8106_Duke_Rogers_IncidentSamplingResults_DIN27259_20160117

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J17010028
Project Name:CLIFFSIDE -
Lab Contact:Peggy Kendall
Date:1/5/2017
Customer Address:573 Duke Power Rd
Customer Name(s):Zach Hall
Mail Code: Clliffside Steam Station
Mooresboro, NC 28024
Phone:
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Peggy Kendall
Page 1 of 8
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2017000120 CLIFFSIDE 02-Jan-17 8:20 AM Brian Kemp Landfill Drainage-42"
2017000121 CLIFFSIDE 03-Jan-17 8:55 AM Brian Kemp SW016-42"
2017000122 CLIFFSIDE 03-Jan-17 10:21 AM Brian Kemp Cliffside 003
2017000123 CLIFFSIDE 03-Jan-17 11:37 AM Brian Kemp Cliffside Contact Pond Landfill
4 Total Samples
Page 2 of 8
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:1/4/2017
Electronic Data Deliverable (EDD) Sent Separately
Page 3 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010028
2017000120
Collection Date:02-Jan-17 8:20 AM
Site:Landfill Drainage-42"
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Boron (B)0.152 mg/L EPA 200.7 01/04/2017 11:02 MHH71310.05 1
Zinc (Zn)0.019 mg/L EPA 200.7 01/04/2017 11:02 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Arsenic (As)9.25 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Chromium (Cr)7.33 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Copper (Cu)4.84 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Lead (Pb)2.11 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Nickel (Ni)4.72 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Selenium (Se)5.96 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 01/04/2017 11:08 CWSPEN30.2 1
TOTAL SUSPENDED SOLIDS
TSS 64 mg/L SM2540D 01/04/2017 09:30 MGIGANT8.2 1
Page 4 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010028
2017000121
Collection Date:03-Jan-17 8:55 AM
Site:SW016-42"
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Boron (B)1.92 mg/L EPA 200.7 01/04/2017 11:14 MHH71310.05 1
Zinc (Zn)0.014 mg/L EPA 200.7 01/04/2017 11:14 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)1.52 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Arsenic (As)9.33 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Chromium (Cr)14.9 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Copper (Cu)4.32 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Lead (Pb)2.80 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Nickel (Ni)4.64 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Selenium (Se)38.5 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN311
Thallium (Tl) Low Level 0.310 ug/L EPA 200.8 01/04/2017 11:01 CWSPEN30.2 1
TOTAL SUSPENDED SOLIDS
TSS 47 mg/L SM2540D 01/04/2017 09:30 MGIGANT51
Page 5 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010028
2017000122
Collection Date:03-Jan-17 10:21 AM
Site:Cliffside 003
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Boron (B)0.566 mg/L EPA 200.7 01/04/2017 11:18 MHH71310.05 1
Zinc (Zn)0.023 mg/L EPA 200.7 01/04/2017 11:18 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)1.02 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Arsenic (As)15.8 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Chromium (Cr)14.1 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Copper (Cu)9.35 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Lead (Pb)4.64 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Nickel (Ni)8.81 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Selenium (Se)13.6 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN311
Thallium (Tl) Low Level 0.492 ug/L EPA 200.8 01/04/2017 11:16 CWSPEN30.2 1
TOTAL SUSPENDED SOLIDS
TSS 110 mg/L SM2540D 01/04/2017 09:30 MGIGANT131
Page 6 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010028
2017000123
Collection Date:03-Jan-17 11:37 AM
Site:Cliffside Contact Pond Landfill
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Boron (B)4.79 mg/L EPA 200.7 01/04/2017 11:22 MHH71310.05 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 01/04/2017 11:22 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)3.37 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Arsenic (As)10.7 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Chromium (Cr)19.7 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Copper (Cu)1.76 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Lead (Pb)1.04 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Nickel (Ni)1.27 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Selenium (Se)92.5 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN311
Thallium (Tl) Low Level 0.464 ug/L EPA 200.8 01/04/2017 11:24 CWSPEN30.2 1
TOTAL SUSPENDED SOLIDS
TSS 22 mg/L SM2540D 01/04/2017 09:30 MGIGANT51
Page 7 of 8
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13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J17010099
Project Name:Cliffside Landfill Stormwater
Lab Contact:Peggy Kendall
Date:1/13/2017
Customer Address:573 Duke Power Rd
Customer Name(s):Steve Hodges, Zach Hall
Mail Code: Clliffside Steam Station
Mooresboro, NC 28024
Phone:
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Peggy Kendall
Page 1 of 10
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2017000418 CLIFFSIDE 03-Jan-17 10:10 AM Brian Kemp Discharge Inlet Structure
2017000419 CLIFFSIDE 03-Jan-17 10:14 AM Brian Kemp Cliffside 001
2017000420 CLIFFSIDE 03-Jan-17 10:17 AM Brian Kemp Cliffside 002
2017000421 CLIFFSIDE 03-Jan-17 10:24 AM Brian Kemp Cliffside 004
2017000422 CLIFFSIDE 03-Jan-17 11:30 AM Brian Kemp Cliffside 005
2017000423 CLIFFSIDE 03-Jan-17 11:42 AM Brian Kemp Cliffside Non Contact 001
6 Total Samples
Page 2 of 10
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:1/13/2017
Electronic Data Deliverable (EDD) Sent Separately
Page 3 of 10
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010099
2017000418
Collection Date:03-Jan-17 10:10 AM
Site:Discharge Inlet Structure
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride 5.4 mg/L EPA 300.0 01/10/2017 16:43 BGN90340.1 1
Fluoride 0.17 mg/L EPA 300.0 01/10/2017 16:43 BGN90340.1 1
Nitrate 1.3 mg/L EPA 300.0 01/10/2017 16:43H2 BGN90340.1 1
Nitrate as N 0.29 mg-N/L EPA 300.0 01/10/2017 16:43 BGN90340.023 1
Sulfate 110 mg/L EPA 300.0 01/10/2017 16:43 BGN9034220
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 01/12/2017 12:39 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.044 mg/L EPA 200.7 01/12/2017 11:30 JJMACKE0.005 1
Boron (B)0.161 mg/L EPA 200.7 01/12/2017 11:30 JJMACKE0.05 1
Iron (Fe)6.26 mg/L EPA 200.7 01/12/2017 11:30 JJMACKE0.01 1
Manganese (Mn)0.064 mg/L EPA 200.7 01/12/2017 11:30 JJMACKE0.005 1
Zinc (Zn)0.016 mg/L EPA 200.7 01/12/2017 11:30 JJMACKE0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Arsenic (As)6.02 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Chromium (Cr)9.34 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Copper (Cu)4.71 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Lead (Pb)3.48 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Nickel (Ni)4.04 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Selenium (Se)3.30 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 01/12/2017 03:13 CWSPEN30.2 1
TOTAL DISSOLVED SOLIDS
TDS 270 mg/L SM2540C 01/10/2017 15:00 MGIGANT251
TOTAL SUSPENDED SOLIDS
TSS 61 mg/L SM2540D 01/06/2017 11:00 MGIGANT7.8 1
Page 4 of 10
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010099
2017000419
Collection Date:03-Jan-17 10:14 AM
Site:Cliffside 001
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride 5.0 mg/L EPA 300.0 01/10/2017 17:00 BGN90340.1 1
Fluoride 0.18 mg/L EPA 300.0 01/10/2017 17:00 BGN90340.1 1
Nitrate 1.5 mg/L EPA 300.0 01/10/2017 17:00H2 BGN90340.1 1
Nitrate as N 0.35 mg-N/L EPA 300.0 01/10/2017 17:00 BGN90340.023 1
Sulfate 120 mg/L EPA 300.0 01/10/2017 17:00 BGN9034220
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 01/12/2017 12:41 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.053 mg/L EPA 200.7 01/12/2017 11:34 JJMACKE0.005 1
Boron (B)0.183 mg/L EPA 200.7 01/12/2017 11:34 JJMACKE0.05 1
Iron (Fe)6.52 mg/L EPA 200.7 01/12/2017 11:34 JJMACKE0.01 1
Manganese (Mn)0.075 mg/L EPA 200.7 01/12/2017 11:34 JJMACKE0.005 1
Zinc (Zn)0.018 mg/L EPA 200.7 01/12/2017 11:34 JJMACKE0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Arsenic (As)10.1 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Chromium (Cr)10.2 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Copper (Cu)6.98 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Lead (Pb)3.21 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Nickel (Ni)5.96 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Selenium (Se)3.71 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 01/12/2017 03:21 CWSPEN30.2 1
TOTAL DISSOLVED SOLIDS
TDS 290 mg/L SM2540C 01/10/2017 15:00 MGIGANT251
TOTAL SUSPENDED SOLIDS
TSS 72 mg/L SM2540D 01/06/2017 11:00 MGIGANT8.9 1
Page 5 of 10
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010099
2017000420
Collection Date:03-Jan-17 10:17 AM
Site:Cliffside 002
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride 4.0 mg/L EPA 300.0 01/10/2017 17:18 BGN90340.1 1
Fluoride 0.17 mg/L EPA 300.0 01/10/2017 17:18 BGN90340.1 1
Nitrate 0.94 mg/L EPA 300.0 01/10/2017 17:18H2 BGN90340.1 1
Nitrate as N 0.21 mg-N/L EPA 300.0 01/10/2017 17:18 BGN90340.023 1
Sulfate 100 mg/L EPA 300.0 01/10/2017 17:18 BGN9034220
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 01/12/2017 12:44 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.059 mg/L EPA 200.7 01/12/2017 11:38 JJMACKE0.005 1
Boron (B)0.186 mg/L EPA 200.7 01/12/2017 11:38 JJMACKE0.05 1
Iron (Fe)8.06 mg/L EPA 200.7 01/12/2017 11:38 JJMACKE0.01 1
Manganese (Mn)0.093 mg/L EPA 200.7 01/12/2017 11:38 JJMACKE0.005 1
Zinc (Zn)0.024 mg/L EPA 200.7 01/12/2017 11:38 JJMACKE0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Arsenic (As)13.6 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Chromium (Cr)12.8 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Copper (Cu)9.21 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Lead (Pb)3.80 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Nickel (Ni)7.84 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Selenium (Se)3.85 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN311
Thallium (Tl) Low Level 0.255 ug/L EPA 200.8 01/12/2017 03:28 CWSPEN30.2 1
TOTAL DISSOLVED SOLIDS
TDS 250 mg/L SM2540C 01/10/2017 15:00 MGIGANT251
TOTAL SUSPENDED SOLIDS
TSS 91 mg/L SM2540D 01/06/2017 11:00 MGIGANT9.8 1
Page 6 of 10
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010099
2017000421
Collection Date:03-Jan-17 10:24 AM
Site:Cliffside 004
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride 4.2 mg/L EPA 300.0 01/10/2017 15:51 BGN90340.1 1
Fluoride 0.16 mg/L EPA 300.0 01/10/2017 15:51 BGN90340.1 1
Nitrate 2.0 mg/L EPA 300.0 01/10/2017 15:51H2 BGN90340.1 1
Nitrate as N 0.45 mg-N/L EPA 300.0 01/10/2017 15:51 BGN90340.023 1
Sulfate 88 mg/L EPA 300.0 01/10/2017 15:51 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 01/12/2017 12:46 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.042 mg/L EPA 200.7 01/12/2017 11:17 JJMACKE0.005 1
Boron (B)0.135 mg/L EPA 200.7 01/12/2017 11:17 JJMACKE0.05 1
Iron (Fe)6.46 mg/L EPA 200.7 01/12/2017 11:17 JJMACKE0.01 1
Manganese (Mn)0.063 mg/L EPA 200.7 01/12/2017 11:17 JJMACKE0.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 01/12/2017 11:17 JJMACKE0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Arsenic (As)5.82 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Chromium (Cr)9.47 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Copper (Cu)4.61 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Lead (Pb)3.70 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Nickel (Ni)3.77 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Selenium (Se)3.00 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 01/12/2017 03:36 CWSPEN30.2 1
TOTAL DISSOLVED SOLIDS
TDS 240 mg/L SM2540C 01/10/2017 15:00 MGIGANT251
TOTAL SUSPENDED SOLIDS
TSS 130 mg/L SM2540D 01/06/2017 11:00 MGIGANT161
Page 7 of 10
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010099
2017000422
Collection Date:03-Jan-17 11:30 AM
Site:Cliffside 005
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride 3.3 mg/L EPA 300.0 01/10/2017 16:08 BGN90340.1 1
Fluoride 0.15 mg/L EPA 300.0 01/10/2017 16:08 BGN90340.1 1
Nitrate 0.36 mg/L EPA 300.0 01/10/2017 16:08H2 BGN90340.1 1
Nitrate as N 0.08 mg-N/L EPA 300.0 01/10/2017 16:08 BGN90340.023 1
Sulfate 46 mg/L EPA 300.0 01/10/2017 16:08 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 01/12/2017 12:48 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.031 mg/L EPA 200.7 01/12/2017 11:42 JJMACKE0.005 1
Boron (B)0.093 mg/L EPA 200.7 01/12/2017 11:42 JJMACKE0.05 1
Iron (Fe)6.48 mg/L EPA 200.7 01/12/2017 11:42 JJMACKE0.01 1
Manganese (Mn)0.049 mg/L EPA 200.7 01/12/2017 11:42 JJMACKE0.005 1
Zinc (Zn)0.007 mg/L EPA 200.7 01/12/2017 11:42 JJMACKE0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Arsenic (As)3.76 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Chromium (Cr)9.12 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Copper (Cu)3.27 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Lead (Pb)3.78 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Nickel (Ni)2.79 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Selenium (Se)2.11 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 01/12/2017 02:42 CWSPEN30.2 1
TOTAL DISSOLVED SOLIDS
TDS 190 mg/L SM2540C 01/10/2017 15:00 MGIGANT251
TOTAL SUSPENDED SOLIDS
TSS 42 mg/L SM2540D 01/06/2017 11:00 MGIGANT5.8 1
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Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J17010099
2017000423
Collection Date:03-Jan-17 11:42 AM
Site:Cliffside Non Contact 001
Matrix:SURF_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride 2.3 mg/L EPA 300.0 01/10/2017 16:25 BGN90340.1 1
Fluoride 0.11 mg/L EPA 300.0 01/10/2017 16:25 BGN90340.1 1
Nitrate 0.24 mg/L EPA 300.0 01/10/2017 16:25H2 BGN90340.1 1
Nitrate as N 0.05 mg-N/L EPA 300.0 01/10/2017 16:25 BGN90340.023 1
Sulfate 35 mg/L EPA 300.0 01/10/2017 16:25 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 01/12/2017 12:51 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.037 mg/L EPA 200.7 01/12/2017 11:46 JJMACKE0.005 1
Boron (B)0.059 mg/L EPA 200.7 01/12/2017 11:46 JJMACKE0.05 1
Iron (Fe)7.60 mg/L EPA 200.7 01/12/2017 11:46 JJMACKE0.01 1
Manganese (Mn)0.065 mg/L EPA 200.7 01/12/2017 11:46 JJMACKE0.005 1
Zinc (Zn)0.009 mg/L EPA 200.7 01/12/2017 11:46 JJMACKE0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Arsenic (As)2.41 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Beryllium (Be)< 1 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Cadmium (Cd)< 1 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Chromium (Cr)8.93 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Copper (Cu)3.31 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Lead (Pb)4.08 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Nickel (Ni)2.78 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Selenium (Se)1.15 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Silver (Ag)< 1 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 01/12/2017 04:07 CWSPEN30.2 1
TOTAL DISSOLVED SOLIDS
TDS 160 mg/L SM2540C 01/10/2017 15:00 MGIGANT251
TOTAL SUSPENDED SOLIDS
TSS 69 mg/L SM2540D 01/06/2017 11:00 MGIGANT9.4 1
Qualifiers:
H2 Sample was received and analyzed past holding time.
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