MMPE-&-GWMR-10-07-14 87p

09/26/14
Technical Report for
GRI (Geological Resources Inc.)
Anson Mart; 1250 E Caswell, Wadesboro, NC
29457
Accutest Job Number: FA18436
Sampling Date: 09/15/14
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
09/26/14
e-Hardcopy 2.0
Automated Report
50
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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FA18436
Table of Contents
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Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: FA18436-1: MW-1 ........................................................................................................10
3.2: FA18436-2: MW-2 ........................................................................................................12
3.3: FA18436-3: MW-3 ........................................................................................................14
3.4: FA18436-4: MW-4 ........................................................................................................16
3.5: FA18436-5: MW-5 ........................................................................................................18
3.6: FA18436-6: MW-6 ........................................................................................................20
3.7: FA18436-7: MW-7 ........................................................................................................22
3.8: FA18436-8: MW-8 ........................................................................................................24
3.9: FA18436-9: MW-9 ........................................................................................................26
3.10: FA18436-10: MW-10 ..................................................................................................28
3.11: FA18436-11: MW-11 ..................................................................................................30
3.12: FA18436-12: MW-12 ..................................................................................................33
3.13: FA18436-13: TW-1 .....................................................................................................35
3.14: FA18436-14: STREAM ..............................................................................................37
Section 4: Misc. Forms ............................................................................................................39
4.1: Chain of Custody ...........................................................................................................40
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................44
5.1: Method Blank Summary ................................................................................................45
5.2: Blank Spike Summary ...................................................................................................47
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................49
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Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA18436
Anson Mart; 1250 E Caswell, Wadesboro, NC
Project No: 29457
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA18436-1 09/15/14 13:47 CB 09/19/14 AQ Ground Water MW-1
FA18436-2 09/15/14 13:36 CB 09/19/14 AQ Ground Water MW-2
FA18436-3 09/15/14 12:40 CB 09/19/14 AQ Ground Water MW-3
FA18436-4 09/15/14 13:33 CB 09/19/14 AQ Ground Water MW-4
FA18436-5 09/15/14 12:16 CB 09/19/14 AQ Ground Water MW-5
FA18436-6 09/15/14 12:25 CB 09/19/14 AQ Ground Water MW-6
FA18436-7 09/15/14 12:04 CB 09/19/14 AQ Ground Water MW-7
FA18436-8 09/15/14 12:07 CB 09/19/14 AQ Ground Water MW-8
FA18436-9 09/15/14 11:47 CB 09/19/14 AQ Ground Water MW-9
FA18436-10 09/15/14 12:35 CB 09/19/14 AQ Ground Water MW-10
FA18436-11 09/15/14 13:01 CB 09/19/14 AQ Ground Water MW-11
FA18436-12 09/15/14 13:11 CB 09/19/14 AQ Ground Water MW-12
FA18436-13 09/15/14 13:21 CB 09/19/14 AQ Ground Water TW-1
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Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA18436
Anson Mart; 1250 E Caswell, Wadesboro, NC
Project No: 29457
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA18436-14 09/15/14 13:17 CB 09/19/14 AQ Surface Water STREAM
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Summary of Hits Page 1 of 4
Job Number:FA18436
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/15/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA18436-1 MW-1
Benzene 538 25 5.0 ug/l SM 6200B
n-Butylbenzene 18.4 J 25 5.0 ug/l SM 6200B
sec-Butylbenzene 11.4 J 25 5.0 ug/l SM 6200B
Ethylbenzene 1120 25 5.0 ug/l SM 6200B
Isopropylbenzene 87.0 25 5.0 ug/l SM 6200B
p-Isopropyltoluene 5.9 J 25 5.0 ug/l SM 6200B
Naphthalene 656 25 5.0 ug/l SM 6200B
n-Propylbenzene 274 25 5.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 1460 25 5.0 ug/l SM 6200B
1,3,5-Trimethylbenzene 361 25 5.0 ug/l SM 6200B
Toluene 852 25 5.0 ug/l SM 6200B
Xylene (total)3710 75 10 ug/l SM 6200B
m,p-Xylene 2800 50 5.0 ug/l SM 6200B
o-Xylene 902 25 5.0 ug/l SM 6200B
FA18436-2 MW-2
Benzene 2.1 J 2.5 0.50 ug/l SM 6200B
n-Butylbenzene 1.2 J 2.5 0.50 ug/l SM 6200B
sec-Butylbenzene 1.3 J 2.5 0.50 ug/l SM 6200B
Ethylbenzene 107 2.5 0.50 ug/l SM 6200B
Isopropylbenzene 8.3 2.5 0.50 ug/l SM 6200B
Naphthalene 23.3 2.5 0.50 ug/l SM 6200B
n-Propylbenzene 22.0 2.5 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 125 2.5 0.50 ug/l SM 6200B
1,3,5-Trimethylbenzene 10.1 2.5 0.50 ug/l SM 6200B
Toluene 1.9 J 2.5 0.50 ug/l SM 6200B
Xylene (total)46.7 7.5 1.0 ug/l SM 6200B
m,p-Xylene 46.7 5.0 0.50 ug/l SM 6200B
FA18436-3 MW-3
Benzene 197 5.0 1.0 ug/l SM 6200B
n-Butylbenzene 1.1 J 5.0 1.0 ug/l SM 6200B
Di-Isopropyl ether 11.9 5.0 1.0 ug/l SM 6200B
Ethylbenzene 99.2 5.0 1.0 ug/l SM 6200B
Isopropylbenzene 6.7 5.0 1.0 ug/l SM 6200B
p-Isopropyltoluene 1.0 J 5.0 1.0 ug/l SM 6200B
Methyl Tert Butyl Ether 17.2 5.0 1.0 ug/l SM 6200B
Naphthalene 19.3 5.0 1.0 ug/l SM 6200B
n-Propylbenzene 18.3 5.0 1.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 133 5.0 1.0 ug/l SM 6200B
1,3,5-Trimethylbenzene 28.8 5.0 1.0 ug/l SM 6200B
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Summary of Hits Page 2 of 4
Job Number:FA18436
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/15/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Toluene 105 5.0 1.0 ug/l SM 6200B
Xylene (total)410 15 2.0 ug/l SM 6200B
m,p-Xylene 313 10 1.0 ug/l SM 6200B
o-Xylene 96.6 5.0 1.0 ug/l SM 6200B
FA18436-4 MW-4
sec-Butylbenzene 0.12 J 0.50 0.10 ug/l SM 6200B
tert-Butylbenzene 0.12 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 23.1 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.12 J 0.50 0.10 ug/l SM 6200B
Methyl chloride 0.19 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 39.8 0.50 0.10 ug/l SM 6200B
Naphthalene 0.26 J 0.50 0.10 ug/l SM 6200B
FA18436-5 MW-5
Benzene 30.3 5.0 1.0 ug/l SM 6200B
n-Butylbenzene 1.1 J 5.0 1.0 ug/l SM 6200B
sec-Butylbenzene 1.1 J 5.0 1.0 ug/l SM 6200B
Di-Isopropyl ether 9.7 5.0 1.0 ug/l SM 6200B
Ethylbenzene 112 5.0 1.0 ug/l SM 6200B
Isopropylbenzene 11.9 5.0 1.0 ug/l SM 6200B
Naphthalene 29.8 5.0 1.0 ug/l SM 6200B
n-Propylbenzene 32.4 5.0 1.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 244 5.0 1.0 ug/l SM 6200B
1,3,5-Trimethylbenzene 53.3 5.0 1.0 ug/l SM 6200B
Toluene 15.0 5.0 1.0 ug/l SM 6200B
Xylene (total)497 15 2.0 ug/l SM 6200B
m,p-Xylene 422 10 1.0 ug/l SM 6200B
o-Xylene 75.1 5.0 1.0 ug/l SM 6200B
FA18436-6 MW-6
Benzene 46.2 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 4.3 0.50 0.10 ug/l SM 6200B
Ethylbenzene 2.6 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.28 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 29.7 0.50 0.10 ug/l SM 6200B
Naphthalene 0.28 J 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 0.51 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.93 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.16 J 0.50 0.10 ug/l SM 6200B
Toluene 2.4 0.50 0.10 ug/l SM 6200B
Xylene (total)4.7 1.5 0.20 ug/l SM 6200B
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Summary of Hits Page 3 of 4
Job Number:FA18436
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/15/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
m,p-Xylene 3.3 1.0 0.10 ug/l SM 6200B
o-Xylene 1.4 0.50 0.10 ug/l SM 6200B
FA18436-7 MW-7
No hits reported in this sample.
FA18436-8 MW-8
Chloroform 0.27 J 0.50 0.10 ug/l SM 6200B
FA18436-9 MW-9
No hits reported in this sample.
FA18436-10 MW-10
Di-Isopropyl ether 37.9 2.5 0.50 ug/l SM 6200B
Methyl Tert Butyl Ether 180 2.5 0.50 ug/l SM 6200B
FA18436-11 MW-11
No hits reported in this sample.
FA18436-12 MW-12
No hits reported in this sample.
FA18436-13 TW-1
Benzene 2.8 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 0.10 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.77 0.50 0.10 ug/l SM 6200B
Ethylbenzene 0.45 J 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.92 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 1.8 0.50 0.10 ug/l SM 6200B
Naphthalene 0.19 J 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 1.3 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.2 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.40 J 0.50 0.10 ug/l SM 6200B
Toluene 1.1 0.50 0.10 ug/l SM 6200B
Xylene (total)4.1 1.5 0.20 ug/l SM 6200B
m,p-Xylene 3.7 1.0 0.10 ug/l SM 6200B
o-Xylene 0.46 J 0.50 0.10 ug/l SM 6200B
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Summary of Hits Page 4 of 4
Job Number:FA18436
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/15/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA18436-14 STREAM
Benzene 2.1 0.50 0.10 ug/l SM 6200B
Ethylbenzene 0.38 J 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 0.12 J 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.24 J 0.50 0.10 ug/l SM 6200B
Toluene 0.23 J 0.50 0.10 ug/l SM 6200B
Xylene (total)0.84 J 1.5 0.20 ug/l SM 6200B
m,p-Xylene 0.84 J 1.0 0.10 ug/l SM 6200B
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Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA18436-1 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033364.D 50 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 538 25 5.0 ug/l
108-86-1 Bromobenzene ND 25 5.0 ug/l
74-97-5 Bromochloromethane ND 25 5.0 ug/l
75-27-4 Bromodichloromethane ND 25 5.0 ug/l
75-25-2 Bromoform ND 25 5.0 ug/l
104-51-8 n-Butylbenzene 18.4 25 5.0 ug/l J
135-98-8 sec-Butylbenzene 11.4 25 5.0 ug/l J
98-06-6 tert-Butylbenzene ND 25 5.0 ug/l
108-90-7 Chlorobenzene ND 25 5.0 ug/l
75-00-3 Chloroethane ND 25 6.1 ug/l
67-66-3 Chloroform ND 25 5.0 ug/l
95-49-8 o-Chlorotoluene ND 25 5.0 ug/l
106-43-4 p-Chlorotoluene ND 25 5.0 ug/l
56-23-5 Carbon tetrachloride ND 25 5.0 ug/l
75-34-3 1,1-Dichloroethane ND 25 5.0 ug/l
75-35-4 1,1-Dichloroethylene ND 25 5.0 ug/l
563-58-6 1,1-Dichloropropene ND 25 5.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 8.6 ug/l
106-93-4 1,2-Dibromoethane ND 25 5.0 ug/l
107-06-2 1,2-Dichloroethane ND 25 5.0 ug/l
78-87-5 1,2-Dichloropropane ND 25 5.0 ug/l
142-28-9 1,3-Dichloropropane ND 25 5.0 ug/l
108-20-3 Di-Isopropyl ether ND 25 5.0 ug/l
594-20-7 2,2-Dichloropropane ND 25 5.0 ug/l
124-48-1 Dibromochloromethane ND 25 5.0 ug/l
75-71-8 Dichlorodifluoromethane ND 25 5.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 5.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 5.0 ug/l
541-73-1 m-Dichlorobenzene ND 25 5.0 ug/l
95-50-1 o-Dichlorobenzene ND 25 5.0 ug/l
106-46-7 p-Dichlorobenzene ND 25 5.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 5.0 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA18436-1 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 25 5.0 ug/l
100-41-4 Ethylbenzene 1120 25 5.0 ug/l
87-68-3 Hexachlorobutadiene ND 25 5.0 ug/l
98-82-8 Isopropylbenzene 87.0 25 5.0 ug/l
99-87-6 p-Isopropyltoluene 5.9 25 5.0 ug/l J
74-83-9 Methyl bromide ND 25 5.0 ug/l
74-87-3 Methyl chloride ND 25 5.0 ug/l
74-95-3 Methylene bromide ND 25 5.0 ug/l
75-09-2 Methylene chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 25 5.0 ug/l
91-20-3 Naphthalene 656 25 5.0 ug/l
103-65-1 n-Propylbenzene 274 25 5.0 ug/l
100-42-5 Styrene ND 25 5.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 5.0 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 5.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 5.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 5.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 5.9 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 5.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 1460 25 5.0 ug/l
108-67-8 1,3,5-Trimethylbenzene 361 25 5.0 ug/l
127-18-4 Tetrachloroethylene ND 25 5.0 ug/l
108-88-3 Toluene 852 25 5.0 ug/l
79-01-6 Trichloroethylene ND 25 5.0 ug/l
75-69-4 Trichlorofluoromethane ND 25 5.0 ug/l
75-01-4 Vinyl chloride ND 25 5.0 ug/l
1330-20-7 Xylene (total)3710 75 10 ug/l
m,p-Xylene 2800 50 5.0 ug/l
95-47-6 o-Xylene 902 25 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA18436-2 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033367.D 5 09/23/14 EG n/a n/a VE1114
Run #2 a E033412.D 5 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.1 2.5 0.50 ug/l J
108-86-1 Bromobenzene ND 2.5 0.50 ug/l
74-97-5 Bromochloromethane ND 2.5 0.50 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.50 ug/l
75-25-2 Bromoform ND 2.5 0.50 ug/l
104-51-8 n-Butylbenzene 1.2 2.5 0.50 ug/l J
135-98-8 sec-Butylbenzene 1.3 2.5 0.50 ug/l J
98-06-6 tert-Butylbenzene ND 2.5 0.50 ug/l
108-90-7 Chlorobenzene ND 2.5 0.50 ug/l
75-00-3 Chloroethane ND 2.5 0.61 ug/l
67-66-3 Chloroform ND 2.5 0.50 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.50 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.50 ug/l
56-23-5 Carbon tetrachloride ND 2.5 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.50 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.50 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.86 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.50 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.50 ug/l
108-20-3 Di-Isopropyl ether ND 2.5 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.50 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 2.5 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 2.5 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 2.5 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.50 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA18436-2 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.50 ug/l
100-41-4 Ethylbenzene 107 2.5 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.50 ug/l
98-82-8 Isopropylbenzene 8.3 2.5 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 2.5 0.50 ug/l
74-87-3 Methyl chloride ND 2.5 0.50 ug/l
74-95-3 Methylene bromide ND 2.5 0.50 ug/l
75-09-2 Methylene chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.50 ug/l
91-20-3 Naphthalene 23.3 2.5 0.50 ug/l
103-65-1 n-Propylbenzene 22.0 2.5 0.50 ug/l
100-42-5 Styrene ND 2.5 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.53 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.59 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 125 2.5 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene 10.1 2.5 0.50 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.50 ug/l
108-88-3 Toluene 1.9 2.5 0.50 ug/l J
79-01-6 Trichloroethylene ND 2.5 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.50 ug/l
75-01-4 Vinyl chloride ND 2.5 0.50 ug/l
1330-20-7 Xylene (total)46.7 7.5 1.0 ug/l
m,p-Xylene 46.7 5.0 0.50 ug/l
95-47-6 o-Xylene ND 2.5 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 119%116%70-130%
17060-07-0 1,2-Dichloroethane-D4 121%122%70-130%
2037-26-5 Toluene-D8 96%95%70-130%
460-00-4 4-Bromofluorobenzene 101%98%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values. Confirmation run for
internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FA18436-3 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033373.D 10 09/23/14 EG n/a n/a VE1114
Run #2 a E033409.D 5 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 197 5.0 1.0 ug/l
108-86-1 Bromobenzene ND 5.0 1.0 ug/l
74-97-5 Bromochloromethane ND 5.0 1.0 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/l
75-25-2 Bromoform ND 5.0 1.0 ug/l
104-51-8 n-Butylbenzene 1.1 5.0 1.0 ug/l J
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/l
108-90-7 Chlorobenzene ND 5.0 1.0 ug/l
75-00-3 Chloroethane ND 5.0 1.2 ug/l
67-66-3 Chloroform ND 5.0 1.0 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/l
56-23-5 Carbon tetrachloride ND 5.0 1.0 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.7 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/l
108-20-3 Di-Isopropyl ether 11.9 5.0 1.0 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/l
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/l
95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/l
106-46-7 p-Dichlorobenzene ND 5.0 1.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FA18436-3 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/l
100-41-4 Ethylbenzene 99.2 5.0 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene 6.7 5.0 1.0 ug/l
99-87-6 p-Isopropyltoluene 1.0 5.0 1.0 ug/l J
74-83-9 Methyl bromide ND 5.0 1.0 ug/l
74-87-3 Methyl chloride ND 5.0 1.0 ug/l
74-95-3 Methylene bromide ND 5.0 1.0 ug/l
75-09-2 Methylene chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 17.2 5.0 1.0 ug/l
91-20-3 Naphthalene 19.3 5.0 1.0 ug/l
103-65-1 n-Propylbenzene 18.3 5.0 1.0 ug/l
100-42-5 Styrene ND 5.0 1.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.2 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 133 5.0 1.0 ug/l
108-67-8 1,3,5-Trimethylbenzene 28.8 5.0 1.0 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/l
108-88-3 Toluene 105 5.0 1.0 ug/l
79-01-6 Trichloroethylene ND 5.0 1.0 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/l
75-01-4 Vinyl chloride ND 5.0 1.0 ug/l
1330-20-7 Xylene (total)410 15 2.0 ug/l
m,p-Xylene 313 10 1.0 ug/l
95-47-6 o-Xylene 96.6 5.0 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%119%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%122%70-130%
2037-26-5 Toluene-D8 97%94%70-130%
460-00-4 4-Bromofluorobenzene 97%96%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA18436-4 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033365.D 1 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 0.12 0.50 0.10 ug/l J
98-06-6 tert-Butylbenzene 0.12 0.50 0.10 ug/l J
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 23.1 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA18436-4 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 0.12 0.50 0.10 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.19 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 39.8 0.50 0.10 ug/l
91-20-3 Naphthalene 0.26 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA18436-5 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033379.D 10 09/23/14 EG n/a n/a VE1114
Run #2 a E033406.D 5 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 30.3 5.0 1.0 ug/l
108-86-1 Bromobenzene ND 5.0 1.0 ug/l
74-97-5 Bromochloromethane ND 5.0 1.0 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/l
75-25-2 Bromoform ND 5.0 1.0 ug/l
104-51-8 n-Butylbenzene 1.1 5.0 1.0 ug/l J
135-98-8 sec-Butylbenzene 1.1 5.0 1.0 ug/l J
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/l
108-90-7 Chlorobenzene ND 5.0 1.0 ug/l
75-00-3 Chloroethane ND 5.0 1.2 ug/l
67-66-3 Chloroform ND 5.0 1.0 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/l
56-23-5 Carbon tetrachloride ND 5.0 1.0 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.7 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/l
108-20-3 Di-Isopropyl ether 9.7 5.0 1.0 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/l
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/l
95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/l
106-46-7 p-Dichlorobenzene ND 5.0 1.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA18436-5 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/l
100-41-4 Ethylbenzene 112 5.0 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene 11.9 5.0 1.0 ug/l
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/l
74-83-9 Methyl bromide ND 5.0 1.0 ug/l
74-87-3 Methyl chloride ND 5.0 1.0 ug/l
74-95-3 Methylene bromide ND 5.0 1.0 ug/l
75-09-2 Methylene chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/l
91-20-3 Naphthalene 29.8 5.0 1.0 ug/l
103-65-1 n-Propylbenzene 32.4 5.0 1.0 ug/l
100-42-5 Styrene ND 5.0 1.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.2 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 244 5.0 1.0 ug/l
108-67-8 1,3,5-Trimethylbenzene 53.3 5.0 1.0 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/l
108-88-3 Toluene 15.0 5.0 1.0 ug/l
79-01-6 Trichloroethylene ND 5.0 1.0 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/l
75-01-4 Vinyl chloride ND 5.0 1.0 ug/l
1330-20-7 Xylene (total)497 15 2.0 ug/l
m,p-Xylene 422 10 1.0 ug/l
95-47-6 o-Xylene 75.1 5.0 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 116%122%70-130%
17060-07-0 1,2-Dichloroethane-D4 122%130%70-130%
2037-26-5 Toluene-D8 96%96%70-130%
460-00-4 4-Bromofluorobenzene 96%97%70-130%
(a) Confirmation run.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA18436-6 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033366.D 1 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 46.2 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 4.3 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA18436-6 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 2.6 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 0.28 0.50 0.10 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 29.7 0.50 0.10 ug/l
91-20-3 Naphthalene 0.28 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene 0.51 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.93 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.16 0.50 0.10 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 2.4 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)4.7 1.5 0.20 ug/l
m,p-Xylene 3.3 1.0 0.10 ug/l
95-47-6 o-Xylene 1.4 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA18436-7 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E033368.D 1 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-7
Lab Sample ID:FA18436-7 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA18436-8 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033372.D 1 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform 0.27 0.50 0.10 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA18436-8 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA18436-9 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033374.D 1 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA18436-9 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 85%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA18436-10 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033376.D 5 09/23/14 EG n/a n/a VE1114
Run #2 a E033397.D 5 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 2.5 0.50 ug/l
108-86-1 Bromobenzene ND 2.5 0.50 ug/l
74-97-5 Bromochloromethane ND 2.5 0.50 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.50 ug/l
75-25-2 Bromoform ND 2.5 0.50 ug/l
104-51-8 n-Butylbenzene ND 2.5 0.50 ug/l
135-98-8 sec-Butylbenzene ND 2.5 0.50 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.50 ug/l
108-90-7 Chlorobenzene ND 2.5 0.50 ug/l
75-00-3 Chloroethane ND 2.5 0.61 ug/l
67-66-3 Chloroform ND 2.5 0.50 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.50 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.50 ug/l
56-23-5 Carbon tetrachloride ND 2.5 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.50 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.50 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.86 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.50 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.50 ug/l
108-20-3 Di-Isopropyl ether 37.9 2.5 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.50 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 2.5 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 2.5 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 2.5 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.50 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA18436-10 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.50 ug/l
100-41-4 Ethylbenzene ND 2.5 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.50 ug/l
98-82-8 Isopropylbenzene ND 2.5 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 2.5 0.50 ug/l
74-87-3 Methyl chloride ND 2.5 0.50 ug/l
74-95-3 Methylene bromide ND 2.5 0.50 ug/l
75-09-2 Methylene chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 180 2.5 0.50 ug/l
91-20-3 Naphthalene ND 2.5 0.50 ug/l
103-65-1 n-Propylbenzene ND 2.5 0.50 ug/l
100-42-5 Styrene ND 2.5 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.53 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.59 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 2.5 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 2.5 0.50 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.50 ug/l
108-88-3 Toluene ND 2.5 0.50 ug/l
79-01-6 Trichloroethylene ND 2.5 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.50 ug/l
75-01-4 Vinyl chloride ND 2.5 0.50 ug/l
1330-20-7 Xylene (total)ND 7.5 1.0 ug/l
m,p-Xylene ND 5.0 0.50 ug/l
95-47-6 o-Xylene ND 2.5 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%113%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%120%70-130%
2037-26-5 Toluene-D8 98%99%70-130%
460-00-4 4-Bromofluorobenzene 99%100%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-11
Lab Sample ID:FA18436-11 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E033375.D 1 09/23/14 EG n/a n/a VE1114
Run #2 b E033410.D 1 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-11
Lab Sample ID:FA18436-11 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%119%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%124%70-130%
2037-26-5 Toluene-D8 97%95%70-130%
460-00-4 4-Bromofluorobenzene 96%97%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
(b) Sample was not preserved to a pH < 2; reported results are considered minimum values. Confirmation run for
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-11
Lab Sample ID:FA18436-11 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-12
Lab Sample ID:FA18436-12 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033377.D 1 09/23/14 EG n/a n/a VE1114
Run #2 a E033411.D 1 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA18436-12 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%111%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%116%70-130%
2037-26-5 Toluene-D8 95%93%70-130%
460-00-4 4-Bromofluorobenzene 96%96%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TW-1
Lab Sample ID:FA18436-13 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033378.D 1 09/23/14 EG n/a n/a VE1114
Run #2 a E033413.D 1 09/24/14 EG n/a n/a VE1115
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.8 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 0.10 0.50 0.10 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.77 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TW-1
Lab Sample ID:FA18436-13 Date Sampled:09/15/14
Matrix:AQ - Ground Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 0.45 0.50 0.10 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 0.92 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.8 0.50 0.10 ug/l
91-20-3 Naphthalene 0.19 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene 1.3 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.2 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.40 0.50 0.10 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 1.1 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)4.1 1.5 0.20 ug/l
m,p-Xylene 3.7 1.0 0.10 ug/l
95-47-6 o-Xylene 0.46 0.50 0.10 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%108%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%114%70-130%
2037-26-5 Toluene-D8 97%94%70-130%
460-00-4 4-Bromofluorobenzene 97%97%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:STREAM
Lab Sample ID:FA18436-14 Date Sampled:09/15/14
Matrix:AQ - Surface Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033380.D 1 09/23/14 EG n/a n/a VE1114
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.1 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:STREAM
Lab Sample ID:FA18436-14 Date Sampled:09/15/14
Matrix:AQ - Surface Water Date Received:09/19/14
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 0.38 0.50 0.10 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene 0.12 0.50 0.10 ug/l J
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.24 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 0.23 0.50 0.10 ug/l J
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)0.84 1.5 0.20 ug/l J
m,p-Xylene 0.84 1.0 0.10 ug/l J
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
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FA18436: Chain of Custody
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Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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Method Blank Summary Page 1 of 2
Job Number:FA18436
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1114-MB E033359.D 1 09/23/14 EG n/a n/a VE1114
The QC reported here applies to the following samples:Method: SM 6200B
FA18436-1, FA18436-2, FA18436-3, FA18436-4, FA18436-5, FA18436-6, FA18436-7, FA18436-8, FA18436-9,
FA18436-10, FA18436-11, FA18436-12, FA18436-13, FA18436-14
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
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Method Blank Summary Page 2 of 2
Job Number:FA18436
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1114-MB E033359.D 1 09/23/14 EG n/a n/a VE1114
The QC reported here applies to the following samples:Method: SM 6200B
FA18436-1, FA18436-2, FA18436-3, FA18436-4, FA18436-5, FA18436-6, FA18436-7, FA18436-8, FA18436-9,
FA18436-10, FA18436-11, FA18436-12, FA18436-13, FA18436-14
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
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Blank Spike Summary Page 1 of 2
Job Number:FA18436
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1114-BS E033357.D 1 09/23/14 EG n/a n/a VE1114
The QC reported here applies to the following samples:Method: SM 6200B
FA18436-1, FA18436-2, FA18436-3, FA18436-4, FA18436-5, FA18436-6, FA18436-7, FA18436-8, FA18436-9,
FA18436-10, FA18436-11, FA18436-12, FA18436-13, FA18436-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.0 100 70-130
108-86-1 Bromobenzene 10 10.4 104 70-130
74-97-5 Bromochloromethane 10 10.2 102 70-130
75-27-4 Bromodichloromethane 10 10.9 109 70-130
75-25-2 Bromoform 10 10.6 106 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 11.9 119 70-130
98-06-6 tert-Butylbenzene 10 12.1 121 70-130
108-90-7 Chlorobenzene 10 11.0 110 70-130
75-00-3 Chloroethane 10 10.7 107 60-140
67-66-3 Chloroform 10 10.6 106 70-130
95-49-8 o-Chlorotoluene 10 11.2 112 70-130
106-43-4 p-Chlorotoluene 10 11.5 115 70-130
56-23-5 Carbon tetrachloride 10 12.0 120 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
75-35-4 1,1-Dichloroethylene 10 11.5 115 70-130
563-58-6 1,1-Dichloropropene 10 11.6 116 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.6 96 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
107-06-2 1,2-Dichloroethane 10 10.9 109 70-130
78-87-5 1,2-Dichloropropane 10 9.6 96 70-130
142-28-9 1,3-Dichloropropane 10 9.9 99 70-130
108-20-3 Di-Isopropyl ether 10 9.2 92 70-130
594-20-7 2,2-Dichloropropane 10 12.6 126 70-130
124-48-1 Dibromochloromethane 10 10.4 104 70-130
75-71-8 Dichlorodifluoromethane 10 10.2 102 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10.3 103 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.3 103 70-130
541-73-1 m-Dichlorobenzene 10 11.5 115 70-130
95-50-1 o-Dichlorobenzene 10 11.4 114 70-130
106-46-7 p-Dichlorobenzene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.5 105 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.2 112 70-130
100-41-4 Ethylbenzene 10 10.4 104 70-130
87-68-3 Hexachlorobutadiene 10 12.0 120 70-130
98-82-8 Isopropylbenzene 10 12.1 121 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 2
Job Number:FA18436
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1114-BS E033357.D 1 09/23/14 EG n/a n/a VE1114
The QC reported here applies to the following samples:Method: SM 6200B
FA18436-1, FA18436-2, FA18436-3, FA18436-4, FA18436-5, FA18436-6, FA18436-7, FA18436-8, FA18436-9,
FA18436-10, FA18436-11, FA18436-12, FA18436-13, FA18436-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 12.0 120 70-130
74-83-9 Methyl bromide 10 11.3 113 60-140
74-87-3 Methyl chloride 10 9.5 95 60-140
74-95-3 Methylene bromide 10 10.4 104 70-130
75-09-2 Methylene chloride 10 8.9 89 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.8 98 70-130
91-20-3 Naphthalene 10 10.3 103 70-130
103-65-1 n-Propylbenzene 10 11.5 115 70-130
100-42-5 Styrene 10 10.6 106 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.9 109 70-130
71-55-6 1,1,1-Trichloroethane 10 11.8 118 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 9.5 95 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.5 105 70-130
96-18-4 1,2,3-Trichloropropane 10 10.5 105 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.5 105 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.8 108 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.7 107 70-130
127-18-4 Tetrachloroethylene 10 11.2 112 70-130
108-88-3 Toluene 10 10 100 70-130
79-01-6 Trichloroethylene 10 10.8 108 70-130
75-69-4 Trichlorofluoromethane 10 12.2 122 60-140
75-01-4 Vinyl chloride 10 10.7 107 60-140
1330-20-7 Xylene (total)30 34.0 113 70-130
m,p-Xylene 20 22.4 112 70-130
95-47-6 o-Xylene 10 11.6 116 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA18436
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA18436-1MS E033369.D 50 09/23/14 EG n/a n/a VE1114
FA18436-1MSD E033370.D 50 09/23/14 EG n/a n/a VE1114
FA18436-1 E033364.D 50 09/23/14 EG n/a n/a VE1114
The QC reported here applies to the following samples:Method: SM 6200B
FA18436-1, FA18436-2, FA18436-3, FA18436-4, FA18436-5, FA18436-6, FA18436-7, FA18436-8, FA18436-9,
FA18436-10, FA18436-11, FA18436-12, FA18436-13, FA18436-14
FA18436-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 538 500 1050 102 500 990 90 6 70-130/20
108-86-1 Bromobenzene ND 500 516 103 500 504 101 2 70-130/20
74-97-5 Bromochloromethane ND 500 519 104 500 492 98 5 70-130/20
75-27-4 Bromodichloromethane ND 500 506 101 500 499 100 1 70-130/20
75-25-2 Bromoform ND 500 337 67*500 423 85 23*70-130/20
104-51-8 n-Butylbenzene 18.4 J 500 570 110 500 551 107 3 70-130/20
135-98-8 sec-Butylbenzene 11.4 J 500 615 121 500 590 116 4 70-130/20
98-06-6 tert-Butylbenzene ND 500 610 122 500 579 116 5 70-130/20
108-90-7 Chlorobenzene ND 500 551 110 500 517 103 6 70-130/20
75-00-3 Chloroethane ND 500 529 106 500 494 99 7 60-140/20
67-66-3 Chloroform ND 500 549 110 500 498 100 10 70-130/20
95-49-8 o-Chlorotoluene ND 500 611 122 500 584 117 5 70-130/20
106-43-4 p-Chlorotoluene ND 500 571 114 500 549 110 4 70-130/20
56-23-5 Carbon tetrachloride ND 500 605 121 500 540 108 11 70-130/20
75-34-3 1,1-Dichloroethane ND 500 525 105 500 485 97 8 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 565 113 500 521 104 8 70-130/20
563-58-6 1,1-Dichloropropene ND 500 583 117 500 541 108 7 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 477 95 500 461 92 3 70-130/20
106-93-4 1,2-Dibromoethane ND 500 521 104 500 494 99 5 70-130/20
107-06-2 1,2-Dichloroethane ND 500 547 109 500 502 100 9 70-130/20
78-87-5 1,2-Dichloropropane ND 500 504 101 500 477 95 6 70-130/20
142-28-9 1,3-Dichloropropane ND 500 495 99 500 468 94 6 70-130/20
108-20-3 Di-Isopropyl ether ND 500 468 94 500 447 89 5 70-130/20
594-20-7 2,2-Dichloropropane ND 500 636 127 500 587 117 8 70-130/20
124-48-1 Dibromochloromethane ND 500 411 82 500 455 91 10 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 512 102 500 451 90 13 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 500 526 105 500 498 100 5 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 516 103 500 485 97 6 70-130/20
541-73-1 m-Dichlorobenzene ND 500 582 116 500 559 112 4 70-130/20
95-50-1 o-Dichlorobenzene ND 500 577 115 500 561 112 3 70-130/20
106-46-7 p-Dichlorobenzene ND 500 522 104 500 505 101 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 530 106 500 483 97 9 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 556 111 500 520 104 7 70-130/20
100-41-4 Ethylbenzene 1120 500 1640 104 500 1530 82 7 70-130/20
87-68-3 Hexachlorobutadiene ND 500 604 121 500 593 119 2 70-130/20
98-82-8 Isopropylbenzene 87.0 500 730 129 500 674 117 8 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA18436
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA18436-1MS E033369.D 50 09/23/14 EG n/a n/a VE1114
FA18436-1MSD E033370.D 50 09/23/14 EG n/a n/a VE1114
FA18436-1 E033364.D 50 09/23/14 EG n/a n/a VE1114
The QC reported here applies to the following samples:Method: SM 6200B
FA18436-1, FA18436-2, FA18436-3, FA18436-4, FA18436-5, FA18436-6, FA18436-7, FA18436-8, FA18436-9,
FA18436-10, FA18436-11, FA18436-12, FA18436-13, FA18436-14
FA18436-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 5.9 J 500 613 121 500 590 117 4 70-130/20
74-83-9 Methyl bromide ND 500 551 110 500 515 103 7 60-140/20
74-87-3 Methyl chloride ND 500 454 91 500 432 86 5 60-140/20
74-95-3 Methylene bromide ND 500 539 108 500 493 99 9 70-130/20
75-09-2 Methylene chloride ND 500 465 93 500 432 86 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 500 497 99 500 474 95 5 70-130/20
91-20-3 Naphthalene 656 500 1240 117 500 1240 117 0 70-130/20
103-65-1 n-Propylbenzene 274 500 863 118 500 826 110 4 70-130/20
100-42-5 Styrene ND 500 541 108 500 511 102 6 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 546 109 500 514 103 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 592 118 500 545 109 8 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 479 96 500 475 95 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 503 101 500 474 95 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 533 107 500 530 106 1 70-130/20
96-18-4 1,2,3-Trichloropropane ND 500 511 102 500 497 99 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 551 110 500 541 108 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1460 500 2040 116 500 1940 96 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene 361 500 922 112 500 877 103 5 70-130/20
127-18-4 Tetrachloroethylene ND 500 572 114 500 532 106 7 70-130/20
108-88-3 Toluene 852 500 1340 98 500 1260 82 6 70-130/20
79-01-6 Trichloroethylene ND 500 543 109 500 505 101 7 70-130/20
75-69-4 Trichlorofluoromethane ND 500 607 121 500 532 106 13 60-140/20
75-01-4 Vinyl chloride ND 500 511 102 500 487 97 5 60-140/20
1330-20-7 Xylene (total)3710 1500 5470 117 1500 5060 90 8 70-130/20
m,p-Xylene 2800 1000 3930 113 1000 3630 83 8 70-130/20
95-47-6 o-Xylene 902 500 1540 128 500 1430 106 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA18436-1 Limits
1868-53-7 Dibromofluoromethane 106%102%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%106%109%70-130%
2037-26-5 Toluene-D8 97%97%97%70-130%
460-00-4 4-Bromofluorobenzene 96%97%97%70-130%
* = Outside of Control Limits.
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