7304_UpperPiedmont_MSWLF_1stSemiGWMReport_DIN27213_20160126

PREPARED FOR:
REPUBLIC SERVICES OF NORTH CAROLINA, LLC
D.B.A. UPPER PIEDMONT ENVIRONMENTAL
9650 OXFORD ROAD
ROUGEMOUNT, NORTH CAROLINA 27572

UPPER PIEDMONT REGIONAL LANDFILL
PERMIT NO. 73-04

FIRST SEMIANNUAL
WATER QUALITY MONITORING REPORT
OF 2016

MARCH 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101 GREENSBORO, NORTH CAROLINA 27407 NC LICENSE NUMBER C-0782 PHONE: [phone] FAX: [phone]
JOYCE ENGINEERING PROJECT NO. 00893.1601.12

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First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering Upper Piedmont Regional Landfill, Permit No. 73-04 March 2016

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EXECUTIVE SUMMARY
This report presents the results of the first semiannual water quality monitoring event of 2016
conducted at the Upper Piedmont Regional Landfill on January 26, 2016. Samples were
collected from the compliance monitoring well network and the leachate collection system. The
analytical results from the January 26, 2016, monitoring event have been provided by Analytical Services, Inc. of Norcross, Georgia.
During the January 2016 water quality monitoring event, five NC Appendix I inorganic
constituents (barium, cobalt, copper, and zinc) and two additional indicator parameters (iron and
manganese) were reported at quantified concentrations above the Solid Waste Section Reporting Limits (SWSLs) in samples from one or more downgradient monitoring wells. No other NC Appendix I inorganic or organic constituents were detected above SWSLs in groundwater during
the January 26, 2016, monitoring event.

Additional indicator parameters, iron and manganese, were analyzed per a DENR request in a letter dated September 28, 2007. The concentrations detected in one or more downgradient wells during the January 26, 2016, sampling event were above their respective SWSLs and NC 2L
Standards. Iron and manganese are common, naturally-occurring, inorganic constituents, and are
not NC Appendix I constituents. Data from the January 26, 2016, event are generally consistent
with historical values. No further action is required for detections of iron and manganese. Cobalt was detected above the Solid Waste Section Groundwater Protection Standards (GWPS)
in downgradient monitoring well GW-8. Cobalt is a common, naturally-occurring element in
soils in this region, and these results are generally consistent with historical values. Based on
interwell statistical analysis, the background value for cobalt is 31.5 µg/L. In accordance with 15A NCAC 13B.1634.(g).(5), we request that background concentrations be considered the applicable Groundwater Protection Standard (GPS) for cobalt for compliance sampling events at
this facility.

Iron and manganese were detected above the respective NC 2B surface water standards in samples collected from SW-2 during the January 2016 event; however, iron and manganese are commonly detected in both the upstream and downstream points and are considered to be
naturally-occurring. No other NC Appendix I constituents were detected above their relevant
NC 2B standard in SW-2 during the first semiannual monitoring event of 2016.
Based on the results summarized herein, Republic Services of NC, LLC, will continue monitoring the uppermost aquifer beneath the Upper Piedmont Regional Landfill in accordance
with the requirements for Detection Monitoring Program as outlined in Title 15A NCAC 13B
.1633.

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First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering Upper Piedmont Regional Landfill, Permit No. 73-04 March 2016

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First Semiannual Water Quality Monitoring Report of 2016
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina

TABLE OF CONTENTS

1.0 INTRODUCTION..............................................................................................................1 
1.1  Site Description and Background ................................................................................ 1 
1.2 Compliance Monitoring History .................................................................................. 1 
1.3 Hydrogeologic Setting ................................................................................................... 1 
2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION ......................2 
2.1 Visual Inspection Program........................................................................................... 2 
2.2 Well Network and Groundwater Elevation Measurements...................................... 3 
2.3 January 2016 Monitoring Event .................................................................................. 4 
2.4 Laboratory Analysis Program ..................................................................................... 5 
2.5 January 2016 Sampling Results ................................................................................... 5 
3.0 LABORATORY AND FIELD QA/QC ............................................................................5 
4.0 DATA EVALUTION .........................................................................................................6 
4.1 Comparisons to Groundwater and Surface Water Standards ................................. 6 
4.1.1   Groundwater Standard Exceedances ........................................................................ 6 
4.1.2   Surface Water Standard Exceedances ...................................................................... 6 
4.2 Statistical Evaluations .................................................................................................. 7 
5.0 CONCLUSIONS ................................................................................................................7 
6.0 REFERENCES ...................................................................................................................7 

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First Semiannual Water Quality Monitoring Report of 2016
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina

TABLE OF CONTENTS CONTINUED

Tables
Table 1 Historical Groundwater Elevations
Table 2 Estimated Hydraulic Gradients and Average Linear Velocities
Table 3 Well Construction Information Table 4 Detections by Monitoring Locations – January 2016 Table 5 Exceedances by Monitoring Locations – January 2016

Drawing
Drawing 1 Potentiometric Surface Map, January 26, 2016

Appendices
Appendix A Historical Tables
Table 6 Historically Detected Constituents/Analytes in Groundwater
Table 7 Historically Detected Constituents/Analytes in Surface Water
Table 8 Historically Detected Constituents/Analytes in Leachate
Table 9 Field Parameters by Location – January 2016
Appendix B Field Sampling Logs
Appendix C Laboratory Analytical Report
Appendix D Statistical Analyses Worksheets and Summary Table

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1.0 INTRODUCTION
The Upper Piedmont Regional Landfill, which is an active municipal solid waste landfill located
in Person County, North Carolina, is owned and operated by Republic Services of North
Carolina, LLC (Republic) under Permit No. 73-04 issued by the North Carolina Department of Environmental Quality (NCDEQ). This report summarizes the monitoring results from the January 26, 2016, water quality monitoring event at the Upper Piedmont Regional Landfill in
accordance with Title 15A of the North Carolina Administrative Code (NCAC) Subchapter 13B
.1632.

1.1 Site Description and Background
The Upper Piedmont Regional Landfill is located approximately nine miles east-southeast of the
town of Roxboro on U.S. Highway 158, in Durham County, North Carolina. The location of the
facility is shown on the inlay on Drawing 1. The landfill is bounded to the north by U.S.
Highway 158, tributaries of Club Creek to the east and south, and Rock Fork Branch to the west. Surrounding land use is primarily rural residential, silvicultural, and agricultural. Access to the facility is via the drive off of Oxford Road (U.S. Highway 158).

As shown on Drawing 1, the landfill is located at an elevation of 500 to 700 feet above mean sea
level. Surface drainage from the landfill and surrounding areas is routed by drainage channels and storm water control structures to tributaries of the easterly flowing Club Creek, a tributary of the Tar River.

1.2 Compliance Monitoring History
Water quality monitoring at the facility was initiated in May 1997 under the Detection Monitoring Program for municipal solid waste landfills. The facility’s monitoring network is comprised of ten monitoring wells (GW-1R through GW-10), which monitor the uppermost
aquifer beneath the facility. Upstream surface water monitoring point SW-1 and downstream
surface water monitoring point SW-2 are also sampled semiannually in accordance with the
approved monitoring plan. A sample from the facility’s leachate collection system is sampled semiannually as part of the facility’s environmental monitoring program.

1.3 Hydrogeologic Setting
Geologically, the facility is located within the Carolina Slate Belt of the Piedmont Physiographic
Province of North Carolina (NCGS 1985). The Carolina Slate Belt is composed of Late Proterozoic to Cambrian meta-sedimentary and meta-volcanic rocks that locally have been
intruded by diabase dikes and felsic intrusive suites. The rocks underlying the facility are
mapped as felsic meta-volcanics (dacitic and rhyolitic tuffs and flows interbedded with mafic
meta-volcanics (NCGS 1985).

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The uppermost groundwater beneath the facility is contained in a shallow, unconfined aquifer
comprised of partially weathered, fractured, meta-volcanic rock. Groundwater occurs at depths
of approximately 30 feet below grade along the western, upgradient side of the waste disposal
area, and at an average depth of five feet below grade along the eastern boundary. Depth-to-water measurements obtained during the January 26, 2016, monitoring event and summarized in Table 1 were used to prepare a groundwater surface contour map presented as Drawing 1.

The groundwater flow in the uppermost aquifer beneath the site is towards the east, with the flow
appearing to converge on the easterly flowing perennial tributary streams of Club Creek. The groundwater surface contour map and interpreted flow directions are consistent with previously submitted groundwater surface contour maps for this facility.

Based on the January 26, 2016, groundwater surface contour map, the hydraulic gradient in the
shallow aquifer underlying the site as measured along the conceptual flow paths shown on the contour map was calculated to be approximately 0.05 to 0.06 ft/ft. The estimated rates of groundwater flow for the uppermost aquifer beneath the facility were calculated using the
following modified Darcy equation:

Vgw = Ki/ne where Vgw = average linear velocity (feet/year), K = hydraulic conductivity (feet/day), i =
horizontal hydraulic gradient, and ne = effective porosity. The calculated linear groundwater
flow velocity under the waste management unit ranges from 5.3 to 6.2 feet/year. The flow
calculations are presented in Table 2. The linear velocity equation and resultant rates are based on the simplified assumptions of a
homogeneous and isotropic aquifer. This equation can be inaccurate when applied to
heterogeneous and/or anisotropic conditions such as in the saprolite wells used for gradient
estimates at this site. The saprolite may have areas that exhibit relict foliation and these structures can result in locally anisotropic groundwater flow and fractured bedrock is inherently
anisotropic and heterogeneous.

2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION
2.1 Visual Inspection Program
In order to detect potential releases of leachate and/or landfill gas migration in a timely manner,
a visual inspection program has been implemented at the Upper Piedmont Regional Landfill.

This inspection program involves field personnel making the following observations:
 Observation of stress induced on the biological community (e.g., dead or dying vegetation),
 Indications of leachate impact (e.g., seeps, impacted surface water),

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 Observations of erosion; and
 Negative changes around the waste facility.
During the January 26, 2016, monitoring event, no physical indicators were observed in the
vicinity of the waste management areas.

2.2 Well Network and Groundwater Elevation Measurements
The network of groundwater monitoring wells at the Upper Piedmont Regional Landfill currently consists of GW-1R, GW-2, GW-3, GW-4, GW-5, GW-6, GW-7, GW-8, GW-9, and GW-10.
Monitoring well construction information is summarized on Table 3 and the well locations are
shown on Drawing 1. The network of monitoring wells was constructed to target the flow path
for groundwater underlying waste disposal areas in the partially weathered fractured rock that
comprises the unconfined uppermost aquifer. Two surface water points are also monitored, including upstream point SW-1 and downstream point SW-2.

Monitoring well GW-1R is the facility’s background well and is located hydraulically upgradient
of the waste disposal area. Monitoring wells GW-2, GW-3, GW-4, GW-5, GW-6, GW-7, GW-8,
GW-9, and GW-10 are located downgradient or side-gradient of the waste disposal area and represent the facility’s downgradient compliance wells. The monitoring wells are equipped with
dedicated bladder pumps and were sampled via the micropurge method.

Monitoring well GW-1R was installed in July 2009 as a replacement for background well GW-1
due to the well being dry during several consecutive sampling events. Well GW-1R was sampled for the first time during the January 2010 sampling event. Well GW-1 was
decommissioned following the July 2009 event.

Downgradient wells GW-9 and GW-10 were installed in July 2009 and wells GW-7 and GW-8
were installed in April 2012 to monitor groundwater downgradient of the new Phase 3 waste unit (Cells 5A and 6A). Background sampling for these four wells began in May 2012 and was
completed in August 2012. Waste placement in Cell 5A began on July 17, 2012.

Depth-to-water measurements were recorded to the nearest 0.01 foot prior to initiating
groundwater purging and sampling activities. The monitoring point summary and respective water level elevations for this event are presented in Table 1. The historical water level data are
also shown on this table.

The water level data indicate that the hydraulic head in the uppermost aquifer beneath the facility
is fairly consistent, with temporal variation from the long-term average limited to less than five feet (plus or minus). As expected, the range in fluctuation generally appears to be greater in the
upgradient wells, as these wells are located in a groundwater recharge area.

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2.3 January 2016 Monitoring Event
Personnel from Joyce Engineering (JOYCE) visited the facility on January 26, 2016, to purge
and sample monitoring wells GW-1R, GW-2, GW-3, GW-4, GW-5, GW-6, GW-7, GW-8,
GW-9, and GW-10; sample surface water monitoring points SW-1 (upstream) and SW-2 (downstream); and collect a leachate sample. Depth-to-water measurements were obtained from the network monitoring wells to the nearest 0.01 foot using an electronic water level indicator
prior to purging the wells.

Monitoring wells were purged with dedicated bladder pumps using micropurge procedures pursuant to the facility’s approved monitoring plan. Measurements of pH, specific conductance, dissolved oxygen, oxidation-reduction potential, temperature, and turbidity were recorded after
each system volume collected during the purge with field-calibrated instruments to monitor for
stabilization of water quality.
During sampling, the laboratory-supplied sample containers were prepared. Each sample container was labeled with the sample identification number, sampling personnel, date and time
of sample collection, project name and number, and requested chemical analyses.

The groundwater samples were collected directly from the discharge hoses on the bladder pumps in the pre-preserved sample containers after purging was completed based on stabilization of water quality parameters. After collection, the samples were placed in a cooler on ice, under
chain-of-custody control.

Surface water sampling during the January 26, 2016 event was affected by seasonally dry conditions. No sample was recovered for SW-1 because the monitoring location was dry. SW-2 had very little flow, but samples were collected for NC Appendix I plus indicator parameters.
Surface water samples were collected directly from the stream, by lowering the sample
containers into the stream, taking care to prevent the over flow of the sample containers and to
minimize sample-induced turbidity. Measurements of pH, specific conductivity, dissolved oxygen, oxidation-reduction potential, temperature, and turbidity are normally recorded during
the collection of the surface water samples.

The leachate sample was collected directly from the leachate piping manifolds that serve the
leachate holding tanks. Measurements of pH, specific conductivity, and temperature were recorded during the collection of the leachate sample.

Copies of the sampling logs are presented in Appendix B. Included in each log is a description of
the sampling equipment, sampling location, sampling method, field observations, and water
quality measurements. The groundwater and leachate samples were shipped under chain-of-custody control to Analytical Services, Inc. (ASI) of Norcross, Georgia for analysis.

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2.4 Laboratory Analysis Program
The January 26, 2016, groundwater and leachate samples were submitted to ASI under chain-of-
custody control for analysis. The groundwater and surface water, including the Field Blank,
were analyzed for North Carolina Appendix I constituents plus iron and manganese. Indicator parameters iron and manganese were analyzed at NCDEQ’s request. The leachate sample was analyzed for NC Appendix I constituents, nitrate as N, nitrite as N, sulfate, biochemical oxygen
demand (BOD), chemical oxygen demand (COD), phosphorus, ammonia, nitrate/nitrite as N,
mercury, and cyanide. The Trip Blank was analyzed for North Carolina Appendix I organic
constituents only. Joyce Engineering requested a Level II data report for the final laboratory report. The groundwater and leachate samples were received by the laboratory on January 27, 2016, in good condition, properly preserved, and within analysis hold times.

2.5 January 2016 Sampling Results
Analytical detection and exceedance results for the January 26, 2016, groundwater and surface water samples are summarized in Tables 4 and 5. Historical analytical data for groundwater, surface water and leachate samples are summarized in Tables 6, 7, and 8 in Appendix A. A
summary of field parameter data from the January 2016 and September 2016 events are included
in Table 9 in Appendix A. The laboratory certificates-of-analysis and chains-of-custody for the
monitoring event are included in Appendix C. Four NC Appendix I inorganic constituents and two indicator parameters were detected in
samples from one or more downgradient compliance monitoring wells or surface water
monitoring points at concentrations above their respective Solid Waste Section Reporting Limits
(SWSLs). The complete list of quantified detections in groundwater and surface water by monitoring location, constituent and result in comparison to SWSLs is found in Table 4.
No NC Appendix I volatile organic constituents were detected in any groundwater wells or
surface water monitoring points during the January 2016 sampling event at concentrations above
their respective SWSL’s.
Constituent concentrations reported for the leachate samples collected during the January 26,
2016, sampling event are typical for leachate at this facility.

3.0 LABORATORY AND FIELD QA/QC
A Field Blank was collected by Joyce Engineering personnel as part of the January 26, 2016,
monitoring event. In addition to the Field Blank, a laboratory-prepared Trip Blank accompanied
the volatile sample containers for the sampling event to and from the laboratory. The Field Blank
was analyzed for NC Appendix I constituents and the Trip Blank for NC Appendix I Volatile
Organic Compounds (VOCs) only. In addition to the Field and Trip Blanks, at least one Method Blank was analyzed by the laboratory for each method used.

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Upon receipt of the laboratory data package, the data was reviewed by Joyce Engineering
personnel for the following:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate, and Laboratory Control Samples;
 Blank qualified data (B-flags);
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.
4.0 DATA EVALUTION
4.1 Comparisons to Groundwater and Surface Water Standards
The complete list of constituents in exceedance of applicable standards in groundwater and surface water samples by monitoring location is presented in Table 5.

4.1.1 Groundwater Standard Exceedances
Cobalt was detected above the Solid Waste Section Groundwater Protection Standards (GWPS)
in downgradient monitoring well GW-8. Cobalt is a common, naturally-occurring element in soils in this region, and these results are generally consistent with historical values. Based on
interwell statistical analysis, the background value for cobalt is 31.5 µg/L (see Section 4.2). In
accordance with 15A NCAC 13B.1634.(g).(5), we request that background concentrations be
considered the applicable groundwater protection standard (GPS) for cobalt for compliance
sampling events at this facility.
Two inorganic indicator parameters, iron and manganese, were analyzed per a NCDEQ request in a
letter dated September 28, 2007. The concentrations of iron detected in downgradient wells GW-4,
GW-5, GW-7, and GW-9 were above the NC 2L Standard during the January 2016 sampling event.
The concentrations of manganese detected in all downgradient wells were above the NC 2L Standard during the January 2016 sampling event. The January 2016 groundwater concentrations for iron and
manganese are generally consistent with historical data.

4.1.2 Surface Water Standard Exceedances
Two inorganic indicator parameters, iron and manganese, were analyzed per a NCDEQ request in a
letter dated September 28, 2007. Iron and manganese have been historically detected in the up-gradient and down-gradient surface water monitoring points at similar concentrations. During the January 2016 sampling event, iron was reported above the NC 2B standard for aquatic life in SW-2.
There is no NC 2B standard for either human health or aquatic life listed for manganese. The
January 2016 surface water concentrations for iron and manganese are generally consistent with historical data.

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4.2 Statistical Evaluations
Background data were evaluated using the Shapiro-Wilk Test, Parametric Prediction Limits,
Parametric Tolerance Intervals, Aitchison’s Adjustment, Non-parametric Prediction Limits, and
Poisson Prediction Limits, as appropriate. Background data, tests for normality, outliers, Aitchison’s adjustment, tolerance interval, or prediction limits are used, as appropriate based on the background data. The statistical test by which downgradient data are compared to facility
background data is based upon the nature of the data and the number of data values that are less
than the laboratory limit of detection. All statistical tests are evaluated at the 0.05 level of
significance, 95% confidence level, and are conducted as one-tailed tests. Cobalt was detected above the SWSL and its GWPS in GW-8 during the January 26, 2016,
sampling event. The cobalt detections were statistically evaluated in accordance with the
procedures outlined in 15A NCAC 13B.1632 (g) and (h) to determine if the reported
concentration exceeded the facility background concentration. Based on interwell non-parametric prediction interval analysis, the background for cobalt is 31.5 µg/L. Based on the statistical evaluation, the detection of cobalt in GW-8 was not identified as statistically significant and is
representative of historical background concentrations. In accordance with 15A NCAC
13B.1634.(g).(5), we request that background concentrations determined by statistical evaluation
be considered the applicable groundwater protection standard (GPS) for cobalt. The statistical analysis worksheets and summary table are included in Appendix D of this report.
5.0 CONCLUSIONS
Based on the results presented herein, Republic Services of NC, LLC, will continue monitoring
the uppermost aquifer beneath the Upper Piedmont Regional Landfill in accordance with the
requirements for Detection Monitoring Program as outlined in Title 15A NCAC 13B .1633. The next compliance monitoring event for this facility is tentatively scheduled for July 2016.
6.0 REFERENCES
BLE (Bunnell-Lammons Engineering, Inc.), December 2004. Report of Ground Water Quality
Results & Statistical Analysis, Second Semi-Annual Sampling Event of 2004 (N18)
Upper Piedmont Regional MSW Landfill, Person County, North Carolina. 3 pp
Golder Associates NC, Inc., February, 2011. First Semi-Annual 2011 Sampling Event. Prepared
for Republic Services of North Carolina, LLC.

HHNT (Hodges, Harbin, Newberry & Tribble), April 2003. Water Monitoring Procedures: Upper Piedmont Regional MSW Landfill, Phase 2 Construction Permit, Person County,
North Carolina. 28 pp.

North Carolina Geologic Survey, 1985, Geologic Map of North Carolina; North Carolina
Department of Natural Resources and Community Development, Geological Survey Section; scale 1:500,000.

Tables

TABLE 1: Historical Groundwater Elevations
Upper Piedmont Regional Landfill
Permit No. 73-04 Joyce Engineering
GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10
TOC Elevation 724.15 724.71 600.39 562.55 560.97 562.13 629.29 584.06 636.91 612.26 619.14
13-Aug-97 693.49 NI 574.91 556.06 554.73 556.61 NI NI NI NI NI
29-Apr-98 711.81 NI 576.70 559.22 557.35 558.63 NI NI NI NI NI
14-Sep-98 692.05 NI 573.88 556.74 554.55 557.69 NI NI NI NI NI08-Apr-99 707.45 NI 575.26 559.45 556.44 558.08 NI NI NI NI NI
08-Sep-99 DRY NI 573.66 557.25 555.10 557.84 NI NI NI NI NI
12-Apr-00 711.08 NI 576.25 557.76 556.28 557.82 NI NI NI NI NI17-Oct-00 692.83 NI 574.06 555.59 554.99 556.66 NI NI NI NI NI23-Apr-01 698.84 NI 575.10 557.24 556.37 557.91 NI NI NI NI NI
17-Oct-01 DRY NI 574.66 555.48 554.94 557.18 NI NI NI NI NI
29-Apr-02 DRY NI 573.70 556.81 556.17 557.83 NI NI NI NI NI23-Oct-02 DRY NI 575.24 557.16 556.64 558.64 NI NI NI NI NI
14-Apr-03 707.86 NI 578.27 559.32 557.93 559.41 NI NI NI NI NI
29-Oct-03 705.73 NI 579.25 558.10 557.69 559.38 NI NI NI NI NI28-Apr-04 708.26 NI 578.19 558.17 557.18 558.62 619.79 NI NI NI NI26-Oct-04 699.87 NI 577.62 558.00 557.37 559.07 617.89 NI NI NI NI
16-Mar-05 706.91 NI 578.35 558.85 558.01 559.79 621.67 NI NI NI NI
21-Jul-05 696.92 NI 576.43 555.64 555.20 556.36 617.62 NI NI NI NI26-Jan-06 <691.40 NI 576.63 558.15 557.44 559.04 611.26 NI NI NI NI
20-Jul-06 692.72 NI 576.49 557.27 556.94 558.32 617.97 NI NI NI NI
22-Jan-07 697.05 NI 575.78 559.05 558.38 559.83 621.78 NI NI NI NI23-Jul-07 692.71 NI 575.77 555.70 555.16 556.48 618.31 NI NI NI NI
10-Jan-08 <691.40 NI 574.04 556.85 556.33 558.03 616.04 NI NI NI NI
21-Jul-08 <691.40 NI 575.27 555.81 555.25 556.93 617.30 NI NI NI NI29-Jan-09 <691.40 NI 577.25 558.60 557.90 559.36 621.55 NI NI NI NI30-Jul-09 698.11 NI 576.48 556.65 555.93 557.48 620.08 NI NI NI NI
14-Jan-10 --689.83 578.32 558.56 557.55 559.28 621.13 NI NI 599.71 --
15-Jul-10 --690.40 577.66 556.21 555.44 556.77 619.97 NI NI 595.35 --20-Jan-11 --679.93 577.34 557.54 556.82 558.19 619.75 NI NI 594.79 601.86
14-Jul-11 --688.89 578.01 556.58 555.73 557.23 618.98 NI NI 595.61 601.56
30-Jan-12 --686.27 577.85 557.82 556.87 557.65 620.14 NI NI 596.84 602.2425-Jul-12 --684.65 576.94 558.41 554.47 556.23 616.79 572.05 593.72 594.96 601.4204-Feb-13 --683.04 578.20 558.68 557.04 558.17 620.53 576.17 597.06 595.64 602.85
08-Jul-13 --695.61 571.79 558.10 557.02 558.81 620.68 572.01 597.46 598.26 602.8221-Jan-14 --691.51 579.49 557.95 557.42 558.96 617.39 575.75 597.70 597.93 604.1621-Jul-14 --692.89 578.93 556.96 556.17 557.83 619.20 574.46 598.46 597.11 606.37
29-Jan-15 --697.36 578.63 558.72 557.93 559.50 619.84 577.31 599.16 598.83 604.04
27-Jul-15 --694.16 579.28 556.77 556.71 558.00 618.14 575.11 598.06 596.81 602.4926-Jan-16 --697.31 579.79 558.77 558.22 559.93 620.44 576.81 598.56 599.16 604.34
MEAN 700.81 690.14 576.62 557.53 556.52 558.15 618.97 574.96 597.52 597.00 603.10
MAXIMUM 711.81 697.36 579.79 559.45 558.38 559.93 621.78 577.31 599.16 599.71 606.37
MINIMUM <691.40 679.93 571.79 555.48 554.47 556.23 611.26 572.01 593.72 594.79 601.42
Notes:
All measurements are given in feet AMSL (above mean sea level).NI = Not installed.
-- = No data available.Dry = Monitoring well was dry and no depth to water value was obtained.
GW-1 was removed from the approved monitoring network prior to the January 2010 Sampling event.
All data prior to 2012 taken from previous report by Golder Associates NC, Inc.
Location Background Downgradient
TABLE 2:
Estimated Hydraulic Gradients and Linear Groundwater Velocities
Groundwater Elevations Measured:January 26, 2016
Flow Ground-Horizontal Hydraulic Effective Linear
Length water Gradient Conductivity Porosity Velocity
Line Elevation i K n e V gw
(feet)(feet)(ft/ft) (ft/day)(ft/year)
700
590
630
560
690
560
Notes:
Horizontal velocities based on the modified Darcy equation V gw = Ki/n e
Values for K and n e were taken from BLE's 2004 report reference in the text.
For flow segments see Drawing 1.
0.05 0.022 0.075 5.350
Gradient Calculation
Segment Flow Direction
i 1 2212 ENE
6.177
i 3 2300 E 0.06 0.022 0.075 6.080
i 2 1219 E 0.06 0.022 0.075
Upper Piedmont Regional Landfill
Permit No. 73-04 Joyce Engineering
TABLE 3:
Well Construction Information
Well
Identification
Ground Surface
Elevation TOC Elevation Well Depth Well
Diameter
Screened
Interval
Screened Geologic
Formation
(Ft-AMSL)(Ft-AMSL)(Feet)(Inches)(Ft-AMSL)
GW-1 721.4 724.15 32.5 2 706.4 - 691.4 Partially Weathered Rock
GW-1R 721.74 724.71 47.9 2 676.6 - 661.6 Bedrock
GW-2 598.0 600.39 45.9 2 569.5 - 554.5 Partially Weathered Rock
GW-3 560.1 562.55 41.6 2 536.7 - 521.7 Partially Weathered Rock
GW-4 558.1 560.97 46.6 2 531.1 - 516.1 Partially Weathered Rock
GW-5 559.4 562.13 22.2 2 554.9 - 539.9 Partially Weathered Rock
GW-6 626.7 629.29 28.1 2 616.2 - 601.2 Partially Weathered Rock
GW-9 609.33 612.26 11.3 2 594.2 - 579.2 Bedrock
GW-10 616.51 619.14 14.0 2 603.7 - 588.7 Bedrock
Notes:
Ft-AMSL = Feet above mean sea level.
TOC = Top of PVC Casing ( Measuring Point ).
Upper Piedmont Regional Landfill
Permit No. 73-04
Joyce Engineering
TABLE 4:
Quantified Detections in Groundwater and Surface Water
(January 2016)
Well or Point
ID Constituent Result Units SWSL Collection Date
GW-2 Total Copper 32.6 µg/L 10 1/26/2016
Total Manganese 572 µg/L 50 1/26/2016
Total Zinc 12.4 µg/L 10 1/26/2016
GW-3 Total Barium 492 µg/L 700 1/26/2016
Total Manganese 306 µg/L 50 1/26/2016
GW-4 Total Barium 452 µg/L 700 1/26/2016
Total Iron 1050 µg/L 300 1/26/2016
GW-5 Total Barium 268 µg/L 700 1/26/2016
Total Iron 3,430 µg/L 300 1/26/2016
Total Manganese 2,690 µg/L 50 1/26/2016
GW-6 Total Iron 408 µg/L 300 1/26/2016
GW-7 Total Barium 199 µg/L 700 1/26/2016
Total Iron 98,300 µg/L 300 1/26/2016
Total Manganese 12,300 µg/L 50 1/26/2016
GW-8 Total Barium 212 µg/L 100 1/26/2016
Total Cobalt 14.2 µg/L 10 1/26/2016
Total Manganese 514 µg/L 50 1/26/2016
Total Zinc 13.0 µg/L 10 1/26/2016
GW-9 Total Barium 164 µg/L 100 1/26/2016
Total Iron 9,020 µg/L 300 1/26/2016
Total Manganese 680 µg/L 50 1/26/2016
Total Manganese 142 µg/L 50 1/26/2016
SW-2 Total Iron 2,290 µg/L 300 1/26/2016
Total Manganese 235 µg/L 50 1/26/2016
Total Zinc 16.8 µg/L 10 1/26/2016
Notes:
Concentrations are in micrograms per liter (µg/L).SWSL = NC DENR Solid Waste Section Reporting Limits
MDL = Method Detection LimitJ = Estimated concentration below the SWSL.
Bold Values= Detections exceeding the NC2L, GWPS, or NC2B stardards. (see Table 5)
Upper Piedmont Regional Landfill
Permot No. 73-04 Joyce Engineering
TA
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Joyce Engineering

Drawing

Appendix A

Historical Tables

TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 1 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Inorganic Compounds
Antimony 05/23/97 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
GWPS = 1 µg/L 06/16/97 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---30.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---30.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---30.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---30.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---30.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---30.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---30.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---30.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---30.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---30.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---30.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---30.0 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---30.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---6.00 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---6.00 ND NI ND ND ND ND 1.02 J NI NI NI NI ND
01/10/08 ---6.00 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---6.00 Dry NI ND ND ND ND 0.79 J NI NI NI NI ND
01/29/09 ---6.00 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---6.00 ND NI ND ND ND ND ND NI NI NI NI ND
01/14/10 ---6.00 ---ND ND ND ND ND 0.233 J NI NI NI NI ND
07/15/10 ---6.00 ---ND ND ND ND ND 0.470 J NI NI NI NI ND
01/20/11 ---6.00 ---ND ND ND ND ND 0.364 J NI NI NI NI ND
07/14/11 ---6.00 ---ND ND ND ND ND 0.339 J NI NI NI NI ND
01/30/12 ---6.00 ---0.37 B 0.18 B 0.17 B 0.15 B ND 0.370 B NI NI NI NI 0.33 J
05/24/12 ---6.00 ---NS NS NS NS NS NS 0.89 J 0.50 J 0.24 J ND ND
06/28/12 ---6.00 ---NS NS NS NS NS NS 1.2 J 0.57 J 0.19 J ND ND
07/25/12 ---6.00 ---1.52 J 0.50 J 0.30 J 0.22 J 0.22 J 0.54 J ND ND ND ND ND
08/24/12 ---6.00 ---NS NS NS NS NS NS 1.38 J 0.63 J 0.25 J ND ND
02/04/13 ---6.00 ---1.24 J 0.39 J 0.34 J 0.24 J ND 0.28 J ND ND ND ND ND
07/08/13 ---6.00 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 0.22 6.00 ---ND ND ND ND ND ND ND ND ND ND ND
07/21/14 1.05 6.00 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 1.05 6.00 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.25 6.00 ---ND 0.49 J ND ND ND 0.28 J ND ND ND ND ND
01/26/16 0.25 6.00 ---ND ND ND ND ND 0.30 J ND ND ND ND ND
Arsenic 05/23/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 10 µg/L 06/16/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---10.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 ND NI ND 2.20 J ND 3.50 J 2.60 J NI NI NI NI ND
07/23/07 ---10.0 ND NI ND ND 2.7 J ND ND NI NI NI NI ND
01/10/08 ---10.0 Dry NI ND 4.10 J ND 4.10 J ND NI NI NI NI ND
07/21/08 ---10.0 Dry NI ND 4.90 J 3.4 J 8.40 J 3.00 J NI NI NI NI ND
01/29/09 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI 4.20 J
07/30/09 ---10.0 ND NI ND 3.85 J 3.49 J 14.00 ND NI NI NI NI ND
01/14/10 ---10.0 ---ND 4.24 J ND ND ND 4.02 J NI NI NI NI ND
07/15/10 ---10.0 ---ND ND ND ND ND 5.15 J NI NI NI NI ND
01/20/11 ---10.0 ---ND 3.48 J 4.37 J 6.27 J ND 8.83 J NI NI NI NI ND
07/14/11 ---10.0 ---4.13 J 5.58 J 4.47 J 5.52 J 6.94 J 4.07 J NI NI NI NI ND
01/30/12 ---10.0 ---ND ND ND ND ND 1.83 J NI NI NI NI ND
05/24/12 ---10.0 ---NS NS NS NS NS NS 3.44 J ND ND ND ND
06/28/12 ---10.0 ---NS NS NS NS NS NS 3.5 J ND ND ND ND
07/25/12 ---10.0 ---ND ND 1.33 B 6.02 B 12.40 B 1.67 B 8 B ND 3.00 B 1.70 B 1.72 J
08/24/12 ---10.0 ---NS NS NS NS NS NS 8.6 J ND ND ND ND J
02/04/13 ---10.0 ---ND ND ND 6.02 J ND ND 5.79 J ND ND ND ND
07/08/13 ---10.0 ---2.02 J ND ND 2.49 J 1.17 J ND 4.23 J ND 3.53 J ND ND
01/21/14 0.78 10.0 ---ND ND 0.85 J 1.42 J ND 1.32 J 5.90 J ND ND ND ND
07/21/14 1.13 10.0 ---ND ND ND 1.58 J 1.80 J 1.29 J 7.03 J ND ND ND ND
01/29/15 1.13 10.0 ---ND 2.47 J 1.91 J ND ND ND 6.49 J ND 2.55 J ND ND
07/27/15 0.75 10.0 ---ND 1.23 J 2.47 J 2.14 J 1.31 J 2.00 J 4.41 J ND 0.84 J ND ND
01/26/16 0.75 10.0 ---ND 1.16 J 2.85 J 3.28 J 4.38 J 1.36 J 4.60 J ND 1.87 J ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 2 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Barium 05/23/97 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 700 µg/L 06/16/97 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---20 Dry NI 40.0 280 380 130 ---NI NI NI NI ND
04/30/98 ---20 40.0 NI 40.0 280 370 170 ---NI NI NI NI ND
09/15/98 ---20 40.0 NI 40.0 270 400 140 ---NI NI NI NI ND
04/08/99 ---20 50.0 NI 30.0 270 250 220 ---NI NI NI NI ND
09/09/99 ---500 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---500 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---500 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---500 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---500 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---500 ---NI ------------ND NI NI NI NI ND
04/28/04 ---500 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---500 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---500 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---500 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---500 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---500 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---100 41.80 J NI 77.90 J 443 322 342 31.6 J NI NI NI NI 0.50 J
07/23/07 ---100 42.10 J NI 44.30 J 455 332 360 40.0 J NI NI NI NI 0.50 J
01/10/08 ---100 Dry NI 49.00 J 469 364 271 57.5 J NI NI NI NI ND
07/21/08 ---100 Dry NI 44.60 J 466 382 415 49.2 J NI NI NI NI ND
01/29/09 ---100 Dry NI 50.20 J 465 361 295 29.9 J NI NI NI NI 0.50 J
07/30/09 ---100 49.50 J NI 39.20 J 466 383 372 42.8 J NI NI NI NI ND
01/14/10 ---100 ---25.30 J 34.80 J 410 320 332 27.0 J NI NI NI NI ND
07/15/10 ---100 ---12.30 J 27.50 J 392 380 282 54.8 J NI NI NI NI ND
01/20/11 ---100 ---15.20 J 41.50 J 454 409 245 21.5 J NI NI NI NI ND
07/14/11 ---100 ---15.70 J 41.10 J 483 447 316 33.2 J NI NI NI NI ND
01/30/12 ---100 ---13.80 J 42.80 J 468 459 238 21.2 J NI NI NI NI 0.14 J
05/24/12 ---100 ---NS NS NS NS NS NS 287 185 107 76.9 J ND
06/28/12 ---100 ---NS NS NS NS NS NS 200 161 39.0 J 70.4 J 0.74 J
07/25/12 ---100 ---14.90 J 39.60 J 441 620 370 19.9 J 267 186 73.5 J 68.4 J 0.79 J
08/24/12 ---100 ---NS NS NS NS NS NS 412 175 62.2 J 82.2 J 0.75 J
02/04/13 ---100 ---12.90 J 43.4 J 418 811 211 23.8 J 254 143 57.7 J 78.0 J ND
07/08/13 ---100 ---51.80 J 48.40 J 474 508 360 49.4 J 227 162 352 92.0 J 0.57 J
01/21/14 0.25 100 ---17.8 J 47.7 J 449 418 194 82.6 J 245 200 110 87.8 J ND
07/21/14 0.1 100 ---9.06 J 58.2 J 444 599 284 17.8 J 242 254 124 88.0 J 0.34 J
01/29/15 0.10 100 ---9.69 J 83.2 J 475 423 187 25.9 J 180 241 234 92.3 J 1.33 J
07/27/15 0.30 100 ---8.09 J 36.4 J 368 350 157 15.8 J 168 171 67.1 J 78.4 J 0.41 J
01/26/16 0.30 100 ---11.50 J 50.6 J 492 452 268 25.8 J 199 212 164.0 88.8 J 0.55 J
Beryllium 07/21/05 ---2.00 ND NI ND ND ND ND ND NI NI NI NI ND
GWPS = 4 µg/L 01/26/06 ---2.00 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---2.00 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---1.00 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---1.00 ---NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---1.00 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---1.00 0.28 J NI ND ND ND ND 0.19 J NI NI NI NI ND
01/14/10 ---1.00 ---0.11 J ND ND ND ND 0.12 J NI NI NI NI ND
07/15/10 ---1.00 ---ND ND ND ND ND ND NI NI NI NI ND
01/20/11 ---1.00 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---1.00 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---1.00 ---ND ND ND ND ND 0.10 J NI NI NI NI ND
05/24/12 ---1.00 ---NS NS NS NS NS NS ND ND 0.47 J ND ND
06/28/12 ---1.00 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---1.00 ---ND ND ND ND ND ND ND ND 0.17 J ND ND
08/24/12 ---1.00 ---NS NS NS NS NS NS ND ND 0.15 J ND ND
02/04/13 ---1.00 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---1.00 ---0.40 J ND ND ND ND ND ND ND 1.20 ND ND
01/21/14 0.11 1.00 ---ND ND ND ND ND 0.16 J ND ND 0.27 J ND ND
07/21/14 0.05 1.00 ---ND ND ND ND ND 0.07 J ND 0.08 J 0.29 J ND ND
01/29/15 0.05 1.00 ---ND ND ND ND ND 0.10 J ND 0.13 J 0.54 J 0.18 J ND
07/27/15 0.09 1.00 ---ND ND ND ND ND ND ND 0.11 J 0.15 J 0.16 J ND
01/26/16 0.09 1.00 ---ND ND ND 0.20 J ND ND ND 0.15 J 0.26 J 0.20 J ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 3 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Cadmium 05/23/97 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 2 µg/L 06/16/97 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---1.00 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---1.00 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---1.00 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---1.00 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---1.00 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---1.00 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---1.00 ---NI ------------ND NI NI NI NI ND
04/28/04 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---1.00 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---1.00 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---1.00 1.0 NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---1.00 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---1.00 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---1.00 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---1.00 1.4 NI 0.2 J 0.24 J 0.197 J 0.3 J 0.13 J NI NI NI NI ND
01/14/10 ---1.00 ---0.46 J 0.2 J 0.39 J ND ND 0.21 J NI NI NI NI ND
07/15/10 ---1.00 ---ND ND 0.53 J ND ND ND NI NI NI NI ND
01/20/11 ---1.00 ---0.55 J ND ND ND ND ND NI NI NI NI ND
07/14/11 ---1.00 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---1.00 ---0.26 J ND 0.22 J 0.18 J ND ND NI NI NI NI ND
05/24/12 ---1.00 ---NS NS NS NS NS NS 0.07 J 0.3 J ND ND ND
06/28/12 ---1.00 ---NS NS NS NS NS NS ND 0.2 J ND 0.07 J ND
07/25/12 ---1.00 ---0.16 J 0.1 J 0.09 J 0.09 J 0.1 J ND ND 0.1 J ND 0.11 J ND
08/24/12 ---1.00 ---NS NS NS NS NS NS ND 0.2 J ND 0.08 J ND
02/04/13 ---1.00 ---0.17 J 0.1 J 0.22 J ND ND ND ND 0.1 J ND 0.06 J ND
07/08/13 ---1.00 ---0.07 J ND 0.63 J 3.46 ND ND 0.36 J 0.1 J 0.06 J ND ND
Resample >07/26/13 ---1.00 ---NS NS NS 0.09 J NS NS NS NS NS NS ND
01/21/14 0.06 1.00 ---0.07 J ND 0.23 J ND ND ND ND 0.09 J 0.11 J 0.06 J ND
07/21/14 0.05 1.00 ---ND ND 0.15 J 0.92 J ND ND ND 0.09 J ND 0.06 J ND
01/29/15 0.05 1.00 ---ND 0.09 B 0.11 B 0.05 B 0.06 B 0.09 B ND 0.13 B ND 0.18 B 0.06 J
07/27/15 0.1 1.00 ---ND ND 0.17 J 0.14 J ND ND ND 0.10 J 0.13 J ND ND
01/26/16 0.1 1.00 ---ND ND 0.12 J ND ND ND ND 0.20 J ND ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 4 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Chromium 05/23/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 10 µg/L 06/16/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---10.0 20 NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---10.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 3.80 J NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---10.0 Dry NI 0.76 J ND 0.563 J ND 0.68 J NI NI NI NI ND
07/30/09 ---10.0 6.02 J NI 0.77 J ND 1.1 J 2.62 J 1.41 J NI NI NI NI ND
01/14/10 ---10.0 ---3.64 J ND ND ND 2.10 J ND NI NI NI NI ND
07/15/10 ---10.0 ---2.42 J ND ND ND ND 1.59 J NI NI NI NI ND
01/20/11 ---10.0 ---2.43 J ND ND ND ND ND NI NI NI NI ND
07/14/11 ---10.0 ---3.35 J ND ND ND 1.4 J 1.49 J NI NI NI NI ND
01/30/12 ---10.0 ---2.11 B ND 1.64 B 0.6 B 1.04 B 1.64 B NI NI NI NI 1.16 J
05/24/12 ---10.0 ---NS NS NS NS NS NS 3.23 B 1.7 B 6.06 B 1.97 B 1.26 J
06/28/12 ---10.0 ---NS NS NS NS NS NS 6.91 B 2.9 B 4.20 B 1.88 B 1.24 J
07/25/12 ---10.0 ---2.85 J 0.81 J ND 2.56 J ND 0.84 J 1.76 J ND 1.78 J ND ND
08/24/12 ---10.0 ---NS NS NS NS NS NS 5.37 J 3.9 J 5.45 J 1.11 J ND
02/04/13 ---10.0 ---3.86 B 2.74 B 3.32 B ND ND 1.98 B 2.93 B ND ND ND 2.66 J
07/08/13 ---10.0 ---11.20 B 2.64 B 1.19 B ND ND 2.61 B 2.08 B ND 13.40 B 3.97 B 1.50 J
01/21/14 0.58 10.0 ---6.54 B 2.10 B 0.72 B ND ND 4.51 B ND ND 7.59 B 1.39 B 1.52 J
07/21/14 0.73 10.0 ---1.45 B ND ND ND ND ND ND ND 1.12 B ND 1.40 J
01/29/15 0.73 10.0 ---0.85 J 1.62 J ND ND 6.53 J 1.65 J ND ND 6.78 J ND ND
07/27/15 0.43 10.0 ---2.31 J ND ND ND ND 1.03 J 1.33 J ND 1.05 J ND ND
01/26/16 0.43 10.0 ---2.96 J 0.58 J ND 0.45 J 0.80 J 2.52 J 1.44 J 1.63 J 3.82 J 0.44 J ND
Cobalt 05/23/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
GWPS = 1 µg/L 06/16/97 ---10.0 ND NI 10.0 ND ND ND ---NI NI NI NI ND
08/14/97 ---10.0 10.0 NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---40.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---40.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---40.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---40.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---10.0 Dry NI ND 20.0 20.0 20.0 ---NI NI NI NI ND
10/23/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---10.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---10.0 ND NI 15.0 ND ND ND ND NI NI NI NI ND
07/21/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 ND NI 16.4 ND ND 2.70 J ND NI NI NI NI ND
04/10/07 ---10.0 ---NI 8.10 J ------------NI NI NI NI ND
07/23/07 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---10.0 Dry NI ND 3.20 J ND 3.10 J ND NI NI NI NI ND
01/29/09 ---10.0 Dry NI 4.63 J 1.53 J ND 1.87 J ND NI NI NI NI ND
07/30/09 ---10.0 2.55 J NI 1.85 J 2.37 J ND 2.91 J ND NI NI NI NI ND
01/14/10 ---10.0 ---0.76 J 3.00 J 2.45 J ND 1.82 J ND NI NI NI NI ND
07/15/10 ---10.0 ---ND 2.25 J 1.84 J ND 2.21 J ND NI NI NI NI ND
01/20/11 ---10.0 ---ND 2.46 J 2.43 J ND ND ND NI NI NI NI ND
07/14/11 ---10.0 ---ND 2.33 J 1.31 J ND 1.61 J ND NI NI NI NI ND
01/30/12 ---10.0 ---0.18 J 4.0 J 3.66 J 0.3 J 0.5 J 0.24 J NI NI NI NI ND
05/24/12 ---10.0 ---NS NS NS NS NS NS 26.2 19.0 0.93 J 2.94 J ND
06/28/12 ---10.0 ---NS NS NS NS NS NS 25.1 14.5 0.17 J 2.27 J ND
07/25/12 ---10.0 ---0.44 J 1.6 J 3.54 J 1.14 J 1.8 J 0.22 J 31.5 19.4 1.12 J 2.13 J ND
08/24/12 ---10.0 ---NS NS NS NS NS NS 29.6 16.9 1.12 J 3.85 J ND
02/04/13 ---10.0 ---0.24 J 4.1 J 2.18 J 1.02 J 0.6 J 0.29 J 19.7 11.2 0.61 J 3.00 J ND
07/08/13 ---10.0 ---2.73 J 3.62 J 1.88 J 0.57 J 1.23 J 0.39 J 12.5 10.7 10.6 8.14 J ND
01/21/14 0.12 10.0 ---0.53 J 6.24 J 4.29 J 0.32 J 0.68 J 0.65 J 13.7 11.2 3.11 J 3.49 J ND
07/21/14 0.26 10.0 ---ND 2.21 J 1.87 J 0.36 J 0.86 J ND 16.8 20.7 4.51 J 11.5 ND
01/29/15 0.26 10.0 ---ND 25.8 3.72 J 0.27 J 0.63 J 0.28 J 8.34 J 16.5 20.3 4.50 J ND
07/27/15 0.29 10.0 ---ND 0.93 J 0.80 J ND ND ND 7.55 J 16.1 5.50 J 3.37 J ND
01/26/16 0.29 10.0 ---ND 5.06 J 5.58 J ND 1.03 J ND 6.89 J 14.2 8.81 J 4.76 J ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 5 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Copper 05/23/97 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 1000 µg/L 06/16/97 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---20 Dry NI ND ND ND ND ---NI NI NI NI 30
04/30/98 ---20 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---20 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---20 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---200 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---200 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---200 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---200 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---200 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---200 ---NI ------------ND NI NI NI NI ND
04/28/04 ---200 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---200 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---200 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---200 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---200 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---200 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 3.30 B NI 10.5 8.20 J 0.8 B ND 3.60 B NI NI NI NI 0.90 J
07/23/07 ---10.0 2.70 B NI 111 ND ND ND 3.20 B NI NI NI NI 1.20 J
01/10/08 ---10.0 Dry NI 35.0 ND ND ND 3.20 J NI NI NI NI ND
07/21/08 ---10.0 Dry NI 122 ND ND ND 3.10 J NI NI NI NI ND
01/29/09 ---10.0 Dry NI 8.77 J ND ND ND 2.61 J NI NI NI NI ND
07/30/09 ---10.0 11.30 NI 79.6 ND ND ND 4.42 B NI NI NI NI 1.48 J
01/14/10 ---10.0 ---ND 27.2 ND ND ND ND NI NI NI NI ND
07/15/10 ---10.0 ---ND 168 ND ND ND 5.08 J NI NI NI NI ND
01/20/11 ---10.0 ---2.09 B 53 2.82 B ND ND 4.48 B NI NI NI NI 2.16 J
07/14/11 ---10.0 ---2.19 B 151 ND ND ND 4.83 B NI NI NI NI 1.85 J
01/30/12 ---10.0 ---1.77 J 127 4.79 J 1.45 J 1.44 J 2.55 J NI NI NI NI ND
05/24/12 ---10.0 ---NS NS NS NS NS NS 3.09 J 4.24 J 2.66 J 2.51 J ND
06/28/12 ---10.0 ---NS NS NS NS NS NS 2.37 J 5.52 J 1.52 J 2.62 J ND
07/25/12 ---10.0 ---1.55 B 142 2.82 B 2.03 B 1.52 B 3.21 B 1.6 J 4.09 J 2.24 J 2.79 J 0.36 J
08/24/12 ---10.0 ---NS NS NS NS NS NS 2.02 J 7.03 J 4.58 J 4.02 J 0.44 J
02/04/13 ---10.0 ---1.29 B 126 19.80 2.71 J 0.94 B 2.89 J 1.55 B 4.06 J 1.63 B 3.10 J 0.19 J
07/08/13 ---10.0 ---8.05 J 545 7.29 J 6.67 J 1.04 J 3.58 J 2.33 J 2.36 J 7.58 J 5.11 J ND
01/21/14 0.38 10.0 ---2.03 J 66.6 6.00 J 2.10 J 0.74 J 6.88 J 1.14 J 2.28 J 3.19 J 2.66 J ND
07/21/14 0.22 10.0 ---1.28 B 1550 4.61 J 3.14 J 0.67 B 2.98 J 1.12 B 2.23 J 3.33 J 2.51 J 0.44 J
Resample >08/20/14 0.22 10.0 ------654 B ------------------------778
01/29/15 0.22 10.0 ---0.77 B 87.3 1.00 B 0.89 B 0.68 B 3.19 B 0.81 B 1.90 B 3.56 B 3.38 B 4.34 J
07/27/15 0.41 10.0 ---1.07 B 31.8 2.38 B 0.63 B ND 2.75 B ND 1.57 B 0.72 B 4.30 B 1.24 J
01/26/16 0.41 10.0 ---0.73 B 32.6 0.44 B 2.24 B 0.44 B 5.56 B ND 2.11 B 1.25 B 2.73 B 3.93 J
Lead 05/23/97 ---10.0 10.0 NI 10.0 ND ND ND ---NI NI NI NI ND
NC 2L = 15 µg/L 06/16/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---15.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---15.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---15.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---15.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---10.0 10.0 NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---10.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 ND NI ND ND ND 3.80 J ND NI NI NI NI ND
07/23/07 ---10.0 4.10 J NI ND ND ND 2.10 J 3.20 J NI NI NI NI ND
01/10/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---10.0 Dry NI 3.90 J ND ND ND 2.50 J NI NI NI NI ND
01/29/09 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---10.0 1.98 J NI 12.70 ND 2.57 J 4.39 J 3.75 J NI NI NI NI ND
01/14/10 ---10.0 ---1.23 J 8.25 J 1.34 J 1.34 J 1.96 J ND NI NI NI NI ND
07/15/10 ---10.0 ---ND 10.90 ND ND ND 3.05 J NI NI NI NI ND
01/20/11 ---10.0 ---ND 23.50 ND ND ND ND NI NI NI NI ND
02/18/11 ---10.0 ------10.20 ------------NI NI NI NI ND
07/14/11 ---10.0 ---ND 12.50 ND ND 2.24 J ND NI NI NI NI ND
01/30/12 ---10.0 ---ND 4.4 J 0.32 J 0.25 J ND 0.65 J NI NI NI NI ND
05/24/12 ---10.0 ---NS NS NS NS NS NS 0.53 J 0.24 J 5.10 J 0.24 J ND
06/28/12 ---10.0 ---NS NS NS NS NS NS 0.4 J 0.30 J 0.59 J 0.23 J ND
07/25/12 ---10.0 ---0.25 B 4.4 J 0.17 B 0.61 B 0.3 B 0.66 B 0.12 J 0.10 J 1.21 J 0.25 J 0.29 J
08/24/12 ---10.0 ---NS NS NS NS NS NS 0.28 J 0.10 J 1.03 J 0.24 J ND
02/04/13 ---10.0 ---0.18 J 11.5 1.73 J 0.95 J 0.2 J 0.79 J 0.16 J ND 0.18 J 0.10 J ND
07/08/13 ---10.0 ---4.97 J 4.7 J 0.85 J 4.86 J 0.1 B 1.73 J 4.92 J 1.6 J 9.46 J 0.89 J 0.09 J
01/21/14 0.05 10.0 ---0.46 J 3.34 J 0.34 J 0.35 J 0.08 J 3.87 J ND 0.22 J 1.73 J 0.16 J ND
07/21/14 0.05 10.0 ---0.07 J 2.45 J 0.42 J 0.21 J 0.05 J 0.57 J 0.07 J 0.19 J 1.03 J 0.19 J ND
01/29/15 0.05 10.0 ---ND 3.44 J ND 0.08 J ND 2.05 J ND ND 3.81 J 0.10 J ND
07/27/15 0.08 10.0 ---0.10 J 0.79 J ND ND ND 0.39 J ND 0.12 J 0.59 J 0.13 J ND
01/26/16 0.08 10.0 ---0.24 J 0.61 J ND 3.97 J 0.09 J 1.14 J ND 0.34 J 1.71 J ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 6 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Nickel 05/23/97 ---50.0 10.0 NI 10.0 ND ND ND ---NI NI NI NI ND
NC 2L = 100 µg/L 06/16/97 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---50.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---50.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---50.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---50.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---50.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---50.0 10.0 NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---50.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---50.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---50.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---50.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---50.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---50.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---50.0 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---50.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---50.0 2.80 J NI 6.30 J ND ND 2.70 J 5.90 J NI NI NI NI ND
07/23/07 ---50.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---50.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---50.0 Dry NI 3.90 J ND ND ND 4.10 J NI NI NI NI ND
01/29/09 ---50.0 Dry NI 2.89 J ND ND 2.39 J 1.88 J NI NI NI NI ND
07/30/09 ---50.0 6.29 J NI 3.71 J 0.90 J 0.724 J 7.34 J 4.29 J NI NI NI NI ND
01/14/10 ---50.0 ---3.95 J ND 1.60 J ND 4.57 J ND NI NI NI NI ND
07/15/10 ---50.0 ---3.23 J 2.97 J ND ND ND ND NI NI NI NI ND
01/20/11 ---50.0 ---4.61 J 2.10 J ND ND 2.22 J ND NI NI NI NI ND
07/14/11 ---50.0 ---5.41 J 3.31 J ND ND ND ND NI NI NI NI ND
01/30/12 ---50.0 ---6.99 J 2.11 J 5.12 J 3.42 J 3.43 J 1.54 J NI NI NI NI ND
05/24/12 ---50.0 ---NS NS NS NS NS NS 18.5 J 9.27 J 4.00 J 6.40 J ND
06/28/12 ---50.0 ---NS NS NS NS NS NS 31.4 J 13.30 J 3.36 J 5.72 J ND
07/25/12 ---50.0 ---6.55 J 2.65 J 3.47 J 4.21 J 3.62 J 1.36 J 15.6 J 6.76 J 3.14 J 5.59 J ND
08/24/12 ---50.0 ---NS NS NS NS NS NS 18.1 J 22.10 J 16.10 J 10.80 J ND
02/04/13 ---50.0 ---6.92 J 1.89 J 4.77 J 5.35 J 3.09 J 1.80 J 7.59 J 11.30 J 3.40 J 4.45 J ND
07/08/13 ---50.0 ---9.66 B 2.58 B 5.66 B 6.03 B 3.29 B 2.26 B 1.56 B 4.62 B 11.10 J 5.62 B 1.99 J
01/21/14 0.41 50.0 ---5.93 J 2.08 J 5.35 J 3.28 J 2.72 J 7.75 J 1.78 J 8.46 J 8.53 J 5.99 J ND
07/21/14 0.22 50.0 ---3.74 J 3.85 J 3.55 J 5.52 J 2.87 J 1.70 J 1.66 J 6.42 J 3.93 J 6.21 J ND
01/29/15 0.22 50.0 ---3.78 J 5.34 J 2.05 J 2.33 J 3.62 J 2.19 J 1.51 J 5.44 J 6.22 J 5.45 J ND
07/27/15 0.48 50.0 ---3.21 J 1.14 J 0.56 J ND ND 1.07 J 0.84 J 4.62 J 2.54 J 4.13 J ND
01/26/16 0.48 50.0 ---5.08 J 2.12 J ND 0.56 J 1.17 J 3.55 J 1.39 J 4.89 J 5.35 J 4.55 J ND
Selenium 05/23/97 ---20.0 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 20 µg/L 06/16/97 ---20.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---20.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---20.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---20.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---20.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---20.0 ND NI ND ND ND 40.0 ---NI NI NI NI ND
10/18/01 ---20.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---20.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---20.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---20.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---20.0 ND NI ND 20.0 ND ND ---NI NI NI NI ND
03/19/04 ---20.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---20.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---20.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---20.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---20.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---20.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---20.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---10.0 Dry NI ND 5.23 J 6.79 J ND ND NI NI NI NI ND
07/30/09 ---10.0 ND NI ND 3.60 J 4.89 J ND ND NI NI NI NI ND
01/14/10 ---10.0 ---ND ND 1.37 J 1.45 J ND ND NI NI NI NI ND
07/15/10 ---10.0 ---ND ND ND ND ND 3.45 B NI NI NI NI 4.36 J
01/20/11 ---10.0 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---10.0 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---10.0 ---ND ND ND ND ND ND NI NI NI NI ND
05/24/12 ---10.0 ---NS NS NS NS NS NS 1.26 J ND ND ND ND
06/28/12 ---10.0 ---NS NS NS NS NS NS 0.79 J 0.56 J ND ND ND
07/25/12 ---10.0 ---ND ND ND 0.65 J ND ND 2.93 J 1.19 J ND ND ND
08/24/12 ---10.0 ---NS NS NS NS NS NS 3.68 J 0.78 J ND ND ND
02/04/13 ---10.0 ---ND ND 1.08 J 0.9 J ND ND 3.6 J 0.84 J ND ND ND
07/08/13 ---10.0 ---ND ND ND ND ND ND 3.25 J ND ND ND ND
01/21/14 0.77 10.0 ---ND ND ND ND ND ND 3.60 B ND ND ND 2.20 J
07/21/14 1.01 10.0 ---ND 1.09 B 1.74 B 1.74 B ND ND 8.69 B 2.10 B 1.81 B 1.27 B 2.88 J
01/29/15 1.01 10.0 ---ND 2.44 J ND ND ND ND 2.44 J ND ND ND ND
07/27/15 0.85 10.0 ---ND ND ND ND ND ND 1.74 J ND ND ND ND
01/26/16 0.85 10.0 ---ND ND ND 0.87 J ND ND 0.88 J ND 1.23 J ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 7 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Silver 07/21/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
NC 2L = 20 µg/L 01/26/06 ---10.0 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---10.0 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---10.0 Dry NI 1.47 J ND ND ND ND NI NI NI NI ND
07/30/09 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/14/10 ---10.0 ---ND 0.79 J 2.29 J ND ND ND NI NI NI NI ND
07/15/10 ---10.0 ---ND ND ND ND ND ND NI NI NI NI ND
01/20/11 ---10.0 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---10.0 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---10.0 ---0.23 J 0.50 J 3.63 J ND 0.14 J ND NI NI NI NI ND
05/24/12 ---10.0 ---NS NS NS NS NS NS ND ND ND ND ND
06/28/12 ---10.0 ---NS NS NS NS NS NS ND 0.54 J 0.16 J ND ND
07/25/12 ---10.0 ---0.43 J 1.99 J 4.03 J 0.7 J 0.35 J ND 0.54 J ND ND ND ND
08/24/12 ---10.0 ---NS NS NS NS NS NS 0.12 J ND 0.12 J 0.11 J ND
02/04/13 ---10.0 ---0.69 J 0.62 J 6.42 J 0.24 J ND ND 0.14 J ND 0.49 J 0.10 J ND
07/08/13 ---10.0 ---0.35 J 0.59 J 1.09 J 4.3 J ND ND ND ND ND ND ND
01/21/14 0.24 10.0 ---2.30 J 0.84 J 0.57 J 0.38 J ND ND ND ND ND ND ND
07/21/14 0.17 10.0 ---0.55 J 0.56 J 0.56 J ND ND ND ND 0.35 J ND ND ND
01/29/15 0.17 10.0 ---0.24 J 3.13 J ND ND 0.35 J ND 0.33 J 0.17 J 0.41 J 1.54 J ND
07/27/15 0.22 10.0 ---0.32 J ND 0.40 J ND ND ND ND ND 0.36 J ND ND
01/26/16 0.22 10.0 ---0.77 J ND ND 0.49 J 0.36 J ND ND ND ND ND ND
Thallium 05/23/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
GWPS = 0.2 µg/L 06/16/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---10.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---10.0 Dry NI ND ND ND 10.00 ND NI NI NI NI ND
07/21/06 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---5.50 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---5.50 ND NI ND ND ND ND ND NI NI NI NI 0.05 J
01/10/08 ---5.50 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---5.50 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---5.50 Dry NI ND ND 0.053 J ND ND NI NI NI NI ND
07/30/09 ---5.50 ND NI ND ND ND ND ND NI NI NI NI ND
01/14/10 ---5.50 ---ND ND ND ND ND ND NI NI NI NI ND
07/15/10 ---5.50 ---ND ND ND ND ND ND NI NI NI NI ND
01/20/11 ---5.50 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---5.50 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---5.50 ---ND ND ND ND ND ND NI NI NI NI ND
05/24/12 ---5.50 ---NS NS NS NS NS NS ND ND ND ND ND
06/28/12 ---5.50 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---5.50 ---ND ND ND ND ND ND ND ND ND ND ND
08/24/12 ---5.50 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---5.50 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---5.50 ---ND ND ND ND ND ND ND ND 0.08 J ND ND
01/21/14 0.06 5.50 ---0.20 J ND ND ND ND ND ND ND ND ND ND
07/21/14 0.09 5.50 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 0.09 5.50 ---ND ND ND ND ND ND ND ND 0.11 J ND ND
07/27/15 0.06 5.50 ---ND 0.38 J 0.09 J ND ND ND 0.15 J ND ND ND 5.50
01/26/16 0.06 5.50 ---0.08 J ND ND ND ND ND ND ND 0.07 J ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 8 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Vanadium 05/23/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
GWPS = 0.3 µg/L 06/16/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/08/99 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---10.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---10.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---10.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---10.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---40.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---40.0 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---40.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---25.0 2.80 J NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---25.0 2.30 J NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---25.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---25.0 Dry NI ND ND ND ND 1.60 J NI NI NI NI ND
01/29/09 ---25.0 Dry NI 1.45 J 1.44 J ND ND 1.32 J NI NI NI NI ND
07/30/09 ---25.0 4.29 J NI ND ND ND ND 1.92 J NI NI NI NI ND
01/14/10 ---25.0 ---4.35 J ND ND ND ND 1.22 J NI NI NI NI ND
07/15/10 ---25.0 ---2.28 J ND ND ND ND 2.16 J NI NI NI NI ND
01/20/11 ---25.0 ---2.13 J ND ND ND ND ND NI NI NI NI ND
07/14/11 ---25.0 ---1.98 J ND ND ND ND ND NI NI NI NI ND
01/30/12 ---25.0 ---ND ND ND ND ND ND NI NI NI NI ND
05/24/12 ---25.0 ---NS NS NS NS NS NS 3.07 J ND 4.78 J ND ND
06/28/12 ---25.0 ---NS NS NS NS NS NS 2.74 J ND ND ND ND
07/25/12 ---25.0 ---3.45 J 2.15 J 2.28 J ND 2.77 J 4.04 J 5.98 J ND 4.58 J ND ND
08/24/12 ---25.0 ---NS NS NS NS NS NS 8.35 J ND 3.94 J ND ND
02/04/13 ---25.0 ---3.72 B 2.34 B 6.74 B ND ND 3.51 B 3.75 J ND ND ND 2.12 J
07/08/13 ---25.0 ---7.94 J ND ND ND ND 11.30 J ND ND 17.10 J ND ND
01/21/14 1.97 25.0 ---10.8 B 9.42 B ND ND ND 4.48 B ND ND 3.28 B ND 14.6 J
07/21/14 0.93 25.0 ---3.01 B ND 3.50 B ND 2.85 B 1.70 B 3.73 B ND 4.34 B 1.40 B 1.69 J
01/29/15 0.93 25.0 ---ND 1.79 J 1.02 J ND ND ND ND ND 10.20 J ND ND
07/27/15 1.57 25.0 ---ND ND 2.19 J ND ND 2.08 J ND ND 1.94 J ND ND
01/26/16 1.57 25.0 ---3.05 J ND ND ND ND ND ND ND 3.33 J ND ND
Zinc 05/23/97 ---50 50 NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 1000 µg/L 06/16/97 ---50 100 NI ND ND ND 130 ---NI NI NI NI 600
08/14/97 ---50 110 NI 90 ND 70 ND ---NI NI NI NI ND
09/30/97 ---20 Dry NI ND 30 50 30 ---NI NI NI NI 140
04/30/98 ---20 70 NI 40 70 90 ND ---NI NI NI NI 100
09/15/98 ---20 ND NI ND ND 50 30 ---NI NI NI NI ND
04/08/99 ---20 30 NI 20 20 ND 40 ---NI NI NI NI ND
09/09/99 ---50 Dry NI 100 80 60 60 ---NI NI NI NI 60
04/13/00 ---50 80 NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---50 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---50 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---50 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---50 Dry NI ND ND 70 ND ---NI NI NI NI ND
10/23/02 ---50 Dry NI ND ND ND 60 ---NI NI NI NI ND
04/14/03 ---50 170 NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---50 ND NI ND ND ND 80 ---NI NI NI NI ND
03/19/04 ---50 ---NI ------------ND NI NI NI NI ND
04/28/04 ---50 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---50 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---50 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---50 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---50 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---50 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---10.0 7.0 J NI 35.1 ND ND 3.9 J 9.4 J NI NI NI NI ND
07/23/07 ---10.0 22.3 NI 168.0 ND ND 11.70 B 14.9 B NI NI NI NI 4.0 J
01/10/08 ---10.0 Dry NI 54.9 ND ND 3.1 J 7.6 J NI NI NI NI ND
07/21/08 ---10.0 Dry NI 411 ND ND 4.7 J 15.5 NI NI NI NI ND
01/29/09 ---10.0 Dry NI 33.0 ND ND 14.9 B 11.7 B NI NI NI NI 5.8 J
07/30/09 ---10.0 39.3 NI 509 5.19 J ND 7.2 J 12.5 NI NI NI NI ND
01/14/10 ---10.0 ---12.80 91.5 6.46 J ND 3.4 J 12.2 NI NI NI NI ND
07/15/10 ---10.0 ---5.32 J 431 ND ND 8.3 J 12.1 NI NI NI NI ND
01/20/11 ---10.0 ---ND 179 ND ND ND 6.06 J NI NI NI NI ND
07/14/11 ---10.0 ---4.04 J 423 ND ND 4.0 J 10.10 NI NI NI NI ND
01/30/12 ---10.0 ---6.39 B 103 2.91 B 5.03 B 2.8 B 6.75 B NI NI NI NI 3.00 J
05/24/12 ---10.0 ---NS NS NS NS NS NS 11 B 14.8 B 20.2 B 8.3 B 2.38 J
06/28/12 ---10.0 ---NS NS NS NS NS NS 5.91 B 14.4 B 6.3 B 7.4 B 27.9
07/25/12 ---10.0 ---4.42 B 103 1.90 B 2.48 B 4.9 B 6.04 B 4.68 B 9.4 B 10.4 B 5.5 B 2.48 J
08/24/12 ---10.0 ---NS NS NS NS NS NS 3.04 B 11.3 B 8.2 B 5.3 B 3.32 J
02/04/13 ---10.0 ---1.87 B 56.6 4.90 B 3.19 B 1.1 B 5.55 B 1.85 B 8.3 J 3.1 B 4.2 B 0.76 J
07/08/13 ---10.0 ---21.2 172 5.20 J 11.0 1.2 B 6.73 J 3.12 B 14.5 59.3 5.7 J 0.96 J
01/21/14 0.87 10.0 ---4.78 B 30.6 4.85 B 3.69 B 5.07 B 18.3 J 2.45 B 15.0 J 17.0 J 8.36 B 2.35 J
07/21/14 0.64 10.0 ---4.90 B 504 1.86 B 1.51 B 1.45 B 5.32 B 1.76 B 14.4 10.3 5.84 B 1.93 J
01/29/15 0.64 10.0 ---2.88 B 18.3 1.31 B 1.79 B 2.28 B 7.32 B 2.56 B 17.9 28.5 7.43 B 1.54 J
07/27/15 1.30 10.0 ---4.63 B 5.19 B 2.89 B 1.66 B ND 4.51 B ND 11.8 6.87 B 7.86 J 1.57 J
01/26/16 1.30 10.0 ---3.65 B 12.4 ND 3.13 B 1.66 B 9.31 J ND 13.0 8.74 J 5.34 B 1.35 J
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 9 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Iron 07/23/07 ---300 2200 NI 20 44 20 7340 676 NI NI NI NI ND
NC 2L = 300 µg/L 01/10/08 ---300 Dry NI 38 J 71 J ND 4600 575 NI NI NI NI ND
07/21/08 ---300 Dry NI 184 J 47 J ND 10400 1950 NI NI NI NI ND
01/29/09 ---300 Dry NI 622 142 J 56.1 B 3520 585 NI NI NI NI 33.80 J
07/30/09 ---300 2540 NI 114 J 92 J 95 J 10900 851 NI NI NI NI ND
01/14/10 ---300 ---1630 249 J 222 J 87 J 5200 597 NI NI NI NI ND
07/15/10 ---300 ---517 185 J 84 J 47.7 J 7880 1350 NI NI NI NI ND
01/20/11 ---300 ---359 325 106 J 60.4 J 2000 489 NI NI NI NI ND
07/14/11 ---300 ---490 239 J 97 J 64.6 J 3220 773 NI NI NI NI ND
01/30/12 ---40.0 ---146 189 775 446 1760 722 NI NI NI NI 8.11 J
07/25/12 ---40.0 ---221 157 1400 4590 10200 708 NS NS NS NS 4.71 J
02/04/13 ---30.0 ---156 318 1790 5430 1840 950 83700 50.90 B 203 186 5.53 J
07/08/13 ---30.0 ---5280 204 7180 2160 1500 1050 45600 44.50 14300 1440 ND
01/21/14 3.02 30.0 ---783 457 7990 1060 1590 2540 87000 132 3730 271 4.96 J
07/21/14 3.1 40.0 ---93.8 138 2120 1700 3000 860 81900 178 1810 1930 ND
01/29/15 3.10 40.0 ---63.0 2950 656 579 1720 726 65900 82.1 14400 225 4.34 J
07/27/15 5.72 40 ---140 153 168 104 561 201 89900 14.9 J 3810 103 ND
01/26/16 5.72 300 ---253 J 197 J 249 J 1050 3430 408 98300 209 J 9020 231 J 9.50 J
Manganese 07/23/07 ---50.0 77.70 NI 31.6 J 314 59.2 4130 21.4 J NI NI NI NI ND
NC 2L = 50 µg/L 01/10/08 ---50.0 Dry NI 21.6 J 249 30 J 2130 23.0 J NI NI NI NI ND
07/21/08 ---50.0 Dry NI 35.8 J 341 41.1 J 4840 23.6 J NI NI NI NI 2.8 J
01/29/09 ---50.0 Dry NI 481 225 25 B 3250 15.6 B NI NI NI NI 13.3 J
07/30/09 ---50.0 48.80 J NI 191 281 55.7 4520 17.1 J NI NI NI NI ND
01/14/10 ---50.0 ---123 355 294 23.8 J 3680 19.5 J NI NI NI NI ND
07/15/10 ---50.0 ---45.6 J 203 203 45.5 J 3500 25.0 J NI NI NI NI ND
01/20/11 ---50.0 ---94.3 224 291 26.3 J 1150 10.7 J NI NI NI NI ND
07/14/11 ---50.0 ---83.7 198 167 49.2 3050 13.7 NI NI NI NI 1.16 J
01/30/12 ---10.0 ---27.1 353 273 38 1140 11.0 NI NI NI NI ND
07/25/12 ---10.0 ---67.2 164 272 218 3690 9.13 J NS NS NS NS ND
02/04/13 ---50.0 ---30.4 J 406 141 393 1560 13.90 J 5190 585 30.3 J 90.2 ND
07/08/13 ---50.0 ---221 363 182 202 3860 24.20 J 4490 442 636.0 206 0.64 J
01/21/14 0.550 50.0 ---101 577 310 52.0 1440 33.2 J 9030 430 184 108 ND
07/21/14 0.395 50.0 ---10.7 B 153 72.0 136 2950 10.4 B 13600 920 181 249 2.27 J
01/29/15 0.395 50.0 ---5.60 B 1950 222 25.1 J 1210 48.9 J 6050 561 1610 110 1.33 J
07/27/15 1.04 50.0 ---12.9 J 141 51.9 41.0 J 1200 13.6 J 12400 536 214 119 ND
01/26/16 1.04 50.0 ---24.0 J 572 306 26.1 J 2690 28.0 J 12300 514 680 142 ND
Organic Compounds
Acetone 07/25/12 ---100 ---ND ND ND 29 J ND ND ND ND ND ND ND
NC 2L = 6000 µg/L 08/24/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---100 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---100 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 1.6 100 ---ND ND ND ND ND ND ND ND ND ND 3.70 J
07/21/14 5.7 100 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 5.7 100 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 3.1 100 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 4.9 100 ---ND ND ND ND ND ND 5.5 J ND ND ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 10 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Benzene 05/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
NC 2L = 1 µg/L 06/28/12 ---1.0 ---NS NS NS NS NS NS 0.2 J ND ND ND ND
07/25/12 ---1.0 ---ND ND ND ND ND ND ND ND ND ND ND
08/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---1.0 ---ND ND ND ND ND ND 0.2 J ND ND ND ND
07/08/13 ---1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 0.3 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/21/14 0.2 1.0 ---ND ND ND ND ND ND 0.2 J ND ND ND ND
01/29/15 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
Carbon Disulfide 05/23/97 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 700 µg/L 06/16/97 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---5 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---5 ND NI ND ND ND 29 ---NI NI NI NI ND
09/15/98 ---5 ND NI ND ND 120 12 ---NI NI NI NI ND
04/08/99 ---5 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---100 ---NI ------------ND NI NI NI NI ND
04/28/04 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/14/10 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
07/15/10 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
01/20/11 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
05/24/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
06/28/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---100 ---ND ND ND ND ND ND ND ND ND ND ND
08/24/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---100 ---ND ND ND ND ND ND ND ND ND ND 3.90 J
07/08/13 ---100 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 1.2 100 ---ND ND ND ND ND ND ND ND ND ND ND
07/21/14 0.8 100 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 0.8 100 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.3 100 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 0.9 100 ---ND ND ND ND ND ND ND ND ND ND ND
Chloroform 05/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
NC 2L = 70 µg/L 06/28/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---1.0 ---ND ND ND ND ND ND 0.6 B 0.5 B 0.5 B ND 1.4 J
08/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND 0.6 J
02/04/13 ---1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---1.0 ---ND ND ND ND ND ND ND ND ND ND 2.2 J
01/21/14 0.3 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/21/14 0.2 5.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 0.2 5.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.2 5.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 0.3 5.0 ---ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 05/24/12 ---5.0 ---NS NS NS NS NS NS ND ND ND ND ND
NC 2L = 600 µg/L 06/28/12 ---5.0 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---5.0 ---ND ND ND ND ND ND 0.5 J ND ND ND ND
08/24/12 ---5.0 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---5.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---5.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 0.5 5.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/21/14 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 0.3 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride 01/26/16 0.5 1 ---ND ND ND ND ND ND ND ND ND ND 0.90 J
NC 2L = 5 µg/L
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 11 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Methyl Ethyl Ketone (2-Butanone)05/23/97 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
06/16/97 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 4000 µg/L 08/14/97 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---100 ND NI ND ND 130 ND ---NI NI NI NI ND
04/08/99 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---100 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---100 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---100 ---NI ------------ND NI NI NI NI ND
04/28/04 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
07/23/07 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---100 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---100 ND NI ND ND ND ND ND NI NI NI NI ND
01/14/10 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
07/15/10 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
01/20/11 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---100 ---ND ND ND ND ND ND NI NI NI NI ND
05/24/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
06/28/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---100 ---ND ND ND 17.0 J ND ND ND ND ND ND ND
08/24/12 ---100 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---100 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---100 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 0.8 100 ---ND ND ND ND ND ND ND ND ND ND 2.7 J
07/21/14 0.8 100 ---ND ND ND ND ND ND ND ND ND ND 1.1 J
01/29/15 0.8 100 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.9 100 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 1.1 100 ---ND ND ND ND ND ND ND ND ND ND ND
Tetrachloroethene 05/23/97 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
NC 2L = 0.7 µg/L 06/16/97 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
08/14/97 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/30/97 ---5.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/30/98 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/15/98 ---5.0 ND NI ND ND 130 ND ---NI NI NI NI ND
04/08/99 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
09/09/99 ---5.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/13/00 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/17/00 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
04/23/01 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/18/01 ---5.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/29/02 ---5.0 Dry NI ND ND ND ND ---NI NI NI NI ND
10/23/02 ---5.0 Dry NI ND ND ND ND ---NI NI NI NI ND
04/14/03 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
10/30/03 ---5.0 ND NI ND ND ND ND ---NI NI NI NI ND
03/19/04 ---5.0 ---NI ------------ND NI NI NI NI ND
04/28/04 ---5.0 ND NI ND ND ND ND ND NI NI NI NI ND
10/27/04 ---5.0 ND NI ND ND ND ND ND NI NI NI NI ND
03/16/05 ---5.0 ND NI ND ND ND ND ND NI NI NI NI ND
07/21/05 ---5.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/26/06 ---5.0 ---NI ND ND ND ND ND NI NI NI NI ND
07/21/06 ---5.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/22/07 ---3.0 0.55 J NI 0.30 J ND ND ND ND NI NI NI NI ND
07/23/07 ---1.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/10/08 ---1.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/21/08 ---1.0 Dry NI ND ND ND ND ND NI NI NI NI ND
01/29/09 ---1.0 Dry NI ND ND ND ND ND NI NI NI NI ND
07/30/09 ---1.0 ND NI ND ND ND ND ND NI NI NI NI ND
01/14/10 ---1.0 ---ND ND ND ND ND ND NI NI NI NI ND
07/15/10 ---1.0 ---ND ND ND ND ND ND NI NI NI NI ND
01/20/11 ---1.0 ---ND ND ND ND ND ND NI NI NI NI ND
07/14/11 ---1.0 ---ND ND ND ND ND ND NI NI NI NI ND
01/30/12 ---1.0 ---ND ND ND ND ND ND NI NI NI NI ND
05/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
06/28/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
07/25/12 ---1.0 ---ND ND ND ND ND ND ND ND ND ND ND
08/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
02/04/13 ---1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/08/13 ---1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/21/14 0.4 1.0 ---ND ND ND ND ND ND ND ND 0.7 J ND ND
07/21/14 0.4 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 0.4 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.3 1.0 ---ND 0.70 J ND ND ND ND ND ND 0.60 J ND ND
01/26/16 0.4 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
Toluene 07/25/12 ---1.0 ---ND ND ND 360 ND ND ND ND ND ND ND
08/24/12 ---1.0 ---NS NS NS NS NS NS ND ND ND ND ND
NC 2L = 600 µg/L 02/04/13 ---1.0 ---ND ND ND 1.3 ND ND ND ND ND ND ND
07/08/13 ---1.0 ---ND ND ND 3.8 ND ND ND ND ND ND ND
01/21/14 0.3 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/21/14 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/29/15 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
07/27/15 0.2 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
01/26/16 0.3 1.0 ---ND ND ND ND ND ND ND ND ND ND ND
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 12 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Field Parameters
pH 05/23/97 ------5.56 NI 6.38 7.50 7.74 6.33 ---NI NI NI NI ---
(S.U.)06/16/97 ------5.67 NI 6.67 7.50 7.84 6.25 ---NI NI NI NI ---
08/14/97 ------5.74 NI 6.50 7.42 7.71 6.18 ---NI NI NI NI ---
09/30/97 ------Dry NI 6.49 7.49 7.4 6.10 ---NI NI NI NI ---
04/30/98 ------5.79 NI 6.24 7.12 7.19 6.56 ---NI NI NI NI ---
09/15/98 ------5.51 NI 6.73 7.66 7.71 6.99 ---NI NI NI NI ---
04/08/99 ------5.70 NI 6.27 7.26 7.42 6.72 ---NI NI NI NI ---
09/09/99 ------Dry NI 6.99 7.63 7.49 6.60 ---NI NI NI NI ---
04/13/00 ------5.14 NI 6.47 7.51 7.43 6.41 ---NI NI NI NI ---
10/17/00 ------8.73 NI 7.82 8.83 7.98 7.46 ---NI NI NI NI ---
04/23/01 ------5.70 NI 6.42 7.45 7.36 6.48 ---NI NI NI NI ---
10/18/01 ------Dry NI 6.42 7.38 7.21 6.27 ---NI NI NI NI ---
04/29/02 ------Dry NI 6.51 7.42 7.4 7.18 ---NI NI NI NI ---
10/23/02 ------Dry NI 6.57 7.80 7.37 6.82 ---NI NI NI NI ---
04/14/03 ------5.00 NI 6.10 7.39 7.24 6.34 ---NI NI NI NI ---
10/30/03 ------6.25 NI 6.75 8.10 7.6 6.67 ---NI NI NI NI ---
03/19/04 ---------NI ------------6.36 NI NI NI NI ---
04/28/04 ------5.91 NI 6.22 7.45 7.41 6.51 6.56 NI NI NI NI ---
10/27/04 ------5.17 NI 5.99 6.96 6.91 6.12 6.31 NI NI NI NI ---
03/16/05 ------6.18 NI 6.30 7.19 7.15 6.16 6.40 NI NI NI NI ---
07/21/05 ------6.55 NI 6.56 7.13 7.21 6.95 6.24 NI NI NI NI ---
01/26/06 ------Dry NI 6.07 8.81 8.18 7.64 6.70 NI NI NI NI ---
07/21/06 ---------NI 6.24 7.22 7.09 6.41 6.18 NI NI NI NI ---
01/22/07 ------5.62 NI 6.51 7.24 7.14 6.40 6.01 NI NI NI NI ---
07/23/07 ------6.84 NI 5.95 7.53 7.27 6.57 6.29 NI NI NI NI ---
01/10/08 ------Dry NI 6.01 7.16 7.1 6.56 6.20 NI NI NI NI ---
07/21/08 ------Dry NI 6.08 7.37 7.07 6.35 6.33 NI NI NI NI ---
01/29/09 ------Dry NI 5.87 7.05 6.91 6.32 6.18 NI NI NI NI ---
07/30/09 ------4.79 NI 5.75 6.60 6.45 5.95 5.89 NI NI NI NI ---
01/14/10 ---------5.22 5.92 6.82 6.82 6.48 5.93 NI NI NI NI ---
07/15/10 ---------5.49 5.72 6.87 6.82 6.30 5.94 NI NI NI NI ---
01/20/11 ---------5.71 5.80 6.95 6.75 6.75 5.93 NI NI NI NI ---
02/18/11 ------------5.65 ------------NI NI NI NI ---
07/14/11 ---------5.47 5.80 6.90 6.7 6.57 5.48 NI NI NI NI ---
01/30/12 ---------5.86 6.03 7.00 6.99 7.00 5.93 NI NI NI NI ---
05/24/12 ---------NS NS NS NS NS NS 5.94 5.39 5.76 5.65 ---
06/28/12 ---------NS NS NS NS NS NS 6.07 5.81 6.20 5.82 ---
07/25/12 ---------6.00 6.20 7.41 6.95 6.94 6.05 6.1 5.52 5.34 5.60 ---
08/24/12 ---------NS NS NS NS NS NS 6.04 5.61 5.46 5.66 ---
02/04/13 ---------5.65 6.07 7.15 7.09 7.25 5.86 6.28 7.06 5.75 5.74 ---
07/08/13 ---------5.37 5.68 6.75 6.68 6.62 5.32 5.89 4.82 4.99 4.91 ---
01/21/14 ---------8.96 6.66 6.60 6.98 7.12 7.43 6.97 6.61 5.66 5.78 ---
07/21/14 ---------5.75 5.94 6.83 6.97 6.98 5.87 5.99 5.24 4.71 5.02 ---
01/29/15 FIELD FIELD ---5.45 ---6.40 6.48 6.92 5.57 6.11 5.39 5.12 4.78 ---
07/27/15 FIELD FIELD ---5.95 6.23 7.42 7.02 7.25 5.99 6.23 5.28 5.34 5.12
01/26/16 FIELD FIELD ---6.63 5.83 6.55 6.99 6.78 5.99 6.38 5.59 5.24 5.10
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 13 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Conductivity 05/23/97 ------82 NI 232 375 278 149 ---NI NI NI NI ---
(µS/cm)06/16/97 ------73 NI 299 441 325 186 ---NI NI NI NI ---
08/14/97 ------94 NI 309 384 306 267 ---NI NI NI NI ---
09/30/97 ------Dry NI 215 327 277 181 ---NI NI NI NI ---
04/30/98 ------12 NI 31 53 47 44 ---NI NI NI NI ---
09/15/98 ------77 NI 180 344 434 274 ---NI NI NI NI ---
04/08/99 ------72 NI 135 232 206 189 ---NI NI NI NI ---
09/09/99 ------Dry NI 102 190 137 130 ---NI NI NI NI ---
04/13/00 ------62 NI 285 413 3.35 351 ---NI NI NI NI ---
10/17/00 ------53 NI 225 245 274 191 ---NI NI NI NI ---
04/23/01 ------67 NI 239 472 445 327 ---NI NI NI NI ---
10/18/01 ------Dry NI 178 297 283 231 ---NI NI NI NI ---
04/29/02 ------Dry NI 91 136 140 161 ---NI NI NI NI ---
10/23/02 ------Dry NI 149 302 289 201 ---NI NI NI NI ---
04/14/03 ------48 NI 73 63 75 81 ---NI NI NI NI ---
10/30/03 ------186 NI 174 487 487 108 ---NI NI NI NI ---
03/19/04 ---------NI ------------971 NI NI NI NI ---
04/28/04 ------82 NI 128 168 154 144 449 NI NI NI NI ---
10/27/04 ------54 NI 235 532 546 488 658 NI NI NI NI ---
03/16/05 ------49 NI 297 481 ---389 322 NI NI NI NI ---
07/21/05 ------62 NI 325 542 501 501 413 NI NI NI NI ---
01/26/06 ------Dry NI 189 468 447 361 367 NI NI NI NI ---
07/21/06 ---------NI 279 607 595 551 442 NI NI NI NI ---
01/22/07 ------57 NI 409 602 634 564 419 NI NI NI NI ---
07/23/07 ------80 NI 295 581 642 577 485 NI NI NI NI ---
01/10/08 ------Dry NI 414 914 999 567 600 NI NI NI NI ---
07/21/08 ------Dry NI 269 617 752 617 406 NI NI NI NI ---
01/29/09 ------Dry NI 259 636 750 508 280 NI NI NI NI ---
07/30/09 ------81 NI 233 623 776 607 279 NI NI NI NI ---
01/14/10 ---------152 236 605 765 543 252 NI NI NI NI ---
07/15/10 ---------154 211 615 800 577 239 NI NI NI NI ---
01/20/11 ---------160 225 621 830 556 209 NI NI NI NI ---
02/18/11 ------------234 ------------NI NI NI NI ---
07/14/11 ---------173 242 660 887 633 224 NI NI NI NI ---
01/30/12 ---------137 199 471 685 424 141 NI NI NI NI ---
05/24/12 ---------NS NS NS NS NS NS 607 193.0 102.0 117.0 ---
06/28/12 ---------NS NS NS NS NS NS 588 220.7 119.1 151.7 ---
07/25/12 ---------146.7 247.3 625 917 625 190.7 694 227.9 75.9 118.9 ---
08/24/12 ---------NS NS NS NS NS NS 689 216.9 82.4 128.2 ---
02/04/13 ---------130.1 173.9 458.9 549 422.6 127.6 634 143.6 64.2 119.8 ---
07/08/13 ---------118.4 211.4 457.3 711 379.6 136.0 519 110.6 78.8 101.1 ---
01/21/14 ---------155.7 252.8 487.9 644 490.3 180.3 771 164.4 76.6 72.1 ---
07/21/14 ---------138.7 278.9 508.0 828 510.0 161.5 749 225.4 84.8 108.9 ---
01/29/15 FIELD FIELD ---149.5 ---475.5 658 430.9 152.6 546 171.4 218.4 81.2 ---
07/27/15 ---------135 277 491 689 459 165 635 173 81 75 ---
01/26/16 ------154.1 283.4 484.7 704 478.6 169.8 449.1 196.1 204.8 75.5 ---
Temperature 05/23/97 ------19.7 NI 17.5 16.9 16.9 16.2 ---NI NI NI NI ---
(ºC)06/16/97 ------19.8 NI 17.6 16.3 15.7 17.7 ---NI NI NI NI ---
08/14/97 ------28.0 NI 19.1 21.9 25 22.1 ---NI NI NI NI ---
09/30/97 ------Dry NI 16.6 19.1 17.1 19.4 ---NI NI NI NI ---
04/30/98 ------22.2 NI 16.0 17.0 16.3 17.7 ---NI NI NI NI ---
09/15/98 ------22.1 NI 15.6 14.2 16.7 22.2 ---NI NI NI NI ---
04/08/99 ------22.1 NI 20.4 18.0 19 16.4 ---NI NI NI NI ---
09/09/99 ------Dry NI 13.3 22.5 22.4 23.3 ---NI NI NI NI ---
04/13/00 ------16.3 NI 18.0 16.3 11.2 11.3 ---NI NI NI NI ---
10/17/00 ------16.7 NI 18.1 16.8 16.8 18.4 ---NI NI NI NI ---
04/23/01 ------17.7 NI 18.5 17.2 17.2 16.1 ---NI NI NI NI ---
10/18/01 ------Dry NI 15.9 15.3 13.6 14.5 ---NI NI NI NI ---
04/29/02 ------Dry NI 17.5 15.8 16 20.0 ---NI NI NI NI ---
10/23/02 ------Dry NI 18.2 17.5 17 20.8 ---NI NI NI NI ---
04/14/03 ------18.8 NI 18.7 17.7 17.5 14.7 ---NI NI NI NI ---
10/30/03 ------17.6 NI 16.8 17.4 16.4 17.6 ---NI NI NI NI ---
03/19/04 ---------NI ------------12.60 NI NI NI NI ---
04/28/04 ------15.1 NI 16.3 16.2 16.7 10.5 14.50 NI NI NI NI ---
10/27/04 ------14.4 NI 16.1 15.0 15.8 17.2 15.40 NI NI NI NI ---
03/16/05 ------11.83 NI 13.66 13.49 12.79 11.16 10.12 NI NI NI NI ---
07/21/05 ------18.62 NI 20.70 17.34 19.71 22.59 19.60 NI NI NI NI ---
01/26/06 ------Dry NI 13.92 14.77 14.27 13.00 13.00 NI NI NI NI ---
07/21/06 ---------NI 22.10 18.93 18.34 18.70 15.70 NI NI NI NI ---
01/22/07 ------14.20 NI 15.20 12.90 13.4 13.40 12.90 NI NI NI NI ---
07/23/07 ------18.50 NI 18.61 18.72 18.5 20.03 16.30 NI NI NI NI ---
01/10/08 ------Dry NI 16.44 15.19 14.92 14.37 14.66 NI NI NI NI ---
07/21/08 ------Dry NI 21.25 22.36 22.78 22.99 17.73 NI NI NI NI ---
01/29/09 ------Dry NI 14.67 11.89 14.16 10.04 12.24 NI NI NI NI ---
07/30/09 ------23.94 NI 20.10 20.26 24.22 22.45 19.95 NI NI NI NI ---
01/14/10 ---------13.74 15.97 13.47 13.35 12.42 13.06 NI NI NI NI ---
07/15/10 ---------22.65 22.56 20.04 21.78 19.57 19.23 NI NI NI NI ---
01/20/11 ---------13.25 15.60 13.65 13.49 13.18 13.25 NI NI NI NI ---
02/18/11 ------------17.03 ------------NI NI NI NI ---
07/14/11 ---------19.07 20.71 19.14 20.08 19.29 16.80 NI NI NI NI ---
01/30/12 ---------14.13 16.91 14.57 16.56 13.70 13.66 NI NI NI NI ---
05/24/12 ---------NS NS NS NS NS NS 16.78 18.24 16.99 16.41 ---
06/28/12 ---------NS NS NS NS NS NS 23.1 26.4 23.0 20.1 ---
07/25/12 ---------19.1 18.9 18.4 22.4 17.3 15.8 17.5 18.5 16.8 16.7 ---
08/24/12 ---------NS NS NS NS NS NS 15.9 16.2 16.7 16.1 ---
02/04/13 ---------14.6 13.2 14.2 10.2 14.5 14.2 13.2 12.4 14.2 14.4 ---
07/08/13 ---------16.0 17.1 16.2 20.4 15.5 14.9 16.2 16.6 15.5 15.1 ---
01/21/14 ---------15.0 16.2 14.6 13.1 15.1 14.5 14.5 15.2 16.0 15.4 ---
07/21/14 ---------16.7 17.4 16.6 20.6 16.9 14.7 18.1 20.1 16.9 16.0 ---
01/29/15 FIELD FIELD ---14.7 ---14.5 13.3 13.5 12.6 13.0 13.2 15.5 14.6 ---
07/27/15 FIELD FIELD ---16.78 18.1 18.56 18.78 17.89 15.70 17.82 17.3 18.4 17.14 ---
01/26/16 FIELD FIELD ---14.9 16.7 14.2 14.0 14.8 14.5 15.1 15.2 15.5 15.0 ---
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 14 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Turbidity 05/23/97 ------19 NI 14.0 2.85 7.89 250 ---NI NI NI NI ---
(NTU)06/16/97 ------100 NI 11.0 5.79 9.82 28.0 ---NI NI NI NI ---
08/14/97 ------770 NI 14.0 8.18 7.13 63.0 ---NI NI NI NI ---
09/30/97 ------Dry NI 4.2 6.56 8.46 47.0 ---NI NI NI NI ---
04/30/98 ------13 NI 23.0 22.00 5.79 16.0 ---NI NI NI NI ---
09/15/98 ------590 NI 19.7 11.20 22.2 62.8 ---NI NI NI NI ---
04/08/99 ------11 NI 9.4 8.81 1.23 7.97 ---NI NI NI NI ---
09/09/99 ------Dry NI 9.1 5.60 5.71 32.0 ---NI NI NI NI ---
04/13/00 ------280 NI 32.0 6.79 1.81 70.0 ---NI NI NI NI ---
10/17/00 ------292 NI 22.1 1.91 1.36 26.9 ---NI NI NI NI ---
04/23/01 ------440 NI 72.0 3.66 4.36 14.0 ---NI NI NI NI ---
10/18/01 ------Dry NI 30.0 1.86 7.92 43.0 ---NI NI NI NI ---
04/29/02 ------Dry NI 42.0 1.96 2.03 4.23 ---NI NI NI NI ---
10/23/02 ------Dry NI 34.0 2.81 6.06 6.76 ---NI NI NI NI ---
04/14/03 ------184 NI 23.0 3.96 1.03 3.86 ---NI NI NI NI ---
10/30/03 ------17 NI 7.2 5.25 3.91 14.0 ---NI NI NI NI ---
03/19/04 ---------NI ------------5.82 NI NI NI NI ---
04/28/04 ------32 NI 19.0 2.99 0.94 25.0 6.45 NI NI NI NI ---
10/27/04 ------19 NI 20.0 4.82 9.72 19.0 25.00 NI NI NI NI ---
03/16/05 ------320 NI 224.0 86.50 35.7 37.0 288.00 NI NI NI NI ---
07/21/05 ------763 NI 438.0 320 240 233.0 426.00 NI NI NI NI ---
01/26/06 ------Dry NI 102.0 88.10 24.2 174.0 126 NI NI NI NI ---
07/21/06 ---------NI 60.3 0.00 0 124.0 147 NI NI NI NI ---
01/22/07 ------290 NI >1000 30.90 0 197.0 34.8 NI NI NI NI ---
07/23/07 ------364 NI 3.70 4.60 7.1 130.0 52.2 NI NI NI NI ---
01/10/08 ------Dry NI 2.46 2.64 0.48 56.7 16.1 NI NI NI NI ---
07/21/08 ------Dry NI 13.60 0.88 0.64 82.4 37.7 NI NI NI NI ---
01/29/09 ------Dry NI 30.70 1.39 1.55 26.6 22.3 NI NI NI NI ---
07/30/09 ------123 NI 7.50 1.67 1.74 85.3 25.0 NI NI NI NI ---
01/14/10 ---------73.90 7.71 0.95 2.37 61.8 21.1 NI NI NI NI ---
07/15/10 ---------15.10 3.79 1.58 1.07 39.0 34.4 NI NI NI NI ---
01/20/11 ---------14.00 6.16 0.30 0.65 32.7 16.3 NI NI NI NI ---
02/18/11 ------------6.26 ------------NI NI NI NI ---
07/14/11 ---------9.18 2.35 1.19 0.67 43.9 15.2 NI NI NI NI ---
01/30/12 ---------17.92 15.30 10.68 10.52 16.39 24.7 NI NI NI NI ---
05/24/12 ---------NS NS NS NS NS NS 16.19 11.81 62.4 13.56 ---
06/28/12 ---------NS NS NS NS NS NS 18.61 6.61 63.7 6.55 ---
07/25/12 ---------5.91 2.84 4.75 5.86 25.8 8.24 3.99 2.83 32.2 5.54 ---
08/24/12 ---------NS NS NS NS NS NS 5.42 4.60 24.9 5.09 ---
02/04/13 ---------15.10 11.19 16.91 16.39 12.04 16.61 11.39 16.11 19.1 11.37 ---
07/08/13 ---------3.27 7.10 10.12 4.22 3.24 7.19 9.68 10.81 31.5 10.07 ---
01/21/14 ---------5.21 3.23 3.62 4.10 3.80 3.97 3.92 4.06 3.91 3.81 ---
07/21/14 ---------3.23 17.90 3.85 7.55 4.31 2.01 5.29 4.27 26.70 4.77 ---
01/29/15 FIELD FIELD ---30.50 ---2.01 ------6.57 1.51 2.07 15.60 3.51 ---
07/27/15 FIELD FIELD ---7.32 9.72 6.4 11.3 8.0 13.1 4.6 4.5 70 10 ---
01/26/16 FIELD FIELD ---5.45 4.39 6.2 10.6 7.66 11.6 3.22 4.06 68 3 ---
Oxidation Reduction Potential 03/16/05 ------194 NI 92 65.0 103 13.0 127.0 NI NI NI NI ---
(mV)07/21/05 ------206 NI 53 -9.0 3 -26.0 110.0 NI NI NI NI ---
01/26/06 ------Dry NI 136 -88.0 -13 35.0 141.0 NI NI NI NI ---
07/21/06 ---------NI 108 -112.0 -74 9.0 180.0 NI NI NI NI ---
01/22/07 ------279 NI 183 -100.0 -38 -2.0 256.0 NI NI NI NI ---
07/23/07 ---------NI 326 -82.0 -28 -28.0 182.0 NI NI NI NI ---
01/10/08 ------Dry NI 193 -88.0 -16 8.0 206.0 NI NI NI NI ---
07/21/08 ------Dry NI 206 -65.0 -33 -52.0 166.0 NI NI NI NI ---
01/29/09 ------Dry NI 210.5 -9.3 103.2 175.8 253.4 NI NI NI NI ---
07/30/09 ------181.6 NI 123.8 -50.2 2.6 -24.1 132.0 NI NI NI NI ---
01/14/10 ---------166.3 70.4 -33.1 20.2 11.1 141.0 NI NI NI NI ---
07/15/10 ---------40.1 187.9 -70.4 48.3 82.0 -13.8 NI NI NI NI ---
01/20/11 ---------199.8 132.5 -18.5 42.4 18.2 195.6 NI NI NI NI ---
02/18/11 ------------187.3 ------------NI NI NI NI ---
07/14/11 ---------94.9 118.3 -23.4 5.4 -12.7 114.6 NI NI NI NI ---
01/30/12 ---------31.3 41.9 -73.6 -32.4 -15.5 42.3 NI NI NI NI ---
05/24/12 ---------NS NS NS NS NS NS 91.4 161.9 147.2 149.1 ---
06/28/12 ---------NS NS NS NS NS NS 13.9 224.3 188.5 219.3 ---
07/25/12 ---------100.8 152.1 -137.3 -137.8 -51.5 148.0 -108.9 166.7 131.0 133.5 ---
08/24/12 ---------NS NS NS NS NS NS 12.1 156.6 129.8 125.1 ---
02/04/13 ---------181.1 210.2 -6.2 -20.8 -13.1 188.1 -30.1 49.6 211.6 202.4 ---
07/08/13 ---------140.4 176.2 89.2 -132 -4.6 153.6 31.4 180.4 162.1 151.0 ---
01/21/14 ---------85.9 100.6 -39.8 37.2 -39.8 95.0 -57.2 33.0 157.2 111.3 ---
07/21/14 ---------95.0 121.5 85.7 82.1 87.6 103.7 -85.4 95.0 146.9 127.5 ---
01/29/15 FIELD FIELD ---48.6 ---27.7 28.1 47.8 123.0 -38.8 124.3 124.7 150.4 ---
07/27/15 FIELD FIELD ---78.1 169.0 -20.9 -21.6 -23.8 64.5 -132.9 165.3 138.0 146.0 ---
01/26/16 FIELD FIELD ---219.7 194.9 -98.4 62.8 14.3 209.5 -59.6 116.4 204.8 235.6 ---
TABLE 6
Historically Detected Constituents/Analytes in Groundwater
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permot No. 73-04 Page 15 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL RL GW-1 GW-1R GW-2 GW-3 GW-4 GW-5 GW-6 GW-7 GW-8 GW-9 GW-10 Blanks
Dissolved Oxygen 03/16/05 ------5.06 NI 4.90 4.81 5.01 5.66 5.50 NI NI NI NI ---
(mg/L)07/21/05 ------11.28 NI 12.58 13.67 11.66 11.35 11.38 NI NI NI NI ---
01/26/06 ------Dry NI ---0*0*3.18 1.37 NI NI NI NI ---
07/21/06 ---------NI 8.67 2.28 2.05 7.06 6.95 NI NI NI NI ---
01/22/07 ---------NI 8.40 0.50 0.5 0.30 5.50 NI NI NI NI ---
07/23/07 ---------NI 4.20 2.30 1.3 3.00 3.90 NI NI NI NI ---
01/10/08 ------Dry NI 3.59 1.04 3.32 2.24 4.58 NI NI NI NI ---
07/21/08 ------Dry NI 3.57 1.78 0.44 0.48 4.19 NI NI NI NI ---
01/29/09 ------Dry NI 1.90 0.79 0.72 0.68 4.38 NI NI NI NI ---
07/30/09 ------4.98 NI 2.98 1.74 1.11 1.30 3.11 NI NI NI NI ---
01/14/10 ---------5.36 2.04 2.07 0.84 1.60 5.16 NI NI NI NI ---
07/15/10 ---------3.26 1.85 2.63 0.27 0.37 2.72 NI NI NI NI ---
01/20/11 ---------3.70 1.28 1.38 0.63 2.49 5.15 NI NI NI NI ---
02/18/11 ------------1.56 ------------NI NI NI NI ---
07/14/11 ---------3.96 1.94 0.57 0.96 0.86 3.32 NI NI NI NI ---
01/30/12 ---------2.87 2.38 0.56 1.91 3.14 5.48 NI NI NI NI ---
05/24/12 ---------NS NS NS NS NS NS 8.67 7.71 8.49 8.91 ---
06/28/12 ---------NS NS NS NS NS NS 0.71 4.40 4.10 2.12 ---
07/25/12 ---------1.09 1.13 0.67 0.29 1.22 2.22 0.51 2.20 1.73 2.55 ---
08/24/12 ---------NS NS NS NS NS NS 1 2.13 1.55 2.66 ---
02/04/13 ---------2.18 4.51 2.89 4.21 3.69 6.29 1.46 7.09 6.47 3.59 ---
07/08/13 ---------236.00 1.37 0.48 0.38 0.21 1.69 0.68 2.01 1.47 0.99 ---
01/21/14 ---------5.99 1.79 2.45 4.59 6.40 5.41 0.40 6.81 2.87 5.67 ---
07/21/14 ---------2.68 1.58 0.56 1.5 0.56 2.36 0.70 2.32 0.81 0.85 ---
01/29/15 FIELD FIELD ---3.16 ---2.75 1.56 5.86 7.27 1.19 4.36 1.22 1.34 ---
07/27/15 FIELD FIELD ---3.32 2.70 0.12 0.29 0.09 1.61 0.11 0.95 0.48 0.33 ---
01/26/16 FIELD FIELD ---2.48 3.55 0.38 1.56 3.41 3.88 0.87 1.84 1.40 5.17 ---
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
PQL = Practical Quantitation Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC 2L = Groundwater Standard established in 15 A NCAC 2L.0202
GWPS = NC DENR Solid Waste Section Groundwater Protection Standard for constituents with no listed NC 2L.
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = insufficient water to sample.
--- = No data.
All inorganic and organic compounds are in µg/L.
µg/L = micrograms per liter
mg/L = milligrams per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2L or Groundwater Protection standards (GWPS) have been bolded.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 1 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Inorganic Compounds
Antimony 01/30/12 ---6.00 ND 0.14 B 0.33 J
No NC 2B Standard 07/25/12 ---6.00 Dry Dry ND
02/04/13 ---6.00 ND ND ND
07/08/13 ---6.00 ND ND ND
01/21/14 0.22 6.00 ND ND ND
07/21/14 1.05 6.00 ND ND ND
01/29/15 1.05 6.00 ND ND ND
07/27/15 0.25 6.00 DRY 9.27 ND
01/26/16 0.25 6.00 DRY 0.81 J ND
Arsenic 01/30/12 ---10.0 ND 1.61 J ND
NC 2B = 50 µg/L 07/25/12 ---10.0 Dry Dry 1.65 J
02/04/13 ---10.0 1.32 J ND ND
07/08/13 ---10.0 0.91 J 1.68 J ND
01/21/14 0.78 10.0 ND 0.80 J ND
07/21/14 1.13 10.0 2.84 J ND ND
01/29/15 1.13 10.0 ND ND ND
07/27/15 0.75 10.0 DRY 4.62 J ND
01/26/16 0.75 10.0 DRY 1.00 J ND
Barium 06/16/97 ---500 ND ND ---
No NC 2B Standard 08/14/97 ---500 ---ND ---
09/30/97 ---20 ---30 ---
04/30/98 ---20 40 30 ---
09/15/98 ---20 ---30 ---
04/08/99 ---20 30 20 ---
09/09/99 ---500 ND ND ND
04/13/00 ---500 ND ND ND
10/17/00 ---500 Dry Dry ND
04/23/01 ---500 ND ND ND
10/18/01 ---500 ND ND ND
04/29/02 ---500 ND ND ND
10/23/02 ---500 ND ND ND
04/14/03 ---500 ND ND ND
10/30/03 ---500 ND ND ND
04/28/04 ---500 1000 ND ND
10/26/04 ---500 ND ND ND
03/16/05 ---500 ND ND ND
07/21/05 ---500 ND Dry ND
01/26/06 ---500 ND ND ND
07/21/06 ---500 ND ND ND
01/22/07 ---100 37.0 J 33.9 J 0.50 J
07/23/07 ---100 Dry 25.8 J 0.50 J
01/10/08 ---100 41.8 J 34.1 J ND
07/21/08 ---100 Dry Dry ND
01/29/09 ---100 36.6 J 30.5 J 0.50 J
07/30/09 ------Dry Dry ---
01/14/10 ---100 32.8 J 28.2 J ND
07/15/10 ---100 Dry Dry ND
01/20/11 ---100 27.9 J 28.1 J ND
07/14/11 ---100 Dry 39.0 J ND
01/30/12 ---100 34.9 J 33.8 J 0.14 J
07/25/12 ---100 Dry Dry 0.79 J
02/04/13 ---100 39.4 J 37.0 J ND
07/08/13 ---100 51.3 J 74.7 J 0.57 J
01/21/14 0.25 100 40.8 J 31.4 J ND
07/21/14 0.1 100 61.9 J 44.1 J 0.34 J
01/29/15 0.10 100 33.3 J 31.7 J 1.33 J
07/27/15 0.30 100 DRY 79.2 J 0.41 J
01/26/16 0.30 100 DRY 37.6 J 0.55 J
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 2 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Beryllium 06/16/97 ---2.00 ND ND ---
NC 2B = 6.5 µg/L 08/14/97 ---2.00 ---ND ---
09/30/97 ---3.00 ---ND ---
04/30/98 ---3.00 ND ND ---
09/15/98 ---3.00 ---ND ---
04/08/99 ---3.00 ND ND ---
09/09/99 ---2.00 ND ND ND
04/13/00 ---2.00 ND ND ND
10/17/00 ---2.00 Dry Dry ND
04/23/01 ---2.00 ND ND ND
10/18/01 ---2.00 ND ND ND
04/29/02 ---2.00 ND ND ND
10/23/02 ---2.00 ND ND ND
04/14/03 ---2.00 ND ND ND
10/30/03 ---2.00 ND ND ND
04/28/04 ---2.00 2.00 ND ND
10/26/04 ---2.00 ND ND ND
03/16/05 ---2.00 ND ND ND
07/21/05 ---2.00 ND Dry ND
01/26/06 ---2.00 ND ND ND
07/21/06 ---2.00 ND ND ND
01/22/07 ---1.00 ND ND ND
07/23/07 ---1.00 Dry ND ND
01/10/08 ---1.00 ND ND ND
07/21/08 ---1.00 Dry Dry ND
01/29/09 ---1.00 ND ND ND
07/30/09 ------Dry Dry ---
01/14/10 ---1.00 0.09 J ND ND
07/15/10 ---1.00 Dry Dry ND
01/20/11 ---1.00 ND ND ND
07/14/11 ---1.00 Dry ND ND
01/30/12 ---1.00 ND 0.05 J ND
07/25/12 ---1.00 Dry Dry ND
02/04/13 ---1.00 ND ND ND
07/08/13 ---1.00 ND 0.12 J ND
01/21/14 0.11 1.00 ND ND ND
07/21/14 0.05 1.00 0.23 J ND ND
01/29/15 0.05 1.00 0.07 J ND ND
07/27/15 0.09 1.00 DRY ND ND
01/26/16 0.09 1.00 DRY ND ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 3 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Cadmium 07/21/05 ---1.00 ND Dry ND
NC 2B = 2 µg/L 01/26/06 ---1.00 ND ND ND
07/21/06 ---1.00 ND ND ND
01/22/07 ---1.00 ND ND ND
07/23/07 ---1.00 Dry ND ND
01/10/08 ---1.00 ND ND ND
07/21/08 ---1.00 Dry Dry ND
01/29/09 ---1.00 ND ND ND
01/14/10 ---1.00 2.04 1.38 ND
07/15/10 ---1.00 Dry Dry ND
01/20/11 ---1.00 ND ND ND
07/14/11 ---1.00 Dry ND ND
01/30/12 ---1.00 0.34 J ND ND
07/25/12 ---1.00 Dry Dry ND
02/04/13 ---1.00 ND ND ND
07/08/13 ---1.00 1.81 ND ND
01/21/14 0.06 1.00 0.17 J ND ND
07/21/14 0.05 1.00 ND ND ND
01/29/15 0.05 1.00 ND ND 0.1 J
07/27/15 0.10 1.00 DRY 0.12 J ND
01/26/16 0.10 1.00 DRY ND ND
Chromium 06/16/97 ---10.0 ND ND ---
NC 2B = 50 µg/L 08/14/97 ---10.0 ---ND ---
09/30/97 ---10.0 ---ND ---
04/30/98 ---10.0 ND ND ---
09/15/98 ---10.0 ---ND ---
04/08/99 ---10.0 ND ND ---
09/09/99 ---10.0 ND ND ND
04/13/00 ---10.0 ND ND ND
10/17/00 ---10.0 Dry Dry ND
04/23/01 ---10.0 ND ND ND
10/18/01 ---10.0 ND ND ND
04/29/02 ---10.0 ND ND ND
10/23/02 ---10.0 ND ND ND
04/14/03 ---10.0 ND ND ND
10/30/03 ---10.0 ND ND ND
04/28/04 ---10.0 80 ND ND
10/26/04 ---10.0 ND ND ND
03/16/05 ---10.0 ND ND ND
07/21/05 ---10.0 ND Dry ND
01/26/06 ---10.0 ND ND ND
07/21/06 ---10.0 ND ND ND
01/22/07 ---10.0 ND ND ND
07/23/07 ---10.0 Dry ND ND
01/10/08 ---10.0 3.90 J ND ND
07/21/08 ---10.0 Dry Dry ND
01/29/09 ---10.0 1.54 J 1.47 J ND
07/30/09 ------Dry Dry ---
01/14/10 ---10.0 ND ND ND
07/15/10 ---10.0 Dry Dry ND
01/20/11 ---10.0 ND ND ND
07/14/11 ---10.0 Dry 4.50 J ND
01/30/12 ---10.0 2.56 B 3.67 B 1.16 J
07/25/12 ---10.0 Dry Dry ND
02/04/13 ---10.0 5.63 B 4.44 B 2.66 J
07/08/13 ---10.0 6.25 B 11.6 1.50 J
01/21/14 0.58 10.0 5.82 3.82 ND
07/21/14 0.73 10.0 9.22 J 1.36 B 1.40 J
01/29/15 0.73 10.0 2.56 J ND ND
07/27/15 0.43 10.0 DRY 0.96 J ND
01/26/16 0.43 10.0 DRY 2.28 J ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 4 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Cobalt 06/16/97 ---10.0 ND ND ---
No NC 2B Standard 08/14/97 ---10.0 ---ND ---
09/30/97 ---40.0 ---ND ---
04/30/98 ---40.0 ND ND ---
09/15/98 ---40.0 ---ND ---
04/08/99 ---40.0 ND ND ---
09/09/99 ---10.0 ND ND ND
04/13/00 ---10.0 ND ND ND
10/17/00 ---10.0 Dry Dry ND
04/23/01 ---10.0 ND ND ND
10/18/01 ---10.0 ND ND ND
04/29/02 ---10.0 ND 10.0 ND
10/23/02 ---10.0 ND ND ND
04/14/03 ---10.0 ND ND ND
10/30/03 ---10.0 ND ND ND
04/28/04 ---10.0 20.0 ND ND
10/26/04 ---10.0 ND ND ND
03/16/05 ---10.0 ND ND ND
07/21/05 ---10.0 ND Dry ND
01/26/06 ---10.0 ND ND ND
07/21/06 ---10.0 ND ND ND
01/22/07 ---10.0 ND ND ND
07/23/07 ---10.0 Dry ND ND
01/10/08 ---10.0 ND ND ND
07/21/08 ---10.0 Dry Dry ND
01/29/09 ---10.0 ND ND ND
07/30/09 ------Dry Dry ---
01/14/10 ---10.0 0.47 J 0.48 J ND
07/15/10 ---10.0 Dry Dry ND
01/20/11 ---10.0 ND ND ND
07/14/11 ---10.0 Dry 1.11 J ND
01/30/12 ---10.0 0.80 J 0.66 J ND
07/25/12 ---10.0 Dry Dry ND
02/04/13 ---10.0 1.17 J 0.71 J ND
07/08/13 ---10.0 1.82 J 3.24 J ND
01/21/14 0.12 10.0 0.97 J 0.80 J ND
07/21/14 0.26 10.0 1.72 J 0.89 J ND
01/29/15 0.26 10.0 1.07 J 0.70 J ND
07/27/15 0.29 10.0 DRY 1.31 J ND
01/26/16 0.29 10.0 DRY 1.37 J ND
Copper 07/21/05 ---200 ND Dry ND
NC 2B = 7 µg/L 01/26/06 ---200 ND ND ND
07/21/06 ---200 ND ND ND
01/22/07 ---10.0 2.80 J 1.30 J 0.90 J
07/23/07 ---10.0 Dry 0.70 B 1.20 J
01/10/08 ---10.0 1.90 J 2.00 J ND
07/21/08 ---10.0 Dry Dry ND
01/29/09 ---10.0 ND 1.40 J ND
07/30/09 ------Dry Dry ---
01/14/10 ---10.0 3.07 J 2.08 J ND
07/15/10 ---10.0 Dry Dry ND
01/20/11 ---10.0 3.79 B 2.59 B 2.16 J
07/14/11 ---10.0 Dry 4.36 B 1.85 J
01/30/12 ---10.0 2.46 J 3.09 J ND
07/25/12 ---10.0 Dry Dry 0.4 J
02/04/13 ---10.0 3.45 J 2.07 J 0.19 J
07/08/13 ---10.0 4.25 J 6.96 J ND
01/21/14 0.38 10.0 3.96 J 2.35 J ND
07/21/14 0.22 10.0 6.31 J 1.95 B 0.44 J
01/29/15 0.22 10.0 2.74 B 3.87 B 4.34 J
07/27/15 0.41 10.0 DRY 9.13 J 1.24 J
01/26/16 0.41 10.0 DRY 3.02 J 3.93 J
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 5 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Lead 06/16/97 ---10.0 ND ND ---
NC 2B = 25 µg/L 08/14/97 ---10.0 ---ND ---
09/30/97 ---15.0 ---ND ---
04/30/98 ---15.0 ND ND ---
09/15/98 ---15.0 ---ND ---
04/08/99 ---15.0 ND ND ---
09/09/99 ---10.0 ND ND ND
04/13/00 ---10.0 ND ND ND
10/17/00 ---10.0 Dry Dry ND
04/23/01 ---10.0 ND ND ND
10/18/01 ---10.0 ND ND ND
04/29/02 ---10.0 ND ND ND
10/23/02 ---10.0 ND ND ND
04/14/03 ---10.0 ND ND ND
10/30/03 ---10.0 ND ND ND
04/28/04 ---10.0 60.0 ND ND
10/26/04 ---10.0 ND ND ND
03/16/05 ---10.0 ND ND ND
07/21/05 ---10.0 ND Dry ND
01/26/06 ---10.0 ND ND ND
07/21/06 ---10.0 ND ND ND
01/22/07 ---10.0 2.80 J 3.50 J ND
07/23/07 ---10.0 Dry ND ND
01/10/08 ---10.0 ND ND ND
07/21/08 ---10.0 Dry Dry ND
01/29/09 ---10.0 ND ND ND
07/30/09 ------Dry Dry ---
01/14/10 ---10.0 1.15 J ND ND
07/15/10 ---10.0 Dry Dry ND
01/20/11 ---10.0 ND ND ND
07/14/11 ---10.0 Dry ND ND
01/30/12 ---10.0 0.87 J 0.69 J ND
07/25/12 ---10.0 Dry Dry 0.29 J
02/04/13 ---10.0 1.37 J 0.47 J ND
07/08/13 ---10.0 4.57 J 6.71 J 0.09 J
01/21/14 0.05 10.0 1.46 J 0.72 J ND
07/21/14 0.05 10.0 3.75 J 6.29 J ND
01/29/15 0.05 10.0 4.15 J 4.13 J ND
07/27/15 0.08 10.0 ---47.4 ND
Verification sample >09/28/15 0.08 10.0 DRY 8.69 J 0.21 J
01/26/16 0.08 10.0 DRY 4.16 J ND
Methylene Chloride 01/26/16 0.5 1.0 ---ND 0.90 J
No NC 2B Standard
Nickel 07/21/05 ---50.0 ND Dry ND
NC 2B = 88 µg/L 01/26/06 ---50.0 ND ND ND
07/21/06 ---50.0 ND ND ND
01/22/07 ---50.0 ND ND ND
07/23/07 ---50.0 Dry ND ND
01/10/08 ---50.0 3.20 J ND ND
07/21/08 ---50.0 Dry Dry ND
01/29/09 ---50.0 0.69 J 0.92 J ND
07/30/09 ------Dry Dry ---
01/14/10 ---50.0 ND ND ND
07/15/10 ---50.0 Dry Dry ND
01/20/11 ---50.0 2.00 J ND ND
07/14/11 ---50.0 Dry 3.07 J ND
01/30/12 ---50.0 2.47 J 1.88 J ND
07/25/12 ---50.0 Dry Dry ND
02/04/13 ---50.0 2.22 J 1.25 J ND
07/08/13 ---50.0 2.20 B 3.36 B 1.99 J
01/21/14 0.41 50.0 2.07 J 1.65 J ND
07/21/14 0.22 50.0 3.51 J 1.30 J ND
01/29/15 0.22 50.0 1.36 J 1.04 J ND
07/27/15 0.48 50.0 DRY 3.29 J ND
01/26/16 0.48 50.0 DRY 1.33 J ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 6 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Selenium 02/04/13 ---10.0 ND 0.73 J ND
NC 2B = 5 µg/L 07/08/13 ---10.0 ND ND ND
01/21/14 0.77 10.0 ND ND 2.20 J
07/21/14 1.01 10.0 ND 1.43 B 2.88 J
01/29/15 1.01 10.0 ND ND ND
07/27/15 0.85 10.0 DRY ND ND
01/26/16 0.85 10.0 DRY ND ND
Silver 01/29/15 0.17 10.0 ND 0.17 J ND
07/27/15 0.22 10.0 DRY 0.81 J ND
01/26/16 0.22 10.0 DRT ND ND
NC 2B = 0.06 µg/L
Thallium 06/16/97 ---10.0 ND ND ---
No NC 2B Standard 08/14/97 ---10.0 ---ND ---
09/30/97 ---10.0 ---ND ---
04/30/98 ---10.0 ND ND ---
09/15/98 ---10.0 ---ND ---
04/08/99 ---10.0 ND ND ---
09/09/99 ---10.0 ND ND ND
04/13/00 ---10.0 ND ND ND
10/17/00 ---10.0 Dry Dry ND
04/23/01 ---10.0 ND ND ND
10/18/01 ---10.0 ND ND ND
04/29/02 ---10.0 ND ND ND
10/23/02 ---10.0 ND ND ND
04/14/03 ---10.0 ND ND ND
10/30/03 ---10.0 ND ND ND
04/28/04 ---10.0 ND ND ND
10/26/04 ---10.0 ND ND ND
03/16/05 ---10.0 ND ND ND
07/21/05 ---10.0 11.00 Dry ND
01/26/06 ---10.0 ND ND ND
07/21/06 ---10.0 ND ND ND
01/22/07 ---5.50 ND ND ND
07/23/07 ---5.50 Dry ND 0.05 J
01/10/08 ---5.50 ND ND ND
07/21/08 ---5.50 Dry Dry ND
01/29/09 ---5.50 ND ND ND
07/30/09 ------Dry Dry ---
01/14/10 ---5.50 ND ND ND
07/15/10 ---5.50 Dry Dry ND
01/20/11 ---5.50 ND ND ND
07/14/11 ---5.50 Dry ND ND
01/30/12 ---5.50 ND ND ND
07/25/12 ---5.50 Dry Dry ND
02/04/13 ---5.50 ND ND ND
07/08/13 ---5.50 ND ND ND
01/21/14 0.06 5.50 ND ND ND
07/21/14 0.09 5.50 ND ND ND
01/29/15 0.09 5.50 ND ND ND
07/27/15 0.06 5.50 DRY ND ND
01/26/16 0.06 5.50 DRY ND ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 7 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Vanadium 06/16/97 ---40.0 ND ND ---
No NC 2B Standard 08/14/97 ---40.0 ---ND ---
09/30/97 ---20.0 ---ND ---
04/30/98 ---20.0 ND ND ---
09/15/98 ---20.0 ---ND ---
04/08/99 ---20.0 ND ND ---
09/09/99 ---40.0 ND ND ND
04/13/00 ---40.0 ND ND ND
10/17/00 ---40.0 Dry Dry ND
04/23/01 ---40.0 ND ND ND
10/18/01 ---40.0 ND ND ND
04/29/02 ---40.0 ND ND ND
10/23/02 ---40.0 ND ND ND
04/14/03 ---40.0 ND ND ND
10/30/03 ---40.0 ND ND ND
04/28/04 ---40.0 130.00 ND ND
10/26/04 ---40.0 ND ND ND
03/16/05 ---40.0 ND ND ND
07/21/05 ---40.0 ND Dry ND
01/26/06 ---40.0 ND ND ND
07/21/06 ---40.0 ND ND ND
01/22/07 ---25.0 1.70 J ND ND
07/23/07 ---25.0 Dry 1.50 J ND
01/10/08 ---25.0 2.50 J 3.00 J ND
07/21/08 ---25.0 Dry Dry ND
01/29/09 ---25.0 2.48 J 2.56 J ND
07/30/09 ------Dry Dry ---
01/14/10 ---25.0 1.59 J 1.12 J ND
07/15/10 ---25.0 Dry Dry ND
01/20/11 ---25.0 2.13 J ND ND
07/14/11 ---25.0 Dry 5.56 J ND
01/30/12 ---25.0 3.80 J 5.50 J ND
07/25/12 ---25.0 Dry Dry ND
02/04/13 ---25.0 8.56 B 2.08 B 2.12 J
07/08/13 ---25.0 8.09 J 19.50 J ND
01/21/14 1.97 25.0 5.96 B 2.11 B ND
07/21/14 0.93 25.0 16.70 J 5.42 B 1.69 J
01/29/15 0.93 25.0 3.15 J 1.10 J ND
07/27/15 1.57 25.0 DRY 1.95 J ND
01/26/16 1.57 25.0 DRY 3.70 J ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 8 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Zinc 06/16/97 ---50 230 510 ---
NC 2B = 50 µg/L 08/14/97 ---50 ---90.0 ---
09/30/97 ---20 ---60.0 ---
04/30/98 ---20 40.0 70.0 ---
09/15/98 ---20 ---ND ---
04/08/99 ---20 30.0 ND ---
09/09/99 ---50 ND ND 60.0
04/13/00 ---50 ND ND ND
10/17/00 ---50 Dry Dry ND
04/23/01 ---50 ND ND ND
10/18/01 ---50 ND ND ND
04/29/02 ---50 ND 90.0 ND
10/23/02 ---50 ND ND ND
04/14/03 ---50 ND ND ND
10/30/03 ---50 ND 60.0 ND
04/28/04 ---50 70 ND ND
10/26/04 ---50 ND ND ND
03/16/05 ---50 ND ND ND
07/21/05 ---50 ND Dry ND
01/26/06 ---50 ND ND ND
07/21/06 ---50 ND ND ND
01/22/07 ---10 32.2 34.0 ND
07/23/07 ---10.0 Dry 7.10 B 4.00 J
01/10/08 ---10.0 5.7 J 2.80 J ND
07/21/08 ---10.0 Dry Dry ND
01/29/09 ---10.0 9.3 J 9.29 J 5.8 J
07/30/09 ------Dry Dry ---
01/14/10 ---10.0 8.9 J 5.34 J ND
07/15/10 ---10.0 Dry Dry ND
01/20/11 ---10.0 10.3 ND ND
07/14/11 ---10.0 Dry 8.29 J ND
01/30/12 ---10.0 8.9 B 8.17 B 3.00 J
07/25/12 ---10.0 Dry Dry 2.5 J
02/04/13 ---10.0 8.4 3.33 B 0.76 J
07/08/13 ---10.0 9.9 J 23.0 0.96 J
01/21/14 0.87 10.0 8.13 B 7.32 B 2.35 J
07/21/14 0.64 10.0 15.8 14.0 1.93 J
01/29/15 0.64 10.0 10.0 8.96 J 1.54 J
07/27/15 1.3 10.0 DRY 13.8 1.57 J
01/26/16 1.3 10.0 DRY 16.8 1.35 J
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 9 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Iron 07/23/07 ---300 Dry 953 ND
NC 2B = 1000 µg/L 01/10/08 ---300 1540 2280 ND
07/21/08 ---300 Dry Dry ND
01/29/09 ---300 1340 1660 33.80 J
07/30/09 ------Dry Dry ---
01/14/10 ---300 959 1110 ND
07/15/10 ---300 Dry Dry ND
01/20/11 ---300 1320 749 ND
07/14/11 ---300 Dry 2710 ND
01/30/12 ---300 2050 2930 8.11 J
07/25/12 ---40.0 Dry Dry 4.71 J
02/04/13 ---30.0 3950 1710 5.53 J
07/08/13 ---30.0 3300 8660 ND
01/21/14 3.02 30.0 4050 2870 4.96 J
07/21/14 3.1 40.0 7160 2040 ND
01/29/15 3.1 40.0 2250 1670 ND
07/27/15 5.72 40.0 DRY 1240 ND
01/26/16 5.72 40.0 DRY 2290 9.50 J
Manganese 07/23/07 ---50.0 Dry 28.7 J ND
NC 2L = 50 µg/L 01/10/08 ---50.0 20.5 J 25.9 J ND
NC 2B water supply = 200 µg/L 07/21/08 ---50.0 Dry Dry 2.80 J
01/29/09 ---50.0 65.0 B 75.6 13.30 J
07/30/09 ------Dry Dry ---
01/14/10 ---50.0 43.0 J 142 ND
07/15/10 ---50.0 Dry Dry ND
01/20/11 ---50.0 31.5 J 41.5 J ND
07/14/11 ---50.0 Dry 91.4 1.16 J
01/30/12 ---50.0 44.6 32.5 ND
07/25/12 ---10.0 Dry Dry ND
02/04/13 ---50.0 55.4 160 ND
07/08/13 ---50.0 134 215 0.64 J
01/21/14 0.55 50.0 33.4 J 123 ND
07/21/14 0.395 50.0 49.8 J 193 2.27 J
01/29/15 0.395 50.0 75.7 128 1.33 J
07/27/15 1.04 50.0 DRY 381 ND
01/26/16 1.04 50.0 DRY 235 ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 10 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Organic Compounds
Acetone 07/21/05 ---100 ND Dry ND
NC 2B = 2000 µg/L 01/26/06 ---100 ND ND ND
07/21/06 ---100 ND ND ND
01/22/07 ---100 ND ND ND
07/23/07 ---100 Dry ND ND
01/10/08 ---100 ND ND ND
07/21/08 ---100 Dry Dry ND
01/29/09 ---100 ND ND 16.0 J
07/30/09 ---100 Dry Dry ND
01/14/10 ---100 ND 9.2 J ND
07/15/10 ---100 Dry Dry ND
01/20/11 ---100 ND ND ND
07/14/11 ---100 Dry ND ND
01/30/12 ---100 ND ND ND
07/25/12 ---100 Dry Dry ND
02/04/13 ---100 Dry Dry ND
07/08/13 ---100 ND ND ND
01/21/14 1.6 100 ND ND 3.7 J
07/21/14 5.7 100 ND ND ND
01/29/15 5.7 100 ND ND ND
07/27/15 3.1 100 DRY ND ND
01/26/16 4.9 100 DRY ND ND
Carbon Disulfide 06/16/97 ---100 ND ND ---
No NC 2B Standard 08/14/97 ---100 ---ND ---
09/30/97 ---5 ---ND ---
04/30/98 ---5 11.00 73.00 ---
09/15/98 ---5 ---ND ---
04/08/99 ---5 ND ND ---
09/09/99 ---100 ND ND ND
04/13/00 ---100 ND ND ND
10/17/00 ---100 Dry Dry ND
04/23/01 ---100 ND ND ND
10/18/01 ---100 ND ND ND
04/29/02 ---100 ND ND ND
10/23/02 ---100 ND ND ND
04/14/03 ---100 ND ND ND
10/30/03 ---100 ND ND ND
04/28/04 ---100 ND ND ND
10/26/04 ---100 ND ND ND
03/16/05 ---100 ND ND ND
07/21/05 ---100 ND Dry ND
01/26/06 ---100 ND ND ND
07/21/06 ---100 ND ND ND
01/22/07 ---100 ND ND ND
07/23/07 ---100 Dry ND ND
01/10/08 ---100 ND ND ND
07/21/08 ---100 Dry Dry ND
01/29/09 ---100 ND ND ND
07/30/09 ------Dry Dry ---
01/14/10 ---100 ND ND ND
07/15/10 ---100 Dry Dry ND
01/20/11 ---100 ND ND ND
07/14/11 ---100 Dry ND ND
01/30/12 ---100 ND ND ND
07/25/12 ---100 Dry Dry ND
02/04/13 ---100 ND ND 3.90 J
07/08/13 ---100 ND ND ND
01/21/14 1.2 100 ND ND ND
07/21/14 0.8 100 ND ND ND
01/29/15 0.8 100 ND ND ND
07/27/15 0.3 100 DRY ND ND
01/26/16 0.9 100 DRY ND ND
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 11 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Field Parameters
pH 06/16/97 ------6.70 7.05 ---
(S.U.)08/14/97 ---------6.90 ---
09/30/97 ---------7.46 ---
04/30/98 ------7.18 7.10 ---
09/15/98 ---------7.10 ---
04/08/99 ------6.97 7.39 ---
09/09/99 ------8.13 7.86 ---
04/13/00 ------7.50 6.45 ---
10/17/00 ------Dry Dry ---
04/23/01 ------6.79 7.14 ---
10/18/01 ------7.49 7.85 ---
04/29/02 ------7.12 6.87 ---
10/23/02 ------7.78 7.79 ---
04/14/03 ------6.99 7.38 ---
10/30/03 ------7.37 7.14 ---
04/28/04 ------7.48 7.70 ---
10/26/04 ------7.43 6.59 ---
03/16/05 ------6.21 7.55 ---
07/21/05 ------6.15 Dry ---
01/26/06 ------7.34 8.75 ---
07/21/06 ------6.67 7.51 ---
01/22/07 ------6.84 7.84 ---
07/23/07 ------Dry 8.07 ---
01/10/08 ------7.15 7.77 ---
07/21/08 ------Dry Dry ---
01/29/09 ------5.76 6.97 ---
07/30/09 ------Dry Dry ---
01/14/10 ------7.66 7.62 ---
07/15/10 ------Dry Dry ---
01/20/11 ------7.97 7.35 ---
07/14/11 ------Dry 7.23 ---
01/30/12 ------8.11 8.16 ---
07/25/12 ------Dry Dry ---
02/04/13 ------6.42 8.36 ---
07/08/13 ------6.40 7.81 ---
01/21/14 ------6.18 5.18 ---
07/21/14 ---------5.18 ---
01/29/15 FIELD ---8.29 5.18 ---
07/27/15 FIELD ------5.18 ---
09/28/15 FIELD ---DRY 5.18 ---
01/26/16 FIELD ---DRY 5.18 ---
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 12 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Conductivity 06/16/97 ------113 179 ---
(µS/cm)08/14/97 ---------111 ---
09/30/97 ---------74.0 ---
04/30/98 ------5.92 13.0 ---
09/15/98 ---------53.0 ---
04/08/99 ------33.0 54.0 ---
09/09/99 ------25.0 42.0 ---
04/13/00 ------39.0 65.0 ---
10/17/00 ------Dry Dry ---
04/23/01 ------84.0 104 ---
10/18/01 ------101 120 ---
04/29/02 ------58.0 74.0 ---
10/23/02 ------38.0 50.0 ---
04/14/03 ------25.0 29.0 ---
10/30/03 ------42.0 139 ---
04/28/04 ------147 109 ---
10/26/04 ------102 125 ---
03/16/05 ------42.0 66.0 ---
07/21/05 ------166 Dry ---
01/26/06 ------36.0 78.0 ---
07/21/06 ------134 124 ---
01/22/07 ------45.0 101 ---
07/23/07 ------Dry 136 ---
01/10/08 ------136 147 ---
07/21/08 ------Dry Dry ---
01/29/09 ------53.0 80.0 ---
01/30/09 ------Dry Dry ---
01/14/10 ------51.0 106 ---
07/15/10 ------Dry Dry ---
01/20/11 ------60.0 144 ---
07/14/11 ------Dry 170 ---
01/30/12 ------47.0 86.0 ---
07/25/12 ------Dry Dry ---
02/04/13 ------32.3 86.1 ---
07/08/13 ------43.7 72.5 ---
01/21/14 ------40.2 122.7 ---
07/21/14 ---------120.5 ---
01/29/15 FIELD ---45.3 828.0 ---
07/27/15 FIELD ------686 ---
09/28/15 FIELD ---DRY 409.9 ---
01/26/16 FIELD ---DRY 86.3 ---
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 13 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Temperature 06/16/97 ------23.8 26.2 ---
(ºC)08/14/97 ---------23.8 ---
09/30/97 ---------19.3 ---
04/30/98 ------19.4 14.7 ---
09/15/98 ---------22.5 ---
04/08/99 ------23.3 24.0 ---
09/09/99 ------23.6 24.0 ---
04/13/00 ------9.7 11.1 ---
10/17/00 ------Dry Dry ---
04/23/01 ------20.4 21.9 ---
10/18/01 ------7.8 7.0 ---
04/29/02 ------17.3 18.4 ---
10/23/02 ------16.9 17.7 ---
04/14/03 ------18.6 20.6 ---
10/30/03 ------12.2 11.5 ---
04/28/04 ------18.5 13.6 ---
10/26/04 ------15.0 14.3 ---
03/16/05 ------5.74 6.71 ---
07/21/05 ------23.57 Dry ---
01/26/06 ------5.14 7.94 ---
07/21/06 ------22.41 25.91 ---
01/22/07 ------7.40 2.50 ---
07/23/07 ------Dry 20.98 ---
01/10/08 ------9.15 9.59 ---
07/21/08 ------Dry Dry ---
01/29/09 ------6.71 7.53 ---
07/30/09 ------Dry Dry ---
01/14/10 ------2.06 3.52 ---
07/15/10 ------Dry Dry ---
01/20/11 ------4.40 6.29 ---
07/14/11 ------Dry 22.92 ---
01/30/12 ------8.82 8.28 ---
07/25/12 ------Dry Dry ---
02/04/13 ------4.90 3.80 ---
07/08/13 ------26.3 25.4 ---
01/21/14 ------6.50 8.10 ---
07/21/14 ---------23.10 ---
01/29/15 FIELD ---5.20 4.50 ---
07/27/15 FIELD ------24.8
09/28/15 FIELD ---DRY 21.2 ---
01/26/16 FIELD ---DRY 6.7 ---
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 14 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Turbidity 06/16/97 ------570 281 ---
(NTU)08/14/97 ---------NT ---
09/30/97 ---------37.0 ---
04/30/98 ------24.0 24.0 ---
04/08/99 ------16.0 28.0 ---
09/09/99 ------37.0 30.0 ---
04/13/00 ------17.0 13.0 ---
10/17/00 ------Dry Dry ---
04/23/01 ------159 21.0 ---
10/18/01 ------5.0 51.0 ---
04/29/02 ------26.0 7.3 ---
10/23/02 ------13.0 22.0 ---
04/14/03 ------15.0 24.0 ---
10/30/03 ------38.0 289 ---
04/28/04 ------137 15.0 ---
10/26/04 ------24.0 28.0 ---
03/16/05 ------184 116 ---
07/21/05 ------>1000 Dry ---
01/26/06 ------188 166 ---
07/21/06 ------188 0.0 ---
01/22/07 ------50.0 54.6 ---
07/23/07 ------Dry 59.0 ---
01/10/08 ------124 163 ---
07/21/08 ------Dry Dry ---
01/29/09 ------32.4 54.5 ---
07/30/09 ------Dry Dry ---
01/14/10 ------26.9 17.7 ---
07/15/10 ------Dry Dry ---
01/20/11 ------24.70 17.50 ---
07/14/11 ------Dry 64.00 ---
01/30/12 ------20.20 19.86 ---
07/25/12 ------Dry Dry ---
02/04/13 ------34.20 22.30 ---
07/08/13 ------22.70 105 ---
01/21/14 ------3.97 4.23 ---
07/21/14 ---------90.00 ---
01/29/15 FIELD ---20.40 13.30 ---
07/27/15 FIELD ------27.6 ---
09/28/15 FIELD ---DRY 13.4 ---
01/26/16 FIELD ---DRY 17.1 ---
Oxidation Reduction Potential 03/16/05 ------186 22.0 ---
(mV)07/21/05 -------99.0 Dry ---
01/26/06 ------102 -77.0 ---
07/21/06 ------110 100 ---
01/22/07 ------132 -91.0 ---
07/23/07 ------Dry 63.0 ---
01/10/08 ------158.0 85.0 ---
07/21/08 ------Dry Dry ---
01/29/09 ------236.6 157.9 ---
07/30/09 ------Dry Dry ---
01/14/10 ------16.8 3.3 ---
07/15/10 ------Dry Dry ---
01/20/11 ------60.2 37.2 ---
07/14/11 ------Dry 72.5 ---
01/30/12 -------49.8 -22.2 ---
07/25/12 ------Dry Dry ---
02/04/13 ------145.3 78.7 ---
07/08/13 ------77.7 36.6 ---
01/21/14 ------104.8 147.1 ---
07/21/14 ---------51.3 ---
01/29/15 FIELD ---25.0 69.3 ---
07/27/15 FIELD ------70.1 ---
09/28/15 FIELD ---DRY 166.7 ---
01/26/16 FIELD ---DRY 64.1 ---
TABLE 7
Historical Surface Water Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 15 of 15
Joyce Engineering
Analyte
Sample
Collection Date DL SWSL SW-1 SW-2 Blanks
Dissolved Oxygen 03/16/05 ------7.22 6.96 ---
(mg/L)07/21/05 ------7.74 Dry ---
01/26/06 ------5.61 2.98 ---
07/21/06 ------7.52 3.45 ---
01/22/07 ------11.10 9.20 ---
07/23/07 ------Dry 6.80 ---
01/10/08 ------8.69 10.54 ---
07/21/08 ------Dry Dry ---
01/29/09 ------10.16 10.90 ---
07/30/09 ------Dry Dry ---
01/14/10 ------14.29 13.20 ---
07/15/10 ------Dry Dry ---
01/20/11 ------11.75 11.46 ---
07/14/11 ------Dry 6.79 ---
01/30/12 ------11.84 11.96 ---
07/25/12 ------Dry Dry ---
02/04/13 ------13.04 13.57 ---
07/08/13 ------8.19 5.61 ---
01/21/14 ------9.67 12.93 ---
07/21/14 ---------9.04 ---
01/29/15 FIELD ---13.25 14.45 ---
07/27/15 FIELD ------10.96 ---
09/28/15 FIELD ---DRY 4.21 ---
01/26/16 FIELD ---DRY 8.78 ---
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
SWSL = NC-DENR Solid Waste Section Limit.
NC 2B = Surface Water Standard established in 15A NCAC 2B (NC Freshwater Aquatic Life Standards)
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = Insufficient water flow for sampling.
--- = No data.
All inorganic and organic compounds are in µg/L.
mg/L = milligrams per liter
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2B Standards.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 1 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Inorganic Compounds
Total Antimony 01/26/06 30.0 ND ND
07/21/06 30.0 ND ND
01/23/07 6.00 5.79 ND
07/23/07 6.00 9.48 ND
01/10/08 6.00 4.80 J ND
07/21/08 6.00 7.22 ND
01/29/09 6.00 4.82 J ND
07/30/09 6.00 6.38 ND
01/14/10 6.00 20.9 ND
07/15/10 6.00 9.01 J ND
01/20/11 6.00 29.7 ND
07/14/11 6.00 14.4 ND
01/30/12 6.00 53.4 0.33 J
07/25/12 6.00 30.7 ND
02/04/13 6.00 17.7 ND
07/08/13 6.00 18.8 ND
01/21/14 6.00 53.4 ND
07/21/14 6.00 31.6 ND
01/29/15 6.00 43.6 ND
07/27/15 6.00 33.3 ND
01/26/16 6.00 31.3 ND
Total Arsenic 08/04/05 10.0 27.0 ND
01/26/06 10.0 14.0 ND
07/21/06 10.0 16.3 ND
01/23/07 10.0 ND ND
07/23/07 10.0 ND ND
01/10/08 10.0 ND ND
07/21/08 10.0 ND 3.8 J
01/29/09 10.0 ND 4.2 J
07/30/09 10.0 31.8 ND
01/14/10 10.0 15.7 ND
07/15/10 10.0 23.5 ND
01/20/11 10.0 67.3 ND
07/14/11 10.0 76.7 ND
01/30/12 10.0 75.7 ND
07/25/12 10.0 89.8 1.65 J
02/04/13 10.0 42.6 ND
07/08/13 10.0 11.0 ND
01/21/14 10.0 33.8 ND
07/21/14 10.0 82.7 ND
01/29/15 50.0 66.2 ND
07/27/15 10.0 93.6 ND
01/26/16 10.0 70.8 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 2 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Barium 08/04/05 500 ND ND
01/26/06 500 ND ND
07/21/06 500 ND ND
01/23/07 100 152 0.50 J
07/23/07 100 334 0.50 J
01/10/08 100 259 ND
07/21/08 100 275 ND
01/29/09 100 193 0.50 J
07/30/09 100 208 ND
01/14/10 100 145 ND
07/15/10 100 131 ND
01/20/11 100 202 ND
07/14/11 100 202 ND
01/30/12 100 225 0.14 J
07/25/12 100 185 0.79 J
02/04/13 100 398 ND
07/08/13 100 271 ND
01/21/14 100 264 ND
07/21/14 100 178 0.34 J
01/29/15 100 190 1.33 J
07/27/15 100 212 0.41 J
01/26/16 100 216 0.55 J
Total Beryllium 07/08/13 1.00 ND ND
07/21/14 1.00 0.08 J ND
01/29/15 1.00 0.08 J ND
07/27/15 1.00 ND ND
01/26/16 1.00 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 3 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Cadmium 08/04/05 1.00 ND ND
01/26/06 1.00 ND ND
07/21/06 1.00 ND ND
01/23/07 1.00 ND ND
07/23/07 1.00 ND ND
01/10/08 1.00 ND ND
07/21/08 1.00 ND ND
01/29/09 1.00 ND ND
07/30/09 1.00 0.17 J ND
01/14/10 1.00 ND ND
07/15/10 1.00 ND ND
01/20/11 1.00 ND ND
07/14/11 1.00 ND ND
01/30/12 1.00 ND ND
07/25/12 1.00 ND ND
02/04/13 1.00 ND ND
07/08/13 1.00 ND ND
01/21/14 1.00 0.06 J ND
07/21/14 1.00 ND ND
01/29/15 1.00 ND 0.06 J
07/27/15 1.00 ND ND
01/26/16 1.00 ND ND
Total Chromium 08/04/05 10.0 ND ND
01/26/06 10.0 ND ND
07/21/06 10.0 ND ND
01/23/07 10.0 ND ND
07/23/07 10.0 ND ND
01/10/08 10.0 ND ND
07/21/08 10.0 6.9 J ND
01/29/09 10.0 ND ND
07/30/09 10.0 67.0 ND
01/14/10 10.0 35.8 ND
07/15/10 10.0 54.0 ND
01/20/11 10.0 93.5 ND
07/14/11 10.0 97.6 ND
01/30/12 10.0 73.8 1.16 J
07/25/12 10.0 65.8 ND
02/04/13 10.0 38.1 2.66 J
07/08/13 10.0 49.6 ND
01/21/14 10.0 56.4 ND
07/21/14 10.0 91.3 1.40 J
01/29/15 10.0 98.8 ND
07/27/15 10.0 156 ND
01/26/16 10.0 142 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 4 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Cobalt 08/04/05 10.0 23.0 ND
01/26/06 10.0 14.0 ND
07/21/06 10.0 13.6 ND
01/23/07 10.0 11.9 ND
07/23/07 10.0 34.0 J ND
01/10/08 10.0 15.7 ND
07/21/08 10.0 24.5 ND
01/29/09 10.0 18.2 ND
07/30/09 10.0 26.6 ND
01/14/10 10.0 13.2 ND
07/15/10 10.0 14.8 ND
01/20/11 10.0 27.3 ND
07/14/11 10.0 30.0 ND
01/30/12 10.0 23.9 ND
07/25/12 10.0 19.6 ND
02/04/13 10.0 16.1 ND
07/08/13 10.0 16.9 ND
01/21/14 10.0 26.0 ND
07/21/14 10.0 37.0 ND
01/29/15 10.0 28.5 ND
07/27/15 10.0 45.8 ND
01/26/16 10.0 33.3 ND
Total Copper 01/30/12 10.0 8.23 J ND
07/25/12 10.0 13.10 0.36 J
02/04/13 10.0 8.57 J 0.19 J
07/08/13 10.0 7.54 J ND
01/21/14 10.0 6.99 J ND
07/21/14 10.0 15.0 0.44 J
01/29/15 10.0 9.4 B 4.34 J
07/27/15 10.0 1.2 B 1.24 J
01/26/16 10.0 8.6 J 3.93 J
Total Iron 01/26/16 40.0 ---9.50 J
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 5 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Lead 08/04/05 10.0 ND ND
01/26/06 10.0 ND ND
07/21/06 10.0 ND ND
01/23/07 10.0 2.40 J ND
07/23/07 10.0 ND ND
01/10/08 10.0 ND ND
07/21/08 10.0 ND ND
01/29/09 10.0 ND ND
07/30/09 10.0 2.03 J ND
01/14/10 10.0 2.54 J ND
07/15/10 10.0 ND ND
01/20/11 10.0 ND ND
01/30/12 10.0 0.97 J ND
07/25/12 10.0 1.36 J 0.29 J
02/04/13 10.0 0.51 J ND
07/08/13 10.0 0.83 J ND
01/21/14 10.0 1.32 J ND
07/21/14 10.0 0.44 J ND
01/29/15 10.0 3.34 J ND
07/27/15 10.0 0.89 J ND
01/26/16 10.0 1.46 J ND
Total Nickel 03/17/05 50.0 76.0 ---
08/04/05 50.0 160 ND
01/26/06 50.0 122 ND
07/21/06 50.0 111 ND
01/23/07 50.0 90.9 ND
07/23/07 50.0 249 ND
01/10/08 50.0 103 ND
07/21/08 50.0 178 ND
01/29/09 50.0 119 ND
07/30/09 50.0 162 ND
01/14/10 50.0 76.3 ND
07/15/10 50.0 97.7 ND
01/20/11 50.0 164 ND
07/14/11 50.0 179 ND
01/30/12 50.0 131 ND
07/25/12 50.0 107 ND
02/04/13 50.0 73.2 ND
07/08/13 50.0 101 ND
01/21/14 50.0 102 ND
07/21/14 50.0 181 ND
01/29/15 50.0 156 ND
07/27/15 50.0 215 ND
01/26/16 50.0 164 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 6 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Selenium 01/30/12 10.0 7.46 J ND
07/25/12 10.0 5.64 J ND
02/04/13 10.0 2.78 J ND
07/08/13 10.0 1.76 J ND
01/21/14 10.0 ND 2.20 J
07/21/14 10.0 8.25 J 2.88 J
01/29/15 10.0 7.65 J ND
07/27/15 10.0 5.58 J ND
01/26/16 10.0 5.94 J ND
Total Silver 08/04/05 10.0 ND ND
01/26/06 10.0 ND ND
07/21/06 10.0 ND ND
01/23/07 10.0 ND ND
07/23/07 10.0 ND ND
01/10/08 10.0 ND ND
07/21/08 10.0 ND ND
01/29/09 10.0 ND ND
07/30/09 10.0 ND ND
01/14/10 10.0 0.81 J ND
07/15/10 10.0 ND ND
01/20/11 10.0 ND ND
07/14/11 10.0 3.28 J ND
01/30/12 10.0 0.88 J ND
07/25/12 10.0 0.79 J ND
02/04/13 10.0 0.40 J ND
07/08/13 10.0 0.53 J ND
01/21/14 10.0 0.38 J ND
07/21/14 10.0 1.08 J ND
01/29/15 10.0 0.72 J ND
07/27/15 10.0 0.82 J ND
01/26/16 10.0 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 7 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Thallium 08/04/05 10.0 ND ND
01/26/06 10.0 ND ND
07/21/06 10.0 ND ND
01/23/07 5.50 ND ND
07/23/07 5.50 ND ND
01/10/08 5.50 ND ND
07/21/08 5.50 ND ND
01/29/09 5.50 ND ND
07/30/09 5.50 ND ND
01/14/10 5.50 ND ND
07/15/10 5.50 1.22 J ND
01/20/11 5.50 ND ND
07/14/11 5.50 ND ND
01/30/12 5.50 ND ND
07/25/12 5.50 ND ND
02/04/13 5.50 ND ND
07/08/13 6.00 ND ND
01/21/14 5.50 ND ND
07/21/14 5.50 ND ND
01/29/15 5.50 ND ND
07/27/15 5.50 0.22 J ND
01/26/16 5.50 ND ND
Total Vanadium 08/04/05 40.0 55.00 ND
01/26/06 40.0 ND ND
07/21/06 40.0 ND ND
01/23/07 25.0 ND ND
07/23/07 25.0 55.50 ND
01/10/08 25.0 ND ND
07/21/08 25.0 26.30 ND
01/29/09 25.0 5.90 J ND
07/30/09 25.0 54.20 ND
01/14/10 25.0 21.30 J ND
07/15/10 25.0 39.20 ND
01/20/11 25.0 60.60 ND
07/14/11 25.0 61.1 ND
01/30/12 25.0 51.6 ND
07/25/12 25.0 47.8 ND
02/04/13 25.0 30.7 2.12 J
07/08/13 25.0 31.6 ND
01/21/14 25.0 41.9 14.6 J
07/21/14 25.0 58.3 1.69 J
01/29/15 25.0 53.1 ND
07/27/15 25.0 94.9 ND
01/26/16 25.0 67.3 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 8 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Total Zinc 08/04/05 50.0 ND ND
01/26/06 50.0 ND ND
07/21/06 50.0 ND ND
01/23/07 10.0 26.9 1.50 J
07/23/07 10.0 43.0 J 4.00 J
01/10/08 10.0 11.4 ND
07/21/08 10.0 11.4 ND
01/29/09 10.0 17.5 B 5.82 J
07/30/09 10.0 13.2 ND
01/14/10 10.0 28.1 ND
07/15/10 10.0 7.55 J ND
01/20/11 10.0 22.6 ND
07/14/11 10.0 27.2 ND
01/30/12 10.0 17.2 3.00 J
07/25/12 10.0 32.6 2.48 J
02/04/13 10.0 40.4 0.76 J
07/08/13 10.0 17.0 0.96 J
01/21/14 10.0 472 2.35 J
07/21/14 10.0 88.5 1.93 J
01/29/15 10.0 107 3.61 J
07/27/15 10.0 58.4 1.57 J
01/26/16 10.0 97.8 1.35 J
Total Mercury 01/29/15 0.50 ND ND
07/27/15 0.20 0.09 J ND
01/26/16 1.33 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 9 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Organic Compounds
Acetone 08/04/05 100 ND ND
01/26/06 25 ND ND
07/21/06 100 329 ND
01/23/07 100 440 ND
07/23/07 100 74 ND
01/10/08 100 2800 ND
07/21/08 100 ND ND
01/29/09 100 71 B 16.0 J
07/30/09 100 ND ND
01/14/10 100 5800 ND
07/15/10 100 ND ND
01/20/11 100 9900 ND
07/14/11 100 77.0 J ND
01/30/12 100 5600 D ND
07/25/12 1000 1400 ND
02/04/13 2500 4100 D ND
07/08/13 100 47.0 J ND
01/21/14 5000 6200 3.7 J
07/21/14 100 8.7 J ND
01/29/15 100 830 ND
07/27/15 100 21.0 J ND
01/26/16 100 100 ND
Benzene 08/04/05 5.0 ND ND
01/26/06 5.0 ND ND
07/21/06 5.0 ND ND
01/23/07 3.0 2.6 ND
07/23/07 1.0 3.8 J ND
01/10/08 1.0 ND ND
07/21/08 1.0 ND ND
01/29/09 1.0 4.6 J ND
07/30/09 1.0 4.1 J 4.1 J
01/14/10 1.0 ND ND
07/15/10 1.0 6.4 ND
01/20/11 1.0 ND ND
07/14/11 1.0 ND ND
01/30/12 1.0 4.7 ND
07/25/12 1.0 ND ND
02/04/13 1.0 5.8 ND
07/08/13 1.0 4.7 ND
01/21/14 1.0 2.8 ND
07/21/14 1.0 2.9 ND
01/29/15 1.0 5.5 ND
07/27/15 1.0 3.9 ND
01/26/16 1.0 2.6 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 10 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Chloroform 01/29/15 5.0 0.300 J ND
07/27/15 5.0 ND ND
01/26/16 5.0 ND ND
1,2-Dibromoethane 01/29/15 1.0 0.400 J ND
07/27/15 1.0 ND ND
01/26/16 1.0 ND ND
Carbon Disulfide 08/04/05 100 ND ND
01/26/06 25 ND ND
07/21/06 100 ND ND
01/23/07 100 1.40 J ND
07/23/07 100 ND ND
01/10/08 100 ND ND
07/21/08 100 ND ND
01/29/09 100 ND ND
07/30/09 100 ND ND
01/14/10 100 ND ND
07/15/10 100 ND ND
01/20/11 100 ND ND
07/14/11 100 ND ND
01/30/12 100 11.0 J ND
07/25/12 100 1.80 J 3.90
02/04/13 100 ND 3.90 J
07/08/13 100 ND ND
01/21/14 100 10 ND
07/21/14 100 0.50 J ND
01/29/15 100 1.50 J ND
07/27/15 100 0.80 J ND
01/26/16 100 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 11 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Chlorobenzene 01/30/12 3.0 0.70 J ND
07/25/12 3.0 0.50 B 0.40 J
02/04/13 3.0 0.70 J ND
07/08/13 3.0 0.80 J ND
01/21/14 3.0 ND ND
07/21/14 3.0 0.60 J ND
01/29/15 3.0 1.50 J ND
07/27/15 3.0 0.50 J ND
01/26/16 3.0 0.70 J ND
Chloroethane 02/04/13 10 0.7 J ND
07/08/13 10 ND ND
01/21/14 10 0.6 ND
07/21/14 10 ND ND
01/29/15 10 ND ND
07/27/15 10 ND ND
01/26/16 10 ND ND
Chloromethane 01/30/12 1.0 0.5 J ND
07/25/12 1.0 ND 0.1 J
02/04/13 1.0 ND 0.1 J
07/08/13 1.0 ND ND
01/21/14 1.0 0.5 ND
07/21/14 1.0 ND ND
01/29/15 1.0 ND ND
07/27/15 1.0 ND ND
01/26/16 1.0 ND ND
1,2-Dichlorobenzene 01/29/15 5.0 0.70 J ND
07/27/15 5.0 ND ND
01/26/16 5.0 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 12 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
1,4-Dichlorobenzene 08/04/05 5.0 ND ND
01/26/06 5.0 5.0 ND
07/21/06 5.0 5.7 ND
01/23/07 3.0 5.6 ND
07/23/07 1.0 4.8 J ND
01/10/08 1.0 ND ND
07/21/08 1.0 4.1 J ND
01/29/09 1.0 9.5 J ND
07/30/09 1.0 6.6 6.6
01/14/10 1.0 ND ND
07/15/10 1.0 9.8 ND
01/20/11 1.0 ND ND
07/14/11 1.0 ND ND
01/30/12 1.0 8.6 ND
07/25/12 1.0 4.1 ND
02/04/13 1.0 7.2 ND
07/08/13 1.0 ND ND
01/21/14 1.0 2.2 ND
07/21/14 1.0 4.4 ND
01/29/15 1.0 9.8 ND
07/27/15 1.0 5.6 ND
01/26/16 1.0 7.2 ND
1,1-Dichloroethane 01/30/12 5.0 0.30 J ND
07/25/12 5.0 ND ND
02/04/13 5.0 0.80 J ND
07/08/13 5.0 ND ND
01/21/14 5.0 ND ND
07/21/14 5.0 ND ND
01/29/15 5.0 0.40 J ND
07/27/15 5.0 ND ND
01/26/16 5.0 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 13 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
1,2-Dichloroethane 08/04/05 5.0 ND ND
01/26/06 5.0 ND ND
07/21/06 5.0 ND ND
01/23/07 3.0 1.3 J ND
07/23/07 1.0 ND ND
01/10/08 1.0 ND ND
07/21/08 1.0 ND ND
01/29/09 1.0 ND ND
07/30/09 1.0 ND ND
01/14/10 1.0 ND ND
07/15/10 1.0 ND ND
01/20/11 1.0 ND ND
07/14/11 1.0 ND ND
01/30/12 1.0 1.0 ND
07/25/12 1.0 ND ND
02/04/13 1.0 5.8 ND
07/08/13 1.0 ND ND
01/21/14 1.0 3.3 ND
07/21/14 1.0 ND ND
01/29/15 1.0 0.8 J ND
07/27/15 1.0 0.3 J ND
01/26/16 1.0 0.3 J ND
cis-1,2-Dichloroethene 02/04/13 5.0 2.8 J ND
07/08/13 5.0 ND ND
01/21/14 5.0 ND ND
07/21/14 5.0 ND ND
01/29/15 5.0 ND ND
07/27/15 5.0 ND ND
01/26/16 5.0 ND ND
Trans-1,2-Dichloroethene 02/04/13 5.0 1.8 J ND
07/08/13 5.0 ND ND
01/21/14 5.0 ND ND
07/21/14 5.0 ND ND
01/29/15 5.0 0.30 J ND
07/27/15 5.0 ND ND
01/26/16 5.0 ND ND
1,2-Dichloropropane 01/29/15 1.0 0.500 J ND
07/27/15 1.0 ND ND
01/26/16 1.0 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 14 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Ethylbenzene 08/04/05 5.0 ND ND
01/26/06 5.0 ND ND
07/21/06 5.0 12.9 ND
01/23/07 5.0 3.8 ND
07/23/07 1.0 2.5 J ND
01/10/08 1.0 28 ND
07/21/08 1.0 7.4 J ND
01/29/09 1.0 ND ND
07/30/09 1.0 5.8 5.8
01/14/10 1.0 42 J ND
07/15/10 1.0 25 ND
01/20/11 1.0 ND ND
07/14/11 1.0 9.6 ND
01/30/12 1.0 9.0 ND
07/25/12 1.0 4.9 ND
02/04/13 1.0 20 ND
07/08/13 1.0 ND ND
01/21/14 1.0 5.3 ND
07/21/14 1.0 7.9 ND
01/29/15 1.0 16.0 ND
07/27/15 1.0 7.4 ND
01/26/16 1.0 2.2 ND
Methylene Chloride 08/04/05 10 ND ND
01/26/06 10 25.0 ND
07/21/06 10 ND ND
01/23/07 5.5 ND ND
07/23/07 1.0 ND ND
01/10/08 1.0 9.0 J ND
07/21/08 1.0 ND ND
01/29/09 1.0 ND ND
07/30/09 1.0 ND ND
01/14/10 1.0 ND ND
07/15/10 1.0 ND ND
01/20/11 1.0 ND ND
07/14/11 1.0 ND ND
01/30/12 1.0 ND ND
07/25/12 1.0 ND 0.5 J
02/04/13 1.0 6.5 ND
07/08/13 1.0 ND ND
01/21/14 1.0 2.6 ND
07/21/14 1.0 ND ND
01/29/15 1.0 ND ND
07/27/15 1.0 1.1 ND
01/26/16 1.0 0.70 J 0.90 J
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 15 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Methyl Butyl Ketone (2-Hexanone)07/25/12 50 3.6 J ND
02/04/13 50 16 J ND
07/08/13 50 ND ND
01/21/14 50 13 ND
07/21/14 50 ND ND
01/29/15 50 7 J ND
07/27/15 50 6.4 J ND
01/26/16 50 3.1 J ND
Methyl Ethyl Ketone (2-Butanone)08/04/05 100 ND ND
01/26/06 25 255 ND
07/21/06 100 478 ND
01/23/07 100 440 ND
07/23/07 100 ND ND
01/10/08 100 4800 ND
07/21/08 100 ND ND
01/29/09 100 ND ND
07/30/09 100 ND ND
01/14/10 100 4800 ND
07/15/10 100 ND ND
01/20/11 100 6200 ND
07/14/11 100 ND ND
01/30/12 100 4800 D ND
07/25/12 1000 1500 ND
02/04/13 2500 3500 ND
07/08/13 200 ND ND
01/21/14 5000 8400 2.70 J
07/21/14 100 ND 1.10 J
01/29/15 100 1200 ND
07/27/15 100 ND ND
01/26/16 100 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 16 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
4-Methyl-2-pentanone (MIBK)08/04/05 100 ND ND
01/26/06 25 25 ND
07/21/06 100 ND ND
01/23/07 100 16 ND
07/23/07 100 ND ND
01/10/08 100 56 J ND
07/21/08 100 ND ND
01/29/09 100 ND ND
07/30/09 100 13 J 13 J
01/14/10 100 350 ND
07/15/10 100 ND ND
01/20/11 100 ND ND
07/14/11 100 37 J ND
01/30/12 100 82 J ND
07/25/12 100 22 ND
02/04/13 100 100 12 J
07/08/13 100 ND ND
01/21/14 100 36 ND
07/21/14 100 15 J ND
01/29/15 100 57 J ND
07/27/15 100 15 J ND
01/26/16 100 25 J ND
Styrene 02/04/13 1.0 2.30 ND
07/08/13 1.0 ND ND
01/21/14 1.0 ND ND
07/21/14 1.0 ND ND
01/29/15 1.0 2.20 ND
07/27/15 1.0 2.6 ND
01/26/16 1.0 2.5 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 17 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Toluene 08/04/05 5.0 ND ND
01/26/06 5.0 11.0 ND
07/21/06 5.0 23.2 ND
01/23/07 5.0 6.4 ND
07/23/07 1.0 3.0 B 0.60 J
01/10/08 1.0 52 ND
07/21/08 1.0 6.8 J ND
01/29/09 1.0 ND ND
07/30/09 1.0 3.6 J 3.60 J
01/14/10 1.0 46 J ND
07/15/10 1.0 11.0 ND
01/20/11 1.0 ND ND
07/14/11 1.0 ND ND
01/30/12 1.0 9.6 ND
07/25/12 1.0 2.0 ND
02/04/13 1.0 46 ND
07/08/13 1.0 44 ND
01/21/14 1.0 29 ND
07/21/14 1.0 8.2 ND
01/29/15 1.0 19.0 ND
07/27/15 1.0 5.3 ND
01/26/16 1.0 5.8 ND
Tetrachloroethene 01/29/15 1.0 0.400 J ND
07/27/15 1.0 ND ND
01/26/16 1.0 ND ND
Trichloroethene 02/04/13 1.0 1.0 J ND
07/08/13 1.0 ND ND
01/21/14 1.0 ND ND
07/21/14 1.0 ND ND
01/29/15 1.0 ND ND
07/27/15 1.0 ND ND
01/26/16 1.0 ND ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 18 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Vinyl chloride 08/04/05 10.0 ND ND
01/26/06 5.0 ND ND
07/21/06 10.0 ND ND
01/23/07 5.5 0.68 J ND
07/23/07 1.0 ND ND
01/10/08 1.0 ND ND
07/21/08 1.0 ND ND
01/29/09 1.0 ND ND
07/30/09 1.0 ND ND
01/14/10 1.0 ND ND
07/15/10 1.0 ND ND
01/20/11 1.0 ND ND
07/14/11 1.0 ND ND
01/30/12 1.0 0.60 J ND
07/25/12 1.0 ND ND
02/04/13 1.0 1.10 ND
07/08/13 1.0 1.20 ND
01/21/14 1.0 0.4 ND
07/21/14 1.0 ND ND
01/29/15 1.0 0.8 J ND
07/27/15 1.0 ND ND
01/26/16 1.0 ND ND
Xylenes, total 08/04/05 5.0 22 ND
01/26/06 5.0 16 ND
07/21/06 5.0 54 ND
01/23/07 ---25 ND
07/23/07 4.0 32 ND
01/10/08 5.0 68 ND
07/21/08 5.0 35 ND
01/29/09 5.0 24 ND
07/30/09 5.0 47 47.0
01/14/10 5.0 90 ND
07/15/10 5.0 70 ND
01/20/11 5.0 44 ND
07/14/11 5.0 28 ND
01/30/12 5.0 33 ND
07/25/12 5.0 28 ND
02/04/13 5.0 68 ND
07/08/13 5.0 41 ND
01/21/14 5.0 11 ND
07/21/14 5.0 24 ND
01/29/15 5.0 50 ND
07/27/15 5.0 33 ND
01/26/16 5.0 20 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 19 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Additional Parameters
Cyanide, Total 01/14/10 10.0 ND ND
07/15/10 0.01 ND ND
01/20/11 0.01 0.01 J ND
07/14/11 0.01 ND ND
01/30/12 20.0 ND ND
07/25/12 10.0 ND ND
02/04/13 10.0 ND 2.0 J
07/08/13 50.0 ND ND
01/21/14 50.0 ND ND
07/21/14 50.0 ND ---
01/29/15 10.0 ND ND
07/27/15 10.0 ND ND
01/26/16 50.0 ND ND
Nitrate as N 03/17/05 0.10 ND ---
08/04/05 0.10 ND ND
01/26/06 0.05 ND ND
07/24/06 0.05 ND ND
01/23/07 ---0.26 ND
06/12/07 ---ND ND
07/23/07 ---0.05 J ND
01/10/08 10.0 0.03 J ND
07/21/08 10.0 ND -
01/29/09 10.0 0.04 J ND
07/30/09 10.0 ND ND
01/14/10 10.0 0.02 J ---
07/15/10 10.0 0.06 J -
01/20/11 10.0 ND ND
07/14/11 10.0 0.12 J ND
01/30/12 50.0 19.0 J ND
07/25/12 50.0 ND ND
02/04/13 250 ND ND
07/08/13 50.0 ND ND
01/21/14 100 ND ND
07/21/14 50 ND ---
02/25/15 100 ND ND
07/27/15 500 ND ND
01/26/16 50 760 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 20 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Nitrite as N 07/23/07 ---0.02 J ND
01/10/08 1.0 0.02 J ND
07/21/08 1.0 0.04 B 0.01 J
01/29/09 1.0 ND ND
07/30/09 1.0 0.02 B 0.01 J
01/14/10 1.0 0.01 J ND
07/15/10 1.0 0.03 J 0.01 J
01/20/11 1.0 0.02 J ND
07/14/11 1.0 0.04 J ND
01/30/12 50.0 190 ND
07/25/12 50.0 ND ND
02/04/13 250 ND ND
07/08/13 50.0 ND ND
01/21/14 100 550 ND
07/21/14 50 ND ---
02/25/15 100 ND ND
07/27/15 500 ND ND
01/26/16 50 1400 ND
Sulfate 03/17/05 2.0 23.0 ---
08/04/05 2.0 13.2 ND
01/26/06 2.0 5.2 ---
07/21/06 0.30 10.6 ND
01/23/07 ---25.0 2.25 J
07/23/07 ---26.0 J ND
01/10/08 250 3.0 J ND
07/21/08 250 3.9 J ND
01/29/09 250 6.8 J ND
07/30/09 250 6.9 J ND
01/14/10 250 4.1 J ND
07/15/10 250 2.0 J ND
01/20/11 250 7.9 J ND
07/14/11 250 2.8 J ND
01/30/12 5000 650 J ND
07/25/12 5000 ND ND
02/04/13 10000 ND ND
07/08/13 10000 ND ND
01/21/14 10000 38000 ND
07/21/14 5000 ND ---
01/29/15 250000 ND ND
07/27/15 5000 ND ND
01/26/16 5000 23000 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 21 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Biochemical Oxygen Demand 03/17/05 2.0 40.0 ---
08/04/05 2.0 55.1 ND
01/26/06 2.0 68.0 ---
07/24/06 2.0 50.0 ND
01/23/07 ---44.0 ND
06/12/07 ---53.0 ND
07/23/07 ---100 ND
01/10/08 ---280 ND
04/17/08 ---66.0 ND
07/21/08 ---72.0 ND
01/29/09 ---ND ND
07/30/09 ---70.0 ND
01/14/10 ---210 ND
07/15/10 ---48.0 ND
01/20/11 ---180.0 ND
07/14/11 ---75.0 ND
01/30/12 31000 246000 ND
07/25/12 24000 98000 ND
02/04/13 13.0 322 ND
07/08/13 16000 97000 20.0 J
01/21/14 69000 69000 ND
07/21/14 23000 45000 10.0
02/25/15 30000 122000 180 J
07/27/15 32000 97000 D ND
01/26/16 33000 103000 D ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 22 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Chemical Oxygen Demand 03/17/05 10 560 ---
08/04/05 10 1030 ND
01/26/06 10 866 ---
07/21/06 10 ND ND
01/23/07 ---708 ND
07/23/07 ---1600 ND
01/10/08 ---1000 ND
07/21/08 ---1200 ND
01/29/09 ---860 ND
07/30/09 ---1200 ND
01/14/10 ---1200 ND
07/15/10 ---1300 ND
01/20/11 ---1600 ND
07/14/11 ---1500 ND
01/30/12 100000 1970000 ND
07/25/12 100000 1510000 ND
02/04/13 100 1370000 6280 J
07/08/13 200 1180000 7700 J
01/21/14 100 4680000 ND
07/21/14 200 1400000 ---
01/29/15 50 1580000 ND
07/27/15 100000 1860000 ND
01/26/16 50000 1930000 ---
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 23 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Phosphorus-Total 03/17/05 0.03 1.8 ---
08/04/05 0.03 2.1 ND
01/26/06 0.03 4.0 ---
07/21/06 0.03 2.0 ND
01/23/07 ---4.3 ND
07/23/07 ---10.0 ND
01/10/08 ---5.8 ND
07/21/08 ---9.2 ND
01/29/09 ---9.7 ND
07/30/09 ---12.0 ND
01/14/10 ---11.0 ND
07/15/10 ---14.0 ND
01/20/11 ---15.0 ND
07/14/11 ---19.0 ND
01/30/12 500 15800 ND
07/25/12 555 13000 ND
02/04/13 0.22 7510 ND
07/08/13 2.00 7000 ND
01/21/14 2.00 6800 ND
07/21/14 2000 18900 ---
01/29/15 222 10500 D ---
07/27/15 0 8270 D ND
01/26/16 222 3360 D ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 24 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Nitrate/Nitrite as N 07/23/07 ---0.07 B 0.02 J
01/10/08 ---0.05 J ND
07/21/08 ---ND ND
01/29/09 ---0.04 J ND
07/30/09 ---ND ND
01/14/10 ---0.03 B 0.03
07/15/10 ---0.08 J ND
01/20/11 ---ND ND
07/14/11 ---0.16 ND
01/30/12 50.0 190 J ND
07/25/12 50.0 ND ND
02/04/13 250 ND ND
07/08/13 50.0 ND ND
01/21/14 100 600 ND
07/21/14 50 ND ---
02/25/15 100 ND ---
07/27/15 500 ND ND
01/26/16 50 2200 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 25 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Diesel Range Organics 01/26/16 2800 ND
Gasoline Range Organics 01/26/16 1000 ND
BTEX. total 01/26/16 30 ND
Ammonia as N 06/12/07 ---470 ---
07/23/07 ---940 ---
01/10/08 ---440 ND
04/17/08 ---280 ND
07/21/08 ---640 0.01
01/29/09 ---500 ND
07/30/09 ---710 ND
01/14/10 ---460 ND
07/15/10 ---760 ND
01/20/11 ---760 ND
07/14/11 ---870 ND
01/30/12 10000.00 640000 ND
07/25/12 20.00 810000 ND
02/04/13 10.00 325000 ND
07/08/13 20.00 608000 ND
01/21/14 10 408000 ND
07/21/14 10000 1180000 ---
01/29/15 10 853000 ---
07/27/15 10 559000 ND
01/26/16 5000 645000 ND
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 26 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Field Parameters
pH 03/17/05 ---6.95 ---
(S.U.)08/04/05 ---7.91 ---
01/26/06 ---3.50 ---
07/21/06 ---7.43 ---
01/23/07 ---7.53 ---
07/23/07 ---8.19 ---
01/10/08 ---7.30 ---
07/21/08 ---7.77 ---
01/29/09 ---7.28 ---
07/30/09 ---7.43 ---
01/14/10 ---6.77 ---
07/15/10 ---7.64 ---
01/20/11 ---7.62 ---
07/14/11 ---7.68 ---
01/30/12 ---7.20 ---
07/25/12 ---7.94 ---
02/04/13 ---7.34 ---
07/08/13 ---7.80 ---
01/21/14 ---6.06 ---
07/21/14 ---7.91 ---
01/29/15 FIELD 7.25 ---
07/27/15 FIELD 7.84 ---
01/26/16 FIELD 7.84 ---
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 27 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Conductivity 03/17/05 ---3240 ---
(µS/cm)08/04/05 ---1078 ---
01/26/06 ---3680 ---
07/21/06 ---7460 ---
01/23/07 ---4860 ---
07/23/07 ---16000 ---
01/10/08 ---7140 ---
07/21/08 ---9000 ---
01/29/09 ---9500 ---
07/30/09 ---12720 ---
01/14/10 ---8756 ---
07/15/10 ---11840 ---
01/20/11 ---12180 ---
07/14/11 ---13250 ---
01/30/12 ---10950 ---
04/19/12 ---8460 ---
07/25/12 ---9019 ---
02/04/13 ---4678 ---
07/08/13 ---9232 ---
01/21/14 ---5917 ---
07/21/14 ---15103 ---
01/29/15 FIELD 834 ---
07/27/15 FIELD 17437 ---
01/26/16 FIELD 9638 ---
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 28 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Temperature 03/17/05 ---2.64 ---
(°C)08/04/05 ---26.70 ---
01/26/06 ---8.87 ---
07/21/06 ---29.69 ---
01/23/07 ---7.76 ---
07/23/07 ---28.19 ---
01/10/08 ---12.40 ---
07/21/08 ---34.28 ---
01/29/09 ---9.33 ---
07/30/09 ---31.69 ---
01/14/10 ---7.25 ---
07/15/10 ---29.77 ---
01/20/11 ---7.31 ---
07/14/11 ---27.90 ---
01/30/12 ---12.10 ---
04/19/12 ---18.80 ---
07/25/12 ---28.20 ---
02/04/13 ---11.00 ---
07/08/13 ---31.00 ---
01/21/14 ---6.90 ---
07/21/14 ---25.60 ---
01/29/15 FIELD 8.20 ---
07/27/15 FIELD 28.41 ---
01/26/16 FIELD 7.70
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 29 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Turbidity 03/17/05 ---56.7 ---
(NTU)08/04/05 ---------
01/26/06 ---302 ---
07/21/06 ---6.70 ---
01/23/07 ---203 ---
07/23/07 ---60.9 ---
01/10/08 ---403 ---
07/21/08 ---164 ---
07/30/09 ---670 ---
01/14/10 ---------
07/15/10 ---------
07/14/11 ---------
01/30/12 ---9.04 ---
04/19/12 ---38.6 ---
07/25/12 ---462 ---
02/04/13 ---1000 ---
07/08/13 --->1000 ---
01/21/14 --->1000 ---
07/21/14 --->1000 ---
01/29/15 FIELD >1000 ---
07/27/15 FIELD >1000 ---
01/26/16 FIELD >1000 ---
TABLE 8
Historical Leachate Constituents/Analytes
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Upper Piedmont Regional Landfill
Permit No. 73-04 Page 30 of 30
Joyce Engineering
Analyte
Sample Collection
Date SWSL Leachate Blanks
Dissolved Oxygen 01/29/15 FIELD 5.73 ---
07/27/15 FIELD 0.54 ---
01/26/16 FIELD 2.44 ---
Oxidation Reduction Potential 01/29/15 FIELD 61.2 ---
07/27/15 FIELD -100.1 ---
01/26/16 FIELD 73.4 ---
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
PQL = Practical Quantitation Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC 2L = Groundwater Standard established in 15 A NCAC 2L.0202
GWPS = NC DENR Solid Waste Section Groundwater Protection Standard for constituents with no listed NC 2L.
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = insufficient water to sample.
--- = No data.
All inorganic and organic compounds are reported in µg/L
Prior to 2012 all "Additional Parameters" were reported in mg/L; beginning with the 1/21/12 event they are reported in µg/L.
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2L or Groundwater Protection standards (GWPS) have been bolded.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
R = Anomalous data.
*8260B analysis diluted by a factor of 10x for the July 2011 event.
*6020A analysis for Antimony and Thallium diluted by a factor of 10x for the July 2011 event.
*Acetone & MEK DF 50x; C.O.D. DF 10x for the January 2012 event.
Phosphorous, total DF 1.11x for Jan. & July 2012 events.
The 1/29/15 samples for BOD, nitrate, & nitrite arrived at the lab. out of hold, so they were resampled on 2/25/15.

Appendix B

Field Sampling Logs
J
O
Y
C
E
E
t
\
J
G
I
t
J
E
S
R
I
P
\
J
G
D
A
T
E
:
1
/
2
6
/
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Appendix C

Laboratory Analytical Report
ASI ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: Upper Piedmont Regional Landfill
Conover, NC 28613
1220 Commerce Street, SW
Mr. Matt Einsmann
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Analytical Services, Inc. certifies that the
following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the samples
analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
March 15, 2016
Report Number:AZA0596
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
7304-GW1R AZA0596-01 01/26/16 10:09 01/27/16 07:35Ground Water
7304-GW2 AZA0596-02 01/26/16 10:43 01/27/16 07:35Ground Water
7304-GW3 AZA0596-03 01/26/16 10:57 01/27/16 07:35Ground Water
7304-GW4 AZA0596-04 01/26/16 11:11 01/27/16 07:35Ground Water
7304-GW5 AZA0596-05 01/26/16 11:33 01/27/16 07:35Ground Water
7304-GW6 AZA0596-06 01/26/16 10:27 01/27/16 07:35Ground Water
7304-GW7 AZA0596-07 01/26/16 11:52 01/27/16 07:35Ground Water
7304-GW8 AZA0596-08 01/26/16 12:09 01/27/16 07:35Ground Water
7304-GW9 AZA0596-09 01/26/16 12:38 01/27/16 07:35Ground Water
7304-GW10 AZA0596-10 01/26/16 12:24 01/27/16 07:35Ground Water
7304-SW2 AZA0596-11 01/26/16 11:15 01/27/16 07:35Surface Water
7304-Leachate AZA0596-12 01/26/16 13:00 01/27/16 07:35Water
7304-Field Blank AZA0596-13 01/26/16 13:17 01/27/16 07:35Water
7304-Trip Blank AZA0596-14 01/26/16 07:00 01/27/16 07:35Water
Page 2 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Upper Piedmont report AZA0596 - 3/15/2016
Work order revised for consultant request to change iron default reporting limit.
Case Narrative
Page 3 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW1R
Ground Water
AZA0596-01 AZA059601/26/16 10:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 14:2602/04/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6020095EPA 3005A 0.75 7440-38-2 02/08/16 14:2602/04/16 08:15
EPA 6020B 11.5 ug/L1Barium100 J 6020095EPA 3005A 0.30 7440-39-3 02/08/16 14:2602/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 14:2602/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 14:2602/04/16 08:15
EPA 6020B 2.96 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 14:2602/04/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6020095EPA 3005A 0.29 7440-48-4 02/08/16 14:2602/04/16 08:15
EPA 6020B 0.73 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 14:2602/04/16 08:15
EPA 6020B 0.24 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 14:2602/04/16 08:15
EPA 6020B 5.08 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 14:2602/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 14:2602/04/16 08:15
EPA 6020B 0.77 ug/L1Silver10.0 J 6020095EPA 3005A 0.22 7440-22-4 02/08/16 14:2602/04/16 08:15
EPA 6020B 0.08 ug/L1Thallium5.50 J 6020095EPA 3005A 0.06 7440-28-0 02/08/16 14:2602/04/16 08:15
EPA 6020B 3.05 ug/L1Vanadium25.0 J 6020095EPA 3005A 1.57 7440-62-2 02/08/16 14:2602/04/16 08:15
EPA 6020B 3.65 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 14:2602/04/16 08:15
EPA 6020B 253 ug/L1Iron300 J 6020095EPA 3005A 5.72 7439-89-6 02/08/16 14:2602/04/16 08:15
EPA 6020B 24.0 ug/L1Manganese50.0 J 6020095EPA 3005A 1.04 7439-96-5 02/08/16 14:2602/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 15:4401/27/16 12:00
Page 4 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW1R
Ground Water
AZA0596-01 AZA059601/26/16 10:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 15:4401/27/16 12:00
Page 5 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW1R
Ground Water
AZA0596-01 AZA059601/26/16 10:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 15:4401/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 15:4401/27/16 12:00
Page 6 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW1R
Ground Water
AZA0596-01 AZA059601/26/16 10:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 15:4401/27/16 12:00
EPA 8260B 98 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 15:4401/27/16 12:0080-120
EPA 8260B 96 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 15:4401/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 15:4401/27/16 12:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 15:4401/27/16 12:0080-120
Page 7 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW2
Ground Water
AZA0596-02 AZA059601/26/16 10:43
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 14:3102/04/16 08:15
EPA 6020B 1.16 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 14:3102/04/16 08:15
EPA 6020B 50.6 ug/L1Barium100 J 6020095EPA 3005A 0.30 7440-39-3 02/08/16 14:3102/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 14:3102/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 14:3102/04/16 08:15
EPA 6020B 0.58 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 14:3102/04/16 08:15
EPA 6020B 5.06 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 14:3102/04/16 08:15
EPA 6020B 32.6 ug/L1Copper10.0 6020095EPA 3005A 0.41 7440-50-8 02/08/16 14:3102/04/16 08:15
EPA 6020B 0.61 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 14:3102/04/16 08:15
EPA 6020B 2.12 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 14:3102/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 14:3102/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 14:3102/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 14:3102/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 14:3102/04/16 08:15
EPA 6020B 12.4 ug/L1Zinc10.0 6020095EPA 3005A 1.30 7440-66-6 02/08/16 14:3102/04/16 08:15
EPA 6020B 197 ug/L1Iron300 J 6020095EPA 3005A 5.72 7439-89-6 02/08/16 14:3102/04/16 08:15
EPA 6020B 572 ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 14:3102/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 16:1401/27/16 12:00
Page 8 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW2
Ground Water
AZA0596-02 AZA059601/26/16 10:43
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 16:1401/27/16 12:00
Page 9 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW2
Ground Water
AZA0596-02 AZA059601/26/16 10:43
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 16:1401/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 16:1401/27/16 12:00
Page 10 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW2
Ground Water
AZA0596-02 AZA059601/26/16 10:43
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 16:1401/27/16 12:00
EPA 8260B 99 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 16:1401/27/16 12:0080-120
EPA 8260B 97 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 16:1401/27/16 12:0078-120
EPA 8260B 90 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 16:1401/27/16 12:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 16:1401/27/16 12:0080-120
Page 11 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW3
Ground Water
AZA0596-03 AZA059601/26/16 10:57
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 14:3602/04/16 08:15
EPA 6020B 2.85 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 14:3602/04/16 08:15
EPA 6020B 492 ug/L1Barium100 6020095EPA 3005A 0.30 7440-39-3 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 14:3602/04/16 08:15
EPA 6020B 0.12 ug/L1Cadmium1.00 J 6020095EPA 3005A 0.10 7440-43-9 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6020095EPA 3005A 0.43 7440-47-3 02/08/16 14:3602/04/16 08:15
EPA 6020B 5.58 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 14:3602/04/16 08:15
EPA 6020B 0.44 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Lead10.0 6020095EPA 3005A 0.08 7439-92-1 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6020095EPA 3005A 0.48 7440-02-0 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 14:3602/04/16 08:15
NDEPA 6020B ug/L1Zinc10.0 6020095EPA 3005A 1.30 7440-66-6 02/08/16 14:3602/04/16 08:15
EPA 6020B 249 ug/L1Iron300 J 6020095EPA 3005A 5.72 7439-89-6 02/08/16 14:3602/04/16 08:15
EPA 6020B 306 ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 14:3602/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 16:4401/27/16 12:00
Page 12 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW3
Ground Water
AZA0596-03 AZA059601/26/16 10:57
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 16:4401/27/16 12:00
Page 13 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW3
Ground Water
AZA0596-03 AZA059601/26/16 10:57
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 16:4401/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 16:4401/27/16 12:00
Page 14 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW3
Ground Water
AZA0596-03 AZA059601/26/16 10:57
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 16:4401/27/16 12:00
EPA 8260B 97 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 16:4401/27/16 12:0080-120
EPA 8260B 97 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 16:4401/27/16 12:0078-120
EPA 8260B 92 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 16:4401/27/16 12:0080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 16:4401/27/16 12:0080-120
Page 15 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW4
Ground Water
AZA0596-04 AZA059601/26/16 11:11
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 14:4102/04/16 08:15
EPA 6020B 3.28 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 14:4102/04/16 08:15
EPA 6020B 452 ug/L1Barium100 6020095EPA 3005A 0.30 7440-39-3 02/08/16 14:4102/04/16 08:15
EPA 6020B 0.20 ug/L1Beryllium1.00 J 6020095EPA 3005A 0.09 7440-41-7 02/08/16 14:4102/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 14:4102/04/16 08:15
EPA 6020B 0.45 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 14:4102/04/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6020095EPA 3005A 0.29 7440-48-4 02/08/16 14:4102/04/16 08:15
EPA 6020B 2.24 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 14:4102/04/16 08:15
EPA 6020B 3.97 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 14:4102/04/16 08:15
EPA 6020B 0.56 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 14:4102/04/16 08:15
EPA 6020B 0.87 ug/L1Selenium10.0 J 6020095EPA 3005A 0.85 7782-49-2 02/08/16 14:4102/04/16 08:15
EPA 6020B 0.49 ug/L1Silver10.0 J 6020095EPA 3005A 0.22 7440-22-4 02/08/16 14:4102/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 14:4102/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 14:4102/04/16 08:15
EPA 6020B 3.13 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 14:4102/04/16 08:15
EPA 6020B 1050 ug/L1Iron300 6020095EPA 3005A 5.72 7439-89-6 02/08/16 14:4102/04/16 08:15
EPA 6020B 26.1 ug/L1Manganese50.0 J 6020095EPA 3005A 1.04 7439-96-5 02/08/16 14:4102/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 17:1301/27/16 12:00
Page 16 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW4
Ground Water
AZA0596-04 AZA059601/26/16 11:11
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 17:1301/27/16 12:00
Page 17 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW4
Ground Water
AZA0596-04 AZA059601/26/16 11:11
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 17:1301/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 17:1301/27/16 12:00
Page 18 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW4
Ground Water
AZA0596-04 AZA059601/26/16 11:11
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 17:1301/27/16 12:00
EPA 8260B 99 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 17:1301/27/16 12:0080-120
EPA 8260B 96 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 17:1301/27/16 12:0078-120
EPA 8260B 90 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 17:1301/27/16 12:0080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 17:1301/27/16 12:0080-120
Page 19 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW5
Ground Water
AZA0596-05 AZA059601/26/16 11:33
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 14:4602/04/16 08:15
EPA 6020B 4.38 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 14:4602/04/16 08:15
EPA 6020B 268 ug/L1Barium100 6020095EPA 3005A 0.30 7440-39-3 02/08/16 14:4602/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 14:4602/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 14:4602/04/16 08:15
EPA 6020B 0.80 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 14:4602/04/16 08:15
EPA 6020B 1.03 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 14:4602/04/16 08:15
EPA 6020B 0.44 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 14:4602/04/16 08:15
EPA 6020B 0.09 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 14:4602/04/16 08:15
EPA 6020B 1.17 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 14:4602/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 14:4602/04/16 08:15
EPA 6020B 0.36 ug/L1Silver10.0 J 6020095EPA 3005A 0.22 7440-22-4 02/08/16 14:4602/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 14:4602/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 14:4602/04/16 08:15
EPA 6020B 1.66 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 14:4602/04/16 08:15
EPA 6020B 3430 ug/L1Iron300 6020095EPA 3005A 5.72 7439-89-6 02/08/16 14:4602/04/16 08:15
EPA 6020B 2690 ug/L5Manganese250 6020095EPA 3005A 5.18 7439-96-5 02/11/16 15:2402/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 18:4301/27/16 12:00
Page 20 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW5
Ground Water
AZA0596-05 AZA059601/26/16 11:33
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 18:4301/27/16 12:00
Page 21 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW5
Ground Water
AZA0596-05 AZA059601/26/16 11:33
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 18:4301/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 18:4301/27/16 12:00
Page 22 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW5
Ground Water
AZA0596-05 AZA059601/26/16 11:33
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 18:4301/27/16 12:00
EPA 8260B 97 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 18:4301/27/16 12:0080-120
EPA 8260B 94 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 18:4301/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 18:4301/27/16 12:0080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 18:4301/27/16 12:0080-120
Page 23 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW6
Ground Water
AZA0596-06 AZA059601/26/16 10:27
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
EPA 6020B 0.30 ug/L1Antimony6.00 J 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:0602/04/16 08:15
EPA 6020B 1.36 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:0602/04/16 08:15
EPA 6020B 25.8 ug/L1Barium100 J 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:0602/04/16 08:15
EPA 6020B 2.52 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:0602/04/16 08:15
EPA 6020B 5.56 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:0602/04/16 08:15
EPA 6020B 1.14 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:0602/04/16 08:15
EPA 6020B 3.55 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:0602/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:0602/04/16 08:15
EPA 6020B 9.31 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:0602/04/16 08:15
EPA 6020B 408 ug/L1Iron300 6020095EPA 3005A 5.72 7439-89-6 02/08/16 15:0602/04/16 08:15
EPA 6020B 28.0 ug/L1Manganese50.0 J 6020095EPA 3005A 1.04 7439-96-5 02/08/16 15:0602/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 19:1201/27/16 12:00
Page 24 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW6
Ground Water
AZA0596-06 AZA059601/26/16 10:27
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 19:1201/27/16 12:00
Page 25 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW6
Ground Water
AZA0596-06 AZA059601/26/16 10:27
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 19:1201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 19:1201/27/16 12:00
Page 26 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW6
Ground Water
AZA0596-06 AZA059601/26/16 10:27
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 19:1201/27/16 12:00
EPA 8260B 100 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 19:1201/27/16 12:0080-120
EPA 8260B 96 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 19:1201/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 19:1201/27/16 12:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 19:1201/27/16 12:0080-120
Page 27 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW7
Ground Water
AZA0596-07 AZA059601/26/16 11:52
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:1102/04/16 08:15
EPA 6020B 4.60 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:1102/04/16 08:15
EPA 6020B 199 ug/L1Barium100 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:1102/04/16 08:15
EPA 6020B 1.44 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:1102/04/16 08:15
EPA 6020B 6.89 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Copper10.0 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Lead10.0 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:1102/04/16 08:15
EPA 6020B 1.39 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:1102/04/16 08:15
EPA 6020B 0.88 ug/L1Selenium10.0 J 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:1102/04/16 08:15
NDEPA 6020B ug/L1Zinc10.0 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:1102/04/16 08:15
EPA 6020B 98300 ug/L50Iron15000 6020095EPA 3005A 286 7439-89-6 02/11/16 15:2902/04/16 08:15
EPA 6020B 12300 ug/L50Manganese2500 6020095EPA 3005A 51.8 7439-96-5 02/08/16 15:2902/04/16 08:15
Volatile Organic Compounds by EPA 8260
EPA 8260B 5.5 ug/L1Acetone100 J 6010562EPA 5030B 4.9 67-64-1 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 19:4201/27/16 12:00
Page 28 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW7
Ground Water
AZA0596-07 AZA059601/26/16 11:52
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 19:4201/27/16 12:00
Page 29 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW7
Ground Water
AZA0596-07 AZA059601/26/16 11:52
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 19:4201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 19:4201/27/16 12:00
Page 30 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW7
Ground Water
AZA0596-07 AZA059601/26/16 11:52
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 19:4201/27/16 12:00
EPA 8260B 97 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 19:4201/27/16 12:0080-120
EPA 8260B 94 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 19:4201/27/16 12:0078-120
EPA 8260B 88 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 19:4201/27/16 12:0080-120
EPA 8260B 83 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 19:4201/27/16 12:0080-120
Page 31 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW8
Ground Water
AZA0596-08 AZA059601/26/16 12:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:1602/04/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:1602/04/16 08:15
EPA 6020B 212 ug/L1Barium100 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:1602/04/16 08:15
EPA 6020B 0.15 ug/L1Beryllium1.00 J 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:1602/04/16 08:15
EPA 6020B 0.20 ug/L1Cadmium1.00 J 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:1602/04/16 08:15
EPA 6020B 1.63 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:1602/04/16 08:15
EPA 6020B 14.2 ug/L1Cobalt10.0 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:1602/04/16 08:15
EPA 6020B 2.11 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:1602/04/16 08:15
EPA 6020B 0.34 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:1602/04/16 08:15
EPA 6020B 4.89 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:1602/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:1602/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:1602/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:1602/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:1602/04/16 08:15
EPA 6020B 13.0 ug/L1Zinc10.0 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:1602/04/16 08:15
EPA 6020B 209 ug/L1Iron300 J 6020095EPA 3005A 5.72 7439-89-6 02/08/16 15:1602/04/16 08:15
EPA 6020B 514 ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 15:1602/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 20:1201/27/16 12:00
Page 32 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW8
Ground Water
AZA0596-08 AZA059601/26/16 12:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 20:1201/27/16 12:00
Page 33 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW8
Ground Water
AZA0596-08 AZA059601/26/16 12:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 20:1201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 20:1201/27/16 12:00
Page 34 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW8
Ground Water
AZA0596-08 AZA059601/26/16 12:09
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 20:1201/27/16 12:00
EPA 8260B 97 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 20:1201/27/16 12:0080-120
EPA 8260B 96 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 20:1201/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 20:1201/27/16 12:0080-120
EPA 8260B 108 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 20:1201/27/16 12:0080-120
Page 35 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW9
Ground Water
AZA0596-09 AZA059601/26/16 12:38
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:2102/04/16 08:15
EPA 6020B 1.87 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:2102/04/16 08:15
EPA 6020B 164 ug/L1Barium100 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:2102/04/16 08:15
EPA 6020B 0.26 ug/L1Beryllium1.00 J 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:2102/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:2102/04/16 08:15
EPA 6020B 3.82 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:2102/04/16 08:15
EPA 6020B 8.81 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:2102/04/16 08:15
EPA 6020B 1.25 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:2102/04/16 08:15
EPA 6020B 1.71 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:2102/04/16 08:15
EPA 6020B 5.35 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:2102/04/16 08:15
EPA 6020B 1.23 ug/L1Selenium10.0 J 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:2102/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:2102/04/16 08:15
EPA 6020B 0.07 ug/L1Thallium5.50 J 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:2102/04/16 08:15
EPA 6020B 3.33 ug/L1Vanadium25.0 J 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:2102/04/16 08:15
EPA 6020B 8.74 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:2102/04/16 08:15
EPA 6020B 9020 ug/L1Iron300 6020095EPA 3005A 5.72 7439-89-6 02/08/16 15:2102/04/16 08:15
EPA 6020B 680 ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 15:2102/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 20:4201/27/16 12:00
Page 36 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW9
Ground Water
AZA0596-09 AZA059601/26/16 12:38
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 20:4201/27/16 12:00
Page 37 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW9
Ground Water
AZA0596-09 AZA059601/26/16 12:38
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 20:4201/27/16 12:00
Page 38 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW9
Ground Water
AZA0596-09 AZA059601/26/16 12:38
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 20:4201/27/16 12:00
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 20:4201/27/16 12:00
EPA 8260B 96 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 20:4201/27/16 12:0080-120
EPA 8260B 96 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 20:4201/27/16 12:0078-120
EPA 8260B 90 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 20:4201/27/16 12:0080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 20:4201/27/16 12:0080-120
Page 39 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW10
Ground Water
AZA0596-10 AZA059601/26/16 12:24
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:2602/04/16 08:15
EPA 6020B 88.8 ug/L1Barium100 J 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:2602/04/16 08:15
EPA 6020B 0.20 ug/L1Beryllium1.00 J 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:2602/04/16 08:15
EPA 6020B 0.44 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:2602/04/16 08:15
EPA 6020B 4.76 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:2602/04/16 08:15
EPA 6020B 2.73 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Lead10.0 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:2602/04/16 08:15
EPA 6020B 4.55 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:2602/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:2602/04/16 08:15
EPA 6020B 5.34 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:2602/04/16 08:15
EPA 6020B 231 ug/L1Iron300 J 6020095EPA 3005A 5.72 7439-89-6 02/08/16 15:2602/04/16 08:15
EPA 6020B 142 ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 15:2602/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 21:1101/27/16 12:00
Page 40 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW10
Ground Water
AZA0596-10 AZA059601/26/16 12:24
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 21:1101/27/16 12:00
Page 41 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW10
Ground Water
AZA0596-10 AZA059601/26/16 12:24
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 21:1101/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 21:1101/27/16 12:00
Page 42 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-GW10
Ground Water
AZA0596-10 AZA059601/26/16 12:24
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 21:1101/27/16 12:00
EPA 8260B 98 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 21:1101/27/16 12:0080-120
EPA 8260B 96 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 21:1101/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 21:1101/27/16 12:0080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 21:1101/27/16 12:0080-120
Page 43 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-SW2
Surface Water
AZA0596-11 AZA059601/26/16 11:15
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
EPA 6020B 0.81 ug/L1Antimony6.00 J 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:3002/04/16 08:15
EPA 6020B 1.00 ug/L1Arsenic10.0 J 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:3002/04/16 08:15
EPA 6020B 37.6 ug/L1Barium100 J 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:3002/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:3002/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:3002/04/16 08:15
EPA 6020B 2.28 ug/L1Chromium10.0 J 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:3002/04/16 08:15
EPA 6020B 1.37 ug/L1Cobalt10.0 J 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:3002/04/16 08:15
EPA 6020B 3.02 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:3002/04/16 08:15
EPA 6020B 4.16 ug/L1Lead10.0 J 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:3002/04/16 08:15
EPA 6020B 1.33 ug/L1Nickel50.0 J 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:3002/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:3002/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:3002/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:3002/04/16 08:15
EPA 6020B 3.70 ug/L1Vanadium25.0 J 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:3002/04/16 08:15
EPA 6020B 16.8 ug/L1Zinc10.0 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:3002/04/16 08:15
EPA 6020B 2290 ug/L1Iron300 6020095EPA 3005A 5.72 7439-89-6 02/08/16 15:3002/04/16 08:15
EPA 6020B 235 ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 15:3002/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 21:4101/27/16 12:00
Page 44 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-SW2
Surface Water
AZA0596-11 AZA059601/26/16 11:15
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 21:4101/27/16 12:00
Page 45 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-SW2
Surface Water
AZA0596-11 AZA059601/26/16 11:15
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010562EPA 5030B 0.5 75-09-2 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 21:4101/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 21:4101/27/16 12:00
Page 46 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-SW2
Surface Water
AZA0596-11 AZA059601/26/16 11:15
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 21:4101/27/16 12:00
EPA 8260B 100 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 21:4101/27/16 12:0080-120
EPA 8260B 99 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 21:4101/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 21:4101/27/16 12:0080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 21:4101/27/16 12:0080-120
Page 47 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Leachate
Water
AZA0596-12 AZA059601/26/16 13:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
General Chemistry
EPA 350.1 645000 ug/L50Ammonia as N 5000 6020080EPA 350.1 5000 NA 02/03/16 13:5102/03/16 09:30
SM 5210 B 103000 ug/L2Biochemical Oxygen Demand 33000 6010554SM 5210 B 2.0 E-10106 02/01/16 09:0701/27/16 09:17
SM 5220 D 1930000 ug/L5Chemical Oxygen Demand 50000 6020050SM 5220 D 50000 E-10117 02/02/16 14:4502/02/16 11:45
NDEPA 9010/9014 ug/L1Cyanide, Total 50.0 R-01 6020010EPA 9010 50.0 57-12-5 02/01/16 16:2502/01/16 11:30
SM 4500-P B,E 3360 ug/L1.11Phosphorus-Total 222 6010584SM 4500-P B 222 7723-14-0 01/28/16 18:5301/28/16 09:20
Inorganic Anions
EPA 9056A 2200 ug/L1Nitrate/Nitrite as N 50 6010583EPA 9056A 50 E-10128 01/27/16 15:4501/27/16 15:45
EPA 9056A 760 ug/L1Nitrate as N 50 6010583EPA 9056A 50 14797-55-8 01/27/16 15:4501/27/16 15:45
EPA 9056A 1400 ug/L1Nitrite as N 50 6010583EPA 9056A 50 1594-56-5 01/27/16 15:4501/27/16 15:45
EPA 9056A 23000 ug/L1Sulfate5000 6010583EPA 9056A 5000 14808-79-8 01/27/16 15:4501/27/16 15:45
Metals, Total
EPA 6020B 31.3 ug/L5Antimony30.0 6020095EPA 3005A 1.25 7440-36-0 02/08/16 17:3202/04/16 08:15
EPA 6020B 70.8 ug/L5Arsenic50.0 6020095EPA 3005A 3.73 7440-38-2 02/08/16 17:3202/04/16 08:15
EPA 6020B 216 ug/L5Barium100 6020095EPA 3005A 1.49 7440-39-3 02/08/16 17:3202/04/16 08:15
NDEPA 6020B ug/L5Beryllium1.00 6020095EPA 3005A 0.47 7440-41-7 02/08/16 17:3202/04/16 08:15
NDEPA 6020B ug/L5Cadmium2.50 R-01 6020095EPA 3005A 0.48 7440-43-9 02/08/16 17:3202/04/16 08:15
EPA 6020B 142 ug/L5Chromium50.0 6020095EPA 3005A 2.16 7440-47-3 02/08/16 17:3202/04/16 08:15
EPA 6020B 33.3 ug/L5Cobalt10.0 6020095EPA 3005A 1.44 7440-48-4 02/08/16 17:3202/04/16 08:15
EPA 6020B 8.56 ug/L5Copper10.0 J 6020095EPA 3005A 2.04 7440-50-8 02/08/16 17:3202/04/16 08:15
EPA 6020B 1.46 ug/L5Lead10.0 J 6020095EPA 3005A 0.42 7439-92-1 02/08/16 17:3202/04/16 08:15
Page 48 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Leachate
Water
AZA0596-12 AZA059601/26/16 13:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
EPA 6020B 164 ug/L5Nickel50.0 6020095EPA 3005A 2.42 7440-02-0 02/08/16 17:3202/04/16 08:15
EPA 6020B 5.94 ug/L5Selenium10.0 J 6020095EPA 3005A 4.27 7782-49-2 02/08/16 17:3202/04/16 08:15
NDEPA 6020B ug/L5Silver10.0 6020095EPA 3005A 1.12 7440-22-4 02/08/16 17:3202/04/16 08:15
NDEPA 6020B ug/L5Thallium5.50 6020095EPA 3005A 0.28 7440-28-0 02/08/16 17:3202/04/16 08:15
EPA 6020B 67.3 ug/L5Vanadium50.0 6020095EPA 3005A 7.86 7440-62-2 02/08/16 17:3202/04/16 08:15
EPA 6020B 97.8 ug/L5Zinc50.0 6020095EPA 3005A 6.52 7440-66-6 02/08/16 17:3202/04/16 08:15
NDEPA 7470A ug/L1Mercury1.33 R-01 6020238EPA 7470A 0.467 7439-97-6 02/11/16 13:2702/10/16 14:55
Volatile Organic Compounds by EPA 8260
EPA 8260B 100 ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 14:1501/27/16 12:00
EPA 8260B 2.5 ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 14:1501/27/16 12:00
EPA 8260B 0.7 ug/L1Chlorobenzene3.0 J 6010562EPA 5030B 0.4 108-90-7 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 14:1501/27/16 12:00
Page 49 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Leachate
Water
AZA0596-12 AZA059601/26/16 13:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 14:1501/27/16 12:00
EPA 8260B 7.2 ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 14:1501/27/16 12:00
EPA 8260B 0.3 ug/L11,2-Dichloroethane 1.0 J 6010562EPA 5030B 0.3 107-06-2 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 14:1501/27/16 12:00
EPA 8260B 2.2 ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 14:1501/27/16 12:00
EPA 8260B 3.1 ug/L1Methyl Butyl Ketone
(2-Hexanone)50 J 6010562EPA 5030B 0.9 591-78-6 01/27/16 14:1501/27/16 12:00
EPA 8260B 0.7 ug/L1Methylene Chloride 1.0 J 6010562EPA 5030B 0.5 75-09-2 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 14:1501/27/16 12:00
EPA 8260B 25 ug/L14-Methyl-2-pentanone (MIBK)100 J 6010562EPA 5030B 1.7 108-10-1 01/27/16 14:1501/27/16 12:00
Page 50 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Leachate
Water
AZA0596-12 AZA059601/26/16 13:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
EPA 8260B 2.5 ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 14:1501/27/16 12:00
EPA 8260B 5.8 ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 14:1501/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 14:1501/27/16 12:00
EPA 8260B 20 ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 14:1501/27/16 12:00
EPA 8260B 98 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 14:1501/27/16 12:0080-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 14:1501/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 14:1501/27/16 12:0080-120
EPA 8260B 90 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 14:1501/27/16 12:0080-120
Page 51 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Field Blank
Water
AZA0596-13 AZA059601/26/16 13:17
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020095EPA 3005A 0.25 7440-36-0 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6020095EPA 3005A 0.75 7440-38-2 02/08/16 15:3502/04/16 08:15
EPA 6020B 0.55 ug/L1Barium100 J 6020095EPA 3005A 0.30 7440-39-3 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6020095EPA 3005A 0.09 7440-41-7 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6020095EPA 3005A 0.10 7440-43-9 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Chromium10.0 6020095EPA 3005A 0.43 7440-47-3 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6020095EPA 3005A 0.29 7440-48-4 02/08/16 15:3502/04/16 08:15
EPA 6020B 3.93 ug/L1Copper10.0 J 6020095EPA 3005A 0.41 7440-50-8 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Lead10.0 6020095EPA 3005A 0.08 7439-92-1 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Nickel50.0 6020095EPA 3005A 0.48 7440-02-0 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6020095EPA 3005A 0.85 7782-49-2 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Silver10.0 6020095EPA 3005A 0.22 7440-22-4 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6020095EPA 3005A 0.06 7440-28-0 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Vanadium25.0 6020095EPA 3005A 1.57 7440-62-2 02/08/16 15:3502/04/16 08:15
EPA 6020B 1.35 ug/L1Zinc10.0 J 6020095EPA 3005A 1.30 7440-66-6 02/08/16 15:3502/04/16 08:15
EPA 6020B 9.50 ug/L1Iron300 J 6020095EPA 3005A 5.72 7439-89-6 02/08/16 15:3502/04/16 08:15
NDEPA 6020B ug/L1Manganese50.0 6020095EPA 3005A 1.04 7439-96-5 02/08/16 15:3502/04/16 08:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 13:1501/27/16 12:00
Page 52 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Field Blank
Water
AZA0596-13 AZA059601/26/16 13:17
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 13:1501/27/16 12:00
Page 53 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Field Blank
Water
AZA0596-13 AZA059601/26/16 13:17
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 13:1501/27/16 12:00
EPA 8260B 0.9 ug/L1Methylene Chloride 1.0 J 6010562EPA 5030B 0.5 75-09-2 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 13:1501/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 13:1501/27/16 12:00
Page 54 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Field Blank
Water
AZA0596-13 AZA059601/26/16 13:17
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 13:1501/27/16 12:00
EPA 8260B 96 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 13:1501/27/16 12:0080-120
EPA 8260B 95 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 13:1501/27/16 12:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 13:1501/27/16 12:0080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 13:1501/27/16 12:0080-120
Page 55 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Trip Blank
Water
AZA0596-14 AZA059601/26/16 07:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010562EPA 5030B 4.9 67-64-1 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6010562EPA 5030B 1.8 107-13-1 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6010562EPA 5030B 0.2 71-43-2 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6010562EPA 5030B 0.7 74-97-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010562EPA 5030B 0.6 75-27-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6010562EPA 5030B 0.5 75-25-2 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6010562EPA 5030B 0.8 74-83-9 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6010562EPA 5030B 0.9 75-15-0 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010562EPA 5030B 0.6 56-23-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6010562EPA 5030B 0.4 108-90-7 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6010562EPA 5030B 0.6 75-00-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6010562EPA 5030B 0.3 67-66-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6010562EPA 5030B 0.4 74-87-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010562EPA 5030B 0.4 124-48-1 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010562EPA 5030B 2.0 96-12-8 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010562EPA 5030B 0.7 106-93-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6010562EPA 5030B 0.7 74-95-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010562EPA 5030B 0.5 95-50-1 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010562EPA 5030B 0.2 106-46-7 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010562EPA 5030B 1.5 110-57-6 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010562EPA 5030B 0.4 75-34-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010562EPA 5030B 0.3 107-06-2 01/27/16 13:4501/27/16 12:00
Page 56 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Trip Blank
Water
AZA0596-14 AZA059601/26/16 07:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010562EPA 5030B 0.5 75-35-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-59-2 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010562EPA 5030B 0.5 156-60-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010562EPA 5030B 0.5 78-87-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-01-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010562EPA 5030B 0.4 10061-02-6 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6010562EPA 5030B 0.3 100-41-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6010562EPA 5030B 0.6 74-88-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6010562EPA 5030B 0.9 591-78-6 01/27/16 13:4501/27/16 12:00
EPA 8260B 0.7 ug/L1Methylene Chloride 1.0 J 6010562EPA 5030B 0.5 75-09-2 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010562EPA 5030B 1.1 78-93-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010562EPA 5030B 1.7 108-10-1 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6010562EPA 5030B 0.4 100-42-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010562EPA 5030B 0.5 630-20-6 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010562EPA 5030B 0.5 79-34-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010562EPA 5030B 0.4 127-18-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6010562EPA 5030B 0.3 108-88-3 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010562EPA 5030B 0.4 71-55-6 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010562EPA 5030B 0.8 79-00-5 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010562EPA 5030B 0.4 79-01-6 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010562EPA 5030B 0.5 75-69-4 01/27/16 13:4501/27/16 12:00
Page 57 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
7304-Trip Blank
Water
AZA0596-14 AZA059601/26/16 07:00
Project:Upper Piedmont Regional Landfill
01/27/16 07:35
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010562EPA 5030B 0.7 96-18-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010562EPA 5030B 0.6 108-05-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010562EPA 5030B 0.7 75-01-4 01/27/16 13:4501/27/16 12:00
NDEPA 8260B ug/L1Xylenes, total 5.0 6010562EPA 5030B 0.4 1330-20-7 01/27/16 13:4501/27/16 12:00
EPA 8260B 99 %Surr: Dibromofluoromethane 6010562EPA 5030B 1868-53-7 01/27/16 13:4501/27/16 12:0080-120
EPA 8260B 93 %Surr: 1,2-Dichloroethane-d4 6010562EPA 5030B 17060-07-0 01/27/16 13:4501/27/16 12:0078-120
EPA 8260B 90 %Surr: Toluene-d8 6010562EPA 5030B 2037-26-5 01/27/16 13:4501/27/16 12:0080-120
EPA 8260B 100 %Surr: 4-Bromofluorobenzene 6010562EPA 5030B 460-00-4 01/27/16 13:4501/27/16 12:0080-120
Page 58 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6010554 - SM 5210 B
Blank (6010554-BLK1)Prepared: 01/27/16 Analyzed: 02/01/16
Biochemical Oxygen Demand ug/L1802000 J
LCS (6010554-BS1)Prepared: 01/27/16 Analyzed: 02/01/16
Biochemical Oxygen Demand ug/L1980002000 198000 85-115100
Duplicate (6010554-DUP1)Prepared: 01/27/16 Analyzed: 02/01/16 Source: AZA0575-02
Biochemical Oxygen Demand ug/L320000164000 344000 207
Batch 6010584 - SM 4500-P B
Blank (6010584-BLK1)Prepared & Analyzed: 01/28/16
Phosphorus-Total ug/LND0.02
LCS (6010584-BS1)Prepared & Analyzed: 01/28/16
Phosphorus-Total ug/L47820.0 500.00 88-11096
Matrix Spike (6010584-MS1)Prepared & Analyzed: 01/28/16 Source: AZA0474-01
Phosphorus-Total ug/L1980222 5000.0 1820 QM-0572-1233
Matrix Spike Dup (6010584-MSD1)Prepared & Analyzed: 01/28/16 Source: AZA0474-01
Phosphorus-Total ug/L1390222 5000.0 1820 11 QM-0672-1230 35
Batch 6020010 - EPA 9010
Blank (6020010-BLK1)Prepared & Analyzed: 02/01/16
Cyanide, Total ug/LND10.0
Page 59 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6020010 - EPA 9010
LCS (6020010-BS1)Prepared & Analyzed: 02/01/16
Cyanide, Total ug/L80.0 10.0 80.000 85-115100
Duplicate (6020010-DUP1)Prepared & Analyzed: 02/01/16 Source: AZA0492-01RE1
Cyanide, Total ug/L14220.0 142 200
Matrix Spike (6020010-MS1)Prepared & Analyzed: 02/01/16 Source: AZA0548-45
Cyanide, Total ug/L78.0 10.0 80.000 ND 85-11998
Matrix Spike Dup (6020010-MSD1)Prepared & Analyzed: 02/01/16 Source: AZA0548-45
Cyanide, Total ug/L81.0 10.0 80.000 ND 1385-119101 4
Batch 6020050 - SM 5220 D
Blank (6020050-BLK1)Prepared & Analyzed: 02/02/16
Chemical Oxygen Demand ug/LND10000
LCS (6020050-BS1)Prepared & Analyzed: 02/02/16
Chemical Oxygen Demand ug/L21000010000 200000 90-110105
Matrix Spike (6020050-MS1)Prepared & Analyzed: 02/02/16 Source: AZA0684-02
Chemical Oxygen Demand ug/L87400010000 200000 706000 QM-0590-11084
Matrix Spike (6020050-MS2)Prepared & Analyzed: 02/02/16 Source: AZA0689-01
Chemical Oxygen Demand ug/L31500010000 200000 104000 90-110105
Matrix Spike Dup (6020050-MSD1)Prepared & Analyzed: 02/02/16 Source: AZA0684-02
Chemical Oxygen Demand ug/L88600010000 200000 706000 1090-11090 1
Page 60 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6020080 - EPA 350.1
Blank (6020080-BLK1)Prepared & Analyzed: 02/03/16
Ammonia as N ug/LND0.10
LCS (6020080-BS1)Prepared & Analyzed: 02/03/16
Ammonia as N ug/L9380100 10000 90-11094
Matrix Spike (6020080-MS1)Prepared & Analyzed: 02/03/16 Source: AZB0025-01
Ammonia as N ug/L9410100 10000 416 90-11090
Page 61 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 6010583 - EPA 9056A
Blank (6010583-BLK1)Prepared & Analyzed: 01/27/16
Nitrate/Nitrite as N ug/LND50
Nitrate as N ug/LND50
Nitrite as N ug/LND50
Sulfate ug/LND5000
LCS (6010583-BS1)Prepared & Analyzed: 01/28/16
Nitrate/Nitrite as N ug/L1840050 20000 90-11092
Nitrate as N ug/L901050 10000 90-11090
Nitrite as N ug/L943050 10000 90-11094
Sulfate ug/L107005000 10000 90-110107
Matrix Spike (6010583-MS1)Prepared & Analyzed: 01/27/16 Source: AZA0609-01
Nitrate/Nitrite as N ug/L1820050 20000 301 90-11090
Nitrate as N ug/L901050 10000 219 QM-0590-11088
Nitrite as N ug/L924050 10000 82.0 90-11092
Sulfate ug/L185005000 10000 9910 QM-0590-11086
Matrix Spike (6010583-MS2)Prepared & Analyzed: 01/27/16 Source: AZA0633-05
Nitrate/Nitrite as N ug/L2160050 20000 8520 QM-0590-11065
Nitrate as N ug/L1080050 10000 1990 QM-0590-11089
Nitrite as N ug/L1480050 10000 6530 QM-0590-11082
Sulfate ug/L2330005000 10000 247000 QM-0590-1100
Matrix Spike Dup (6010583-MSD1)Prepared & Analyzed: 01/27/16 Source: AZA0609-01
Nitrate/Nitrite as N ug/L1800050 20000 301 15 QM-0590-11089 1
Nitrate as N ug/L894050 10000 219 15 QM-0590-11087 0.8
Nitrite as N ug/L909050 10000 82.0 1590-11090 2
Sulfate ug/L180005000 10000 9910 15 QM-0590-11081 3
Page 62 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 6010583 - EPA 9056A
Matrix Spike Dup (6010583-MSD1)Prepared & Analyzed: 01/27/16 Source: AZA0609-01
Page 63 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6020095 - EPA 3005A
Blank (6020095-BLK1)Prepared: 02/04/16 Analyzed: 02/08/16
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Iron ug/LND300
Lead ug/LND10.0
Manganese ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6020095-BS1)Prepared: 02/04/16 Analyzed: 02/08/16
Antimony ug/L1086.00 100.00 80-120108
Arsenic ug/L10310.0 100.00 80-120103
Barium ug/L103100 100.00 80-120103
Beryllium ug/L1101.00 100.00 80-120110
Cadmium ug/L1031.00 100.00 80-120103
Chromium ug/L10910.0 100.00 80-120109
Cobalt ug/L10310.0 100.00 80-120103
Copper ug/L10610.0 100.00 80-120106
Page 64 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6020095 - EPA 3005A
LCS (6020095-BS1)Prepared: 02/04/16 Analyzed: 02/08/16
Iron ug/L1050300 1000.0 80-120105
Lead ug/L10410.0 100.00 80-120104
Manganese ug/L10510.0 100.00 80-120105
Nickel ug/L11050.0 100.00 80-120110
Selenium ug/L96.8 10.0 100.00 80-12097
Silver ug/L10610.0 100.00 80-120106
Thallium ug/L1015.50 100.00 80-120101
Vanadium ug/L11025.0 100.00 80-120110
Zinc ug/L11010.0 100.00 80-120110
Matrix Spike (6020095-MS1)Prepared: 02/04/16 Analyzed: 02/08/16 Source: AZA0596-04
Antimony ug/L92.8 6.00 100.00 ND 75-12593
Arsenic ug/L10210.0 100.00 3.28 75-12598
Barium ug/L595100 100.00 452 QM-0275-125143
Beryllium ug/L94.7 1.00 100.00 0.20 75-12594
Cadmium ug/L98.4 1.00 100.00 ND 75-12598
Chromium ug/L10310.0 100.00 0.45 75-125103
Cobalt ug/L96.3 10.0 100.00 ND 75-12596
Copper ug/L98.0 10.0 100.00 2.24 75-12596
Iron ug/L2210300 1000.0 1050 75-125116
Lead ug/L10010.0 100.00 3.97 75-12596
Manganese ug/L12810.0 100.00 26.1 75-125102
Nickel ug/L10050.0 100.00 0.56 75-125100
Selenium ug/L96.0 10.0 100.00 0.87 75-12595
Silver ug/L99.1 10.0 100.00 0.49 75-12599
Thallium ug/L95.7 5.50 100.00 ND 75-12596
Vanadium ug/L10725.0 100.00 ND 75-125107
Page 65 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6020095 - EPA 3005A
Matrix Spike (6020095-MS1)Prepared: 02/04/16 Analyzed: 02/08/16 Source: AZA0596-04
Zinc ug/L10610.0 100.00 3.13 75-125103
Matrix Spike Dup (6020095-MSD1)Prepared: 02/04/16 Analyzed: 02/08/16 Source: AZA0596-04
Antimony ug/L92.4 6.00 100.00 ND 2075-12592 0.4
Arsenic ug/L10410.0 100.00 3.28 2075-125100 2
Barium ug/L577100 100.00 452 2075-125125 3
Beryllium ug/L95.1 1.00 100.00 0.20 2075-12595 0.5
Cadmium ug/L1011.00 100.00 ND 2075-125101 3
Chromium ug/L10210.0 100.00 0.45 2075-125102 1
Cobalt ug/L95.2 10.0 100.00 ND 2075-12595 1
Copper ug/L98.9 10.0 100.00 2.24 2075-12597 0.9
Iron ug/L2260300 1000.0 1050 2075-125122 2
Lead ug/L99.1 10.0 100.00 3.97 2075-12595 1
Manganese ug/L13210.0 100.00 26.1 2075-125106 3
Nickel ug/L10250.0 100.00 0.56 2075-125102 2
Selenium ug/L95.9 10.0 100.00 0.87 2075-12595 0.08
Silver ug/L98.9 10.0 100.00 0.49 2075-12598 0.2
Thallium ug/L93.3 5.50 100.00 ND 2075-12593 2
Vanadium ug/L10525.0 100.00 ND 2075-125105 2
Zinc ug/L10610.0 100.00 3.13 2075-125103 0.3
Post Spike (6020095-PS1)Prepared: 02/04/16 Analyzed: 02/08/16 Source: AZA0596-04
Antimony ug/L103 100.00 0.18 80-120102
Arsenic ug/L106 100.00 3.28 80-120103
Barium ug/L567 100.00 452 80-120115
Beryllium ug/L98.9 100.00 0.20 80-12099
Cadmium ug/L101 100.00 0.04 80-120101
Page 66 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6020095 - EPA 3005A
Post Spike (6020095-PS1)Prepared: 02/04/16 Analyzed: 02/08/16 Source: AZA0596-04
Chromium ug/L107 100.00 0.45 80-120107
Cobalt ug/L103 100.00 0.14 80-120103
Copper ug/L104 100.00 2.24 80-120101
Iron ug/L2130 1000.0 1050 80-120108
Lead ug/L106 100.00 3.97 80-120102
Manganese ug/L138 100.00 26.1 80-120111
Nickel ug/L105 100.00 0.56 80-120105
Selenium ug/L101 100.00 0.87 80-120100
Silver ug/L98.8 100.00 0.49 80-12098
Thallium ug/L99.0 100.00 0.02 80-12099
Vanadium ug/L110 100.00 -0.27 80-120110
Zinc ug/L110 100.00 3.13 80-120107
Batch 6020238 - EPA 7470A
Blank (6020238-BLK1)Prepared: 02/10/16 Analyzed: 02/11/16
Mercury ug/LND0.200
LCS (6020238-BS1)Prepared: 02/10/16 Analyzed: 02/11/16
Mercury ug/L2.39 0.200 2.5000 80-12096
Matrix Spike (6020238-MS1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZB0188-14
Mercury ug/L2.58 0.200 2.5000 ND 75-125103
Matrix Spike Dup (6020238-MSD1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZB0188-14
Mercury ug/L2.69 0.200 2.5000 ND 2075-125108 4
Page 67 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6020238 - EPA 7470A
Post Spike (6020238-PS1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZB0188-14
Mercury ug/L1.80 1.6667 -0.031 80-120110
Page 68 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010562 - EPA 5030B
Blank (6010562-BLK1)Prepared & Analyzed: 01/27/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Page 69 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010562 - EPA 5030B
Blank (6010562-BLK1)Prepared & Analyzed: 01/27/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 9749
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9347
ug/L 50.000 80-120Surr: Toluene-d8 9045
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10151
LCS (6010562-BS1)Prepared & Analyzed: 01/27/16
Page 70 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010562 - EPA 5030B
LCS (6010562-BS1)Prepared & Analyzed: 01/27/16
Benzene ug/L55 50.000 67-134110
Chlorobenzene ug/L49 50.000 69-12298
1,1-Dichloroethene ug/L55 50.000 58-142109
Toluene ug/L54 50.000 68-127107
Trichloroethene ug/L51 50.000 72-132103
ug/L 50.000 80-120Surr: Dibromofluoromethane 10754
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9949
ug/L 50.000 80-120Surr: Toluene-d8 9045
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9246
Matrix Spike (6010562-MS1)Prepared & Analyzed: 01/27/16 Source: AZA0596-04
Benzene ug/L54 50.000 ND 67-134108
Chlorobenzene ug/L49 50.000 ND 69-12298
1,1-Dichloroethene ug/L52 50.000 ND 58-142104
Toluene ug/L53 50.000 ND 68-127106
Trichloroethene ug/L51 50.000 ND 72-132101
ug/L 50.000 80-120Surr: Dibromofluoromethane 10653
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 9246
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9045
Matrix Spike Dup (6010562-MSD1)Prepared & Analyzed: 01/27/16 Source: AZA0596-04
Benzene ug/L53 50.000 ND 967-134107 1
Chlorobenzene ug/L47 50.000 ND 1369-12294 5
1,1-Dichloroethene ug/L51 50.000 ND 958-142102 2
Page 71 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010562 - EPA 5030B
Matrix Spike Dup (6010562-MSD1)Prepared & Analyzed: 01/27/16 Source: AZA0596-04
Toluene ug/L51 50.000 ND 968-127101 5
Trichloroethene ug/L48 50.000 ND 1172-13297 5
ug/L 50.000 80-120Surr: Dibromofluoromethane 10854
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10050
ug/L 50.000 80-120Surr: Toluene-d8 9145
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9045
Page 72 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2016TX
1340Virginia 12/14/2016VA
Page 73 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
R-01 Elevated reporting limit due to matrix interference.
QM-06 Due to suspected matrix interference, RPD and Percent Recovery values for the MS and/or MSD were outside control limits. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix interference. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 74 of 75
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Matt Einsmann March 15, 2016
COC Goes Here
Page 75 of 75
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
Upper Piedmont Regional LandfillProject:
Client:
Printed: 3/15/2016 10:54:13AM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Norcross, GA 30092
ANALYTICAL SERVICES, INC.ASI
Date Received:01/27/16 07:35 Logged In By:Mohammad M. Rahman
Work Order:AZA0596
OBSERVATIONS
Attn: Mr. Matt Einsmann
#Samples: 14 #Containers: 67
1.0 1.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
The NH3/COD/P/NO2-NO3 and metals for Leachate sample were pH adjusted by the Lab with H2SO4 and HNO3
respectively. MMR
Comments:
Page 1 of 1

Appendix D

Statistical Analyses Worksheets and Summary Table
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Joyce Engineering
JOYCE Project:Upper Piedmont Landfill
Project No: 893.1601.12
Date: March 2016
Analyte:Cobalt Quantitation
Concentration Limit
Sample No. Sample Date Location (µg/L) (µg/L)
1 23-May-97 GW-1 ND 10 0.17 31.5
2 16-Jun-97 GW-1 ND 10 0.18 29.6
3 14-Aug-97 GW-1 10 10 0.24 26.2
4 30-Apr-98 GW-1 ND 40 0.44 25.1
5 15-Sep-98 GW-1 ND 40 0.53 19.4
6 08-Apr-99 GW-1 ND 40 0.757 19.0
7 13-Apr-00 GW-1 ND 10 0.93 16.9
8 17-Oct-00 GW-1 ND 10 1.12 14.5
9 23-Apr-01 GW-1 ND 10 1.12 10
10 14-Apr-03 GW-1 ND 10 2.13 3.85
11 30-Oct-03 GW-1 ND 10 2.27 2.94
12 28-Apr-04 GW-1 ND 10 2.55 2.73
13 27-Oct-04 GW-1 ND 10 2.73 2.55
14 16-Mar-05 GW-1 ND 10 2.94 2.27
15 21-Jul-05 GW-1 ND 10 3.85 2.13
16 21-Jul-06 GW-1 ND 10 10 1.12
17 22-Jan-07 GW-1 ND 10 14.5 1.12
18 23-Jul-07 GW-1 ND 10 16.9 0.93
19 30-Jul-09 GW-1 2.55 10 19.0 0.757
20 24-May-12 GW-7 26.2 10 19.4 0.53
21 28-Jun-12 GW-7 25.1 10 25.1 0.44
22 25-Jul-12 GW-7 31.5 10 26.2 0.24
23 24-Aug-12 GW-7 29.6 10 29.6 0.18
24 24-May-12 GW-8 19.0 10 31.5 0.17
25 28-Jun-12 GW-8 14.5 10
26 25-Jul-12 GW-8 19.4 10
27 24-Aug-12 GW-8 16.9 10
28 24-May-12 GW-9 0.93 10
29 28-Jun-12 GW-9 0.17 10
30 25-Jul-12 GW-9 1.12 10
31 24-Aug-12 GW-9 1.12 10
32 24-May-12 GW-10 2.94 10
33 28-Jun-12 GW-10 2.27 10
34 25-Jul-12 GW-10 2.13 10
35 24-Aug-12 GW-10 3.85 10
36 14-Jan-10 GW-1R 0.757 10
37 15-Jul-10 GW-1R ND 10
38 20-Jan-11 GW-1R ND 10
39 14-Jul-11 GW-1R ND 10
40 30-Jan-12 GW-1R 0.18 10
41 25-Jul-12 GW-1R 0.44 10
42 04-Feb-13 GW-1R 0.24 10
43 08-Jul-13 GW-1R 2.73 10
44 21-Jan-14 GW-1R 0.53 10
45 21-Jul-14 GW-1R ND 10
46 29-Jan-15 GW-1R ND 10
47 27-Jul-15 GW-1R ND 10
48 26-Jan-16 GW-1R ND 10
Number of Data 48
Number of Truncated Data 24
Percentage of Truncated Data 50%
Non-Parmetric Prediction Interval: 31.5 µg/L
Notes:
All concentrations in micrograms per liter (µg/L).
ND = Not detected (truncated).
Sorted
Concentration (µg/L)