2602_FortBragg_MSWLF_1stSemiGWMReport_DIN27220_20160517

DRAFT May 2016 (N=39) GROUNDWATER, SURFACE-WATER, AND
METHANE MONITORING REPORT

FOR

LONGSTREET ROAD MSW LANDFILL
NCDENR LANDFILL PERMIT #26-02
FORT BRAGG, NORTH CAROLINA

Prepared by:

US Army Corps of Engineers
Savannah District
Geology/Hydrogeology and HTRW design section
CESAS-EN-GG
100 W. Oglethorpe Avenue
Savannah, GA 31401 August 2016

Prepared by:

August 31, 2016

John Markov, P.G.
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TABLE OF CONTENTS
SECTION PAGE

1.0 INTRODUCTION .......................................................................................................................... 1
1.1 Project Background ............................................................................................. 1
1.2 Project Scope ...................................................................................................... 2
2.0 PROJECT HISTORY .................................................................................................................... 2
2.1 Site Description ................................................................................................... 2
2.2 General Site Geology and Hydrology ................................................................. 3
2.3 Previous Investigation and Results ..................................................................... 3
3.0 METHODS ..................................................................................................................................... 3
3.1 Methane Monitoring ........................................................................................... 3
3.2 Water-Level Gauging.......................................................................................... 4
3.3 Groundwater and Surface-Water Sampling ....................................................... 4
3.4 Investigation Derived Wastes Handling ............................................................. 5
4.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS ................................................. 5
4.1 Analytical Data Summary ................................................................................... 6
4.2 Statistical Analysis Results ................................................................................. 8
4.3 Methane Monitoring Results ............................................................................... 9
5.0 CONCLUSIONS AND RECOMMENATIONS .......................................................................... 9
6.0 REFERENCES ............................................................................................................................... 9
In Order
Following Page 10

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FIGURES

Figure 1 Site Map – Ft. Bragg, NC
Figure 2 Location Map – Longstreet Road Landfill, Ft. Bragg, NC
Figure 3 Methane Monitoring Results
Figure 4 Potentiometric Map
Figure 5 Groundwater Analytical Results
TABLES
Table 1 Methane Monitoring Results

Table 2 Groundwater Elevation Data
Table 3 Field Parameter Measurements

APPENDICES

Appendix A – Groundwater Sampling Logs
Appendix B – Chains of Custody and Laboratory Analytical Reports
Appendix C – Statistical Reports
Appendix D – Historical Sampling Results

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LIST OF ACRONYMS

C&D Construction and Demolition COCs Chemicals of Concern
DPW Directorate of Public Works
IDW Investigation Derived Waste
LCID Land Clearing and Inert Debris
µg/L Micrograms Per Liter
MSWLF Municipal Solid Waste Landfill Facility
NC2L North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDENR North Carolina Department of Environmental and Natural Resources RCRA Resource Conservation and Recovery Act SAP Sampling and Analysis Plan
SSI Statistically Significant Increase
USACE US Army Corps of Engineers
VOCs Volatile Organic Compounds

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May 2016 (N=39) GROUNDWATER, SURFACE-WATER, AND METHANE MONITORING REPORT FOR
LONGSTREET ROAD MSW LANDFILL
NCDENR LANDFILL PERMIT #26-02 FORT BRAGG, NORTH CAROLINA

1.0 INTRODUCTION
The report for the groundwater, surface-water, and methane monitoring for the
Longstreet Landfill (Figure 1) was performed by the United States Army Corps of
Engineers (USACE), Savannah District in May 2016. The monitoring is required by the
North Carolina Department of Environmental and Natural Resources (NCDENR) Solid
Waste Management Division. This is the thirty-ninth (N=39) monitoring event for the
site. This report summarizes the methods used for the groundwater, surface-water, and
methane monitoring and presents the results of the sampling event.

3.2 Project Background

The Longstreet Road landfill is a closed Municipal Solid Waste Landfill Facility
(MSWLF) located north of Longstreet Road at Fort Bragg in Cumberland County, North
Carolina. The landfill was closed on August 3, 1999. Figure 1 is a map of the site
location. The United States Army Corps of Engineers (USACE), Savannah District has
been contracted by the Fort Bragg Directorate of Public Works (DPW) to conduct water
quality and methane sampling for the Environmental Branch to satisfy the permit and the
Sampling and Analysis Plan (SAP) requirements. Groundwater, surface-water, and
methane monitoring locations are shown on Figure 2. The current SAP, approved by
NCDENR, includes sampling nine groundwater monitoring wells, two surface-water
stations, fifteen methane monitoring wells and four buildings for methane. The
groundwater monitoring wells are SLMW-6, SLMW-7R, SLMW-8R, SLMW-9R,
SLMW-10, SLMW-11R, SLMW-12AR, SLMW-12BR, and SLMW-13R; the surface-
water stations are SW-1 & SW-2; the methane monitoring wells are GP-1R2, GP-2R,
GP-3R, GP-4R, GP-5R, GP-6, GP-7, GP-8R, GP-9R, GP-10R, GP-11R2, GP-12R2, GP-
13R2, GP-14R2, and GP-15R2; and the buildings are O-9388, O-9389, the former scale
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house, and the wash rack control booth ( O-9382). In May 2015 three groundwater
monitoring wells were installed to the south and east, SLMW-14, SLMW-15 and SLMW-
16. All sampling was conducted according to North Carolina Solid Waste Management
Guidelines.

3.3 Project Scope

The scope for this project included collecting groundwater samples from the nine
wells identified in the SAP as well as the three wells that were installed in May 2015.
Groundwater samples were analyzed for all Appendix I and triggered Appendix II
constituents. The scope also included collecting two surface-water samples for all
Appendix I & II constituents, performing methane monitoring at 15 methane monitoring
wells and four buildings on site, evaluating the analytical results, and reporting the results
of the investigation. The groundwater sampling and data analyses included obtaining
field parameter measurements (i.e. pH, temperature, etc.), measuring water levels at the
monitoring well locations, determining groundwater flow directions, validating
laboratory analytical data, performing statistical analyses for each detected constituent as
required by NC regulations, and determining the concentration changes of chemicals of
concern (COCs) with time.

2.0 PROJECT HISTORY

2.1 Site Description

The MSWLF is located north of Longstreet Road at Fort Bragg in Cumberland
County, North Carolina. Figures 1 and 2 show the site location and layout. The MSWLF
is west of the main post and east of Cooleyconch Mountain. Cooleyconch Mountain is
the prominent terrain feature west of the main post. A vehicle washing facility borders
the site to the east, the Lamont Road LCID and C&D Landfills are approximately 1.5
miles west/northwest of the site (on the west side of Cooleyconch Mountain).

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2.2 General Site Geology and Hydrology

Lithologic descriptions of soil borings and monitoring well borings from previous
investigations at Fort Bragg indicate that in general Fort Bragg is underlain by alternating
sands, silty sands, clayey sands, sandy clays, and clays, likely belonging to the
Middendorf Formation. The sands and silty sands range in thickness from
approximately 2 to 22 ft and are coarse grained. The clay units range in thickness from
approximately 2 to 7 ft and are typically plastic.

2.3 Previous Investigation and Results

Several sampling events have been conducted at the Landfill. Initially, four
monthly sampling events were conducted in July, August, September, and October 1996
by R, S & H Architect, Engineering, & Planning, Inc. Law & Company, Inc. conducted
two sampling events in March and September, 1999 in conjunction with the installation
of new wells. Then until 2005, sampling events were conducted by BPA Environmental
& Engineering, Inc. The USACE has monitored the site since 2005.

The previous sampling event, held in May 2015 for Longstreet Landfill, was
conducted by the USACE, Savannah District. Low levels of VOCs, SVOCs, pesticides
and Appendix II inorganics were detected, but most detections were below NC2L
standards. Monitoring wells, SLMW-8R, SLMW-9R, SLMW-10, SLMW-14 and
SLMW-16, contained analytes above the NC2L standard. These wells remain in
assessment monitoring.

3.0 METHODS
3.1 Methane Monitoring
Methane monitoring was performed at 15 wells and 4 buildings. The monitoring
included measuring levels of methane, carbon dioxide, hydrogen sulfide and oxygen at
each of the locations. The results of the monitoring are summarized in Table 1 and are
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also presented on Figure 3.

3.2 Water-Level Gauging
During this sampling event, USACE personnel measured the water levels in 9
monitoring wells. Measured water levels and calculated groundwater elevations are
presented in Table 2. A Potentiometric map was developed based on the groundwater
elevations; the map is presented as Figure 4. The map shows that the general direction of
the groundwater flow at the Longstreet Landfill is towards the east-southeast.
3.3 Groundwater and Surface-Water Sampling
The groundwater sampling was conducted in accordance with the SAP for the
Longstreet Road MSWLF (NCDENR Landfill Permit #26-02, which has been updated to
reflect the most recent SAP). Groundwater samples were collected from nine monitoring
wells and two surface-water stations. Water quality parameters pH, specific conductivity,
temperature, turbidity, dissolved oxygen (DO), and oxidation-reduction potential (ORP)
were measured during the purge cycle of each well and prior to sampling the surface-
water stations. The measurements are summarized in Table 3.

The surface-water sampling was conducted using a peristaltic pump. The water to
be collected for VOC analysis was not allowed to pass through the head of the pump,
instead the tubing was filled and the flow was reversed to fill the bottles. Groundwater
samples were collected using a low-flow purge method with a bladder pump.
Immediately before purging a well, the static water level below the top of the well casing
and the total depth of the well were measured to the nearest 0.01 foot and recorded in the
field notebook. The volume of water in the well was calculated based on the static water
level and the well construction information. Well volume calculations were placed in the
field notebook. The inlet of the sampling pump was placed at the mid-point of the
screened interval. This level was adjusted for wells where the static water level is within
the well screen. The monitoring wells were purged using a variable-flow bladder pump at
a rate of 500 ml/min or less.

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The wells were purged until the water quality had stabilized or five purge volumes
were removed. The wells were considered stable when the following requirements were
met for three consecutive readings: turbidity values within 10% or lower than 10
Nephelometric Turbidity Units (NTUs), temperature values within a range of 0.5 degrees
Celsius, pH readings within 0.1 Standard Units (SU), ORP values within a range of 10
millivolts (mV), and conductivity values within 3%, and DO values within 10%.

The rate of pumping was determined and noted in the field notebook. The purge
rate was adjusted, as necessary, to avoid purging any well to dryness and to equal the
recharge of the aquifer. All sampling equipment was protected from contaminated soil
surfaces to prevent contamination of the samples (e.g., equipment may be placed on
disposable polyethylene plastic sheeting). Groundwater samples were collected after
purging was complete. The tubing was disconnected from the flow through cell and the
samples were collected from the pump outlet. The samples were labeled and placed into
an ice-filled cooler for preservation.

Groundwater sampling data (including sample number, location, quantity of water
purged, field parameters, site conditions, etc.) were documented in the field notebook.
Water samples for Resource Conservation and Recovery Act (RCRA) metal analyses
were un-filtered. The results of the groundwater sampling are presented in Appendix D
and on Figure 5. The groundwater sampling field data logs are presented in Appendix A.

3.4 Investigation Derived Wastes Handling The investigation derived wastes (IDW), including the waste water from well
purging and decontamination water, were containerized in 55-gallon drums. Those
drums were appropriately labeled, sealed, and staged within designated areas until
analytical results had been received and reviewed. Based on the analytical results of the
groundwater samples, the IDW was classified as non-hazardous. With the concurrence of
the Fort Bragg Installation Restoration Program Manager, the IDW was disposed of at an
appropriate disposal facility.

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4.0 ANALYTICAL RESULTS AND STATISTICAL ANALYSIS
4.1 Analytical Data Summary Groundwater samples were analyzed for VOCs, SVOCs, Pesticides, PCBs,
Organophosphorus Pesticides, and Appendix II Inorganics. The surface-water samples
were analyzed for all Appendix I and Appendix II constituents. The summary of
detections of the COCs is presented in Appendix D. Figure 5 shows the distribution of
the detections and their concentrations from this sampling event. The laboratory reports
of analytical results are included as Appendix B. For comparison, the analytical results
of previous investigations are also presented in the Statistical Analyses Summary Report
included in Appendix C. For comparison, the analytical results of previous
investigations are presented in Appendix D.

In accordance with North Carolina guidance, analytical results are compared to
North Carolina Groundwater 2L Standards (NC2L standards) or the North Carolina
Surface Water 2B Standards (NC2B standards). The analytical data of the first 2016
sampling event indicate that some VOCs and inorganics were detected at low levels, and
most detections were below NC2L or NC2B standards (Appendix D). Five sampling
locations had detections exceeding the remedial standards: wells SLMW-8R, SLMW-9R,
SLMW-11R, SLMW-14, and SLMW-16. A summary of the analytical results for each
of those wells are as follows:

• Well SLMW-8R
Two compounds were detected above the 2L standard as listed below:
Compound 2L Concentration
Benzene 1 µg/L 2.3 µg/L Vinyl Chloride 0.03 µg/L 5.5 µg/L
No other constituents were above their 2L standards.

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• Well SLMW-9R
Two compounds were detected above the 2L standard as listed below:
Compound 2L Concentration Benzene 1 µg/L 2.5 µg/L
Arsenic 10 µg/L 24 µg/L

No other constituents were above their 2L standards.

• Well SLMW-11R
Four compounds were detected above the 2L standards as listed below:
Compound 2L Concentration Benzene 1 µg/L 1.6 µg/L
Tetrachloroethene 0.7 µg/L 1.3 µg/L
Trichloroethene 3 µg/L 4.2 µg/L
Vinyl Chloride 0.03 µg/L 0.6 J µg/L
No other constituents were above their 2L standard.

• Well SLMW-14
One compound was detected above the 2L standard as listed below:
Compound 2L Concentration Vinyl Chloride 0.03 µg/L 1.5 µg/L

No other constituents were above their 2L standard.

• Well SLMW-16
Three compounds were detected above the 2B standard as listed below:
Compound 2L Concentration Benzene 1 µg/L 2.8 µg/L
Vinyl Chloride 0.03 µg/L 2.5 µg/L
Arsenic 10 µg/L 15 µg/L

No other constituents were above their 2B standard.

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Though samples had constituent detections above method detection limits, all
other detections were below the respective NC2L and NC2B standards and most
detections were estimated values that were detected above the method detection limits but
below the reporting limit (Appendix D).

4.2 Statistical Analysis Results
A statistical test predicts the average behavior (distribution) of a random variable
by comparing the means (normal distribution) or medians (lognormal and non-parametric
distributions) of the compliance well data to background well data. Different statistical
tests were used as appropriate for the different distributional patterns that occur within
the data. Prior to testing for statistical significance, the distribution of each parameter
was determined to be normal, lognormal, or non-normal.
If the data were non-normally distributed, or the fraction of nondetects exceeded
15% but were less than 90%, then the Kruskal-Wallis Test was applied. However, the
Kruskal-Wallis test is prone to false positives. Therefore, additional statistical analyses
were used to determine the validity of the positive results. If the fraction of non-detects
exceeded 90%, then the Non-Parametric Prediction Limit was applied. Intra-well
comparisons of data from a single well to previous data from the same well were
performed to confirm if a trend of increasing concentration is occurring. The Mann-
Kendall Trend Analysis and the Shewhart-CUSUM Control Chart statistical tests were
selected for these additional analyses.
A detailed discussion of the statistical methods is presented in Appendix C. The
results of the analysis indicated that the samples collected at the Longstreet Road
Municipal Solid Waste Landfill indicated evidence that statistically significant increases
(SSIs) were still present in a few wells and that assessment monitoring should continue.
According to North Carolina Administrative Code Title 15A Chapter 13 Subchapter
B Section 1634 paragraph f [15A NC3AC 13B.1634 (f)], assessment monitoring shall
continue if Appendix II parameters are detected at statistically significant levels above
background. Assessment monitoring will have to continue at the landfill until the
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presence of no SSIs is confirmed in two consecutive monitoring events.

4.3 Methane Monitoring Results
Methane monitoring was performed at 15 wells and 4 buildings. The monitoring
included measuring levels of methane, carbon dioxide, hydrogen sulfide and oxygen at
each of the locations. The results of the monitoring are summarized in Table 1 and are
also presented on Figure 3. One methane monitoring well contained methane at a
concentration above 5% by volume, GP-14R2 (9.6% by volume). No other monitoring
points or buildings contained high levels of methane (> 5% methane by volume).

5.0 CONCLUSIONS AND RECOMMENATIONS
The annual monitoring program consists of two sampling events (this was the first
of 2016) conducted six months apart. This was the N=39 sampling event for the
Longstreet Road Landfill. Low levels of VOCs, SVOCs, and Appendix II inorganics
were detected, but most detections were at estimated levels and/or were below remedial
standards. Analytes were detected above the NC2L standards at monitoring wells
SLMW-8R, SLMW-9R, SLMW-11R, SLMW-14, and SLMW-16.
According to the Statistical Analysis of groundwater Data (Appendix D), the
results of the analysis indicated that several locations at the Longstreet Road Municipal
Solid Waste Landfill had statistically significant increases (SSIs).
According to North Carolina Administrative Code Title 15A Chapter 13
Subchapter B Section 1634 paragraph f [15A NC3AC 13B.1634 (f)], assessment
monitoring shall continue if Appendix II parameters are detected at statistically
significant levels above background. Assessment monitoring will continue until no SSIs
are confirmed in two consecutive sampling events.
The methane levels were measured at 19 locations at Longstreet. One methane
monitoring well contained methane at a concentration above 5% by volume, GP-14R2
(9.6% by volume). No other monitoring points or buildings contained high levels of
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methane (> 5% methane by volume).

6.0 REFERENCES

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, Subchapter 13B, Solid
Waste Management, Section .1600 (January 4, 1994).

North Carolina Administrative Code, Title 15A, Department of Environment, Health, and
Natural Resources, Division of Solid Waste, Management, SubchapterNC2L,
Classifications and Water Quality Standards Applicable to the Groundwaters of
North Carolina, Sections .0100, .0200, and .0300 (November 8, 1993): from the
Environmental Management Commission, Raleigh, North Carolina.
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FIGURES
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Site Map -- Ft. Bragg, NC
U.S. ARMY ENGINEER DISTRICTCORPS OF ENGINEERSSAVANNAH, GEORGIA
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DATE: JULY 2016 FIGURE: 2
LONGSTREET ROAD LANDFILL
LOCATION MAP
FORT BRAGG, NC
$0 350 700175'
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DATE: JULY 2016 FIGURE: 3
LONGSTREET ROAD LANDFILL
METHANE MONITORING RESULTSNOVEMBER 2015
FORT BRAGG, NC
$0 400 800200'
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0.1% Methane
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0.1% Methane
0.1% Methane
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DATE: JULY 2016 FIGURE: 4
LONGSTREET ROAD LANDFILL
POTENTIOMETRIC SURFACE MAPMAY 2016
FORT BRAGG, NC
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TABLES
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Monitoring Date:Facility Name:Facility Permit #:Monitoring Personnel (Name/Position):
NC Landfill Rule:Monitoring Personnel (Name/Position):County (Location):Equipment Field Calibrated by:
Equipment Type:Manufacturer Cal/Service Date:Equipment Serial #:Date/Time of Field Calibration:
Calibration Gas:Cal Gas Expiration Date:Meter pump rate:
Gas Monitoring Wells
Time Initial %CH4 Initial %LEL Purge Time Stable %CH4 Stable %LEL Stable *H2S Stable %O2 Stable %CO2
1433 0 1434 0.1 0 12.1 8.8
1505 0 1506 0 0 17.5 4.5
1509 0 1510 0.1 0 15.9 5.1
1515 0.1 1516 0.1 0 16.9 3
1556 0 1557 0 0 20.1 0.8
1520 0.1 1521 0.1 0 14.6 5.9
1525 0.1 1526 0.1 0 7.6 11.3
1536 0.1 1537 0.1 0 8.9 11.7
1543 0.1 1544 0.1 0 13.7 6
1456 0 1457 0.1 0 19.3 0.9
1452 0 1453 0.1 0 19.3 1.4
1449 0.1 1450 0.1 0 17.8 2.2
1447 0.1 1448 0.1 0 18.7 1.1
1443 0 1444 9.6 0 1 9.6
1439 0.1 1440 0.1 0 18.6 1.4
Notes:
H2S recorded in ppm
Gas MW-9R
Periodic Methane Monitoring Report
Monitoring Point ID
Gas MW-7
Gas MW-12R2
Gas MW-1R2
Gas MW-3R
Gas MW-4R
Gas MW-5R
Gas MW-6
Gas MW-8R
Gas MW-2R
Gas MW-14R2
Gas MW-10R
Gas MW-11R2
Gas MW-13R2
Gas MW-15R2
Longstreet Road MSW LandfillJ. Wood-Physical Scientist
M. Senktas-ChemistJ. Wood
May 14,2016 1230
#26-02May 14,2016
0.1600
5-Aug-19CH4-50% CO2-35% O2-4%
GM 12051109GEM 2000
Cumberland
May 9,2016
Table 1.
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Facility Structures
Time Initial %CH4 Initial %LEL Purge Time Stable %CH4 Stable %LEL Stable *H2S Stable %O2 Stable %CO2
1606 0 1607 0 0 21 0
1546 0.1 1547 0.1 0 21 0
1549 0 1550 0 0 21 0
1550 0 1551 0 0 21 0
Drawings identifying location where each building sampled (include north arrow):
Climatic/Physical Conditions at Site
a. Soil Conditions:
b. Weather Conditions:
c. Temperature:
d. Barometric Conditions:Rising Falling Steady Reading:29.8 (mmHg)
e. Relative Humidity within range of 10%-90%? Yes Value:
f. Condition and Access: Are all monitoring points identified in the field (signage) in accordance
with approved monitoring plan; are they secured; has the owner/operator maintained access? Yes
O-9389
O-9389
O-9382
O-9388
40%
If no, explain in space provided below.
85°F
Sunny
Monitoring Point ID
Former Scalehouse
Samples must be collected under normal/average conditions of temperature, pressure, and climate for the season. Barhole punch sampling
should not be performed during or immediately after rain events, or when soils are saturated or frozen. All sampling must be performed after
12:00 pm (subsurface gases have a diurnal cycle and generally are at a maximum during the afternoon), and preferably when barometric
conditions are not rising (subsurface gas pressures will be less than atmospheric pressure under these conditions and gas will therefore not
migrate), or representative samples may not be obtained. Barometric information can be obtained from many locations (i.e.
http://weather.noaa.gov).
O-9388
O-9382Former Scale House
N
N
N
N
X
X
X
X
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Additional Comments:
Certification:
Geologist
SIGNATURE TITLE
g. If stressed vegetation is noted, describe the extent and location in the space provided below.
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. I am
Description of Sampling Techniques: (e.g., wells are vented or not, barhole punch methodology, etc.)
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Table 2. Summary of GroundwaterElevations Longstreet Landfill, Fort Bragg, NC
Nov-08 Nov-08 Jun-09 Jun-09 Nov-09 Nov-09 Jun-10 Jun-10 Nov-10 Nov-10 Jun-11 Jun-11 Nov-11 Nov-11 May-12 May-12 Nov-12 Nov-12 May-13 May-13 Nov-13 Nov-13 May-14 May-14 May-15 May-15 Nov-15 Nov-15 May-16 May-16
SLMW-6 293.55 26.27 267.28 26.11 267.44 28.22 265.33 25.08 268.47 28.02 265.53 30.31 263.24 31.55 262.00 30.84 262.71 30.72 262.83 29.75 263.8 27.4 266.15 25.6 267.95 26.27 267.28 25.73 267.82 21.5 272.05
SLMW-
7R**289.74 20.76 269.74 20.59 269.91 22.19 268.31 20.43 270.07 22.14 268.36 21.86 268.64 22.06 268.44 21.78 267.96 22.28 267.46 20.89 268.85 21.89 267.85 20.27 269.47 20.61 267.13 21.14 268.6 21 268.74
SLMW-
8R**289.4 22.91 267.43 23.03 267.31 24.21 266.13 22.91 267.43 24.31 266.03 24 266.34 24.3 266.04 24.15 265.25 24.3 265.10 22.95 266.45 23.8 265.6 21.77 267.63 22.47 266.93 22.1 267.3 22.93 266.47
SLMW-
9R**288.44 38.31 251.23 37.3 252.24 38.72 250.82 36.66 252.88 38.34 251.2 40.2 249.34 41.75 247.79 42.53 245.91 43.51 244.93 42.9 245.54 41.5 246.94 36.68 251.76 38 250.44 37.15 251.29 36.03 252.41
SLMW-
10 305.99 19.42 286.57 19.59 286.4 20.39 285.6 19.7 286.29 20.59 285.4 20.57 285.42 20.87 285.12 20.8 285.19 20.86 285.13 20.14 285.85 19.8 286.19 30.97 275.02 19.21 286.78 17.7 288.29 18.9 287.09
SLMW-
11R 354.61 78.96 278.84 77.62 280.18 79.2 278.6 74.31 283.49 76.42 281.38 81.12 276.68 82.13 275.67 83.14 271.47 83.92 270.69 84.44 270.17 86.7 267.91 80.02 274.59 78.96 275.65 79.39 275.22 75.04 279.57
SLMW-12AR 243.36 8.45 234.91 9.03 234.33 9.53 233.83 8.75 234.61 9.44 233.92 8.65 23.71 9.6 233.76 9.45 233.91 9.92 233.44 8.5 234.86 9.7 233.66 8.02 235.34 8.69 234.67 7.56 235.8 8.4 234.96
SLMW-
12BR 243.42 9.23 234.19 8.09 235.33 9.2 234.22 8.79 234.63 9.19 234.23 9.25 234.17 9.61 233.81 9.52 233.9 10 233.42 9.72 233.7 9.8 233.62 9.23 234.19 9.18 234.24 8.98 234.44 8.73 234.69
SLMW-
13R**340.42 53.14 286.88 51.9 288.12 53.29 286.73 50.58 289.44 53.05 286.97 55.07 284.95 56.91 283.11 ****60.45 279.97 56.7 283.75 54.85 285.57 53.86 286.56 54.28 286.14 50.05 290.37
SLMW-
14 265.22 NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI 16.63 NA 15.13 NA 14.75 250.47
SLMW-15 304.48 NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI 29.05 NA 29.15 NA 40.49 263.99
SLMW-
16 279.47 NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI NI 29.08 NA 28.06 NA 27.16 252.31
Note:
* - well was dry
** - Elevation is for replacement well but data is for original well up through May 2013
NA-Not Available-New wells were not surveyed at the time of sampling
NI-Not Installed
Water Level
(ft. BTOC)
Water
Level Elev. (ft.
amsl)
Water
Level (ft.
BTOC)
Water
Level Elev. (ft.
amsl)
D --- Selected Well for Long Term Monitoring
TOC – Top of casing
bgs – Below ground surface,
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
TOC elevation is based on vertical datum NGVD29 (source: USGS RFI, Aug. 1999)
btoc – below top of casing
amsl – above mean sea level
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)Well ID TOC Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
Water Level Elev.
(ft. amsl)
Water Level
(ft. BTOC)
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Table 3. Field Parameter Measurements Longstreet Landfill, Fort Bragg, NC

Sample Specific Temperature Turbidity Dissolved
Well Identification pH Conductivity (µs/cm) (°C) (N.T.U.) Oxygen (mg/L) ORP
SLMW-6 SLMW-6-5-16 4.88 0.020 17.69 1.47 1.34 131.2
SLMW-7R SLMW-7R-5-16 5.94 0.445 19.05 22.3 1.31 -40.5
SLMW-8R SLMW-8R-5-16 5.92 0.549 21.12 3.57 1.56 -23.3
SLMW-9R SLMW-9R-5-16 6.36 1.125 18.78 9.7 1.24 -121.2
SLMW-10 SLMW-10-5-16 6.27 0.904 17.06 4.93 1.75 -74.6
SLMW-11R SLMW-11R-5-16 5.88 0.154 18.26 6.63 1.61 -11.2
SLMW-12AR SLMW-12AR-5-16 2.63 0.036 19.06 6.14 3.56 200.0
SLMW-12BR SLMW-12BR-5-16 4.77 0.069 20.83 7.06 2.24 127.0
SLMW-13R SLMW-13R-5-16 4.66 0.016 17.55 9.48 10.11 219.0
SLMW-14 SLMW-14-5-16 5.88 0.483 17.47 8.53 2.10 -40.8
SLMW-15 SLMW-15-5-16 4.62 0.020 17.46 9.9 6.24 242.3
SLMW-16 SLMW-16-5-16 6.14 1.038 18.61 17.3 1.65 -111.8
SW-1* SW-1-5-16 -- -- -- -- -- --
SW-2* SW-2-5-16 -- -- -- -- -- --
Note:
N.T.U. --- Nephelometric Turbidity Unit
ORP --- Oxidation Reduction Potential

NS - Not Sampled
* - Not recorded

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APPENDIX A
GROUNDWATER SAMPLING LOGS
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 18 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 910
WEATHER CONDITIONS: Overcast, light mist, 64°

Location: Longstreet Landfill Sample ID: SLMW-11R-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):86.7 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):75.04 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.91 (gallons)
Flow Rate:444.71 (ml/min)Purge Vol:4.0 (gallons)
Length of Time Purged:34 (minutes)Purge Time:836
Amount Purged:4 (gallons)Pump Depth:84
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 855 858 901 904 907
pH 5.84 5.85 5.86 5.86 5.88
Cond 0.150 0.150 0.153 0.153 0.154
Temp. °C 18.26 18.28 18.26 18.26 18.24
Turbidity 16.8 10.0 6.63 - -
DO 2.07 1.90 1.78 1.66 1.61
ORP -15.3 -13.7 -12.8 -12.2 -11.2
Water Level 75.21 75.21 75.21 75.21 75.21

5. NOTES: EQB Blank taken here
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 17 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 1210
WEATHER CONDITIONS: Overcast, 65˚

Location: Longstreet Landfill Sample ID: SLMW-13R-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):67 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):50.05 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.78 (gallons)
Flow Rate:446.73 (ml/min)Purge Vol:6.5 (gallons)
Length of Time Purged:55 (minutes)Purge Time:1115
Amount Purged:6.5 (gallons)Pump Depth:65
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1152 1155 1158 1201 1204
pH 4.64 4.65 4.65 4.65 4.66
Cond 0.016 0.015 0.016 0.015 0.016
Temp. °C 17.54 17.55 17.53 17.55 17.55
Turbidity 77.2 19.0 15.0 14.4 9.48
DO 9.98 9.97 10.03 9.99 10.11
ORP 213.6 214.9 216.4 218.0 219.0
Water Level 50.07 50.07 50.07 50.07 50.07

5. NOTES:
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 13 May 2016
SAMPLED BY: J. Wood & R. Hill TIME : 1350
WEATHER CONDITIONS: Overcast, 73˚

Location: Longstreet Landfill Sample ID: SLMW-8R-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):32.78 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):22.93 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.62 (gallons)
Flow Rate:160.85 (ml/min)Purge Vol:2.0 (gallons)
Length of Time Purged:47 (minutes)Purge Time:1303
Amount Purged:2 (gallons)Pump Depth:28
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1325 1330 1335 1340 1345
pH 5.88 5.88 5.89 5.91 5.92
Cond 0.496 0.509 0.523 0.541 0.549
Temp. °C 20.84 21.11 21.13 21.44 21.12
Turbidity 6.94 5.67 4.24 3.57 -
DO 1.74 1.69 1.64 1.59 1.56
ORP -14.0 -17.0 -20.0 -23.3 -23.3
Water Level 23.40 23.98 24.30 24.57 -

5. NOTES:
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 13 May 2016
SAMPLED BY: R. Hill & J. Wood TIME : 1650
WEATHER CONDITIONS: Sunny, 78˚

Location: Longstreet Landfill Sample ID: SLMW-7R-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):32.25 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):21 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.85 (gallons)
Flow Rate:289.8 (ml/min)Purge Vol:5.8 (gallons)
Length of Time Purged:75 (minutes)Purge Time:1535
Amount Purged:5.75 (gallons)Pump Depth:29
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1633 1636 1639 1642 1645 1648
pH 5.49 5.93 5.93 5.93 5.94
Cond 0.444 0.444 0.444 0.444 0.445
Temp. °C 19.50 19.48 19.22 19.12 19.05
Turbidity 63 26.9 31.3 21.7 22.3
DO 1.32 1.31 1.32 1.31 1.31
ORP -43.3 -42.2 -41.5 -40.8 -40.5
Water Level 22.07 22.20 22.25 22.29 22.33

5. NOTES: Purges >3 times volume. Turbidity stable.
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 15 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 1600
WEATHER CONDITIONS: Clear, 73˚

Location: Longstreet Landfill Sample ID: SLMW-10-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):27.76 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):18.9 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.45 (gallons)
Flow Rate:437.68 (ml/min)Purge Vol:4.4 (gallons)
Length of Time Purged:38 (minutes)Purge Time:1522
Amount Purged:4.4 (gallons)Pump Depth:25.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1543 1546 1549 1552 1555
pH 6.26 6.27 6.26 6.27 6.27
Cond 0.910 0.905 0.900 0.901 0.904
Temp. °C 16.87 16.93 16.87 16.95 17.06
Turbidity 21.4 12.3 7.68 4.93 -
DO 2.15 2.00 1.89 1.83 1.75
ORP -70.8 -71.5 -72.5 -73.2 -74.6
Water Level 19.86 20.00 19.96 - -

5. NOTES:
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 1050
WEATHER CONDITIONS: Sunny 60˚

Location: Longstreet Landfill Sample ID: SLMW-9R-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):54.7 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):36.03 (ft)Diameter (d):0.167 (ft)
40.28 e = (5.904 x d2(wd-dw)) =3.06 (gallons)
Flow Rate:428.4 (ml/min)Purge Vol:8.5 (gallons)
Length of Time Purged:75 (minutes)Purge Time:935
Amount Purged:8.5 (gallons)Pump Depth:52.5
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1030 1033 1036 1039 1042 1045
pH 6.37 6.37 6.37 6.37 6.36 6.36
Cond 1.135 1.134 1.131 1.131 1.127 1.125
Temp. °C 18.91 18.92 18.90 18.94 18.85 18.78
Turbidity 274 - 48.8 39.4 24.3 9.7
DO 1.30 1.26 1.27 1.25 1.28 1.24
ORP -120.7 -119.6 -118.8 -121.2 -124.2 -121.2
Water Level 36.03 36.03 36.03 36.03 36.03 36.03

5. NOTES: Dup-1 taken here
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 17 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 945
WEATHER CONDITIONS: Overcast/light rain 63°

Location: Longstreet Landfill Sample ID: SLMW-6-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):37.8 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):25.1 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.08 (gallons)
Flow Rate:378 (ml/min)Purge Vol:3.5 (gallons)
Length of Time Purged:35 (minutes)Purge Time:910
Amount Purged:3.5 (gallons)Pump Depth:35
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 929 932 935 938 941
pH 4.82 4.83 4.84 4.86 4.88
Cond 0.022 0.022 0.021 0.021 0.020
Temp. °C 17.54 17.54 17.58 17.65 17.69
Turbidity 10.7 1.97 - - 1.47
DO 1.51 1.51 1.46 1.39 1.34
ORP 122.7 123.6 127.2 129.7 131.2
Water Level 25.35 25.35 25.35 25.35 25.35

5. NOTES: MS/MSD taken here
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 12 May 2016
SAMPLED BY: J. Wood, M. Senktas TIME : 1525
WEATHER CONDITIONS: Sunny 78°

Location: Longstreet Landfill Sample ID: SLMW-12BR-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):64.7 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):8.73 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =9.18 (gallons)
Flow Rate:137.68 (ml/min)Purge Vol:5.5 (gallons)
Length of Time Purged:151 (minutes)Purge Time:1254
Amount Purged:5.5 (gallons)Pump Depth:58
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1508 1511 1514 1517 1520
pH 4.76 4.76 4.77 4.77 4.77
Cond 0.068 0.069 0.069 0.069 0.069
Temp. °C 20.51 20.59 20.66 20.74 20.83
Turbidity 16.8 - - - 7.06
DO 1.76 1.96 2.05 2.13 2.24
ORP 125.0 125.6 126.0 126.5 127.0
Water Level 9.1 15.7 24.1 - -

5. NOTES:
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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 12 May 2016
SAMPLED BY: J. Wood, M. Senktas TIME : 1345
WEATHER CONDITIONS: Sunny, 78˚

Location: Longstreet Landfill Sample ID: SLMW-12AR-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):19.9 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):8.4 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.89 (gallons)
Flow Rate:504 (ml/min)Purge Vol:6.0 (gallons)
Length of Time Purged:45 (minutes)Purge Time:1300
Amount Purged:6 (gallons)Pump Depth:18
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1331 1334 1337 1340 1343
pH 2.43 2.50 2.68 2.65 2.63
Cond 0.034 0.034 0.035 0.035 0.036
Temp. °C 19.17 19.21 19.30 18.88 19.06
Turbidity 40.7 15.8 - - 6.14
DO 3.63 3.68 3.76 3.71 3.56
ORP 190.2 189.8 183.3 189.7 200.0
Water Level 9.80 9.80 9.80 9.80 9.80

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U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 15 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 1430
WEATHER CONDITIONS: Sunny, 65˚

Location: Longstreet Landfill Sample ID: SLMW-15-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):26.33 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):40.49 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =-2.32 (gallons)
Flow Rate:414.88 (ml/min)Purge Vol:4.5 (gallons)
Length of Time Purged:41 (minutes)Purge Time:1349
Amount Purged:4.5 (gallons)Pump Depth:38
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1414 1417 1420 1423 1426
pH 4.53 4.55 4.59 4.62 4.62
Cond 0.020 0.020 0.020 0.020 0.020
Temp. °C 17.21 17.24 17.35 17.45 17.46
Turbidity 27.4 14.7 9.9 - -
DO 6.22 6.20 6.17 6.17 6.24
ORP 235.0 237.6 239.0 240.6 242.3
Water Level 27.09 27.22 27.29 27.29 27.29

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SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 1345
WEATHER CONDITIONS: Sunny, 74˚

Location: Longstreet Landfill Sample ID: SLMW-16-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):37.26 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):27.16 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =1.66 (gallons)
Flow Rate:417.27 (ml/min)Purge Vol:8.5 (gallons)
Length of Time Purged:77 (minutes)Purge Time:1228
Amount Purged:8.5 (gallons)Pump Depth:35
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1328 1331 1334 1337 1340 1343
pH 6.14 6.14 6.14 6.14 6.14 6.14
Cond 1.025 1.025 1.028 1.043 1.042 1.038
Temp. °C 18.49 18.56 18.55 18.55 18.52 18.61
Turbidity >1000 29.9 26.7 27.3 23.1 17.3
DO 1.71 1.70 1.69 1.66 1.66 1.65
ORP -111.7 -111.2 -111.2 -111.7 -111.7 -111.8
Water Level 27.23 27.23 27.23 27.23 27.23 27.23

5. NOTES: Purged >5 times volume

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SAVANNAH DISTRICT
GEOLOGY and HYDROGEOLOGY

GROUNDWATER
FIELD DATA LOG

1. CLIENT: Fort Bragg DATE: 16 May 2016
SAMPLED BY: J. Wood & P. Bazemore TIME : 1530
WEATHER CONDITIONS: Sunny, 75˚

Location: Longstreet Landfill Sample ID: SLMW-14-5-16

PRESERVATIVE: Ice, HNO3 & NaOH
ANALYSES REQUESTED: EPA 8260B, 6020_App II, 300-Nitrate, 8181-8082, 8151A, 8270D, 9034, 9012B
& 8140B
# OF CONTAINERS: 14
SAMPLING METHOD: Peristaltic Pump LOW FLOW: YES NO
Bladder Pump DUPLICATE SAMPLE: YES NO
SAMPLES FILTERED: YES NO

2. WATER LEVEL DATA
MEASURING POINT: Top of casing Other:
METHOD OF MEASUREMENT: Water Level Indicator

3. WELL EVACUATION DATA
Well Depth (wd):29.05 (ft)Diameter (d):2.00 (in)
Depth to Water (dw):14.75 (ft)Diameter (d):0.167 (ft)
Well Volume = (5.904 x d2(wd-dw)) =2.35 (gallons)
Flow Rate:529.2 (ml/min)Purge Vol:7.0 (gallons)
Length of Time Purged:50 (minutes)Purge Time:1440
Amount Purged:7 (gallons)Pump Depth:27
4. FIELD PARAMETERS
INSTRUMENT CALIBRATED
pH Meter –YSI 556MPS
Conductivity Meter – YSI 556MPS
Temperature – YSI 556MPS
Turbidity Meter – Hach 2100 Q
DO Meter – YSI 556MPS
ORP Meter – YSI 556MPS
CO2– Hach Digital Titrator

Time 1511 1514 1517 1520 1523
pH 5.81 5.82 5.83 5.86 5.88
Cond 0.452 0.455 0.464 0.473 0.483
Temp. °C 17.53 17.42 17.34 17.39 17.47
Turbidity 35.1 15.6 8.92 8.53 -
DO 2.21 2.19 2.20 2.11 2.10
ORP -25.5 -27.9 -32.7 -36.6 -40.8
Water Level 15.78 15.78 15.78 15.78 15.78

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APPENDIX B

CHAINS OF CUSTODY & LAB ANALYTICAL REPORTS
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-125233-1
Client Project/Site: Ft.Bragg - Longstreet Landfill
For:
U.S. Army Corps of Engineers
100 W. Oglethorpe Ave.
Savannah, Georgia 31401
Attn: John P. Markov
Authorized for release by:
5/26/2016 2:58:04 PM
Robert Bearden, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
TestAmerica Job ID: 680-125233-1
Page 2 of 43 TestAmerica Savannah5/26/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125233-1
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-125233-1
Laboratory: TestAmerica Savannah
Narrative
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Longstreet Landfill
Report Number: 680-125233-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 05/13/2016; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.3 C.
SEMIVOLATILE ORGANIC COMPOUNDS (AQUEOUS)
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for Semivolatile Organic Compounds (Aqueous) in accordance with EPA
SW-846 Method 8270D. The samples were prepared on 05/18/2016 and analyzed on 05/24/2016.
The continuing calibration verification (CCV) analyzed in batch 680-434682 was outside the method criteria for the following analyte(s):
2-Methylnaphthalene and Nitrobenzene. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and
found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected
analyte(s) is considered estimated.
.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PESTICIDES AND PCBS
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for Pesticides and PCBs in accordance with EPA SW-846 Method 8081B_8082A.
The samples were prepared on 05/16/2016 and analyzed on 05/19/2016.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ORGANOPHOSPHORUS PESTICIDES
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for organophosphorus pesticides in accordance with EPA SW-846 Method
8141B. The samples were prepared on 05/18/2016 and analyzed on 05/23/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHLORINATED HERBICIDES
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for chlorinated herbicides in accordance with EPA SW-846 Method 8151A. The
samples were prepared on 05/19/2016 and analyzed on 05/21/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
METALS (ICPMS)
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for Metals (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples
were prepared on 05/15/2016 and analyzed on 05/20/2016 and 05/22/2016.
Selenium was detected in method blank MB 680-433402/1-A at a level that was above the method detection limit but below the reporting
limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the MDL
and/or RL, the result has been flagged.
TestAmerica SavannahPage 3 of 43 5/26/2016
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125233-1
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-125233-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS BY ION CHROMATOGRAPHY (48 HOUR)
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for Anions by Ion Chromatography (48 Hour) in accordance with EPA Method
300.0. The samples were analyzed on 05/14/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL CYANIDE
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for total cyanide in accordance with EPA SW-846 Method 9012B. The samples
were prepared and analyzed on 05/19/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SULFIDE
Sample SLMW-12AR-5-16 (680-125233-1) was analyzed for sulfide in accordance with EPA SW-846 Method 9034. The samples were
prepared and analyzed on 05/18/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Sample Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-125233-1 SLMW-12AR-5-16 Water 05/12/16 13:45 05/13/16 09:13
TestAmerica Savannah
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Method Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method Method Description LaboratoryProtocol
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL SAV
SW8468081B/8082A Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography TAL SAV
SW8468141BOrganophosphorous Compounds by Gas Chromatography, Capillary Column Technique TAL PIT
SW8468151AHerbicides (GC)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
SW8466020AMetals (ICP/MS)TAL SAV
SW8469012BCyanide, Total andor Amenable TAL SAV
SW8469034Sulfide, Acid Soluble and Insoluble (Titrimetric)TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Qualifiers
GC/MS Semi VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Q One or more quality control criteria failed.
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
J Estimated: The analyte was positively identified; the quantitation is an estimation
GC Semi VOA
Qualifier Description
M Manual integrated compound.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
U Undetected at the Limit of Detection.
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
HPLC/IC
Qualifier Description
J Estimated: The analyte was positively identified; the quantitation is an estimation
Qualifier
U Undetected at the Limit of Detection.
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
General Chemistry
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
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Detection Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: SLMW-12AR-5-16 Lab Sample ID: 680-125233-1
Nitrate as N
RL
0.050 mg/L
MDL
0.023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.041 300.0
Arsenic 1.0 ug/L0.40 Total/NA10.48 J 6020A
Barium 1.0 ug/L0.15 Total/NA1256020A
Beryllium 0.20 ug/L0.070 Total/NA10.11 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.53 6020A
Lead 0.30 ug/L0.080 Total/NA10.29 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.54 J 6020A
Selenium 0.50 ug/L0.21 Total/NA12.0 6020A
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125233-1Client Sample ID: SLMW-12AR-5-16
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.53 U 9.5 0.53 ug/L 05/18/16 16:30 05/24/16 19:53 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
9.5 0.50 ug/L 05/18/16 16:30 05/24/16 19:53 11,2-Dichlorobenzene 0.50 U
9.5 0.56 ug/L 05/18/16 16:30 05/24/16 19:53 11,3-Dichlorobenzene 0.56 U
9.5 0.51 ug/L 05/18/16 16:30 05/24/16 19:53 11,4-Dichlorobenzene 0.51 U
9.5 1.1 ug/L 05/18/16 16:30 05/24/16 19:53 12,4,5-Trichlorophenol 1.1 U
9.5 0.81 ug/L 05/18/16 16:30 05/24/16 19:53 12,4,6-Trichlorophenol 0.81 U
9.5 1.0 ug/L 05/18/16 16:30 05/24/16 19:53 12,4-Dichlorophenol 1.0 U
9.5 3.8 ug/L 05/18/16 16:30 05/24/16 19:53 12,4-Dimethylphenol 3.8 U
48 9.5 ug/L 05/18/16 16:30 05/24/16 19:53 12,4-Dinitrophenol 9.5 U
9.5 1.1 ug/L 05/18/16 16:30 05/24/16 19:53 12,4-Dinitrotoluene 1.1 U
9.5 0.83 ug/L 05/18/16 16:30 05/24/16 19:53 12-Chlorophenol 0.83 U
9.5 0.76 ug/L 05/18/16 16:30 05/24/16 19:53 12-Chloronaphthalene 0.76 U
9.5 0.74 ug/L 05/18/16 16:30 05/24/16 19:53 12-Methylnaphthalene 0.74 U Q
9.5 0.85 ug/L 05/18/16 16:30 05/24/16 19:53 12-Methylphenol 0.85 U
48 1.2 ug/L 05/18/16 16:30 05/24/16 19:53 12-Nitroaniline 1.2 U
9.5 0.72 ug/L 05/18/16 16:30 05/24/16 19:53 12-Nitrophenol 0.72 U
9.5 1.2 ug/L 05/18/16 16:30 05/24/16 19:53 13 & 4 Methylphenol 1.2 U
57 29 ug/L 05/18/16 16:30 05/24/16 19:53 13,3'-Dichlorobenzidine 29 U
48 4.8 ug/L 05/18/16 16:30 05/24/16 19:53 13-Nitroaniline 4.8 U
48 9.5 ug/L 05/18/16 16:30 05/24/16 19:53 14,6-Dinitro-2-methylphenol 9.5 U
9.5 0.73 ug/L 05/18/16 16:30 05/24/16 19:53 14-Bromophenyl phenyl ether 0.73 U
9.5 0.95 ug/L 05/18/16 16:30 05/24/16 19:53 14-Chloro-3-methylphenol 0.95 U
19 2.1 ug/L 05/18/16 16:30 05/24/16 19:53 14-Chloroaniline 2.1 U
9.5 0.80 ug/L 05/18/16 16:30 05/24/16 19:53 14-Chlorophenyl phenyl ether 0.80 U
48 4.8 ug/L 05/18/16 16:30 05/24/16 19:53 14-Nitroaniline 4.8 U
9.5 0.72 ug/L 05/18/16 16:30 05/24/16 19:53 1Acenaphthene0.72 U
9.5 0.81 ug/L 05/18/16 16:30 05/24/16 19:53 1Acenaphthylene0.81 U
9.5 0.66 ug/L 05/18/16 16:30 05/24/16 19:53 1Anthracene0.66 U
9.5 0.52 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzo[a]anthracene 0.52 U
9.5 0.68 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzo[a]pyrene 0.68 U
9.5 2.5 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzo[b]fluoranthene 2.5 U
9.5 0.83 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzo[g,h,i]perylene 0.83 U
9.5 1.1 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzo[k]fluoranthene 1.1 U
9.5 1.0 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzyl alcohol 1.0 U
9.5 0.89 ug/L 05/18/16 16:30 05/24/16 19:53 1Bis(2-chloroethoxy)methane 0.89 U
9.5 1.0 ug/L 05/18/16 16:30 05/24/16 19:53 1Bis(2-chloroethyl)ether 1.0 U
9.5 1.5 ug/L 05/18/16 16:30 05/24/16 19:53 1Bis(2-ethylhexyl) phthalate 1.5 U
9.5 0.49 ug/L 05/18/16 16:30 05/24/16 19:53 1Chrysene0.49 U
9.5 0.95 ug/L 05/18/16 16:30 05/24/16 19:53 1Dibenz(a,h)anthracene 0.95 U
9.5 0.75 ug/L 05/18/16 16:30 05/24/16 19:53 1Dibenzofuran0.75 U
9.5 0.79 ug/L 05/18/16 16:30 05/24/16 19:53 1Di-n-butyl phthalate 0.79 U
9.5 0.84 ug/L 05/18/16 16:30 05/24/16 19:53 1Diethyl phthalate 0.84 U
9.5 0.94 ug/L 05/18/16 16:30 05/24/16 19:53 1Dimethyl phthalate 0.94 U
9.5 1.3 ug/L 05/18/16 16:30 05/24/16 19:53 1Di-n-octyl phthalate 1.3 U
9.5 0.70 ug/L 05/18/16 16:30 05/24/16 19:53 1Fluoranthene0.70 U
9.5 0.91 ug/L 05/18/16 16:30 05/24/16 19:53 1Fluorene0.91 U
9.5 0.75 ug/L 05/18/16 16:30 05/24/16 19:53 1Hexachlorobenzene0.75 U
9.5 0.59 ug/L 05/18/16 16:30 05/24/16 19:53 1Hexachlorobutadiene0.59 U
9.5 0.72 ug/L 05/18/16 16:30 05/24/16 19:53 1Hexachloroethane0.72 U
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125233-1Client Sample ID: SLMW-12AR-5-16
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Indeno[1,2,3-cd]pyrene 0.95 U 9.5 0.95 ug/L 05/18/16 16:30 05/24/16 19:53 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
9.5 0.86 ug/L 05/18/16 16:30 05/24/16 19:53 1Isophorone0.86 U
9.5 0.67 ug/L 05/18/16 16:30 05/24/16 19:53 1Naphthalene0.67 U
9.5 0.69 ug/L 05/18/16 16:30 05/24/16 19:53 1Nitrobenzene0.69 U Q
9.5 0.88 ug/L 05/18/16 16:30 05/24/16 19:53 1N-Nitrosodiphenylamine 0.88 U
9.5 0.68 ug/L 05/18/16 16:30 05/24/16 19:53 1N-Nitrosodi-n-propylamine 0.68 U
48 1.9 ug/L 05/18/16 16:30 05/24/16 19:53 1Pentachlorophenol1.9 U
9.5 0.73 ug/L 05/18/16 16:30 05/24/16 19:53 1Phenanthrene0.73 U
9.5 0.79 ug/L 05/18/16 16:30 05/24/16 19:53 1Phenol0.79 U
9.5 0.60 ug/L 05/18/16 16:30 05/24/16 19:53 1Pyrene0.60 U
9.5 1.1 ug/L 05/18/16 16:30 05/24/16 19:53 1Butyl benzyl phthalate 1.1 U
9.5 0.74 ug/L 05/18/16 16:30 05/24/16 19:53 1bis(chloroisopropyl) ether 0.74 U
48 4.8 ug/L 05/18/16 16:30 05/24/16 19:53 1Benzoic acid 4.8 U
9.5 1.0 ug/L 05/18/16 16:30 05/24/16 19:53 12,6-Dinitrotoluene 1.0 U
48 1.8 ug/L 05/18/16 16:30 05/24/16 19:53 14-Nitrophenol 1.8 U
2,4,6-Tribromophenol 70 39-124 05/18/16 16:30 05/24/16 19:53 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 57 05/18/16 16:30 05/24/16 19:53 132-113
2-Fluorophenol 43 05/18/16 16:30 05/24/16 19:53 126-109
Terphenyl-d14 44 05/18/16 16:30 05/24/16 19:53 110-126
Phenol-d5 44 05/18/16 16:30 05/24/16 19:53 127-110
Nitrobenzene-d5 54 05/18/16 16:30 05/24/16 19:53 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 05/16/16 16:28 05/19/16 20:42 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.048 0.0072 ug/L 05/16/16 16:28 05/19/16 20:42 1delta-BHC 0.0072 U
0.048 0.0036 ug/L 05/16/16 16:28 05/19/16 20:42 1Dieldrin0.0036 U
0.048 0.0033 ug/L 05/16/16 16:28 05/19/16 20:42 1Endosulfan I 0.0033 U
0.048 0.0040 ug/L 05/16/16 16:28 05/19/16 20:42 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 05/16/16 16:28 05/19/16 20:42 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 05/16/16 16:28 05/19/16 20:42 1Endrin0.0051 U
0.048 0.0058 ug/L 05/16/16 16:28 05/19/16 20:42 1Endrin aldehyde 0.0058 U
0.048 0.0044 ug/L 05/16/16 16:28 05/19/16 20:42 1Endrin ketone 0.0044 U
0.048 0.0034 ug/L 05/16/16 16:28 05/19/16 20:42 1gamma-BHC (Lindane)0.0034 U
0.048 0.0068 ug/L 05/16/16 16:28 05/19/16 20:42 1Heptachlor0.0068 U
0.048 0.0035 ug/L 05/16/16 16:28 05/19/16 20:42 1Heptachlor epoxide 0.0035 U
0.048 0.0094 ug/L 05/16/16 16:28 05/19/16 20:42 1Methoxychlor0.0094 U
0.96 0.17 ug/L 05/16/16 16:28 05/19/16 20:42 1PCB-1016 0.17 U
0.048 0.0060 ug/L 05/16/16 16:28 05/19/16 20:42 14,4'-DDD 0.0060 U
0.048 0.0049 ug/L 05/16/16 16:28 05/19/16 20:42 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 05/16/16 16:28 05/19/16 20:42 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 05/16/16 16:28 05/19/16 20:42 1Aldrin0.0069 U
0.048 0.0032 ug/L 05/16/16 16:28 05/19/16 20:42 1alpha-BHC 0.0032 U
0.048 0.0087 ug/L 05/16/16 16:28 05/19/16 20:42 1beta-BHC 0.0087 U
0.48 0.091 ug/L 05/16/16 16:28 05/19/16 20:42 1Chlordane (technical)0.091 U
0.96 0.18 ug/L 05/16/16 16:28 05/19/16 20:42 1PCB-1221 0.18 U
0.96 0.24 ug/L 05/16/16 16:28 05/19/16 20:42 1PCB-1232 0.24 U
0.96 0.18 ug/L 05/16/16 16:28 05/19/16 20:42 1PCB-1242 0.18 U
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Client Sample Results
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125233-1Client Sample ID: SLMW-12AR-5-16
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued)
RL MDL
PCB-1248 0.20 U 0.96 0.20 ug/L 05/16/16 16:28 05/19/16 20:42 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.96 0.11 ug/L 05/16/16 16:28 05/19/16 20:42 1PCB-1254 0.11 U
0.96 0.11 ug/L 05/16/16 16:28 05/19/16 20:42 1PCB-1260 0.11 U
Tetrachloro-m-xylene 63 40-130 05/16/16 16:28 05/19/16 20:42 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 30 05/16/16 16:28 05/19/16 20:42 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.17 U 0.94 0.17 ug/L 05/18/16 12:45 05/23/16 23:17 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.94 0.062 ug/L 05/18/16 12:45 05/23/16 23:17 1Bolstar0.062 U
0.94 0.068 ug/L 05/18/16 12:45 05/23/16 23:17 1Chlorpyrifos0.068 U
0.94 0.18 ug/L 05/18/16 12:45 05/23/16 23:17 1Coumaphos0.18 U
1.9 0.099 ug/L 05/18/16 12:45 05/23/16 23:17 1Demeton, Total 0.099 U
0.94 0.071 ug/L 05/18/16 12:45 05/23/16 23:17 1Diazinon0.071 U
0.94 0.094 ug/L 05/18/16 12:45 05/23/16 23:17 1Dichlorvos0.094 U
0.94 0.17 ug/L 05/18/16 12:45 05/23/16 23:17 1Dimethoate0.17 U
0.94 0.087 ug/L 05/18/16 12:45 05/23/16 23:17 1Disulfoton0.087 U
0.94 0.13 ug/L 05/18/16 12:45 05/23/16 23:17 1EPN0.13 U
0.94 0.11 ug/L 05/18/16 12:45 05/23/16 23:17 1Mocap0.11 U
0.94 0.10 ug/L 05/18/16 12:45 05/23/16 23:17 1Famphur0.10 U
0.94 0.092 ug/L 05/18/16 12:45 05/23/16 23:17 1Fensulfothion0.092 U
0.94 0.074 ug/L 05/18/16 12:45 05/23/16 23:17 1Fenthion0.074 U
0.94 0.080 ug/L 05/18/16 12:45 05/23/16 23:17 1Malathion0.080 U
0.94 0.10 ug/L 05/18/16 12:45 05/23/16 23:17 1Parathion0.10 U
0.94 0.11 ug/L 05/18/16 12:45 05/23/16 23:17 1Methyl parathion 0.11 U
0.94 0.15 ug/L 05/18/16 12:45 05/23/16 23:17 1Mevinphos0.15 U
0.94 0.073 ug/L 05/18/16 12:45 05/23/16 23:17 1Phorate0.073 U
0.94 0.10 ug/L 05/18/16 12:45 05/23/16 23:17 1Ronnel0.10 U
0.94 0.13 ug/L 05/18/16 12:45 05/23/16 23:17 1Stirophos0.13 U
0.94 0.067 ug/L 05/18/16 12:45 05/23/16 23:17 1Sulfotepp0.067 U
0.94 0.081 ug/L 05/18/16 12:45 05/23/16 23:17 1Thionazin0.081 U
0.94 0.068 ug/L 05/18/16 12:45 05/23/16 23:17 1Tokuthion0.068 U
0.94 0.067 ug/L 05/18/16 12:45 05/23/16 23:17 1Trichloronate0.067 U
0.94 0.090 ug/L 05/18/16 12:45 05/23/16 23:17 1O,O,O-Triethyl phosphorothioate 0.090 U
Tributyl phosphate 78 49-122 05/18/16 12:45 05/23/16 23:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 59 05/18/16 12:45 05/23/16 23:17 149-122
Triphenylphosphate 89 05/18/16 12:45 05/23/16 23:17 145-145
Triphenylphosphate 100 05/18/16 12:45 05/23/16 23:17 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.035 U 0.48 0.035 ug/L 05/19/16 08:53 05/21/16 04:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/21/16 04:45 12,4-DB 0.14 U
0.24 0.059 ug/L 05/19/16 08:53 05/21/16 04:45 12,4,5-T 0.059 U
0.24 0.059 ug/L 05/19/16 08:53 05/21/16 04:45 1Silvex (2,4,5-TP)0.059 U
4.8 0.095 ug/L 05/19/16 08:53 05/21/16 04:45 1Dalapon0.095 U
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Client Sample Results
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125233-1Client Sample ID: SLMW-12AR-5-16
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Method: 8151A - Herbicides (GC) (Continued)
RL MDL
Dicamba 0.081 U 0.48 0.081 ug/L 05/19/16 08:53 05/21/16 04:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/21/16 04:45 1Dichlorprop0.14 U
0.95 0.15 ug/L 05/19/16 08:53 05/21/16 04:45 1Dinoseb0.15 U
110 16 ug/L 05/19/16 08:53 05/21/16 04:45 1MCPA16 U
110 18 ug/L 05/19/16 08:53 05/21/16 04:45 1Mecoprop18 U
0.24 0.035 ug/L 05/19/16 08:53 05/21/16 04:45 1Pentachlorophenol0.035 U
DCAA 81 45-130 05/19/16 08:53 05/21/16 04:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.041 J 0.050 0.023 mg/L 05/14/16 10:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/15/16 10:00 05/20/16 23:17 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 23:17 1Arsenic0.48 J
1.0 0.15 ug/L 05/15/16 10:00 05/20/16 23:17 1Barium25
0.20 0.070 ug/L 05/15/16 10:00 05/20/16 23:17 1Beryllium0.11 J
0.50 0.20 ug/L 05/15/16 10:00 05/20/16 23:17 1Cadmium0.20 U
1.0 0.16 ug/L 05/15/16 10:00 05/20/16 23:17 1Chromium0.16 U
0.20 0.078 ug/L 05/15/16 10:00 05/20/16 23:17 1Cobalt0.53
1.0 0.21 ug/L 05/15/16 10:00 05/20/16 23:17 1Copper0.21 U
0.30 0.080 ug/L 05/15/16 10:00 05/20/16 23:17 1Lead0.29 J
0.20 0.080 ug/L 05/15/16 10:00 05/20/16 23:17 1Mercury0.080 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 23:17 1Nickel0.54 J
0.50 0.21 ug/L 05/15/16 10:00 05/22/16 06:25 1Selenium2.0
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 23:17 1Silver0.10 U
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 23:17 1Thallium0.10 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 23:17 1Tin0.40 U
5.0 1.4 ug/L 05/15/16 10:00 05/20/16 23:17 1Vanadium1.4 U
10 2.6 ug/L 05/15/16 10:00 05/20/16 23:17 1Zinc2.6 U
General Chemistry
RL MDL
Cyanide, Total 0.0025 U 0.010 0.0025 mg/L 05/19/16 06:22 05/19/16 11:37 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
RL RL
Sulfide 10 U 10 10 mg/L 05/18/16 06:45 05/18/16 08:24 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Surrogate Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (39-124) (32-113) (26-109) (10-126) (27-110) (32-118)
TBP FBP 2FP TPH PHL NBZ
70 57 43 44 44 54680-125233-1
Percent Surrogate Recovery (Acceptance Limits)
SLMW-12AR-5-16
71 48 41 5761 64680-125287-F-1-A MS Matrix Spike
76 41 29 3461 38680-125287-F-1-B MSD Matrix Spike Duplicate
72 60 53 6056 63LCS 680-433837/10-A Lab Control Sample
74 58 62 6258 67MB 680-433837/9-A Method Blank
Surrogate Legend
TBP = 2,4,6-Tribromophenol
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol
TPH = Terphenyl-d14
PHL = Phenol-d5
NBZ = Nitrobenzene-d5
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-130) (14-130)
TCX1 DCB1
63 30680-125233-1
Percent Surrogate Recovery (Acceptance Limits)
SLMW-12AR-5-16
65 69LCS 680-433502/22-A Lab Control Sample
72 M 75LCS 680-433502/25-A Lab Control Sample
71 65LCS 680-433502/28-A Lab Control Sample
74 55LCSD 680-433502/29-A Lab Control Sample Dup
68 65MB 680-433502/21-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-130) (14-130)
TCX1 DCB2
76 M 25680-125272-D-5-A MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
74 M 20680-125272-D-5-B MSD Matrix Spike Duplicate
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
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Surrogate Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-130) (14-130)
TCX2 DCB2
50 M J 19680-125272-F-7-A MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-130) (14-130)
TCX2 DCB1
47 J 13 J680-125272-F-7-B MSD
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike Duplicate
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column
Technique
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (49-122) (49-122) (45-145) (45-145)
TBPH1 TBPH2 TPP1 TPP2
78 59 89 100680-125233-1
Percent Surrogate Recovery (Acceptance Limits)
SLMW-12AR-5-16
105 115 M 103 116LCS 180-176662/2-A Lab Control Sample
111 122 M 110 121LCSD 180-176662/3-A Lab Control Sample Dup
57 40 J 73 82MB 180-176662/1-A Method Blank
Surrogate Legend
TBPH = Tributyl phosphate
TPP = Triphenylphosphate
Method: 8151A - Herbicides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (45-130)
DCPA1
67560-61466-D-3-B MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
73560-61466-D-3-C MSD Matrix Spike Duplicate
81680-125233-1 SLMW-12AR-5-16
81 MLCS 680-433921/13-A Lab Control Sample
80MB 680-433921/12-A Method Blank
Surrogate Legend
DCPA = DCAA
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-433837/9-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
RL MDL
1,2,4-Trichlorobenzene 0.56 U 10 0.56 ug/L 05/18/16 16:30 05/24/16 19:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.53 U 0.5310 ug/L 05/18/16 16:30 05/24/16 19:09 11,2-Dichlorobenzene
0.59 U 0.5910 ug/L 05/18/16 16:30 05/24/16 19:09 11,3-Dichlorobenzene
0.54 U 0.5410 ug/L 05/18/16 16:30 05/24/16 19:09 11,4-Dichlorobenzene
1.2 U 1.210 ug/L 05/18/16 16:30 05/24/16 19:09 12,4,5-Trichlorophenol
0.85 U 0.8510 ug/L 05/18/16 16:30 05/24/16 19:09 12,4,6-Trichlorophenol
1.1 U 1.110 ug/L 05/18/16 16:30 05/24/16 19:09 12,4-Dichlorophenol
4.0 U 4.010 ug/L 05/18/16 16:30 05/24/16 19:09 12,4-Dimethylphenol
10 U 1050 ug/L 05/18/16 16:30 05/24/16 19:09 12,4-Dinitrophenol
1.2 U 1.210 ug/L 05/18/16 16:30 05/24/16 19:09 12,4-Dinitrotoluene
0.87 U 0.8710 ug/L 05/18/16 16:30 05/24/16 19:09 12-Chlorophenol
0.80 U 0.8010 ug/L 05/18/16 16:30 05/24/16 19:09 12-Chloronaphthalene
0.78 U 0.7810 ug/L 05/18/16 16:30 05/24/16 19:09 12-Methylnaphthalene
0.89 U 0.8910 ug/L 05/18/16 16:30 05/24/16 19:09 12-Methylphenol
1.3 U 1.350 ug/L 05/18/16 16:30 05/24/16 19:09 12-Nitroaniline
0.76 U 0.7610 ug/L 05/18/16 16:30 05/24/16 19:09 12-Nitrophenol
1.3 U 1.310 ug/L 05/18/16 16:30 05/24/16 19:09 13 & 4 Methylphenol
30 U 3060 ug/L 05/18/16 16:30 05/24/16 19:09 13,3'-Dichlorobenzidine
5.0 U 5.050 ug/L 05/18/16 16:30 05/24/16 19:09 13-Nitroaniline
10 U 1050 ug/L 05/18/16 16:30 05/24/16 19:09 14,6-Dinitro-2-methylphenol
0.77 U 0.7710 ug/L 05/18/16 16:30 05/24/16 19:09 14-Bromophenyl phenyl ether
1.0 U 1.010 ug/L 05/18/16 16:30 05/24/16 19:09 14-Chloro-3-methylphenol
2.2 U 2.220 ug/L 05/18/16 16:30 05/24/16 19:09 14-Chloroaniline
0.84 U 0.8410 ug/L 05/18/16 16:30 05/24/16 19:09 14-Chlorophenyl phenyl ether
5.0 U 5.050 ug/L 05/18/16 16:30 05/24/16 19:09 14-Nitroaniline
0.76 U 0.7610 ug/L 05/18/16 16:30 05/24/16 19:09 1Acenaphthene
0.85 U 0.8510 ug/L 05/18/16 16:30 05/24/16 19:09 1Acenaphthylene
0.69 U 0.6910 ug/L 05/18/16 16:30 05/24/16 19:09 1Anthracene
0.55 U 0.5510 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzo[a]anthracene
0.71 U 0.7110 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzo[a]pyrene
2.6 U 2.610 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzo[b]fluoranthene
0.87 U 0.8710 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzo[g,h,i]perylene
1.2 U 1.210 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzo[k]fluoranthene
1.1 U 1.110 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzyl alcohol
0.94 U 0.9410 ug/L 05/18/16 16:30 05/24/16 19:09 1Bis(2-chloroethoxy)methane
1.1 U 1.110 ug/L 05/18/16 16:30 05/24/16 19:09 1Bis(2-chloroethyl)ether
1.6 U 1.610 ug/L 05/18/16 16:30 05/24/16 19:09 1Bis(2-ethylhexyl) phthalate
0.51 U 0.5110 ug/L 05/18/16 16:30 05/24/16 19:09 1Chrysene
1.0 U 1.010 ug/L 05/18/16 16:30 05/24/16 19:09 1Dibenz(a,h)anthracene
0.79 U 0.7910 ug/L 05/18/16 16:30 05/24/16 19:09 1Dibenzofuran
0.83 U 0.8310 ug/L 05/18/16 16:30 05/24/16 19:09 1Di-n-butyl phthalate
0.88 U 0.8810 ug/L 05/18/16 16:30 05/24/16 19:09 1Diethyl phthalate
0.99 U 0.9910 ug/L 05/18/16 16:30 05/24/16 19:09 1Dimethyl phthalate
1.4 U 1.410 ug/L 05/18/16 16:30 05/24/16 19:09 1Di-n-octyl phthalate
0.74 U 0.7410 ug/L 05/18/16 16:30 05/24/16 19:09 1Fluoranthene
0.96 U 0.9610 ug/L 05/18/16 16:30 05/24/16 19:09 1Fluorene
0.79 U 0.7910 ug/L 05/18/16 16:30 05/24/16 19:09 1Hexachlorobenzene
0.62 U 0.6210 ug/L 05/18/16 16:30 05/24/16 19:09 1Hexachlorobutadiene
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-433837/9-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
RL MDL
Hexachloroethane 0.76 U 10 0.76 ug/L 05/18/16 16:30 05/24/16 19:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
1.0 U 1.010 ug/L 05/18/16 16:30 05/24/16 19:09 1Indeno[1,2,3-cd]pyrene
0.90 U 0.9010 ug/L 05/18/16 16:30 05/24/16 19:09 1Isophorone
0.70 U 0.7010 ug/L 05/18/16 16:30 05/24/16 19:09 1Naphthalene
0.73 U 0.7310 ug/L 05/18/16 16:30 05/24/16 19:09 1Nitrobenzene
0.92 U 0.9210 ug/L 05/18/16 16:30 05/24/16 19:09 1N-Nitrosodiphenylamine
0.72 U 0.7210 ug/L 05/18/16 16:30 05/24/16 19:09 1N-Nitrosodi-n-propylamine
2.0 U 2.050 ug/L 05/18/16 16:30 05/24/16 19:09 1Pentachlorophenol
0.77 U 0.7710 ug/L 05/18/16 16:30 05/24/16 19:09 1Phenanthrene
0.83 U 0.8310 ug/L 05/18/16 16:30 05/24/16 19:09 1Phenol
0.63 U 0.6310 ug/L 05/18/16 16:30 05/24/16 19:09 1Pyrene
1.2 U 1.210 ug/L 05/18/16 16:30 05/24/16 19:09 1Butyl benzyl phthalate
0.78 U 0.7810 ug/L 05/18/16 16:30 05/24/16 19:09 1bis(chloroisopropyl) ether
5.0 U 5.050 ug/L 05/18/16 16:30 05/24/16 19:09 1Benzoic acid
1.1 U 1.110 ug/L 05/18/16 16:30 05/24/16 19:09 12,6-Dinitrotoluene
1.9 U 1.950 ug/L 05/18/16 16:30 05/24/16 19:09 14-Nitrophenol
2,4,6-Tribromophenol 74 39-124 05/24/16 19:09 1
MB MB
Surrogate
05/18/16 16:30
Dil FacPrepared AnalyzedQualifier Limits%Recovery
58 05/18/16 16:30 05/24/16 19:09 12-Fluorobiphenyl 32-113
62 05/18/16 16:30 05/24/16 19:09 12-Fluorophenol 26-109
58 05/18/16 16:30 05/24/16 19:09 1Terphenyl-d14 10-126
62 05/18/16 16:30 05/24/16 19:09 1Phenol-d5 27-110
67 05/18/16 16:30 05/24/16 19:09 1Nitrobenzene-d5 32-118
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433837/10-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
1,2,4-Trichlorobenzene 100 53.4 ug/L 53 33 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichlorobenzene 100 48.0 ug/L 48 31 -130
1,3-Dichlorobenzene 100 45.0 ug/L 45 30 -130
1,4-Dichlorobenzene 100 46.1 ug/L 46 31 -130
2,4,5-Trichlorophenol 100 71.7 ug/L 72 48 -130
2,4,6-Trichlorophenol 100 72.5 ug/L 73 47 -130
2,4-Dichlorophenol 100 66.6 ug/L 67 44 -130
2,4-Dimethylphenol 100 71.0 ug/L 71 37 -130
2,4-Dinitrophenol 200 134 ug/L 67 31 -130
2,4-Dinitrotoluene 100 78.7 ug/L 79 52 -130
2-Chlorophenol 100 60.9 ug/L 61 39 -130
2-Chloronaphthalene 100 64.7 ug/L 65 44 -130
2-Methylnaphthalene 100 88.9 ug/L 89 40 -130
2-Methylphenol 100 73.1 ug/L 73 40 -130
2-Nitroaniline 100 78.1 ug/L 78 51 -130
2-Nitrophenol 100 63.8 ug/L 64 43 -130
3 & 4 Methylphenol 100 69.0 ug/L 69 42 -130
3,3'-Dichlorobenzidine 100 47.2 J ug/L 47 46 -130
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433837/10-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
3-Nitroaniline 100 70.5 ug/L 70 53 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4,6-Dinitro-2-methylphenol 200 135 ug/L 68 42 -130
4-Bromophenyl phenyl ether 100 67.0 ug/L 67 47 -130
4-Chloro-3-methylphenol 100 79.9 ug/L 80 47 -130
4-Chloroaniline 100 56.1 ug/L 56 42 -130
4-Chlorophenyl phenyl ether 100 67.8 ug/L 68 45 -130
4-Nitroaniline 100 67.2 ug/L 67 49 -130
Acenaphthene 100 68.3 ug/L 68 48 -130
Acenaphthylene 100 68.8 ug/L 69 48 -130
Anthracene 100 67.0 ug/L 67 49 -130
Benzo[a]anthracene 100 70.7 ug/L 71 44 -130
Benzo[a]pyrene 100 65.2 ug/L 65 44 -130
Benzo[b]fluoranthene 100 65.1 ug/L 65 43 -130
Benzo[g,h,i]perylene 100 69.9 ug/L 70 41 -130
Benzo[k]fluoranthene 100 72.5 ug/L 73 40 -130
Benzyl alcohol 100 64.4 ug/L 64 29 -130
Bis(2-chloroethoxy)methane 100 73.2 ug/L 73 47 -130
Bis(2-chloroethyl)ether 100 65.8 ug/L 66 32 -130
Bis(2-ethylhexyl) phthalate 100 76.0 ug/L 76 45 -130
Chrysene 100 68.2 ug/L 68 47 -130
Dibenz(a,h)anthracene 100 67.2 ug/L 67 41 -130
Dibenzofuran 100 73.1 ug/L 73 50 -130
Di-n-butyl phthalate 100 72.7 ug/L 73 51 -130
Diethyl phthalate 100 74.0 ug/L 74 53 -130
Dimethyl phthalate 100 74.9 ug/L 75 53 -130
Di-n-octyl phthalate 100 74.9 ug/L 75 42 -130
Fluoranthene 100 81.4 ug/L 81 47 -130
Fluorene 100 69.9 ug/L 70 50 -130
Hexachlorobenzene 100 66.4 ug/L 66 43 -130
Hexachlorobutadiene 100 48.1 ug/L 48 27 -130
Hexachloroethane 100 46.9 ug/L 47 29 -130
Indeno[1,2,3-cd]pyrene 100 69.5 ug/L 70 31 -130
Isophorone 100 69.4 ug/L 69 47 -130
Naphthalene 100 56.0 ug/L 56 39 -130
Nitrobenzene 100 88.2 ug/L 88 43 -130
N-Nitrosodiphenylamine 100 68.5 ug/L 68 50 -130
N-Nitrosodi-n-propylamine 100 71.5 ug/L 71 42 -130
Pentachlorophenol 200 131 ug/L 66 33 -130
Phenanthrene 100 70.0 ug/L 70 51 -130
Phenol 100 59.6 ug/L 60 35 -130
Pyrene 100 80.8 ug/L 81 52 -130
Butyl benzyl phthalate 100 76.3 ug/L 76 50 -130
bis(chloroisopropyl) ether 100 66.7 ug/L 67 26 -130
Benzoic acid 100 68.3 ug/L 68 10 -130
2,6-Dinitrotoluene 100 79.3 ug/L 79 52 -130
4-Nitrophenol 200 151 ug/L 76 44 -130
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433837/10-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
2,4,6-Tribromophenol 39 -124
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
602-Fluorobiphenyl 32 -113
532-Fluorophenol 26 -109
56Terphenyl-d14 10 -126
60Phenol-d5 27 -110
63Nitrobenzene-d5 32 -118
Client Sample ID: Matrix SpikeLab Sample ID: 680-125287-F-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
1,2,4-Trichlorobenzene 0.56 U J 99.1 23.0 J ug/L 23 33 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dichlorobenzene 0.53 U J 99.1 25.5 J ug/L 26 31 -130
1,3-Dichlorobenzene 0.59 U J 99.1 23.1 J ug/L 23 30 -130
1,4-Dichlorobenzene 0.54 U J 99.1 23.9 J ug/L 24 31 -130
2,4,5-Trichlorophenol 1.2 U 99.1 56.3 ug/L 57 48 -130
2,4,6-Trichlorophenol 0.85 U 99.1 56.3 ug/L 57 47 -130
2,4-Dichlorophenol 1.1 U J 99.1 55.1 ug/L 56 44 -130
2,4-Dimethylphenol 4.0 U 99.1 50.8 ug/L 51 37 -130
2,4-Dinitrophenol 10 U 198 128 ug/L 65 31 -130
2,4-Dinitrotoluene 1.2 U 99.1 66.4 ug/L 67 52 -130
2-Chlorophenol 0.87 U J 99.1 51.7 ug/L 52 39 -130
2-Chloronaphthalene 0.80 U J 99.1 38.7 J ug/L 39 44 -130
2-Methylnaphthalene 0.78 U Q 99.1 59.3 ug/L 60 40 -130
2-Methylphenol 0.89 U J 99.1 57.9 ug/L 58 40 -130
2-Nitroaniline 1.3 U 99.1 64.5 ug/L 65 51 -130
2-Nitrophenol 0.76 U J 99.1 53.6 ug/L 54 43 -130
3 & 4 Methylphenol 1.3 U 99.1 55.5 ug/L 56 42 -130
3,3'-Dichlorobenzidine 30 U J 99.1 46.4 J ug/L 47 46 -130
3-Nitroaniline 5.0 U 99.1 67.4 ug/L 68 53 -130
4,6-Dinitro-2-methylphenol 10 U 198 139 ug/L 70 42 -130
4-Bromophenyl phenyl ether 0.77 U 99.1 55.8 ug/L 56 47 -130
4-Chloro-3-methylphenol 1.0 U 99.1 68.3 ug/L 69 47 -130
4-Chloroaniline 2.2 U J 99.1 50.4 ug/L 51 42 -130
4-Chlorophenyl phenyl ether 0.84 U 99.1 52.5 ug/L 53 45 -130
4-Nitroaniline 5.0 U 99.1 74.1 ug/L 75 49 -130
Acenaphthene 0.76 U 99.1 48.1 ug/L 49 48 -130
Acenaphthylene 0.85 U J 99.1 46.9 J ug/L 47 48 -130
Anthracene 0.69 U 99.1 58.9 ug/L 59 49 -130
Benzo[a]anthracene 0.55 U 99.1 61.5 ug/L 62 44 -130
Benzo[a]pyrene 0.71 U 99.1 58.0 ug/L 59 44 -130
Benzo[b]fluoranthene 2.6 U 99.1 63.4 ug/L 64 43 -130
Benzo[g,h,i]perylene 0.87 U 99.1 59.4 ug/L 60 41 -130
Benzo[k]fluoranthene 1.2 U 99.1 58.7 ug/L 59 40 -130
Benzyl alcohol 2.8 J 99.1 56.1 ug/L 54 29 -130
Bis(2-chloroethoxy)methane 0.94 U 99.1 62.9 ug/L 64 47 -130
Bis(2-chloroethyl)ether 1.1 U 99.1 55.8 ug/L 56 32 -130
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 680-125287-F-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
Bis(2-ethylhexyl) phthalate 1.6 U 99.1 67.4 ug/L 68 45 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Chrysene 0.51 U 99.1 60.4 ug/L 61 47 -130
Dibenz(a,h)anthracene 1.0 U 99.1 56.2 ug/L 57 41 -130
Dibenzofuran 0.79 U J 99.1 48.9 J ug/L 49 50 -130
Di-n-butyl phthalate 0.83 U 99.1 78.0 ug/L 79 51 -130
Diethyl phthalate 0.88 U 99.1 63.0 ug/L 64 53 -130
Dimethyl phthalate 0.99 U 99.1 63.3 ug/L 64 53 -130
Di-n-octyl phthalate 1.4 U 99.1 69.3 ug/L 70 42 -130
Fluoranthene 0.74 U 99.1 63.3 ug/L 64 47 -130
Fluorene 0.96 U 99.1 49.7 ug/L 50 50 -130
Hexachlorobenzene 0.79 U 99.1 58.6 ug/L 59 43 -130
Hexachlorobutadiene 0.62 U J 99.1 17.2 J ug/L 17 27 -130
Hexachloroethane 0.76 U J 99.1 17.5 J ug/L 18 29 -130
Indeno[1,2,3-cd]pyrene 1.0 U 99.1 60.9 ug/L 61 31 -130
Isophorone 0.90 U 99.1 60.5 ug/L 61 47 -130
Naphthalene 0.70 U J 99.1 32.8 J ug/L 33 39 -130
Nitrobenzene 0.73 U Q 99.1 77.9 ug/L 79 43 -130
N-Nitrosodiphenylamine 0.92 U 99.1 61.0 ug/L 62 50 -130
N-Nitrosodi-n-propylamine 0.72 U 99.1 56.4 ug/L 57 42 -130
Pentachlorophenol 2.0 U 198 121 ug/L 61 33 -130
Phenanthrene 0.77 U 99.1 58.2 ug/L 59 51 -130
Phenol 0.83 U J 99.1 51.2 ug/L 52 35 -130
Pyrene 0.63 U 99.1 72.2 ug/L 73 52 -130
Butyl benzyl phthalate 1.2 U 99.1 69.1 ug/L 70 50 -130
bis(chloroisopropyl) ether 0.78 U 99.1 51.1 ug/L 52 26 -130
Benzoic acid 5.0 U 99.1 59.9 ug/L 60 10 -130
2,6-Dinitrotoluene 1.1 U 99.1 64.5 ug/L 65 52 -130
4-Nitrophenol 1.9 U 198 131 ug/L 66 44 -130
2,4,6-Tribromophenol 39 -124
Surrogate
71
MS MS
Qualifier Limits%Recovery
482-Fluorobiphenyl 32 -113
412-Fluorophenol 26 -109
61Terphenyl-d14 10 -126
57Phenol-d5 27 -110
64Nitrobenzene-d5 32 -118
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125287-F-1-B MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
1,2,4-Trichlorobenzene 0.56 U J 91.9 22.6 J ug/L 25 33 -130 2 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dichlorobenzene 0.53 U J 91.9 23.0 J ug/L 25 31 -130 10 50
1,3-Dichlorobenzene 0.59 U J 91.9 20.1 J ug/L 22 30 -130 14 50
1,4-Dichlorobenzene 0.54 U J 91.9 20.4 J ug/L 22 31 -130 16 50
2,4,5-Trichlorophenol 1.2 U 91.9 46.4 ug/L 50 48 -130 19 50
2,4,6-Trichlorophenol 0.85 U 91.9 46.4 ug/L 50 47 -130 19 50
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125287-F-1-B MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
2,4-Dichlorophenol 1.1 U J 91.9 36.0 J ug/L 39 44 -130 42 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2,4-Dimethylphenol 4.0 U 91.9 36.8 ug/L 40 37 -130 32 50
2,4-Dinitrophenol 10 U 184 109 ug/L 60 31 -130 16 50
2,4-Dinitrotoluene 1.2 U 91.9 61.0 ug/L 66 52 -130 9 50
2-Chlorophenol 0.87 U J 91.9 30.0 J ug/L 33 39 -130 53 50
2-Chloronaphthalene 0.80 U J 91.9 36.4 J ug/L 40 44 -130 6 50
2-Methylnaphthalene 0.78 U Q 91.9 52.2 ug/L 57 40 -130 13 50
2-Methylphenol 0.89 U J 91.9 36.1 J ug/L 39 40 -130 46 50
2-Nitroaniline 1.3 U 91.9 59.8 ug/L 65 51 -130 8 50
2-Nitrophenol 0.76 U J 91.9 36.1 J ug/L 39 43 -130 39 50
3 & 4 Methylphenol 1.3 U 91.9 38.8 ug/L 42 42 -130 36 50
3,3'-Dichlorobenzidine 30 U J 91.9 41.4 J ug/L 45 46 -130 11 50
3-Nitroaniline 5.0 U 91.9 57.4 ug/L 62 53 -130 16 50
4,6-Dinitro-2-methylphenol 10 U 184 112 ug/L 61 42 -130 21 50
4-Bromophenyl phenyl ether 0.77 U 91.9 48.1 ug/L 52 47 -130 15 50
4-Chloro-3-methylphenol 1.0 U 91.9 51.5 ug/L 56 47 -130 28 50
4-Chloroaniline 2.2 U J 91.9 33.1 J ug/L 36 42 -130 41 50
4-Chlorophenyl phenyl ether 0.84 U 91.9 47.6 ug/L 52 45 -130 10 50
4-Nitroaniline 5.0 U 91.9 62.6 ug/L 68 49 -130 17 50
Acenaphthene 0.76 U 91.9 45.2 ug/L 49 48 -130 6 50
Acenaphthylene 0.85 U J 91.9 46.3 ug/L 50 48 -130 1 50
Anthracene 0.69 U 91.9 49.9 ug/L 54 49 -130 17 50
Benzo[a]anthracene 0.55 U 91.9 54.0 ug/L 59 44 -130 13 50
Benzo[a]pyrene 0.71 U 91.9 50.0 ug/L 54 44 -130 15 50
Benzo[b]fluoranthene 2.6 U 91.9 55.0 ug/L 60 43 -130 14 50
Benzo[g,h,i]perylene 0.87 U 91.9 44.9 ug/L 49 41 -130 28 50
Benzo[k]fluoranthene 1.2 U 91.9 52.1 ug/L 57 40 -130 12 50
Benzyl alcohol 2.8 J 91.9 40.8 ug/L 41 29 -130 31 50
Bis(2-chloroethoxy)methane 0.94 U 91.9 42.7 ug/L 47 47 -130 38 50
Bis(2-chloroethyl)ether 1.1 U 91.9 33.4 ug/L 36 32 -130 50 50
Bis(2-ethylhexyl) phthalate 1.6 U 91.9 55.5 ug/L 60 45 -130 19 50
Chrysene 0.51 U 91.9 51.3 ug/L 56 47 -130 16 50
Dibenz(a,h)anthracene 1.0 U 91.9 44.7 ug/L 49 41 -130 23 50
Dibenzofuran 0.79 U J 91.9 44.7 J ug/L 49 50 -130 9 50
Di-n-butyl phthalate 0.83 U 91.9 58.0 ug/L 63 51 -130 29 50
Diethyl phthalate 0.88 U 91.9 61.0 ug/L 66 53 -130 3 50
Dimethyl phthalate 0.99 U 91.9 60.9 ug/L 66 53 -130 4 50
Di-n-octyl phthalate 1.4 U 91.9 62.5 ug/L 68 42 -130 10 50
Fluoranthene 0.74 U 91.9 52.7 ug/L 57 47 -130 18 50
Fluorene 0.96 U 91.9 49.0 ug/L 53 50 -130 1 50
Hexachlorobenzene 0.79 U 91.9 47.1 ug/L 51 43 -130 22 50
Hexachlorobutadiene 0.62 U J 91.9 14.8 J ug/L 16 27 -130 15 50
Hexachloroethane 0.76 U J 91.9 16.4 J ug/L 18 29 -130 6 50
Indeno[1,2,3-cd]pyrene 1.0 U 91.9 52.7 ug/L 57 31 -130 14 50
Isophorone 0.90 U 91.9 47.1 ug/L 51 47 -130 25 50
Naphthalene 0.70 U J 91.9 29.7 J ug/L 32 39 -130 10 50
Nitrobenzene 0.73 U Q 91.9 48.4 ug/L 53 43 -130 47 50
N-Nitrosodiphenylamine 0.92 U 91.9 51.6 ug/L 56 50 -130 17 50
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125287-F-1-B MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434682 Prep Batch: 433837
N-Nitrosodi-n-propylamine 0.72 U 91.9 43.2 ug/L 47 42 -130 27 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Pentachlorophenol 2.0 U 184 110 ug/L 60 33 -130 9 50
Phenanthrene 0.77 U 91.9 52.7 ug/L 57 51 -130 10 50
Phenol 0.83 U J 91.9 30.7 J ug/L 33 35 -130 50 50
Pyrene 0.63 U 91.9 53.0 ug/L 58 52 -130 31 50
Butyl benzyl phthalate 1.2 U 91.9 56.9 ug/L 62 50 -130 19 50
bis(chloroisopropyl) ether 0.78 U 91.9 33.8 ug/L 37 26 -130 41 50
Benzoic acid 5.0 U 91.9 45.7 J ug/L 50 10 -130 27 50
2,6-Dinitrotoluene 1.1 U 91.9 58.9 ug/L 64 52 -130 9 50
4-Nitrophenol 1.9 U 184 129 ug/L 70 44 -130 2 50
2,4,6-Tribromophenol 39 -124
Surrogate
76
MSD MSD
Qualifier Limits%Recovery
412-Fluorobiphenyl 32 -113
292-Fluorophenol 26 -109
61Terphenyl-d14 10 -126
34Phenol-d5 27 -110
38Nitrobenzene-d5 32 -118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-433502/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
RL MDL
Toxaphene 0.40 U 5.0 0.40 ug/L 05/16/16 16:28 05/19/16 19:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.0075 U 0.00750.050 ug/L 05/16/16 16:28 05/19/16 19:16 1delta-BHC
0.0038 U 0.00380.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Dieldrin
0.0035 U 0.00350.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Endosulfan I
0.0042 U 0.00420.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Endosulfan II
0.0051 U 0.00510.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Endosulfan sulfate
0.0053 U 0.00530.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Endrin
0.0061 U 0.00610.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Endrin aldehyde
0.0046 U 0.00460.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Endrin ketone
0.0036 U 0.00360.050 ug/L 05/16/16 16:28 05/19/16 19:16 1gamma-BHC (Lindane)
0.0071 U 0.00710.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Heptachlor
0.0037 U 0.00370.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Heptachlor epoxide
0.0098 U 0.00980.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Methoxychlor
0.18 U 0.181.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1016
0.0063 U 0.00630.050 ug/L 05/16/16 16:28 05/19/16 19:16 14,4'-DDD
0.0051 U 0.00510.050 ug/L 05/16/16 16:28 05/19/16 19:16 14,4'-DDE
0.0070 U 0.00700.050 ug/L 05/16/16 16:28 05/19/16 19:16 14,4'-DDT
0.0072 U 0.00720.050 ug/L 05/16/16 16:28 05/19/16 19:16 1Aldrin
0.0034 U 0.00340.050 ug/L 05/16/16 16:28 05/19/16 19:16 1alpha-BHC
0.0091 U 0.00910.050 ug/L 05/16/16 16:28 05/19/16 19:16 1beta-BHC
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-433502/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
RL MDL
Chlordane (technical)0.095 U 0.50 0.095 ug/L 05/16/16 16:28 05/19/16 19:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.19 U 0.191.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1221
0.25 U 0.251.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1232
0.19 U 0.191.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1242
0.21 U 0.211.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1248
0.11 U 0.111.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1254
0.12 U 0.121.0 ug/L 05/16/16 16:28 05/19/16 19:16 1PCB-1260
Tetrachloro-m-xylene 68 40-130 05/19/16 19:16 1
MB MB
Surrogate
05/16/16 16:28
Dil FacPrepared AnalyzedQualifier Limits%Recovery
65 05/16/16 16:28 05/19/16 19:16 1DCB Decachlorobiphenyl 14-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433502/22-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
delta-BHC 0.100 0.0851 ug/L 85 44 -142
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Dieldrin 0.100 0.0879 ug/L 88 54 -130
Endosulfan I 0.100 0.0871 ug/L 87 40 -131
Endosulfan II 0.100 0.0846 ug/L 85 44 -137
Endosulfan sulfate 0.100 0.0942 ug/L 94 49 -139
Endrin 0.100 0.0838 ug/L 84 59 -143
Endrin aldehyde 0.100 0.0901 ug/L 90 45 -166
Endrin ketone 0.100 0.0900 ug/L 90 56 -137
gamma-BHC (Lindane)0.100 0.0847 ug/L 85 52 -130
Heptachlor 0.100 0.0683 ug/L 68 35 -130
Heptachlor epoxide 0.100 0.0862 ug/L 86 52 -130
Methoxychlor 0.100 0.106 ug/L 106 52 -136
4,4'-DDD 0.100 0.0880 ug/L 88 54 -135
4,4'-DDE 0.100 0.0809 ug/L 81 47 -130
4,4'-DDT 0.100 0.0875 ug/L 87 47 -134
Aldrin 0.100 0.0689 ug/L 69 34 -130
alpha-BHC 0.100 0.0834 ug/L 83 48 -130
beta-BHC 0.100 0.0875 ug/L 87 29 -174
Tetrachloro-m-xylene 40 -130
Surrogate
65
LCS LCS
Qualifier Limits%Recovery
69DCB Decachlorobiphenyl 14 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433502/25-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
PCB-1016 6.00 5.16 ug/L 86 44 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433502/25-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
PCB-1260 6.00 5.68 ug/L 95 35 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Tetrachloro-m-xylene M 40 -130
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
75DCB Decachlorobiphenyl 14 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433502/28-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
Toxaphene 8.00 8.28 ug/L 104 56 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Chlordane (technical)4.00 4.09 ug/L 102 62 -130
Tetrachloro-m-xylene 40 -130
Surrogate
71
LCS LCS
Qualifier Limits%Recovery
65DCB Decachlorobiphenyl 14 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-433502/29-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
Toxaphene 8.00 8.55 ug/L 107 56 -130 3 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Chlordane (technical)4.00 4.25 ug/L 106 62 -130 4 30
Tetrachloro-m-xylene 40 -130
Surrogate
74
LCSD LCSD
Qualifier Limits%Recovery
55DCB Decachlorobiphenyl 14 -130
Client Sample ID: Matrix SpikeLab Sample ID: 680-125272-D-5-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
delta-BHC 0.015 U J 0.0999 0.137 M ug/L 137 44 -142
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Dieldrin 0.0076 U J 0.0999 0.0954 M J ug/L 95 54 -130
Endosulfan I 0.0070 U J 0.0999 0.144 M J ug/L 144 40 -131
Endosulfan II 0.0084 U 0.0999 0.0605 M J ug/L 61 44 -137
Endosulfan sulfate 0.010 U 0.0999 0.113 M ug/L 114 49 -139
Endrin 0.011 U 0.0999 0.0813 M J ug/L 81 59 -143
Endrin aldehyde 0.012 U 0.0999 0.0727 M ug/L 73 45 -166
Endrin ketone 0.0092 U 0.0999 0.102 M ug/L 102 56 -137
gamma-BHC (Lindane)0.0072 U 0.0999 0.0721 M J ug/L 72 52 -130
Heptachlor 0.014 U 0.0999 0.0777 M J ug/L 78 35 -130
Heptachlor epoxide 0.0074 U J 0.0999 0.0919 M J ug/L 92 52 -130
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 680-125272-D-5-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
Methoxychlor 0.020 U J 0.0999 0.157 M J ug/L 157 52 -136
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4,4'-DDD 0.013 U 0.0999 0.0588 M J ug/L 59 54 -135
4,4'-DDE 0.010 U 0.0999 0.0784 M ug/L 78 47 -130
4,4'-DDT 0.014 U J 0.0999 0.0955 M ug/L 96 47 -134
Aldrin 0.14 J 0.0999 0.180 J ug/L 38 34 -130
alpha-BHC 0.0068 U 0.0999 0.105 M ug/L 105 48 -130
beta-BHC 0.018 U 0.0999 0.137 M ug/L 137 29 -174
Tetrachloro-m-xylene M 40 -130
Surrogate
76
MS MS
Qualifier Limits%Recovery
25DCB Decachlorobiphenyl 14 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125272-D-5-B MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
delta-BHC 0.015 U J 0.0920 0.136 M J ug/L 148 44 -142 1 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Dieldrin 0.0076 U J 0.0920 0.0948 M J ug/L 103 54 -130 1 50
Endosulfan I 0.0070 U J 0.0920 0.170 M J ug/L 184 40 -131 17 50
Endosulfan II 0.0084 U 0.0920 0.0586 M J ug/L 64 44 -137 3 50
Endosulfan sulfate 0.010 U 0.0920 0.0704 M J ug/L 76 49 -139 47 50
Endrin 0.011 U 0.0920 0.124 M ug/L 135 59 -143 42 50
Endrin aldehyde 0.012 U 0.0920 0.0752 M ug/L 82 45 -166 3 50
Endrin ketone 0.0092 U 0.0920 0.0921 M ug/L 100 56 -137 10 50
gamma-BHC (Lindane)0.0072 U 0.0920 0.0948 M ug/L 103 52 -130 27 50
Heptachlor 0.014 U 0.0920 0.110 M ug/L 120 35 -130 34 50
Heptachlor epoxide 0.0074 U J 0.0920 0.0971 M J ug/L 106 52 -130 6 50
Methoxychlor 0.020 U J 0.0920 0.0874 M J ug/L 95 52 -136 57 50
4,4'-DDD 0.013 U 0.0920 0.0635 M J ug/L 69 54 -135 8 50
4,4'-DDE 0.010 U 0.0920 0.0806 M ug/L 88 47 -130 3 50
4,4'-DDT 0.014 U J 0.0920 0.0532 M J ug/L 58 47 -134 57 50
Aldrin 0.14 J 0.0920 0.138 M J ug/L -4 34 -130 26 50
alpha-BHC 0.0068 U 0.0920 0.0934 M ug/L 102 48 -130 12 50
beta-BHC 0.018 U 0.0920 0.121 M ug/L 131 29 -174 13 50
Tetrachloro-m-xylene M 40 -130
Surrogate
74
MSD MSD
Qualifier Limits%Recovery
20DCB Decachlorobiphenyl 14 -130
Client Sample ID: Matrix SpikeLab Sample ID: 680-125272-F-7-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
PCB-1016 0.36 U J 5.91 6.38 J ug/L 108 44 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas
Chromatography (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 680-125272-F-7-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
PCB-1260 0.24 U 5.91 4.03 ug/L 68 35 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Tetrachloro-m-xylene M J 40 -130
Surrogate
50
MS MS
Qualifier Limits%Recovery
19DCB Decachlorobiphenyl 14 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125272-F-7-B MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434119 Prep Batch: 433502
PCB-1016 0.36 U J 5.56 5.69 J ug/L 102 44 -130 11 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
PCB-1260 0.24 U 5.56 3.05 ug/L 55 35 -130 28 50
Tetrachloro-m-xylene J 40 -130
Surrogate
47
MSD MSD
Qualifier Limits%Recovery
13 JDCB Decachlorobiphenyl 14 -130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column
Technique
Client Sample ID: Method BlankLab Sample ID: MB 180-176662/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 177026 Prep Batch: 176662
RL MDL
Azinphos-methyl 0.18 U 1.0 0.18 ug/L 05/18/16 12:45 05/23/16 22:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.066 U 0.0661.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Bolstar
0.073 U 0.0731.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Chlorpyrifos
0.19 U 0.191.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Coumaphos
0.10 U 0.102.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Demeton, Total
0.075 U 0.0751.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Diazinon
0.10 U 0.101.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Dichlorvos
0.18 U 0.181.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Dimethoate
0.093 U 0.0931.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Disulfoton
0.14 U 0.141.0 ug/L 05/18/16 12:45 05/23/16 22:44 1EPN
0.11 U 0.111.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Mocap
0.11 U 0.111.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Famphur
0.097 U 0.0971.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Fensulfothion
0.079 U 0.0791.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Fenthion
0.085 U 0.0851.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Malathion
0.11 U 0.111.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Parathion
0.12 U 0.121.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Methyl parathion
0.16 U 0.161.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Mevinphos
0.078 U 0.0781.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Phorate
0.11 U 0.111.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Ronnel
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column
Technique (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-176662/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 177026 Prep Batch: 176662
RL MDL
Stirophos 0.14 U 1.0 0.14 ug/L 05/18/16 12:45 05/23/16 22:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.071 U 0.0711.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Sulfotepp
0.086 U 0.0861.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Thionazin
0.073 U 0.0731.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Tokuthion
0.071 U 0.0711.0 ug/L 05/18/16 12:45 05/23/16 22:44 1Trichloronate
0.096 U 0.0961.0 ug/L 05/18/16 12:45 05/23/16 22:44 1O,O,O-Triethyl phosphorothioate
Tributyl phosphate 57 49-122 05/23/16 22:44 1
MB MB
Surrogate
05/18/16 12:45
Dil FacPrepared AnalyzedQualifier Limits%Recovery
40 J 05/18/16 12:45 05/23/16 22:44 1Tributyl phosphate 49-122
73 05/18/16 12:45 05/23/16 22:44 1Triphenylphosphate45-145
82 05/18/16 12:45 05/23/16 22:44 1Triphenylphosphate45-145
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-176662/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 177026 Prep Batch: 176662
Azinphos-methyl 10.0 9.28 ug/L 93 40 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Bolstar 10.0 11.1 ug/L 111 50 -150
Chlorpyrifos 10.0 10.7 ug/L 107 50 -130
Coumaphos 10.0 9.87 ug/L 99 50 -150
Demeton, Total 10.0 12.9 ug/L 129 10 -150
Diazinon 10.0 10.9 ug/L 109 50 -150
Dichlorvos 10.0 9.52 ug/L 95 30 -150
Dimethoate 10.0 9.89 ug/L 99 26 -136
Disulfoton 10.0 10.6 ug/L 106 45 -124
EPN 10.0 9.49 ug/L 95 50 -150
Mocap 10.0 10.8 ug/L 108 40 -150
Famphur 10.0 11.3 ug/L 113 52 -131
Fensulfothion 10.0 9.51 ug/L 95 38 -150
Fenthion 10.0 11.7 ug/L 117 10 -150
Malathion 10.0 11.9 ug/L 119 50 -150
Parathion 10.0 11.4 ug/L 114 56 -125
Methyl parathion 10.0 9.67 ug/L 97 41 -148
Mevinphos 10.0 8.14 ug/L 81 30 -150
Phorate 10.0 10.2 ug/L 102 41 -135
Ronnel 10.0 11.4 ug/L 114 50 -150
Stirophos 10.0 11.3 ug/L 113 50 -150
Sulfotepp 10.0 11.8 ug/L 118 56 -128
Thionazin 10.0 11.1 ug/L 111 44 -128
Tokuthion 10.0 10.6 ug/L 106 50 -150
Trichloronate 10.0 10.1 ug/L 101 10 -150
O,O,O-Triethyl phosphorothioate 10.0 10.8 ug/L 108 31 -131
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column
Technique (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-176662/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 177026 Prep Batch: 176662
Tributyl phosphate 49 -122
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
115 MTributyl phosphate 49 -122
103Triphenylphosphate 45 -145
116Triphenylphosphate 45 -145
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-176662/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 177026 Prep Batch: 176662
Azinphos-methyl 10.0 9.79 ug/L 98 40 -150 5 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Bolstar 10.0 11.8 ug/L 118 50 -150 6 30
Chlorpyrifos 10.0 11.5 ug/L 115 50 -130 7 25
Coumaphos 10.0 10.3 ug/L 103 50 -150 4 30
Demeton, Total 10.0 13.4 ug/L 134 10 -150 3 30
Diazinon 10.0 11.5 ug/L 115 50 -150 5 30
Dichlorvos 10.0 10.1 ug/L 101 30 -150 6 30
Dimethoate 10.0 10.5 ug/L 105 26 -136 6 22
Disulfoton 10.0 11.2 ug/L 112 45 -124 5 30
EPN 10.0 10.0 ug/L 100 50 -150 6 30
Mocap 10.0 11.3 ug/L 113 40 -150 5 30
Famphur 10.0 12.0 ug/L 120 52 -131 6 24
Fensulfothion 10.0 9.93 ug/L 99 38 -150 4 30
Fenthion 10.0 12.5 ug/L 125 10 -150 7 30
Malathion 10.0 12.7 ug/L 127 50 -150 7 30
Parathion 10.0 12.3 ug/L 123 56 -125 7 21
Methyl parathion 10.0 10.3 ug/L 103 41 -148 7 30
Mevinphos 10.0 8.76 ug/L 88 30 -150 7 30
Phorate 10.0 10.6 ug/L 106 41 -135 4 24
Ronnel 10.0 12.1 ug/L 121 50 -150 6 30
Stirophos 10.0 11.9 ug/L 119 50 -150 5 30
Sulfotepp 10.0 12.5 ug/L 125 56 -128 6 23
Thionazin 10.0 11.8 ug/L 118 44 -128 5 21
Tokuthion 10.0 11.1 ug/L 111 50 -150 5 30
Trichloronate 10.0 10.7 ug/L 107 10 -150 6 30
O,O,O-Triethyl phosphorothioate 10.0 11.4 ug/L 114 31 -131 5 30
Tributyl phosphate 49 -122
Surrogate
111
LCSD LCSD
Qualifier Limits%Recovery
122 MTributyl phosphate 49 -122
110Triphenylphosphate 45 -145
121Triphenylphosphate 45 -145
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8151A - Herbicides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-433921/12-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434312 Prep Batch: 433921
RL MDL
2,4-D 0.037 U 0.50 0.037 ug/L 05/19/16 08:53 05/20/16 20:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.15 U 0.150.50 ug/L 05/19/16 08:53 05/20/16 20:35 12,4-DB
0.062 U 0.0620.25 ug/L 05/19/16 08:53 05/20/16 20:35 12,4,5-T
0.062 U 0.0620.25 ug/L 05/19/16 08:53 05/20/16 20:35 1Silvex (2,4,5-TP)
0.10 U 0.105.0 ug/L 05/19/16 08:53 05/20/16 20:35 1Dalapon
0.085 U 0.0850.50 ug/L 05/19/16 08:53 05/20/16 20:35 1Dicamba
0.15 U 0.150.50 ug/L 05/19/16 08:53 05/20/16 20:35 1Dichlorprop
0.16 U 0.161.0 ug/L 05/19/16 08:53 05/20/16 20:35 1Dinoseb
17 U 17120 ug/L 05/19/16 08:53 05/20/16 20:35 1MCPA
19 U 19120 ug/L 05/19/16 08:53 05/20/16 20:35 1Mecoprop
0.037 U 0.0370.25 ug/L 05/19/16 08:53 05/20/16 20:35 1Pentachlorophenol
DCAA 80 45-130 05/20/16 20:35 1
MB MB
Surrogate
05/19/16 08:53
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433921/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434312 Prep Batch: 433921
2,4-D 2.00 1.82 M ug/L 91 55 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2,4-DB 2.00 1.93 M ug/L 97 60 -147
2,4,5-T 0.500 0.461 M ug/L 92 58 -130
Silvex (2,4,5-TP)0.500 0.492 M ug/L 98 60 -130
Dalapon 2.00 1.54 J ug/L 77 40 -130
Dicamba 1.00 0.901 M ug/L 90 64 -130
Dichlorprop 2.00 1.93 M ug/L 97 52 -130
Dinoseb 2.00 1.49 M ug/L 74 14 -130
MCPA 200 195 M ug/L 97 52 -130
Mecoprop 200 184 M ug/L 92 55 -134
Pentachlorophenol 0.500 0.488 M ug/L 98 57 -130
DCAA M 45 -130
Surrogate
81
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 560-61466-D-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434312 Prep Batch: 433921
2,4-D 0.037 U 1.98 1.55 M ug/L 78 55 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
2,4-DB 0.15 U 1.98 2.13 M ug/L 107 60 -147
2,4,5-T 0.062 U 0.495 0.402 M ug/L 81 58 -130
Silvex (2,4,5-TP)0.062 U 0.495 0.453 M ug/L 91 60 -130
Dalapon 0.099 U Q 1.98 1.36 J ug/L 69 40 -130
Dicamba 0.084 U 0.991 0.741 ug/L 75 64 -130
Dichlorprop 0.15 U 1.98 1.70 M ug/L 86 52 -130
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8151A - Herbicides (GC) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 560-61466-D-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434312 Prep Batch: 433921
Dinoseb 0.16 U 1.98 1.13 ug/L 57 14 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
MCPA 17 U 198 135 ug/L 68 52 -130
Mecoprop 19 U 198 144 ug/L 73 55 -134
Pentachlorophenol 0.037 U 0.495 0.373 M ug/L 75 57 -130
DCAA 45 -130
Surrogate
67
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 560-61466-D-3-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434312 Prep Batch: 433921
2,4-D 0.037 U 2.13 1.87 M ug/L 88 55 -130 19 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2,4-DB 0.15 U 2.13 2.10 M ug/L 99 60 -147 1 50
2,4,5-T 0.062 U 0.532 0.456 M ug/L 86 58 -130 13 50
Silvex (2,4,5-TP)0.062 U 0.532 0.532 M ug/L 100 60 -130 16 50
Dalapon 0.099 U Q 2.13 1.55 J ug/L 73 40 -130 13 50
Dicamba 0.084 U 1.06 0.880 ug/L 83 64 -130 17 50
Dichlorprop 0.15 U 2.13 1.95 M ug/L 92 52 -130 14 50
Dinoseb 0.16 U 2.13 1.34 ug/L 63 14 -130 17 50
MCPA 17 U 213 161 M ug/L 75 52 -130 17 50
Mecoprop 19 U 213 168 ug/L 79 55 -134 15 50
Pentachlorophenol 0.037 U 0.532 0.419 M ug/L 79 57 -130 11 50
DCAA 45 -130
Surrogate
73
MSD MSD
Qualifier Limits%Recovery
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-433321/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433321
RL MDL
Nitrate as N 0.023 U 0.050 0.023 mg/L 05/14/16 08:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433321/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433321
Nitrate as N 0.999 1.02 mg/L 102 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-433321/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433321
Nitrate as N 0.999 1.02 mg/L 102 90 -110 0 15
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: SLMW-12AR-5-16Lab Sample ID: 680-125233-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433321
Nitrate as N 0.041 J 0.999 1.07 mg/L 103 80 -120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SLMW-12AR-5-16Lab Sample ID: 680-125233-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433321
Nitrate as N 0.041 J 0.999 1.08 mg/L 104 80 -120 0 15
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: SLMW-12AR-5-16Lab Sample ID: 680-125233-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433321
Nitrate as N 0.041 J 0.0414 J mg/L 0 15
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-433402/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434433 Prep Batch: 433402
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/15/16 10:00 05/20/16 20:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.40 U 0.401.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Arsenic
0.15 U 0.151.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Barium
0.070 U 0.0700.20 ug/L 05/15/16 10:00 05/20/16 20:51 1Beryllium
0.20 U 0.200.50 ug/L 05/15/16 10:00 05/20/16 20:51 1Cadmium
0.16 U 0.161.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Chromium
0.078 U 0.0780.20 ug/L 05/15/16 10:00 05/20/16 20:51 1Cobalt
0.21 U 0.211.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Copper
0.080 U 0.0800.30 ug/L 05/15/16 10:00 05/20/16 20:51 1Lead
0.080 U 0.0800.20 ug/L 05/15/16 10:00 05/20/16 20:51 1Mercury
0.40 U 0.401.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Nickel
0.10 U 0.100.20 ug/L 05/15/16 10:00 05/20/16 20:51 1Silver
0.10 U 0.100.20 ug/L 05/15/16 10:00 05/20/16 20:51 1Thallium
0.40 U 0.401.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Tin
1.4 U 1.45.0 ug/L 05/15/16 10:00 05/20/16 20:51 1Vanadium
2.6 U 2.610 ug/L 05/15/16 10:00 05/20/16 20:51 1Zinc
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-433402/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434443 Prep Batch: 433402
RL MDL
Selenium 0.224 J 0.50 0.21 ug/L 05/15/16 10:00 05/22/16 04:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433402/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434433 Prep Batch: 433402
Antimony 20.0 21.5 ug/L 108 75 -125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 40.0 48.4 ug/L 121 75 -125
Barium 40.0 40.6 ug/L 102 75 -125
Beryllium 20.0 22.5 ug/L 112 75 -125
Cadmium 20.0 22.1 ug/L 110 75 -125
Chromium 40.0 38.3 ug/L 96 75 -125
Cobalt 20.0 20.1 ug/L 100 75 -125
Copper 40.0 39.5 ug/L 99 75 -125
Lead 200 190 ug/L 95 75 -125
Mercury 2.00 2.05 ug/L 103 75 -125
Nickel 40.0 39.2 ug/L 98 75 -125
Silver 20.0 20.1 ug/L 100 75 -125
Thallium 16.0 15.2 ug/L 95 75 -125
Tin 80.0 78.9 ug/L 99 75 -125
Vanadium 40.0 37.3 ug/L 93 75 -125
Zinc 40.0 48.4 ug/L 121 75 -125
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433402/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434443 Prep Batch: 433402
Selenium 40.0 39.0 ug/L 98 75 -125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 680-125208-B-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434433 Prep Batch: 433402
Antimony 0.99 U 20.0 21.5 ug/L 108 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.40 U 40.0 46.1 ug/L 115 75 -125
Barium 33 40.0 75.1 ug/L 105 75 -125
Beryllium 0.24 20.0 23.0 ug/L 114 75 -125
Cadmium 0.20 U 20.0 22.1 ug/L 111 75 -125
Chromium 0.18 J 40.0 36.7 ug/L 91 75 -125
Cobalt 0.71 20.0 20.2 ug/L 97 75 -125
Copper 0.33 J 40.0 38.1 ug/L 94 75 -125
Lead 0.34 200 193 ug/L 96 75 -125
Mercury 0.095 J 2.00 2.24 ug/L 107 75 -125
Nickel 0.64 J 40.0 37.5 ug/L 92 75 -125
Silver 0.10 U 20.0 20.4 ug/L 102 75 -125
Thallium 0.15 J 16.0 15.5 ug/L 96 75 -125
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QC Sample Results
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 680-125208-B-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434433 Prep Batch: 433402
Tin 0.40 U 80.0 79.8 ug/L 100 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vanadium 1.4 U 40.0 36.4 ug/L 91 75 -125
Zinc 2.6 U J 40.0 47.6 ug/L 119 75 -125
Client Sample ID: Matrix SpikeLab Sample ID: 680-125208-B-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434443 Prep Batch: 433402
Selenium 0.44 J 40.0 38.7 ug/L 96 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125208-B-3-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434433 Prep Batch: 433402
Antimony 0.99 U 20.0 21.3 ug/L 106 75 -125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 0.40 U 40.0 45.3 ug/L 113 75 -125 2 20
Barium 33 40.0 73.7 ug/L 101 75 -125 2 20
Beryllium 0.24 20.0 22.6 ug/L 112 75 -125 2 20
Cadmium 0.20 U 20.0 22.0 ug/L 110 75 -125 1 20
Chromium 0.18 J 40.0 37.0 ug/L 92 75 -125 1 20
Cobalt 0.71 20.0 20.0 ug/L 97 75 -125 1 20
Copper 0.33 J 40.0 38.3 ug/L 95 75 -125 1 20
Lead 0.34 200 191 ug/L 95 75 -125 1 20
Mercury 0.095 J 2.00 2.17 ug/L 104 75 -125 3 20
Nickel 0.64 J 40.0 38.1 ug/L 94 75 -125 2 20
Silver 0.10 U 20.0 20.3 ug/L 102 75 -125 0 20
Thallium 0.15 J 16.0 15.6 ug/L 97 75 -125 1 20
Tin 0.40 U 80.0 78.6 ug/L 98 75 -125 2 20
Vanadium 1.4 U 40.0 36.8 ug/L 92 75 -125 1 20
Zinc 2.6 U J 40.0 47.2 ug/L 118 75 -125 1 20
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125208-B-3-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434443 Prep Batch: 433402
Selenium 0.44 J 40.0 38.3 ug/L 95 75 -125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 9012B - Cyanide, Total andor Amenable
Client Sample ID: Method BlankLab Sample ID: MB 680-433963/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434042 Prep Batch: 433963
RL MDL
Cyanide, Total 0.0025 U 0.010 0.0025 mg/L 05/19/16 06:22 05/19/16 11:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 9012B - Cyanide, Total andor Amenable (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433963/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434042 Prep Batch: 433963
Cyanide, Total 0.0500 0.0497 mg/L 99 85 -115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 680-125287-C-2-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434042 Prep Batch: 433963
Cyanide, Total 0.0025 U 0.0500 0.0533 mg/L 107 85 -115
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-125287-C-2-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434042 Prep Batch: 433963
Cyanide, Total 0.0025 U 0.0500 0.0516 mg/L 103 85 -115 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 660-73820-M-1-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434042 Prep Batch: 433963
Cyanide, Total 0.0025 U 0.0025 U mg/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric)
Client Sample ID: Method BlankLab Sample ID: MB 680-433793/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433803 Prep Batch: 433793
RL RL
Sulfide 10 U 10 10 mg/L 05/18/16 06:45 05/18/16 08:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-433793/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433803 Prep Batch: 433793
Sulfide 208 117 mg/L 56 50 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: SLMW-12AR-5-16Lab Sample ID: 680-125233-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433803 Prep Batch: 433793
Sulfide 10 U 208 122 mg/L 58 50 -150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric) (Continued)
Client Sample ID: SLMW-12AR-5-16Lab Sample ID: 680-125233-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433803 Prep Batch: 433793
Sulfide 10 U 208 120 mg/L 58 50 -150 1 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 680-125316-J-1-B DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433803 Prep Batch: 433793
Sulfide 10 U 10 U mg/L NC 50
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
GC/MS Semi VOA
Prep Batch: 433837
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C680-125233-1 SLMW-12AR-5-16 Total/NA
Water 3520C680-125287-F-1-A MS Matrix Spike Total/NA
Water 3520C680-125287-F-1-B MSD Matrix Spike Duplicate Total/NA
Water 3520CLCS 680-433837/10-A Lab Control Sample Total/NA
Water 3520CMB 680-433837/9-A Method Blank Total/NA
Analysis Batch: 434682
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 433837680-125233-1 SLMW-12AR-5-16 Total/NA
Water 8270D 433837680-125287-F-1-A MS Matrix Spike Total/NA
Water 8270D 433837680-125287-F-1-B MSD Matrix Spike Duplicate Total/NA
Water 8270D 433837LCS 680-433837/10-A Lab Control Sample Total/NA
Water 8270D 433837MB 680-433837/9-A Method Blank Total/NA
GC Semi VOA
Prep Batch: 176662
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-125233-1 SLMW-12AR-5-16 Total/NA
Water 3510CLCS 180-176662/2-A Lab Control Sample Total/NA
Water 3510CLCSD 180-176662/3-A Lab Control Sample Dup Total/NA
Water 3510CMB 180-176662/1-A Method Blank Total/NA
Analysis Batch: 177026
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8141B 176662680-125233-1 SLMW-12AR-5-16 Total/NA
Water 8141B 176662LCS 180-176662/2-A Lab Control Sample Total/NA
Water 8141B 176662LCSD 180-176662/3-A Lab Control Sample Dup Total/NA
Water 8141B 176662MB 180-176662/1-A Method Blank Total/NA
Prep Batch: 433502
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C680-125233-1 SLMW-12AR-5-16 Total/NA
Water 3520C680-125272-D-5-A MS Matrix Spike Total/NA
Water 3520C680-125272-D-5-B MSD Matrix Spike Duplicate Total/NA
Water 3520C680-125272-F-7-A MS Matrix Spike Total/NA
Water 3520C680-125272-F-7-B MSD Matrix Spike Duplicate Total/NA
Water 3520CLCS 680-433502/22-A Lab Control Sample Total/NA
Water 3520CLCS 680-433502/25-A Lab Control Sample Total/NA
Water 3520CLCS 680-433502/28-A Lab Control Sample Total/NA
Water 3520CLCSD 680-433502/29-A Lab Control Sample Dup Total/NA
Water 3520CMB 680-433502/21-A Method Blank Total/NA
Prep Batch: 433921
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A560-61466-D-3-B MS Matrix Spike Total/NA
Water 8151A560-61466-D-3-C MSD Matrix Spike Duplicate Total/NA
Water 8151A680-125233-1 SLMW-12AR-5-16 Total/NA
Water 8151ALCS 680-433921/13-A Lab Control Sample Total/NA
Water 8151AMB 680-433921/12-A Method Blank Total/NA
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
GC Semi VOA (Continued)
Analysis Batch: 434119
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B/8082A 433502680-125233-1 SLMW-12AR-5-16 Total/NA
Water 8081B/8082A 433502680-125272-D-5-A MS Matrix Spike Total/NA
Water 8081B/8082A 433502680-125272-D-5-B MSD Matrix Spike Duplicate Total/NA
Water 8081B/8082A 433502680-125272-F-7-A MS Matrix Spike Total/NA
Water 8081B/8082A 433502680-125272-F-7-B MSD Matrix Spike Duplicate Total/NA
Water 8081B/8082A 433502LCS 680-433502/22-A Lab Control Sample Total/NA
Water 8081B/8082A 433502LCS 680-433502/25-A Lab Control Sample Total/NA
Water 8081B/8082A 433502LCS 680-433502/28-A Lab Control Sample Total/NA
Water 8081B/8082A 433502LCSD 680-433502/29-A Lab Control Sample Dup Total/NA
Water 8081B/8082A 433502MB 680-433502/21-A Method Blank Total/NA
Analysis Batch: 434312
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A 433921560-61466-D-3-B MS Matrix Spike Total/NA
Water 8151A 433921560-61466-D-3-C MSD Matrix Spike Duplicate Total/NA
Water 8151A 433921680-125233-1 SLMW-12AR-5-16 Total/NA
Water 8151A 433921LCS 680-433921/13-A Lab Control Sample Total/NA
Water 8151A 433921MB 680-433921/12-A Method Blank Total/NA
HPLC/IC
Analysis Batch: 433321
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0680-125233-1 SLMW-12AR-5-16 Total/NA
Water 300.0680-125233-1 DU SLMW-12AR-5-16 Total/NA
Water 300.0680-125233-1 MS SLMW-12AR-5-16 Total/NA
Water 300.0680-125233-1 MSD SLMW-12AR-5-16 Total/NA
Water 300.0LCS 680-433321/3 Lab Control Sample Total/NA
Water 300.0LCSD 680-433321/4 Lab Control Sample Dup Total/NA
Water 300.0MB 680-433321/2 Method Blank Total/NA
Metals
Prep Batch: 433402
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3030C680-125208-B-3-B MS Matrix Spike Total/NA
Water 3030C680-125208-B-3-C MSD Matrix Spike Duplicate Total/NA
Water 3030C680-125233-1 SLMW-12AR-5-16 Total/NA
Water 3030CLCS 680-433402/2-A Lab Control Sample Total/NA
Water 3030CMB 680-433402/1-A Method Blank Total/NA
Analysis Batch: 434433
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 433402680-125208-B-3-B MS Matrix Spike Total/NA
Water 6020A 433402680-125208-B-3-C MSD Matrix Spike Duplicate Total/NA
Water 6020A 433402680-125233-1 SLMW-12AR-5-16 Total/NA
Water 6020A 433402LCS 680-433402/2-A Lab Control Sample Total/NA
Water 6020A 433402MB 680-433402/1-A Method Blank Total/NA
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-125233-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Metals (Continued)
Analysis Batch: 434443
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 433402680-125208-B-3-B MS Matrix Spike Total/NA
Water 6020A 433402680-125208-B-3-C MSD Matrix Spike Duplicate Total/NA
Water 6020A 433402680-125233-1 SLMW-12AR-5-16 Total/NA
Water 6020A 433402LCS 680-433402/2-A Lab Control Sample Total/NA
Water 6020A 433402MB 680-433402/1-A Method Blank Total/NA
General Chemistry
Prep Batch: 433793
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9030B680-125233-1 SLMW-12AR-5-16 Total/NA
Water 9030B680-125233-1 MS SLMW-12AR-5-16 Total/NA
Water 9030B680-125233-1 MSD SLMW-12AR-5-16 Total/NA
Water 9030B680-125316-J-1-B DU Duplicate Total/NA
Water 9030BLCS 680-433793/2-A Lab Control Sample Total/NA
Water 9030BMB 680-433793/1-A Method Blank Total/NA
Analysis Batch: 433803
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9034 433793680-125233-1 SLMW-12AR-5-16 Total/NA
Water 9034 433793680-125233-1 MS SLMW-12AR-5-16 Total/NA
Water 9034 433793680-125233-1 MSD SLMW-12AR-5-16 Total/NA
Water 9034 433793680-125316-J-1-B DU Duplicate Total/NA
Water 9034 433793LCS 680-433793/2-A Lab Control Sample Total/NA
Water 9034 433793MB 680-433793/1-A Method Blank Total/NA
Prep Batch: 433963
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9012B660-73820-M-1-B DU Duplicate Total/NA
Water 9012B680-125233-1 SLMW-12AR-5-16 Total/NA
Water 9012B680-125287-C-2-B MS Matrix Spike Total/NA
Water 9012B680-125287-C-2-C MSD Matrix Spike Duplicate Total/NA
Water 9012BLCS 680-433963/2-A Lab Control Sample Total/NA
Water 9012BMB 680-433963/1-A Method Blank Total/NA
Analysis Batch: 434042
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9012B 433963660-73820-M-1-B DU Duplicate Total/NA
Water 9012B 433963680-125233-1 SLMW-12AR-5-16 Total/NA
Water 9012B 433963680-125287-C-2-B MS Matrix Spike Total/NA
Water 9012B 433963680-125287-C-2-C MSD Matrix Spike Duplicate Total/NA
Water 9012B 433963LCS 680-433963/2-A Lab Control Sample Total/NA
Water 9012B 433963MB 680-433963/1-A Method Blank Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125233-1
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: SLMW-12AR-5-16 Lab Sample ID: 680-125233-1
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Prep 3520C 05/18/16 16:30 RBS433837 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270D 1 434682 05/24/16 19:53 JEM TAL SAVTotal/NA
Prep 3520C 433502 05/16/16 16:28 RBS TAL SAVTotal/NA
Analysis 8081B/8082A 1 434119 05/19/16 20:42 JCK TAL SAVTotal/NA
Prep 3510C 176662 05/18/16 12:45 CBY TAL PITTotal/NA
Analysis 8141B 1 177026 05/23/16 23:17 JMO TAL PITTotal/NA
Prep 8151A 433921 05/19/16 08:53 MAV TAL SAVTotal/NA
Analysis 8151A 1 434312 05/21/16 04:45 JCK TAL SAVTotal/NA
Analysis 300.0 1 433321 05/14/16 10:39 JRJ TAL SAVTotal/NA
Prep 3030C 433402 05/15/16 10:00 CRW TAL SAVTotal/NA
Analysis 6020A 1 434433 05/20/16 23:17 BJB TAL SAVTotal/NA
Prep 3030C 433402 05/15/16 10:00 CRW TAL SAVTotal/NA
Analysis 6020A 1 434443 05/22/16 06:25 BWR TAL SAVTotal/NA
Prep 9012B 433963 05/19/16 06:22 DAM TAL SAVTotal/NA
Analysis 9012B 1 434042 05/19/16 11:37 DAM TAL SAVTotal/NA
Prep 9030B 433793 05/18/16 06:45 DAM TAL SAVTotal/NA
Analysis 9034 1 433803 05/18/16 08:24 DAM TAL SAVTotal/NA
Laboratory References:
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-125233-1
Login Number: 125233
Question Answer Comment
Creator: Murray, Thomas J
List Source: TestAmerica Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-125233-1
Login Number: 125233
Question Answer Comment
Creator: Watson, Debbie
List Source: TestAmerica Pittsburgh
List Creation: 05/14/16 11:49 AMList Number: 2
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah
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Certification Summary
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125233-1
Project/Site: Ft.Bragg - Longstreet Landfill
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA 399.01DoD ELAP 02-28-17
North Carolina (DW)State Program 4 13701 07-31-16 *
Laboratory: TestAmerica Pittsburgh
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Arkansas DEQ 88-06906State Program 06-27-16
California State Program 9 2891 03-31-18
Connecticut State Program 1 PH-0688 09-30-16
Florida NELAP 4 E871008 06-30-16
Illinois NELAP 5 200005 06-30-16
Kansas NELAP 7 E-10350 07-31-16
Louisiana NELAP 6 04041 06-30-16
New Hampshire NELAP 1 2030 04-04-17
New Jersey NELAP 2 PA005 06-30-16
New York NELAP 2 11182 03-31-17
North Carolina (WW/SW)State Program 4 434 12-31-16
Pennsylvania NELAP 3 02-00416 04-30-17
South Carolina State Program 4 89014 04-30-16 *
Texas NELAP 6 T104704528-15-2 03-31-17
US Fish & Wildlife Federal LE94312A-1 10-31-16
USDA Federal P-Soil-01 05-23-16 *
Utah NELAP 8 PA001462015-4 05-31-16 *
Virginia NELAP 3 460189 09-14-16
West Virginia DEP State Program 3 142 01-31-17
Wisconsin State Program 5 998027800 08-31-16
TestAmerica Savannah
* Certification renewal pending - certification considered valid.
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-125257-1
Client Project/Site: Ft.Bragg - Longstreet Landfill
For:
U.S. Army Corps of Engineers
100 W. Oglethorpe Ave.
Savannah, Georgia 31401
Attn: John P. Markov
Authorized for release by:
5/26/2016 10:20:31 AM
Robert Bearden, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
TestAmerica Job ID: 680-125257-1
Page 2 of 23 TestAmerica Savannah5/26/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125257-1
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-125257-1
Laboratory: TestAmerica Savannah
Narrative
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Longstreet Landfill
Report Number: 680-125257-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 05/13/2016; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 2.2 C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples SLMW-12AR-5-16 (680-125257-1), Trip Blank (680-125257-2) and SLMW-12BR-5-16 (680-125257-3) were analyzed for Volatile
Organic Compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 05/25/2016.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with analytical batch 680-434853.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica SavannahPage 3 of 23 5/26/2016
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Sample Summary
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-125257-1 SLMW-12AR-5-16 Water 05/12/16 13:45 05/13/16 09:13
680-125257-2 Trip Blank Water 05/12/16 12:00 05/13/16 09:13
680-125257-3 SLMW-12BR-5-16 Water 05/12/16 15:25 05/13/16 09:13
TestAmerica Savannah
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Method Summary
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL SAV
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Definitions/Glossary
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Qualifiers
GC/MS VOA
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
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Detection Summary
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: SLMW-12AR-5-16 Lab Sample ID: 680-125257-1
No Detections.
Client Sample ID: Trip Blank Lab Sample ID: 680-125257-2
No Detections.
Client Sample ID: SLMW-12BR-5-16 Lab Sample ID: 680-125257-3
No Detections.
TestAmerica Savannah
This Detection Summary does not include radiochemical test results.
Page 7 of 23 5/26/2016
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Client Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125257-1Client Sample ID: SLMW-12AR-5-16
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 7.0 U 10 7.0 ug/L 05/25/16 20:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.43 ug/L 05/25/16 20:51 1Benzene0.43 U
1.0 0.50 ug/L 05/25/16 20:51 1Bromobenzene0.50 U
1.0 0.43 ug/L 05/25/16 20:51 1Bromoform0.43 U
5.0 2.5 ug/L 05/25/16 20:51 1Bromomethane2.5 U
10 3.4 ug/L 05/25/16 20:51 12-Butanone (MEK)3.4 U
1.0 0.33 ug/L 05/25/16 20:51 1Carbon tetrachloride 0.33 U
1.0 0.26 ug/L 05/25/16 20:51 1Chlorobenzene0.26 U
1.0 0.45 ug/L 05/25/16 20:51 1Chlorobromomethane0.45 U
1.0 0.32 ug/L 05/25/16 20:51 1Chlorodibromomethane0.32 U
5.0 2.5 ug/L 05/25/16 20:51 1Chloroethane2.5 U
1.0 0.50 ug/L 05/25/16 20:51 1Chloroform0.50 U
5.0 1.1 ug/L 05/25/16 20:51 11-Chlorohexane 1.1 U
1.0 0.40 ug/L 05/25/16 20:51 1Chloromethane0.40 U
1.0 0.27 ug/L 05/25/16 20:51 12-Chlorotoluene 0.27 U
1.0 0.45 ug/L 05/25/16 20:51 14-Chlorotoluene 0.45 U
1.0 0.41 ug/L 05/25/16 20:51 1cis-1,2-Dichloroethene 0.41 U
1.0 0.40 ug/L 05/25/16 20:51 1cis-1,3-Dichloropropene 0.40 U
5.0 1.1 ug/L 05/25/16 20:51 11,2-Dibromo-3-Chloropropane 1.1 U
1.0 0.37 ug/L 05/25/16 20:51 11,2-Dichlorobenzene 0.37 U
1.0 0.43 ug/L 05/25/16 20:51 11,3-Dichlorobenzene 0.43 U
1.0 0.46 ug/L 05/25/16 20:51 11,4-Dichlorobenzene 0.46 U
1.0 0.44 ug/L 05/25/16 20:51 1Dichlorobromomethane0.44 U
1.0 0.60 ug/L 05/25/16 20:51 1Dichlorodifluoromethane0.60 U
1.0 0.38 ug/L 05/25/16 20:51 11,1-Dichloroethane 0.38 U
1.0 0.50 ug/L 05/25/16 20:51 11,2-Dichloroethane 0.50 U
1.0 0.36 ug/L 05/25/16 20:51 11,1-Dichloroethene 0.36 U
1.0 0.67 ug/L 05/25/16 20:51 11,2-Dichloropropane 0.67 U
1.0 0.34 ug/L 05/25/16 20:51 11,3-Dichloropropane 0.34 U
1.0 0.37 ug/L 05/25/16 20:51 12,2-Dichloropropane 0.37 U
1.0 0.34 ug/L 05/25/16 20:51 11,1-Dichloropropene 0.34 U
1.0 0.33 ug/L 05/25/16 20:51 1Ethylbenzene0.33 U
1.0 0.44 ug/L 05/25/16 20:51 1Ethylene Dibromide 0.44 U
5.0 2.5 ug/L 05/25/16 20:51 1Hexachlorobutadiene2.5 U
1.0 0.35 ug/L 05/25/16 20:51 1Isopropylbenzene0.35 U
10 1.0 ug/L 05/25/16 20:51 1Isopropyl ether 1.0 U
1.0 0.48 ug/L 05/25/16 20:51 14-Isopropyltoluene 0.48 U
5.0 2.5 ug/L 05/25/16 20:51 1Methylene Chloride 2.5 U
10 2.1 ug/L 05/25/16 20:51 14-Methyl-2-pentanone (MIBK)2.1 U
10 0.30 ug/L 05/25/16 20:51 1Methyl tert-butyl ether 0.30 U
5.0 2.5 ug/L 05/25/16 20:51 1Naphthalene2.5 U
1.0 0.47 ug/L 05/25/16 20:51 1n-Butylbenzene 0.47 U
1.0 0.38 ug/L 05/25/16 20:51 1N-Propylbenzene 0.38 U
1.0 0.42 ug/L 05/25/16 20:51 1sec-Butylbenzene 0.42 U
1.0 0.27 ug/L 05/25/16 20:51 1Styrene0.27 U
1.0 0.45 ug/L 05/25/16 20:51 1tert-Butylbenzene 0.45 U
1.0 0.37 ug/L 05/25/16 20:51 11,1,1,2-Tetrachloroethane 0.37 U
1.0 0.62 ug/L 05/25/16 20:51 11,1,2,2-Tetrachloroethane 0.62 U
1.0 0.74 ug/L 05/25/16 20:51 1Tetrachloroethene0.74 U
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Client Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125257-1Client Sample ID: SLMW-12AR-5-16
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.48 U 1.0 0.48 ug/L 05/25/16 20:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.37 ug/L 05/25/16 20:51 1trans-1,2-Dichloroethene 0.37 U
1.0 0.42 ug/L 05/25/16 20:51 1trans-1,3-Dichloropropene 0.42 U
5.0 2.5 ug/L 05/25/16 20:51 11,2,3-Trichlorobenzene 2.5 U
5.0 2.5 ug/L 05/25/16 20:51 11,2,4-Trichlorobenzene 2.5 U
1.0 0.37 ug/L 05/25/16 20:51 11,1,1-Trichloroethane 0.37 U
1.0 0.33 ug/L 05/25/16 20:51 11,1,2-Trichloroethane 0.33 U
1.0 0.48 ug/L 05/25/16 20:51 1Trichloroethene0.48 U
1.0 0.42 ug/L 05/25/16 20:51 1Trichlorofluoromethane0.42 U
1.0 0.39 ug/L 05/25/16 20:51 11,2,3-Trichloropropane 0.39 U
1.0 0.47 ug/L 05/25/16 20:51 11,2,4-Trimethylbenzene 0.47 U
1.0 0.31 ug/L 05/25/16 20:51 11,3,5-Trimethylbenzene 0.31 U
1.0 0.50 ug/L 05/25/16 20:51 1Vinyl chloride 0.50 U
Toluene-d8 (Surr)107 70-130 05/25/16 20:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)106 05/25/16 20:51 170-130
Dibromofluoromethane (Surr)106 05/25/16 20:51 170-130
4-Bromofluorobenzene (Surr)100 05/25/16 20:51 170-130
Lab Sample ID: 680-125257-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 05/12/16 12:00
Date Received: 05/13/16 09:13
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 7.0 U 10 7.0 ug/L 05/25/16 19:47 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.43 ug/L 05/25/16 19:47 1Benzene0.43 U
1.0 0.50 ug/L 05/25/16 19:47 1Bromobenzene0.50 U
1.0 0.43 ug/L 05/25/16 19:47 1Bromoform0.43 U
5.0 2.5 ug/L 05/25/16 19:47 1Bromomethane2.5 U
10 3.4 ug/L 05/25/16 19:47 12-Butanone (MEK)3.4 U
1.0 0.33 ug/L 05/25/16 19:47 1Carbon tetrachloride 0.33 U
1.0 0.26 ug/L 05/25/16 19:47 1Chlorobenzene0.26 U
1.0 0.45 ug/L 05/25/16 19:47 1Chlorobromomethane0.45 U
1.0 0.32 ug/L 05/25/16 19:47 1Chlorodibromomethane0.32 U
5.0 2.5 ug/L 05/25/16 19:47 1Chloroethane2.5 U
1.0 0.50 ug/L 05/25/16 19:47 1Chloroform0.50 U
5.0 1.1 ug/L 05/25/16 19:47 11-Chlorohexane 1.1 U
1.0 0.40 ug/L 05/25/16 19:47 1Chloromethane0.40 U
1.0 0.27 ug/L 05/25/16 19:47 12-Chlorotoluene 0.27 U
1.0 0.45 ug/L 05/25/16 19:47 14-Chlorotoluene 0.45 U
1.0 0.41 ug/L 05/25/16 19:47 1cis-1,2-Dichloroethene 0.41 U
1.0 0.40 ug/L 05/25/16 19:47 1cis-1,3-Dichloropropene 0.40 U
5.0 1.1 ug/L 05/25/16 19:47 11,2-Dibromo-3-Chloropropane 1.1 U
1.0 0.37 ug/L 05/25/16 19:47 11,2-Dichlorobenzene 0.37 U
1.0 0.43 ug/L 05/25/16 19:47 11,3-Dichlorobenzene 0.43 U
1.0 0.46 ug/L 05/25/16 19:47 11,4-Dichlorobenzene 0.46 U
1.0 0.44 ug/L 05/25/16 19:47 1Dichlorobromomethane0.44 U
1.0 0.60 ug/L 05/25/16 19:47 1Dichlorodifluoromethane0.60 U
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Client Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125257-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 05/12/16 12:00
Date Received: 05/13/16 09:13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane 0.38 U 1.0 0.38 ug/L 05/25/16 19:47 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.50 ug/L 05/25/16 19:47 11,2-Dichloroethane 0.50 U
1.0 0.36 ug/L 05/25/16 19:47 11,1-Dichloroethene 0.36 U
1.0 0.67 ug/L 05/25/16 19:47 11,2-Dichloropropane 0.67 U
1.0 0.34 ug/L 05/25/16 19:47 11,3-Dichloropropane 0.34 U
1.0 0.37 ug/L 05/25/16 19:47 12,2-Dichloropropane 0.37 U
1.0 0.34 ug/L 05/25/16 19:47 11,1-Dichloropropene 0.34 U
1.0 0.33 ug/L 05/25/16 19:47 1Ethylbenzene0.33 U
1.0 0.44 ug/L 05/25/16 19:47 1Ethylene Dibromide 0.44 U
5.0 2.5 ug/L 05/25/16 19:47 1Hexachlorobutadiene2.5 U
1.0 0.35 ug/L 05/25/16 19:47 1Isopropylbenzene0.35 U
10 1.0 ug/L 05/25/16 19:47 1Isopropyl ether 1.0 U
1.0 0.48 ug/L 05/25/16 19:47 14-Isopropyltoluene 0.48 U
5.0 2.5 ug/L 05/25/16 19:47 1Methylene Chloride 2.5 U
10 2.1 ug/L 05/25/16 19:47 14-Methyl-2-pentanone (MIBK)2.1 U
10 0.30 ug/L 05/25/16 19:47 1Methyl tert-butyl ether 0.30 U
5.0 2.5 ug/L 05/25/16 19:47 1Naphthalene2.5 U
1.0 0.47 ug/L 05/25/16 19:47 1n-Butylbenzene 0.47 U
1.0 0.38 ug/L 05/25/16 19:47 1N-Propylbenzene 0.38 U
1.0 0.42 ug/L 05/25/16 19:47 1sec-Butylbenzene 0.42 U
1.0 0.27 ug/L 05/25/16 19:47 1Styrene0.27 U
1.0 0.45 ug/L 05/25/16 19:47 1tert-Butylbenzene 0.45 U
1.0 0.37 ug/L 05/25/16 19:47 11,1,1,2-Tetrachloroethane 0.37 U
1.0 0.62 ug/L 05/25/16 19:47 11,1,2,2-Tetrachloroethane 0.62 U
1.0 0.74 ug/L 05/25/16 19:47 1Tetrachloroethene0.74 U
1.0 0.48 ug/L 05/25/16 19:47 1Toluene0.48 U
1.0 0.37 ug/L 05/25/16 19:47 1trans-1,2-Dichloroethene 0.37 U
1.0 0.42 ug/L 05/25/16 19:47 1trans-1,3-Dichloropropene 0.42 U
5.0 2.5 ug/L 05/25/16 19:47 11,2,3-Trichlorobenzene 2.5 U
5.0 2.5 ug/L 05/25/16 19:47 11,2,4-Trichlorobenzene 2.5 U
1.0 0.37 ug/L 05/25/16 19:47 11,1,1-Trichloroethane 0.37 U
1.0 0.33 ug/L 05/25/16 19:47 11,1,2-Trichloroethane 0.33 U
1.0 0.48 ug/L 05/25/16 19:47 1Trichloroethene0.48 U
1.0 0.42 ug/L 05/25/16 19:47 1Trichlorofluoromethane0.42 U
1.0 0.39 ug/L 05/25/16 19:47 11,2,3-Trichloropropane 0.39 U
1.0 0.47 ug/L 05/25/16 19:47 11,2,4-Trimethylbenzene 0.47 U
1.0 0.31 ug/L 05/25/16 19:47 11,3,5-Trimethylbenzene 0.31 U
1.0 0.50 ug/L 05/25/16 19:47 1Vinyl chloride 0.50 U
Toluene-d8 (Surr)105 70-130 05/25/16 19:47 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)107 05/25/16 19:47 170-130
Dibromofluoromethane (Surr)104 05/25/16 19:47 170-130
4-Bromofluorobenzene (Surr)97 05/25/16 19:47 170-130
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Client Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125257-3Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/13/16 09:13
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 7.0 U 10 7.0 ug/L 05/25/16 21:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.43 ug/L 05/25/16 21:12 1Benzene0.43 U
1.0 0.50 ug/L 05/25/16 21:12 1Bromobenzene0.50 U
1.0 0.43 ug/L 05/25/16 21:12 1Bromoform0.43 U
5.0 2.5 ug/L 05/25/16 21:12 1Bromomethane2.5 U
10 3.4 ug/L 05/25/16 21:12 12-Butanone (MEK)3.4 U
1.0 0.33 ug/L 05/25/16 21:12 1Carbon tetrachloride 0.33 U
1.0 0.26 ug/L 05/25/16 21:12 1Chlorobenzene0.26 U
1.0 0.45 ug/L 05/25/16 21:12 1Chlorobromomethane0.45 U
1.0 0.32 ug/L 05/25/16 21:12 1Chlorodibromomethane0.32 U
5.0 2.5 ug/L 05/25/16 21:12 1Chloroethane2.5 U
1.0 0.50 ug/L 05/25/16 21:12 1Chloroform0.50 U
5.0 1.1 ug/L 05/25/16 21:12 11-Chlorohexane 1.1 U
1.0 0.40 ug/L 05/25/16 21:12 1Chloromethane0.40 U
1.0 0.27 ug/L 05/25/16 21:12 12-Chlorotoluene 0.27 U
1.0 0.45 ug/L 05/25/16 21:12 14-Chlorotoluene 0.45 U
1.0 0.41 ug/L 05/25/16 21:12 1cis-1,2-Dichloroethene 0.41 U
1.0 0.40 ug/L 05/25/16 21:12 1cis-1,3-Dichloropropene 0.40 U
5.0 1.1 ug/L 05/25/16 21:12 11,2-Dibromo-3-Chloropropane 1.1 U
1.0 0.37 ug/L 05/25/16 21:12 11,2-Dichlorobenzene 0.37 U
1.0 0.43 ug/L 05/25/16 21:12 11,3-Dichlorobenzene 0.43 U
1.0 0.46 ug/L 05/25/16 21:12 11,4-Dichlorobenzene 0.46 U
1.0 0.44 ug/L 05/25/16 21:12 1Dichlorobromomethane0.44 U
1.0 0.60 ug/L 05/25/16 21:12 1Dichlorodifluoromethane0.60 U
1.0 0.38 ug/L 05/25/16 21:12 11,1-Dichloroethane 0.38 U
1.0 0.50 ug/L 05/25/16 21:12 11,2-Dichloroethane 0.50 U
1.0 0.36 ug/L 05/25/16 21:12 11,1-Dichloroethene 0.36 U
1.0 0.67 ug/L 05/25/16 21:12 11,2-Dichloropropane 0.67 U
1.0 0.34 ug/L 05/25/16 21:12 11,3-Dichloropropane 0.34 U
1.0 0.37 ug/L 05/25/16 21:12 12,2-Dichloropropane 0.37 U
1.0 0.34 ug/L 05/25/16 21:12 11,1-Dichloropropene 0.34 U
1.0 0.33 ug/L 05/25/16 21:12 1Ethylbenzene0.33 U
1.0 0.44 ug/L 05/25/16 21:12 1Ethylene Dibromide 0.44 U
5.0 2.5 ug/L 05/25/16 21:12 1Hexachlorobutadiene2.5 U
1.0 0.35 ug/L 05/25/16 21:12 1Isopropylbenzene0.35 U
10 1.0 ug/L 05/25/16 21:12 1Isopropyl ether 1.0 U
1.0 0.48 ug/L 05/25/16 21:12 14-Isopropyltoluene 0.48 U
5.0 2.5 ug/L 05/25/16 21:12 1Methylene Chloride 2.5 U
10 2.1 ug/L 05/25/16 21:12 14-Methyl-2-pentanone (MIBK)2.1 U
10 0.30 ug/L 05/25/16 21:12 1Methyl tert-butyl ether 0.30 U
5.0 2.5 ug/L 05/25/16 21:12 1Naphthalene2.5 U
1.0 0.47 ug/L 05/25/16 21:12 1n-Butylbenzene 0.47 U
1.0 0.38 ug/L 05/25/16 21:12 1N-Propylbenzene 0.38 U
1.0 0.42 ug/L 05/25/16 21:12 1sec-Butylbenzene 0.42 U
1.0 0.27 ug/L 05/25/16 21:12 1Styrene0.27 U
1.0 0.45 ug/L 05/25/16 21:12 1tert-Butylbenzene 0.45 U
1.0 0.37 ug/L 05/25/16 21:12 11,1,1,2-Tetrachloroethane 0.37 U
1.0 0.62 ug/L 05/25/16 21:12 11,1,2,2-Tetrachloroethane 0.62 U
1.0 0.74 ug/L 05/25/16 21:12 1Tetrachloroethene0.74 U
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Client Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125257-3Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/13/16 09:13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene 0.48 U 1.0 0.48 ug/L 05/25/16 21:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.37 ug/L 05/25/16 21:12 1trans-1,2-Dichloroethene 0.37 U
1.0 0.42 ug/L 05/25/16 21:12 1trans-1,3-Dichloropropene 0.42 U
5.0 2.5 ug/L 05/25/16 21:12 11,2,3-Trichlorobenzene 2.5 U
5.0 2.5 ug/L 05/25/16 21:12 11,2,4-Trichlorobenzene 2.5 U
1.0 0.37 ug/L 05/25/16 21:12 11,1,1-Trichloroethane 0.37 U
1.0 0.33 ug/L 05/25/16 21:12 11,1,2-Trichloroethane 0.33 U
1.0 0.48 ug/L 05/25/16 21:12 1Trichloroethene0.48 U
1.0 0.42 ug/L 05/25/16 21:12 1Trichlorofluoromethane0.42 U
1.0 0.39 ug/L 05/25/16 21:12 11,2,3-Trichloropropane 0.39 U
1.0 0.47 ug/L 05/25/16 21:12 11,2,4-Trimethylbenzene 0.47 U
1.0 0.31 ug/L 05/25/16 21:12 11,3,5-Trimethylbenzene 0.31 U
1.0 0.50 ug/L 05/25/16 21:12 1Vinyl chloride 0.50 U
Toluene-d8 (Surr)105 70-130 05/25/16 21:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)106 05/25/16 21:12 170-130
Dibromofluoromethane (Surr)105 05/25/16 21:12 170-130
4-Bromofluorobenzene (Surr)99 05/25/16 21:12 170-130
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Surrogate Summary
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130) (70-130) (70-130) (70-130)
TOL 12DCE DBFM BFB
107 106 106 100680-125257-1
Percent Surrogate Recovery (Acceptance Limits)
SLMW-12AR-5-16
105 107 104 97680-125257-2 Trip Blank
105 106 105 99680-125257-3 SLMW-12BR-5-16
96 101 101 88LCS 680-434853/4 Lab Control Sample
96 101 101 89LCSD 680-434853/5 Lab Control Sample Dup
106 107 105 100MB 680-434853/9 Method Blank
Surrogate Legend
TOL = Toluene-d8 (Surr)
12DCE = 1,2-Dichloroethane-d4 (Surr)
DBFM = Dibromofluoromethane (Surr)
BFB = 4-Bromofluorobenzene (Surr)
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QC Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-434853/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434853
RL MDL
Acetone 7.0 U 10 7.0 ug/L 05/25/16 19:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.43 U 0.431.0 ug/L 05/25/16 19:26 1Benzene
0.50 U 0.501.0 ug/L 05/25/16 19:26 1Bromobenzene
0.43 U 0.431.0 ug/L 05/25/16 19:26 1Bromoform
2.5 U 2.55.0 ug/L 05/25/16 19:26 1Bromomethane
3.4 U 3.410 ug/L 05/25/16 19:26 12-Butanone (MEK)
0.33 U 0.331.0 ug/L 05/25/16 19:26 1Carbon tetrachloride
0.26 U 0.261.0 ug/L 05/25/16 19:26 1Chlorobenzene
0.45 U 0.451.0 ug/L 05/25/16 19:26 1Chlorobromomethane
0.32 U 0.321.0 ug/L 05/25/16 19:26 1Chlorodibromomethane
2.5 U 2.55.0 ug/L 05/25/16 19:26 1Chloroethane
0.50 U 0.501.0 ug/L 05/25/16 19:26 1Chloroform
1.1 U 1.15.0 ug/L 05/25/16 19:26 11-Chlorohexane
0.40 U 0.401.0 ug/L 05/25/16 19:26 1Chloromethane
0.27 U 0.271.0 ug/L 05/25/16 19:26 12-Chlorotoluene
0.45 U 0.451.0 ug/L 05/25/16 19:26 14-Chlorotoluene
0.41 U 0.411.0 ug/L 05/25/16 19:26 1cis-1,2-Dichloroethene
0.40 U 0.401.0 ug/L 05/25/16 19:26 1cis-1,3-Dichloropropene
1.1 U 1.15.0 ug/L 05/25/16 19:26 11,2-Dibromo-3-Chloropropane
0.37 U 0.371.0 ug/L 05/25/16 19:26 11,2-Dichlorobenzene
0.43 U 0.431.0 ug/L 05/25/16 19:26 11,3-Dichlorobenzene
0.46 U 0.461.0 ug/L 05/25/16 19:26 11,4-Dichlorobenzene
0.44 U 0.441.0 ug/L 05/25/16 19:26 1Dichlorobromomethane
0.60 U 0.601.0 ug/L 05/25/16 19:26 1Dichlorodifluoromethane
0.38 U 0.381.0 ug/L 05/25/16 19:26 11,1-Dichloroethane
0.50 U 0.501.0 ug/L 05/25/16 19:26 11,2-Dichloroethane
0.36 U 0.361.0 ug/L 05/25/16 19:26 11,1-Dichloroethene
0.67 U 0.671.0 ug/L 05/25/16 19:26 11,2-Dichloropropane
0.34 U 0.341.0 ug/L 05/25/16 19:26 11,3-Dichloropropane
0.37 U 0.371.0 ug/L 05/25/16 19:26 12,2-Dichloropropane
0.34 U 0.341.0 ug/L 05/25/16 19:26 11,1-Dichloropropene
0.33 U 0.331.0 ug/L 05/25/16 19:26 1Ethylbenzene
0.44 U 0.441.0 ug/L 05/25/16 19:26 1Ethylene Dibromide
2.5 U 2.55.0 ug/L 05/25/16 19:26 1Hexachlorobutadiene
0.35 U 0.351.0 ug/L 05/25/16 19:26 1Isopropylbenzene
1.0 U 1.010 ug/L 05/25/16 19:26 1Isopropyl ether
0.48 U 0.481.0 ug/L 05/25/16 19:26 14-Isopropyltoluene
2.5 U 2.55.0 ug/L 05/25/16 19:26 1Methylene Chloride
2.1 U 2.110 ug/L 05/25/16 19:26 14-Methyl-2-pentanone (MIBK)
0.30 U 0.3010 ug/L 05/25/16 19:26 1Methyl tert-butyl ether
2.5 U 2.55.0 ug/L 05/25/16 19:26 1Naphthalene
0.47 U 0.471.0 ug/L 05/25/16 19:26 1n-Butylbenzene
0.38 U 0.381.0 ug/L 05/25/16 19:26 1N-Propylbenzene
0.42 U 0.421.0 ug/L 05/25/16 19:26 1sec-Butylbenzene
0.27 U 0.271.0 ug/L 05/25/16 19:26 1Styrene
0.45 U 0.451.0 ug/L 05/25/16 19:26 1tert-Butylbenzene
0.37 U 0.371.0 ug/L 05/25/16 19:26 11,1,1,2-Tetrachloroethane
0.62 U 0.621.0 ug/L 05/25/16 19:26 11,1,2,2-Tetrachloroethane
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-434853/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434853
RL MDL
Tetrachloroethene 0.74 U 1.0 0.74 ug/L 05/25/16 19:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.48 U 0.481.0 ug/L 05/25/16 19:26 1Toluene
0.37 U 0.371.0 ug/L 05/25/16 19:26 1trans-1,2-Dichloroethene
0.42 U 0.421.0 ug/L 05/25/16 19:26 1trans-1,3-Dichloropropene
2.5 U 2.55.0 ug/L 05/25/16 19:26 11,2,3-Trichlorobenzene
2.5 U 2.55.0 ug/L 05/25/16 19:26 11,2,4-Trichlorobenzene
0.37 U 0.371.0 ug/L 05/25/16 19:26 11,1,1-Trichloroethane
0.33 U 0.331.0 ug/L 05/25/16 19:26 11,1,2-Trichloroethane
0.48 U 0.481.0 ug/L 05/25/16 19:26 1Trichloroethene
0.42 U 0.421.0 ug/L 05/25/16 19:26 1Trichlorofluoromethane
0.39 U 0.391.0 ug/L 05/25/16 19:26 11,2,3-Trichloropropane
0.47 U 0.471.0 ug/L 05/25/16 19:26 11,2,4-Trimethylbenzene
0.31 U 0.311.0 ug/L 05/25/16 19:26 11,3,5-Trimethylbenzene
0.50 U 0.501.0 ug/L 05/25/16 19:26 1Vinyl chloride
Toluene-d8 (Surr)106 70-130 05/25/16 19:26 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
107 05/25/16 19:26 11,2-Dichloroethane-d4 (Surr)70-130
105 05/25/16 19:26 1Dibromofluoromethane (Surr)70-130
100 05/25/16 19:26 14-Bromofluorobenzene (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-434853/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434853
Acetone 250 246 ug/L 99 60 -154
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 44.0 ug/L 88 73 -131
Bromobenzene 50.0 48.8 ug/L 98 79 -124
Bromoform 50.0 51.7 ug/L 103 69 -135
Bromomethane 50.0 62.6 ug/L 125 20 -180
2-Butanone (MEK)250 235 ug/L 94 75 -133
Carbon tetrachloride 50.0 49.1 ug/L 98 75 -130
Chlorobenzene 50.0 46.8 ug/L 94 80 -120
Chlorobromomethane 50.0 49.1 ug/L 98 77 -122
Chlorodibromomethane 50.0 52.6 ug/L 105 71 -136
Chloroethane 50.0 49.1 ug/L 98 50 -151
Chloroform 50.0 44.5 ug/L 89 79 -122
Chloromethane 50.0 43.8 ug/L 88 63 -126
2-Chlorotoluene 50.0 47.4 ug/L 95 77 -121
4-Chlorotoluene 50.0 47.5 ug/L 95 80 -120
cis-1,2-Dichloroethene 50.0 50.6 ug/L 101 80 -122
cis-1,3-Dichloropropene 50.0 46.9 ug/L 94 80 -133
1,2-Dibromo-3-Chloropropane 50.0 47.8 ug/L 96 59 -141
1,2-Dichlorobenzene 50.0 45.7 ug/L 91 80 -120
1,3-Dichlorobenzene 50.0 45.2 ug/L 90 80 -120
1,4-Dichlorobenzene 50.0 44.4 ug/L 89 80 -120
Dichlorobromomethane 50.0 48.9 ug/L 98 77 -129
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-434853/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434853
Dichlorodifluoromethane 50.0 50.7 ug/L 101 51 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1-Dichloroethane 50.0 47.0 ug/L 94 80 -120
1,2-Dichloroethane 50.0 49.0 ug/L 98 75 -130
1,1-Dichloroethene 50.0 46.3 ug/L 93 74 -125
1,2-Dichloropropane 50.0 46.6 ug/L 93 80 -123
1,3-Dichloropropane 50.0 46.7 ug/L 93 78 -127
2,2-Dichloropropane 50.0 51.7 ug/L 103 72 -133
1,1-Dichloropropene 50.0 46.4 ug/L 93 78 -127
Ethylbenzene 50.0 47.0 ug/L 94 80 -120
Ethylene Dibromide 50.0 47.8 ug/L 96 77 -131
Hexachlorobutadiene 50.0 51.2 ug/L 102 77 -129
Isopropylbenzene 50.0 49.0 ug/L 98 80 -120
4-Isopropyltoluene 50.0 47.2 ug/L 94 80 -120
Methylene Chloride 50.0 44.5 ug/L 89 76 -129
4-Methyl-2-pentanone (MIBK)250 302 ug/L 121 75 -135
Methyl tert-butyl ether 50.0 47.1 ug/L 94 74 -135
Naphthalene 50.0 50.1 ug/L 100 69 -148
n-Butylbenzene 50.0 46.8 ug/L 94 78 -124
N-Propylbenzene 50.0 47.3 ug/L 95 80 -120
sec-Butylbenzene 50.0 49.2 ug/L 98 76 -125
Styrene 50.0 50.0 ug/L 100 80 -122
tert-Butylbenzene 50.0 48.6 ug/L 97 80 -120
1,1,1,2-Tetrachloroethane 50.0 51.7 ug/L 103 80 -120
1,1,2,2-Tetrachloroethane 50.0 46.4 ug/L 93 72 -128
Tetrachloroethene 50.0 50.0 ug/L 100 77 -123
Toluene 50.0 46.1 ug/L 92 80 -122
trans-1,2-Dichloroethene 50.0 46.7 ug/L 93 78 -123
trans-1,3-Dichloropropene 50.0 50.6 ug/L 101 74 -140
1,2,3-Trichlorobenzene 50.0 50.8 ug/L 102 61 -151
1,2,4-Trichlorobenzene 50.0 50.7 ug/L 101 77 -131
1,1,1-Trichloroethane 50.0 50.3 ug/L 101 74 -128
1,1,2-Trichloroethane 50.0 46.9 ug/L 94 79 -125
Trichloroethene 50.0 47.9 ug/L 96 80 -123
Trichlorofluoromethane 50.0 48.0 ug/L 96 58 -145
1,2,3-Trichloropropane 50.0 48.0 ug/L 96 70 -132
1,2,4-Trimethylbenzene 50.0 50.3 ug/L 101 80 -124
1,3,5-Trimethylbenzene 50.0 49.3 ug/L 99 80 -120
Vinyl chloride 50.0 56.6 ug/L 113 68 -132
Toluene-d8 (Surr)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
1011,2-Dichloroethane-d4 (Surr)70 -130
101Dibromofluoromethane (Surr)70 -130
884-Bromofluorobenzene (Surr)70 -130
TestAmerica Savannah
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QC Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-434853/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434853
Acetone 250 249 ug/L 100 60 -154 1 40
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 43.6 ug/L 87 73 -131 1 30
Bromobenzene 50.0 49.4 ug/L 99 79 -124 1 20
Bromoform 50.0 53.2 ug/L 106 69 -135 3 20
Bromomethane 50.0 69.0 ug/L 138 20 -180 10 40
2-Butanone (MEK)250 242 ug/L 97 75 -133 3 30
Carbon tetrachloride 50.0 49.2 ug/L 98 75 -130 0 20
Chlorobenzene 50.0 47.8 ug/L 96 80 -120 2 20
Chlorobromomethane 50.0 50.3 ug/L 101 77 -122 2 20
Chlorodibromomethane 50.0 53.5 ug/L 107 71 -136 2 20
Chloroethane 50.0 52.3 ug/L 105 50 -151 6 30
Chloroform 50.0 44.8 ug/L 90 79 -122 1 20
Chloromethane 50.0 42.3 ug/L 85 63 -126 4 30
2-Chlorotoluene 50.0 47.8 ug/L 96 77 -121 1 20
4-Chlorotoluene 50.0 48.6 ug/L 97 80 -120 2 20
cis-1,2-Dichloroethene 50.0 49.4 ug/L 99 80 -122 2 20
cis-1,3-Dichloropropene 50.0 45.7 ug/L 91 80 -133 3 20
1,2-Dibromo-3-Chloropropane 50.0 51.0 ug/L 102 59 -141 6 30
1,2-Dichlorobenzene 50.0 47.7 ug/L 95 80 -120 4 20
1,3-Dichlorobenzene 50.0 46.1 ug/L 92 80 -120 2 20
1,4-Dichlorobenzene 50.0 45.1 ug/L 90 80 -120 1 20
Dichlorobromomethane 50.0 48.8 ug/L 98 77 -129 0 20
Dichlorodifluoromethane 50.0 48.1 ug/L 96 51 -140 5 40
1,1-Dichloroethane 50.0 46.2 ug/L 92 80 -120 2 20
1,2-Dichloroethane 50.0 49.4 ug/L 99 75 -130 1 20
1,1-Dichloroethene 50.0 46.0 ug/L 92 74 -125 1 20
1,2-Dichloropropane 50.0 45.8 ug/L 92 80 -123 2 20
1,3-Dichloropropane 50.0 46.8 ug/L 94 78 -127 0 20
2,2-Dichloropropane 50.0 49.6 ug/L 99 72 -133 4 20
1,1-Dichloropropene 50.0 45.7 ug/L 91 78 -127 2 20
Ethylbenzene 50.0 47.4 ug/L 95 80 -120 1 20
Ethylene Dibromide 50.0 49.1 ug/L 98 77 -131 3 30
Hexachlorobutadiene 50.0 52.9 ug/L 106 77 -129 3 30
Isopropylbenzene 50.0 49.1 ug/L 98 80 -120 0 20
4-Isopropyltoluene 50.0 47.3 ug/L 95 80 -120 0 20
Methylene Chloride 50.0 43.7 ug/L 87 76 -129 2 20
4-Methyl-2-pentanone (MIBK)250 307 ug/L 123 75 -135 2 30
Methyl tert-butyl ether 50.0 48.3 ug/L 97 74 -135 3 20
Naphthalene 50.0 52.0 ug/L 104 69 -148 4 40
n-Butylbenzene 50.0 47.3 ug/L 95 78 -124 1 20
N-Propylbenzene 50.0 47.6 ug/L 95 80 -120 1 20
sec-Butylbenzene 50.0 49.2 ug/L 98 76 -125 0 30
Styrene 50.0 50.4 ug/L 101 80 -122 1 20
tert-Butylbenzene 50.0 48.9 ug/L 98 80 -120 1 20
1,1,1,2-Tetrachloroethane 50.0 52.2 ug/L 104 80 -120 1 20
1,1,2,2-Tetrachloroethane 50.0 47.5 ug/L 95 72 -128 2 20
Tetrachloroethene 50.0 49.1 ug/L 98 77 -123 2 20
Toluene 50.0 46.5 ug/L 93 80 -122 1 20
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QC Sample Results
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-434853/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 434853
trans-1,2-Dichloroethene 50.0 45.7 ug/L 91 78 -123 2 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
trans-1,3-Dichloropropene 50.0 50.6 ug/L 101 74 -140 0 20
1,2,3-Trichlorobenzene 50.0 52.7 ug/L 105 61 -151 4 40
1,2,4-Trichlorobenzene 50.0 51.9 ug/L 104 77 -131 2 20
1,1,1-Trichloroethane 50.0 49.9 ug/L 100 74 -128 1 20
1,1,2-Trichloroethane 50.0 47.1 ug/L 94 79 -125 0 20
Trichloroethene 50.0 48.2 ug/L 96 80 -123 1 20
Trichlorofluoromethane 50.0 47.0 ug/L 94 58 -145 2 30
1,2,3-Trichloropropane 50.0 49.8 ug/L 100 70 -132 4 30
1,2,4-Trimethylbenzene 50.0 50.7 ug/L 101 80 -124 1 20
1,3,5-Trimethylbenzene 50.0 50.0 ug/L 100 80 -120 1 20
Vinyl chloride 50.0 44.8 ug/L 90 68 -132 23 30
Toluene-d8 (Surr)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
1011,2-Dichloroethane-d4 (Surr)70 -130
101Dibromofluoromethane (Surr)70 -130
894-Bromofluorobenzene (Surr)70 -130
TestAmerica Savannah
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QC Association Summary
TestAmerica Job ID: 680-125257-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
GC/MS VOA
Analysis Batch: 434853
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-125257-1 SLMW-12AR-5-16 Total/NA
Water 8260B680-125257-2 Trip Blank Total/NA
Water 8260B680-125257-3 SLMW-12BR-5-16 Total/NA
Water 8260BLCS 680-434853/4 Lab Control Sample Total/NA
Water 8260BLCSD 680-434853/5 Lab Control Sample Dup Total/NA
Water 8260BMB 680-434853/9 Method Blank Total/NA
TestAmerica Savannah
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Lab Chronicle
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125257-1
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: SLMW-12AR-5-16 Lab Sample ID: 680-125257-1
Matrix: WaterDate Collected: 05/12/16 13:45
Date Received: 05/13/16 09:13
Analysis 8260B 05/25/16 20:51 CEJ1 434853 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: Trip Blank Lab Sample ID: 680-125257-2
Matrix: WaterDate Collected: 05/12/16 12:00
Date Received: 05/13/16 09:13
Analysis 8260B 05/25/16 19:47 CEJ1 434853 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SLMW-12BR-5-16 Lab Sample ID: 680-125257-3
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/13/16 09:13
Analysis 8260B 05/25/16 21:12 CEJ1 434853 TAL SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: U.S. Army Corps of Engineers Job Number: 680-125257-1
Login Number: 125257
Question Answer Comment
Creator: Banda, Christy S
List Source: TestAmerica Savannah
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Savannah
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Certification Summary
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125257-1
Project/Site: Ft.Bragg - Longstreet Landfill
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA 399.01DoD ELAP 02-28-17
North Carolina (DW)State Program 4 13701 07-31-16 *
TestAmerica Savannah
* Certification renewal pending - certification considered valid.
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-125287-1
Client Project/Site: Ft.Bragg - Longstreet Landfill
For:
U.S. Army Corps of Engineers
100 W. Oglethorpe Ave.
Savannah, Georgia 31401
Attn: John P. Markov
Authorized for release by:
5/31/2016 12:39:11 PM
Robert Bearden, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
TestAmerica Job ID: 680-125287-1
Page 2 of 70 TestAmerica Savannah5/31/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .70
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125287-1
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-125287-1
Laboratory: TestAmerica Savannah
Narrative
Client: U.S. Army Corps of Engineers
Project: Ft.Bragg - Longstreet Landfill
Report Number: 680-125287-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 05/14/2016; the samples arrived in good condition, properly preserved and on ice. The temperatures of
the 5 coolers at receipt time were 1.1º C, 1.7º C, 1.9º C, 2.3º C and 2.3º C.
SEMIVOLATILE ORGANIC COMPOUNDS (AQUEOUS)
Samples SLMW-12BR-5-16 (680-125287-1), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for Semivolatile Organic Compounds (Aqueous) in accordance with EPA SW-846 Method
8270D. The samples were prepared on 05/17/2016 and 05/18/2016 and analyzed on 05/21/2016 and 05/24/2016.
The laboratory control sample and the laboratory control sample duplicate (LCS/LCSD) for preparation batch 680-433686 and analytical
batch 680-434291 recovered outside control limits for the following analyte: 3,3'-Dichlorobenzidine. 3,3'-Dichlorobenzidine has been
identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed.
Several analytes failed the recovery criteria low for the MS/MSD of sample SLMW-12BR-5-16 (680-125287-1) in batch 680-434682.
2-Chlorophenol exceeded the RPD limit.
Several analytes failed the recovery criteria low for the MS of sample SW-2-5-16 (680-125287-3), 3,3'-Dichlorobenzidine failed the recovery
criteria low for the MSD, and 3,3'-Dichlorobenzidine and 4-Chloroaniline exceeded the RPD limit in batch 680-434291.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PESTICIDES AND PCBS
Samples SLMW-12BR-5-16 (680-125287-1), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for Pesticides and PCBs in accordance with EPA SW-846 Method 8081B_8082A. The
samples were prepared on 05/17/2016 and analyzed on 05/19/2016.
Surrogate recovery for the following sample was outside control limits: SLMW-8R-5-16 (680-125287-5). Re-extraction and/or re-analysis
was performed with concurring results. The original analysis has been reported
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ORGANOPHOSPHORUS PESTICIDES
Samples SLMW-12BR-5-16 (680-125287-1), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for organophosphorus pesticides in accordance with EPA SW-846 Method 8141B. The
samples were prepared on 05/18/2016 and analyzed on 05/23/2016 and 05/24/2016.
The Tributyl phosphate surrogate recovery for the following samples was outside acceptance limits (low biased) on the confirmation
column: (MB 180-176662/1-A). The recovery is within acceptance limits on the other column, indicating that the extraction process was in
control.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch
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Case Narrative
Client: U.S. Army Corps of Engineers TestAmerica Job ID: 680-125287-1
Project/Site: Ft.Bragg - Longstreet Landfill
Job ID: 680-125287-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
180-176662.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHLORINATED HERBICIDES
Samples SLMW-12BR-5-16 (680-125287-1), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for chlorinated herbicides in accordance with EPA SW-846 Method 8151A. The samples
were prepared on 05/19/2016 and analyzed on 05/20/2016 and 05/21/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
METALS (ICPMS)
Samples SLMW-12BR-5-16 (680-125287-2), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for Metals (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were
prepared on 05/15/2016 and analyzed on 05/20/2016 and 05/22/2016.
Selenium was detected in method blank MB 680-433402/1-A at a level that was above the method detection limit but below the reporting
limit. The value should be considered an estimate, and has been flagged.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS BY ION CHROMATOGRAPHY (48 HOUR)
Samples SLMW-12BR-5-16 (680-125287-2), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for Anions by Ion Chromatography (48 Hour) in accordance with EPA Method 300.0. The
samples were analyzed on 05/14/2016 and 05/16/2016.
The following sample was analyzed outside of analytical holding time due to instrument error: SLMW-7R-5-16 (680-125287-6).
The following samples: SLMW-12BR-5-16 (680-125287-2), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16
(680-125287-5), (680-125287-E-2 MS) and (680-125287-E-2 MSD) were analyzed in hold, but due to instrument error the capping CCV did
not run. The samples were re-analyzed outside of holding time in batch 680-433503 and the results confirmed. Only the original analysis
is reported.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL CYANIDE
Samples SLMW-12BR-5-16 (680-125287-2), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for total cyanide in accordance with EPA SW-846 Method 9012B. The samples were
prepared on 05/17/2016 and 05/19/2016 and analyzed on 05/18/2016 and 05/19/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SULFIDE
Samples SLMW-12BR-5-16 (680-125287-2), SW-2-5-16 (680-125287-3), SW-1-5-16 (680-125287-4), SLMW-8R-5-16 (680-125287-5) and
SLMW-7R-5-16 (680-125287-6) were analyzed for sulfide in accordance with EPA SW-846 Method 9034. The samples were prepared and
analyzed on 05/18/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Sample Summary
TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-125287-1 SLMW-12BR-5-16 Water 05/12/16 15:25 05/14/16 09:55
680-125287-2 SLMW-12BR-5-16 Water 05/13/16 09:10 05/14/16 09:55
680-125287-3 SW-2-5-16 Water 05/13/16 10:15 05/14/16 09:55
680-125287-4 SW-1-5-16 Water 05/13/16 11:00 05/14/16 09:55
680-125287-5 SLMW-8R-5-16 Water 05/13/16 13:50 05/14/16 09:55
680-125287-6 SLMW-7R-5-16 Water 05/13/16 16:50 05/14/16 09:55
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Method Summary
TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Method Method Description LaboratoryProtocol
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL SAV
SW8468081B/8082A Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography TAL SAV
SW8468141BOrganophosphorous Compounds by Gas Chromatography, Capillary Column Technique TAL PIT
SW8468151AHerbicides (GC)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
SW8466020AMetals (ICP/MS)TAL SAV
SW8469012BCyanide, Total andor Amenable TAL SAV
SW8469034Sulfide, Acid Soluble and Insoluble (Titrimetric)TAL SAV
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
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Definitions/Glossary
TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Qualifiers
GC/MS Semi VOA
Qualifier Description
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
Qualifier
U Undetected at the Limit of Detection.
Q One or more quality control criteria failed.
J Estimated: The analyte was positively identified; the quantitation is an estimation
GC Semi VOA
Qualifier Description
M Manual integrated compound.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
U Undetected at the Limit of Detection.
J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
HPLC/IC
Qualifier Description
Q One or more quality control criteria failed.
Qualifier
U Undetected at the Limit of Detection.
J Estimated: The analyte was positively identified; the quantitation is an estimation
H Sample was prepped or analyzed beyond the specified holding time
Metals
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
General Chemistry
Qualifier Description
U Undetected at the Limit of Detection.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
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Definitions/Glossary
TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Glossary (Continued)
These commonly used abbreviations may or may not be present in this report.
TEQ Toxicity Equivalent Quotient (Dioxin)
Abbreviation
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Detection Summary
TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: SLMW-12BR-5-16 Lab Sample ID: 680-125287-1
Benzyl alcohol
RL
10 ug/L
MDL
1.1
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J2.8 8270D
Client Sample ID: SLMW-12BR-5-16 Lab Sample ID: 680-125287-2
Barium
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1396020A
Beryllium 0.20 ug/L0.070 Total/NA10.39 6020A
Chromium 1.0 ug/L0.16 Total/NA10.44 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA11.1 6020A
Copper 1.0 ug/L0.21 Total/NA10.39 J 6020A
Lead 0.30 ug/L0.080 Total/NA10.49 6020A
Nickel 1.0 ug/L0.40 Total/NA11.6 6020A
Zinc 10 ug/L2.6 Total/NA17.2 J 6020A
Client Sample ID: SW-2-5-16 Lab Sample ID: 680-125287-3
Nitrate as N
RL
0.050 mg/L
MDL
0.023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J Q0.037 300.0
Arsenic 1.0 ug/L0.40 Total/NA10.46 J 6020A
Barium 1.0 ug/L0.15 Total/NA1226020A
Chromium 1.0 ug/L0.16 Total/NA10.21 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.28 6020A
Copper 1.0 ug/L0.21 Total/NA10.25 J 6020A
Lead 0.30 ug/L0.080 Total/NA10.12 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.45 J 6020A
Selenium 0.50 ug/L0.21 Total/NA10.30 J 6020A
Zinc 10 ug/L2.6 Total/NA12.6 J 6020A
Sulfide
RL
10 mg/L
RL
10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1139034
Client Sample ID: SW-1-5-16 Lab Sample ID: 680-125287-4
1,4-Dichlorobenzene
RL
9.5 ug/L
MDL
0.52
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.99 8270D
Diethyl phthalate 9.5 ug/L0.84 Total/NA11.8 J 8270D
2,4-D 0.48 ug/L0.035 Total/NA10.055 J 8151A
Arsenic 1.0 ug/L0.40 Total/NA17.7 6020A
Barium 1.0 ug/L0.15 Total/NA1376020A
Cobalt 0.20 ug/L0.078 Total/NA10.27 6020A
Selenium 0.50 ug/L0.21 Total/NA11.0 6020A
Zinc 10 ug/L2.6 Total/NA13.2 J 6020A
Cyanide, Total 0.010 mg/L0.0025 Total/NA10.0048 J 9012B
Client Sample ID: SLMW-8R-5-16 Lab Sample ID: 680-125287-5
3 & 4 Methylphenol
RL
9.6 ug/L
MDL
1.2
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J3.5 8270D
Arsenic 1.0 ug/L0.40 Total/NA13.4 6020A
Barium 1.0 ug/L0.15 Total/NA1536020A
Chromium 1.0 ug/L0.16 Total/NA10.20 J 6020A
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This Detection Summary does not include radiochemical test results.
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Client Sample ID: SLMW-8R-5-16 (Continued)Lab Sample ID: 680-125287-5
Cobalt
RL
0.20 ug/L
MDL
0.078
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.29 6020A
Copper 1.0 ug/L0.21 Total/NA10.32 J 6020A
Selenium 0.50 ug/L0.21 Total/NA14.6 6020A
Vanadium 5.0 ug/L1.4 Total/NA11.4 J 6020A
Cyanide, Total 0.010 mg/L0.0025 Total/NA10.014 9012B
Client Sample ID: SLMW-7R-5-16 Lab Sample ID: 680-125287-6
3 & 4 Methylphenol
RL
9.5 ug/L
MDL
1.2
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J1.8 8270D
Arsenic 1.0 ug/L0.40 Total/NA12.3 6020A
Barium 1.0 ug/L0.15 Total/NA1386020A
Chromium 1.0 ug/L0.16 Total/NA10.26 J 6020A
Cobalt 0.20 ug/L0.078 Total/NA10.95 6020A
Copper 1.0 ug/L0.21 Total/NA11.9 6020A
Lead 0.30 ug/L0.080 Total/NA10.14 J 6020A
Nickel 1.0 ug/L0.40 Total/NA10.55 J 6020A
Selenium 0.50 ug/L0.21 Total/NA14.1 6020A
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This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-1Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.56 U J 10 0.56 ug/L 05/18/16 16:30 05/24/16 19:31 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10 0.53 ug/L 05/18/16 16:30 05/24/16 19:31 11,2-Dichlorobenzene 0.53 U J
10 0.59 ug/L 05/18/16 16:30 05/24/16 19:31 11,3-Dichlorobenzene 0.59 U J
10 0.54 ug/L 05/18/16 16:30 05/24/16 19:31 11,4-Dichlorobenzene 0.54 U J
10 1.2 ug/L 05/18/16 16:30 05/24/16 19:31 12,4,5-Trichlorophenol 1.2 U
10 0.85 ug/L 05/18/16 16:30 05/24/16 19:31 12,4,6-Trichlorophenol 0.85 U
10 1.1 ug/L 05/18/16 16:30 05/24/16 19:31 12,4-Dichlorophenol 1.1 U J
10 4.0 ug/L 05/18/16 16:30 05/24/16 19:31 12,4-Dimethylphenol 4.0 U
50 10 ug/L 05/18/16 16:30 05/24/16 19:31 12,4-Dinitrophenol 10 U
10 1.2 ug/L 05/18/16 16:30 05/24/16 19:31 12,4-Dinitrotoluene 1.2 U
10 0.87 ug/L 05/18/16 16:30 05/24/16 19:31 12-Chlorophenol 0.87 U J
10 0.80 ug/L 05/18/16 16:30 05/24/16 19:31 12-Chloronaphthalene 0.80 U J
10 0.78 ug/L 05/18/16 16:30 05/24/16 19:31 12-Methylnaphthalene 0.78 U Q
10 0.89 ug/L 05/18/16 16:30 05/24/16 19:31 12-Methylphenol 0.89 U J
50 1.3 ug/L 05/18/16 16:30 05/24/16 19:31 12-Nitroaniline 1.3 U
10 0.76 ug/L 05/18/16 16:30 05/24/16 19:31 12-Nitrophenol 0.76 U J
10 1.3 ug/L 05/18/16 16:30 05/24/16 19:31 13 & 4 Methylphenol 1.3 U
60 30 ug/L 05/18/16 16:30 05/24/16 19:31 13,3'-Dichlorobenzidine 30 U J
50 5.0 ug/L 05/18/16 16:30 05/24/16 19:31 13-Nitroaniline 5.0 U
50 10 ug/L 05/18/16 16:30 05/24/16 19:31 14,6-Dinitro-2-methylphenol 10 U
10 0.77 ug/L 05/18/16 16:30 05/24/16 19:31 14-Bromophenyl phenyl ether 0.77 U
10 1.0 ug/L 05/18/16 16:30 05/24/16 19:31 14-Chloro-3-methylphenol 1.0 U
20 2.2 ug/L 05/18/16 16:30 05/24/16 19:31 14-Chloroaniline 2.2 U J
10 0.84 ug/L 05/18/16 16:30 05/24/16 19:31 14-Chlorophenyl phenyl ether 0.84 U
50 5.0 ug/L 05/18/16 16:30 05/24/16 19:31 14-Nitroaniline 5.0 U
10 0.76 ug/L 05/18/16 16:30 05/24/16 19:31 1Acenaphthene0.76 U
10 0.85 ug/L 05/18/16 16:30 05/24/16 19:31 1Acenaphthylene0.85 U J
10 0.69 ug/L 05/18/16 16:30 05/24/16 19:31 1Anthracene0.69 U
10 0.55 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzo[a]anthracene 0.55 U
10 0.71 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzo[a]pyrene 0.71 U
10 2.6 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzo[b]fluoranthene 2.6 U
10 0.87 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzo[g,h,i]perylene 0.87 U
10 1.2 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzo[k]fluoranthene 1.2 U
10 1.1 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzyl alcohol 2.8 J
10 0.94 ug/L 05/18/16 16:30 05/24/16 19:31 1Bis(2-chloroethoxy)methane 0.94 U
10 1.1 ug/L 05/18/16 16:30 05/24/16 19:31 1Bis(2-chloroethyl)ether 1.1 U
10 1.6 ug/L 05/18/16 16:30 05/24/16 19:31 1Bis(2-ethylhexyl) phthalate 1.6 U
10 0.51 ug/L 05/18/16 16:30 05/24/16 19:31 1Chrysene0.51 U
10 1.0 ug/L 05/18/16 16:30 05/24/16 19:31 1Dibenz(a,h)anthracene 1.0 U
10 0.79 ug/L 05/18/16 16:30 05/24/16 19:31 1Dibenzofuran0.79 U J
10 0.83 ug/L 05/18/16 16:30 05/24/16 19:31 1Di-n-butyl phthalate 0.83 U
10 0.88 ug/L 05/18/16 16:30 05/24/16 19:31 1Diethyl phthalate 0.88 U
10 0.99 ug/L 05/18/16 16:30 05/24/16 19:31 1Dimethyl phthalate 0.99 U
10 1.4 ug/L 05/18/16 16:30 05/24/16 19:31 1Di-n-octyl phthalate 1.4 U
10 0.74 ug/L 05/18/16 16:30 05/24/16 19:31 1Fluoranthene0.74 U
10 0.96 ug/L 05/18/16 16:30 05/24/16 19:31 1Fluorene0.96 U
10 0.79 ug/L 05/18/16 16:30 05/24/16 19:31 1Hexachlorobenzene0.79 U
10 0.62 ug/L 05/18/16 16:30 05/24/16 19:31 1Hexachlorobutadiene0.62 U J
10 0.76 ug/L 05/18/16 16:30 05/24/16 19:31 1Hexachloroethane0.76 U J
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-1Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Indeno[1,2,3-cd]pyrene 1.0 U 10 1.0 ug/L 05/18/16 16:30 05/24/16 19:31 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10 0.90 ug/L 05/18/16 16:30 05/24/16 19:31 1Isophorone0.90 U
10 0.70 ug/L 05/18/16 16:30 05/24/16 19:31 1Naphthalene0.70 U J
10 0.73 ug/L 05/18/16 16:30 05/24/16 19:31 1Nitrobenzene0.73 U Q
10 0.92 ug/L 05/18/16 16:30 05/24/16 19:31 1N-Nitrosodiphenylamine 0.92 U
10 0.72 ug/L 05/18/16 16:30 05/24/16 19:31 1N-Nitrosodi-n-propylamine 0.72 U
50 2.0 ug/L 05/18/16 16:30 05/24/16 19:31 1Pentachlorophenol2.0 U
10 0.77 ug/L 05/18/16 16:30 05/24/16 19:31 1Phenanthrene0.77 U
10 0.83 ug/L 05/18/16 16:30 05/24/16 19:31 1Phenol0.83 U J
10 0.63 ug/L 05/18/16 16:30 05/24/16 19:31 1Pyrene0.63 U
10 1.2 ug/L 05/18/16 16:30 05/24/16 19:31 1Butyl benzyl phthalate 1.2 U
10 0.78 ug/L 05/18/16 16:30 05/24/16 19:31 1bis(chloroisopropyl) ether 0.78 U
50 5.0 ug/L 05/18/16 16:30 05/24/16 19:31 1Benzoic acid 5.0 U
10 1.1 ug/L 05/18/16 16:30 05/24/16 19:31 12,6-Dinitrotoluene 1.1 U
50 1.9 ug/L 05/18/16 16:30 05/24/16 19:31 14-Nitrophenol 1.9 U
2,4,6-Tribromophenol 68 39-124 05/18/16 16:30 05/24/16 19:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 53 05/18/16 16:30 05/24/16 19:31 132-113
2-Fluorophenol 54 05/18/16 16:30 05/24/16 19:31 126-109
Terphenyl-d14 62 05/18/16 16:30 05/24/16 19:31 110-126
Phenol-d5 54 05/18/16 16:30 05/24/16 19:31 127-110
Nitrobenzene-d5 60 05/18/16 16:30 05/24/16 19:31 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 05/17/16 16:25 05/19/16 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.048 0.0072 ug/L 05/17/16 16:25 05/19/16 18:34 1delta-BHC 0.0072 U
0.048 0.0036 ug/L 05/17/16 16:25 05/19/16 18:34 1Dieldrin0.0036 U
0.048 0.0033 ug/L 05/17/16 16:25 05/19/16 18:34 1Endosulfan I 0.0033 U
0.048 0.0040 ug/L 05/17/16 16:25 05/19/16 18:34 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 18:34 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 05/17/16 16:25 05/19/16 18:34 1Endrin0.0051 U
0.048 0.0058 ug/L 05/17/16 16:25 05/19/16 18:34 1Endrin aldehyde 0.0058 U
0.048 0.0044 ug/L 05/17/16 16:25 05/19/16 18:34 1Endrin ketone 0.0044 U
0.048 0.0034 ug/L 05/17/16 16:25 05/19/16 18:34 1gamma-BHC (Lindane)0.0034 U
0.048 0.0068 ug/L 05/17/16 16:25 05/19/16 18:34 1Heptachlor0.0068 U
0.048 0.0035 ug/L 05/17/16 16:25 05/19/16 18:34 1Heptachlor epoxide 0.0035 U
0.048 0.0094 ug/L 05/17/16 16:25 05/19/16 18:34 1Methoxychlor0.0094 U
0.96 0.17 ug/L 05/17/16 16:25 05/19/16 18:34 1PCB-1016 0.17 U
0.048 0.0060 ug/L 05/17/16 16:25 05/19/16 18:34 14,4'-DDD 0.0060 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 18:34 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 05/17/16 16:25 05/19/16 18:34 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 05/17/16 16:25 05/19/16 18:34 1Aldrin0.0069 U
0.048 0.0033 ug/L 05/17/16 16:25 05/19/16 18:34 1alpha-BHC 0.0033 U
0.048 0.0087 ug/L 05/17/16 16:25 05/19/16 18:34 1beta-BHC 0.0087 U
0.48 0.091 ug/L 05/17/16 16:25 05/19/16 18:34 1Chlordane (technical)0.091 U
0.96 0.18 ug/L 05/17/16 16:25 05/19/16 18:34 1PCB-1221 0.18 U
0.96 0.24 ug/L 05/17/16 16:25 05/19/16 18:34 1PCB-1232 0.24 U
0.96 0.18 ug/L 05/17/16 16:25 05/19/16 18:34 1PCB-1242 0.18 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-1Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/14/16 09:55
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued)
RL MDL
PCB-1248 0.20 U 0.96 0.20 ug/L 05/17/16 16:25 05/19/16 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.96 0.11 ug/L 05/17/16 16:25 05/19/16 18:34 1PCB-1254 0.11 U
0.96 0.11 ug/L 05/17/16 16:25 05/19/16 18:34 1PCB-1260 0.11 U
Tetrachloro-m-xylene 60 40-130 05/17/16 16:25 05/19/16 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 31 05/17/16 16:25 05/19/16 18:34 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.17 U 0.95 0.17 ug/L 05/18/16 12:45 05/23/16 23:50 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.95 0.063 ug/L 05/18/16 12:45 05/23/16 23:50 1Bolstar0.063 U
0.95 0.069 ug/L 05/18/16 12:45 05/23/16 23:50 1Chlorpyrifos0.069 U
0.95 0.18 ug/L 05/18/16 12:45 05/23/16 23:50 1Coumaphos0.18 U
1.9 0.10 ug/L 05/18/16 12:45 05/23/16 23:50 1Demeton, Total 0.10 U
0.95 0.071 ug/L 05/18/16 12:45 05/23/16 23:50 1Diazinon0.071 U
0.95 0.095 ug/L 05/18/16 12:45 05/23/16 23:50 1Dichlorvos0.095 U
0.95 0.18 ug/L 05/18/16 12:45 05/23/16 23:50 1Dimethoate0.18 U
0.95 0.088 ug/L 05/18/16 12:45 05/23/16 23:50 1Disulfoton0.088 U
0.95 0.13 ug/L 05/18/16 12:45 05/23/16 23:50 1EPN0.13 U
0.95 0.11 ug/L 05/18/16 12:45 05/23/16 23:50 1Mocap0.11 U
0.95 0.11 ug/L 05/18/16 12:45 05/23/16 23:50 1Famphur0.11 U
0.95 0.092 ug/L 05/18/16 12:45 05/23/16 23:50 1Fensulfothion0.092 U
0.95 0.075 ug/L 05/18/16 12:45 05/23/16 23:50 1Fenthion0.075 U
0.95 0.080 ug/L 05/18/16 12:45 05/23/16 23:50 1Malathion0.080 U
0.95 0.10 ug/L 05/18/16 12:45 05/23/16 23:50 1Parathion0.10 U
0.95 0.11 ug/L 05/18/16 12:45 05/23/16 23:50 1Methyl parathion 0.11 U
0.95 0.15 ug/L 05/18/16 12:45 05/23/16 23:50 1Mevinphos0.15 U
0.95 0.074 ug/L 05/18/16 12:45 05/23/16 23:50 1Phorate0.074 U
0.95 0.10 ug/L 05/18/16 12:45 05/23/16 23:50 1Ronnel0.10 U
0.95 0.13 ug/L 05/18/16 12:45 05/23/16 23:50 1Stirophos0.13 U
0.95 0.067 ug/L 05/18/16 12:45 05/23/16 23:50 1Sulfotepp0.067 U
0.95 0.082 ug/L 05/18/16 12:45 05/23/16 23:50 1Thionazin0.082 U
0.95 0.069 ug/L 05/18/16 12:45 05/23/16 23:50 1Tokuthion0.069 U
0.95 0.068 ug/L 05/18/16 12:45 05/23/16 23:50 1Trichloronate0.068 U
0.95 0.091 ug/L 05/18/16 12:45 05/23/16 23:50 1O,O,O-Triethyl phosphorothioate 0.091 U
Tributyl phosphate 72 49-122 05/18/16 12:45 05/23/16 23:50 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 52 05/18/16 12:45 05/23/16 23:50 149-122
Triphenylphosphate 88 05/18/16 12:45 05/23/16 23:50 145-145
Triphenylphosphate 97 05/18/16 12:45 05/23/16 23:50 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.035 U 0.48 0.035 ug/L 05/19/16 08:53 05/20/16 22:52 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/20/16 22:52 12,4-DB 0.14 U
0.24 0.059 ug/L 05/19/16 08:53 05/20/16 22:52 12,4,5-T 0.059 U
0.24 0.059 ug/L 05/19/16 08:53 05/20/16 22:52 1Silvex (2,4,5-TP)0.059 U
4.8 0.095 ug/L 05/19/16 08:53 05/20/16 22:52 1Dalapon0.095 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-1Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/12/16 15:25
Date Received: 05/14/16 09:55
Method: 8151A - Herbicides (GC) (Continued)
RL MDL
Dicamba 0.081 U 0.48 0.081 ug/L 05/19/16 08:53 05/20/16 22:52 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/20/16 22:52 1Dichlorprop0.14 U
0.95 0.15 ug/L 05/19/16 08:53 05/20/16 22:52 1Dinoseb0.15 U
110 16 ug/L 05/19/16 08:53 05/20/16 22:52 1MCPA16 U
110 18 ug/L 05/19/16 08:53 05/20/16 22:52 1Mecoprop18 U
0.24 0.035 ug/L 05/19/16 08:53 05/20/16 22:52 1Pentachlorophenol0.035 U
DCAA 74 45-130 05/19/16 08:53 05/20/16 22:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 680-125287-2Client Sample ID: SLMW-12BR-5-16
Matrix: WaterDate Collected: 05/13/16 09:10
Date Received: 05/14/16 09:55
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.023 U Q 0.050 0.023 mg/L 05/14/16 17:22 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/15/16 10:00 05/20/16 22:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:10 1Arsenic0.40 U
1.0 0.15 ug/L 05/15/16 10:00 05/20/16 22:10 1Barium39
0.20 0.070 ug/L 05/15/16 10:00 05/20/16 22:10 1Beryllium0.39
0.50 0.20 ug/L 05/15/16 10:00 05/20/16 22:10 1Cadmium0.20 U
1.0 0.16 ug/L 05/15/16 10:00 05/20/16 22:10 1Chromium0.44 J
0.20 0.078 ug/L 05/15/16 10:00 05/20/16 22:10 1Cobalt1.1
1.0 0.21 ug/L 05/15/16 10:00 05/20/16 22:10 1Copper0.39 J
0.30 0.080 ug/L 05/15/16 10:00 05/20/16 22:10 1Lead0.49
0.20 0.080 ug/L 05/15/16 10:00 05/20/16 22:10 1Mercury0.080 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:10 1Nickel1.6
0.50 0.21 ug/L 05/15/16 10:00 05/22/16 05:23 1Selenium0.21 U
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 22:10 1Silver0.10 U
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 22:10 1Thallium0.10 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:10 1Tin0.40 U
5.0 1.4 ug/L 05/15/16 10:00 05/20/16 22:10 1Vanadium1.4 U
10 2.6 ug/L 05/15/16 10:00 05/20/16 22:10 1Zinc7.2 J
General Chemistry
RL MDL
Cyanide, Total 0.0025 U 0.010 0.0025 mg/L 05/19/16 06:22 05/19/16 11:33 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
RL RL
Sulfide 10 U 10 10 mg/L 05/18/16 06:45 05/18/16 08:24 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-3Client Sample ID: SW-2-5-16
Matrix: WaterDate Collected: 05/13/16 10:15
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.56 U J 10 0.56 ug/L 05/17/16 16:25 05/21/16 02:03 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10 0.53 ug/L 05/17/16 16:25 05/21/16 02:03 11,2-Dichlorobenzene 0.53 U J
10 0.59 ug/L 05/17/16 16:25 05/21/16 02:03 11,3-Dichlorobenzene 0.59 U J
10 0.54 ug/L 05/17/16 16:25 05/21/16 02:03 11,4-Dichlorobenzene 0.54 U J
10 1.2 ug/L 05/17/16 16:25 05/21/16 02:03 12,4,5-Trichlorophenol 1.2 U J
10 0.85 ug/L 05/17/16 16:25 05/21/16 02:03 12,4,6-Trichlorophenol 0.85 U
10 1.1 ug/L 05/17/16 16:25 05/21/16 02:03 12,4-Dichlorophenol 1.1 U J
10 4.0 ug/L 05/17/16 16:25 05/21/16 02:03 12,4-Dimethylphenol 4.0 U
50 10 ug/L 05/17/16 16:25 05/21/16 02:03 12,4-Dinitrophenol 10 U
10 1.2 ug/L 05/17/16 16:25 05/21/16 02:03 12,4-Dinitrotoluene 1.2 U
10 0.87 ug/L 05/17/16 16:25 05/21/16 02:03 12-Chlorophenol 0.87 U
10 0.80 ug/L 05/17/16 16:25 05/21/16 02:03 12-Chloronaphthalene 0.80 U J
10 0.78 ug/L 05/17/16 16:25 05/21/16 02:03 12-Methylnaphthalene 0.78 U
10 0.89 ug/L 05/17/16 16:25 05/21/16 02:03 12-Methylphenol 0.89 U
50 1.3 ug/L 05/17/16 16:25 05/21/16 02:03 12-Nitroaniline 1.3 U
10 0.76 ug/L 05/17/16 16:25 05/21/16 02:03 12-Nitrophenol 0.76 U J
10 1.3 ug/L 05/17/16 16:25 05/21/16 02:03 13 & 4 Methylphenol 1.3 U
60 30 ug/L 05/17/16 16:25 05/21/16 02:03 13,3'-Dichlorobenzidine 30 U J Q
50 5.0 ug/L 05/17/16 16:25 05/21/16 02:03 13-Nitroaniline 5.0 U J
50 10 ug/L 05/17/16 16:25 05/21/16 02:03 14,6-Dinitro-2-methylphenol 10 U
10 0.77 ug/L 05/17/16 16:25 05/21/16 02:03 14-Bromophenyl phenyl ether 0.77 U
10 1.0 ug/L 05/17/16 16:25 05/21/16 02:03 14-Chloro-3-methylphenol 1.0 U
20 2.2 ug/L 05/17/16 16:25 05/21/16 02:03 14-Chloroaniline 2.2 U J
10 0.84 ug/L 05/17/16 16:25 05/21/16 02:03 14-Chlorophenyl phenyl ether 0.84 U J
50 5.0 ug/L 05/17/16 16:25 05/21/16 02:03 14-Nitroaniline 5.0 U
10 0.76 ug/L 05/17/16 16:25 05/21/16 02:03 1Acenaphthene0.76 U J
10 0.85 ug/L 05/17/16 16:25 05/21/16 02:03 1Acenaphthylene0.85 U J
10 0.69 ug/L 05/17/16 16:25 05/21/16 02:03 1Anthracene0.69 U
10 0.55 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzo[a]anthracene 0.55 U
10 0.71 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzo[a]pyrene 0.71 U
10 2.6 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzo[b]fluoranthene 2.6 U
10 0.87 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzo[g,h,i]perylene 0.87 U
10 1.2 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzo[k]fluoranthene 1.2 U
10 1.1 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzyl alcohol 1.1 U
10 0.94 ug/L 05/17/16 16:25 05/21/16 02:03 1Bis(2-chloroethoxy)methane 0.94 U J
10 1.1 ug/L 05/17/16 16:25 05/21/16 02:03 1Bis(2-chloroethyl)ether 1.1 U
10 1.6 ug/L 05/17/16 16:25 05/21/16 02:03 1Bis(2-ethylhexyl) phthalate 1.6 U
10 0.51 ug/L 05/17/16 16:25 05/21/16 02:03 1Chrysene0.51 U
10 1.0 ug/L 05/17/16 16:25 05/21/16 02:03 1Dibenz(a,h)anthracene 1.0 U
10 0.79 ug/L 05/17/16 16:25 05/21/16 02:03 1Dibenzofuran0.79 U J
10 0.83 ug/L 05/17/16 16:25 05/21/16 02:03 1Di-n-butyl phthalate 0.83 U
10 0.88 ug/L 05/17/16 16:25 05/21/16 02:03 1Diethyl phthalate 0.88 U
10 0.99 ug/L 05/17/16 16:25 05/21/16 02:03 1Dimethyl phthalate 0.99 U
10 1.4 ug/L 05/17/16 16:25 05/21/16 02:03 1Di-n-octyl phthalate 1.4 U
10 0.74 ug/L 05/17/16 16:25 05/21/16 02:03 1Fluoranthene0.74 U
10 0.96 ug/L 05/17/16 16:25 05/21/16 02:03 1Fluorene0.96 U J
10 0.79 ug/L 05/17/16 16:25 05/21/16 02:03 1Hexachlorobenzene0.79 U
10 0.62 ug/L 05/17/16 16:25 05/21/16 02:03 1Hexachlorobutadiene0.62 U J
10 0.76 ug/L 05/17/16 16:25 05/21/16 02:03 1Hexachloroethane0.76 U J
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-3Client Sample ID: SW-2-5-16
Matrix: WaterDate Collected: 05/13/16 10:15
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Indeno[1,2,3-cd]pyrene 1.0 U 10 1.0 ug/L 05/17/16 16:25 05/21/16 02:03 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10 0.90 ug/L 05/17/16 16:25 05/21/16 02:03 1Isophorone0.90 U J
10 0.70 ug/L 05/17/16 16:25 05/21/16 02:03 1Naphthalene0.70 U J
10 0.73 ug/L 05/17/16 16:25 05/21/16 02:03 1Nitrobenzene0.73 U
10 0.92 ug/L 05/17/16 16:25 05/21/16 02:03 1N-Nitrosodiphenylamine 0.92 U J
10 0.72 ug/L 05/17/16 16:25 05/21/16 02:03 1N-Nitrosodi-n-propylamine 0.72 U
50 2.0 ug/L 05/17/16 16:25 05/21/16 02:03 1Pentachlorophenol2.0 U
10 0.77 ug/L 05/17/16 16:25 05/21/16 02:03 1Phenanthrene0.77 U
10 0.83 ug/L 05/17/16 16:25 05/21/16 02:03 1Phenol0.83 U
10 0.63 ug/L 05/17/16 16:25 05/21/16 02:03 1Pyrene0.63 U
10 1.2 ug/L 05/17/16 16:25 05/21/16 02:03 1Butyl benzyl phthalate 1.2 U
10 0.78 ug/L 05/17/16 16:25 05/21/16 02:03 1bis(chloroisopropyl) ether 0.78 U
50 5.0 ug/L 05/17/16 16:25 05/21/16 02:03 1Benzoic acid 5.0 U
10 1.1 ug/L 05/17/16 16:25 05/21/16 02:03 12,6-Dinitrotoluene 1.1 U J
50 1.9 ug/L 05/17/16 16:25 05/21/16 02:03 14-Nitrophenol 1.9 U
2,4,6-Tribromophenol 71 39-124 05/17/16 16:25 05/21/16 02:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 54 05/17/16 16:25 05/21/16 02:03 132-113
2-Fluorophenol 51 05/17/16 16:25 05/21/16 02:03 126-109
Terphenyl-d14 57 05/17/16 16:25 05/21/16 02:03 110-126
Phenol-d5 49 05/17/16 16:25 05/21/16 02:03 127-110
Nitrobenzene-d5 58 05/17/16 16:25 05/21/16 02:03 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 05/17/16 16:25 05/19/16 18:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.048 0.0072 ug/L 05/17/16 16:25 05/19/16 18:49 1delta-BHC 0.0072 U
0.048 0.0036 ug/L 05/17/16 16:25 05/19/16 18:49 1Dieldrin0.0036 U
0.048 0.0033 ug/L 05/17/16 16:25 05/19/16 18:49 1Endosulfan I 0.0033 U
0.048 0.0040 ug/L 05/17/16 16:25 05/19/16 18:49 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 18:49 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 05/17/16 16:25 05/19/16 18:49 1Endrin0.0051 U
0.048 0.0058 ug/L 05/17/16 16:25 05/19/16 18:49 1Endrin aldehyde 0.0058 U
0.048 0.0044 ug/L 05/17/16 16:25 05/19/16 18:49 1Endrin ketone 0.0044 U
0.048 0.0034 ug/L 05/17/16 16:25 05/19/16 18:49 1gamma-BHC (Lindane)0.0034 U
0.048 0.0068 ug/L 05/17/16 16:25 05/19/16 18:49 1Heptachlor0.0068 U
0.048 0.0035 ug/L 05/17/16 16:25 05/19/16 18:49 1Heptachlor epoxide 0.0035 U
0.048 0.0094 ug/L 05/17/16 16:25 05/19/16 18:49 1Methoxychlor0.0094 U
0.96 0.17 ug/L 05/17/16 16:25 05/19/16 18:49 1PCB-1016 0.17 U
0.048 0.0060 ug/L 05/17/16 16:25 05/19/16 18:49 14,4'-DDD 0.0060 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 18:49 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 05/17/16 16:25 05/19/16 18:49 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 05/17/16 16:25 05/19/16 18:49 1Aldrin0.0069 U
0.048 0.0033 ug/L 05/17/16 16:25 05/19/16 18:49 1alpha-BHC 0.0033 U
0.048 0.0087 ug/L 05/17/16 16:25 05/19/16 18:49 1beta-BHC 0.0087 U
0.48 0.091 ug/L 05/17/16 16:25 05/19/16 18:49 1Chlordane (technical)0.091 U
0.96 0.18 ug/L 05/17/16 16:25 05/19/16 18:49 1PCB-1221 0.18 U
0.96 0.24 ug/L 05/17/16 16:25 05/19/16 18:49 1PCB-1232 0.24 U
0.96 0.18 ug/L 05/17/16 16:25 05/19/16 18:49 1PCB-1242 0.18 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-3Client Sample ID: SW-2-5-16
Matrix: WaterDate Collected: 05/13/16 10:15
Date Received: 05/14/16 09:55
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued)
RL MDL
PCB-1248 0.20 U 0.96 0.20 ug/L 05/17/16 16:25 05/19/16 18:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.96 0.11 ug/L 05/17/16 16:25 05/19/16 18:49 1PCB-1254 0.11 U
0.96 0.11 ug/L 05/17/16 16:25 05/19/16 18:49 1PCB-1260 0.11 U
Tetrachloro-m-xylene 61 40-130 05/17/16 16:25 05/19/16 18:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 24 05/17/16 16:25 05/19/16 18:49 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.17 U 0.94 0.17 ug/L 05/18/16 12:45 05/24/16 00:24 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.94 0.062 ug/L 05/18/16 12:45 05/24/16 00:24 1Bolstar0.062 U
0.94 0.068 ug/L 05/18/16 12:45 05/24/16 00:24 1Chlorpyrifos0.068 U
0.94 0.18 ug/L 05/18/16 12:45 05/24/16 00:24 1Coumaphos0.18 U
1.9 0.099 ug/L 05/18/16 12:45 05/24/16 00:24 1Demeton, Total 0.099 U
0.94 0.071 ug/L 05/18/16 12:45 05/24/16 00:24 1Diazinon0.071 U
0.94 0.094 ug/L 05/18/16 12:45 05/24/16 00:24 1Dichlorvos0.094 U
0.94 0.17 ug/L 05/18/16 12:45 05/24/16 00:24 1Dimethoate0.17 U
0.94 0.087 ug/L 05/18/16 12:45 05/24/16 00:24 1Disulfoton0.087 U
0.94 0.13 ug/L 05/18/16 12:45 05/24/16 00:24 1EPN0.13 U
0.94 0.11 ug/L 05/18/16 12:45 05/24/16 00:24 1Mocap0.11 U
0.94 0.10 ug/L 05/18/16 12:45 05/24/16 00:24 1Famphur0.10 U
0.94 0.092 ug/L 05/18/16 12:45 05/24/16 00:24 1Fensulfothion0.092 U
0.94 0.074 ug/L 05/18/16 12:45 05/24/16 00:24 1Fenthion0.074 U
0.94 0.080 ug/L 05/18/16 12:45 05/24/16 00:24 1Malathion0.080 U
0.94 0.10 ug/L 05/18/16 12:45 05/24/16 00:24 1Parathion0.10 U
0.94 0.11 ug/L 05/18/16 12:45 05/24/16 00:24 1Methyl parathion 0.11 U
0.94 0.15 ug/L 05/18/16 12:45 05/24/16 00:24 1Mevinphos0.15 U
0.94 0.073 ug/L 05/18/16 12:45 05/24/16 00:24 1Phorate0.073 U
0.94 0.10 ug/L 05/18/16 12:45 05/24/16 00:24 1Ronnel0.10 U
0.94 0.13 ug/L 05/18/16 12:45 05/24/16 00:24 1Stirophos0.13 U
0.94 0.067 ug/L 05/18/16 12:45 05/24/16 00:24 1Sulfotepp0.067 U
0.94 0.081 ug/L 05/18/16 12:45 05/24/16 00:24 1Thionazin0.081 U
0.94 0.068 ug/L 05/18/16 12:45 05/24/16 00:24 1Tokuthion0.068 U
0.94 0.067 ug/L 05/18/16 12:45 05/24/16 00:24 1Trichloronate0.067 U
0.94 0.090 ug/L 05/18/16 12:45 05/24/16 00:24 1O,O,O-Triethyl phosphorothioate 0.090 U
Tributyl phosphate 78 49-122 05/18/16 12:45 05/24/16 00:24 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 59 05/18/16 12:45 05/24/16 00:24 149-122
Triphenylphosphate 88 05/18/16 12:45 05/24/16 00:24 145-145
Triphenylphosphate 98 05/18/16 12:45 05/24/16 00:24 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.035 U 0.48 0.035 ug/L 05/19/16 08:53 05/20/16 23:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/20/16 23:12 12,4-DB 0.14 U
0.24 0.059 ug/L 05/19/16 08:53 05/20/16 23:12 12,4,5-T 0.059 U
0.24 0.059 ug/L 05/19/16 08:53 05/20/16 23:12 1Silvex (2,4,5-TP)0.059 U
4.8 0.096 ug/L 05/19/16 08:53 05/20/16 23:12 1Dalapon0.096 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-3Client Sample ID: SW-2-5-16
Matrix: WaterDate Collected: 05/13/16 10:15
Date Received: 05/14/16 09:55
Method: 8151A - Herbicides (GC) (Continued)
RL MDL
Dicamba 0.081 U 0.48 0.081 ug/L 05/19/16 08:53 05/20/16 23:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/20/16 23:12 1Dichlorprop0.14 U
0.96 0.15 ug/L 05/19/16 08:53 05/20/16 23:12 1Dinoseb0.15 U
110 16 ug/L 05/19/16 08:53 05/20/16 23:12 1MCPA16 U
110 18 ug/L 05/19/16 08:53 05/20/16 23:12 1Mecoprop18 U
0.24 0.035 ug/L 05/19/16 08:53 05/20/16 23:12 1Pentachlorophenol0.035 U
DCAA 75 45-130 05/19/16 08:53 05/20/16 23:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.037 J Q 0.050 0.023 mg/L 05/14/16 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/15/16 10:00 05/20/16 22:15 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:15 1Arsenic0.46 J
1.0 0.15 ug/L 05/15/16 10:00 05/20/16 22:15 1Barium22
0.20 0.070 ug/L 05/15/16 10:00 05/20/16 22:15 1Beryllium0.070 U
0.50 0.20 ug/L 05/15/16 10:00 05/20/16 22:15 1Cadmium0.20 U
1.0 0.16 ug/L 05/15/16 10:00 05/20/16 22:15 1Chromium0.21 J
0.20 0.078 ug/L 05/15/16 10:00 05/20/16 22:15 1Cobalt0.28
1.0 0.21 ug/L 05/15/16 10:00 05/20/16 22:15 1Copper0.25 J
0.30 0.080 ug/L 05/15/16 10:00 05/20/16 22:15 1Lead0.12 J
0.20 0.080 ug/L 05/15/16 10:00 05/20/16 22:15 1Mercury0.080 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:15 1Nickel0.45 J
0.50 0.21 ug/L 05/15/16 10:00 05/22/16 05:28 1Selenium0.30 J
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 22:15 1Silver0.10 U
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 22:15 1Thallium0.10 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:15 1Tin0.40 U
5.0 1.4 ug/L 05/15/16 10:00 05/20/16 22:15 1Vanadium1.4 U
10 2.6 ug/L 05/15/16 10:00 05/20/16 22:15 1Zinc2.6 J
General Chemistry
RL MDL
Cyanide, Total 0.0025 U 0.010 0.0025 mg/L 05/17/16 08:30 05/18/16 05:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
RL RL
Sulfide 13 10 10 mg/L 05/18/16 06:45 05/18/16 08:24 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Lab Sample ID: 680-125287-4Client Sample ID: SW-1-5-16
Matrix: WaterDate Collected: 05/13/16 11:00
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.53 U 9.5 0.53 ug/L 05/17/16 16:25 05/21/16 02:23 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
9.5 0.51 ug/L 05/17/16 16:25 05/21/16 02:23 11,2-Dichlorobenzene 0.51 U
9.5 0.56 ug/L 05/17/16 16:25 05/21/16 02:23 11,3-Dichlorobenzene 0.56 U
9.5 0.52 ug/L 05/17/16 16:25 05/21/16 02:23 11,4-Dichlorobenzene 0.99 J
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-4Client Sample ID: SW-1-5-16
Matrix: WaterDate Collected: 05/13/16 11:00
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2,4,5-Trichlorophenol 1.1 U 9.5 1.1 ug/L 05/17/16 16:25 05/21/16 02:23 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
9.5 0.81 ug/L 05/17/16 16:25 05/21/16 02:23 12,4,6-Trichlorophenol 0.81 U
9.5 1.0 ug/L 05/17/16 16:25 05/21/16 02:23 12,4-Dichlorophenol 1.0 U
9.5 3.8 ug/L 05/17/16 16:25 05/21/16 02:23 12,4-Dimethylphenol 3.8 U
48 9.5 ug/L 05/17/16 16:25 05/21/16 02:23 12,4-Dinitrophenol 9.5 U
9.5 1.1 ug/L 05/17/16 16:25 05/21/16 02:23 12,4-Dinitrotoluene 1.1 U
9.5 0.83 ug/L 05/17/16 16:25 05/21/16 02:23 12-Chlorophenol 0.83 U
9.5 0.76 ug/L 05/17/16 16:25 05/21/16 02:23 12-Chloronaphthalene 0.76 U
9.5 0.74 ug/L 05/17/16 16:25 05/21/16 02:23 12-Methylnaphthalene 0.74 U
9.5 0.85 ug/L 05/17/16 16:25 05/21/16 02:23 12-Methylphenol 0.85 U
48 1.2 ug/L 05/17/16 16:25 05/21/16 02:23 12-Nitroaniline 1.2 U
9.5 0.72 ug/L 05/17/16 16:25 05/21/16 02:23 12-Nitrophenol 0.72 U
9.5 1.2 ug/L 05/17/16 16:25 05/21/16 02:23 13 & 4 Methylphenol 1.2 U
57 29 ug/L 05/17/16 16:25 05/21/16 02:23 13,3'-Dichlorobenzidine 29 U Q
48 4.8 ug/L 05/17/16 16:25 05/21/16 02:23 13-Nitroaniline 4.8 U
48 9.5 ug/L 05/17/16 16:25 05/21/16 02:23 14,6-Dinitro-2-methylphenol 9.5 U
9.5 0.73 ug/L 05/17/16 16:25 05/21/16 02:23 14-Bromophenyl phenyl ether 0.73 U
9.5 0.95 ug/L 05/17/16 16:25 05/21/16 02:23 14-Chloro-3-methylphenol 0.95 U
19 2.1 ug/L 05/17/16 16:25 05/21/16 02:23 14-Chloroaniline 2.1 U
9.5 0.80 ug/L 05/17/16 16:25 05/21/16 02:23 14-Chlorophenyl phenyl ether 0.80 U
48 4.8 ug/L 05/17/16 16:25 05/21/16 02:23 14-Nitroaniline 4.8 U
9.5 0.72 ug/L 05/17/16 16:25 05/21/16 02:23 1Acenaphthene0.72 U
9.5 0.81 ug/L 05/17/16 16:25 05/21/16 02:23 1Acenaphthylene0.81 U
9.5 0.66 ug/L 05/17/16 16:25 05/21/16 02:23 1Anthracene0.66 U
9.5 0.52 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzo[a]anthracene 0.52 U
9.5 0.68 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzo[a]pyrene 0.68 U
9.5 2.5 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzo[b]fluoranthene 2.5 U
9.5 0.83 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzo[g,h,i]perylene 0.83 U
9.5 1.1 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzo[k]fluoranthene 1.1 U
9.5 1.0 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzyl alcohol 1.0 U
9.5 0.90 ug/L 05/17/16 16:25 05/21/16 02:23 1Bis(2-chloroethoxy)methane 0.90 U
9.5 1.0 ug/L 05/17/16 16:25 05/21/16 02:23 1Bis(2-chloroethyl)ether 1.0 U
9.5 1.5 ug/L 05/17/16 16:25 05/21/16 02:23 1Bis(2-ethylhexyl) phthalate 1.5 U
9.5 0.49 ug/L 05/17/16 16:25 05/21/16 02:23 1Chrysene0.49 U
9.5 0.95 ug/L 05/17/16 16:25 05/21/16 02:23 1Dibenz(a,h)anthracene 0.95 U
9.5 0.75 ug/L 05/17/16 16:25 05/21/16 02:23 1Dibenzofuran0.75 U
9.5 0.79 ug/L 05/17/16 16:25 05/21/16 02:23 1Di-n-butyl phthalate 0.79 U
9.5 0.84 ug/L 05/17/16 16:25 05/21/16 02:23 1Diethyl phthalate 1.8 J
9.5 0.94 ug/L 05/17/16 16:25 05/21/16 02:23 1Dimethyl phthalate 0.94 U
9.5 1.3 ug/L 05/17/16 16:25 05/21/16 02:23 1Di-n-octyl phthalate 1.3 U
9.5 0.71 ug/L 05/17/16 16:25 05/21/16 02:23 1Fluoranthene0.71 U
9.5 0.92 ug/L 05/17/16 16:25 05/21/16 02:23 1Fluorene0.92 U
9.5 0.75 ug/L 05/17/16 16:25 05/21/16 02:23 1Hexachlorobenzene0.75 U
9.5 0.59 ug/L 05/17/16 16:25 05/21/16 02:23 1Hexachlorobutadiene0.59 U
9.5 0.72 ug/L 05/17/16 16:25 05/21/16 02:23 1Hexachloroethane0.72 U
9.5 0.95 ug/L 05/17/16 16:25 05/21/16 02:23 1Indeno[1,2,3-cd]pyrene 0.95 U
9.5 0.86 ug/L 05/17/16 16:25 05/21/16 02:23 1Isophorone0.86 U
9.5 0.67 ug/L 05/17/16 16:25 05/21/16 02:23 1Naphthalene0.67 U
9.5 0.70 ug/L 05/17/16 16:25 05/21/16 02:23 1Nitrobenzene0.70 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-4Client Sample ID: SW-1-5-16
Matrix: WaterDate Collected: 05/13/16 11:00
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
N-Nitrosodiphenylamine 0.88 U 9.5 0.88 ug/L 05/17/16 16:25 05/21/16 02:23 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
9.5 0.69 ug/L 05/17/16 16:25 05/21/16 02:23 1N-Nitrosodi-n-propylamine 0.69 U
48 1.9 ug/L 05/17/16 16:25 05/21/16 02:23 1Pentachlorophenol1.9 U
9.5 0.73 ug/L 05/17/16 16:25 05/21/16 02:23 1Phenanthrene0.73 U
9.5 0.79 ug/L 05/17/16 16:25 05/21/16 02:23 1Phenol0.79 U
9.5 0.60 ug/L 05/17/16 16:25 05/21/16 02:23 1Pyrene0.60 U
9.5 1.1 ug/L 05/17/16 16:25 05/21/16 02:23 1Butyl benzyl phthalate 1.1 U
9.5 0.74 ug/L 05/17/16 16:25 05/21/16 02:23 1bis(chloroisopropyl) ether 0.74 U
48 4.8 ug/L 05/17/16 16:25 05/21/16 02:23 1Benzoic acid 4.8 U
9.5 1.0 ug/L 05/17/16 16:25 05/21/16 02:23 12,6-Dinitrotoluene 1.0 U
48 1.8 ug/L 05/17/16 16:25 05/21/16 02:23 14-Nitrophenol 1.8 U
2,4,6-Tribromophenol 80 39-124 05/17/16 16:25 05/21/16 02:23 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 54 05/17/16 16:25 05/21/16 02:23 132-113
2-Fluorophenol 60 05/17/16 16:25 05/21/16 02:23 126-109
Terphenyl-d14 38 05/17/16 16:25 05/21/16 02:23 110-126
Phenol-d5 57 05/17/16 16:25 05/21/16 02:23 127-110
Nitrobenzene-d5 66 05/17/16 16:25 05/21/16 02:23 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 05/17/16 16:25 05/19/16 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.048 0.0072 ug/L 05/17/16 16:25 05/19/16 19:03 1delta-BHC 0.0072 U
0.048 0.0037 ug/L 05/17/16 16:25 05/19/16 19:03 1Dieldrin0.0037 U
0.048 0.0034 ug/L 05/17/16 16:25 05/19/16 19:03 1Endosulfan I 0.0034 U
0.048 0.0040 ug/L 05/17/16 16:25 05/19/16 19:03 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 19:03 1Endosulfan sulfate 0.0049 U
0.048 0.0051 ug/L 05/17/16 16:25 05/19/16 19:03 1Endrin0.0051 U
0.048 0.0059 ug/L 05/17/16 16:25 05/19/16 19:03 1Endrin aldehyde 0.0059 U
0.048 0.0044 ug/L 05/17/16 16:25 05/19/16 19:03 1Endrin ketone 0.0044 U
0.048 0.0035 ug/L 05/17/16 16:25 05/19/16 19:03 1gamma-BHC (Lindane)0.0035 U
0.048 0.0068 ug/L 05/17/16 16:25 05/19/16 19:03 1Heptachlor0.0068 U
0.048 0.0036 ug/L 05/17/16 16:25 05/19/16 19:03 1Heptachlor epoxide 0.0036 U
0.048 0.0094 ug/L 05/17/16 16:25 05/19/16 19:03 1Methoxychlor0.0094 U
0.96 0.17 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1016 0.17 U
0.048 0.0061 ug/L 05/17/16 16:25 05/19/16 19:03 14,4'-DDD 0.0061 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 19:03 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 05/17/16 16:25 05/19/16 19:03 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 05/17/16 16:25 05/19/16 19:03 1Aldrin0.0069 U
0.048 0.0033 ug/L 05/17/16 16:25 05/19/16 19:03 1alpha-BHC 0.0033 U
0.048 0.0087 ug/L 05/17/16 16:25 05/19/16 19:03 1beta-BHC 0.0087 U
0.48 0.091 ug/L 05/17/16 16:25 05/19/16 19:03 1Chlordane (technical)0.091 U
0.96 0.18 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1221 0.18 U
0.96 0.24 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1232 0.24 U
0.96 0.18 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1242 0.18 U
0.96 0.20 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1248 0.20 U
0.96 0.11 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1254 0.11 U
0.96 0.12 ug/L 05/17/16 16:25 05/19/16 19:03 1PCB-1260 0.12 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-4Client Sample ID: SW-1-5-16
Matrix: WaterDate Collected: 05/13/16 11:00
Date Received: 05/14/16 09:55
Tetrachloro-m-xylene 70 40-130 05/17/16 16:25 05/19/16 19:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 16 05/17/16 16:25 05/19/16 19:03 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.17 U 0.94 0.17 ug/L 05/18/16 12:45 05/24/16 00:57 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.94 0.062 ug/L 05/18/16 12:45 05/24/16 00:57 1Bolstar0.062 U
0.94 0.068 ug/L 05/18/16 12:45 05/24/16 00:57 1Chlorpyrifos0.068 U
0.94 0.18 ug/L 05/18/16 12:45 05/24/16 00:57 1Coumaphos0.18 U
1.9 0.099 ug/L 05/18/16 12:45 05/24/16 00:57 1Demeton, Total 0.099 U
0.94 0.071 ug/L 05/18/16 12:45 05/24/16 00:57 1Diazinon0.071 U
0.94 0.094 ug/L 05/18/16 12:45 05/24/16 00:57 1Dichlorvos0.094 U
0.94 0.17 ug/L 05/18/16 12:45 05/24/16 00:57 1Dimethoate0.17 U
0.94 0.087 ug/L 05/18/16 12:45 05/24/16 00:57 1Disulfoton0.087 U
0.94 0.13 ug/L 05/18/16 12:45 05/24/16 00:57 1EPN0.13 U
0.94 0.11 ug/L 05/18/16 12:45 05/24/16 00:57 1Mocap0.11 U
0.94 0.10 ug/L 05/18/16 12:45 05/24/16 00:57 1Famphur0.10 U
0.94 0.092 ug/L 05/18/16 12:45 05/24/16 00:57 1Fensulfothion0.092 U
0.94 0.074 ug/L 05/18/16 12:45 05/24/16 00:57 1Fenthion0.074 U
0.94 0.080 ug/L 05/18/16 12:45 05/24/16 00:57 1Malathion0.080 U
0.94 0.10 ug/L 05/18/16 12:45 05/24/16 00:57 1Parathion0.10 U
0.94 0.11 ug/L 05/18/16 12:45 05/24/16 00:57 1Methyl parathion 0.11 U
0.94 0.15 ug/L 05/18/16 12:45 05/24/16 00:57 1Mevinphos0.15 U
0.94 0.073 ug/L 05/18/16 12:45 05/24/16 00:57 1Phorate0.073 U
0.94 0.10 ug/L 05/18/16 12:45 05/24/16 00:57 1Ronnel0.10 U
0.94 0.13 ug/L 05/18/16 12:45 05/24/16 00:57 1Stirophos0.13 U
0.94 0.067 ug/L 05/18/16 12:45 05/24/16 00:57 1Sulfotepp0.067 U
0.94 0.081 ug/L 05/18/16 12:45 05/24/16 00:57 1Thionazin0.081 U
0.94 0.068 ug/L 05/18/16 12:45 05/24/16 00:57 1Tokuthion0.068 U
0.94 0.067 ug/L 05/18/16 12:45 05/24/16 00:57 1Trichloronate0.067 U
0.94 0.090 ug/L 05/18/16 12:45 05/24/16 00:57 1O,O,O-Triethyl phosphorothioate 0.090 U
Tributyl phosphate 108 49-122 05/18/16 12:45 05/24/16 00:57 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tributyl phosphate 90 05/18/16 12:45 05/24/16 00:57 149-122
Triphenylphosphate 107 05/18/16 12:45 05/24/16 00:57 145-145
Triphenylphosphate 119 05/18/16 12:45 05/24/16 00:57 145-145
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D 0.055 J 0.48 0.035 ug/L 05/19/16 08:53 05/20/16 23:32 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.48 0.14 ug/L 05/19/16 08:53 05/20/16 23:32 12,4-DB 0.14 U
0.24 0.059 ug/L 05/19/16 08:53 05/20/16 23:32 12,4,5-T 0.059 U
0.24 0.059 ug/L 05/19/16 08:53 05/20/16 23:32 1Silvex (2,4,5-TP)0.059 U
4.8 0.095 ug/L 05/19/16 08:53 05/20/16 23:32 1Dalapon0.095 U
0.48 0.081 ug/L 05/19/16 08:53 05/20/16 23:32 1Dicamba0.081 U
0.48 0.14 ug/L 05/19/16 08:53 05/20/16 23:32 1Dichlorprop0.14 U
0.95 0.15 ug/L 05/19/16 08:53 05/20/16 23:32 1Dinoseb0.15 U
110 16 ug/L 05/19/16 08:53 05/20/16 23:32 1MCPA16 U
110 18 ug/L 05/19/16 08:53 05/20/16 23:32 1Mecoprop18 U
0.24 0.035 ug/L 05/19/16 08:53 05/20/16 23:32 1Pentachlorophenol0.035 U
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
DCAA 84 45-130 05/19/16 08:53 05/20/16 23:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Nitrate as N 0.023 U Q 0.050 0.023 mg/L 05/14/16 18:28 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony 0.99 U 2.0 0.99 ug/L 05/15/16 10:00 05/20/16 22:21 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:21 1Arsenic7.7
1.0 0.15 ug/L 05/15/16 10:00 05/20/16 22:21 1Barium37
0.20 0.070 ug/L 05/15/16 10:00 05/20/16 22:21 1Beryllium0.070 U
0.50 0.20 ug/L 05/15/16 10:00 05/20/16 22:21 1Cadmium0.20 U
1.0 0.16 ug/L 05/15/16 10:00 05/20/16 22:21 1Chromium0.16 U
0.20 0.078 ug/L 05/15/16 10:00 05/20/16 22:21 1Cobalt0.27
1.0 0.21 ug/L 05/15/16 10:00 05/20/16 22:21 1Copper0.21 U
0.30 0.080 ug/L 05/15/16 10:00 05/20/16 22:21 1Lead0.080 U
0.20 0.080 ug/L 05/15/16 10:00 05/20/16 22:21 1Mercury0.080 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:21 1Nickel0.40 U
0.50 0.21 ug/L 05/15/16 10:00 05/22/16 05:33 1Selenium1.0
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 22:21 1Silver0.10 U
0.20 0.10 ug/L 05/15/16 10:00 05/20/16 22:21 1Thallium0.10 U
1.0 0.40 ug/L 05/15/16 10:00 05/20/16 22:21 1Tin0.40 U
5.0 1.4 ug/L 05/15/16 10:00 05/20/16 22:21 1Vanadium1.4 U
10 2.6 ug/L 05/15/16 10:00 05/20/16 22:21 1Zinc3.2 J
General Chemistry
RL MDL
Cyanide, Total 0.0048 J 0.010 0.0025 mg/L 05/17/16 08:30 05/18/16 05:09 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
RL RL
Sulfide 10 U 10 10 mg/L 05/18/16 06:45 05/18/16 08:24 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Lab Sample ID: 680-125287-5Client Sample ID: SLMW-8R-5-16
Matrix: WaterDate Collected: 05/13/16 13:50
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,2,4-Trichlorobenzene 0.54 U 9.6 0.54 ug/L 05/17/16 16:25 05/21/16 02:43 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
9.6 0.51 ug/L 05/17/16 16:25 05/21/16 02:43 11,2-Dichlorobenzene 0.51 U
9.6 0.57 ug/L 05/17/16 16:25 05/21/16 02:43 11,3-Dichlorobenzene 0.57 U
9.6 0.52 ug/L 05/17/16 16:25 05/21/16 02:43 11,4-Dichlorobenzene 0.52 U
9.6 1.2 ug/L 05/17/16 16:25 05/21/16 02:43 12,4,5-Trichlorophenol 1.2 U
9.6 0.81 ug/L 05/17/16 16:25 05/21/16 02:43 12,4,6-Trichlorophenol 0.81 U
9.6 1.1 ug/L 05/17/16 16:25 05/21/16 02:43 12,4-Dichlorophenol 1.1 U
9.6 3.8 ug/L 05/17/16 16:25 05/21/16 02:43 12,4-Dimethylphenol 3.8 U
48 9.6 ug/L 05/17/16 16:25 05/21/16 02:43 12,4-Dinitrophenol 9.6 U
9.6 1.2 ug/L 05/17/16 16:25 05/21/16 02:43 12,4-Dinitrotoluene 1.2 U
9.6 0.83 ug/L 05/17/16 16:25 05/21/16 02:43 12-Chlorophenol 0.83 U
9.6 0.77 ug/L 05/17/16 16:25 05/21/16 02:43 12-Chloronaphthalene 0.77 U
9.6 0.75 ug/L 05/17/16 16:25 05/21/16 02:43 12-Methylnaphthalene 0.75 U
9.6 0.85 ug/L 05/17/16 16:25 05/21/16 02:43 12-Methylphenol 0.85 U
48 1.2 ug/L 05/17/16 16:25 05/21/16 02:43 12-Nitroaniline 1.2 U
9.6 0.73 ug/L 05/17/16 16:25 05/21/16 02:43 12-Nitrophenol 0.73 U
9.6 1.2 ug/L 05/17/16 16:25 05/21/16 02:43 13 & 4 Methylphenol 3.5 J
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-5Client Sample ID: SLMW-8R-5-16
Matrix: WaterDate Collected: 05/13/16 13:50
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine 29 U Q 58 29 ug/L 05/17/16 16:25 05/21/16 02:43 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
48 4.8 ug/L 05/17/16 16:25 05/21/16 02:43 13-Nitroaniline 4.8 U
48 9.6 ug/L 05/17/16 16:25 05/21/16 02:43 14,6-Dinitro-2-methylphenol 9.6 U
9.6 0.74 ug/L 05/17/16 16:25 05/21/16 02:43 14-Bromophenyl phenyl ether 0.74 U
9.6 0.96 ug/L 05/17/16 16:25 05/21/16 02:43 14-Chloro-3-methylphenol 0.96 U
19 2.1 ug/L 05/17/16 16:25 05/21/16 02:43 14-Chloroaniline 2.1 U
9.6 0.81 ug/L 05/17/16 16:25 05/21/16 02:43 14-Chlorophenyl phenyl ether 0.81 U
48 4.8 ug/L 05/17/16 16:25 05/21/16 02:43 14-Nitroaniline 4.8 U
9.6 0.73 ug/L 05/17/16 16:25 05/21/16 02:43 1Acenaphthene0.73 U
9.6 0.81 ug/L 05/17/16 16:25 05/21/16 02:43 1Acenaphthylene0.81 U
9.6 0.66 ug/L 05/17/16 16:25 05/21/16 02:43 1Anthracene0.66 U
9.6 0.53 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzo[a]anthracene 0.53 U
9.6 0.68 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzo[a]pyrene 0.68 U
9.6 2.5 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzo[b]fluoranthene 2.5 U
9.6 0.83 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzo[g,h,i]perylene 0.83 U
9.6 1.2 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzo[k]fluoranthene 1.2 U
9.6 1.1 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzyl alcohol 1.1 U
9.6 0.90 ug/L 05/17/16 16:25 05/21/16 02:43 1Bis(2-chloroethoxy)methane 0.90 U
9.6 1.1 ug/L 05/17/16 16:25 05/21/16 02:43 1Bis(2-chloroethyl)ether 1.1 U
9.6 1.5 ug/L 05/17/16 16:25 05/21/16 02:43 1Bis(2-ethylhexyl) phthalate 1.5 U
9.6 0.49 ug/L 05/17/16 16:25 05/21/16 02:43 1Chrysene0.49 U
9.6 0.96 ug/L 05/17/16 16:25 05/21/16 02:43 1Dibenz(a,h)anthracene 0.96 U
9.6 0.76 ug/L 05/17/16 16:25 05/21/16 02:43 1Dibenzofuran0.76 U
9.6 0.80 ug/L 05/17/16 16:25 05/21/16 02:43 1Di-n-butyl phthalate 0.80 U
9.6 0.84 ug/L 05/17/16 16:25 05/21/16 02:43 1Diethyl phthalate 0.84 U
9.6 0.95 ug/L 05/17/16 16:25 05/21/16 02:43 1Dimethyl phthalate 0.95 U
9.6 1.3 ug/L 05/17/16 16:25 05/21/16 02:43 1Di-n-octyl phthalate 1.3 U
9.6 0.71 ug/L 05/17/16 16:25 05/21/16 02:43 1Fluoranthene0.71 U
9.6 0.92 ug/L 05/17/16 16:25 05/21/16 02:43 1Fluorene0.92 U
9.6 0.76 ug/L 05/17/16 16:25 05/21/16 02:43 1Hexachlorobenzene0.76 U
9.6 0.59 ug/L 05/17/16 16:25 05/21/16 02:43 1Hexachlorobutadiene0.59 U
9.6 0.73 ug/L 05/17/16 16:25 05/21/16 02:43 1Hexachloroethane0.73 U
9.6 0.96 ug/L 05/17/16 16:25 05/21/16 02:43 1Indeno[1,2,3-cd]pyrene 0.96 U
9.6 0.86 ug/L 05/17/16 16:25 05/21/16 02:43 1Isophorone0.86 U
9.6 0.67 ug/L 05/17/16 16:25 05/21/16 02:43 1Naphthalene0.67 U
9.6 0.70 ug/L 05/17/16 16:25 05/21/16 02:43 1Nitrobenzene0.70 U
9.6 0.88 ug/L 05/17/16 16:25 05/21/16 02:43 1N-Nitrosodiphenylamine 0.88 U
9.6 0.69 ug/L 05/17/16 16:25 05/21/16 02:43 1N-Nitrosodi-n-propylamine 0.69 U
48 1.9 ug/L 05/17/16 16:25 05/21/16 02:43 1Pentachlorophenol1.9 U
9.6 0.74 ug/L 05/17/16 16:25 05/21/16 02:43 1Phenanthrene0.74 U
9.6 0.80 ug/L 05/17/16 16:25 05/21/16 02:43 1Phenol0.80 U
9.6 0.60 ug/L 05/17/16 16:25 05/21/16 02:43 1Pyrene0.60 U
9.6 1.2 ug/L 05/17/16 16:25 05/21/16 02:43 1Butyl benzyl phthalate 1.2 U
9.6 0.75 ug/L 05/17/16 16:25 05/21/16 02:43 1bis(chloroisopropyl) ether 0.75 U
48 4.8 ug/L 05/17/16 16:25 05/21/16 02:43 1Benzoic acid 4.8 U
9.6 1.1 ug/L 05/17/16 16:25 05/21/16 02:43 12,6-Dinitrotoluene 1.1 U
48 1.8 ug/L 05/17/16 16:25 05/21/16 02:43 14-Nitrophenol 1.8 U
2,4,6-Tribromophenol 74 39-124 05/17/16 16:25 05/21/16 02:43 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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TestAmerica Job ID: 680-125287-1Client: U.S. Army Corps of Engineers
Project/Site: Ft.Bragg - Longstreet Landfill
Lab Sample ID: 680-125287-5Client Sample ID: SLMW-8R-5-16
Matrix: WaterDate Collected: 05/13/16 13:50
Date Received: 05/14/16 09:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2-Fluorobiphenyl 50 32-113 05/17/16 16:25 05/21/16 02:43 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol 48 05/17/16 16:25 05/21/16 02:43 126-109
Terphenyl-d14 56 05/17/16 16:25 05/21/16 02:43 110-126
Phenol-d5 49 05/17/16 16:25 05/21/16 02:43 127-110
Nitrobenzene-d5 52 05/17/16 16:25 05/21/16 02:43 132-118
Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography
RL MDL
Toxaphene 0.38 U 4.8 0.38 ug/L 05/17/16 16:25 05/19/16 19:18 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.048 0.0071 ug/L 05/17/16 16:25 05/19/16 19:18 1delta-BHC 0.0071 U
0.048 0.0036 ug/L 05/17/16 16:25 05/19/16 19:18 1Dieldrin0.0036 U
0.048 0.0033 ug/L 05/17/16 16:25 05/19/16 19:18 1Endosulfan I 0.0033 U
0.048 0.0040 ug/L 05/17/16 16:25 05/19/16 19:18 1Endosulfan II 0.0040 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 19:18 1Endosulfan sulfate 0.0049 U
0.048 0.0050 ug/L 05/17/16 16:25 05/19/16 19:18 1Endrin0.0050 U
0.048 0.0058 ug/L 05/17/16 16:25 05/19/16 19:18 1Endrin aldehyde 0.0058 U
0.048 0.0044 ug/L 05/17/16 16:25 05/19/16 19:18 1Endrin ketone 0.0044 U
0.048 0.0034 ug/L 05/17/16 16:25 05/19/16 19:18 1gamma-BHC (Lindane)0.0034 U
0.048 0.0068 ug/L 05/17/16 16:25 05/19/16 19:18 1Heptachlor0.0068 U
0.048 0.0035 ug/L 05/17/16 16:25 05/19/16 19:18 1Heptachlor epoxide 0.0035 U
0.048 0.0093 ug/L 05/17/16 16:25 05/19/16 19:18 1Methoxychlor0.0093 U
0.95 0.17 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1016 0.17 U
0.048 0.0060 ug/L 05/17/16 16:25 05/19/16 19:18 14,4'-DDD 0.0060 U
0.048 0.0049 ug/L 05/17/16 16:25 05/19/16 19:18 14,4'-DDE 0.0049 U
0.048 0.0067 ug/L 05/17/16 16:25 05/19/16 19:18 14,4'-DDT 0.0067 U
0.048 0.0069 ug/L 05/17/16 16:25 05/19/16 19:18 1Aldrin0.0069 U
0.048 0.0032 ug/L 05/17/16 16:25 05/19/16 19:18 1alpha-BHC 0.0032 U
0.048 0.0087 ug/L 05/17/16 16:25 05/19/16 19:18 1beta-BHC 0.0087 U
0.48 0.090 ug/L 05/17/16 16:25 05/19/16 19:18 1Chlordane (technical)0.090 U
0.95 0.18 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1221 0.18 U
0.95 0.24 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1232 0.24 U
0.95 0.18 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1242 0.18 U
0.95 0.20 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1248 0.20 U
0.95 0.10 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1254 0.10 U
0.95 0.11 ug/L 05/17/16 16:25 05/19/16 19:18 1PCB-1260 0.11 U
Tetrachloro-m-xylene 68 40-130 05/17/16 16:25 05/19/16 19:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 11 J 05/17/16 16:25 05/19/16 19:18 114-130
Method: 8141B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique
RL MDL
Azinphos-methyl 0.17 U 0.94 0.17 ug/L 05/18/16 12:45 05/24/16 01:30 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.94 0.062 ug/L 05/18/16 12:45 05/24/16 01:30 1Bolstar0.062 U
0.94 0.068 ug/L 05/18/16 12:45 05/24/16 01:30 1Chlorpyrifos0.068 U
0.94 0.18 ug/L 05/18/16 12:45 05/24/16 01:30 1Coumaphos0.18 U
1.9 0.099 ug/L 05/18/16 12:45 05/24/16 01:30 1Demeton, Total 0.099 U
0.94 0.071 ug/L 05/18/16 12:45 05/24/16 01:30 1Diazinon0.071 U
0.94 0.094 ug/L 05/18/16 12:45 05/24/16 01:30 1Dichlorvos0.094 U
0.94 0.17 ug/L 05/18/16 12:45 05/24/16 01:30 1Dimethoate0.17 U
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