1 1/22/16 16:35 1 1/ 2 2 / 1 6 1 6 : 3 5 NA 13 . 3 0 fe e t 1 Fi e l d - W at e r L e v e l 61 10687 NA WL 1 1/22/16 16:35 1 1/ 2 2 / 1 6 1 6 : 3 5 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 25 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 14 8 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 86 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 05:57 1 1/ 2 8 / 1 6 1 1:00 EP A 9 0 5 6 A 56 0 0 0 ug / L 2 Su l f a t e 10 0 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 0 14 8 0 8 - 7 9 - 8 1 1/30/16 01:52 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 12 8 ug / L 1 Ba r i u m 10 0 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 3. 1 5 ug / L 1 Co b a l t 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 Page 7 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 2 Gr o u n d W at e r AZ K 0 7 6 4 - 0 2 AZK0764 1 1/ 2 2 / 1 6 1 6 : 3 5 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 1. 3 4 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 1 6 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 4. 2 5 ug / L 1 Ni c k e l 50 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 2. 4 5 ug / L 1 Zi n c 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 45 2 ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 74 . 2 ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 22:23 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:05 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 5. 0 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 8 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 2 Gr o u n d W at e r AZ K 0 7 6 4 - 0 2 AZK0764 1 1/ 2 2 / 1 6 1 6 : 3 5 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 9 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 2 Gr o u n d W at e r AZ K 0 7 6 4 - 0 2 AZK0764 1 1/ 2 2 / 1 6 1 6 : 3 5 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 12 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 98 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 16:09 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 10 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 3 Gr o u n d W at e r AZ K 0 7 6 4 - 0 3 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 3 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 On S i t e EP A 9 0 5 0 A 16 9 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10687 NA 1 CO N D 1 1/22/16 16:03 1 1/ 2 2 / 1 6 1 6 : 0 3 EP A 9 0 4 0 C 5. 11 pH U n i t s 1 Fi e l d - p H 61 10687 NA PH 1 1/22/16 16:03 1 1/ 2 2 / 1 6 1 6 : 0 3 SM 2 5 5 0 B 16 . 1 °C 1 Fi e l d - T em p e r a t u r e 61 10687 NA TE M P 1 1/22/16 16:03 1 1/ 2 2 / 1 6 1 6 : 0 3 EP A 1 8 0 . 1 2. 11 NT U 1 Fi e l d - T ur b i d i t y 61 10687 NA TU R B 1 1/22/16 16:03 1 1/ 2 2 / 1 6 1 6 : 0 3 NA 13 . 0 5 fe e t 1 Fi e l d - W at e r L e v e l 61 10687 NA WL 1 1/22/16 16:03 1 1/ 2 2 / 1 6 1 6 : 0 3 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 25 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 13 1 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 21 0 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 08:26 1 1/ 2 8 / 1 6 1 1:00 EP A 9 0 5 6 A 11 0 0 0 ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 08:26 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 53 . 2 ug / L 1 Ba r i u m 10 0 J 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 1. 3 6 ug / L 1 Ch r o m i u m 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 7. 2 8 ug / L 1 Co b a l t 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 Page 11 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 3 Gr o u n d W at e r AZ K 0 7 6 4 - 0 3 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 3 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 4. 4 6 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 4 4 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 2. 4 8 ug / L 1 Ni c k e l 50 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 3. 4 5 ug / L 1 Zi n c 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 16 2 0 ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 43 5 ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 22:29 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:07 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 7. 2 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 12 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 3 Gr o u n d W at e r AZ K 0 7 6 4 - 0 3 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 3 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 Ch l o r o m e t h a n e 1. 0 J 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 13 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 3 Gr o u n d W at e r AZ K 0 7 6 4 - 0 3 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 3 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 J 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 15 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 98 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 16:39 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 14 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 5 Gr o u n d W at e r AZ K 0 7 6 4 - 0 4 AZK0764 1 1/ 2 2 / 1 6 1 5 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 On S i t e EP A 9 0 5 0 A 19 1 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10687 NA 1 CO N D 1 1/22/16 15:24 1 1/ 2 2 / 1 6 1 5 : 2 4 EP A 9 0 4 0 C 6. 0 2 pH U n i t s 1 Fi e l d - p H 61 10687 NA PH 1 1/22/16 15:24 1 1/ 2 2 / 1 6 1 5 : 2 4 SM 2 5 5 0 B 15 . 1 °C 1 Fi e l d - T em p e r a t u r e 61 10687 NA TE M P 1 1/22/16 15:24 1 1/ 2 2 / 1 6 1 5 : 2 4 EP A 1 8 0 . 1 6. 1 7 NT U 1 Fi e l d - T ur b i d i t y 61 10687 NA TU R B 1 1/22/16 15:24 1 1/ 2 2 / 1 6 1 5 : 2 4 NA 14 . 2 1 fe e t 1 Fi e l d - W at e r L e v e l 61 10687 NA WL 1 1/22/16 15:24 1 1/ 2 2 / 1 6 1 5 : 2 4 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 60 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 13 7 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 52 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 08:47 1 1/ 2 8 / 1 6 1 1:00 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 08:47 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 21 . 3 ug / L 1 Ba r i u m 10 0 J 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 8 5 ug / L 1 Co b a l t 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 Page 15 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 5 Gr o u n d W at e r AZ K 0 7 6 4 - 0 4 AZK0764 1 1/ 2 2 / 1 6 1 5 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 0. 6 0 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 2 0 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 4. 3 0 ug / L 1 Zi n c 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 10 5 0 ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 92 1 ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 22:35 12 / 0 6 / 1 6 1 5 : 3 7 EP A 7 4 7 0 A 0. 1 0 9 ug / L 1 Me r c u r y 0. 2 0 0 J 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:09 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 5. 4 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 16 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 5 Gr o u n d W at e r AZ K 0 7 6 4 - 0 4 AZK0764 1 1/ 2 2 / 1 6 1 5 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 17 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - M W 5 Gr o u n d W at e r AZ K 0 7 6 4 - 0 4 AZK0764 1 1/ 2 2 / 1 6 1 5 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 18 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 99 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 17:10 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 18 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - D u p l i c a t e Gr o u n d W at e r AZ K 0 7 6 4 - 0 5 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 55 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 14 6 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 52 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 09:08 1 1/ 2 8 / 1 6 1 1:00 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 09:08 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 21 . 5 ug / L 1 Ba r i u m 10 0 J 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 9 4 ug / L 1 Co b a l t 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 6 5 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 2 2 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 Page 19 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - D u p l i c a t e Gr o u n d W at e r AZ K 0 7 6 4 - 0 5 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 4. 5 0 ug / L 1 Zi n c 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 1 16 0 ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 93 0 ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 22:41 12 / 0 6 / 1 6 1 5 : 3 7 EP A 7 4 7 0 A 0. 11 6 ug / L 1 Me r c u r y 0. 2 0 0 J 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:12 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 20 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - D u p l i c a t e Gr o u n d W at e r AZ K 0 7 6 4 - 0 5 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 21 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - D u p l i c a t e Gr o u n d W at e r AZ K 0 7 6 4 - 0 5 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 16 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 98 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 17:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 22 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - E q u i p m e n t B l a n k W at e r AZ K 0 7 6 4 - 0 6 AZK0764 1 1/ 2 3 / 1 6 1 1: 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Ge n e r a l C h e m i s t r y ND SM 2 3 2 0 B ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 15 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s ND EP A 9 0 5 6 A ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 09:30 1 1/ 2 8 / 1 6 1 1:00 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 09:30 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 4 6 ug / L 1 Ba r i u m 10 0 J 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 5. 2 3 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 2 6 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 1. 1 4 ug / L 1 Se l e n i u m 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 Page 23 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - E q u i p m e n t B l a n k W at e r AZ K 0 7 6 4 - 0 6 AZK0764 1 1/ 2 3 / 1 6 1 1: 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 Zi n c 10 . 0 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 33 . 3 ug / L 1 Ir o n 40 . 0 J 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 1. 1 9 ug / L 1 Ma n g a n e s e 10 . 0 J 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 22:58 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:19 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 7. 5 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 24 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - E q u i p m e n t B l a n k W at e r AZ K 0 7 6 4 - 0 6 AZK0764 1 1/ 2 3 / 1 6 1 1: 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 25 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - E q u i p m e n t B l a n k W at e r AZ K 0 7 6 4 - 0 6 AZK0764 1 1/ 2 3 / 1 6 1 1: 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 5 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 14 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 99 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 18:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 26 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - F i e l d B l a n k W at e r AZ K 0 7 6 4 - 0 7 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Ge n e r a l C h e m i s t r y ND SM 2 3 2 0 B ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 23 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s ND EP A 9 0 5 6 A ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 09:51 1 1/ 2 8 / 1 6 1 1:00 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 09:51 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ba r i u m 10 0 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 2. 9 8 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Zi n c 10 . 0 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 Page 27 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - F i e l d B l a n k W at e r AZ K 0 7 6 4 - 0 7 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 23:04 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:21 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 5. 3 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 28 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - F i e l d B l a n k W at e r AZ K 0 7 6 4 - 0 7 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 29 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - F i e l d B l a n k W at e r AZ K 0 7 6 4 - 0 7 AZK0764 1 1/ 2 2 / 1 6 1 6 : 0 8 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 17 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 97 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 18:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 30 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - T ri p B l a n k W at e r AZ K 0 7 6 4 - 0 8 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 31 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - T ri p B l a n k W at e r AZ K 0 7 6 4 - 0 8 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 32 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - T ri p B l a n k W at e r AZ K 0 7 6 4 - 0 8 AZK0764 1 1/ 2 2 / 1 6 0 0 : 0 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 15 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 99 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 3 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 19:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 33 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 1 Su r f a c e W at e r AZ K 0 7 6 4 - 0 9 AZK0764 1 1/ 2 2 / 1 6 1 3 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 On S i t e EP A 9 0 5 0 A 13 5 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10687 NA 1 CO N D 1 1/22/16 13:24 1 1/ 2 2 / 1 6 1 3 : 2 4 SM 4 5 0 0 - O G 39 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10687 NA 0. 0 NA 1 1/22/16 13:24 1 1/ 2 2 / 1 6 1 3 : 2 4 EP A 9 0 4 0 C 5. 4 2 pH U n i t s 1 Fi e l d - p H 61 10687 NA PH 1 1/22/16 13:24 1 1/ 2 2 / 1 6 1 3 : 2 4 SM 2 5 5 0 B 5. 4 6 °C 1 Fi e l d - T em p e r a t u r e 61 10687 NA TE M P 1 1/22/16 13:24 1 1/ 2 2 / 1 6 1 3 : 2 4 EP A 1 8 0 . 1 3. 0 8 NT U 1 Fi e l d - T ur b i d i t y 61 10687 NA TU R B 1 1/22/16 13:24 1 1/ 2 2 / 1 6 1 3 : 2 4 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 51 5 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 10 8 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 60 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 10:33 1 1/ 2 8 / 1 6 1 1:00 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 10:33 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 39 . 9 ug / L 1 Ba r i u m 10 0 J 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 Page 34 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 1 Su r f a c e W at e r AZ K 0 7 6 4 - 0 9 AZK0764 1 1/ 2 2 / 1 6 1 3 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 0. 5 5 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 1 5 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 1. 2 7 ug / L 1 Se l e n i u m 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 9. 4 5 ug / L 1 Zi n c 10 . 0 B- 0 1 , J 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 15 7 0 ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 18 0 ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 23:09 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:23 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 6. 6 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 35 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 1 Su r f a c e W at e r AZ K 0 7 6 4 - 0 9 AZK0764 1 1/ 2 2 / 1 6 1 3 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 36 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 1 Su r f a c e W at e r AZ K 0 7 6 4 - 0 9 AZK0764 1 1/ 2 2 / 1 6 1 3 : 2 4 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 3 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 15 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 99 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 4 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 19:41 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 37 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 2 Su r f a c e W at e r AZ K 0 7 6 4 - 1 0 AZK0764 1 1/ 2 2 / 1 6 1 6 : 5 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 On S i t e EP A 9 0 5 0 A 25 6 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10687 NA 1 CO N D 1 1/22/16 16:50 1 1/ 2 2 / 1 6 1 6 : 5 0 SM 4 5 0 0 - O G 37 6 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10687 NA 0. 0 NA 1 1/22/16 16:50 1 1/ 2 2 / 1 6 1 6 : 5 0 EP A 9 0 4 0 C 5. 7 2 pH U n i t s 1 Fi e l d - p H 61 10687 NA PH 1 1/22/16 16:50 1 1/ 2 2 / 1 6 1 6 : 5 0 SM 2 5 5 0 B 6. 1 2 °C 1 Fi e l d - T em p e r a t u r e 61 10687 NA TE M P 1 1/22/16 16:50 1 1/ 2 2 / 1 6 1 6 : 5 0 EP A 1 8 0 . 1 7. 7 3 NT U 1 Fi e l d - T ur b i d i t y 61 10687 NA TU R B 1 1/22/16 16:50 1 1/ 2 2 / 1 6 1 6 : 5 0 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 80 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 6120032 SM 2 3 2 0 B 10 0 0 AL K 12/01/16 15:15 12 / 0 1 / 1 6 1 5 : 1 5 SM 2 5 4 0 C 17 3 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10641 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/28/16 14:53 1 1/ 2 8 / 1 6 1 4 : 5 3 In o r g a n i c An i o n s EP A 9 0 5 6 A 12 0 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10656 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/29/16 10:54 1 1/ 2 8 / 1 6 1 1:00 EP A 9 0 5 6 A 11 0 0 0 ug / L 1 Su l f a t e 50 0 0 61 10656 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/29/16 10:54 1 1/ 2 8 / 1 6 1 1:00 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 6120131 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 6120131 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 10 1 ug / L 1 Ba r i u m 10 0 6120131 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 6120131 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 6120131 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 6120131 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 Page 38 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 2 Su r f a c e W at e r AZ K 0 7 6 4 - 1 0 AZK0764 1 1/ 2 2 / 1 6 1 6 : 5 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 Me t a l s , T ot a l EP A 6 0 2 0 B 1. 3 2 ug / L 1 Co p p e r 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 0. 3 4 ug / L 1 Le a d 10 . 0 J 6120131 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 6120131 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 6120131 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 6120131 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 6120131 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 14 . 8 ug / L 1 Zi n c 10 . 0 B- 0 1 6120131 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 54 1 ug / L 1 Ir o n 40 . 0 6120131 EP A 3 0 0 5 A 9. 5 4 74 3 9 - 8 9 - 6 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 EP A 6 0 2 0 B 13 9 ug / L 1 Ma n g a n e s e 10 . 0 6120131 EP A 3 0 0 5 A 1. 0 2 74 3 9 - 9 6 - 5 12/07/16 23:15 12 / 0 6 / 1 6 1 5 : 3 7 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10661 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 12/02/16 14:26 12 / 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 5. 0 ug / L 1 Ac e t o n e 10 0 J 6120077 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 6120077 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 6120077 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 39 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 2 Su r f a c e W at e r AZ K 0 7 6 4 - 1 0 AZK0764 1 1/ 2 2 / 1 6 1 6 : 5 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 6120077 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 6120077 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 2 - 8 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 6120077 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 6120077 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 6120077 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 6120077 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 Page 40 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 55 0 4 - S W 2 Su r f a c e W at e r AZ K 0 7 6 4 - 1 0 AZK0764 1 1/ 2 2 / 1 6 1 6 : 5 0 Pr o j e c t : La k e N o r m a n C & D L a n d f i l l 1 1/ 2 3 / 1 6 1 1: 2 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 6120077 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 50 6120077 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 6120077 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 6120077 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 6120077 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 6120077 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 4. 0 6120077 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 6120077 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 4 % Su r r : D i b r o m o f l u o r o m e t h a n e 6120077 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 1 15 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 6120077 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 98 % Su r r : T ol u e n e - d 8 6120077 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 6120077 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/28/16 20:11 1 1/ 2 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 41 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 6 4 1 - S M 2 5 4 0 C Bl a n k ( 6 1 10 6 4 1 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 T ot a l D i s s o l v e d S o l i d s ug / L ND 10 0 0 0 LC S ( 6 1 10 6 4 1 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 T ot a l D i s s o l v e d S o l i d s ug / L 39 7 0 0 0 10 0 0 0 40 0 0 0 0 84 - 1 0 8 99 Du p l i c a t e ( 6 1 10 6 4 1 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 So u r ce : AZ K 0 7 6 4 - 1 0 T ot a l D i s s o l v e d S o l i d s ug / L 17 8 0 0 0 10 0 0 0 17 3 0 0 0 10 3 Ba t c h 6 1 2 0 0 3 2 - S M 2 3 2 0 B Bl a n k ( 6 1 2 0 0 3 2 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 1 / 1 6 Al k a l i n i t y a s C a C O 3 ug / L ND 10 0 0 LC S ( 6 1 2 0 0 3 2 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 1 / 1 6 Al k a l i n i t y a s C a C O 3 ug / L 10 1 0 0 0 10 0 0 10 0 0 0 0 85 - 11 5 10 1 Du p l i c a t e ( 6 1 2 0 0 3 2 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 1 / 1 6 So u r ce : AZ K 0 6 2 4 - 0 1 Al k a l i n i t y a s C a C O 3 ug / L 27 5 0 0 10 0 0 28 0 0 0 10 2 Page 42 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e In o r g a n i c An i o n s - Q u a l i t y C o n t r o l Ba t c h 6 1 10 6 5 6 - E P A 9 0 5 6 A Bl a n k ( 6 1 10 6 5 6 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 Ch l o r i d e ug / L ND 10 0 0 Su l f a t e ug / L ND 50 0 0 LC S ( 6 1 10 6 5 6 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 Ch l o r i d e ug / L 10 5 0 0 10 0 0 10 0 1 0 90 - 11 0 10 5 Su l f a t e ug / L 10 4 0 0 50 0 0 10 0 2 0 90 - 11 0 10 4 Ma t r i x S p i k e ( 6 1 10 6 5 6 - M S 1 ) Pr e p a r e d : 1 1/ 2 8 / 1 6 An a l y z e d : 1 1/29/16 So u r ce : AZ K 0 7 6 4 - 0 2 Ch l o r i d e ug / L 19 4 0 0 10 0 0 10 0 1 0 85 7 0 90 - 11 0 10 9 Su l f a t e ug / L 60 0 0 0 50 0 0 10 0 2 0 56 0 0 0 QM-05 90 - 11 0 39 Ma t r i x S p i k e ( 6 1 10 6 5 6 - M S 2 ) Pr e p a r e d : 1 1/ 2 8 / 1 6 An a l y z e d : 1 1/29/16 So u r ce : AZ K 0 7 6 4 - 0 7 Ch l o r i d e ug / L 10 0 0 0 10 0 0 10 0 1 0 ND 90 - 11 0 10 0 Su l f a t e ug / L 97 8 0 50 0 0 10 0 2 0 ND 90 - 11 0 98 Ma t r i x S p i k e D u p ( 6 1 10 6 5 6 - M S D 1 ) Pr e p a r e d : 1 1/ 2 8 / 1 6 An a l y z e d : 1 1/29/16 So u r ce : AZ K 0 7 6 4 - 0 2 Ch l o r i d e ug / L 20 2 0 0 10 0 0 10 0 1 0 85 7 0 15 QM-05 90 - 11 0 11 6 4 Su l f a t e ug / L 60 3 0 0 50 0 0 10 0 2 0 56 0 0 0 15 90 - 11 0 43 0. 6 Page 43 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 6 6 1 - E P A 7 4 7 0 A Bl a n k ( 6 1 10 6 6 1 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 2 / 1 6 Me r c u r y ug / L ND 0. 2 0 0 LC S ( 6 1 10 6 6 1 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 2 / 1 6 Me r c u r y ug / L 2. 4 2 0. 2 0 0 2. 5 0 0 0 80 - 1 2 0 97 Ma t r i x S p i k e ( 6 1 10 6 6 1 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 2 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 1 Me r c u r y ug / L 2. 4 6 0. 2 0 0 2. 5 0 0 0 ND 75 - 1 2 5 98 Ma t r i x S p i k e D u p ( 6 1 10 6 6 1 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 2 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 1 Me r c u r y ug / L 2. 3 8 0. 2 0 0 2. 5 0 0 0 ND 20 75 - 1 2 5 95 3 Po s t S p i k e ( 6 1 10 6 6 1 - P S 1 ) Pr e p a r e d & An a l y z e d : 1 2 / 0 2 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 1 Me r c u r y ug / L 1. 6 8 1. 6 6 6 7 0. 0 1 0 80 - 1 2 0 10 0 Ba t c h 6 1 2 0 1 3 1 - E P A 3 0 0 5 A Bl a n k ( 6 1 2 0 1 3 1 - B L K 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 An t i m o n y ug / L ND 6. 0 0 Ar s e n i c ug / L ND 10 . 0 Ba r i u m ug / L ND 10 0 Be r y l l i u m ug / L ND 1. 0 0 Ca d m i u m ug / L ND 1. 0 0 Ch r o m i u m ug / L ND 10 . 0 Co b a l t ug / L ND 10 . 0 Co p p e r ug / L ND 10 . 0 Ir o n ug / L ND 40 . 0 Le a d ug / L ND 10 . 0 Ma n g a n e s e ug / L ND 10 . 0 Ni c k e l ug / L ND 50 . 0 Page 44 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 1 3 1 - E P A 3 0 0 5 A Bl a n k ( 6 1 2 0 1 3 1 - B L K 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 Se l e n i u m ug / L 1. 0 9 10 . 0 J Si l v e r ug / L ND 10 . 0 Th a l l i u m ug / L ND 5. 5 0 V an a d i u m ug / L ND 25 . 0 Zi n c ug / L 2. 7 9 10 . 0 J LC S ( 6 1 2 0 1 3 1 - B S 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 An t i m o n y ug / L 10 9 6. 0 0 10 0 . 0 0 80 - 1 2 0 10 9 Ar s e n i c ug / L 10 1 10 . 0 10 0 . 0 0 80 - 1 2 0 10 1 Ba r i u m ug / L 10 4 10 0 10 0 . 0 0 80 - 1 2 0 10 4 Be r y l l i u m ug / L 10 4 1. 0 0 10 0 . 0 0 80 - 1 2 0 10 4 Ca d m i u m ug / L 10 7 1. 0 0 10 0 . 0 0 80 - 1 2 0 10 7 Ch r o m i u m ug / L 10 6 10 . 0 10 0 . 0 0 80 - 1 2 0 10 6 Co b a l t ug / L 99 . 5 10 . 0 10 0 . 0 0 80 - 1 2 0 10 0 Co p p e r ug / L 10 1 10 . 0 10 0 . 0 0 80 - 1 2 0 10 1 Ir o n ug / L 10 4 0 40 . 0 10 0 0 . 0 80 - 1 2 0 10 4 Le a d ug / L 10 6 10 . 0 10 0 . 0 0 80 - 1 2 0 10 6 Ma n g a n e s e ug / L 10 7 10 . 0 10 0 . 0 0 80 - 1 2 0 10 7 Ni c k e l ug / L 10 4 50 . 0 10 0 . 0 0 80 - 1 2 0 10 4 Se l e n i u m ug / L 10 2 10 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Si l v e r ug / L 10 8 10 . 0 10 0 . 0 0 80 - 1 2 0 10 8 Th a l l i u m ug / L 10 4 5. 5 0 10 0 . 0 0 80 - 1 2 0 10 4 V an a d i u m ug / L 10 6 25 . 0 10 0 . 0 0 80 - 1 2 0 10 6 Zi n c ug / L 10 5 10 . 0 10 0 . 0 0 80 - 1 2 0 10 5 Ma t r i x S p i k e ( 6 1 2 0 1 3 1 - M S 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 5 An t i m o n y ug / L 11 3 6. 0 0 10 0 . 0 0 ND 75 - 1 2 5 11 3 Ar s e n i c ug / L 10 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 4 Page 45 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 1 3 1 - E P A 3 0 0 5 A Ma t r i x S p i k e ( 6 1 2 0 1 3 1 - M S 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 5 Ba r i u m ug / L 12 8 10 0 10 0 . 0 0 21 . 5 75 - 1 2 5 10 7 Be r y l l i u m ug / L 10 2 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 2 Ca d m i u m ug / L 10 5 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 5 Ch r o m i u m ug / L 10 9 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 9 Co b a l t ug / L 10 5 10 . 0 10 0 . 0 0 0. 9 4 75 - 1 2 5 10 4 Co p p e r ug / L 10 3 10 . 0 10 0 . 0 0 0. 6 5 75 - 1 2 5 10 2 Ir o n ug / L 23 0 0 40 . 0 10 0 0 . 0 1 16 0 75 - 1 2 5 11 4 Le a d ug / L 10 5 10 . 0 10 0 . 0 0 0. 2 2 75 - 1 2 5 10 5 Ma n g a n e s e ug / L 10 5 0 10 . 0 10 0 . 0 0 93 0 75 - 1 2 5 12 5 Ni c k e l ug / L 10 8 50 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 8 Se l e n i u m ug / L 10 3 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 3 Si l v e r ug / L 10 7 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 7 Th a l l i u m ug / L 10 3 5. 5 0 10 0 . 0 0 ND 75 - 1 2 5 10 3 V an a d i u m ug / L 11 5 25 . 0 10 0 . 0 0 ND 75 - 1 2 5 11 5 Zi n c ug / L 10 7 10 . 0 10 0 . 0 0 4. 5 0 75 - 1 2 5 10 3 Ma t r i x S p i k e D u p ( 6 1 2 0 1 3 1 - M S D 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 5 An t i m o n y ug / L 10 9 6. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 9 4 Ar s e n i c ug / L 10 1 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 1 2 Ba r i u m ug / L 12 7 10 0 10 0 . 0 0 21 . 5 20 75 - 1 2 5 10 5 1 Be r y l l i u m ug / L 10 1 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 1 1 Ca d m i u m ug / L 10 6 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 6 0. 1 Ch r o m i u m ug / L 10 8 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 8 1 Co b a l t ug / L 10 2 10 . 0 10 0 . 0 0 0. 9 4 20 75 - 1 2 5 10 1 3 Co p p e r ug / L 10 2 10 . 0 10 0 . 0 0 0. 6 5 20 75 - 1 2 5 10 1 1 Ir o n ug / L 21 6 0 40 . 0 10 0 0 . 0 1 16 0 20 75 - 1 2 5 10 0 6 Le a d ug / L 10 4 10 . 0 10 0 . 0 0 0. 2 2 20 75 - 1 2 5 10 4 0. 9 Ma n g a n e s e ug / L 99 5 10 . 0 10 0 . 0 0 93 0 20 QM-02 75 - 1 2 5 65 6 Page 46 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 1 3 1 - E P A 3 0 0 5 A Ma t r i x S p i k e D u p ( 6 1 2 0 1 3 1 - M S D 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 5 Ni c k e l ug / L 10 5 50 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 5 3 Se l e n i u m ug / L 10 2 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 2 0. 3 Si l v e r ug / L 10 5 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 5 2 Th a l l i u m ug / L 10 4 5. 5 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 4 0. 1 V an a d i u m ug / L 11 3 25 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 11 3 2 Zi n c ug / L 10 7 10 . 0 10 0 . 0 0 4. 5 0 20 75 - 1 2 5 10 2 0. 2 Po s t S p i k e ( 6 1 2 0 1 3 1 - P S 1 ) Pr e p a r e d : 1 2 / 0 6 / 1 6 An a l y z e d : 1 2 / 0 7 / 1 6 So u r ce : AZ K 0 7 6 4 - 0 5 An t i m o n y ug / L 98 . 6 10 0 . 0 0 0. 1 2 80 - 1 2 0 99 Ar s e n i c ug / L 99 . 7 10 0 . 0 0 0. 4 1 80 - 1 2 0 99 Ba r i u m ug / L 12 3 10 0 . 0 0 21 . 5 80 - 1 2 0 10 2 Be r y l l i u m ug / L 10 0 10 0 . 0 0 0. 0 2 80 - 1 2 0 10 0 Ca d m i u m ug / L 10 4 10 0 . 0 0 0. 0 4 80 - 1 2 0 10 4 Ch r o m i u m ug / L 10 8 10 0 . 0 0 0. 3 0 80 - 1 2 0 10 8 Co b a l t ug / L 10 2 10 0 . 0 0 0. 9 4 80 - 1 2 0 10 1 Co p p e r ug / L 10 1 10 0 . 0 0 0. 6 5 80 - 1 2 0 10 0 Ir o n ug / L 21 8 0 10 0 0 . 0 1 16 0 80 - 1 2 0 10 2 Le a d ug / L 10 2 10 0 . 0 0 0. 2 2 80 - 1 2 0 10 2 Ma n g a n e s e ug / L 10 1 0 10 0 . 0 0 93 0 QM-02 80 - 1 2 0 78 Ni c k e l ug / L 10 2 10 0 . 0 0 0. 3 9 80 - 1 2 0 10 2 Se l e n i u m ug / L 96 . 9 10 0 . 0 0 0. 8 6 80 - 1 2 0 96 Si l v e r ug / L 10 3 10 0 . 0 0 0. 0 0 8 80 - 1 2 0 10 3 Th a l l i u m ug / L 10 1 10 0 . 0 0 0. 0 2 80 - 1 2 0 10 1 V an a d i u m ug / L 11 5 10 0 . 0 0 5. 4 3 80 - 1 2 0 11 0 Zi n c ug / L 10 5 10 0 . 0 0 4. 5 0 80 - 1 2 0 10 1 Page 47 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 0 7 7 - E P A 5 0 3 0 B Bl a n k ( 6 1 2 0 0 7 7 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 Ac e t o n e ug / L ND 10 0 Ac r y l o n i t r i l e ug / L ND 20 0 Be n z e n e ug / L ND 1. 0 Br o m o c h l o r o m e t h a n e ug / L ND 3. 0 Br o m o d i c h l o r o m e t h a n e ug / L ND 1. 0 Br o m o f o r m ug / L ND 3. 0 Br o m o m e t h a n e ug / L ND 10 Ca r b o n D i s u l f i d e ug / L ND 10 0 Ca r b o n T et r a c h l o r i d e ug / L ND 1. 0 Ch l o r o b e n z e n e ug / L ND 3. 0 Ch l o r o e t h a n e ug / L ND 10 Ch l o r o f o r m ug / L ND 5. 0 Ch l o r o m e t h a n e ug / L ND 1. 0 Di b r o m o c h l o r o m e t h a n e ug / L ND 1. 0 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e ug / L ND 13 1, 2 - D i b r o m o e t h a n e ug / L ND 1. 0 Di b r o m o m e t h a n e ug / L ND 10 1, 2 - D i c h l o r o b e n z e n e ug / L ND 5. 0 1, 4 - D i c h l o r o b e n z e n e ug / L ND 1. 0 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e ug / L ND 10 0 1, 1 - D i c h l o r o e t h a n e ug / L ND 5. 0 1, 2 - D i c h l o r o e t h a n e ug / L ND 1. 0 1, 1 - D i c h l o r o e t h e n e ug / L ND 5. 0 ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 tr a n s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 1, 2 - D i c h l o r o p r o p a n e ug / L ND 1. 0 ci s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Page 48 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 0 7 7 - E P A 5 0 3 0 B Bl a n k ( 6 1 2 0 0 7 7 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Et h y l b e n z e n e ug / L ND 1. 0 Io d o m e t h a n e ug / L ND 10 Me t h y l B u t y l K e t o n e ( 2 - H e x a n o n e ) ug / L ND 50 Me t h y l e n e C h l o r i d e ug / L ND 1. 0 Me t h y l E t h y l K e t o n e ( 2 - B u t a n o n e ) ug / L ND 10 0 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) ug / L ND 50 St y r e n e ug / L ND 1. 0 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e ug / L ND 5. 0 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e ug / L ND 1. 0 T et r a c h l o r o e t h e n e ug / L ND 1. 0 T olu e n e ug / L ND 1. 0 1, 1 , 1 - T ri c h l o r o e t h a n e ug / L ND 1. 0 1, 1 , 2 - T ri c h l o r o e t h a n e ug / L ND 1. 0 T ri c h l o r o e t h e n e ug / L ND 1. 0 T ri c h l o r o f l u o r o m e t h a n e ug / L ND 1. 0 1, 2 , 3 - T ri c h l o r o p r o p a n e ug / L ND 1. 0 V in y l Ac e t a t e ug / L ND 50 V in y l C h l o r i d e ug / L ND 1. 0 Xy l e n e s , t o t a l ug / L ND 4. 0 T et r a h y d r o f u r a n ug / L ND 10 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 0 50 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 11 1 55 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 99 49 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 10 4 52 LC S ( 6 1 2 0 0 7 7 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 Page 49 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 0 7 7 - E P A 5 0 3 0 B LC S ( 6 1 2 0 0 7 7 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 Be n z e n e ug / L 51 1. 0 50 . 0 0 0 67 - 1 3 4 10 2 Ch l o r o b e n z e n e ug / L 46 3. 0 50 . 0 0 0 69 - 1 2 2 92 1, 1 - D i c h l o r o e t h e n e ug / L 56 5. 0 50 . 0 0 0 58 - 1 4 2 11 3 T olu e n e ug / L 48 1. 0 50 . 0 0 0 68 - 1 2 7 97 T ri c h l o r o e t h e n e ug / L 50 1. 0 50 . 0 0 0 72 - 1 3 2 10 0 T et r a h y d r o f u r a n ug / L 12 0 10 10 0 . 0 0 62 - 1 4 4 11 6 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 11 0 55 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 11 2 56 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 99 49 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 10 1 51 Ma t r i x S p i k e ( 6 1 2 0 0 7 7 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 2 8 / 1 6 So u r ce : AZ K 0 7 6 9 - 0 2 Be n z e n e ug / L 53 1. 0 50 . 0 0 0 ND 67 - 1 3 4 10 5 Ch l o r o b e n z e n e ug / L 47 3. 0 50 . 0 0 0 ND 69 - 1 2 2 93 1, 1 - D i c h l o r o e t h e n e ug / L 55 5. 0 50 . 0 0 0 ND 58 - 1 4 2 11 0 T olu e n e ug / L 50 1. 0 50 . 0 0 0 ND 68 - 1 2 7 99 T ri c h l o r o e t h e n e ug / L 50 1. 0 50 . 0 0 0 ND 72 - 1 3 2 10 0 T et r a h y d r o f u r a n ug / L 12 0 10 10 0 . 0 0 ND 62 - 1 4 4 12 4 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 11 4 57 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 11 4 57 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 10 0 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 98 49 Ma t r i x S p i k e D u p ( 6 1 2 0 0 7 7 - M S D 1 ) Pr e p a r e d : 1 1/ 2 8 / 1 6 An a l y z e d : 1 2 / 0 2 / 1 6 So u r ce : AZ K 0 7 6 9 - 0 2 Be n z e n e ug / L 55 1. 0 50 . 0 0 0 ND 9 67 - 1 3 4 10 9 3 Ch l o r o b e n z e n e ug / L 47 3. 0 50 . 0 0 0 ND 13 69 - 1 2 2 94 0. 6 Page 50 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 2 0 0 7 7 - E P A 5 0 3 0 B Ma t r i x S p i k e D u p ( 6 1 2 0 0 7 7 - M S D 1 ) Pr e p a r e d : 1 1/ 2 8 / 1 6 An a l y z e d : 1 2 / 0 2 / 1 6 So u r ce : AZ K 0 7 6 9 - 0 2 1, 1 - D i c h l o r o e t h e n e ug / L 62 5. 0 50 . 0 0 0 ND 9 QR-02 58 - 1 4 2 12 4 12 T olu e n e ug / L 50 1. 0 50 . 0 0 0 ND 9 68 - 1 2 7 10 1 2 T ri c h l o r o e t h e n e ug / L 53 1. 0 50 . 0 0 0 ND 11 72 - 1 3 2 10 6 6 T et r a h y d r o f u r a n ug / L 11 0 10 10 0 . 0 0 ND 53 62 - 1 4 4 11 3 9 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 9 55 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 4 52 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 95 47 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 96 48 Page 51 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 La b o r a t o r y C e r t i f i c a t i o n s Co d e De s c r i p t i o n Nu m b e r Expires 81 2 Ge o r g i a D W I n o r g a n i c s E f f: 0 7 / 0 1 / 2 0 1 6 06/30/2017 GA D W 81 2 Ge o r g i a D W M i c r o b i o l o g y E f f: 0 7 / 0 1 / 2 0 1 5 12/09/2016 GA D W M 38 1 No r t h C a r o l i n a 12/31/2016 NC E8 7 3 1 5 F L D O H ( N o n - P o t . W at e r , S o l i d s ) E f f: : 0 7 / 0 1 / 2 0 1 6 06/30/2017 NE L A C E8 7 3 1 5 F L D O H N E L A C ( D r i n k i n g W at e r ) E f f: 0 7 / 0 1 / 2 0 1 6 06/30/2017 NE L D W 98 0 11 0 0 1 So u t h C a r o l i n a 06/30/2017 SC T1 0 4 7 0 4 3 9 7 - 0 8 - T X T ex a s 03/31/2017 TX 13 4 0 V ir g i n i a 12/14/2016 VA Page 52 of 54 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , L L C . BF I W as t e S y s t e m s o f N o r t h Am e r i c a , L L C 51 0 5 M o r e h e a d R d . Co n c o r d N C , 2 8 0 2 7 At t e n t i o n : M r . M i k e G u r l e y December 12, 2016 Le g e n d De f i n a t i o n o f L a b o r a t o r y T er m s - N o t D e t e c t e d a t l e v e l s g r e a t e r t h a n o r e q u a l t o S W S L / R L ND SW S L / R L MD L - NC D E N R S o l i d W as t e S e c t i o n L I m i t /R e p o r t i n g L i m i t ( A d j u s t e d f o r D F / P r e p F a c t o r ) - M e t h o d D e t e c t i o n L i m i t Qu a l i f i e r s - D i l u t i o n F a c t o r DF QR - 0 2 Th e R P D r e s u l t e x c e e d e d t h e Q C c o n t r o l l i m i t s ; h o w e v e r , b o t h p e r c e n t r e c o v e r i e s w e r e a c c e p t a b l e . S a m p l e r e s u l t s f o r t h e Q C b a t c h w e r e a c c e p t e d b a s e d o n pe r c e n t r e c o v e r i e s . QM - 0 5 Th e s p i k e r e c o v e r y w a s o u t s i d e a c c e p t a n c e l i m i t s f o r t h e M S a n d / o r M S D a n d / o r P D S d u e t o s u s p e c t e d m a t r i x i n t e r f e r e n c e . S a m p l e r e s u l t s f o r t h e Q C b a t c h we r e a c c e p t e d b a s e d o n a c c e p t a b l e L C S r e c o v e r i e s . QM - 0 2 Th e s p i k e r e c o v e r y i s o u t s i d e a c c e p t a n c e l i m i t s d u e t o i n s i g n i f i c a n t s p i k e a m o u n t a s c o m p a r e d t o s a m p l e c o n c e n t r a t i o n . J Es t i m a t e d v a l u e l e s s t h a n R e p o r t i n g L i m i t ( R L ) b u t g r e a t e r t h a n M e t h o d D e t e c t i o n L i m i t ( M D L ) ( C L P J - F l a g ) . B- 0 1 An a l y t e w a s d e t e c t e d i n t h e a s s o c i a t e d m e t h o d b l a n k a t a n e s t i m a t e d l e v e l e q u a l t o o r g r e a t e r t h a n t h e M D L . Sa m p l e v a l u e s r e p o r t e d a s g r e a t e r t h a n t h e M D L an d l e s s t h a n 1 0 x t h e m e t h o d b l a n k v a l u e a r e r e p o r t e d a s e s t i m a t e d v a l u e s . No t e : U n l e s s o t h e r w i s e n o t e d , a l l r e s u l t s a r e r e p o r t e d o n a n a s r e c e i v e d b a s i s . Page 53 of 54 Page 54 of 54