7502_PolkCoCDLF_Sept2016_2ndSemiAnnual_DIN27319_20170125

January 2017
Polk County Construction and Demolition Debris Landfill
And Municipal Solid Waste Landfill
Permit Number 75-02
Route 9, Polk County, North Carolina
Fall 2016
Semiannual Water Quality Monitoring Report
Prepared for Polk County, North Carolina

Fall 2016 Semiannual Water Quality Report 1 January 2017
TABLE OF CONTENTS
1 Introduction ................................................................................................................................ 2
2 C&D Landfill ................................................................................................................................ 3
2.1 Sampling and Analysis Methods ................................................................................................................... 3
2.2 Analytical Results ................................................................................................................................................. 4
2.2.1 Groundwater Samples ....................................................................................................................... 5
2.2.2 Surface Water Samples ..................................................................................................................... 6
3 MSW Landfill ............................................................................................................................... 7
3.1 Sampling and Analysis Methods ................................................................................................................... 7
3.2 Analytical Results ................................................................................................................................................. 8
4 Background Monitoring Well ................................................................................................. 9
4.1 Statistical Analysis Methodology .................................................................................................................. 9
4.2 Results of Statistical Analysis .......................................................................................................................... 9
5 Summary .................................................................................................................................... 10
5.1 Future Activities ................................................................................................................................................ 10
TABLES
Table 1 Summary of Groundwater Elevation Data—September 2016
Table 2 Summary of Laboratory Analyses Performed on Samples
Table 3 Summary of Detected Constituents
Table 4 VOCs Background Well Comparison
Table 5 Metals Background Well Comparison
FIGURES
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Groundwater Elevation Map
APPENDICES
Appendix A Sampling Logs and Equipment Documentation and Instrument Calibration Data
Sheets
Appendix B Report of Laboratory Analysis and Chain-of-Custody Documentation
Appendix C Environmental Monitoring Reporting Form and Electronic Submittal of
Environmental Monitoring Data 7502Sept2016 (Electronic Format Only

Fall 2016 Semiannual Water Quality Report 2 January 2017
1 Introduction
The Polk County Solid Waste Department (County) maintains two landfills at the Polk County Route 9
Landfill Facility (Site), located on the west side of North Carolina Route 9, approximately 1.5 miles
northwest of the community of Mill Spring (Figure 1).
The northernmost landfill area is an inactive, closed, permitted Construction and Demolition Debris
(C&D) Landfill (Figure 2). The 3.5-acre C&D Landfill (formerly known as the “Operating Landfill”) was
capped during the summer of 2006, and a Closure Plan was submitted to Mr. James Coffey at the
North Carolina Department of Environment and Natural Resources (DENR), now known as the
Department of Environmental Quality (DEQ), on August 21, 2006.
The second landfill is a Municipal Solid Waste (MSW) Landfill composed of two discrete areas in the
west-central and southern parts of the Site (Figure 2). The MSW Landfill (formerly known as the
“Closed Landfill”) is inactive, closed, and maintained by the County. It was officially closed on April 9,
1994.
Both landfills are regulated by the DEQ, Division of Waste Management (DWM), under Permit No.
75-02 (Polk County C&D Landfill and MSW Landfill) as well as DEQ Solid Waste Management Rules
Title 15A, North Carolina Administrative Code (NCAC) Subchapter 13B, Section .0500 (C&D Landfill)
and Title 15A NCAC 13B.1600 (MSW Landfill). The permit requires semiannual monitoring of
groundwater and surface water quality. This report is being submitted by Anchor QEA of North
Carolina, PLLC (Anchor QEA), on behalf of the County, in accordance with the monitoring and
reporting requirements stated in the permit as well as the rules, and it provides an evaluation of
surface water and groundwater quality for the C&D Landfill and an evaluation of the groundwater
quality for the closed MSW Landfill.

Fall 2016 Semiannual Water Quality Report 3 January 2017
2 C&D Landfill
2.1 Sampling and Analysis Methods
Four monitoring wells (MW-01CD, MW-02CD, MW-03CD, and MW-04CD) and three surface water
locations (SS-1, SS-2, and SP-1) are monitored in association with the C&D Landfill. All monitoring
points, with the exception of MW-03CD, were sampled on September 21, and 22, 2016 by Altamont
Environmental, Inc. (Altamont), which became Anchor QEA on December 29, 2016. Monitoring well
MW-04CD was installed in January 2016 to replace MW-03CD, per the approval letter from Ms.
Elizabeth Werner of the DEQ. The approximate locations of the groundwater monitoring wells and
surface water sampling points are shown on Figure 2. Field sampling logs are included in Appendix
A.
Monitoring wells MW-01CD, MW-02CD, and MW-04CD are constructed of 2-inch-diameter Schedule
40 polyvinyl chloride (PVC) well material. Well construction logs for MW-01CD and MW-02CD are
not available. The well construction log for MW-04CD was included in Appendix B of the Spring 2016
Semiannual Water Quality Report (Altamont 2016). Prior to sampling, water level measurements were
obtained. Table 1 and Figure 3 present the groundwater elevation data relative to an assumed
benchmark elevation.
Monitoring wells MW-01CD and MW-04CD were each purged and sampled using a new, disposable
polyethylene bailer. The wells were purged of three successive well volumes prior to sample
collection. During purging, the pH, specific conductivity, dissolved oxygen (DO), oxidation reduction
potential (ORP), turbidity, and temperature were measured and recorded at the start of purging and
after each consecutive well volume was purged. After the third consecutive well volume was purged,
technicians collected a sample in laboratory-supplied sample containers, while wearing a new pair of
nitrile gloves. MW-02CD was purged and sampled in a similar manner; however, this well was purged
dry after the first well volume. Altamont personnel waited for the well to recharge sufficiently, then
collected a sample.
The surface water sample collected at the SS-1 location is representative of surface water quality
upstream of the landfill. The surface water sample collected at the SS-2 location is representative of
surface water quality downstream of the landfill. The surface water sample collected from the SP-1
location is representative of surface water quality at a nearby spring that is situated at an elevation
lower than the landfill in an apparent downgradient direction (Figure 2). At each of these surface
water sampling locations, pH, specific conductivity, DO, ORP, turbidity, and temperature were
measured and a grab sample was collected by a technician wearing a new pair of nitrile gloves.
Collected groundwater and surface water samples were immediately placed on ice in sample coolers
for transport to the laboratory. Proper chain-of-custody documentation was maintained during the

Fall 2016 Semiannual Water Quality Report 4 January 2017
collection and transport of each sample. A trip blank was also transported in the sample cooler and
analyzed for Appendix I volatile organic compounds (VOCs).
The groundwater and surface water samples were analyzed by TestAmerica Laboratories, Inc.
(TestAmerica), a laboratory certified in North Carolina, for Appendix I VOCs by United States
Environmental Protection Agency (EPA) Method 8260B and for Appendix I metals by EPA Methods
6010D, 6020B, and 7470A (Table 2). Additional observations and descriptions pertaining to individual
wells are provided on the sampling logs that are included in Appendix A. The report of laboratory
analysis and chain-of-custody forms are included in Appendix B. Additionally, water level
measurements and field parameters are summarized in the Electronic Data Deliverable (EDD) format
included in Appendix C.
2.2 Analytical Results
The laboratory analytical results for groundwater, surface water, and trip blank samples collected at
the C&D Landfill are provided in the report of laboratory analysis issued by TestAmerica and
included in Appendix C. In addition, all the laboratory analytical results are summarized in the EDD
format specified by the Solid Waste Section (SWS) on May 5, 2010.
As stipulated in the DWM document referenced above, all laboratory analytical results were reported
and appropriately qualified. Non-detections (non-detects), which are values reported by the
laboratory as below method detection limits (MDLs), are tabulated in Table 3 and the EDD, and are
qualified with the “U” qualifier. The MDL is the minimum concentration of a substance that can be
measured and reported by a laboratory with 99 percent confidence that the analyte concentration is
greater than zero. All detections (values above the MDL) were compared to analyte-specific Solid
Waste Section Limits (SWSLs) established by the SWS. The SWSL is the lowest concentration of an
analyte in a sample that can be quantitatively determined with suitable precision and accuracy. If the
reported concentration is above the laboratory MDL and below the method reporting limit (MRL),
the analytical result is qualified by the laboratory as estimated, and is flagged with a “J” qualifier (J-
flag). The MRL is the minimum concentration of a target analyte that can be accurately determined
by the referenced method. If the reported concentration is above the laboratory MRL and below the
SWSL, the analytical result is qualified as estimated, and is flagged with an italicized “J” qualifier
(italicized J-flag) by Altamont per DEQ requirements. The MRL is listed in the “Report Limit” (RL)
column in the report of laboratory analysis (Appendix C). Concentrations below the respective SWSLs
are not discussed in the text of this report unless they exceed their contaminant-specific water
quality standards.
Detected concentrations of analytes in groundwater samples were compared to current groundwater
quality standards specified in 15A NCAC 2L.0202, which are referred to as “2L standards”. Detected
concentrations of analytes in groundwater with no established 2L standards were compared either to

Fall 2016 Semiannual Water Quality Report 5 January 2017
the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]) or Groundwater Protection (GWP) Standards, pursuant to
15A NCAC 13B.1634. Detections of analytes in surface-water samples were compared to 15A NCAC
2B surface-water quality standards (2B standards).
Table 3 presents the summary of laboratory analytical results for detected constituents only. Also
outlined in Table 3 are detections that were above their applicable SWSLs, as well as any analytes
that exceeded their respective 2L standards (including IMACs, if applicable), GWP Standards, or 2B
standards.
In the EDD (Appendix C), the identification of a well (“WELL ID” on the table) consists of the name of
the well prefaced by the un-hyphenated permit number for the facility. For example, the
groundwater sample from monitoring well MW-01CD is identified on the tables as 7502-MW01CD.
However, in the tables and figures of this report, the identification of a well consists of the name of
the well without the permit number associated with the facility.
2.2.1 Groundwater Samples
Eleven metals were detected in one or more of the groundwater samples collected from the
monitoring wells at the C&D landfill. All of the detected metals, with the exception of thallium, were
reported at concentrations above their respective SWSLs in monitoring well MW-04CD (Table 3).
Nine of these metals exceeded their respective 2L standards or IMACs in MW-04CD (Table 3). The
referenced exceedances in MW-04CD are likely due to well development issues. This well has proven
challenging to develop, due to its deep water level and limited water production. The turbidity
reading recorded for this monitoring well was 44.25 NTUs. Altamont sampling personnel noted that
while the turbidity was relatively low for this monitoring well, the groundwater that was purged and
sampled was brown in color and appeared saturated with sediment. Altamont is investigating
methods for further development of MW-04CD.
The sample collected from monitoring well MW-01CD had one metal that was detected above the
SWSL (zinc), while the sample collected from MW-02CD had three metals detected above respective
SWSLs (barium, lead, and zinc). Three metals (cobalt, lead, and vanadium) were detected above
respective 2L or IMAC standards in either MW-01CD or MW-02CD (Table 3). These results are
consistent with historical metals concentrations in these wells, and may be attributed to high
turbidity values (Table 3). Turbidity values for MW-01CD and MW-02CD were 194.7 NTUs and 442.3
NTUs, respectively.
One VOC (tetrahydrofuran) was detected in monitoring well MW-04CD at a concentration below the
laboratory MRL. No VOCs were detected at concentrations above their respective SWSLs (Table 3) or
water quality standards at the C&D Landfill.

Fall 2016 Semiannual Water Quality Report 6 January 2017
Groundwater pH readings were obtained from all monitoring wells sampled. The measured
groundwater pH values in MW-01CD, MW-02CD, and MW-04CD ranged from 5.96 Standard Units
(SU) to 6.27 SU, and were outside the 2L standard pH range of 6.5 to 8.5 SU (Table 3). These results
are consistent with historical data and are considered naturally occurring for groundwater in this
region.
2.2.2 Surface Water Samples
Three metals (barium, cobalt, and vanadium) were detected in one or more surface water samples
collected at designated sampling locations (Table 3). Barium exceeded its SWSL in SP-1 (SP-1). All
other results were below their respective SWSLs and 2B surface water standards.
No VOCs were detected in any of the collected surface water samples (Table 3).
The pH readings obtained from all sampled locations were within the 2B standard range of 6.00 to
9.00 SU (Table 3).
Turbidity values measured in the surface water samples ranged from 9.63 NTUs (SS-1) to 17.25 NTUs
(SP-1) (Table 3). These values were all below the 2B surface water standard of 25 NTUs.

Fall 2016 Semiannual Water Quality Report 7 January 2017
3 MSW Landfill
3.1 Sampling and Analysis Methods
During the Fall 2016 sampling event, monitoring wells MW-2R, MW-3R, and MW-4 were sampled by
Altamont on September 21 and 22, 2016. Monitoring well MW-4 was installed to replace MW-1R, per
the approval letter from Ms. Elizabeth Werner of the DEQ. The approximate locations of the
groundwater monitoring wells are shown on Figure 2. Field sampling logs are included in Appendix
A.
Monitoring wells MW-2R and MW-4 were purged and sampled using low-flow techniques in
accordance with the procedures described in “Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures” (Groundwater Issues [EPA April 1996]). During purging, the pH, specific
conductivity, DO, ORP, turbidity, and temperature were measured and recorded approximately every
3 minutes. Well purging continued until these parameters stabilized, as determined by three
successive readings in which each parameter was within a range of values, as follows:
 pH +/- 0.1 unit
 Specific conductivity +/- 3 percent
 Temperature +/- 10 percent
 DO +/- 10 percent
 Turbidity +/- 10 percent
 ORP +/- 10 millivolts
Once all these parameters stabilized, a groundwater sample was collected in laboratory-supplied
sample containers by a technician wearing a new pair of nitrile gloves. A duplicate sample was taken
at MW-2R to ensure consistency with laboratory practices, and is listed as MW-2RDUP.
The wells MW-1R, MW-2R, and MW-4 are constructed of 2-inch-diameter Schedule 40 PVC well
material, while MW-3R is constructed of 6-inch-diameter Schedule 40 PVC well material. Well
construction logs for MW-1R and MW-2R are not available. The well construction record for the
monitoring well MW-3R is available and was included in Appendix D of the Fall 2012 Semiannual
Water Quality Monitoring Report. The well construction record for the newly installed monitoring
well MW-4 is available and included in Appendix B of the Spring 2016 Semiannual Water Quality
Report (Altamont 2016).
Prior to sampling the wells, field parameters and water level measurements were obtained. Table 1
and Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation.
Field parameters are presented in the sampling logs (Appendix A) and in the EDD (Appendix C).

Fall 2016 Semiannual Water Quality Report 8 January 2017
Monitoring well MW-3R was pumped dry using a Grundfos Redi-Flo2 Electrical Submersible Pump on
September 20, 2016 and the groundwater sample was collected following recharge the next day,
September 21, 2016.
Proper chain-of-custody documentation procedures were followed during collection and transport of
the samples. Analysis of the groundwater samples was performed by TestAmerica using the same
methods described in Section 2.1 (Table 2). Additional observations and descriptions pertaining to
individual wells are provided on the sampling logs included in Appendix A.
3.2 Analytical Results
Four metals were detected in one or more of the groundwater samples collected from the
monitoring wells. Of the detected metals, barium and zinc were present at concentrations above
their respective SWSL in one or more groundwater samples collected from the monitoring wells
(Table 3). Vanadium exceeded its IMAC in all of the samples collected from monitoring wells
associated with the MSW Landfill. Reported concentrations of vanadium in the monitoring wells at
the MSW landfill are consistent with historical concentrations.
Six VOCs were detected in one or more of the groundwater samples collected from the monitoring
wells (Table 3). Cis-1,2-dichloroethene was the only VOC detected above the SWSL (Table 3). None of
the VOCs were present at concentrations above established 2L groundwater quality standards.
The measured pH was below the acceptable range established as the 2L standard in MW-2R and
MW-4. Refer to Table 3 for sample results.
Turbidity values at the time of sampling monitoring wells MW-2R, MW-3R, and MW-4 ranged from
8.88 NTUs to 33.53 NTUs (Table 3).

Fall 2016 Semiannual Water Quality Report 9 January 2017
4 Background Monitoring Well
4.1 Statistical Analysis Methodology
In 2012, background monitoring well MW-3R was installed upgradient of the other two MSW
monitoring wells and three C&D monitoring wells. MW-3R was installed to establish background
concentrations of Appendix I VOCs and metals upgradient of the MSW Landfill and C&D Landfill.
MW-3R, consistent with the other five monitoring wells, is sampled on a semiannual basis. MW-3R
has been sampled nine times from October 2012 to September 2016.
A brief statistical analysis presented herein compares background concentrations in MW-3R to
downgradient monitoring wells, and applicable groundwater standards. Historical data was
summarized for MW-01CD, MW-02CD, MW-04CD, MW-2R, and MW-4 from the nine sampling
events occurring from September 2012 to September 2016. As previously noted in this report, MW-
03CD and MW-1R were not sampled during this event. Data from newly installed monitoring wells
MW-4 and MW-04CD is included in the summary. Tables 4 and 5 list the constituents detected in
each well for the subject monitoring period, minimum concentration, maximum concentration, and
average concentration of each detected constituent, as well as the frequency of detection in each
well. Results below the MDL were assumed to equal half of the MDL.
4.2 Results of Statistical Analysis
A comparison of VOCs is presented in Table 4. No VOCs were detected in the background well (MW-
3R) during the subject statistical analysis period. Six VOCs (1,1-dichloroethane, 1,4-dichlorobenzene,
chlorobenzene, cis-1,2-dichloroethene, tetrahydrofuran, and trichloroethene) were detected in one
or more of the downgradient monitoring wells. However, all detections were at concentrations below
the respective 2L standards. A comparison of the average concentrations of VOCs in downgradient
wells with the average concentrations of VOCs in the background well shows that the majority of
average concentrations in downgradient wells exceed those of the background well.
A comparison of metals is presented in Table 5. During the subject monitoring period, barium,
cadmium, chromium, and lead were detected in MW-3R at concentrations below applicable
groundwater quality standards. Vanadium was detected below its SWSL, but above its IMAC standard
in MW-3R. Thirteen metals were detected in one or more of the downgradient monitoring wells
(Table 5). Eight of the average concentrations of these metals exceeded groundwater quality
standards in one or more downgradient monitoring wells. Average concentrations for the majority of
metals in downgradient monitoring wells exceeded the average concentrations of those metals in
the background well.

Fall 2016 Semiannual Water Quality Report 10 January 2017
5 Summary
Altamont completed the second semiannual water quality monitoring event of 2016 at the Polk
County Landfills on September 20, 21, and 22, 2016.
Table 3 of this report, the TestAmerica report of laboratory analysis (Appendix B), and the EDD
(Appendix C) provide detailed analytical results and field data demonstrating the groundwater and
surface water quality at the Polk County Landfills.
Results for the newly installed replacement monitoring wells (MW-04CD and MW-4) are somewhat
mixed. Monitoring well MW-4 produces adequate water and exhibits lower turbidity levels than
those typically measured in the monitoring well that it replaced—MW-1R. As a result, metals
concentrations in the sample collected from MW-4 were lower than the average metals
concentrations historically measured in monitoring well MW-1R. In contrast, MW-04CD compares
closely to the monitoring well that it replaced (MW-03CD) in terms of water production.
Consequently, this monitoring well has been difficult to fully develop, resulting in highly turbid
samples that yield metals concentrations similar to those historically measured in MW-03CD.
5.1 Future Activities
Anchor QEA recommends that Polk County continue to monitor VOCs and metals concentrations in
groundwater and surface water at the closed C&D and MSW landfills. Based on the data trends and
evaluation presented in this report, Anchor QEA has discussed with Polk County options for
addressing the water quality impacts identified at the Site. Based on these discussions, Anchor QEA
proposes to implement additional sampling methods at monitoring well MW-04CD, which may
include filtering the sample or collecting a no-purge sample.
Anchor QEA will continue to monitor the groundwater and surface water on a semiannual basis at
the Polk County C&D and MSW Landfills. The next sampling event is scheduled for March 2017.

Fall 2016 Semiannual Water Quality Report 11 January 2017

Tables
Table 1
Summary of Groundwater Elevation Data - September 2016
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
(feet)(feet TOC)(feet)
MW-01CD 2,955.50 109.5 2,846.00
MW-02CD 2,951.90 116.98 2,834.92
MW-03CD 2,969.60 117.18 2,852.42
MW-04CD NM 133.26 NA
MW-1R 2,867.70 27.16 2,840.54
MW-2R 2,837.20 32.71 2,804.49
MW-3R 2,962.00 76.81 2,885.19
MW-4 NM 10.2 NA
Notes:
C&D
MSW
Elevation Datum
Well Survey
MW-4 & MW-04CD
Depth to Water
NM Not measured
NA Not available
Monitoring wells MW-1R and MW-2R were surveyed on November 13, 2010. MW-3R was
surveyed on November 8, 2012. Remaining wells were surveyed on December 9, 2006. All
wells were surveyed by Wes Cole Land Surveying, PA.
All elevations were based on an assumed datum of 3,000 feet.
Installed in January 2016. These wells have not yet been surveyed.
Measured on September 20, 21, or 22, 2016.
Construction and Demolition
Municipal Solid Waste
Well ID
Depth
to
Water
Groundwater Elevation
C&D Landfill
MSW Landfill
Top of Casting
Elevation (From
Assumed Datum)
Fall 2016 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
January 2017
Table 2
Summary of Laboratory Analyses Performed on Samples
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
GROUNDWATER SAMPLES
VOCs
EPA 8260B EPA 60101D EPA 6020B EPA 7470A
75-02 MW-01CD 9/21/2016 X X X X
75-02 MW-02CD 9/21/2016 X X X X
75-02 MW-04CD 9/21/2016 X X X X
75-02 MW-2R 9/22/2016 X X X X
75-02 MW-2RDUP 9/22/2016 X X X X
75-02 MW-3R 9/21/2016 X X X X
75-02 MW-4 9/21/2016 X X X X
SURFACE WATER SAMPLES
VOCs
EPA 8260B EPA 60101D EPA 6020B EPA 7470A
75-02 SP-1 9/22/2016 X X X X
75-02 SS-1 9/22/2016 X X X X
75-02 SS-2 9/22/2016 X X X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
75-02 TRIP BLANK 9/22/2016 X
Notes:
VOCs
Analyses
Well ID Collect Date
MW-04CD and
MW-4
Volatile organic compounds
VOCs and metals analyses include Appendix I constituents per 40 CFR Part 258
Installed in January 2016. These wells were sampled for the second time during this sampling event,
and replaced monitoring wells MW-03CD and MW-1R, respectively.
Facility
Permit
Facility
Permit Well ID Collect Date Metals
C&D Landfill
MSW Landfill
Facility
Permit Well ID Collect Date Metals
C&D Landfill
Fall 2016 Semiannual Water Quality Monitoring Report
Polk county Construction and Demolition Debrisw Landfill and Municipal Solid Waste Landfill
Page 1 of 1
January 2017
Table 3
Summary of Detected Constituents
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Laboratory CertificationLaboratory Methods
Parameter Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Thallium Vanadium Zinc
1,1-Dichloro-
ethane
1,4-
Dichloro-
benzene
Chloro-
benzene
cis-1,2-
Dichloro-
ethene
Tetrahydro-
furan
Trichloro-
ethene pH Turbidity
CAS Number 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7440-28-0 7440-62-2 7440-66-6 75-34-3 106-46-7 108-90-7 156-59-2 109-99-9 79-01-6 SW320 SW330
SWS ID 15 23 34 51 53 54 131 152 194 209 213 75 71 39 78 458 201 320 330Unitsµg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result ResultGroundwater Samples C&D Landfill
MW-01CD 9/21/2016 93.2 J 0.340 J 0.500 U 3.00 U 2.57 J 5.6 J 6.0 J 3.00 U 0.800 U 8.05 J, B 12.2 J 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 6.27 194.7
MW-02CD 9/21/2016 336 0.963 J 0.500 U 4.00 J 3.91 J 5.00 U 18.8 3.80 J 0.800 U 18.3 J, B 28.3 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 5.99 442.3
MW-04CD 9/21/2016 3,130 10.3 21.0 417 125 278 102 114 1.44 J 532 B 784 0.240 U 0.170 U 0.180 U 0.210 U 1.46 J 0.200 U 5.96 44.25
MSW Landfill
MW-2R 9/22/2016 175 0.100 U 0.500 U 3.00 U 0.100 U 5.00 U 2.00 U 3.00 U 0.800 U 2.13 J, B 25.1 0.512 J 0.170 U 0.180 U 14.4 0.820 U 0.768 J 5.95 8.88
MW-2RDUP 9/22/2016 169 0.100 U 0.500 U 3.00 U 0.100 U 5.00 U 2.00 U 3.00 U 0.800 U 2.05 J, B 20.4 J 0.460 J 0.170 U 0.180 U 14.0 0.820 U 0.708 J 5.95 8.88
MW-3R 9/21/2016 8.80 J 0.100 U 0.500 U 3.00 U 0.100 U 5.00 U 2.00 U 3.00 U 0.800 U 1.86 J, B 5.20 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 6.72 22.57
MW-4 9/21/2016 318 0.100 U 0.500 U 3.00 U 0.823 J 5.00 U 2.00 U 3.00 U 0.800 U 3.30 J, B 5.20 U 0.240 U 0.317 J 0.347 J 1.71 J 1.50 J 0.200 U 5.77 33.53
Surface Water Samples
SP-1 9/22/2016 126 0.100 U 0.500 U 3.00 U 0.959 J 5.00 U 2.00 U 3.00 U 0.800 U 3.03 J, B 5.20 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 6.61 17.25
SS-1 9/22/2016 38.3 J 0.100 U 0.500 U 3.00 U 0.268 J 5.00 U 2.00 U 3.00 U 0.800 U 2.38 J, B 5.20 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 6.78 9.63
SS-2 9/22/2016 33.3 J 0.100 U 0.500 U 3.00 U 0.146 J 5.00 U 2.00 U 3.00 U 0.800 U 2.59 J, B 5.20 U 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U 6.85 14.22
Quality Control Samples
TripBlank 9/22/2016 NA NA NA NA NA NA NA NA NA NA NA 0.240 U 0.170 U 0.180 U 0.210 U 0.820 U 0.200 U NA NA
MDL 5.00/50 0.100 0.500/5.0 3.00/30 0.100/0.500/1.0 5.00/50 2.00/20 3.00/30 0.800 0.700/7.0 5.20 0.240 0.170 0.180 0.210 0.820 0.200 NA NA
MRL 10/100 2.0 1.0/10 5.0/50 2.0/10/20 10/100 5.0/50 10/100 2.0 2.0/20 25 1.0 1.0 1.0 1.0 10 1.0 NA NA
SWSL 100 1 1 10 10 10 10 50 5.5 25 10 5 1 3 5 NE 1 NE NE
2L 700 NE 2 10 NE 1,000 15 100 NE NE 1,000 6 6 50 70 NE 3 6.5-8.5 NE
IMAC NE 4 NE NE 1 NE NE NE 0.2 0.3 NE NE NE NE NE NE NE NE NE
GWP NE 4 NE NE 1 NE NE NE 0.28 0.3 NE NE NE NE NE NE NE NE NE
2B 200,000 6.5 0.15 35 4 2.7 0.54 16 0.47 NE 36 100 100 140 720 NE 3 6.0-9.0 25
Notes:
Parameters Only detected constituents are listed on this table. Please refer to TestAmerica Report of Laboratory Analysis (Appendix B) for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for a compound that was found in both the laboratory blank and the sample.
2L
IMAC Interim maximum allowable concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
GWP
2B
NE Not Established
NA Not Applicable
5.00/50 The sample from MW-04CD was diluted by a magnitude of 10 by the laboratory in order to provide more accurate results. This increases the MDL and MRL each by 10, respectively.
336 Indicates a result in exceedance of the SWSL.
18.8 Indicates a result in exceedance of the 2L, IMAC, GWP, or 2B standard.
MW-04CD The turbidity reading on this sample was relatively low; however, the water produced by this well was brown in color and appeared saturated with sediment.
EPA 6010D, EPA 6020B, EPA 7470A
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ (Amended April 1, 2013).
Groundwater Protection standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-list (last updated
June, 2011). GWP standard is used only if 2L or IMAC standards are not established for specific constituent.
Surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards," (last amended March, 2016) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
VOCs (Appendix I)
387EPA 8260B
Field Parameters
5445 (pH only)
Metals (Appendix I)
387
Fall 2016 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
January 2017
Table 4
VOCs Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.1/9 Acetone 1.41 U 10 U 3.05 6,000
8/9 Trichlorofluoromethane 0.28 J 0.65 J 0.39 2,000
1/5 Acetone 2.53 J 2.66 U 1.57 6,000
3/5 Trichlorofluoromethane 0.210 U 0.42 J 0.26 2,000
1/5 Xylene (Total)0.38 U 0.58 U 0.31 500
1/7 1,2-Dichlorobenzene 0.12 U 0.30 U 0.14 20
2/7 1,4-Dichlorobenzene 0.288 J 0.463 U 0.22 6
2/7 Acetone 2.66 U 10 U 4.12 6,000
2/6 Tetrahydrofuran 2.53 J 7.04 J 2.63 NE
7/7 Trichlorofluoromethane 0.301 J 0.52 J 0.39 2,000
1/7 Xylene (Total)0.38 U 0.66 U 0.34 500
2/2 Tetrahydrofuran 1.46 J 2.91 J 2.19 NE
1/2 Trichlorofluoromethane 0.21 U 0.496 J 0.30 2,000
1/7 1,4-Dichlorobenzene 0.17 J 0.33 U 0.14 6
2/7 cis-1,2-Dichloroethene 0.19 U 2.0 J 0.62 70
1/6 Tetrahydrofuran 0.82 U 3.1 U 1.39 NE
13/17 1,1-Dichloroethane 0.24 U 1.06 J 0.55 6
16/17 cis-1,2-Dichloroethene 5.2 13.9 10.64 70
3/17 Tetrachloroethene 0.14 U 0.46 U 0.16 0.7
15/17 Trichloroethene 0.47 U 1.56 0.93 3
1/17 Vinyl chloride 0.1 J 0.62 U 0.17 0.03
0/9 1,1-Dichloroethane 0.215 U 0.32 U 0.14 6
0/9 1,2-Dichlorobenzene 0.19 U 2.5 U 0.25 20
0/9 1,4-Dichlorobenzene 0.17 U 0.463 U 0.14 6
0/9 cis-1,2-Dichloroethene 0.19 U 0.299 U 0.11 70
0/9 Acetone 1.41 U 10 U 2.89 6,000
0/9 Tetrachloroethene 0.14 U 0.46 U 0.15 0.7
0/9 Tetrahydrofuran 0.82 U 3.1 U 0.98 NE
0/9 Trichloroethene 0.2 U 0.47 U 0.16 3
0/9 Trichlorofluoromethane 0.139 U 0.48 U 0.11 2,000
0/9 Vinyl chloride 0.18 U 0.62 U 0.19 0.03
0/9 Xylene (Total)0.298 U 0.66 U 0.28 500
2/2 1,4-Dichlorobenzene 0.317 J 0.530 J 0.42 6
2/2 cis-1,2-Dichloroethene 1.28 J 1.71 J 1.50 70
2/2 Chlorobenzene 0.262 J 0.347 J 0.30 50
1/2 Tetrahydrofuran 0.82 U 1.50 J 0.96 NE
Notes:
µg/L micrograms per liter
Min.minimum concentration (µg/L)
Max.maximum concentration (µg/L)
Avg.
2L
IMAC The IMAC concentrations listed in Appendix #1 of Subchapter 2L.
U A laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
J A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
NA not applicable
# Detections
MW-02CD Only sampled in September 2012, March 2015, September 2015, and March 2016 due to a lack of well recharge during other sampling events.
MW-2R
MW-3R The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-4 and
MW-04CD
Installed in January 2016 and were sampled for the first time during the March 2016 event.
MW-1R and
MW-03CD
Not sampled during the March or September 2016 events.
MW-2R (and
MW-2RDUP)
MW-3R
MW-2R had duplicate samples collected during 7 of the 8 sampling events, thus there are 15 total samples representing MW-2R.
Number of times the constituent was detected during the sample collection period.
MW-4
Average concentration (µg/L). Average concentrations were calculated by summing the constituent detections and dividing by the number of samples. When the sample
was below the MDL, half of the MDL value was used as the result. Results flagged with a "J" are estimated average concentrations.
Groundwater standard from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater
Classifications and Standards," DENR (Amended April 1, 2013).
MW-1R
September 2012 to September 2016
Well # Detections Detected Constituents Concentration (µg/L)2L Standard or
IMAC
MW-01CD
MW-04CD
MW-03CD
MW-02CD
Fall 2016 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
January 2017
Table 5
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina

Min.Max.Avg.
9/9 Barium 12.5 J 104 46.6 700
2/9 Beryllium 0.5 U 1.0 U 0.42 4
1/9 Cadmium 0.3 J 1.0 U 0.61 2
1/9 Chromium 2.5 U 5.0 U 2.00 10
2/9 Cobalt 0.5 U 5.0 U 1.93 1
3/9 Copper 2.5 U 8.30 J 3.88 1,000
4/9 Lead 2.5 U 7.72 J 4.20 15
1/9 Silver 2.5 U 5.02 J 2.34 20
2/9 Thallium 0.019 U 0.641 U 0.18 0.2
4/9 Vanadium 1.8 J 12.8 J 4.72 0.3
5/9 Zinc 10.0 U 105 19.44 1,000
5/5 Barium 41.0 J 627 268.32 700
2/5 Beryllium 0.5 U 1.58 J 0.72 4
2/5 Cadmium 0.3 J 1.5 0.56 2
3/5 Chromium 3.0 U 3.66 J 2.81 10
3/5 Cobalt 1.31 J 6.1 J 3.10 1
2/5 Copper 5.0 U 5.52 J 3.60 1,000
4/5 Lead 2.0 U 30.7 13.48 15
2/5 Nickel 3.0 U 3.9 J 2.45 100
1/5 Silver 2.5 U 4.99 J 2.15 20
1/5 Thallium 0.2 U 0.641 U 0.33 0.2
4/5 Vanadium 1.6 J 43.6 16.88 0.3
4/5 Zinc 10 U 38.8 17.34 1,000
1/7 Arsenic 4.9 J 10 U 3.52 10
7/7 Barium 184 768 362.71 700
2/7 Beryllium 0.570 J 1.7 0.62 4
1/7 Cadmium 0.155 U 1.0 U 0.37 2
4/7 Chromium 3.0 U 20.3 6.89 10
3/7 Cobalt 3.39 U 10.1 3.79 1
4/7 Copper 5.0 U 21.8 8.80 1,000
4/7 Lead 5.0 U 18.6 7.42 15
4/7 Nickel 3.0 U 10.9 J 5.85 100
1/7 Silver 2.5 U 5.97 J 2.50 20
6/7 Thallium 0.026 J 0.644 J 0.23 0.2
7/7 Vanadium 4.0 J 54 16.35 0.3
7/7 Zinc 13.1 J 223 52.26 1,000
September 2012 to September 2016
Well # Detections
Detected
Constituents
Concentration (µg/L)2L Standard or
IMAC
MW-01CD
MW-02CD
MW-03CD
Fall 2016 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 3
January 2017
Table 5
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina

Min.Max.Avg.
September 2012 to September 2016
Well # Detections
Detected
Constituents
Concentration (µg/L)2L Standard or
IMAC
2/2 Barium 645 3,130 1,888 700
2/2 Beryllium 1.73 J 10.3 6.02 4
2/2 Cadmium 0.70 J 21 10.85 2
2/2 Chromium 58.8 417 237.9 10
2/2 Cobalt 23.9 125 74.5 1
2/2 Copper 35.2 278 156.6 1,000
2/2 Lead 28.6 102 65.3 15
2/2 Nickel 25.9 114 70.0 100
0/1 Silver 3.0 U 30 U 16.50 20
1/2 Thallium 0.5 U 1.44 J 0.85 0.2
2/2 Vanadium 74.5 532 303.3 0.3
2/2 Zinc 90.0 784.0 437.0 1,000
1/7 Arsenic 2.5 U 25.6 5.94 10
7/7 Barium 41.4 J 2,270 350.71 700
3/7 Beryllium 0.50 U 13.3 2.33 4
3/7 Cadmium 0.3 J 5.8 1.36 2
3/7 Chromium 2.5 U 51.5 9.57 10
3/7 Copper 2.5 U 122 21.35 1,000
3/7 Lead 2.0 U 64.7 11.55 15
3/7 Nickel 2.5 U 29.1 J 6.81 100
1/7 Silver 2.5 U 5.0 U 2.36 20
3/7 Thallium 0.025 U 1.2 J 0.28 0.2
4/7 Vanadium 2.5 U 407 64.46 0.3
6/7 Zinc 10 U 428 12.24 1,000
17/17 Barium 63.3 J 217 155.66 700
1/17 Cadmium 0.155 U 1.0 U 0.32 2
2/17 Chromium 2.5 U 5.0 U 2.00 10
2/17 Copper 2.5 U 7.01 J 2.87 1,000
2/17 Lead 2.0 U 5.41 U 2.11 15
1/17 Nickel 2.5 U 5.0 U 1.91 100
2/17 Silver 2.5 U 5.88 J 2.18 20
1/17 Thallium 0.019 U 0.641 U 0.14 0.2
6/17 Vanadium 0.2 U 8.87 J 2.48 0.3
8/17 Zinc 10.0 U 25.1 10.36 1,000
MW-2R (and MW-
2RDUP)
MW-04CD
MW-1R
Fall 2016 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 2 of 3
January 2017
Table 5
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina

Min.Max.Avg.
September 2012 to September 2016
Well # Detections
Detected
Constituents
Concentration (µg/L)2L Standard or
IMAC
0/9 Arsenic 3.69 U 10.0 U 3.29 10
8/9 Barium 3.25 J 12.3 J 7.02 700
0/9 Beryllium 0.13 U 1.0 U 0.32 4
1/9 Cadmium 0.04 J 1.0 U 0.31 2
1/9 Chromium 2.02 J 5.0 U 1.86 10
0/9 Cobalt 3.39 U 5.0 U 1.77 1
0/9 Copper 0.672 U 5.0 U 2.12 1,000
1/9 Lead 2.0 U 5.41 U 2.02 15
0/9 Nickel 2.5 U 5.0 U 1.81 100
0/9 Silver 1.05 U 5.0 U 1.64 20
0/9 Thallium 0.019U 0.641 U 0.14 0.2
3/9 Vanadium 0.2 U 8.27 J 2.38 0.3
0/9 Zinc 2.26 U 10.0 U 3.74 1,000
2/2 Barium 297 318 308 700
2/2 Cobalt 0.823 J 2.38 J 1.60 1
2/2 Vanadium 3.3 J 11.5 J 7.4 0.3
Notes:
µg/L micrograms per liter
Min.Minimum concentration (µg/L)
Max.Maximum concentration (ug/L)
Avg.
2L
IMAC Interim maximum allowable concentration. Concentrations are listed in Appendix #1 of the 2L.
U
J
NA not applicable
# Detections
1.85 Indicates result above 2L Standard or IMAC.
MW-02CD
MW-3R
MW-4 and MW-04CD
MW-1R and MW-03CD Monitoring wells MW-1R and MW-03CD were not sampled during the September 2016 event.
Number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples
collected during 8 of the 9 sampling events, thus there are 17 total samples representing MW-2R.
MW-02CD was only sampled in September 2012, March 2015, September 2015, and March 2016 due to a lack of well
recharge during subsequent sampling events.
The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September
2012.
Monitoring wells MW-4 and MW-04CD were installed in January 2016 and were sampled for the first time during the March
2016 event.
MW-3R
MW-4
Average concentration (µg/L). Average concentrations were calculated by summing the constituent detections and dividing
by the number of samples. When the sample was below the MDL, half of the MDL value was used as the result. Results
flagged with a "J" are estimated averages.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural
Resources, Subchapter 2L - Groundwater Classifications and Standards," DENR (Amended April 1, 2013).
A laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit
(MDL).
A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method
reporting limit (MRL).
Fall 2016 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 3 of 3
January 2017

Figures
[0 2,0001,000
Feet
LEGEND:
Landfill Site Boundary
Publish Date: 2017/01/26, 9:12 AM | User: alesueurFilepath: P:\Projects\Polk County\Route 9 LF\Figures\2016\AQ Template\7502Sept2016 Figure 1-Site Location Map AQ.mxd
Figure 1Site Location MapPolk County Route 9 Landfill Water Quality ReportPolk County C&D and MSW Landfills, Permit #75-02, Polk County, NC
SOURCE(S):Basemap: USGS 1:24,000 Scale Topo Maps, Mill Spring,North Carolina Quadrangle, 1990.Parcels: Polk County GIS
Anchor QEA of North Carolina, PLLC
@A@A
@A
@A
@A
@A
@A
@A #*
#*
#*
Transfer Station
Scale Station
Inactive C & D Landfill
Inactive Closed
MSW Landfill Cell
Inactive Closed
MSW Landfill Cell
MW-1R
MW-2R
SS-1
MW-4
MW-03CD
MW-04CD SP-01
MW-02CD MW-01CD
SS-2
MW-3R
NC 9 H
W
Y
GA
R
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T

R
D
LANDFILL RD
BU
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B
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

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[0 350 700
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NOTE(S):-Background monitoring well MW-3Rwas installed on September 25, 2012.-Monitoring wells MW-04CD andMW-4 were installed January 4 toJanuary 11, 2016.-Locations of MW-04CD and MW-4are approximate.
LEGEND:
#*Surface Water Sample Locations
@A Monitoring Well Locations
Landfill Site Boundary
Creeks and Streams
20-Foot Interval Contours
Polk County Roads
Publish Date: 2017/01/26, 9:34 AM | User: alesueurFilepath: P:\Projects\Polk County\Route 9 LF\Figures\2016\AQ Template\7502Sept2016 Figure 2-Site Layout Map AQ.mxd
Figure 2Site Layout MapPolk County Route 9 Landfill Water Quality ReportPolk County C&D and MSW Landfills, Permit #75-02, Polk County, NC
SOURCE(S):Basemap: NC OneMap 2010Elevation Contours: NCDOT Lidar 2007Streams: NCDEQ Division of Water Quality DatabaseParcels: Polk County GIS
Anchor QEA of North Carolina, PLLC
#*
#*
#*
@A@A
@A
@A
@A
@A
@A
@A
E
E
E
Transfer Station
Scale Station
Inactive C & D Landfill
Inactive Closed
MSW Landfill Cell
Inactive Closed
MSW Landfill Cell










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
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NC 9 H
W
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BU
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e
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a
m
[
0 300 600
Feet
NOTE(S):-All water level elevations based onassumed datum of 3,000 feet.Groundwater elevation is calculated fromdepth to water measurements collectedSeptember 20, 21, and 22, 2016.-Monitoring wells MW-04CD and MW-4were installed January 2016 and have notyet been surveyed.
LEGEND:
Landfill Site Boundary
@A Approximate Sample Locations
Creeks and Streams
20-Foot Interval Contours
Polk County Roads
E
Approximate Groundwater Flow Direction
Publish Date: 2017/01/26, 9:35 AM | User: alesueurFilepath: P:\Projects\Polk County\Route 9 LF\Figures\2016\AQ Template\7502Sept2016 Figure 3-GW Contour Map AQ.mxd
Figure 3Groundwater Elevation MapPolk County Route 9 Landfill Water Quality ReportPolk County C&D and MSW Landfills, Permit #75-02, Polk County, NC
SOURCE(S):Basemap: NC OneMap 2010Elevation Contours: NCDOT Lidar 2007Streams: NCDEQ Division of Water Quality Database.Parcels: Polk County GIS
Anchor QEA of North Carolina, PLLC

Appendix A
Sampling Logs and Equipment
Documentation and Instrument
Calibration Data Sheets

Appendix B
Report of Laboratory Analysis and
Chain-of-Custody Documentation
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-112432-1
Client Project/Site: Polk County Route 9 Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
10/3/2016 2:46:54 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
TestAmerica Job ID: 490-112432-1
Page 2 of 55 TestAmerica Nashville10/3/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
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Sample Summary
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-112432-1 MW-01CD Water 09/21/16 12:45 09/23/16 09:25
490-112432-2 MW-02CD Water 09/21/16 11:15 09/23/16 09:25
490-112432-3 MW-04CD Water 09/21/16 10:20 09/23/16 09:25
490-112432-4 MW-2R Water 09/22/16 10:34 09/23/16 09:25
490-112432-5 MW-2RDUP Water 09/22/16 10:34 09/23/16 09:25
490-112432-6 MW-3R Water 09/22/16 14:30 09/23/16 09:25
490-112432-7 MW-4 Water 09/22/16 14:03 09/23/16 09:25
490-112432-8 SP-1 Water 09/22/16 11:30 09/23/16 09:25
490-112432-9 SS-1 Water 09/22/16 10:55 09/23/16 09:25
490-112432-10 SS-2 Water 09/22/16 11:05 09/23/16 09:25
490-112432-11 Trip Blank Water 09/22/16 00:01 09/23/16 09:25
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-112432-1
Project/Site: Polk County Route 9 Landfill
Job ID: 490-112432-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-112432-1
Comments
No additional comments.
Receipt
The samples were received on 9/23/2016 9:25 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 0.9º C.
GC/MS VOA
Method(s) 8260B: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation
batch 490-373601 recovered outside control limits for the following analytes: Iodomethane.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 6010D: The following sample was diluted due to the abundance of non-target analytes: MW-04CD (490-112432-3) at 10.0.
Elevated reporting limits (RLs) are provided. Dilution prepared by mixing 1 mL of sample with 9 mL of blank.
Method(s) 6020B: The method blank for preparation batch 490-373112 and analytical batch 490-374458 contained Vanadium above the
method detection limit (MDL). Associated samples were not re-analyzed because results were less than the reporting limit (RL) OR
practical quantitation limit (PQL).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Qualifiers
GC/MS VOA
Qualifier Description
*RPD of the LCS and LCSD exceeds the control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 09/21/16 12:45
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 15:09 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 15:09 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 15:09 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 15:09 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 15:09 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 15:09 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 15:09 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 15:09 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 15:09 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 15:09 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 15:09 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 15:09 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 15:09 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 15:09 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 15:09 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 15:09 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/27/16 15:09 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 15:09 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 15:09 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 15:09 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 15:09 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 15:09 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 15:09 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 15:09 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 15:09 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 15:09 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 15:09 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 15:09 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 15:09 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 15:09 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 15:09 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 15:09 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 15:09 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 15:09 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 15:09 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 15:09 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 15:09 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 15:09 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 15:09 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 15:09 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 15:09 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 15:09 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 15:09 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 15:09 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 15:09 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 15:09 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 15:09 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 15:09 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 09/21/16 12:45
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)99 70-130 09/27/16 15:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 09/27/16 15:09 170-130
1,2-Dichloroethane-d4 (Surr)95 09/27/16 15:09 170-130
Toluene-d8 (Surr)99 09/27/16 15:09 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 13:43 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 13:43 1Barium0.0932
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 13:43 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 13:43 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 13:43 1Copper0.00560 J
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 13:43 1Lead0.00600
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 13:43 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 13:43 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 13:43 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 02:36 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 02:36 1Beryllium0.340 J
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 02:36 1Cobalt2.57
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 02:36 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 02:36 1Vanadium8.05 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 02:36 1Zinc12.2 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 10:48 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-2Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 09/21/16 11:15
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 16:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 16:39 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 16:39 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 16:39 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 16:39 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 16:39 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 16:39 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 16:39 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 16:39 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 16:39 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 16:39 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 16:39 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 16:39 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 16:39 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 16:39 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 16:39 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/27/16 16:39 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 16:39 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 16:39 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 16:39 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 16:39 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 16:39 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 16:39 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 16:39 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 16:39 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 16:39 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 16:39 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 16:39 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 16:39 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 16:39 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 16:39 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 16:39 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 16:39 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 16:39 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 16:39 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 16:39 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 16:39 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 16:39 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 16:39 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 16:39 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 16:39 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 16:39 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 16:39 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 16:39 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 16:39 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 16:39 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 16:39 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 16:39 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-2Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 09/21/16 11:15
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)97 70-130 09/27/16 16:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 09/27/16 16:39 170-130
1,2-Dichloroethane-d4 (Surr)96 09/27/16 16:39 170-130
Toluene-d8 (Surr)100 09/27/16 16:39 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:08 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:08 1Barium0.336
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:08 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:08 1Chromium0.00400 J
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:08 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:08 1Lead0.0188
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:08 1Nickel0.00380 J
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:08 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:08 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 02:09 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 02:09 1Beryllium0.963 J
10.0 0.500 ug/L 09/26/16 10:20 09/30/16 15:15 5Cobalt3.91 J
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 02:09 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 02:09 1Vanadium18.3 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 02:09 1Zinc28.3
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 10:58 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-3Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 09/21/16 10:20
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 17:08 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 17:08 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 17:08 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 17:08 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 17:08 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 17:08 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 17:08 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 17:08 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 17:08 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 17:08 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 17:08 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 17:08 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 17:08 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 17:08 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 17:08 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 17:08 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/27/16 17:08 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 17:08 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 17:08 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 17:08 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 17:08 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 17:08 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 17:08 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 17:08 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 17:08 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 17:08 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 17:08 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 17:08 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 17:08 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 17:08 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 17:08 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 17:08 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 17:08 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 17:08 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 17:08 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 17:08 1Tetrahydrofuran1.46 J
1.00 0.170 ug/L 09/27/16 17:08 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 17:08 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 17:08 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 17:08 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 17:08 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 17:08 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 17:08 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 17:08 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 17:08 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 17:08 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 17:08 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 17:08 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-3Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 09/21/16 10:20
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)99 70-130 09/27/16 17:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 09/27/16 17:08 170-130
1,2-Dichloroethane-d4 (Surr)95 09/27/16 17:08 170-130
Toluene-d8 (Surr)100 09/27/16 17:08 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.0860 0.100 0.0860 mg/L 09/26/16 10:16 09/27/16 14:24 10
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.100 0.0500 mg/L 09/26/16 10:16 09/27/16 14:24 10Barium3.13
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:24 10Cadmium0.0210
0.0500 0.0300 mg/L 09/26/16 10:16 09/27/16 14:24 10Chromium0.417
0.100 0.0500 mg/L 09/26/16 10:16 09/27/16 14:24 10Copper0.278
0.0500 0.0200 mg/L 09/26/16 10:16 09/27/16 14:24 10Lead0.102
0.100 0.0300 mg/L 09/26/16 10:16 09/27/16 14:24 10Nickel0.114
0.100 0.0500 mg/L 09/26/16 10:16 09/27/16 14:24 10Selenium<0.0500
0.0500 0.0300 mg/L 09/26/16 10:16 09/27/16 14:24 10Silver<0.0300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 15:31 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 15:31 1Beryllium10.3
20.0 1.00 ug/L 09/26/16 10:20 09/30/16 02:41 10Cobalt125
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 15:31 1Thallium1.44 J
20.0 7.00 ug/L 09/26/16 10:20 09/30/16 02:41 10Vanadium532 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 15:31 1Zinc784
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:01 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 09/22/16 10:34
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 17:38 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 17:38 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 17:38 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 17:38 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 17:38 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 17:38 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 17:38 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 17:38 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 17:38 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 17:38 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 17:38 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 17:38 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 17:38 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 17:38 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 17:38 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 17:38 1cis-1,2-Dichloroethene 14.4
1.00 0.170 ug/L 09/27/16 17:38 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 17:38 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 17:38 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 17:38 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 17:38 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 17:38 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 17:38 11,1-Dichloroethane 0.512 J
1.00 0.200 ug/L 09/27/16 17:38 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 17:38 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 17:38 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 17:38 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 17:38 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 17:38 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 17:38 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 17:38 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 17:38 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 17:38 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 17:38 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 17:38 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 17:38 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 17:38 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 17:38 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 17:38 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 17:38 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 17:38 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 17:38 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 17:38 1Trichloroethene0.768 J
1.00 0.210 ug/L 09/27/16 17:38 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 17:38 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 17:38 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 17:38 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 17:38 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 09/22/16 10:34
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)98 70-130 09/27/16 17:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 09/27/16 17:38 170-130
1,2-Dichloroethane-d4 (Surr)95 09/27/16 17:38 170-130
Toluene-d8 (Surr)100 09/27/16 17:38 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:29 1Barium0.175
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:29 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:29 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:29 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:29 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:29 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:29 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:29 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 02:47 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 02:47 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 02:47 1Cobalt<0.100
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 02:47 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 02:47 1Vanadium2.13 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 02:47 1Zinc25.1
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:04 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 09/22/16 10:34
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 18:08 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 18:08 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 18:08 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 18:08 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 18:08 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 18:08 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 18:08 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 18:08 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 18:08 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 18:08 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 18:08 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 18:08 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 18:08 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 18:08 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 18:08 1cis-1,2-Dichloroethene 14.0
1.00 0.170 ug/L 09/27/16 18:08 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 18:08 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 18:08 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 18:08 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 18:08 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 18:08 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 18:08 11,1-Dichloroethane 0.460 J
1.00 0.200 ug/L 09/27/16 18:08 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 18:08 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 18:08 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 18:08 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 18:08 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 18:08 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 18:08 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 18:08 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 18:08 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 18:08 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 18:08 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 18:08 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 18:08 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 18:08 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 18:08 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 18:08 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 18:08 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 18:08 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 18:08 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 18:08 1Trichloroethene0.708 J
1.00 0.210 ug/L 09/27/16 18:08 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 18:08 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 18:08 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 18:08 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 18:08 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 09/22/16 10:34
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)97 70-130 09/27/16 18:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)99 09/27/16 18:08 170-130
1,2-Dichloroethane-d4 (Surr)94 09/27/16 18:08 170-130
Toluene-d8 (Surr)100 09/27/16 18:08 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:34 1Barium0.169
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:34 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:34 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:34 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:34 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:34 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:34 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:34 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:03 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:03 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:03 1Cobalt<0.100
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:03 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 03:03 1Vanadium2.05 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 03:03 1Zinc20.4 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 09/22/16 14:30
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 18:38 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 18:38 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 18:38 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 18:38 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 18:38 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 18:38 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 18:38 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 18:38 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 18:38 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 18:38 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 18:38 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 18:38 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 18:38 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 18:38 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 18:38 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 18:38 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/27/16 18:38 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 18:38 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 18:38 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 18:38 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 18:38 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 18:38 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 18:38 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 18:38 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 18:38 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 18:38 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 18:38 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 18:38 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 18:38 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 18:38 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 18:38 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 18:38 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 18:38 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 18:38 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 18:38 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 18:38 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 18:38 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 18:38 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 18:38 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 18:38 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 18:38 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 18:38 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 18:38 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 18:38 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 18:38 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 18:38 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 18:38 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 18:38 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 09/22/16 14:30
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)100 70-130 09/27/16 18:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 09/27/16 18:38 170-130
1,2-Dichloroethane-d4 (Surr)94 09/27/16 18:38 170-130
Toluene-d8 (Surr)99 09/27/16 18:38 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:39 1Barium0.00880 J
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:39 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:39 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:39 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:39 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:39 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:39 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:39 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:09 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:09 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:09 1Cobalt<0.100
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:09 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 03:09 1Vanadium1.86 J B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 03:09 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-7Client Sample ID: MW-4
Matrix: WaterDate Collected: 09/22/16 14:03
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 19:08 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 19:08 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 19:08 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 19:08 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 19:08 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 19:08 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 19:08 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 19:08 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 19:08 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 19:08 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 19:08 1Chlorobenzene0.347 J
1.00 0.250 ug/L 09/27/16 19:08 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 19:08 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 19:08 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 19:08 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 19:08 1cis-1,2-Dichloroethene 1.71
1.00 0.170 ug/L 09/27/16 19:08 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 19:08 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 19:08 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 19:08 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 19:08 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 19:08 11,4-Dichlorobenzene 0.317 J
1.00 0.240 ug/L 09/27/16 19:08 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 19:08 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 19:08 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 19:08 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 19:08 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 19:08 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 19:08 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 19:08 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 19:08 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 19:08 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 19:08 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 19:08 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 19:08 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 19:08 1Tetrahydrofuran1.50 J
1.00 0.170 ug/L 09/27/16 19:08 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 19:08 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 19:08 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 19:08 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 19:08 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 19:08 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 19:08 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 19:08 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 19:08 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 19:08 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 19:08 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 19:08 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-7Client Sample ID: MW-4
Matrix: WaterDate Collected: 09/22/16 14:03
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)97 70-130 09/27/16 19:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)97 09/27/16 19:08 170-130
1,2-Dichloroethane-d4 (Surr)93 09/27/16 19:08 170-130
Toluene-d8 (Surr)100 09/27/16 19:08 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:44 1Barium0.318
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:44 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:44 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:44 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:44 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:44 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:44 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:44 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:14 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:14 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:14 1Cobalt0.823 J
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:14 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 03:14 1Vanadium3.30 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 03:14 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:14 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-8Client Sample ID: SP-1
Matrix: WaterDate Collected: 09/22/16 11:30
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 19:38 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 19:38 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 19:38 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 19:38 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 19:38 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 19:38 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 19:38 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 19:38 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 19:38 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 19:38 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 19:38 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/27/16 19:38 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/27/16 19:38 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 19:38 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 19:38 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 19:38 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/27/16 19:38 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/27/16 19:38 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 19:38 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 19:38 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 19:38 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 19:38 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 19:38 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 19:38 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 19:38 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 19:38 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 19:38 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 19:38 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 19:38 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 19:38 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 19:38 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 19:38 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 19:38 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 19:38 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 19:38 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 19:38 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 19:38 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 19:38 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 19:38 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 19:38 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 19:38 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 19:38 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 19:38 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 19:38 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 19:38 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 19:38 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 19:38 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 19:38 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-8Client Sample ID: SP-1
Matrix: WaterDate Collected: 09/22/16 11:30
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)97 70-130 09/27/16 19:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 09/27/16 19:38 170-130
1,2-Dichloroethane-d4 (Surr)95 09/27/16 19:38 170-130
Toluene-d8 (Surr)99 09/27/16 19:38 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:49 1Barium0.126
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:49 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:49 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:49 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:49 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:49 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:49 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:49 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:20 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:20 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:20 1Cobalt0.959 J
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:20 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 03:20 1Vanadium3.03 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 03:20 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:17 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-9Client Sample ID: SS-1
Matrix: WaterDate Collected: 09/22/16 10:55
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/28/16 04:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/28/16 04:34 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/28/16 04:34 1Benzene<0.200
1.00 0.150 ug/L 09/28/16 04:34 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/28/16 04:34 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/28/16 04:34 1Bromoform<0.290
1.00 0.350 ug/L 09/28/16 04:34 1Bromomethane<0.350
50.0 2.64 ug/L 09/28/16 04:34 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/28/16 04:34 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/28/16 04:34 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/28/16 04:34 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/28/16 04:34 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/28/16 04:34 1Chloroethane<0.360
1.00 0.230 ug/L 09/28/16 04:34 1Chloroform<0.230
1.00 0.360 ug/L 09/28/16 04:34 1Chloromethane<0.360
1.00 0.210 ug/L 09/28/16 04:34 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/28/16 04:34 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/28/16 04:34 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/28/16 04:34 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/28/16 04:34 1Dibromomethane<0.450
1.00 0.190 ug/L 09/28/16 04:34 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/28/16 04:34 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/28/16 04:34 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/28/16 04:34 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/28/16 04:34 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/28/16 04:34 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/28/16 04:34 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/28/16 04:34 12-Hexanone <1.28
10.0 1.50 ug/L 09/28/16 04:34 1Iodomethane<1.50 *
5.00 1.00 ug/L 09/28/16 04:34 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/28/16 04:34 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/28/16 04:34 1Styrene<0.280
1.00 0.150 ug/L 09/28/16 04:34 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/28/16 04:34 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/28/16 04:34 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/28/16 04:34 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/28/16 04:34 1Toluene<0.170
5.00 0.460 ug/L 09/28/16 04:34 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/28/16 04:34 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/28/16 04:34 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/28/16 04:34 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/28/16 04:34 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/28/16 04:34 1Trichloroethene<0.200
1.00 0.210 ug/L 09/28/16 04:34 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/28/16 04:34 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/28/16 04:34 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/28/16 04:34 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/28/16 04:34 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-9Client Sample ID: SS-1
Matrix: WaterDate Collected: 09/22/16 10:55
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)99 70-130 09/28/16 04:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)99 09/28/16 04:34 170-130
1,2-Dichloroethane-d4 (Surr)93 09/28/16 04:34 170-130
Toluene-d8 (Surr)100 09/28/16 04:34 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 14:55 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:55 1Barium0.0383
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 14:55 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:55 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:55 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 14:55 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 14:55 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 14:55 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 14:55 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:25 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:25 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:25 1Cobalt0.268 J
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:25 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 03:25 1Vanadium2.38 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 03:25 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:20 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-10Client Sample ID: SS-2
Matrix: WaterDate Collected: 09/22/16 11:05
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/28/16 04:04 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/28/16 04:04 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/28/16 04:04 1Benzene<0.200
1.00 0.150 ug/L 09/28/16 04:04 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/28/16 04:04 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/28/16 04:04 1Bromoform<0.290
1.00 0.350 ug/L 09/28/16 04:04 1Bromomethane<0.350
50.0 2.64 ug/L 09/28/16 04:04 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/28/16 04:04 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/28/16 04:04 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/28/16 04:04 1Chlorobenzene<0.180
1.00 0.250 ug/L 09/28/16 04:04 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 09/28/16 04:04 1Chloroethane<0.360
1.00 0.230 ug/L 09/28/16 04:04 1Chloroform<0.230
1.00 0.360 ug/L 09/28/16 04:04 1Chloromethane<0.360
1.00 0.210 ug/L 09/28/16 04:04 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/28/16 04:04 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 09/28/16 04:04 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/28/16 04:04 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/28/16 04:04 1Dibromomethane<0.450
1.00 0.190 ug/L 09/28/16 04:04 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/28/16 04:04 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/28/16 04:04 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/28/16 04:04 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/28/16 04:04 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/28/16 04:04 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/28/16 04:04 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/28/16 04:04 12-Hexanone <1.28
10.0 1.50 ug/L 09/28/16 04:04 1Iodomethane<1.50 *
5.00 1.00 ug/L 09/28/16 04:04 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/28/16 04:04 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/28/16 04:04 1Styrene<0.280
1.00 0.150 ug/L 09/28/16 04:04 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/28/16 04:04 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/28/16 04:04 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/28/16 04:04 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/28/16 04:04 1Toluene<0.170
5.00 0.460 ug/L 09/28/16 04:04 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/28/16 04:04 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/28/16 04:04 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/28/16 04:04 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/28/16 04:04 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/28/16 04:04 1Trichloroethene<0.200
1.00 0.210 ug/L 09/28/16 04:04 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/28/16 04:04 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/28/16 04:04 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/28/16 04:04 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/28/16 04:04 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-10Client Sample ID: SS-2
Matrix: WaterDate Collected: 09/22/16 11:05
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)101 70-130 09/28/16 04:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)104 09/28/16 04:04 170-130
1,2-Dichloroethane-d4 (Surr)91 09/28/16 04:04 170-130
Toluene-d8 (Surr)100 09/28/16 04:04 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 15:00 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 15:00 1Barium0.0333
0.00100 0.000500 mg/L 09/26/16 10:16 09/27/16 15:00 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 15:00 1Chromium<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 15:00 1Copper<0.00500
0.00500 0.00200 mg/L 09/26/16 10:16 09/27/16 15:00 1Lead<0.00200
0.0100 0.00300 mg/L 09/26/16 10:16 09/27/16 15:00 1Nickel<0.00300
0.0100 0.00500 mg/L 09/26/16 10:16 09/27/16 15:00 1Selenium<0.00500
0.00500 0.00300 mg/L 09/26/16 10:16 09/27/16 15:00 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:31 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:31 1Beryllium<0.100
2.00 0.100 ug/L 09/26/16 10:20 09/30/16 03:31 1Cobalt0.146 J
2.00 0.800 ug/L 09/26/16 10:20 09/30/16 03:31 1Thallium<0.800
2.00 0.700 ug/L 09/26/16 10:20 09/30/16 03:31 1Vanadium2.59 B
25.0 5.20 ug/L 09/26/16 10:20 09/30/16 03:31 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 11:23 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-11Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 09/22/16 00:01
Date Received: 09/23/16 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 14:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 09/27/16 14:39 1Acrylonitrile<0.500
1.00 0.200 ug/L 09/27/16 14:39 1Benzene<0.200
1.00 0.150 ug/L 09/27/16 14:39 1Bromochloromethane<0.150
1.00 0.170 ug/L 09/27/16 14:39 1Bromodichloromethane<0.170
1.00 0.290 ug/L 09/27/16 14:39 1Bromoform<0.290
1.00 0.350 ug/L 09/27/16 14:39 1Bromomethane<0.350
50.0 2.64 ug/L 09/27/16 14:39 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 09/27/16 14:39 1Carbon disulfide <0.220
1.00 0.180 ug/L 09/27/16 14:39 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 09/27/16 14:39 1Chlorobenzene<0.180
1.00 0.360 ug/L 09/27/16 14:39 1Chloroethane<0.360
1.00 0.230 ug/L 09/27/16 14:39 1Chloroform<0.230
1.00 0.360 ug/L 09/27/16 14:39 1Chloromethane<0.360
1.00 0.210 ug/L 09/27/16 14:39 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 09/27/16 14:39 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 09/27/16 14:39 1Dibromochloromethane<0.250
10.0 0.940 ug/L 09/27/16 14:39 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 09/27/16 14:39 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 09/27/16 14:39 1Dibromomethane<0.450
1.00 0.190 ug/L 09/27/16 14:39 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 09/27/16 14:39 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 09/27/16 14:39 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 09/27/16 14:39 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 09/27/16 14:39 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 09/27/16 14:39 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 09/27/16 14:39 1Ethylbenzene<0.190
10.0 1.28 ug/L 09/27/16 14:39 12-Hexanone <1.28
10.0 1.50 ug/L 09/27/16 14:39 1Iodomethane<1.50
5.00 1.00 ug/L 09/27/16 14:39 1Methylene Chloride <1.00
10.0 0.810 ug/L 09/27/16 14:39 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 09/27/16 14:39 1Styrene<0.280
1.00 0.150 ug/L 09/27/16 14:39 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 09/27/16 14:39 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 09/27/16 14:39 1Tetrachloroethene<0.140
10.0 0.820 ug/L 09/27/16 14:39 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 09/27/16 14:39 1Toluene<0.170
5.00 0.460 ug/L 09/27/16 14:39 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 09/27/16 14:39 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 09/27/16 14:39 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 09/27/16 14:39 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 09/27/16 14:39 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 09/27/16 14:39 1Trichloroethene<0.200
1.00 0.210 ug/L 09/27/16 14:39 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 09/27/16 14:39 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 09/27/16 14:39 1Vinyl acetate <1.71
1.00 0.180 ug/L 09/27/16 14:39 1Vinyl chloride <0.180
3.00 0.580 ug/L 09/27/16 14:39 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-112432-11Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 09/22/16 00:01
Date Received: 09/23/16 09:25
4-Bromofluorobenzene (Surr)97 70-130 09/27/16 14:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 09/27/16 14:39 170-130
1,2-Dichloroethane-d4 (Surr)93 09/27/16 14:39 170-130
Toluene-d8 (Surr)99 09/27/16 14:39 170-130
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-373413/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373413
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/27/16 14:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 09/27/16 14:10 1Acrylonitrile
<0.200 0.2001.00 ug/L 09/27/16 14:10 1Benzene
<0.150 0.1501.00 ug/L 09/27/16 14:10 1Bromochloromethane
<0.170 0.1701.00 ug/L 09/27/16 14:10 1Bromodichloromethane
<0.290 0.2901.00 ug/L 09/27/16 14:10 1Bromoform
<0.350 0.3501.00 ug/L 09/27/16 14:10 1Bromomethane
<2.64 2.6450.0 ug/L 09/27/16 14:10 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 09/27/16 14:10 1Carbon disulfide
<0.180 0.1801.00 ug/L 09/27/16 14:10 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 09/27/16 14:10 1Chlorobenzene
<0.360 0.3601.00 ug/L 09/27/16 14:10 1Chloroethane
<0.230 0.2301.00 ug/L 09/27/16 14:10 1Chloroform
<0.360 0.3601.00 ug/L 09/27/16 14:10 1Chloromethane
<0.210 0.2101.00 ug/L 09/27/16 14:10 1cis-1,2-Dichloroethene
<0.250 0.2501.00 ug/L 09/27/16 14:10 1Chlorodibromomethane
<0.170 0.1701.00 ug/L 09/27/16 14:10 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 09/27/16 14:10 1Dibromochloromethane
<0.940 0.94010.0 ug/L 09/27/16 14:10 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 09/27/16 14:10 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 09/27/16 14:10 1Dibromomethane
<0.190 0.1901.00 ug/L 09/27/16 14:10 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 09/27/16 14:10 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 09/27/16 14:10 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 09/27/16 14:10 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 09/27/16 14:10 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 09/27/16 14:10 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 09/27/16 14:10 1Ethylbenzene
<1.28 1.2810.0 ug/L 09/27/16 14:10 12-Hexanone
<1.50 1.5010.0 ug/L 09/27/16 14:10 1Iodomethane
<1.00 1.005.00 ug/L 09/27/16 14:10 1Methylene Chloride
<0.810 0.81010.0 ug/L 09/27/16 14:10 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 09/27/16 14:10 1Styrene
<0.150 0.1501.00 ug/L 09/27/16 14:10 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 09/27/16 14:10 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 09/27/16 14:10 1Tetrachloroethene
<0.820 0.82010.0 ug/L 09/27/16 14:10 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 09/27/16 14:10 1Toluene
<0.460 0.4605.00 ug/L 09/27/16 14:10 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 09/27/16 14:10 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 09/27/16 14:10 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 09/27/16 14:10 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 09/27/16 14:10 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 09/27/16 14:10 1Trichloroethene
<0.210 0.2101.00 ug/L 09/27/16 14:10 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 09/27/16 14:10 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 09/27/16 14:10 1Vinyl acetate
<0.180 0.1801.00 ug/L 09/27/16 14:10 1Vinyl chloride
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-373413/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373413
RL MDL
Xylenes, Total <0.580 3.00 0.580 ug/L 09/27/16 14:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromofluorobenzene (Surr)98 70-130 09/27/16 14:10 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
98 09/27/16 14:10 1Dibromofluoromethane (Surr)70-130
93 09/27/16 14:10 11,2-Dichloroethane-d4 (Surr)70 -130
100 09/27/16 14:10 1Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373413/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373413
Acetone 100 103.7 ug/L 104 39 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 192.4 ug/L 96 63 -135
Benzene 20.0 19.67 ug/L 98 70 -130
Bromochloromethane 20.0 19.74 ug/L 99 70 -130
Bromodichloromethane 20.0 17.77 ug/L 89 70 -130
Bromoform 20.0 15.43 ug/L 77 70 -137
Bromomethane 20.0 10.62 ug/L 53 53 -150
2-Butanone (MEK)100 98.33 ug/L 98 55 -143
Carbon disulfide 20.0 18.62 ug/L 93 64 -135
Carbon tetrachloride 20.0 19.02 ug/L 95 70 -147
Chlorobenzene 20.0 19.56 ug/L 98 70 -130
Chloroethane 20.0 19.71 ug/L 99 60 -138
Chloroform 20.0 19.29 ug/L 96 70 -130
Chloromethane 20.0 13.79 ug/L 69 33 -150
cis-1,2-Dichloroethene 20.0 20.80 ug/L 104 70 -130
Chlorodibromomethane 20.0 18.07 ug/L 90 70 -133
cis-1,3-Dichloropropene 20.0 18.89 ug/L 94 70 -133
Dibromochloromethane 20.0 18.07 ug/L 90 70 -133
1,2-Dibromo-3-Chloropropane 20.0 18.51 ug/L 93 45 -138
1,2-Dibromoethane (EDB)20.0 18.74 ug/L 94 70 -130
Dibromomethane 20.0 19.49 ug/L 97 70 -130
1,2-Dichlorobenzene 20.0 19.48 ug/L 97 70 -130
1,4-Dichlorobenzene 20.0 18.88 ug/L 94 70 -130
1,1-Dichloroethane 20.0 20.87 ug/L 104 70 -130
1,2-Dichloroethane 20.0 18.75 ug/L 94 70 -130
1,1-Dichloroethene 20.0 20.20 ug/L 101 70 -132
1,2-Dichloropropane 20.0 19.20 ug/L 96 70 -130
Ethylbenzene 20.0 19.76 ug/L 99 70 -130
2-Hexanone 100 95.03 ug/L 95 54 -142
Iodomethane 20.0 17.36 ug/L 87 40 -150
Methylene Chloride 20.0 19.22 ug/L 96 70 -130
4-Methyl-2-pentanone (MIBK)100 95.61 ug/L 96 60 -137
Styrene 20.0 19.14 ug/L 96 70 -130
1,1,1,2-Tetrachloroethane 20.0 18.36 ug/L 92 70 -130
1,1,2,2-Tetrachloroethane 20.0 18.57 ug/L 93 69 -131
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373413/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373413
Tetrachloroethene 20.0 19.68 ug/L 98 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Tetrahydrofuran 40.0 36.61 ug/L 92 51 -136
Toluene 20.0 20.00 ug/L 100 70 -130
trans-1,4-Dichloro-2-butene 20.0 15.72 ug/L 79 41 -150
trans-1,2-Dichloroethene 20.0 19.41 ug/L 97 70 -130
trans-1,3-Dichloropropene 20.0 18.31 ug/L 92 63 -142
1,1,1-Trichloroethane 20.0 18.80 ug/L 94 70 -135
1,1,2-Trichloroethane 20.0 19.51 ug/L 98 70 -130
Trichloroethene 20.0 19.81 ug/L 99 70 -130
Trichlorofluoromethane 20.0 20.99 ug/L 105 59 -150
1,2,3-Trichloropropane 20.0 18.61 ug/L 93 70 -131
Vinyl acetate 40.0 40.74 ug/L 102 54 -146
Vinyl chloride 20.0 18.47 ug/L 92 57 -137
Xylenes, Total 40.0 38.09 ug/L 95 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-373601/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
RL MDL
Acetone <2.66 25.0 2.66 ug/L 09/28/16 03:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 09/28/16 03:05 1Acrylonitrile
<0.200 0.2001.00 ug/L 09/28/16 03:05 1Benzene
<0.150 0.1501.00 ug/L 09/28/16 03:05 1Bromochloromethane
<0.170 0.1701.00 ug/L 09/28/16 03:05 1Bromodichloromethane
<0.290 0.2901.00 ug/L 09/28/16 03:05 1Bromoform
<0.350 0.3501.00 ug/L 09/28/16 03:05 1Bromomethane
<2.64 2.6450.0 ug/L 09/28/16 03:05 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 09/28/16 03:05 1Carbon disulfide
<0.180 0.1801.00 ug/L 09/28/16 03:05 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 09/28/16 03:05 1Chlorobenzene
<0.360 0.3601.00 ug/L 09/28/16 03:05 1Chloroethane
<0.230 0.2301.00 ug/L 09/28/16 03:05 1Chloroform
<0.360 0.3601.00 ug/L 09/28/16 03:05 1Chloromethane
<0.210 0.2101.00 ug/L 09/28/16 03:05 1cis-1,2-Dichloroethene
<0.250 0.2501.00 ug/L 09/28/16 03:05 1Chlorodibromomethane
<0.170 0.1701.00 ug/L 09/28/16 03:05 1cis-1,3-Dichloropropene
<0.940 0.94010.0 ug/L 09/28/16 03:05 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 09/28/16 03:05 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 09/28/16 03:05 1Dibromomethane
<0.190 0.1901.00 ug/L 09/28/16 03:05 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 09/28/16 03:05 11,4-Dichlorobenzene
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-373601/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
RL MDL
1,1-Dichloroethane <0.240 1.00 0.240 ug/L 09/28/16 03:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.200 0.2001.00 ug/L 09/28/16 03:05 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 09/28/16 03:05 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 09/28/16 03:05 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 09/28/16 03:05 1Ethylbenzene
<1.28 1.2810.0 ug/L 09/28/16 03:05 12-Hexanone
<1.50 1.5010.0 ug/L 09/28/16 03:05 1Iodomethane
<1.00 1.005.00 ug/L 09/28/16 03:05 1Methylene Chloride
<0.810 0.81010.0 ug/L 09/28/16 03:05 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 09/28/16 03:05 1Styrene
<0.150 0.1501.00 ug/L 09/28/16 03:05 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 09/28/16 03:05 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 09/28/16 03:05 1Tetrachloroethene
<0.820 0.82010.0 ug/L 09/28/16 03:05 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 09/28/16 03:05 1Toluene
<0.460 0.4605.00 ug/L 09/28/16 03:05 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 09/28/16 03:05 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 09/28/16 03:05 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 09/28/16 03:05 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 09/28/16 03:05 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 09/28/16 03:05 1Trichloroethene
<0.210 0.2101.00 ug/L 09/28/16 03:05 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 09/28/16 03:05 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 09/28/16 03:05 1Vinyl acetate
<0.180 0.1801.00 ug/L 09/28/16 03:05 1Vinyl chloride
<0.580 0.5803.00 ug/L 09/28/16 03:05 1Xylenes, Total
4-Bromofluorobenzene (Surr)98 70-130 09/28/16 03:05 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
98 09/28/16 03:05 1Dibromofluoromethane (Surr)70-130
92 09/28/16 03:05 11,2-Dichloroethane-d4 (Surr)70 -130
101 09/28/16 03:05 1Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373601/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
Acetone 100 103.4 ug/L 103 39 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 204.2 ug/L 102 63 -135
Benzene 20.0 20.14 ug/L 101 70 -130
Bromochloromethane 20.0 20.68 ug/L 103 70 -130
Bromodichloromethane 20.0 18.51 ug/L 93 70 -130
Bromoform 20.0 16.53 ug/L 83 70 -137
Bromomethane 20.0 12.86 ug/L 64 53 -150
2-Butanone (MEK)100 101.6 ug/L 102 55 -143
Carbon disulfide 20.0 18.54 ug/L 93 64 -135
Carbon tetrachloride 20.0 19.20 ug/L 96 70 -147
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373601/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
Chlorobenzene 20.0 20.22 ug/L 101 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Chloroethane 20.0 20.30 ug/L 101 60 -138
Chloroform 20.0 19.67 ug/L 98 70 -130
Chloromethane 20.0 14.91 ug/L 75 33 -150
cis-1,2-Dichloroethene 20.0 21.43 ug/L 107 70 -130
Chlorodibromomethane 20.0 18.83 ug/L 94 70 -133
cis-1,3-Dichloropropene 20.0 19.03 ug/L 95 70 -133
1,2-Dibromo-3-Chloropropane 20.0 18.61 ug/L 93 45 -138
1,2-Dibromoethane (EDB)20.0 19.67 ug/L 98 70 -130
Dibromomethane 20.0 20.06 ug/L 100 70 -130
1,2-Dichlorobenzene 20.0 19.41 ug/L 97 70 -130
1,4-Dichlorobenzene 20.0 19.49 ug/L 97 70 -130
1,1-Dichloroethane 20.0 20.98 ug/L 105 70 -130
1,2-Dichloroethane 20.0 19.54 ug/L 98 70 -130
1,1-Dichloroethene 20.0 21.13 ug/L 106 70 -132
1,2-Dichloropropane 20.0 19.70 ug/L 99 70 -130
Ethylbenzene 20.0 20.38 ug/L 102 70 -130
2-Hexanone 100 103.0 ug/L 103 54 -142
Iodomethane 20.0 17.42 ug/L 87 40 -150
Methylene Chloride 20.0 20.02 ug/L 100 70 -130
4-Methyl-2-pentanone (MIBK)100 100.3 ug/L 100 60 -137
Styrene 20.0 19.59 ug/L 98 70 -130
1,1,1,2-Tetrachloroethane 20.0 19.18 ug/L 96 70 -130
1,1,2,2-Tetrachloroethane 20.0 18.57 ug/L 93 69 -131
Tetrachloroethene 20.0 20.08 ug/L 100 70 -130
Tetrahydrofuran 40.0 39.57 ug/L 99 51 -136
Toluene 20.0 20.33 ug/L 102 70 -130
trans-1,4-Dichloro-2-butene 20.0 17.27 ug/L 86 41 -150
trans-1,2-Dichloroethene 20.0 19.73 ug/L 99 70 -130
trans-1,3-Dichloropropene 20.0 18.76 ug/L 94 63 -142
1,1,1-Trichloroethane 20.0 19.19 ug/L 96 70 -135
1,1,2-Trichloroethane 20.0 20.49 ug/L 102 70 -130
Trichloroethene 20.0 20.03 ug/L 100 70 -130
Trichlorofluoromethane 20.0 21.39 ug/L 107 59 -150
1,2,3-Trichloropropane 20.0 19.88 ug/L 99 70 -131
Vinyl acetate 40.0 39.85 ug/L 100 54 -146
Vinyl chloride 20.0 18.97 ug/L 95 57 -137
Xylenes, Total 40.0 39.18 ug/L 98 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-373601/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
Acetone 100 108.3 ug/L 108 39 -150 5 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 203.7 ug/L 102 63 -135 0 16
Benzene 20.0 21.50 ug/L 108 70 -130 7 12
Bromochloromethane 20.0 21.77 ug/L 109 70 -130 5 16
Bromodichloromethane 20.0 19.91 ug/L 100 70 -130 7 14
Bromoform 20.0 16.63 ug/L 83 70 -137 1 14
Bromomethane 20.0 14.28 ug/L 71 53 -150 10 19
2-Butanone (MEK)100 104.1 ug/L 104 55 -143 2 19
Carbon disulfide 20.0 20.95 ug/L 105 64 -135 12 16
Carbon tetrachloride 20.0 21.48 ug/L 107 70 -147 11 16
Chlorobenzene 20.0 21.45 ug/L 107 70 -130 6 12
Chloroethane 20.0 22.51 ug/L 113 60 -138 10 15
Chloroform 20.0 21.67 ug/L 108 70 -130 10 14
Chloromethane 20.0 16.85 ug/L 84 33 -150 12 20
cis-1,2-Dichloroethene 20.0 23.09 ug/L 115 70 -130 7 15
Chlorodibromomethane 20.0 19.28 ug/L 96 70 -133 2 13
cis-1,3-Dichloropropene 20.0 19.83 ug/L 99 70 -133 4 15
1,2-Dibromo-3-Chloropropane 20.0 18.57 ug/L 93 45 -138 0 19
1,2-Dibromoethane (EDB)20.0 19.90 ug/L 99 70 -130 1 13
Dibromomethane 20.0 21.12 ug/L 106 70 -130 5 14
1,2-Dichlorobenzene 20.0 20.17 ug/L 101 70 -130 4 12
1,4-Dichlorobenzene 20.0 20.79 ug/L 104 70 -130 6 12
1,1-Dichloroethane 20.0 23.31 ug/L 117 70 -130 11 17
1,2-Dichloroethane 20.0 20.64 ug/L 103 70 -130 5 13
1,1-Dichloroethene 20.0 23.80 ug/L 119 70 -132 12 20
1,2-Dichloropropane 20.0 21.06 ug/L 105 70 -130 7 15
Ethylbenzene 20.0 21.57 ug/L 108 70 -130 6 12
2-Hexanone 100 98.91 ug/L 99 54 -142 4 17
Iodomethane 20.0 21.73 *ug/L 109 40 -150 22 20
Methylene Chloride 20.0 21.33 ug/L 107 70 -130 6 15
4-Methyl-2-pentanone (MIBK)100 97.93 ug/L 98 60 -137 2 21
Styrene 20.0 21.08 ug/L 105 70 -130 7 12
1,1,1,2-Tetrachloroethane 20.0 20.15 ug/L 101 70 -130 5 13
1,1,2,2-Tetrachloroethane 20.0 19.23 ug/L 96 69 -131 3 15
Tetrachloroethene 20.0 21.61 ug/L 108 70 -130 7 17
Tetrahydrofuran 40.0 38.34 ug/L 96 51 -136 3 20
Toluene 20.0 21.72 ug/L 109 70 -130 7 13
trans-1,4-Dichloro-2-butene 20.0 16.66 ug/L 83 41 -150 4 20
trans-1,2-Dichloroethene 20.0 21.65 ug/L 108 70 -130 9 15
trans-1,3-Dichloropropene 20.0 19.20 ug/L 96 63 -142 2 13
1,1,1-Trichloroethane 20.0 21.11 ug/L 106 70 -135 10 15
1,1,2-Trichloroethane 20.0 21.00 ug/L 105 70 -130 2 13
Trichloroethene 20.0 22.46 ug/L 112 70 -130 11 14
Trichlorofluoromethane 20.0 24.19 ug/L 121 59 -150 12 22
1,2,3-Trichloropropane 20.0 19.89 ug/L 99 70 -131 0 14
Vinyl acetate 40.0 40.66 ug/L 102 54 -146 2 20
Vinyl chloride 20.0 21.74 ug/L 109 57 -137 14 15
Xylenes, Total 40.0 41.36 ug/L 103 70 -132 5 11
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-112404-D-10 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
Acetone <2.66 100 105.4 ug/L 105 39 -150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 200.6 ug/L 100 50 -135
Benzene <0.200 20.0 21.64 ug/L 108 55 -147
Bromochloromethane <0.150 20.0 21.86 ug/L 109 59 -132
Bromodichloromethane <0.170 20.0 19.62 ug/L 98 70 -140
Bromoform <0.290 20.0 16.05 ug/L 80 53 -150
Bromomethane <0.350 20.0 11.95 ug/L 60 30 -150
2-Butanone (MEK)<2.64 100 99.25 ug/L 99 50 -143
Carbon disulfide <0.220 20.0 20.68 ug/L 103 35 -150
Carbon tetrachloride <0.180 20.0 21.76 ug/L 109 56 -150
Chlorobenzene <0.180 20.0 20.79 ug/L 104 70 -130
Chloroethane <0.360 20.0 22.62 ug/L 113 58 -141
Chloroform <0.230 20.0 22.41 ug/L 112 66 -138
Chloromethane <0.360 20.0 18.57 ug/L 93 10 -150
cis-1,2-Dichloroethene <0.210 20.0 23.28 ug/L 116 68 -131
Chlorodibromomethane <0.250 20.0 19.11 ug/L 96 66 -140
cis-1,3-Dichloropropene <0.170 20.0 19.29 ug/L 96 70 -133
1,2-Dibromo-3-Chloropropane <0.940 20.0 18.15 ug/L 91 38 -138
1,2-Dibromoethane (EDB)<0.210 20.0 19.92 ug/L 100 65 -137
Dibromomethane <0.450 20.0 21.63 ug/L 108 70 -130
1,2-Dichlorobenzene <0.190 20.0 19.96 ug/L 100 70 -130
1,4-Dichlorobenzene <0.170 20.0 19.58 ug/L 98 70 -130
1,1-Dichloroethane <0.240 20.0 23.88 ug/L 119 61 -139
1,2-Dichloroethane <0.200 20.0 20.49 ug/L 102 64 -136
1,1-Dichloroethene <0.250 20.0 25.00 ug/L 125 54 -150
1,2-Dichloropropane <0.250 20.0 20.68 ug/L 103 67 -130
Ethylbenzene <0.190 20.0 21.68 ug/L 108 65 -139
2-Hexanone <1.28 100 94.00 ug/L 94 44 -150
Iodomethane <1.50 *20.0 18.59 ug/L 93 34 -150
Methylene Chloride <1.00 20.0 21.10 ug/L 106 64 -130
4-Methyl-2-pentanone (MIBK)<0.810 100 96.35 ug/L 96 50 -140
Styrene <0.280 20.0 20.19 ug/L 101 70 -130
1,1,1,2-Tetrachloroethane <0.150 20.0 19.78 ug/L 99 70 -131
1,1,2,2-Tetrachloroethane <0.190 20.0 18.52 ug/L 93 56 -145
Tetrachloroethene <0.140 20.0 21.91 ug/L 110 57 -138
Tetrahydrofuran <0.820 40.0 39.28 ug/L 98 40 -136
Toluene <0.170 20.0 21.87 ug/L 109 64 -136
trans-1,4-Dichloro-2-butene <0.460 20.0 15.90 ug/L 79 39 -150
trans-1,2-Dichloroethene <0.230 20.0 22.13 ug/L 111 59 -143
trans-1,3-Dichloropropene <0.170 20.0 18.74 ug/L 94 63 -142
1,1,1-Trichloroethane <0.190 20.0 21.55 ug/L 108 68 -144
1,1,2-Trichloroethane <0.190 20.0 20.59 ug/L 103 70 -130
Trichloroethene <0.200 20.0 22.70 ug/L 114 63 -135
Trichlorofluoromethane <0.210 20.0 24.69 ug/L 123 44 -150
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-112404-D-10 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
1,2,3-Trichloropropane <0.230 20.0 18.73 ug/L 94 65 -131
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vinyl acetate <1.71 40.0 37.93 ug/L 95 43 -146
Vinyl chloride <0.180 20.0 21.87 ug/L 109 57 -150
Xylenes, Total <0.580 40.0 41.46 ug/L 104 69 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
MS MS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
921,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-112404-E-10 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
Acetone <2.66 100 100.9 ug/L 101 39 -150 4 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 209.7 ug/L 105 50 -135 4 23
Benzene <0.200 20.0 22.34 ug/L 112 55 -147 3 22
Bromochloromethane <0.150 20.0 21.94 ug/L 110 59 -132 0 21
Bromodichloromethane <0.170 20.0 19.95 ug/L 100 70 -140 2 196
Bromoform <0.290 20.0 16.68 ug/L 83 53 -150 4 20
Bromomethane <0.350 20.0 15.00 ug/L 75 30 -150 23 44
2-Butanone (MEK)<2.64 100 103.5 ug/L 103 50 -143 4 28
Carbon disulfide <0.220 20.0 20.83 ug/L 104 35 -150 1 34
Carbon tetrachloride <0.180 20.0 21.83 ug/L 109 56 -150 0 18
Chlorobenzene <0.180 20.0 21.58 ug/L 108 70 -130 4 15
Chloroethane <0.360 20.0 22.80 ug/L 114 58 -141 1 31
Chloroform <0.230 20.0 22.11 ug/L 111 66 -138 1 21
Chloromethane <0.360 20.0 16.89 ug/L 84 10 -150 9 43
cis-1,2-Dichloroethene <0.210 20.0 23.40 ug/L 117 68 -131 1 21
Chlorodibromomethane <0.250 20.0 19.65 ug/L 98 66 -140 3 19
cis-1,3-Dichloropropene <0.170 20.0 19.86 ug/L 99 70 -133 3 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 18.70 ug/L 93 38 -138 3 26
1,2-Dibromoethane (EDB)<0.210 20.0 20.37 ug/L 102 65 -137 2 21
Dibromomethane <0.450 20.0 21.00 ug/L 105 70 -130 3 19
1,2-Dichlorobenzene <0.190 20.0 20.52 ug/L 103 70 -130 3 15
1,4-Dichlorobenzene <0.170 20.0 20.41 ug/L 102 70 -130 4 14
1,1-Dichloroethane <0.240 20.0 23.69 ug/L 118 61 -139 1 23
1,2-Dichloroethane <0.200 20.0 20.71 ug/L 104 64 -136 1 22
1,1-Dichloroethene <0.250 20.0 23.35 ug/L 117 54 -150 7 24
1,2-Dichloropropane <0.250 20.0 20.94 ug/L 105 67 -130 1 19
Ethylbenzene <0.190 20.0 22.00 ug/L 110 65 -139 1 18
2-Hexanone <1.28 100 98.39 ug/L 98 44 -150 5 21
Iodomethane <1.50 *20.0 20.73 ug/L 104 34 -150 11 37
Methylene Chloride <1.00 20.0 21.03 ug/L 105 64 -130 0 22
4-Methyl-2-pentanone (MIBK)<0.810 100 101.0 ug/L 101 50 -140 5 24
Styrene <0.280 20.0 20.39 ug/L 102 70 -130 1 16
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-112404-E-10 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373601
1,1,1,2-Tetrachloroethane <0.150 20.0 20.27 ug/L 101 70 -131 2 16
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane <0.190 20.0 19.21 ug/L 96 56 -145 4 19
Tetrachloroethene <0.140 20.0 22.10 ug/L 111 57 -138 1 17
Tetrahydrofuran <0.820 40.0 36.34 ug/L 91 40 -136 8 27
Toluene <0.170 20.0 22.23 ug/L 111 64 -136 2 18
trans-1,4-Dichloro-2-butene <0.460 20.0 16.17 ug/L 81 39 -150 2 28
trans-1,2-Dichloroethene <0.230 20.0 21.92 ug/L 110 59 -143 1 25
trans-1,3-Dichloropropene <0.170 20.0 18.64 ug/L 93 63 -142 1 18
1,1,1-Trichloroethane <0.190 20.0 21.69 ug/L 108 68 -144 1 17
1,1,2-Trichloroethane <0.190 20.0 21.23 ug/L 106 70 -130 3 18
Trichloroethene <0.200 20.0 22.58 ug/L 113 63 -135 1 17
Trichlorofluoromethane <0.210 20.0 24.65 ug/L 123 44 -150 0 32
1,2,3-Trichloropropane <0.230 20.0 19.54 ug/L 98 65 -131 4 19
Vinyl acetate <1.71 40.0 38.13 ug/L 95 43 -146 1 20
Vinyl chloride <0.180 20.0 21.76 ug/L 109 57 -150 0 37
Xylenes, Total <0.580 40.0 42.40 ug/L 106 69 -132 2 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
MSD MSD
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-374875/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
Acetone 100 107.3 ug/L 107 39 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 215.9 ug/L 108 63 -135
Benzene 20.0 20.81 ug/L 104 70 -130
Bromochloromethane 20.0 19.52 ug/L 98 70 -130
Bromodichloromethane 20.0 19.31 ug/L 97 70 -130
Bromoform 20.0 17.03 ug/L 85 70 -137
Bromomethane 20.0 13.82 ug/L 69 53 -150
2-Butanone (MEK)100 99.37 ug/L 99 55 -143
Carbon disulfide 20.0 19.90 ug/L 99 64 -135
Carbon tetrachloride 20.0 20.59 ug/L 103 70 -147
Chlorobenzene 20.0 20.07 ug/L 100 70 -130
Chloroethane 20.0 21.81 ug/L 109 60 -138
Chloroform 20.0 21.27 ug/L 106 70 -130
Chloromethane 20.0 19.31 ug/L 97 33 -150
cis-1,2-Dichloroethene 20.0 21.29 ug/L 106 70 -130
Chlorodibromomethane 20.0 19.27 ug/L 96 70 -133
cis-1,3-Dichloropropene 20.0 20.43 ug/L 102 70 -133
Dibromochloromethane 20.0 19.27 ug/L 96 70 -133
1,2-Dibromo-3-Chloropropane 20.0 19.55 ug/L 98 45 -138
1,2-Dibromoethane (EDB)20.0 19.53 ug/L 98 70 -130
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-374875/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
Dibromomethane 20.0 19.89 ug/L 99 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichlorobenzene 20.0 19.88 ug/L 99 70 -130
1,4-Dichlorobenzene 20.0 19.75 ug/L 99 70 -130
1,1-Dichloroethane 20.0 23.14 ug/L 116 70 -130
1,2-Dichloroethane 20.0 20.64 ug/L 103 70 -130
1,1-Dichloroethene 20.0 21.82 ug/L 109 70 -132
1,2-Dichloropropane 20.0 20.79 ug/L 104 70 -130
Ethylbenzene 20.0 21.15 ug/L 106 70 -130
2-Hexanone 100 105.8 ug/L 106 54 -142
Iodomethane 20.0 18.00 ug/L 90 40 -150
Methylene Chloride 20.0 19.25 ug/L 96 70 -130
4-Methyl-2-pentanone (MIBK)100 107.4 ug/L 107 60 -137
Styrene 20.0 20.21 ug/L 101 70 -130
1,1,1,2-Tetrachloroethane 20.0 19.76 ug/L 99 70 -130
1,1,2,2-Tetrachloroethane 20.0 20.17 ug/L 101 69 -131
Tetrachloroethene 20.0 20.73 ug/L 104 70 -130
Tetrahydrofuran 40.0 46.35 ug/L 116 51 -136
Toluene 20.0 21.27 ug/L 106 70 -130
trans-1,4-Dichloro-2-butene 20.0 19.55 ug/L 98 41 -150
trans-1,2-Dichloroethene 20.0 22.53 ug/L 113 70 -130
trans-1,3-Dichloropropene 20.0 20.10 ug/L 100 63 -142
1,1,1-Trichloroethane 20.0 20.80 ug/L 104 70 -135
1,1,2-Trichloroethane 20.0 20.25 ug/L 101 70 -130
Trichloroethene 20.0 19.87 ug/L 99 70 -130
Trichlorofluoromethane 20.0 23.68 ug/L 118 59 -150
1,2,3-Trichloropropane 20.0 19.52 ug/L 98 70 -131
Vinyl acetate 40.0 40.89 ug/L 102 54 -146
Vinyl chloride 20.0 20.99 ug/L 105 57 -137
Xylenes, Total 40.0 41.01 ug/L 103 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1041,2-Dichloroethane-d4 (Surr)70 -130
104Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-374875/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
Acetone 100 102.9 ug/L 103 39 -150 4 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 206.8 ug/L 103 63 -135 4 16
Benzene 20.0 20.66 ug/L 103 70 -130 1 12
Bromochloromethane 20.0 19.12 ug/L 96 70 -130 2 16
Bromodichloromethane 20.0 19.45 ug/L 97 70 -130 1 14
Bromoform 20.0 16.14 ug/L 81 70 -137 5 14
Bromomethane 20.0 14.61 ug/L 73 53 -150 6 19
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-374875/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
2-Butanone (MEK)100 96.54 ug/L 97 55 -143 3 19
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Carbon disulfide 20.0 19.67 ug/L 98 64 -135 1 16
Carbon tetrachloride 20.0 20.51 ug/L 103 70 -147 0 16
Chlorobenzene 20.0 20.40 ug/L 102 70 -130 2 12
Chloroethane 20.0 22.13 ug/L 111 60 -138 1 15
Chloroform 20.0 21.21 ug/L 106 70 -130 0 14
Chloromethane 20.0 18.72 ug/L 94 33 -150 3 20
cis-1,2-Dichloroethene 20.0 21.59 ug/L 108 70 -130 1 15
Chlorodibromomethane 20.0 19.21 ug/L 96 70 -133 0 13
cis-1,3-Dichloropropene 20.0 20.26 ug/L 101 70 -133 1 15
Dibromochloromethane 20.0 19.21 ug/L 96 70 -133 0 13
1,2-Dibromo-3-Chloropropane 20.0 19.35 ug/L 97 45 -138 1 19
1,2-Dibromoethane (EDB)20.0 19.28 ug/L 96 70 -130 1 13
Dibromomethane 20.0 19.76 ug/L 99 70 -130 1 14
1,2-Dichlorobenzene 20.0 19.99 ug/L 100 70 -130 1 12
1,4-Dichlorobenzene 20.0 19.88 ug/L 99 70 -130 1 12
1,1-Dichloroethane 20.0 23.57 ug/L 118 70 -130 2 17
1,2-Dichloroethane 20.0 20.68 ug/L 103 70 -130 0 13
1,1-Dichloroethene 20.0 21.70 ug/L 108 70 -132 1 20
1,2-Dichloropropane 20.0 21.13 ug/L 106 70 -130 2 15
Ethylbenzene 20.0 21.47 ug/L 107 70 -130 2 12
2-Hexanone 100 102.8 ug/L 103 54 -142 3 17
Iodomethane 20.0 18.69 ug/L 93 40 -150 4 20
Methylene Chloride 20.0 19.40 ug/L 97 70 -130 1 15
4-Methyl-2-pentanone (MIBK)100 103.7 ug/L 104 60 -137 4 21
Styrene 20.0 20.16 ug/L 101 70 -130 0 12
1,1,1,2-Tetrachloroethane 20.0 19.86 ug/L 99 70 -130 1 13
1,1,2,2-Tetrachloroethane 20.0 19.64 ug/L 98 69 -131 3 15
Tetrachloroethene 20.0 20.97 ug/L 105 70 -130 1 17
Tetrahydrofuran 40.0 42.39 ug/L 106 51 -136 9 20
Toluene 20.0 21.73 ug/L 109 70 -130 2 13
trans-1,4-Dichloro-2-butene 20.0 18.93 ug/L 95 41 -150 3 20
trans-1,2-Dichloroethene 20.0 22.49 ug/L 112 70 -130 0 15
trans-1,3-Dichloropropene 20.0 19.63 ug/L 98 63 -142 2 13
1,1,1-Trichloroethane 20.0 20.59 ug/L 103 70 -135 1 15
1,1,2-Trichloroethane 20.0 20.33 ug/L 102 70 -130 0 13
Trichloroethene 20.0 20.17 ug/L 101 70 -130 1 14
Trichlorofluoromethane 20.0 23.61 ug/L 118 59 -150 0 22
1,2,3-Trichloropropane 20.0 19.13 ug/L 96 70 -131 2 14
Vinyl acetate 40.0 38.17 ug/L 95 54 -146 7 20
Vinyl chloride 20.0 21.07 ug/L 105 57 -137 0 15
Xylenes, Total 40.0 40.76 ug/L 102 70 -132 1 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
104Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-3RLab Sample ID: 490-112432-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
Bromomethane <0.350 20.0 16.41 ug/L 82 30 -150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Chloroethane <0.360 20.0 24.76 ug/L 124 58 -141
Chloromethane <0.360 20.0 19.24 ug/L 96 10 -150
Trichlorofluoromethane <0.210 20.0 26.63 ug/L 133 44 -150
Vinyl chloride <0.180 20.0 24.60 ug/L 123 57 -150
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
MS MS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
1021,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: MW-3RLab Sample ID: 490-112432-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
Acetone <2.66 100 113.0 ug/L 113 39 -150 1 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 225.4 ug/L 113 50 -135 2 23
Benzene <0.200 20.0 23.64 ug/L 118 55 -147 0 22
Bromochloromethane <0.150 20.0 20.97 ug/L 105 59 -132 1 21
Bromodichloromethane <0.170 20.0 21.99 ug/L 110 70 -140 2 196
Bromoform <0.290 20.0 18.38 ug/L 92 53 -150 2 20
Bromomethane <0.350 20.0 16.84 ug/L 84 30 -150 3 44
2-Butanone (MEK)<2.64 100 107.4 ug/L 107 50 -143 3 28
Carbon disulfide <0.220 20.0 22.47 ug/L 112 35 -150 1 34
Carbon tetrachloride <0.180 20.0 24.61 ug/L 123 56 -150 2 18
Chlorobenzene <0.180 20.0 22.56 ug/L 113 70 -130 0 15
Chloroethane <0.360 20.0 25.04 ug/L 125 58 -141 1 31
Chloroform <0.230 20.0 24.11 ug/L 121 66 -138 1 21
Chloromethane <0.360 20.0 18.38 ug/L 92 10 -150 5 43
cis-1,2-Dichloroethene <0.210 20.0 24.25 ug/L 121 68 -131 0 21
Chlorodibromomethane <0.250 20.0 21.34 ug/L 107 66 -140 3 19
cis-1,3-Dichloropropene <0.170 20.0 23.50 ug/L 117 70 -133 3 19
Dibromochloromethane <0.250 20.0 21.34 ug/L 107 66 -140 3 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 21.35 ug/L 107 38 -138 2 26
1,2-Dibromoethane (EDB)<0.210 20.0 21.12 ug/L 106 65 -137 1 21
Dibromomethane <0.450 20.0 21.91 ug/L 110 70 -130 4 19
1,2-Dichlorobenzene <0.190 20.0 22.76 ug/L 114 70 -130 4 15
1,4-Dichlorobenzene <0.170 20.0 22.36 ug/L 112 70 -130 1 14
1,1-Dichloroethane <0.240 20.0 26.23 ug/L 131 61 -139 2 23
1,2-Dichloroethane <0.200 20.0 22.85 ug/L 114 64 -136 1 22
1,1-Dichloroethene <0.250 20.0 25.46 ug/L 127 54 -150 0 24
1,2-Dichloropropane <0.250 20.0 23.42 ug/L 117 67 -130 2 19
Ethylbenzene <0.190 20.0 24.56 ug/L 123 65 -139 0 18
2-Hexanone <1.28 100 111.6 ug/L 112 44 -150 0 21
Iodomethane <1.50 20.0 21.57 ug/L 108 34 -150 2 37
Methylene Chloride <1.00 20.0 21.61 ug/L 108 64 -130 0 22
4-Methyl-2-pentanone (MIBK)<0.810 100 111.5 ug/L 112 50 -140 2 24
Styrene <0.280 20.0 22.82 ug/L 114 70 -130 0 16
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-3RLab Sample ID: 490-112432-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374875
1,1,1,2-Tetrachloroethane <0.150 20.0 21.85 ug/L 109 70 -131 0 16
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane <0.190 20.0 21.18 ug/L 106 56 -145 0 19
Tetrachloroethene <0.140 20.0 24.44 ug/L 122 57 -138 1 17
Tetrahydrofuran <0.820 40.0 45.00 ug/L 113 40 -136 0 27
Toluene <0.170 20.0 24.41 ug/L 122 64 -136 0 18
trans-1,4-Dichloro-2-butene <0.460 20.0 21.25 ug/L 106 39 -150 1 28
trans-1,2-Dichloroethene <0.230 20.0 25.79 ug/L 129 59 -143 0 25
trans-1,3-Dichloropropene <0.170 20.0 22.30 ug/L 111 63 -142 0 18
1,1,1-Trichloroethane <0.190 20.0 23.92 ug/L 120 68 -144 0 17
1,1,2-Trichloroethane <0.190 20.0 22.48 ug/L 112 70 -130 3 18
Trichloroethene <0.200 20.0 22.85 ug/L 114 63 -135 1 17
Trichlorofluoromethane <0.210 20.0 26.81 ug/L 134 44 -150 1 32
1,2,3-Trichloropropane <0.230 20.0 21.50 ug/L 108 65 -131 2 19
Vinyl acetate <1.71 40.0 44.51 ug/L 111 43 -146 6 20
Vinyl chloride <0.180 20.0 24.23 ug/L 121 57 -150 2 37
Xylenes, Total <0.580 40.0 47.29 ug/L 118 69 -132 2 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MSD MSD
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1011,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-373109/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373674 Prep Batch: 373109
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/26/16 10:16 09/27/16 13:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 09/26/16 10:16 09/27/16 13:27 1Barium
<0.000500 0.0005000.00100 mg/L 09/26/16 10:16 09/27/16 13:27 1Cadmium
<0.00300 0.003000.00500 mg/L 09/26/16 10:16 09/27/16 13:27 1Chromium
<0.00500 0.005000.0100 mg/L 09/26/16 10:16 09/27/16 13:27 1Copper
<0.00200 0.002000.00500 mg/L 09/26/16 10:16 09/27/16 13:27 1Lead
<0.00300 0.003000.0100 mg/L 09/26/16 10:16 09/27/16 13:27 1Nickel
<0.00500 0.005000.0100 mg/L 09/26/16 10:16 09/27/16 13:27 1Selenium
<0.00300 0.003000.00500 mg/L 09/26/16 10:16 09/27/16 13:27 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373109/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373674 Prep Batch: 373109
Arsenic 0.0500 0.04340 mg/L 87 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 1.976 mg/L 99 80 -120
Cadmium 0.0500 0.04980 mg/L 100 80 -120
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373109/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373674 Prep Batch: 373109
Chromium 0.200 0.2070 mg/L 104 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Copper 0.250 0.2500 mg/L 100 80 -120
Lead 0.0500 0.05340 mg/L 107 80 -120
Nickel 0.500 0.5176 mg/L 104 80 -120
Selenium 0.0500 0.04750 mg/L 95 80 -120
Silver 0.0500 0.05160 mg/L 103 80 -120
Client Sample ID: MW-01CDLab Sample ID: 490-112432-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373674 Prep Batch: 373109
Arsenic <0.00860 0.0500 0.04870 mg/L 97 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0932 2.00 2.038 mg/L 97 75 -125
Cadmium <0.000500 0.0500 0.04890 mg/L 98 75 -125
Chromium <0.00300 0.200 0.2038 mg/L 102 75 -125
Copper 0.00560 J 0.250 0.2527 mg/L 99 75 -125
Lead 0.00600 0.0500 0.05690 mg/L 102 75 -125
Nickel <0.00300 0.500 0.5043 mg/L 101 75 -125
Selenium <0.00500 0.0500 0.04780 mg/L 96 75 -125
Silver <0.00300 0.0500 0.05060 mg/L 101 75 -125
Client Sample ID: MW-01CDLab Sample ID: 490-112432-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373674 Prep Batch: 373109
Arsenic <0.00860 0.0500 0.04970 mg/L 99 75 -125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0932 2.00 2.059 mg/L 98 75 -125 1 20
Cadmium <0.000500 0.0500 0.04930 mg/L 99 75 -125 1 20
Chromium <0.00300 0.200 0.2069 mg/L 103 75 -125 2 20
Copper 0.00560 J 0.250 0.2561 mg/L 100 75 -125 1 20
Lead 0.00600 0.0500 0.05810 mg/L 104 75 -125 2 20
Nickel <0.00300 0.500 0.5079 mg/L 102 75 -125 1 20
Selenium <0.00500 0.0500 0.04790 mg/L 96 75 -125 0 20
Silver <0.00300 0.0500 0.05060 mg/L 101 75 -125 0 20
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-373112/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374458 Prep Batch: 373112
RL MDL
Antimony <0.800 2.00 0.800 ug/L 09/26/16 10:20 09/30/16 01:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.100 0.1002.00 ug/L 09/26/16 10:20 09/30/16 01:58 1Beryllium
<0.100 0.1002.00 ug/L 09/26/16 10:20 09/30/16 01:58 1Cobalt
<0.800 0.8002.00 ug/L 09/26/16 10:20 09/30/16 01:58 1Thallium
1.059 J 0.7002.00 ug/L 09/26/16 10:20 09/30/16 01:58 1Vanadium
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-373112/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374458 Prep Batch: 373112
RL MDL
Zinc <5.20 25.0 5.20 ug/L 09/26/16 10:20 09/30/16 01:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373112/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374458 Prep Batch: 373112
Antimony 100 94.42 ug/L 94 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 93.45 ug/L 93 80 -120
Cobalt 100 92.29 ug/L 92 80 -120
Thallium 100 96.94 ug/L 97 80 -120
Vanadium 100 97.72 ug/L 98 80 -120
Zinc 100 89.16 ug/L 89 80 -120
Client Sample ID: MW-02CDLab Sample ID: 490-112432-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374458 Prep Batch: 373112
Antimony <0.800 100 78.87 ug/L 79 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium 0.963 J 100 90.64 ug/L 90 75 -125
Thallium <0.800 100 94.40 ug/L 94 75 -125
Vanadium 18.3 B 100 106.6 ug/L 88 75 -125
Zinc 28.3 100 110.0 ug/L 82 75 -125
Client Sample ID: MW-02CDLab Sample ID: 490-112432-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374768 Prep Batch: 373112
Cobalt 3.91 J 100 93.00 ug/L 89 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-02CDLab Sample ID: 490-112432-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374458 Prep Batch: 373112
Antimony <0.800 100 80.00 ug/L 80 75 -125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium 0.963 J 100 92.36 ug/L 91 75 -125 2 20
Thallium <0.800 100 96.11 ug/L 96 75 -125 2 20
Vanadium 18.3 B 100 107.9 ug/L 90 75 -125 1 20
Zinc 28.3 100 114.3 ug/L 86 75 -125 4 20
Client Sample ID: MW-02CDLab Sample ID: 490-112432-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374768 Prep Batch: 373112
Cobalt 3.91 J 100 94.95 ug/L 91 75 -125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-373162/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373506 Prep Batch: 373162
RL MDL
Mercury <0.100 0.200 0.100 ug/L 09/26/16 11:47 09/27/16 10:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-373162/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373506 Prep Batch: 373162
Mercury 1.00 1.006 ug/L 101 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-112291-G-1-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373506 Prep Batch: 373162
Mercury <0.100 1.00 1.015 ug/L 102 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-112291-G-1-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 373506 Prep Batch: 373162
Mercury <0.100 1.00 0.9900 ug/L 99 75 -125 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
GC/MS VOA
Analysis Batch: 373413
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-112432-1 MW-01CD Total/NA
Water 8260B490-112432-2 MW-02CD Total/NA
Water 8260B490-112432-3 MW-04CD Total/NA
Water 8260B490-112432-4 MW-2R Total/NA
Water 8260B490-112432-5 MW-2RDUP Total/NA
Water 8260B490-112432-6 MW-3R Total/NA
Water 8260B490-112432-7 MW-4 Total/NA
Water 8260B490-112432-8 SP-1 Total/NA
Water 8260B490-112432-11 Trip Blank Total/NA
Water 8260BMB 490-373413/7 Method Blank Total/NA
Water 8260BLCS 490-373413/4 Lab Control Sample Total/NA
Analysis Batch: 373601
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-112432-9 SS-1 Total/NA
Water 8260B490-112432-10 SS-2 Total/NA
Water 8260BMB 490-373601/7 Method Blank Total/NA
Water 8260BLCS 490-373601/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-373601/4 Lab Control Sample Dup Total/NA
Water 8260B490-112404-D-10 MS Matrix Spike Total/NA
Water 8260B490-112404-E-10 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 374875
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260BLCS 490-374875/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-374875/4 Lab Control Sample Dup Total/NA
Water 8260B490-112432-6 MS MW-3R Total/NA
Water 8260B490-112432-6 MSD MW-3R Total/NA
Metals
Prep Batch: 373109
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-112432-1 MW-01CD Total/NA
Water 3010A490-112432-2 MW-02CD Total/NA
Water 3010A490-112432-3 MW-04CD Total/NA
Water 3010A490-112432-4 MW-2R Total/NA
Water 3010A490-112432-5 MW-2RDUP Total/NA
Water 3010A490-112432-6 MW-3R Total/NA
Water 3010A490-112432-7 MW-4 Total/NA
Water 3010A490-112432-8 SP-1 Total/NA
Water 3010A490-112432-9 SS-1 Total/NA
Water 3010A490-112432-10 SS-2 Total/NA
Water 3010AMB 490-373109/1-A Method Blank Total/NA
Water 3010ALCS 490-373109/2-A Lab Control Sample Total/NA
Water 3010A490-112432-1 MS MW-01CD Total/NA
Water 3010A490-112432-1 MSD MW-01CD Total/NA
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QC Association Summary
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 373112
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-112432-1 MW-01CD Total/NA
Water 3010A490-112432-2 MW-02CD Total/NA
Water 3010A490-112432-3 MW-04CD Total/NA
Water 3010A490-112432-4 MW-2R Total/NA
Water 3010A490-112432-5 MW-2RDUP Total/NA
Water 3010A490-112432-6 MW-3R Total/NA
Water 3010A490-112432-7 MW-4 Total/NA
Water 3010A490-112432-8 SP-1 Total/NA
Water 3010A490-112432-9 SS-1 Total/NA
Water 3010A490-112432-10 SS-2 Total/NA
Water 3010AMB 490-373112/1-A Method Blank Total/NA
Water 3010ALCS 490-373112/2-A Lab Control Sample Total/NA
Water 3010A490-112432-2 MS MW-02CD Total/NA
Water 3010A490-112432-2 MSD MW-02CD Total/NA
Prep Batch: 373162
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-112432-1 MW-01CD Total/NA
Water 7470A490-112432-2 MW-02CD Total/NA
Water 7470A490-112432-3 MW-04CD Total/NA
Water 7470A490-112432-4 MW-2R Total/NA
Water 7470A490-112432-5 MW-2RDUP Total/NA
Water 7470A490-112432-6 MW-3R Total/NA
Water 7470A490-112432-7 MW-4 Total/NA
Water 7470A490-112432-8 SP-1 Total/NA
Water 7470A490-112432-9 SS-1 Total/NA
Water 7470A490-112432-10 SS-2 Total/NA
Water 7470AMB 490-373162/1-A Method Blank Total/NA
Water 7470ALCS 490-373162/2-A Lab Control Sample Total/NA
Water 7470A490-112291-G-1-C MS Matrix Spike Total/NA
Water 7470A490-112291-G-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 373506
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 373162490-112432-1 MW-01CD Total/NA
Water 7470A 373162490-112432-2 MW-02CD Total/NA
Water 7470A 373162490-112432-3 MW-04CD Total/NA
Water 7470A 373162490-112432-4 MW-2R Total/NA
Water 7470A 373162490-112432-5 MW-2RDUP Total/NA
Water 7470A 373162490-112432-6 MW-3R Total/NA
Water 7470A 373162490-112432-7 MW-4 Total/NA
Water 7470A 373162490-112432-8 SP-1 Total/NA
Water 7470A 373162490-112432-9 SS-1 Total/NA
Water 7470A 373162490-112432-10 SS-2 Total/NA
Water 7470A 373162MB 490-373162/1-A Method Blank Total/NA
Water 7470A 373162LCS 490-373162/2-A Lab Control Sample Total/NA
Water 7470A 373162490-112291-G-1-C MS Matrix Spike Total/NA
Water 7470A 373162490-112291-G-1-D MSD Matrix Spike Duplicate Total/NA
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QC Association Summary
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Analysis Batch: 373674
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 373109490-112432-1 MW-01CD Total/NA
Water 6010D 373109490-112432-2 MW-02CD Total/NA
Water 6010D 373109490-112432-3 MW-04CD Total/NA
Water 6010D 373109490-112432-4 MW-2R Total/NA
Water 6010D 373109490-112432-5 MW-2RDUP Total/NA
Water 6010D 373109490-112432-6 MW-3R Total/NA
Water 6010D 373109490-112432-7 MW-4 Total/NA
Water 6010D 373109490-112432-8 SP-1 Total/NA
Water 6010D 373109490-112432-9 SS-1 Total/NA
Water 6010D 373109490-112432-10 SS-2 Total/NA
Water 6010D 373109MB 490-373109/1-A Method Blank Total/NA
Water 6010D 373109LCS 490-373109/2-A Lab Control Sample Total/NA
Water 6010D 373109490-112432-1 MS MW-01CD Total/NA
Water 6010D 373109490-112432-1 MSD MW-01CD Total/NA
Analysis Batch: 374458
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 373112490-112432-1 MW-01CD Total/NA
Water 6020B 373112490-112432-2 MW-02CD Total/NA
Water 6020B 373112490-112432-3 MW-04CD Total/NA
Water 6020B 373112490-112432-4 MW-2R Total/NA
Water 6020B 373112490-112432-5 MW-2RDUP Total/NA
Water 6020B 373112490-112432-6 MW-3R Total/NA
Water 6020B 373112490-112432-7 MW-4 Total/NA
Water 6020B 373112490-112432-8 SP-1 Total/NA
Water 6020B 373112490-112432-9 SS-1 Total/NA
Water 6020B 373112490-112432-10 SS-2 Total/NA
Water 6020B 373112MB 490-373112/1-A Method Blank Total/NA
Water 6020B 373112LCS 490-373112/2-A Lab Control Sample Total/NA
Water 6020B 373112490-112432-2 MS MW-02CD Total/NA
Water 6020B 373112490-112432-2 MSD MW-02CD Total/NA
Analysis Batch: 374768
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 373112490-112432-2 MW-02CD Total/NA
Water 6020B 373112490-112432-3 MW-04CD Total/NA
Water 6020B 373112490-112432-2 MS MW-02CD Total/NA
Water 6020B 373112490-112432-2 MSD MW-02CD Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-112432-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-01CD Lab Sample ID: 490-112432-1
Matrix: WaterDate Collected: 09/21/16 12:45
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 15:091 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 13:43 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 02:36 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 10:48 LCS TAL NSHTotal/NA
Client Sample ID: MW-02CD Lab Sample ID: 490-112432-2
Matrix: WaterDate Collected: 09/21/16 11:15
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 16:391 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:08 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 02:09 KKK TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 5 374768 09/30/16 15:15 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 10:58 LCS TAL NSHTotal/NA
Client Sample ID: MW-04CD Lab Sample ID: 490-112432-3
Matrix: WaterDate Collected: 09/21/16 10:20
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 17:081 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 10 373674 09/27/16 14:24 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 10 374458 09/30/16 02:41 KKK TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374768 09/30/16 15:31 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:01 LCS TAL NSHTotal/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-112432-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-2R Lab Sample ID: 490-112432-4
Matrix: WaterDate Collected: 09/22/16 10:34
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 17:381 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:29 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 02:47 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:04 LCS TAL NSHTotal/NA
Client Sample ID: MW-2RDUP Lab Sample ID: 490-112432-5
Matrix: WaterDate Collected: 09/22/16 10:34
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 18:081 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:34 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 03:03 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:07 LCS TAL NSHTotal/NA
Client Sample ID: MW-3R Lab Sample ID: 490-112432-6
Matrix: WaterDate Collected: 09/22/16 14:30
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 18:381 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:39 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 03:09 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:10 LCS TAL NSHTotal/NA
Client Sample ID: MW-4 Lab Sample ID: 490-112432-7
Matrix: WaterDate Collected: 09/22/16 14:03
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 19:081 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:44 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-112432-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-4 Lab Sample ID: 490-112432-7
Matrix: WaterDate Collected: 09/22/16 14:03
Date Received: 09/23/16 09:25
Analysis 6020B KKK09/30/16 03:141 TAL NSH374458
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:14 LCS TAL NSHTotal/NA
Client Sample ID: SP-1 Lab Sample ID: 490-112432-8
Matrix: WaterDate Collected: 09/22/16 11:30
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 19:381 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:49 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 03:20 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:17 LCS TAL NSHTotal/NA
Client Sample ID: SS-1 Lab Sample ID: 490-112432-9
Matrix: WaterDate Collected: 09/22/16 10:55
Date Received: 09/23/16 09:25
Analysis 8260B NC09/28/16 04:341 TAL NSH373601
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 14:55 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 03:25 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:20 LCS TAL NSHTotal/NA
Client Sample ID: SS-2 Lab Sample ID: 490-112432-10
Matrix: WaterDate Collected: 09/22/16 11:05
Date Received: 09/23/16 09:25
Analysis 8260B NC09/28/16 04:041 TAL NSH373601
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 373109 09/26/16 10:16 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 373674 09/27/16 15:00 RDF TAL NSHTotal/NA
Prep 3010A 373112 09/26/16 10:20 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 374458 09/30/16 03:31 KKK TAL NSHTotal/NA
Prep 7470A 373162 09/26/16 11:47 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 373506 09/27/16 11:23 LCS TAL NSHTotal/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-112432-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: Trip Blank Lab Sample ID: 490-112432-11
Matrix: WaterDate Collected: 09/22/16 00:01
Date Received: 09/23/16 09:25
Analysis 8260B JRV09/27/16 14:391 TAL NSH373413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-112432-1Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-112432-1
Project/Site: Polk County Route 9 Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16 *
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-112432-1
Login Number: 112432
Question Answer Comment
Creator: Ngo, Phiet
List Source: TestAmerica Nashville
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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Appendix C
Environmental Monitoring Reporting Form
and Electronic Submittal of Environmental
Monitoring Data 7502Sept2016 (Electronic
Format Only)