19040_ATANDO_AVE_PRII 20131101

HRP Associates, Inc.
Creating the Right Solutions Together

H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\WP\GOU4000.GW- Gould Atando Facility P2.docx

November 1, 2013

527 Atando Property
C/o Mr. William Stokesbury, Esq.
Shipman, Stokesbury & Fingold, LLC
20 Batterson Park Road, Suite 120
Farmington, CT 06032

RE: LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT
527 ATANDO AVENUE, CHARLOTTE, NC
HRP#: GOU4000.GW

Dear Mr. Stokesbury:

HRP Associates, Inc. (HRP) has completed a Limited Phase II Environmental Site
Assessment (ESA) at the property located at 527 Atando Avenue, Charlotte, North
Carolina (herein referred to as the Site). A Site location map is included as Figure 1.

Please note that this ESA was performed at your request as a “limited” assessment in
order to further assess the extent of chlorinated solvents in groundwater at the Site
(MW-5, F&R report dated June 2013) and to evaluate whether the source of
contamination exists on-site, or is a result of an unidentified off-site source. Of note,
a 2011 Phase I ESA indicated a former industrial laundry service historically operated
to the northwest of the Site.

This ESA included the advancement of three (3) soil borings at the Site to further
assess the above-noted concern. Each soil boring was converted to a permanent
groundwater monitoring well, for a total of three (3) permanent groundwater
monitoring wells. Permanent groundwater monitoring wells were selected in order
to: 1) provide accurate evaluation of groundwater flow direction at the Site; and, 2) to
provide a means of ongoing monitoring at the Site, which is anticipated.

Task 1: Ground Penetrating Radar Survey

Utility Mark-out and Ground Penetrating Radar Survey

North Carolina 811 (a utility protection service) was contacted to identify public
underground utilities at the Site prior to initiation of the subsurface investigation. In
addition, a ground-penetrating radar (GPR) survey was performed at the Site prior to
drilling activities to protect unidentified subsurface utility lines and other unforeseen
obstructions. Unidentified subsurface objects were not observed in the immediate
vicinity of the well locations during the GPR survey.
CONNECTICUT
Corporate Headquarters 197 Scott Swamp Road Farmington, CT 06032
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860-674-9570
FAX [phone]

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888-341-7244
727-375-2323
FAX [phone] MASSACHUSETTS
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508-407-0009
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NEW YORK
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Suite 110
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888-823-6427 518-877-7101 FAX [phone]
PENNSYLVANIA
313 West Liberty Street Suite 230
Lancaster, PA 17603
888-960-4018
717-945-6084
FAX [phone]
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1327 Miller Road
Suite D Greenville, SC 29607 800-752-3922 864-289-0311 FAX [phone]

TEXAS
P.O. Box 191329
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800-752-3922
FAX [phone]

www.hrpassociates.com
527 Atando Avenue
November 1, 2013
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HRP Associates, Inc. Creating the Right Solutions Together
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Task 2: Limited Soil/Groundwater Investigation

On October 10, 2013, HRP advanced three (3) soil borings to assess site conditions. The location of
each of the borings is summarized in the table below and presented in Figure 2. A Geoprobe
7720DT mobile drill rig was used to advance each soil boring. During advancement of the bore hole,
soil cuttings were screened for volatile organic compounds (VOCs) at one-foot intervals using a
calibrated MiniRae 2000 photo-ionization detector (PID). Detailed soil boring logs are included in
Attachment B. The following table provides a brief description of each boring advanced at the Site.

Soil Boring /
MW ID Location of MW Total Depth
(ft bgs)
Depth to
Groundwater
(ft bgs)
SB-6/MW-6 Northeast Site boundary; south of Site
building 30.0 17.0
SB-7/MW-7 Northeast Site boundary; north of Site
building 29.1 (Refusal) 15.1
SB-8/MW-8 Northwest Site boundary 34.0 10.5
*ft bgs = feet below ground surface

Soil Boring Location (Figure 2) and Description

SB-6 was advanced along the northeastern boundary of the Site and south of the Site building. PID
detections were not identified above background levels (>1.2 ppm) in soils screened throughout the
boring. One soil sample was collected from the depth interval of 14 to 16 feet below ground surface
(bgs) and immediately above the water table. Groundwater was first encountered at a depth of 17.0
feet bgs. The boring was then advanced to a total depth of 30 ft bgs and converted to a permanent
groundwater monitoring well (MW-6).

SB-7 was advanced along the northeastern Site boundary and north of the Site building. The boring was
advanced to a total depth of 29.1 feet bgs before encountering refusal on presumed weathered bedrock.
PID detections above background levels were not identified in soils screened throughout the boring.
One soil sample was collected from the depth interval of 12 to 14 feet bgs. Groundwater was encountered
within this boring at a depth of 15.1 feet bgs. The boring was then advanced to a total depth of 29.1 feet
bgs and converted to a permanent groundwater monitoring well (MW-7).

SB-8 was advanced along the northwest Site boundary. PID detections above background levels were
not identified in soils screened throughout the boring. One (1) soil sample was collected at the depth
interval of 13-15 feet bgs, where HRP personnel observed a green-colored fill-dirt. A second soil
sample was collected at the depth interval of 23-25 feet bgs, where native soils were believed to have
been encountered. Groundwater was first encountered at a depth of 10.5 feet bgs. The boring was then
advanced to a total depth of 34 feet bgs and converted to a permanent groundwater monitoring well (MW-
8).

Soil Investigation

A total of four (4) soil samples were collected from the three (3) borings advanced at the Site. Each soil
sample was collected at the depth interval above the soil/groundwater interface, or where PID readings
were observed above background levels.

527 Atando Avenue
November 1, 2013
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HRP Associates, Inc. Creating the Right Solutions Together
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\WP\GOU4000.GW- Gould Atando Facility P2.docx
Soil Boring ID Total Boring
Depth (ft bgs)
Soil Sample
Collection Depth (ft bgs)
Observed PID Reading
(ppm)
SB -6 30 14-16 1.1
SB -7 29.1 12-14 1.7
SB -8 34 13-15 0.7
SB -8 34 23-25 0.7
* ppm = parts per million

Groundwater Investigation

Permanent groundwater monitoring wells were installed at the three (3) soil boring locations (MW-6,
MW-7, and MW-8). Each monitoring well was constructed of a 2-inch PVC riser with a ten (10) foot
0.010-slot screen interval. A filter-pack, composed of silica sand, was extended two (2) feet above the top
of the screened interval. The filter-pack was followed by two (2) feet of bentonite chips and then tremie
grouted to the ground surface. Each monitoring well was completed at the surface with a flush-mounted
well cover and was set in a 2’ x 2’ concrete pad.

Upon well completion and prior to groundwater sample collection, each monitoring well was developed
using a decontaminated submersible pump and dedicated tubing. Monitoring well development was
considered complete when turbidity was reduced and water quality parameters (i.e., turbidity,
temperature, conductivity and pH) stabilized. Well development logs are included in Attachment C.

Prior to collecting a groundwater sample, each monitoring well was purged using a decontaminated,
disposable bailer. Each well was evacuated by removing a minimum of three (3) well volumes, or until
water quality parameters stabilized. HRP personnel monitored water groundwater pH, temperature,
turbidity, and conductivity at discrete volumes during well purging and immediately prior to sample
collection using portable field instruments. These meters were calibrated daily before use per the
manufacturer’s instructions and in accordance with HRP’s NC DENR laboratory certification
requirements. Water quality data was collected in accordance with the EPA Region IV Science and
Ecosystem Support Division’s (SESD) operating procedures. Groundwater sampling Field Data Sheets
are presented in Attachment D.

Task 3: Certified Land Survey

Following the installation of the three (3) new permanent groundwater monitoring wells, a NC
DENR accredited land surveyor performed a certified land survey measured from the top of the
casings of each monitoring well at the Site (total 8 wells). During the survey MW-1 (located within
the building) was discovered to have been abandoned and covered.

Groundwater Flow Direction

Depth to water was recorded within each well in order to estimate groundwater flow direction at the
Site. Groundwater flow direction was calculated by contouring groundwater elevation data obtained
via a certified land survey. Flow direction is estimated to be perpendicular to the elevation contours,
or equipotential lines.

On October 16, 2013 and prior to well purging, depth to static water level was measured in each
viable Site monitoring well using a decontaminated air/water interface probe and recorded on a
Water Level Log (Attachment D). Measurements were made to the nearest 0.1-foot from the
surveyed top of the casing. Groundwater elevations are presented in Table 1 and groundwater
527 Atando Avenue
November 1, 2013
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HRP Associates, Inc. Creating the Right Solutions Together
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\WP\GOU4000.GW- Gould Atando Facility P2.docx
elevation contours are presented in Figure 3. Site groundwater generally flows south-southeast
towards Little Sugar Creek.

Hydraulic Gradient

The hydraulic gradient was estimated using groundwater elevations measured at seven (7) on-site
wells. The gradient magnitude was calculated using the equation:

i =Δh/ΔL

Where Δh is the change in head measured along the direction of groundwater flow, and ΔL is the
straight-line distance between the measurement locations. A copy of the certified land survey is
included as Attachment E. The calculated hydraulic conductivities and estimated linear velocities
are included in Table 2.

Task 4: Sample Analysis

Soil Samples

Four (4) soil samples were collected from the soil borings advanced at the Site on October 10, 2013. As
previously noted, soil samples were collected from SB-6, SB-7, and SB-8. All soil samples were
submitted for analysis under chain-of-custody to a certified North Carolina laboratory (Accutest
Laboratories) and analyzed for the following constituents:

 Volatile Organic Compounds (VOCs) – EPA Method 8260B

In summary, no constituents were detected in soils above the applicable North Carolina Industrial
Preliminary Soil Remediation Goals (IPSRG). Acetone was detected in the soil sample collected
from SB-6; however, at a concentration significantly below the NC IPSRG.

Analytical results of the soil assessment are summarized in Table 3. Soil concentration results were
compared to the North Carolina Department of Environmental and Natural Resources (NCDENR)
Industrial Preliminary Soil Remediation Goals (IPSRG). Laboratory reports, quality assurance/quality
control (QA/QC) information, and chain-of-custody records are included as Attachment A.

Groundwater Samples

Groundwater samples were collected from the three (3) newly installed monitoring wells. Groundwater
samples were submitted for analysis under chain-of-custody to a North Carolina certified laboratory
(Accutest Laboratories). Groundwater samples collected from the monitoring wells were analyzed for the
following constituents:

 Volatile Organic Compounds (VOCs) – EPA Method 8260B

Groundwater sample results were compared to the North Carolina groundwater standard established by
the Division of Water Quality’s Classifications and Standards Unit. Regulations pertaining to
groundwater quality standards are located in Title 15A of the North Carolina Administrative Code,
Subchapter 2L, Sections .202 (15 NCAC 2L.0202).

527 Atando Avenue
November 1, 2013
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In summary, the constituents detected above the applicable 15A NCAC 2L.0202 Groundwater Standards
included:
 Methyl chloride in MW-6
 Methylene Chloride in MW-8
 Tetrachloroethylene in MW-7 and MW-8
 Trichloroethylene in MW-8

The constituents detected above reporting limits, but below the applicable 15A NCAC 2L.0202
Groundwater Standards included:
 Chloroform in MW-6 and MW-7
 Cis-1,2-dichloroethylene in MW-8

Groundwater analytical results are summarized in Table 4 and depicted on Figure 2. Laboratory reports,
quality assurance/quality control (QA/QC) information, and chain-of-custody records are included as
Attachment A.

Investigative Derived Waste (IDW) disposal

All soil cuttings and purge water generated during this assessment are temporarily staged on-site in six (6)
55-gallon steel drums. These drums were positioned to the west of the equipment shed, along the
southwestern boundary of the paved portion of the Site on October 10, 2013. A label was placed on each
drum noting its content, origin of materials (i.e. MW-6), and HRP’s contact information.

Conclusions

A Limited Phase II Environmental Site Assessment was performed on October 10, 2013 to further
assess the extent of chlorinated solvents in groundwater at the Site (MW-5, F&R report dated June
2013) and to evaluate whether the source of contamination exists on-site, or is a result of an
unidentified off-site source. Three (3) soil borings were advanced at the Site, which were
subsequently converted to permanent groundwater monitoring wells. Four (4) soil samples and three
(3) groundwater samples were collected and analyzed to evaluate soil and groundwater quality.

Tetrachloroethylene was detected above the applicable regulatory standard in the groundwater
samples collected within MW-7 and MW-8. Of note, both MW-7 and MW-8 are located
hydraulically up-gradient of the Site building. Trichloroethylene was detected in MW-8 above the
applicable regulatory screening standards. Cis-1,2-dichloroethylene, a breakdown product of
trichloroethylene, was also detected in well MW-8.

Methylene chloride was also detected above the applicable regulatory standard in the groundwater
sample collected from well MW-8. Methyl chloride, a breakdown product of methylene chloride,
was detected in well MW-6 above the applicable regulatory standards. Chloroform, a parent product
of methylene chloride was detected in wells MW-6 and MW-7.

The concentrations of tetrachloroethylene and trichloroethylene detected in MW-6, MW-7, and MW-8
were significantly less than what was observed in well MW-5 on May 31, 2013. The calculated area
groundwater flow is to the south-southeast. Due to the fact that MW-5, MW-7, and MW-8 are positioned
hydraulically upgradient of the Subject Site, and the fact that chlorinated constituents were not previously
detected in the down-gradient wells MW-2, MW-4, DW-1, or MW-3, the presence of chlorinated solvents
in Site groundwater is likely a result of an off-site, unidentified source.

527 Atando Avenue
November 1, 2013
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HRP Associates, Inc. Creating the Right Solutions Together
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\WP\GOU4000.GW- Gould Atando Facility P2.docx
If you have any questions regarding this report or the laboratory results, please do not hesitate to
contact us at [phone].

Sincerely,

HRP Associates, Inc.

Salley Gould, GIT #26 Robert “Ty” Hawkins Traci Fulkerson, P.G.
Project Geologist Project Manager Licensed Geologist # 2280

Attachments

HRP Associates, Inc.
SITE FIGURES

FIGURE 1 
TOPOGRAPHIC MAP 
SITE LAYOUT 
527 ATLANDO AVENUE  
CHARLOTTE, NC 

COMPILED: OCTOBER 17, 2013 
HRP Associates, Inc.
Environmental/Civil Engineering and Hydrogeology 
Creating the Right Solutions Together 
CT – NY – MA – SC – FL – TX  
1327 Miller Road, Suite D 
Greenville, SC 29607 
Ph: (864) 289‐0311  Fax: (864) 281‐9846 
http://www.hrpassociates.com 
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Figure 3Site Plan527 Atando AvenueCharlotte, North CarolinaHRP# GOU7000.GWScale 1" = 80'
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HRP Associates, Inc.
TABLES

MONITORING
LOCATION
MEASURING
POINT
ELEVATION1
(ft AMSL)
DEPTH TO
WATER
(ft TOC)
WATER
ELEVATION
(ft AMSL)
TOTAL
DEPTH (ft
BGS)
TEMPERATURE
(oF)
CONDUCTIVITY
(uS/cm)
pH
MW-1 744.02 NA NA NA NA NA NA
MW-2 743.65 19.3 724.4 33.8 NA NA NA
MW-3 738.71 14.6 724.1 32.0 NA NA NA
MW-4 738.95 14.0 725.0 31.9 NA NA NA
MW-5 740.64 11.5 729.1 31.3 NA NA NA
MW-6 742.83 17.0 725.8 30.0 69.3 140.8 5.73
MW-7 743.84 15.1 728.7 29.1 68.1 203.0 6.64
MW-8 739.80 10.5 729.3 34.0 70.3 278.0 6.45
DW-1 739.05 13.5 725.6 87.3 NA NA NA
NOTES:
[1] Measuring point elevations obtained from the Monitoring Well Location Plan surveyed by AccuTech Surveying & Mapping, LLP 10/16/2013
AMSL - Above Mean Sea Level
TOC - Top of PVC Casing
TABLE 1
FIELD MEASUREMENTS
527 Atando Avenue
Charlotte, NC
10/16/2013
WELL PAIR
Horizontal
Separation
Distance
Flow
Direction
Date
Measured MW-7 MW-6 i ft/month MW-8 MW-7 i ft/month MW-8 MW-6 i ft/month
10/16/2013 728.7 725.8 0.01 0.066 729.30 728.74 0.002 0.01 729.30 725.83 0.01 0.05
NOTES:
Average linear velocity = K i / ne; assume effective porosity (ne) of 0.20 for aquifer, and homogeneous isotropic porous aquifer.
1.20
AMSL - above mean sea level
Horiz Grad, i - horizontal gradient
Average Hydraulic Conductivity for silty/sandy clay (Clapp & Hornberger, 1978) (ft/month):
Groundwater
Elevation Action
(ft AMSL)
Horiz Grad Linear
Velocity
Groundwater
Elevation Action
(ft AMSL)
Horiz
Grad
Linear
Velocity
Groundwater
Elevation Action
(ft AMSL)
Horiz
Grad
Linear
Velocity
[1]
269 FT 319 FT 413 FT
South-Southeast South-Southeast South-Southeast
TABLE 2
ESTIMATED HYDRAULIC GRADIENT AND AVERAGE LINEAR VELOCITY
527 Atando Avenue
Charlotte, NC
MW-7 to MW-6 MW-8 to MW-7 MW-8 to MW-6
10/16/2013
MW-5 MW-6 MW-7 MW-8
Compound 5/31/13* 10/16/13 10/16/13 10/16/13
Not
Available 17.0 / 30.0 15.1 / 29.1 10.5 / 34.0
MCL (μg/l)GCL
(μg/l)
2L.0202
Groundwater
Standard
(μg/l)
VOCs (Total) (ug/L)
Chloroform 80 70,000 70 <10 22.1 0.63 J <5.0
cis-1,2-Dichloroethylene 70 70,000 70 1,100 <1.0 <1.0 24.8
Methyl chloride NE 3,000 3 <10 15.0 <2.0 <10
Methylene chloride 5 5,000 5.0 <20 <5.0 <5.0 10.5 J
Tetrachloroethylene 5 700 0.7 4,900 <1.0 1.3 236
trans-1,2-dichloroethylene 100 100,000 100.0 12 <1.0 <1.0 <5.0
Trichloroethylene 5 3,000 3 3,000 <1.0 <1.0 34.9
Vinyl Chloride 2 30 0.03 120 <1.0 <1.0 <5.0
NOTES:
* MW-5 was sampled by F&R on May 31, 2013
-Values in bold represent constituent detections above Laboratory Reporting Limits
-Shaded cells indicate detections above applicable 15A NCAC 2L.0202 Groundwater Standards
-VOCs- Volatile Organic Compounds
-MCL- EPA Maximum Contaminant Level Standard for Drinking Water, May 2013
-GCL- Gross Contamination levels for Groundwater, April 16, 2012
-MW - Monitoring Well
-J values indicate the consituent was detected, but below the laboratory Reporting Limits; therefore, the result is an estimated concentration.
527 Atando Avenue
LOCATION
DATE
TABLE 3
GROUNDWATER ANALYTICAL DATA
Charlotte, NC
Depth to water (ft bgs) / Well Depth
(ft bgs)
10/16/2013
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\Data\Gould P2 ResultsTable 3 - Groundwater HRP Associates, Inc.
SAMPLE ID: MW-6 MW-7 MW-8 MW-8
(FT BGS):14-16 12-14 13-15 23-25
VOCs (ug/kg)SAMPLE DATE: 05/14/13 05/14/13 05/14/13 05/17/13
IPSRGA
Acetone 100,000 28.8J1 <46 <42 <46
NOTES:
A Industrial Preliminary Soil Remediation Goal (IPSRG) obtained from the Inactive Hazardous Sites Branch July 2013
bgs - below ground surface
MW - Monitoring Well
¹J values indicate the consituent was detected but below the laboratory Reporting Limit; therefore, the result is an estimated concentration
SOIL ANALYTICAL DATA
TABLE 4
Charlotte, NC
527 Atando Avenue
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\Data\Gould P2 ResultsTable 4 - Soil Page 1 of 1 HRP Associates, Inc.

HRP Associates, Inc.

ATTACHMENT A

LABORATORY REPORT

10/23/13
Technical Report for
HRP Associates, Inc
Gould P-2; Atando Ave, Charlotte, NC
GOU7000
Accutest Job Number: FA9201
Sampling Date: 10/16/13
Report to:
HRP Associates, Inc
1327-D Miller Rd
Greenville, SC 24618
[e-mail]; [e-mail]
ATTN: Ty Hawkins
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
10/23/13
e-Hardcopy 2.0
Automated Report
28
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 28
FA9201
Table of Contents
-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3
Section 2: Summary of Hits .................................................................................................... 4
Section 3: Sample Results ........................................................................................................5
3.1: FA9201-1: MW-6 .......................................................................................................... 6
3.2: FA9201-2: MW-7 .......................................................................................................... 9
3.3: FA9201-3: MW-8 .......................................................................................................... 12
Section 4: Misc. Forms ............................................................................................................15
4.1: Certification Exceptions ................................................................................................ 16
4.2: Chain of Custody ........................................................................................................... 17
Section 5: GC/MS Volatiles - QC Data Summaries .............................................................. 19
5.1: Method Blank Summary ................................................................................................ 20
5.2: Blank Spike Summary ................................................................................................... 23
5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 26
1
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Accutest Laboratories
Sample Summary
HRP Associates, Inc
Job No:FA9201
Gould P-2; Atando Ave, Charlotte, NC
Project No: GOU7000
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA9201-1 10/16/13 09:50 DS 10/18/13 AQ Ground Water MW-6
FA9201-2 10/16/13 10:30 DS 10/18/13 AQ Ground Water MW-7
FA9201-3 10/16/13 11:00 DS 10/18/13 AQ Ground Water MW-8
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Summary of Hits Page 1 of 1
Job Number:FA9201
Account:HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Collected:10/16/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA9201-1 MW-6
Chloroform 22.1 1.0 0.26 ug/l SW846 8260B
Methyl chloride 15.0 2.0 0.50 ug/l SW846 8260B
FA9201-2 MW-7
Chloroform 0.63 J 1.0 0.26 ug/l SW846 8260B
Tetrachloroethylene 1.3 1.0 0.32 ug/l SW846 8260B
FA9201-3 MW-8
cis-1,2-Dichloroethylene 24.8 5.0 1.2 ug/l SW846 8260B
Methylene chloride 10.5 J 25 10 ug/l SW846 8260B
Tetrachloroethylene 236 5.0 1.6 ug/l SW846 8260B
Trichloroethylene 34.9 5.0 1.6 ug/l SW846 8260B
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 3
Client Sample ID:MW-6
Lab Sample ID:FA9201-1 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P19973.D 1 10/22/13 EG n/a n/a VP757
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone
a ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.21 ug/l
108-86-1 Bromobenzene ND 1.0 0.22 ug/l
74-97-5 Bromochloromethane ND 1.0 0.23 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.20 ug/l
75-25-2 Bromoform ND 1.0 0.34 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.20 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.21 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.29 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.50 ug/l
67-66-3 Chloroform 22.1 1.0 0.26 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.21 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.20 ug/l
56-23-5 Carbon tetrachloride ND 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.30 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.26 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.27 ug/l
108-20-3 Di-Isopropyl ether ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane
a ND 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.22 ug/l
541-73-1 m-Dichlorobenzene ND 1.0 0.25 ug/l
95-50-1 o-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 p-Dichlorobenzene ND 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.23 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-6
Lab Sample ID:FA9201-1 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
100-41-4 Ethylbenzene ND 1.0 0.29 ug/l
64-17-5 Ethyl Alcohol ND 100 21 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone ND 5.0 2.3 ug/l
74-83-9 Methyl bromide ND 2.0 0.79 ug/l
74-87-3 Methyl chloride 15.0 2.0 0.50 ug/l
75-09-2 Methylene chloride ND 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone ND 5.0 3.1 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.21 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.23 ug/l
100-42-5 Styrene ND 1.0 0.20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.23 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.56 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 2.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 2.0 0.20 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.32 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
79-01-6 Trichloroethylene ND 1.0 0.31 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
75-01-4 Vinyl chloride ND 1.0 0.44 ug/l
108-05-4 Vinyl Acetate ND 10 3.1 ug/l
1330-20-7 Xylene (total)ND 3.0 0.50 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.20 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%83-118%
17060-07-0 1,2-Dichloroethane-D4 100%79-125%
2037-26-5 Toluene-D8 98%85-112%
460-00-4 4-Bromofluorobenzene 100%83-118%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-6
Lab Sample ID:FA9201-1 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-7
Lab Sample ID:FA9201-2 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P19974.D 1 10/22/13 EG n/a n/a VP757
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone
a ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.21 ug/l
108-86-1 Bromobenzene ND 1.0 0.22 ug/l
74-97-5 Bromochloromethane ND 1.0 0.23 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.20 ug/l
75-25-2 Bromoform ND 1.0 0.34 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.20 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.21 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.29 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.50 ug/l
67-66-3 Chloroform 0.63 1.0 0.26 ug/l J
95-49-8 o-Chlorotoluene ND 1.0 0.21 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.20 ug/l
56-23-5 Carbon tetrachloride ND 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.30 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.26 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.27 ug/l
108-20-3 Di-Isopropyl ether ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane
a ND 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.22 ug/l
541-73-1 m-Dichlorobenzene ND 1.0 0.25 ug/l
95-50-1 o-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 p-Dichlorobenzene ND 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.23 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-7
Lab Sample ID:FA9201-2 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
100-41-4 Ethylbenzene ND 1.0 0.29 ug/l
64-17-5 Ethyl Alcohol ND 100 21 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone ND 5.0 2.3 ug/l
74-83-9 Methyl bromide ND 2.0 0.79 ug/l
74-87-3 Methyl chloride ND 2.0 0.50 ug/l
75-09-2 Methylene chloride ND 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone ND 5.0 3.1 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.21 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.23 ug/l
100-42-5 Styrene ND 1.0 0.20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.23 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.56 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 2.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 2.0 0.20 ug/l
127-18-4 Tetrachloroethylene 1.3 1.0 0.32 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
79-01-6 Trichloroethylene ND 1.0 0.31 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
75-01-4 Vinyl chloride ND 1.0 0.44 ug/l
108-05-4 Vinyl Acetate ND 10 3.1 ug/l
1330-20-7 Xylene (total)ND 3.0 0.50 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.20 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 99%85-112%
460-00-4 4-Bromofluorobenzene 105%83-118%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-7
Lab Sample ID:FA9201-2 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-8
Lab Sample ID:FA9201-3 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P19975.D 5 10/22/13 EG n/a n/a VP757
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone
a ND 130 50 ug/l
71-43-2 Benzene ND 5.0 1.1 ug/l
108-86-1 Bromobenzene ND 5.0 1.1 ug/l
74-97-5 Bromochloromethane ND 5.0 1.1 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/l
75-25-2 Bromoform ND 5.0 1.7 ug/l
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/l
135-98-8 sec-Butylbenzene ND 5.0 1.1 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.5 ug/l
108-90-7 Chlorobenzene ND 5.0 1.0 ug/l
75-00-3 Chloroethane ND 10 2.5 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.1 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/l
56-23-5 Carbon tetrachloride ND 5.0 1.6 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.1 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.5 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.1 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
108-20-3 Di-Isopropyl ether ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.2 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/l
75-71-8 Dichlorodifluoromethane
a ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene 24.8 5.0 1.2 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.1 ug/l
541-73-1 m-Dichlorobenzene ND 5.0 1.3 ug/l
95-50-1 o-Dichlorobenzene ND 5.0 1.1 ug/l
106-46-7 p-Dichlorobenzene ND 5.0 1.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.1 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-8
Lab Sample ID:FA9201-3 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/l
100-41-4 Ethylbenzene ND 5.0 1.5 ug/l
64-17-5 Ethyl Alcohol ND 500 110 ug/l
591-78-6 2-Hexanone ND 50 10 ug/l
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/l
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone ND 25 11 ug/l
74-83-9 Methyl bromide ND 10 3.9 ug/l
74-87-3 Methyl chloride ND 10 2.5 ug/l
75-09-2 Methylene chloride 10.5 25 10 ug/l J
78-93-3 Methyl ethyl ketone ND 25 16 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/l
91-20-3 Naphthalene ND 25 5.0 ug/l
103-65-1 n-Propylbenzene ND 5.0 1.1 ug/l
100-42-5 Styrene ND 5.0 1.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.2 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.2 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 2.5 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.8 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 10 1.0 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 10 1.0 ug/l
127-18-4 Tetrachloroethylene 236 5.0 1.6 ug/l
108-88-3 Toluene ND 5.0 1.0 ug/l
79-01-6 Trichloroethylene 34.9 5.0 1.6 ug/l
75-69-4 Trichlorofluoromethane ND 10 2.5 ug/l
75-01-4 Vinyl chloride ND 5.0 2.2 ug/l
108-05-4 Vinyl Acetate ND 50 16 ug/l
1330-20-7 Xylene (total)ND 15 2.5 ug/l
m,p-Xylene ND 10 1.5 ug/l
95-47-6 o-Xylene ND 5.0 1.0 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%83-118%
17060-07-0 1,2-Dichloroethane-D4 104%79-125%
2037-26-5 Toluene-D8 101%85-112%
460-00-4 4-Bromofluorobenzene 102%83-118%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-8
Lab Sample ID:FA9201-3 Date Sampled:10/16/13
Matrix:AQ - Ground Water Date Received:10/18/13
Method:SW846 8260B Percent Solids:n/a
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Chain of Custody
Southeast
Section 4
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Parameter Certification Exceptions Page 1 of 1
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
The following parameters included in this report are exceptions to NELAC certification.
The certification status of each is indicated below.
Parameter CAS# Method Mat Certification Status
Di-Isopropyl ether 108-20-3 SW846 8260B AQ Certified by SOP MS005
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FA9201: Chain of Custody
Page 1 of 2
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FA9201: Chain of Custody
Page 2 of 2
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Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VP757-MB P19971.D 1 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.21 ug/l
108-86-1 Bromobenzene ND 1.0 0.22 ug/l
74-97-5 Bromochloromethane ND 1.0 0.23 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.20 ug/l
75-25-2 Bromoform ND 1.0 0.34 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.20 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.21 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.29 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.50 ug/l
67-66-3 Chloroform ND 1.0 0.26 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.21 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.20 ug/l
56-23-5 Carbon tetrachloride ND 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.30 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.26 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.27 ug/l
108-20-3 Di-Isopropyl ether ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.22 ug/l
541-73-1 m-Dichlorobenzene ND 1.0 0.25 ug/l
95-50-1 o-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 p-Dichlorobenzene ND 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
100-41-4 Ethylbenzene ND 1.0 0.29 ug/l
64-17-5 Ethyl Alcohol ND 100 21 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VP757-MB P19971.D 1 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
CAS No. Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 1.0 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone ND 5.0 2.3 ug/l
74-83-9 Methyl bromide ND 2.0 0.79 ug/l
74-87-3 Methyl chloride ND 2.0 0.50 ug/l
75-09-2 Methylene chloride ND 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone ND 5.0 3.1 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.21 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.23 ug/l
100-42-5 Styrene ND 1.0 0.20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.23 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.56 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 2.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 2.0 0.20 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.32 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
79-01-6 Trichloroethylene ND 1.0 0.31 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
75-01-4 Vinyl chloride ND 1.0 0.44 ug/l
108-05-4 Vinyl Acetate ND 10 3.1 ug/l
1330-20-7 Xylene (total)ND 3.0 0.50 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.20 ug/l
CAS No. Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99% 83-118%
17060-07-0 1,2-Dichloroethane-D4 104% 79-125%
2037-26-5 Toluene-D8 101% 85-112%
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Method Blank Summary Page 3 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VP757-MB P19971.D 1 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 103% 83-118%
CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q
Total TIC, Volatile a 0 ug/l
(a) No TICs detected.
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Blank Spike Summary Page 1 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VP757-BS P19970.D 1 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
Spike BSP BSP
CAS No. Compound ug/l ug/l % Limits
67-64-1 Acetone 125 231 185* 50-147
71-43-2 Benzene 25 26.7 107 81-122
108-86-1 Bromobenzene 25 25.1 100 80-121
74-97-5 Bromochloromethane 25 22.2 89 76-123
75-27-4 Bromodichloromethane 25 26.4 106 79-123
75-25-2 Bromoform 25 23.2 93 66-123
104-51-8 n-Butylbenzene 25 25.9 104 79-126
135-98-8 sec-Butylbenzene 25 30.1 120 83-133
98-06-6 tert-Butylbenzene 25 28.5 114 80-133
108-90-7 Chlorobenzene 25 27.1 108 82-124
75-00-3 Chloroethane 25 24.1 96 62-144
67-66-3 Chloroform 25 25.1 100 80-124
95-49-8 o-Chlorotoluene 25 28.9 116 81-127
106-43-4 p-Chlorotoluene 25 29.3 117 83-130
56-23-5 Carbon tetrachloride 25 27.6 110 76-136
75-34-3 1,1-Dichloroethane 25 25.9 104 81-122
75-35-4 1,1-Dichloroethylene 25 27.6 110 78-137
563-58-6 1,1-Dichloropropene 25 28.6 114 79-131
106-93-4 1,2-Dibromoethane 25 25.0 100 75-120
107-06-2 1,2-Dichloroethane 25 25.8 103 75-125
78-87-5 1,2-Dichloropropane 25 25.6 102 76-124
142-28-9 1,3-Dichloropropane 25 26.2 105 80-118
108-20-3 Di-Isopropyl ether 25 23.7 95 68-123
594-20-7 2,2-Dichloropropane 25 23.0 92 74-139
124-48-1 Dibromochloromethane 25 25.2 101 78-122
75-71-8 Dichlorodifluoromethane 25 43.6 174* 42-167
156-59-2 cis-1,2-Dichloroethylene 25 24.0 96 78-120
10061-01-5 cis-1,3-Dichloropropene 25 24.9 100 75-118
541-73-1 m-Dichlorobenzene 25 27.6 110 84-125
95-50-1 o-Dichlorobenzene 25 26.6 106 82-124
106-46-7 p-Dichlorobenzene 25 26.1 104 78-120
156-60-5 trans-1,2-Dichloroethylene 25 26.4 106 76-127
10061-02-6 trans-1,3-Dichloropropene 25 29.1 116 80-120
100-41-4 Ethylbenzene 25 25.8 103 81-121
64-17-5 Ethyl Alcohol 500 442 88 46-145
591-78-6 2-Hexanone 125 148 118 61-129
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VP757-BS P19970.D 1 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
Spike BSP BSP
CAS No. Compound ug/l ug/l % Limits
98-82-8 Isopropylbenzene 25 26.8 107 83-132
99-87-6 p-Isopropyltoluene 25 28.9 116 79-130
108-10-1 4-Methyl-2-pentanone 125 133 106 66-122
74-83-9 Methyl bromide 25 27.0 108 59-143
74-87-3 Methyl chloride 25 30.5 122 50-159
75-09-2 Methylene chloride 25 25.1 100 69-135
78-93-3 Methyl ethyl ketone 125 158 126 56-143
1634-04-4 Methyl Tert Butyl Ether 25 22.7 91 72-117
91-20-3 Naphthalene 25 26.1 104 63-132
103-65-1 n-Propylbenzene 25 29.1 116 82-133
100-42-5 Styrene 25 25.1 100 78-119
630-20-6 1,1,1,2-Tetrachloroethane 25 26.1 104 77-122
71-55-6 1,1,1-Trichloroethane 25 24.9 100 75-130
79-34-5 1,1,2,2-Tetrachloroethane 25 25.5 102 72-120
79-00-5 1,1,2-Trichloroethane 25 26.4 106 76-119
87-61-6 1,2,3-Trichlorobenzene 25 26.6 106 68-131
96-18-4 1,2,3-Trichloropropane 25 28.0 112 77-120
120-82-1 1,2,4-Trichlorobenzene 25 23.9 96 73-129
95-63-6 1,2,4-Trimethylbenzene 25 25.6 102 79-120
108-67-8 1,3,5-Trimethylbenzene 25 26.8 107 79-120
127-18-4 Tetrachloroethylene 25 31.7 127 76-135
108-88-3 Toluene 25 26.4 106 80-120
79-01-6 Trichloroethylene 25 27.4 110 81-126
75-69-4 Trichlorofluoromethane 25 20.0 80 71-156
75-01-4 Vinyl chloride 25 30.1 120 69-159
108-05-4 Vinyl Acetate 125 118 94 43-154
1330-20-7 Xylene (total)75 83.5 111 80-126
m,p-Xylene 50 55.6 111 79-126
95-47-6 o-Xylene 25 27.9 112 80-127
CAS No. Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 96% 83-118%
17060-07-0 1,2-Dichloroethane-D4 102% 79-125%
2037-26-5 Toluene-D8 99% 85-112%
* = Outside of Control Limits.
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Blank Spike Summary Page 3 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VP757-BS P19970.D 1 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
CAS No. Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 98% 83-118%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9083-21MS P19981.D 20 10/22/13 EG n/a n/a VP757
FA9083-21MSD P19982.D 20 10/22/13 EG n/a n/a VP757
FA9083-21 P19977.D 20 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
FA9083-21 Spike MS MS MSD MSD Limits
CAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD
67-64-1 Acetone 500 U 2500 2260 90 2450 98 8 50-147/21
71-43-2 Benzene 20 U 500 535 107 512 102 4 81-122/14
108-86-1 Bromobenzene 20 U 500 493 99 487 97 1 80-121/14
74-97-5 Bromochloromethane 20 U 500 477 95 428 86 11 76-123/14
75-27-4 Bromodichloromethane 20 U 500 509 102 464 93 9 79-123/19
75-25-2 Bromoform 20 U 500 404 81 361 72 11 66-123/21
104-51-8 n-Butylbenzene 20 U 500 524 105 490 98 7 79-126/16
135-98-8 sec-Butylbenzene 20 U 500 591 118 564 113 5 83-133/16
98-06-6 tert-Butylbenzene 20 U 500 558 112 522 104 7 80-133/16
108-90-7 Chlorobenzene 20 U 500 522 104 516 103 1 82-124/14
75-00-3 Chloroethane 40 U 500 442 88 427 85 3 62-144/20
67-66-3 Chloroform 20 U 500 506 101 485 97 4 80-124/15
95-49-8 o-Chlorotoluene 20 U 500 566 113 533 107 6 81-127/15
106-43-4 p-Chlorotoluene 20 U 500 593 119 555 111 7 83-130/15
56-23-5 Carbon tetrachloride 20 U 500 533 107 483 97 10 76-136/23
75-34-3 1,1-Dichloroethane 20 U 500 529 106 498 100 6 81-122/15
75-35-4 1,1-Dichloroethylene 20 U 500 550 110 511 102 7 78-137/18
563-58-6 1,1-Dichloropropene 20 U 500 581 116 547 109 6 79-131/16
106-93-4 1,2-Dibromoethane 20 U 500 499 100 456 91 9 75-120/13
107-06-2 1,2-Dichloroethane 20 U 500 494 99 490 98 1 75-125/14
78-87-5 1,2-Dichloropropane 20 U 500 533 107 501 100 6 76-124/14
142-28-9 1,3-Dichloropropane 20 U 500 501 100 481 96 4 80-118/13
108-20-3 Di-Isopropyl ether 20 U 500 442 88 432 86 2 68-123/16
594-20-7 2,2-Dichloropropane 20 U 500 486 97 440 88 10 74-139/17
124-48-1 Dibromochloromethane 20 U 500 444 89 415 83 7 78-122/19
75-71-8 Dichlorodifluoromethane 40 U 500 839 168* 736 147 13 42-167/19
156-59-2 cis-1,2-Dichloroethylene 1170 500 1620 90 1530 72* a 6 78-120/15
10061-01-5 cis-1,3-Dichloropropene 20 U 500 499 100 446 89 11 75-118/23
541-73-1 m-Dichlorobenzene 20 U 500 559 112 522 104 7 84-125/14
95-50-1 o-Dichlorobenzene 20 U 500 518 104 508 102 2 82-124/14
106-46-7 p-Dichlorobenzene 20 U 500 513 103 489 98 5 78-120/15
156-60-5 trans-1,2-Dichloroethylene 5.1 I 500 532 105 486 96 9 76-127/17
10061-02-6 trans-1,3-Dichloropropene 20 U 500 531 106 510 102 4 80-120/22
100-41-4 Ethylbenzene 20 U 500 510 102 495 99 3 81-121/14
64-17-5 Ethyl Alcohol 2000 U 10000 9370 94 7940 79 17 46-145/30
591-78-6 2-Hexanone 200 U 2500 2220 89 2330 93 5 61-129/18
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9083-21MS P19981.D 20 10/22/13 EG n/a n/a VP757
FA9083-21MSD P19982.D 20 10/22/13 EG n/a n/a VP757
FA9083-21 P19977.D 20 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
FA9083-21 Spike MS MS MSD MSD Limits
CAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD
98-82-8 Isopropylbenzene 20 U 500 531 106 494 99 7 83-132/15
99-87-6 p-Isopropyltoluene 20 U 500 573 115 539 108 6 79-130/16
108-10-1 4-Methyl-2-pentanone 100 U 2500 2370 95 2500 100 5 66-122/16
74-83-9 Methyl bromide 40 U 500 508 102 470 94 8 59-143/19
74-87-3 Methyl chloride 40 U 500 581 116 550 110 5 50-159/19
75-09-2 Methylene chloride 43.4 I 500 563 104 476 87 17* 69-135/16
78-93-3 Methyl ethyl ketone 100 U 2500 2270 91 2280 91 0 56-143/18
1634-04-4 Methyl Tert Butyl Ether 20 U 500 438 88 432 86 1 72-117/14
91-20-3 Naphthalene 100 U 500 465 93 488 98 5 63-132/25
103-65-1 n-Propylbenzene 20 U 500 588 118 549 110 7 82-133/15
100-42-5 Styrene 20 U 500 480 96 459 92 4 78-119/23
630-20-6 1,1,1,2-Tetrachloroethane 20 U 500 515 103 467 93 10 77-122/19
71-55-6 1,1,1-Trichloroethane 20 U 500 507 101 475 95 7 75-130/16
79-34-5 1,1,2,2-Tetrachloroethane 20 U 500 478 96 494 99 3 72-120/14
79-00-5 1,1,2-Trichloroethane 20 U 500 493 99 503 101 2 76-119/14
87-61-6 1,2,3-Trichlorobenzene 20 U 500 461 92 493 99 7 68-131/25
96-18-4 1,2,3-Trichloropropane 40 U 500 495 99 515 103 4 77-120/16
120-82-1 1,2,4-Trichlorobenzene 20 U 500 444 89 459 92 3 73-129/20
95-63-6 1,2,4-Trimethylbenzene 40 U 500 523 105 496 99 5 79-120/18
108-67-8 1,3,5-Trimethylbenzene 40 U 500 550 110 510 102 8 79-120/19
127-18-4 Tetrachloroethylene 532 500 1000 94 930 80 7 76-135/16
108-88-3 Toluene 20 U 500 517 103 500 100 3 80-120/14
79-01-6 Trichloroethylene 617 500 1120 101 1090 95 3 81-126/15
75-69-4 Trichlorofluoromethane 40 U 500 415 83 414 83 0 71-156/21
75-01-4 Vinyl chloride 103 500 642 108 581 96 10 69-159/18
108-05-4 Vinyl Acetate 200 U 2500 2460 98 2450 98 0 43-154/14
1330-20-7 Xylene (total)60 U 1500 1660 111 1570 105 6 80-126/15
m,p-Xylene 40 U 1000 1110 111 1050 105 6 79-126/15
95-47-6 o-Xylene 20 U 500 555 111 520 104 7 80-127/14
CAS No. Surrogate Recoveries MS MSD FA9083-21 Limits
1868-53-7 Dibromofluoromethane 98%98%99% 83-118%
17060-07-0 1,2-Dichloroethane-D4 101%100%105% 79-125%
2037-26-5 Toluene-D8 98%98%99% 85-112%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA9201
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9083-21MS P19981.D 20 10/22/13 EG n/a n/a VP757
FA9083-21MSD P19982.D 20 10/22/13 EG n/a n/a VP757
FA9083-21 P19977.D 20 10/22/13 EG n/a n/a VP757
The QC reported here applies to the following samples:Method: SW846 8260B
FA9201-1, FA9201-2, FA9201-3
CAS No. Surrogate Recoveries MS MSD FA9083-21 Limits
460-00-4 4-Bromofluorobenzene 98%97%101% 83-118%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
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10/21/13
Technical Report for
HRP Associates, Inc
Gould P-2; Atando Ave, Charlotte, NC
GOU4000
Accutest Job Number: FA9018
Sampling Date: 10/10/13
Report to:
HRP Associates, Inc
1327-D Miller Rd
Greenville, SC 24618
[e-mail]; [e-mail]
ATTN: Ty Hawkins
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
10/21/13
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FA9018
Table of Contents
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Sections:
Section 1: Sample Summary ................................................................................................... 3
Section 2: Summary of Hits .................................................................................................... 4
Section 3: Sample Results ........................................................................................................5
3.1: FA9018-1: MW-7 (12-14) ............................................................................................. 6
3.2: FA9018-2: MW-6 (14-16) ............................................................................................. 8
3.3: FA9018-3: MW-8 (13-15) ............................................................................................. 10
3.4: FA9018-4: MW-8 (23-25) ............................................................................................. 13
Section 4: Misc. Forms ............................................................................................................15
4.1: Chain of Custody ........................................................................................................... 16
Section 5: GC/MS Volatiles - QC Data Summaries .............................................................. 18
5.1: Method Blank Summary ................................................................................................ 19
5.2: Blank Spike Summary ................................................................................................... 28
5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 37
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Accutest Laboratories
Sample Summary
HRP Associates, Inc
Job No:FA9018
Gould P-2; Atando Ave, Charlotte, NC
Project No: GOU4000
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA9018-1 10/10/13 12:05 SG 10/12/13 SO Soil MW-7 (12-14)
FA9018-2 10/10/13 13:05 SG 10/12/13 SO Soil MW-6 (14-16)
FA9018-3 10/10/13 15:30 SG 10/12/13 SO Soil MW-8 (13-15)
FA9018-4 10/10/13 15:40 SG 10/12/13 SO Soil MW-8 (23-25)
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Summary of Hits Page 1 of 1
Job Number:FA9018
Account:HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Collected:10/10/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA9018-1 MW-7 (12-14)
No hits reported in this sample.
FA9018-2 MW-6 (14-16)
Acetone 28.8 J 49 20 ug/kg SW846 8260B
FA9018-3 MW-8 (13-15)
No hits reported in this sample.
FA9018-4 MW-8 (23-25)
No hits reported in this sample.
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:MW-7 (12-14)
Lab Sample ID:FA9018-1 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:90.1
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0062118.D 1 10/14/13 AH n/a n/a VF2000
Run #2
Initial Weight
Run #1 6.06 g
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 46 18 ug/kg
71-43-2 Benzene ND 4.6 0.92 ug/kg
108-86-1 Bromobenzene ND 4.6 0.99 ug/kg
74-97-5 Bromochloromethane ND 4.6 1.3 ug/kg
75-27-4 Bromodichloromethane ND 4.6 1.3 ug/kg
75-25-2 Bromoform ND 4.6 0.92 ug/kg
104-51-8 n-Butylbenzene ND 4.6 1.2 ug/kg
135-98-8 sec-Butylbenzene ND 4.6 1.1 ug/kg
98-06-6 tert-Butylbenzene ND 4.6 1.1 ug/kg
108-90-7 Chlorobenzene ND 4.6 0.92 ug/kg
75-00-3 Chloroethane ND 4.6 1.8 ug/kg
67-66-3 Chloroform ND 4.6 0.92 ug/kg
95-49-8 o-Chlorotoluene ND 4.6 0.92 ug/kg
106-43-4 p-Chlorotoluene ND 4.6 1.1 ug/kg
56-23-5 Carbon tetrachloride ND 4.6 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 4.6 0.92 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.6 1.1 ug/kg
563-58-6 1,1-Dichloropropene ND 4.6 0.92 ug/kg
106-93-4 1,2-Dibromoethane ND 4.6 0.92 ug/kg
107-06-2 1,2-Dichloroethane ND 4.6 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 4.6 0.92 ug/kg
142-28-9 1,3-Dichloropropane ND 4.6 0.92 ug/kg
108-20-3 Di-Isopropyl ether ND 4.6 0.94 ug/kg
594-20-7 2,2-Dichloropropane ND 4.6 0.92 ug/kg
124-48-1 Dibromochloromethane ND 4.6 0.92 ug/kg
75-71-8 Dichlorodifluoromethane ND 4.6 0.92 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.6 0.92 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.6 0.92 ug/kg
541-73-1 m-Dichlorobenzene ND 4.6 0.92 ug/kg
95-50-1 o-Dichlorobenzene ND 4.6 1.0 ug/kg
106-46-7 p-Dichlorobenzene ND 4.6 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.6 0.92 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-7 (12-14)
Lab Sample ID:FA9018-1 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:90.1
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.6 0.92 ug/kg
64-17-5 Ethyl alcohol ND 370 60 ug/kg
100-41-4 Ethylbenzene ND 4.6 1.0 ug/kg
591-78-6 2-Hexanone ND 23 4.6 ug/kg
98-82-8 Isopropylbenzene ND 4.6 1.2 ug/kg
99-87-6 p-Isopropyltoluene ND 4.6 1.2 ug/kg
108-10-1 4-Methyl-2-pentanone ND 23 4.6 ug/kg
74-83-9 Methyl bromide ND 4.6 1.8 ug/kg
74-87-3 Methyl chloride ND 4.6 1.9 ug/kg
75-09-2 Methylene chloride ND 9.2 4.2 ug/kg
78-93-3 Methyl ethyl ketone ND 23 4.6 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 4.6 0.92 ug/kg
91-20-3 Naphthalene ND 4.6 1.8 ug/kg
103-65-1 n-Propylbenzene ND 4.6 0.94 ug/kg
100-42-5 Styrene ND 4.6 0.92 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.6 0.98 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.6 0.92 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.6 0.92 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.6 0.92 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.6 0.96 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.6 1.5 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.6 1.1 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.6 0.99 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.6 0.96 ug/kg
127-18-4 Tetrachloroethylene ND 4.6 1.1 ug/kg
108-88-3 Toluene ND 4.6 0.92 ug/kg
79-01-6 Trichloroethylene ND 4.6 0.92 ug/kg
75-69-4 Trichlorofluoromethane ND 4.6 1.8 ug/kg
75-01-4 Vinyl chloride ND 4.6 0.92 ug/kg
108-05-4 Vinyl Acetate ND 23 3.8 ug/kg
1330-20-7 Xylene (total)ND 14 2.8 ug/kg
m,p-Xylene ND 9.2 1.9 ug/kg
95-47-6 o-Xylene ND 4.6 0.92 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%75-124%
2037-26-5 Toluene-D8 91%75-126%
460-00-4 4-Bromofluorobenzene 107%71-133%
17060-07-0 1,2-Dichloroethane-D4 127%72-135%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-6 (14-16)
Lab Sample ID:FA9018-2 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:80.3
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0062119.D 1 10/14/13 AH n/a n/a VF2000
Run #2
Initial Weight
Run #1 6.35 g
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone 28.8 49 20 ug/kg J
71-43-2 Benzene ND 4.9 0.98 ug/kg
108-86-1 Bromobenzene ND 4.9 1.1 ug/kg
74-97-5 Bromochloromethane ND 4.9 1.4 ug/kg
75-27-4 Bromodichloromethane ND 4.9 1.4 ug/kg
75-25-2 Bromoform ND 4.9 0.98 ug/kg
104-51-8 n-Butylbenzene ND 4.9 1.3 ug/kg
135-98-8 sec-Butylbenzene ND 4.9 1.2 ug/kg
98-06-6 tert-Butylbenzene ND 4.9 1.2 ug/kg
108-90-7 Chlorobenzene ND 4.9 0.98 ug/kg
75-00-3 Chloroethane ND 4.9 2.0 ug/kg
67-66-3 Chloroform ND 4.9 0.98 ug/kg
95-49-8 o-Chlorotoluene ND 4.9 0.98 ug/kg
106-43-4 p-Chlorotoluene ND 4.9 1.1 ug/kg
56-23-5 Carbon tetrachloride ND 4.9 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 4.9 0.98 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.9 1.2 ug/kg
563-58-6 1,1-Dichloropropene ND 4.9 0.98 ug/kg
106-93-4 1,2-Dibromoethane ND 4.9 0.98 ug/kg
107-06-2 1,2-Dichloroethane ND 4.9 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 4.9 0.98 ug/kg
142-28-9 1,3-Dichloropropane ND 4.9 0.98 ug/kg
108-20-3 Di-Isopropyl ether ND 4.9 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 4.9 0.98 ug/kg
124-48-1 Dibromochloromethane ND 4.9 0.98 ug/kg
75-71-8 Dichlorodifluoromethane ND 4.9 0.98 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.9 0.98 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.9 0.98 ug/kg
541-73-1 m-Dichlorobenzene ND 4.9 0.98 ug/kg
95-50-1 o-Dichlorobenzene ND 4.9 1.1 ug/kg
106-46-7 p-Dichlorobenzene ND 4.9 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.9 0.98 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-6 (14-16)
Lab Sample ID:FA9018-2 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:80.3
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.9 0.98 ug/kg
64-17-5 Ethyl alcohol ND 390 64 ug/kg
100-41-4 Ethylbenzene ND 4.9 1.1 ug/kg
591-78-6 2-Hexanone ND 25 4.9 ug/kg
98-82-8 Isopropylbenzene ND 4.9 1.3 ug/kg
99-87-6 p-Isopropyltoluene ND 4.9 1.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 4.9 ug/kg
74-83-9 Methyl bromide ND 4.9 2.0 ug/kg
74-87-3 Methyl chloride ND 4.9 2.0 ug/kg
75-09-2 Methylene chloride ND 9.8 4.5 ug/kg
78-93-3 Methyl ethyl ketone ND 25 4.9 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 4.9 0.98 ug/kg
91-20-3 Naphthalene ND 4.9 2.0 ug/kg
103-65-1 n-Propylbenzene ND 4.9 1.0 ug/kg
100-42-5 Styrene ND 4.9 0.98 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.9 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.9 0.98 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 0.98 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.9 0.98 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.9 1.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.9 1.6 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.9 1.2 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.9 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.9 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 4.9 1.1 ug/kg
108-88-3 Toluene ND 4.9 0.98 ug/kg
79-01-6 Trichloroethylene ND 4.9 0.98 ug/kg
75-69-4 Trichlorofluoromethane ND 4.9 2.0 ug/kg
75-01-4 Vinyl chloride ND 4.9 0.98 ug/kg
108-05-4 Vinyl Acetate ND 25 4.1 ug/kg
1330-20-7 Xylene (total)ND 15 3.0 ug/kg
m,p-Xylene ND 9.8 2.0 ug/kg
95-47-6 o-Xylene ND 4.9 0.98 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%75-124%
2037-26-5 Toluene-D8 93%75-126%
460-00-4 4-Bromofluorobenzene 109%71-133%
17060-07-0 1,2-Dichloroethane-D4 119%72-135%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-8 (13-15)
Lab Sample ID:FA9018-3 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:83.7
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C096280.D 1 10/16/13 AH n/a n/a VC3831
Run #2 a F0062139.D 1 10/15/13 AH n/a n/a VF2001
Initial Weight
Run #1 7.19 g
Run #2 6.83 g
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 42 17 ug/kg
71-43-2 Benzene ND 4.2 0.83 ug/kg
108-86-1 Bromobenzene ND 4.2 0.90 ug/kg
74-97-5 Bromochloromethane ND 4.2 1.2 ug/kg
75-27-4 Bromodichloromethane ND 4.2 1.2 ug/kg
75-25-2 Bromoform ND 4.2 0.83 ug/kg
104-51-8 n-Butylbenzene ND 4.2 1.1 ug/kg
135-98-8 sec-Butylbenzene ND 4.2 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 4.2 0.99 ug/kg
108-90-7 Chlorobenzene ND 4.2 0.83 ug/kg
75-00-3 Chloroethane ND 4.2 1.7 ug/kg
67-66-3 Chloroform ND 4.2 0.83 ug/kg
95-49-8 o-Chlorotoluene ND 4.2 0.83 ug/kg
106-43-4 p-Chlorotoluene ND 4.2 0.96 ug/kg
56-23-5 Carbon tetrachloride ND 4.2 0.95 ug/kg
75-34-3 1,1-Dichloroethane ND 4.2 0.83 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.2 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 4.2 0.83 ug/kg
106-93-4 1,2-Dibromoethane ND 4.2 0.83 ug/kg
107-06-2 1,2-Dichloroethane ND 4.2 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 4.2 0.83 ug/kg
142-28-9 1,3-Dichloropropane ND 4.2 0.83 ug/kg
108-20-3 Di-Isopropyl ether ND 4.2 0.86 ug/kg
594-20-7 2,2-Dichloropropane ND 4.2 0.83 ug/kg
124-48-1 Dibromochloromethane ND 4.2 0.83 ug/kg
75-71-8 Dichlorodifluoromethane ND 4.2 0.83 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.2 0.83 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.2 0.83 ug/kg
541-73-1 m-Dichlorobenzene ND 4.2 0.83 ug/kg
95-50-1 o-Dichlorobenzene ND 4.2 0.91 ug/kg
106-46-7 p-Dichlorobenzene ND 4.2 1.1 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.2 0.83 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8 (13-15)
Lab Sample ID:FA9018-3 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:83.7
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.2 0.83 ug/kg
64-17-5 Ethyl alcohol ND 330 54 ug/kg
100-41-4 Ethylbenzene ND 4.2 0.91 ug/kg
591-78-6 2-Hexanone ND 21 4.2 ug/kg
98-82-8 Isopropylbenzene ND 4.2 1.1 ug/kg
99-87-6 p-Isopropyltoluene ND 4.2 1.1 ug/kg
108-10-1 4-Methyl-2-pentanone ND 21 4.2 ug/kg
74-83-9 Methyl bromide ND 4.2 1.7 ug/kg
74-87-3 Methyl chloride ND 4.2 1.7 ug/kg
75-09-2 Methylene chloride ND 8.3 3.8 ug/kg
78-93-3 Methyl ethyl ketone ND 21 4.2 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 4.2 0.83 ug/kg
91-20-3 Naphthalene ND 4.2 1.7 ug/kg
103-65-1 n-Propylbenzene ND 4.2 0.86 ug/kg
100-42-5 Styrene ND 4.2 0.83 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.2 0.89 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.2 0.83 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.2 0.83 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.2 0.83 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.2 0.87 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.2 1.3 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.2 0.98 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.2 0.90 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.2 0.87 ug/kg
127-18-4 Tetrachloroethylene ND 4.2 0.96 ug/kg
108-88-3 Toluene ND 4.2 0.83 ug/kg
79-01-6 Trichloroethylene ND 4.2 0.83 ug/kg
75-69-4 Trichlorofluoromethane ND 4.2 1.7 ug/kg
75-01-4 Vinyl chloride ND 4.2 0.83 ug/kg
108-05-4 Vinyl Acetate ND 21 3.4 ug/kg
1330-20-7 Xylene (total)ND 12 2.5 ug/kg
m,p-Xylene ND 8.3 1.7 ug/kg
95-47-6 o-Xylene ND 4.2 0.83 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%105% 75-124%
2037-26-5 Toluene-D8 97%100% 75-126%
460-00-4 4-Bromofluorobenzene 105%110% 71-133%
17060-07-0 1,2-Dichloroethane-D4 131%124% 72-135%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-8 (13-15)
Lab Sample ID:FA9018-3 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:83.7
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Confirmation run for internal standard areas.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8 (23-25)
Lab Sample ID:FA9018-4 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:86.7
Project:Gould P-2; Atando Ave, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0062138.D 1 10/15/13 AH n/a n/a VF2001
Run #2
Initial Weight
Run #1 6.23 g
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 46 19 ug/kg
71-43-2 Benzene ND 4.6 0.93 ug/kg
108-86-1 Bromobenzene ND 4.6 1.0 ug/kg
74-97-5 Bromochloromethane ND 4.6 1.3 ug/kg
75-27-4 Bromodichloromethane ND 4.6 1.3 ug/kg
75-25-2 Bromoform ND 4.6 0.93 ug/kg
104-51-8 n-Butylbenzene ND 4.6 1.2 ug/kg
135-98-8 sec-Butylbenzene ND 4.6 1.1 ug/kg
98-06-6 tert-Butylbenzene ND 4.6 1.1 ug/kg
108-90-7 Chlorobenzene ND 4.6 0.93 ug/kg
75-00-3 Chloroethane ND 4.6 1.9 ug/kg
67-66-3 Chloroform ND 4.6 0.93 ug/kg
95-49-8 o-Chlorotoluene ND 4.6 0.93 ug/kg
106-43-4 p-Chlorotoluene ND 4.6 1.1 ug/kg
56-23-5 Carbon tetrachloride ND 4.6 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 4.6 0.93 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.6 1.1 ug/kg
563-58-6 1,1-Dichloropropene ND 4.6 0.93 ug/kg
106-93-4 1,2-Dibromoethane ND 4.6 0.93 ug/kg
107-06-2 1,2-Dichloroethane ND 4.6 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 4.6 0.93 ug/kg
142-28-9 1,3-Dichloropropane ND 4.6 0.93 ug/kg
108-20-3 Di-Isopropyl ether ND 4.6 0.95 ug/kg
594-20-7 2,2-Dichloropropane ND 4.6 0.93 ug/kg
124-48-1 Dibromochloromethane ND 4.6 0.93 ug/kg
75-71-8 Dichlorodifluoromethane ND 4.6 0.93 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.6 0.93 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.6 0.93 ug/kg
541-73-1 m-Dichlorobenzene ND 4.6 0.93 ug/kg
95-50-1 o-Dichlorobenzene ND 4.6 1.0 ug/kg
106-46-7 p-Dichlorobenzene ND 4.6 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.6 0.93 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-8 (23-25)
Lab Sample ID:FA9018-4 Date Sampled:10/10/13
Matrix:SO - Soil Date Received:10/12/13
Method:SW846 8260B Percent Solids:86.7
Project:Gould P-2; Atando Ave, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.6 0.93 ug/kg
64-17-5 Ethyl alcohol ND 370 61 ug/kg
100-41-4 Ethylbenzene ND 4.6 1.0 ug/kg
591-78-6 2-Hexanone ND 23 4.6 ug/kg
98-82-8 Isopropylbenzene ND 4.6 1.2 ug/kg
99-87-6 p-Isopropyltoluene ND 4.6 1.2 ug/kg
108-10-1 4-Methyl-2-pentanone ND 23 4.6 ug/kg
74-83-9 Methyl bromide ND 4.6 1.9 ug/kg
74-87-3 Methyl chloride ND 4.6 1.9 ug/kg
75-09-2 Methylene chloride ND 9.3 4.2 ug/kg
78-93-3 Methyl ethyl ketone ND 23 4.6 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 4.6 0.93 ug/kg
91-20-3 Naphthalene ND 4.6 1.9 ug/kg
103-65-1 n-Propylbenzene ND 4.6 0.95 ug/kg
100-42-5 Styrene ND 4.6 0.93 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.6 0.99 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.6 0.93 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.6 0.93 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.6 0.93 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.6 0.97 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.6 1.5 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.6 1.1 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.6 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.6 0.97 ug/kg
127-18-4 Tetrachloroethylene ND 4.6 1.1 ug/kg
108-88-3 Toluene ND 4.6 0.93 ug/kg
79-01-6 Trichloroethylene ND 4.6 0.93 ug/kg
75-69-4 Trichlorofluoromethane ND 4.6 1.9 ug/kg
75-01-4 Vinyl chloride ND 4.6 0.93 ug/kg
108-05-4 Vinyl Acetate ND 23 3.8 ug/kg
1330-20-7 Xylene (total)ND 14 2.8 ug/kg
m,p-Xylene ND 9.3 1.9 ug/kg
95-47-6 o-Xylene ND 4.6 0.93 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%75-124%
2037-26-5 Toluene-D8 95%75-126%
460-00-4 4-Bromofluorobenzene 104%71-133%
17060-07-0 1,2-Dichloroethane-D4 120%72-135%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
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Page 2 of 2
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GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2000-MB F0062107.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.0 ug/kg
108-86-1 Bromobenzene ND 5.0 1.1 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.4 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.4 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.3 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.2 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.2 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.0 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.2 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg
95-50-1 o-Dichlorobenzene ND 5.0 1.1 ug/kg
106-46-7 p-Dichlorobenzene ND 5.0 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
64-17-5 Ethyl alcohol ND 400 65 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
591-78-6 2-Hexanone ND 25 5.0 ug/kg
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Method Blank Summary Page 2 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2000-MB F0062107.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
CAS No. Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 5.0 1.3 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.1 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 5.0 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.1 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.2 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 4.1 ug/kg
1330-20-7 Xylene (total)ND 15 3.1 ug/kg
m,p-Xylene ND 10 2.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
CAS No. Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 92% 75-124%
2037-26-5 Toluene-D8 98% 75-126%
460-00-4 4-Bromofluorobenzene 106% 71-133%
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2000-MB F0062107.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
CAS No. Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 98% 72-135%
CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q
Total TIC, Volatile 0 ug/kg
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2001-MB F0062136.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.0 ug/kg
108-86-1 Bromobenzene ND 5.0 1.1 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.4 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.4 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.3 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.2 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.2 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.0 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.2 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg
95-50-1 o-Dichlorobenzene ND 5.0 1.1 ug/kg
106-46-7 p-Dichlorobenzene ND 5.0 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
64-17-5 Ethyl alcohol ND 400 65 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
591-78-6 2-Hexanone ND 25 5.0 ug/kg
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Method Blank Summary Page 2 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2001-MB F0062136.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
CAS No. Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 5.0 1.3 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.1 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 5.0 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.1 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.2 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 4.1 ug/kg
1330-20-7 Xylene (total)ND 15 3.1 ug/kg
m,p-Xylene ND 10 2.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
CAS No. Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99% 75-124%
2037-26-5 Toluene-D8 96% 75-126%
460-00-4 4-Bromofluorobenzene 110% 71-133%
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Method Blank Summary Page 3 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2001-MB F0062136.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
CAS No. Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 105% 72-135%
CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q
Total TIC, Volatile a 0 ug/kg
(a) No TICs detected.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC3831-MB C096278.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.0 ug/kg
108-86-1 Bromobenzene ND 5.0 1.1 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.4 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.4 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.3 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.2 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.2 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.0 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.2 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg
95-50-1 o-Dichlorobenzene ND 5.0 1.1 ug/kg
106-46-7 p-Dichlorobenzene ND 5.0 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
64-17-5 Ethyl alcohol ND 400 65 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
591-78-6 2-Hexanone ND 25 5.0 ug/kg
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Method Blank Summary Page 2 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC3831-MB C096278.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
CAS No. Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 5.0 1.3 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.1 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 5.0 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.1 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.2 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 4.1 ug/kg
1330-20-7 Xylene (total)ND 15 3.1 ug/kg
m,p-Xylene ND 10 2.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
CAS No. Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 107% 75-124%
2037-26-5 Toluene-D8 104% 75-126%
460-00-4 4-Bromofluorobenzene 105% 71-133%
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Method Blank Summary Page 3 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC3831-MB C096278.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
CAS No. Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 110% 72-135%
CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q
Total TIC, Volatile a 0 ug/kg
(a) No TICs detected.
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Blank Spike Summary Page 1 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2000-BS F0062106.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
67-64-1 Acetone 250 255 102 61-152
71-43-2 Benzene 50 52.1 104 76-126
108-86-1 Bromobenzene 50 48.6 97 76-122
74-97-5 Bromochloromethane 50 50.3 101 77-120
75-27-4 Bromodichloromethane 50 52.9 106 74-130
75-25-2 Bromoform 50 50.7 101 76-127
104-51-8 n-Butylbenzene 50 53.9 108 71-128
135-98-8 sec-Butylbenzene 50 52.4 105 79-135
98-06-6 tert-Butylbenzene 50 52.4 105 77-133
108-90-7 Chlorobenzene 50 49.6 99 81-129
75-00-3 Chloroethane 50 49.7 99 68-133
67-66-3 Chloroform 50 50.1 100 72-123
95-49-8 o-Chlorotoluene 50 49.5 99 77-129
106-43-4 p-Chlorotoluene 50 50.5 101 80-134
56-23-5 Carbon tetrachloride 50 55.9 112 78-133
75-34-3 1,1-Dichloroethane 50 49.1 98 73-125
75-35-4 1,1-Dichloroethylene 50 53.1 106 81-136
563-58-6 1,1-Dichloropropene 50 51.7 103 75-130
106-93-4 1,2-Dibromoethane 50 48.2 96 77-126
107-06-2 1,2-Dichloroethane 50 50.8 102 74-128
78-87-5 1,2-Dichloropropane 50 52.1 104 74-125
142-28-9 1,3-Dichloropropane 50 47.9 96 76-122
108-20-3 Di-Isopropyl ether 50 53.0 106 75-122
594-20-7 2,2-Dichloropropane 50 57.8 116 77-133
124-48-1 Dibromochloromethane 50 49.2 98 76-127
75-71-8 Dichlorodifluoromethane 50 51.1 102 68-168
156-59-2 cis-1,2-Dichloroethylene 50 50.2 100 74-126
10061-01-5 cis-1,3-Dichloropropene 50 51.1 102 80-123
541-73-1 m-Dichlorobenzene 50 51.9 104 81-129
95-50-1 o-Dichlorobenzene 50 50.8 102 80-129
106-46-7 p-Dichlorobenzene 50 49.5 99 76-130
156-60-5 trans-1,2-Dichloroethylene 50 51.9 104 70-127
10061-02-6 trans-1,3-Dichloropropene 50 49.6 99 75-131
64-17-5 Ethyl alcohol 1000 883 88 53-154
100-41-4 Ethylbenzene 50 49.9 100 77-123
591-78-6 2-Hexanone 250 239 96 72-133
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2000-BS F0062106.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
98-82-8 Isopropylbenzene 50 54.7 109 80-136
99-87-6 p-Isopropyltoluene 50 52.3 105 77-131
108-10-1 4-Methyl-2-pentanone 250 244 98 76-132
74-83-9 Methyl bromide 50 49.8 100 65-139
74-87-3 Methyl chloride 50 49.1 98 71-144
75-09-2 Methylene chloride 50 52.7 105 74-137
78-93-3 Methyl ethyl ketone 250 239 96 75-137
1634-04-4 Methyl Tert Butyl Ether 50 52.4 105 77-120
91-20-3 Naphthalene 50 48.2 96 79-129
103-65-1 n-Propylbenzene 50 50.4 101 80-135
100-42-5 Styrene 50 52.3 105 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 52.8 106 78-126
71-55-6 1,1,1-Trichloroethane 50 53.9 108 70-129
79-34-5 1,1,2,2-Tetrachloroethane 50 47.2 94 71-126
79-00-5 1,1,2-Trichloroethane 50 47.6 95 74-124
87-61-6 1,2,3-Trichlorobenzene 50 51.0 102 77-128
96-18-4 1,2,3-Trichloropropane 50 45.9 92 74-127
120-82-1 1,2,4-Trichlorobenzene 50 52.1 104 78-130
95-63-6 1,2,4-Trimethylbenzene 50 52.8 106 74-123
108-67-8 1,3,5-Trimethylbenzene 50 51.4 103 73-122
127-18-4 Tetrachloroethylene 50 48.4 97 79-130
108-88-3 Toluene 50 51.5 103 76-124
79-01-6 Trichloroethylene 50 51.9 104 75-128
75-69-4 Trichlorofluoromethane 50 46.0 92 73-145
75-01-4 Vinyl chloride 50 47.6 95 76-141
108-05-4 Vinyl Acetate 250 258 103 48-164
1330-20-7 Xylene (total)150 158 105 80-129
m,p-Xylene 100 105 105 80-128
95-47-6 o-Xylene 50 53.2 106 80-132
CAS No. Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 94% 75-124%
2037-26-5 Toluene-D8 99% 75-126%
460-00-4 4-Bromofluorobenzene 101% 71-133%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2000-BS F0062106.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
CAS No. Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 91% 72-135%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2001-BS F0062135.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
67-64-1 Acetone 250 279 112 61-152
71-43-2 Benzene 50 51.2 102 76-126
108-86-1 Bromobenzene 50 49.5 99 76-122
74-97-5 Bromochloromethane 50 50.5 101 77-120
75-27-4 Bromodichloromethane 50 54.5 109 74-130
75-25-2 Bromoform 50 53.9 108 76-127
104-51-8 n-Butylbenzene 50 53.2 106 71-128
135-98-8 sec-Butylbenzene 50 50.4 101 79-135
98-06-6 tert-Butylbenzene 50 51.4 103 77-133
108-90-7 Chlorobenzene 50 48.7 97 81-129
75-00-3 Chloroethane 50 47.3 95 68-133
67-66-3 Chloroform 50 50.1 100 72-123
95-49-8 o-Chlorotoluene 50 49.3 99 77-129
106-43-4 p-Chlorotoluene 50 51.1 102 80-134
56-23-5 Carbon tetrachloride 50 52.3 105 78-133
75-34-3 1,1-Dichloroethane 50 50.8 102 73-125
75-35-4 1,1-Dichloroethylene 50 50.7 101 81-136
563-58-6 1,1-Dichloropropene 50 51.6 103 75-130
106-93-4 1,2-Dibromoethane 50 52.0 104 77-126
107-06-2 1,2-Dichloroethane 50 53.8 108 74-128
78-87-5 1,2-Dichloropropane 50 52.4 105 74-125
142-28-9 1,3-Dichloropropane 50 52.5 105 76-122
108-20-3 Di-Isopropyl ether 50 53.4 107 75-122
594-20-7 2,2-Dichloropropane 50 52.0 104 77-133
124-48-1 Dibromochloromethane 50 53.3 107 76-127
75-71-8 Dichlorodifluoromethane 50 48.1 96 68-168
156-59-2 cis-1,2-Dichloroethylene 50 49.7 99 74-126
10061-01-5 cis-1,3-Dichloropropene 50 54.4 109 80-123
541-73-1 m-Dichlorobenzene 50 51.2 102 81-129
95-50-1 o-Dichlorobenzene 50 51.2 102 80-129
106-46-7 p-Dichlorobenzene 50 49.8 100 76-130
156-60-5 trans-1,2-Dichloroethylene 50 50.5 101 70-127
10061-02-6 trans-1,3-Dichloropropene 50 54.0 108 75-131
64-17-5 Ethyl alcohol 1000 965 97 53-154
100-41-4 Ethylbenzene 50 49.2 98 77-123
591-78-6 2-Hexanone 250 288 115 72-133
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2001-BS F0062135.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
98-82-8 Isopropylbenzene 50 50.8 102 80-136
99-87-6 p-Isopropyltoluene 50 51.1 102 77-131
108-10-1 4-Methyl-2-pentanone 250 279 112 76-132
74-83-9 Methyl bromide 50 46.5 93 65-139
74-87-3 Methyl chloride 50 46.4 93 71-144
75-09-2 Methylene chloride 50 51.8 104 74-137
78-93-3 Methyl ethyl ketone 250 276 110 75-137
1634-04-4 Methyl Tert Butyl Ether 50 52.0 104 77-120
91-20-3 Naphthalene 50 49.5 99 79-129
103-65-1 n-Propylbenzene 50 51.7 103 80-135
100-42-5 Styrene 50 51.0 102 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 50.0 100 78-126
71-55-6 1,1,1-Trichloroethane 50 49.9 100 70-129
79-34-5 1,1,2,2-Tetrachloroethane 50 52.6 105 71-126
79-00-5 1,1,2-Trichloroethane 50 51.8 104 74-124
87-61-6 1,2,3-Trichlorobenzene 50 49.7 99 77-128
96-18-4 1,2,3-Trichloropropane 50 51.0 102 74-127
120-82-1 1,2,4-Trichlorobenzene 50 51.5 103 78-130
95-63-6 1,2,4-Trimethylbenzene 50 51.1 102 74-123
108-67-8 1,3,5-Trimethylbenzene 50 50.9 102 73-122
127-18-4 Tetrachloroethylene 50 48.5 97 79-130
108-88-3 Toluene 50 51.3 103 76-124
79-01-6 Trichloroethylene 50 50.8 102 75-128
75-69-4 Trichlorofluoromethane 50 45.4 91 73-145
75-01-4 Vinyl chloride 50 45.0 90 76-141
108-05-4 Vinyl Acetate 250 305 122 48-164
1330-20-7 Xylene (total)150 149 99 80-129
m,p-Xylene 100 97.8 98 80-128
95-47-6 o-Xylene 50 50.8 102 80-132
CAS No. Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 95% 75-124%
2037-26-5 Toluene-D8 98% 75-126%
460-00-4 4-Bromofluorobenzene 102% 71-133%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2001-BS F0062135.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
CAS No. Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 98% 72-135%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC3831-BS C096277.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
67-64-1 Acetone 250 201 80 61-152
71-43-2 Benzene 50 48.8 98 76-126
108-86-1 Bromobenzene 50 49.6 99 76-122
74-97-5 Bromochloromethane 50 46.6 93 77-120
75-27-4 Bromodichloromethane 50 49.4 99 74-130
75-25-2 Bromoform 50 49.3 99 76-127
104-51-8 n-Butylbenzene 50 51.2 102 71-128
135-98-8 sec-Butylbenzene 50 49.5 99 79-135
98-06-6 tert-Butylbenzene 50 47.9 96 77-133
108-90-7 Chlorobenzene 50 47.6 95 81-129
75-00-3 Chloroethane 50 53.4 107 68-133
67-66-3 Chloroform 50 48.4 97 72-123
95-49-8 o-Chlorotoluene 50 50.6 101 77-129
106-43-4 p-Chlorotoluene 50 50.3 101 80-134
56-23-5 Carbon tetrachloride 50 52.4 105 78-133
75-34-3 1,1-Dichloroethane 50 47.9 96 73-125
75-35-4 1,1-Dichloroethylene 50 51.0 102 81-136
563-58-6 1,1-Dichloropropene 50 49.9 100 75-130
106-93-4 1,2-Dibromoethane 50 47.6 95 77-126
107-06-2 1,2-Dichloroethane 50 47.4 95 74-128
78-87-5 1,2-Dichloropropane 50 49.8 100 74-125
142-28-9 1,3-Dichloropropane 50 47.0 94 76-122
108-20-3 Di-Isopropyl ether 50 49.4 99 75-122
594-20-7 2,2-Dichloropropane 50 53.2 106 77-133
124-48-1 Dibromochloromethane 50 47.7 95 76-127
75-71-8 Dichlorodifluoromethane 50 54.6 109 68-168
156-59-2 cis-1,2-Dichloroethylene 50 48.1 96 74-126
10061-01-5 cis-1,3-Dichloropropene 50 50.2 100 80-123
541-73-1 m-Dichlorobenzene 50 49.2 98 81-129
95-50-1 o-Dichlorobenzene 50 48.6 97 80-129
106-46-7 p-Dichlorobenzene 50 48.2 96 76-130
156-60-5 trans-1,2-Dichloroethylene 50 48.1 96 70-127
10061-02-6 trans-1,3-Dichloropropene 50 47.0 94 75-131
64-17-5 Ethyl alcohol 1000 990 99 53-154
100-41-4 Ethylbenzene 50 48.9 98 77-123
591-78-6 2-Hexanone 250 228 91 72-133
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC3831-BS C096277.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
98-82-8 Isopropylbenzene 50 50.1 100 80-136
99-87-6 p-Isopropyltoluene 50 51.5 103 77-131
108-10-1 4-Methyl-2-pentanone 250 232 93 76-132
74-83-9 Methyl bromide 50 61.0 122 65-139
74-87-3 Methyl chloride 50 53.9 108 71-144
75-09-2 Methylene chloride 50 47.4 95 74-137
78-93-3 Methyl ethyl ketone 250 216 86 75-137
1634-04-4 Methyl Tert Butyl Ether 50 49.6 99 77-120
91-20-3 Naphthalene 50 48.0 96 79-129
103-65-1 n-Propylbenzene 50 50.5 101 80-135
100-42-5 Styrene 50 51.9 104 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 46.0 92 78-126
71-55-6 1,1,1-Trichloroethane 50 51.9 104 70-129
79-34-5 1,1,2,2-Tetrachloroethane 50 47.8 96 71-126
79-00-5 1,1,2-Trichloroethane 50 46.5 93 74-124
87-61-6 1,2,3-Trichlorobenzene 50 48.0 96 77-128
96-18-4 1,2,3-Trichloropropane 50 46.3 93 74-127
120-82-1 1,2,4-Trichlorobenzene 50 47.5 95 78-130
95-63-6 1,2,4-Trimethylbenzene 50 50.2 100 74-123
108-67-8 1,3,5-Trimethylbenzene 50 49.9 100 73-122
127-18-4 Tetrachloroethylene 50 45.1 90 79-130
108-88-3 Toluene 50 46.4 93 76-124
79-01-6 Trichloroethylene 50 48.3 97 75-128
75-69-4 Trichlorofluoromethane 50 52.6 105 73-145
75-01-4 Vinyl chloride 50 54.4 109 76-141
108-05-4 Vinyl Acetate 250 213 85 48-164
1330-20-7 Xylene (total)150 150 100 80-129
m,p-Xylene 100 100 100 80-128
95-47-6 o-Xylene 50 49.9 100 80-132
CAS No. Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100% 75-124%
2037-26-5 Toluene-D8 100% 75-126%
460-00-4 4-Bromofluorobenzene 105% 71-133%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC3831-BS C096277.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
CAS No. Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 99% 72-135%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA8923-12MS F0062127.D 1 10/14/13 AH n/a n/a VF2000
FA8923-12MSD F0062128.D 1 10/14/13 AH n/a n/a VF2000
FA8923-12 F0062108.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
FA8923-12 Spike MS MS MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD
67-64-1 Acetone 36.6 J 340 331 87 399 104 19 61-152/27
71-43-2 Benzene ND 68 50.1 74* 64.6 93 25 76-126/26
108-86-1 Bromobenzene ND 68 41.1 60* 57.6 83 33* 76-122/32
74-97-5 Bromochloromethane ND 68 50.3 74* 63.1 91 23 77-120/24
75-27-4 Bromodichloromethane ND 68 52.9 78 68.6 99 26* 74-130/25
75-25-2 Bromoform ND 68 49.4 73* 64.6 93 27* 76-127/26
104-51-8 n-Butylbenzene ND 68 32.4 48* 45.6 66*34 71-128/35
135-98-8 sec-Butylbenzene ND 68 36.8 54* 51.9 75*34 79-135/34
98-06-6 tert-Butylbenzene ND 68 39.8 59* 57.8 83 37* 77-133/34
108-90-7 Chlorobenzene ND 68 46.5 68* 62.3 90 29 81-129/29
75-00-3 Chloroethane ND 68 48.4 71 60.9 88 23 68-133/29
67-66-3 Chloroform ND 68 50.3 74 63.6 92 23 72-123/26
95-49-8 o-Chlorotoluene ND 68 40.6 60* 58.6 84 36* 77-129/33
106-43-4 p-Chlorotoluene ND 68 42.4 62* 60.0 86 34* 80-134/33
56-23-5 Carbon tetrachloride ND 68 50.6 74* 64.2 92 24 78-133/29
75-34-3 1,1-Dichloroethane ND 68 52.6 77 64.0 92 20 73-125/27
75-35-4 1,1-Dichloroethylene ND 68 57.6 85 67.6 97 16 81-136/28
563-58-6 1,1-Dichloropropene ND 68 52.2 77 64.2 92 21 75-130/28
106-93-4 1,2-Dibromoethane ND 68 49.4 73* 63.5 91 25 77-126/26
107-06-2 1,2-Dichloroethane ND 68 56.8 84 70.1 101 21 74-128/23
78-87-5 1,2-Dichloropropane ND 68 50.3 74 65.1 94 26* 74-125/25
142-28-9 1,3-Dichloropropane ND 68 49.1 72* 67.3 97 31* 76-122/26
108-20-3 Di-Isopropyl ether ND 68 53.9 79 67.4 97 22 75-122/25
594-20-7 2,2-Dichloropropane ND 68 50.2 74* 63.0 91 23 77-133/28
124-48-1 Dibromochloromethane ND 68 48.8 72* 64.2 92 27 76-127/27
75-71-8 Dichlorodifluoromethane ND 68 50.6 74 58.9 85 15 68-168/29
156-59-2 cis-1,2-Dichloroethylene ND 68 47.7 70* 58.9 85 21 74-126/26
10061-01-5 cis-1,3-Dichloropropene ND 68 47.6 70* 63.0 91 28* 80-123/26
541-73-1 m-Dichlorobenzene ND 68 39.9 59* 55.8 80*33 81-129/33
95-50-1 o-Dichlorobenzene ND 68 41.4 61* 56.6 81 31 80-129/32
106-46-7 p-Dichlorobenzene ND 68 38.0 56* 51.4 74*30 76-130/32
156-60-5 trans-1,2-Dichloroethylene ND 68 51.4 76 62.0 89 19 70-127/27
10061-02-6 trans-1,3-Dichloropropene ND 68 49.1 72* 62.9 91 25 75-131/28
64-17-5 Ethyl alcohol ND 1360 982 72 1310 94 29 53-154/42
100-41-4 Ethylbenzene ND 68 43.7 64* 58.7 85 29 77-123/31
591-78-6 2-Hexanone ND 340 293 86 384 111 27* 72-133/26
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA8923-12MS F0062127.D 1 10/14/13 AH n/a n/a VF2000
FA8923-12MSD F0062128.D 1 10/14/13 AH n/a n/a VF2000
FA8923-12 F0062108.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
FA8923-12 Spike MS MS MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD
98-82-8 Isopropylbenzene ND 68 43.5 64* 58.6 84 30 80-136/32
99-87-6 p-Isopropyltoluene ND 68 35.3 52* 50.7 73*36* 77-131/34
108-10-1 4-Methyl-2-pentanone ND 340 295 87 368 106 22 76-132/26
74-83-9 Methyl bromide ND 68 51.0 75 61.1 88 18 65-139/31
74-87-3 Methyl chloride ND 68 48.8 72 60.2 87 21 71-144/27
75-09-2 Methylene chloride ND 68 63.4 93 78.3 113 21 74-137/28
78-93-3 Methyl ethyl ketone ND 340 307 90 378 109 21 75-137/25
1634-04-4 Methyl Tert Butyl Ether ND 68 54.8 81 66.7 96 20 77-120/24
91-20-3 Naphthalene ND 68 38.6 57* 45.5 66*16 79-129/33
103-65-1 n-Propylbenzene ND 68 40.9 60* 58.9 85 36* 80-135/33
100-42-5 Styrene ND 68 41.8 61* 56.8 82 30 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 68 48.4 71* 65.0 94 29* 78-126/27
71-55-6 1,1,1-Trichloroethane ND 68 53.5 79 66.5 96 22 70-129/27
79-34-5 1,1,2,2-Tetrachloroethane ND 68 49.0 72 66.5 96 30 71-126/30
79-00-5 1,1,2-Trichloroethane ND 68 49.7 73* 63.3 91 24 74-124/28
87-61-6 1,2,3-Trichlorobenzene ND 68 33.0 49* 39.1 56*17 77-128/35
96-18-4 1,2,3-Trichloropropane ND 68 50.1 74 66.9 96 29* 74-127/27
120-82-1 1,2,4-Trichlorobenzene ND 68 33.7 50* 41.0 59*20 78-130/34
95-63-6 1,2,4-Trimethylbenzene 2.8 J 68 40.2 55* 56.1 77 33 74-123/34
108-67-8 1,3,5-Trimethylbenzene 1.6 J 68 37.8 53* 55.2 77 37* 73-122/33
127-18-4 Tetrachloroethylene 47.5 68 46.4 -2* 65.5 26*34* 79-130/31
108-88-3 Toluene 119 68 55.1 -94* 83.4 -51*41* 76-124/30
79-01-6 Trichloroethylene ND 68 49.2 72* 64.2 92 26 75-128/27
75-69-4 Trichlorofluoromethane ND 68 45.7 67* 55.3 80 19 73-145/31
75-01-4 Vinyl chloride ND 68 47.2 69* 56.3 81 18 76-141/27
108-05-4 Vinyl Acetate ND 340 171 50 145 42*16 48-164/37
1330-20-7 Xylene (total)6.5 J 204 136 63* 187 87 32* 80-129/30
m,p-Xylene 4.7 J 136 90.3 63* 125 87 32* 80-128/30
95-47-6 o-Xylene 1.8 J 68 45.6 64* 62.5 87 31* 80-132/30
CAS No. Surrogate Recoveries MS MSD FA8923-12 Limits
1868-53-7 Dibromofluoromethane 97%93%96% 75-124%
2037-26-5 Toluene-D8 95%97%101% 75-126%
460-00-4 4-Bromofluorobenzene 97%102%112% 71-133%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA8923-12MS F0062127.D 1 10/14/13 AH n/a n/a VF2000
FA8923-12MSD F0062128.D 1 10/14/13 AH n/a n/a VF2000
FA8923-12 F0062108.D 1 10/14/13 AH n/a n/a VF2000
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-1, FA9018-2
CAS No. Surrogate Recoveries MS MSD FA8923-12 Limits
17060-07-0 1,2-Dichloroethane-D4 100%97%99% 72-135%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9018-4MS F0062156.D 1 10/15/13 AH n/a n/a VF2001
FA9018-4MSD F0062157.D 1 10/15/13 AH n/a n/a VF2001
FA9018-4 F0062138.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
FA9018-4 Spike MS MS MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD
67-64-1 Acetone ND 367 444 121 458 125 3 61-152/27
71-43-2 Benzene ND 73.4 63.0 86 72.4 99 14 76-126/26
108-86-1 Bromobenzene ND 73.4 56.2 77 65.5 89 15 76-122/32
74-97-5 Bromochloromethane ND 73.4 62.4 85 75.2 103 19 77-120/24
75-27-4 Bromodichloromethane ND 73.4 69.9 95 75.9 104 8 74-130/25
75-25-2 Bromoform ND 73.4 68.2 93 74.0 101 8 76-127/26
104-51-8 n-Butylbenzene ND 73.4 56.0 76 65.5 89 16 71-128/35
135-98-8 sec-Butylbenzene ND 73.4 60.0 82 70.2 96 16 79-135/34
98-06-6 tert-Butylbenzene ND 73.4 61.3 84 69.5 95 13 77-133/34
108-90-7 Chlorobenzene ND 73.4 62.3 85 73.2 100 16 81-129/29
75-00-3 Chloroethane ND 73.4 54.7 75 72.3 99 28 68-133/29
67-66-3 Chloroform ND 73.4 64.2 87 76.7 105 18 72-123/26
95-49-8 o-Chlorotoluene ND 73.4 58.5 80 70.2 96 18 77-129/33
106-43-4 p-Chlorotoluene ND 73.4 63.1 86 74.0 101 16 80-134/33
56-23-5 Carbon tetrachloride ND 73.4 66.8 91 75.4 103 12 78-133/29
75-34-3 1,1-Dichloroethane ND 73.4 65.5 89 76.7 105 16 73-125/27
75-35-4 1,1-Dichloroethylene ND 73.4 72.4 99 80.0 109 10 81-136/28
563-58-6 1,1-Dichloropropene ND 73.4 65.1 89 78.8 108 19 75-130/28
106-93-4 1,2-Dibromoethane ND 73.4 64.8 88 71.6 98 10 77-126/26
107-06-2 1,2-Dichloroethane ND 73.4 71.0 97 82.2 112 15 74-128/23
78-87-5 1,2-Dichloropropane ND 73.4 66.4 90 74.7 102 12 74-125/25
142-28-9 1,3-Dichloropropane ND 73.4 63.5 87 72.2 99 13 76-122/26
108-20-3 Di-Isopropyl ether ND 73.4 66.9 91 77.9 106 15 75-122/25
594-20-7 2,2-Dichloropropane ND 73.4 64.1 87 73.8 101 14 77-133/28
124-48-1 Dibromochloromethane ND 73.4 64.6 88 72.8 99 12 76-127/27
75-71-8 Dichlorodifluoromethane ND 73.4 58.3 79 68.3 93 16 68-168/29
156-59-2 cis-1,2-Dichloroethylene ND 73.4 61.0 83 71.1 97 15 74-126/26
10061-01-5 cis-1,3-Dichloropropene ND 73.4 63.6 87 69.9 96 9 80-123/26
541-73-1 m-Dichlorobenzene ND 73.4 60.7 83 70.5 96 15 81-129/33
95-50-1 o-Dichlorobenzene ND 73.4 60.8 83 70.7 97 15 80-129/32
106-46-7 p-Dichlorobenzene ND 73.4 57.0 78 64.8 89 13 76-130/32
156-60-5 trans-1,2-Dichloroethylene ND 73.4 63.9 87 74.3 102 15 70-127/27
10061-02-6 trans-1,3-Dichloropropene ND 73.4 66.0 90 75.4 103 13 75-131/28
64-17-5 Ethyl alcohol ND 1470 1320 90 1690 115 25 53-154/42
100-41-4 Ethylbenzene ND 73.4 61.1 83 70.6 96 14 77-123/31
591-78-6 2-Hexanone ND 367 419 114 425 116 1 72-133/26
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9018-4MS F0062156.D 1 10/15/13 AH n/a n/a VF2001
FA9018-4MSD F0062157.D 1 10/15/13 AH n/a n/a VF2001
FA9018-4 F0062138.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
FA9018-4 Spike MS MS MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD
98-82-8 Isopropylbenzene ND 73.4 63.0 86 72.3 99 14 80-136/32
99-87-6 p-Isopropyltoluene ND 73.4 57.1 78 66.9 91 16 77-131/34
108-10-1 4-Methyl-2-pentanone ND 367 406 111 406 111 0 76-132/26
74-83-9 Methyl bromide ND 73.4 59.4 81 70.9 97 18 65-139/31
74-87-3 Methyl chloride ND 73.4 59.4 81 71.0 97 18 71-144/27
75-09-2 Methylene chloride ND 73.4 70.5 96 78.9 108 11 74-137/28
78-93-3 Methyl ethyl ketone ND 367 414 113 440 120 6 75-137/25
1634-04-4 Methyl Tert Butyl Ether ND 73.4 66.6 91 73.8 101 10 77-120/24
91-20-3 Naphthalene ND 73.4 56.4 77* 60.3 82 7 79-129/33
103-65-1 n-Propylbenzene ND 73.4 60.3 82 71.6 98 17 80-135/33
100-42-5 Styrene ND 73.4 59.3 81 68.8 94 15 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 73.4 64.8 88 73.5 100 13 78-126/27
71-55-6 1,1,1-Trichloroethane ND 73.4 66.5 91 78.3 107 16 70-129/27
79-34-5 1,1,2,2-Tetrachloroethane ND 73.4 65.2 89 72.4 99 10 71-126/30
79-00-5 1,1,2-Trichloroethane ND 73.4 64.3 88 72.8 99 12 74-124/28
87-61-6 1,2,3-Trichlorobenzene ND 73.4 51.2 70* 56.7 77 10 77-128/35
96-18-4 1,2,3-Trichloropropane ND 73.4 62.9 86 70.0 96 11 74-127/27
120-82-1 1,2,4-Trichlorobenzene ND 73.4 52.8 72* 61.5 84 15 78-130/34
95-63-6 1,2,4-Trimethylbenzene ND 73.4 57.1 78 66.6 91 15 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 73.4 53.2 73 66.4 91 22 73-122/33
127-18-4 Tetrachloroethylene ND 73.4 56.4 77* 65.6 90 15 79-130/31
108-88-3 Toluene ND 73.4 61.5 84 70.6 96 14 76-124/30
79-01-6 Trichloroethylene ND 73.4 63.9 87 73.0 100 13 75-128/27
75-69-4 Trichlorofluoromethane ND 73.4 56.8 77 64.3 88 12 73-145/31
75-01-4 Vinyl chloride ND 73.4 55.0 75* 66.3 91 19 76-141/27
108-05-4 Vinyl Acetate ND 367 437 119 489 134 11 48-164/37
1330-20-7 Xylene (total)ND 220 192 87 220 100 14 80-129/30
m,p-Xylene ND 147 129 88 145 99 12 80-128/30
95-47-6 o-Xylene ND 73.4 63.6 87 74.5 102 16 80-132/30
CAS No. Surrogate Recoveries MS MSD FA9018-4 Limits
1868-53-7 Dibromofluoromethane 98%100%104% 75-124%
2037-26-5 Toluene-D8 96%97%95% 75-126%
460-00-4 4-Bromofluorobenzene 95%98%104% 71-133%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9018-4MS F0062156.D 1 10/15/13 AH n/a n/a VF2001
FA9018-4MSD F0062157.D 1 10/15/13 AH n/a n/a VF2001
FA9018-4 F0062138.D 1 10/15/13 AH n/a n/a VF2001
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-4
CAS No. Surrogate Recoveries MS MSD FA9018-4 Limits
17060-07-0 1,2-Dichloroethane-D4 102%102%120% 72-135%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9018-3MS C096299.D 1 10/17/13 AH n/a n/a VC3831
FA9018-3MSD C096300.D 1 10/17/13 AH n/a n/a VC3831
FA9018-3 C096280.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
FA9018-3 Spike MS MS MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD
67-64-1 Acetone ND 343 361 105 352 102 3 61-152/27
71-43-2 Benzene ND 68.5 54.4 79 52.5 76 4 76-126/26
108-86-1 Bromobenzene ND 68.5 42.3 62* 37.6 55*12 76-122/32
74-97-5 Bromochloromethane ND 68.5 60.8 89 55.5 80 9 77-120/24
75-27-4 Bromodichloromethane ND 68.5 54.5 80 53.4 77 2 74-130/25
75-25-2 Bromoform ND 68.5 50.3 73* 49.4 72*2 76-127/26
104-51-8 n-Butylbenzene ND 68.5 22.0 32* 18.5 27*17 71-128/35
135-98-8 sec-Butylbenzene ND 68.5 28.8 42* 24.6 36*16 79-135/34
98-06-6 tert-Butylbenzene ND 68.5 32.6 48* 26.8 39*20 77-133/34
108-90-7 Chlorobenzene ND 68.5 43.4 63* 39.9 58*8 81-129/29
75-00-3 Chloroethane ND 68.5 59.5 87 62.1 90 4 68-133/29
67-66-3 Chloroform ND 68.5 57.1 83 55.0 80 4 72-123/26
95-49-8 o-Chlorotoluene ND 68.5 35.8 52* 30.5 44*16 77-129/33
106-43-4 p-Chlorotoluene ND 68.5 34.5 50* 29.6 43*15 80-134/33
56-23-5 Carbon tetrachloride ND 68.5 50.1 73* 50.8 74*1 78-133/29
75-34-3 1,1-Dichloroethane ND 68.5 57.3 84 56.0 81 2 73-125/27
75-35-4 1,1-Dichloroethylene ND 68.5 57.6 84 59.6 86 3 81-136/28
563-58-6 1,1-Dichloropropene ND 68.5 50.6 74* 46.9 68*8 75-130/28
106-93-4 1,2-Dibromoethane ND 68.5 56.1 82 52.4 76*7 77-126/26
107-06-2 1,2-Dichloroethane ND 68.5 60.4 88 56.5 82 7 74-128/23
78-87-5 1,2-Dichloropropane ND 68.5 57.5 84 54.9 80 5 74-125/25
142-28-9 1,3-Dichloropropane ND 68.5 55.2 81 51.8 75*6 76-122/26
108-20-3 Di-Isopropyl ether ND 68.5 62.3 91 61.1 89 2 75-122/25
594-20-7 2,2-Dichloropropane ND 68.5 48.5 71* 48.8 71*1 77-133/28
124-48-1 Dibromochloromethane ND 68.5 52.3 76 49.1 71*6 76-127/27
75-71-8 Dichlorodifluoromethane ND 68.5 56.3 82 60.6 88 7 68-168/29
156-59-2 cis-1,2-Dichloroethylene ND 68.5 54.4 79 53.5 78 2 74-126/26
10061-01-5 cis-1,3-Dichloropropene ND 68.5 48.0 70* 46.6 68*3 80-123/26
541-73-1 m-Dichlorobenzene ND 68.5 35.4 52* 30.4 44*15 81-129/33
95-50-1 o-Dichlorobenzene ND 68.5 39.6 58* 34.7 50*13 80-129/32
106-46-7 p-Dichlorobenzene ND 68.5 33.2 48* 28.6 41*15 76-130/32
156-60-5 trans-1,2-Dichloroethylene ND 68.5 52.8 77 51.6 75 2 70-127/27
10061-02-6 trans-1,3-Dichloropropene ND 68.5 49.8 73* 46.6 68*7 75-131/28
64-17-5 Ethyl alcohol ND 1370 1320 96 1190 86 10 53-154/42
100-41-4 Ethylbenzene ND 68.5 37.5 55* 33.3 48*12 77-123/31
591-78-6 2-Hexanone ND 343 302 88 278 81 8 72-133/26
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9018-3MS C096299.D 1 10/17/13 AH n/a n/a VC3831
FA9018-3MSD C096300.D 1 10/17/13 AH n/a n/a VC3831
FA9018-3 C096280.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
FA9018-3 Spike MS MS MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD
98-82-8 Isopropylbenzene ND 68.5 34.2 50* 30.4 44*12 80-136/32
99-87-6 p-Isopropyltoluene ND 68.5 27.0 39* 23.3 34*15 77-131/34
108-10-1 4-Methyl-2-pentanone ND 343 341 100 314 91 8 76-132/26
74-83-9 Methyl bromide ND 68.5 61.1 89 69.7 101 13 65-139/31
74-87-3 Methyl chloride ND 68.5 60.3 88 65.0 94 8 71-144/27
75-09-2 Methylene chloride ND 68.5 56.6 83 57.1 83 1 74-137/28
78-93-3 Methyl ethyl ketone ND 343 343 100 311 90 10 75-137/25
1634-04-4 Methyl Tert Butyl Ether ND 68.5 63.4 93 63.6 92 0 77-120/24
91-20-3 Naphthalene ND 68.5 45.9 67* 39.5 57*15 79-129/33
103-65-1 n-Propylbenzene ND 68.5 32.0 47* 27.5 40*15 80-135/33
100-42-5 Styrene ND 68.5 37.4 55* 33.1 48*12 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 68.5 49.5 72* 45.8 66*8 78-126/27
71-55-6 1,1,1-Trichloroethane ND 68.5 57.2 83 57.7 84 1 70-129/27
79-34-5 1,1,2,2-Tetrachloroethane ND 68.5 59.6 87 55.0 80 8 71-126/30
79-00-5 1,1,2-Trichloroethane ND 68.5 57.3 84 54.8 79 4 74-124/28
87-61-6 1,2,3-Trichlorobenzene ND 68.5 33.7 49* 28.4 41*17 77-128/35
96-18-4 1,2,3-Trichloropropane ND 68.5 61.6 90 56.6 82 8 74-127/27
120-82-1 1,2,4-Trichlorobenzene ND 68.5 31.9 47* 26.9 39*17 78-130/34
95-63-6 1,2,4-Trimethylbenzene ND 68.5 32.4 47* 27.7 40*16 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 68.5 31.8 46* 27.2 39*16 73-122/33
127-18-4 Tetrachloroethylene ND 68.5 57.0 83 50.7 73*12 79-130/31
108-88-3 Toluene ND 68.5 46.3 68* 41.8 61*10 76-124/30
79-01-6 Trichloroethylene ND 68.5 51.2 75 47.3 69*8 75-128/27
75-69-4 Trichlorofluoromethane ND 68.5 57.0 83 59.5 86 4 73-145/31
75-01-4 Vinyl chloride ND 68.5 62.6 91 65.0 94 4 76-141/27
108-05-4 Vinyl Acetate ND 343 27.5 8* 21.5 6*24 48-164/37
1330-20-7 Xylene (total)ND 206 117 57* 104 50*12 80-129/30
m,p-Xylene ND 137 76.3 56* 67.7 49*12 80-128/30
95-47-6 o-Xylene ND 68.5 40.6 59* 36.4 53*11 80-132/30
CAS No. Surrogate Recoveries MS MSD FA9018-3 Limits
1868-53-7 Dibromofluoromethane 103%97%115% 75-124%
2037-26-5 Toluene-D8 104%103%97% 75-126%
460-00-4 4-Bromofluorobenzene 105%103%105% 71-133%
* = Outside of Control Limits.
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Job Number:FA9018
Account:HRPASCG HRP Associates, Inc
Project:Gould P-2; Atando Ave, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9018-3MS C096299.D 1 10/17/13 AH n/a n/a VC3831
FA9018-3MSD C096300.D 1 10/17/13 AH n/a n/a VC3831
FA9018-3 C096280.D 1 10/16/13 AH n/a n/a VC3831
The QC reported here applies to the following samples:Method: SW846 8260B
FA9018-3
CAS No. Surrogate Recoveries MS MSD FA9018-3 Limits
17060-07-0 1,2-Dichloroethane-D4 96%97%131% 72-135%
* = Outside of Control Limits.
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HRP Associates, Inc.
ATTACHMENT B

SOIL BORING LOGS

Sampler
Type
trace: 0 to 10% some: O.D. (inch)
little: 10 to 20% and: I.D. (inch)
Sampler
Blows per
6"
Recov. (ft) Moisture Soil Type
Contact Interval
(ft)
from to Depth Reading Interval ID
0-0.2' bgs:1 0.8
0 5 5 dry 2 0.8
.02-0.5' bgs:3 0.8
5 10 5 dry 4 0.8
0.5'-1.2' bgs 5 1.0
10 15 5 dry 6 0.8
1.2-5' bgs 7 0.8
15 20 5 dry/damp 8 0.8
5-13' bgs tan, lean clay, slightly damp 9 0.9
20 25 5 damp/wet 10 0.9
13-15' bgs 11 1.0
25 30 5 wet 12 1.7
15-18' bgs 13 1.0
14 1.0
18-20' bgs 15 1.0
16 0.6
20-25' bgs:17 0.8
18 0.7
25-30' bgs:19 0.8
20 0.6
21 0.6
22 Wet
23 Wet
24 Wet
from to
Screen
Material
4.75" 2" SCH. 40 PVC 2"PVC 10 slot
from to
# Blows/ft
very loose 0-2 very soft
loose 3-4 soft
medium dens 5-8 medium stiff
dense 15-Sep stiff
very dense 16-30 very stiff
31+hard

tan clay with some sand, transitions into wet
sediments at 22'
sandy clay, few mica grains, fine to med grained,
tan, wet, no odor
Screen Slot Size
Cohesive Consistence
PID (ppm)
Grass/A horizon
red/tan mottled lean clay, some black mineral
banding, dry no odor
Material
* Well installed at 30 ft
B horizon
E horizon, visible leaching to clay below
clayey sand, white and brown mottling, sand is
fine to med grained, no odors
tan/yellow lean clay, similar to 5-13' bgs, damp,
no odor
Same clayey sand as above, damp, no odor
OH (Organic Clay / Silt of High Plasticity
Monitoring Well Details
ML (Silt)
CL (Lean Clay)
GW (Well-Graded Gravel)
GP (Poorly Graded Gravel) SM (Silty Sand)
SP (Poorly Graded Sand)
OL (Organic Clay / Silt of Low Plasticity)
PT (Highly Organic Soil / Peat)
MH (Elastic Silt) SW (Well-Graded Sand)
Test Boring/Monitor Well ID: MW-6
Date:10/10/2013
35 to 50%
Soil Description (proportions, grain size, etc.)
20 to 35%
Sampler Depth
interval (ft)
Depth to Bedrock:
HRP# GOU4000.GW
Project: Gould Property facility
Location: Charlotte, NC
HRP Associates, Inc.
DRILLING/SOIL LOG
Sheet No. _1___ of _1___
Rig Type: Geoprobe 772ODT
Hammer (weight [lb] / fall [inches])
Core Barrel
Driller: Probe-Tech
Ground Elevation:
Total Boring Depth:
HRP Rep. Salley Gould
Soil Sample Details
Casing
PROPORTIONS
30-49
50+
5-9
# Blows/ft
0-4
Penetration Resistance-140 lb./30" on 2" O.D. sampler
Cohesionless Density
Borehole Diam. (in.)Screen Diam. (in.)
10-29
SC (Clayey Sand)
GC (Clayey Gravel)
GM ( Silty Gravel)
ANNULAR FILL MATERIALSSOIL TYPE
CH (Fat Clay)
Riser
Material
Riser Diam.
(in.)Casing Diam. (in.) Casing Material
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\Data\Soil Logs
Sampler
Type
trace: 0 to 10% some: O.D. (inch)
little: 10 to 20% and: I.D. (inch)
Sampler Blows per 6"Recov. (ft) Moisture Soil Type
Contact Interval (ft)
from to Depth Reading Interval ID
0-0.2' bgs:1 0.4
0 5 4.5 dry 2 0.4
.02-1' bgs:3 0.3
5 10 5 dry 4 0.3
1'-4' bgs 5 0.4
10 15 5 dry 6 0.3
4-5' bgs red/orange mottled clay, dry, no odor 7 0.4
15 20 3.5 dry 8 0.5
5-8.5' bgs brown/tan clay, few small gravels, very tight 9 0.4
10 0.5
8.5-9' bgs 11 0.6
12 0.7
9-10' bgs 13 0.6
14 0.6
10-14' bgs 15 1.7
16 1.7
14-15' bgs:17 1.8
18 1.0
15-17' bgs:19 1.4
20 2.8
17-19 21 1.9
22 2.8
19-23 23 2.4
from to
Screen
Material
4.75" 2" SCH. 40 PVC 2" PVC 10 slot
from to
# Blows/ft
very loose 0-2 very soft
loose 3-4 soft
medium dens 5-8 medium stiff
dense 15-Sep stiff
very dense 16-30 very stiff
31+hard

MH (Elastic Silt) SW (Well-Graded Sand)50+
ML (Silt)
GP (Poorly Graded Gravel) SM (Silty Sand)10-29
GW (Well-Graded Gravel)SP (Poorly Graded Sand)30-49
GC (Clayey Gravel)PT (Highly Organic Soil / Peat)0-4
GM ( Silty Gravel)SC (Clayey Sand)5-9
CL (Lean Clay)OL (Organic Clay / Silt of Low Plasticity)# Blows/ft
SOIL TYPE ANNULAR FILL MATERIALS Penetration Resistance-140 lb./30" on 2" O.D. sampler
CH (Fat Clay)OH (Organic Clay / Silt of High Plasticity)Material Cohesionless Density Cohesive Consistence
Monitoring Well Details
Borehole Diam. (in.) Casing Diam. (in.) Casing Material
Riser Diam.
(in.)
Riser
Material Screen Diam. (in.) Screen Slot Size
gravel/asphalt
clayey silt, tan/yellow some gravels, clay content
decreases with depth
gravel layer transitions into silty clay, dlighlty
damp, no odors
red fat clay, very compact, very
tight, dry, no odors
red/slightly orange silty clay, few small gravels,
dry, no odor
brown/tan clay, some gravels, dry, no odors
tan clayey silt, very tioght, dry, no odors
large/med sized gravels, in clay matrix,
transitions to brown clay
tran silt, dry, no odors
* Well installed at 28.5 ft bgs
clayey silt, little sand at 23' transitions into very
tight red/orange clay, dry, no odors
**macrocores hit refusal at 23' bgs
Depth to Bedrock:35 to 50%
Sampler Depth
interval (ft)Soil Description (proportions, grain size, etc.) PID (ppm) Soil Sample Details
Ground Elevation:PROPORTIONS
Total Boring Depth:20 to 35%
Date:10/10/2013 Hammer (weight [lb] / fall [inches])Driller: Probe-Tech
HRP Rep. Salley Gould Casing Core Barrel
Project: Gould Property facility HRP Associates, Inc.Test Boring/Monitor Well ID: MW-7
Location: Charlotte, NC DRILLING/SOIL LOG
HRP# GOU4000.GW Sheet No. _1___ of _1___
Rig Type: Geoprobe 772ODT
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\Data\Soil Logs
Sampler
Type
trace: 0 to 10% some: O.D. (inch)
little: 10 to 20% and: I.D. (inch)
Sampler Blows per 6"Recov. (ft) Moisture Soil Type
Contact Interval (ft)
from to Depth Reading Interval ID
0-0.2' bgs:1 0.5
0 5 2 dry 2 0.6
.02-5' bgs:3 0.6
5 10 4 dry 4 0.7
5 0.6
10 15 3.5 dry 5-10' bgs:6 0.7
7 0.7
15 20 4.5 dry/damp 8 0.7
10-15' bgs:9 0.7
20 25 2 damp/wet 10 0.7
11 0.7
15-20' bgs:12 0.6
13 0.6
14 0.6
20-25' bgs:15 0.7
16 0.6
17 0.6
25-30' bgs 18 0.7
19 0.7
20 0.7
21 0.6
22 0.6
23 0.7
24 0.6
25 0.7
from to
Screen
Material
4.75" 2" SCH. 40 PVC 2" PVC 10 slot
from to
# Blows/ft
very loose 0-2 very soft
loose 3-4 soft
medium dens 5-8 medium stiff
dense 15-Sep stiff
very dense 16-30 very stiff
31+hard

MH (Elastic Silt) SW (Well-Graded Sand)50+
ML (Silt)
GP (Poorly Graded Gravel) SM (Silty Sand)10-29
GW (Well-Graded Gravel)SP (Poorly Graded Sand)30-49
GC (Clayey Gravel)PT (Highly Organic Soil / Peat)0-4
GM ( Silty Gravel)SC (Clayey Sand)5-9
CL (Lean Clay)OL (Organic Clay / Silt of Low Plasticity)# Blows/ft
SOIL TYPE ANNULAR FILL MATERIALS Penetration Resistance-140 lb./30" on 2" O.D. sampler
CH (Fat Clay)OH (Organic Clay / Silt of High Plasticity)Material Cohesionless Density Cohesive Consistence
Monitoring Well Details
Borehole Diam. (in.) Casing Diam. (in.) Casing Material
Riser Diam.
(in.)
Riser
Material Screen Diam. (in.) Screen Slot Size
Asphalt
fill dirt, red clay, damp, no odors
same description as above
red/gray mottled clay, transition into gray clay,
transitions into green clay, all fill, damp, no odors
gray/green clay transitions into a tan clayey
sand, damp, no odors
same clayey sand as above, transitions into silty
sandy clay, dry, no odors
silty sandy clay, tan, same as above, damp, no
odors
Depth to Bedrock:35 to 50%
Sampler Depth
interval (ft)Soil Description (proportions, grain size, etc.) PID (ppm) Soil Sample Details
Ground Elevation:PROPORTIONS
Total Boring Depth:20 to 35%
Date:10/10/2013 Hammer (weight [lb] / fall [inches])Driller: Probe-Tech
HRP Rep. Salley Gould Casing Core Barrel
Project: Gould Property facility HRP Associates, Inc.Test Boring/Monitor Well ID: MW-8
Location: Charlotte, NC DRILLING/SOIL LOG
HRP# GOU4000.GW Sheet No. _1___ of _1___
Rig Type: Geoprobe 772ODT
H:\G\Gould Family Properties II\GOU7000.GW - Atando Ave MW Install\Data\Soil Logs
Resources ugust
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

_______________
Mike Tynan
2725-A
Probe Technology, Inc.
✔
10-10-13 MW-8
Gould Family Properties, LLC
527 Atando Ave, Charlotte, NC 28206
Mecklenburg
35 15 29.828 80 49 03.869
✔
✔
1
34
10.5
6.5
Auger
10 34 saprolite
0 24 2 Sch40 PVC
24 34 2 0.010 Sch40 PVC
0 8 neat cement gravity
8 22 bentonite gravity
22 34 #2 silica sand gravity
See Geologist's log
10-15-13
Resources ugust
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

_______________
Mike Tynan
2725-A
Probe Technology, Inc.
✔
10-10-13 MW-7
Gould Family Properties, LLC
527 Atando Ave, Charlotte, NC 28206
Mecklenburg
35 15 32.162 80 49 00.463
✔
✔
1
28
15.7
8.25
Auger
15 28 saprolite
0 18 2 Sch40 PVC
18 28 2 0.010 Sch40 PVC
0 2 concrete gravity
2 16 bentonite gravity
16 28 #2 silica sand gravity
See Geologist's log
10-15-13
Resources ugust
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

_______________
Mike Tynan
2725-A
Probe Technology, Inc.
✔
10-10-13 MW-6
Gould Family Properties, LLC
527 Atando Ave, Charlotte, NC 28206
Mecklenburg
35 15 30.666 80 49 00.000
✔
✔
1
30
17.5
6.5
Auger
17.5 30 saprolite
0 20 2 Sch40 PVC
20 30 2 0.010 Sch40 PVC
0 8 neat cement gravity
8 18 bentonite gravity
18 30 #2 silica sand gravity
See Geologist's log
10-15-13

HRP Associates, Inc.
ATTACHMENT C

WELL DEVELOPMENT LOGS

HRP Associates, Inc.
ATTACHMENT D

GROUNDWATER SAMPLING: WATER LEVEL LOG
FIELD DATA SHEETS

HRP Associates, Inc.
ATTACHMENT E

CERTIFIED LAND SURVEY