9902_YadkinCoMSWLF_GWMR_DIN27328_20160219

Greene County Active C&D over Closed Unlined Landfill
Walstonburg, North Carolina
March 2015
MESCO Project Number: G15010.0
Semi-Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
Permit Number: 40-02
P.O. Box 97
Garner, NC 27529
License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Sampling Procedures Page 1
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 2
Surface Water Samples Page 2
Surface Water Characterization Page 2
Findings Page 2
Closing Page 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, or 2B (Appendix 1) Table 5
FIGURES
Water Quality Monitoring Locations Figure 1
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
February 19, 2016
Mr. Ervin Lane
Solid Waste Section
Division of Waste Management
North Carolina Department of Environment and Natural Resources
217 West Jones Street
Raleigh, NC 27603
Re: Semi-Annual Water Quality Monitoring Report
Yadkin County New Closed MSWLF and Closed C&D Landfill
Permit No. 99-02
MESCO Project No. G15017.0
Event Date: March 6, 2015
Dear Mr. Lane:
Introduction
The Yadkin County New Closed Unlined Municipal Solid Waste Landfill (MSWLF) and Closed Construction and
Demolition (C&D) Landfill located near Yadkinville NC, that operated under Permit #99-02, is required to submit
semi-annual compliance reports as a condition of its water quality monitoring program. Municipal Engineering
Services Company, P.A. (MESCO) personnel of Garner NC performed this water quality monitoring event on March
6, 2015 in accordance with the established semi-annual schedule prescribed by the NC Solid Waste Section (SWS)
rules/regulations. Laboratory analytical results indicate that no constituents were detected in any sample in
concentrations above NC 2L groundwater Standards except for total cadmium in the sample collected from the
upgradient background well MW-1.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and a recent SWS
memorandum, this report contains sampling procedures, field and laboratory results, surface water characterization.
Well construction summary table, field observations table, field parameter data table, sampling and analysis summary
table, detections compared to Standards tables, facility map with monitoring locations, quality assurance/quality
control data, and laboratory analytical data results are enclosed herein.
Sampling Procedure
This monitoring event entailed collection and analysis of water samples from all eight downgradient monitoring wells
(MW-2, MW-3, MW-4, MW-5S, MW-5D, MW-6, MW-7 and MW-8), one hydraulically upgradient background well
(MW-1), and both surface water points (SW-1 and SW-2). Quality control samples including equipment blanks (EB)
field blanks (FB) and travel blanks (TB) were also analyzed. Monitoring locations are shown on Figure 1.
MESCO personnel performed this sampling event utilizing portable monitoring methodology in general accordance
with the Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. A
summary detailing the construction of the water monitoring wells is presented on Table 1. The function and integrity
of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table 2. The
depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low-flow pumping methodology or bailing was used to adequately purge the wells to a minimum of three times the
volume of standing water in the well or until dry. Surface water samples were dipped from the surface of the creeks
at previously designated locations. Samples were then placed into laboratory-prepared pre-preserved containers.
Samples were kept on ice and transported to a NC-certified laboratory under proper C-O-C protocol within the
specified hold times for each analysis.

Figures
P-1
MW-6
MW-7
MW-8
MW-3
MW-2
1
0
0
1
2
0
1
1
0
1
3
0
1
4
0
9 0
WATER QUALITY MONITORING LOCATIONS
FIGURE 1
NOTE:
1.Water table contour is based on water
levels measured on May 22, 2003.
2.Water table contour elevations are
assumed, and are in units of feet.3.MW-5S/D approximate locations
Monitoring Well
Water Table Contour
500 FT
C&D Waste Limits
SW-1
Surface Water Monitoring Point
Piezometer
MW-4
MW-5S MW-5D
MW-1
Date of Event 03/06/2015
Created By
Project Name Semi-Annual Water Quality Monitoring
Site Name
Project Number G15027.0
Municipal Engineering Services Company, PA
J. Pfohl
Yadkin County Unlined New Closed and CDLF
SW-2
Scalehouse
Shop
Tables
Yadkin County New Closed MSWLF and Closed C&D Landfill Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
March 6, 2015
Latitude Longitude
(inches)(ft)
MW-1 12/10/91 2 39.0 24 15 Sandy Silt NA NA NA 33.18 36.181425 80.641475
MW-2 12/18/91 2 18.0 3 15 Sandy Silt NA NA NA 4.73 36.179352 80.639692
MW-3 12/12/91 2 20.5 5.5 15 Sandy Silt NA NA NA 6.21 36.179959 80.636438
MW-4 12/16/91 2 20.0 5 15 Sandy Silt NA NA NA 8.21 36.177767 80.636605
MW-5S 8/16/01 2 20.0 5 15 Soil NA NA NA 5.23 36.179047 80.639751
MW-5D 8/17/01 2 71.0 51 20 Rock NA NA NA 10.41 36.179047 80.639751
MW-6 4/22/03 2 21.0 6 15 Soil NA NA NA 15.01 36.180815 80.637854
MW-7 4/22/03 2 45.0 30 15 Soil NA NA NA 38.89 36.181373 80.636025
MW-8 4/22/03 2 45.0 30 15 Soil NA NA NA 40.13 36.180992 80.635990
NA = Not available at this time
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length Geology of
Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
Yadkin County New Closed MSWLF and Closed C&D Landfill Page 1 of 1
Table 2
Field Observations of Monitoring Locations
March 6, 2015
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes Fast Recharge
MW-3 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-4 Yes Yes Yes Yes Yes ?Surface pad cracked
MW-5S Yes Yes Yes Yes Yes Yes
MW-5D Yes Yes Yes Yes Yes Yes
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes
MW-8 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----Low flow & gage height
SW-2 Yes -----Low flow & gage height
Any unusual field conditions, observations, or events:
Nothing noteworthy
Sample
Location
Viable
Monitoring
Location
Lack of
Any
Evidence
of
Tampering
Hinge/Hasp
Operates
Tagged
or
Labeled
Concrete
Surface Pad
Effective
Yadkin County New Closed MSWLF and Closed C&D Landfill Page 1 of 1
Table 3
Field Parameter Data Summary
March 6, 2015
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L Visual
MW-1 33.18 NA NA 16.3 NR NR 5.53 180 80 Very
MW-2 4.73 NA NA 9.3 NR NR 5.31 60 30 Clear
MW-3 6.21 NA NA 12.5 NR NR 5.42 80 40 Slight
MW-4 8.21 NA NA 12.8 NR NR 5.53 50 30 Slight
MW-5S 5.23 NA NA 11.7 NR NR 6.31 90 40 Slight
MW-5D 10.41 NA NA 13.3 NR NR 7.53 320 150 Clear
MW-6 15.01 NA NA 14.4 NR NR 5.18 90 40 Clear
MW-7 38.89 NA NA 14.1 NR NR 5.31 50 20 Mod
MW-8 40.13 NA NA 14.9 NR NR 5.68 30 10 Mod
Minimum 4.73 NA NA 9.3 NR NR 5.18 30 10 Clear
Average 18.00 NA NA 13.3 NR NR 5.76 106 49 Slight
Maximum 40.13 NA NA 16.3 NR NR 7.53 320 150 Very
SW-1 ---10.3 NR NR 6.63 30 10 Clear
SW-2 ---10.2 NR NR 6.65 20 10 Clear
Minimum ---10.2 NR NR 6.63 20 10 Clear
Average ---10.3 NR NR 6.64 25 10 Clear
Maximum ---10.3 NR NR 6.65 30 10 Clear
NR = No Reading Attempted
Water
Depth
Water
Elevation
TOC
Elevation
Specific
Conductance
Turbidity
of Metal
Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
Yadkin County New Closed MSWLF and Closed C&D Landfill Page 1 of 1
Table 4
Sampling and Analysis Summary
March 6, 2015
C&D Field Parameter
Re
a
s
o
n

N
o
t

S
a
m
p
l
e
d
To
t
a
l

M
e
t
a
l
s

Ox
i
d
a
t
i
o
n

R
e
d
u
c
t
i
o
n

P
o
t
e
n
t
i
a
l

(
O
R
P
)
Te
m
p
e
r
a
t
u
r
e
Co
n
d
u
c
t
i
v
i
t
y
To
t
a
l

D
i
s
s
o
l
v
e
d

S
o
l
i
d
s

(
T
D
S
)
pH Tu
r
b
i
d
i
t
y
La
b

E
P
A

8
2
6
0
B
L
a
b

E
P
A

6
0
0
0
/
7
0
0
0
La
b

E
P
A

8
2
6
0
B
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

V
i
s
u
a
l
MW-1 x x x x x x x x
MW-2 x x x x x x x x
MW-3 x x x x x x x x
MW-4 x x x x x x x x
MW-5S x x x x x x x x
MW-5D x x x x x x x x
MW-6 x x x x x x x x
MW-7 x x x x x x x x
MW-8 x x x x x x x x
SW-1 x x x x x x x x
SW-2 x x x x x x x x
EB x x x
FB x x x
TB x x
Appendix I = List from current 40 CFR 258
App. I
VO
C
s

Te
t
r
a
h
y
dr
o
f
ur
a
n
Yadkin County New Closed MSWLF and Closed C&D Landfill Page 1 of 1
Table 5
Detections in Water Samples above SWSL, GWP, 2L or 2B
March 6, 2015
Sample ID Result Unit
MW-1 Cadmium, total 3/6/15 2.2 0.5 1 2 5 N & B
MW-1 Vanadium, total 3/6/15 15.4,j 2.5 25 3.5 NE
MW-1 Cobalt, total 3/6/15 10 2.5 10 70 NE
MW-1 Zinc, total 3/6/15 13.6 5 10 1000 5000
MW-2 Zinc, total 3/6/15 15 5 10 1000 5000
MW-4 Vanadium, total 3/6/15 3.7,j 2.5 25 3.5 NE
MW-5S Zinc, total 3/6/15 18.6 5 10 1000 5000
MW-6 Zinc, total 3/6/15 16.4 5 10 1000 5000
SW-1 Vanadium, total 3/6/15 5.2,j 2.5 25 NE NE
SW-1 Zinc, total 3/6/15 11 5 10 50 5000
SW-2 Vanadium, total 3/6/15 13.9,j 2.5 25 NE NE
SW-2 Zinc, total 3/6/15 23.9 5 10 50 5000
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
BOLD = Concentration > 2L, 2B or MCL Standard
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
B = Background as detected upgradient/upstream of landfill
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
March 26, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92240549
92240549
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
YADKIN MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between March 10, 2015
and March 11, 2015. The results relate only to the samples included in this report. Results reported
herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 53
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 53
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92240549001 MW-1 Water 03/06/15 12:00 03/10/15 16:20
92240549002 MW-2 Water 03/06/15 15:30 03/10/15 16:20
92240549003 MW-3 Water 03/06/15 09:40 03/10/15 16:20
92240549004 MW-4 Water 03/06/15 08:45 03/10/15 16:20
92240549005 MW-5S Water 03/06/15 14:40 03/10/15 16:20
92240549006 MW-5D Water 03/06/15 14:20 03/10/15 16:20
92240549007 MW-6 Water 03/06/15 11:50 03/10/15 16:20
92240549008 MW-7 Water 03/06/15 11:25 03/10/15 16:20
92240549009 MW-8 Water 03/06/15 10:40 03/10/15 16:20
92240549010 SW-1 Water 03/06/15 10:00 03/10/15 16:20
92240549011 EB Water 03/06/15 08:10 03/10/15 16:20
92240549012 FB Water 03/06/15 08:00 03/10/15 16:20
92240549013 TB Water 03/06/15 00:00 03/10/15 16:20
92240549014 SW-2 Water 03/08/15 09:00 03/11/15 16:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 53
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92240549001 MW-1 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549002 MW-2 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549003 MW-3 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549004 MW-4 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549005 MW-5S EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549006 MW-5D EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549007 MW-6 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549008 MW-7 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549009 MW-8 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549010 SW-1 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549011 EB EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549012 FB EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
92240549013 TB EPA 8260 52 PASI-CGAW
92240549014 SW-2 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-1 Lab ID: 92240549001 Collected: 03/06/15 12:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 04:55 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 04:55 7440-38-203/11/15 15:0510.0 2.5 1
Barium 86.6J ug/L 03/12/15 04:55 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 04:55 7440-41-703/11/15 15:051.0 0.50 1
Cadmium 2.2 ug/L 03/12/15 04:55 7440-43-903/11/15 15:051.0 0.50 1
Chromium 8.7J ug/L 03/12/15 04:55 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt 4.0J ug/L 03/12/15 04:55 7440-48-403/11/15 15:0510.0 2.5 1
Copper 7.1J ug/L 03/12/15 04:55 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 04:55 7439-92-103/11/15 15:0510.0 2.5 1
Nickel 6.3J ug/L 03/12/15 04:55 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 04:55 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 04:55 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 04:55 7440-28-003/11/15 15:055.5 5.0 1
Vanadium 15.4J ug/L 03/12/15 04:55 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 13.6 ug/L 03/12/15 04:55 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 17:51 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 17:51 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 17:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 17:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 17:51 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 17:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 17:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 17:51 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 17:51 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 17:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 17:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 17:51 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 17:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 17:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 17:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 17:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 17:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 17:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 17:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 17:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 17:51 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 17:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 17:51 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 17:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 17:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 17:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 17:51 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 17:51 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 17:51 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-1 Lab ID: 92240549001 Collected: 03/06/15 12:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 17:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 17:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 17:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 17:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 17:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 17:51 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 17:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 17:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 17:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 17:51 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 17:51 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 17:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 17:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 17:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 17:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 17:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 17:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 17:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 17:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 17:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %03/18/15 17:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)116 %03/18/15 17:51 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 17:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-2 Lab ID: 92240549002 Collected: 03/06/15 15:30 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 04:59 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 04:59 7440-38-203/11/15 15:0510.0 2.5 1
Barium 36.0J ug/L 03/12/15 04:59 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 04:59 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 04:59 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 04:59 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 04:59 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 04:59 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 04:59 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 04:59 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 04:59 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 04:59 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 04:59 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 04:59 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 15.0 ug/L 03/12/15 04:59 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 30.2J ug/L 03/18/15 18:08 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 18:08 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 18:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 18:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 18:08 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 18:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 18:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 18:08 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 18:08 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 18:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 18:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 18:08 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 18:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 18:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 18:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 18:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 18:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 18:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 18:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 18:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 18:08 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 18:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 18:08 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 18:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 18:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 18:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 18:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 18:08 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 18:08 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-2 Lab ID: 92240549002 Collected: 03/06/15 15:30 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 18:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 18:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 18:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 18:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 18:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 18:08 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 18:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 18:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 18:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 18:08 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 18:08 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 18:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 18:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 18:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 18:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 18:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 18:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 18:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 18:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 18:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %03/18/15 18:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)115 %03/18/15 18:08 17060-07-070-130 1
Toluene-d8 (S)96 %03/18/15 18:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-3 Lab ID: 92240549003 Collected: 03/06/15 09:40 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:02 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:02 7440-38-203/11/15 15:0510.0 2.5 1
Barium 12.0J ug/L 03/12/15 05:02 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:02 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:02 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:02 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:02 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:02 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:02 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:02 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:02 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:02 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:02 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:02 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 9.3J ug/L 03/12/15 05:02 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 18:25 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 18:25 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 18:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 18:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 18:25 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 18:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 18:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 18:25 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 18:25 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 18:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 18:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 18:25 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 18:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 18:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 18:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 18:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 18:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 18:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 18:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 18:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 18:25 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 18:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 18:25 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 18:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 18:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 18:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 18:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 18:25 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 18:25 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-3 Lab ID: 92240549003 Collected: 03/06/15 09:40 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 18:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 18:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 18:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 18:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 18:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 18:25 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 18:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 18:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 18:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 18:25 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 18:25 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 18:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 18:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 18:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 18:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 18:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 18:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 18:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 18:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 18:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %03/18/15 18:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)117 %03/18/15 18:25 17060-07-070-130 1
Toluene-d8 (S)96 %03/18/15 18:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-4 Lab ID: 92240549004 Collected: 03/06/15 08:45 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:05 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:05 7440-38-203/11/15 15:0510.0 2.5 1
Barium 14.5J ug/L 03/12/15 05:05 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:05 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:05 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:05 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:05 7440-48-403/11/15 15:0510.0 2.5 1
Copper 3.5J ug/L 03/12/15 05:05 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:05 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:05 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:05 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:05 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:05 7440-28-003/11/15 15:055.5 5.0 1
Vanadium 3.7J ug/L 03/12/15 05:05 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 7.7J ug/L 03/12/15 05:05 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 18:42 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 18:42 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 18:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 18:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 18:42 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 18:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 18:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 18:42 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 18:42 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 18:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 18:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 18:42 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 18:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 18:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 18:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 18:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 18:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 18:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 18:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 18:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 18:42 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 18:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 18:42 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 18:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 18:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 18:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 18:42 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 18:42 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 18:42 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-4 Lab ID: 92240549004 Collected: 03/06/15 08:45 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 18:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 18:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 18:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 18:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 18:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 18:42 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 18:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 18:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 18:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 18:42 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 18:42 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 18:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 18:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 18:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 18:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 18:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 18:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 18:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 18:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 18:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %03/18/15 18:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)116 %03/18/15 18:42 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 18:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-5S Lab ID: 92240549005 Collected: 03/06/15 14:40 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:08 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:08 7440-38-203/11/15 15:0510.0 2.5 1
Barium 43.0J ug/L 03/12/15 05:08 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:08 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:08 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:08 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:08 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:08 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:08 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:08 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:08 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:08 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:08 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:08 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 18.6 ug/L 03/12/15 05:08 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 18:59 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 18:59 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 18:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 18:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 18:59 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 18:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 18:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 18:59 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 18:59 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 18:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 18:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 18:59 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 18:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 18:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 18:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 18:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 18:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 18:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 18:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 18:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 18:59 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 18:59 75-34-35.0 0.32 1
1,2-Dichloroethane 0.34J ug/L 03/18/15 18:59 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 18:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 18:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 18:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 18:59 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 18:59 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 18:59 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-5S Lab ID: 92240549005 Collected: 03/06/15 14:40 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 18:59 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 18:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 18:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 18:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 18:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 18:59 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 18:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 18:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 18:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 18:59 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 18:59 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 18:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 18:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 18:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 18:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 18:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 18:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 18:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 18:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 18:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %03/18/15 18:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)121 %03/18/15 18:59 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 18:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-5D Lab ID: 92240549006 Collected: 03/06/15 14:20 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:11 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:11 7440-38-203/11/15 15:0510.0 2.5 1
Barium 8.9J ug/L 03/12/15 05:11 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:11 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:11 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:11 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:11 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:11 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:11 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:11 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:11 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:11 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:11 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:11 7440-62-203/11/15 15:0525.0 2.5 1
Zinc ND ug/L 03/12/15 05:11 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 19:15 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 19:15 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 19:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 19:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 19:15 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 19:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 19:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 19:15 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 19:15 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 19:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 19:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 19:15 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 19:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 19:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 19:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 19:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 19:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 19:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 19:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 19:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 19:15 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 19:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 19:15 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 19:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 19:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 19:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 19:15 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 19:15 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 19:15 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-5D Lab ID: 92240549006 Collected: 03/06/15 14:20 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 19:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 19:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 19:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 19:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 19:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 19:15 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 19:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 19:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 19:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 19:15 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 19:15 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 19:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 19:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 19:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 19:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 19:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 19:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 19:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 19:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 19:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %03/18/15 19:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)122 %03/18/15 19:15 17060-07-070-130 1
Toluene-d8 (S)96 %03/18/15 19:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-6 Lab ID: 92240549007 Collected: 03/06/15 11:50 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:14 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:14 7440-38-203/11/15 15:0510.0 2.5 1
Barium 75.6J ug/L 03/12/15 05:14 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:14 7440-41-703/11/15 15:051.0 0.50 1
Cadmium 0.86J ug/L 03/12/15 05:14 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:14 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt 8.1J ug/L 03/12/15 05:14 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:14 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:14 7439-92-103/11/15 15:0510.0 2.5 1
Nickel 4.9J ug/L 03/12/15 05:14 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:14 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:14 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:14 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:14 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 16.4 ug/L 03/12/15 05:14 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 19:49 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 19:49 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 19:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 19:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 19:49 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 19:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 19:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 19:49 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 19:49 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 19:49 56-23-5 M11.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 19:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 19:49 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 19:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 19:49 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 19:49 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 19:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 19:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 19:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 19:49 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 19:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 19:49 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 19:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 19:49 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 19:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 19:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 19:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 19:49 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 19:49 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 19:49 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-6 Lab ID: 92240549007 Collected: 03/06/15 11:50 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 19:49 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 19:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 19:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 19:49 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 19:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 19:49 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 19:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 19:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 19:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 19:49 127-18-4 M11.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 19:49 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 19:49 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 19:49 71-55-6 M11.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 19:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 19:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 19:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 19:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 19:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 19:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 19:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %03/18/15 19:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %03/18/15 19:49 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 19:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-7 Lab ID: 92240549008 Collected: 03/06/15 11:25 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:17 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:17 7440-38-203/11/15 15:0510.0 2.5 1
Barium 39.0J ug/L 03/12/15 05:17 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:17 7440-41-703/11/15 15:051.0 0.50 1
Cadmium 0.64J ug/L 03/12/15 05:17 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:17 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:17 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:17 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:17 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:17 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:17 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:17 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:17 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:17 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 7.0J ug/L 03/12/15 05:17 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 20:57 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 20:57 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 20:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 20:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 20:57 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 20:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 20:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 20:57 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 20:57 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 20:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 20:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 20:57 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 20:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 20:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 20:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 20:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 20:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 20:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 20:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 20:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 20:57 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 20:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 20:57 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 20:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 20:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 20:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 20:57 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 20:57 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 20:57 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-7 Lab ID: 92240549008 Collected: 03/06/15 11:25 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 20:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 20:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 20:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 20:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 20:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 20:57 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 20:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 20:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 20:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 20:57 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 20:57 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 20:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 20:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 20:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 20:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 20:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 20:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 20:57 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 20:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 20:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %03/18/15 20:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)123 %03/18/15 20:57 17060-07-070-130 1
Toluene-d8 (S)98 %03/18/15 20:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-8 Lab ID: 92240549009 Collected: 03/06/15 10:40 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:20 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:20 7440-38-203/11/15 15:0510.0 2.5 1
Barium 82.9J ug/L 03/12/15 05:20 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:20 7440-41-703/11/15 15:051.0 0.50 1
Cadmium 0.81J ug/L 03/12/15 05:20 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:20 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:20 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:20 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:20 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:20 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:20 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:20 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:20 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:20 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 5.9J ug/L 03/12/15 05:20 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 21:14 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 21:14 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 21:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 21:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 21:14 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 21:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 21:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 21:14 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 21:14 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 21:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 21:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 21:14 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 21:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 21:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 21:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 21:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 21:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 21:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 21:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 21:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 21:14 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 21:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 21:14 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 21:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 21:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 21:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 21:14 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 21:14 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 21:14 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: MW-8 Lab ID: 92240549009 Collected: 03/06/15 10:40 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 21:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 21:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 21:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 21:14 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 21:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 21:14 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 21:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 21:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 21:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 21:14 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 21:14 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 21:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 21:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 21:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 21:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 21:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 21:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 21:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 21:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 21:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %03/18/15 21:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %03/18/15 21:14 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 21:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: SW-1 Lab ID: 92240549010 Collected: 03/06/15 10:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:32 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:32 7440-38-203/11/15 15:0510.0 2.5 1
Barium 31.7J ug/L 03/12/15 05:32 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:32 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:32 7440-43-903/11/15 15:051.0 0.50 1
Chromium 2.6J ug/L 03/12/15 05:32 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:32 7440-48-403/11/15 15:0510.0 2.5 1
Copper 2.7J ug/L 03/12/15 05:32 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:32 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:32 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:32 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:32 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:32 7440-28-003/11/15 15:055.5 5.0 1
Vanadium 5.2J ug/L 03/12/15 05:32 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 11.0 ug/L 03/12/15 05:32 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 21:31 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 21:31 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 21:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 21:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 21:31 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 21:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 21:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 21:31 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 21:31 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 21:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 21:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 21:31 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 21:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 21:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 21:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 21:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 21:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 21:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 21:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 21:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 21:31 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 21:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 21:31 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 21:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 21:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 21:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 21:31 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 21:31 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 21:31 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: SW-1 Lab ID: 92240549010 Collected: 03/06/15 10:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 21:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 21:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 21:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 21:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 21:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 21:31 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 21:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 21:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 21:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 21:31 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 21:31 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 21:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 21:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 21:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 21:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 21:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 21:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 21:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 21:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 21:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %03/18/15 21:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)121 %03/18/15 21:31 17060-07-070-130 1
Toluene-d8 (S)99 %03/18/15 21:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: EB Lab ID: 92240549011 Collected: 03/06/15 08:10 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:35 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:35 7440-38-203/11/15 15:0510.0 2.5 1
Barium ND ug/L 03/12/15 05:35 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:35 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:35 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:35 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:35 7440-48-403/11/15 15:0510.0 2.5 1
Copper 4.7J ug/L 03/12/15 05:35 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:35 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:35 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:35 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:35 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:35 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:35 7440-62-203/11/15 15:0525.0 2.5 1
Zinc ND ug/L 03/12/15 05:35 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 20:06 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 20:06 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 20:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 20:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 20:06 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 20:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 20:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 20:06 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 20:06 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 20:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 20:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 20:06 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 20:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 20:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 20:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 20:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 20:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 20:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 20:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 20:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 20:06 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 20:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 20:06 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 20:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 20:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 20:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 20:06 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 20:06 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 20:06 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: EB Lab ID: 92240549011 Collected: 03/06/15 08:10 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 20:06 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 20:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 20:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 20:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 20:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 20:06 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 20:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 20:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 20:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 20:06 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 20:06 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 20:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 20:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 20:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 20:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 20:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 20:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 20:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 20:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 20:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %03/18/15 20:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)118 %03/18/15 20:06 17060-07-070-130 1
Toluene-d8 (S)98 %03/18/15 20:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: FB Lab ID: 92240549012 Collected: 03/06/15 08:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/12/15 05:38 7440-36-003/11/15 15:056.0 3.8 1
Arsenic ND ug/L 03/12/15 05:38 7440-38-203/11/15 15:0510.0 2.5 1
Barium ND ug/L 03/12/15 05:38 7440-39-303/11/15 15:05100 2.5 1
Beryllium ND ug/L 03/12/15 05:38 7440-41-703/11/15 15:051.0 0.50 1
Cadmium ND ug/L 03/12/15 05:38 7440-43-903/11/15 15:051.0 0.50 1
Chromium ND ug/L 03/12/15 05:38 7440-47-303/11/15 15:0510.0 2.5 1
Cobalt ND ug/L 03/12/15 05:38 7440-48-403/11/15 15:0510.0 2.5 1
Copper ND ug/L 03/12/15 05:38 7440-50-803/11/15 15:0510.0 2.5 1
Lead ND ug/L 03/12/15 05:38 7439-92-103/11/15 15:0510.0 2.5 1
Nickel ND ug/L 03/12/15 05:38 7440-02-003/11/15 15:0550.0 2.5 1
Selenium ND ug/L 03/12/15 05:38 7782-49-203/11/15 15:0510.0 5.0 1
Silver ND ug/L 03/12/15 05:38 7440-22-403/11/15 15:0510.0 2.5 1
Thallium ND ug/L 03/12/15 05:38 7440-28-003/11/15 15:055.5 5.0 1
Vanadium ND ug/L 03/12/15 05:38 7440-62-203/11/15 15:0525.0 2.5 1
Zinc 5.5J ug/L 03/12/15 05:38 7440-66-603/11/15 15:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 20:23 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 20:23 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 20:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 20:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 20:23 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 20:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 20:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 20:23 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 20:23 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 20:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 20:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 20:23 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 20:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 20:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 20:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 20:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 20:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 20:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 20:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 20:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 20:23 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 20:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 20:23 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 20:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 20:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 20:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 20:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 20:23 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 20:23 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: FB Lab ID: 92240549012 Collected: 03/06/15 08:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 20:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 20:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 20:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 20:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 20:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 20:23 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 20:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 20:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 20:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 20:23 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 20:23 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 20:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 20:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 20:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 20:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 20:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 20:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 20:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 20:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 20:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %03/18/15 20:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)122 %03/18/15 20:23 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 20:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: TB Lab ID: 92240549013 Collected: 03/06/15 00:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 20:40 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 20:40 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 20:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 20:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 20:40 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 20:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 20:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 20:40 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 20:40 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 20:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 20:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 20:40 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 20:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 20:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 20:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 20:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 20:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 20:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 20:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 20:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 20:40 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 20:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 20:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 20:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 20:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 20:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 20:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 20:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 20:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/18/15 20:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 20:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 20:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 20:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 20:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 20:40 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 20:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 20:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 20:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 20:40 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 20:40 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 20:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 20:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 20:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 20:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 20:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 20:40 96-18-41.0 0.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: TB Lab ID: 92240549013 Collected: 03/06/15 00:00 Received: 03/10/15 16:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl acetate ND ug/L 03/18/15 20:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 20:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 20:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %03/18/15 20:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)124 %03/18/15 20:40 17060-07-070-130 1
Toluene-d8 (S)96 %03/18/15 20:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: SW-2 Lab ID: 92240549014 Collected: 03/08/15 09:00 Received: 03/11/15 16:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 03/25/15 20:58 7440-36-003/25/15 15:256.0 3.8 1
Arsenic 3.6J ug/L 03/25/15 20:58 7440-38-203/25/15 15:2510.0 2.5 1
Barium 59.5J ug/L 03/25/15 20:58 7440-39-303/25/15 15:25100 2.5 1
Beryllium ND ug/L 03/25/15 20:58 7440-41-703/25/15 15:251.0 0.50 1
Cadmium ND ug/L 03/25/15 20:58 7440-43-903/25/15 15:251.0 0.50 1
Chromium 6.7J ug/L 03/25/15 20:58 7440-47-303/25/15 15:2510.0 2.5 1
Cobalt ND ug/L 03/25/15 20:58 7440-48-403/25/15 15:2510.0 2.5 1
Copper 3.3J ug/L 03/25/15 20:58 7440-50-803/25/15 15:2510.0 2.5 1
Lead ND ug/L 03/25/15 20:58 7439-92-103/25/15 15:2510.0 2.5 1
Nickel 3.2J ug/L 03/25/15 20:58 7440-02-003/25/15 15:2550.0 2.5 1
Selenium ND ug/L 03/25/15 20:58 7782-49-203/25/15 15:2510.0 5.0 1
Silver ND ug/L 03/25/15 20:58 7440-22-403/25/15 15:2510.0 2.5 1
Thallium ND ug/L 03/25/15 20:58 7440-28-003/25/15 15:255.5 5.0 1
Vanadium 13.9J ug/L 03/25/15 20:58 7440-62-203/25/15 15:2525.0 2.5 1
Zinc 23.9 ug/L 03/25/15 20:58 7440-66-603/25/15 15:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 03/18/15 22:04 67-64-1100 10.0 1
Acrylonitrile ND ug/L 03/18/15 22:04 107-13-1200 1.9 1
Benzene ND ug/L 03/18/15 22:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/18/15 22:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 03/18/15 22:04 75-27-41.0 0.18 1
Bromoform ND ug/L 03/18/15 22:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 03/18/15 22:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 03/18/15 22:04 78-93-3100 0.96 1
Carbon disulfide ND ug/L 03/18/15 22:04 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 03/18/15 22:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/18/15 22:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 03/18/15 22:04 75-00-310.0 0.54 1
Chloroform ND ug/L 03/18/15 22:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 03/18/15 22:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 03/18/15 22:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 03/18/15 22:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/18/15 22:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/18/15 22:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/18/15 22:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 03/18/15 22:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/18/15 22:04 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 03/18/15 22:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 03/18/15 22:04 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/18/15 22:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/18/15 22:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/18/15 22:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 03/18/15 22:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/18/15 22:04 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 03/18/15 22:04 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
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Page 31 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Sample: SW-2 Lab ID: 92240549014 Collected: 03/08/15 09:00 Received: 03/11/15 16:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 03/18/15 22:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/18/15 22:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 03/18/15 22:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 03/18/15 22:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 03/18/15 22:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/18/15 22:04 108-10-1100 0.33 1
Styrene ND ug/L 03/18/15 22:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/18/15 22:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/18/15 22:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 03/18/15 22:04 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 03/18/15 22:04 109-99-910.0 3.1 1
Toluene ND ug/L 03/18/15 22:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/18/15 22:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/18/15 22:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/18/15 22:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/18/15 22:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/18/15 22:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/18/15 22:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 03/18/15 22:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/18/15 22:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %03/18/15 22:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %03/18/15 22:04 17060-07-070-130 1
Toluene-d8 (S)97 %03/18/15 22:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18050
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92240549001, 92240549002, 92240549003, 92240549004, 92240549005, 92240549006, 92240549007,
92240549008, 92240549009, 92240549010, 92240549011, 92240549012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1408110
Associated Lab Samples: 92240549001, 92240549002, 92240549003, 92240549004, 92240549005, 92240549006, 92240549007,
92240549008, 92240549009, 92240549010, 92240549011, 92240549012
Matrix: Water
Analyzed
Antimony ug/L ND 6.0 03/12/15 04:29
Arsenic ug/L ND 10.0 03/12/15 16:12
Barium ug/L ND 100 03/12/15 04:29
Beryllium ug/L ND 1.0 03/12/15 04:29
Cadmium ug/L ND 1.0 03/12/15 04:29
Chromium ug/L ND 10.0 03/12/15 04:29
Cobalt ug/L ND 10.0 03/12/15 04:29
Copper ug/L ND 10.0 03/12/15 04:29
Lead ug/L ND 10.0 03/12/15 16:12
Nickel ug/L ND 50.0 03/12/15 04:29
Selenium ug/L ND 10.0 03/12/15 04:29
Silver ug/L ND 10.0 03/12/15 04:29
Thallium ug/L ND 5.5 03/12/15 04:29
Vanadium ug/L ND 25.0 03/12/15 04:29
Zinc ug/L ND 10.0 03/12/15 04:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1408111LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 486500 97 80-120
Arsenic ug/L 491500 98 80-120
Barium ug/L 462500 92 80-120
Beryllium ug/L 469500 94 80-120
Cadmium ug/L 472500 94 80-120
Chromium ug/L 462500 92 80-120
Cobalt ug/L 466500 93 80-120
Copper ug/L 480500 96 80-120
Lead ug/L 498500 100 80-120
Nickel ug/L 467500 93 80-120
Selenium ug/L 477500 95 80-120
Silver ug/L 237250 95 80-120
Thallium ug/L 463500 93 80-120
Vanadium ug/L 463500 93 80-120
Zinc ug/L 456500 91 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1408112MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92240430001
1408113
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-12598 2 25500ND499 491
Arsenic ug/L 500 103 75-125101 1 255009.3J 524 516
Barium ug/L 500 93 75-12591 2 2550014.3 480 472
Beryllium ug/L 500 95 75-12593 2 25500ND474 466
Cadmium ug/L 500 96 75-12594 2 25500ND479 471
Chromium ug/L 500 93 75-12591 2 25500ND465 456
Cobalt ug/L 500 92 75-12591 1 25500ND461 455
Copper ug/L 500 98 75-12596 2 25500ND492 483
Lead ug/L 500 98 75-12597 1 25500ND490 486
Nickel ug/L 500 92 75-12591 2 25500ND463 456
Selenium ug/L 500 96 75-12595 2 25500ND485 478
Silver ug/L 250 96 75-12594 2 25250ND240 236
Thallium ug/L 500 91 75-12591 0 25500ND459 456
Vanadium ug/L 500 95 75-12593 2 25500ND474 467
Zinc ug/L 500 91 75-12589 2 255005.6J 458 451
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18144
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples: 92240549014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1419120
Associated Lab Samples:92240549014
Matrix: Water
Analyzed
Antimony ug/L ND 6.0 03/25/15 20:52
Arsenic ug/L ND 10.0 03/25/15 20:52
Barium ug/L ND 100 03/25/15 20:52
Beryllium ug/L ND 1.0 03/25/15 20:52
Cadmium ug/L ND 1.0 03/25/15 20:52
Chromium ug/L ND 10.0 03/25/15 20:52
Cobalt ug/L ND 10.0 03/25/15 20:52
Copper ug/L ND 10.0 03/25/15 20:52
Lead ug/L ND 10.0 03/25/15 20:52
Nickel ug/L ND 50.0 03/25/15 20:52
Selenium ug/L ND 10.0 03/25/15 20:52
Silver ug/L ND 10.0 03/25/15 20:52
Thallium ug/L ND 5.5 03/25/15 20:52
Vanadium ug/L ND 25.0 03/25/15 20:52
Zinc ug/L ND 10.0 03/25/15 20:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1419121LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 487500 97 80-120
Arsenic ug/L 468500 94 80-120
Barium ug/L 506500 101 80-120
Beryllium ug/L 504500 101 80-120
Cadmium ug/L 484500 97 80-120
Chromium ug/L 482500 96 80-120
Cobalt ug/L 475500 95 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 465500 93 80-120
Nickel ug/L 474500 95 80-120
Selenium ug/L 474500 95 80-120
Silver ug/L 239250 96 80-120
Thallium ug/L 470500 94 80-120
Vanadium ug/L 481500 96 80-120
Zinc ug/L 455500 91 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1419122MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92240549014
1419123
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12597 1 25500ND488 484
Arsenic ug/L 500 94 75-12592 2 255003.6J 472 464
Barium ug/L 500 102 75-125101 1 2550059.5J 571 567
Beryllium ug/L 500 102 75-125101 1 25500ND513 508
Cadmium ug/L 500 98 75-12597 1 25500ND491 485
Chromium ug/L 500 97 75-12596 1 255006.7J 490 486
Cobalt ug/L 500 96 75-12595 1 25500ND481 475
Copper ug/L 500 102 75-125100 1 255003.3J 512 506
Lead ug/L 500 95 75-12593 1 25500ND474 468
Nickel ug/L 500 96 75-12595 1 255003.2J 482 477
Selenium ug/L 500 95 75-12594 1 25500ND477 473
Silver ug/L 250 97 75-12596 1 25250ND243 240
Thallium ug/L 500 96 75-12595 1 25500ND480 477
Vanadium ug/L 500 97 75-12596 1 2550013.9J 497 494
Zinc ug/L 500 90 75-12589 1 2550023.9 472 468
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30788
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92240549001, 92240549002, 92240549003, 92240549004, 92240549005, 92240549006, 92240549007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1413615
Associated Lab Samples:92240549001, 92240549002, 92240549003, 92240549004, 92240549005, 92240549006, 92240549007
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 03/18/15 12:29
1,1,1-Trichloroethane ug/L ND 1.0 03/18/15 12:29
1,1,2,2-Tetrachloroethane ug/L ND 3.0 03/18/15 12:29
1,1,2-Trichloroethane ug/L ND 1.0 03/18/15 12:29
1,1-Dichloroethane ug/L ND 5.0 03/18/15 12:29
1,1-Dichloroethene ug/L ND 5.0 03/18/15 12:29
1,2,3-Trichloropropane ug/L ND 1.0 03/18/15 12:29
1,2-Dibromo-3-chloropropane ug/L ND 13.0 03/18/15 12:29
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/18/15 12:29
1,2-Dichlorobenzene ug/L ND 5.0 03/18/15 12:29
1,2-Dichloroethane ug/L ND 1.0 03/18/15 12:29
1,2-Dichloropropane ug/L ND 1.0 03/18/15 12:29
1,3-Dichloropropane ug/L ND 1.0 03/18/15 12:29
1,4-Dichlorobenzene ug/L ND 1.0 03/18/15 12:29
2-Butanone (MEK)ug/L ND 100 03/18/15 12:29
2-Hexanone ug/L ND 50.0 03/18/15 12:29
4-Methyl-2-pentanone (MIBK)ug/L ND 100 03/18/15 12:29
Acetone ug/L ND 100 03/18/15 12:29
Acrylonitrile ug/L ND 200 03/18/15 12:29
Benzene ug/L ND 1.0 03/18/15 12:29
Bromochloromethane ug/L ND 3.0 03/18/15 12:29
Bromodichloromethane ug/L ND 1.0 03/18/15 12:29
Bromoform ug/L ND 3.0 03/18/15 12:29
Bromomethane ug/L ND 10.0 03/18/15 12:29
Carbon disulfide ug/L ND 100 03/18/15 12:29
Carbon tetrachloride ug/L ND 1.0 03/18/15 12:29
Chlorobenzene ug/L ND 3.0 03/18/15 12:29
Chloroethane ug/L ND 10.0 03/18/15 12:29
Chloroform ug/L ND 5.0 03/18/15 12:29
Chloromethane ug/L ND 1.0 03/18/15 12:29
cis-1,2-Dichloroethene ug/L ND 5.0 03/18/15 12:29
cis-1,3-Dichloropropene ug/L ND 1.0 03/18/15 12:29
Dibromochloromethane ug/L ND 3.0 03/18/15 12:29
Dibromomethane ug/L ND 10.0 03/18/15 12:29
Ethylbenzene ug/L ND 1.0 03/18/15 12:29
Iodomethane ug/L ND 10.0 03/18/15 12:29
Methylene Chloride ug/L ND 1.0 03/18/15 12:29
Styrene ug/L ND 1.0 03/18/15 12:29
Tetrachloroethene ug/L ND 1.0 03/18/15 12:29
Tetrahydrofuran ug/L ND 10.0 03/18/15 12:29
Toluene ug/L ND 1.0 03/18/15 12:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1413615
Associated Lab Samples:92240549001, 92240549002, 92240549003, 92240549004, 92240549005, 92240549006, 92240549007
Matrix: Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 03/18/15 12:29
trans-1,3-Dichloropropene ug/L ND 1.0 03/18/15 12:29
trans-1,4-Dichloro-2-butene ug/L ND 100 03/18/15 12:29
Trichloroethene ug/L ND 1.0 03/18/15 12:29
Trichlorofluoromethane ug/L ND 1.0 03/18/15 12:29
Vinyl acetate ug/L ND 50.0 03/18/15 12:29
Vinyl chloride ug/L ND 1.0 03/18/15 12:29
Xylene (Total)ug/L ND 5.0 03/18/15 12:29
1,2-Dichloroethane-d4 (S)%115 70-130 03/18/15 12:29
4-Bromofluorobenzene (S)%99 70-130 03/18/15 12:29
Toluene-d8 (S)%96 70-130 03/18/15 12:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413616LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.950 112 80-125
1,1,1-Trichloroethane ug/L 59.850 120 71-129
1,1,2,2-Tetrachloroethane ug/L 49.150 98 79-124
1,1,2-Trichloroethane ug/L 53.450 107 85-125
1,1-Dichloroethane ug/L 55.150 110 73-126
1,1-Dichloroethene ug/L 55.150 110 66-135
1,2,3-Trichloropropane ug/L 49.050 98 75-130
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 54.550 109 83-124
1,2-Dichlorobenzene ug/L 54.450 109 80-133
1,2-Dichloroethane ug/L 50.550 101 67-128
1,2-Dichloropropane ug/L 53.650 107 75-132
1,3-Dichloropropane ug/L 54.050 108 76-131
1,4-Dichlorobenzene ug/L 51.750 103 78-130
2-Butanone (MEK)ug/L 88.0J100 88 61-144
2-Hexanone ug/L 96.0100 96 68-143
4-Methyl-2-pentanone (MIBK)ug/L 89.7J100 90 72-135
Acetone ug/L 85.3J100 85 48-146
Acrylonitrile ug/L 243250 97 40-160
Benzene ug/L 58.350 117 80-125
Bromochloromethane ug/L 57.150 114 71-125
Bromodichloromethane ug/L 50.150 100 78-124
Bromoform ug/L 50.450 101 71-128
Bromomethane ug/L 51.650 103 40-160
Carbon disulfide ug/L 55.7J50 111 50-160
Carbon tetrachloride ug/L 54.950 110 69-131
Chlorobenzene ug/L 53.650 107 81-122
Chloroethane ug/L 53.750 107 39-148
Chloroform ug/L 49.250 98 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413616LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 51.150 102 44-146
cis-1,2-Dichloroethene ug/L 55.250 110 74-124
cis-1,3-Dichloropropene ug/L 49.350 99 72-132
Dibromochloromethane ug/L 49.850 100 78-125
Dibromomethane ug/L 53.350 107 82-120
Ethylbenzene ug/L 57.650 115 79-121
Iodomethane ug/L 117100 117 39-154
Methylene Chloride ug/L 54.050 108 64-133
Styrene ug/L 53.650 107 84-126
Tetrachloroethene ug/L 59.750 119 78-122
Tetrahydrofuran ug/L 489500 98 69-148
Toluene ug/L 56.350 113 80-121
trans-1,2-Dichloroethene ug/L 53.850 108 71-127
trans-1,3-Dichloropropene ug/L 50.350 101 69-141
trans-1,4-Dichloro-2-butene ug/L 44.6J50 89 40-160
Trichloroethene ug/L 57.250 114 78-122
Trichlorofluoromethane ug/L 46.250 92 53-137
Vinyl acetate ug/L 110100 110 40-160
Vinyl chloride ug/L 55.950 112 58-137
Xylene (Total)ug/L 167150 111 81-126
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1413618MATRIX SPIKE SAMPLE:
MSSpike
Result
92240549007
1,1,1,2-Tetrachloroethane ug/L 23.420 117 70-130ND
1,1,1-Trichloroethane ug/L 26.3 M120131 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,2-Trichloroethane ug/L 21.920 109 70-130ND
1,1-Dichloroethane ug/L 23.620 118 70-130ND
1,1-Dichloroethene ug/L 24.420 122 70-166ND
1,2,3-Trichloropropane ug/L 20.620 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 100 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.320 112 70-130ND
1,2-Dichlorobenzene ug/L 22.720 113 70-130ND
1,2-Dichloroethane ug/L 20.920 104 70-130ND
1,2-Dichloropropane ug/L 22.420 112 70-130ND
1,3-Dichloropropane ug/L 22.320 111 70-130ND
1,4-Dichlorobenzene ug/L 22.320 112 70-130ND
2-Butanone (MEK)ug/L 35.5J40 89 70-130ND
2-Hexanone ug/L 39.3J40 98 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.5J40 94 70-130ND
Acetone ug/L 38.9J40 86 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1413618MATRIX SPIKE SAMPLE:
MSSpike
Result
92240549007
Acrylonitrile ug/L 100J100 100 70-130ND
Benzene ug/L 24.820 124 70-148ND
Bromochloromethane ug/L 23.920 119 70-130ND
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 19.720 98 70-130ND
Bromomethane ug/L 22.720 113 70-130ND
Carbon disulfide ug/L 23.9J20 120 70-130ND
Carbon tetrachloride ug/L 26.4 M120132 70-130ND
Chlorobenzene ug/L 23.220 116 70-146ND
Chloroethane ug/L 23.520 117 70-130ND
Chloroform ug/L 20.720 104 70-130ND
Chloromethane ug/L 21.720 109 70-130ND
cis-1,2-Dichloroethene ug/L 23.520 118 70-130ND
cis-1,3-Dichloropropene ug/L 19.220 96 70-130ND
Dibromochloromethane ug/L 20.020 100 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Ethylbenzene ug/L 25.020 125 70-130ND
Iodomethane ug/L 44.640 111 70-130ND
Methylene Chloride ug/L 20.420 102 70-130ND
Styrene ug/L 22.620 113 70-130ND
Tetrachloroethene ug/L 26.5 M120133 70-130ND
Tetrahydrofuran ug/L 199200 99 70-130ND
Toluene ug/L 23.720 118 70-155ND
trans-1,2-Dichloroethene ug/L 23.520 118 70-130ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.8J20 99 70-130ND
Trichloroethene ug/L 24.820 124 69-151ND
Trichlorofluoromethane ug/L 23.320 116 70-130ND
Vinyl acetate ug/L 36.4J40 91 70-130ND
Vinyl chloride ug/L 24.820 124 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92240549006
1413617SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92240549006
1413617SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%121 1122
4-Bromofluorobenzene (S)%105 2106
Toluene-d8 (S)%97 196
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30789
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92240549008, 92240549009, 92240549010, 92240549011, 92240549012, 92240549013, 92240549014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1413730
Associated Lab Samples:92240549008, 92240549009, 92240549010, 92240549011, 92240549012, 92240549013, 92240549014
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 03/18/15 12:45
1,1,1-Trichloroethane ug/L ND 1.0 03/18/15 12:45
1,1,2,2-Tetrachloroethane ug/L ND 3.0 03/18/15 12:45
1,1,2-Trichloroethane ug/L ND 1.0 03/18/15 12:45
1,1-Dichloroethane ug/L ND 5.0 03/18/15 12:45
1,1-Dichloroethene ug/L ND 5.0 03/18/15 12:45
1,2,3-Trichloropropane ug/L ND 1.0 03/18/15 12:45
1,2-Dibromo-3-chloropropane ug/L ND 13.0 03/18/15 12:45
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/18/15 12:45
1,2-Dichlorobenzene ug/L ND 5.0 03/18/15 12:45
1,2-Dichloroethane ug/L ND 1.0 03/18/15 12:45
1,2-Dichloropropane ug/L ND 1.0 03/18/15 12:45
1,3-Dichloropropane ug/L ND 1.0 03/18/15 12:45
1,4-Dichlorobenzene ug/L ND 1.0 03/18/15 12:45
2-Butanone (MEK)ug/L ND 100 03/18/15 12:45
2-Hexanone ug/L ND 50.0 03/18/15 12:45
4-Methyl-2-pentanone (MIBK)ug/L ND 100 03/18/15 12:45
Acetone ug/L ND 100 03/18/15 12:45
Acrylonitrile ug/L ND 200 03/18/15 12:45
Benzene ug/L ND 1.0 03/18/15 12:45
Bromochloromethane ug/L ND 3.0 03/18/15 12:45
Bromodichloromethane ug/L ND 1.0 03/18/15 12:45
Bromoform ug/L ND 3.0 03/18/15 12:45
Bromomethane ug/L ND 10.0 03/18/15 12:45
Carbon disulfide ug/L ND 100 03/18/15 12:45
Carbon tetrachloride ug/L ND 1.0 03/18/15 12:45
Chlorobenzene ug/L ND 3.0 03/18/15 12:45
Chloroethane ug/L ND 10.0 03/18/15 12:45
Chloroform ug/L ND 5.0 03/18/15 12:45
Chloromethane ug/L ND 1.0 03/18/15 12:45
cis-1,2-Dichloroethene ug/L ND 5.0 03/18/15 12:45
cis-1,3-Dichloropropene ug/L ND 1.0 03/18/15 12:45
Dibromochloromethane ug/L ND 3.0 03/18/15 12:45
Dibromomethane ug/L ND 10.0 03/18/15 12:45
Ethylbenzene ug/L ND 1.0 03/18/15 12:45
Iodomethane ug/L ND 10.0 03/18/15 12:45
Methylene Chloride ug/L ND 1.0 03/18/15 12:45
Styrene ug/L ND 1.0 03/18/15 12:45
Tetrachloroethene ug/L ND 1.0 03/18/15 12:45
Tetrahydrofuran ug/L ND 10.0 03/18/15 12:45
Toluene ug/L ND 1.0 03/18/15 12:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1413730
Associated Lab Samples:92240549008, 92240549009, 92240549010, 92240549011, 92240549012, 92240549013, 92240549014
Matrix: Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 03/18/15 12:45
trans-1,3-Dichloropropene ug/L ND 1.0 03/18/15 12:45
trans-1,4-Dichloro-2-butene ug/L ND 100 03/18/15 12:45
Trichloroethene ug/L ND 1.0 03/18/15 12:45
Trichlorofluoromethane ug/L ND 1.0 03/18/15 12:45
Vinyl acetate ug/L ND 50.0 03/18/15 12:45
Vinyl chloride ug/L ND 1.0 03/18/15 12:45
Xylene (Total)ug/L ND 5.0 03/18/15 12:45
1,2-Dichloroethane-d4 (S)%112 70-130 03/18/15 12:45
4-Bromofluorobenzene (S)%98 70-130 03/18/15 12:45
Toluene-d8 (S)%96 70-130 03/18/15 12:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413731LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.150 106 80-125
1,1,1-Trichloroethane ug/L 57.050 114 71-129
1,1,2,2-Tetrachloroethane ug/L 47.850 96 79-124
1,1,2-Trichloroethane ug/L 50.750 101 85-125
1,1-Dichloroethane ug/L 52.850 106 73-126
1,1-Dichloroethene ug/L 55.450 111 66-135
1,2,3-Trichloropropane ug/L 48.150 96 75-130
1,2-Dibromo-3-chloropropane ug/L 52.750 105 71-133
1,2-Dibromoethane (EDB)ug/L 53.750 107 83-124
1,2-Dichlorobenzene ug/L 53.250 106 80-133
1,2-Dichloroethane ug/L 48.750 97 67-128
1,2-Dichloropropane ug/L 52.150 104 75-132
1,3-Dichloropropane ug/L 51.650 103 76-131
1,4-Dichlorobenzene ug/L 50.150 100 78-130
2-Butanone (MEK)ug/L 95.3J100 95 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 93.4J100 93 72-135
Acetone ug/L 93.2J100 93 48-146
Acrylonitrile ug/L 247250 99 40-160
Benzene ug/L 55.450 111 80-125
Bromochloromethane ug/L 53.650 107 71-125
Bromodichloromethane ug/L 48.050 96 78-124
Bromoform ug/L 48.650 97 71-128
Bromomethane ug/L 45.550 91 40-160
Carbon disulfide ug/L 52.8J50 106 50-160
Carbon tetrachloride ug/L 53.850 108 69-131
Chlorobenzene ug/L 51.350 103 81-122
Chloroethane ug/L 47.550 95 39-148
Chloroform ug/L 47.050 94 73-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413731LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 49.750 99 44-146
cis-1,2-Dichloroethene ug/L 53.650 107 74-124
cis-1,3-Dichloropropene ug/L 47.450 95 72-132
Dibromochloromethane ug/L 48.150 96 78-125
Dibromomethane ug/L 51.150 102 82-120
Ethylbenzene ug/L 54.950 110 79-121
Iodomethane ug/L 113100 113 39-154
Methylene Chloride ug/L 52.450 105 64-133
Styrene ug/L 51.150 102 84-126
Tetrachloroethene ug/L 57.050 114 78-122
Tetrahydrofuran ug/L 511500 102 69-148
Toluene ug/L 54.050 108 80-121
trans-1,2-Dichloroethene ug/L 54.450 109 71-127
trans-1,3-Dichloropropene ug/L 47.950 96 69-141
trans-1,4-Dichloro-2-butene ug/L 48.3J50 97 40-160
Trichloroethene ug/L 54.750 109 78-122
Trichlorofluoromethane ug/L 44.050 88 53-137
Vinyl acetate ug/L 109100 109 40-160
Vinyl chloride ug/L 53.950 108 58-137
Xylene (Total)ug/L 159150 106 81-126
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1413733MATRIX SPIKE SAMPLE:
MSSpike
Result
92240549014
1,1,1,2-Tetrachloroethane ug/L 22.620 113 70-130ND
1,1,1-Trichloroethane ug/L 25.520 128 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.520 97 70-130ND
1,1,2-Trichloroethane ug/L 20.820 104 70-130ND
1,1-Dichloroethane ug/L 22.220 111 70-130ND
1,1-Dichloroethene ug/L 24.420 122 70-166ND
1,2,3-Trichloropropane ug/L 20.120 101 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.820 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.620 108 70-130ND
1,2-Dichlorobenzene ug/L 22.520 112 70-130ND
1,2-Dichloroethane ug/L 20.220 101 70-130ND
1,2-Dichloropropane ug/L 22.120 110 70-130ND
1,3-Dichloropropane ug/L 21.320 106 70-130ND
1,4-Dichlorobenzene ug/L 22.620 112 70-130ND
2-Butanone (MEK)ug/L 34.1J40 85 70-130ND
2-Hexanone ug/L 38.9J40 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.4J40 89 70-130ND
Acetone ug/L 38.7J40 97 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1413733MATRIX SPIKE SAMPLE:
MSSpike
Result
92240549014
Acrylonitrile ug/L 91.9J100 92 70-130ND
Benzene ug/L 24.520 123 70-148ND
Bromochloromethane ug/L 23.420 117 70-130ND
Bromodichloromethane ug/L 19.920 99 70-130ND
Bromoform ug/L 19.020 95 70-130ND
Bromomethane ug/L 20.520 102 70-130ND
Carbon disulfide ug/L 23.0J20 115 70-130ND
Carbon tetrachloride ug/L 25.720 128 70-130ND
Chlorobenzene ug/L 22.520 112 70-146ND
Chloroethane ug/L 21.320 106 70-130ND
Chloroform ug/L 20.120 100 70-130ND
Chloromethane ug/L 21.320 106 70-130ND
cis-1,2-Dichloroethene ug/L 22.520 112 70-130ND
cis-1,3-Dichloropropene ug/L 18.420 92 70-130ND
Dibromochloromethane ug/L 19.520 97 70-130ND
Dibromomethane ug/L 21.220 106 70-130ND
Ethylbenzene ug/L 24.120 121 70-130ND
Iodomethane ug/L 42.840 107 70-130ND
Methylene Chloride ug/L 20.020 100 70-130ND
Styrene ug/L 21.520 108 70-130ND
Tetrachloroethene ug/L 25.520 127 70-130ND
Tetrahydrofuran ug/L 182200 91 70-130ND
Toluene ug/L 23.020 115 70-155ND
trans-1,2-Dichloroethene ug/L 22.520 112 70-130ND
trans-1,3-Dichloropropene ug/L 20.320 102 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.6J20 98 70-130ND
Trichloroethene ug/L 23.820 119 69-151ND
Trichlorofluoromethane ug/L 21.620 108 70-130ND
Vinyl acetate ug/L 36.7J40 92 70-130ND
Vinyl chloride ug/L 24.020 120 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92240549010
1413732SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92240549010
1413732SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%123 2121
4-Bromofluorobenzene (S)%107 1107
Toluene-d8 (S)%98 199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
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Huntersville, NC 28078
[phone]
Page 46 of 53
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92240549
YADKIN MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 53
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92240549
YADKIN MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92240549001 MPRP/18050 ICP/16229MW-1 EPA 3010 EPA 6010
92240549002 MPRP/18050 ICP/16229MW-2 EPA 3010 EPA 6010
92240549003 MPRP/18050 ICP/16229MW-3 EPA 3010 EPA 6010
92240549004 MPRP/18050 ICP/16229MW-4 EPA 3010 EPA 6010
92240549005 MPRP/18050 ICP/16229MW-5S EPA 3010 EPA 6010
92240549006 MPRP/18050 ICP/16229MW-5D EPA 3010 EPA 6010
92240549007 MPRP/18050 ICP/16229MW-6 EPA 3010 EPA 6010
92240549008 MPRP/18050 ICP/16229MW-7 EPA 3010 EPA 6010
92240549009 MPRP/18050 ICP/16229MW-8 EPA 3010 EPA 6010
92240549010 MPRP/18050 ICP/16229SW-1 EPA 3010 EPA 6010
92240549011 MPRP/18050 ICP/16229EBEPA 3010 EPA 6010
92240549012 MPRP/18050 ICP/16229FBEPA 3010 EPA 6010
92240549014 MPRP/18144 ICP/16304SW-2 EPA 3010 EPA 6010
92240549001 MSV/30788MW-1 EPA 8260
92240549002 MSV/30788MW-2 EPA 8260
92240549003 MSV/30788MW-3 EPA 8260
92240549004 MSV/30788MW-4 EPA 8260
92240549005 MSV/30788MW-5S EPA 8260
92240549006 MSV/30788MW-5D EPA 8260
92240549007 MSV/30788MW-6 EPA 8260
92240549008 MSV/30789MW-7 EPA 8260
92240549009 MSV/30789MW-8 EPA 8260
92240549010 MSV/30789SW-1 EPA 8260
92240549011 MSV/30789EBEPA 8260
92240549012 MSV/30789FBEPA 8260
92240549013 MSV/30789TBEPA 8260
92240549014 MSV/30789SW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 12:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 53
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Appendix B
Field Sampling Parameter Data Sheet(s)