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HomeMy WebLinkAbout19001_Caroline_Courtyard_2016_Annual_GW_Monitoring_Rpt_20170105 TABLES Table 1 Caroline Courtyard, North Generals Blvd, Lincolnton, North Carolina Summary of Historical EPA 8260 Ground Water Analyses Collected At Monitoring Well Locations Sample ID Depth (ft)Collected Date Matrix Units cis-1,2-Dichloroethene trans-1,2-Dichloroethene Tetrachloroethene Toluene Trichloroethene MW-11 21.58 12/20/2016 Water ug/L BDL BDL BDL BDL BDL MW-11 20.46 12/10/2015 Water ug/L BDL BDL BDL BDL BDL MW-11 21.09 09/03/2014 Water ug/L 1.2 BDL 2.6 BDL BDL MW-16 22.53 12/20/2016 Water ug/L BDL BDL 17.9 1.07 BDL MW-16 21.84 12/10/2015 Water ug/L BDL BDL 8.7 BDL BDL MW-16 22.89 09/03/2014 Water ug/L BDL BDL 7.8 BDL BDL MW-18 7.59 12/20/2016 Water ug/L 1.06 BDL 278 1.8 BDL MW-18 7.29 12/10/2015 Water ug/L BDL BDL 127 BDL BDL MW-18 7.63 09/03/2014 Water ug/L 1.4 BDL 261 BDL 1.1 MW-19 9.83 12/20/2016 Water ug/L 1.34 BDL 6.24 1.69 BDL MW-19 9.47 12/10/2015 Water ug/L BDL BDL 2.1 BDL BDL MW-19 9.95 09/03/2014 Water ug/L BDL BDL 22.4 BDL BDL MW-22D 7.15 12/20/2016 Water ug/L BDL BDL 93.8 BDL BDL MW-22D 6.34 12/10/2015 Water ug/L BDL BDL 161 BDL BDL MW-22D 7.12 09/03/2014 Water ug/L BDL BDL 130 BDL BDL MW-23 7.80 12/20/2016 Water ug/L BDL BDL 62.9 BDL BDL MW-23 7.66 12/10/2015 Water ug/L BDL BDL 25.3 BDL BDL MW-23 7.79 09/03/2014 Water ug/L BDL BDL 9 BDL BDL MW-25 8.31 12/20/2016 Water ug/L 357 3.24 1,010 BDL 147 MW-25 8.19 12/10/2015 Water ug/L 446 8 738 BDL 163 MW-25 8.29 09/03/2014 Water ug/L 977 BDL 1,720 BDL 407 NCDEQ NCAC 2L Ground Water Standards Water ug/L 70 100 0.7 600 3 Note 1: Volatile organic compound concentrations increased in 2016 from observed 2015 levels at monitoring well locations MW-16, MW-18, MW-19, MW-23 and MW-25. Note 2: Volatile organic compound concentrations decreased in 2016 from observed 2015 levels at monitoring well location MW-22D. Note 3: Yellow shaded values indicate compound concentrations above NCDEQ NCAC 2L Ground Water Standards. FIGURES BDL PCE: 17.9 ug/l PCE: 278 ug/l PCE: 6.24 ug/l PCE: 93.8 ug/l PCE: 62.9 ug/l PCE: 1,010 ug/l TCE: 147 ug/l cis-1,2-DCE: 357 ug/lDecember 20, 2016 EPA Method 8260 Ground Water Constituent Concentrations Only Concentrations Exceeding NCAC 2L Standards Are Displayed Refer to Table 1 For Complete Analytical Results Historical Ground Water Flow Direction APPENDICES ANALYTICAL REPORT December 29, 2016 Griffith Enterprise Sample Delivery Group:L880165 Samples Received:12/21/2016 Project Number: Description:Caroline Courtyard Report To:Mr. Alan Griffith 353 Jonestown Road, PMB 312 Winston-Salem, NC 27104 Entire Report Reviewed By: December 29, 2016 [Preliminary Report] Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com December 29, 2016 Jason Romer Technical Service Representative ONE LAB. NATIONWIDE.TABLE OF CONTENTS ¹Cp: Cover Page 1 ²Tc: Table of Contents 2 ³Ss: Sample Summary 3 ⁴Cn: Case Narrative 4 ⁵Sr: Sample Results 5 MW-11 L880165-01 5 MW-16 L880165-02 7 MW-18 L880165-03 9 MW-19 L880165-04 11 MW-22D L880165-05 13 MW-23 L880165-06 15 MW-25 L880165-07 17 ⁶Qc: Quality Control Summary 19 Volatile Organic Compounds (GC/MS) by Method 8260B 19 ⁷Gl: Glossary of Terms 23 ⁸Al: Accreditations & Locations 24 ⁹Sc: Chain of Custody 25 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 2 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 2 of 26 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-11 L880165-01 GW M. Alan Griffith 12/20/16 08:30 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 02:09 12/26/16 02:09 JAH Collected by Collected date/time Received date/time MW-16 L880165-02 GW M. Alan Griffith 12/20/16 09:00 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 02:30 12/26/16 02:30 JAH Collected by Collected date/time Received date/time MW-18 L880165-03 GW M. Alan Griffith 12/20/16 11:55 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 02:51 12/26/16 02:51 JAH Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 10 12/28/16 23:05 12/28/16 23:05 ACG Collected by Collected date/time Received date/time MW-19 L880165-04 GW M. Alan Griffith 12/20/16 11:00 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 03:11 12/26/16 03:11 JAH Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/28/16 23:18 12/28/16 23:18 ACG Collected by Collected date/time Received date/time MW-22D L880165-05 GW M. Alan Griffith 12/20/16 12:30 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 03:32 12/26/16 03:32 JAH Collected by Collected date/time Received date/time MW-23 L880165-06 GW M. Alan Griffith 12/20/16 11:25 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 03:53 12/26/16 03:53 JAH Collected by Collected date/time Received date/time MW-25 L880165-07 GW M. Alan Griffith 12/20/16 13:00 12/21/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 1 12/26/16 04:13 12/26/16 04:13 JAH Volatile Organic Compounds (GC/MS) by Method 8260B WG938396 25 12/28/16 23:30 12/28/16 23:30 ACG 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 3 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 3 of 26 ONE LAB. NATIONWIDE.CASE NARRATIVE All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Jimmy Hunt Technical Service Representative Sample Handling and Receiving The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container. ESC Sample ID Project Sample ID Method L880165-01 MW-11 8260B L880165-02 MW-16 8260B L880165-03 MW-18 8260B L880165-04 MW-19 8260B L880165-05 MW-22D 8260B L880165-06 MW-23 8260B L880165-07 MW-25 8260B 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 4 of 26 Jason Romer Technical Service Representative ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 4 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L880165 MW-11 Collected date/time: 12/20/16 08:30 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 02:09 WG938396 Acrolein ND 0.0500 1 12/26/2016 02:09 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 02:09 WG938396 Benzene ND 0.00100 1 12/26/2016 02:09 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 02:09 WG938396 Bromoform ND 0.00100 1 12/26/2016 02:09 WG938396 Bromomethane ND 0.00500 1 12/26/2016 02:09 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 02:09 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 02:09 WG938396 Chloroethane ND 0.00500 1 12/26/2016 02:09 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 02:09 WG938396 Chloroform ND 0.00500 1 12/26/2016 02:09 WG938396 Chloromethane ND 0.00250 1 12/26/2016 02:09 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 02:09 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 02:09 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 02:09 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 02:09 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 02:09 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 02:09 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 02:09 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 02:09 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 02:09 WG938396 cis-1,2-Dichloroethene ND 0.00100 1 12/26/2016 02:09 WG938396 trans-1,2-Dichloroethene ND 0.00100 1 12/26/2016 02:09 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 02:09 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 02:09 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 02:09 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 02:09 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 02:09 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 02:09 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 02:09 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 02:09 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 02:09 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 02:09 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 02:09 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 02:09 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 02:09 WG938396 Naphthalene ND 0.00500 1 12/26/2016 02:09 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Styrene ND 0.00100 1 12/26/2016 02:09 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 02:09 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 02:09 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 02:09 WG938396 Tetrachloroethene ND 0.00100 1 12/26/2016 02:09 WG938396 Toluene ND 0.00100 1 12/26/2016 02:09 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 5 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 5 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L880165 MW-11 Collected date/time: 12/20/16 08:30 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 02:09 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 02:09 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 02:09 WG938396 Trichloroethene ND 0.00100 1 12/26/2016 02:09 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 02:09 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 02:09 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 02:09 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 02:09 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 02:09 WG938396 (S) Toluene-d8 101 90.0-115 12/26/2016 02:09 WG938396 (S) Dibromofluoromethane 95.3 79.0-121 12/26/2016 02:09 WG938396 (S) 4-Bromofluorobenzene 111 80.1-120 12/26/2016 02:09 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 6 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 6 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L880165 MW-16 Collected date/time: 12/20/16 09:00 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 02:30 WG938396 Acrolein ND 0.0500 1 12/26/2016 02:30 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 02:30 WG938396 Benzene ND 0.00100 1 12/26/2016 02:30 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 02:30 WG938396 Bromoform ND 0.00100 1 12/26/2016 02:30 WG938396 Bromomethane ND 0.00500 1 12/26/2016 02:30 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 02:30 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 02:30 WG938396 Chloroethane ND 0.00500 1 12/26/2016 02:30 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 02:30 WG938396 Chloroform ND 0.00500 1 12/26/2016 02:30 WG938396 Chloromethane ND 0.00250 1 12/26/2016 02:30 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 02:30 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 02:30 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 02:30 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 02:30 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 02:30 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 02:30 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 02:30 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 02:30 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 02:30 WG938396 cis-1,2-Dichloroethene ND 0.00100 1 12/26/2016 02:30 WG938396 trans-1,2-Dichloroethene ND 0.00100 1 12/26/2016 02:30 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 02:30 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 02:30 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 02:30 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 02:30 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 02:30 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 02:30 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 02:30 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 02:30 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 02:30 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 02:30 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 02:30 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 02:30 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 02:30 WG938396 Naphthalene ND 0.00500 1 12/26/2016 02:30 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Styrene ND 0.00100 1 12/26/2016 02:30 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 02:30 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 02:30 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 02:30 WG938396 Tetrachloroethene 0.0179 0.00100 1 12/26/2016 02:30 WG938396 Toluene 0.00107 0.00100 1 12/26/2016 02:30 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 7 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 7 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L880165 MW-16 Collected date/time: 12/20/16 09:00 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 02:30 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 02:30 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 02:30 WG938396 Trichloroethene ND 0.00100 1 12/26/2016 02:30 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 02:30 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 02:30 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 02:30 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 02:30 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 02:30 WG938396 (S) Toluene-d8 104 90.0-115 12/26/2016 02:30 WG938396 (S) Dibromofluoromethane 93.0 79.0-121 12/26/2016 02:30 WG938396 (S) 4-Bromofluorobenzene 107 80.1-120 12/26/2016 02:30 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 8 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 8 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L880165 MW-18 Collected date/time: 12/20/16 11:55 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 02:51 WG938396 Acrolein ND 0.0500 1 12/26/2016 02:51 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 02:51 WG938396 Benzene ND 0.00100 1 12/26/2016 02:51 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 02:51 WG938396 Bromoform ND 0.00100 1 12/26/2016 02:51 WG938396 Bromomethane ND 0.00500 1 12/26/2016 02:51 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 02:51 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 02:51 WG938396 Chloroethane ND 0.00500 1 12/26/2016 02:51 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 02:51 WG938396 Chloroform ND 0.00500 1 12/26/2016 02:51 WG938396 Chloromethane ND 0.00250 1 12/26/2016 02:51 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 02:51 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 02:51 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 02:51 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 02:51 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 02:51 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 02:51 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 02:51 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 02:51 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 02:51 WG938396 cis-1,2-Dichloroethene 0.00106 0.00100 1 12/26/2016 02:51 WG938396 trans-1,2-Dichloroethene ND 0.00100 1 12/26/2016 02:51 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 02:51 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 02:51 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 02:51 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 02:51 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 02:51 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 02:51 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 02:51 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 02:51 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 02:51 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 02:51 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 02:51 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 02:51 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 02:51 WG938396 Naphthalene ND 0.00500 1 12/26/2016 02:51 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Styrene ND 0.00100 1 12/26/2016 02:51 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 02:51 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 02:51 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 02:51 WG938396 Tetrachloroethene 0.278 0.0100 10 12/28/2016 23:05 WG938396 Toluene 0.00180 0.00100 1 12/26/2016 02:51 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 9 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 9 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L880165 MW-18 Collected date/time: 12/20/16 11:55 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 02:51 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 02:51 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 02:51 WG938396 Trichloroethene ND 0.00100 1 12/26/2016 02:51 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 02:51 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 02:51 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 02:51 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 02:51 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 02:51 WG938396 (S) Toluene-d8 101 90.0-115 12/26/2016 02:51 WG938396 (S) Toluene-d8 99.7 90.0-115 12/28/2016 23:05 WG938396 (S) Dibromofluoromethane 89.1 79.0-121 12/28/2016 23:05 WG938396 (S) Dibromofluoromethane 95.0 79.0-121 12/26/2016 02:51 WG938396 (S) 4-Bromofluorobenzene 106 80.1-120 12/26/2016 02:51 WG938396 (S) 4-Bromofluorobenzene 96.6 80.1-120 12/28/2016 23:05 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 10 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 10 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L880165 MW-19 Collected date/time: 12/20/16 11:00 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 03:11 WG938396 Acrolein ND 0.0500 1 12/26/2016 03:11 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 03:11 WG938396 Benzene ND 0.00100 1 12/26/2016 03:11 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 03:11 WG938396 Bromoform ND 0.00100 1 12/26/2016 03:11 WG938396 Bromomethane ND 0.00500 1 12/26/2016 03:11 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 03:11 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 03:11 WG938396 Chloroethane ND 0.00500 1 12/26/2016 03:11 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 03:11 WG938396 Chloroform ND 0.00500 1 12/26/2016 03:11 WG938396 Chloromethane ND 0.00250 1 12/26/2016 03:11 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 03:11 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 03:11 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 03:11 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 03:11 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 03:11 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 03:11 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 03:11 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 03:11 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 03:11 WG938396 cis-1,2-Dichloroethene 0.00134 0.00100 1 12/26/2016 03:11 WG938396 trans-1,2-Dichloroethene ND 0.00100 1 12/26/2016 03:11 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 03:11 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 03:11 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 03:11 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 03:11 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 03:11 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 03:11 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 03:11 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 03:11 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 03:11 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 03:11 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 03:11 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 03:11 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 03:11 WG938396 Naphthalene ND 0.00500 1 12/26/2016 03:11 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Styrene ND 0.00100 1 12/26/2016 03:11 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 03:11 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 03:11 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 03:11 WG938396 Tetrachloroethene 0.00624 0.00100 1 12/28/2016 23:18 WG938396 Toluene 0.00169 0.00100 1 12/26/2016 03:11 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 11 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 11 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L880165 MW-19 Collected date/time: 12/20/16 11:00 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 03:11 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 03:11 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 03:11 WG938396 Trichloroethene ND 0.00100 1 12/26/2016 03:11 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 03:11 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 03:11 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 03:11 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 03:11 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 03:11 WG938396 (S) Toluene-d8 103 90.0-115 12/26/2016 03:11 WG938396 (S) Toluene-d8 100 90.0-115 12/28/2016 23:18 WG938396 (S) Dibromofluoromethane 92.4 79.0-121 12/28/2016 23:18 WG938396 (S) Dibromofluoromethane 95.1 79.0-121 12/26/2016 03:11 WG938396 (S) 4-Bromofluorobenzene 104 80.1-120 12/26/2016 03:11 WG938396 (S) 4-Bromofluorobenzene 99.2 80.1-120 12/28/2016 23:18 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 12 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 12 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L880165 MW-22D Collected date/time: 12/20/16 12:30 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 03:32 WG938396 Acrolein ND 0.0500 1 12/26/2016 03:32 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 03:32 WG938396 Benzene ND 0.00100 1 12/26/2016 03:32 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 03:32 WG938396 Bromoform ND 0.00100 1 12/26/2016 03:32 WG938396 Bromomethane ND 0.00500 1 12/26/2016 03:32 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 03:32 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 03:32 WG938396 Chloroethane ND 0.00500 1 12/26/2016 03:32 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 03:32 WG938396 Chloroform ND 0.00500 1 12/26/2016 03:32 WG938396 Chloromethane ND 0.00250 1 12/26/2016 03:32 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 03:32 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 03:32 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 03:32 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 03:32 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 03:32 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 03:32 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 03:32 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 03:32 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 03:32 WG938396 cis-1,2-Dichloroethene ND 0.00100 1 12/26/2016 03:32 WG938396 trans-1,2-Dichloroethene ND 0.00100 1 12/26/2016 03:32 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 03:32 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 03:32 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 03:32 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 03:32 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 03:32 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 03:32 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 03:32 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 03:32 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 03:32 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 03:32 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 03:32 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 03:32 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 03:32 WG938396 Naphthalene ND 0.00500 1 12/26/2016 03:32 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Styrene ND 0.00100 1 12/26/2016 03:32 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 03:32 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 03:32 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 03:32 WG938396 Tetrachloroethene 0.0938 0.00100 1 12/26/2016 03:32 WG938396 Toluene ND 0.00100 1 12/26/2016 03:32 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 13 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 13 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L880165 MW-22D Collected date/time: 12/20/16 12:30 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 03:32 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 03:32 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 03:32 WG938396 Trichloroethene ND 0.00100 1 12/26/2016 03:32 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 03:32 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 03:32 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 03:32 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 03:32 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 03:32 WG938396 (S) Toluene-d8 101 90.0-115 12/26/2016 03:32 WG938396 (S) Dibromofluoromethane 91.7 79.0-121 12/26/2016 03:32 WG938396 (S) 4-Bromofluorobenzene 104 80.1-120 12/26/2016 03:32 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 14 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 14 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L880165 MW-23 Collected date/time: 12/20/16 11:25 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 03:53 WG938396 Acrolein ND 0.0500 1 12/26/2016 03:53 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 03:53 WG938396 Benzene ND 0.00100 1 12/26/2016 03:53 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 03:53 WG938396 Bromoform ND 0.00100 1 12/26/2016 03:53 WG938396 Bromomethane ND 0.00500 1 12/26/2016 03:53 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 03:53 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 03:53 WG938396 Chloroethane ND 0.00500 1 12/26/2016 03:53 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 03:53 WG938396 Chloroform ND 0.00500 1 12/26/2016 03:53 WG938396 Chloromethane ND 0.00250 1 12/26/2016 03:53 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 03:53 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 03:53 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 03:53 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 03:53 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 03:53 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 03:53 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 03:53 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 03:53 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 03:53 WG938396 cis-1,2-Dichloroethene ND 0.00100 1 12/26/2016 03:53 WG938396 trans-1,2-Dichloroethene ND 0.00100 1 12/26/2016 03:53 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 03:53 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 03:53 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 03:53 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 03:53 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 03:53 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 03:53 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 03:53 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 03:53 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 03:53 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 03:53 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 03:53 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 03:53 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 03:53 WG938396 Naphthalene ND 0.00500 1 12/26/2016 03:53 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Styrene ND 0.00100 1 12/26/2016 03:53 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 03:53 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 03:53 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 03:53 WG938396 Tetrachloroethene 0.0629 0.00100 1 12/26/2016 03:53 WG938396 Toluene ND 0.00100 1 12/26/2016 03:53 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 15 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 15 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L880165 MW-23 Collected date/time: 12/20/16 11:25 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 03:53 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 03:53 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 03:53 WG938396 Trichloroethene ND 0.00100 1 12/26/2016 03:53 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 03:53 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 03:53 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 03:53 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 03:53 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 03:53 WG938396 (S) Toluene-d8 102 90.0-115 12/26/2016 03:53 WG938396 (S) Dibromofluoromethane 91.9 79.0-121 12/26/2016 03:53 WG938396 (S) 4-Bromofluorobenzene 106 80.1-120 12/26/2016 03:53 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 16 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 16 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L880165 MW-25 Collected date/time: 12/20/16 13:00 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time Acetone ND 0.0500 1 12/26/2016 04:13 WG938396 Acrolein ND 0.0500 1 12/26/2016 04:13 WG938396 Acrylonitrile ND 0.0100 1 12/26/2016 04:13 WG938396 Benzene ND 0.00100 1 12/26/2016 04:13 WG938396 Bromobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Bromodichloromethane ND 0.00100 1 12/26/2016 04:13 WG938396 Bromoform ND 0.00100 1 12/26/2016 04:13 WG938396 Bromomethane ND 0.00500 1 12/26/2016 04:13 WG938396 n-Butylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 sec-Butylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 tert-Butylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Carbon tetrachloride ND 0.00100 1 12/26/2016 04:13 WG938396 Chlorobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Chlorodibromomethane ND 0.00100 1 12/26/2016 04:13 WG938396 Chloroethane ND 0.00500 1 12/26/2016 04:13 WG938396 2-Chloroethyl vinyl ether ND 0.0500 1 12/26/2016 04:13 WG938396 Chloroform ND 0.00500 1 12/26/2016 04:13 WG938396 Chloromethane ND 0.00250 1 12/26/2016 04:13 WG938396 2-Chlorotoluene ND 0.00100 1 12/26/2016 04:13 WG938396 4-Chlorotoluene ND 0.00100 1 12/26/2016 04:13 WG938396 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/26/2016 04:13 WG938396 1,2-Dibromoethane ND 0.00100 1 12/26/2016 04:13 WG938396 Dibromomethane ND 0.00100 1 12/26/2016 04:13 WG938396 1,2-Dichlorobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 1,3-Dichlorobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 1,4-Dichlorobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Dichlorodifluoromethane ND 0.00500 1 12/26/2016 04:13 WG938396 1,1-Dichloroethane ND 0.00100 1 12/26/2016 04:13 WG938396 1,2-Dichloroethane ND 0.00100 1 12/26/2016 04:13 WG938396 1,1-Dichloroethene ND 0.00100 1 12/26/2016 04:13 WG938396 cis-1,2-Dichloroethene 0.357 0.0250 25 12/28/2016 23:30 WG938396 trans-1,2-Dichloroethene 0.00324 0.00100 1 12/26/2016 04:13 WG938396 1,2-Dichloropropane ND 0.00100 1 12/26/2016 04:13 WG938396 1,1-Dichloropropene ND 0.00100 1 12/26/2016 04:13 WG938396 1,3-Dichloropropane ND 0.00100 1 12/26/2016 04:13 WG938396 cis-1,3-Dichloropropene ND 0.00100 1 12/26/2016 04:13 WG938396 trans-1,3-Dichloropropene ND 0.00100 1 12/26/2016 04:13 WG938396 2,2-Dichloropropane ND 0.00100 1 12/26/2016 04:13 WG938396 Di-isopropyl ether ND 0.00100 1 12/26/2016 04:13 WG938396 Ethylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Hexachloro-1,3-butadiene ND 0.00100 1 12/26/2016 04:13 WG938396 Isopropylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 p-Isopropyltoluene ND 0.00100 1 12/26/2016 04:13 WG938396 2-Butanone (MEK)ND 0.0100 1 12/26/2016 04:13 WG938396 Methylene Chloride ND 0.00500 1 12/26/2016 04:13 WG938396 4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/26/2016 04:13 WG938396 Methyl tert-butyl ether ND 0.00100 1 12/26/2016 04:13 WG938396 Naphthalene ND 0.00500 1 12/26/2016 04:13 WG938396 n-Propylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Styrene ND 0.00100 1 12/26/2016 04:13 WG938396 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/26/2016 04:13 WG938396 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/26/2016 04:13 WG938396 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/26/2016 04:13 WG938396 Tetrachloroethene 1.01 0.0250 25 12/28/2016 23:30 WG938396 Toluene ND 0.00100 1 12/26/2016 04:13 WG938396 1,2,3-Trichlorobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 17 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 17 of 26 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L880165 MW-25 Collected date/time: 12/20/16 13:00 Volatile Organic Compounds (GC/MS) by Method 8260B 5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK $Qal\te mg/l mg/l date / time 1,2,4-Trichlorobenzene ND 0.00100 1 12/26/2016 04:13 WG938396 1,1,1-Trichloroethane ND 0.00100 1 12/26/2016 04:13 WG938396 1,1,2-Trichloroethane ND 0.00100 1 12/26/2016 04:13 WG938396 Trichloroethene 0.147 0.00100 1 12/26/2016 04:13 WG938396 Trichlorofluoromethane ND 0.00500 1 12/26/2016 04:13 WG938396 1,2,3-Trichloropropane ND 0.00250 1 12/26/2016 04:13 WG938396 1,2,4-Trimethylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 1,2,3-Trimethylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 1,3,5-Trimethylbenzene ND 0.00100 1 12/26/2016 04:13 WG938396 Vinyl chloride ND 0.00100 1 12/26/2016 04:13 WG938396 Xylenes, Total ND 0.00300 1 12/26/2016 04:13 WG938396 (S) Toluene-d8 98.4 90.0-115 12/26/2016 04:13 WG938396 (S) Toluene-d8 99.9 90.0-115 12/28/2016 23:30 WG938396 (S) Dibromofluoromethane 91.1 79.0-121 12/28/2016 23:30 WG938396 (S) Dibromofluoromethane 94.0 79.0-121 12/26/2016 04:13 WG938396 (S) 4-Bromofluorobenzene 105 80.1-120 12/26/2016 04:13 WG938396 (S) 4-Bromofluorobenzene 95.5 80.1-120 12/28/2016 23:30 WG938396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 18 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 18 of 26 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938396 Volatile Organic Compounds (GC/MS) by Method 8260B L880165-01,02,03,04,05,06,07 Method Blank (MB) (MB) R3187738-3 12/26/16 01:27 0% 5eVXlt 0% 4XaliIieU 0% 0'L 0% 5'L $Qal\te mg/l mg/l mg/l Acetone U 0.0100 0.0500 Acrolein U 0.00887 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromobenzene U 0.000352 0.00100 Bromodichloromethane U 0.000380 0.00100 Bromoform U 0.000469 0.00100 Bromomethane U 0.000866 0.00500 n-Butylbenzene U 0.000361 0.00100 sec-Butylbenzene U 0.000365 0.00100 tert-Butylbenzene U 0.000399 0.00100 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 2-Chloroethyl vinyl ether U 0.00301 0.0500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 2-Chlorotoluene U 0.000375 0.00100 4-Chlorotoluene U 0.000351 0.00100 1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 1,2-Dibromoethane U 0.000381 0.00100 Dibromomethane U 0.000346 0.00100 1,2-Dichlorobenzene U 0.000349 0.00100 1,3-Dichlorobenzene U 0.000220 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 Dichlorodifluoromethane U 0.000551 0.00500 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 cis-1,2-Dichloroethene U 0.000260 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 1,1-Dichloropropene U 0.000352 0.00100 1,3-Dichloropropane U 0.000366 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 2,2-Dichloropropane U 0.000321 0.00100 Di-isopropyl ether U 0.000320 0.00100 Ethylbenzene U 0.000384 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 19 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 19 of 26 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938396 Volatile Organic Compounds (GC/MS) by Method 8260B L880165-01,02,03,04,05,06,07 Method Blank (MB) (MB) R3187738-3 12/26/16 01:27 0% 5eVXlt 0% 4XaliIieU 0% 0'L 0% 5'L $Qal\te mg/l mg/l mg/l Hexachloro-1,3-butadiene U 0.000256 0.00100 Isopropylbenzene U 0.000326 0.00100 p-Isopropyltoluene U 0.000350 0.00100 2-Butanone (MEK)U 0.00393 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100 Methyl tert-butyl ether U 0.000367 0.00100 Naphthalene U 0.00100 0.00500 n-Propylbenzene U 0.000349 0.00100 Styrene U 0.000307 0.00100 1,1,1,2-Tetrachloroethane U 0.000385 0.00100 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000412 0.00100 1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 1,2,3-Trichlorobenzene U 0.000230 0.00100 1,2,4-Trichlorobenzene U 0.000355 0.00100 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 Trichlorofluoromethane U 0.00120 0.00500 1,2,3-Trichloropropane U 0.000807 0.00250 1,2,3-Trimethylbenzene U 0.000321 0.00100 1,2,4-Trimethylbenzene U 0.000373 0.00100 1,3,5-Trimethylbenzene U 0.000387 0.00100 Vinyl chloride U 0.000259 0.00100 Xylenes, Total U 0.00106 0.00300 (S) Toluene-d8 101 90.0-115 (S) Dibromofluoromethane 92.4 79.0-121 (S) 4-Bromofluorobenzene 105 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3187738-1 12/25/16 23:07 • (LCSD) R3187738-2 12/25/16 23:28 6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ecLC6' 5ec5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53'53' LimitV $Qal\te mg/l mg/l mg/l %%%%% Acetone 0.125 0.104 0.101 83.1 80.8 28.7-175 2.74 20.9 Acrolein 0.125 0.143 0.119 114 95.3 40.4-172 18.2 20 Acrylonitrile 0.125 0.103 0.0996 82.0 79.7 58.2-145 2.86 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 20 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 20 of 26 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938396 Volatile Organic Compounds (GC/MS) by Method 8260B L880165-01,02,03,04,05,06,07 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3187738-1 12/25/16 23:07 • (LCSD) R3187738-2 12/25/16 23:28 6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ecLC6' 5ec5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53'53' LimitV $Qal\te mg/l mg/l mg/l %%%%% Benzene 0.0250 0.0220 0.0219 87.8 87.8 73.0-122 0.0300 20 Bromobenzene 0.0250 0.0249 0.0257 99.8 103 81.5-115 2.84 20 Bromodichloromethane 0.0250 0.0233 0.0238 93.4 95.4 75.5-121 2.08 20 Bromoform 0.0250 0.0266 0.0262 106 105 71.5-131 1.50 20 Bromomethane 0.0250 0.0238 0.0219 95.1 87.7 22.4-187 8.01 20 n-Butylbenzene 0.0250 0.0231 0.0241 92.3 96.5 75.9-134 4.43 20 sec-Butylbenzene 0.0250 0.0278 0.0274 111 110 80.6-126 1.48 20 tert-Butylbenzene 0.0250 0.0284 0.0279 114 111 79.3-127 1.89 20 Carbon tetrachloride 0.0250 0.0210 0.0215 83.9 85.9 70.9-129 2.35 20 Chlorobenzene 0.0250 0.0274 0.0279 110 112 79.7-122 1.91 20 Chlorodibromomethane 0.0250 0.0266 0.0267 106 107 78.2-124 0.550 20 Chloroethane 0.0250 0.0204 0.0196 81.6 78.3 41.2-153 4.15 20 2-Chloroethyl vinyl ether 0.125 0.124 0.135 99.5 108 23.4-162 8.30 23.5 Chloroform 0.0250 0.0224 0.0222 89.6 88.7 73.2-125 0.980 20 Chloromethane 0.0250 0.0196 0.0194 78.6 77.6 55.8-134 1.31 20 2-Chlorotoluene 0.0250 0.0262 0.0264 105 106 76.4-125 0.810 20 4-Chlorotoluene 0.0250 0.0265 0.0266 106 106 81.5-121 0.310 20 1,2-Dibromo-3-Chloropropane 0.0250 0.0215 0.0221 86.1 88.3 64.8-131 2.56 20 1,2-Dibromoethane 0.0250 0.0271 0.0279 108 112 79.8-122 2.94 20 Dibromomethane 0.0250 0.0245 0.0259 98.1 104 79.5-118 5.52 20 1,2-Dichlorobenzene 0.0250 0.0245 0.0263 97.8 105 84.7-118 7.18 20 1,3-Dichlorobenzene 0.0250 0.0288 0.0291 115 116 77.6-127 1.21 20 1,4-Dichlorobenzene 0.0250 0.0237 0.0256 94.8 102 82.2-114 7.71 20 Dichlorodifluoromethane 0.0250 0.0230 0.0233 92.0 93.1 56.0-134 1.11 20 1,1-Dichloroethane 0.0250 0.0211 0.0212 84.5 84.7 71.7-127 0.210 20 1,2-Dichloroethane 0.0250 0.0201 0.0207 80.2 82.6 65.3-126 2.95 20 1,1-Dichloroethene 0.0250 0.0216 0.0214 86.3 85.7 59.9-137 0.720 20 cis-1,2-Dichloroethene 0.0250 0.0231 0.0234 92.3 93.7 77.3-122 1.53 20 trans-1,2-Dichloroethene 0.0250 0.0231 0.0232 92.5 92.9 72.6-125 0.450 20 1,2-Dichloropropane 0.0250 0.0227 0.0237 91.0 94.7 77.4-125 4.03 20 1,1-Dichloropropene 0.0250 0.0226 0.0225 90.4 89.9 72.5-127 0.610 20 1,3-Dichloropropane 0.0250 0.0245 0.0258 97.8 103 80.6-115 5.19 20 cis-1,3-Dichloropropene 0.0250 0.0229 0.0239 91.5 95.7 77.7-124 4.51 20 trans-1,3-Dichloropropene 0.0250 0.0237 0.0243 94.9 97.1 73.5-127 2.23 20 2,2-Dichloropropane 0.0250 0.0203 0.0208 81.2 83.0 61.3-134 2.15 20 Di-isopropyl ether 0.0250 0.0195 0.0197 78.1 78.7 65.1-135 0.810 20 Ethylbenzene 0.0250 0.0271 0.0273 108 109 80.9-121 0.820 20 Hexachloro-1,3-butadiene 0.0250 0.0251 0.0254 100 102 73.7-133 1.11 20 Isopropylbenzene 0.0250 0.0275 0.0274 110 109 81.6-124 0.430 20 p-Isopropyltoluene 0.0250 0.0284 0.0280 113 112 77.6-129 1.38 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 21 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 21 of 26 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938396 Volatile Organic Compounds (GC/MS) by Method 8260B L880165-01,02,03,04,05,06,07 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3187738-1 12/25/16 23:07 • (LCSD) R3187738-2 12/25/16 23:28 6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ecLC6' 5ec5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53'53' LimitV $Qal\te mg/l mg/l mg/l %%%%% 2-Butanone (MEK)0.125 0.0859 0.0887 68.7 71.0 46.4-155 3.25 20 Methylene Chloride 0.0250 0.0218 0.0216 87.2 86.4 69.5-120 0.930 20 4-Methyl-2-pentanone (MIBK)0.125 0.0991 0.105 79.2 83.8 63.3-138 5.62 20 Methyl tert-butyl ether 0.0250 0.0208 0.0212 83.3 84.7 70.1-125 1.59 20 Naphthalene 0.0250 0.0189 0.0192 75.5 76.9 69.7-134 1.88 20 n-Propylbenzene 0.0250 0.0272 0.0273 109 109 81.9-122 0.400 20 Styrene 0.0250 0.0274 0.0278 110 111 79.9-124 1.60 20 1,1,1,2-Tetrachloroethane 0.0250 0.0280 0.0283 112 113 78.5-125 1.00 20 1,1,2,2-Tetrachloroethane 0.0250 0.0252 0.0253 101 101 79.3-123 0.550 20 Tetrachloroethene 0.0250 0.0295 0.0295 118 118 73.5-130 0.200 20 Toluene 0.0250 0.0240 0.0248 95.9 99.1 77.9-116 3.20 20 1,1,2-Trichlorotrifluoroethane 0.0250 0.0225 0.0219 90.0 87.6 62.0-141 2.75 20 1,2,3-Trichlorobenzene 0.0250 0.0212 0.0219 85.0 87.5 75.7-134 2.96 20 1,2,4-Trichlorobenzene 0.0250 0.0230 0.0235 91.8 93.9 76.1-136 2.26 20 1,1,1-Trichloroethane 0.0250 0.0232 0.0229 92.8 91.5 71.1-129 1.34 20 1,1,2-Trichloroethane 0.0250 0.0256 0.0265 102 106 81.6-120 3.53 20 Trichloroethene 0.0250 0.0264 0.0271 106 108 79.5-121 2.41 20 Trichlorofluoromethane 0.0250 0.0224 0.0224 89.5 89.4 49.1-157 0.120 20 1,2,3-Trichloropropane 0.0250 0.0252 0.0252 101 101 74.9-124 0.0900 20 1,2,3-Trimethylbenzene 0.0250 0.0229 0.0239 91.8 95.6 79.9-118 4.04 20 1,2,4-Trimethylbenzene 0.0250 0.0272 0.0269 109 108 79.0-122 1.27 20 1,3,5-Trimethylbenzene 0.0250 0.0276 0.0269 110 108 81.0-123 2.46 20 Vinyl chloride 0.0250 0.0211 0.0206 84.5 82.3 61.5-134 2.58 20 Xylenes, Total 0.0750 0.0822 0.0826 110 110 79.2-122 0.470 20 (S) Toluene-d8 100 102 90.0-115 (S) Dibromofluoromethane 93.8 92.2 79.0-121 (S) 4-Bromofluorobenzene 108 106 80.1-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 22 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 22 of 26 ONE LAB. NATIONWIDE.GLOSSARY OF TERMS Abbreviations and Definitions SDG Sample Delivery Group. MDL Method Detection Limit. RDL Reported Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. (S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. Rec.Recovery. Qualifier Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 23 of 26 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 23 of 26 ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 09:33 24 of 26 Our Locations Alabama 40660 Alaska UST-080 Arizona AZ0612 Arkansas 88-0469 California 01157CA Colorado TN00003 Conneticut PH-0197 Florida E87487 Georgia NELAP Georgia 1 923 Idaho TN00003 Illinois 200008 Indiana C-TN-01 Iowa 364 Kansas E-10277 Kentucky 1 90010 Kentucky 2 16 Louisiana AI30792 Maine TN0002 Maryland 324 Massachusetts M-TN003 Michigan 9958 Minnesota 047-999-395 Mississippi TN00003 Missouri 340 Montana CERT0086 Nebraska NE-OS-15-05 Nevada TN-03-2002-34 New Hampshire 2975 New Jersey–NELAP TN002 New Mexico TN00003 New York 11742 North Carolina Env375 North Carolina 1 DW21704 North Carolina 2 41 North Dakota R-140 Ohio–VAP CL0069 Oklahoma 9915 Oregon TN200002 Pennsylvania 68-02979 Rhode Island 221 South Carolina 84004 South Dakota n/a Tennessee 1 4 2006 Texas T 104704245-07-TX Texas 5 LAB0152 Utah 6157585858 Vermont VT2006 Virginia 109 Washington C1915 West Virginia 233 Wisconsin 9980939910 Wyoming A2LA A2LA – ISO 17025 1461.01 Canada 1461.01 EPA–Crypto TN00003 AIHA 100789 DOD 1461.01 USDA S-67674 State Accreditations Third Party & Federal Accreditations ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. 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Chemical/Microbiological 5. Mold n/a Accreditation not applicable 1461.02A2LA – ISO 170255 * Not all certifications held by the laboratory are applicable to the results reported in the attached report. ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Griffith Enterprise L880165 12/29/16 10:17 24 of 26