0803_EastCarolina_20160727_GWMonReport_DIN27219

PREPARED FOR:
REPUBLIC SERVICES OF NORTH CAROLINA, LLC
D.B.A. EAST CAROLINA ENVIRONMENTAL
1922 REPUBLICAN ROAD
AULANDER, NORTH CAROLINA 27805

EAST CAROLINA REGIONAL LANDFILL
PERMIT NO. 08-03

SECOND SEMIANNUAL WATER QUALITY
MONITORING REPORT OF 2016

SEPTEMBER 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE ENGINEERING PROJECT NO. 00894.1601.12

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Second Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
East Carolina Regional Landfill, Permit No. 08-03 September 2016

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EXECUTIVE SUMMARY

This report presents the results of the second semiannual water quality monitoring event
conducted at the East Carolina Regional Landfill on July 27, 2016. Samples were collected by
representatives of Joyce Engineering from groundwater monitoring wells, surface water
monitoring points, and the leachate collection system on July 27th, 2016. The complete analytical
results from the second semiannual 2016 monitoring event have been reported by Analytical
Services, Inc. of Norcross, Georgia laboratory certification number 381.

Four inorganic constituents (barium, beryllium, cobalt, and zinc) were detected in samples from
one or more groundwater or surface water monitoring points at concentrations above their
respective Solid Waste Section (SWS) Reporting Limits (SWSLs). Barium was detected above
the SWSL in GW-2, GW-8, GW-9, GW-10, GW-13, GW-15, GW-16R, GW-17, and GW-18.
Beryllium and cobalt were detected above the SWSL in GW-7. Zinc was detected above the
SWSL in GW-9, GW-10 and PW-1. No other inorganic or organic constituents were detected
above their respective SWSLs in monitoring wells or surface water monitoring points during the
July 2016 sampling event.

One inorganic constituent (cobalt) was detected at a concentration above the Solid Waste Section
Groundwater Protection Standard (GWPS). Cobalt was detected above its SWS Groundwater
Protection Standard (GWPS) in monitoring well GW-7 at 37.4 µg/l. The cobalt detection in
GW-7 was not a statistically significant increase (SSI) above background; therefore, we request
that the background (50.7 µg/l) can be considered the Groundwater Protection Standard (GPS)
for cobalt in accordance with 15A NCAC 13B.1634.(g).(5).

No inorganic or organic constituents were detected in surface water samples at quantified
concentrations above applicable NC2B standards.

Based on the results summarized herein, Republic Services of NC, LLC, will continue
monitoring the uppermost aquifer beneath the East Carolina Regional Landfill in accordance
with the requirements for Detection Monitoring Program as outlined in Title 15A NCAC 13B
.1633.

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Second Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
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Second Semiannual Water Quality Monitoring Report of 2016
East Carolina Regional Landfill, Permit No. 08-03
Bertie County, North Carolina

TABLE OF CONTENTS

EXECUTIVE SUMMARY ........................................................................................................... i
1.0 INTRODUCTION..............................................................................................................1
1.1 Site Description and Background ................................................................................ 1
1.2 Compliance Monitoring History .................................................................................. 1
1.3 Hydrogeologic Setting ................................................................................................... 2
2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION ......................3
2.1 Visual Inspection Program........................................................................................... 3
2.2 Well Network and Groundwater Elevation Measurements ..................................... 4
2.3 July 2016 Monitoring Event ......................................................................................... 4
2.4 Laboratory Analysis Program ..................................................................................... 5
2.5 July 2016 Sampling Results ......................................................................................... 5
3.0 LABORATORY AND FIELD QA/QC ............................................................................6
4.0 DATA EVALUATION ......................................................................................................6
4.1 Comparisons to Groundwater and Surface Water Standards ................................. 6
4.2 Statistical Evaluations .................................................................................................. 7
5.0 CONCLUSIONS ................................................................................................................8
6.0 REFERENCES ...................................................................................................................8

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TABLE OF CONTENTS
(CONTINUED)

Tables

Table 1 Historical Groundwater Elevations for the Yorktown Formation
Table 2 Historical Groundwater Elevations for the Black Creek Formation
Table 3 Estimated Hydraulic Gradients and Linear Groundwater Velocities
Table 4 Well Construction Information
Table 5 Quantified Detections by Monitoring Locations
Table 6 Exceedances of Groundwater Standards
Table 7 Field Parameters by Location

Drawing

Drawing 1 Potentiometric Surface Map, July 27, 2016

Appendices

Appendix A Historical Tables
Table 8 Historical Constituents/Analytes in Groundwater
Table 9 Historical Constituents/Analytes in Surface Water
Table 10 Historical Constituents/Analytes in Leachate
Appendix B Groundwater and Surface Water Field Data Logs
Appendix C Laboratory Analytical Reports
Appendix D Statistical Analyses Worksheets and Summary Table

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Second Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
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1.0 INTRODUCTION
This report summarizes the monitoring results from the July 27, 2016, water quality monitoring
event at the East Carolina Regional Landfill in Bertie County, North Carolina, in accordance
with Title 15A of the North Carolina Administrative Code (NCAC) Subchapter 13B .1632. The
East Carolina Regional Landfill, which is an active municipal solid waste landfill, is owned and
operated by Republic Services of North Carolina, LLC (Republic) under Permit No. 08-03,
issued by the North Carolina Department of Environmental and Quality (NCDEQ).

1.1 Site Description and Background
The East Carolina Regional Landfill is an active Subtitle D municipal solid waste landfill that
began operating in 1993. The location of the facility is shown on the inlay on Drawing 1. The
East Carolina Regional Landfill is located approximately 7.5 miles northwest of Windsor, NC at
the intersection of State Routes 1221 and 1225. The facility is bounded to the north and east by
undeveloped property and the Connaritsa Swamp, to the west by State Route 1225 and
undeveloped and agricultural property, and to the south by State Route 1221, wooded property,
and undeveloped bottomlands associated with the easterly flowing Cashie River.

Topographic elevations at the facility range from approximately 30 to 70 feet above mean sea
level. Along the northern and eastern portions of the facility, surface drainage from the facility
and surrounding areas is routed by drainage channels and stormwater control structures to
tributaries of the southerly-flowing Connaritsa Swamp, a tributary system of the Cashie River.
Along the western and southern portions of the facility, surface drainage from the facility and
surrounding areas is routed by drainage channels and stormwater control structures to tributaries
of the southeasterly flowing Cashie River. The Cashie River discharges to the Roanoke River
south of the Town of Windsor.

1.2 Compliance Monitoring History
Groundwater monitoring at the facility was initiated in January 1995 under the Detection
Monitoring Program for municipal solid waste landfills. The facility’s monitoring network
historically consisted of 14 monitoring wells (GW-1 through GW-14), which monitored the
uppermost Yorktown Formation (GW-2, GW-3, GW-5, GW-7 through GW-11, GW-13, and
GW-14) and the lower Black Creek Formation (GW-1, GW-4, GW-6, and GW-12). Monitoring
wells GW-1 and GW-2 were considered upgradient background wells and the remaining wells
were considered to be downgradient or side-gradient compliance wells. Well GW-16 was
decommissioned following the January 2007 sampling event during the construction of Cell 12.
Bunnell Lammons Engineering, Inc. (BLE) installed monitoring well GW-16R as a replacement
well prior to the January 2008 monitoring event. BLE installed GW-17 following the January
2008 sampling event as an additional monitoring well during the construction of Cell 12.
Monitoring well GW-14 was decommissioned and GW-18 was installed March 22, 2009, in
order to construct Cell 13. Piezometer PZ-110 was installed May 17, 2005, to monitoring well

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specifications. On June 3, 2009, PZ-110 was converted into a monitoring well and was renamed
GW-21. A background sampling event for GW-18 and GW-21 was performed during the
January 2009 monitoring event. Cell 13 began receiving waste in the first quarter of 2014 and
wells GW-18 and GW-21 became part of the compliance network with the July 2014 sampling
event. Due to damage, GW-11 was abandoned and replaced with GW-11R on July 21, 2014.

In accordance with the facility’s permit, the current compliance monitoring network monitors the
Yorktown formation and is composed of GW-2 (background), GW-7, GW-8, GW-9, GW-10,
GW-11R, GW-13, GW-15, GW-16R, GW-17, GW-18, and GW-21, with the remaining
monitoring wells used for static water level observation. Per the June 2005 revision to the Water
Monitoring Procedures (BLE, 2005), the groundwater wells screened in the Black Creek
Formation are no longer sampled.

In addition to the routine groundwater monitoring points, the facility’s monitoring network
includes one upstream surface water monitoring point (SW-1), and three downstream surface
water sampling points (SW-2, SW-3, and SW-4), which are sampled in conjunction with the
groundwater monitoring wells. Water supply well PW-1 is sampled during each routine
monitoring event. The leachate is also sampled semiannually per the Solid Waste Section
requirements.

1.3 Hydrogeologic Setting
Geologically, the facility is located within the Carolina Coastal Plain Physiographic Province
(NCGS, 1985). The Coastal Plain Province is composed of easterly-dipping sedimentary strata
that thicken towards the east. Based on hydrogeologic characteristics, these strata are generally
classified as aquifer systems separated by aquitard units. The strata underlying the facility
include the Tertiary Yorktown Formation and the Cretaceous Black Creek Formation, both of
which are classified as aquifers. The Yorktown Formation is unconfined at this location, and the
lower Black Creek Formation, which is separated from the overlying Yorktown Formation by a
low permeability unit, is confined.

The uppermost groundwater beneath the facility is present in the shallow, unconfined Yorktown
Aquifer. Depending on topographic elevation, the depth to water in the Yorktown Formation
ranges from approximately 5 feet below grade along the southwestern perimeter of the facility to
approximately 25 feet below grade near the central and northeastern portion of the facility. In the
lower Black Creek Formation, the depth to water ranges from 10 to 20 feet below grade in the
monitoring wells screened in this unit. Historical static water level data are presented in Tables 1
and 2.

As presented in Table 1, the water level in the uppermost Yorktown aquifer beneath the facility
is fairly consistent, with temporal variation from the long-term average limited to approximately
four-five feet in the upgradient wells and three-four feet in the downgradient wells. Similarly, as
presented in Table 2, the fluctuation in the Black Creek aquifer is limited to approximately three

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feet from the average. As expected, the range in fluctuation appears to be greater in the
upgradient wells, as these wells are more centrally located to the regional groundwater recharge
area. The range in fluctuation in the downgradient compliance wells, which are generally located
near groundwater discharge areas, is less likely due to the stabilizing effect of hydraulic
discharge boundaries.

Static water level measurements obtained during the July 27, 2016, sampling event were used to
prepare the groundwater surface contours presented on Drawing 1. In the upper Yorktown
Formation, groundwater flow across most of the site is toward the south-southwest. This is
consistent with previously submitted interpretations for this facility. Previous maps of the Black
Creek Formation show an apparent flow direction towards the southeast.

Based on the July 27, 2016, potentiometric surface map, the hydraulic gradient in the uppermost
aquifer underlying the site, as measured along the conceptual flow paths shown on the contour
map, was calculated to be approximately 0.0031 to 0.0053 ft/ft (Table 3). The estimated rate of
groundwater flow for the uppermost aquifer beneath the facility was calculated using the
following modified Darcy equation:

Vgw = Ki/ne

Where Vgw = average linear velocity (feet per day), K = hydraulic conductivity (feet per day),
i = horizontal hydraulic gradient, and ne = effective porosity.

The estimated linear groundwater flow velocity under the waste management unit is
approximately 3.98 to 6.74 ft/year, generally to the southwest (Table 3). The linear velocity
equation and resultant rates are based on the simplifying assumptions of a homogeneous and
isotropic aquifer, and may not be accurate when applied to heterogeneous and/or anisotropic
conditions.

2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION
2.1 Visual Inspection Program
In order to detect potential releases of leachate and/or landfill gas migration in a timely manner,
a visual inspection program has been implemented at the East Carolina Regional Landfill. This
inspection program involves field personnel making the following observations:

 Observation of stress induced on the biological community (i.e., dead or dying vegetation);
 Indications of leachate impact (i.e., seeps, impacted surface water);
 Observations of erosion; and
 Negative changes around the waste facility.

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During the July 2016 monitoring event, no physical indications of impacts were observed in the
vicinity of the waste management areas.

2.2 Well Network and Groundwater Elevation Measurements
Monitoring well GW-2 is the facility’s background well and monitoring wells GW-7, GW-8,
GW-9, GW-10, GW-11R, GW-13, GW-15, GW-16R, GW-17, GW-18, and GW-21 are the
facility’s compliance wells. These wells are all screened within the upper Yorktown Formation.
The remaining monitoring wells are screened in the deeper Black Creek Formation and are used
as observation wells to monitor the depth to groundwater. Monitoring well construction
information is summarized in Table 4 and the well locations are shown on Drawing 1. The
network of monitoring wells was constructed to intercept the flow path for groundwater in the
uppermost aquifer underlying the waste disposal areas.

Depth-to-water measurements were recorded to the nearest 0.01 foot prior to initiating
groundwater purging and sampling activities. The groundwater elevations for this event, as well
as historical groundwater elevations for the Yorktown Formation wells and Black Creek
Formation wells are presented in Tables 1 and 2, respectively.

2.3 July 2016 Monitoring Event
Personnel from Joyce Engineering visited the facility on July 27, 2016, to purge and sample
monitoring wells GW-2, GW-7, GW-8, GW-9, GW-10, GW-11R, GW-13, GW-15, GW-16R,
GW-17, GW-18, and GW-21. In addition to the groundwater samples from the monitoring wells,
a groundwater sample was collected from the on-site water supply well (PW-1) and a leachate
sample was collected from the facility’s holding tank (Tank B). Additional depth-to-water
measurements were obtained from GW-1, GW-4, GW-5, GW-6 and GW-12. Surface water
samples were collected from two downstream monitoring points, SW-2 and SW-3. SW-1 and
SW-4 were dry and were not sampled during the July 2016 monitoring event.

Monitoring wells GW-2, GW-7, GW-8, GW-9, GW-10, GW-11R, GW-13, GW-15, GW-16R,
GW-17, GW-18, and GW-21 were purged with dedicated bladder pumps using micropurge
procedures pursuant to the facility’s approved monitoring plan. Measurements of pH, specific
conductance, dissolved oxygen, oxidation-reduction potential, temperature, and turbidity were
recorded after each system volume collected during the purge with field-calibrated instruments to
monitor for stabilization of water quality. Field parameters from the July 2016 event are
presented in Table 7.

Prior to sampling, the laboratory-supplied sample containers were prepared. Each sample
container was labeled with the sample identification number, sampling personnel, date and time
of sample collection, project name and number, and requested chemical analyses.

The required groundwater samples were collected directly from the dedicated bladder pump
discharge lines in the labeled, laboratory-supplied, pre-preserved sample containers after purging

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was completed based on stabilization of all field parameters. The on-site supply well was purged
for 15 minutes by the spigot prior to sample collection. The supply well sample was then
collected directly from the spigot.

The surface water sample was collected directly from the stream flow, by lowering the sample
containers into the stream flow, taking care to prevent the overflow of the sample containers and
to minimize sample induced turbidity. Measurements of temperature, pH, specific conductivity,
and turbidity were recorded during the collection of the surface water samples.

The leachate sample was collected directly from the leachate piping manifold that serves the
leachate holding tank (Tank B). Measurements of temperature, pH, specific conductivity, and
turbidity were recorded during the collection of the leachate sample.

After collection, the samples were placed in a cooler on ice, under chain-of-custody control.
Copies of the sampling logs are presented in Appendix B. Included in each log is a description
of the sampling location, sampling equipment, sampling method, field observations, and field
parameters.

2.4 Laboratory Analysis Program
The July 27, 2016, groundwater, surface water, and leachate samples were submitted to Pace
Analytical Laboratories Inc. (formerly Analytical Services, Inc. of Norcross, Georgia under
chain-of-custody control for analysis. The groundwater and surface water, including the Field
Blank, were analyzed for North Carolina Appendix I constituents. The leachate sample was
analyzed for NC Appendix I constituents, mercury, biochemical oxygen demand, chemical
oxygen demand, cyanide, nitrate as N, nitrate/nitrite as N, nitrite as N, phosphorous, sulfate, total
kjeldahl nitrogen, total suspended solids, phenolics, and oil & grease. The Trip Blank was
analyzed for North Carolina Appendix I organic constituents only. Joyce Engineering requested
a Level II data report for the final laboratory report. The samples were kept on ice and received
by the laboratory on July 28, 2016 in good condition, properly preserved, and within analysis
hold times.

2.5 July 2016 Sampling Results
Constituents detected at quantified concentrations above the SWSL for the July 27, 2016,
samples are summarized in Table 5, and exceedances of groundwater standards for the event are
summarized in Table 6. Historical analytical data for groundwater, surface water, and leachate
are summarized in Appendix A. The laboratory’s certificates-of-analysis and chains-of-custody
for this monitoring event and the resampling event are included in Appendix C.

Cobalt was detected above its Solid Waste Section Groundwater Protection Standard (GWPS) in
monitoring well GW-7. Four inorganic constituents (barium, beryllium, cobalt, and zinc) were
detected at concentrations above their respective SWSLs in monitoring wells, but Cobalt was the

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only constituent exceeding its respective 15A NCAC 2L.0202 Groundwater Protection Standards
(NC2L) or GWPS.

No other inorganic or organic constituents were detected above their respective SWSLs in
monitoring wells or surface water monitoring points during the July 2016 monitoring event.

There were no detections above the SWSL or exceedances of NC2B surface water standards in
the surface water samples collected during the July 2016 sampling event. The constituent
concentrations reported for the leachate samples collected during the July 2016 monitoring event
are generally consistent with historical data.

3.0 LABORATORY AND FIELD QA/QC
A Field blank was collected by Joyce Engineering as part of the July 27, 2016, monitoring event.
In addition to the field blank, laboratory-prepared a trip blank accompanied the volatile sample
containers for the sampling event to and from the laboratory. The field blank was analyzed for
NC Appendix I constituents and the trip blank for NC Appendix I VOCs only. In addition to the
field and trip blank, at least one method blank was analyzed by the laboratory for each method
used.

Upon receipt of the laboratory data package, the data was reviewed by Joyce Engineering for the
following:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Correct reporting limits;
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate,
and Laboratory Control Samples;
 Blank qualified data (B-flags);
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.

4.0 DATA EVALUATION
4.1 Comparisons to Groundwater and Surface Water Standards
Cobalt was detected above its GWPS in monitoring well GW-7 at 37.4 µg/L. Note that the
GWPS for cobalt is 1 µg/L but the SWSL for cobalt in 10 µg/L. Since the SWSL is higher than
the GWPS, and since only quantified detections above the SWSL are considered by the NCDEQ,
the SWSL is the effective standard for comparison. The cobalt detection in GW-7 was
statistically evaluated in accordance with the procedures outlined in 15A NCAC 13B.1632 (g)
and (h) to determine whether the reported concentrations exceeded the facility background

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concentration (see Section 4.2). The cobalt detection in GW-7 was not identified as a
statistically significant increase (SSI) above background according to intrawell statistical
analyses for the monitoring location; therefore, we request that the SWS approve using the
background as the Groundwater Protection Standard (GPS) in accordance with 15A NCAC
13B.1634.(g).(5).

4.2 Statistical Evaluations
The facility background data were evaluated through the use of the Shapiro-Wilkes Test,
Parametric Prediction Limits, Parametric Tolerance Intervals, Aitchison’s Adjustment, Non-
parametric Prediction Limits, and Poisson Prediction Limits, as appropriate. Background data,
tests for normality, outliers, Aitchison’s adjustment, tolerance interval, or prediction limits are
used, as appropriate based on the background data.

The statistical test by which downgradient data are compared to facility background data is based
upon the nature of the data and the number of data values that are less than the laboratory limit of
detection. All statistical tests are evaluated at the 0.05 level of significance, 95% confidence
level, and are conducted as one-tailed tests.

The data from the facility background well, GW-2, from October 1998 through July 2016 were
used for interwell statistical analyses. For intrawell statistical analyses, the data from the well in
question, excluding the most recent eight sampling events, were used in the evaluation.

Cobalt was detected above its SWSL and GWPS in the sample from the downgradient
monitoring well GW-7 during the July 2016 sampling event. Cobalt has often been detected in
the facility’s upgradient background well, GW-2, at concentrations above the SWSL; although
the GW-2 result from the July 2016 event were below the SWSL.

The cobalt detection in GW-7 was statistically evaluated in accordance with the procedures
outlined in 15A NCAC 13B.1632 (g) and (h) to determine if the reported concentrations
exceeded the facility background concentrations. The interwell statistical background calculated
based on historical cobalt concentrations from GW-2 between October 1998 and July 2016 is
17.4 µg/L. In the case of GW-7, cobalt has historically and consistently been detected at
concentrations above 17.4 µg/L, suggesting a different geochemistry for the monitoring area of
GW-7 and the need to perform intrawell statistical evaluation based on the specific background
history of GW-7 itself. For the intrawell statistics, the background data consisted of the
historical cobalt concentrations from MW-7 from October 1998 through July 2012 (i.e.,
excluding the last eight sampling events). The intrawell statistical background for GW-7 was
50.7 µg/L. Based on the statistical evaluations, the detections of cobalt are not identified as SSIs
above background and are representative of historical background concentrations. A summary
table and statistical worksheets are presented in Appendix D.

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5.0 CONCLUSIONS
Based on the results summarized herein, Republic Services of NC, LLC will continue monitoring
the uppermost aquifer beneath the East Carolina Regional Landfill in accordance with the
requirements for Detection Monitoring Program as outlined in Title 15A NCAC 13B .1633.
The next compliance monitoring event for this facility is tentatively scheduled for January 2017.

6.0 REFERENCES
BLE (Bunnell-Lammons Engineering, Inc.), December 2004. Report of Ground Water Quality
Results & Statistical Analysis, Second Semi-Annual Sampling Event of 2004 (N27) East Carolina
Regional MSW Landfill, Bertie County, North Carolina. 5 pp.

BLE (Bunnell-Lammons Engineering, Inc.), 2005. Water Monitoring Procedures, June 2005
Revision.

Law Engineering, August 1996. Design Hydrogeologic Report Phase II (Cells 7 and 8). 15 pp.

Golder Associates NC, Inc., August, 2011. Second Semi-Annual 2011 Sampling Event.
Prepared for Republic Services of North Carolina, LLC.

North Carolina Dept. Environment, Health, and Natural Resources (NCDEHNR), 1995, N.C.
Water Quality Monitoring Guidance Document for Solid Waste Facilities.

North Carolina Geologic Survey, 1985, Geologic Map of North Carolina; North Carolina
Department of Natural Resources and Community Development, Geological Survey Section;
scale 1:500,000.

Tables

TABLE 1:
Historical Groundwater Elevations for the Yorktown Formation
Background
GW-2 GW-3 GW-5 GW-7 GW-8 GW-9 GW-10 GW-11 GW-11R GW-13 GW-14 GW-15 GW-16 GW-16R GW-17 GW-18 GW-21
TOC Elevation:66.36 66.23 62.60 58.79 60.04 51.94 53.22 72.42 70.90 74.76 78.74 78.23 63.02 66.12 85.68 62.00 62.07
Jan-95 51.79 54.53 48.45 47.12 46.43 47.89 -----------
Jul-95 55.85 51.80 50.42 53.84 48.12 48.13 -----------
Jan-96 58.36 53.73 51.42 49.89 49.09 49.43 -----------
Oct-96 59.92 55.53 53.05 49.87 49.14 50.32 50.32 ----------
Apr-97 57.00 51.96 50.85 47.77 47.50 49.15 49.67 50.20 ---------
Oct-97 50.20 48.05 46.74 44.79 44.41 45.61 45.41 43.67 ---------
Apr-98 55.12 51.65 50.52 47.78 47.26 48.01 47.00 44.22 ---------
Oct-98 51.35 49.25 48.24 46.30 45.58 47.82 45.43 DRY ---------
07-Apr-99 53.54 51.25 50.01 48.15 47.50 47.45 45.85 DRY ---------
20-Oct-99 57.26 52.67 51.25 48.79 52.38 49.12 47.80 45.82 ---------
26-Apr-00 54.03 50.93 49.56 48.02 47.52 47.46 45.75 DRY ---------
18-Oct-00 52.71 49.70 48.56 46.80 46.23 45.57 43.40 DRY ---------
18-Apr-01 53.54 50.36 48.94 47.37 46.85 46.32 43.93 DRY -48.31 -------
24-Oct-01 50.78 47.97 47.00 45.50 44.75 44.84 44.48 43.99 -47.95 -------
22-Apr-02 51.64 49.10 47.94 46.92 46.38 45.67 46.46 46.07 -49.30 -------
21-Oct-02 50.06 47.73 46.41 45.70 45.30 46.22 47.07 46.61 -48.82 -------
01-Apr-03 56.58 51.55 50.37 48.69 48.07 48.30 49.81 48.94 -53.08 -------
27-Oct-03 54.61 50.14 48.86 46.99 46.42 47.81 48.57 48.63 -51.91 53.64 ------
26-Apr-04 55.24 50.59 49.25 47.69 47.10 48.45 48.82 48.74 -52.02 54.55 ------
26-Oct-04 53.01 48.53 47.38 45.91 45.49 46.99 48.20 48.27 -50.79 52.11 ------
15-Mar-05 54.56 49.40 47.93 46.88 46.57 47.72 48.48 48.42 -51.96 54.34 ------
12-Jul-05 53.25 48.88 47.74 46.35 45.86 47.22 47.98 48.34 -51.00 52.71 ------
19-Jan-06 55.12 49.82 48.23 46.81 46.60 48.28 48.74 48.40 -51.66 53.92 53.10 -----
11-Jul-06 54.89 49.63 48.44 47.28 46.79 47.78 48.06 48.25 -51.46 53.16 52.90 51.00 ----
17-Jan-07 56.09 51.21 47.81 48.67 48.00 49.68 48.67 48.28 -52.23 54.74 53.59 53.11 ----
09-Jul-07 52.58 48.30 47.41 45.21 44.69 46.44 46.82 46.11 -50.50 50.84 51.42 49.53 ----
14-Jan-08 50.15 46.67 45.64 44.76 44.95 46.45 <32.68 47.54 -49.43 49.93 49.75 -47.23 --
30-Apr-08 --------------52.99 --
14-Jul-08 51.58 47.34 46.60 46.22 46.11 46.67 <32.68 47.91 -50.00 50.19 50.60 -47.40 49.54 --
02-Oct-08 --------------48.44 --
19-Jan-09 50.24 46.83 45.93 46.51 47.00 47.80 48.69 48.28 -49.63 49.29 49.88 -46.92 48.96 --
20-Jul-09 51.00 47.38 46.39 46.22 46.00 46.29 47.49 47.70 -49.64 -50.16 -48.33 49.60 46.67 48.69
25-Jan-10 53.27 48.91 47.84 49.17 49.39 49.15 50.01 48.70 -51.24 -51.83 -54.40 56.38 49.24 53.82
06-Jul-10 52.53 48.86 47.87 47.67 47.09 47.01 47.06 47.86 -50.61 -51.38 -50.97 51.49 49.85 50.68
04-Jan-11 51.80 48.72 47.50 48.04 47.81 48.06 48.58 48.17 -50.60 -51.08 -53.27 53.50 52.30 50.32
05-Jul-11 51.86 48.14 47.21 46.61 46.00 46.15 46.67 47.47 -49.77 -50.69 -50.32 51.07 49.50 50.11
09-Jan-12 51.53 48.64 47.41 47.15 46.84 47.47 48.34 47.95 -49.68 -50.49 -51.53 52.48 50.55 49.75
09-Jul-12 51.12 48.79 47.62 46.79 46.19 46.66 47.24 47.68 -48.33 -49.39 -50.88 51.47 49.98 50.08
28-Jan-13 49.73 47.62 46.65 47.01 47.00 47.36 48.34 48.00 -48.64 -49.12 -51.09 51.44 49.88 48.69
17-Jul-13 50.85 48.91 47.53 47.61 47.54 47.13 48.08 47.98 -49.01 -49.62 -53.41 54.58 52.68 49.37
28-Jan-14 49.73 47.64 46.63 47.30 47.56 47.24 48.31 47.92 -48.56 -49.02 -51.06 54.58 49.85 48.72
24-Jul-14 49.28 49.07 47.87 47.88 46.44 46.26 44.79 -42.39 45.23 -46.96 -53.02 53.54 53.25 49.66
28-Jan-15 49.11 50.83 47.50 47.04 47.12 46.60 44.78 -40.99 44.82 -46.53 -54.81 55.58 54.00 49.62
30-Jul-15 --46.66 44.69 44.13 44.44 42.77 --43.54 -45.29 -49.80 50.13 49.09 49.47
27-Jan-16 46.81 48.99 47.36 46.84 47.14 46.49 44.67 --43.26 -42.23 -54.77 55.66 54.25 49.82
27-Jul-16 46.96 48.33 47.29 45.84 45.44 45.45 43.47 40.20 43.46 45.18 51.08 51.08 50.25 49.97
MEAN 52.71 49.67 48.19 47.24 46.81 47.28 47.08 47.54 41.19 49.26 52.45 49.56 51.21 51.13 52.24 50.76 49.92
MAXIMUM 59.92 55.53 53.05 53.84 52.38 50.32 50.32 50.20 42.39 53.08 54.74 53.59 53.11 54.81 56.38 54.25 53.82
MINIMUM 46.81 46.67 45.64 44.69 44.13 44.44 42.77 43.67 40.20 43.26 49.29 42.23 49.53 46.92 48.44 46.67 48.69
Notes: Elevations in Ft-AMSL = Feet above mean sea level.*MW-16 was decommissioned after the installation of MW-16R.
TOC = Top of casing.MW-11 was abandonded and MW-11R was installed on July 21, 2014.
'- = not measured All data prior to 2012 taken from previous report by Golder Associates NC, Inc.
Location:Downgradient
East Carolina Regional Landfill
Permit No. 08-03
Joyce Engineering
TABLE 2:
Historical Groundwater Elevations for the Black Creek Formation
Background
GW-1 GW-4 GW-6 GW-12
TOC Elevation 65.87 62.53 58.95 66.13
Jan-95 48.13 47.31 47.78 51.62
Jul-95 51.12 49.35 49.95 49.51
Jan-96 51.98 49.68 50.10 49.89
Oct-96 53.44 51.38 51.85 51.70
Apr-97 53.46 51.00 51.60 51.38
Oct-97 47.00 46.10 46.44 46.24
Apr-98 52.44 50.03 50.33 50.29
Oct-98 48.24 48.23 48.00 47.70
07-Apr-99 51.94 49.27 49.64 49.50
20-Oct-99 52.13 49.56 49.45 49.83
26-Apr-00 52.15 49.13 49.60 49.37
18-Oct-00 51.04 48.09 48.49 48.36
18-Apr-01 52.14 48.40 48.81 48.64
24-Oct-01 48.58 46.29 46.73 48.20
22-Apr-02 50.40 47.41 47.85 49.45
21-Oct-02 48.08 45.93 46.37 45.93
01-Apr-03 53.40 49.65 50.18 49.75
27-Oct-03 52.07 48.91 49.32 49.03
26-Apr-04 52.83 49.05 49.66 49.16
26-Oct-04 50.57 47.45 48.00 47.54
15-Mar-05 53.10 48.31 48.96 48.47
12-Jul-05 50.96 47.51 48.29 47.82
19-Jan-06 52.27 48.24 48.85 48.40
11-Jul-06 50.95 47.82 48.30 47.92
17-Jan-07 52.62 48.11 49.95 49.14
09-Jul-07 49.96 46.83 47.34 46.80
14-Jan-08 47.41 45.14 45.64 45.02
14-Jul-08 48.65 45.92 46.46 45.90
19-Jan-09 48.13 45.31 45.92 45.35
20-Jul-09 48.79 45.78 46.27 45.78
25-Jan-10 51.98 47.45 48.15 47.56
06-Jul-10 50.61 47.22 47.77 47.37
04-Jan-11 50.35 46.98 47.53 47.16
05-Jul-11 49.88 46.64 46.47 46.79
09-Jan-12 50.39 47.10 47.71 47.25
09-Jul-12 50.09 47.13 47.64 47.31
28-Jan-13 49.00 45.94 46.54 45.99
17-Jul-13 50.47 46.88 47.40 46.98
28-Jan-14 49.08 45.92 46.55 46.02
24-Jul-14 50.50 47.03 46.99 47.27
28-Jan-15 51.27 47.13 47.59 NM
30-Jul-15 47.27 47.21 47.46 NM
27-Jan-16 51.22 47.11 47.16 47.38
27-Jul-16 49.57 46.68 47.10 46.93
MEAN 50.58 47.67 48.14 48.04
MAXIMUM 53.46 51.38 51.85 51.70
MINIMUM 47.00 45.14 45.64 45.02
Notes:
Elevations in Ft-AMSL = Feet above mean sea level.
TOC = Top of casing.
All data prior to 2012 taken from previous report by Golder Associates NC. Inc.
Location Downgradient
East Carolina Regional Landfill
Permit No. 08-03
Joyce Engineering
TABLE 3: Hydraulic Gradients and Linear Groundawater Velocities
Date of Water Table Measurements:
SEGMENT HORIZ.HYDRAULIC EFFECTIVE LINEAR
FLOW BEGIN & END GRADIENT CONDUCTIVITY POROSITY VELOCITY
DIRECTION GW ELEVATION i K n e V
(feet)(feet-AMSL)(ft/ft) (ft/day)(ft/year)
50
40
52
40
48
44
Average 0.0046 Average 5.76
Notes:
Linear flow velocity: V = Ki/n e (modified Darcy equation).
Hydraulic conductivity (K ) is based on the arithmetic mean of values from slug tests conducted at the facility.
Effective porosity (n e ) value is estimated at 85% of the laboratory-determined porosity for soil samples from the facility.
Refer to Drawing 1 for flow line segments.
FLOW LINE
SEGMENT
i 1 1927 SW 0.0052
SEGMENT
LENGTH
6.56
i 2 2250 SW 0.0053 9.35E-01 0.27 6.74
July 27, 2016
3.98i31271SW0.0031 9.35E-01 0.27
9.35E-01 0.27
East Carolina Regional Landfill
Permit No. 08-03 Joyce Engineering Inc.
TABLE 4: Well Construction Information
Well Identification Construction
Date
Ground
Surface
Elevation
TOC
Elevation Well Depth Well
Diameter Screened Interval Screened Geologic
Formation
(Ft-AMSL)(Ft-AMSL)(Feet)(Inches)(Ft-AMSL)
GW-1 1993 63.72 65.87 62 2 11.72 to 1.72 Black Creek Formation
GW-2 1993 64.02 66.36 26 2 48.02 to 38.02 Yorktown Formation
GW-3 1993 63.72 66.23 26 2 47.72 to 37.72 Yorktown Formation
GW-4 1993 60.68 62.53 59 2 11.68 to 1.68 Black Creek Formation
GW-5 1993 60.94 62.60 24 2 46.94 to 36.94 Yorktown Formation
GW-6 1993 57.53 58.95 63 2 4.53 to -5.47 Black Creek Formation
GW-7 1993 57.44 58.79 18 2 49.44 to 39.44 Yorktown Formation
GW-8 1993 58.60 60.04 18 2 50.60 to 40.60 Yorktown Formation
GW-9 1993 50.14 51.94 13 2 47.14 to 37.14 Yorktown Formation
GW-10 1996 50.47 53.22 22 2 40.47 to 30.47 Yorktown Formation
GW-11 1997 68.60 72.42 28 2 49.60 to 39.60 Yorktown Formation
GW-11R 2014 48.00 51.00 40 2 20.00 to 40.00 Yorktown Formation
GW-12 1993 63.70 66.13 54 2 19.70 to 9.70 Black Creek Formation
GW-13 2001 72.16 74.76 41.30 2 45.86 to 30.86 Yorktown Formation
GW-14 2003 76.7 78.74 47.8 2 38.9 to 28.9 Yorktown Formation
GW-15 2005 75.25 78.23 39.22 2 51.03 to 36.03 Yorktown Formation
GW-16 2006 60.99 63.02 23 2 13.0 to 23 Yorktown Formation
GW-16R 2007 63.02 66.12 24.24 2 53.78 to 38.78 Yorktown Formation
GW-17 2008 82.92 85.68 41.33 2 51.59 to 41.59 Yorktown Formation
GW-18 2009 59.20 62.07 26.71 2 47.49 to 32.49 Yorktown Formation
GW-21 2006 60.86 62.98 28.00 2 47.86 to 32.86 Yorktown Formation
Notes:
Ft-AMSL = Feet above mean sea level.GW-1, -3, -4, -5, -6, -12, -18, and -21 are used for collection of water level data only.
TOC - Top of casing (measureing point).All data prior to 2012 taken from report by Golder Associates NC, Inc.
Shaded wells have been decommissioned or abandoned.
East Carolina Regional Landfill
Permit No. 08-03
Joyce Engineering
Table 5: Quantified Detections by Monitoring Locations
WELL ID PARAMETER RESULT UNITS SWSL DATE
0803-GW2 Total Barium 357 ug/L 100 07/27/2016
0803-GW7 Total Beryllium 1.65 ug/L 1 07/27/2016
0803-GW7 Total Cobalt 37.4 ug/L 10 07/27/2016
0803-GW8 Total Barium 122 ug/L 100 07/27/2016
0803-GW9 Total Barium 151 ug/L 100 07/27/2016
0803-GW9 Total Zinc 10.0 ug/L 10 07/27/2016
0803-GW10 Total Barium 109 ug/L 100 07/27/2016
0803-GW10 Total Zinc 10.1 ug/L 10 07/27/2016
0803-GW13 Total Barium 307 ug/L 100 07/27/2016
0803-GW15 Total Barium 159 ug/L 100 07/27/2016
0803-GW16R Total Barium 104 ug/L 100 07/27/2016
0803-GW17 Total Barium 144 ug/L 100 07/27/2016
0803-GW18 Total Barium 192 ug/L 100 07/27/2016
0803-PW1 Total Zinc 36.8 ug/L 10 07/27/2016
Notes: µg/L = micorgrams per liter.
SWSL = NC Soild Waste Section Reporting Limit.
Laboratory Reporting Limit used when SWSL has not been established.
Republic - East Carolina Landfill
Permit No. 08-03
Joyce Engineering
Table 6: Exceedances of Groundwater Standards
WELL ID PARAMETER RESULT UNITS SWSL NC2L/*GWPS BACKGROUND DATE
0803-GW7 Total Cobalt 37.4 µg/L 10 1*50.7 07/27/2016
NOTES: µg/L = micorgrams per liter.
SWSL = NC Soild Waste Section Reporting Limit.
Laboratory Reporting Limit used when SWSL has not been established.
NC 2L = NC Groundwater Standard from 15A NCAC 2L.0202.
GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC 2L).
GPS = Groundwater Protection Standard as defined by 15A NCAC 13B.1634(g).
Bold indicates confirmed GPS exceedance.
Republic- East Carolina landfill
Permit No. 08-03
Joyce Engineering
Table 7: Field Parameters by Location
WELL ID PARAMETER RESULT UNITS DATE
0803-GW2 Temperature 19.8 C°7/27/2016
0803-GW2 Dissolved oxygen 6.17 mg/L 7/27/2016
0803-GW2 Conductivity 128.9 µS/cm 7/27/2016
0803-GW2 pH 4.78 S.U.7/27/2016
0803-GW2 Oxidation Reduction Potential 104.5 mV 7/27/2016
0803-GW2 Turbidity 4.01 ntu 7/27/2016
0803-GW2 Static Water Level 19.40 ft 7/27/2016
0803-GW2 Well Depth 30.00 ft 7/27/2016
0803-GW7 Temperature 19.8 C°7/27/2016
0803-GW7 Dissolved oxygen 4.42 mg/L 7/27/2016
0803-GW7 Conductivity 179.4 µS/cm 7/27/2016
0803-GW7 pH 4.83 S.U.7/27/2016
0803-GW7 Oxidation Reduction Potential 115.7 mV 7/27/2016
0803-GW7 Turbidity 3.87 ntu 7/27/2016
0803-GW7 Static Water Level 12.95 ft 7/27/2016
0803-GW7 Well Depth 18.00 ft 7/27/2016
0803-GW8 Temperature 19.4 C°7/27/2016
0803-GW8 Dissolved oxygen 1.78 mg/L 7/27/2016
0803-GW8 Conductivity 135.8 µS/cm 7/27/2016
0803-GW8 pH 5.34 S.U.7/27/2016
0803-GW8 Oxidation Reduction Potential 96.1 mV 7/27/2016
0803-GW8 Turbidity 4 ntu 7/27/2016
0803-GW8 Static Water Level 14.60 ft 7/27/2016
0803-GW8 Well Depth 18.00 ft 7/27/2016
0803-GW9 Temperature 20.5 C°7/27/2016
0803-GW9 Dissolved oxygen 0.42 mg/L 7/27/2016
0803-GW9 Conductivity 178.0 µS/cm 7/27/2016
0803-GW9 pH 5.02 S.U.7/27/2016
0803-GW9 Oxidation Reduction Potential 88.6 mV 7/27/2016
0803-GW9 Turbidity 4.18 ntu 7/27/2016
0803-GW9 Static Water Level 6.49 ft 7/27/2016
0803-GW9 Well Depth 17.00 ft 7/27/2016
0803-GW10 Temperature 16.3 C°7/27/2016
0803-GW10 Dissolved oxygen 0.49 mg/L 7/27/2016
0803-GW10 Conductivity 131.6 µS/cm 7/27/2016
0803-GW10 pH 4.77 S.U.7/27/2016
0803-GW10 Oxidation Reduction Potential 94.1 mV 7/27/2016
0803-GW10 Turbidity 2.98 ntu 7/27/2016
0803-GW10 Static Water Level 9.75 ft 7/27/2016
0803-GW10 Well Depth 20.00 ft 7/27/2016
Republic- East Carolina Landfill
Permit No. 08-03 Page 1 of 3
Joyce Engineering
Table 7: Field Parameters by Location
WELL ID PARAMETER RESULT UNITS DATE
0803-GW11R Temperature 23.5 C°7/27/2016
0803-GW11R Dissolved oxygen 2.92 mg/L 7/27/2016
0803-GW11R Conductivity 54.2 µS/cm 7/27/2016
0803-GW11R pH 5.03 S.U.7/27/2016
0803-GW11R Oxidation Reduction Potential 85.4 mV 7/27/2016
0803-GW11R Turbidity 5.69 ntu 7/27/2016
0803-GW11R Static Water Level 30.70 ft 7/27/2016
0803-GW11R Well Depth 42.24 ft 7/27/2016
0803-GW13 Temperature 20.8 C°7/27/2016
0803-GW13 Dissolved oxygen 2.72 mg/L 7/27/2016
0803-GW13 Conductivity 105.2 µS/cm 7/27/2016
0803-GW13 pH 4.85 S.U.7/27/2016
0803-GW13 Oxidation Reduction Potential 108.2 mV 7/27/2016
0803-GW13 Turbidity 4.28 ntu 7/27/2016
0803-GW13 Static Water Level 31.30 ft 7/27/2016
0803-GW13 Well Depth 41.60 ft 7/27/2016
0803-GW15 Temperature 20.8 C°7/27/2016
0803-GW15 Dissolved oxygen 5.33 mg/L 7/27/2016
0803-GW15 Conductivity 107.0 µS/cm 7/27/2016
0803-GW15 pH 4.88 S.U.7/27/2016
0803-GW15 Oxidation Reduction Potential 95.1 mV 7/27/2016
0803-GW15 Turbidity 11.70 ntu 7/27/2016
0803-GW15 Static Water Level 33.05 ft 7/27/2016
0803-GW15 Well Depth 39.05 ft 7/27/2016
0803-GW16R Temperature 17.9 C°7/27/2016
0803-GW16R Dissolved oxygen 0.80 mg/L 7/27/2016
0803-GW16R Conductivity 56.5 µS/cm 7/27/2016
0803-GW16R pH 5.09 S.U.7/27/2016
0803-GW16R Oxidation Reduction Potential 118.1 mV 7/27/2016
0803-GW16R Turbidity 3.68 ntu 7/27/2016
0803-GW16R Static Water Level 15.04 ft 7/27/2016
0803-GW16R Well Depth 27.20 ft 7/27/2016
0803-GW17 Temperature 20.6 C°7/27/2016
0803-GW17 Dissolved oxygen 2.72 mg/L 7/27/2016
0803-GW17 Conductivity 76.4 µS/cm 7/27/2016
0803-GW17 pH 5.02 S.U.7/27/2016
0803-GW17 Oxidation Reduction Potential 96.4 mV 7/27/2016
0803-GW17 Turbidity 6.95 ntu 7/27/2016
0803-GW17 Static Water Level 34.60 ft 7/27/2016
0803-GW17 Well Depth 44.30 ft 7/27/2016
Republic- East Carolina Landfill
Permit No. 08-03 Page 2 of 3
Joyce Engineering
Table 7: Field Parameters by Location
WELL ID PARAMETER RESULT UNITS DATE
0803-GW18 Temperature 19.5 C°7/27/2016
0803-GW18 Dissolved oxygen 6.67 mg/L 7/27/2016
0803-GW18 Conductivity 151.8 µS/cm 7/27/2016
0803-GW18 pH 5.11 S.U.7/27/2016
0803-GW18 Oxidation Reduction Potential 107.0 mV 7/27/2016
0803-GW18 Turbidity 4.64 ntu 7/27/2016
0803-GW18 Static Water Level 11.75 ft 7/27/2016
0803-GW18 Well Depth 29.60 ft 7/27/2016
0803-GW21 Temperature 20.9 C°7/27/2016
0803-GW21 Dissolved oxygen 2.38 mg/L 7/27/2016
0803-GW21 Conductivity 29.6 µS/cm 7/27/2016
0803-GW21 pH 4.60 S.U.7/27/2016
0803-GW21 Oxidation Reduction Potential 100.3 mV 7/27/2016
0803-GW21 Turbidity 4.66 ntu 7/27/2016
0803-GW21 Static Water Level 12.10 ft 7/27/2016
0803-GW21 Well Depth 29.95 ft 7/27/2016
0803-PW1 Temperature 20.5 C°7/27/2016
0803-PW1 Dissolved oxygen 5.11 mg/L 7/27/2016
0803-PW1 Conductivity 493 µS/cm 7/27/2016
0803-PW1 pH 8.18 S.U.7/27/2016
0803-PW1 Oxidation Reduction Potential 98.3 mV 7/27/2016
0803-PW1 Turbidity 4.89 ntu 7/27/2016
0803-SW2 Temperature 27.9 C°7/27/2016
0803-SW2 Dissolved oxygen 3.49 mg/L 7/27/2016
0803-SW2 Conductivity 840 µS/cm 7/27/2016
0803-SW2 pH 5.66 S.U.7/27/2016
0803-SW2 Oxidation Reduction Potential 33.9 mV 7/27/2016
0803-SW2 Turbidity 24.3 ntu 7/27/2016
0803-SW3 Temperature 26.7 C°7/27/2016
0803-SW3 Dissolved oxygen 1.8 mg/L 7/27/2016
0803-SW3 Conductivity 229.8 µS/cm 7/27/2016
0803-SW3 pH 5.51 S.U.7/27/2016
0803-SW3 Oxidation Reduction Potential 44.2 mV 7/27/2016
0803-SW3 Turbidity 49.4 ntu 7/27/2016
Notes: ºC= degrees Centigrade
S.U..= Standard Units
µS/cm = micro-Siemens per centimeter
ntu = Nephelometric Turbidity Units
mg/L = milligrams per liter
mV = millivolts.
Republic- East Carolina Landfill
Permit No. 08-03 Page 3 of 3
Joyce Engineering

Drawing

Appendix A

Historical Tables

TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Inorganic Compounds
Total Antimony 01/09/12 ---6.00 ND ND ND ND ND ND 0.18 J ND ND ND ------ND
GWPS = 1 µg/L 07/09/12 ---6.00 0.70 J 0.24 J ND ND ND ND ND ND ND ND ------ND
01/28/13 ---6.00 1.47 J 0.40 J ND ND ND ND ND ND ND ND ------ND
07/17/13 ---6.00 2.85 B 0.97 B 0.55 B 0.34 B ND 0.58 B 0.28 B ND ND ND ------0.39 J
01/28/14 ---6.00 2.12 J 0.50 J ND ND ND ---ND ND ND ND ------ND
05/31/14 ---6.00 ------------------------------ND ND ND
06/24/14 ---6.00 ------------------------------ND ND ND
07/24/14 EPA 6020A 1.05 6.00 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 6020A 1.05 6.00 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 6020A 0.25 6.00 ---1.77 J ND ND ND ---ND ND 0.37 J ND ND ND ND
09/16/15 EPA 6020A 0.25 6.00 ND ---------------------------------ND
01/27/16 EPA 6020B 0.25 6.00 ND 1.17 J ND ND ND ---ND ND 0.35 J ND ND ND ND
07/27/16 EPA 6020B 0.25 6.00 2.02 J 0.69 J 0.36 J ND ND 0.33 J ND ND ND ND ND ND ND
Total Arsenic 07/12/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
NC 2L = 10 µg/L 01/19/06 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---10.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---10.0 ---------------------ND ------------ND
01/17/07 ---10.0 2.10 B ND 2.10 B ND ND 2.10 B ND ND ------------3.40 J
07/09/07 ---10.0 ND ND 2.10 J ND ND ND ND ND ------------ND
01/14/08 ---10.0 ND ND 2.10 J 2.70 J ND 2.30 J ND ND ND ---------ND
04/30/08 ---10.0 ---------------------------ND ------2.20 J
07/14/08 ---10.0 ND ND ND ND ND ND ND 2.9 J ND 3.50 J ------ND
10/03/08 ---10.0 ---------------------------ND ------ND
01/19/09 ---10.0 3.80 B ND 2.80 B 5.20 B 3.70 B 3.90 B 4.40 B 4.5 B 4.10 B ND ------3.60 J
07/20/09 ---10.0 ND ND ND ND ND ND ND ND ND ND 4.02 J ND ND
01/25/10 ---10.0 ND 4.61 J 3.57 J 5.19 J ND ND 4.10 J 4.24 J ND ND ------ND
07/06/10 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---10.0 3.06 J 5.85 J ND 6.00 J ND ND ND 8.04 J ND ND ------ND
07/05/11 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/09/12 ---10.0 ND 1.35 J 1.74 J 2.11 J 1.45 J 1.77 J ND ND ND ND ------ND
01/28/13 ---10.0 ND ND ND 3.49 J ND ND ND ND ND ND ------ND
07/17/13 ---10.0 ND ND ND 3.68 J ND ND ND ND ND 0.93 J ------ND
01/28/14 ---10.0 ND ND ND 0.85 J 1.06 J ---ND 1.23 J 0.94 J 1.80 J ------ND
05/31/14 ---10.0 ------------------------------ND ND ND
06/24/14 ---10.0 ------------------------------ND ND ND
07/24/14 EPA 6020A 1.13 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 6020A 1.13 10.0 ND 1.65 J ND 1.43 J ND ND ND ND ND 2.98 J ND ND ND
07/30/15 EPA 6020A 0.75 10.0 ---1.72 J ND ND ND ---ND 1.12 J ND 1.82 J 1.88 J ND ND
09/16/15 EPA 6020A 0.75 10.0 ND ---------------------------------ND
01/27/16 EPA 6020B 0.75 10.0 ND 0.75 J ND ND ND ---ND 3.17 J ND ND 0.85 J ND ND
07/27/16 EPA 6020B 0.75 10.0 ND 1.4 J ND ND ND ND ND ND ND ND 0.85 J ND ND
Total Barium 10/28/98 ---500 ND ND ND ND ND Dry ------------------ND
NC 2L = 700 µg/L 04/07/99 ---500 ND ND ND ND ND Dry ------------------ND
12/08/99 ---500 ND ND ND ND ND ND ------------------ND
04/27/00 ---500 ND ND ND ND ND Dry ------------------ND
10/18/00 ---500 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---500 ------------------ND ------------------
01/03/01 ---500 ------------------ND ------------------
02/08/01 ---500 ------------------ND ------------------
04/19/01 ---500 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---500 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---500 ND ND ND ND ND ND ND ---------------ND
10/23/02 ---500 ND ND ND ND ND ND ND ---------------ND
04/01/03 ---500 ND ND ND ND ND ND ND ---------------ND
10/28/03 ---500 ND ND ND ND ND ND ND ---------------ND
04/27/04 ---500 500 ND ND ND ND ND ND ---------------ND
10/26/04 ---500 ND ND ND ND ND ND ND ---------------ND
03/15/05 ---500 500 ND ND ND ND ND ND ---------------ND
07/12/05 ---500 ND ND ND ND ND ND ND ---------------ND
01/12/06 ---30 ---------------------ND ------------ND
01/19/06 ---500 523 ND ND ND ND ND ND ---------------ND
07/11/06 ---500 517 ND ND ND ND ND ND ND ------------ND
10/31/06 ---500 ---------------------ND ------------ND
01/17/07 ---100 516 122 137 82.1 95.7 17.8 273 98.3 ------------0.30 J
07/09/07 ---100 448 162 121 93.5 J 89.3 J 20.8 J 259 114 ------------0.80 J
01/14/08 ---100 405 129 127 59.0 J 94.6 J 18.5 J 291 117 38 J ---------0.30 J
04/30/08 ---100 ---------------------------106 ------0.50 J
07/14/08 ---100 500 130 123 76.0 J 103 18.7 J 317 94.7 J 32.2 J 127 ------ND
10/03/08 ---100 ---------------------------116 ------ND
01/19/09 ---100 534 135 148 62.9 J 88.4 J 20.1 J 357 116 41.2 J 138 ------ND
07/20/09 ---100 534 96.4 J 145 89.2 J 88.6 J 20.0 J 332 112 39.3 J 168 445 37.2 J ND
01/25/10 ---100 545 116 0.68 B 67.6 J 91.3 J 22.0 J 312 117 32.9 J 143 ------0.43 J
07/06/10 ---100 419 49.1 J 103 89.2 J 73.5 J 18.1 J 245 92.7 J 32.5 J 117 ------ND
01/04/11 ---100 409 100 120 207 92.8 J 21.8 J 261 105 37.8 J 156 ------1.11 J
07/05/11 ---100 455 53.8 J 119 167 101 27.5 J 317 115 41.5 J 149 ------ND
01/09/12 ---100 427 21.8 J 105 212 93.8 J 19.2 J 343 120 38.8 J 156 ------0.24 J
07/09/12 ---100 414 45.1 J 108 196 114 21.1 J 369 124 46.9 J 135 ------0.75 J
01/28/13 ---100 387 72.0 J 91.9 J 257 107 19.2 J 331 125 46.3 J 140 ------ND
07/17/13 ---100 426 72.0 86.9 J 186 91.2 J 21.2 J 318 154 55.3 J 150 ------0.37 J
01/28/14 ---100 382 63.7 J 78.4 J 251 117 ---320 141 69.1 J 214 ------ND
05/31/14 ---100 ------------------------------261 29.8 J ND
06/24/14 ---100 ------------------------------285 27.3 J ND
07/24/14 EPA 6020A 0.10 100 390 42.7 J 91.1 J 222 107 48.2 J 233 123 64.6 J 146 209 23.9 J 0.32 J
01/28/15 EPA 6020A 0.10 100 370 71.3 J 83.0 J 241 124 30.7 J 332 127 59.8 J 340 237 28.6 J 0.12 J
07/30/15 EPA 6020A 0.30 100 ---53.2 J 110 171 106 ---308 144 84.4 J 179 237 26.7 J 0.45 J
09/16/15 EPA 6020A 0.30 100 543 ---------------------------------0.47 J
01/27/16 EPA 6020B 0.30 100 377 46.9 J 118 180 109 ---344 547 51.2 J 159 220 30.0 J 0.42 J
07/27/16 EPA 6020B 0.30 100 357 40.1 J 122 151 109 30.4 J 307 159 104 144 192 28.2 J 0.31 J
East Carolina Regional Landfill
Permit No. 08-03 Page 1 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Total Beryllium 10/28/98 ---2.00 ND ND ND ND ND Dry ------------------ND
GWPS = 4 µg/L 04/07/99 ---2.00 ND 2.00 ND ND ND Dry ------------------ND
12/08/99 ---2.00 ND ND ND ND ND ND ------------------ND
04/27/00 ---2.00 ND ND ND ND ND Dry ------------------ND
10/18/00 ---2.00 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---2.00 ------------------ND ------------------
01/03/01 ---2.00 ------------------ND ------------------
02/08/01 ---2.00 ------------------4.00 ------------------
04/19/01 ---2.00 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---2.00 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---2.00 ND ND ND ND ND ND ND ---------------ND
10/23/02 ---2.00 ND 3.00 ND ND ND ND ND ---------------ND
04/01/03 ---2.00 ND ND ND ND ND ND ND ---------------ND
10/28/03 ---2.00 ND 3.00 ND ND ND ND ND ---------------ND
04/27/04 ---2.00 ND 3.00 ND ND ND ND ND ---------------ND
10/26/04 ---2.00 ND 3.00 ND ND ND ND ND ---------------ND
03/15/05 ---2.00 ND ND ND ND ND ND ND ---------------ND
07/12/05 ---2.00 ND 2.20 ND ND ND ND ND ---------------ND
01/12/06 ---2.00 ---------------------ND ------------ND
01/19/06 ---2.00 ND 2.00 ND ND ND ND ND ---------------ND
07/11/06 ---2.00 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---2.00 ---------------------ND ------------ND
01/17/07 ---1.00 1.0 1.90 ND ND ND ND ND ND ------------ND
07/09/07 ---1.00 0.7 J 1.90 ND ND ND ND ND ND ------------ND
01/14/08 ---1.00 ND 1.50 ND ND ND ND ND ND ND ---------ND
04/30/08 ---1.00 ---------------------------ND ------ND
07/14/08 ---1.00 0.80 J 1.60 ND ND ND ND 0.10 J ND ND 0.10 J ------ND
10/03/08 ---1.00 ---------------------------0.20 J ------ND
01/19/09 ---1.00 0.90 J 1.30 ND ND ND ND 0.30 J ND ND 0.10 J ------ND
07/20/09 ---1.00 1.3 2.11 0.80 J 0.49 J 0.252 B 0.39 J 0.60 J 0.31 B 0.12 B 0.59 J 1.66 0.359 B 0.0779 J
01/25/10 ---1.00 1.34 2.11 1.52 0.46 J 0.256 J 0.45 J 0.61 J 0.35 J 0.15 J 0.35 J ------ND
07/06/10 ---1.00 0.87 J 1.98 0.47 J 0.45 J 0.164 J 0.25 J 0.37 J 0.23 J ND 0.21 J ------ND
01/04/11 ---1.00 1.08 2.38 0.80 J 0.57 J 0.296 J 0.43 J 0.51 J 0.28 J 0.15 J 0.42 J ------ND
07/05/11 ---1.00 0.98 J 2.01 0.70 J 0.95 J 0.312 J 0.40 J 0.56 J 0.30 J ND 0.38 J ------ND
01/09/12 ---1.00 0.99 J 0.80 J 0.60 J 0.49 J 0.16 J 0.29 J 0.58 J 0.44 J 0.07 J 0.50 J ------ND
07/09/12 ---1.00 1.03 1.94 0.62 J 1.11 0.52 J 0.28 J 0.61 J 0.27 J 0.10 J 0.31 J ------ND
01/28/13 ---1.00 0.85 J 2.01 0.46 J 1.38 0.22 J 0.23 J 0.52 J 0.27 J ND 0.35 J ------ND
07/17/13 ---1.00 1.23 2.19 0.57 J 1.34 0.12 J 0.36 J 0.64 J 1.05 0.15 J 0.43 J ------ND
01/28/14 ---1.00 0.95 J 1.91 0.57 J 1.10 0.68 J ---0.61 J 0.50 J 0.25 J 0.83 J ------ND
05/31/14 ---1.00 ------------------------------1.27 0.09 J ND
06/24/14 ---1.00 ------------------------------1.18 ND ND
07/24/14 EPA 6020A 0.05 1.00 1.02 1.68 0.55 J 1.05 0.34 J 0.69 J 0.39 J 0.29 J 0.15 J 0.29 J 0.91 J 0.09 J ND
01/28/15 EPA 6020A 0.05 1.00 0.63 J 2.03 0.53 J 0.89 J 0.51 J 0.12 J 0.60 J 0.35 J 0.17 J 1.78 0.97 J 0.07 J ND
07/30/15 EPA 6020A 0.09 1.00 ---1.65 0.60 J 0.97 J 0.24 J ---0.54 J 0.39 J 0.20 J 0.60 J 1.01 ND ND
09/16/15 EPA 6020A 0.09 1.00 0.94 J ---------------------------------ND
01/27/16 EPA 6020B 0.09 1.00 0.95 J 1.94 0.71 J 0.87 J 0.39 J ---0.62 J 32.0 0.11 J 0.45 J 0.94 J ND ND
Resample >>03/09/16 EPA 6020A 0.09 1.00 ---------------------0.9 J ------------ND
07/27/16 EPA 6020B 0.09 1.00 0.85 J 1.65 0.70 J 0.87 J 0.29 J 0.14 J 0.56 J 0.43 J 0.21 J 0.29 J 0.83 J ND ND
Total Cadmium 10/28/98 ---1.00 ND ND ND ND ND Dry ------------------ND
NC 2L = 2 µg/L 04/07/99 ---1.00 ND ND ND ND ND Dry ------------------ND
12/08/99 ---1.00 ND ND ND ND ND ND ------------------ND
04/27/00 ---1.00 ND ND ND ND ND Dry ------------------ND
10/18/00 ---1.00 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---1.00 ------------------ND ------------------
01/03/01 ---1.00 ------------------5.00 ------------------
02/08/01 ---1.00 ------------------ND ------------------
04/19/01 ---1.00 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---1.00 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---1.00 ND ND ND ND ND ND ND ---------------ND
10/23/02 ---1.00 ND ND ND ND ND ND ND ---------------ND
04/01/03 ---1.00 ND ND ND ND ND ND ND ---------------ND
10/28/03 ---1.00 ND ND ND ND ND ND ND ---------------ND
04/27/04 ---1.00 ND ND ND ND ND ND ND ---------------ND
10/26/04 ---1.00 ND ND ND ND ND ND ND ---------------ND
03/15/05 ---1.00 ND ND ND ND ND ND ND ---------------ND
07/12/05 ---1.00 ND ND ND ND ND ND ND ---------------ND
01/12/06 ---1.00 ---------------------ND ------------ND
01/19/06 ---1.00 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---1.00 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---1.00 ---------------------ND ------------ND
01/17/07 ---1.00 ND ND ND ND ND ND ND ND ------------ND
07/09/07 ---1.00 ND ND ND ND ND ND ND ND ------------ND
01/14/08 ---1.00 ND ND ND ND ND ND ND ND ND ---------ND
04/30/08 ---1.00 ---------------------------ND ------ND
07/14/08 ---1.00 ND ND ND ND ND ND ND ND ND ND ------ND
10/03/08 ---1.00 ---------------------------ND ------ND
01/19/09 ---1.00 ND ND ND ND ND ND ND ND ND ND ------ND
07/20/09 ---1.00 0.14 B 0.26 B 0.11 B ND 0.159 B 0.10 B ND ND 0.18 B 0.09 B 0.252 B 0.328 B 0.11 J
01/25/10 ---1.00 0.39 B 0.35 B 1.59 0.88 B 0.357 B 0.26 B 0.33 B 0.391 B 0.36 B 0.43 B ------0.28 J
07/06/10 ---1.00 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---1.00 0.43 J ND ND ND ND ND ND ND ND ND ------ND
07/05/11 ---1.00 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---1.00 ND ND ND ND ND ND ND ND ND ND ------ND
07/09/12 ---1.00 0.07 J ND ND ND ND ND ND 0.06 J 0.28 J ND ------ND
01/28/13 ---1.00 ND ND ND ND ND ND ND ND ND ND ------ND
07/17/13 ---1.00 ND ND ND ND ND 0.19 J 0.14 J ND 0.19 J ND ------ND
01/28/14 ---1.00 0.20 J 0.09 J ND ND 0.16 J ---ND 0.21 J 0.07 J ND ------ND
05/31/14 ---1.00 ------------------------------0.05 J ND ND
06/24/14 ---1.00 ------------------------------ND ND ND
07/24/14 EPA 6020A 0.05 1.00 0.05 J ND ND ND ND 0.05 J ND ND ND ND 0.05 J ND ND
01/28/15 EPA 6020A 0.05 1.00 ND 0.06 J 0.08 J ND 0.06 J ND 0.05 J ND ND 0.05 J ND ND ND
07/30/15 EPA 6020A 0.1 1.00 ---0.93 J ND 0.24 J ND ---ND ND ND ND ND ND ND
09/16/15 EPA 6020A 0.1 1.00 0.15 J ---------------------------------ND
01/27/16 EPA 6020B 0.1 1.00 ND 0.10 J ND ND ND ---0.12 J 0.19 J ND ND ND ND ND
07/27/16 EPA 6020B 0.1 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 2 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Total Chromium 10/28/98 ---10.0 ND ND ND ND ND Dry ------------------ND
NC 2L = 10 µg/L 04/07/99 ---10.0 ND ND ND ND ND Dry ------------------ND
12/08/99 ---10.0 ND ND ND ND ND ND ------------------ND
04/27/00 ---10.0 ND ND ND ND ND Dry ------------------ND
10/18/00 ---10.0 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---10.0 ------------------ND ------------------
01/03/01 ---10.0 ------------------ND ------------------
02/08/01 ---10.0 ------------------ND ------------------
04/19/01 ---10.0 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---10.0 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---10.0 ND ND 10.0 ND ND ND ND ---------------ND
10/23/02 ---10.0 ND ND ND ND ND ND ND ---------------ND
04/01/03 ---10.0 ND ND 10.0 ND ND ND ND ---------------ND
10/28/03 ---10.0 ND ND ND ND ND ND ND ---------------ND
04/27/04 ---10.0 ND ND ND ND ND ND ND ---------------ND
10/26/04 ---10.0 ND ND 10.0 ND ND ND ND ---------------ND
03/15/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/12/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
01/12/06 ---10.0 ---------------------ND ------------ND
01/19/06 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---10.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---10.0 ---------------------ND ------------ND
01/17/07 ---10.0 ND ND ND ND ND 4.30 J ND ND ------------ND
07/09/07 ---10.0 ND ND ND ND ND 2.50 J ND ND ------------ND
01/14/08 ---10.0 2.60 J ND ND ND ND 5.90 J 3.80 J ND ND ---------ND
04/30/08 ---10.0 ---------------------------8.80 J ------ND
07/14/08 ---10.0 ND ND ND ND ND 2.80 J ND ND 1.40 J 2.0 J ------ND
10/03/08 ---10.0 ---------------------------1.60 J ------ND
01/19/09 ---10.0 3.70 J ND ND 1.20 J ND 4.60 J ND ND 3.0 J 1.6 J ------ND
07/20/09 ---10.0 0.94 J 0.78 J 0.80 J ND ND 4.17 J ND 1.56 J 1.0 J 7.4 J 2.55 J 4.63 J ND
01/25/10 ---10.0 ND ND ND ND ND 5.97 J ND ND ND ND ------ND
07/06/10 ---10.0 10.4 2.17 J 1.15 J ND ND 3.08 J ND ND ND 1.58 J ------ND
01/04/11 ---10.0 1.46 J 4.26 J 1.42 J 4.41 J ND 4.82 J ND 1.23 J ND 5.21 J ------ND
07/05/11 ---10.0 1.44 J 1.40 J ND 3.65 J 1.9 J 9.73 J ND 1.67 J ND 2.96 J ------ND
01/09/12 ---10.0 ND ND 0.60 J ND ND 4.20 J ND 2.62 J ND 4.00 J ------ND
07/09/12 ---10.0 1.88 J 2.28 J ND ND ND 3.82 J ND ND ND ND ------ND
01/28/13 ---10.0 2.40 B 2.06 B 1.82 B 3.18 B 1.27 B 5.98 B 0.75 B 2.24 B 0.78 B 3.08 B ------1.38 J
07/17/13 ---10.0 3.22 J 2.53 J 1.96 J 2.55 J ND 4.64 J ND 9.5 J ND 2.20 J ------ND
01/28/14 ---10.0 1.85 3.38 2.35 2.79 3.96 ---ND 2.85 4.98 11.1 ------2.84 J
05/31/14 ---10.0 ------------------------------2.18 B 2.93 B 3.93 J
06/24/14 ---10.0 ------------------------------9.44 B 7.42 B 8.19 J
07/24/14 EPA 6020A 0.73 10.0 0.83 J 1.32 J ND ND ND 6.64 J ND ND ND ND ND ND ND
01/28/15 EPA 6020A 0.73 10.0 1.86 J 2.84 J 1.00 J ND 2.27 J 1.78 J ND 1.98 J 1.45 J 32.4 1.34 J ND ND
Resample >>03/05/15 ---10.0 ---------------------------9.28 J ------ND
07/30/15 EPA 6020A 0.43 10.0 ---2.02 J ND ND ND ---ND 0.89 J ND 9.48 J 0.91 J ND ND
09/16/15 EPA 6020A 0.43 10.0 1.82 J ---------------------------------ND
01/27/16 EPA 6020B 0.43 10.0 2.86 J 1.90 J 0.98 J 1.31 J 0.49 J ---1.25 J 90.0 0.47 J 9.39 J 1.25 J 0.48 J ND
Resample >>03/09/16 EPA 6020A 0.09 1.00 ---------------------13.0 ------------0.49 J
07/27/16 EPA 6020B 0.43 10.00 1.55 J 1.20 J 1.04 J 0.57 J ND 4.28 J 0.54 J 3.11 J ND 2.95 J 0.84 J ND ND
Total Cobalt 10/28/98 ---10.0 ND 30 ND ND ND Dry ------------------ND
GWPS = 1 µg/L 04/07/99 ---10.0 ND 20 ND ND ND Dry ------------------ND
12/08/99 ---10.0 10 20 ND ND ND ND ------------------ND
04/27/00 ---10.0 ND 30 ND ND ND Dry ------------------ND
10/18/00 ---10.0 ND 30 ND ND ND Dry 30.00 ---------------ND
11/28/00 ---10.0 ------------------10.00 ------------------
01/03/01 ---10.0 ------------------ND ------------------
02/08/01 ---10.0 ------------------ND ------------------
04/19/01 ---10.0 ND 30 ND ---ND Dry ND ---------------ND
12/24/01 ---10.0 ND 30 ND ND ND ND ND ---------------ND
04/23/02 ---10.0 ND 30 ND ND ND ND ND ---------------ND
10/23/02 ---10.0 ND 50 ND ND ND ND ND ---------------ND
04/01/03 ---10.0 10 40 ND ND ND ND ND ---------------ND
10/28/03 ---10.0 ND 50 ND ND ND ND ND ---------------ND
04/27/04 ---10.0 ND 30 ND ND ND ND ND ---------------ND
10/26/04 ---10.0 ND 40 ND ND ND ND ND ---------------ND
03/15/05 ---10.0 10 36 ND ND ND ND ND ---------------ND
07/12/05 ---10.0 ND 40 ND ND ND ND ND ---------------ND
01/12/06 ---10.0 ---------------------ND ------------ND
01/19/06 ---10.0 11.9 30 ND ND ND ND ND ---------------ND
07/11/06 ---10.0 12.5 31.6 ND ND ND ND ND ND ------------ND
10/31/06 ---10.0 ---------------------ND ------------ND
01/17/07 ---10.0 10.30 34.9 3.9 J ND ND ND 3.0 J 2.90 J ------------ND
07/09/07 ---10.0 10.00 37.5 2.9 J ND ND ND ND 2.60 J ------------ND
01/14/08 ---10.0 11.30 35.1 4.2 J 3.20 J 3.8 J 2.0 J 3.30 J 3.40 J 2.60 J ---------ND
04/30/08 ---10.0 ---------------------------20.50 ------ND
07/14/08 ---10.0 10.10 37.3 2.6 J ND ND ND 2.70 J 2.10 J 1.20 J 4.50 J ------ND
10/03/08 ---10.0 ---------------------------6.30 J ------ND
01/19/09 ---10.0 12.0 23.7 3.7 J 3.00 J 4.6 J ND 1.80 J 1.70 J 1.80 J 5.20 J ------ND
07/20/09 ---10.0 11.40 35.4 3.93 J 1.47 J 2.91 J 0.59 J 2.00 J 2.67 J 0.77 J 3.93 J 7.69 J 0.895 J ND
01/25/10 ---10.0 12.6 21.5 2.0 B 2.46 J 0.858 B 1.6 B 2.71 J 3.62 J 1.57 B 3.02 B ------0.49 J
07/06/10 ---10.0 8.59 J 26.6 2.62 J 1.15 J ND ND 1.66 J 2.07 J 1.89 J 2.14 J ------ND
01/04/11 ---10.0 9.65 J 29.8 3.63 J 3.19 J ND 1.19 J 2.24 J 2.6 J 1.77 J 5.07 J ------ND
07/05/11 ---10.0 10.40 39.0 3.19 J 2.17 J 2.03 J 1.40 J 2.34 J 2.8 J 2.18 J 3.65 J ------ND
01/09/12 ---10.0 9.51 J 13.8 2.92 J 2.44 J 1.63 J 0.73 J 2.73 J 3.29 J 1.84 J 3.93 J ------ND
07/09/12 ---10.0 9.76 J 26.1 3.39 J 2.19 J 2.52 J 0.78 J 3.44 J 2.94 J 3.29 J 3.13 J ------ND
01/28/13 ---10.0 9.53 J 33.3 2.98 J 2.84 J 3.22 J 0.82 J 3.28 J 3.13 J 1.83 J 3.49 J ------ND
07/17/13 ---10.0 10.80 28.0 2.50 J 2.67 J 1.14 J 0.95 J 2.89 J 6.64 J 3.91 J 3.79 J ------ND
01/28/14 ---10.0 9.72 J 28.2 2.24 J 2.88 J 7.80 J ---2.83 J 4.06 J 4.70 J 5.35 J ------ND
05/31/14 ---10.0 ------------------------------5.78 J 0.42 J ND
06/24/14 ---10.0 ------------------------------5.64 J ND ND
07/24/14 EPA 6020A 0.26 10.0 9.08 J 23.0 2.53 J 2.50 J 5.34 J 9.10 J 2.02 J 2.92 J 2.93 J 2.56 J 4.06 J 0.33 J ND
01/28/15 EPA 6020A 0.26 10.0 6.52 J 34.3 2.35 J 2.82 J 8.05 J 2.81 J 3.29 J 3.25 J 7.03 J 11.9 4.83 J 0.33 J ND
07/30/15 EPA 6020A 0.29 10.0 ---38.0 3.13 J 2.02 J 4.38 J ---3.06 J 3.50 J 5.08 J 3.93 J 4.88 J ND ND
09/16/15 EPA 6020A 0.29 10.0 10.2 ---------------------------------ND
01/27/16 EPA 6020B 0.29 10.0 8.44 J 34.0 3.83 J 2.25 J 7.67 J ---2.37 J 34.1 4.78 J 3.11 J 4.47 J ND ND
Resample >>03/09/16 EPA 6020A 0.09 1.00 ---------------------6.5 J ------------ND
07/27/16 EPA 6020B 0.29 10.00 8.68 J 37.40 4.21 J 2.05 J 6.98 J 2.26 J 4.28 J 4.61 J 3.88 J 2.35 J 4.19 J ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 3 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Total Copper 07/12/05 ---200 ND ND ND ND ND ND ND ---------------ND
NC 2L = 1000 µg/L 01/19/06 ---200 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---200 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---200 ---------------------ND ------------ND
01/17/07 ---10.0 ND 0.80 J ND ND ND ND ND ND ------------ND
07/09/07 ---10.0 ND 5.40 J ND ND 1 J ND ND ND ------------ND
01/14/08 ---10.0 4.70 J 1.60 B 1.30 B 1.30 B ND 1.00 B 0.80 B 0.8 B 1.10 B ---------0.70 J
04/30/08 ---10.0 ---------------------------2.60 B ------1.40 J
07/14/08 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
10/03/08 ---10.0 ---------------------------ND ------ND
01/19/09 ---10.0 ND ND 1.70 J ND ND ND ND ND 2.00 J ND ------ND
07/20/09 ---10.0 ND ND 0.868 B ND ND ND ND ND ND 2.19 B ND 1.09 B 1.25 J
01/25/10 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/06/10 ---10.0 ND ND ND 2.56 J ND ND ND ND ND ND ------ND
01/04/11 ---10.0 2.3 J 2.16 J ND 3.09 J 1.8 J 4.68 J ND ND ND 3.49 J ------ND
07/05/11 ---10.0 8.78 J 1.60 J ND 2.66 J ND ND ND ND ND ND ------ND
01/09/12 ---10.0 1.57 B 1.54 B 1.06 B 0.62 B 0.62 B 0.68 B 0.59 B 1.87 B 0.32 B 2.32 B ------0.66 J
07/09/12 ---10.0 1.24 J 0.88 J 0.31 J ND 0.64 J 0.24 J ND ND 0.65 J 0.45 J ------ND
01/28/13 ---10.0 1.12 B 1.13 B 1.23 B 1.39 B 1.45 B 1.15 B 0.84 B 1.19 B 0.46 B 1.74 B ------0.26 J
07/17/13 ---10.0 1.67 J 1.18 J 1.05 J 1.15 J 0.63 J 1.03 J 0.39 J 3.59 J 0.91 J 1.73 J ------ND
01/28/14 ---10.0 2.05 J 1.48 J 1.51 J 0.68 J 1.65 J ---ND 1.96 J 4.48 J 5.79 J ------ND
05/31/14 ---10.0 ------------------------------0.98 J 0.81 J ND
06/24/14 ---10.0 ------------------------------0.79 B 0.42 B 0.23 J
07/24/14 EPA 6020A 0.22 10.0 1.39 J 3.05 J 1.09 J 0.50 J 0.45 J 3.19 J 0.25 J 0.54 J 0.32 J 0.93 J 0.39 J 0.46 J ND
01/28/15 EPA 6020A 0.22 10.0 1.38 J 1.68 J 2.16 J 0.72 J 7.30 J 4.40 J 0.56 J 0.73 J 1.26 J 13.6 0.64 J 0.49 J ND
07/30/15 EPA 6020A 0.41 10.0 ---8.18 J 1.38 B 1.27 B 7.65 J ---0.42 B 0.89 B 0.56 B 4.4 B 0.51 B ND 1.31 J
09/16/15 EPA 6020A 0.41 10.0 2.32 J ---------------------------------ND
01/27/16 EPA 6020B 0.41 10.0 1.28 B 1.24 B 0.41 B ND 0.61 B ---1.43 B 25.0 0.54 B 2.89 B 0.61 B ND 2.44 J
07/27/16 EPA 6020B 0.41 10.0 0.76 B 1.13 B ND ND 2.49 B 0.66 B ND 0.98 B 1.19 B 1.21 B 0.55 B ND 8.47 J
Total Lead 10/28/98 ---10.0 ND ND ND ND ND Dry ------------------ND
NC 2L = 15 µg/L 04/07/99 ---10.0 ND ND ND ND ND Dry ------------------ND
12/08/99 ---10.0 ND ND ND ND ND ND ------------------ND
04/27/00 ---10.0 ND ND ND ND ND Dry ------------------ND
10/18/00 ---10.0 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---10.0 ------------------ND ------------------
01/03/01 ---10.0 ------------------ND ------------------
02/08/01 ---10.0 ------------------ND ------------------
04/19/01 ---10.0 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---10.0 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---10.0 ND ND ND ND ND ND ND ---------------ND
10/23/02 ---10.0 ND ND ND ND ND ND ND ---------------ND
04/01/03 ---10.0 ND ND ND ND ND ND ND ---------------ND
10/28/03 ---10.0 ND ND ND ND ND ND ND ---------------ND
04/27/04 ---10.0 ND ND ND ND ND ND ND ---------------ND
10/26/04 ---10.0 ND ND ND ND ND ND ND ---------------ND
03/15/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/12/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
01/12/06 ---10.0 ---------------------ND ------------ND
01/19/06 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---10.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---10.0 ---------------------ND ------------ND
01/17/07 ---10.0 ND 2.30 J ND ND ND ND ND ND ------------ND
07/09/07 ---10.0 2.30 J 2.90 J 2.90 J ND ND 2.00 J ND 2.2 J ------------ND
01/14/08 ---10.0 ND ND ND ND ND ND ND ND ND ---------ND
04/30/08 ---10.0 ---------------------------4.30 J ------ND
07/14/08 ---10.0 ND ND ND ND ND ND ND ND ND 2.10 J ------ND
10/03/08 ---10.0 ---------------------------2.20 J ------ND
01/19/09 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/20/09 ---10.0 2.82 B 2.21 B ND 1.71 B 2.73 B ND ND ND 2.68 B 6.81 B 6.11 B 5.83 B 2.16 J
01/25/10 ---10.0 ND 1.70 J 7.56 J 1.55 J ND ND ND ND ND 2.06 J ------ND
07/06/10 ---10.0 ND 2.40 J ND ND ND ND ND ND ND ND ------ND
01/04/11 ---10.0 ND 3.03 J ND ND ND ND ND ND ND ND ------ND
07/05/11 ---10.0 ND 3.52 J ND 2.16 J ND ND ND ND ND ND ------ND
01/09/12 ---10.0 0.77 B 1.21 B 0.47 B 0.75 B 0.45 B 0.20 B 2.43 B 2.33 B 0.43 B 3.19 B ------0.94 J
07/09/12 ---10.0 0.84 J 2.69 J 0.22 J 0.29 J 0.37 J ND 0.21 J 0.11 J 0.21 J 1.34 J ------ND
01/28/13 ---10.0 0.25 J 1.14 J 0.22 J 1.77 J 0.52 J ND 0.24 J 0.11 J 0.36 J 2.73 J ------ND
07/17/13 ---10.0 0.68 J 1.55 J 0.42 J 0.76 J 0.11 J 0.15 J 0.18 J 3.59 J 0.57 J 2.43 J ------ND
01/28/14 ---10.0 0.34 J 1.25 J 0.56 J 0.26 J 1.57 J ---0.23 J 0.98 J 7.74 J 11.7 ------ND
05/31/14 ---10.0 ------------------------------2.40 J 2.59 J ND
06/24/14 ---10.0 ------------------------------3.26 J 0.70 J ND
07/24/14 EPA 6020A 0.05 10.0 0.27 J 1.62 J 0.23 J 0.11 J 0.66 J 2.07 J 0.13 J 0.05 J 0.48 J 0.96 J 2.78 J 1.62 J ND
01/28/15 EPA 6020A 0.05 10.0 0.18 B 1.94 J 0.21 B 0.06 B 1.55 B 0.10 B 0.38 B ND 1.95 J 18.3 2.35 J 1.35 B 0.34 J
Resample >>03/05/15 0.05 10.0 ---------------------------3.39 J ------ND
07/30/15 EPA 6020A 0.08 10.0 ---1.63 J 0.18 J 0.26 J 0.66 J ---0.20 J 0.30 J 0.78 J 4.06 J 2.63 J 0.74 J ND
09/16/15 EPA 6020A 0.08 10.0 0.43 J ---------------------------------ND
01/27/16 EPA 6020B 0.08 10.0 0.27 J 0.78 J 0.16 J 0.21 J 0.14 J ---0.29 J 34.4 0.93 J 2.77 J 2.46 J 0.91 J ND
Resample>>03/09/16 EPA 6020A 0.09 1.00 ---------------------2.6 J ------------ND
07/27/16 EPA 6020B 0.08 10.00 0.10 J 0.73 J 0.16 J ND 0.4 J 0.30 J 0.21 J 0.53 J 1.12 J 0.87 J 2.26 J 0.86 J ND
East Carolina Regional Landfill
Permit No. 08-03 Page 4 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Total Nickel 10/28/98 ---50.0 ND ND ND ND ND Dry ------------------ND
NC 2L = 100 µg/L 04/07/99 ---50.0 ND ND ND ND ND Dry ------------------ND
12/08/99 ---50.0 ND ND ND ND ND ND ------------------ND
04/27/00 ---50.0 ND ND ND ND ND Dry ------------------ND
10/18/00 ---50.0 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---50.0 ------------------ND ------------------
01/03/01 ---50.0 ------------------ND ------------------
02/08/01 ---50.0 ------------------ND ------------------
04/19/01 ---50.0 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---50.0 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---50.0 ND ND ND ND ND ND ND ---------------ND
10/23/02 ---50.0 ND ND ND ND ND ND ND ---------------ND
04/01/03 ---50.0 ND ND 20.00 ND ND ND ND ---------------ND
10/28/03 ---50.0 ND ND ND ND ND ND ND ---------------ND
04/27/04 ---50.0 ND ND ND ND ND ND ND ---------------ND
10/26/04 ---50.0 ND ND ND ND ND ND ND ---------------ND
03/15/05 ---50.0 ND ND ND ND ND ND ND ---------------ND
07/12/05 ---50.0 ND ND ND ND ND ND ND ---------------ND
01/12/06 ---50.0 ---------------------ND ------------ND
01/19/06 ---50.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---50.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---50.0 ---------------------ND ------------ND
01/17/07 ---50.0 7.40 J 10.40 3.70 J 4.10 J ND ND 3.00 J 3.6 J ------------ND
07/09/07 ---50.0 6.00 J 9.10 J 3.80 J 2.00 J ND ND 2.30 J 2.5 J ------------ND
01/14/08 ---50.0 11.00 J 8.00 J 5.80 J 3.70 J 2.0 J 3.20 J 4.70 J 3.8 J ND ---------ND
04/30/08 ---50.0 ---------------------------4.10 J ------ND
07/14/08 ---50.0 3.90 J 7.10 J 2.40 J 2.00 J ND ND 2.50 J ND ND ND ------ND
10/03/08 ---50.0 ---------------------------2.40 J ------ND
01/19/09 ---50.0 7.80 B 7.10 B 3.40 B 4.10 B 3.1 B 2.40 B 4.40 B 5.2 B ND ND ------2.20 J
07/20/09 ---50.0 6.08 J 9.00 J 3.27 J 3.03 J 1.07 J 0.72 J 2.48 J 2.59 J ND 2.56 J 9.37 J 1.49 J ND
01/25/10 ---50.0 4.55 J 6.31 J ND ND ND ND ND 1.75 J ND ND ------ND
07/06/10 ---50.0 5.31 J 10.00 J ND ND ND ND ND ND ND ND ------ND
01/04/11 ---50.0 6.42 J 9.32 J 2.17 J 4.60 J ND ND 2.50 J 2.92 J ND 2.54 J ------ND
07/05/11 ---50.0 6.82 J 10.60 J 2.64 J 6.35 J ND ND 2.94 J 3.22 J ND ND ------ND
01/09/12 ---50.0 6.14 J 6.14 J 3.28 J 6.42 J 1.37 J 1.14 J 3.10 J 3.66 J 0.67 J 1.76 J ------ND
07/09/12 ---50.0 7.09 J 10.80 J 2.78 J 6.67 J 1.68 J 1.45 J 3.75 J 3.52 J 0.70 J 1.16 J ------ND
01/28/13 ---50.0 7.35 J 9.57 J 2.6 J 8.82 J 5.06 J 2.37 J 3.48 J 3.57 J 0.74 J 1.70 J ------ND
07/17/13 ---50.0 7.88 J 9.55 J 2.48 J 6.23 J 1.52 J 1.43 J 2.75 J 5.84 J 1.31 J 2.04 J ------ND
01/28/14 ---50.0 7.86 J 13.60 J 3.19 J 8.60 J 3.67 J ---3.25 J 5.79 J 2.88 J 3.37 J ------ND
05/31/14 ---50.0 ------------------------------6.80 J 0.59 J ND
06/24/14 ---50.0 ------------------------------6.61 J ND ND
07/24/14 EPA 6020A 0.22 50.0 7.21 J 8.60 J 2.36 J 7.56 J 2.59 J 5.87 J 1.86 J 3.2 J 1.07 J 1.29 J 4.58 J 0.38 J ND
01/28/15 EPA 6020A 0.22 50.0 6.07 J 10.6 J 2.55 J 9.41 J 5.19 J 1.76 J 3.13 J 3.68 J 1.41 J 5.89 J 5.64 J 0.41 J ND
07/30/15 EPA 6020A 0.48 50.0 ---15.4 J 2.84 J 6.23 J 2.67 J ---2.81 J 3.54 J 1.24 J 2.43 J 5.45 J ND ND
09/16/15 EPA 6020A 0.48 50.0 8.68 J ---------------------------------ND
01/27/16 EPA 6020B 0.48 50.0 8.04 J 9.75 J 3.21 J 6.79 J 3.38 J ---11.3 J 25.8 J 0.82 J 2.82 J 4.66 J ND ND
07/27/16 EPA 6020B 0.48 50.0 7.78 J 8.86 J 3.68 J 5.87 J 4.23 J 1.98 J 3.76 J 4.42 J 1.54 J 1.55 J 4.54 J ND ND
Total Selenium 07/12/05 ---20.0 ND ND ND ND ND ND ND ---------------ND
NC 2L = 20 µg/L 01/19/06 ---20.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---20.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---20.0 ---------------------ND ------------ND
01/17/07 ---10.0 ND ND ND ND ND ND ND ND ------------ND
07/09/07 ---10.0 ND ND ND ND 2.0 J ND ND ND ------------ND
01/14/08 ---10.0 2.30 J ND 2.00 J ND ND ND ND 2.3 J ND ---------ND
04/30/08 ---10.0 ---------------------------ND ------ND
07/14/08 ---10.0 ND 3.30 J ND ND ND ND 2.90 J ND 2.70 J ND ------ND
10/03/08 ---10.0 ---------------------------ND ------ND
01/19/09 ---10.0 5.60 J ND 4.40 J 2.90 J ND ND ND ND ND ND ------ND
07/20/09 ---10.0 ND 4.33 B 3.90 B ND 5.08 B ND ND ND ND 4.21 B 7.32 B 8.27 B 3.58 J
01/25/10 ---10.0 ND 1.62 J 1.08 J 1.86 J 1.32 J ND ND 0.918 J 0.88 J 0.86 J ------ND
07/06/10 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---10.0 ND ND ND 1.89 J ND ND ND ND ND ND ------ND
07/05/11 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---10.0 ND ND ND 0.80 J ND ND ND ND ND ND ------ND
07/09/12 ---10.0 ND 1.43 ND ND ND ND ND ND ND ND ------ND
01/28/13 ---10.0 ND 1.10 J ND 1.49 J ND ND ND ND ND ND ------ND
07/17/13 ---10.0 ND 1.44 J ND 1.09 J ND ND ND ND ND ND ------ND
01/28/14 ---10.0 ND 0.83 J ND 1.02 J ND ---ND ND ND ND ------ND
05/31/14 ---10.0 ------------------------------ND ND ND
06/24/14 ---10.0 ------------------------------1.28 J ND ND
07/24/14 EPA 6020A 1.01 10.0 ND 1.20 J ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 6020A 1.01 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 6020A 0.85 10.0 ---6.23 J 0.91 J ND ND ---ND ND ND 2.55 J 5.11 J ND ND
09/16/15 EPA 6020A 0.85 10.0 ND ---------------------------------ND
01/27/16 EPA 6020B 0.85 10.0 ND 3.63 J ND ND ND ---ND 7.07 J ND 1.10 J 3.58 J ND ND
07/27/16 EPA 6020B 0.85 10.0 ND 5.56 J ND ND ND ND ND ND ND ND 3.49 J ND ND
Total Silver 07/12/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
NC 2L = 20 µg/L 01/19/06 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---10.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---10.0 ---------------------ND ------------ND
01/17/07 ---10.0 ND ND ND ND ND ND ND ND ------------ND
07/09/07 ---10.0 ND ND ND ND ND ND ND ND ------------ND
01/14/08 ---10.0 2.10 J ND ND 3.10 J ND ND ND 2.1 J ND ---------ND
04/30/08 ---10.0 ---------------------------ND ------ND
07/14/08 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
10/03/08 ---10.0 ---------------------------ND ------ND
01/19/09 ---10.0 ND ND ND ND ND ND ND ND 3.60 J ND ------ND
07/20/09 ---10.0 ND ND ND ND ND ND ND ND ND 2.05 J ND 2.61 J ND
01/25/10 ---10.0 1.59 B 1.20 B 6.82 J 1.68 B 1.76 B 1.55 B 1.79 B 1.74 B 2.07 B 2.55 B ------1.25 J
07/06/10 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/05/11 ---10.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---10.0 ND 1.58 J ND ND ND ND 0.43 J 0.27 J ND 0.83 J ------ND
07/09/12 ---10.0 ND 0.25 J ND 0.50 J 0.43 J 0.68 J 1.00 J 0.83 J ND 1.25 J ------ND
01/28/13 ---10.0 ND 0.34 J ND 0.90 J 1.17 J 0.86 J 1.09 J 0.17 J ND 2.13 J ------ND
07/17/13 ---10.0 ND ND ND 0.27 J ND ND ND 1.64 J ND 5.64 J ------ND
01/28/14 ---10.0 ND 0.57 J ND ND 1.02 J ---ND 16.0 1.91 J 3.70 J ------ND
05/31/14 ---10.0 ------------------------------ND ND ND
06/24/14 ---10.0 ------------------------------ND ND ND
07/24/14 EPA 6020A 0.17 10.0 ND 0.23 J ND ND 0.80 J ND 0.32 J 4.32 J ND 6.50 J ND ND ND
01/28/15 EPA 6020A 0.17 10.0 ND 3.68 J 0.44 J 0.32 J 2.94 J ND 1.01 J 0.18 J 0.49 J 5.38 J ND ND ND
07/30/15 EPA 6020A 0.22 10.0 ---16.9 ND 0.29 J 0.58 J ---0.57 J ND ND 4.62 J ND ND ND
09/16/15 EPA 6020A 0.22 10.0 4.27 B ---------------------------------4.12 J
01/27/16 EPA 6020B 0.22 10.0 ND 1.27 J ND ND ND ---18.1 1.02 J ND 5.21 J ND ND ND
07/27/16 EPA 6020B 0.22 10.0 ND 0.93 J ND ND 0.94 J ND ND 0.78 J ND 6.45 J ND ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 5 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Total Thallium 07/12/05 ---10.0 ND ND ND ND ND ND ND ---------------ND
GWPS = 0.2 µg/L 01/19/06 ---10.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---10.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---10.0 ---------------------ND ------------ND
01/17/07 ---5.50 0.07 J 0.05 J ND ND ND ND 0.05 J ND ------------ND
07/09/07 ---5.50 0.07 J 0.05 J 0.06 J 0.05 J ND ND 0.06 J ND ------------ND
01/14/08 ---5.50 0.08 J 0.07 J ND ND ND ND 0.06 J ND ND ---------ND
04/30/08 ---5.50 ---------------------------0.14 J ------ND
07/14/08 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
10/03/08 ---5.50 ---------------------------0.16 J ------ND
01/19/09 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
07/20/09 ---5.50 0.04 J 0.05 J ND ND ND ND ND ND ND ND ND ND ND
01/25/10 ---5.50 0.12 J 0.15 J ND ND ND ND ND ND ND ND ------ND
07/06/10 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---5.50 ND 0.12 J ND ND ND ND ND ND ND ND ------ND
07/05/11 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
07/09/12 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/13 ---5.50 ND ND ND ND ND ND ND ND ND ND ------ND
07/17/13 ---5.50 0.15 J 0.10 J ND ND ND ND ND ND ND ND ------ND
01/28/14 ---5.50 0.13 J 0.09 J ND ND ND ---ND ND ND 0.08 J ------ND
05/31/14 ---5.50 ------------------------------ND ND ND
06/24/14 ---5.50 ------------------------------ND ND ND
07/24/14 EPA 6020A 0.09 5.50 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 6020A 0.09 5.50 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 6020A 0.06 5.50 ---1.10 J ND ND ND ---ND ND 0.09 J ND ND ND ND
09/16/15 EPA 6020A 0.06 5.50 0.06 J ---------------------------------ND
01/27/16 EPA 6020B 0.06 5.50 ND 0.17 J ND ND ND ---ND 0.33 J ND 0.07 J ND ND ND
07/27/16 EPA 6020B 0.06 5.50 0.16 J 0.09 J ND ND ND ND ND ND ND ND ND ND ND
Total Vanadium 07/12/05 ---40.0 ND ND ND ND ND ND ND ---------------ND
GWPS = 0.3 µg/L 01/19/06 ---40.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---40.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---40.0 ---------------------ND ------------ND
01/17/07 ---25.0 ND ND ND ND ND ND 1.00 J 1.1 J ------------ND
07/09/07 ---25.0 ND ND ND 1.50 B ND ND ND ND ------------1.00 J
01/14/08 ---25.0 1.60 B ND 1.10 B 2.70 B ND 2.00 B ND 1 B ND ---------1.00 J
04/30/08 ---25.0 ---------------------------13.70 J ------1.30 J
07/14/08 ---25.0 ND ND ND ND ND ND ND ND ND 2.00 J ------ND
10/03/08 ---25.0 ---------------------------ND ------ND
01/19/09 ---25.0 ND ND ND ND ND ND ND ND 1.40 J ND ------ND
07/20/09 ---25.0 1.55 B 0.78 B ND 1.63 B ND ND 0.75 B 0.856 B 0.89 B 10.40 J 4.71 J 9.74 J 0.803 J
01/25/10 ---25.0 ND ND 3.64 J ND ND 1.83 J ND ND ND 0.51 J ------ND
07/06/10 ---25.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---25.0 ND 6.03 J ND 10.50 J ND ND ND ND ND 8.25 J ------ND
07/05/11 ---25.0 ND 1.84 J ND 7.12 J 1.42 J 2.51 J ND ND ND 3.39 J ------ND
01/09/12 ---25.0 ND ND ND ND ND ND ND ND ND 8.37 J ------ND
07/09/12 ---25.0 2.41 J 1.85 J ND ND ND ND ND ND ND 1.71 J ------ND
01/28/13 ---25.0 2.24 B ND ND 15.30 B ND ND ND ND ND 6.45 B ------2.68 J
07/17/13 ---25.0 3.64 J ND ND 11.80 J ND ND 2.29 J 15.3 J ND 5.57 J ------ND
01/28/14 ---25.0 ND ND ND 2.50 B ND ---ND 2.65 B 13.9 B 34.3 B ------8.09 J
05/31/14 ---25.0 ------------------------------ND 4.36 J ND
06/24/14 ---25.0 ------------------------------ND ND ND
07/24/14 EPA 6020A 0.93 25.0 1.24 B ND ND 1.44 B ND 10.8 J 1.47 B ND 0.97 B 2.30 B 1.20 B 4.69 B 1.41 J
01/28/15 EPA 6020A 0.93 25.0 1.11 J 2.35 J ND ND 1.38 J ND ND ND 2.37 J 60.7 ND 1.07 J ND
Resample >>03/05/15 ---25.0 ---------------------------15.3 J ------1.40 J
07/30/15 EPA 6020A 1.57 25.0 ---2.09 J ND ND ND ---ND ND 1.79 J 16.4 J ND 2.23 J ND
09/16/15 EPA 6020A 1.57 25.0 1.81 J ---------------------------------ND
01/27/16 EPA 6020B 1.57 25.0 ND ND ND ND ND ---ND 159 ND 13.0 J 1.61 J ND ND
Resample>>03/09/16 EPA 6020A 0.09 1.00 ---------------------17.7 J ------------ND
07/27/16 EPA 6020B 1.57 25.00 ND 1.63 J ND ND ND 1.90 J ND 2.64 J ND 3.21 J ND ND ND
Total Zinc 10/28/98 ---50 ND ND ND ND ND Dry ------------------ND
NC 2L = 1000 µg/L 04/07/99 ---50 50.0 40.0 30.0 ND ND Dry ------------------30.0
12/08/99 ---50 ND 40.0 80.0 ND 60 30.0 ------------------ND
04/27/00 ---50 90.0 70.0 ND 150 ND Dry ------------------ND
10/18/00 ---50 ND ND ND ND ND Dry ND ---------------ND
11/28/00 ---50 ------------------60.0 ------------------
01/03/01 ---50 ------------------ND ------------------
02/08/01 ---50 ------------------ND ------------------
04/19/01 ---50 ND ND ND ---ND Dry ND ---------------ND
12/24/01 ---50 ND ND ND ND ND ND ND ---------------ND
04/23/02 ---50 ND ND ND ND ND ND ND ---------------ND
10/23/02 ---50 ND ND ND 90.0 ND ND ND ---------------ND
04/01/03 ---50 110.0 120.0 50.0 90.0 50.0 70.0 40.0 ---------------30.0
10/28/03 ---50 ND ND ND ND ND ND ND ---------------ND
04/27/04 ---50 ND ND ND ND ND ND ND ---------------ND
10/26/04 ---50 ND ND ND ND ND ND ND ---------------ND
03/15/05 ---50 ND ND ND ND ND ND ND ---------------ND
07/12/05 ---50 ND ND ND ND ND ND ND ---------------ND
01/12/06 ---50 ---------------------ND ------------ND
01/19/06 ---50 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---50 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---50 ---------------------ND ------------ND
01/17/07 ---10.0 18.80 B 23.30 B 12.20 B 12.70 B 5.9 B 10.40 B 15.60 B 7.7 B ------------5.50 J
07/09/07 ---10.0 8.30 J 21.50 3.90 J 4.80 J 4.4 J ND 3.90 J 5.2 J ------------ND
01/14/08 ---10.0 13.30 5.70 B 4.10 B 6.00 B 2.9 B 5.20 B 4.80 B 3.7 B 13.60 ---------1.30 J
04/30/08 ---10.0 ---------------------------18.80 ------ND
07/14/08 ---10.0 10.20 B 7.40 B 4.90 B 6.10 B ND ND 4.40 B 5.9 B ND 6.70 B ------5.00 J
10/03/08 ---10.0 ---------------------------8.70 J ------ND
01/19/09 ---10.0 10.90 4.10 J 4.10 J 10.60 ND ND 4.30 J ND ND ND ------ND
07/20/09 ---10.0 10.30 28.00 9.27 J 12.20 ND ND 7.25 J 5.4 J 8.07 J 17.60 21.7 ND ND
01/25/10 ---10.0 13.00 6.56 J ND 15.30 6.86 J 2.89 J 6.92 J 4.45 J 6.07 J 4.26 J ------ND
07/06/10 ---10.0 12.00 5.01 J ND 9.64 J ND 4.54 J 5.00 J ND 6.07 J ND ------ND
01/04/11 ---10.0 9.70 J 7.51 J ND 14.00 ND ND ND ND ND 8.51 J ------ND
07/05/11 ---10.0 20.60 8.55 J 6.18 J 19.60 4.28 J 7.45 J 7.77 J 5.46 J ND 6.28 J ------ND
01/09/12 ---10.0 12.40 B 3.07 B 3.85 B 13.80 B 2.31 B 3.53 B 7.41 B 73.8 B 3.38 B 7.26 B ------15.90
07/09/12 ---10.0 10.40 J 4.69 J 2.52 B 14.10 3.42 J 2.21 B 5.46 J 5.74 J 6.37 J 3.83 J ------0.30 J
01/28/13 ---10.0 8.93 J 4.76 B 2.66 B 9.37 J 3.84 B 1.55 B 5.26 B 3.96 B 2.93 B 5.01 B ------0.57 J
07/17/13 ---10.0 11.50 5.40 J 3.49 J 11.20 1.66 J 3.98 J 9.59 J 13.0 5.46 J 7.94 J ------ND
01/28/14 ---10.0 10.10 6.11 J 2.11 J 13.10 5.09 J ---4.09 J 6.70 J 9.31 J 15.2 ------ND
05/31/14 ---10.0 ------------------------------15.2 2.42 B 1.03 J
06/24/14 ---10.0 ------------------------------19.0 3.04 B 1.70 J
07/24/14 EPA 6020A 0.64 10.0 11.7 4.34 J 1.85 B 13.0 3.06 B 14.10 3.01 B 5.24 J 4.29 J 4.31 J 7.39 J 1.29 B 0.71 J
01/28/15 EPA 6020A 0.64 10.0 9.68 7.77 5.38 B 14.8 24.8 4.73 B 5.83 B 4.43 B 5.89 B 34.9 11.1 3.41 B 1.38 J
07/30/15 EPA 6020A 1.3 10.0 ---21.5 2.71 J 11.2 13.9 ---9.39 J 5.70 J 5.44 J 15.1 9.79 J 1.97 J ND
09/16/15 EPA 6020A 1.3 10.0 16.10 ---------------------------------1.41 J
01/27/16 EPA 6020B 1.3 10.0 9.58 J 6.70 J 3.17 J 12.6 5.79 J ---7.93 J 85.6 3.42 J 8.98 J 10.0 ND ND
07/27/16 EPA 6020B 1.3 10.0 9.68 J 5.37 B 3.02 B 10.0 J 10.1 J 5.83 B 5.94 B 6.56 B 6.28 B 6.33 B 9.75 B 1.70 B 1.51 J
East Carolina Regional Landfill
Permit No. 08-03 Page 6 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Organic Compounds
Benzene 01/28/13 ---1.0 0.70 J ND ND ND ND ND ND ND ND ND ------ND
NC 2L= 1 µg/L 07/17/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/14 ---1.0 ND ND ND ND ND ---ND ND ND ND ------ND
05/31/14 ---1.0 ------------------------------ND ND ND
06/24/14 ---1.0 ------------------------------ND ND ND
07/24/14 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 8260B 0.2 1.0 ---ND ND ND ND ---ND ND ND ND ND ND ND
09/16/15 EPA 8260B 0.2 1.0 ND ---------------------------------ND
01/27/16 EPA 8260B 0.2 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND
07/27/16 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Carbon Disulfide 07/24/14 EPA 8260B 0.8 100 ND ND ND ND ND 0.80 J ND ND ND ND ND ND ND
NC 2L = 700 µg/L 01/28/15 EPA 8260B 0.8 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 8260B 0.3 100 ---ND ND ND ND ---ND ND ND ND ND ND ND
09/16/15 EPA 8260B 0.5 100 ND ---------------------------------ND
01/27/16 EPA 8260B 0.9 100 ND ND ND ND ND ---ND ND ND ND ND ND ND
07/27/16 EPA 8260B 0.6 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
Chloroform 01/17/07 ---5.0 ND ND ND ND ND 0.63 J ND ND ------------ND
NC 2L = 70 µg/L 07/09/07 ---5.0 ND ND ND ND ND 0.37 J ND ND ------------ND
01/14/08 ---5.0 ND ND ND ND ND 0.62 J ND ND 0.54 J ---------ND
04/30/08 ---5.0 ---------------------------1.0 J ------ND
07/14/08 ---5.0 ND ND ND ND ND 0.66 J ND ND 1.10 J 2.0 J ------ND
10/03/08 ---5.0 ---------------------------2.7 J ------ND
01/19/09 ---5.0 ND ND ND ND ND 0.58 J ND ND 0.52 J 2.6 J ------ND
07/20/09 ---5.0 ND ND ND ND ND 0.52 J ND ND 0.65 J 1.5 J ND 1.30 J ND
01/25/10 ---5.0 ND ND ND ND ND 0.68 J ND ND 1.10 J 3.2 J ------ND
07/06/10 ---5.0 ND ND ND ND ND 0.55 J ND ND ND 1.3 J ------ND
01/04/11 ---5.0 ND ND ND ND ND 0.44 J ND ND ND 2.3 J ------ND
07/05/11 ---5.0 ND ND ND ND ND ND ND ND ND 1.2 J ------ND
01/09/12 ---5.0 ND ND ND ND ND ND ND ND ND 1.2 J ------ND
07/09/12 ---5.0 ND ND ND ND ND 0.50 J ND ND ND 1.1 J ------ND
01/28/13 ---5.0 ND ND ND ND ND 0.50 J ND ND ND 1.2 J ------ND
07/17/13 ---5.0 ND ND ND ND ND 0.50 J ND ND ND 1.8 J ------ND
01/28/14 ---5.0 ND ND ND ND ND ---ND ND ND 1.0 J ------ND
05/31/14 ---5.0 ------------------------------ND 3.2 J ND
06/24/14 ---5.0 ------------------------------ND 4.2 J ND
07/24/14 EPA 8260B 0.2 5.0 ND ND ND ND ND ND ND ND ND 0.5 J ND 3.8 J ND
01/28/15 EPA 8260B 0.2 5.0 ND ND ND ND ND 0.2 J ND ND ND 0.6 J ND 4.7 J ND
07/30/15 EPA 8260B 0.2 5.0 ---ND ND ND ND ---ND ND ND 0.4 J ND 4.4 J ND
09/16/15 EPA 8260B 0.4 5.0 ND ---------------------------------ND
01/27/16 EPA 8260B 0.3 5.0 ND ND ND ND 0.50 J ---ND ND ND 0.60 J ND 2.0 J ND
07/27/16 EPA 8260B 0.3 5.0 ND ND ND ND 3.1 J 0.40 J ND ND ND 0.60 J ND 0.90 J ND
Chloromethane 07/06/10 ---1.0 ND ND ND ND ND ND ND ND 0.43 J ND ------ND
NC 2L = 3 µg/L 01/04/11 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/05/11 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/09/12 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/17/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/14 ---1.0 ND ND ND ND ND ---ND ND ND ND ------ND
05/31/14 ---1.0 ------------------------------ND ND ND
06/24/14 ---1.0 ------------------------------ND ND ND
07/24/14 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 8260B 0.4 1.0 ---ND ND ND ND ---ND ND ND ND ND ND ND
09/16/15 EPA 8260B 0.6 1.0 ND ---------------------------------ND
01/27/16 EPA 8260B 0.4 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND
07/27/16 EPA 8260B 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
1,4- Dichlorobenzene 07/09/12 ---1.0 0.40 J ND ND ND ND ND ND ND ND ND ------ND
NC 2L = 6 µg/L 01/28/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/17/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/14 ---1.0 ND ND ND ND ND ---ND ND ND ND ------ND
05/31/14 ---1.0 ------------------------------ND ND ND
06/24/14 ---1.0 ------------------------------ND ND ND
07/24/14 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/27/16 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride 01/28/13 ---1.0 0.50 J ND ND ND ND ND ND ND ND ND ------ND
NC 2L = 5 µg/L 07/17/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/14 ---1.0 ND ND ND ND ND ---ND ND ND ND ------ND
05/31/14 ---1.0 ------------------------------ND ND ND
06/24/14 ---1.0 ------------------------------ND ND ND
07/24/14 EPA 8260B 0.6 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 8260B 0.6 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 8260B 0.3 1.0 ---ND ND ND ND ---ND ND ND ND ND ND ND
09/16/15 EPA 8260B 0.6 1.0 ND ---------------------------------ND
01/27/16 EPA 8260B 0.5 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND
07/27/16 EPA 8260B 0.5 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 7 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Toluene 01/28/13 ---1.0 1.50 B 0.20 B ND ND ND ND ND ND ND ND ------0.20 J
NC 2L = 200 µg/L 07/17/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/14 ---1.0 ND ND ND ND ND ---ND ND ND ND ------ND
05/31/14 ---1.0 ------------------------------ND ND 0.30 J
06/24/14 ---1.0 ------------------------------ND ND 0.20 J
07/24/14 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 8260B 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 8260B 0.2 1.0 ---ND ND ND ND ---ND ND ND ND ND ND ND
09/16/15 EPA 8260B 0.2 1.0 ND ---------------------------------0.50 J
01/27/16 EPA 8260B 0.3 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND
07/27/16 EPA 8260B 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Trichloroethene 07/12/05 ---5.0 ND ND ND ND ND ND ND ---------------ND
NC 2L = 3 µg/L 01/19/06 ---5.0 ND ND ND ND ND ND ND ---------------ND
07/11/06 ---5.0 ND ND ND ND ND ND ND ND ------------ND
10/31/06 ---5.0 ---------------------ND ------------ND
01/17/07 ---3.0 ND ND ND ND ND ND ND ND ------------ND
07/09/07 ---1.0 0.47 J ND 0.35 J ND ND ND ND ND ------------ND
01/14/08 ---1.0 ND ND ND ND ND ND ND ND ND ---------ND
04/30/08 ---1.0 ---------------------------ND ------ND
07/14/08 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
10/03/08 ---1.0 ---------------------------ND ------ND
01/19/09 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/20/09 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/25/10 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/06/10 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/04/11 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/05/11 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/09/12 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/09/12 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
07/17/13 ---1.0 ND ND ND ND ND ND ND ND ND ND ------ND
01/28/14 ---1.0 ND ND ND ND ND ---ND ND ND ND ------ND
05/31/14 1.0 ------------------------------ND ND ND
06/24/14 1.0 ------------------------------ND ND ND
07/24/14 EPA 8260B 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/28/15 EPA 8260B 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/30/15 EPA 8260B 0.4 1.0 ---ND ND ND ND ---ND ND ND ND ND ND ND
09/16/15 EPA 8260B 0.4 1.0 ND ------------------------------------
01/27/16 EPA 8260B 0.4 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND
07/27/16 EPA 8260B 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Field Parameters
pH 10/28/98 ------5.38 4.61 5.58 5.76 6.63 Dry ---------------------
(S.U.)04/07/99 ------5.14 4.60 5.38 5.66 6.32 Dry ---------------------
12/08/99 ------5.11 6.31 5.20 5.30 6.02 7.50 ---------------------
04/27/00 ------5.06 4.50 5.28 5.64 5.84 Dry ---------------------
10/18/00 ------4.93 4.19 5.04 5.41 6.04 Dry 6.00 ------------------
11/28/00 ------------------------4.24 ------------------
01/03/01 ------------------------5.83 ------------------
02/08/01 ------------------------5.94 ------------------
04/19/01 ------4.98 4.26 5.07 ---6.27 Dry 5.76 ------------------
12/24/01 ------5.13 4.27 5.03 5.57 6.41 5.46 5.19 ------------------
04/23/02 ------4.97 4.24 4.91 5.40 6.5 5.05 4.89 ------------------
10/23/02 ------4.62 4.02 4.67 5.03 6.05 4.90 5.00 ------------------
04/01/03 ------4.92 4.26 4.99 5.46 6.25 5.41 5.28 ------------------
10/28/03 ------4.74 4.13 5.01 5.31 6.29 5.13 4.97 ------------------
04/27/04 ------4.70 4.19 4.70 5.08 6.03 5.16 4.59 ------------------
10/26/04 ------4.45 3.97 4.49 5.05 5.73 4.74 4.55 ------------------
03/15/05 ------4.70 4.21 5.04 5.32 6.03 5.26 4.78 ------------------
07/12/05 ------4.15 4.17 4.88 4.73 5.6 4.85 4.33 ------------------
01/19/06 ------2.69 2.38 5.05 4.68 6.58 3.56 5.76 ------------------
07/11/06 ------4.64 4.23 4.94 5.17 5.67 5.17 4.81 5.13 ---------------
10/31/06 ---------------------------4.67 ---------------
01/17/07 ------4.01 4.1 4.72 5.1 6.04 5.18 4.7 4.89 ---------------
07/09/07 ------4.31 4.18 5.00 5.20 6.08 4.98 4.65 4.84 ---------------
01/14/08 ------4.34 4.25 4.88 5.42 5.77 5.27 4.99 5.18 5.08 ------------
04/30/08 ---------------------------------4.51 ---------
07/14/08 ------4.47 4.13 4.82 5.22 5.7 5.10 4.72 4.99 5.02 4.68 ---------
10/03/08 ---------------------------------4.33 ---------
01/19/09 ------4.63 4.06 4.85 4.72 5.08 4.75 4.75 4.95 4.50 4.23 ---------
07/20/09 ------4.79 4.29 4.80 5.34 5.55 4.16 3.83 4.46 4.74 4.39 4.23 4.65 ---
01/25/10 ------4.30 4.01 4.63 4.94 5.51 5.02 4.62 4.89 4.51 4.36 ---------
07/06/10 ------4.17 4.08 4.70 5.09 5.49 4.66 4.73 4.17 4.48 4.41 ---------
01/04/11 ------4.55 4.07 4.71 5.73 5.73 5.00 4.72 4.86 4.46 4.48 ---------
07/05/11 ------3.71 3.69 4.29 4.98 4.47 4.43 3.89 4.71 3.68 3.50 ---------
01/09/12 ------4.76 4.42 4.60 5.47 5.81 5.07 4.64 5.38 4.50 4.6 ---------
07/09/12 ------4.83 4.24 4.9 5.24 5.82 5.33 4.89 5.24 4.94 4.8 ---------
01/28/13 ------4.96 4.33 4.98 5.90 5.79 5.21 5.04 5.22 4.79 4.93 ---------
07/17/13 ------4.19 4.00 4.7 5.10 5.29 4.29 4.24 5.01 4.03 4.70 ---------
01/28/14 ------4.99 6.11 5.41 5.66 5.9 5.15 5.28 5.29 4.89 4.98 ---------
05/31/14 ------------------------------------4.01 4.22 ---
06/24/14 ------------------------------------4.15 4.03 ---
07/24/14 ---------4.49 4.18 4.51 4.87 5.14 5.15 4.87 5.36 4.35 4.65 4.22 4.01 ---
01/28/15 FIELD ------5.46 3.85 4.62 4.88 4.83 5.42 4.29 5.08 4.43 4.51 4.39 4.33 ---
03/05/15 ---------------------------------4.63 ---------
07/30/15 FIELD ---------4.38 4.92 5.15 5.68 ---4.89 5.17 4.64 4.98 4.39 4.81 ---
09/16/15 FIELD ------4.58 ------------------------------------
01/27/16 ------4.68 4.43 5.08 4.92 5.00 ---5.04 4.95 4.43 4.66 4.05 4.43 ---
07/27/16 ------4.78 4.83 5.34 5.02 4.77 5.03 4.85 4.88 5.09 5.02 5.11 4.60 ---
East Carolina Regional Landfill
Permit No. 08-03 Page 8 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Conductivity 10/28/98 ------83 257.0 98 78.00 115 Dry ---------------------
(µS/cm)04/07/99 ------69.41 173.0 75.21 52.07 67.89 Dry ---------------------
12/08/99 ------61 306.0 52 89.00 48 41 ---------------------
04/27/00 ------78 210.0 87 57.00 57 Dry ---------------------
10/18/00 ------110 317.0 130 76.00 108 Dry ---------------------
11/28/00 ------------------------191.0 ------------------
01/03/01 ------------------------7.3 ------------------
02/08/01 ------------------------75.0 ------------------
04/19/01 ------106.0 284.0 130.0 ---125 Dry 5.8 ------------------
12/24/01 ------85.0 224.0 105.0 71.00 104 46.0 80.0 ------------------
04/23/02 ------112.0 282.0 136.0 84.00 131 62.0 156.0 ------------------
10/23/02 ------62.0 161.0 77.0 49.00 75 37.0 41.0 ------------------
04/01/03 ------71.0 131.0 86.0 54.00 72 43.0 83.0 ------------------
10/28/03 ------84.0 221.0 89.0 64.00 85 38.0 93.0 ------------------
04/27/04 ------99.0 227.0 108.0 82.00 102 53.0 118.0 ------------------
10/26/04 ------110.0 259.0 115.0 95.00 122 51.0 97.0 ------------------
03/15/05 ------108.0 223.0 94.0 79.00 97 47.0 91.0 ------------------
07/12/05 ------106.0 231.0 98.0 84.00 88 49.0 91.0 ------------------
01/19/06 ------103.0 214.0 100.0 66.00 98 47.0 89.0 ------------------
07/11/06 ------147.0 307.0 146.0 121.00 129 70.0 126.0 106 ---------------
10/31/06 ---------------------------90 ---------------
01/17/07 ------136.0 291.0 164.0 112.00 132 52.0 98.0 92 ---------------
07/09/07 ------134.0 268.0 133.0 115.00 109 54.0 89.0 92 ---------------
01/14/08 ------212.00 442.0 208.0 128.00 279 120.0 252.0 248 53.0 ------------
04/30/08 ---------------------------------77.0 ---------
07/14/08 ------146.00 301.0 155.00 113.00 127 69.0 118.0 107 39.0 82.0 ---------
10/03/08 ---------------------------------79.0 ---------
01/19/09 ------138.0 264.0 164.0 84.00 108 64.0 113.0 100 38.0 86.0 ---------
07/20/09 ------138.0 266.0 161.0 122.0 119 67.0 113.0 100 33.0 77.0 198 26 ---
01/25/10 ------139.0 260.0 149.0 90.0 127 61.0 108.0 100 33.0 76.0 ---------
07/06/10 ------134.0 233.0 145.0 138.0 123 61.0 97.0 134 33.0 76.0 ---------
01/04/11 ------140.0 269.0 148.0 342.0 135 62.0 101.0 100 32.0 82.0 ---------
07/05/11 ------143.0 251.0 145.0 205.0 135 71.0 111.0 100 33.0 78.0 ---------
01/09/12 ------116.0 201.0 111.0 219.0 105 51.0 93.0 79 29.0 62.0 ---------
07/09/12 ------123.9 220.2 136.3 220.9 133.2 63.6 127.4 91.5 36.5 75.7 ---------
01/28/13 ------117.6 190.1 105.1 4.2 108.9 45.9 96.5 79.8 27.5 61.4 ---------
07/17/13 ------104.8 208.1 121.3 220.1 98.7 49.7 92.0 83.9 34.3 69.9 ---------
01/28/14 ------109.1 184.2 115.3 242.7 106.2 45.0 96.1 55.6 29.3 66.7 ---------
05/31/14 ------------------------------------145 22.3 ---
06/24/14 ------------------------------------163.3 23.3 ---
07/24/14 ---------131.1 182.1 118.4 251.6 128.2 53.2 102.8 93.8 45.2 79.0 164.5 23.7 ---
01/28/15 FIELD ------175.3 202.9 102.8 233.0 111.1 42.5 98.0 83.1 38.3 65.2 129.4 22.4 ---
03/05/15 ---------------------------------64.9 ---------
07/30/15 FIELD ---------213 114 187 123 ---98 89 49 72 143 24 ---
09/16/15 FIELD ------129.10 ------------------------------------
01/27/16 ------122.2 177.6 124.8 171.9 123.4 ---145.8 125.3 41.4 64.7 138.9 25.9 ---
07/27/16 ------128.9 179.4 135.8 178.0 131.6 54.2 105.2 107.0 56.5 76.4 151.8 29.6 ---
Temperature 10/28/98 ------15.30 19.00 19.70 18.60 15.9 Dry ---------------------
(ºC)04/07/99 ------16.70 17.30 17.30 15.60 17.6 Dry ---------------------
12/08/99 ------15.10 17.00 25.00 17.10 16.7 17.00 ---------------------
04/27/00 ------15.60 13.10 14.40 13.70 12.9 Dry ---------------------
10/18/00 ------16.70 19.10 19.30 20.40 16.6 Dry ---------------------
11/28/00 ------------------------15.60 ------------------
01/03/01 ------------------------14.50 ------------------
02/08/01 ------------------------16.90 ------------------
04/19/01 ------14.90 31.00 14.70 ---13.7 Dry 17.10 ------------------
12/24/01 ------17.90 20.20 20.70 20.80 17.7 20.10 21.60 ------------------
04/23/02 ------15.90 16.00 15.70 15.60 14.5 18.40 17.10 ------------------
10/23/02 ------15.80 19.10 19.40 20.30 17 17.80 15.70 ------------------
04/01/03 ------16.90 16.40 17.00 14.40 15.7 18.50 17.30 ------------------
10/28/03 ------16.50 19.10 18.00 18.10 15.9 16.60 18.30 ------------------
04/27/04 ------16.00 17.00 15.50 14.00 15 17.30 19.40 ------------------
10/26/04 ------16.80 18.80 19.10 19.70 17 18.00 15.90 ------------------
03/15/05 ------16.18 15.79 15.80 12.86 14.6 17.44 16.39 ------------------
07/12/05 ------16.32 16.80 16.56 18.09 15.97 17.78 17.92 ------------------
01/19/06 ------16.61 17.50 17.51 15.06 15.39 17.88 17.19 ------------------
07/11/06 ------16.10 16.80 17.00 18.20 15.7 17.70 17.30 19.9 ---------------
10/31/06 ---------------------------17.6 ---------------
01/17/07 ------15.60 15.60 15.80 14.50 15 16.60 16.00 14.9 ---------------
07/09/07 ------17.09 17.81 17.53 18.90 17 17.75 17.80 18.61 ---------------
01/14/08 ------16.26 17.88 15.93 15.44 14.32 16.65 17.53 16.65 16.6 ------------
04/30/08 ---------------------------------15.09 ---------
07/14/08 ------17.17 19.03 18.84 20.55 18.13 19.59 18.67 18.44 18.38 16.22 ---------
10/03/08 ---------------------------------16.30 ---------
01/19/09 ------15.32 14.69 15.59 13.80 13.94 16.71 15.22 15.18 13.25 12.81 ---------
07/20/09 ------17.08 19.47 18.99 19.25 16.87 19.62 18.99 19.18 17.43 18.09 18.25 17.64 ---
01/25/10 ------16.60 16.99 16.89 14.08 14.52 18.16 17.10 16.5 15.94 15.68 ---------
07/06/10 ------17.58 20.10 18.72 21.4 16.4 19.7 25.6 17.58 17.78 18.99 ---------
01/04/11 ------16.52 17.09 16.38 14.2 14.7 17.5 16.5 15.5 15.51 15.44 ---------
07/05/11 ------17.6 19.52 19.02 22.2 17.5 21.1 17.9 19.67 16.82 17.90 ---------
01/09/12 ------15.4 15.82 14.83 13.7 13.8 16.0 15.8 13.81 16.40 14.89 ---------
07/09/12 ------17.0 18.30 18.80 19.3 16.2 18.3 19.0 19.3 16.60 18.30 ---------
01/28/13 ------16.7 16.60 16.50 13.20 14.6 17.30 16.90 14.8 16.60 17.00 ---------
07/17/13 ------16.4 18.10 17.90 18.10 15.9 18.00 18.60 21.6 19.80 23.30 ---------
01/28/14 ------14.3 13.30 16.90 10.30 14.6 14.60 14.40 14.4 14.30 14.40 ---------
05/31/14 ------------------------------------15.50 15.90 ---
06/24/14 ------------------------------------16.20 16.60 ---
07/24/14 ---------16.2 17.50 18.00 19.20 15.7 21.00 18.50 19.2 17.00 18.60 19.20 18.10 ---
01/28/15 FIELD ------16.7 16.60 16.20 13.00 11.4 15.40 17.80 15.1 14.60 15.70 13.90 15.30 ---
03/05/15 ---------------------------------13.40 ---------
07/30/15 FIELD ---------23.10 18.56 20.02 16.31 ---20 19.3 17.86 20.10 18.60 19.67 ---
09/16/15 FIELD ------17.00 ------------------------------------
01/27/16 ------16.7 17.1 15.7 14.7 15.3 ---15.5 11.9 15.4 15.3 14.5 15.4 ---
07/27/16 ------19.8 17.8 19.4 20.5 16.3 23.5 20.8 20.8 17.9 20.6 19.5 20.9 ---
East Carolina Regional Landfill
Permit No. 08-03 Page 9 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Turbidity 10/28/98 ------80.0 65.00 19.00 13.00 17 Dry ---------------------
(NTU)04/07/99 ------20.00 1.51 3.13 2.61 2.96 Dry ---------------------
12/08/99 ------20.00 9.46 5.04 2.24 26 19.00 ---------------------
04/27/00 ------32.00 18.00 14.00 7.07 1.76 Dry ---------------------
10/18/00 ------20.40 38.10 9.20 6.39 1.6 Dry 15.90 ------------------
11/28/00 ------------------------11.40 ------------------
01/03/01 ------------------------11.00 ------------------
02/08/01 ------------------------18.00 ------------------
04/19/01 ------169.00 31.00 11.00 ---11 Dry 16.00 ------------------
12/24/01 ------28.00 60.00 5.31 33.00 2.45 61.00 29.00 ------------------
04/23/02 ------27.00 26.00 2.08 290.00 450 11.00 4.28 ------------------
10/23/02 ------6.54 5.77 1.84 3.97 1.35 71.00 6.58 ------------------
04/01/03 ------44.00 23.00 2.63 15.00 91 44.00 10.00 ------------------
10/28/03 ------34.00 25.00 1.80 25.00 7.99 20.00 13.00 ------------------
04/27/04 ------32.00 13.00 0.85 33.00 34 20.00 2.37 ------------------
10/26/04 ------10.00 10.00 0.89 38.00 5.89 29.00 44.00 ------------------
03/15/05 ------68.60 17.90 15.40 43.50 45.1 50.30 26.30 ------------------
07/12/05 ------78.00 29.70 30.30 37.30 30.3 45.20 36.30 ------------------
01/19/06 ------39.20 0.00 0.00 0.00 0 0.00 0.00 ------------------
07/11/06 ------33.60 3.40 1.70 25.40 31 34.50 15.00 78.2 ---------------
10/31/06 ---------------------------193 ---------------
01/17/07 ------13.00 0.00 9.50 23.70 97.2 6.90 8.80 8.3 ---------------
07/09/07 ------0.00 0.00 0.00 0.00 65.8 0.00 0.00 0 ---------------
01/14/08 ------7.31 5.39 1.19 37.50 24 1.29 0.68 9.48 4.1 ------------
04/30/08 --------------------------------->1000 ---------
07/14/08 ------10.60 1.10 1.46 29.50 50.6 2.61 0.40 2.03 8.77 33.10 ---------
10/03/08 ---------------------------------9.54 ---------
01/19/09 ------13.80 1.81 0.41 20.90 5.82 2.99 0.39 1.76 3.04 2.45 ---------
07/20/09 ------8.53 1.50 21.00 36.20 7.84 2.22 1.45 1.67 6.42 45.90 92.0 85.2 ---
01/25/10 ------4.45 3.91 1.46 57.00 29 20.90 3.56 2.75 8.8 14.30 ---------
07/06/10 ------7.74 2.34 0.87 34.90 40 3.37 1.26 7.74 11.3 1.73 ---------
01/04/11 ------9.95 14.30 5.51 42.20 29.8 8.01 1.41 0.78 0.67 82.20 ---------
07/05/11 ------12.90 74.40 1.22 87.50 41.9 29.40 0.94 2.23 0.77 30.60 ---------
01/09/12 ------10.93 9.11 7.20 5.69 10.96 6.21 6.10 28.2 6.07 49.10 ---------
07/09/12 ------15.30 18.70 4.74 19.70 42 4.16 10.10 14.7 7.80 11.50 ---------
01/28/13 ------19.79 20.71 21.09 91.31 11.91 15.29 27.10 20.1 15.26 37.80 ---------
07/17/13 ------7.24 9.71 8.43 11.23 8.61 8.09 7.92 20.92 7.42 8.98 ---------
01/28/14 ------10.28 4.34 3.86 15.80 10.31 14.02 5.94 8.16 9.20 17.02 ---------
05/31/14 ------------------------------------7.26 29.9 ---
06/24/14 ------------------------------------5.60 7.48 ---
07/24/14 ---------5.10 6.50 2.77 3.31 3.9 8.70 3.81 3.76 3.78 18.70 4.12 ------
01/28/15 FIELD ------3.30 8.50 1.25 2.28 9.7 5.29 1.99 1.97 14.30 45.00 2.02 18.20 ---
03/05/15 ---------------------------------------------
07/30/15 FIELD ---------4.1 6.5 4.1 8.1 ---4.8 13.5 12.50 21.00 4.20 ------
09/16/15 FIELD ------16.30 ------------------------------------
01/27/16 ------13.7 4.7 5.21 8.57 3.97 ---5.01 120 8.06 9.86 3.19 4.93 ---
07/27/16 ------4.01 3.9 4.00 4.18 2.98 5.69 4.28 11.70 3.68 6.95 4.64 4.66 ---
Oxidation Reduction Potential 03/15/05 ------363.0 411.0 236.0 121.0 14.0 270.0 319.0 ------------------
(mV)07/12/05 ------407.0 412.0 234.0 173.0 5.0 279.0 375.0 ------------------
01/19/06 ------361.0 370.0 222.0 174.0 16.0 283.0 339.0 ------------------
07/11/06 ------382.0 309.0 312.0 216.0 115.0 317.0 363.0 290.0 ---------------
10/31/06 ---------------------------343.0 ---------------
01/17/07 ------347.0 391.0 306.0 153.0 32.0 290.0 318.0 305.0 ---------------
07/09/07 ------371.0 431.0 309.0 204.0 81.0 290.0 352.0 328.0 ---------------
01/14/08 ------363.0 403.0 342.0 166.0 147.0 317.0 336.0 317.0 308.0 ------------
07/14/08 ------314.0 365.0 248.0 114.0 6.0 247.0 274.0 257.0 243.0 291.0 ---------
10/03/08 ---------------------------------260.0 ---------
01/19/09 ------203.8 260.9 254.4 152.1 193.3 159.2 238.9 213.8 216.4 179.8 ---------
07/20/09 ------302.4 289.1 245.3 122.3 110.0 238.0 223.1 202.5 253.0 285.4 285.2 251.8 ---
01/25/10 ------255.6 310.6 243.0 185.9 144.4 245.0 264.1 244.5 285.2 300.7 ---------
07/06/10 ------76.9 101.1 48.2 151.4 -26.2 57.2 93.5 76.9 224.2 94.6 ---------
01/04/11 ------163.4 274.2 211.4 -5.9 85.4 138.1 160.0 151.7 219.2 243.4 ---------
07/05/11 ------224.2 273.0 245.9 131.1 151.5 207.3 261.7 231.9 260.7 271.0 ---------
01/09/12 ------121.5 95.1 104.1 33.7 -4.9 76.8 99.9 94.0 35.6 63.9 ---------
07/09/12 ------105.2 177.0 135.5 42.6 -41.2 75.7 116.0 103.8 53.1 127.1 ---------
01/28/13 ------289.9 385.8 220.1 19.8 150.1 249.1 288.4 269.7 261.4 287.6 ---------
07/17/13 ------253.1 263.7 100.6 77.3 58.6 214.6 267.1 187.4 196.1 155.3 ---------
01/28/14 ------288.3 202.1 81.4 108.4 159.9 246.0 268.3 269.1 273.5 269.1 ---------
05/31/14 ------------------------------------180.3 171.9 ---
06/24/14 ------------------------------------171.2 181.4 ---
07/24/14 ---------137.5 166.1 146.0 93.8 109.2 84.0 126.4 98.0 145.3 122.9 153.2 171.5 ---
01/28/15 FIELD ------145.9 132.1 150.7 88.7 160.4 177.0 180.8 162.6 190.8 184.3 200.7 170.5 ---
03/05/15 ---------------------------------134.87 ---------
07/30/15 FIELD ---------261.7 239.1 111.3 65.6 ---197.6 182.1 417.1 202.8 275.6 241.3 ---
09/16/15 FIELD ------307.1 ------------------------------------
01/27/16 ------258.9 273.3 339.9 103.3 150.1 ---221.6 227.9 244.1 268.2 342.3 371.0 ---
07/27/16 ------104.5 115.7 96.1 88.6 94.1 85.4 108.2 95.1 118.1 96.4 107.0 100.3 ---
East Carolina Regional Landfill
Permit No. 08-03 Page 10 of 11 Joyce Engineering
TABLE 8
Historical Groundwater Constituents/Analytes
Sample EPA
Analyte
Collection
Date Method DL SWSL GW-2 GW-7 GW-8 GW-9 GW-10 GW-11/11R GW-13 GW-15 GW-16R GW-17 GW-18 GW-21 Blanks
Dissolved Oxygen 03/15/05 ------4.65 2.69 1.61 1.23 1.39 2.10 5.55 ------------------
(mg/L)07/12/05 ------6.22 3.06 0.53 1.83 1.12 2.48 6.90 ------------------
01/19/06 ------3.34 0.00 0.00 0.00 0 0.21 3.71 ------------------
07/11/06 ------9.31 5.50 3.00 3.32 1.6 3.52 7.88 8.05 ---------------
10/31/06 ---------------------------6.3 ---------------
01/17/07 ------8.80 3.90 1.70 2.70 2.1 4.60 7.80 7.9 ---------------
07/09/07 ------6.30 3.20 0.90 1.60 2.3 2.70 6.80 7 ---------------
01/14/08 ------8.12 4.09 4.87 2.56 3.44 3.96 8.25 8.66 6.37 ------------
07/14/08 ------7.46 3.42 1.49 2.37 0.86 2.29 6.24 6.53 4.27 4.21 ---------
10/03/08 ---------------------------------5.07 ---------
01/19/09 ------8.53 3.27 1.79 1.62 1.26 3.01 6.69 7.15 7.2 6.07 ---------
07/20/09 ------7.63 4.89 3.50 2.99 0.99 2.63 6.76 6.81 3.9 4.76 4.97 6.19 ---
01/25/10 ------7.95 4.55 3.54 4.67 1.29 4.89 7.10 7.27 4.4 3.95 ---------
07/06/10 ------7.26 4.86 3.50 0.30 4.04 5.37 5.72 7.26 2.7 3.33 ---------
01/04/11 ------8.43 4.15 4.46 2.30 1.84 6.24 7.95 7.07 1.0 4.04 ---------
07/05/11 ------6.37 3.11 1.25 3.58 0.64 1.84 7.27 7.08 2.4 5.20 ---------
01/09/12 ------6.04 4.44 1.87 0.60 1.41 2.75 4.91 5.5 0.4 2.64 ---------
07/09/12 ------0.45 4.99 3.12 0.52 0.32 1.10 2.62 1.03 0.4 3.18 ---------
01/28/13 ------5.43 5.81 5.79 8.63 0.69 4.09 7.15 7.26 1.9 4.51 ---------
07/17/13 ------5.27 1.64 2.31 0.40 0.18 1.79 5.91 4.95 1.06 3.49 ---------
01/28/14 ------4.93 3.86 3.11 4.52 1.18 5.95 7.68 7.78 7.30 5.26 ---------
05/31/14 ------------------------------------6.57 5.48 ---
06/24/14 ------------------------------------3.54 3.33 ---
07/24/14 ---------4.32 4.40 3.18 1.49 1.61 4.03 4.12 4.34 1.33 3.47 4.51 4.44 ---
01/28/15 FIELD ------7.07 3.51 4.96 1.39 5.07 2.98 5.44 6.05 3.77 4.34 7.66 6.95 ---
03/05/15 ---------------------------------------------
07/30/15 FIELD ---------9.21 2.95 0.63 0.22 ---5.67 4.99 1.41 2.59 7.45 5.84 ---
09/16/15 FIELD ------5.31 ------------------------------------
01/27/16 ------5.59 3.82 4.36 1.01 0.39 ---5.78 8.29 1.85 3.65 5.08 4.80 ---
07/27/16 ------6.17 4.42 1.78 0.42 0.49 2.92 2.72 5.33 0.80 2.72 6.67 2.38 ---
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
PQL = Practical Quantitation Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC 2L = Groundwater Standard established in 15 A NCAC 2L.0202
GWPS = NC DENR Solid Waste Section Groundwater Protection Standard for constituents with no listed NC 2L.
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = insufficient water to sample.
--- = No data.
All inorganic and organic compunds are reported in µg/L
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2L or Groundwater Protection standards (GWPS) have been bolded.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
GW-11 was abandonded and replaced with GW-11R on July 21, 2014.
GW-2 became infested with ants, blocking bladder pump use. The blockage was removed and the system decontaminated before sampling on September 16, 2015.
East Carolina Regional Landfill
Permit No. 08-03 Page 11 of 11 Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Inorganic Compounds
Total Antimony 07/12/05 ---30.00 ND ND ND ND ND
No NC 2B Standard 01/19/06 ---30.00 ND ND ND ND ND
07/12/06 ---30.00 ND ND ND ND ND
01/17/07 ---6.00 ND ND ND ND ND
01/15/08 ---6.00 ND ND ---ND ND
07/14/08 ---6.00 ND ---ND ---ND
01/19/09 ---6.00 ND ---ND ND ND
07/20/09 ---6.00 ------ND ND ND
01/26/10 ---6.00 ND 0.44 J 0.08 J ND ND
07/06/10 ---6.00 ------------ND
01/04/11 ---6.00 ND ---ND ND ND
07/05/11 ---6.00 ND ---------ND
01/10/12 ---6.00 ND 1.19 J ND ND ND
07/09/12 ---6.00 ------ND ---ND
01/28/13 ---6.00 ND 1.60 J ND ND ND
07/17/13 ---6.00 ND ---ND ---0.39 J
01/28/14 ---6.00 ND ---0.24 J ---ND
07/24/14 1.05 6.00 ND ---ND ---ND
01/28/15 1.05 6.00 ND ---ND ---ND
07/30/15 0.25 6.00 ------ND ---ND
01/27/16 0.25 6.00 ---1.52 J ND ---ND
07/27/16 0.25 6.00 ---1.06 J 0.27 J ---ND
Total Arsenic 07/12/05 ---10.0 ND ND ND ND ND
NC 2B = 50 µg/L 01/19/06 ---10.0 ND ND ND ND ND
07/12/06 ---10.0 ND ND ND ND ND
01/17/07 ---10.0 ND ND ND ND 3.40 J
01/15/08 ---10.0 ND ND ---2.60 J ND
07/14/08 ---10.0 ND ---ND ---ND
01/19/09 ---10.0 7.90 B ---ND ND 3.60 J
07/20/09 ---10.0 ------ND 6.32 J ND
01/26/10 ---10.0 ND 6.48 J ND 7.95 J ND
01/04/11 ---10.0 5.15 J ---ND ND ND
07/05/11 ---10.0 ND ---------ND
01/10/12 ---10.0 ND ND ND ND ND
07/09/12 ---10.0 ------1.31 J ---ND
01/28/13 ---10.0 ND ND ND ND ND
07/17/13 ---10.0 1.24 J ---1.01 J ---ND
01/28/14 ---10.0 ND ---ND ---ND
07/24/14 1.13 10.0 ND ---2.28 J ---ND
01/28/15 1.13 10.0 ND ---ND ---ND
07/30/15 0.75 10.0 ------1.12 J ---ND
01/27/16 0.75 10.0 ---1.45 J ND ---ND
07/27/16 0.75 10.0 ---5.13 J 1.26 J ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 1 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Barium 09/16/93 ------100 60.0 90.0 ------
No NC 2B Standard 09/20/93 ------80.0 50.0 120 ------
09/22/93 ------50.0 60.0 140 ------
09/24/93 ------210 50.0 230 ------
10/04/93 ------40.0 70.0 70.0 ------
01/20/94 ------50.0 130 60.0 40.0 ---
07/28/94 ------40.0 ---60.0 50.0 ---
01/26/95 ------80.0 80.0 100 10.0 ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------ND ND ND ND ---
03/15/05 ---500 ND ND ND ND ---
07/12/05 ---500 ND ND ND ND ND
01/19/06 ---500 ND ND ND ND ND
07/12/06 ---500 ND ND ND ND ND
01/17/07 ---100 35.5 44.80 51.90 34.90 0.30 J
01/15/08 ---100 81.3 J 92.10 J ---24.10 J 0.30 J
07/14/08 ---100 60.5 J ---78.8 J ---ND
01/19/09 ---100 82.3 J ---65.2 J 72.20 J ND
07/20/09 ---100 ------112 159 ND
01/26/10 ---100 63.1 J 79.7 J 58.8 J 63.4 J 0.43 J
01/04/11 ---100 56.9 J ---59.60 J 87.60 J 1.11 J
07/05/11 ---100 110 ---------ND
01/10/12 ---100 47.4 J 82.1 J 65.0 J 112 0.24 J
07/09/12 ---100 ------105 ---0.75 J
01/28/13 ---100 124 49.60 J 72.6 J 92.70 J ND
07/17/13 ---100 64.8 J ---69.1 J ---0.37 J
01/28/14 ---100 74.5 J ---73.3 J ---ND
07/24/14 0.10 100 54.2 J ---101 ---0.32 J
01/28/15 0.10 100 46.5 J ---45.8 J ---0.12 J
07/30/15 0.30 100 ------16.5 J ---0.45 J
01/27/16 0.30 100 ---58.8 J 30.6 J ---0.42 J
07/27/16 0.30 100 ---53.1 J ------0.31 J
Total Beryllium 07/12/05 ---2.00 ND ND ND ND ND
NC 2B = 6.5 µg/L 01/19/06 ---2.00 ND ND ND ND ND
07/12/06 ---2.00 ND ND ND ND ND
01/17/07 ---1.00 ND ND ND ND ND
01/15/08 ---1.00 ND ND ---ND ND
07/14/08 ---1.00 ND ---ND ---ND
01/19/09 ---1.00 0.10 J ---ND ND ND
07/20/09 ---1.00 ------ND 1.0 0.08 J
01/26/10 ---1.00 0.26 J 0.3 J 0.21 J 0.4 J ND
01/04/11 ---1.00 0.21 J ---0.18 J 0.2 J ND
07/05/11 ---1.00 0.27 J ---------ND
01/10/12 ---1.00 0.15 J ND 0.70 J 0.4 J ND
07/09/12 ---1.00 ------ND ---ND
01/28/13 ---1.00 0.25 J ND ND 0.2 J ND
07/17/13 ---1.00 0.30 J ---0.32 J ---ND
01/28/14 ---1.00 0.25 J ---ND ---ND
07/24/14 0.05 1.00 0.24 J ---0.21 J ---ND
01/28/15 0.05 1.00 0.18 J ---0.14 J ---ND
07/30/15 0.09 1.00 ------ND ---ND
01/27/16 0.09 1.00 ---ND 0.12 J ---ND
07/27/16 0.09 1.00 ---ND 0.10 J ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 2 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Cadmium 09/16/93 ------ND ND 1.0 ------
NC 2B = 2 µg/L 09/20/93 ------1.0 ND ND ------
09/22/93 ------ND ND ND ------
09/24/93 ------ND ND ND ------
10/04/93 ------ND ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------5.00 ---ND ND ---
01/26/95 ------ND ---ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------1.30 ND ND ND ---
03/15/05 ---1.00 ND ND ND ND ---
07/12/05 ---1.00 ND ND ND ND ND
01/19/06 ---1.00 ND ND ND ND ND
07/12/06 ---1.00 ND ND ND ND ND
01/17/07 ---1.00 ND ND ND ND ND
01/15/08 ---1.00 ND ND ---ND ND
07/14/08 ---1.00 ND ---ND ---ND
01/19/09 ---1.00 0.40 J ---ND ND ND
07/20/09 ---1.00 ------ND 0.27 B 0.11 J
01/26/10 ---1.00 0.35 B 0.41 B 0.24 B 0.69 B 0.28 J
01/04/11 ---1.00 ND ---ND ND ND
07/05/11 ---1.00 ND ---------ND
01/10/12 ---1.00 ND ND ND ND ND
07/09/12 ---1.00 ------ND ---ND
01/28/13 ---1.00 ND ND ND ND ND
07/17/13 ---1.00 ND ---0.6 J ---ND
01/28/14 ---1.00 0.06 J ---ND ---ND
07/24/14 0.05 1.00 ND ---ND ---ND
01/28/15 0.05 1.00 ND ---ND ---ND
07/30/15 0.05 1.00 ------ND ---ND
01/27/16 0.1 1.00 ---ND ND ---ND
07/27/16 0.1 1.00 ---ND ND ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 3 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Chromium 09/16/93 ------ND ND 10 ------
NC 2B = 50 µg/L 09/20/93 ------ND ND ND ------
09/22/93 ------ND ND 10.00 ------
09/24/93 ------70.00 ND 70.00 ------
10/04/93 ------1.00 ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND ND ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------ND ND ND ND ---
10/28/98 ---10.0 ND ND ---------
04/07/99 ---10.0 ND ND ND ND ---
12/08/99 ---10.0 ND ---ND ND ---
04/27/00 ---10.0 ND ND ND ND ---
10/18/00 ---10.0 ND ---ND ------
04/18/01 ---10.0 ND ND ND ND ---
10/24/01 ---10.0 ND ND ND ND ---
04/23/02 ---10.0 ND ND ND ND ---
10/23/02 ---10.0 ND ND ND ND ---
04/01/03 ---10.0 ND ND ND ND ---
10/27/03 ---10.0 ND 40.00 ND ------
04/27/04 ---10.0 ND 40.00 ND ND ---
10/26/04 ---10.0 ND ND ND ND ---
03/15/05 ---10.0 ND ND ND ND ND
07/12/05 ---10.0 ND ND ND ND ND
01/19/06 ---10.0 ND ND ND ND ND
07/12/06 ---10.0 ND ND ND ND ND
01/17/07 ---10.0 ND 3.30 J ND ND ND
01/15/08 ---10.0 ND ND ---ND ND
07/14/08 ---10.0 1.6 J ---ND ---ND
01/19/09 ---10.0 2.90 J ---ND 3.40 J ND
07/20/09 ---10.0 ------ND 38.30 ND
01/26/10 ---10.0 ND 12.10 2.12 J 13.10 ND
01/04/11 ---10.0 1.10 J ---1.40 J 5.21 J ND
07/05/11 ---10.0 5.03 J ---------ND
01/10/12 ---10.0 2.60 J 1.63 J 0.63 J 8.60 J ND
07/09/12 ---10.0 ------ND ---ND
01/28/13 ---10.0 1.82 B 3.22 B 2.92 B 7.65 B 1.38 J
07/17/13 ---10.0 2.99 J ---4.30 J ---ND
01/28/14 ---10.0 6.12 J ---2.13 J ---2.84 J
07/24/14 0.73 10.0 1.00 J ---2.49 J ---ND
01/28/15 0.73 10.0 1.89 J ---1.55 J ---ND
07/30/15 0.43 10.0 ------ND ---ND
01/27/16 0.43 10.0 ---4.06 J 1.71 J ---ND
07/27/16 0.43 10.0 ---3.05 J 1.53 J ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 4 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Cobalt 09/16/93 ------ND ND ND ------
No NC 2B Standard 09/20/93 ------ND ND ND ------
09/22/93 ------ND ND ND ------
09/24/93 ------ND ND ND ------
10/04/93 ------ND ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND 10.00 ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------ND ND ND ND ---
10/28/98 ---10.0 ND ND ---------
04/07/99 ---10.0 ND ND ND ND ---
12/08/99 ---10.0 ND ---ND ND ---
04/27/00 ---10.0 ND ND ND ND ---
10/18/00 ---10.0 ND ---ND ------
04/18/01 ---10.0 ND ND ND ND ---
10/24/01 ---10.0 ND ND ND ND ---
04/23/02 ---10.0 ND ND ND ND ---
10/23/02 ---10.0 ND ND ND ND ---
04/01/03 ---10.0 ND ND ND ND ---
10/27/03 ---10.0 ND 10.00 ND ------
04/27/04 ---10.0 ND ND ND ND ---
10/26/04 ---10.0 ND ND ND ND ---
03/15/05 ---10.0 ND ND ND ND ND
07/12/05 ---10.0 ND ND ND ND ND
01/19/06 ---10.0 ND ND ND ND ND
07/12/06 ---10.0 ND ND ND ND ND
01/17/07 ---10.0 ND ND ND ND ND
01/15/08 ---10.0 ND 2.90 J ---ND ND
07/14/08 ---10.0 ND ---ND ---ND
01/19/09 ---10.0 4.40 J ---ND 1.50 J ND
07/20/09 ---10.0 ------0.97 J 5.81 J ND
01/26/10 ---10.0 2.14 B 2.85 J 1.29 B 2.70 J 0.49 J
01/04/11 ---10.0 1.51 J ---ND 3.01 J ND
07/05/11 ---10.0 ND ---------ND
01/10/12 ---10.0 1.50 J 0.69 J 0.86 J 5.03 J ND
07/09/12 ---10.0 ------1.63 J ---ND
01/28/13 ---10.0 2.30 J 1.03 J 1.32 J 3.34 J ND
07/17/13 ---10.0 2.40 J ---1.73 J ---ND
01/28/14 ---10.0 1.77 J ---0.77 J ---ND
07/24/14 0.26 10.0 1.64 J ---1.81 J ---ND
01/28/15 0.26 10.0 1.46 J ---0.85 J ---ND
07/30/15 0.29 10.0 ------0.36 J ---ND
01/27/16 0.29 10.0 ---1.54 J 0.63 J ---ND
07/27/16 0.29 10.0 ---1.32 J 2.94 J ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 5 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Copper 09/16/93 ------ND ND ND ------
NC 2B = 7 µg/L 09/20/93 ------ND ND 30.0 ------
09/22/93 ------ND ND 30.0 ------
09/24/93 ------20.0 ND 30.0 ------
10/04/93 ------ND ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND ND ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND 50.0 ND ------
04/28/98 ------ND ND ND ND ---
03/15/05 ---200 ND ND ND ND ND
07/12/05 ---200 ND ND ND ND ND
01/19/06 ---200 ND ND ND ND ND
07/12/06 ---200 ND ND ND ND ND
01/17/07 ---10.0 ND 4.50 J ND ND ND
01/15/08 ---10.0 ND ND ---ND 0.70 J
07/14/08 ---10.0 ND ---ND ---ND
01/19/09 ---10.0 3.20 J ---ND ND ND
07/20/09 ---10.0 ------ND 6.67 J 1.25 J
01/26/10 ---10.0 ND 3.19 J ND 4.25 J ND
01/04/11 ---10.0 ND ---1.67 J 2.02 J ND
07/05/11 ---10.0 1.83 J ---------ND
01/10/12 ---10.0 1.74 B 2.04 B 0.98 B 4.10 J 0.66 J
07/09/12 ---10.0 ------ND ---ND
01/28/13 ---10.0 1.27 B 6.90 J 1.30 B 3.79 J 0.26 J
07/17/13 ---10.0 2.44 J ---3.70 J ---ND
01/28/14 ---10.0 2.34 J ---17.6 ---ND
07/24/14 0.22 10.0 1.67 J ---2.54 J ---ND
01/28/15 0.22 10.0 0.86 J ---2.47 J ---ND
07/30/15 0.41 10.0 ------1.29 B ---1.31 J
01/27/16 0.41 10.0 ---12.8 1.79 J ---2.44 J
07/27/16 0.41 10.0 ---2.94 J 0.65 J ---8.47 J
East Carolina Regional Landfill
Permit No. 08-03 Page 6 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Lead 09/16/93 ------ND ND 31.0 ------
NC 2B = 25 µg/L 09/20/93 ------16.0 9.0 19.0 ------
09/22/93 ------7.0 ND 33.0 ------
09/24/93 ------36.0 ND 44.0 ------
10/04/93 ------9.0 ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND ND ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------ND ND ND ND ---
10/28/98 ---10.0 ND ND ---------
04/07/99 ---10.0 ND ND ND ND ---
12/08/99 ---10.0 ND ---ND ND ---
04/27/00 ---10.0 ND ND ND ND ---
10/18/00 ---10.0 ND ---ND ------
04/18/01 ---10.0 ND ND ND ND ---
10/24/01 ---10.0 ND ND ND ND ---
04/23/02 ---10.0 ND ND ND ND ---
10/23/02 ---10.0 ND ND ND ND ---
04/01/03 ---10.0 ND ND ND ND ---
10/27/03 ---10.0 ND 30.0 ND ------
04/27/04 ---10.0 ND 20.0 ND ND ---
10/26/04 ---10.0 ND ND ND ND ---
03/15/05 ---10.0 ND ND ND ND ND
07/12/05 ---10.0 ND ND ND ND ND
01/19/06 ---10.0 ND ND ND ND ND
07/12/06 ---10.0 ND ND ND ND ND
01/17/07 ---10.0 ND ND 2.70 J ND ND
01/15/08 ---10.0 ND ND ---ND ND
07/14/08 ---10.0 2.40 J ---ND ---ND
01/19/09 ---10.0 ND ---ND ND ND
07/20/09 ---10.0 ------1.65 B 18.40 2.16 J
01/26/10 ---10.0 ND 7.63 J 1.42 J 9.38 J ND
01/04/11 ---10.0 ND ---ND ND ND
07/05/11 ---10.0 10.3 ---------ND
01/10/12 ---10.0 2.59 B 3.04 B 1.40 B 4.39 B 0.94 J
07/09/12 ---10.0 ------0.41 J ---ND
01/28/13 ---10.0 0.94 J 1.26 J 0.65 J 4.32 J ND
07/17/13 ---10.0 3.02 J ---2.60 J ---ND
01/28/14 ---10.0 1.77 J ---0.82 J ---ND
07/24/14 0.05 10.0 1.98 J ---1.93 J ---ND
01/28/15 0.05 10.0 0.69 B ---0.71 B ---0.34 J
07/30/15 0.08 10.0 ------ND ---ND
01/27/16 0.08 10.0 ---0.36 J 0.72 J ---ND
07/27/16 0.08 10.0 ---1.65 J 0.66 J ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 7 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Nickel 09/16/93 ------ND ND ND ------
NC 2B = 25 µg/L 09/20/93 ------ND ND ND ------
09/22/93 ------ND ND ND ------
09/24/93 ------ND ND ND ------
10/04/93 ------30.0 ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND ND ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------ND ND ND ND ---
10/28/98 ---50.0 ND ND ---------
04/07/99 ---50.0 ND ND ND ND ---
12/08/99 ---50.0 50.0 ---ND ND ---
04/27/00 ---50.0 ND ND ND ND ---
10/18/00 ---50.0 ND ---ND ------
04/18/01 ---50.0 ND ND ND ND ---
10/24/01 ---50.0 ND ND ND ND ---
04/23/02 ---50.0 ND ND ND ND ---
10/23/02 ---50.0 ND ND ND ND ---
04/01/03 ---50.0 ND ND ND ND ---
10/27/03 ---50.0 ND ND ND ------
04/27/04 ---50.0 ND ND ND ND ---
10/26/04 ---50.0 ND ND ND ND ---
03/15/05 ---50.0 ND ND ND ND ND
07/12/05 ---50.0 ND ND ND ND ND
01/19/06 ---50.0 ND ND ND ND ND
07/12/06 ---50.0 ND ND ND ND ND
01/17/07 ---50.0 ND 3.80 J 2.80 J 3.00 J ND
01/15/08 ---50.0 ND 2.40 J ---ND ND
07/14/08 ---50.0 ND ---ND ---ND
01/19/09 ---50.0 ND ---2.10 B 4.00 B 2.20 J
07/20/09 ---50.0 ------1.72 J 11.40 J ND
01/26/10 ---50.0 ND 2.83 J ND 2.43 J ND
01/04/11 ---50.0 ND ---ND 3.41 J ND
07/05/11 ---50.0 2.76 J ---------ND
01/10/12 ---50.0 2.09 J 3.92 J 1.67 J 7.58 J ND
07/09/12 ---50.0 ------1.10 J ---ND
01/28/13 ---50.0 2.08 J 5.04 J 1.90 J 4.94 J ND
07/17/13 ---50.0 3.23 J ---3.40 J ---ND
01/28/14 ---50.0 2.25 J ---3.88 J ---ND
07/24/14 0.22 50.0 2.27 J ---3.28 J ---ND
01/28/15 0.22 50.0 1.28 J ---2.09 J ---ND
07/30/15 0.48 50.0 ------0.78 J ---ND
01/27/16 0.48 50.0 ---8.69 J 1.52 J ---ND
07/27/16 0.48 50.0 ---7.46 J 2.06 J ---ND
Total Selenium 07/12/05 ---20.00 ND ND ND ND ND
NC 2B = 5 µg/L 01/19/06 ---20.0 ND ND ND ND ND
07/12/06 ---20.0 ND ND ND ND ND
01/17/07 ---10.0 ND ND 3.40 J ND ND
01/15/08 ---10.0 ND ND ---ND ND
07/14/08 ---10.0 ND ---ND ---ND
01/19/09 ---10.0 ND ---ND ND ND
07/20/09 ---10.0 ------ND 6.2 B 3.58 J
01/26/10 ---10.0 ND 1.74 J 0.937 J ND ND
01/04/11 ---10.0 ND ---ND ND ND
07/05/11 ---10.0 ND ---------ND
01/10/12 ---10.0 ND ND ND ND ND
07/09/12 ---10.0 ------ND ---ND
01/28/13 ---10.0 ND 0.99 J ND ND ND
07/17/13 ---10.0 ND ---ND ---ND
01/28/14 ---10.0 ND ---ND ---ND
07/24/14 1.01 10.0 ND ---ND ---ND
01/28/15 1.01 10.0 ND ---ND ---ND
07/30/15 0.85 10.0 ------ND ---ND
01/27/16 0.85 10.0 ---0.98 J ND ---ND
07/27/16 0.85 10.0 ---1.00 J ND ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 8 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Silver 09/16/93 ------ND ND ND ------
NC 2B = 0.06 µg/L 09/20/93 ------ND ND ND ------
09/22/93 ------ND 10.00 ND ------
09/24/93 ------ND ND ND ------
10/04/93 ------ND ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND ND ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
03/15/05 ---10.0 ND ND ND ND ND
07/12/05 ---10.0 ND ND ND ND ND
01/19/06 ---10.0 ND ND ND ND ND
07/12/06 ---10.0 ND ND ND ND ND
01/17/07 ---10.0 ND ND ND ND ND
01/15/08 ---10.0 ND ND ---ND ND
07/14/08 ---10.0 ND ---ND ---ND
01/19/09 ---10.0 2.40 J ---ND ND ND
07/20/09 ---10.0 ------ND ND ND
01/26/10 ---10.0 1.93 B 2.43 B 1.68 B 2.19 B 1.25 J
01/04/11 ---10.0 ND ---ND ND ND
07/05/11 ---10.0 ND ---------ND
01/10/12 ---10.0 ND ND ND ND ND
07/09/12 ---10.0 ------ND ---ND
01/28/13 ---10.0 ND ND ND ND ND
07/17/13 ---10.0 ND ---ND ---ND
01/28/14 ---10.0 ND ---ND ---ND
07/24/14 0.17 10.0 ND ---ND ---ND
01/28/15 0.17 10.0 ND ---ND ---ND
07/30/15 0.22 10.0 ------ND ---ND
01/27/16 0.22 10.0 ---ND ND ---ND
07/27/16 0.22 10.0 ---ND ND ---ND
Total Thallium 07/12/05 ---10.0 ND ND ND ND ND
NC 2B=0.47 µg/L, HH* (3/2016)01/19/06 ---10.0 ND ND ND ND ND
07/12/06 ---10.0 ND ND ND ND ND
01/17/07 ---5.5 ND ND ND ND ND
01/15/08 ---5.5 0.04 J 0.06 J ---ND ND
07/14/08 ---5.5 ND ---ND ---ND
01/19/09 ---5.5 ND ---ND ND ND
07/20/09 ---5.5 ------ND 0.05 J ND
01/26/10 ---5.5 ND ND ND ND ND
01/04/11 ---5.5 ND ---ND ND ND
07/05/11 ---5.5 ND ---------ND
01/10/12 ---5.5 ND ND ND 0.08 J ND
07/09/12 ---5.5 ------ND ---ND
01/28/13 ---5.5 ND ND ND ND ND
07/17/13 ---5.5 ND ---ND ---ND
01/28/14 ---5.5 ND ---ND ---ND
07/24/14 0.09 5.5 ND ---ND ---ND
01/28/15 0.09 5.5 ND ---ND ---ND
07/30/15 0.06 5.5 ------ND ---ND
01/27/16 0.06 5.5 ---ND ND ---ND
07/27/16 0.06 5.5 ---ND ND ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 9 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Vanadium 09/16/93 ------ND ND 40.0 ------
No NC 2B Standard 09/20/93 ------ND ND 70.0 ------
09/22/93 ------30.0 ND 100 ------
09/24/93 ------280 ND 200 ------
10/04/93 ------ND ND ND ------
01/20/94 ------ND ND ND ND ---
07/28/94 ------ND ---ND ND ---
01/26/95 ------ND ND ND ND ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------ND ND ND ------
10/23/97 ------ND ND ND ------
04/28/98 ------ND ND ND ND ---
10/28/98 ---40.0 ND ND ---------
04/07/99 ---40.0 ND ND ND ND ---
12/08/99 ---40.0 ND ---ND ND ---
04/27/00 ---40.0 ND ND ND ND ---
10/18/00 ---40.0 ND ---ND ------
04/18/01 ---40.0 ND ND ND ND ---
10/24/01 ---40.0 ND ND ND ND ---
04/23/02 ---40.0 ND ND ND ND ---
10/23/02 ---40.0 ND ND ND ND ---
04/01/03 ---40.0 ND ND ND ND ---
10/27/03 ---40.0 ND 60.0 ND ------
04/27/04 ---40.0 ND 60.0 ND ND ---
10/26/04 ---40.0 ND ND ND ND ---
03/15/05 ---40.0 ND ND ND ND ND
07/12/05 ---40.0 ND ND ND ND ND
01/19/06 ---40.0 ND ND ND ND ND
07/12/06 ---40.0 ND ND ND ND ND
01/17/07 ---25.0 2.20 J 2.80 J 2.30 J 2.20 J ND
01/15/08 ---25.0 4.10 J ND ---1.00 B 1.00 J
07/14/08 ---25.0 6.30 J ---ND ---ND
01/19/09 ---25.0 2.30 J ---ND 5.70 J ND
07/20/09 ---25.0 ------2.11 B 69.00 0.80 J
01/26/10 ---25.0 1.01 J 23.80 J 4.21 J 23.80 J ND
01/04/11 ---25.0 1.51 J ---2.02 J 10.00 J ND
07/05/11 ---25.0 17.20 J ---------ND
01/10/12 ---25.0 7.62 J 3.93 J ND 13.20 J ND
07/09/12 ---25.0 ------ND ---ND
01/28/13 ---25.0 3.62 B 9.56 B 3.68 B 10.60 B 2.7 J
07/17/13 ---25.0 5.65 J ---8.30 J ---ND
01/28/14 ---25.0 2.37 J ---3.11 J ---ND
07/24/14 0.93 25.0 4.77 B ---7.41 J ---1.41 J
01/28/15 0.93 25.0 1.03 J ---1.97 J ---ND
07/30/15 1.57 25.0 ------2.73 J ---ND
01/27/16 1.57 25.0 ---4.05 J 3.34 J ---ND
07/27/16 1.57 25.0 ---4.54 J 1.93 J ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 10 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Total Zinc 09/16/93 ------30.0 20.0 60.0 ------
NC 2B = 50 µg/L 09/20/93 ------130 40.0 120 ------
09/22/93 ------100 60.0 340 ------
09/24/93 ------240 70.0 420 ------
10/04/93 ------1000 190 70 ------
01/20/94 ------60.0 200 70 70.0 ---
07/28/94 ------120 ---ND 30.0 ---
01/26/95 ------ND 30 60 60.0 ---
07/26/95 ------ND ND ND ------
01/23/96 ------ND ND ND ------
10/10/96 ------ND ND ND ------
04/15/97 ------80.0 60.0 60.0 ------
10/23/97 ------100 60.0 30.0 ------
04/28/98 ------50.0 ND ND ND ---
10/28/98 ---50.0 ND ND ---------
04/07/99 ---50.0 30.0 40.0 30.0 40.0 ---
12/08/99 ---50.0 60.0 ---50.0 60.0 ---
04/27/00 ---50.0 ND 70.0 60.0 ND ---
10/18/00 ---50.0 50.0 ---70.0 ------
04/18/01 ---50.0 ND ND ND ND ---
10/24/01 ---50.0 ND ND ND ND ---
04/23/02 ---50.0 ND 50.0 ND ND ---
10/23/02 ---50.0 ND 60.0 ND ND ---
04/01/03 ---50.0 60.0 30.0 50 70.0 ---
10/27/03 ---50.0 ND 130 70 ------
04/27/04 ---50.0 ND 60.0 ND ND ---
10/26/04 ---50.0 ND ND ND ND ---
03/15/05 ---50.0 ND ND ND ND ND
07/12/05 ---50.0 100 ND ND ND ND
01/19/06 ---50.0 ND ND 79.0 ND ND
07/12/06 ---50.0 ND ND ND ND ND
01/17/07 ---10.0 15.8 B 9.20 B 16.90 B 11.60 B 5.50 J
01/15/08 ---10.0 8.7 J 13.60 ---5.70 B 1.30 J
07/14/08 ---10.0 17.3 B ---7.80 B ---5.00 J
01/19/09 ---10.0 17.0 ---14.00 33.20 ND
07/20/09 ---10.0 ------6.05 J 55.60 ND
01/26/10 ---10.0 8.1 J 17.40 9.78 J 35.20 ND
01/04/11 ---10.0 5.8 J ---8.05 J 64.00 ND
07/05/11 ---10.0 10.5 ---------ND
01/10/12 ---10.0 10.2 B 57.30 B 5.39 B 132.00 15.90
07/09/12 ---10.0 ------1.37 J ---0.30 J
01/28/13 ---10.0 10.9 5.11 B 4.93 B 86.50 0.57 J
07/17/13 ---10.0 17.8 ---11.80 ---ND
01/28/14 ---10.0 15.7 ---4.51 J ---ND
07/24/14 0.64 10.0 6.84 J ---10.2 ---0.71 J
01/28/15 0.64 10.0 6.30 B ---6.99 J ---1.38 J
07/30/15 0.64 10.0 ------4.76 J ---ND
01/27/16 1.3 10.0 ---7.24 J 5.42 J ---ND
07/27/16 1.3 10.0 ---7.01 J 5.20 J ---1.51 J
East Carolina Regional Landfill
Permit No. 08-03 Page 11 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Organic Compounds
Acetone 07/12/05 ---100 ND ND ND ND ND
No NC 2B Standard 01/19/06 ---100 ND ND ND ND ND
07/12/06 ---100 ND ND ND ND ND
01/17/07 ---100 ND ND ND ND ND
01/15/08 ---100 ND ND ---ND ND
07/14/08 ---100 ND ---8.90 J ---ND
01/19/09 ---100 ND ---ND ND ND
07/20/09 ---100 ------5.70 J ND ND
01/26/10 ---100 ND ND ND ND ND
01/04/11 ---100 ND ---ND ND ND
07/05/11 ---100 7.40 J ---------ND
01/10/12 ---100 ND ND ND ND ND
07/09/12 ---100 ------ND ---ND
01/28/13 ---100 ND ND ND ND ND
07/17/13 ---100 ND ---ND ---ND
01/28/14 ---100 ND ---ND ---5.80 J
07/24/14 5.7 100 ND ---5.8 J ---ND
01/28/15 5.7 100 ND ---ND ---ND
07/30/15 3.1 100 ------ND ---ND
01/27/16 4.9 100 ---ND ND ---ND
07/27/16 4.9 100 ---ND ND ---ND
Benzene 01/28/15 0.2 1.0 0.2 J ---ND ---ND
NC 2B = 51 µg/L 07/30/15 0.2 1.0 ------ND ---ND
01/27/16 0.2 1.0 ---ND ND ---ND
07/27/16 0.2 1.0 ---ND ND ---ND
Chloroform 07/30/15 0.2 5.0 ------1.0 J ---ND
01/27/16 0.3 5.0 ---ND ND ---ND
07/27/16 0.3 5.0 ---ND ND ---ND
4-Methyl-2-pentanone (MIBK)09/24/93 ------150.00 ND ND ---ND
NC 2B = 26 µg/L 03/15/05 ---100 ND ND ND ND ND
07/12/05 ---100 ND ND ND ND ND
01/19/06 ---10 ND ND ND ND ND
07/12/06 ---100 ND ND ND ND ND
01/17/07 ---100 ND ND ND ND ND
01/15/08 ---100 ND ND ---ND ND
07/14/08 ---100 ND ---ND ---ND
01/19/09 ---100 ND ---ND ND ND
07/20/09 ---100 ------ND ND ND
01/26/10 ---100 ND ND ND ND ND
01/04/11 ---100 ND ---ND ND ND
07/05/11 ---100 ND ---------ND
01/10/12 ---100 ND ND ND ND ND
07/09/12 ---100 ------ND ---ND
01/28/13 ---100 ND ND ND ND ND
07/17/13 ---100 ND ---ND ---ND
01/28/14 ---100 ND ---ND ---ND
07/24/14 1.4 100 ND ---6.0 J ---ND
01/28/15 1.4 100 ND ---ND ---ND
07/30/15 1 100 ------ND ---ND
01/27/16 1.7 100 ---ND ND ---ND
07/27/16 1.7 100 ---ND ND ---ND
East Carolina Regional Landfill
Permit No. 08-03 Page 12 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Toluene 10/23/97 ------ND ND 20.0 ------
NC 2B = 11 µg/L 10/28/98 ---5.0 ND ND ---------
04/07/99 ---5.0 ND ND ND ND ---
12/08/99 ---5.0 ND ---ND ND ---
04/27/00 ---5.0 ND ND ND ND ---
10/18/00 ---5.0 ND ---ND ------
04/18/01 ---5.0 ND ND ND ND ---
10/24/01 ---5.0 ND ND ND ND ---
04/23/02 ---5.0 ND ND ND ND ---
10/23/02 ---5.0 ND ND ND ND ---
04/01/03 ---5.0 ND ND ND ND ---
10/27/03 ---5.0 ND ND ND ------
04/27/04 ---5.0 ND ND ND ND ---
10/26/04 ---5.0 ND ND ND ND ---
3/15/2005 ---5.0 ND ND ND ND ND
07/12/05 ---5.0 ND ND ND ND ND
01/19/06 ---5.0 ND ND ND ND ND
07/12/06 ---5.0 ND ND ND ND ND
01/17/07 ---5.0 ND ND ND ND ND
01/15/08 ---1.0 ND ND ---ND ND
07/14/08 ---1.0 ND ---ND ---ND
01/19/09 ---1.0 ND ---ND ND ND
07/20/09 ---1.0 ------ND ND 0.44 J
01/26/10 ---1.0 ND ND ND ND ND
01/04/11 ---1.0 ND ---ND ND ND
07/05/11 ---1.0 ND ---------ND
01/10/12 ---1.0 ND ND 0.50 J ND ND
07/09/12 ---1.0 ------ND ---ND
01/28/13 ---1.0 ND ND ND ND ND
07/17/13 ---1.0 ND ---0.40 J ---ND
01/28/14 ---1.0 ND ---ND ---ND
07/24/14 0.2 1.0 ND ---ND ---ND
01/28/15 0.2 1.0 ND ---ND ---ND
07/30/15 0.2 1.0 ------ND ---ND
01/27/16 0.3 1.0 ---ND ND ---ND
07/27/16 0.3 1.0 ---ND 0.30 J ---ND
Xylenes, total 10/23/97 ------ND ND 10.00 ------
NC 2B = 670 µg/L 10/28/98 ---5.0 ND ND ---------
04/07/99 ---5.0 ND ND ND ND ---
12/08/99 ---5.0 ND ---ND ND ---
04/27/00 ---5.0 ND ND ND ND ---
10/18/00 ---5.0 ND ---ND ------
04/18/01 ---5.0 ND ND ND ND ---
10/24/01 ---5.0 ND ND ND ND ---
04/23/02 ---5.0 ND ND ND ND ---
10/23/02 ---5.0 ND ND ND ND ---
04/01/03 ---5.0 ND ND ND ND ---
10/27/03 ---5.0 ND ND ND ------
04/27/04 ---5.0 ND ND ND ND ---
10/26/04 ---5.0 ND ND ND ND ---
03/15/05 ---5.0 ND ND ND ND ND
07/12/05 ---5.0 ND ND ND ND ND
01/19/06 ---5.0 ND ND ND ND ND
07/12/06 ---5.0 ND ND ND ND ND
01/17/07 ---5.0 ND ND ND ND ND
07/14/08 ---5.0 ND ---ND ---ND
01/19/09 ---5.0 ND ---ND ND ND
07/20/09 ---5.0 ------ND ND ND
01/26/10 ---5.0 ND ND ND ND ND
01/04/11 ---5.0 ND ---ND ND ND
01/10/12 ---5.0 ND ND ND ND ND
07/09/12 ---5.0 ------ND ---ND
01/28/13 ---5.0 ND ND ND ND ND
07/17/13 ---5.0 ND ---ND ---ND
01/28/14 ---5.0 ND ---ND ---ND
07/24/14 0.5 5.0 ND ---ND ---ND
01/28/15 0.5 5.0 ND ---ND ---ND
07/30/15 0.2 5.0 ------ND ---ND
01/27/16 0.4 5.0 ---ND ND ---ND
07/27/16 0.4 5.0 ---ND ------ND
East Carolina Regional Landfill
Permit No. 08-03 Page 13 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Field Parameters
pH 10/28/98 ------7.05 5.47 ---------
(S.U.)04/07/99 ------5.26 7.18 6.22 6.74 ---
12/08/99 ------5.04 ---5.56 5.24 ---
04/27/00 ------5.15 6.47 6.02 5.80 ---
10/18/00 ------8.28 ---6.07 ------
04/18/01 ------5.67 7.75 5.96 6.29 ---
10/24/01 ------6.64 6.27 6.39 6.02 ---
04/23/02 ------5.70 6.07 8.16 7.71 ---
10/23/02 ------4.03 6.31 4.78 5.19 ---
04/01/03 ------4.67 8.23 5.80 5.73 ---
10/27/03 ------4.57 5.20 5.55 ------
04/27/04 ------4.88 6.12 5.77 6.62 ---
10/26/04 ------5.82 6.04 5.62 5.57 ---
03/15/05 ------4.51 5.96 5.63 5.67 ---
07/13/05 ------5.55 6.18 5.83 5.38 ---
01/19/06 ------3.54 7.25 5.49 4.51 ---
07/12/06 ------7.10 6.07 5.88 5.65 ---
01/17/07 ------4.57 4.20 5.36 5.26 ---
01/15/08 ------5.63 5.42 ---5.56 ---
07/14/08 ------6.17 ---6.05 ------
01/19/09 ------5.46 ---4.38 4.42 ---
07/20/09 ------------5.92 5.31 ---
01/26/10 ------3.67 6.56 6.49 7.01 ---
01/04/11 ------4.24 ---5.51 4.30 ---
07/05/11 ------7.26 ------------
01/10/12 ------7.30 6.96 7.30 6.72 ---
07/09/12 ------------6.74 ------
01/28/13 ------5.82 8.63 8.98 7.81 ---
07/17/13 ------4.71 ---5.68 ------
01/28/14 ------9.39 ---5.14 ------
07/24/14 ------5.26 ---6.00 ------
01/28/15 ------5.76 ---7.24 ------
07/30/15 ------------9.68 ------
01/27/16 ---------5.26 5.41 ------
07/27/16 ---------5.66 5.51 ---
Conductivity 10/28/98 ------50.0 109.0 ---------
(µS/cm)04/07/99 ------31.9 88.3 67.0 55.3 ---
12/08/99 ------29.0 ---32.0 24.0 ---
04/27/00 ------26.0 143.0 48.0 31.0 ---
10/18/00 ------72.0 ---136.0 ------
04/18/01 ------21.0 75.0 48.0 28.0 ---
10/24/01 ------41.0 99.0 72.0 51.0 ---
04/23/02 ------64.0 79.0 80.0 43.0 ---
10/23/02 ------39.0 87.0 50.0 26.0 ---
04/01/03 ------35.0 121.0 42.0 45.0 ---
10/27/03 ------31.0 48.0 50.0 ------
04/27/04 ------58.0 399.0 74.0 72.0 ---
10/26/04 ------62.0 190.0 88.0 40.0 ---
03/15/05 ------32.0 46.0 51.0 38.0 ---
07/13/05 ------64.0 155.0 141.0 76.0 ---
01/19/06 ------31.0 50.0 52.0 43.0 ---
07/12/06 ------50.0 200.0 97.0 101.0 ---
01/17/07 ------14.0 103.0 81.0 51.0 ---
01/15/08 ------108.0 353.0 ---65.0 ---
01/19/09 ------49.0 ---121.0 72.0 ---
07/20/09 ------------149.0 85.0 ---
01/26/10 ------40.0 427.0 87.0 45.0 ---
01/04/11 ------34.0 ---126.0 87.0 ---
07/05/11 ------140.0 ------------
01/10/12 ------80.7 510.0 153.0 97.8 ---
07/09/12 ------------245.3 ------
01/28/13 ------136.3 567.4 191.5 85.8 ---
07/17/13 ------57.6 ---97.4 ------
01/28/14 ------98.4 ---154.2 ------
07/24/14 ------37.8 ---20.1 ------
01/28/15 ------220.0 ---73.5 ------
07/30/15 ------------136 ------
01/27/16 ---------457.1 47.8 ------
07/27/16 ---------840 229.8 ------
East Carolina Regional Landfill
Permit No. 08-03 Page 14 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Temperature 10/28/98 ------13.00 20.30 ---------
(°C)04/07/99 ------18.10 25.10 29.30 23.90 ---
12/08/99 ------8.50 ---11.50 10.60 ---
04/27/00 ------13.10 14.00 13.60 12.60 ---
10/18/00 ------18.10 ---20.10 ------
04/18/01 ------9.20 7.30 8.00 9.10 ---
10/24/01 ------19.30 23.80 25.90 24.90 ---
04/23/02 ------18.70 16.30 26.20 25.40 ---
10/23/02 ------13.50 12.20 12.00 12.00 ---
04/01/03 ------15.40 21.60 26.00 24.20 ---
10/27/03 ------18.60 20.10 20.80 ------
04/27/04 ------16.70 21.90 20.60 22.90 ---
10/26/04 ------15.60 17.40 18.10 17.60 ---
03/15/05 ------12.09 14.65 15.57 10.80 ---
07/13/05 ------25.58 25.31 26.40 24.82 ---
01/19/06 ------8.41 6.76 9.79 9.97 ---
07/12/06 ------24.50 29.70 27.40 25.50 ---
01/17/07 ------11.70 11.80 11.70 11.70 ---
07/17/08 ------23.97 ---27.12 ------
01/19/09 ------5.40 ---2.95 3.76 ---
07/20/09 ------------24.00 21.65 ---
01/26/10 ------8.51 8.97 11.07 8.78 ---
01/04/11 ------4.82 ---6.06 6.16 ---
07/05/11 ------24.60 ------------
01/10/12 ------8.90 9.20 8.00 8.70 ---
07/09/12 ------------29.10 ------
01/28/13 ------5.40 5.00 2.00 4.70 ---
07/17/13 ------24.70 ---27.70 ------
01/28/14 ------2.80 ---5.00 ------
07/24/14 ------23.20 ---26.10 ------
01/28/15 ------4.30 ---4.40 ------
07/30/15 ------------25.5 ------
01/27/16 ---------6.90 5.30 ------
07/27/16 ---------27.9 26.7 ------
Turbidity 10/28/98 ------93.0 99.0 ---------
(NTU)04/07/99 ------4.4 16.0 58.0 20.0 ---
12/08/99 ------13.0 ---50.0 143.0 ---
04/27/00 ------25.0 202.0 148.0 80.0 ---
10/18/00 ------20.0 ---58.0 ------
04/18/01 ------16.1 183.0 23.0 192.0 ---
10/24/01 ------38.0 44.0 78.0 94.0 ---
04/23/02 ------20.0 38.0 34.0 9.3 ---
10/23/02 ------23.0 292.0 75.0 179.0 ---
04/01/03 ------3.0 75.0 16.0 153.0 ---
10/27/03 ------37.0 780.0 2.3 ------
04/27/04 ------18.0 750.0 16.0 11.0 ---
10/26/04 ------73.0 74.0 37.0 79.0 ---
03/15/05 ------24.8 64.3 41.7 274.0 ---
07/13/05 ------141.0 401.0 150.0 546.0 ---
01/19/06 ------62.5 33.2 0.0 242.0 ---
07/12/06 ------16.1 116.0 17.8 71.3 ---
01/17/07 ------1.5 32.8 28.0 121.0 ---
01/15/08 ------177.0 182.0 ---205.0 ---
07/17/08 ------264.0 ---13.3 ------
01/19/09 ------2.9 ---24.7 111.0 ---
07/20/09 ------------25.4 465.0 ---
01/26/10 ------7.1 297.0 65.1 308.0 ---
01/04/11 ------1.5 ---12.9 40.4 ---
07/05/11 ------185.0 ------------
01/10/12 ------13.2 28.7 10.2 53.3 ---
07/09/12 ------------8.1 ------
01/28/13 ------27.9 32.4 21.2 116.0 ---
07/17/13 ------42.6 ---47.6 ------
01/28/14 ------12.8 ---48.1 ------
07/24/14 ------137.0 ---142.0 ------
01/28/15 ------16.8 ---5.2 ------
07/30/15 ------------11.8 ------
01/27/16 ---------9.88 18.6 ------
07/27/16 ---------24.3 49.4 ------
East Carolina Regional Landfill
Permit No. 08-03 Page 15 of 16
Joyce Engineering
TABLE 9
Historical Surface Water Constituents/Analytes
Analyte
Sample Collection
Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Oxidation Reduction Potential 03/15/05 ------345.0 139.0 160.0 152.0 ---
(mV)07/13/05 ------148.0 22.0 73.0 32.0 ---
01/19/06 ------338.0 107.0 122.0 186.0 ---
07/12/06 ------196.0 203.0 193.0 196.0 ---
01/15/08 ------186.0 163.0 ---218.0 ---
07/17/08 ------160.0 ---79.0 ------
01/19/09 ------360.3 ---196.3 131.0 ---
07/20/09 ------------129.9 234.3 ---
01/26/10 ------322.8 203.4 203.6 205.7 ---
01/04/11 ------211.1 ---288.5 281.2 ---
07/05/11 ------63.8 ------------
01/10/12 ---------------------
07/09/12 ------------108.5 ------
01/28/13 ------141.8 46.2 59.6 136.8 ---
07/17/13 ------323.9 ---69.5 ------
01/28/14 ------16.2 ---167.3 ------
07/24/14 ------122.8 ---38.7 ------
01/28/15 ------119.6 ---106.9 ------
07/30/15 ------------74.2 ------
01/27/16 ---------180.7 195.7 ------
07/27/16 ---------33.9 44.2 ------
Dissolved Oxygen 03/15/05 ------6.9 6.9 6.1 7.4 ---
(mg/L)07/13/05 ------5.0 7.5 8.1 5.8 ---
01/19/06 ------5.1 5.9 5.2 6.3 ---
01/17/07 ------5.4 5.4 4.7 6.2 ---
01/15/08 ------11.3 6.0 ---13.5 ---
07/17/08 ------8.0 ---5.8 ------
01/19/09 ------10.0 ---13.1 12.7 ---
07/20/09 ------------6.4 7.1 ---
01/26/10 ------8.74 10.77 9.52 10.49 ---
01/04/11 ------8.08 ---10.95 10.59 ---
07/05/11 ------3.16 ------------
01/10/12 ---------------------
07/09/12 ------------6.7 ------
01/28/13 ------7.4 10.2 11.9 9.5 ---
07/17/13 ------3.2 ---69.5 ------
01/28/14 ------6.4 ---8.0 ------
07/24/14 ------2.7 ---0.3 ------
01/28/15 ------12.4 ---8.8 ------
07/30/15 ------------7.04 ------
01/27/16 ---------6.48 12.24 ------
07/27/16 ---------3.49 1.81 ------
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
PQL = Practical Quantitation Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC 2B = Surface Water Standard established in 15A NCAC 2B (NC Freshwater Aquatic Life Standards)
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = Insufficient water flow for sampling.
--- = No data.
All inorganic and organic compunds are reported in µg/L
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2B Standards.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
East Carolina Regional Landfill
Permit No. 08-03 Page 16 of 16
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Inorganic Compounds
Total Antimony 13-Jul-05 ---30 ND ND
20-Jan-06 ---30 ND ND
12-Jul-06 ---30 ND ND
18-Jan-07 0.58 6.00 5.08 ND
10-Jul-07 0.68 6.00 3.07 J ND
15-Jan-08 0.68 6.00 9.02 ND
15-Jul-08 0.68 6.00 4.20 J ND
20-Jan-09 0.68 6.00 4.21 J ND
21-Jul-09 0.680 6.00 4.05 J ND
26-Jan-10 0.0730 6.00 5.00 J ND
07-Jul-10 2.20 6.00 12.4 J ND
05-Jan-11 2.20 6.00 20.0 ND
06-Jul-11 2.20 6.00 14.1 J ND
10-Jan-12 ---6.00 16.0 ND
09-Jul-12 ---6.00 12.0 ND
29-Jan-13 ---6.00 31.1 ND
17-Jul-13 ---6.00 29.7 B 0.39 J
29-Jan-14 EPA 6020A 0.22 6.00 26.2 ND
24-Jul-14 EPA 6020A 1.05 6.00 30.3 ND
28-Jan-15 EPA 6020A 5.26 6.00 24.6 ND
30-Jul-15 EPA 6020A 1.25 30.0 104 ND
27-Jan-16 EPA 6020B 1.25 30.0 40.5 ND
27-Jul-16 EPA 6020B 0.25 6.0 58.2 ND
Total Arsenic 07-Apr-99 ---10.0 ND ---
08-Dec-99 ---10.0 10.0 ---
27-Apr-00 ---10.0 10.0 ---
15-Mar-05 ---10.0 21.0 ND
13-Jul-05 ---10.0 34.0 ND
20-Jan-06 ---10.0 24.0 ND
12-Jul-06 ---10.0 18.4 ND
18-Jan-07 2 10.0 ND ND
10-Jul-07 2 10.0 ND ND
15-Jan-08 2 10.0 21.8 ND
15-Jul-08 2.8 10.0 26.2 ND
20-Jan-09 2.8 10.0 5.7 B 3.6 J
21-Jul-09 2.80 10.0 43.4 ND
26-Jan-10 3.90 10.0 38.6 ---
07-Jul-10 2.80 10.0 92.6 ND
05-Jan-11 2.80 10.0 72.7 ND
06-Jul-11 2.80 10.0 146 ND
10-Jan-12 ---10.0 107 ND
09-Jul-12 ---10.0 109 ND
29-Jan-13 ---10.0 192 ND
17-Jul-13 ---10.0 175 ND
29-Jan-14 EPA 6020A 0.78 10.0 126 ND
24-Jul-14 EPA 6020A 1.13 10.0 222 ND
28-Jan-15 EPA 6020A 5.66 10.0 132 ND
30-Jul-15 EPA 6020A 3.73 50.0 393 ND
27-Jan-16 EPA 6020B 3.73 50.0 218 ND
27-Jul-16 EPA 6020B 0.75 10.0 325 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 1 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Barium 07-Apr-99 ---500 ND ---
08-Dec-99 ---500 ND ---
27-Apr-00 ---500 ND ---
15-Mar-05 ---500 630 ND
13-Jul-05 ---500 510 ND
20-Jan-06 ---500 883 ND
12-Jul-06 ---500 678 ND
18-Jan-07 0.2 100 624 ND
10-Jul-07 0.2 100 547 ND
15-Jan-08 0.2 100 645 0.3 J
15-Jul-08 1 100 303 ND
20-Jan-09 1 100 347 ND
21-Jul-09 4.20 100 100 ND
26-Jan-10 0.250 100 273 ND
07-Jul-10 1.00 100 392 ND
05-Jan-11 1.00 100 426 ND
06-Jul-11 1.00 100 496 ND
10-Jan-12 ---100 374 0.24 J
09-Jul-12 ---100 449 0.75 J
29-Jan-13 ---100 394 ND
17-Jul-13 ---100 391 ND
29-Jan-14 EPA 6020A 0.25 100 309 ND
24-Jul-14 EPA 6020A 0.10 100 571 0.32 J
28-Jan-15 EPA 6020A 0.48 100 328 ---
30-Jul-15 EPA 6020A 1.49 100 224 0.45 J
27-Jan-16 EPA 6020B 1.49 100 267 0.42 J
27-Jul-16 EPA 6020B 0.30 100 349 0.31 J
Total Beryllium 10-Jan-12 ---1.00 0.10 J ND
09-Jul-12 ---1.00 0.60 J ND
29-Jan-13 ---1.00 ND ND
17-Jul-13 ---1.00 ND ND
29-Jan-14 EPA 6020A 0.11 1.00 ND ND
24-Jul-14 EPA 6020A 0.05 1.00 0.20 J ND
28-Jan-15 EPA 6020A 0.24 1.00 ND ND
30-Jul-15 EPA 6020A 1.88 20.00 ND ND
27-Jan-16 EPA 6020B 0.47 1.00 ND ND
27-Jul-16 EPA 6020B 0.09 1.00 0.14 J ND
East Carolina Regional Landfill
Permit No. 08-03 Page 2 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Cadmium 13-Jul-05 ---1.00 ND ND
20-Jan-06 ---1.00 ND ND
12-Jul-06 ---1.00 ND ND
18-Jan-07 0.5 1.00 ND ND
10-Jul-07 0.5 1.00 ND ND
15-Jan-08 0.5 1.00 ND ND
15-Jul-08 0.36 1.00 ND ND
20-Jan-09 0.36 1.00 ND ND
21-Jul-09 0.0870 1.00 0.126 J ND
26-Jan-10 0.130 1.00 0.347 B 0.226 J
07-Jul-10 0.360 1.00 ND ND
05-Jan-11 0.360 1.00 ND ND
06-Jul-11 0.360 1.00 ND ND
10-Jan-12 ---1.00 ND ND
09-Jul-12 ---1.00 0.34 J ND
29-Jan-13 ---1.00 0.17 J ND
17-Jul-13 ---1.00 ND ND
29-Jan-14 EPA 6020A 0.060 1.00 0.15 J ND
24-Jul-14 EPA 6020A 0.050 1.00 0.23 J ND
28-Jan-15 EPA 6020A 0.23 1.00 0.25 J ND
30-Jul-15 EPA 6020A 0.48 1.00 ND ND
27-Jan-16 EPA 6020B 0.48 2.50 ND ND
27-Jul-16 EPA 6020B 0.10 1.00 ND ND
Total Chromium 13-Jul-05 ---10.0 ND ND
20-Jan-06 ---10.0 ND ND
12-Jul-06 ---10.0 ND ND
18-Jan-07 2 10.0 ND ND
10-Jul-07 2 10.0 ND ND
15-Jan-08 2 10.0 ND ND
15-Jul-08 1 10.0 ND ND
20-Jan-09 1 10.0 ND ND
21-Jul-09 0.710 10.0 57.7 ND
26-Jan-10 1.70 10.0 40.8 ND
07-Jul-10 1.00 10.0 70.5 ND
05-Jan-11 1.00 10.0 59.7 ND
06-Jul-11 1.00 10.0 108 ND
10-Jan-12 ---10.0 92.7 ND
09-Jul-12 ---10.0 168.0 ND
29-Jan-13 ---10.0 121.0 1.38 J
17-Jul-13 ---50.0 132 ND
29-Jan-14 EPA 6020A 0.58 10.0 70 ND
24-Jul-14 EPA 6020A 0.73 10.0 103 ND
28-Jan-15 EPA 6020A 3.64 10.0 97.8 ND
30-Jul-15 EPA 6020A 2.16 50.0 164 ND
27-Jan-16 EPA 6020B 2.16 50.0 205 ND
27-Jul-16 EPA 6020B 0.43 10.0 384 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 3 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Cobalt 07-Apr-99 ---10.0 10.0 ---
08-Dec-99 ---10.0 60.0 ---
27-Apr-00 ---10.0 10.0 ---
15-Mar-05 ---10.0 43.0 ND
13-Jul-05 ---10.0 40.0 ND
20-Jan-06 ---10.0 60.0 ND
12-Jul-06 ---10.0 63.5 ND
18-Jan-07 2 10.0 16.1 ND
10-Jul-07 2 10.0 18.3 ND
15-Jan-08 2 10.0 23.0 ND
15-Jul-08 1.1 10.0 17.1 ND
20-Jan-09 1.1 10.0 13.3 1.1 J
21-Jul-09 0.580 10.0 19.9 ND
26-Jan-10 0.410 10.0 14.8 0.468 J
07-Jul-10 1.10 10.0 20.2 ND
05-Jan-11 1.10 10.0 19.8 ND
06-Jul-11 1.10 10.0 24.7 ND
10-Jan-12 ---10.0 23.0 ND
09-Jul-12 ---10.0 24.6 ND
29-Jan-13 ---10.0 21.0 ND
17-Jul-13 ---20.0 26.5 ND
29-Jan-14 EPA 6020A ---10.0 26.2 ND
24-Jul-14 EPA 6020A ---10.0 15.0 ND
28-Jan-15 EPA 6020A 1.29 10.0 15.5 ND
30-Jul-15 EPA 6020A 1.44 10.0 29.1 ND
27-Jan-16 EPA 6020B 1.44 10.0 26.6 ND
27-Jul-16 EPA 6020B 0.29 10.0 32.8 ND
Total Copper 13-Jul-05 ---200 ND ND
20-Jan-06 ---200 ND ND
12-Jul-06 ---200 ND ND
18-Jan-07 0.6 10.0 ND ND
10-Jul-07 0.6 10.0 ND ND
15-Jan-08 0.6 10.0 ND ND
15-Jul-08 1.6 10.0 8.20 J ND
20-Jan-09 1.6 10.0 ND ND
21-Jul-09 0.810 10.0 ND 1.25 J
26-Jan-10 1.90 10.0 ND ND
07-Jul-10 1.60 10.0 ND ND
05-Jan-11 1.60 10.0 2.57 J ND
06-Jul-11 1.60 10.0 ND ND
10-Jan-12 ---10.0 11.6 0.66 J
09-Jul-12 ---10.0 53.7 ND
29-Jan-13 ---10.0 17.3 0.26 J
17-Jul-13 ---10.0 16.4 ND
29-Jan-14 EPA 6020A 0.38 10.0 12.6 ND
24-Jul-14 EPA 6020A 0.22 10.0 18.0 ND
28-Jan-15 EPA 6020A 1.10 10.0 64.6 ND
30-Jul-15 EPA 6020A 2.04 10.0 17.3 1.31 J
27-Jan-16 EPA 6020B 2.04 50.0 63.8 2.44 J
27-Jul-16 EPA 6020B 0.41 10.0 4.2 J 8.47 J
East Carolina Regional Landfill
Permit No. 08-03 Page 4 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Lead 13-Jul-05 ---10.0 ND ND
20-Jan-06 ---10.0 ND ND
15-Mar-06 ---10.0 ND ND
12-Jul-06 ---10.0 13.0 ND
26-Oct-06 ---10.0 ------
18-Jan-07 2 10.0 ND ND
10-Jul-07 2 10.0 ND ND
15-Jan-08 2 10.0 ND ND
15-Jul-08 1.9 10.0 2.3 J ND
20-Jan-09 1.9 10.0 ND 2.0 J
21-Jul-09 1.60 10.0 5.28 B 2.16 J
26-Jan-10 1.10 10.0 5.68 B 1.84 J
07-Jul-10 1.90 10.0 3.84 J ND
05-Jan-11 1.90 10.0 ND ND
06-Jul-11 1.90 10.0 ND ND
10-Jan-12 ---10.0 2.75 B 0.94 J
09-Jul-12 ---10.0 45.2 ND
29-Jan-13 ---10.0 3.38 J ND
17-Jul-13 ---10.0 0.51 J ND
29-Jan-14 EPA 6020A 0.050 10.0 3.66 J ND
24-Jul-14 EPA 6020A 0.050 10.0 5.53 J ND
28-Jan-15 EPA 6020A 0.24 10.0 4.15 J ND
30-Jul-15 EPA 6020A 0.42 10.0 1.7 J ND
27-Jan-16 EPA 6020B 0.42 10.0 3.00 J ND
27-Jul-16 EPA 6020B 0.08 10.0 3.20 J ND
Total Mercury 29-Jan-14 EPA 7470A 0.064 0.20 0.119 J ND
24-Jul-14 EPA 7470A 0.064 0.20 0.203 ND
28-Jan-15 EPA 7470A 0.064 0.200 0.084 J ND
30-Jul-15 EPA 7470A 0.070 0.200 0.122 J ND
27-Jan-16 EPA 7470A 0.070 0.200 ND ND
27-Jul-16 EPA 7470A 0.880 1.330 ND ---
Total Nickel 07-Apr-99 ---50.0 ND ---
08-Dec-99 ---50.0 30.0 ---
27-Apr-00 ---50.0 50.0 ---
15-Mar-05 ---50.0 85.0 ND
13-Jul-05 ---50.0 86.0 ND
20-Jan-06 ---50.0 74.0 ND
12-Jul-06 ---50.0 ND ND
18-Jan-07 2 50.0 72.2 ND
10-Jul-07 2 50.0 75.8 ND
15-Jan-08 2 50.0 91.6 ND
15-Jul-08 1.8 50.0 55.6 ND
20-Jan-09 1.8 50.0 41.1 J ND
21-Jul-09 0.650 50.0 84.2 ND
26-Jan-10 1.60 50.0 61.1 ND
07-Jul-10 1.80 50.0 89.0 ND
05-Jan-11 1.80 50.0 86.3 ND
06-Jul-11 1.80 50.0 95.0 ND
10-Jan-12 ---50.0 92.0 ND
09-Jul-12 ---50.0 114.0 ND
29-Jan-13 ---50.0 95.0 ND
17-Jul-13 ---100 108 ND
29-Jan-14 EPA 6020A 0.41 50.0 59.0 ND
24-Jul-14 EPA 6020A 0.22 50.0 60.7 ND
28-Jan-15 EPA 6020A 1.08 50.0 81.0 ND
30-Jul-15 EPA 6020A 2.42 50.0 130 ND
27-Jan-16 EPA 6020B 2.42 50.0 123 ND
27-Jul-16 EPA 6020B 0.48 50.0 146 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 5 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Selenium 13-Jul-05 ---20.0 ND ND
20-Jan-06 ---20.0 ND ND
12-Jul-06 ---20.0 ND ND
18-Jan-07 2 10.0 ND ND
10-Jul-07 2 10.0 ND ND
15-Jan-08 2 10.0 3.2 J ND
15-Jul-08 2.7 10.0 ND ND
20-Jan-09 2.7 10.0 ND ND
21-Jul-09 3.40 10.0 5.82 B 3.58 J
26-Jan-10 4.40 10.0 ND ND
07-Jul-10 2.70 10.0 ND ND
05-Jan-11 2.70 10.0 ND ND
06-Jul-11 2.70 10.0 ND ND
10-Jan-12 ---10.0 ND ND
09-Jul-12 ---10.0 4.32 ND
29-Jan-13 ---10.0 1.41 J ND
17-Jul-13 ---10.0 2.74 ND
29-Jan-14 EPA 6020A 0.77 10.0 3.65 J ND
24-Jul-14 EPA 6020A 1.01 10.0 ND ND
28-Jan-15 EPA 6020A 5.06 10.0 ND ND
30-Jul-15 EPA 6020A 4.27 10.0 ND ND
27-Jan-16 EPA 6020B 4.27 10.0 5.74 J ND
27-Jul-16 EPA 6020B 0.85 10.0 ND ND
Total Silver 13-Jul-05 ---10.0 ND ND
20-Jan-06 ---10.0 ND ND
12-Jul-06 ---10.0 ND ND
18-Jan-07 2 10.0 ND ND
10-Jul-07 2 10.0 ND ND
15-Jan-08 2 10.0 ND ND
15-Jul-08 1.9 10.0 ND ND
20-Jan-09 1.9 10.0 ND ND
21-Jul-09 0.960 10.0 1.69 J ND
26-Jan-10 0.480 10.0 2.33 B 1.36 J
07-Jul-10 1.90 10.0 ND ND
05-Jan-11 ---10.0 ND ND
05-Jan-11 1.90 10.0 ND ND
06-Jul-11 1.90 10.0 ND ND
10-Jan-12 ---10.0 0.20 J ND
09-Jul-12 ---10.0 0.47 ND
29-Jan-13 ---10.0 0.29 J ND
17-Jul-13 ---10.0 0.37 J ND
29-Jan-14 EPA 6020A 0.24 10.0 ND ND
24-Jul-14 EPA 6020A 0.17 10.0 0.29 J ND
28-Jan-15 EPA 6020A 0.84 10.0 ND ND
30-Jul-15 EPA 6020A 1.12 10.0 ND ND
27-Jan-16 EPA 6020B 1.12 10.0 ND ND
27-Jul-16 EPA 6020B 0.22 10.0 ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 6 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Thallium 13-Jul-05 ---10.0 ND ND
20-Jan-06 ---10.0 16.0 ND
15-Mar-06 ---10.0 ND ND
12-Jul-06 ---10.0 22.0 ND
26-Oct-06 ---10.0 ------
18-Jan-07 0.044 5.5 0.046 J ND
10-Jul-07 0.036 5.5 ND ND
15-Jan-08 0.036 5.5 ND ND
15-Jul-08 0.036 5.5 ND ND
20-Jan-09 0.036 5.5 ND ND
21-Jul-09 0.0360 5.5 ND ND
26-Jan-10 0.110 5.5 ND ND
07-Jul-10 1.10 5.5 ND ND
05-Jan-11 ---5.5 ND ND
05-Jan-11 1.10 5.5 ND ND
06-Jul-11 1.10 5.5 6.28 J ND
10-Jan-12 ---5.5 ND ND
09-Jul-12 ---5.5 ND ND
29-Jan-13 ---5.5 ND ND
17-Jul-13 ---5.5 ND ND
29-Jan-14 EPA 6020A 0.06 5.5 ND ND
24-Jul-14 EPA 6020A 0.09 5.5 ND ND
28-Jan-15 EPA 6020A 0.46 5.50 ND ND
30-Jul-15 EPA 6020A 0.28 5.50 ND ND
27-Jan-16 EPA 6020B 0.28 5.50 ND ND
27-Jul-16 EPA 6020B 0.06 5.50 ND ND
Total Vanadium 13-Jul-05 ---40.0 ND ND
20-Jan-06 ---40.0 ND ND
12-Jul-06 ---40.0 ND ND
18-Jan-07 1 25.0 24.6 ND
10-Jul-07 1 25.0 39.7 ND
15-Jan-08 1 25.0 55.4 ND
15-Jul-08 1.4 25.0 23.7 J ND
20-Jan-09 1.4 25.0 ND ND
21-Jul-09 0.680 25.0 638 0.803 J
26-Jan-10 0.400 25.0 102 ND
07-Jul-10 1.40 25.0 189 ND
05-Jan-11 1.40 25.0 110 ND
06-Jul-11 1.40 25.0 87.5 ND
10-Jan-12 ---25.0 127 ND
09-Jul-12 ---25.0 199 ND
29-Jan-13 ---125 130 2.68 J
17-Jul-13 ---25.0 123 ND
29-Jan-14 EPA 6020A 1.97 25.0 79.8 ND
24-Jul-14 EPA 6020A 0.93 25.0 88.8 1.41 J
28-Jan-15 EPA 6020A 4.67 25.0 79.6 1.1 J
30-Jul-15 EPA 6020A 7.86 125.0 151 ND
27-Jan-16 EPA 6020B 7.86 125.0 162 ND
27-Jul-16 EPA 6020B 1.57 25.0 238 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 7 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Zinc 07-Apr-99 ---50.0 50 ---
08-Dec-99 ---50.0 160 ---
27-Apr-00 ---50.0 30 ---
15-Mar-05 ---50.0 120 ND
13-Jul-05 ---50.0 100 ND
20-Jan-06 ---50.0 63.0 ND
12-Jul-06 ---50.0 99.6 ND
18-Jan-07 1 10.0 22.1 4.8 J
10-Jul-07 1 10.0 37.5 ND
15-Jan-08 1 10.0 15.2 1.3 J
15-Jul-08 3.8 10.0 80.9 5.0 J
20-Jan-09 3.8 10.0 17.7 ND
21-Jul-09 3.40 10.0 21.0 ND
26-Jan-10 1.60 10.0 14.5 ND
07-Jul-10 3.80 10.0 64.2 ND
05-Jan-11 3.80 10.0 34.9 ND
06-Jul-11 3.80 10.0 41.6 ND
10-Jan-12 ---10.0 62.4 B ND
09-Jul-12 ---10.0 183.0 0.3 J
29-Jan-13 ---10.0 39.9 0.57 J
17-Jul-13 ---10.0 14.2 ND
29-Jan-14 EPA 6020A 0.87 10.0 40.1 ND
24-Jul-14 EPA 6020A 0.64 10.0 314 0.71 J
28-Jan-15 EPA 6020A 3.20 10.0 120 3.15 J
30-Jul-15 EPA 6020A 6.52 10.0 37.3 ND
27-Jan-16 EPA 6020B 6.52 50.0 54.9 ND
27-Jul-16 EPA 6020B 1.30 10.0 181.0 1.51 J
Organic Compounds
Acetone 07-Apr-99 ---100 830 ---
08-Dec-99 ---100 4,300 ---
27-Apr-00 ---100 2,000 ---
15-Mar-05 ---100 28,000 ND
13-Jul-05 ---100 2000 ND
20-Jan-06 ---11,000 11,200 ND
12-Jul-06 ---100 4,810 ND
18-Jan-07 0.9 100 13,000 ND
10-Jul-07 4.5 100 27 J ND
15-Jan-08 45 100 6,700 ND
15-Jul-08 6.2 100 980 ND
20-Jan-09 75 100 4,900 ND
21-Jul-09 15 100 580 ND
26-Jan-10 30 100 3,300 ND
07-Jul-10 30 100 2,800 ND
05-Jan-11 75 100 3,600 ND
06-Jul-11 120 100 12,000 ND
10-Jan-12 ---10,000 16,000 D ND
09-Jul-12 ---5,000 11,000 ND
29-Jan-13 ---10,000 21,000 ND
17-Jul-13 ---2,500 5,800 ND
29-Jan-14 EPA 8260B 6 100 10,000 5.8 J
24-Jul-14 EPA 8260B 6 100 13,000 ND
28-Jan-15 EPA 8260B 570 2,000 5,000 ND
30-Jul-15 EPA 8260B 150 1,000 1,800 ND
27-Jan-16 EPA 8260B 5 100 160 ND
27-Jul-16 EPA 8260B 5 100 9,400 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 8 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Acrylonitrile 29-Jan-14 EPA 8260B 1 200 1.1 J ND
24-Jul-14 EPA 8260B 1 200 ND ND
28-Jan-15 EPA 8260B 0.6 200 ND ND
30-Jul-15 EPA 8260B 0.9 200 ND ND
27-Jan-16 EPA 8260B 1.8 200 ND ND
27-Jul-16 EPA 8260B 1.8 200 ND ND
Benzene 07-Apr-99 ---5.0 ND ---
08-Dec-99 ---5.0 5.0 ---
27-Apr-00 ---5.0 ND ---
15-Mar-05 ---500 ND ND
13-Jul-05 ---5.0 ND ND
20-Jan-06 ---550 ND ND
12-Jul-06 ---5.0 ND ND
18-Jan-07 0.12 3.0 ND ND
10-Jul-07 0.6 1.0 2.0 J ND
15-Jan-08 6 1.0 ND ND
15-Jul-08 2 1.0 ND ND
20-Jan-09 10 1.0 ND ND
21-Jul-09 2.0 1.0 ND ND
26-Jan-10 1.0 1.0 ND ND
07-Jul-10 4.0 1.0 ND ND
05-Jan-11 10 1.0 ND ND
06-Jul-11 68 1.0 ND ND
10-Jan-12 ---1.0 2.9 ND
09-Jul-12 ---1.0 1.0 ND
29-Jan-13 ---1.0 2.4 ND
17-Jul-13 ---1.0 0.8 J ND
29-Jan-14 EPA 8260B 0 1.0 3.5 ND
24-Jul-14 EPA 8260B 0 1.0 1.9 ND
28-Jan-15 EPA 8260B 0.2 1.0 2.6 ND
30-Jul-15 EPA 8260B 0.2 1.0 0.7 J ND
27-Jan-16 EPA 8260B 0.2 1.0 1.0 J ND
27-Jul-16 EPA 8260B 0.2 1.0 2.0 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 9 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Carbon Disulfide 17-Jul-13 ---100 3.3 J ND
29-Jan-14 EPA 8260B 0.8 100 ND ND
24-Jul-14 EPA 8260B 0.8 100 ND ND
28-Jan-15 EPA 8260B 0.8 100 ND ND
30-Jul-15 EPA 8260B 0.3 100 0.5 J ND
27-Jan-16 EPA 8260B 0.9 100 5.0 J ND
27-Jul-16 EPA 8260B 0.6 100 1.2 J ND
Chlorobenzene 10-Jan-12 ---3.0 0.8 J ND
09-Jul-12 ---3.0 3.0 ND
29-Jan-13 ---3.0 0.8 J ND
17-Jul-13 ---3.0 ND 0.8 J
29-Jan-14 EPA 8260B 0.2 3.0 0.9 J ND
24-Jul-14 EPA 8260B 0.2 3.0 0.3 J ND
28-Jan-15 EPA 8260B 0.2 3.0 0.3 J ND
30-Jul-15 EPA 8260B 0.5 3.0 ND ND
27-Jan-16 EPA 8260B 0.4 3.0 ND ND
27-Jul-16 EPA 8260B 0.4 3.0 0.6 J ND
Chloroform 27-Jul-16 EPA 8260B 0.3 5.0 0.3 J ND
1,2-Dichlorobenzene 29-Jan-13 ---5.0 0.4 J ND
17-Jul-13 ---5.0 ND ND
29-Jan-14 EPA 8260B 0.3 5.0 0.4 J ND
24-Jul-14 EPA 8260B 0.3 5.0 ND ND
28-Jan-15 EPA 8260B 0.3 5.0 ND ND
30-Jul-15 EPA 8260B 0.2 5.0 ND ND
27-Jan-16 EPA 8260B 0.5 5.0 ND ND
27-Jul-16 EPA 8260B 0.5 5.0 ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 10 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
1,4-Dichlorobenzene 07-Apr-99 ---5.0 ND ---
08-Dec-99 ---5.0 5.0 ---
27-Apr-00 ---5.0 7.0 ---
15-Mar-05 ---500 ND ND
13-Jul-05 ---5.0 ND ND
20-Jan-06 ---550 ND ND
12-Jul-06 ---5.0 ND ND
18-Jan-07 0.15 3.0 ND ND
10-Jul-07 0.75 1.0 6.6 ND
15-Jan-08 7.5 1.0 ND ND
15-Jul-08 2 1.0 7.2 J ND
20-Jan-09 19 1.0 ND ND
21-Jul-09 3.8 1.0 ND ND
26-Jan-10 2.0 1.0 9.4 J ND
07-Jul-10 7.6 1.0 9.0 J ND
05-Jan-11 19 1.0 ND ND
06-Jul-11 79 1.0 ND ND
10-Jan-12 ---1.0 11 ND
09-Jul-12 ---1.0 1.8 ND
29-Jan-13 ---1.0 9.6 ND
17-Jul-13 ---1.0 4.4 ND
29-Jan-14 EPA 8260B 0.3 1.0 12 ND
24-Jul-14 EPA 8260B 0.3 1.0 5.0 ND
28-Jan-15 EPA 8260B 0.3 1.0 4.8 ND
30-Jul-15 EPA 8260B 0.3 1.0 2.7 ND
27-Jan-16 EPA 8260B 0.2 1.0 3.2 ND
27-Jul-16 EPA 8260B 0.3 1.0 7.0 ND
trans-1,4-Dichloro-2-butene 24-Jul-14 EPA 8260B 2 100 9.4 J ND
28-Jan-15 EPA 8260B 2 100 ND ND
30-Jul-15 EPA 8260B 1 100 ND ND
27-Jan-16 EPA 8260B 2 100 ND ND
27-Jul-16 EPA 8260B 2 100 ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 11 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
1,1-Dichloroethane 07-Apr-99 ---5.0 9.0 ---
08-Dec-99 ---5.0 9.0 ---
27-Apr-00 ---5.0 ND ---
15-Mar-05 ---500 ND ND
13-Jul-05 ---5.0 ND ND
20-Jan-06 ---550 ND ND
12-Jul-06 ---5.0 ND ND
18-Jan-07 0.09 5.0 ND ND
10-Jul-07 0.45 5.0 ND ND
15-Jan-08 4.5 5.0 ND ND
15-Jul-08 3.3 5.0 ND ND
20-Jan-09 16 5.0 ND ND
21-Jul-09 3.3 5.0 ND ND
26-Jan-10 1.0 5.0 ND ND
07-Jul-10 6.6 5.0 ND ND
05-Jan-11 16 5.0 ND ND
06-Jul-11 8.0 5.0 ND ND
10-Jan-12 ---5.0 ND ND
09-Jul-12 ---5.0 ND ND
29-Jan-13 ---5.0 ND ND
17-Jul-13 ---5.0 ND ND
29-Jan-14 EPA 8260B 0.2 5.0 ND ND
24-Jul-14 EPA 8260B 0.2 5.0 ND ND
28-Jan-15 EPA 8260B 0.2 5.0 ND ND
30-Jul-15 EPA 8260B 0.2 5.0 ND ND
27-Jan-16 EPA 8260B 0.4 5.0 ND ND
27-Jul-16 EPA 8260B 0.4 5.0 ND ND
1,2-Dichloroethane 10-Jan-12 ---1.0 1.3 ND
09-Jul-12 ---1.0 0.6 ND
29-Jan-13 ---1.0 1.7 ND
17-Jul-13 ---1.0 ND ND
29-Jan-14 EPA 8260B 0.4 1.0 0.9 J ND
24-Jul-14 EPA 8260B 0.4 1.0 11 ND
28-Jan-15 EPA 8260B 0.4 1.0 ND ND
30-Jul-15 EPA 8260B 0.2 1.0 ND ND
27-Jan-16 EPA 8260B 0.3 1.0 ND ND
27-Jul-16 EPA 8260B 0.3 1.0 0.3 J ND
cis-1,2-Dichloroethene 10-Jan-12 ---5.0 1.3 J ND
09-Jul-12 ---5.0 0.3 ND
29-Jan-13 ---5.0 1.4 J ND
17-Jul-13 ---5.0 0.5 J ND
29-Jan-14 EPA 8260B 0.2 5.0 1.8 J ND
24-Jul-14 EPA 8260B 0.2 5.0 1.4 J ND
28-Jan-15 EPA 8260B 0.2 5.0 ND ND
30-Jul-15 EPA 8260B 0.3 5.0 ND ND
27-Jan-16 EPA 8260B 0.5 5.0 ND ND
27-Jul-16 EPA 8260B 0.5 5.0 ND ND
1,2-Dichloropropane 29-Jan-14 EPA 8260B 0.2 1.0 0.8 J ND
24-Jul-14 EPA 8260B 0.2 1.0 ND ND
30-Jul-15 EPA 8260B 0.2 1.0 ND ND
27-Jan-16 EPA 8260B 0.5 1.0 ND ND
27-Jul-16 EPA 8260B 0.5 1.0 ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 12 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Ethylbenzene 07-Apr-99 ---5.0 26.0 ---
08-Dec-99 ---5.0 49.0 ---
27-Apr-00 ---5.0 35.0 ---
15-Mar-05 ---500 ND ND
13-Jul-05 ---5.0 ND ND
20-Jan-06 ---550 ND ND
12-Jul-06 ---5.0 ND ND
18-Jan-07 0.17 5.0 35.0 J ND
10-Jul-07 0.85 1.0 15.0 ND
15-Jan-08 8.5 1.0 29.0 J ND
15-Jul-08 2 1.0 24.0 ND
20-Jan-09 10 1.0 71.0 ND
21-Jul-09 2.0 1.0 4.0 J ND
26-Jan-10 2.0 1.0 16.0 J ND
07-Jul-10 4.0 1.0 12.0 J ND
05-Jan-11 10 1.0 31.0 J ND
06-Jul-11 62 1.0 ND ND
10-Jan-12 ---1.0 25.0 ND
09-Jul-12 ---1.0 4.1 ND
29-Jan-13 ---1.0 31 ND
17-Jul-13 ---1.0 6.4 ND
29-Jan-14 EPA 8260B 0.2 1.0 38 ND
24-Jul-14 EPA 8260B 0.2 1.0 17 ND
28-Jan-15 EPA 8260B 0.2 1.0 17 ND
30-Jul-15 EPA 8260B 0.2 1.0 4.4 ND
27-Jan-16 EPA 8260B 0.3 1.0 8.00 ND
27-Jul-16 EPA 8260B 0.2 1.0 18.00 ND
Methyl Butyl Ketone (2-Hexanone)13-Jul-05 ---50 ND ND
20-Jan-06 ---5500 ND ND
12-Jul-06 ---50 ND ND
18-Jan-07 0.24 50 17.0 J ND
10-Jul-07 1.2 50 ND ND
15-Jan-08 12 50 ND ND
15-Jul-08 6 50 ND ND
20-Jan-09 34 50 ND ND
21-Jul-09 6.9 50 ND ND
26-Jan-10 14 50 ND ND
07-Jul-10 14 50 ND ND
05-Jan-11 34 50 ND ND
06-Jul-11 88 50 ND ND
10-Jan-12 ---50 27.0 J ND
09-Jul-12 ---50 21.0 ND
29-Jan-13 ---50 41 J ND
17-Jul-13 ---50 8.5 J ND
29-Jan-14 EPA 8260B 0.6 50 41 J ND
24-Jul-14 EPA 8260B 0.6 50 15 J ND
28-Jan-15 EPA 8260B 0.6 50 13 J ND
30-Jul-15 EPA 8260B 0.4 50 6.6 J ND
27-Jan-16 EPA 8260B 0.9 50 12.0 J ND
27-Jul-16 EPA 8260B 0.9 50 16.0 J ND
East Carolina Regional Landfill
Permit No. 08-03 Page 13 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Methylene chloride 07-Apr-99 ---10 68.0 ---
08-Dec-99 ---10 21.0 ---
27-Apr-00 ---10 ND ---
15-Mar-05 ---1000 ND ND
13-Jul-05 ---10 ND ND
20-Jan-06 ---1100 ND ND
12-Jul-06 ---10 ND ND
18-Jan-07 0.088 5.5 ND ND
10-Jul-07 0.44 1.0 ND ND
15-Jan-08 4.4 1.0 ND ND
15-Jul-08 2.4 1.0 ND ND
20-Jan-09 26 1.0 30.0 J ND
21-Jul-09 5.3 1.0 ND ND
26-Jan-10 1.4 1.0 ND ND
07-Jul-10 11 1.0 ND ND
05-Jan-11 26 1.0 ND ND
06-Jul-11 14 1.0 ND ND
10-Jan-12 ---1.0 1.4 B 0.8 J
09-Jul-12 ---1.0 0.2 ND
29-Jan-13 ---1.0 0.2 J ND
17-Jul-13 ---1.0 ND ND
29-Jan-14 EPA 8260B 0.2 1.0 ND ND
24-Jul-14 EPA 8260B 0.6 1.0 9.6 ND
28-Jan-15 EPA 8260B 0.6 1.0 ND ND
30-Jul-15 EPA 8260B 0.3 1.0 ND ND
27-Jan-16 EPA 8260B 0.5 1.0 ND ND
27-Jul-16 EPA 8260B 0.5 1.0 ND ND
Methyl Ethyl Ketone (2-Butanone)07-Apr-99 ---100 660 ---
08-Dec-99 ---100 12,000 ---
27-Apr-00 ---100 4,400 ---
15-Mar-05 ---100 34,000 ND
13-Jul-05 ---100 1800 ND
20-Jan-06 ---11000 16,600 ND
12-Jul-06 ---100 7,870 ND
18-Jan-07 0.56 100 7,300 ND
10-Jul-07 2.8 100 ND ND
15-Jan-08 28 100 7,800 ND
15-Jul-08 4.4 100 960 ND
20-Jan-09 50 100 6,500 ND
21-Jul-09 10 100 660 ND
26-Jan-10 20 100 3,800 ND
07-Jul-10 20 100 3,800 ND
05-Jan-11 50 100 3,900 ND
06-Jul-11 130 100 12,000 ND
10-Jan-12 ---20,000 26,000 ND
09-Jul-12 ---5,000 8,100 ND
29-Jan-13 ---20,000 47,000 ND
17-Jul-13 ---100 3,800 ND
29-Jan-14 EPA 8260B 0.8 100 14,000 ND
24-Jul-14 EPA 8260B 0.8 100 15,000 ND
28-Jan-15 EPA 8260B 85 5,000 5,000 ND
30-Jul-15 EPA 8260B 45 5,000 1,200 J ND
27-Jan-16 EPA 8260B 1 100 160 ND
27-Jul-16 EPA 8260B 1 100 8,100 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 14 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
4-Methyl-2-pentanone (MIBK)07-Apr-99 ---100 ND ---
08-Dec-99 ---100 ND ---
27-Apr-00 ---100 110 ---
15-Mar-05 ---10000 ND ND
13-Jul-05 ---100 ND ND
20-Jan-06 ---11000 ND ND
12-Jul-06 ---100 ND ND
18-Jan-07 0.36 100 95 J ND
10-Jul-07 1.8 100 7.4 J ND
15-Jan-08 18 100 ND ND
15-Jul-08 5.6 100 ND ND
20-Jan-09 55 100 110 J ND
21-Jul-09 11 100 27.0 J ND
26-Jan-10 22 100 180 ND
07-Jul-10 22 100 42.0 J ND
05-Jan-11 55 100 66.0 J ND
06-Jul-11 110 100 160 J ND
10-Jan-12 ---100 220 ND
09-Jul-12 ---100 140 ND
29-Jan-13 ---500 680 ND
17-Jul-13 ---100 98 ND
29-Jan-14 EPA 8260B 1.4 100 190 ND
24-Jul-14 EPA 8260B 1.4 100 85 J ND
28-Jan-15 EPA 8260B 1.4 100 95 J ND
30-Jul-15 EPA 8260B 1.0 100 31 J ND
27-Jan-16 EPA 8260B 1.7 100 140 ND
27-Jul-16 EPA 8260B 1.7 100 90 J ND
Styrene 29-Jan-13 ---1.0 2.4 ND
17-Jul-13 ---1.0 ND ND
29-Jan-14 EPA 8260B 0.2 1.0 7.1 ND
24-Jul-14 EPA 8260B 0.2 1.0 2.4 ND
28-Jan-15 EPA 8260B 0.2 1.0 1.7 ND
30-Jul-15 EPA 8260B 0.2 1.0 2.6 ND
27-Jan-16 EPA 8260B 0.4 1.0 ND ND
27-Jul-16 EPA 8260B 0.4 1.0 3.1 ND
East Carolina Regional Landfill
Permit No. 08-03 Page 15 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Toluene 07-Apr-99 ---5.0 100 ---
08-Dec-99 ---5.0 150 ---
27-Apr-00 ---5.0 120 ---
15-Mar-05 ---500 ND ND
13-Jul-05 ---5.0 ND ND
20-Jan-06 ---550 ND ND
12-Jul-06 ---5.0 255 ND
18-Jan-07 0.15 5.0 36.0 J ND
10-Jul-07 0.75 1.0 9.0 ND
15-Jan-08 7.5 1.0 35.0 J ND
15-Jul-08 2 1.0 23.0 ND
20-Jan-09 14 1.0 120 ND
21-Jul-09 2.7 1.0 ND 0.44 J
26-Jan-10 1.1 1.0 24.0 ND
07-Jul-10 5.4 1.0 14.0 J ND
05-Jan-11 14 1.0 26.0 J ND
06-Jul-11 85 1.0 ND ND
10-Jan-12 ---1.0 33.0 ND
09-Jul-12 ---1.0 7.1 ND
29-Jan-13 ---1.0 33 ND
17-Jul-13 ---1.0 8.7 ND
29-Jan-14 EPA 8260B 0.2 1.0 45 ND
24-Jul-14 EPA 8260B 0.2 1.0 35 ND
28-Jan-15 EPA 8260B 0.2 1.0 100 ND
30-Jul-15 EPA 8260B 0.2 1.0 4.1 ND
27-Jan-16 EPA 8260B 0.3 1.0 12.0 ND
27-Jul-16 EPA 8260B 0.3 1.0 23.0 ND
Trichloroethene 29-Jan-13 ---1.0 0.2 J ND
17-Jul-13 ---1.0 ND 0.4 J
29-Jan-14 EPA 8260B 0.4 1.0 ND ND
24-Jul-14 EPA 8260B 0.4 1.0 ND ND
28-Jan-15 EPA 8260B 0.4 1.0 ND ND
30-Jul-15 EPA 8260B 0.4 1.0 ND ND
27-Jan-16 EPA 8260B 0.4 1.0 ND ND
27-Jul-16 EPA 8260B 0.4 1.0 ND ND
1,1,2-Trichloroethane 10-Jan-12 ---1.0 2.0 ND
09-Jul-12 ---1.0 ND ND
29-Jan-13 ---1.0 ND ND
17-Jul-13 ---1.0 ND ND
29-Jan-14 EPA 8260B 0.3 1.0 ND ND
24-Jul-14 EPA 8260B 0.3 1.0 ND ND
28-Jan-15 EPA 8260B 0.3 1.0 ND ND
30-Jul-15 EPA 8260B 0.4 1.0 ND ND
27-Jan-16 EPA 8260B 0.8 1.0 ND ND
27-Jul-16 EPA 8260B 0.8 1.0 ND ND
Vinyl Chloride 29-Jan-13 ---1.0 0.2 J ND
17-Jul-13 ---1.0 ND ND
29-Jan-14 EPA 8260B 0.3 1.0 ND ND
24-Jul-14 EPA 8260B 0.3 1.0 ND ND
28-Jan-15 EPA 8260B 0.3 1.0 ND ND
30-Jul-15 EPA 8260B 0.4 1.0 ND ND
27-Jan-16 EPA 8260B 0.7 1.0 ND ND
27-Jul-16 EPA 8260B 0.7 1.0 ND ND
East Carolina Regional Landfill
Permit No. 08-03 Page 16 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Xylenes, total 07-Apr-99 ---5.0 30.0 ---
08-Dec-99 ---5.0 62.0 ---
27-Apr-00 ---5.0 56.0 ---
15-Mar-05 ---500 ND ND
13-Jul-05 ---5.0 ND ND
20-Jan-06 ---550 ND ND
12-Jul-06 ---5.0 ND ND
18-Jan-07 0.14 ---60.0 J ND
10-Jul-07 1 4.0 22.0 ND
15-Jan-08 10 5.0 42.0 J ND
15-Jul-08 4 5.0 39.0 ND
20-Jan-09 20 5.0 100 ND
21-Jul-09 4.0 5.0 ND ND
26-Jan-10 4.4 5.0 31.0 ND
07-Jul-10 8.0 5.0 29.0 ND
05-Jan-11 20 5.0 39.0 J ND
06-Jul-11 210 5.0 ND ND
10-Jan-12 ---5.0 51.0 ND
09-Jul-12 ---5.0 10.0 ND
29-Jan-13 ---5.0 57.0 ND
17-Jul-13 ---5.0 16 ND
29-Jan-14 EPA 8260B 0.5 5.0 77 ND
24-Jul-14 EPA 8260B 0.5 5.0 25 ND
28-Jan-15 EPA 8260B 0.5 5.0 32 ND
30-Jul-15 EPA 8260B 0.2 5.0 15 ND
27-Jan-16 EPA 8260B 0.4 5.0 19.0 ND
27-Jul-16 EPA 8260B 0.4 5.0 34.0 ND
Other Parameters
Cyanide, Total 20-Jan-06 ---0.01 ND ND
12-Jul-06 ---0.05 ND ND
18-Jan-07 0.0058 10 ND ND
10-Jul-07 0.01 10 ND ND
15-Jan-08 0.004 10 ND ND
15-Jul-08 0.004 10 ND ND
20-Jan-09 0.004 10 0.0041 J ND
21-Jul-09 0.0047 10 ND ND
26-Jan-10 0.0047 10 0.0054 J ND
07-Jul-10 0.005 0.01 ND ND
05-Jan-11 0.005 0.01 0.0059 J ND
06-Jul-11 0.0039 0.01 ND ND
10-Jan-12 ---20 ND ND
09-Jul-12 ---10 ND ND
29-Jan-13 ---10 14.0 ND
17-Jul-13 ---10 ND ND
29-Jan-14 EPA 9010/9014 10.0 10 10.0 ND
24-Jul-14 EPA 9010/9014 10.0 10 ND ND
28-Jan-15 EPA 9010/9014 50.0 50.0 ND ND
30-Jul-15 EPA 9010/9014 50.0 50.0 ND ND
27-Jan-16 EPA 9010/9014 50.0 50.0 ND ND
27-Jul-16 EPA 9010C/9014 100.0 100.0 ND ---
East Carolina Regional Landfill
Permit No. 08-03 Page 17 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Oil & Grease (HEM)20-Jan-06 ---2 5 ND
12-Jul-06 ---2 19 ND
18-Jan-07 2 ---5 ND
10-Jul-07 3 ---ND ND
15-Jan-08 3 ---9.15 ND
15-Jul-08 3 ---3.00 J ND
20-Jan-09 3 ---5.11 ND
21-Jul-09 3.00 ---5.29 ND
26-Jan-10 3.00 ---ND ND
07-Jul-10 3.56 ---ND ND
05-Jan-11 3 ---7.34 ND
06-Jul-11 3 ---4.82 J ND
10-Jan-12 ---5,200 10,000 ND
09-Jul-12 ---5,700 13,000 ND
29-Jan-13 ---5,400 6,600 ND
17-Jul-13 ---5,300 9,800 ND
29-Jan-14 EPA 1664B 6,600 6,600 7,300 ND
24-Jul-14 EPA 1664B 5,800 5,800 17,000 ND
28-Jan-15 EPA 1664B 6,200 6,200 8,100 ND
30-Jul-15 EPA 1664B 5,800 5,800 14,000 ND
27-Jan-16 EPA 1664B 5,700 5,700 6,000 ND
27-Jul-16 EPA 1664B 6,000 6,000 14,000 ---
Total Phenols as Phenol 15-Mar-05 ---0.05 0.84 ND
20-Jan-06 ---0.2 1 ND
12-Jul-06 ---0.1 1 ND
18-Jan-07 0.01 ---0.92 ND
10-Jul-07 0.02 ---0.03 J ND
15-Jan-08 0.03 ---1.1 ND
15-Jul-08 0.02 ---0.20 ND
20-Jan-09 0.02 ---0.53 ND
21-Jul-09 0.02 ---0.23 ND
26-Jan-10 0.01 ---0.43 ND
07-Jul-10 0.01 ---0.56 ND
05-Jan-11 0.02 ---0.95 ND
06-Jul-11 0.12 ---2.60 ND
10-Jan-12 ---1,000 5,380 ND
09-Jul-12 ---50.0 1,480 ND
29-Jan-13 ---100 3,260 ND
17-Jul-13 ---50.0 448 ND
29-Jan-14 EPA 420.1 100 100 2,420 ND
24-Jul-14 EPA 420.1 250 250 4,340 ND
28-Jan-15 EPA 420.1 250 250 2,190 ND
30-Jul-15 EPA 420.1 50 50 1,040 ND
27-Jan-16 EPA 420.1 50 50 188 ND
27-Jul-16 EPA 420.1 250 250 2,860 ---
East Carolina Regional Landfill
Permit No. 08-03 Page 18 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Total Kjeldahl Nitrogen as N 15-Mar-05 ---0.05 480 ND
20-Jan-06 ---1 495 ND
12-Jul-06 ---0.05 396 ND
18-Jan-07 4 ---440 ND
10-Jul-07 22 ---570 ND
15-Jan-08 22 ---560 0.088
15-Jul-08 2.2 ---320 ND
20-Jan-09 3 ---340 ND
21-Jul-09 9.0 ---550 ND
26-Jan-10 9.0 ---460 ND
07-Jul-10 9 ---720 ND
05-Jan-11 14 ---720 ND
06-Jul-11 16 ---1,000 B 250 J
10-Jan-12 ---40,000 593,000 ND
09-Jul-12 ---40.0 519,000 ND
29-Jan-13 ---80.0 840,000 ND
17-Jul-13 ---50.0 884,000 ND
29-Jan-14 EPA 351.2 8 8000 466,000 ND
24-Jul-14 EPA 351.2 80,000 80,000 700,000 ND
28-Jan-15 EPA 351.2 80,000 80,000 714,000 ---
30-Jul-15 EPA 351.2 20,000 20,000 1,160,000 ---
27-Jan-16 EPA 351.2 80,000 80,000 1,160,000 ND
27-Jul-16 EPA 351.2 200,000 200,000 2,220,000 ---
Nitrate as N 13-Jul-05 ---0.1 ND ND
05-Jan-11 0.025 10 0.072 J ND
06-Jul-11 0.025 10 ND ND
10-Jan-12 ---50.0 280 ND
09-Jul-12 ---50.0 ND ND
29-Jan-13 ---500.0 ND ND
17-Jul-13 ---100 120 ND
29-Jan-14 EPA 9056A 50 50 1500 ND
24-Jul-14 EPA 9056A 50 50 ND ND
28-Jan-15 EPA 9056A 100 100 ND ND
30-Jul-15 EPA 9056A 250 250 ND ND
27-Jan-16 EPA 9056A 50 50 ND ND
27-Jul-16 EPA 9056A 50 50 ND ---
Nitrite as N 29-Jan-14 EPA 9056A 50 50 680 ND
24-Jul-14 EPA 9056A 50 50 340 ND
28-Jan-15 EPA 9056A 100 100 ND ND
30-Jul-15 EPA 9056A 250 250 ND ND
27-Jan-16 EPA 9056A 50 50 ND ND
27-Jul-16 EPA 9056A 50 50 ND ---
Nitrate/Nitrite as N 29-Jan-14 EPA 9056A 50 50 2200 ND
24-Jul-14 EPA 9056A 50 50 350 ND
28-Jan-15 EPA 9056A 100 100 ND ND
30-Jul-15 EPA 9056A 250 250 ND ND
27-Jan-16 EPA 9056A 50 50 ND ND
27-Jul-16 EPA 9056A 50 50 ND ---
East Carolina Regional Landfill
Permit No. 08-03 Page 19 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Sulfate 13-Jul-05 ---2 ND ND
20-Jan-06 ---2 ND ND
12-Jul-06 ---2 6.23 ND
18-Jan-07 0.6 ---29.3 2.25 J
10-Jul-07 0.6 ---34.0 1.1
15-Jan-08 0.06 250 5.6 J ND
15-Jul-08 0.05 250 3.8 J ND
20-Jan-09 0.05 250 2.5 J ND
21-Jul-09 0.078 250 3.1 J ND
26-Jan-10 0.18 250 1.6 B 1.1 J
07-Jul-10 0.12 250 5.4 J ND
05-Jan-11 0.12 250 10.0 J ND
06-Jul-11 0.02 250 4.00 B 1.90 J
10-Jan-12 ---5,000 2,900 J ND
09-Jul-12 ---5,000 ND ND
29-Jan-13 ---10,000 ND ND
17-Jul-13 ---10,000 ND ND
29-Jan-14 EPA 9056A 5,000 5,000 9100.0 ND
24-Jul-14 EPA 9056A 5,000 5,000 ND ND
28-Jan-15 EPA 9056A 1,000 1,000 ND ND
30-Jul-15 EPA 9056A 5,000 5,000 9200.0 ND
27-Jan-16 EPA 9056A 5,000 5,000 ND ND
27-Jul-16 EPA 9056A 5,000 5,000 ND ---
Biochemical Oxygen Demand 15-Mar-05 ---2 1,300 ND
13-Jul-05 ---2 220 J ND
20-Jan-06 ---2 1,910 ND
12-Jul-06 ---2 1,770 ND
18-Jan-07 2 ---593 ND
10-Jul-07 2 ---97.0 ND
15-Jan-08 2 ---620 ND
15-Jul-08 2 ---110 ND
20-Jan-09 2 ---630 ND
21-Jul-09 2.0 ---130 ND
26-Jan-10 2.0 ---130 ND
07-Jul-10 2 ---420 ND
05-Jan-11 2 ---460 ND
06-Jul-11 2 ---890 ND
10-Jan-12 ---45,000 1,380,000 ND
09-Jul-12 ---32.0 560 ND
29-Jan-13 ---65.0 1,820 ND
17-Jul-13 ---25,000 513,000 130
29-Jan-14 SM 5210 B 2.0 32,000 1,470,000 D ND
24-Jul-14 SM 5210 B 2.0 55,000 2,950,000 D ND
28-Jan-15 SM 5210 B 2.0 19,000 375,000 D 120 J
30-Jul-15 SM 5210 B 2.0 34,000 481,000 D ND
27-Jan-16 SM 5210 B 2.0 42,000 244,000 ND
27-Jul-16 SM 5210 B 2.0 213,000 1,890,000 D ---
East Carolina Regional Landfill
Permit No. 08-03 Page 20 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Chemical Oxygen Demand 15-Mar-05 ---10 2,500.00 ND
13-Jul-05 ---10 1,120.00 ND
27-Feb-06 ---40 1,710.00 ND
12-Jul-06 ---10 2,990.00 ND
18-Jan-07 10 ---1,810.00 ND
10-Jul-07 10 ---980.00 ND
15-Jan-08 20 ---1,600.00 ND
15-Jul-08 41 ---950.00 ND
20-Jan-09 20 ---1,300.00 ND
21-Jul-09 6.2 ---990.00 ND
26-Jan-10 5.6 ---920.00 ND
07-Jul-10 28 ---1,700.00 ND
05-Jan-11 14 ---1,700.00 ND
06-Jul-11 100 ---2,500.00 ND
10-Jan-12 ---200,000 4,050,000 ND
09-Jul-12 ---200 3,050,000 ND
29-Jan-13 ---200 4,770,000 5830
17-Jul-13 ---200 2,590,000 ND
29-Jan-14 SM 5220 D 100 100 3,470,000 ND
24-Jul-14 SM 5220 D 200000 200,000 7,850,000 ND
28-Jan-15 SM 5220 D 100 10 2,270,000 ND
30-Jul-15 SM 5220 D 100000 100,000 2,400,000 ND
27-Jan-16 SM 5220 D 50 50 2,630,000 ND
27-Jul-16 SM 5220 D 100000 100,000 5,780,000 ---
Chloroform 27-Jul-16 EPA 8260B 0.3 5 0.30 J ---
Total Suspended Solids 15-Mar-05 ---2 140 ND
12-Jul-06 ---2 264 ND
18-Jan-07 1 ---45.0 ND
10-Jul-07 1 ---21.0 ND
15-Jan-08 1 ---26.0 ND
15-Jul-08 1 ---59.0 ND
20-Jan-09 1 ---85.0 ND
21-Jul-09 1.0 ---17.0 ND
26-Jan-10 1.0 ---23.0 ND
07-Jul-10 1 ---67.0 ND
05-Jan-11 1 ---23.0 ND
06-Jul-11 1 ---36.0 ND
10-Jan-12 ---10,000 78,000 ND
09-Jul-12 ---33 780,000 ND
29-Jan-13 ---5 46,000 ND
17-Jul-13 ---5,000 20,500 ND
29-Jan-14 SM 2540 D 5,000 5,000 49,000 ND
24-Jul-14 SM 2540 D 10,000 10,000 160,000 D ND
28-Jan-15 SM 2540 D 10,000 10,000 46,000 D ND
30-Jul-15 SM 2540 D 9,090 9,090 197,000 D ND
27-Jan-16 SM 2540 D 5,000 5,000 52,500 ND
27-Jul-16 SM 2540 D 10,000 10,000 117,000 D ---
East Carolina Regional Landfill
Permit No. 08-03 Page 21 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Phosphorus-Total 15-Mar-05 ---0.03 1.8 ND
13-Jul-05 ---0.03 2.2 ND
20-Jan-06 ---0.1 2.0 ND
12-Jul-06 ---0.03 1.0 ND
18-Jan-07 0.02 ---1.7 ND
10-Jul-07 0.02 ---2.8 ND
15-Jan-08 0.02 ---2.6 ND
15-Jul-08 0.05 ---1.2 ND
20-Jan-09 0.05 ---0.82 ND
21-Jul-09 0.050 ---0.69 ND
26-Jan-10 0.025 ---1.7 ND
20-Jan-09 0.017 ---0.084 J ND
21-Jul-09 0.021 ---ND ND
26-Jan-10 0.021 ---0.059 B 0.021
07-Jul-10 0.025 ---0.034 J ND
05-Jan-11 0.025 ---0.097 J ND
06-Jul-11 0.025 ---0.041 J ND
10-Jan-12 ---50 280 ND
09-Jul-12 ---50 ND ND
29-Jan-13 ---500 ND ND
17-Jul-13 ---100 120 ND
29-Jan-14 SM 4500-P B,E 0.220 0.22 1240 D ND
24-Jul-14 SM 4500-P B,E 222 222 1900 D ND
28-Jan-15 SM 4500-P B,E 0.22 0.22 4030 D ND
30-Jul-15 SM 4500-P B,E 0.22 0.22 3270 D ND
27-Jan-16 SM 4500-P B,E 222.00 222 2940 D ND
27-Jul-16 SM 4500-P B,E 0.22 222 6930 D ---
Field Parameters
pH 07-Apr-99 ------6.82 ---
(S.U.)15-Mar-05 ------6.34 ---
13-Jul-05 ------7.36 ---
20-Jan-06 ------9.48 ---
12-Jul-06 ------7.22 ---
18-Jan-07 ------6.00 ---
10-Jul-07 ------8.31 ---
15-Jan-08 ------7.53 ---
15-Jul-08 ------7.39 ---
20-Jan-09 ------6.97 ---
21-Jul-09 ------7.93 ---
26-Jan-10 ------7.03 ---
06-Jul-10 ------7.36 ---
05-Jan-11 ------7.50 ---
06-Jul-11 ------7.42 ---
10-Jan-12 ------7.60 ---
09-Jul-12 ------8.15 ---
29-Jan-13 ------7.67 ---
17-Jul-13 ------7.90 ---
29-Jan-14 ---------7.84 ---
24-Jul-14 ---------7.55 ---
28-Jan-15 FIELD FIELD FIELD ------
30-Jul-15 FIELD FIELD 7.82 ---
27-Jan-16 FIELD FIELD 8.27 ---
East Carolina Regional Landfill
Permit No. 08-03 Page 22 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Conductivity 07-Apr-99 ------2,061 ---
(µS/cm)15-Mar-05 ------6,310 ---
13-Jul-05 ------14,500 ---
20-Jan-06 ------4,940 ---
12-Jul-06 ------7,940 ---
18-Jan-07 ------3,400 ---
10-Jul-07 ------9,800 ---
15-Jan-08 ------13,100 ---
15-Jul-08 ------5,700 ---
20-Jan-09 ------4,816 ---
21-Jul-09 ------10,430 ---
26-Jan-10 ------8,672 ---
06-Jul-10 ------11,900 ---
05-Jan-11 ------11,370 ---
06-Jul-11 ------12,810 ---
10-Jan-12 ------12,470 ---
09-Jul-12 ------13,336 ---
29-Jan-13 ------11,016 ---
17-Jul-13 ------14,908 ---
29-Jan-14 ---------12,520 ---
24-Jul-14 ---------11,310 ---
28-Jan-15 FIELD FIELD FIELD ------
30-Jul-15 FIELD FIELD FIELD 19027 ---
27-Jan-16 FIELD FIELD FIELD 55251 ---
Temperature 15-Mar-05 ------12.8 ---
(°C)13-Jul-05 ------28.82 ---
20-Jan-06 ------16.07 ---
12-Jul-06 ------30.0 ---
18-Jan-07 ------7.0 ---
10-Jul-07 ------33.2 ---
15-Jan-08 ------9.95 ---
15-Jul-08 ------29.93 ---
20-Jan-09 ------6.96 ---
21-Jul-09 ------31.07 ---
26-Jan-10 ------13.84 ---
06-Jul-10 ------28.01 ---
05-Jan-11 ------13.21 ---
29-Jan-14 ---------16.20 ---
24-Jul-14 ---------32.70 ---
28-Jan-15 FIELD FIELD FIELD ------
30-Jul-15 FIELD FIELD FIELD 38.90 ---
27-Jan-16 FIELD FIELD 8.40 ---
East Carolina Regional Landfill
Permit No. 08-03 Page 23 of 24
Joyce Engineering
TABLE 10
Historical Leachate Constituents/Analytes
EPA
Analyte
Sample Collection
Date Method DL RL Leachate Blanks
Turbidity 18-Jan-07 ------71.7 ---
(NTU)10-Jul-07 ------33.2 ---
15-Jan-08 ------800.7 ---
15-Jan-08 ------9.95 ---
15-Jul-08 ------294 ---
15-Jul-08 ------294 ---
20-Jan-09 ------212 ---
21-Jul-09 ------189 ---
06-Jul-11 ------27.02 ---
10-Jan-12 ------15.8 ---
09-Jul-12 ------29.6 ---
29-Jan-13 ------17.4 ---
17-Jul-13 ------37.1 ---
29-Jan-14 ---------1000 ---
28-Jan-15 FIELD FIELD FIELD ------
30-Jul-15 FIELD FIELD FIELD >1000 ---
27-Jan-16 FIELD FIELD FIELD >1000 ---
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
SWSL = NC-DENR Solid Waste Section Limit.
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
--- = No data.
Prior to 2012 all "Other Parameters" were reported in mg/L. beginning with the 1/10/12 event they are reported in µg/L
mg/L = milligrams per liter
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
R = Anomalous data.
*8260B analysis diluted by a factor of 10x for the July 2011 event.
*6020A analysis for Antimony and Thallium diluted by a factor of 10x for the July 2011 event.
*Acetone & MEK DF 50x; C.O.D. DF 10x for the January 2012 event.
Phosphorous, total DF 1.11x for Jan. & July 2012 events.
East Carolina Regional Landfill
Permit No. 08-03 Page 24 of 24
Joyce Engineering

Appendix B

Groundwater and Surface Water Field Data Logs

Appendix C

Laboratory Analytical Reports

PACE ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: East Carolina Regional Landfill
Conover, NC 28613
1220 Commerce Street, SW
Mr. Matt Einsmann
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, Inc. certifies
that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the
samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
August 15, 2016
Report Number:AZG0817
Approved:
This report may not be reproduced, except in full, without written approval from Pace Analytical Services, Inc.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
0803-GW2 AZG0817-01 07/27/16 10:50 07/28/16 09:00Ground Water
0803-GW7 AZG0817-02 07/27/16 12:36 07/28/16 09:00Ground Water
0803-GW8 AZG0817-03 07/27/16 09:36 07/28/16 09:00Ground Water
0803-GW9 AZG0817-04 07/27/16 09:48 07/28/16 09:00Ground Water
0803-GW10 AZG0817-05 07/27/16 11:08 07/28/16 09:00Ground Water
0803-GW11R AZG0817-06 07/27/16 10:06 07/28/16 09:00Ground Water
0803-GW13 AZG0817-07 07/27/16 11:23 07/28/16 09:00Ground Water
0803-GW15 AZG0817-08 07/27/16 10:26 07/28/16 09:00Ground Water
0803-GW16R AZG0817-09 07/27/16 11:58 07/28/16 09:00Ground Water
0803-GW17 AZG0817-10 07/27/16 11:38 07/28/16 09:00Ground Water
0803-GW18 AZG0817-11 07/27/16 12:16 07/28/16 09:00Ground Water
0803-GW21 AZG0817-12 07/27/16 12:54 07/28/16 09:00Ground Water
0803-PW1 AZG0817-13 07/27/16 14:34 07/28/16 09:00Ground Water
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW2
Ground Water
AZG0817-01 AZG081707/27/16 10:50
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
EPA 6020B 2.02 ug/L1Antimony6.00 B-01, J 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:0508/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:0508/10/16 08:35
EPA 6020B 357 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:0508/10/16 08:35
EPA 6020B 0.85 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:0508/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:0508/10/16 08:35
EPA 6020B 1.55 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:0508/10/16 08:35
EPA 6020B 8.68 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:0508/10/16 08:35
EPA 6020B 0.76 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:0508/10/16 08:35
EPA 6020B 0.10 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:0508/10/16 08:35
EPA 6020B 7.78 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:0508/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:0508/10/16 08:35
NDEPA 6020B ug/L1Silver10.0 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:0508/10/16 08:35
EPA 6020B 0.16 ug/L1Thallium5.50 J 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:0508/10/16 08:35
NDEPA 6020B ug/L1Vanadium25.0 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:0508/10/16 08:35
EPA 6020B 9.68 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:0508/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 07:4107/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW2
Ground Water
AZG0817-01 AZG081707/27/16 10:50
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 07:4107/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW2
Ground Water
AZG0817-01 AZG081707/27/16 10:50
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 07:4107/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 07:4107/29/16 06:30
EPA 8260B 100 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 07:4107/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW2
Ground Water
AZG0817-01 AZG081707/27/16 10:50
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 106 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 07:4107/29/16 06:3078-120
EPA 8260B 107 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 07:4107/29/16 06:3080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 07:4107/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW7
Ground Water
AZG0817-02 AZG081707/27/16 12:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
EPA 6020B 0.69 ug/L1Antimony6.00 B-01, J 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:1108/10/16 08:35
EPA 6020B 1.40 ug/L1Arsenic10.0 J 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:1108/10/16 08:35
EPA 6020B 40.1 ug/L1Barium100 J 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:1108/10/16 08:35
EPA 6020B 1.65 ug/L1Beryllium1.00 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:1108/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:1108/10/16 08:35
EPA 6020B 1.20 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:1108/10/16 08:35
EPA 6020B 37.4 ug/L1Cobalt10.0 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:1108/10/16 08:35
EPA 6020B 1.13 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:1108/10/16 08:35
EPA 6020B 0.73 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:1108/10/16 08:35
EPA 6020B 8.86 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:1108/10/16 08:35
EPA 6020B 5.56 ug/L1Selenium10.0 J 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:1108/10/16 08:35
EPA 6020B 0.93 ug/L1Silver10.0 J 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:1108/10/16 08:35
EPA 6020B 0.09 ug/L1Thallium5.50 J 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:1108/10/16 08:35
EPA 6020B 1.63 ug/L1Vanadium25.0 J 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:1108/10/16 08:35
EPA 6020B 5.37 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:1108/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 08:0707/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW7
Ground Water
AZG0817-02 AZG081707/27/16 12:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 08:0707/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW7
Ground Water
AZG0817-02 AZG081707/27/16 12:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 08:0707/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 08:0707/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW7
Ground Water
AZG0817-02 AZG081707/27/16 12:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 101 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 08:0707/29/16 06:3080-120
EPA 8260B 104 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 08:0707/29/16 06:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 08:0707/29/16 06:3080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 08:0707/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW8
Ground Water
AZG0817-03 AZG081707/27/16 09:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
EPA 6020B 0.36 ug/L1Antimony6.00 B-01, J 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:1708/10/16 08:35
EPA 6020B 122 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:1708/10/16 08:35
EPA 6020B 0.70 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:1708/10/16 08:35
EPA 6020B 1.04 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:1708/10/16 08:35
EPA 6020B 4.21 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Copper10.0 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:1708/10/16 08:35
EPA 6020B 0.16 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:1708/10/16 08:35
EPA 6020B 3.68 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Silver10.0 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:1708/10/16 08:35
NDEPA 6020B ug/L1Vanadium25.0 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:1708/10/16 08:35
EPA 6020B 3.02 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:1708/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 12:3007/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW8
Ground Water
AZG0817-03 AZG081707/27/16 09:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 12:3007/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW8
Ground Water
AZG0817-03 AZG081707/27/16 09:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 12:3007/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 12:3007/29/16 06:30
EPA 8260B 101 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 12:3007/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW8
Ground Water
AZG0817-03 AZG081707/27/16 09:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 105 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 12:3007/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 12:3007/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 12:3007/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW9
Ground Water
AZG0817-04 AZG081707/27/16 09:48
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:2308/10/16 08:35
EPA 6020B 151 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:2308/10/16 08:35
EPA 6020B 0.87 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:2308/10/16 08:35
EPA 6020B 0.57 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:2308/10/16 08:35
EPA 6020B 2.05 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Copper10.0 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Lead10.0 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:2308/10/16 08:35
EPA 6020B 5.87 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Silver10.0 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:2308/10/16 08:35
NDEPA 6020B ug/L1Vanadium25.0 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:2308/10/16 08:35
EPA 6020B 10.0 ug/L1Zinc10.0 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:2308/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 08:5507/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW9
Ground Water
AZG0817-04 AZG081707/27/16 09:48
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 08:5507/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW9
Ground Water
AZG0817-04 AZG081707/27/16 09:48
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 08:5507/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 08:5507/29/16 06:30
EPA 8260B 100 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 08:5507/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW9
Ground Water
AZG0817-04 AZG081707/27/16 09:48
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 104 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 08:5507/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 08:5507/29/16 06:3080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 08:5507/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW10
Ground Water
AZG0817-05 AZG081707/27/16 11:08
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:2808/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:2808/10/16 08:35
EPA 6020B 109 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:2808/10/16 08:35
EPA 6020B 0.29 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:2808/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:2808/10/16 08:35
NDEPA 6020B ug/L1Chromium10.0 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:2808/10/16 08:35
EPA 6020B 6.98 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:2808/10/16 08:35
EPA 6020B 2.49 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:2808/10/16 08:35
EPA 6020B 0.40 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:2808/10/16 08:35
EPA 6020B 4.23 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:2808/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:2808/10/16 08:35
EPA 6020B 0.94 ug/L1Silver10.0 J 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:2808/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:2808/10/16 08:35
NDEPA 6020B ug/L1Vanadium25.0 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:2808/10/16 08:35
EPA 6020B 10.1 ug/L1Zinc10.0 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:2808/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 09:2107/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW10
Ground Water
AZG0817-05 AZG081707/27/16 11:08
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 09:2107/29/16 06:30
EPA 8260B 3.1 ug/L1Chloroform5.0 J 6080016EPA 5030B 0.3 67-66-3 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 09:2107/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW10
Ground Water
AZG0817-05 AZG081707/27/16 11:08
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 09:2107/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 09:2107/29/16 06:30
EPA 8260B 102 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 09:2107/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW10
Ground Water
AZG0817-05 AZG081707/27/16 11:08
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 105 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 09:2107/29/16 06:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 09:2107/29/16 06:3080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 09:2107/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW11R
Ground Water
AZG0817-06 AZG081707/27/16 10:06
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
EPA 6020B 0.33 ug/L1Antimony6.00 B-01, J 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:4608/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:4608/10/16 08:35
EPA 6020B 30.4 ug/L1Barium100 J 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:4608/10/16 08:35
EPA 6020B 0.14 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:4608/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:4608/10/16 08:35
EPA 6020B 4.28 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:4608/10/16 08:35
EPA 6020B 2.26 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:4608/10/16 08:35
EPA 6020B 0.66 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:4608/10/16 08:35
EPA 6020B 0.30 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:4608/10/16 08:35
EPA 6020B 1.98 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:4608/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:4608/10/16 08:35
NDEPA 6020B ug/L1Silver10.0 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:4608/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:4608/10/16 08:35
EPA 6020B 1.90 ug/L1Vanadium25.0 J 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:4608/10/16 08:35
EPA 6020B 5.83 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:4608/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 09:4607/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW11R
Ground Water
AZG0817-06 AZG081707/27/16 10:06
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 09:4607/29/16 06:30
EPA 8260B 0.4 ug/L1Chloroform5.0 J 6080016EPA 5030B 0.3 67-66-3 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 09:4607/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW11R
Ground Water
AZG0817-06 AZG081707/27/16 10:06
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 09:4607/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 09:4607/29/16 06:30
EPA 8260B 101 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 09:4607/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW11R
Ground Water
AZG0817-06 AZG081707/27/16 10:06
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 107 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 09:4607/29/16 06:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 09:4607/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 09:4607/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW13
Ground Water
AZG0817-07 AZG081707/27/16 11:23
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:5108/10/16 08:35
EPA 6020B 307 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:5108/10/16 08:35
EPA 6020B 0.56 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:5108/10/16 08:35
EPA 6020B 0.54 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:5108/10/16 08:35
EPA 6020B 4.28 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Copper10.0 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:5108/10/16 08:35
EPA 6020B 0.21 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:5108/10/16 08:35
EPA 6020B 3.76 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Silver10.0 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:5108/10/16 08:35
NDEPA 6020B ug/L1Vanadium25.0 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:5108/10/16 08:35
EPA 6020B 5.94 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:5108/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 10:1107/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW13
Ground Water
AZG0817-07 AZG081707/27/16 11:23
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 10:1107/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW13
Ground Water
AZG0817-07 AZG081707/27/16 11:23
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 10:1107/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 10:1107/29/16 06:30
EPA 8260B 102 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 10:1107/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW13
Ground Water
AZG0817-07 AZG081707/27/16 11:23
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 106 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 10:1107/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 10:1107/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 10:1107/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW15
Ground Water
AZG0817-08 AZG081707/27/16 10:26
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080255EPA 3005A 0.25 7440-36-0 08/10/16 21:5708/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 21:5708/10/16 08:35
EPA 6020B 159 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 21:5708/10/16 08:35
EPA 6020B 0.43 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 21:5708/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 21:5708/10/16 08:35
EPA 6020B 3.11 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 21:5708/10/16 08:35
EPA 6020B 4.61 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 21:5708/10/16 08:35
EPA 6020B 0.98 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 21:5708/10/16 08:35
EPA 6020B 0.53 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 21:5708/10/16 08:35
EPA 6020B 4.42 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 21:5708/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 21:5708/10/16 08:35
EPA 6020B 0.78 ug/L1Silver10.0 J 6080255EPA 3005A 0.22 7440-22-4 08/10/16 21:5708/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 21:5708/10/16 08:35
EPA 6020B 2.64 ug/L1Vanadium25.0 J 6080255EPA 3005A 1.57 7440-62-2 08/10/16 21:5708/10/16 08:35
EPA 6020B 6.56 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 21:5708/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 10:3607/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW15
Ground Water
AZG0817-08 AZG081707/27/16 10:26
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 10:3607/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW15
Ground Water
AZG0817-08 AZG081707/27/16 10:26
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 10:3607/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 10:3607/29/16 06:30
EPA 8260B 100 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 10:3607/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW15
Ground Water
AZG0817-08 AZG081707/27/16 10:26
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 107 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 10:3607/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 10:3607/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 10:3607/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW16R
Ground Water
AZG0817-09 AZG081707/27/16 11:58
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080255EPA 3005A 0.25 7440-36-0 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 22:0308/10/16 08:35
EPA 6020B 104 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 22:0308/10/16 08:35
EPA 6020B 0.21 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Chromium10.0 6080255EPA 3005A 0.43 7440-47-3 08/10/16 22:0308/10/16 08:35
EPA 6020B 3.88 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 22:0308/10/16 08:35
EPA 6020B 1.19 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 22:0308/10/16 08:35
EPA 6020B 1.12 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 22:0308/10/16 08:35
EPA 6020B 1.54 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Silver10.0 6080255EPA 3005A 0.22 7440-22-4 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 22:0308/10/16 08:35
NDEPA 6020B ug/L1Vanadium25.0 6080255EPA 3005A 1.57 7440-62-2 08/10/16 22:0308/10/16 08:35
EPA 6020B 6.28 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 22:0308/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 11:0207/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW16R
Ground Water
AZG0817-09 AZG081707/27/16 11:58
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 11:0207/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW16R
Ground Water
AZG0817-09 AZG081707/27/16 11:58
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 11:0207/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 11:0207/29/16 06:30
EPA 8260B 101 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 11:0207/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW16R
Ground Water
AZG0817-09 AZG081707/27/16 11:58
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 106 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 11:0207/29/16 06:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 11:0207/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 11:0207/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW17
Ground Water
AZG0817-10 AZG081707/27/16 11:38
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080255EPA 3005A 0.25 7440-36-0 08/10/16 22:0908/10/16 08:35
NDEPA 6020B ug/L1Arsenic10.0 6080255EPA 3005A 0.75 7440-38-2 08/10/16 22:0908/10/16 08:35
EPA 6020B 144 ug/L1Barium100 6080255EPA 3005A 0.30 7440-39-3 08/10/16 22:0908/10/16 08:35
EPA 6020B 0.29 ug/L1Beryllium1.00 J 6080255EPA 3005A 0.09 7440-41-7 08/10/16 22:0908/10/16 08:35
NDEPA 6020B ug/L1Cadmium1.00 6080255EPA 3005A 0.10 7440-43-9 08/10/16 22:0908/10/16 08:35
EPA 6020B 2.95 ug/L1Chromium10.0 J 6080255EPA 3005A 0.43 7440-47-3 08/10/16 22:0908/10/16 08:35
EPA 6020B 2.35 ug/L1Cobalt10.0 J 6080255EPA 3005A 0.29 7440-48-4 08/10/16 22:0908/10/16 08:35
EPA 6020B 1.21 ug/L1Copper10.0 J 6080255EPA 3005A 0.41 7440-50-8 08/10/16 22:0908/10/16 08:35
EPA 6020B 0.87 ug/L1Lead10.0 J 6080255EPA 3005A 0.08 7439-92-1 08/10/16 22:0908/10/16 08:35
EPA 6020B 1.55 ug/L1Nickel50.0 J 6080255EPA 3005A 0.48 7440-02-0 08/10/16 22:0908/10/16 08:35
NDEPA 6020B ug/L1Selenium10.0 6080255EPA 3005A 0.85 7782-49-2 08/10/16 22:0908/10/16 08:35
EPA 6020B 6.45 ug/L1Silver10.0 J 6080255EPA 3005A 0.22 7440-22-4 08/10/16 22:0908/10/16 08:35
NDEPA 6020B ug/L1Thallium5.50 6080255EPA 3005A 0.06 7440-28-0 08/10/16 22:0908/10/16 08:35
EPA 6020B 3.21 ug/L1Vanadium25.0 J 6080255EPA 3005A 1.57 7440-62-2 08/10/16 22:0908/10/16 08:35
EPA 6020B 6.33 ug/L1Zinc10.0 J 6080255EPA 3005A 1.30 7440-66-6 08/10/16 22:0908/10/16 08:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 11:2707/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW17
Ground Water
AZG0817-10 AZG081707/27/16 11:38
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 11:2707/29/16 06:30
EPA 8260B 0.6 ug/L1Chloroform5.0 J 6080016EPA 5030B 0.3 67-66-3 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 11:2707/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW17
Ground Water
AZG0817-10 AZG081707/27/16 11:38
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 11:2707/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 11:2707/29/16 06:30
EPA 8260B 100 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 11:2707/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW17
Ground Water
AZG0817-10 AZG081707/27/16 11:38
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 107 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 11:2707/29/16 06:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 11:2707/29/16 06:3080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 11:2707/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW18
Ground Water
AZG0817-11 AZG081707/27/16 12:16
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080214EPA 3005A 0.25 7440-36-0 08/09/16 20:5908/09/16 09:20
EPA 6020B 0.85 ug/L1Arsenic10.0 J 6080214EPA 3005A 0.75 7440-38-2 08/09/16 20:5908/09/16 09:20
EPA 6020B 192 ug/L1Barium100 6080214EPA 3005A 0.30 7440-39-3 08/09/16 20:5908/09/16 09:20
EPA 6020B 0.83 ug/L1Beryllium1.00 J 6080214EPA 3005A 0.09 7440-41-7 08/09/16 20:5908/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 20:5908/09/16 09:20
EPA 6020B 0.84 ug/L1Chromium10.0 J 6080214EPA 3005A 0.43 7440-47-3 08/09/16 20:5908/09/16 09:20
EPA 6020B 4.19 ug/L1Cobalt10.0 J 6080214EPA 3005A 0.29 7440-48-4 08/09/16 20:5908/09/16 09:20
EPA 6020B 0.55 ug/L1Copper10.0 J 6080214EPA 3005A 0.41 7440-50-8 08/09/16 20:5908/09/16 09:20
EPA 6020B 2.26 ug/L1Lead10.0 J 6080214EPA 3005A 0.08 7439-92-1 08/09/16 20:5908/09/16 09:20
EPA 6020B 4.54 ug/L1Nickel50.0 J 6080214EPA 3005A 0.48 7440-02-0 08/09/16 20:5908/09/16 09:20
EPA 6020B 3.49 ug/L1Selenium10.0 J 6080214EPA 3005A 0.85 7782-49-2 08/09/16 20:5908/09/16 09:20
NDEPA 6020B ug/L1Silver10.0 6080214EPA 3005A 0.22 7440-22-4 08/09/16 20:5908/09/16 09:20
NDEPA 6020B ug/L1Thallium5.50 6080214EPA 3005A 0.06 7440-28-0 08/09/16 20:5908/09/16 09:20
NDEPA 6020B ug/L1Vanadium25.0 6080214EPA 3005A 1.57 7440-62-2 08/09/16 20:5908/09/16 09:20
EPA 6020B 9.75 ug/L1Zinc10.0 B-01, J 6080214EPA 3005A 1.30 7440-66-6 08/09/16 20:5908/09/16 09:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 11:5207/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW18
Ground Water
AZG0817-11 AZG081707/27/16 12:16
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 11:5207/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW18
Ground Water
AZG0817-11 AZG081707/27/16 12:16
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 11:5207/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 11:5207/29/16 06:30
EPA 8260B 102 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 11:5207/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW18
Ground Water
AZG0817-11 AZG081707/27/16 12:16
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 106 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 11:5207/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 11:5207/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 11:5207/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW21
Ground Water
AZG0817-12 AZG081707/27/16 12:54
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080214EPA 3005A 0.25 7440-36-0 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Arsenic10.0 6080214EPA 3005A 0.75 7440-38-2 08/09/16 21:0408/09/16 09:20
EPA 6020B 28.2 ug/L1Barium100 J 6080214EPA 3005A 0.30 7440-39-3 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Beryllium1.00 6080214EPA 3005A 0.09 7440-41-7 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Chromium10.0 6080214EPA 3005A 0.43 7440-47-3 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Cobalt10.0 6080214EPA 3005A 0.29 7440-48-4 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Copper10.0 6080214EPA 3005A 0.41 7440-50-8 08/09/16 21:0408/09/16 09:20
EPA 6020B 0.86 ug/L1Lead10.0 J 6080214EPA 3005A 0.08 7439-92-1 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Nickel50.0 6080214EPA 3005A 0.48 7440-02-0 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Selenium10.0 6080214EPA 3005A 0.85 7782-49-2 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Silver10.0 6080214EPA 3005A 0.22 7440-22-4 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Thallium5.50 6080214EPA 3005A 0.06 7440-28-0 08/09/16 21:0408/09/16 09:20
NDEPA 6020B ug/L1Vanadium25.0 6080214EPA 3005A 1.57 7440-62-2 08/09/16 21:0408/09/16 09:20
EPA 6020B 1.70 ug/L1Zinc10.0 B-01, J 6080214EPA 3005A 1.30 7440-66-6 08/09/16 21:0408/09/16 09:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 14:2407/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW21
Ground Water
AZG0817-12 AZG081707/27/16 12:54
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 14:2407/29/16 06:30
EPA 8260B 0.9 ug/L1Chloroform5.0 J 6080016EPA 5030B 0.3 67-66-3 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 14:2407/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW21
Ground Water
AZG0817-12 AZG081707/27/16 12:54
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 14:2407/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 14:2407/29/16 06:30
EPA 8260B 104 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 14:2407/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-GW21
Ground Water
AZG0817-12 AZG081707/27/16 12:54
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 107 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 14:2407/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 14:2407/29/16 06:3080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 14:2407/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-PW1
Ground Water
AZG0817-13 AZG081707/27/16 14:34
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080214EPA 3005A 0.25 7440-36-0 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Arsenic10.0 6080214EPA 3005A 0.75 7440-38-2 08/09/16 21:1008/09/16 09:20
EPA 6020B 56.5 ug/L1Barium100 J 6080214EPA 3005A 0.30 7440-39-3 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Beryllium1.00 6080214EPA 3005A 0.09 7440-41-7 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Chromium10.0 6080214EPA 3005A 0.43 7440-47-3 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Cobalt10.0 6080214EPA 3005A 0.29 7440-48-4 08/09/16 21:1008/09/16 09:20
EPA 6020B 1.06 ug/L1Copper10.0 J 6080214EPA 3005A 0.41 7440-50-8 08/09/16 21:1008/09/16 09:20
EPA 6020B 0.17 ug/L1Lead10.0 J 6080214EPA 3005A 0.08 7439-92-1 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Nickel50.0 6080214EPA 3005A 0.48 7440-02-0 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Selenium10.0 6080214EPA 3005A 0.85 7782-49-2 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Silver10.0 6080214EPA 3005A 0.22 7440-22-4 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Thallium5.50 6080214EPA 3005A 0.06 7440-28-0 08/09/16 21:1008/09/16 09:20
NDEPA 6020B ug/L1Vanadium25.0 6080214EPA 3005A 1.57 7440-62-2 08/09/16 21:1008/09/16 09:20
EPA 6020B 36.8 ug/L1Zinc10.0 B-01 6080214EPA 3005A 1.30 7440-66-6 08/09/16 21:1008/09/16 09:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 14:5007/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-PW1
Ground Water
AZG0817-13 AZG081707/27/16 14:34
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 14:5007/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-PW1
Ground Water
AZG0817-13 AZG081707/27/16 14:34
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 14:5007/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 14:5007/29/16 06:30
EPA 8260B 102 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 14:5007/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-PW1
Ground Water
AZG0817-13 AZG081707/27/16 14:34
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 107 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 14:5007/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 14:5007/29/16 06:3080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 14:5007/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Blank (6080214-BLK1)Prepared & Analyzed: 08/09/16
Antimony ug/L0.45 6.00 J
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/L4.04 10.0 J
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Antimony ug/L1076.00 100.00 80-120107
Arsenic ug/L99.1 10.0 100.00 80-12099
Barium ug/L93.8 100 100.00 J80-12094
Beryllium ug/L91.1 1.00 100.00 80-12091
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L10310.0 100.00 80-120103
Cobalt ug/L98.2 10.0 100.00 80-12098
Copper ug/L98.6 10.0 100.00 80-12099
Lead ug/L91.7 10.0 100.00 80-12092
Nickel ug/L10250.0 100.00 80-120102
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Selenium ug/L97.0 10.0 100.00 80-12097
Silver ug/L98.1 10.0 100.00 80-12098
Thallium ug/L93.0 5.50 100.00 80-12093
Vanadium ug/L99.9 25.0 100.00 80-120100
Zinc ug/L10710.0 100.00 80-120107
Matrix Spike (6080214-MS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L97.7 6.00 100.00 ND 75-12598
Arsenic ug/L10810.0 100.00 3.51 75-125105
Barium ug/L507100 100.00 453 QM-0275-12554
Beryllium ug/L84.6 1.00 100.00 0.21 75-12584
Cadmium ug/L1041.00 100.00 0.18 75-125104
Chromium ug/L10510.0 100.00 ND 75-125105
Cobalt ug/L98.6 10.0 100.00 ND 75-12599
Copper ug/L10110.0 100.00 3.71 75-12597
Lead ug/L93.2 10.0 100.00 4.00 75-12589
Nickel ug/L10350.0 100.00 0.97 75-125102
Selenium ug/L10410.0 100.00 1.00 75-125103
Silver ug/L97.0 10.0 100.00 0.40 75-12597
Thallium ug/L91.3 5.50 100.00 ND 75-12591
Vanadium ug/L10625.0 100.00 ND 75-125106
Zinc ug/L11410.0 100.00 4.78 75-125109
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L1026.00 100.00 ND 2075-125102 4
Arsenic ug/L10410.0 100.00 3.51 2075-125100 4
Barium ug/L525100 100.00 453 20 QM-0275-12572 3
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Beryllium ug/L85.2 1.00 100.00 0.21 2075-12585 0.8
Cadmium ug/L1001.00 100.00 0.18 2075-125100 4
Chromium ug/L10810.0 100.00 ND 2075-125108 3
Cobalt ug/L10010.0 100.00 ND 2075-125100 1
Copper ug/L98.8 10.0 100.00 3.71 2075-12595 2
Lead ug/L92.8 10.0 100.00 4.00 2075-12589 0.4
Nickel ug/L10150.0 100.00 0.97 2075-125100 2
Selenium ug/L94.5 10.0 100.00 1.00 2075-12593 9
Silver ug/L98.2 10.0 100.00 0.40 2075-12598 1
Thallium ug/L90.7 5.50 100.00 ND 2075-12591 0.7
Vanadium ug/L11025.0 100.00 ND 2075-125110 3
Zinc ug/L10910.0 100.00 4.78 2075-125104 5
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L98.0 100.00 0.15 80-12098
Arsenic ug/L109 100.00 3.51 80-120105
Barium ug/L543 100.00 453 80-12090
Beryllium ug/L82.8 100.00 0.21 80-12083
Cadmium ug/L100 100.00 0.18 80-120100
Chromium ug/L102 100.00 0.34 80-120102
Cobalt ug/L97.3 100.00 0.17 80-12097
Copper ug/L95.3 100.00 3.71 80-12092
Lead ug/L92.0 100.00 4.00 80-12088
Nickel ug/L95.0 100.00 0.97 80-12094
Selenium ug/L99.8 100.00 1.00 80-12099
Silver ug/L96.4 100.00 0.40 80-12096
Thallium ug/L91.5 100.00 0.01 80-12091
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Vanadium ug/L104 100.00 0.31 80-120103
Zinc ug/L111 100.00 4.78 80-120106
Batch 6080255 - EPA 3005A
Blank (6080255-BLK1)Prepared & Analyzed: 08/10/16
Antimony ug/L0.28 6.00 J
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6080255-BS1)Prepared & Analyzed: 08/10/16
Antimony ug/L1106.00 100.00 80-120110
Arsenic ug/L10210.0 100.00 80-120102
Barium ug/L98.6 100 100.00 J80-12099
Beryllium ug/L1011.00 100.00 80-120101
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080255 - EPA 3005A
LCS (6080255-BS1)Prepared & Analyzed: 08/10/16
Cadmium ug/L98.4 1.00 100.00 80-12098
Chromium ug/L10310.0 100.00 80-120103
Cobalt ug/L10210.0 100.00 80-120102
Copper ug/L99.5 10.0 100.00 80-12099
Lead ug/L96.7 10.0 100.00 80-12097
Nickel ug/L10350.0 100.00 80-120103
Selenium ug/L99.8 10.0 100.00 80-120100
Silver ug/L99.4 10.0 100.00 80-12099
Thallium ug/L95.5 5.50 100.00 80-12096
Vanadium ug/L10125.0 100.00 80-120101
Zinc ug/L10810.0 100.00 80-120108
Matrix Spike (6080255-MS1)Prepared & Analyzed: 08/10/16 Source: AZG0817-02
Antimony ug/L1136.00 100.00 0.69 75-125112
Arsenic ug/L10310.0 100.00 1.40 75-125102
Barium ug/L139100 100.00 40.1 75-12599
Beryllium ug/L97.9 1.00 100.00 1.65 75-12596
Cadmium ug/L1001.00 100.00 ND 75-125100
Chromium ug/L11010.0 100.00 1.20 75-125109
Cobalt ug/L14310.0 100.00 37.4 75-125106
Copper ug/L10110.0 100.00 1.13 75-125100
Lead ug/L95.7 10.0 100.00 0.73 75-12595
Nickel ug/L11450.0 100.00 8.86 75-125105
Selenium ug/L10410.0 100.00 5.56 75-12598
Silver ug/L99.4 10.0 100.00 0.93 75-12598
Thallium ug/L97.3 5.50 100.00 0.09 75-12597
Vanadium ug/L11225.0 100.00 1.63 75-125110
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080255 - EPA 3005A
Matrix Spike (6080255-MS1)Prepared & Analyzed: 08/10/16 Source: AZG0817-02
Zinc ug/L11010.0 100.00 5.37 75-125105
Matrix Spike Dup (6080255-MSD1)Prepared & Analyzed: 08/10/16 Source: AZG0817-02
Antimony ug/L1106.00 100.00 0.69 2075-125109 3
Arsenic ug/L10010.0 100.00 1.40 2075-12599 3
Barium ug/L141100 100.00 40.1 2075-125101 1
Beryllium ug/L1011.00 100.00 1.65 2075-125100 3
Cadmium ug/L1021.00 100.00 ND 2075-125102 2
Chromium ug/L10610.0 100.00 1.20 2075-125104 5
Cobalt ug/L13910.0 100.00 37.4 2075-125102 3
Copper ug/L10410.0 100.00 1.13 2075-125103 3
Lead ug/L96.3 10.0 100.00 0.73 2075-12596 0.7
Nickel ug/L11150.0 100.00 8.86 2075-125103 2
Selenium ug/L10110.0 100.00 5.56 2075-12596 3
Silver ug/L10210.0 100.00 0.93 2075-125101 3
Thallium ug/L95.0 5.50 100.00 0.09 2075-12595 2
Vanadium ug/L10525.0 100.00 1.63 2075-125104 6
Zinc ug/L10810.0 100.00 5.37 2075-125103 2
Post Spike (6080255-PS1)Prepared & Analyzed: 08/10/16 Source: AZG0817-02
Antimony ug/L98.0 100.00 0.69 80-12097
Arsenic ug/L105 100.00 1.40 80-120104
Barium ug/L136 100.00 40.1 80-12096
Beryllium ug/L102 100.00 1.65 80-120100
Cadmium ug/L104 100.00 0.09 80-120104
Chromium ug/L105 100.00 1.20 80-120104
Cobalt ug/L145 100.00 37.4 80-120108
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080255 - EPA 3005A
Post Spike (6080255-PS1)Prepared & Analyzed: 08/10/16 Source: AZG0817-02
Copper ug/L104 100.00 1.13 80-120103
Lead ug/L97.4 100.00 0.73 80-12097
Nickel ug/L110 100.00 8.86 80-120101
Selenium ug/L107 100.00 5.56 80-120101
Silver ug/L102 100.00 0.93 80-120101
Thallium ug/L96.8 100.00 0.09 80-12097
Vanadium ug/L108 100.00 1.63 80-120107
Zinc ug/L112 100.00 5.37 80-120106
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
Blank (6080016-BLK1)Prepared & Analyzed: 07/29/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
Blank (6080016-BLK1)Prepared & Analyzed: 07/29/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 9949
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10351
ug/L 50.000 80-120Surr: Toluene-d8 10753
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10050
LCS (6080016-BS1)Prepared & Analyzed: 07/29/16
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
LCS (6080016-BS1)Prepared & Analyzed: 07/29/16
Benzene ug/L44 50.000 67-13488
Chlorobenzene ug/L49 50.000 69-12299
1,1-Dichloroethene ug/L50 50.000 58-142100
Toluene ug/L45 50.000 68-12790
Trichloroethene ug/L49 50.000 72-13297
ug/L 50.000 80-120Surr: Dibromofluoromethane 10050
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10050
ug/L 50.000 80-120Surr: Toluene-d8 10653
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10050
Matrix Spike (6080016-MS1)Prepared & Analyzed: 07/29/16 Source: AZG0817-02
Benzene ug/L45 50.000 ND 67-13489
Chlorobenzene ug/L48 50.000 ND 69-12296
1,1-Dichloroethene ug/L51 50.000 ND 58-142103
Toluene ug/L45 50.000 ND 68-12789
Trichloroethene ug/L48 50.000 ND 72-13296
ug/L 50.000 80-120Surr: Dibromofluoromethane 10050
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10653
ug/L 50.000 80-120Surr: Toluene-d8 10553
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
Matrix Spike Dup (6080016-MSD1)Prepared & Analyzed: 07/29/16 Source: AZG0817-02
Benzene ug/L46 50.000 ND 967-13493 4
Chlorobenzene ug/L51 50.000 ND 1369-122101 5
1,1-Dichloroethene ug/L54 50.000 ND 958-142107 4
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
Matrix Spike Dup (6080016-MSD1)Prepared & Analyzed: 07/29/16 Source: AZG0817-02
Toluene ug/L48 50.000 ND 968-12795 6
Trichloroethene ug/L51 50.000 ND 1172-132103 6
ug/L 50.000 80-120Surr: Dibromofluoromethane 9949
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10553
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10150
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Laboratory Certifications
Code Description Number Expires
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2016 06/30/2017NELAC
98011001South Carolina 08/30/2016SC
T104704397-08-TXTexas 03/31/2017TX
1340Virginia 12/14/2016VA
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
B-01 Analyte was detected in the associated method blank at an estimated level equal to or greater than the MDL. Sample values reported as greater than the MDL
and less than 10x the method blank value are reported as estimated values.
Note: Unless otherwise noted, all results are reported on an as received basis.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
COC Goes Here
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
East Carolina Regional LandfillProject:
Client:
Printed: 8/15/2016 4:27:11PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, INC.
Date Received:07/28/16 09:00 Logged In By:Charles Hawks
Work Order:AZG0817
OBSERVATIONS
Attn: Mr. Matt Einsmann
#Samples: 13 #Containers: 56
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
Comments:
Page 1 of 1
PACE ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: East Carolina Regional Landfill
Conover, NC 28613
1220 Commerce Street, SW
Mr. Matt Einsmann
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, Inc. certifies
that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the
samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
August 15, 2016
Report Number:AZG0820
Approved:
This report may not be reproduced, except in full, without written approval from Pace Analytical Services, Inc.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
0803-SW2 AZG0820-01 07/27/16 13:47 07/28/16 09:00Surface Water
0803-SW3 AZG0820-02 07/27/16 13:35 07/28/16 09:00Surface Water
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW2
Surface Water
AZG0820-01 AZG082007/27/16 13:47
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
EPA 6020B 1.06 ug/L1Antimony6.00 B-01, J 6080214EPA 3005A 0.25 7440-36-0 08/09/16 21:2708/09/16 09:20
EPA 6020B 5.13 ug/L1Arsenic10.0 J 6080214EPA 3005A 0.75 7440-38-2 08/09/16 21:2708/09/16 09:20
EPA 6020B 53.1 ug/L1Barium100 J 6080214EPA 3005A 0.30 7440-39-3 08/09/16 21:2708/09/16 09:20
NDEPA 6020B ug/L1Beryllium1.00 6080214EPA 3005A 0.09 7440-41-7 08/09/16 21:2708/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 21:2708/09/16 09:20
EPA 6020B 3.05 ug/L1Chromium10.0 J 6080214EPA 3005A 0.43 7440-47-3 08/09/16 21:2708/09/16 09:20
EPA 6020B 1.32 ug/L1Cobalt10.0 J 6080214EPA 3005A 0.29 7440-48-4 08/09/16 21:2708/09/16 09:20
EPA 6020B 2.94 ug/L1Copper10.0 J 6080214EPA 3005A 0.41 7440-50-8 08/09/16 21:2708/09/16 09:20
EPA 6020B 1.65 ug/L1Lead10.0 J 6080214EPA 3005A 0.08 7439-92-1 08/09/16 21:2708/09/16 09:20
EPA 6020B 7.46 ug/L1Nickel50.0 J 6080214EPA 3005A 0.48 7440-02-0 08/09/16 21:2708/09/16 09:20
EPA 6020B 1.00 ug/L1Selenium10.0 J 6080214EPA 3005A 0.85 7782-49-2 08/09/16 21:2708/09/16 09:20
NDEPA 6020B ug/L1Silver10.0 6080214EPA 3005A 0.22 7440-22-4 08/09/16 21:2708/09/16 09:20
NDEPA 6020B ug/L1Thallium5.50 6080214EPA 3005A 0.06 7440-28-0 08/09/16 21:2708/09/16 09:20
EPA 6020B 4.54 ug/L1Vanadium25.0 J 6080214EPA 3005A 1.57 7440-62-2 08/09/16 21:2708/09/16 09:20
EPA 6020B 7.01 ug/L1Zinc10.0 B-01, J 6080214EPA 3005A 1.30 7440-66-6 08/09/16 21:2708/09/16 09:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080019EPA 5030B 4.9 67-64-1 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6080019EPA 5030B 1.8 107-13-1 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6080019EPA 5030B 0.2 71-43-2 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6080019EPA 5030B 0.7 74-97-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080019EPA 5030B 0.6 75-27-4 07/29/16 22:5207/29/16 12:00
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW2
Surface Water
AZG0820-01 AZG082007/27/16 13:47
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080019EPA 5030B 0.7 75-25-2 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6080019EPA 5030B 0.8 74-83-9 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6080019EPA 5030B 0.6 75-15-0 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080019EPA 5030B 0.6 56-23-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6080019EPA 5030B 0.4 108-90-7 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6080019EPA 5030B 0.4 75-00-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6080019EPA 5030B 0.3 67-66-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6080019EPA 5030B 0.4 74-87-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080019EPA 5030B 0.7 124-48-1 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080019EPA 5030B 2.0 96-12-8 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080019EPA 5030B 0.7 106-93-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6080019EPA 5030B 0.7 74-95-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080019EPA 5030B 0.5 95-50-1 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080019EPA 5030B 0.3 106-46-7 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080019EPA 5030B 1.5 110-57-6 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080019EPA 5030B 0.4 75-34-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080019EPA 5030B 0.3 107-06-2 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080019EPA 5030B 0.5 75-35-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080019EPA 5030B 0.5 156-59-2 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080019EPA 5030B 0.4 156-60-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080019EPA 5030B 0.5 78-87-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080019EPA 5030B 0.4 10061-01-5 07/29/16 22:5207/29/16 12:00
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW2
Surface Water
AZG0820-01 AZG082007/27/16 13:47
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080019EPA 5030B 0.4 10061-02-6 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6080019EPA 5030B 0.2 100-41-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6080019EPA 5030B 0.6 74-88-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080019EPA 5030B 0.9 591-78-6 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080019EPA 5030B 0.5 75-09-2 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080019EPA 5030B 1.1 78-93-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080019EPA 5030B 1.7 108-10-1 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6080019EPA 5030B 0.4 100-42-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080019EPA 5030B 0.6 630-20-6 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080019EPA 5030B 0.5 79-34-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080019EPA 5030B 0.4 127-18-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6080019EPA 5030B 0.3 108-88-3 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080019EPA 5030B 0.4 71-55-6 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080019EPA 5030B 0.8 79-00-5 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6080019EPA 5030B 0.4 79-01-6 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080019EPA 5030B 0.5 75-69-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080019EPA 5030B 0.7 96-18-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6080019EPA 5030B 0.8 108-05-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080019EPA 5030B 0.7 75-01-4 07/29/16 22:5207/29/16 12:00
NDEPA 8260B ug/L1Xylenes, total 5.0 6080019EPA 5030B 0.4 1330-20-7 07/29/16 22:5207/29/16 12:00
EPA 8260B 101 %Surr: Dibromofluoromethane 6080019EPA 5030B 1868-53-7 07/29/16 22:5207/29/16 12:0080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW2
Surface Water
AZG0820-01 AZG082007/27/16 13:47
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 108 %Surr: 1,2-Dichloroethane-d4 6080019EPA 5030B 17060-07-0 07/29/16 22:5207/29/16 12:0078-120
EPA 8260B 105 %Surr: Toluene-d8 6080019EPA 5030B 2037-26-5 07/29/16 22:5207/29/16 12:0080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 6080019EPA 5030B 460-00-4 07/29/16 22:5207/29/16 12:0080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW3
Surface Water
AZG0820-02 AZG082007/27/16 13:35
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
EPA 6020B 0.27 ug/L1Antimony6.00 B-01, J 6080214EPA 3005A 0.25 7440-36-0 08/09/16 21:3308/09/16 09:20
EPA 6020B 1.26 ug/L1Arsenic10.0 J 6080214EPA 3005A 0.75 7440-38-2 08/09/16 21:3308/09/16 09:20
EPA 6020B 222 ug/L1Barium100 6080214EPA 3005A 0.30 7440-39-3 08/09/16 21:3308/09/16 09:20
EPA 6020B 0.10 ug/L1Beryllium1.00 J 6080214EPA 3005A 0.09 7440-41-7 08/09/16 21:3308/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 21:3308/09/16 09:20
EPA 6020B 1.53 ug/L1Chromium10.0 J 6080214EPA 3005A 0.43 7440-47-3 08/09/16 21:3308/09/16 09:20
EPA 6020B 2.94 ug/L1Cobalt10.0 J 6080214EPA 3005A 0.29 7440-48-4 08/09/16 21:3308/09/16 09:20
EPA 6020B 0.65 ug/L1Copper10.0 J 6080214EPA 3005A 0.41 7440-50-8 08/09/16 21:3308/09/16 09:20
EPA 6020B 0.66 ug/L1Lead10.0 J 6080214EPA 3005A 0.08 7439-92-1 08/09/16 21:3308/09/16 09:20
EPA 6020B 2.06 ug/L1Nickel50.0 J 6080214EPA 3005A 0.48 7440-02-0 08/09/16 21:3308/09/16 09:20
NDEPA 6020B ug/L1Selenium10.0 6080214EPA 3005A 0.85 7782-49-2 08/09/16 21:3308/09/16 09:20
NDEPA 6020B ug/L1Silver10.0 6080214EPA 3005A 0.22 7440-22-4 08/09/16 21:3308/09/16 09:20
NDEPA 6020B ug/L1Thallium5.50 6080214EPA 3005A 0.06 7440-28-0 08/09/16 21:3308/09/16 09:20
EPA 6020B 1.93 ug/L1Vanadium25.0 J 6080214EPA 3005A 1.57 7440-62-2 08/09/16 21:3308/09/16 09:20
EPA 6020B 5.20 ug/L1Zinc10.0 B-01, J 6080214EPA 3005A 1.30 7440-66-6 08/09/16 21:3308/09/16 09:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080019EPA 5030B 4.9 67-64-1 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6080019EPA 5030B 1.8 107-13-1 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6080019EPA 5030B 0.2 71-43-2 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6080019EPA 5030B 0.7 74-97-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080019EPA 5030B 0.6 75-27-4 07/29/16 23:1707/29/16 12:00
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW3
Surface Water
AZG0820-02 AZG082007/27/16 13:35
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080019EPA 5030B 0.7 75-25-2 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6080019EPA 5030B 0.8 74-83-9 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6080019EPA 5030B 0.6 75-15-0 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080019EPA 5030B 0.6 56-23-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6080019EPA 5030B 0.4 108-90-7 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6080019EPA 5030B 0.4 75-00-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6080019EPA 5030B 0.3 67-66-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6080019EPA 5030B 0.4 74-87-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080019EPA 5030B 0.7 124-48-1 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080019EPA 5030B 2.0 96-12-8 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080019EPA 5030B 0.7 106-93-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6080019EPA 5030B 0.7 74-95-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080019EPA 5030B 0.5 95-50-1 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080019EPA 5030B 0.3 106-46-7 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080019EPA 5030B 1.5 110-57-6 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080019EPA 5030B 0.4 75-34-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080019EPA 5030B 0.3 107-06-2 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080019EPA 5030B 0.5 75-35-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080019EPA 5030B 0.5 156-59-2 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080019EPA 5030B 0.4 156-60-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080019EPA 5030B 0.5 78-87-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080019EPA 5030B 0.4 10061-01-5 07/29/16 23:1707/29/16 12:00
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW3
Surface Water
AZG0820-02 AZG082007/27/16 13:35
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080019EPA 5030B 0.4 10061-02-6 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6080019EPA 5030B 0.2 100-41-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6080019EPA 5030B 0.6 74-88-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080019EPA 5030B 0.9 591-78-6 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080019EPA 5030B 0.5 75-09-2 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080019EPA 5030B 1.1 78-93-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080019EPA 5030B 1.7 108-10-1 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6080019EPA 5030B 0.4 100-42-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080019EPA 5030B 0.6 630-20-6 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080019EPA 5030B 0.5 79-34-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080019EPA 5030B 0.4 127-18-4 07/29/16 23:1707/29/16 12:00
EPA 8260B 0.3 ug/L1Toluene1.0 J 6080019EPA 5030B 0.3 108-88-3 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080019EPA 5030B 0.4 71-55-6 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080019EPA 5030B 0.8 79-00-5 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6080019EPA 5030B 0.4 79-01-6 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080019EPA 5030B 0.5 75-69-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080019EPA 5030B 0.7 96-18-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6080019EPA 5030B 0.8 108-05-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080019EPA 5030B 0.7 75-01-4 07/29/16 23:1707/29/16 12:00
NDEPA 8260B ug/L1Xylenes, total 5.0 6080019EPA 5030B 0.4 1330-20-7 07/29/16 23:1707/29/16 12:00
EPA 8260B 101 %Surr: Dibromofluoromethane 6080019EPA 5030B 1868-53-7 07/29/16 23:1707/29/16 12:0080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-SW3
Surface Water
AZG0820-02 AZG082007/27/16 13:35
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 104 %Surr: 1,2-Dichloroethane-d4 6080019EPA 5030B 17060-07-0 07/29/16 23:1707/29/16 12:0078-120
EPA 8260B 105 %Surr: Toluene-d8 6080019EPA 5030B 2037-26-5 07/29/16 23:1707/29/16 12:0080-120
EPA 8260B 99 %Surr: 4-Bromofluorobenzene 6080019EPA 5030B 460-00-4 07/29/16 23:1707/29/16 12:0080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Blank (6080214-BLK1)Prepared & Analyzed: 08/09/16
Antimony ug/L0.45 6.00 J
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/L4.04 10.0 J
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Antimony ug/L1076.00 100.00 80-120107
Arsenic ug/L99.1 10.0 100.00 80-12099
Barium ug/L93.8 100 100.00 J80-12094
Beryllium ug/L91.1 1.00 100.00 80-12091
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L10310.0 100.00 80-120103
Cobalt ug/L98.2 10.0 100.00 80-12098
Copper ug/L98.6 10.0 100.00 80-12099
Lead ug/L91.7 10.0 100.00 80-12092
Nickel ug/L10250.0 100.00 80-120102
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Selenium ug/L97.0 10.0 100.00 80-12097
Silver ug/L98.1 10.0 100.00 80-12098
Thallium ug/L93.0 5.50 100.00 80-12093
Vanadium ug/L99.9 25.0 100.00 80-120100
Zinc ug/L10710.0 100.00 80-120107
Matrix Spike (6080214-MS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L97.7 6.00 100.00 ND 75-12598
Arsenic ug/L10810.0 100.00 3.51 75-125105
Barium ug/L507100 100.00 453 QM-0275-12554
Beryllium ug/L84.6 1.00 100.00 0.21 75-12584
Cadmium ug/L1041.00 100.00 0.18 75-125104
Chromium ug/L10510.0 100.00 ND 75-125105
Cobalt ug/L98.6 10.0 100.00 ND 75-12599
Copper ug/L10110.0 100.00 3.71 75-12597
Lead ug/L93.2 10.0 100.00 4.00 75-12589
Nickel ug/L10350.0 100.00 0.97 75-125102
Selenium ug/L10410.0 100.00 1.00 75-125103
Silver ug/L97.0 10.0 100.00 0.40 75-12597
Thallium ug/L91.3 5.50 100.00 ND 75-12591
Vanadium ug/L10625.0 100.00 ND 75-125106
Zinc ug/L11410.0 100.00 4.78 75-125109
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L1026.00 100.00 ND 2075-125102 4
Arsenic ug/L10410.0 100.00 3.51 2075-125100 4
Barium ug/L525100 100.00 453 20 QM-0275-12572 3
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Beryllium ug/L85.2 1.00 100.00 0.21 2075-12585 0.8
Cadmium ug/L1001.00 100.00 0.18 2075-125100 4
Chromium ug/L10810.0 100.00 ND 2075-125108 3
Cobalt ug/L10010.0 100.00 ND 2075-125100 1
Copper ug/L98.8 10.0 100.00 3.71 2075-12595 2
Lead ug/L92.8 10.0 100.00 4.00 2075-12589 0.4
Nickel ug/L10150.0 100.00 0.97 2075-125100 2
Selenium ug/L94.5 10.0 100.00 1.00 2075-12593 9
Silver ug/L98.2 10.0 100.00 0.40 2075-12598 1
Thallium ug/L90.7 5.50 100.00 ND 2075-12591 0.7
Vanadium ug/L11025.0 100.00 ND 2075-125110 3
Zinc ug/L10910.0 100.00 4.78 2075-125104 5
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L98.0 100.00 0.15 80-12098
Arsenic ug/L109 100.00 3.51 80-120105
Barium ug/L543 100.00 453 80-12090
Beryllium ug/L82.8 100.00 0.21 80-12083
Cadmium ug/L100 100.00 0.18 80-120100
Chromium ug/L102 100.00 0.34 80-120102
Cobalt ug/L97.3 100.00 0.17 80-12097
Copper ug/L95.3 100.00 3.71 80-12092
Lead ug/L92.0 100.00 4.00 80-12088
Nickel ug/L95.0 100.00 0.97 80-12094
Selenium ug/L99.8 100.00 1.00 80-12099
Silver ug/L96.4 100.00 0.40 80-12096
Thallium ug/L91.5 100.00 0.01 80-12091
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Vanadium ug/L104 100.00 0.31 80-120103
Zinc ug/L111 100.00 4.78 80-120106
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080019 - EPA 5030B
Blank (6080019-BLK1)Prepared & Analyzed: 07/29/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080019 - EPA 5030B
Blank (6080019-BLK1)Prepared & Analyzed: 07/29/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 10151
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10553
ug/L 50.000 80-120Surr: Toluene-d8 10552
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10150
LCS (6080019-BS1)Prepared & Analyzed: 07/29/16
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080019 - EPA 5030B
LCS (6080019-BS1)Prepared & Analyzed: 07/29/16
Benzene ug/L43 50.000 67-13487
Chlorobenzene ug/L47 50.000 69-12294
1,1-Dichloroethene ug/L48 50.000 58-14297
Toluene ug/L44 50.000 68-12787
Trichloroethene ug/L46 50.000 72-13293
ug/L 50.000 80-120Surr: Dibromofluoromethane 10151
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10452
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10050
Matrix Spike (6080019-MS1)Prepared & Analyzed: 07/29/16 Source: AZG0789-09
Benzene ug/L45 50.000 ND 67-13491
Chlorobenzene ug/L49 50.000 ND 69-12297
1,1-Dichloroethene ug/L53 50.000 ND 58-142107
Toluene ug/L47 50.000 ND 68-12794
Trichloroethene ug/L49 50.000 ND 72-13297
ug/L 50.000 80-120Surr: Dibromofluoromethane 10954
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10552
ug/L 50.000 80-120Surr: Toluene-d8 10653
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10150
Matrix Spike Dup (6080019-MSD1)Prepared: 07/29/16 Analyzed: 07/30/16 Source: AZG0789-09
Benzene ug/L46 50.000 ND 967-13492 1
Chlorobenzene ug/L48 50.000 ND 1369-12296 0.7
1,1-Dichloroethene ug/L52 50.000 ND 958-142104 3
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080019 - EPA 5030B
Matrix Spike Dup (6080019-MSD1)Prepared: 07/29/16 Analyzed: 07/30/16 Source: AZG0789-09
Toluene ug/L46 50.000 ND 968-12793 0.9
Trichloroethene ug/L48 50.000 ND 1172-13296 2
ug/L 50.000 80-120Surr: Dibromofluoromethane 10754
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10552
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9949
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Laboratory Certifications
Code Description Number Expires
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2016 06/30/2017NELAC
98011001South Carolina 08/30/2016SC
T104704397-08-TXTexas 03/31/2017TX
1340Virginia 12/14/2016VA
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
B-01 Analyte was detected in the associated method blank at an estimated level equal to or greater than the MDL. Sample values reported as greater than the MDL
and less than 10x the method blank value are reported as estimated values.
Note: Unless otherwise noted, all results are reported on an as received basis.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
COC Goes Here
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
East Carolina Regional LandfillProject:
Client:
Printed: 8/15/2016 4:30:21PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, INC.
Date Received:07/28/16 09:00 Logged In By:Charles Hawks
Work Order:AZG0820
OBSERVATIONS
Attn: Mr. Matt Einsmann
#Samples: 2 #Containers: 8
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
Comments:
Page 1 of 1
PACE ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: East Carolina Regional Landfill
Conover, NC 28613
1220 Commerce Street, SW
Mr. Matt Einsmann
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, Inc. certifies
that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the
samples analyzed.
Laboratory Report
Project #:(none)
Prepared For:
Attention:
August 15, 2016
Report Number:AZG0821
Approved:
This report may not be reproduced, except in full, without written approval from Pace Analytical Services, Inc.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
0803-Field Blank AZG0821-01 07/27/16 14:36 07/28/16 09:00Water
0803-Trip Blank AZG0821-02 07/26/16 08:00 07/28/16 09:00Water
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Field Blank
Water
AZG0821-01 AZG082107/27/16 14:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6080214EPA 3005A 0.25 7440-36-0 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Arsenic10.0 6080214EPA 3005A 0.75 7440-38-2 08/09/16 21:3908/09/16 09:20
EPA 6020B 0.31 ug/L1Barium100 J 6080214EPA 3005A 0.30 7440-39-3 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Beryllium1.00 6080214EPA 3005A 0.09 7440-41-7 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Chromium10.0 6080214EPA 3005A 0.43 7440-47-3 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Cobalt10.0 6080214EPA 3005A 0.29 7440-48-4 08/09/16 21:3908/09/16 09:20
EPA 6020B 8.47 ug/L1Copper10.0 J 6080214EPA 3005A 0.41 7440-50-8 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Lead10.0 6080214EPA 3005A 0.08 7439-92-1 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Nickel50.0 6080214EPA 3005A 0.48 7440-02-0 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Selenium10.0 6080214EPA 3005A 0.85 7782-49-2 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Silver10.0 6080214EPA 3005A 0.22 7440-22-4 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Thallium5.50 6080214EPA 3005A 0.06 7440-28-0 08/09/16 21:3908/09/16 09:20
NDEPA 6020B ug/L1Vanadium25.0 6080214EPA 3005A 1.57 7440-62-2 08/09/16 21:3908/09/16 09:20
EPA 6020B 1.51 ug/L1Zinc10.0 B-01, J 6080214EPA 3005A 1.30 7440-66-6 08/09/16 21:3908/09/16 09:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 15:1507/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Field Blank
Water
AZG0821-01 AZG082107/27/16 14:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 15:1507/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Field Blank
Water
AZG0821-01 AZG082107/27/16 14:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 15:1507/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 15:1507/29/16 06:30
EPA 8260B 102 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 15:1507/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Field Blank
Water
AZG0821-01 AZG082107/27/16 14:36
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 106 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 15:1507/29/16 06:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 15:1507/29/16 06:3080-120
EPA 8260B 100 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 15:1507/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Trip Blank
Water
AZG0821-02 AZG082107/26/16 08:00
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6080016EPA 5030B 4.9 67-64-1 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Acrylonitrile200 6080016EPA 5030B 1.8 107-13-1 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Benzene1.0 6080016EPA 5030B 0.2 71-43-2 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6080016EPA 5030B 0.7 74-97-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080016EPA 5030B 0.6 75-27-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Bromoform3.0 6080016EPA 5030B 0.7 75-25-2 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Bromomethane10 6080016EPA 5030B 0.8 74-83-9 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6080016EPA 5030B 0.6 75-15-0 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080016EPA 5030B 0.6 56-23-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6080016EPA 5030B 0.4 108-90-7 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Chloroethane10 6080016EPA 5030B 0.4 75-00-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Chloroform5.0 6080016EPA 5030B 0.3 67-66-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Chloromethane1.0 6080016EPA 5030B 0.4 74-87-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080016EPA 5030B 0.7 124-48-1 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080016EPA 5030B 2.0 96-12-8 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080016EPA 5030B 0.7 106-93-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Dibromomethane10 6080016EPA 5030B 0.7 74-95-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080016EPA 5030B 0.5 95-50-1 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6080016EPA 5030B 0.3 106-46-7 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080016EPA 5030B 1.5 110-57-6 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080016EPA 5030B 0.4 75-34-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6080016EPA 5030B 0.3 107-06-2 07/29/16 15:4007/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Trip Blank
Water
AZG0821-02 AZG082107/26/16 08:00
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080016EPA 5030B 0.5 75-35-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.5 156-59-2 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080016EPA 5030B 0.4 156-60-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080016EPA 5030B 0.5 78-87-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-01-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080016EPA 5030B 0.4 10061-02-6 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6080016EPA 5030B 0.2 100-41-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Iodomethane10 6080016EPA 5030B 0.6 74-88-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6080016EPA 5030B 0.9 591-78-6 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080016EPA 5030B 0.5 75-09-2 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6080016EPA 5030B 1.1 78-93-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6080016EPA 5030B 1.7 108-10-1 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Styrene1.0 6080016EPA 5030B 0.4 100-42-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080016EPA 5030B 0.6 630-20-6 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080016EPA 5030B 0.5 79-34-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080016EPA 5030B 0.4 127-18-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Toluene1.0 6080016EPA 5030B 0.3 108-88-3 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080016EPA 5030B 0.4 71-55-6 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080016EPA 5030B 0.8 79-00-5 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Trichloroethene1.0 6080016EPA 5030B 0.4 79-01-6 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080016EPA 5030B 0.5 75-69-4 07/29/16 15:4007/29/16 06:30
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Trip Blank
Water
AZG0821-02 AZG082107/26/16 08:00
Project:East Carolina Regional Landfill
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080016EPA 5030B 0.7 96-18-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6080016EPA 5030B 0.8 108-05-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080016EPA 5030B 0.7 75-01-4 07/29/16 15:4007/29/16 06:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6080016EPA 5030B 0.4 1330-20-7 07/29/16 15:4007/29/16 06:30
EPA 8260B 102 %Surr: Dibromofluoromethane 6080016EPA 5030B 1868-53-7 07/29/16 15:4007/29/16 06:3080-120
EPA 8260B 106 %Surr: 1,2-Dichloroethane-d4 6080016EPA 5030B 17060-07-0 07/29/16 15:4007/29/16 06:3078-120
EPA 8260B 103 %Surr: Toluene-d8 6080016EPA 5030B 2037-26-5 07/29/16 15:4007/29/16 06:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6080016EPA 5030B 460-00-4 07/29/16 15:4007/29/16 06:3080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Blank (6080214-BLK1)Prepared & Analyzed: 08/09/16
Antimony ug/L0.45 6.00 J
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/L4.04 10.0 J
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Antimony ug/L1076.00 100.00 80-120107
Arsenic ug/L99.1 10.0 100.00 80-12099
Barium ug/L93.8 100 100.00 J80-12094
Beryllium ug/L91.1 1.00 100.00 80-12091
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L10310.0 100.00 80-120103
Cobalt ug/L98.2 10.0 100.00 80-12098
Copper ug/L98.6 10.0 100.00 80-12099
Lead ug/L91.7 10.0 100.00 80-12092
Nickel ug/L10250.0 100.00 80-120102
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Selenium ug/L97.0 10.0 100.00 80-12097
Silver ug/L98.1 10.0 100.00 80-12098
Thallium ug/L93.0 5.50 100.00 80-12093
Vanadium ug/L99.9 25.0 100.00 80-120100
Zinc ug/L10710.0 100.00 80-120107
Matrix Spike (6080214-MS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L97.7 6.00 100.00 ND 75-12598
Arsenic ug/L10810.0 100.00 3.51 75-125105
Barium ug/L507100 100.00 453 QM-0275-12554
Beryllium ug/L84.6 1.00 100.00 0.21 75-12584
Cadmium ug/L1041.00 100.00 0.18 75-125104
Chromium ug/L10510.0 100.00 ND 75-125105
Cobalt ug/L98.6 10.0 100.00 ND 75-12599
Copper ug/L10110.0 100.00 3.71 75-12597
Lead ug/L93.2 10.0 100.00 4.00 75-12589
Nickel ug/L10350.0 100.00 0.97 75-125102
Selenium ug/L10410.0 100.00 1.00 75-125103
Silver ug/L97.0 10.0 100.00 0.40 75-12597
Thallium ug/L91.3 5.50 100.00 ND 75-12591
Vanadium ug/L10625.0 100.00 ND 75-125106
Zinc ug/L11410.0 100.00 4.78 75-125109
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L1026.00 100.00 ND 2075-125102 4
Arsenic ug/L10410.0 100.00 3.51 2075-125100 4
Barium ug/L525100 100.00 453 20 QM-0275-12572 3
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Beryllium ug/L85.2 1.00 100.00 0.21 2075-12585 0.8
Cadmium ug/L1001.00 100.00 0.18 2075-125100 4
Chromium ug/L10810.0 100.00 ND 2075-125108 3
Cobalt ug/L10010.0 100.00 ND 2075-125100 1
Copper ug/L98.8 10.0 100.00 3.71 2075-12595 2
Lead ug/L92.8 10.0 100.00 4.00 2075-12589 0.4
Nickel ug/L10150.0 100.00 0.97 2075-125100 2
Selenium ug/L94.5 10.0 100.00 1.00 2075-12593 9
Silver ug/L98.2 10.0 100.00 0.40 2075-12598 1
Thallium ug/L90.7 5.50 100.00 ND 2075-12591 0.7
Vanadium ug/L11025.0 100.00 ND 2075-125110 3
Zinc ug/L10910.0 100.00 4.78 2075-125104 5
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L98.0 100.00 0.15 80-12098
Arsenic ug/L109 100.00 3.51 80-120105
Barium ug/L543 100.00 453 80-12090
Beryllium ug/L82.8 100.00 0.21 80-12083
Cadmium ug/L100 100.00 0.18 80-120100
Chromium ug/L102 100.00 0.34 80-120102
Cobalt ug/L97.3 100.00 0.17 80-12097
Copper ug/L95.3 100.00 3.71 80-12092
Lead ug/L92.0 100.00 4.00 80-12088
Nickel ug/L95.0 100.00 0.97 80-12094
Selenium ug/L99.8 100.00 1.00 80-12099
Silver ug/L96.4 100.00 0.40 80-12096
Thallium ug/L91.5 100.00 0.01 80-12091
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Vanadium ug/L104 100.00 0.31 80-120103
Zinc ug/L111 100.00 4.78 80-120106
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
Blank (6080016-BLK1)Prepared & Analyzed: 07/29/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
Blank (6080016-BLK1)Prepared & Analyzed: 07/29/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 9949
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10351
ug/L 50.000 80-120Surr: Toluene-d8 10753
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10050
LCS (6080016-BS1)Prepared & Analyzed: 07/29/16
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
LCS (6080016-BS1)Prepared & Analyzed: 07/29/16
Benzene ug/L44 50.000 67-13488
Chlorobenzene ug/L49 50.000 69-12299
1,1-Dichloroethene ug/L50 50.000 58-142100
Toluene ug/L45 50.000 68-12790
Trichloroethene ug/L49 50.000 72-13297
ug/L 50.000 80-120Surr: Dibromofluoromethane 10050
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10050
ug/L 50.000 80-120Surr: Toluene-d8 10653
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10050
Matrix Spike (6080016-MS1)Prepared & Analyzed: 07/29/16 Source: AZG0817-02
Benzene ug/L45 50.000 ND 67-13489
Chlorobenzene ug/L48 50.000 ND 69-12296
1,1-Dichloroethene ug/L51 50.000 ND 58-142103
Toluene ug/L45 50.000 ND 68-12789
Trichloroethene ug/L48 50.000 ND 72-13296
ug/L 50.000 80-120Surr: Dibromofluoromethane 10050
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10653
ug/L 50.000 80-120Surr: Toluene-d8 10553
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
Matrix Spike Dup (6080016-MSD1)Prepared & Analyzed: 07/29/16 Source: AZG0817-02
Benzene ug/L46 50.000 ND 967-13493 4
Chlorobenzene ug/L51 50.000 ND 1369-122101 5
1,1-Dichloroethene ug/L54 50.000 ND 958-142107 4
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080016 - EPA 5030B
Matrix Spike Dup (6080016-MSD1)Prepared & Analyzed: 07/29/16 Source: AZG0817-02
Toluene ug/L48 50.000 ND 968-12795 6
Trichloroethene ug/L51 50.000 ND 1172-132103 6
ug/L 50.000 80-120Surr: Dibromofluoromethane 9949
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10553
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10150
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Laboratory Certifications
Code Description Number Expires
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2016 06/30/2017NELAC
98011001South Carolina 08/30/2016SC
T104704397-08-TXTexas 03/31/2017TX
1340Virginia 12/14/2016VA
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
B-01 Analyte was detected in the associated method blank at an estimated level equal to or greater than the MDL. Sample values reported as greater than the MDL
and less than 10x the method blank value are reported as estimated values.
Note: Unless otherwise noted, all results are reported on an as received basis.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
COC Goes Here
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
East Carolina Regional LandfillProject:
Client:
Printed: 8/15/2016 4:32:59PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, INC.
Date Received:07/28/16 09:00 Logged In By:Charles Hawks
Work Order:AZG0821
OBSERVATIONS
Attn: Mr. Matt Einsmann
#Samples: 2 #Containers: 7
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
Comments:
Page 1 of 1
PACE ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: East Carolina Regional Landfill Leachate
Conover, NC 28613
1220 Commerce Street, SW
Mr. Matt Einsmann
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, Inc. certifies
that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the
samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
August 15, 2016
Report Number:AZG0823
Approved:
This report may not be reproduced, except in full, without written approval from Pace Analytical Services, Inc.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
0803-Leachate AZG0823-01 07/27/16 14:08 07/28/16 09:00Water
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Leachate
Water
AZG0823-01 AZG082307/27/16 14:08
Project:East Carolina Regional Landfill Leachate
07/28/16 09:00
General Chemistry
SM 5210 B 1890000 ug/L5Biochemical Oxygen Demand 213000 6070655SM 5210 B 2.0 E-10106 08/02/16 11:1507/28/16 13:30
SM 5220 D 5780000 ug/L10Chemical Oxygen Demand 100000 6080191EPA 410.4 100000 E-10117 08/08/16 12:4008/06/16 14:00
NDEPA 9010C/9014 ug/L1Cyanide, Total 100 R-01 6080192EPA 9010 100 57-12-5 08/08/16 14:4508/06/16 13:00
EPA 1664B 14000 ug/L1Oil & Grease (HEM)6000 P-04 6080073EPA 1664 6000 C-007 08/03/16 07:4508/03/16 07:45
EPA 420.1 2860 ug/L5Total Phenols as Phenol 250 6070669EPA 420.1 250 E-10253 07/29/16 14:3207/29/16 10:41
SM 4500-P B,E 6930 ug/L1.11Phosphorus-Total 222 6070691SM 4500-P B 0.22 7723-14-0 08/01/16 16:4708/01/16 10:50
EPA 351.2 2220000 ug/L500Total Kjeldahl Nitrogen as N 200000 6080226EPA 351.2 200000 E-10264 08/10/16 11:1608/09/16 10:45
SM 2540 D 117000 ug/L1Total Suspended Solids 10000 6080010SM 2540 D 10000 E-10162 08/01/16 15:2408/01/16 15:24
Inorganic Anions
NDEPA 9056A ug/L1Nitrate/Nitrite as N 50 6070658EPA 300.0 50 E-10128 07/28/16 15:0707/28/16 11:20
NDEPA 9056A ug/L1Nitrate as N 50 6070658EPA 300.0 50 14797-55-8 07/28/16 15:0707/28/16 11:20
NDEPA 9056A ug/L1Nitrite as N 50 6070658EPA 300.0 50 1594-56-5 07/28/16 15:0707/28/16 11:20
NDEPA 9056A ug/L1Sulfate5000 6070658EPA 300.0 5000 14808-79-8 07/28/16 15:0707/28/16 11:20
Metals, Total
EPA 6020B 58.2 ug/L5Antimony30.0 B-01 6080214EPA 3005A 1.25 7440-36-0 08/11/16 15:1708/09/16 09:20
EPA 6020B 325 ug/L5Arsenic50.0 6080214EPA 3005A 3.73 7440-38-2 08/11/16 15:1708/09/16 09:20
EPA 6020B 349 ug/L5Barium100 6080214EPA 3005A 1.49 7440-39-3 08/11/16 15:1708/09/16 09:20
EPA 6020B 0.14 ug/L1Beryllium1.00 J 6080214EPA 3005A 0.09 7440-41-7 08/09/16 22:0808/09/16 09:20
NDEPA 6020B ug/L1Cadmium1.00 6080214EPA 3005A 0.10 7440-43-9 08/09/16 22:0808/09/16 09:20
EPA 6020B 384 ug/L1Chromium10.0 6080214EPA 3005A 0.43 7440-47-3 08/09/16 22:0808/09/16 09:20
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Leachate
Water
AZG0823-01 AZG082307/27/16 14:08
Project:East Carolina Regional Landfill Leachate
07/28/16 09:00
Metals, Total
EPA 6020B 32.8 ug/L1Cobalt10.0 6080214EPA 3005A 0.29 7440-48-4 08/09/16 22:0808/09/16 09:20
EPA 6020B 4.15 ug/L1Copper10.0 J 6080214EPA 3005A 0.41 7440-50-8 08/09/16 22:0808/09/16 09:20
EPA 6020B 3.20 ug/L5Lead10.0 J 6080214EPA 3005A 0.42 7439-92-1 08/09/16 22:0808/09/16 09:20
EPA 6020B 146 ug/L1Nickel50.0 6080214EPA 3005A 0.48 7440-02-0 08/09/16 22:0808/09/16 09:20
NDEPA 6020B ug/L5Selenium10.0 6080214EPA 3005A 4.27 7782-49-2 08/12/16 12:1108/09/16 09:20
NDEPA 6020B ug/L5Silver10.0 6080214EPA 3005A 1.12 7440-22-4 08/11/16 15:1708/09/16 09:20
NDEPA 6020B ug/L5Thallium5.50 6080214EPA 3005A 0.28 7440-28-0 08/11/16 15:1708/09/16 09:20
EPA 6020B 238 ug/L1Vanadium25.0 6080214EPA 3005A 1.57 7440-62-2 08/09/16 22:0808/09/16 09:20
EPA 6020B 181 ug/L1Zinc10.0 B-01 6080214EPA 3005A 1.30 7440-66-6 08/11/16 15:1708/09/16 09:20
NDEPA 7470A ug/L1Mercury1.33 R-01 6080217EPA 7470A 0.880 7439-97-6 08/10/16 15:2108/09/16 14:50
Volatile Organic Compounds by EPA 8260
EPA 8260B 9400 ug/L100Acetone5000 6080022EPA 5030B 490 67-64-1 08/01/16 20:1608/01/16 15:00
NDEPA 8260B ug/L1Acrylonitrile200 6080022EPA 5030B 1.8 107-13-1 08/01/16 16:4508/01/16 15:00
EPA 8260B 2.0 ug/L1Benzene1.0 B-01 6080022EPA 5030B 0.2 71-43-2 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6080022EPA 5030B 0.7 74-97-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6080022EPA 5030B 0.6 75-27-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Bromoform3.0 6080022EPA 5030B 0.7 75-25-2 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Bromomethane10 6080022EPA 5030B 0.8 74-83-9 08/01/16 16:4508/01/16 15:00
EPA 8260B 1.2 ug/L1Carbon Disulfide 100 J 6080022EPA 5030B 0.6 75-15-0 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6080022EPA 5030B 0.6 56-23-5 08/01/16 16:4508/01/16 15:00
EPA 8260B 0.6 ug/L1Chlorobenzene3.0 J 6080022EPA 5030B 0.4 108-90-7 08/01/16 16:4508/01/16 15:00
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Leachate
Water
AZG0823-01 AZG082307/27/16 14:08
Project:East Carolina Regional Landfill Leachate
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chloroethane10 6080022EPA 5030B 0.4 75-00-3 08/01/16 16:4508/01/16 15:00
EPA 8260B 0.3 ug/L1Chloroform5.0 B-01, J 6080022EPA 5030B 0.3 67-66-3 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Chloromethane1.0 6080022EPA 5030B 0.4 74-87-3 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6080022EPA 5030B 0.7 124-48-1 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6080022EPA 5030B 2.0 96-12-8 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6080022EPA 5030B 0.7 106-93-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Dibromomethane10 6080022EPA 5030B 0.7 74-95-3 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6080022EPA 5030B 0.5 95-50-1 08/01/16 16:4508/01/16 15:00
EPA 8260B 7.0 ug/L11,4-Dichlorobenzene 1.0 6080022EPA 5030B 0.3 106-46-7 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6080022EPA 5030B 1.5 110-57-6 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6080022EPA 5030B 0.4 75-34-3 08/01/16 16:4508/01/16 15:00
EPA 8260B 0.3 ug/L11,2-Dichloroethane 1.0 J 6080022EPA 5030B 0.3 107-06-2 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6080022EPA 5030B 0.5 75-35-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6080022EPA 5030B 0.5 156-59-2 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6080022EPA 5030B 0.4 156-60-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6080022EPA 5030B 0.5 78-87-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6080022EPA 5030B 0.4 10061-01-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6080022EPA 5030B 0.4 10061-02-6 08/01/16 16:4508/01/16 15:00
EPA 8260B 18 ug/L1Ethylbenzene1.0 6080022EPA 5030B 0.2 100-41-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Iodomethane10 6080022EPA 5030B 0.6 74-88-4 08/01/16 16:4508/01/16 15:00
EPA 8260B 16 ug/L1Methyl Butyl Ketone
(2-Hexanone)50 J 6080022EPA 5030B 0.9 591-78-6 08/01/16 16:4508/01/16 15:00
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Leachate
Water
AZG0823-01 AZG082307/27/16 14:08
Project:East Carolina Regional Landfill Leachate
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 6080022EPA 5030B 0.5 75-09-2 08/01/16 16:4508/01/16 15:00
EPA 8260B 8100 ug/L100Methyl Ethyl Ketone
(2-Butanone)5000 6080022EPA 5030B 110 78-93-3 08/01/16 20:1608/01/16 15:00
EPA 8260B 90 ug/L14-Methyl-2-pentanone (MIBK)100 J 6080022EPA 5030B 1.7 108-10-1 08/01/16 16:4508/01/16 15:00
EPA 8260B 3.1 ug/L1Styrene1.0 6080022EPA 5030B 0.4 100-42-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6080022EPA 5030B 0.6 630-20-6 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6080022EPA 5030B 0.5 79-34-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6080022EPA 5030B 0.4 127-18-4 08/01/16 16:4508/01/16 15:00
EPA 8260B 23 ug/L1Toluene1.0 6080022EPA 5030B 0.3 108-88-3 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6080022EPA 5030B 0.4 71-55-6 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6080022EPA 5030B 0.8 79-00-5 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Trichloroethene1.0 6080022EPA 5030B 0.4 79-01-6 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6080022EPA 5030B 0.5 75-69-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6080022EPA 5030B 0.7 96-18-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6080022EPA 5030B 0.8 108-05-4 08/01/16 16:4508/01/16 15:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6080022EPA 5030B 0.7 75-01-4 08/01/16 16:4508/01/16 15:00
EPA 8260B 34 ug/L1Xylenes, total 5.0 6080022EPA 5030B 0.4 1330-20-7 08/01/16 16:4508/01/16 15:00
EPA 8260B 86 %Surr: Dibromofluoromethane 6080022EPA 5030B 1868-53-7 08/01/16 20:1608/01/16 15:0080-120
EPA 8260B 83 %Surr: Dibromofluoromethane 6080022EPA 5030B 1868-53-7 08/01/16 16:4508/01/16 15:0080-120
EPA 8260B 83 %Surr: 1,2-Dichloroethane-d4 6080022EPA 5030B 17060-07-0 08/01/16 16:4508/01/16 15:0078-120
EPA 8260B 86 %Surr: 1,2-Dichloroethane-d4 6080022EPA 5030B 17060-07-0 08/01/16 20:1608/01/16 15:0078-120
EPA 8260B 99 %Surr: Toluene-d8 6080022EPA 5030B 2037-26-5 08/01/16 20:1608/01/16 15:0080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
0803-Leachate
Water
AZG0823-01 AZG082307/27/16 14:08
Project:East Carolina Regional Landfill Leachate
07/28/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 96 %Surr: Toluene-d8 6080022EPA 5030B 2037-26-5 08/01/16 16:4508/01/16 15:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6080022EPA 5030B 460-00-4 08/01/16 16:4508/01/16 15:0080-120
EPA 8260B 107 %Surr: 4-Bromofluorobenzene 6080022EPA 5030B 460-00-4 08/01/16 20:1608/01/16 15:0080-120
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6070655 - SM 5210 B
Blank (6070655-BLK1)Prepared: 07/28/16 Analyzed: 08/02/16
Biochemical Oxygen Demand ug/L50.0 2000 J
LCS (6070655-BS1)Prepared: 07/28/16 Analyzed: 08/02/16
Biochemical Oxygen Demand ug/L1910002000 198000 85-11596
Duplicate (6070655-DUP1)Prepared: 07/28/16 Analyzed: 08/02/16 Source: AZG0843-01
Biochemical Oxygen Demand ug/L26000043000 248000 205
Batch 6070669 - EPA 420.1
Blank (6070669-BLK1)Prepared & Analyzed: 07/29/16
Total Phenols as Phenol ug/LND50.0
LCS (6070669-BS1)Prepared & Analyzed: 07/29/16
Total Phenols as Phenol ug/L53350.0 500.00 80-120107
Duplicate (6070669-DUP1)Prepared & Analyzed: 07/29/16 Source: AZG0588-01
Total Phenols as Phenol ug/L73050.0 720 201
Matrix Spike (6070669-MS1)Prepared & Analyzed: 07/29/16 Source: AZG0794-01
Total Phenols as Phenol ug/L41950.0 500.00 ND 80-12084
Matrix Spike Dup (6070669-MSD1)Prepared & Analyzed: 07/29/16 Source: AZG0794-01
Total Phenols as Phenol ug/L40950.0 500.00 ND 2080-12082 2
Batch 6070691 - SM 4500-P B
Blank (6070691-BLK1)Prepared & Analyzed: 08/01/16
Phosphorus-Total ug/L1.00 20.0 J
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6070691 - SM 4500-P B
LCS (6070691-BS1)Prepared & Analyzed: 08/01/16
Phosphorus-Total ug/L50520.0 500.00 88-110101
Batch 6080010 - SM 2540 D
Blank (6080010-BLK1)Prepared & Analyzed: 08/01/16
Total Suspended Solids ug/LND5000
LCS (6080010-BS1)Prepared & Analyzed: 08/01/16
Total Suspended Solids ug/L990005000 100000 90-11099
Duplicate (6080010-DUP1)Prepared & Analyzed: 08/01/16 Source: AZG0823-01
Total Suspended Solids ug/L11500010000 117000 102
Batch 6080073 - EPA 1664
Blank (6080073-BLK1)Prepared & Analyzed: 08/03/16
Oil & Grease (HEM)ug/LND5000
LCS (6080073-BS1)Prepared & Analyzed: 08/03/16
Oil & Grease (HEM)ug/L360005000 40000 78-11491
Duplicate (6080073-DUP1)Prepared & Analyzed: 08/03/16 Source: AZG0871-02
Oil & Grease (HEM)ug/LND6800 ND 75 P-04
Matrix Spike (6080073-MS1)Prepared & Analyzed: 08/03/16 Source: AZG0806-02
Oil & Grease (HEM)ug/L420005500 43956 ND 78-11496
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6080191 - EPA 410.4
Blank (6080191-BLK1)Prepared: 08/06/16 Analyzed: 08/08/16
Chemical Oxygen Demand ug/LND10000
LCS (6080191-BS1)Prepared: 08/06/16 Analyzed: 08/08/16
Chemical Oxygen Demand ug/L18900010000 200000 90-11094
Duplicate (6080191-DUP1)Prepared: 08/06/16 Analyzed: 08/08/16 Source: AZH0125-01
Chemical Oxygen Demand ug/L31300010000 323000 103
Matrix Spike (6080191-MS1)Prepared: 08/06/16 Analyzed: 08/08/16 Source: AZH0101-01
Chemical Oxygen Demand ug/L8680000200000 4000000 4370000 90-110108
Matrix Spike (6080191-MS2)Prepared: 08/06/16 Analyzed: 08/08/16 Source: AZH0101-02
Chemical Oxygen Demand ug/L10500000200000 4000000 6950000 90-11090
Matrix Spike Dup (6080191-MSD1)Prepared: 08/06/16 Analyzed: 08/08/16 Source: AZH0101-01
Chemical Oxygen Demand ug/L8150000200000 4000000 4370000 1090-11094 6
Batch 6080192 - EPA 9010
Blank (6080192-BLK1)Prepared: 08/06/16 Analyzed: 08/08/16
Cyanide, Total ug/LND10.0
LCS (6080192-BS1)Prepared: 08/06/16 Analyzed: 08/08/16
Cyanide, Total ug/L82.0 10.0 80.000 85-115102
Matrix Spike (6080192-MS1)Prepared: 08/06/16 Analyzed: 08/08/16 Source: AZG0888-01
Cyanide, Total ug/L83.0 10.0 80.000 ND 85-119104
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6080192 - EPA 9010
Matrix Spike Dup (6080192-MSD1)Prepared: 08/06/16 Analyzed: 08/08/16 Source: AZG0888-01
Cyanide, Total ug/L84.0 10.0 80.000 ND 1385-119105 1
Batch 6080226 - EPA 351.2
Blank (6080226-BLK1)Prepared: 08/09/16 Analyzed: 08/10/16
Total Kjeldahl Nitrogen as N ug/LND400
LCS (6080226-BS1)Prepared: 08/09/16 Analyzed: 08/10/16
Total Kjeldahl Nitrogen as N ug/L10700400 10000 90-110107
Matrix Spike (6080226-MS1)Prepared: 08/09/16 Analyzed: 08/10/16 Source: AZH0086-01
Total Kjeldahl Nitrogen as N ug/L10800400 10000 ND 90-110108
Matrix Spike (6080226-MS2)Prepared: 08/09/16 Analyzed: 08/10/16 Source: AZH0093-01
Total Kjeldahl Nitrogen as N ug/L11700400 10000 913 90-110108
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 6070658 - EPA 300.0
Blank (6070658-BLK1)Prepared & Analyzed: 07/28/16
Nitrate/Nitrite as N ug/LND50
Nitrate as N ug/LND50
Nitrite as N ug/LND50
Sulfate ug/LND5000
LCS (6070658-BS1)Prepared & Analyzed: 07/28/16
Nitrate/Nitrite as N ug/L2010050 20010 90-110100
Nitrate as N ug/L989050 10010 90-11099
Nitrite as N ug/L1020050 10000 90-110102
Sulfate ug/L98705000 10010 90-11099
Matrix Spike (6070658-MS1)Prepared & Analyzed: 07/28/16 Source: AZG0801-01
Nitrate/Nitrite as N ug/L1830050 20010 207 90-11090
Nitrate as N ug/L908050 10010 207 QM-0590-11089
Nitrite as N ug/L918050 10000 ND 90-11092
Sulfate ug/L163005000 10010 7860 QM-0590-11084
Matrix Spike Dup (6070658-MSD1)Prepared & Analyzed: 07/28/16 Source: AZG0801-01
Nitrate/Nitrite as N ug/L1960050 20010 207 1590-11097 7
Nitrate as N ug/L974050 10010 207 1590-11095 7
Nitrite as N ug/L984050 10000 ND 1590-11098 7
Sulfate ug/L169005000 10010 7860 1590-11090 4
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Blank (6080214-BLK1)Prepared & Analyzed: 08/09/16
Antimony ug/L0.45 6.00 J
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/L4.04 10.0 J
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Antimony ug/L1076.00 100.00 80-120107
Arsenic ug/L99.1 10.0 100.00 80-12099
Barium ug/L93.8 100 100.00 J80-12094
Beryllium ug/L91.1 1.00 100.00 80-12091
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L10310.0 100.00 80-120103
Cobalt ug/L98.2 10.0 100.00 80-12098
Copper ug/L98.6 10.0 100.00 80-12099
Lead ug/L91.7 10.0 100.00 80-12092
Nickel ug/L10250.0 100.00 80-120102
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
LCS (6080214-BS1)Prepared & Analyzed: 08/09/16
Selenium ug/L97.0 10.0 100.00 80-12097
Silver ug/L98.1 10.0 100.00 80-12098
Thallium ug/L93.0 5.50 100.00 80-12093
Vanadium ug/L99.9 25.0 100.00 80-120100
Zinc ug/L10710.0 100.00 80-120107
Matrix Spike (6080214-MS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L97.7 6.00 100.00 ND 75-12598
Arsenic ug/L10810.0 100.00 3.51 75-125105
Barium ug/L507100 100.00 453 QM-0275-12554
Beryllium ug/L84.6 1.00 100.00 0.21 75-12584
Cadmium ug/L1041.00 100.00 0.18 75-125104
Chromium ug/L10510.0 100.00 ND 75-125105
Cobalt ug/L98.6 10.0 100.00 ND 75-12599
Copper ug/L10110.0 100.00 3.71 75-12597
Lead ug/L93.2 10.0 100.00 4.00 75-12589
Nickel ug/L10350.0 100.00 0.97 75-125102
Selenium ug/L10410.0 100.00 1.00 75-125103
Silver ug/L97.0 10.0 100.00 0.40 75-12597
Thallium ug/L91.3 5.50 100.00 ND 75-12591
Vanadium ug/L10625.0 100.00 ND 75-125106
Zinc ug/L11410.0 100.00 4.78 75-125109
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L1026.00 100.00 ND 2075-125102 4
Arsenic ug/L10410.0 100.00 3.51 2075-125100 4
Barium ug/L525100 100.00 453 20 QM-0275-12572 3
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Matrix Spike Dup (6080214-MSD1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Beryllium ug/L85.2 1.00 100.00 0.21 2075-12585 0.8
Cadmium ug/L1001.00 100.00 0.18 2075-125100 4
Chromium ug/L10810.0 100.00 ND 2075-125108 3
Cobalt ug/L10010.0 100.00 ND 2075-125100 1
Copper ug/L98.8 10.0 100.00 3.71 2075-12595 2
Lead ug/L92.8 10.0 100.00 4.00 2075-12589 0.4
Nickel ug/L10150.0 100.00 0.97 2075-125100 2
Selenium ug/L94.5 10.0 100.00 1.00 2075-12593 9
Silver ug/L98.2 10.0 100.00 0.40 2075-12598 1
Thallium ug/L90.7 5.50 100.00 ND 2075-12591 0.7
Vanadium ug/L11025.0 100.00 ND 2075-125110 3
Zinc ug/L10910.0 100.00 4.78 2075-125104 5
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Antimony ug/L98.0 100.00 0.15 80-12098
Arsenic ug/L109 100.00 3.51 80-120105
Barium ug/L543 100.00 453 80-12090
Beryllium ug/L82.8 100.00 0.21 80-12083
Cadmium ug/L100 100.00 0.18 80-120100
Chromium ug/L102 100.00 0.34 80-120102
Cobalt ug/L97.3 100.00 0.17 80-12097
Copper ug/L95.3 100.00 3.71 80-12092
Lead ug/L92.0 100.00 4.00 80-12088
Nickel ug/L95.0 100.00 0.97 80-12094
Selenium ug/L99.8 100.00 1.00 80-12099
Silver ug/L96.4 100.00 0.40 80-12096
Thallium ug/L91.5 100.00 0.01 80-12091
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6080214 - EPA 3005A
Post Spike (6080214-PS1)Prepared & Analyzed: 08/09/16 Source: AZG0767-04
Vanadium ug/L104 100.00 0.31 80-120103
Zinc ug/L111 100.00 4.78 80-120106
Batch 6080217 - EPA 7470A
Blank (6080217-BLK1)Prepared: 08/09/16 Analyzed: 08/10/16
Mercury ug/LND0.200
LCS (6080217-BS1)Prepared: 08/09/16 Analyzed: 08/10/16
Mercury ug/L2.24 0.200 2.5000 80-12090
Matrix Spike (6080217-MS1)Prepared: 08/09/16 Analyzed: 08/10/16 Source: AZH0185-01
Mercury ug/L2.33 0.200 2.5000 ND 75-12593
Matrix Spike Dup (6080217-MSD1)Prepared: 08/09/16 Analyzed: 08/10/16 Source: AZH0185-01
Mercury ug/L2.21 0.200 2.5000 ND 2075-12588 6
Post Spike (6080217-PS1)Prepared: 08/09/16 Analyzed: 08/10/16 Source: AZH0185-01
Mercury ug/L1.51 1.6667 0.003 80-12090
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080022 - EPA 5030B
Blank (6080022-BLK1)Prepared & Analyzed: 08/01/16
Acetone ug/LND50
Acrylonitrile ug/LND200
Benzene ug/L0.2 1.0 J
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/L0.4 5.0 J
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080022 - EPA 5030B
Blank (6080022-BLK1)Prepared & Analyzed: 08/01/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/L1.7 1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND50
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 8542
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 8040
ug/L 50.000 80-120Surr: Toluene-d8 9547
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Blank (6080022-BLK2)Prepared & Analyzed: 08/02/16
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080022 - EPA 5030B
Blank (6080022-BLK2)Prepared & Analyzed: 08/02/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/L0.3 1.0 J
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/L0.5 5.0 J
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080022 - EPA 5030B
Blank (6080022-BLK2)Prepared & Analyzed: 08/02/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 8844
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 8643
ug/L 50.000 80-120Surr: Toluene-d8 9950
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10955
LCS (6080022-BS1)Prepared & Analyzed: 08/01/16
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080022 - EPA 5030B
LCS (6080022-BS1)Prepared & Analyzed: 08/01/16
Benzene ug/L46 50.000 67-13492
Chlorobenzene ug/L46 50.000 69-12293
1,1-Dichloroethene ug/L40 50.000 58-14279
Toluene ug/L45 50.000 68-12790
Trichloroethene ug/L49 50.000 72-13298
ug/L 50.000 80-120Surr: Dibromofluoromethane 9648
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 8241
ug/L 50.000 80-120Surr: Toluene-d8 9447
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9547
Matrix Spike (6080022-MS1)Prepared & Analyzed: 08/01/16 Source: AZG0767-12
Benzene ug/L65 50.000 0.4 67-134129
Chlorobenzene ug/L65 50.000 ND QM-0569-122131
1,1-Dichloroethene ug/L53 50.000 ND 58-142105
Toluene ug/L61 50.000 0.4 68-127121
Trichloroethene ug/L69 50.000 ND QM-0572-132137
ug/L 50.000 80-120Surr: Dibromofluoromethane 8241
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 8844
ug/L 50.000 80-120Surr: Toluene-d8 9447
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
Matrix Spike Dup (6080022-MSD1)Prepared & Analyzed: 08/01/16 Source: AZG0767-12
Benzene ug/L67 50.000 0.4 967-134133 3
Chlorobenzene ug/L80 50.000 ND 13 QM-0669-122160 20
1,1-Dichloroethene ug/L55 50.000 ND 958-142110 4
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6080022 - EPA 5030B
Matrix Spike Dup (6080022-MSD1)Prepared & Analyzed: 08/01/16 Source: AZG0767-12
Toluene ug/L67 50.000 0.4 9 QM-0668-127133 10
Trichloroethene ug/L72 50.000 ND 11 QM-0572-132145 6
ug/L 50.000 80-120Surr: Dibromofluoromethane 8141
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 8744
ug/L 50.000 80-120Surr: Toluene-d8 9648
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10050
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Laboratory Certifications
Code Description Number Expires
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2016 06/30/2017NELAC
98011001South Carolina 08/30/2016SC
T104704397-08-TXTexas 03/31/2017TX
1340Virginia 12/14/2016VA
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
R-01 Elevated reporting limit due to matrix interference.
QM-06 Due to suspected matrix interference, RPD and Percent Recovery values for the MS and/or MSD were outside control limits. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix interference. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
P-04 Sample was received preserved with proper preservative and pH within method specified limits but, due to sample matrix buffering during storage, required
further adjustment prior to extraction and/or analysis.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
B-01 Analyte was detected in the associated method blank at an estimated level equal to or greater than the MDL. Sample values reported as greater than the MDL
and less than 10x the method blank value are reported as estimated values.
Note: Unless otherwise noted, all results are reported on an as received basis.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann August 15, 2016
COC Goes Here
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
East Carolina Regional Landfill LeachateProject:
Client:
Printed: 8/15/2016 4:43:41PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, INC.
Date Received:07/28/16 09:00 Logged In By:Charles Hawks
Work Order:AZG0823
OBSERVATIONS
Attn: Mr. Matt Einsmann
#Samples: 1 #Containers: 12
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
The O/G, Metals, Phenols/TKN were pH adjusted from 7 to <2 with HCL, HNO3 and H2SO4 respectively. The Phenol
sample arrived with each vial being a different color. The darker black colored vial arrived unpreserved. The lighter beige
colored vial arrived with a pH <2. The darker vial was pH adjusted to <2 with H2SO4 but did not change color and was
consistent with the other containers that arrived. Consequently, the phenol was analyzed from the darker container. CFH
Comments:
Page 1 of 1

Appendix D

Statistical Analyses Worksheets and Summary Table

Summary of Statistical Analyses
(July 2016 Sampling Event)
Constituent NC 2L GWPS Data Distribution Statistical Method used to Establish
Background
Calculated
Background
Concentration
(µg/L)
Sample
Location
Sample Result
(µg/L) SSI
Cobalt N/E 1 34% Truncated
Normal Upper Tolerance Limit - Interwell 17.4 GW-2 8.68 J N/A
Cobalt N/E 1 0% Truncated
Normal Upper Tolerance Limit - Intrawell MW-7 50.7 GW-7 37.4 NO
Notes:
Concentrations are in micrograms per liter (µg/L).
GWPS = NC DENR Solid Waste Section Groundwater Protect Standard.
SSI = Statistically significant increase over background.
N/E = Not established.
N/A = Not applicable.
Republic - East Carolina Landfill
Permit # 08-03 Joyce Engineering