7502_PolkCoCDLF_March2016_1stSemiAnnual_DIN27322_20160711

Prepared for
Polk County, North Carolina
Project Number 2036.13

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Spring 2016 Semiannual
Water Quality Monitoring Report
Polk County
Construction and Demolition Debris Landfill
and Municipal Solid Waste Landfill
Permit No. 75-02
Route 9, Polk County, North Carolina
July 11, 2016

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Table of Contents
1.0 Introduction .................................................................................................................... 1
2.0 C&D Landfill.................................................................................................................... 2
2.1 Sampling and Analysis Methods....................................................................................2
2.2 Analytical Results ..........................................................................................................3
2.2.1 Groundwater Samples ......................................................................................3
2.2.2 Surface Water Samples ....................................................................................4
3.0 MSW Landfill .................................................................................................................. 5
3.1 Sampling and Analysis Methods....................................................................................5
3.2 Analytical Results ..........................................................................................................5
4.0 Background Monitoring Well .......................................................................................... 7
4.1 Statistical Analysis Methodology ...................................................................................7
4.2 Results of Statistical Analysis ........................................................................................7
5.0 Summary ........................................................................................................................ 8
5.1 Future Activities .............................................................................................................8

Figures
1. Site Location Map
2. Site Layout Map
3. Groundwater Elevation Map
Tables
1. Summary of Groundwater Elevation Data—March 2016
2. Summary of Laboratory Analyses Performed on Samples
3. Summary of Detected Constituents
4. VOCs Background Well Comparison
5. Metals Background Well Comparison

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Appendices
A. Sampling Logs and Equipment Documentation and Instrument Calibration Data Sheets
B. Drilling Logs for Newly Installed Monitoring Wells MW-4 and MW-04CD
C. Report of Laboratory Analysis and Chain-of-Custody Documentation
D. Environmental Monitoring Reporting Form and Electronic Submittal of Environmental Monitoring
Data 7502Mar2016 (Electronic Format Only)

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1.0 Introduction
The Polk County Solid Waste Department (County) maintains two landfills at the Polk County Route 9 Landfill
Facility (Site), located on the west side of North Carolina Route 9, approximately 1.5 miles northwest of the
community of Mill Spring (Figure 1).
The northernmost landfill area is an inactive, closed, permitted Construction and Demolition Debris (C&D)
Landfill (Figure 2). The 3.5-acre C&D Landfill (formerly known as the “Operating Landfill”) was capped during
the summer of 2006, and a Closure Plan was submitted to Mr. James Coffey at the North Carolina
Department of Environment and Natural Resources (DENR), now known as the Department of Environmental
Quality (DEQ), on August 21, 2006.
The second landfill is a Municipal Solid Waste (MSW) Landfill composed of two discrete areas in the west-
central and southern parts of the Site (Figure 2). The MSW Landfill (formerly known as the “Closed Landfill”)
is inactive, closed, and maintained by the County. It was officially closed on April 9, 1994.
Both landfills are regulated by the DEQ, Division of Waste Management (DWM), under Permit No. 75-02
(Polk County C&D Landfill and MSW Landfill) as well as DEQ Solid Waste Management Rules Title 15A, North
Carolina Administrative Code (NCAC) Subchapter 13B, Section .0500 (C&D Landfill) and Title 15A NCAC
13B.1600 (MSW Landfill). The permit requires semiannual monitoring of groundwater and surface water
quality. This report is being submitted in accordance with the monitoring and reporting requirements stated
in the permit as well as the rules, and it provides an evaluation of surface water and groundwater quality for
the C&D Landfill and an evaluation of the groundwater quality for the closed MSW Landfill.
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2.0 C&D Landfill
2.1 Sampling and Analysis Methods
Four monitoring wells (MW-01CD, MW-02CD, MW-03CD, and newly installed monitoring well MW-04CD) and
three surface water locations (SS-1, SS-2, and SP-1) are monitored in association with the C&D Landfill. All
monitoring points, with the exception of MW-03CD, were sampled by Altamont Environmental, Inc. (Altamont)
on March 16 and 17, 2016. Monitoring well MW-04CD was installed in January 2016 to replace MW-03CD,
per the approval letter from Ms. Elizabeth Werner of the DEQ. The approximate locations of the groundwater
monitoring wells and surface water sampling points are shown on Figure 2. Field sampling logs are included
in Appendix A.
Monitoring wells MW-01CD, MW-02CD, and MW-04CD are constructed of 2-inch-diameter Schedule 40
polyvinyl chloride (PVC) well material. Well construction logs for MW-01CD and MW-02CD are not available.
The well construction log for MW-04CD is included in this report in Appendix B. Prior to sampling, water level
measurements were obtained. Table 1 and Figure 3 present the groundwater elevation data relative to an
assumed benchmark elevation.
Monitoring wells MW-01CD and MW-02CD were purged and sampled using a new, disposable polyethylene
bailer. Both wells were purged of three successive well volumes prior to sample collection. During purging,
the pH, specific conductivity, dissolved oxygen (DO), oxidation reduction potential (ORP), turbidity, and
temperature were measured and recorded at the start of purging and after each consecutive well volume
was purged. After the third consecutive well volume was purged, technicians collected a sample in
laboratory-supplied sample containers, while wearing a new pair of nitrile gloves.
Monitoring well MW-04CD was installed in January 2016. Due to limited time for well development and a
slow groundwater recharge rate for MW-04CD, technicians purged the well dry two times before sample
collection in order to further develop the well prior to sample collection. After purging the well dry for the
second time, the well was allowed to recharge for approximately 3 hours prior to sample collection.
Technicians collected a sample from MW-04CD in laboratory-supplied sample containers, while wearing a
new pair of nitrile gloves.
The surface water sample collected at the SS-1 location is representative of surface water quality upstream
of the landfill. The surface water sample collected at the SS-2 location is representative of surface water
quality downstream of the landfill. The surface water sample collected from the SP-1 location is
representative of surface water quality at a nearby spring that is situated at an elevation lower than the
landfill in an apparent downgradient direction (Figure 2). At each of these surface water sampling locations,
pH, specific conductivity, DO, ORP, turbidity, and temperature were measured and a grab sample was
collected by a technician wearing a new pair of nitrile gloves.
Collected groundwater and surface water samples were immediately placed on ice in sample coolers for
transport to the laboratory. Proper chain-of-custody documentation was maintained during the collection and
transport of each sample. A trip blank was also transported in the sample cooler and analyzed for Appendix I
volatile organic compounds (VOCs).
The groundwater and surface water samples were analyzed by TestAmerica Laboratories, Inc. (TestAmerica),
a laboratory certified in North Carolina, for Appendix I VOCs by United States Environmental Protection
Agency (EPA) Method 8260B and for Appendix I metals by EPA Methods 6010D, 6020B, and 7470A (Table
2). The report of laboratory analysis and chain-of-custody forms are included in Appendix C. Additional
observations and descriptions pertaining to individual wells are provided on the sampling logs that are
included in Appendix A. Additionally, water level measurements and field parameters are summarized in the
Electronic Data Deliverable (EDD) format included in Appendix D.
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2.2 Analytical Results
The laboratory analytical results for groundwater, surface water, and trip blank samples collected at the C&D
Landfill are provided in the report of laboratory analysis issued by TestAmerica and included in Appendix C.
In addition, all the laboratory analytical results are summarized in the EDD format specified by the Solid
Waste Section (SWS) on May 5, 2010.
As stipulated in the DWM document referenced above, all laboratory analytical results were reported and
appropriately qualified. Non-detections (non-detects), which are values reported by the laboratory as below
method detection limits (MDLs), are tabulated in Table 3 and the EDD, and are qualified with the “U”
qualifier. The MDL is the minimum concentration of a substance that can be measured and reported by a
laboratory with 99 percent confidence that the analyte concentration is greater than zero. All detections
(values above the MDL) were compared to analyte-specific Solid Waste Section Limits (SWSLs) established
by the SWS. The SWSL is the lowest concentration of an analyte in a sample that can be quantitatively
determined with suitable precision and accuracy. If the reported concentration is above the laboratory MDL
and below the method reporting limit (MRL), the analytical result is qualified by the laboratory as estimated,
and is flagged with a “J” qualifier (J-flag). The MRL is the minimum concentration of a target analyte that can
be accurately determined by the referenced method. If the reported concentration is above the laboratory
MRL and below the SWSL, the analytical result is qualified as estimated, and is flagged with an italicized “J”
qualifier (italicized J-flag) by Altamont per DEQ requirements. The MRL is listed in the “Report Limit” (RL)
column in the report of laboratory analysis (Appendix C). Concentrations below the respective SWSLs are not
discussed in the text of this report unless they exceed their contaminant-specific water quality standards.
Detected concentrations of analytes in groundwater samples were compared to current groundwater quality
standards specified in 15A NCAC 2L.0202, which are referred to as “2L standards”. Detected concentrations
of analytes in groundwater with no established 2L standards were compared either to the interim maximum
allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with 15A NCAC 02L
.0202 [c]) or Groundwater Protection (GWP) Standards, pursuant to 15A NCAC 13B.1634. Detections of
analytes in surface-water samples were compared to 15A NCAC 2B surface-water quality standards (2B
standards).
Table 3 presents the summary of laboratory analytical results for detected constituents only. Also outlined in
Table 3 are detections that were above their applicable SWSLs, as well as any analytes that exceeded their
respective 2L standards (including IMACs, if applicable), GWP Standards, or 2B standards.
In the EDD (Appendix D), the identification of a well (“WELL ID” on the table) consists of the name of the well
prefaced by the un-hyphenated permit number for the facility. For example, the groundwater sample from
monitoring well MW-01CD is identified on the tables as 7502-MW01CD. However, in the tables and figures
of this report, the identification of a well consists of the name of the well without the permit number
associated with the facility.
2.2.1 Groundwater Samples
Ten metals were detected in one or more of the groundwater samples collected from the monitoring wells at
the C&D landfill. Eight of the detected metals (barium, beryllium, chromium, cobalt, copper, lead, vanadium,
and zinc) were detected at concentrations above their respective SWSLs in one or more groundwater
samples collected from the monitoring wells (Table 3). In addition, chromium, cobalt, lead, and vanadium
exceeded their respective 2L standards or IMAC in one or more groundwater samples collected at the C&D
landfill (Table 3). Vanadium exceeded its IMAC in all of the groundwater samples collected from the
monitoring wells at the C&D Landfill. Chromium, cobalt, and lead exceeded their respective 2L standards or
IMAC in only monitoring well MW-04CD. The referenced exceedances in MW-4 are likely due to high turbidity
levels that are a result of limited water production. Lack of water production has led to the inability to fully
develop this monitoring well.
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Two VOCs were detected in one or more of the groundwater samples collected at the C&D Landfill. No VOCs
were detected at concentrations above their respective SWSLs (Table 3) or water quality standards.
Groundwater pH readings were obtained from all monitoring wells sampled. The measured groundwater pH
value in MW-01CD, MW-02CD, and MW-04CD were outside the 2L standard pH range of 6.5 to 8.5 Standard
Units (SU) (Table 3).
Turbidity values at the time of sampling monitoring wells MW-01CD and MW-02CD were 22.1 nephelometric
turbidity units (NTUs) and 90.7 NTUs, respectively (Table 3). At the time of sampling MW-04CD, the turbidity
was too high to register on the turbidity meter, and is reflected as “Out of range” in Table 3. MW-04CD will
require continued development in order to remove sediment left in the well from the drilling process.
2.2.2 Surface Water Samples
Four metals were detected in one or more surface water samples collected at designated sampling locations
(Table 3). Lead exceeded its 2B surface water standard in surface water samples SP-1 and SS-2. Both
results are flagged with a “J” qualifier in the analytical report, which indicates the results are estimated by
the laboratory.
No VOCs were detected in any of the collected surface water samples (Table 3).
The pH readings obtained from all sampled locations were within the 2B standard range of 6.00 to 9.00 SU
(Table 3).
Turbidity values measured in the surface water samples ranged from 3.95 NTUs (SP-1) to 9.27 NTUs (SS-1)
(Table 3). These values were all below the 2B surface water standard of 25 NTUs.

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3.0 MSW Landfill
3.1 Sampling and Analysis Methods
During the spring 2016 sampling event, monitoring wells MW-2R, MW-3R, and MW-4 were sampled by
Altamont on March 16 and 17, 2016. Monitoring well was installed to replace MW-1, per the approval letter
from Ms. Elizabeth Werner of the DEQ. The approximate locations of the groundwater monitoring wells are
shown on Figure 2. Field sampling logs are included in Appendix A.
Monitoring wells MW-2R and MW-4 were purged and sampled using low-flow techniques in accordance with
the procedures described in “Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures”
(Groundwater Issues [EPA April 1996]). During purging, the pH, specific conductivity, DO, ORP, turbidity, and
temperature were measured and recorded approximately every 3 minutes. Well purging continued until
these parameters stabilized, as determined by three successive readings in which each parameter was
within a range of values, as follows:
 pH +/- 0.1 unit
 Specific conductivity +/- 3 percent
 Temperature +/- 10 percent
 DO +/- 10 percent
 Turbidity +/- 10 percent
 ORP +/- 10 millivolts
Once all these parameters stabilized, a groundwater sample was collected in laboratory-supplied sample
containers by a technician wearing a new pair of nitrile gloves. A duplicate sample was taken at MW-2R to
ensure consistency with laboratory practices, and is listed as MW-2RDUP.
The wells MW-1R, MW-2R, and MW-4 are constructed of 2-inch-diameter Schedule 40 PVC well material.
Well construction logs for MW-1R and MW-2R are not available. The well construction record for the
monitoring well MW-3R is available and was included in Appendix D of the Fall 2012 Semiannual Water
Quality Monitoring Report. The well construction record for the newly installed monitoring well MW-4 is
available and is included in Appendix B of this report.
Prior to sampling the wells, field parameters and water level measurements were obtained. Table 1 and
Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation. Field
parameters are presented in the sampling logs (Appendix A) and in the EDD (Appendix D).
Monitoring well MW-3R was pumped dry using a Grundfos Redi Flow 2 pump on March 15, 2016 and the
groundwater sample was collected following recharge the next day, March 16, 2016.
Proper chain-of-custody documentation procedures were followed during collection and transport of the
samples. Analysis of the groundwater samples was performed by TestAmerica using the same methods
described in Section 2.1 (Table 2). Additional observations and descriptions pertaining to individual wells are
provided on the sampling logs included in Appendix A.
3.2 Analytical Results
Three metals were detected in one or more of the groundwater samples collected from the monitoring wells.
Of the detected metals, barium was present at concentrations above the SWSL in one or more groundwater
samples collected from the monitoring wells (Table 3). Cobalt exceeded its IMAC in monitoring well MW-4
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(Table 3). Vanadium exceeded its IMAC in all of the samples collected from monitoring wells associated with
the MSW Landfill.
Five VOCs were detected in one or more of the groundwater samples collected from the monitoring wells
(Table 3). Cis-1,2-dichloroethene was detected above the SWSL, but below the applicable 2L groundwater
standard in the samples collected from MW-2R. None of the VOCs were present at concentrations above
established 2L groundwater quality standards.
The measured pH was below the acceptable range established as the 2L standard in MW-2R and MW-4.
Refer to Table 3 for sample results.
Turbidity values at the time of sampling monitoring wells MW-2R, MW-3R, and MW-4 ranged from 1.61 NTUs
to 14.7 NTUs (Table 3).
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4.0 Background Monitoring Well
4.1 Statistical Analysis Methodology
In 2012, background monitoring well, MW-3R, was installed upgradient of the other two MSW monitoring
wells and three C&D monitoring wells. MW-3R was installed to establish background concentrations of
Appendix I VOCs and metals upgradient of the MSW Landfill and C&D Landfill. MW-3R, consistent with the
other five monitoring wells, is sampled on a semiannual basis. MW-3R has been sampled eight times from
October 2012 to March 2016.
A brief statistical analysis presented herein compares background concentrations in MW-3R to downgradient
monitoring wells, and applicable groundwater standards. Historical data was summarized for MW-01CD,
MW-02CD, MW03CD, MW-1R, and MW-2R from the eight sampling events occurring from September 2012
to March 2016. As previously noted in this report, MW-03CD and MW-1R were not sampled during this
event. Data from newly installed monitoring wells MW-4 and MW-04CD is included in the summary, as this
event was the first time these monitoring wells have been sampled. Data from MW-3R was summarized from
the eight sampling events occurring from October 2012 to March 2016. Tables 4 and 5 list the constituents
detected in each well for the subject monitoring period, minimum concentration, maximum concentration,
and average concentration of each detected constituent, as well as the frequency of detection in each well.
Results below the MDL were assumed to equal half of the MDL.
4.2 Results of Statistical Analysis
A comparison of VOCs is presented in Table 4. No VOCs were detected in the background well (MW-3R)
during the subject statistical analysis period. Seven VOCs (1,1-dichloroethane, 1,4-dichlorobenzene,
chlorobenzene, cis-1,2-dichloroethene, tetrahydrofuran, trichloroethene, and trichlorofluoromethane) were
detected in one or more of the downgradient monitoring wells. However, all detections were at
concentrations below the respective 2L standards. A comparison of the average concentrations of VOCs in
downgradient wells with the average concentrations of VOCs in the background well shows that the majority
of average concentrations in downgradient wells exceed those of the background well.
A comparison of metals is presented in Table 5. Barium was detected in MW-3R at concentrations below
groundwater quality standards. Vanadium was detected below its SWSL, but above its IMAC standard in
MW-3R. Ten metals (barium, beryllium, cadmium, chromium, cobalt, copper, lead, nickel, vanadium, and
zinc) were detected in one or more of the downgradient monitoring wells. Five of the average concentrations
of these metals (cobalt, chromium, lead, thallium, and vanadium) exceeded groundwater quality standards
in one or more downgradient monitoring wells. Additionally, average concentrations for the majority of
metals in downgradient monitoring wells exceeded the average concentrations of those metals in the
background well.

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5.0 Summary
Altamont completed the first semiannual water quality monitoring event of 2016 at the Polk County Landfills
on March 15, 16, and 17, 2016.
Table 3 of this report, the TestAmerica report of laboratory analysis (Appendix C), and the EDD (Appendix D)
provide detailed analytical results and field data demonstrating the groundwater and surface water quality at
the Polk County Landfills.
Results for the newly installed replacement monitoring wells (MW-04CD and MW-4) are somewhat mixed.
Monitoring well MW-4 produces adequate water and exhibits lower turbidity levels than those typically
measured in the monitoring well that it replaced—MW-1R. As a result, metals concentrations in the sample
collected from MW-4 were lower than the average metals concentrations historically measured in monitoring
well MW-1R. In contrast, MW-04CD compares closely to the monitoring well that it replaced (MW-03CD) in
terms of water production. Consequently, this monitoring well has been difficult to fully develop, resulting in
highly turbid samples.
5.1 Future Activities
Altamont recommends that Polk County continues to monitor VOCs and metals concentrations in
groundwater and surface water at the closed C&D and MSW landfills. Based on the data trends and
evaluation presented in this report, Altamont has discussed with Polk County options for addressing the
water quality impacts identified at the Site. Based on these discussions, Altamont proposes to continue to
purge monitoring well MW-04CD during each visit to the Site, which includes quarterly landfill gas
measurements and semiannual sampling events. Additionally, Altamont intends to prepare a letter to the
DEQ to request the use of no-purge sampling methodology for monitoring well MW-04CD.
Altamont will continue to monitor the groundwater and surface water on a semiannual basis at the Polk
County C&D and MSW Landfills. The next sampling event is scheduled for September 2016.

FIGURES

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
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

1

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




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Inactive Closed
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
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


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


¦


!U 




P:\POLK COUNTY\ROUTE 9 LF\FIGURES\2015\SPRING\7502MARCH2015 FIGURE 2-SITE LAYOUT MAP.MXD0300600150

!U
!U
E
E
E
Transfer Station
Scale Station
Inactive C & D Landfill
Inactive Closed
MSW Landfill Cell
Inactive Closed
MSW Landfill Cell
!U
MW-4
MW-1R
2,842.96
MW-2R
2,807.12
MW-03CD
2,852.63
MW-04CD
MW-02CD
2,832.21
MW-01CD
2,846.19
SS-1
SP-01
SS-2
MW-3R
2,886.82
!U!U
!U
!U
!U
!U
!U
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NC
9

H
W
Y
GA
R
R
E
T
T

R
D
LANDFILL RD
B
U
R
T

B
L
A
C
K
W
E
L
L

R
D
MARTIN WALKER R
D
G
R
E
E
N

H
I
L
L
S

R
D
KEL
S
E
Y

L
N
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

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
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
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Feet


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
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
E


TABLES

Table 1
Summary of Groundwater Elevation Data---March 2016
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Top Of Casing (TOC)
Elevation (From
Assumed Datum)
Depth To Water Groundwater
Elevation
(feet) (feet TOC)(feet)
C&D Landfill
MW-01CD 2,955.50 109.31 2,846.19
MW-02CD 2,951.90 119.69 2,832.21
MW-03CD 2,969.60 116.97 2,852.63
MW-04CD NM 132.42 NA
MSW Landfill
MW-1R 2,867.70 24.74 2,842.96
MW-2R 2,837.20 30.08 2,807.12
MW-3R 2,962.00 75.18 2,886.82
MW-4 NM 8.15 NA
Notes:
C&D Construction and Demolition
MSW Municipal Solid Waste
Elevation Datum
Well Survey
MW-4 & MW-04CD
Depth to Water
NM Not measured
NA Not available
Monitoring wells MW-1R and MW-2R were surveyed on November 13,
2010. MW-3R was surveyed on November 8, 2012. Remaining wells
were surveyed on December 9, 2006. All wells were surveyed by Wes
Cole Land Surveying, PA.
Installed in January 2016. These wells have not yet been surveyed.
Measured on May 9, 2016 for all monitoring wells.
Well ID
All elevations were based on an assumed datum of 3,000 feet.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\7502March2016 T1 GW Elevation Data Page 1 of 1
Table 2
Summary of Laboratory Analyses Performed on Samples
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
GROUNDWATER SAMPLES
VOCs
EPA 8260B EPA 6010D EPA 6020B EPA 7470A
C&D Landfill
75-02 MW-01CD 3/16/2016 X X X X
75-02 MW-02CD 3/16/2016 X X X X
75-02 MW-04CD 3/17/2016 X X X X
MSW Landfill
75-02 MW-2R 3/17/2016 X X X X
75-02 MW-2RDUP 3/17/2016 X X X X
75-02 MW-3R 3/16/2016 X X X X
75-02 MW-4 3/16/2016 X X X X
SURFACE WATER SAMPLES
VOCs
EPA 8260B EPA 6010D EPA 6020B EPA 7470A
C&D Landfill
75-02 SP-1 3/16/2016 X X X X
75-02 SS-1 3/16/2016 X X X X
75-02 SS-2 3/16/2016 X X X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
75-02 TRIP BLANK 3/16/2016 X
Notes:
VOCs
Analyses
MW-04CD
and MW-4
Volatile organic compounds
VOCs and metals analyses include Appendix I constituents per 40 CFR Part 258
Installed in January 2016. These wells were sampled for the first time during this sampling event, and
replaced monitoring wells MW-03CD and MW-1R, respectively.
Facility
Permit Sample ID Collect Date
Facility
Permit Sample ID Collect Date
Metals
Metals
Facility
Permit Well ID Collect Date
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\7502March2016 T2, T3 Page 1 of 1
Table 3
Summary of Detected Constituents
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Metals (Appendix I)VOCs (Appendix I)Field Parameters
Laboratory Certification 387 387
Laboratory Methods EPA 6010D, EPA 6020B, EPA 7470A EPA 8260B 5445 (pH only)
Parameter Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Vanadium Zinc
1,1-
Dichloro-
ethane
1,4-
Dichloro-
benzene
Chloro-
benzene
cis-1,2-
Dichloro-
ethene
Tetrahydro-
furan
Trichloro-
ethene
Trichloro-
fluoro-
methane
pH Turbidity
CAS Number 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7440-62-2 7440-66-6 75-34-3 106-46-7 108-90-7 156-59-2 109-99-9 79-01-6 75-69-4 SW320 SW330
SWS ID 15 23 34 51 53 54 131 152 209 213 75 71 39 78 458 201 203 320 330
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Groundwater Samples
C&D Landfill
MW-01CD 3/16/2016 34.4 J 1.00 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 3.00 U 12.8 B, J 10.0 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.396 J 6.46 22.1
MW-02CD 3/16/2016 258 1.00 U 0.500 U 3.00 U 1.31 J 5.00 U 6.00 J 3.00 U 15.9 B, J 14.6 J 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.400 J 5.61 90.7
MW-04CD 3/17/2016 645 1.73 J 0.700 J 58.8 23.9 35.2 28.6 25.9 J 74.5 B 90.0 0.240 U 0.170 U 0.180 U 0.210 U 2.91 J 0.200 U 0.496 J 6.25 Out of range
MSW Landfill
MW-2R 3/17/2016 115 1.00 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 3.00 U 8.87 B, J 10.0 U 0.446 J 0.170 U 0.180 U 6.85 0.820 U 0.536 J 0.210 U 5.91 2.44
MW-2RDUP 3/17/2016 116 1.00 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 3.00 U 8.25 B, J 10.0 U 0.360 J 0.170 U 0.180 U 6.88 0.820 U 0.561 J 0.210 U 5.91 2.44
MW-3R 3/16/2016 8.6 J 1.00 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 3.00 U 8.27 B, J 10.0 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.210 U 7.22 1.61
MW-4 3/16/2016 297 1.00 U 0.500 U 3.00 U 2.38 J 5.00 U 2.00 U 3.00 U 11.5 B, J 10.0 U 0.240 U 0.530 J 0.262 J 1.28 J 0.820 U 0.200 U 0.210 U 5.76 14.7
Surface Water Samples
SP-1 3/16/2016 94.4 J 1.00 U 0.500 U 3.00 U 1.29 J 5.00 U 2.80 J 3.00 U 9.24 B, J 10.0 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.210 U 6.82 3.95
SS-1 3/16/2016 35.1 J 1.00 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 3.00 U 11.9 B, J 10.0 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.210 U 7.25 9.27
SS-2 3/16/2016 31.8 J 1.00 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 J 3.00 U 11.9 B, J 10.0 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.210 U 7.38 7.41
Quality Control Samples
TripBlank 3/16/2016 NA NA NA NA NA NA NA NA NA NA 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 0.210 U NA NA
MDL 5.00 1.00 0.500 3.00 0.500 5.00 2.00 3.00 2.10 10.0 0.240 0.170 0.180 0.210 0.820 0.200 0.210 NA NA
MRL 10 2.0 1.0 5.0 2.0 10.0 5.0 10 4.0 25 1.0 1.0 1.0 1.0 10 1.0 1.0 NA NA
SWSL 100 1 1 10 10 10 10 50 25 10 5 1 3 5 NE 1 1 NE NE
2L 700 NE 2 10 NE 1,000 15 100 NE 1,000 6 6 50 70 NE 3 2,000 6.5-8.5 NE
IMAC NE 4 NE NE 1 NE NE NE 0.3 NE NE NE NE NE NE NE NE NE NE
GWP NE 4 NE NE 1 NE NE NE 0.3 NE NE NE NE NE NE NE NE NE NE
2B 200,000 6.5 0.15 35 4 2.7 0.54 16 NE 36 100 100 140 720 NE 3 67,000 6.0-9.0 25
Notes:
Parameters Only detected constituents are listed on this table. Please refer to TestAmerica Report of Laboratory Analysis (Appendix B) for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for a compound that was found in both the laboratory blank and the sample.
2L
IMAC Interim maximum allowable concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
GWP
2B Surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards," (last amended March, 2016) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
NE Not Established.
NA Not Applicable.
258 Indicates a result in exceedance of the SWSL.
6.46 Indicates a result in exceedance of the 2L, IMAC, GWP, or 2B standard.
MW-04CD & MW-4 Sampled for the first time during this sampling event.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ (Amended April 1, 2013).
Groundwater Protection standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-list (last updated June,
2011). GWP standard is used only if 2L or IMAC standards are not established for specific constituent.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\7502March2016 T2, T3 Page 1 of 1
Table 4
VOCs Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
1/8 Acetone 1.41 U 10 U 3.26 6,000
8/8 Trichlorofluoromethane 0.28 J 0.65 J 0.42 2,000
1/4 Acetone 2.53 J 2.66 U 1.63 6,000
3/4 Trichlorofluoromethane 0.210 U 0.42 J 0.30 2,000
1/4 Xylene (Total)0.38 U 0.58 U 0.31 500
1/7 1,2-Dichlorobenzene 0.12 U 0.30 U 0.14 20
2/7 1,4-Dichlorobenzene 0.288 J 0.463 U 0.22 6
2/7 Acetone 2.66 U 10 U 4.12 6,000
2/6 Tetrahydrofuran 2.53 J 7.04 J 2.63 NE
7/7 Trichlorofluoromethane 0.301 J 0.52 J 0.39 2,000
1/7 Xylene (Total)0.38 U 0.66 U 0.34 500
1/1 Tetrahydrofuran 2.91 J 2.91 J 2.91 NE
1/1 Trichlorofluoromethane 0.496 J 0.496 J 0.50 2,000
1/7 1,4-Dichlorobenzene 0.17 J 0.33 U 0.14 6
2/7 cis-1,2-Dichloroethene 0.19 U 2.0 J 0.62 70
1/6 Tetrahydrofuran 0.82 U 3.1 U 1.39 NE
11/15 1,1-Dichloroethane 0.24 U 1.06 J 0.56 6
14/15 cis-1,2-Dichloroethene 5.2 13.9 10.17 70
3/15 Tetrachloroethene 0.14 U 0.46 U 2.06 0.7
14/15 Trichloroethene 0.47 U 1.56 0.96 3
1/15 Vinyl chloride 0.1 J 0.62 U 0.19 0.03
0/8 1,1-Dichloroethane 0.215 U 0.32 U 0.14 6
0/8 1,2-Dichlorobenzene 0.19 U 2.5 U 0.27 20
0/8 1,4-Dichlorobenzene 0.17 U 0.463 U 0.14 6
0/8 cis-1,2-Dichloroethene 0.19 U 0.299 U 0.11 70
0/8 Acetone 1.41 U 10 U 3.09 6,000
0/8 Tetrachloroethene 0.14 U 0.46 U 0.16 0.7
0/8 Tetrahydrofuran 0.82 U 3.1 U 1.06 NE
0/8 Trichloroethene 0.2 U 0.47 U 0.17 3
0/8 Trichlorofluoromethane 0.139 U 0.48 U 0.11 2,000
0/8 Vinyl chloride 0.18 U 0.62 U 0.20 0.03
0/8 Xylene (Total)0.298 U 0.66 U 0.28 500
1/1 1,4-Dichlorobenzene 0.530 J 0.530 J 0.53 6
1/1 cis-1,2-Dichloroethene 1.28 1.28 1.28 70
1/1 Chlorobenzene 0.262 J 0.262 J 0.26 50
Notes:
µg/L micrograms per liter
Min.minimum concentration (µg/L)
Max.maximum concentration (µg/L)
Avg.
2L
IMAC The IMAC concentrations listed in Appendix #1 of Subchapter 2L.
U A laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
J A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
NA not applicable
# Detections
MW-02CD Only sampled in September 2012, March 2015, September 2015, and March 2016 due to a lack of well recharge during other sampling events.
MW-2R
MW-3R The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-4 and
MW-04CD
Installed in January 2016 and were sampled for the first time during the March 2016 event.
MW-1R and
MW-03CD
Not sampled during the March 2016 event.
MW-1R
MW-2R had duplicate samples collected during 7 of the 8 sampling events, thus there are 15 total samples representing MW-2R.
Average concentration (µg/L). Average concentrations were calculated by summing the constituent detections and dividing by the number of samples. When the
sample was below the MDL, half of the MDL value was used as the result. Results flagged with a "J" are estimated average concentrations.
Groundwater standard from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater
Classifications and Standards," DENR (Amended April 1, 2013).
Number of times the constituent was detected during the sample collection period.
MW-4
MW-2R (and
MW-2RDUP)
MW-3R
MW-01CD
MW-04CD
MW-03CD
September 2012 - March 2016
Well # Detections Detected Constituents Concentration (µg/L)2L Standard or
IMAC
MW-02CD
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\Statistics_Background March 2016 Page 1 of 1
Table 5
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
8/8 Barium 12.5 J 104 40.8 700
1/8 Beryllium 0.5 U 1.0 U 0.43 4
1/8 Cadmium 0.3 J 1.0 U 0.35 2
1/8 Chromium 2.5 U 5.0 U 2.07 10
1/8 Cobalt 0.5 U 5.0 U 1.85 1
2/8 Copper 2.5 U 8.30 J 3.67 1,000
3/8 Lead 2.5 U 7.72 J 3.97 15
1/8 Silver 2.5 U 5.02 J 2.25 20
2/8 Thallium 0.019 U 0.641 U 0.16 0.2
3/8 Vanadium 1.8 J 12.8 J 4.31 0.3
4/8 Zinc 10.0 U 105 20.35 1,000
4/4 Barium 41.0 J 627 251.40 700
1/4 Beryllium 0.5 U 1.58 J 0.66 4
2/4 Cadmium 0.3 J 1.5 0.58 2
2/4 Chromium 3.0 U 3.66 J 2.52 10
2/4 Cobalt 1.31 J 6.1 J 2.90 1
2/4 Copper 5.0 U 5.52 J 3.88 1,000
3/4 Lead 2.0 U 30.7 12.15 15
1/4 Nickel 3.0 U 3.9 J 2.11 100
1/4 Silver 2.5 U 4.99 J 2.31 20
1/4 Thallium 0.2 U 0.641 U 0.32 0.2
3/4 Vanadium 1.6 J 43.6 16.53 0.3
3/4 Zinc 10 U 38.8 18.50 1,000
7/7 Barium 184 768 362.7 700
2/7 Beryllium 0.570 J 1.7 0.62 4
4/7 Chromium 3.0 U 20.3 6.89 10
3/7 Cobalt 3.39 U 10.1 3.79 1
4/7 Copper 5.0 U 21.8 8.80 1,000
4/7 Lead 5.0 U 18.6 7.42 15
4/7 Nickel 3.0 U 10.9 J 5.85 100
1/7 Silver 2.5 U 5.97 J 2.50 20
6/7 Thallium 0.026 J 0.644 J 0.23 0.2
7/7 Vanadium 4.0 J 54 16.35 0.3
7/7 Zinc 13.1 J 223 52.26 1,000
September 2012 - March 2016
MW-01CD
MW-03CD
MW-02CD
# Detections
Concentration (µg/L)
Detected Constituents
2L Standard or IMAC
Well
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\Statistics_Background March 2016 Page 1 of 3
Table 5
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
September 2012 - March 2016
MW-01CD
# Detections
Concentration (µg/L)
Detected Constituents
2L Standard or IMAC
Well
1/1 Barium 645 645 645 700
1/1 Beryllium 1.73 J 1.73 J 1.73 4
1/1 Cadmium 0.70 J 0.70 J 0.70 2
1/1 Chromium 58.8 58.8 58.8 10
1/1 Cobalt 23.9 23.9 23.9 1
1/1 Copper 35.2 35.2 35.2 1,000
1/1 Lead 28.6 28.6 28.6 15
1/1 Nickel 25.9 25.9 25.9 100
0/1 Silver 3.0 U 3.0 U 1.50 20
0/1 Thallium 0.5 U 0.5 U 0.25 0.2
1/1 Vanadium 74.5 74.5 74.5 0.3
1/1 Zinc 90.0 90.0 90.0 1,000
1/7 Arsenic 2.5 U 25.6 4.11 10
7/7 Barium 41.4 J 2,270 350.71 700
3/7 Beryllium 0.50 U 13.3 1.27 4
3/7 Cadmium 0.3 J 5.8 0.79 2
3/7 Chromium 2.5 U 51.5 5.34 10
3/7 Copper 2.5 U 122 11.30 1,000
3/7 Lead 2.0 U 64.7 6.52 15
3/7 Nickel 2.5 U 29.1 J 3.96 100
1/7 Silver 2.5 U 5.0 U 2.00 20
3/7 Thallium 0.025 U 1.2 J 0.17 0.2
4/7 Vanadium 2.5 U 407 32.67 0.3
6/7 Zinc 10 U 428 12.24 1,000
15/15 Barium 63.3 J 217 153.49 700
1/15 Cadmium 0.155 U 1.0 U 0.33 2
2/15 Chromium 2.5 U 5.0 U 2.07 10
2/15 Copper 2.5 U 7.01 J 2.92 1,000
2/15 Lead 2.0 U 5.41 U 2.26 15
1/15 Nickel 2.5 U 5.0 U 1.96 100
2/15 Silver 2.5 U 5.88 J 2.28 20
1/15 Thallium 0.019 U 0.641 U 0.11 0.2
4/15 Vanadium 0.2 U 8.87 J 2.53 0.3
6/15 Zinc 10.0 U 19.5 9.51 1,000
MW-04CD
MW-2R (and MW-
2RDUP)
MW-1R
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\Statistics_Background March 2016 Page 2 of 3
Table 5
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
September 2012 - March 2016
MW-01CD
# Detections
Concentration (µg/L)
Detected Constituents
2L Standard or IMAC
Well
0/8 Arsenic 3.69 U 10.0 U 3.16 10
7/8 Barium 3.25 J 12.3 J 6.79 700
0/8 Beryllium 0.13 U 1.0 U 0.35 4
1/8 Cadmium 0.04 J 1.0 U 0.32 2
1/8 Chromium 2.02 J 5.0 U 1.91 10
0/8 Cobalt 3.39 U 5.0 U 1.96 1
0/8 Copper 0.672 U 5.0 U 2.07 1,000
1/8 Lead 2.0 U 5.41 U 2.14 15
0/8 Nickel 2.5 U 5.0 U 1.85 100
0/8 Silver 1.05 U 5.0 U 1.66 20
0/8 Thallium 0.019U 0.641 U 0.10 0.2
2/8 Vanadium 0.2 U 8.27 J 1.61 0.3
0/8 Zinc 2.26 U 10.0 U 4.20 1,000
0/1 Arsenic 8.6 U 8.6 U 4.30 10
1/1 Barium 297 297 297 700
0/1 Beryllium 1.0 U 1.0 U 0.50 4
0/1 Cadmium 0.5 U 0.5 U 0.25 2
0/1 Chromium 3.0 U 3.0 U 1.50 10
0/1 Copper 5.0 U 5.0 U 2.50 1,000
1/1 Cobalt 2.38 J 2.38 J 2.38 1
0/1 Lead 2.0 U 2.0 U 1.00 15
0/1 Nickel 3.0 U 3.0 U 1.50 100
0/1 Silver 3.0 U 3.0 U 1.50 20
0/1 Thallium 0.5 U 0.5 U 0.25 0.2
1/1 Vanadium 11.5 J 11.5 J 11.5 0.3
0/1 Zinc 10.0 U 10.0 U 5.00 1,000
Notes:
µg/L micrograms per liter
Min.Minimum concentration (µg/L).
Max.Maximum concentration (ug/L).
Avg.
2L
IMAC Interim maximum allowable concentration. Concentrations are listed in Appendix #1 of the 2L.
U A laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
J A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
NA not applicable
# Detections
1.85 Indicates result above 2L Standard or IMAC.
MW-02CD
MW-3R The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-4 and MW-04CD Monitoring wells MW-4 and MW-04CD were installed in January 2016 and were sampled for the first time during the March 2016 event.
MW-1R and MW-03CD Monitoring wells MW-1R and MW-03CD were not sampled during the March 2016 event.
Average concentration (µg/L). Average concentrations were calculated by summing the constituent detections and dividing by the number of samples. When
the sample was below the MDL, half of the MDL value was used as the result. Results flagged with a "J" are estimated averages.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2L -
Groundwater Classifications and Standards," DENR (Amended April 1, 2013).
Number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples collected during 7 of the 8 sampling
events, thus there are 15 total samples representing MW-2R.
MW-02CD was only sampled in September 2012, March 2015, September 2015, and March 2016 due to a lack of well recharge during subsequent
sampling events.
MW-4
MW-3R
P:\Polk County\Route 9 LF\Analytical & Data\Water\2016\Spring\Tables\Statistics_Background March 2016 Page 3 of 3

APPENDICES

APPENDIX A

Sampling Logs and
Equipment Documentation and
Instrument Calibration Data Sheets

APPENDIX B

Drilling Logs for Newly Installed
Monitoring Wells MW-4 and MW-04CD

WELL CONSTRUCTION RECORD
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2S93A
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SAEDACCO Inc
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\"at~r SUIII,I,~'Well:oo'\g.rkuJmral
DGroillenllal (lieminglCooling Supply)
o1l1dus'ri~VCol1lmercial
OMlIlli;,;i~t.liPnblic
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ORc:;i\'kmial Wilier Supply (S!~lrOO)
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5~. Well Location:
POLK COUNTY TRANFER STATION
rao;:!li1~•.O~\rcr NUII~
MW-4R
FaOllil~'lD#if aJlPIX',lbl~1
322 LANDFILL RD, MILL SPRING,NC, 28756
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23. Site d~rlllIi or additional well details;You mar use lbe back of this page to provide 'lddilional well sue detail·or well
construction d~lails.You Ifill)'also illiadl adLlitional pages if necessary.
SUBMITTAL INSTHCTIONS
2-1a.~'Dr All Wdl~: Submil Ibis Fortn within 3D'davs of complerio of well
consrrnctlon to lIte ,oltOni n!r
Dh'i~ilm ufWat~r Resources, hlruruulfiulll'm4!cssjn~ Unit
1617 M.aH Service Center,Rale~,~C 2/69'J-1617
2.Jb.for Jllj~n"Wells ONL Y:III addinon [0sending Ille form to tJ.~address inUOlabo\e.also submit a copy of this form \Iilliin ~O days of compl lion of well
ceustruction [0 llieIol h:lII ing.
MItlGW·[
DMsion yfWater Resourees,Underg,rolllld llljel:lI(J[]Conn'nIP"gr-.UII,tOR WATERSLi'PPLY WELL,S Ol''LY:1636 Milil Service C~nrt!r,R:d\."i~h,XC 276~·1636
2k Fill' W:UCI"S"l!ph ,\(nj«tion Wells:Ja,Yic!d UqlI1I)Method (lftc~t:_Also submit one copy of this form within 3Cldays or complericuof
lb.ObillfL"CtillIIIYll~-'Anmullt;wctl consrmcrlon ~D11",counry 1u;<1l1hdcpanm~lil of the '01lnf~'wilenL+=..::=:::::.:::::::.:~::...:======:::.--.::===~==::::=====-J constructed
SS
SS
SS
SS
SS
SS
RC
75
83
67
100
100
100
(66)
ML
ML
ML
CL-ML
CL-
ML
ML
ML
ML
CC-
ML
SM
SM
PWR
PWR
ROCK
4.0
9.0
10.511.0
14.0
15.516.0
19.0
20.0
21.0
24.0
29.0
32.5
35.0
SILT with sand and trace mica, orangish brown, soft, moist.
SILT with minor clay, sand, and mica, orangish brown, soft, moist.
Same as above but medium density.
CLAY with silt, yellowish light brown, medium density, moderateplasticity, moist.
Same as above.
SILT with minor clay with trace sand and mica, orangish brown,
medium density, moist.
Same as above but yellow to orange to grey.
Same as above.
CLAY with silt and trace sand, orangish brown, soft, moist.
SAND and SILT, variegated reddish brown to light tan, interlayered,moist.
Same as above.
SAND, coarse to medium-grained, white to light grey, very dense,
moist.
SAND, medium-grained, dark grey.
White with grey fine-grained foliated granodiorite, hard rock with closehorizontal fractures parallel to foliation, some weathering along
fractures.
1-2-2-3
(4)
2-3-3-3
(6)
2-3-4-10
(7)
2-2-3-5
(5)
50/4"
50/3"
Cement groutbetween riserand 8" auger
hole2" PVC riser
2' bentonite
seal
#2 Sand,bottom of
borehole to 2'above screen0.010 mill slot
20' screen,pre-packed w/#2 sand
NOTES D50 Turbo, HSA to top of rock (32.5'), rock coring to 40'.
GROUND ELEVATION
LOGGED BY Brett Engard
DRILLING METHOD HSA AT TIME OF DRILLING 2.5 ft
AT END OF DRILLING ---
AFTER DRILLING 8.2 ft
HOLE SIZE 8" auger diameter
DRILLING CONTRACTOR SAEDACCO GROUND WATER LEVELS:
CHECKED BY
DATE STARTED 1/4/16 COMPLETED 1/5/16
SA
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)
0
5
10
15
20
25
30
35
(Continued Next Page)
PAGE 1 OF 2
WELL NUMBER MW-4
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
NORTHING, EASTING ,
RIV
E
R
B
E
N
D
/
J
B

D
R
I
L
L
I
N
G

L
O
G
S
.
G
P
J

G
I
N
T

U
S
.
G
D
T

6
/
2
7
/
1
6
RE
C
O
V
E
R
Y

%
(R
Q
D
)
U.
S
.
C
.
S
.
MATERIAL DESCRIPTION
GR
A
P
H
I
C
LO
G
BL
O
W
CO
U
N
T
S
(N

V
A
L
U
E
)
WELL DIAGRAM
RC 100
(45)ROCK
40.0
Same as above, moderate weathering 35' to 37.5', then extremelyfractured. Close horizontal fracturing 35' to 37.5'. Close vertical and
horizontal fracturing 37.5' to 40' with moderately severe weatheringalong fractures.
Boring terminated at 40.0 feet.
0.5-feet of #2sand belowscreen
SA
M
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P
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DE
P
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(f
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)
35
40
PAGE 2 OF 2
WELL NUMBER MW-4
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
NORTHING, EASTING ,
RIV
E
R
B
E
N
D
/
J
B

D
R
I
L
L
I
N
G

L
O
G
S
.
G
P
J

G
I
N
T

U
S
.
G
D
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6
/
2
7
/
1
6
RE
C
O
V
E
R
Y

%
(R
Q
D
)
U.
S
.
C
.
S
.
MATERIAL DESCRIPTION
GR
A
P
H
I
C
LO
G
BL
O
W
CO
U
N
T
S
(N

V
A
L
U
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)
WELL DIAGRAM
I /O(L) ()
'oVELL CONSTRUCTION RECORD --
For [I l'flkllUlC ONT.'1':This fcnn elm 00 used fll!'siQij:lc(If lllllll'ililc"ells
1.Well C4lllh"lC'IOr In'rorrnatiftu:
t.•.WA1'EJlWNL'>
Robert Miller FRO~I TO DEsfRIPni)'i
Well Cl>r4rJ~11)t Nanoc n.fl.
It.n,2675
NC wen Co~IJ'J(IQrCcr1if,c:llillllNIIJlDC'f 15. OUTERCASlNG (r!lr mubHiI!1td wellS!OR LINER {if a.nnrkablrl
fRO'1 I TO (lt~'I(TER TfII(,KNfSS ~Un:RHI.
SAEDACCO Inc 0 fl.122'n,2"ili~SCH40 PVC
("(1lI'J1:U1r N~tlle 11l.'N1II£}t cAsJN~OR 'WOJNG •••••I~Rlliil clilliCd-I,)fill
fROM TO Dl.••.\If.TER TlII('KNt:SS M.urRHL
2.W~lI (:On~tl'!ll;'!illll PC;I·mi·t#~ft.fl.ilL
Jjs.tatt .l.·pptifYiPIt~~j.JJ {.wJJujlJ.(i_it..CfJlmry~Stmo,\'ariwrc.,..irjectjal ~JI-.)ft.[I.,sn,
J.Well l"~(th«l.wcllll.\iC);n.SCRtl:N I
Water Su,I,II)""Ydh F"ROM yi)DI.~M.:TF:R !;1.{lT $17.•..ylllOC';F:SS I ~IMF.R1>\I.
122'ft.142 '(1.2"ill..010 SCH40 I PV(Cl,o\~fkuIIU nil ClMullio;ipaLPublic
ClOroil!.eIDIaIHiC;J!illg.iCoolil1g Slll>Ply)ORl!SidlillIial Walcr Supply (sin!l-l~)n,fl.ift,Io!udUSIJial.'C'ommcrcial ClRl!Sidtlltial Water Supply (slnred)tll.GROUT I
FROM TO !\fATERt~L E.'fP'L\(Iltf£.Yi'~iI:"TIIOII"I.-~IO!JNT
D!mg)tl.iOH 0 n.118''t.Portland Trimie
NItti-W.itr:r Su liP I;,;'Well:rt.n,IXIM(llIi10rill.~.[JR~(I'Y(:I)'I
ltl.jenilltl.Well:ft.n..I
tJ Aq~lif(:r Hcchargl'tJGroundw,ucr RCIlLCdimi(lfl IIf,S.>\NDrGRAVliL "ACt{{J'aa".lic:iIlM
.·RI)~1 "In ~.I,\"rKII[~f.nlP1 .•\n~'n:STMKTI )11D Aqllrf<;r SIOlllgC ~11);:IR~Q\'cl}'D Salini!)'Barrier 120'11••144'ft.Silica Sand 20/30
D Aquifer Test DSlomm-atcr Dr.liflllge ft.ft.DE~ril\fcnl,d Tl;\;lm(ll"g~'DSubsjdcn.;c CQl;\1ll1
DG::.~111t!11l1iJ.1(Closed Loop'.211.DRILU!,;G WG (aUIK"additional sbm.ir II«Cli~8"1DTrucC'r .·~Q~I TO P.E'oj(OlllpnO"ll'9I9••.•,,~nI""'~.!IiI.Ji.,ln","k "Ik ••~qjp'..;.(:,("t(\J
pG::.'lOlIlenlial <H<!a!illJ!!'Coolirl~Return)DOlller le!I:!11ainunder #21 Remaeks)It.rL
n,It.
4.D;it~Weli(s)Compl~lcll:1--11-2018,'r'€-JIID#MW-04CD II.a,
5:..Wclll...o~lItion:ft.n,
POLK COUNTY TRANFER STATION H.n,
Fa.ci1i1',Th'oor NUIlI¢FaClll1rJD#(if ~lic.,bJc~ft.fl,
322 LANDFILL RD,MILL SPRING,NC,28756 ft.fl.
PI"j\'sicalAdd.ress.Cil)'. and Zip U.REMAKKS
POLK Bentonite seal from 118'to 120'
('ClllIll~JJ:an:c]]do~lIi:lrLCi!lifn!lNet (I~IN)I
5b,L._tiwl'lt ;!ndl.{).1I!!itu!le in 'kgn.:t~min!lt~/sc;eQI!I!~1)1'd«imlll d\':gl'«~:22.Cct1if"lcalion:(If"dll>':ld,(liIC lal.',)u,yi••"rfie bJl}
"'m,""~~.a::"~41~N W 1/11/20 6.DaJ~
6.I!J (lIrc)the'~t!lIl.!i):iiDPc-milillelil (II'oTelflponry By ~:t!;nrIIS lhu ftJmr,.J lfl;~JJy •.'rrrih'aW!Ihe weiUSIIo\:(,'l'f"'i'?,f:i·J C071'iU'JU'IW ,ifr (.'ll:on},((lJct:"·,,ft IH Io.'C,\C ()J(,,.1)[(10 ,JI'I.1A Io.'C,I('()~C »s»w.·,'J Ci>.U'{rl"llli(!I1 Sr()l~M'd$olt:f rJ)J.p<T
't,'oS thi~.11n:,'lIITtu an r:xhtin1;"'ell:;::J\'.1."!i or !X1NfI l'l;Py "-Irlti'f rN£mi has be~1Jlunl'l,L'd rlt'Jh.,moll Uk'JI,·y,
If lIds lj.11'fJ~lir.p,ll {~i ~i'il".""'~h.'df {'{l'Ib'IIlft./I{lfJ 1JI'ft.-·~iI.'[»1(Il~·f/l.'~pl!Jhl rhe JItWJf<t"0/rJI 23.She di~rllm or additional well detaib;n!t'-'{,'jr rmd.'rr,ejT"marks xt!'L·.riJR Dr 0,11t1J~hCIJ:J.:oJ tlli.!f form.You may use tlie back of ihis.[XIge to prmide .illdilional well site detai or we'll
8.JtiiJitlber of wells oon:slJ'tttted;1 construction details.You may also <llIach.•i.dditiolliil P<'I.(",!S;ifll~ess.n:)".
l.r-vr lttilillple ir{f.n:rl.f.~1 t.q (,1j.yI-If.'!;!;t'"SJIPP."il'.'lis ONJ~r 1l'Irit rill'Stitt/p'('(l'lfstr.u<'fimt ..\;f..'lI nlr~SUBMITIAL lNSTUCTJQNSf.o!l/lJlIit ()UC jorm.
!.I.Total" (,'11dellih b~/i)w land.surface:142'(fl.)2·b.For All Wdh:Submi:Ihis form witlnn ;U days of complctio of well
~(,oP'JHMlsipIr 1':I,'.'If.H.\i (,'If di.'prhi il"r.1if/i".'JI!t~~.Y(I/.llpf~'·J@JOO'".J/l4t 'IV!'IfNi)consrrncrion to 11K:follo'l\in~r
lU.Statie \nttL:'r l~n~1 bclu\\'luP lIf £li~in::;133'(fl.)J}h'i~illn uf\"atl:r Resnurees,Infurmation Prncc~~in~Unit
If 'J'd/"'"1t'\Jr!J is .{(bf.ti'.f.'f..;'Uill~·.uJ.t!•...;.,.1617 Mall Service Center,Rald::".:'iC 2769")-1611
It.BnI'l:blllt! diamfOtcrl 8 "(in.)2~b.Fnr Jnftt!!on w~nsONLY:In addition to sendill-J!.l~fonn 10 Il e address ill
Hi!above.also ~i1b1liiI a copy of lliis form Iritbln 30 days (If camp].[ion of well
12:.W"I! ~••)tl5Iruetiol! n~tl!od;Auger/Air Drill censrructieu [I}lilt!,follo\\ illg:
'l.c.311~r.rC4UI}·.ceble,diTl.'C41l'.l51l etc.f DMsioH of Water Rescnrces,Ui1d('rgI'ollllll[lIj~~CiCHl COlltrolPI gr-.lm,
FOR \VATIR SL"l'PLY WELLS ONLY:1636 Mliil Serviee Celller,R:tl~i~h.XC 17t)~)9·16J6
13a.Yield (j,OPIll)MC:~IO"!If test:2.1~FlU'W",ter-S!'l!ply &Inj«1iotl W~Il~:
Also sl1i:}mi[one cop}'of this form wi thin 30 days of ~ompM iOIl of
JJU.Di~illh'i:til!u Iyper Aultlunl;well cousnucrion !D the "QUlCllyhcahh depanl1l~lt of the C~lIll1~'wbcn
;;OflMIlIC!:;Q
~nllGW-l Nfm.1tCarohna ~JI<lnjJlC1l£of Em jlO}fl1l~IU3111IN:ttur.1lResources -Dit'iSlollofWmcr R.~l.f"CE!!;R,:,·iscd.ugUSOIH:i
I ---
SS
SS
SS
SS
SS
SS
75
38
0
33
83
71
ML
ML
SW
SW
SM
SM
SM
SM
SM
4.0
5.0
9.0
14.0
19.0
24.0
29.0
34.0
SILT with trace sand and mica, light brown, dry.
8" of SILT with trace sand and mica, light brown, moist, soft.
4" of SAND with pebbles, dark grey to light black, dry, loose.
SAND with gravel, white, loose, dry.
SAND with pebbles, reddish brown to orange and tan, loose, dry.
No recovery.
SAND with silt, reddish brown to tan, loose, dry.
Same as above.
SAND with silt, white, iron stained, medium density, dry.
SAND with silt, white and brown, thin banding, medium density, dry.
6-4-8-6
(12)
5-6-4-5
(10)
9-6-5-7
(11)
4-4-6-8
(10)
5-4-7-9
(11)
6-7-9-10
(16)
6-7-10-14
NOTES HSA on D50 Turbo to 134', then Gus Pech 1100E air rotary to 164'.
GROUND ELEVATION
LOGGED BY Brett Engard
DRILLING METHOD HSA AT TIME OF DRILLING 133.0 ft
AT END OF DRILLING ---
AFTER DRILLING 132.4 ft
HOLE SIZE 8" auger diameter
DRILLING CONTRACTOR SAEDACCO GROUND WATER LEVELS:
CHECKED BY
DATE STARTED 1/5/16 COMPLETED 1/11/16
SA
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5
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20
25
30
35
(Continued Next Page)
PAGE 1 OF 5
WELL NUMBER MW-04CD
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
NORTHING, EASTING ,
RIV
E
R
B
E
N
D
/
J
B

D
R
I
L
L
I
N
G

L
O
G
S
.
G
P
J

G
I
N
T

U
S
.
G
D
T

6
/
2
7
/
1
6
RE
C
O
V
E
R
Y

%
U.
S
.
C
.
S
.
MATERIAL DESCRIPTION
GR
A
P
H
I
C
LO
G
BL
O
W
CO
U
N
T
S
(N

V
A
L
U
E
)
WELL DIAGRAM
SS
SS
SS
SS
SS
SS
SS
SS
63
42
83
63
75
83
79
88
SM
SM
SW
SW
SM
SM
SM
SM
SM
40.0
44.0
49.0
54.0
59.0
64.0
69.0
74.0
SAND with silt, white and brown, thin banding, medium density, dry.(continued)
SAND with silt, light tan to white, medium density, dry.
10" of SAND with pebbles and trace silt, white, medium density, dry.
10" of Silt with sand and mica, light brown to reddish brown, mediumdensity, dry.
10" of SILT with sand and mica, light brown to reddish brown, medium
density, dry.5" of SAND with pebbles, gravel, and trace silt, white, medium dense todense, dry.
SAND with silt and trace pebbles, olive grey to olive brown, dense, dry.
10" of SILT with fine sand and mica, olive brown to tan, loose, dry.
SAND with silt and trace pebbles, light orangish tan to pinkish tan,
medium density, moist to dry.
SAND with silt and mica, light grey to light tan with white, medium
density, dry.
SAND with silt, light tan to grey, medium density, dry.
(17)
7-6-10-13
(16)
8-7-7-10
(14)
6-9-10-22
(19)
13-16-19-10(35)
7-7-8-18
(15)
8-8-12-16
(20)
7-8-10-12
(18)
7-9-11-15
Cement grout
between riserand 8"borehole
2-inch PVCRiser
SA
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35
40
45
50
55
60
65
70
75
(Continued Next Page)
PAGE 2 OF 5
WELL NUMBER MW-04CD
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
NORTHING, EASTING ,
RIV
E
R
B
E
N
D
/
J
B

D
R
I
L
L
I
N
G

L
O
G
S
.
G
P
J

G
I
N
T

U
S
.
G
D
T

6
/
2
7
/
1
6
RE
C
O
V
E
R
Y

%
U.
S
.
C
.
S
.
MATERIAL DESCRIPTION
GR
A
P
H
I
C
LO
G
BL
O
W
CO
U
N
T
S
(N

V
A
L
U
E
)
WELL DIAGRAM
SS
SS
SS
SS
SS
SS
SS
SS
83
92
83
79
100
100
92
75
SM
SM
SM
SM
SM
SM
SM
SM
SM
79.0
84.0
89.0
94.0
99.0
105.0
109.0
114.0
SAND with silt, light tan to grey, medium density, dry. (continued)
SAND with silt, orangish tan, loose, dry.
SAND with silt, light greyish tan, medium density, dry.
SAND with silt, light grey, medium density, dry.
SAND with silt, light brown to grey, medium density, dry, with quartz
veins (GRAVEL with sand, white).
SAND with silt, orange and tan, medium density, dry.
11" of SAND with silt, grey with white lenses, medium density, dry.11" of SILT with sand, light orangish brown, medium density, dry.
SAND with silt, white with orange and brown, dense, dry.
SAND with silt, white with orange and brown, dense, slightly moist.
(20)
6-7-10-13
(17)
8-9-11-13
(20)
8-10-12-18
(22)
9-12-18-34
(30)
10-10-4-14
(14)
10-11-16-20(27)
16-21-28-28(49)
7-20-22-35
SA
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)
75
80
85
90
95
100
105
110
115
(Continued Next Page)
PAGE 3 OF 5
WELL NUMBER MW-04CD
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
NORTHING, EASTING ,
RIV
E
R
B
E
N
D
/
J
B

D
R
I
L
L
I
N
G

L
O
G
S
.
G
P
J

G
I
N
T

U
S
.
G
D
T

6
/
2
7
/
1
6
RE
C
O
V
E
R
Y

%
U.
S
.
C
.
S
.
MATERIAL DESCRIPTION
GR
A
P
H
I
C
LO
G
BL
O
W
CO
U
N
T
S
(N

V
A
L
U
E
)
WELL DIAGRAM
SS
SS
SS
83
67
80
SM
PWR
PWR
PWR
PWR
PWR
COMP
119.0
124.0
134.0
135.0
140.0
144.0
SAND with silt, white with orange and brown, dense, slightly moist.(continued)
SAND with silt, white and light brown, very dense, dry.
SAND with silt and some pebbles, white and light brown, very dense,
possible epidote/pyroxene/apatite present, dry.
Auger at refusal. Use tricone bit to clean borehole, then swith to air
rotary to advance boring.
Drilling very dry, no moisture, cuttings are fine dust white with some
quartz grains and mica visible.
No moisture, cuttings are fine dust, white, some quartz grains and micavisible.
Same as above, but light grey cuttings.
Competent bedrock. Air rotary hammer in and out of hard material. No
water.
Cuttings light grey, quartz grains and mica present.
(42)
18-31-42-50(73)
50/5"
2-footbentonite seal
#2 sand filterpack0.010 mill slot
20-footscreen,prepackedwith #2 sand
20-feet of #2sand below
screen
SA
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115
120
125
130
135
140
145
150
155
(Continued Next Page)
PAGE 4 OF 5
WELL NUMBER MW-04CD
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
NORTHING, EASTING ,
RIV
E
R
B
E
N
D
/
J
B

D
R
I
L
L
I
N
G

L
O
G
S
.
G
P
J

G
I
N
T

U
S
.
G
D
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6
/
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7
/
1
6
RE
C
O
V
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R
Y

%
U.
S
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C
.
S
.
MATERIAL DESCRIPTION
GR
A
P
H
I
C
LO
G
BL
O
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CO
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S
(N

V
A
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U
E
)
WELL DIAGRAM
COMP
164.0
Competent bedrock. Air rotary hammer in and out of hard material. Nowater.
Cuttings light grey, quartz grains and mica present. (continued)
Boring terminated at 164.0 feet.
SA
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P
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(f
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155
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PAGE 5 OF 5
WELL NUMBER MW-04CD
PROJECT LOCATION Mill Spring, NC
CLIENT Polk County PROJECT NAME (NUMBER)Route 9 Landfill (2036)
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MATERIAL DESCRIPTION
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WELL DIAGRAM

APPENDIX C

Report of Laboratory Analysis
and
Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-99876-1
Client Project/Site: Polk County Route 9 Landfill
Revision: 1
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
4/22/2016 5:52:28 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
TestAmerica Job ID: 490-99876-1
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49
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Sample Summary
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-99876-1 MW-01CD Water 03/16/16 12:22 03/18/16 10:30
490-99876-2 MW-04CD Water 03/17/16 13:19 03/18/16 10:30
490-99876-3 MW-4 Water 03/16/16 10:38 03/18/16 10:30
490-99876-4 MW-2R Water 03/17/16 12:21 03/18/16 10:30
490-99876-5 MW-2RDUP Water 03/17/16 12:21 03/18/16 10:30
490-99876-6 MW-3R Water 03/16/16 13:07 03/18/16 10:30
490-99876-7 SP-1 Water 03/16/16 13:37 03/18/16 10:30
490-99876-8 SS-1 Water 03/16/16 14:04 03/18/16 10:30
490-99876-9 SS-2 Water 03/16/16 14:22 03/18/16 10:30
490-99876-10 Trip Blank Water 03/16/16 00:01 03/18/16 10:30
490-99876-11 MW-02CD Water 03/16/16 11:33 03/18/16 10:30
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-99876-1
Project/Site: Polk County Route 9 Landfill
Job ID: 490-99876-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-99876-1
REVISED REPORT: Revised to add Tetrahydrofuran to samle 490-99876-9. This report replaces the one generated on 04/14/16 @ 1659.
Comments
No additional comments.
Receipt
The samples were received on 3/18/2016 10:30 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 3.5º C.
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
Method(s) 6020B: The second Interference Check Standard B (ICSAB) was not within the acceptable control limits for Antimony. The
ICSAB recovery was biased high and the sample concentrations were not detected so the data was qualified and reported.
MW-01CD (490-99876-1), MW-04CD (490-99876-2), MW-4 (490-99876-3), MW-2R (490-99876-4), MW-2RDUP (490-99876-5), MW-3R
(490-99876-6), SP-1 (490-99876-7), SS-1 (490-99876-8), SS-2 (490-99876-9) and MW-02CD (490-99876-11)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
Qualifier
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 03/16/16 12:22
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 16:38 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 16:38 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 16:38 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 16:38 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 16:38 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 16:38 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 16:38 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 16:38 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 16:38 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 16:38 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 16:38 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 16:38 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 16:38 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 16:38 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 16:38 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 16:38 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 16:38 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 16:38 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 16:38 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 16:38 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 16:38 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 16:38 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 16:38 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 16:38 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 16:38 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 16:38 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 16:38 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 16:38 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 16:38 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 16:38 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 16:38 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 16:38 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 16:38 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 16:38 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 16:38 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 16:38 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 16:38 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 16:38 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 16:38 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 16:38 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 16:38 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 16:38 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 16:38 1Trichlorofluoromethane0.396 J
1.00 0.230 ug/L 03/22/16 16:38 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 16:38 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 16:38 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 16:38 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 03/16/16 12:22
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)111 70-130 03/22/16 16:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)111 03/22/16 16:38 170-130
1,2-Dichloroethane-d4 (Surr)117 03/22/16 16:38 170-130
Toluene-d8 (Surr)105 03/22/16 16:38 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 18:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:19 1Barium0.0344
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 18:19 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:19 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:19 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 18:19 1Lead<0.00200
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 18:19 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:19 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:19 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 05:42 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:42 1Cobalt<0.500
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:42 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 05:42 1Vanadium12.8 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 14:54 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-2Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 03/17/16 13:19
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 16:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 16:10 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 16:10 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 16:10 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 16:10 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 16:10 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 16:10 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 16:10 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 16:10 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 16:10 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 16:10 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 16:10 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 16:10 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 16:10 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 16:10 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 16:10 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 16:10 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 16:10 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 16:10 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 16:10 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 16:10 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 16:10 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 16:10 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 16:10 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 16:10 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 16:10 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 16:10 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 16:10 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 16:10 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 16:10 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 16:10 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 16:10 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 16:10 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 16:10 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 16:10 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 16:10 1Tetrahydrofuran2.91 J
1.00 0.170 ug/L 03/22/16 16:10 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 16:10 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 16:10 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 16:10 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 16:10 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 16:10 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 16:10 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 16:10 1Trichlorofluoromethane0.496 J
1.00 0.230 ug/L 03/22/16 16:10 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 16:10 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 16:10 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 16:10 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-2Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 03/17/16 13:19
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)105 70-130 03/22/16 16:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 03/22/16 16:10 170-130
1,2-Dichloroethane-d4 (Surr)113 03/22/16 16:10 170-130
Toluene-d8 (Surr)105 03/22/16 16:10 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:41 1Barium0.645
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 18:41 1Cadmium0.000700 J
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:41 1Chromium0.0588
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:41 1Copper0.0352
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 18:41 1Lead0.0286
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 18:41 1Nickel0.0259
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:41 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:41 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 05:14 1Beryllium1.73 J
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:14 1Cobalt23.9
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:14 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 05:14 1Vanadium74.5 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 14:21 1Zinc90.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-3Client Sample ID: MW-4
Matrix: WaterDate Collected: 03/16/16 10:38
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 17:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 17:07 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 17:07 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 17:07 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 17:07 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 17:07 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 17:07 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 17:07 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 17:07 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 17:07 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 17:07 1Chlorobenzene0.262 J
1.00 0.360 ug/L 03/22/16 17:07 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 17:07 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 17:07 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 17:07 1cis-1,2-Dichloroethene 1.28
1.00 0.170 ug/L 03/22/16 17:07 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 17:07 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 17:07 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 17:07 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 17:07 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 17:07 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 17:07 11,4-Dichlorobenzene 0.530 J
1.00 0.240 ug/L 03/22/16 17:07 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 17:07 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 17:07 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 17:07 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 17:07 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 17:07 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 17:07 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 17:07 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 17:07 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 17:07 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 17:07 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 17:07 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 17:07 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 17:07 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 17:07 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 17:07 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 17:07 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 17:07 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 17:07 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 17:07 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 17:07 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 17:07 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 17:07 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 17:07 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 17:07 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 17:07 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-3Client Sample ID: MW-4
Matrix: WaterDate Collected: 03/16/16 10:38
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)101 70-130 03/22/16 17:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 03/22/16 17:07 170-130
1,2-Dichloroethane-d4 (Surr)117 03/22/16 17:07 170-130
Toluene-d8 (Surr)105 03/22/16 17:07 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 18:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:54 1Barium0.297
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 18:54 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:54 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:54 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 18:54 1Lead<0.00200
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 18:54 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:54 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:54 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 05:48 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:48 1Cobalt2.38
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:48 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 05:48 1Vanadium11.5 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:00 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 03/17/16 12:21
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 17:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 17:35 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 17:35 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 17:35 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 17:35 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 17:35 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 17:35 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 17:35 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 17:35 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 17:35 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 17:35 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 17:35 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 17:35 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 17:35 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 17:35 1cis-1,2-Dichloroethene 6.85
1.00 0.170 ug/L 03/22/16 17:35 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 17:35 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 17:35 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 17:35 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 17:35 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 17:35 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 17:35 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 17:35 11,1-Dichloroethane 0.446 J
1.00 0.200 ug/L 03/22/16 17:35 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 17:35 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 17:35 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 17:35 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 17:35 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 17:35 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 17:35 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 17:35 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 17:35 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 17:35 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 17:35 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 17:35 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 17:35 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 17:35 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 17:35 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 17:35 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 17:35 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 17:35 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 17:35 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 17:35 1Trichloroethene0.536 J
1.00 0.210 ug/L 03/22/16 17:35 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 17:35 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 17:35 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 17:35 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 17:35 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 03/17/16 12:21
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)108 70-130 03/22/16 17:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 03/22/16 17:35 170-130
1,2-Dichloroethane-d4 (Surr)114 03/22/16 17:35 170-130
Toluene-d8 (Surr)103 03/22/16 17:35 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:58 1Barium0.115
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 18:58 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:58 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:58 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 18:58 1Lead<0.00200
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 18:58 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 18:58 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 18:58 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 05:53 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:53 1Cobalt<0.500
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:53 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 05:53 1Vanadium8.87 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:16 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 03/17/16 12:21
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 18:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 18:04 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 18:04 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 18:04 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 18:04 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 18:04 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 18:04 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 18:04 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 18:04 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 18:04 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 18:04 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 18:04 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 18:04 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 18:04 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 18:04 1cis-1,2-Dichloroethene 6.88
1.00 0.170 ug/L 03/22/16 18:04 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 18:04 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 18:04 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 18:04 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 18:04 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 18:04 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 18:04 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 18:04 11,1-Dichloroethane 0.360 J
1.00 0.200 ug/L 03/22/16 18:04 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 18:04 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 18:04 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 18:04 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 18:04 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 18:04 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 18:04 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 18:04 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 18:04 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 18:04 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 18:04 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 18:04 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 18:04 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 18:04 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 18:04 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 18:04 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 18:04 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 18:04 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 18:04 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 18:04 1Trichloroethene0.561 J
1.00 0.210 ug/L 03/22/16 18:04 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 18:04 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 18:04 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 18:04 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 18:04 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 03/17/16 12:21
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)108 70-130 03/22/16 18:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 03/22/16 18:04 170-130
1,2-Dichloroethane-d4 (Surr)116 03/22/16 18:04 170-130
Toluene-d8 (Surr)105 03/22/16 18:04 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:03 1Barium0.116
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 19:03 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:03 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:03 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 19:03 1Lead<0.00200
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 19:03 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:03 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:03 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 06:10 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:10 1Cobalt<0.500
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:10 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 06:10 1Vanadium8.25 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:22 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 03/16/16 13:07
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 18:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 18:32 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 18:32 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 18:32 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 18:32 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 18:32 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 18:32 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 18:32 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 18:32 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 18:32 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 18:32 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 18:32 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 18:32 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 18:32 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 18:32 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 18:32 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 18:32 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 18:32 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 18:32 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 18:32 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 18:32 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 18:32 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 18:32 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 18:32 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 18:32 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 18:32 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 18:32 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 18:32 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 18:32 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 18:32 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 18:32 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 18:32 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 18:32 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 18:32 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 18:32 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 18:32 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 18:32 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 18:32 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 18:32 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 18:32 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 18:32 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 18:32 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 18:32 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 18:32 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 18:32 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 18:32 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 18:32 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 18:32 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 03/16/16 13:07
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)109 70-130 03/22/16 18:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)110 03/22/16 18:32 170-130
1,2-Dichloroethane-d4 (Surr)108 03/22/16 18:32 170-130
Toluene-d8 (Surr)106 03/22/16 18:32 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 19:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:07 1Barium0.00860 J
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 19:07 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:07 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:07 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 19:07 1Lead<0.00200
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 19:07 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:07 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:07 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 06:16 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:16 1Cobalt<0.500
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:16 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 06:16 1Vanadium8.27 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:27 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 03/16/16 13:37
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 19:00 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 19:00 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 19:00 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 19:00 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 19:00 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 19:00 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 19:00 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 19:00 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 19:00 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 19:00 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 19:00 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 19:00 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 19:00 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 19:00 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 19:00 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 19:00 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 19:00 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 19:00 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 19:00 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 19:00 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 19:00 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 19:00 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 19:00 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 19:00 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 19:00 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 19:00 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 19:00 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 19:00 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 19:00 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 19:00 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 19:00 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 19:00 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 19:00 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 19:00 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 19:00 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 19:00 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 19:00 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 19:00 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 19:00 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 19:00 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 19:00 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 19:00 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 19:00 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 19:00 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 19:00 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 19:00 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 19:00 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 03/16/16 13:37
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)102 70-130 03/22/16 19:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 03/22/16 19:00 170-130
1,2-Dichloroethane-d4 (Surr)113 03/22/16 19:00 170-130
Toluene-d8 (Surr)104 03/22/16 19:00 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 19:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:12 1Barium0.0944
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 19:12 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:12 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:12 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 19:12 1Lead0.00280 J
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 19:12 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:12 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:12 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 06:21 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:21 1Cobalt1.29 J
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:21 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 06:21 1Vanadium9.24 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:33 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 03/16/16 14:04
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 19:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 19:29 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 19:29 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 19:29 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 19:29 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 19:29 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 19:29 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 19:29 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 19:29 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 19:29 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 19:29 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 19:29 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 19:29 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 19:29 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 19:29 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 19:29 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 19:29 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 19:29 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 19:29 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 19:29 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 19:29 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 19:29 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 19:29 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 19:29 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 19:29 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 19:29 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 19:29 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 19:29 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 19:29 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 19:29 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 19:29 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 19:29 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 19:29 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 19:29 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 19:29 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 19:29 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 19:29 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 19:29 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 19:29 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 19:29 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 19:29 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 19:29 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 19:29 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 19:29 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 19:29 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 19:29 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 19:29 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 19:29 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 03/16/16 14:04
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)104 70-130 03/22/16 19:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 03/22/16 19:29 170-130
1,2-Dichloroethane-d4 (Surr)114 03/22/16 19:29 170-130
Toluene-d8 (Surr)105 03/22/16 19:29 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 19:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:16 1Barium0.0351
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 19:16 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:16 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:16 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 19:16 1Lead<0.00200
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 19:16 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:16 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:16 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 06:27 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:27 1Cobalt<0.500
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:27 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 06:27 1Vanadium11.9 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:38 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 03/16/16 14:22
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 19:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 19:57 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 19:57 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 19:57 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 19:57 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 19:57 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 19:57 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 19:57 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 19:57 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 19:57 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 19:57 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 19:57 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 19:57 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 19:57 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 19:57 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 19:57 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 19:57 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 19:57 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 19:57 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 19:57 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 19:57 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 19:57 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 19:57 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 19:57 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 19:57 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 19:57 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 19:57 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 19:57 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 19:57 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 19:57 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 19:57 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 19:57 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 19:57 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 19:57 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 19:57 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 19:57 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 19:57 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 19:57 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 19:57 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 19:57 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 19:57 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 19:57 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 19:57 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 19:57 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 19:57 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 19:57 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 19:57 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 19:57 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 03/16/16 14:22
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)104 70-130 03/22/16 19:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 03/22/16 19:57 170-130
1,2-Dichloroethane-d4 (Surr)111 03/22/16 19:57 170-130
Toluene-d8 (Surr)105 03/22/16 19:57 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 19:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:21 1Barium0.0318
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 19:21 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:21 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:21 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 19:21 1Lead0.00200 J
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 19:21 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:21 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:21 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 06:33 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:33 1Cobalt<0.500
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:33 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 06:33 1Vanadium11.9 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:44 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/16/16 00:01
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 15:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 15:13 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 15:13 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 15:13 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 15:13 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 15:13 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 15:13 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 15:13 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 15:13 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 15:13 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 15:13 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 15:13 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 15:13 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 15:13 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 15:13 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 15:13 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 15:13 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 15:13 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 15:13 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 15:13 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 15:13 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 15:13 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 15:13 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 15:13 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 15:13 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 15:13 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 15:13 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 15:13 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 15:13 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 15:13 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 15:13 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 15:13 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 15:13 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 15:13 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 15:13 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 15:13 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 15:13 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 15:13 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 15:13 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 15:13 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 15:13 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 15:13 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 15:13 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 15:13 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/22/16 15:13 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 15:13 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 15:13 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 15:13 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/16/16 00:01
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)105 70-130 03/22/16 15:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 03/22/16 15:13 170-130
1,2-Dichloroethane-d4 (Surr)110 03/22/16 15:13 170-130
Toluene-d8 (Surr)110 03/22/16 15:13 170-130
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-11Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 03/16/16 11:33
Date Received: 03/18/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 20:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/22/16 20:26 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/22/16 20:26 1Benzene<0.200
1.00 0.150 ug/L 03/22/16 20:26 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/22/16 20:26 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/22/16 20:26 1Bromoform<0.290
1.00 0.350 ug/L 03/22/16 20:26 1Bromomethane<0.350
50.0 2.64 ug/L 03/22/16 20:26 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/22/16 20:26 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/22/16 20:26 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/22/16 20:26 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/22/16 20:26 1Chloroethane<0.360
1.00 0.230 ug/L 03/22/16 20:26 1Chloroform<0.230
1.00 0.360 ug/L 03/22/16 20:26 1Chloromethane<0.360
1.00 0.210 ug/L 03/22/16 20:26 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/22/16 20:26 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/22/16 20:26 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/22/16 20:26 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/22/16 20:26 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/22/16 20:26 1Dibromomethane<0.450
1.00 0.190 ug/L 03/22/16 20:26 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/22/16 20:26 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/22/16 20:26 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/22/16 20:26 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/22/16 20:26 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/22/16 20:26 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/22/16 20:26 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/22/16 20:26 12-Hexanone <1.28
10.0 1.50 ug/L 03/22/16 20:26 1Iodomethane<1.50
5.00 1.00 ug/L 03/22/16 20:26 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/22/16 20:26 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/22/16 20:26 1Styrene<0.280
1.00 0.150 ug/L 03/22/16 20:26 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/22/16 20:26 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/22/16 20:26 1Tetrachloroethene<0.140
10.0 0.820 ug/L 03/22/16 20:26 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 03/22/16 20:26 1Toluene<0.170
5.00 0.460 ug/L 03/22/16 20:26 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/22/16 20:26 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/22/16 20:26 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/22/16 20:26 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/22/16 20:26 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/22/16 20:26 1Trichloroethene<0.200
1.00 0.210 ug/L 03/22/16 20:26 1Trichlorofluoromethane0.400 J
1.00 0.230 ug/L 03/22/16 20:26 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/22/16 20:26 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/22/16 20:26 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/22/16 20:26 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-99876-11Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 03/16/16 11:33
Date Received: 03/18/16 10:30
4-Bromofluorobenzene (Surr)103 70-130 03/22/16 20:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 03/22/16 20:26 170-130
1,2-Dichloroethane-d4 (Surr)114 03/22/16 20:26 170-130
Toluene-d8 (Surr)105 03/22/16 20:26 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:25 1Barium0.258
0.00100 0.000500 mg/L 03/22/16 11:28 03/23/16 19:25 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:25 1Chromium<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:25 1Copper<0.00500
0.00500 0.00200 mg/L 03/22/16 11:28 03/23/16 19:25 1Lead0.00600
0.0100 0.00300 mg/L 03/22/16 11:28 03/23/16 19:25 1Nickel<0.00300
0.0100 0.00500 mg/L 03/22/16 11:28 03/23/16 19:25 1Selenium<0.00500
0.00500 0.00300 mg/L 03/22/16 11:28 03/23/16 19:25 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 1.00 ug/L 03/22/16 11:28 04/08/16 06:38 1Beryllium<1.00
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:38 1Cobalt1.31 J
2.00 0.500 ug/L 03/22/16 11:28 04/08/16 06:38 1Thallium<0.500
4.00 2.10 ug/L 03/22/16 11:28 04/08/16 06:38 1Vanadium15.9 B
25.0 10.0 ug/L 03/22/16 11:28 04/12/16 15:49 1Zinc14.6 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 21:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-325836/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/22/16 14:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 03/22/16 14:45 1Acrylonitrile
<0.200 0.2001.00 ug/L 03/22/16 14:45 1Benzene
<0.150 0.1501.00 ug/L 03/22/16 14:45 1Bromochloromethane
<0.170 0.1701.00 ug/L 03/22/16 14:45 1Bromodichloromethane
<0.290 0.2901.00 ug/L 03/22/16 14:45 1Bromoform
<0.350 0.3501.00 ug/L 03/22/16 14:45 1Bromomethane
<2.64 2.6450.0 ug/L 03/22/16 14:45 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 03/22/16 14:45 1Carbon disulfide
<0.180 0.1801.00 ug/L 03/22/16 14:45 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 03/22/16 14:45 1Chlorobenzene
<0.360 0.3601.00 ug/L 03/22/16 14:45 1Chloroethane
<0.230 0.2301.00 ug/L 03/22/16 14:45 1Chloroform
<0.360 0.3601.00 ug/L 03/22/16 14:45 1Chloromethane
<0.210 0.2101.00 ug/L 03/22/16 14:45 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/22/16 14:45 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 03/22/16 14:45 1Dibromochloromethane
<0.940 0.94010.0 ug/L 03/22/16 14:45 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 03/22/16 14:45 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 03/22/16 14:45 1Dibromomethane
<0.190 0.1901.00 ug/L 03/22/16 14:45 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 03/22/16 14:45 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 03/22/16 14:45 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 03/22/16 14:45 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 03/22/16 14:45 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 03/22/16 14:45 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 03/22/16 14:45 1Ethylbenzene
<1.28 1.2810.0 ug/L 03/22/16 14:45 12-Hexanone
<1.50 1.5010.0 ug/L 03/22/16 14:45 1Iodomethane
<1.00 1.005.00 ug/L 03/22/16 14:45 1Methylene Chloride
<0.810 0.81010.0 ug/L 03/22/16 14:45 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 03/22/16 14:45 1Styrene
<0.150 0.1501.00 ug/L 03/22/16 14:45 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 03/22/16 14:45 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 03/22/16 14:45 1Tetrachloroethene
<0.820 0.82010.0 ug/L 03/22/16 14:45 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 03/22/16 14:45 1Toluene
<0.460 0.4605.00 ug/L 03/22/16 14:45 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 03/22/16 14:45 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/22/16 14:45 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 03/22/16 14:45 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 03/22/16 14:45 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 03/22/16 14:45 1Trichloroethene
<0.210 0.2101.00 ug/L 03/22/16 14:45 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 03/22/16 14:45 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 03/22/16 14:45 1Vinyl acetate
<0.180 0.1801.00 ug/L 03/22/16 14:45 1Vinyl chloride
<0.580 0.5803.00 ug/L 03/22/16 14:45 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
4-Bromofluorobenzene (Surr)112 70-130 03/22/16 14:45 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 03/22/16 14:45 1Dibromofluoromethane (Surr)70 -130
114 03/22/16 14:45 11,2-Dichloroethane-d4 (Surr)70 -130
106 03/22/16 14:45 1Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-325836/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
Acetone 250 253.1 ug/L 101 54 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 537.2 ug/L 107 61 -140
Benzene 50.0 49.43 ug/L 99 80 -121
Bromochloromethane 50.0 53.24 ug/L 106 78 -129
Bromodichloromethane 50.0 53.71 ug/L 107 75 -129
Bromoform 50.0 50.07 ug/L 100 46 -145
Bromomethane 50.0 48.80 ug/L 98 41 -150
2-Butanone (MEK)250 268.0 ug/L 107 62 -133
Carbon disulfide 50.0 49.41 ug/L 99 77 -126
Carbon tetrachloride 50.0 50.76 ug/L 102 64 -147
Chlorobenzene 50.0 50.19 ug/L 100 80 -120
Chloroethane 50.0 49.46 ug/L 99 72 -120
Chloroform 50.0 53.49 ug/L 107 73 -129
Chloromethane 50.0 40.83 ug/L 82 12 -150
cis-1,2-Dichloroethene 50.0 55.17 ug/L 110 76 -125
cis-1,3-Dichloropropene 50.0 57.62 ug/L 115 74 -140
Dibromochloromethane 50.0 52.72 ug/L 105 69 -133
1,2-Dibromo-3-Chloropropane 50.0 50.45 ug/L 101 54 -125
1,2-Dibromoethane (EDB)50.0 53.07 ug/L 106 80 -129
Dibromomethane 50.0 51.61 ug/L 103 71 -125
1,2-Dichlorobenzene 50.0 52.69 ug/L 105 80 -121
1,4-Dichlorobenzene 50.0 51.04 ug/L 102 80 -120
1,1-Dichloroethane 50.0 56.06 ug/L 112 78 -125
1,2-Dichloroethane 50.0 57.65 ug/L 115 77 -121
1,1-Dichloroethene 50.0 50.69 ug/L 101 79 -124
1,2-Dichloropropane 50.0 50.07 ug/L 100 75 -120
Ethylbenzene 50.0 54.43 ug/L 109 80 -130
2-Hexanone 250 289.8 ug/L 116 60 -142
Iodomethane 50.0 56.02 ug/L 112 40 -150
Methylene Chloride 50.0 49.71 ug/L 99 79 -123
4-Methyl-2-pentanone (MIBK)250 300.7 ug/L 120 60 -137
Styrene 50.0 57.17 ug/L 114 80 -127
1,1,1,2-Tetrachloroethane 50.0 52.58 ug/L 105 74 -135
1,1,2,2-Tetrachloroethane 50.0 56.45 ug/L 113 69 -131
Tetrachloroethene 50.0 47.81 ug/L 96 80 -126
Tetrahydrofuran 100 109.0 ug/L 109 51 -124
Toluene 50.0 53.97 ug/L 108 80 -126
trans-1,4-Dichloro-2-butene 50.0 59.03 ug/L 118 41 -147
trans-1,2-Dichloroethene 50.0 56.15 ug/L 112 79 -126
trans-1,3-Dichloropropene 50.0 60.18 ug/L 120 63 -134
1,1,1-Trichloroethane 50.0 52.74 ug/L 105 78 -135
1,1,2-Trichloroethane 50.0 52.75 ug/L 106 80 -124
Trichloroethene 50.0 47.84 ug/L 96 80 -123
Trichlorofluoromethane 50.0 51.04 ug/L 102 65 -124
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-325836/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
1,2,3-Trichloropropane 50.0 57.34 ug/L 115 70 -131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 100 127.0 ug/L 127 54 -139
Vinyl chloride 50.0 45.07 ug/L 90 68 -120
Xylenes, Total 100 109.8 ug/L 110 80 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
105Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-325836/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
Acetone 250 266.6 ug/L 107 54 -145 5 21
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 538.8 ug/L 108 61 -140 0 18
Benzene 50.0 48.24 ug/L 96 80 -121 2 17
Bromochloromethane 50.0 51.55 ug/L 103 78 -129 3 17
Bromodichloromethane 50.0 51.65 ug/L 103 75 -129 4 18
Bromoform 50.0 49.96 ug/L 100 46 -145 0 16
Bromomethane 50.0 48.25 ug/L 96 41 -150 1 50
2-Butanone (MEK)250 277.4 ug/L 111 62 -133 3 19
Carbon disulfide 50.0 47.29 ug/L 95 77 -126 4 21
Carbon tetrachloride 50.0 49.09 ug/L 98 64 -147 3 19
Chlorobenzene 50.0 49.67 ug/L 99 80 -120 1 14
Chloroethane 50.0 47.32 ug/L 95 72 -120 4 20
Chloroform 50.0 51.71 ug/L 103 73 -129 3 18
Chloromethane 50.0 39.69 ug/L 79 12 -150 3 31
cis-1,2-Dichloroethene 50.0 54.71 ug/L 109 76 -125 1 17
cis-1,3-Dichloropropene 50.0 56.07 ug/L 112 74 -140 3 15
Dibromochloromethane 50.0 52.73 ug/L 105 69 -133 0 15
1,2-Dibromo-3-Chloropropane 50.0 50.36 ug/L 101 54 -125 0 24
1,2-Dibromoethane (EDB)50.0 52.48 ug/L 105 80 -129 1 15
Dibromomethane 50.0 50.86 ug/L 102 71 -125 1 16
1,2-Dichlorobenzene 50.0 52.17 ug/L 104 80 -121 1 15
1,4-Dichlorobenzene 50.0 51.04 ug/L 102 80 -120 0 15
1,1-Dichloroethane 50.0 54.49 ug/L 109 78 -125 3 17
1,2-Dichloroethane 50.0 55.72 ug/L 111 77 -121 3 17
1,1-Dichloroethene 50.0 48.59 ug/L 97 79 -124 4 17
1,2-Dichloropropane 50.0 47.29 ug/L 95 75 -120 6 17
Ethylbenzene 50.0 53.69 ug/L 107 80 -130 1 15
2-Hexanone 250 299.2 ug/L 120 60 -142 3 15
Iodomethane 50.0 56.18 ug/L 112 40 -150 0 23
Methylene Chloride 50.0 48.92 ug/L 98 79 -123 2 17
4-Methyl-2-pentanone (MIBK)250 307.6 ug/L 123 60 -137 2 17
Styrene 50.0 55.89 ug/L 112 80 -127 2 24
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-325836/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
1,1,1,2-Tetrachloroethane 50.0 51.56 ug/L 103 74 -135 2 16
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 50.0 56.31 ug/L 113 69 -131 0 20
Tetrachloroethene 50.0 47.00 ug/L 94 80 -126 2 16
Tetrahydrofuran 100 115.7 ug/L 116 51 -124 6 18
Toluene 50.0 52.99 ug/L 106 80 -126 2 15
trans-1,4-Dichloro-2-butene 50.0 58.50 ug/L 117 41 -147 1 26
trans-1,2-Dichloroethene 50.0 54.43 ug/L 109 79 -126 3 16
trans-1,3-Dichloropropene 50.0 59.76 ug/L 120 63 -134 1 14
1,1,1-Trichloroethane 50.0 50.42 ug/L 101 78 -135 4 17
1,1,2-Trichloroethane 50.0 52.34 ug/L 105 80 -124 1 15
Trichloroethene 50.0 46.66 ug/L 93 80 -123 2 17
Trichlorofluoromethane 50.0 50.85 ug/L 102 65 -124 0 18
1,2,3-Trichloropropane 50.0 57.44 ug/L 115 70 -131 0 19
Vinyl acetate 100 122.3 ug/L 122 54 -139 4 21
Vinyl chloride 50.0 42.84 ug/L 86 68 -120 5 17
Xylenes, Total 100 108.1 ug/L 108 80 -132 2 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1011,2-Dichloroethane-d4 (Surr)70 -130
105Toluene-d8 (Surr)70 -130
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
Acetone <2.66 250 239.7 ug/L 96 45 -141
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 502.6 ug/L 101 50 -148
Benzene <0.200 50.0 47.00 ug/L 94 75 -133
Bromochloromethane <0.150 50.0 49.64 ug/L 99 67 -139
Bromodichloromethane <0.170 50.0 52.16 ug/L 104 70 -140
Bromoform <0.290 50.0 44.64 ug/L 89 42 -147
Bromomethane <0.350 50.0 39.41 ug/L 79 16 -163
2-Butanone (MEK)<2.64 250 253.0 ug/L 101 50 -138
Carbon disulfide <0.220 50.0 33.36 ug/L 67 48 -152
Carbon tetrachloride <0.180 50.0 49.30 ug/L 99 62 -164
Chlorobenzene <0.180 50.0 49.27 ug/L 99 80 -129
Chloroethane <0.360 50.0 42.08 ug/L 84 58 -137
Chloroform <0.230 50.0 52.32 ug/L 105 66 -138
Chloromethane <0.360 50.0 30.40 ug/L 61 10 -169
cis-1,2-Dichloroethene <0.210 50.0 52.80 ug/L 106 68 -138
cis-1,3-Dichloropropene <0.170 50.0 55.61 ug/L 111 71 -141
Dibromochloromethane <0.250 50.0 51.84 ug/L 104 66 -140
1,2-Dibromo-3-Chloropropane <0.940 50.0 47.18 ug/L 94 52 -126
1,2-Dibromoethane (EDB)<0.210 50.0 50.34 ug/L 101 75 -137
Dibromomethane <0.450 50.0 48.29 ug/L 97 58 -140
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
1,2-Dichlorobenzene <0.190 50.0 51.38 ug/L 103 79 -128
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 50.0 49.77 ug/L 100 78 -126
1,1-Dichloroethane <0.240 50.0 54.41 ug/L 109 71 -139
1,2-Dichloroethane <0.200 50.0 53.84 ug/L 108 64 -136
1,1-Dichloroethene <0.250 50.0 44.64 ug/L 89 70 -142
1,2-Dichloropropane <0.250 50.0 49.38 ug/L 99 67 -131
Ethylbenzene <0.190 50.0 52.94 ug/L 106 79 -139
2-Hexanone <1.28 250 275.6 ug/L 110 50 -150
Iodomethane <1.50 50.0 48.61 ug/L 97 34 -191
Methylene Chloride <1.00 50.0 45.39 ug/L 91 64 -139
4-Methyl-2-pentanone (MIBK)<0.810 250 286.1 ug/L 114 50 -147
Styrene <0.280 50.0 54.94 ug/L 110 61 -148
1,1,1,2-Tetrachloroethane <0.150 50.0 51.98 ug/L 104 73 -141
1,1,2,2-Tetrachloroethane <0.190 50.0 52.60 ug/L 105 56 -143
Tetrachloroethene <0.140 50.0 45.73 ug/L 91 72 -145
Tetrahydrofuran <0.820 100 105.8 ug/L 106 34 -133
Toluene <0.170 50.0 51.24 ug/L 102 75 -136
trans-1,4-Dichloro-2-butene <0.460 50.0 54.01 ug/L 108 29 -156
trans-1,2-Dichloroethene <0.230 50.0 48.64 ug/L 97 66 -143
trans-1,3-Dichloropropene <0.170 50.0 57.62 ug/L 115 59 -135
1,1,1-Trichloroethane <0.190 50.0 51.84 ug/L 104 76 -149
1,1,2-Trichloroethane <0.190 50.0 51.41 ug/L 103 74 -134
Trichloroethene <0.200 50.0 45.98 ug/L 92 73 -144
Trichlorofluoromethane 0.396 J 50.0 53.35 ug/L 106 58 -139
1,2,3-Trichloropropane <0.230 50.0 54.30 ug/L 109 53 -144
Vinyl acetate <1.71 100 118.9 ug/L 119 37 -154
Vinyl chloride <0.180 50.0 35.73 ug/L 71 56 -129
Xylenes, Total <0.580 100 105.7 ug/L 106 74 -141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MS MS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
105Toluene-d8 (Surr)70 -130
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
Acetone <2.66 250 222.4 ug/L 89 45 -141 7 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 478.9 ug/L 96 50 -148 5 18
Benzene <0.200 50.0 44.49 ug/L 89 75 -133 5 17
Bromochloromethane <0.150 50.0 47.42 ug/L 95 67 -139 5 17
Bromodichloromethane <0.170 50.0 49.69 ug/L 99 70 -140 5 18
Bromoform <0.290 50.0 42.74 ug/L 85 42 -147 4 16
Bromomethane <0.350 50.0 39.09 ug/L 78 16 -163 1 50
2-Butanone (MEK)<2.64 250 240.2 ug/L 96 50 -138 5 19
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 325836
Carbon disulfide <0.220 50.0 31.39 ug/L 63 48 -152 6 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 50.0 46.82 ug/L 94 62 -164 5 19
Chlorobenzene <0.180 50.0 46.64 ug/L 93 80 -129 5 14
Chloroethane <0.360 50.0 39.87 ug/L 80 58 -137 5 20
Chloroform <0.230 50.0 49.49 ug/L 99 66 -138 6 18
Chloromethane <0.360 50.0 29.33 ug/L 59 10 -169 4 31
cis-1,2-Dichloroethene <0.210 50.0 49.87 ug/L 100 68 -138 6 17
cis-1,3-Dichloropropene <0.170 50.0 52.40 ug/L 105 71 -141 6 15
Dibromochloromethane <0.250 50.0 48.96 ug/L 98 66 -140 6 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 43.83 ug/L 88 52 -126 7 24
1,2-Dibromoethane (EDB)<0.210 50.0 47.37 ug/L 95 75 -137 6 15
Dibromomethane <0.450 50.0 45.79 ug/L 92 58 -140 5 16
1,2-Dichlorobenzene <0.190 50.0 49.36 ug/L 99 79 -128 4 15
1,4-Dichlorobenzene <0.170 50.0 47.84 ug/L 96 78 -126 4 15
1,1-Dichloroethane <0.240 50.0 50.88 ug/L 102 71 -139 7 17
1,2-Dichloroethane <0.200 50.0 51.62 ug/L 103 64 -136 4 17
1,1-Dichloroethene <0.250 50.0 43.12 ug/L 86 70 -142 3 17
1,2-Dichloropropane <0.250 50.0 45.80 ug/L 92 67 -131 8 17
Ethylbenzene <0.190 50.0 50.34 ug/L 101 79 -139 5 15
2-Hexanone <1.28 250 262.3 ug/L 105 50 -150 5 15
Iodomethane <1.50 50.0 45.36 ug/L 91 34 -191 7 23
Methylene Chloride <1.00 50.0 43.44 ug/L 87 64 -139 4 17
4-Methyl-2-pentanone (MIBK)<0.810 250 270.7 ug/L 108 50 -147 6 17
Styrene <0.280 50.0 52.43 ug/L 105 61 -148 5 24
1,1,1,2-Tetrachloroethane <0.150 50.0 49.01 ug/L 98 73 -141 6 16
1,1,2,2-Tetrachloroethane <0.190 50.0 50.85 ug/L 102 56 -143 3 20
Tetrachloroethene <0.140 50.0 43.67 ug/L 87 72 -145 5 16
Tetrahydrofuran <0.820 100 104.3 ug/L 104 34 -133 1 18
Toluene <0.170 50.0 48.98 ug/L 98 75 -136 5 15
trans-1,4-Dichloro-2-butene <0.460 50.0 53.00 ug/L 106 29 -156 2 26
trans-1,2-Dichloroethene <0.230 50.0 46.09 ug/L 92 66 -143 5 16
trans-1,3-Dichloropropene <0.170 50.0 53.49 ug/L 107 59 -135 7 14
1,1,1-Trichloroethane <0.190 50.0 50.21 ug/L 100 76 -149 3 17
1,1,2-Trichloroethane <0.190 50.0 48.95 ug/L 98 74 -134 5 15
Trichloroethene <0.200 50.0 43.89 ug/L 88 73 -144 5 17
Trichlorofluoromethane 0.396 J 50.0 50.93 ug/L 101 58 -139 5 18
1,2,3-Trichloropropane <0.230 50.0 51.65 ug/L 103 53 -144 5 19
Vinyl acetate <1.71 100 111.6 ug/L 112 37 -154 6 21
Vinyl chloride <0.180 50.0 33.75 ug/L 67 56 -129 6 17
Xylenes, Total <0.580 100 100.9 ug/L 101 74 -141 5 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
MSD MSD
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
105Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-325825/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326310 Prep Batch: 325825
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/22/16 11:28 03/23/16 18:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00500 0.005000.0100 mg/L 03/22/16 11:28 03/23/16 18:06 1Barium
<0.000500 0.0005000.00100 mg/L 03/22/16 11:28 03/23/16 18:06 1Cadmium
<0.00300 0.003000.00500 mg/L 03/22/16 11:28 03/23/16 18:06 1Chromium
<0.00500 0.005000.0100 mg/L 03/22/16 11:28 03/23/16 18:06 1Copper
<0.00200 0.002000.00500 mg/L 03/22/16 11:28 03/23/16 18:06 1Lead
<0.00300 0.003000.0100 mg/L 03/22/16 11:28 03/23/16 18:06 1Nickel
<0.00500 0.005000.0100 mg/L 03/22/16 11:28 03/23/16 18:06 1Selenium
<0.00300 0.003000.00500 mg/L 03/22/16 11:28 03/23/16 18:06 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-325825/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326310 Prep Batch: 325825
Arsenic 0.0500 0.04770 mg/L 95 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.001 mg/L 100 80 -120
Cadmium 0.0500 0.04900 mg/L 98 80 -120
Chromium 0.200 0.1989 mg/L 99 80 -120
Copper 0.250 0.2494 mg/L 100 80 -120
Lead 0.0500 0.05280 mg/L 106 80 -120
Nickel 0.500 0.5071 mg/L 101 80 -120
Selenium 0.0500 0.05010 mg/L 100 80 -120
Silver 0.0500 0.04830 mg/L 97 80 -120
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326310 Prep Batch: 325825
Arsenic <0.00860 0.0500 0.04750 mg/L 95 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0344 2.00 1.987 mg/L 98 75 -125
Cadmium <0.000500 0.0500 0.04770 mg/L 95 75 -125
Chromium <0.00300 0.200 0.1940 mg/L 97 75 -125
Copper <0.00500 0.250 0.2448 mg/L 98 75 -125
Lead <0.00200 0.0500 0.05090 mg/L 102 75 -125
Nickel <0.00300 0.500 0.4910 mg/L 98 75 -125
Selenium <0.00500 0.0500 0.04850 mg/L 97 75 -125
Silver <0.00300 0.0500 0.04760 mg/L 95 75 -125
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326310 Prep Batch: 325825
Arsenic <0.00860 0.0500 0.04480 mg/L 90 75 -125 6 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0344 2.00 1.937 mg/L 95 75 -125 3 20
Cadmium <0.000500 0.0500 0.04650 mg/L 93 75 -125 3 20
Chromium <0.00300 0.200 0.1889 mg/L 94 75 -125 3 20
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: MW-01CDLab Sample ID: 490-99876-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326310 Prep Batch: 325825
Copper <0.00500 0.250 0.2385 mg/L 95 75 -125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Lead <0.00200 0.0500 0.05030 mg/L 101 75 -125 1 20
Nickel <0.00300 0.500 0.4777 mg/L 96 75 -125 3 20
Selenium <0.00500 0.0500 0.04490 mg/L 90 75 -125 8 20
Silver <0.00300 0.0500 0.04640 mg/L 93 75 -125 3 20
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-325828/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330093 Prep Batch: 325828
RL MDL
Antimony <0.500 ^2.00 0.500 ug/L 03/22/16 11:28 04/08/16 05:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.00 1.002.00 ug/L 03/22/16 11:28 04/08/16 05:03 1Beryllium
<0.500 0.5002.00 ug/L 03/22/16 11:28 04/08/16 05:03 1Cobalt
<0.500 0.5002.00 ug/L 03/22/16 11:28 04/08/16 05:03 1Thallium
6.902 2.104.00 ug/L 03/22/16 11:28 04/08/16 05:03 1Vanadium
Client Sample ID: Method BlankLab Sample ID: MB 490-325828/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330577 Prep Batch: 325828
RL MDL
Antimony <0.500 2.00 0.500 ug/L 03/22/16 11:28 04/10/16 18:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.00 1.002.00 ug/L 03/22/16 11:28 04/10/16 18:35 1Beryllium
<0.500 0.5002.00 ug/L 03/22/16 11:28 04/10/16 18:35 1Cobalt
<0.500 0.5002.00 ug/L 03/22/16 11:28 04/10/16 18:35 1Thallium
Client Sample ID: Method BlankLab Sample ID: MB 490-325828/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331103 Prep Batch: 325828
RL MDL
Zinc <10.0 25.0 10.0 ug/L 03/22/16 11:28 04/12/16 14:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-325828/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330093 Prep Batch: 325828
Antimony 100 107.2 ^ug/L 107 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 109.1 ug/L 109 80 -120
Cobalt 100 96.07 ug/L 96 80 -120
Thallium 100 105.8 ug/L 106 80 -120
Vanadium 100 109.3 ug/L 109 80 -120
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-325828/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330577 Prep Batch: 325828
Antimony 100 106.5 ug/L 107 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 99.44 ug/L 99 80 -120
Cobalt 100 103.1 ug/L 103 80 -120
Thallium 100 101.1 ug/L 101 80 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-325828/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331103 Prep Batch: 325828
Zinc 100 96.75 ug/L 97 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330093 Prep Batch: 325828
Antimony <0.500 ^100 84.49 ^ug/L 84 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium 1.73 J 100 111.4 ug/L 110 75 -125
Cobalt 23.9 100 124.2 ug/L 100 75 -125
Thallium <0.500 100 103.8 ug/L 104 75 -125
Vanadium 74.5 B 100 171.3 ug/L 97 75 -125
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330577 Prep Batch: 325828
Antimony <0.500 100 82.10 ug/L 82 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium 1.68 J 100 105.9 ug/L 104 75 -125
Cobalt 24.6 100 127.0 ug/L 102 75 -125
Thallium 0.544 J 100 104.2 ug/L 104 75 -125
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331103 Prep Batch: 325828
Zinc 90.0 100 172.2 ug/L 82 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330093 Prep Batch: 325828
Antimony <0.500 ^100 94.75 ^ug/L 95 75 -125 11 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium 1.73 J 100 116.7 ug/L 115 75 -125 5 20
Cobalt 23.9 100 118.9 ug/L 95 75 -125 4 20
Thallium <0.500 100 112.3 ug/L 112 75 -125 8 20
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QC Sample Results
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330093 Prep Batch: 325828
Vanadium 74.5 B 100 167.6 ug/L 93 75 -125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330577 Prep Batch: 325828
Antimony <0.500 100 82.05 ug/L 82 75 -125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium 1.68 J 100 100.5 ug/L 99 75 -125 5 20
Cobalt 24.6 100 123.2 ug/L 99 75 -125 3 20
Thallium 0.544 J 100 100.8 ug/L 100 75 -125 3 20
Client Sample ID: MW-04CDLab Sample ID: 490-99876-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331103 Prep Batch: 325828
Zinc 90.0 100 168.0 ug/L 78 75 -125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-326114/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326329 Prep Batch: 326114
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/23/16 10:56 03/23/16 20:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-326114/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326329 Prep Batch: 326114
Mercury 1.00 0.8444 ug/L 84 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-99915-F-2-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326329 Prep Batch: 326114
Mercury <0.100 1.00 0.8776 ug/L 88 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-99915-F-2-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 326329 Prep Batch: 326114
Mercury <0.100 1.00 0.8762 ug/L 88 75 -125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
GC/MS VOA
Analysis Batch: 325836
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-99876-1 MW-01CD Total/NA
Water 8260B490-99876-1 MS MW-01CD Total/NA
Water 8260B490-99876-1 MSD MW-01CD Total/NA
Water 8260B490-99876-2 MW-04CD Total/NA
Water 8260B490-99876-3 MW-4 Total/NA
Water 8260B490-99876-4 MW-2R Total/NA
Water 8260B490-99876-5 MW-2RDUP Total/NA
Water 8260B490-99876-6 MW-3R Total/NA
Water 8260B490-99876-7 SP-1 Total/NA
Water 8260B490-99876-8 SS-1 Total/NA
Water 8260B490-99876-9 SS-2 Total/NA
Water 8260B490-99876-10 Trip Blank Total/NA
Water 8260B490-99876-11 MW-02CD Total/NA
Water 8260BLCS 490-325836/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-325836/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-325836/7 Method Blank Total/NA
Metals
Prep Batch: 325825
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-99876-1 MW-01CD Total/NA
Water 3010A490-99876-1 MS MW-01CD Total/NA
Water 3010A490-99876-1 MSD MW-01CD Total/NA
Water 3010A490-99876-2 MW-04CD Total/NA
Water 3010A490-99876-3 MW-4 Total/NA
Water 3010A490-99876-4 MW-2R Total/NA
Water 3010A490-99876-5 MW-2RDUP Total/NA
Water 3010A490-99876-6 MW-3R Total/NA
Water 3010A490-99876-7 SP-1 Total/NA
Water 3010A490-99876-8 SS-1 Total/NA
Water 3010A490-99876-9 SS-2 Total/NA
Water 3010A490-99876-11 MW-02CD Total/NA
Water 3010ALCS 490-325825/2-A Lab Control Sample Total/NA
Water 3010AMB 490-325825/1-A Method Blank Total/NA
Prep Batch: 325828
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-99876-1 MW-01CD Total/NA
Water 3010A490-99876-2 MW-04CD Total/NA
Water 3010A490-99876-2 MS MW-04CD Total/NA
Water 3010A490-99876-2 MSD MW-04CD Total/NA
Water 3010A490-99876-3 MW-4 Total/NA
Water 3010A490-99876-4 MW-2R Total/NA
Water 3010A490-99876-5 MW-2RDUP Total/NA
Water 3010A490-99876-6 MW-3R Total/NA
Water 3010A490-99876-7 SP-1 Total/NA
Water 3010A490-99876-8 SS-1 Total/NA
Water 3010A490-99876-9 SS-2 Total/NA
Water 3010A490-99876-11 MW-02CD Total/NA
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QC Association Summary
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 325828 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010ALCS 490-325828/2-A Lab Control Sample Total/NA
Water 3010AMB 490-325828/1-A Method Blank Total/NA
Prep Batch: 326114
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-99876-1 MW-01CD Total/NA
Water 7470A490-99876-2 MW-04CD Total/NA
Water 7470A490-99876-3 MW-4 Total/NA
Water 7470A490-99876-4 MW-2R Total/NA
Water 7470A490-99876-5 MW-2RDUP Total/NA
Water 7470A490-99876-6 MW-3R Total/NA
Water 7470A490-99876-7 SP-1 Total/NA
Water 7470A490-99876-8 SS-1 Total/NA
Water 7470A490-99876-9 SS-2 Total/NA
Water 7470A490-99876-11 MW-02CD Total/NA
Water 7470A490-99915-F-2-B MS Matrix Spike Total/NA
Water 7470A490-99915-F-2-C MSD Matrix Spike Duplicate Total/NA
Water 7470ALCS 490-326114/2-A Lab Control Sample Total/NA
Water 7470AMB 490-326114/1-A Method Blank Total/NA
Analysis Batch: 326310
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 325825490-99876-1 MW-01CD Total/NA
Water 6010D 325825490-99876-1 MS MW-01CD Total/NA
Water 6010D 325825490-99876-1 MSD MW-01CD Total/NA
Water 6010D 325825490-99876-2 MW-04CD Total/NA
Water 6010D 325825490-99876-3 MW-4 Total/NA
Water 6010D 325825490-99876-4 MW-2R Total/NA
Water 6010D 325825490-99876-5 MW-2RDUP Total/NA
Water 6010D 325825490-99876-6 MW-3R Total/NA
Water 6010D 325825490-99876-7 SP-1 Total/NA
Water 6010D 325825490-99876-8 SS-1 Total/NA
Water 6010D 325825490-99876-9 SS-2 Total/NA
Water 6010D 325825490-99876-11 MW-02CD Total/NA
Water 6010D 325825LCS 490-325825/2-A Lab Control Sample Total/NA
Water 6010D 325825MB 490-325825/1-A Method Blank Total/NA
Analysis Batch: 326329
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 326114490-99876-1 MW-01CD Total/NA
Water 7470A 326114490-99876-2 MW-04CD Total/NA
Water 7470A 326114490-99876-3 MW-4 Total/NA
Water 7470A 326114490-99876-4 MW-2R Total/NA
Water 7470A 326114490-99876-5 MW-2RDUP Total/NA
Water 7470A 326114490-99876-6 MW-3R Total/NA
Water 7470A 326114490-99876-7 SP-1 Total/NA
Water 7470A 326114490-99876-8 SS-1 Total/NA
Water 7470A 326114490-99876-9 SS-2 Total/NA
Water 7470A 326114490-99876-11 MW-02CD Total/NA
Water 7470A 326114490-99915-F-2-B MS Matrix Spike Total/NA
Water 7470A 326114490-99915-F-2-C MSD Matrix Spike Duplicate Total/NA
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QC Association Summary
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Analysis Batch: 326329 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 326114LCS 490-326114/2-A Lab Control Sample Total/NA
Water 7470A 326114MB 490-326114/1-A Method Blank Total/NA
Analysis Batch: 330093
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 325828490-99876-1 MW-01CD Total/NA
Water 6020B 325828490-99876-2 MW-04CD Total/NA
Water 6020B 325828490-99876-2 MS MW-04CD Total/NA
Water 6020B 325828490-99876-2 MSD MW-04CD Total/NA
Water 6020B 325828490-99876-3 MW-4 Total/NA
Water 6020B 325828490-99876-4 MW-2R Total/NA
Water 6020B 325828490-99876-5 MW-2RDUP Total/NA
Water 6020B 325828490-99876-6 MW-3R Total/NA
Water 6020B 325828490-99876-7 SP-1 Total/NA
Water 6020B 325828490-99876-8 SS-1 Total/NA
Water 6020B 325828490-99876-9 SS-2 Total/NA
Water 6020B 325828490-99876-11 MW-02CD Total/NA
Water 6020B 325828LCS 490-325828/2-A Lab Control Sample Total/NA
Water 6020B 325828MB 490-325828/1-A Method Blank Total/NA
Analysis Batch: 330577
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 325828490-99876-2 MS MW-04CD Total/NA
Water 6020B 325828490-99876-2 MSD MW-04CD Total/NA
Water 6020B 325828LCS 490-325828/2-A Lab Control Sample Total/NA
Water 6020B 325828MB 490-325828/1-A Method Blank Total/NA
Analysis Batch: 331103
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 325828490-99876-1 MW-01CD Total/NA
Water 6020B 325828490-99876-2 MW-04CD Total/NA
Water 6020B 325828490-99876-2 MS MW-04CD Total/NA
Water 6020B 325828490-99876-2 MSD MW-04CD Total/NA
Water 6020B 325828490-99876-3 MW-4 Total/NA
Water 6020B 325828490-99876-4 MW-2R Total/NA
Water 6020B 325828490-99876-5 MW-2RDUP Total/NA
Water 6020B 325828490-99876-6 MW-3R Total/NA
Water 6020B 325828490-99876-7 SP-1 Total/NA
Water 6020B 325828490-99876-8 SS-1 Total/NA
Water 6020B 325828490-99876-9 SS-2 Total/NA
Water 6020B 325828490-99876-11 MW-02CD Total/NA
Water 6020B 325828LCS 490-325828/2-A Lab Control Sample Total/NA
Water 6020B 325828MB 490-325828/1-A Method Blank Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-99876-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-01CD Lab Sample ID: 490-99876-1
Matrix: WaterDate Collected: 03/16/16 12:22
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 16:381 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 18:19 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 05:42 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 14:54 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:08 BLG TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-04CD Lab Sample ID: 490-99876-2
Matrix: WaterDate Collected: 03/17/16 13:19
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 16:101 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 18:41 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 05:14 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 14:21 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:11 BLG TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-4 Lab Sample ID: 490-99876-3
Matrix: WaterDate Collected: 03/16/16 10:38
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 17:071 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 18:54 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 05:48 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:00 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:13 BLG TAL NSHTotal/NA 30 mL 30 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-99876-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-2R Lab Sample ID: 490-99876-4
Matrix: WaterDate Collected: 03/17/16 12:21
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 17:351 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 18:58 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 05:53 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:16 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:15 BLG TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-2RDUP Lab Sample ID: 490-99876-5
Matrix: WaterDate Collected: 03/17/16 12:21
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 18:041 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 19:03 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 06:10 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:22 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:18 BLG TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-3R Lab Sample ID: 490-99876-6
Matrix: WaterDate Collected: 03/16/16 13:07
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 18:321 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 19:07 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 06:16 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:27 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:20 BLG TAL NSHTotal/NA 30 mL 30 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-99876-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: SP-1 Lab Sample ID: 490-99876-7
Matrix: WaterDate Collected: 03/16/16 13:37
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 19:001 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 19:12 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 06:21 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:33 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:27 BLG TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SS-1 Lab Sample ID: 490-99876-8
Matrix: WaterDate Collected: 03/16/16 14:04
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 19:291 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 19:16 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 06:27 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:38 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:29 BLG TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SS-2 Lab Sample ID: 490-99876-9
Matrix: WaterDate Collected: 03/16/16 14:22
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 19:571 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 19:21 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 06:33 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:44 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:31 BLG TAL NSHTotal/NA 30 mL 30 mL
TestAmerica Nashville
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-99876-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: Trip Blank Lab Sample ID: 490-99876-10
Matrix: WaterDate Collected: 03/16/16 00:01
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 15:131 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Client Sample ID: MW-02CD Lab Sample ID: 490-99876-11
Matrix: WaterDate Collected: 03/16/16 11:33
Date Received: 03/18/16 10:30
Analysis 8260B KS03/22/16 20:261 TAL NSH325836
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 325825 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 326310 03/23/16 19:25 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 330093 04/08/16 06:38 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 325828 03/22/16 11:28 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 331103 04/12/16 15:49 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 326114 03/23/16 10:56 KMS TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 326329 03/23/16 21:34 BLG TAL NSHTotal/NA 30 mL 30 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-99876-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-99876-1
Project/Site: Polk County Route 9 Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-99876-1
Login Number: 99876
Question Answer Comment
Creator: Armstrong, Daniel
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.3.5C
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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APPENDIX D

Environmental Monitoring Reporting Form
and Electronic Submittal of
Environmental Monitoring Data
7502Mar2016
(Electronic Format Only)