MMPE-&-GWMR-04-16-15 98p

03/24/15
Technical Report for
GRI (Geological Resources Inc.)
Anson Mart; 1250 E Caswell, Wadesboro, NC
29457
Accutest Job Number: FA22769
Sampling Date: 03/09/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
03/24/15
e-Hardcopy 2.0
Automated Report
61
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 61
FA22769
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: FA22769-1: MW-5 ........................................................................................................10
3.2: FA22769-2: MW-6 ........................................................................................................12
3.3: FA22769-3: MW-3 ........................................................................................................14
3.4: FA22769-4: MW-7 ........................................................................................................16
3.5: FA22769-5: MW-8 ........................................................................................................18
3.6: FA22769-6: MW-2 ........................................................................................................20
3.7: FA22769-7: TW-1 .........................................................................................................22
3.8: FA22769-8: MW-1 ........................................................................................................24
3.9: FA22769-9: MW-4 ........................................................................................................26
3.10: FA22769-10: MW-12 ..................................................................................................28
3.11: FA22769-11: MW-11 ..................................................................................................30
3.12: FA22769-12: MW-10 ..................................................................................................32
3.13: FA22769-13: STREAM ..............................................................................................34
3.14: FA22769-14: TRIP BLANK .......................................................................................36
Section 4: Misc. Forms ............................................................................................................38
4.1: Chain of Custody ...........................................................................................................39
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................43
5.1: Method Blank Summary ................................................................................................44
5.2: Blank Spike Summary ...................................................................................................50
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................56
1
2
3
4
5
2 of 61
FA22769
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA22769
Anson Mart; 1250 E Caswell, Wadesboro, NC
Project No: 29457
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA22769-1 03/09/15 10:28 DB 03/12/15 AQ Ground Water MW-5
FA22769-2 03/09/15 10:39 DB 03/12/15 AQ Ground Water MW-6
FA22769-3 03/09/15 10:51 DB 03/12/15 AQ Ground Water MW-3
FA22769-4 03/09/15 11:04 DB 03/12/15 AQ Ground Water MW-7
FA22769-5 03/09/15 11:22 DB 03/12/15 AQ Ground Water MW-8
FA22769-6 03/09/15 11:36 DB 03/12/15 AQ Ground Water MW-2
FA22769-7 03/09/15 11:58 DB 03/12/15 AQ Ground Water TW-1
FA22769-8 03/09/15 12:14 DB 03/12/15 AQ Ground Water MW-1
FA22769-9 03/09/15 12:28 DB 03/12/15 AQ Ground Water MW-4
FA22769-10 03/09/15 12:45 DB 03/12/15 AQ Ground Water MW-12
FA22769-11 03/09/15 12:58 DB 03/12/15 AQ Ground Water MW-11
FA22769-12 03/09/15 13:17 DB 03/12/15 AQ Ground Water MW-10
FA22769-13 03/09/15 13:24 DB 03/12/15 AQ Surface Water STREAM
3 of 61
FA22769
1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA22769
Anson Mart; 1250 E Caswell, Wadesboro, NC
Project No: 29457
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA22769-14 03/09/15 00:00 DB 03/12/15 AQ Trip Blank Water TRIP BLANK
4 of 61
FA22769
1
Summary of Hits Page 1 of 4
Job Number:FA22769
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:03/09/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA22769-1 MW-5
Benzene 24.4 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 1.7 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 1.2 0.50 0.14 ug/l SM 6200B
Di-Isopropyl Ether 1.8 0.50 0.16 ug/l SM 6200B
Ethylbenzene a 62.1 2.5 0.76 ug/l SM 6200B
Isopropylbenzene 10.6 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.86 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 2.5 0.50 0.16 ug/l SM 6200B
Naphthalene 15.7 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 32.7 0.50 0.16 ug/l SM 6200B
Toluene 18.9 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene a 114 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 40.2 0.50 0.14 ug/l SM 6200B
m,p-Xylene a 215 5.0 1.5 ug/l SM 6200B
o-Xylene a 21.2 2.5 0.67 ug/l SM 6200B
Xylene (total) a 237 7.5 2.2 ug/l SM 6200B
FA22769-2 MW-6
Benzene 20.3 0.50 0.17 ug/l SM 6200B
Di-Isopropyl Ether 0.52 0.50 0.16 ug/l SM 6200B
Ethylbenzene 0.99 0.50 0.15 ug/l SM 6200B
Methyl Tert Butyl Ether 3.2 0.50 0.16 ug/l SM 6200B
n-Propylbenzene 0.23 J 0.50 0.16 ug/l SM 6200B
Toluene 3.0 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.43 J 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.18 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 2.6 1.0 0.30 ug/l SM 6200B
o-Xylene 0.62 0.50 0.13 ug/l SM 6200B
Xylene (total)3.2 1.5 0.43 ug/l SM 6200B
FA22769-3 MW-3
Benzene 70.9 1.0 0.34 ug/l SM 6200B
n-Butylbenzene 0.29 J 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.20 J 0.50 0.14 ug/l SM 6200B
Di-Isopropyl Ether 26.6 0.50 0.16 ug/l SM 6200B
Ethylbenzene 16.8 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 1.2 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.17 J 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 41.4 0.50 0.16 ug/l SM 6200B
Naphthalene 2.3 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 3.5 0.50 0.16 ug/l SM 6200B
5 of 61
FA22769
2
Summary of Hits Page 2 of 4
Job Number:FA22769
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:03/09/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Toluene 1.7 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 9.2 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.6 0.50 0.14 ug/l SM 6200B
m,p-Xylene 9.1 1.0 0.30 ug/l SM 6200B
o-Xylene 1.4 0.50 0.13 ug/l SM 6200B
Xylene (total)10.5 1.5 0.43 ug/l SM 6200B
FA22769-4 MW-7
No hits reported in this sample.
FA22769-5 MW-8
No hits reported in this sample.
FA22769-6 MW-2
Benzene 1.4 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 3.0 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 2.3 0.50 0.14 ug/l SM 6200B
Ethylbenzene 99.0 2.5 0.76 ug/l SM 6200B
Isopropylbenzene 13.1 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.99 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.21 J 0.50 0.16 ug/l SM 6200B
Naphthalene 26.2 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 37.4 0.50 0.16 ug/l SM 6200B
Toluene 2.8 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 102 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 19.6 0.50 0.14 ug/l SM 6200B
m,p-Xylene 93.1 5.0 1.5 ug/l SM 6200B
o-Xylene 12.6 0.50 0.13 ug/l SM 6200B
Xylene (total)102 7.5 2.2 ug/l SM 6200B
FA22769-7 TW-1
Di-Isopropyl Ether 0.33 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.79 0.50 0.16 ug/l SM 6200B
FA22769-8 MW-1
Benzene a 384 13 4.3 ug/l SM 6200B
n-Butylbenzene a 29.3 13 3.6 ug/l SM 6200B
sec-Butylbenzene a 17.5 13 3.5 ug/l SM 6200B
Ethylbenzene 1590 50 15 ug/l SM 6200B
Isopropylbenzene a 133 13 3.0 ug/l SM 6200B
6 of 61
FA22769
2
Summary of Hits Page 3 of 4
Job Number:FA22769
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:03/09/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
p-Isopropyltoluene a 7.5 J 13 3.1 ug/l SM 6200B
Methyl Tert Butyl Ether a 5.7 J 13 4.1 ug/l SM 6200B
Naphthalene a 537 13 3.1 ug/l SM 6200B
n-Propylbenzene a 425 13 3.9 ug/l SM 6200B
Toluene 2210 50 17 ug/l SM 6200B
1,2,4-Trimethylbenzene 1420 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene a 415 13 3.4 ug/l SM 6200B
m,p-Xylene 3620 100 30 ug/l SM 6200B
o-Xylene 938 50 13 ug/l SM 6200B
Xylene (total)4560 150 43 ug/l SM 6200B
FA22769-9 MW-4
Benzene b 3.2 0.50 0.17 ug/l SM 6200B
sec-Butylbenzene b 0.16 J 0.50 0.14 ug/l SM 6200B
Di-Isopropyl Ether b 38.8 0.50 0.16 ug/l SM 6200B
Ethylbenzene b 1.8 0.50 0.15 ug/l SM 6200B
Isopropylbenzene b 0.70 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 73.0 1.0 0.33 ug/l SM 6200B
Naphthalene b 0.17 J 0.50 0.12 ug/l SM 6200B
n-Propylbenzene b 0.22 J 0.50 0.16 ug/l SM 6200B
1,2,4-Trimethylbenzene b 0.78 0.50 0.14 ug/l SM 6200B
m,p-Xylene b 0.73 J 1.0 0.30 ug/l SM 6200B
FA22769-10 MW-12
Naphthalene a 0.32 J 0.50 0.12 ug/l SM 6200B
FA22769-11 MW-11
No hits reported in this sample.
FA22769-12 MW-10
Benzene a 0.92 0.50 0.17 ug/l SM 6200B
Chlorobenzene a 0.24 J 0.50 0.16 ug/l SM 6200B
Di-Isopropyl Ether a 51.8 5.0 1.6 ug/l SM 6200B
Ethylbenzene a 0.33 J 0.50 0.15 ug/l SM 6200B
Methyl Tert Butyl Ether a 230 5.0 1.6 ug/l SM 6200B
FA22769-13 STREAM
Benzene 0.47 J 0.50 0.17 ug/l SM 6200B
Ethylbenzene 0.22 J 0.50 0.15 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.16 J 0.50 0.14 ug/l SM 6200B
7 of 61
FA22769
2
Summary of Hits Page 4 of 4
Job Number:FA22769
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:03/09/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
m,p-Xylene 0.46 J 1.0 0.30 ug/l SM 6200B
Xylene (total)0.46 J 1.5 0.43 ug/l SM 6200B
FA22769-14 TRIP BLANK
No hits reported in this sample.
(a) Internal standard areas outside method criteria.
(b) Sample was not preserved to a pH < 2; reported results are considered minimum values.
8 of 61
FA22769
2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
9 of 61
FA22769
3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA22769-1 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193062.D 1 03/19/15 TD n/a n/a VA1662
Run #2 a A0193073.D 5 03/19/15 TD n/a n/a VA1663
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 24.4 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 1.7 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 1.2 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 61
FA22769
3
3
.
1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA22769-1 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.8 0.50 0.16 ug/l
100-41-4 Ethylbenzene 62.1 b 2.5 0.76 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 10.6 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.86 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.5 0.50 0.16 ug/l
91-20-3 Naphthalene 15.7 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 32.7 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 18.9 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 114 b 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 40.2 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 215 b 5.0 1.5 ug/l
95-47-6 o-Xylene 21.2 b 2.5 0.67 ug/l
1330-20-7 Xylene (total)237 b 7.5 2.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%117%70-130%
17060-07-0 1,2-Dichloroethane-D4 117%125%70-130%
2037-26-5 Toluene-D8 96%92%70-130%
460-00-4 4-Bromofluorobenzene 105%96%70-130%
(a) Internal standard areas outside method criteria.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 61
FA22769
3
3
.
1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA22769-2 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193079.D 1 03/19/15 TD n/a n/a VA1663
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 20.3 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 61
FA22769
3
3
.
2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA22769-2 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.52 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.99 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.2 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.23 0.50 0.16 ug/l J
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 3.0 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.43 0.50 0.14 ug/l J
108-67-8 1,3,5-Trimethylbenzene 0.18 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 2.6 1.0 0.30 ug/l
95-47-6 o-Xylene 0.62 0.50 0.13 ug/l
1330-20-7 Xylene (total)3.2 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 61
FA22769
3
3
.
2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA22769-3 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193111.D 1 03/20/15 TD n/a n/a VA1664
Run #2 A0193082.D 2 03/19/15 TD n/a n/a VA1663
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 70.9 a 1.0 0.34 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.29 0.50 0.14 ug/l J
135-98-8 sec-Butylbenzene 0.20 0.50 0.14 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 61
FA22769
3
3
.
3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA22769-3 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 26.6 0.50 0.16 ug/l
100-41-4 Ethylbenzene 16.8 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 1.2 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.17 0.50 0.12 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 41.4 0.50 0.16 ug/l
91-20-3 Naphthalene 2.3 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 3.5 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 1.7 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 9.2 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.6 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 9.1 1.0 0.30 ug/l
95-47-6 o-Xylene 1.4 0.50 0.13 ug/l
1330-20-7 Xylene (total)10.5 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%111%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%117%70-130%
2037-26-5 Toluene-D8 97%94%70-130%
460-00-4 4-Bromofluorobenzene 101%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 61
FA22769
3
3
.
3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA22769-4 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193083.D 1 03/19/15 TD n/a n/a VA1663
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 61
FA22769
3
3
.
4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA22769-4 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 61
FA22769
3
3
.
4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA22769-5 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193084.D 1 03/20/15 TD n/a n/a VA1663
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 61
FA22769
3
3
.
5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA22769-5 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 61
FA22769
3
3
.
5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA22769-6 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193112.D 1 03/20/15 TD n/a n/a VA1664
Run #2 A0193085.D 5 03/20/15 TD n/a n/a VA1663
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.4 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 3.0 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 2.3 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 61
FA22769
3
3
.
6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA22769-6 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 99.0 a 2.5 0.76 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 13.1 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.99 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.21 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 26.2 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 37.4 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 2.8 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 102 a 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 19.6 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 93.1 a 5.0 1.5 ug/l
95-47-6 o-Xylene 12.6 0.50 0.13 ug/l
1330-20-7 Xylene (total)102 a 7.5 2.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%124%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%133%70-130%
2037-26-5 Toluene-D8 99%91%70-130%
460-00-4 4-Bromofluorobenzene 117%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 61
FA22769
3
3
.
6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TW-1
Lab Sample ID:FA22769-7 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193086.D 1 03/20/15 TD n/a n/a VA1663
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 61
FA22769
3
3
.
7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TW-1
Lab Sample ID:FA22769-7 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.33 0.50 0.16 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.79 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 61
FA22769
3
3
.
7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA22769-8 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193116.D 25 03/20/15 TD n/a n/a VA1664
Run #2 A0193087.D 100 03/20/15 TD n/a n/a VA1663
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 384 13 4.3 ug/l
108-86-1 Bromobenzene ND 13 4.0 ug/l
74-97-5 Bromochloromethane ND 13 4.0 ug/l
75-27-4 Bromodichloromethane ND 13 3.7 ug/l
75-25-2 Bromoform ND 13 2.7 ug/l
104-51-8 n-Butylbenzene 29.3 13 3.6 ug/l
135-98-8 sec-Butylbenzene 17.5 13 3.5 ug/l
98-06-6 tert-Butylbenzene ND 13 3.6 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.8 ug/l
108-90-7 Chlorobenzene ND 13 4.0 ug/l
75-00-3 Chloroethane ND 13 5.2 ug/l
67-66-3 Chloroform ND 13 4.3 ug/l
95-49-8 o-Chlorotoluene ND 13 3.8 ug/l
106-43-4 p-Chlorotoluene ND 13 3.4 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.5 ug/l
75-71-8 Dichlorodifluoromethane ND 13 3.2 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.2 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.8 ug/l
75-34-3 1,1-Dichloroethane ND 13 4.5 ug/l
107-06-2 1,2-Dichloroethane ND 13 4.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 4.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 4.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 4.2 ug/l
78-87-5 1,2-Dichloropropane ND 13 4.3 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.7 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.0 ug/l
563-58-6 1,1-Dichloropropene ND 13 4.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.2 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 61
FA22769
3
3
.
8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA22769-8 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 13 4.0 ug/l
100-41-4 Ethylbenzene 1590 b 50 15 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 133 13 3.0 ug/l
99-87-6 p-Isopropyltoluene 7.5 13 3.1 ug/l J
74-83-9 Methyl Bromide ND 13 4.6 ug/l
74-87-3 Methyl Chloride ND 13 4.0 ug/l
74-95-3 Methylene Bromide ND 13 4.3 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.7 13 4.1 ug/l J
91-20-3 Naphthalene 537 13 3.1 ug/l
103-65-1 n-Propylbenzene 425 13 3.9 ug/l
100-42-5 Styrene ND 13 3.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.6 ug/l
127-18-4 Tetrachloroethylene ND 13 3.7 ug/l
108-88-3 Toluene 2210 b 50 17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.4 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 4.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.5 ug/l
79-01-6 Trichloroethylene ND 13 3.7 ug/l
75-69-4 Trichlorofluoromethane ND 13 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.2 ug/l
95-63-6 1,2,4-Trimethylbenzene 1420 b 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 415 13 3.4 ug/l
75-01-4 Vinyl Chloride ND 13 3.3 ug/l
m,p-Xylene 3620 b 100 30 ug/l
95-47-6 o-Xylene 938 b 50 13 ug/l
1330-20-7 Xylene (total)4560 b 150 43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%113%70-130%
2037-26-5 Toluene-D8 97%98%70-130%
460-00-4 4-Bromofluorobenzene 101%99%70-130%
(a) Internal standard areas outside method criteria.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 61
FA22769
3
3
.
8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA22769-9 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193088.D 1 03/20/15 TD n/a n/a VA1663
Run #2 A0193113.D 2 03/20/15 TD n/a n/a VA1664
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.2 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 0.16 0.50 0.14 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 61
FA22769
3
3
.
9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA22769-9 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 38.8 0.50 0.16 ug/l
100-41-4 Ethylbenzene 1.8 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.70 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 73.0 b 1.0 0.33 ug/l
91-20-3 Naphthalene 0.17 0.50 0.12 ug/l J
103-65-1 n-Propylbenzene 0.22 0.50 0.16 ug/l J
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.78 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.73 1.0 0.30 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND b 3.0 0.86 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%109%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%113%70-130%
2037-26-5 Toluene-D8 97%95%70-130%
460-00-4 4-Bromofluorobenzene 102%98%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 61
FA22769
3
3
.
9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA22769-10 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193117.D 1 03/20/15 TD n/a n/a VA1664
Run #2 b A0193177.D 1 03/23/15 TD n/a n/a VA1666
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 61
FA22769
3
3
.
1
0
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA22769-10 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 0.32 0.50 0.12 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%106%70-130%
2037-26-5 Toluene-D8 93%98%70-130%
460-00-4 4-Bromofluorobenzene 100%100%70-130%
(a) Internal standard areas outside method criteria.
(b) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 61
FA22769
3
3
.
1
0
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA22769-11 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193090.D 1 03/20/15 TD n/a n/a VA1663
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 61
FA22769
3
3
.
1
1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA22769-11 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 61
FA22769
3
3
.
1
1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA22769-12 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0193091.D 1 03/20/15 TD n/a n/a VA1663
Run #2 a A0193120.D 10 03/20/15 TD n/a n/a VA1664
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.92 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene 0.24 0.50 0.16 ug/l J
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 61
FA22769
3
3
.
1
2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA22769-12 Date Sampled:03/09/15
Matrix:AQ - Ground Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 51.8 b 5.0 1.6 ug/l
100-41-4 Ethylbenzene 0.33 0.50 0.15 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 230 b 5.0 1.6 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%111%70-130%
2037-26-5 Toluene-D8 97%98%70-130%
460-00-4 4-Bromofluorobenzene 101%100%70-130%
(a) Internal standard areas outside method criteria.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 61
FA22769
3
3
.
1
2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:STREAM
Lab Sample ID:FA22769-13 Date Sampled:03/09/15
Matrix:AQ - Surface Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193114.D 1 03/20/15 TD n/a n/a VA1664
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.47 0.50 0.17 ug/l J
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 61
FA22769
3
3
.
1
3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:STREAM
Lab Sample ID:FA22769-13 Date Sampled:03/09/15
Matrix:AQ - Surface Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.22 0.50 0.15 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.16 0.50 0.14 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.46 1.0 0.30 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)0.46 1.5 0.43 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 61
FA22769
3
3
.
1
3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA22769-14 Date Sampled:03/09/15
Matrix:AQ - Trip Blank Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193115.D 1 03/20/15 TD n/a n/a VA1664
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 61
FA22769
3
3
.
1
4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA22769-14 Date Sampled:03/09/15
Matrix:AQ - Trip Blank Water Date Received:03/12/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 61
FA22769
3
3
.
1
4
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
38 of 61
FA22769
4
FA22769: Chain of Custody
Page 1 of 4
39 of 61
FA22769
4
4
.
1
FA22769: Chain of Custody
Page 2 of 4
40 of 61
FA22769
4
4
.
1
FA22769: Chain of Custody
Page 3 of 4
41 of 61
FA22769
4
4
.
1
FA22769: Chain of Custody
Page 4 of 4
42 of 61
FA22769
4
4
.
1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
43 of 61
FA22769
5
Method Blank Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1662-MB A0193050.D 1 03/19/15 TD n/a n/a VA1662
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
44 of 61
FA22769
5
5
.
1
.
1
Method Blank Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1662-MB A0193050.D 1 03/19/15 TD n/a n/a VA1662
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1
CAS No.Compound Result RL MDL Units Q
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
45 of 61
FA22769
5
5
.
1
.
1
Method Blank Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1663-MB A0193071.D 1 03/19/15 TD n/a n/a VA1663
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1, FA22769-2, FA22769-3, FA22769-4, FA22769-5, FA22769-6, FA22769-7, FA22769-8, FA22769-9,
FA22769-11, FA22769-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
46 of 61
FA22769
5
5
.
1
.
2
Method Blank Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1663-MB A0193071.D 1 03/19/15 TD n/a n/a VA1663
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1, FA22769-2, FA22769-3, FA22769-4, FA22769-5, FA22769-6, FA22769-7, FA22769-8, FA22769-9,
FA22769-11, FA22769-12
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
47 of 61
FA22769
5
5
.
1
.
2
Method Blank Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1664-MB A0193103.D 1 03/20/15 TD n/a n/a VA1664
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-3, FA22769-6, FA22769-8, FA22769-9, FA22769-10, FA22769-12, FA22769-13, FA22769-14
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
48 of 61
FA22769
5
5
.
1
.
3
Method Blank Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1664-MB A0193103.D 1 03/20/15 TD n/a n/a VA1664
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-3, FA22769-6, FA22769-8, FA22769-9, FA22769-10, FA22769-12, FA22769-13, FA22769-14
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
49 of 61
FA22769
5
5
.
1
.
3
Blank Spike Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1662-BS A0193051.D 1 03/19/15 TD n/a n/a VA1662
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10 100 70-130
108-86-1 Bromobenzene 10 10 100 70-130
74-97-5 Bromochloromethane 10 9.2 92 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 9.4 94 70-130
104-51-8 n-Butylbenzene 10 10.2 102 70-130
135-98-8 sec-Butylbenzene 10 11.3 113 70-130
98-06-6 tert-Butylbenzene 10 11.0 110 70-130
56-23-5 Carbon Tetrachloride 10 10.7 107 70-130
108-90-7 Chlorobenzene 10 10.6 106 70-130
75-00-3 Chloroethane 10 13.7 137 60-140
67-66-3 Chloroform 10 10.2 102 70-130
95-49-8 o-Chlorotoluene 10 10.7 107 70-130
106-43-4 p-Chlorotoluene 10 10.9 109 70-130
124-48-1 Dibromochloromethane 10 9.8 98 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.8 88 70-130
106-93-4 1,2-Dibromoethane 10 9.8 98 70-130
75-71-8 Dichlorodifluoromethane 10 12.7 127 60-140
95-50-1 1,2-Dichlorobenzene 10 10.6 106 70-130
541-73-1 1,3-Dichlorobenzene 10 10.9 109 70-130
106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130
75-34-3 1,1-Dichloroethane 10 9.9 99 70-130
107-06-2 1,2-Dichloroethane 10 10.0 100 70-130
75-35-4 1,1-Dichloroethylene 10 10.6 106 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.1 101 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 10.0 100 70-130
142-28-9 1,3-Dichloropropane 10 9.8 98 70-130
594-20-7 2,2-Dichloropropane 10 10.4 104 70-130
563-58-6 1,1-Dichloropropene 10 10.9 109 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.6 96 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.2 102 70-130
108-20-3 Di-Isopropyl Ether 10 9.1 91 70-130
87-68-3 Hexachlorobutadiene 10 10.5 105 70-130
98-82-8 Isopropylbenzene 10 11.0 110 70-130
99-87-6 p-Isopropyltoluene 10 11.0 110 70-130
* = Outside of Control Limits.
50 of 61
FA22769
5
5
.
2
.
1
Blank Spike Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1662-BS A0193051.D 1 03/19/15 TD n/a n/a VA1662
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
74-83-9 Methyl Bromide 10 13.4 134 60-140
74-87-3 Methyl Chloride 10 13.0 130 60-140
74-95-3 Methylene Bromide 10 10 100 70-130
75-09-2 Methylene Chloride 10 9.2 92 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.3 93 70-130
91-20-3 Naphthalene 10 9.0 90 70-130
103-65-1 n-Propylbenzene 10 11.2 112 70-130
100-42-5 Styrene 10 9.6 96 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.2 102 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.4 94 70-130
127-18-4 Tetrachloroethylene 10 11.0 110 70-130
108-88-3 Toluene 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.5 95 70-130
71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130
79-00-5 1,1,2-Trichloroethane 10 9.8 98 70-130
79-01-6 Trichloroethylene 10 10.5 105 70-130
75-69-4 Trichlorofluoromethane 10 12.5 125 60-140
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.0 100 70-130
75-01-4 Vinyl Chloride 10 12.4 124 60-140
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
51 of 61
FA22769
5
5
.
2
.
1
Blank Spike Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1663-BS A0193072.D 1 03/19/15 TD n/a n/a VA1663
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1, FA22769-2, FA22769-3, FA22769-4, FA22769-5, FA22769-6, FA22769-7, FA22769-8, FA22769-9,
FA22769-11, FA22769-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.6 106 70-130
108-86-1 Bromobenzene 10 10.5 105 70-130
74-97-5 Bromochloromethane 10 9.8 98 70-130
75-27-4 Bromodichloromethane 10 11.2 112 70-130
75-25-2 Bromoform 10 9.8 98 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 11.7 117 70-130
98-06-6 tert-Butylbenzene 10 11.7 117 70-130
56-23-5 Carbon Tetrachloride 10 11.9 119 70-130
108-90-7 Chlorobenzene 10 11.2 112 70-130
75-00-3 Chloroethane 10 10.7 107 60-140
67-66-3 Chloroform 10 11.2 112 70-130
95-49-8 o-Chlorotoluene 10 11.3 113 70-130
106-43-4 p-Chlorotoluene 10 11.5 115 70-130
124-48-1 Dibromochloromethane 10 10.6 106 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
75-71-8 Dichlorodifluoromethane 10 11.2 112 60-140
95-50-1 1,2-Dichlorobenzene 10 11.2 112 70-130
541-73-1 1,3-Dichlorobenzene 10 11.4 114 70-130
106-46-7 1,4-Dichlorobenzene 10 10.4 104 70-130
75-34-3 1,1-Dichloroethane 10 10.6 106 70-130
107-06-2 1,2-Dichloroethane 10 11.4 114 70-130
75-35-4 1,1-Dichloroethylene 10 11.6 116 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.8 108 70-130
78-87-5 1,2-Dichloropropane 10 10.6 106 70-130
142-28-9 1,3-Dichloropropane 10 10.2 102 70-130
594-20-7 2,2-Dichloropropane 10 11.2 112 70-130
563-58-6 1,1-Dichloropropene 10 11.8 118 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.0 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.7 107 70-130
108-20-3 Di-Isopropyl Ether 10 9.8 98 70-130
100-41-4 Ethylbenzene 10 10.5 105 70-130
87-68-3 Hexachlorobutadiene 10 11.0 110 70-130
98-82-8 Isopropylbenzene 10 11.3 113 70-130
* = Outside of Control Limits.
52 of 61
FA22769
5
5
.
2
.
2
Blank Spike Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1663-BS A0193072.D 1 03/19/15 TD n/a n/a VA1663
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1, FA22769-2, FA22769-3, FA22769-4, FA22769-5, FA22769-6, FA22769-7, FA22769-8, FA22769-9,
FA22769-11, FA22769-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.4 114 70-130
74-83-9 Methyl Bromide 10 10.7 107 60-140
74-87-3 Methyl Chloride 10 11.8 118 60-140
74-95-3 Methylene Bromide 10 10.8 108 70-130
75-09-2 Methylene Chloride 10 10.2 102 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.8 98 70-130
91-20-3 Naphthalene 10 9.3 93 70-130
103-65-1 n-Propylbenzene 10 11.7 117 70-130
100-42-5 Styrene 10 9.8 98 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.0 110 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.8 98 70-130
127-18-4 Tetrachloroethylene 10 11.4 114 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.1 101 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 11.4 114 70-130
79-00-5 1,1,2-Trichloroethane 10 10.3 103 70-130
79-01-6 Trichloroethylene 10 11.5 115 70-130
75-69-4 Trichlorofluoromethane 10 11.3 113 60-140
96-18-4 1,2,3-Trichloropropane 10 10.4 104 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.2 102 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.5 105 70-130
75-01-4 Vinyl Chloride 10 10.5 105 60-140
m,p-Xylene 20 21.7 109 70-130
95-47-6 o-Xylene 10 11.1 111 70-130
1330-20-7 Xylene (total)30 32.8 109 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
53 of 61
FA22769
5
5
.
2
.
2
Blank Spike Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1664-BS A0193102.D 1 03/20/15 TD n/a n/a VA1664
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-3, FA22769-6, FA22769-8, FA22769-9, FA22769-10, FA22769-12, FA22769-13, FA22769-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 10.2 102 70-130
74-97-5 Bromochloromethane 10 9.5 95 70-130
75-27-4 Bromodichloromethane 10 10.5 105 70-130
75-25-2 Bromoform 10 9.8 98 70-130
104-51-8 n-Butylbenzene 10 10.2 102 70-130
135-98-8 sec-Butylbenzene 10 11.4 114 70-130
98-06-6 tert-Butylbenzene 10 11.2 112 70-130
56-23-5 Carbon Tetrachloride 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 10.8 108 70-130
75-00-3 Chloroethane 10 11.2 112 60-140
67-66-3 Chloroform 10 10.6 106 70-130
95-49-8 o-Chlorotoluene 10 11.0 110 70-130
106-43-4 p-Chlorotoluene 10 11.2 112 70-130
124-48-1 Dibromochloromethane 10 10.3 103 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.3 93 70-130
106-93-4 1,2-Dibromoethane 10 9.8 98 70-130
75-71-8 Dichlorodifluoromethane 10 11.1 111 60-140
95-50-1 1,2-Dichlorobenzene 10 10.7 107 70-130
541-73-1 1,3-Dichlorobenzene 10 11.0 110 70-130
106-46-7 1,4-Dichlorobenzene 10 10.0 100 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 10.5 105 70-130
75-35-4 1,1-Dichloroethylene 10 11.2 112 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.4 104 70-130
78-87-5 1,2-Dichloropropane 10 10.2 102 70-130
142-28-9 1,3-Dichloropropane 10 9.8 98 70-130
594-20-7 2,2-Dichloropropane 10 11.1 111 70-130
563-58-6 1,1-Dichloropropene 10 11.2 112 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.8 98 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.3 103 70-130
108-20-3 Di-Isopropyl Ether 10 9.5 95 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 10.9 109 70-130
98-82-8 Isopropylbenzene 10 10.9 109 70-130
* = Outside of Control Limits.
54 of 61
FA22769
5
5
.
2
.
3
Blank Spike Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1664-BS A0193102.D 1 03/20/15 TD n/a n/a VA1664
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-3, FA22769-6, FA22769-8, FA22769-9, FA22769-10, FA22769-12, FA22769-13, FA22769-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.0 110 70-130
74-83-9 Methyl Bromide 10 11.1 111 60-140
74-87-3 Methyl Chloride 10 11.6 116 60-140
74-95-3 Methylene Bromide 10 10.3 103 70-130
75-09-2 Methylene Chloride 10 9.7 97 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.4 94 70-130
91-20-3 Naphthalene 10 9.0 90 70-130
103-65-1 n-Propylbenzene 10 11.4 114 70-130
100-42-5 Styrene 10 9.5 95 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.3 103 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.7 97 70-130
127-18-4 Tetrachloroethylene 10 11.0 110 70-130
108-88-3 Toluene 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.8 98 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.8 98 70-130
71-55-6 1,1,1-Trichloroethane 10 10.8 108 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10.8 108 70-130
75-69-4 Trichlorofluoromethane 10 11.1 111 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.0 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.1 101 70-130
75-01-4 Vinyl Chloride 10 10.8 108 60-140
m,p-Xylene 20 21.0 105 70-130
95-47-6 o-Xylene 10 10.7 107 70-130
1330-20-7 Xylene (total)30 31.7 106 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
55 of 61
FA22769
5
5
.
2
.
3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22766-14MS A0193066.D 1 03/19/15 TD n/a n/a VA1662
FA22766-14MSD A0193067.D 1 03/19/15 TD n/a n/a VA1662
FA22766-14 A0193053.D 1 03/19/15 TD n/a n/a VA1662
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1
FA22766-14 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 9.2 92 10 8.4 84 9 70-130/20
108-86-1 Bromobenzene ND 10 9.2 92 10 8.2 82 11 70-130/20
74-97-5 Bromochloromethane ND 10 8.7 87 10 8.2 82 6 70-130/20
75-27-4 Bromodichloromethane ND 10 9.7 97 10 8.9 89 9 70-130/20
75-25-2 Bromoform ND 10 8.8 88 10 8.1 81 8 70-130/20
104-51-8 n-Butylbenzene ND 10 9.2 92 10 7.9 79 15 70-130/20
135-98-8 sec-Butylbenzene ND 10 10.2 102 10 8.9 89 14 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.1 101 10 8.9 89 13 70-130/20
56-23-5 Carbon Tetrachloride ND 10 10.5 105 10 9.4 94 11 70-130/20
108-90-7 Chlorobenzene ND 10 9.7 97 10 8.7 87 11 70-130/20
75-00-3 Chloroethane ND 10 7.2 72 10 6.4 64 12 60-140/20
67-66-3 Chloroform ND 10 9.8 98 10 9.0 90 9 70-130/20
95-49-8 o-Chlorotoluene ND 10 9.8 98 10 8.8 88 11 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.1 101 10 9.0 90 12 70-130/20
124-48-1 Dibromochloromethane ND 10 9.2 92 10 8.5 85 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.4 84 10 7.9 79 6 70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.0 90 10 8.3 83 8 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.0 80 10 7.1 71 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 9.7 97 10 8.9 89 9 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 10 100 10 8.9 89 12 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 9.1 91 10 8.2 82 10 70-130/20
75-34-3 1,1-Dichloroethane ND 10 9.3 93 10 8.5 85 9 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.7 97 10 9.2 92 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.2 102 10 9.2 92 10 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.5 95 10 8.6 86 10 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 9.5 95 10 8.5 85 11 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.3 93 10 8.6 86 8 70-130/20
142-28-9 1,3-Dichloropropane ND 10 8.9 89 10 8.3 83 7 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10 100 10 8.9 89 12 70-130/20
563-58-6 1,1-Dichloropropene ND 10 10.3 103 10 9.2 92 11 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.8 88 10 7.9 79 11 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 9.3 93 10 8.4 84 10 70-130/20
108-20-3 Di-Isopropyl Ether 0.20 J 10 8.8 86 10 8.2 80 7 70-130/20
87-68-3 Hexachlorobutadiene ND 10 9.4 94 10 8.2 82 14 70-130/20
98-82-8 Isopropylbenzene ND 10 9.8 98 10 8.8 88 11 70-130/20
99-87-6 p-Isopropyltoluene ND 10 9.8 98 10 8.7 87 12 70-130/20
* = Outside of Control Limits.
56 of 61
FA22769
5
5
.
3
.
1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22766-14MS A0193066.D 1 03/19/15 TD n/a n/a VA1662
FA22766-14MSD A0193067.D 1 03/19/15 TD n/a n/a VA1662
FA22766-14 A0193053.D 1 03/19/15 TD n/a n/a VA1662
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1
FA22766-14 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
74-83-9 Methyl Bromide ND 10 7.6 76 10 6.6 66 14 60-140/20
74-87-3 Methyl Chloride ND 10 8.4 84 10 7.5 75 11 60-140/20
74-95-3 Methylene Bromide ND 10 9.4 94 10 8.8 88 7 70-130/20
75-09-2 Methylene Chloride ND 10 8.8 88 10 8.2 82 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether 2.3 10 11.0 87 10 10.3 80 7 70-130/20
91-20-3 Naphthalene ND 10 8.4 84 10 7.5 75 11 70-130/20
103-65-1 n-Propylbenzene ND 10 10.2 102 10 8.9 89 14 70-130/20
100-42-5 Styrene ND 10 8.3 83 10 7.5 75 10 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.4 94 10 8.6 86 9 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 8.8 88 10 8.1 81 8 70-130/20
127-18-4 Tetrachloroethylene ND 10 9.9 99 10 8.7 87 13 70-130/20
108-88-3 Toluene ND 10 8.9 89 10 7.9 79 12 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.0 90 10 8.0 80 12 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 8.9 89 10 7.9 79 12 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.8 98 10 8.9 89 10 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.1 91 10 8.4 84 8 70-130/20
79-01-6 Trichloroethylene ND 10 9.8 98 10 8.8 88 11 70-130/20
75-69-4 Trichlorofluoromethane ND 10 7.5 75 10 6.6 66 13 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 9.1 91 10 8.2 82 10 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.0 90 10 8.0 80 12 70-130/20
75-01-4 Vinyl Chloride ND 10 7.5 75 10 6.5 65 14 60-140/20
CAS No.Surrogate Recoveries MS MSD FA22766-14 Limits
1868-53-7 Dibromofluoromethane 105%106%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%111%105%70-130%
2037-26-5 Toluene-D8 96%96%95%70-130%
460-00-4 4-Bromofluorobenzene 99%98%100%70-130%
* = Outside of Control Limits.
57 of 61
FA22769
5
5
.
3
.
1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22769-8MS A0193080.D 100 03/19/15 TD n/a n/a VA1663
FA22769-8MSD A0193081.D 100 03/19/15 TD n/a n/a VA1663
FA22769-8 A0193087.D 100 03/20/15 TD n/a n/a VA1663
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1, FA22769-2, FA22769-3, FA22769-4, FA22769-5, FA22769-6, FA22769-7, FA22769-8, FA22769-9,
FA22769-11, FA22769-12
FA22769-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 357 1000 1350 99 1000 1370 101 1 70-130/20
108-86-1 Bromobenzene ND 1000 976 98 1000 1010 101 3 70-130/20
74-97-5 Bromochloromethane ND 1000 945 95 1000 965 97 2 70-130/20
75-27-4 Bromodichloromethane ND 1000 1030 103 1000 1060 106 3 70-130/20
75-25-2 Bromoform ND 1000 788 79 1000 917 92 15 70-130/20
104-51-8 n-Butylbenzene 25.0 J 1000 994 97 1000 1050 103 5 70-130/20
135-98-8 sec-Butylbenzene 14.8 J 1000 1080 107 1000 1140 113 5 70-130/20
98-06-6 tert-Butylbenzene ND 1000 1080 108 1000 1130 113 5 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 1110 111 1000 1130 113 2 70-130/20
108-90-7 Chlorobenzene ND 1000 1040 104 1000 1050 105 1 70-130/20
75-00-3 Chloroethane ND 1000 892 89 1000 879 88 1 60-140/20
67-66-3 Chloroform ND 1000 1070 107 1000 1070 107 0 70-130/20
95-49-8 o-Chlorotoluene ND 1000 1100 110 1000 1140 114 4 70-130/20
106-43-4 p-Chlorotoluene ND 1000 1080 108 1000 1120 112 4 70-130/20
124-48-1 Dibromochloromethane ND 1000 916 92 1000 985 99 7 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 1050 105 1000 1070 107 2 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 984 98 1000 1010 101 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 937 94 1000 959 96 2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 1050 105 1000 1080 108 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 1070 107 1000 1110 111 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 968 97 1000 1010 101 4 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1020 102 1000 1040 104 2 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 1080 108 1000 1100 110 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1100 110 1000 1110 111 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 1020 102 1000 1040 104 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 1030 103 1000 1040 104 1 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 1010 101 1000 1040 104 3 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 974 97 1000 988 99 1 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 952 95 1000 943 94 1 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1090 109 1000 1100 110 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 937 94 1000 952 95 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 1010 101 1000 1020 102 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 936 94 1000 972 97 4 70-130/20
100-41-4 Ethylbenzene 1590 1000 2560 97 1000 2600 101 2 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 997 100 1000 1040 104 4 70-130/20
98-82-8 Isopropylbenzene 111 1000 1190 108 1000 1200 109 1 70-130/20
* = Outside of Control Limits.
58 of 61
FA22769
5
5
.
3
.
2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22769-8MS A0193080.D 100 03/19/15 TD n/a n/a VA1663
FA22769-8MSD A0193081.D 100 03/19/15 TD n/a n/a VA1663
FA22769-8 A0193087.D 100 03/20/15 TD n/a n/a VA1663
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-1, FA22769-2, FA22769-3, FA22769-4, FA22769-5, FA22769-6, FA22769-7, FA22769-8, FA22769-9,
FA22769-11, FA22769-12
FA22769-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 1000 1050 105 1000 1100 110 5 70-130/20
74-83-9 Methyl Bromide ND 1000 887 89 1000 921 92 4 60-140/20
74-87-3 Methyl Chloride ND 1000 981 98 1000 1010 101 3 60-140/20
74-95-3 Methylene Bromide ND 1000 1050 105 1000 1050 105 0 70-130/20
75-09-2 Methylene Chloride ND 1000 997 100 1000 1010 101 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 1000 941 94 1000 969 97 3 70-130/20
91-20-3 Naphthalene 455 1000 1400 95 1000 1460 101 4 70-130/20
103-65-1 n-Propylbenzene 360 1000 1440 108 1000 1510 115 5 70-130/20
100-42-5 Styrene ND 1000 937 94 1000 959 96 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 1030 103 1000 1050 105 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 971 97 1000 985 99 1 70-130/20
127-18-4 Tetrachloroethylene ND 1000 1060 106 1000 1060 106 0 70-130/20
108-88-3 Toluene 2210 1000 3140 93 1000 3180 97 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 941 94 1000 997 100 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 950 95 1000 1000 100 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 1060 106 1000 1090 109 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 1020 102 1000 1040 104 2 70-130/20
79-01-6 Trichloroethylene ND 1000 1050 105 1000 1050 105 0 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 919 92 1000 912 91 1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 993 99 1000 1010 101 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1420 1000 2390 97 1000 2480 106 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 356 1000 1340 98 1000 1400 104 4 70-130/20
75-01-4 Vinyl Chloride ND 1000 877 88 1000 894 89 2 60-140/20
m,p-Xylene 3620 2000 5570 98 2000 5650 102 1 70-130/20
95-47-6 o-Xylene 938 1000 2020 108 1000 2050 111 1 70-130/20
1330-20-7 Xylene (total)4560 3000 7590 101 3000 7700 105 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA22769-8 Limits
1868-53-7 Dibromofluoromethane 107%107%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%108%113%70-130%
2037-26-5 Toluene-D8 98%98%98%70-130%
460-00-4 4-Bromofluorobenzene 98%101%99%70-130%
* = Outside of Control Limits.
59 of 61
FA22769
5
5
.
3
.
2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22767-6MS A0193123.D 1 03/20/15 TD n/a n/a VA1664
FA22767-6MSD A0193124.D 1 03/20/15 TD n/a n/a VA1664
FA22767-6 A0193104.D 1 03/20/15 TD n/a n/a VA1664
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-3, FA22769-6, FA22769-8, FA22769-9, FA22769-10, FA22769-12, FA22769-13, FA22769-14
FA22767-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.7 107 10 10.5 105 2 70-130/20
108-86-1 Bromobenzene ND 10 10.5 105 10 10.4 104 1 70-130/20
74-97-5 Bromochloromethane ND 10 10.2 102 10 10 100 2 70-130/20
75-27-4 Bromodichloromethane ND 10 11.6 116 10 9.9 99 16 70-130/20
75-25-2 Bromoform ND 10 9.9 99 10 7.9 79 22*70-130/20
104-51-8 n-Butylbenzene ND 10 10.5 105 10 10.6 106 1 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.7 117 10 11.7 117 0 70-130/20
98-06-6 tert-Butylbenzene ND 10 11.6 116 10 11.7 117 1 70-130/20
56-23-5 Carbon Tetrachloride ND 10 12.5 125 10 10.9 109 14 70-130/20
108-90-7 Chlorobenzene ND 10 11.3 113 10 11.1 111 2 70-130/20
75-00-3 Chloroethane ND 10 10.7 107 10 10.3 103 4 60-140/20
67-66-3 Chloroform ND 10 11.6 116 10 11.4 114 2 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.4 114 10 11.3 113 1 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.7 117 10 11.5 115 2 70-130/20
124-48-1 Dibromochloromethane ND 10 11.0 110 10 8.9 89 21*70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 10.2 102 10 10.0 100 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.4 104 10 10.2 102 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 11.0 110 10 10.9 109 1 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 11.2 112 10 11.1 111 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 11.7 117 10 11.4 114 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10.6 106 10 10.5 105 1 70-130/20
75-34-3 1,1-Dichloroethane ND 10 11.1 111 10 11.0 110 1 70-130/20
107-06-2 1,2-Dichloroethane ND 10 11.6 116 10 11.4 114 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 12.0 120 10 12.2 122 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 11.0 110 10 10.8 108 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 11.3 113 10 10.9 109 4 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.9 109 10 10.6 106 3 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.4 104 10 10.1 101 3 70-130/20
594-20-7 2,2-Dichloropropane ND 10 11.9 119 10 11.6 116 3 70-130/20
563-58-6 1,1-Dichloropropene ND 10 12.0 120 10 11.6 116 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.1 101 10 8.2 82 21*70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10.9 109 10 8.9 89 20 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 10.1 101 10 10.1 101 0 70-130/20
100-41-4 Ethylbenzene ND 10 10.7 107 10 10.6 106 1 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.2 102 10 10.1 101 1 70-130/20
98-82-8 Isopropylbenzene ND 10 11.4 114 10 11.3 113 1 70-130/20
* = Outside of Control Limits.
60 of 61
FA22769
5
5
.
3
.
3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA22769
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22767-6MS A0193123.D 1 03/20/15 TD n/a n/a VA1664
FA22767-6MSD A0193124.D 1 03/20/15 TD n/a n/a VA1664
FA22767-6 A0193104.D 1 03/20/15 TD n/a n/a VA1664
The QC reported here applies to the following samples:Method: SM 6200B
FA22769-3, FA22769-6, FA22769-8, FA22769-9, FA22769-10, FA22769-12, FA22769-13, FA22769-14
FA22767-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 11.4 114 10 11.4 114 0 70-130/20
74-83-9 Methyl Bromide ND 10 10.9 109 10 10.3 103 6 60-140/20
74-87-3 Methyl Chloride ND 10 11.7 117 10 11.3 113 3 60-140/20
74-95-3 Methylene Bromide ND 10 11.4 114 10 11.1 111 3 70-130/20
75-09-2 Methylene Chloride ND 10 10.7 107 10 10.4 104 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.49 J 10 10.6 101 10 10.6 101 0 70-130/20
91-20-3 Naphthalene ND 10 9.4 94 10 9.4 94 0 70-130/20
103-65-1 n-Propylbenzene ND 10 11.7 117 10 11.6 116 1 70-130/20
100-42-5 Styrene ND 10 9.7 97 10 9.0 90 7 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 11.1 111 10 10.6 106 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.1 101 10 10.1 101 0 70-130/20
127-18-4 Tetrachloroethylene ND 10 11.0 110 10 10.7 107 3 70-130/20
108-88-3 Toluene ND 10 10.2 102 10 10.2 102 0 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10.2 102 10 10.4 104 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.1 101 10 10.2 102 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.9 119 10 11.6 116 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.7 107 10 10.4 104 3 70-130/20
79-01-6 Trichloroethylene ND 10 11.5 115 10 11.1 111 4 70-130/20
75-69-4 Trichlorofluoromethane ND 10 11.0 110 10 10.7 107 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 10.6 106 10 10.4 104 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 10.3 103 10 10.3 103 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.4 104 10 10.5 105 1 70-130/20
75-01-4 Vinyl Chloride ND 10 10.3 103 10 10.2 102 1 60-140/20
m,p-Xylene ND 20 21.9 110 20 21.6 108 1 70-130/20
95-47-6 o-Xylene ND 10 11.2 112 10 11.1 111 1 70-130/20
1330-20-7 Xylene (total)ND 30 33.1 110 30 32.7 109 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA22767-6 Limits
1868-53-7 Dibromofluoromethane 110%107%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%109%109%70-130%
2037-26-5 Toluene-D8 96%97%98%70-130%
460-00-4 4-Bromofluorobenzene 100%98%100%70-130%
* = Outside of Control Limits.
61 of 61
FA22769
5
5
.
3
.
3