9702_WilkesCounty_2ndSemi2016MonitorReport_DIN27208_20152610

2211 W. Meadowview Road, Suite 101
Greensboro, NC 27407
tel: [phone]
fax: [phone]
www.JoyceEngineering.com

February 23, 2016

Mr. Ervin Lane
Compliance Hydrogeologist
Division of Waste Management/Solid Waste Section
1646 Mail Service Center
Raleigh, NC 27699-1646

RE: Second Semiannual Water Quality Monitoring Reports of 2015
Wilkes County Landfills: Dan Johnson Landfill, Permit No. 97-02
JOYCE Project No. 356.1601.12, Task No. 02

Dear Ervin:

On behalf of Wilkes County, Joyce Engineering is submitting the Second Semiannual Water
Quality Monitoring Report of 2015 for the Wilkes County Dan Johnson Landfill, Permit No. 97-02.
The attached report contains electronic versions of the complete report and all appendices for the
October 2015 sampling event. Also attached is the North Carolina Environmental Monitoring
Reporting Form for the October 2015 monitoring event.

If you wish to have a hard copy of the report, drawings, or appendices, we will be happy to provide
it upon your request. Please feel free to contact me or Alex Everhart at [phone] if you have
any questions regarding this report.

Sincerely,
JOYCE ENGINEERING

Hannu Kemppinen P.G.
Senior Project Consultant

Enclosures
C: Kent Brandon - Wilkes County, Solid Waste Director (2 copies)

PREPARED FOR:
WILKES COUNTY DEPARTMENT OF SOLID WASTE
9219 ELKIN HIGHWAY
ROARING RIVER, NORTH CAROLINA 27298

DAN JOHNSON LANDFILL
PERMIT NO. 97-02

SECOND SEMIANNUAL WATER QUALITY MONITORING
REPORT OF 2015

FEBRUARY 2015

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE PROJECT NO. 00356.1601.12

______________________________________________________________________________
Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Dan Johnson Landfill, Permit No. 97-02 February 2015

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Second Semiannual Water Quality Monitoring Report of 2015
Dan Johnson Landfill
Wilkes County, North Carolina

TABLE OF CONTENTS

1.0 INTRODUCTION.................................................................................................................1
1.1 Site Information ....................................................................................................................1
1.2 Site Geology ...........................................................................................................................1
1.3 Regulatory Status ..................................................................................................................1
2.0 FACILITY MONITORING PROGRAM ..........................................................................1
2.1 Groundwater Monitoring Program ....................................................................................1
2.2 Surface Water Monitoring Program ...................................................................................2
3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2015 ...............................................2
3.1 Field Work and Visual Inspection .......................................................................................2
3.2 Laboratory Analysis and JOYCE Quality Control ...........................................................3
4.0 DATA ANALYSIS ................................................................................................................4
4.1 Groundwater Data Analysis and Comparisons to Standards ..........................................4
4.2 Surface Water Data Analysis and Comparisons to Standards .........................................5
5.0 CONCLUSION .....................................................................................................................5
6.0 REFERENCES ......................................................................................................................5

Table

Table 1 Summary of Historical Detected Constituents
Table 2 Summary of Groundwater Elevations

Figure

Figure No. 1 Site Location Map

Drawing

Drawing No. 1 Groundwater Surface Map

Appendices

Appendix 1 Laboratory Analytical Reports and Field Data Logs
Appendix 2 Summary of Detections, Exceedances, and Field Parameters
Appendix 3 Horizontal Groundwater Flow Velocities

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Dan Johnson Landfill, Permit No. 97-02 February 2015

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1.0 INTRODUCTION

1.1 Site Information

The Dan Johnson Landfill is a closed, unlined municipal solid waste (MSW) landfill maintained
by Wilkes County. The landfill property is located near the town of Austin, North Carolina.
The property boundary is indicated on an excerpt from the 7.5 minutes USGS topographic map
for Thurmond, North Carolina (Figure No. 1.).

The area surrounding the landfill is primarily residential/ agricultural and contains open fields
and woodlands. The landfill is bounded to the south and east by an unnamed tributary of Little
Elkin Creek.

1.2 Site Geology

The Dan Johnson Landfill is located in the Blue Ridge Belt in the Alligator Back Formation. It
consists of laminated to thin layered mica schist and phyllite interlayered with biotite, muscovite,
gneiss and amphibolite.

1.3 Regulatory Status

Wilkes County is currently monitoring groundwater at the Dan Johnson Landfill in accordance
with criteria set forth in Rule .0500 of the North Carolina Solid Waste Management Rules
(NCSWMR) for municipal solid waste landfills (MSWLF) closed prior to October 9, 1993.

2.0 FACILITY MONITORING PROGRAM

2.1 Groundwater Monitoring Program

The current groundwater compliance monitoring network includes three monitoring wells,
including one upgradient well and two downgradient wells. These wells are summarized below,
along with their current monitoring program status.

Monitoring Well Classification Monitoring Program Total Depth from
TOC (ft)
MW-1 Background Detection (.0500) 60.12
MW-2 Compliance Detection (.0500) 40.08
MW-3 Compliance Detection (.0500) 29.43
TOC = Top of casing.

Groundwater samples are collected semiannually during the second and fourth quarters.
Samples are analyzed for all constituents listed in the NCSWMR Appendix I during the first and
second semiannual events.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Dan Johnson Landfill, Permit No. 97-02 February 2015

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2.2 Surface Water Monitoring Program

Surface water at the Dan Johnson Landfill is monitored semiannually in conjunction with the
groundwater sampling events. Samples are collected from two surface water monitoring points
(Upstream and Downstream).

Surface water samples are collected and analyzed for the NCSWMR Appendix I list of
constituents during both semiannual monitoring events. The results are compared to the 15A
NCAC 2B (NC 2B) Surface Water Standards in a value-to-value comparison. These surface
water monitoring points are summarized below, along with their current monitoring program
status.

Surface Point Classification Monitoring Program
Upstream Up Stream/Compliance Surface Water
Downstream Compliance Surface Water

3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2015

3.1 Field Work and Visual Inspection

In order to detect potential releases of leachate and/or landfill gas migration in a timely manner,
a visual inspection program has been implemented at the Dan Johnson Landfill. This inspection
program involves field personnel making the following observations:

 Observation of stress induced on the biological community (i.e., dead or dying vegetation),
 Indications of leachate impact (i.e., seeps, impacted surface water),
 Observations of erosion; and
 Negative changes around the waste facility.

On October 26, 2015, Joyce Engineering (JOYCE) personnel purged and sampled facility
monitoring wells MW-1, MW-2, and MW-3. Prior to purging, the depth to static water level was
measured for all monitoring wells with an electronic water level indicator, accurate to 0.01 foot.

Monitoring wells were purged and sampled using either disposable bailers or a 12 volt plastic
pump. Measurements of temperature, pH, specific conductivity, and turbidity were recorded in
the site specific log book prior to purging, after each purge volume, and during sampling. Prior
to sampling, laboratory-supplied containers were prepared with the following information:

 Monitoring well number (completed by field personnel),
 Date and time of sample collection (completed by field personnel),
 Initials of sampling personnel (completed by field personnel),
 Project name and number (completed by the laboratory),

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Dan Johnson Landfill, Permit No. 97-02 February 2015

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 Chemical preservative (completed by the laboratory); and
 Requested chemical analysis (completed by the laboratory).

Groundwater samples from each monitoring well were collected directly from the disposable
bailers or 12 volt pump in the provided laboratory containers either immediately after purging or
within 24 hours of the final purge volume. Immediately after collection, the samples were
placed in a laboratory provided cooler and chilled on ice. Field data logs are provided in the
Appendix to this report.

Surface water samples were collected directly from stream flow by lowering the prepared sample
containers into the stream flow with the opening facing into the current flow. Care was taken not
to overfill the sample containers (which could lead to preservative loss) and to avoid sampling-
induced turbidity. At the time of sampling, surface water was also measured for temperature,
pH, specific conductivity, and turbidity. After sample collection, the samples were placed in a
laboratory provided cooler and chilled on ice. Field data logs are provided in the Appendix.

3.2 Laboratory Analysis and JOYCE Quality Control

The October 2015 groundwater and surface water samples were submitted to Pace Analytical
Services, Inc. of Huntersville, North Carolina under chain-of-custody control for analysis. As
presented earlier, the groundwater samples were analyzed for the NCSWMR Appendix I
constituents. JOYCE requested a Level II data report for the final laboratory report. The
samples were received by the laboratory on October 28, 2015, in good condition, properly
preserved, and within analysis hold times.

In addition to samples collected for compliance monitoring at the Dan Johnson Landfill, a Field
Blank was collected by JOYCE personnel as part of the October 2015 sampling event. Also, a
Trip Blank was prepared by the laboratory to accompany the volatile sampling containers during
shipment to and from the laboratory. The October 2015 Field Blank was analyzed for the
NCSWMR Appendix I constituents while the October 2015 Trip Blanks was analyzed for the
NCSWMR Appendix I volatile organics only.

Upon receipt of the laboratory data package, the data was reviewed by JOYCE personnel for the
following:

 General typographical errors,
 Correct analyses performed and within method specified hold times,
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate,
and Laboratory Control Samples,
 Blank qualified data (B-flags),
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Dan Johnson Landfill, Permit No. 97-02 February 2015

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4.0 DATA ANALYSIS

4.1 Groundwater Data Analysis and Comparisons to Standards

Results from the October 2015 sampling event were received November 6, 2015 from Pace
Analytical Services, Inc. and are found in Appendix 1. Analytical results from monitoring wells
were compared directly to the NC 2L Groundwater Standards (NC 2L) or Groundwater
Protection Standards (GWPS).

The following inorganic and organic constituents were detected at quantified concentrations in
groundwater during the October 2015 sampling event. All concentrations are reported in
micrograms per liter (µg/L). Concentrations with a “J” are considered to be estimated.
Concentrations with a “B” are attributed to lab or field contamination. Bold concentrations were
detected above the NC 2L or GWPS in downgradient wells.

Constituent NC2L/
(GWPS)
Background Downgradient Blanks MW-1 MW-2 MW-3
Barium 700 34.5 J 92.9 J 104 ND
Cobalt (1) 59.2 32.4 25.3 ND
Zinc 1000 ND 70.1 ND ND
Benzene 1 2.2 ND 0.39 J ND
1,4-Dichlorobenzene 6 2.4 3.3 5.2 ND
Cis-1,2-Dichloroethylene 70 7.8 1.5 J 1.2 J ND
Vinyl Chloride 0.03 1.7 ND ND ND
ND = Not Detected
In general, the organic and inorganic results are consistent with historical data. Historical
groundwater data can be found in Table 1.
4.2 Surface Water Data Analysis and Comparisons to Standards

No organic or inorganic constituents were detected at quantified concentrations in surface water
monitoring points during the October 2015 sampling event. In general, the results are consistent
with historical data. Historical surface water data can be found in Table 1.

5.0 CONCLUSION

Based on historical groundwater data, inorganic and organic constituents detected above the NC
2L and GWPS in groundwater samples collected during the October 2015 sampling event are
consistent with previous events. In addition, there were no constituents detected at the surface
water monitoring points above the NC 2B Standards. The Dan Johnson Landfill will remain in
Detection Monitoring under Rule .0500 of the NCSWMR and the next semiannual sampling
event is tentatively scheduled for the April 2016.

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Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Dan Johnson Landfill, Permit No. 97-02 February 2015

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6.0 REFERENCES

Brown, Philip M., Chief Geologist, 1985, Geologic Map of North Carolina, The North Carolina
Geologic Survey, scale 1:500,000.

Fetter, C.W., 2001, Applied Hydrogeology, Fourth Edition: Prentice-Hall, Inc.

Johnson, A.I., 1967, Specific Yield - Compilation of Specific Yields For Various Materials: U.S.
Geological Survey Water Supply Paper 1662-D.

North Carolina Department of Environment and Natural Resources, 1990-2011, Solid Waste
Management Regulations.

USEPA, 1986, RCRA Ground Water Monitoring Technical Enforcement Guidance Document
(TEGD).

USEPA, 1992, Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance, Chapter 2, July.

Tables
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
INORGANICS COMPOUNDS
Antimony Apr-93 NR 30 NS NS NS NS NS NA
Sep-93 NR 30 NS NS NS NS NS NA
Apr-94 NR 30 NS NS NS NS NS NA
Oct-94 NR 30 30 ND ND ND ND NA
Apr-95 NR 30 ND ND ND ND ND NA
Nov-95 NR 30 ND ND ND ND ND ND
May-96 NR 30 ND ND ND ND ND NA
Nov-96 NR 30 ND ND ND ND ND ND
Mar-97 NR 30 ND ND ND ND ND ND
Sep-97 NR 30 ND ND ND ND ND ND
Mar-98 NR 30 ND ND ND ND ND ND
Sep-98 NR 30 ND ND ND ND ND ND
Mar-99 NR 30 ND ND ND ND ND ND
Sep-99 NR 30 ND ND ND ND ND ND
Apr-00 NR 30 ND ND ND ND ND ND
Sep-00 NR 30 ND ND ND ND ND ND
Mar-01 NR 30 ND ND ND ND ND ND
Oct-01 NR 30 ND ND ND ND ND ND
Apr-02 NR 30 ND ND ND ND ND ND
Nov-02 NR 30 ND ND ND ND ND ND
May-03 NR 30 ND ND ND ND ND ND
Nov-03 NR 30 ND ND ND ND ND ND
May-04 NR 30 ND ND ND ND ND ND
Nov-04 NR 30 ND ND ND ND ND ND
May-05 NR 30 ND ND ND ND ND ND
Nov-05 NR 30 ND ND ND ND ND ND
29-Jun-06 NR 30 ND ND ND ND ND ND
20-Dec-06 NR 6 ND ND ND ND ND ND
28-Jun-07 1.2 6.0 ND ND ND ND ND ND
GWPS = 1.4 µg/L (10/23/07)27-Dec-07 1.2 6.0 ND ND ND (ND)ND 1.4 B 4.1 J
NC 2B = NE (05/01/07)28-Apr-08 1.2 6.0 ND 1.3 J ND (ND)ND ND ND
08-Dec-08 1.2 6.0 ND 2.5 J ND (ND)ND ND ND
24-Jun-09 1.2 6.0 2.5 B 1.9 (4.8 B)B ND 2.6 B 2.2 B 3.1 J
15-Dec-09 1.2 6.0 ND 9.8 B 2.4 (3.2 B)B ND 4.2 B 3.0 J
22-Jun-10 1.2 6.0 4.8 B ND (1.6 B)6.9 B 4.8 B 2.4 B 3.3 J
GWPS = 1 µg/L (8/1/10)02-Nov-10 1.2 6.0 ND ND ND (ND)ND ND ND
11-Apr-11 2.6 6.0 ND ND ND ND ND ND
17-Oct-11 5.0 6.0 ND ND ND ND ND ND
09-Apr-12 5.0 6.0 ND ND ND ND ND ND
15-Oct-12 5.0 6.0 ND ND ND ND ND ND
15-Apr-13 5.0 6.0 ND ND ND ND ND ND
07-Oct-13 5.0 6.0 ND ND ND ND ND ND
28-Apr-14 5.0 6.0 ND ND ND ND ND ND
13-Oct-14 5.0 6.0 ND 7.0 ND ND ND ND
08-Apr-15 3.8 6.0 ND ND ND ND ND ND
26-Oct-15 3.8 6.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 1 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Barium Apr-93 NR 100 <100 <100 698 <50 <50 NA
Sep-93 NR 250 <250 <250 371 <250 <250 NA
Apr-94 NR 250 <250 <250 <250 <125 <125 NA
Oct-94 NR 500 ND ND ND ND ND NA
Apr-95 NR 500 ND ND 602 ND ND NA
Nov-95 NR 500 ND ND ND ND ND NA
May-96 NR 500 ND ND ND ND ND NA
Nov-96 NR 500 ND ND ND ND ND ND
Mar-97 NR 500 ND ND ND ND ND ND
Sep-97 NR 500 ND ND ND ND ND ND
Mar-98 NR 500 ND ND ND ND ND ND
Sep-98 NR 500 ND ND ND ND ND ND
Mar-99 NR 500 ND ND ND ND ND ND
Sep-99 NR 500 ND ND ND ND ND ND
Apr-00 NR 500 ND ND ND ND ND ND
Sep-00 NR 500 ND ND ND ND ND ND
Mar-01 NR 500 ND ND ND ND ND ND
Oct-01 NR 500 ND ND ND ND ND ND
Apr-02 NR 500 ND ND ND ND ND ND
Nov-02 NR 500 ND ND ND ND ND ND
May-03 NR 500 ND ND ND ND ND ND
Nov-03 NR 500 ND ND ND ND ND ND
May-04 NR 500 ND ND ND ND ND ND
Nov-04 NR 500 ND ND ND ND ND ND
May-05 NR 500 ND ND ND ND ND ND
Nov-05 NR 500 ND ND ND ND ND ND
29-Jun-06 NR 500 ND ND ND ND ND ND
20-Dec-06 NR 100 ND ND 152 ND 1660 ND
28-Jun-07 1.1 100 24.4 B 91 J 196 (189)18.1 B 16.7 B 12.6 J
NC 2L = 2,000 µg/L (10/23/07)27-Dec-07 1.1 100 22.1 B 119 132 (140)14.9 B 13.2 B 17.8 J
NC 2B = NE (05/01/07)28-Apr-08 1.1 100 22.2 B 87.8 J 143 (90.3)15.7 B 7.2 B 13.8 J
08-Dec-08 1.1 100 23.5 J 87.8 J 168 (168)13.7 J 9.8 J ND
24-Jun-09 1.1 100 36.1 B 97.4 (124)J 79.7 J 14.6 B 13.8 B 9.9 J
15-Dec-09 1.1 100 21.3 B 83.8 J 66.2 (60.9 J)J 14.3 B 13.9 B 9.9 J
NC 2L = 700 µg/L (01/01/10)22-Jun-10 1.1 100 24.0 J 138 (136)107 15.5 J 15.2 J 1.8 J
02-Nov-10 1.1 100 22.8 B 91.0 J 62.2 (63.5 B)B 11.3 B 14.4 B 15.6 J
11-Apr-11 0.20 100 26.4 B 131 197 11.8 B 12.1 B 13.2 J
17-Oct-11 5.0 100 27.1 J 110 173 11.9 J 13.1 J ND
09-Apr-12 5.0 100 29.4 B 89.7 J 119 13.9 B 13.8 B 15.8 J
15-Oct-12 5.0 100 24.0 J 106 146 15.5 J 16.2 J ND
15-Apr-13 5.0 100 32.3 J 139 82.0 J 16.5 J 15.4 J ND
07-Oct-13 5.0 100 32.3 J 156 98.7 J 33.2 J 37.9 J ND
28-Apr-14 5.0 100 35.4 J 147 82.0 J 17.6 J 18.5 J ND
13-Oct-14 5.0 100 29.4 J 154 117 15.3 J 15.4 J ND
08-Apr-15 2.5 100 31.7 J 75.8 J 110 15.6 J 17.1 J ND
26-Oct-15 2.5 100 34.5 J 92.9 J 104 13.0 J 14.2 J ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 2 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Beryllium Apr-93 NR 2 NS NS NS NS NS NA
Sep-93 NR 2 NS NS NS NS NS NA
Apr-94 NR 2 NS NS NS NS NS NA
Oct-94 NR 2 ND ND ND ND ND NA
Apr-95 NR 2 ND 3 ND ND ND NA
Nov-95 NR 2 ND 2 ND ND ND NA
May-96 NR 2 2 4 ND 2 2 NA
Nov-96 NR 2 ND 2 6 ND ND ND
Mar-97 NR 2 ND ND ND ND ND ND
Sep-97 NR 2 ND 2 ND ND ND ND
Mar-98 NR 2 ND 2 ND ND ND ND
Sep-98 NR 2 ND 4 ND ND ND ND
Mar-99 NR 2 ND 2 ND ND ND ND
Sep-99 NR 2 ND ND ND ND ND ND
Apr-00 NR 2 ND ND ND ND ND ND
Sep-00 NR 2 ND ND ND ND ND ND
Mar-01 NR 2 ND ND ND ND ND ND
Oct-01 NR 2 ND ND ND ND ND ND
Apr-02 NR 2 ND ND ND ND ND ND
Nov-02 NR 2 ND ND ND ND ND ND
May-03 NR 2 ND ND ND ND ND ND
Nov-03 NR 2 ND ND ND ND ND ND
May-04 NR 2 ND ND ND ND ND ND
Nov-04 NR 2 ND ND ND ND ND ND
May-05 NR 2 ND ND ND ND ND ND
Nov-05 NR 2 ND ND ND ND ND ND
29-Jun-06 NR 2 ND ND ND ND ND ND
20-Dec-06 NR 1 ND ND ND ND ND ND
28-Jun-07 0.2 1.0 ND ND ND ND ND ND
GWPS = 4 µg/L (10/23/07)27-Dec-07 0.2 1.0 ND ND 0.3 (0.3 J)J ND ND ND
NC 2B = 6.5 µg/L (05/01/07)28-Apr-08 0.2 1.0 0.2 J ND 0.2 ( 0.6 J)J ND ND ND
08-Dec-08 0.2 1.0 ND ND 0.5 (0.4 J)J ND ND ND
24-Jun-09 0.2 1.0 ND 0.27 (0.2 B)B 0.4 B 0.2 B ND 0.3 J
15-Dec-09 0.2 1.0 ND ND ND (ND)ND ND ND
22-Jun-10 0.2 1.0 ND ND (ND)ND ND ND ND
02-Nov-10 0.2 1.0 0.3 J 0.2 J 0.5 (0.4 J)J ND ND ND
11-Apr-11 0.10 1.0 ND ND ND ND ND ND
17-Oct-11 1.0 1.0 ND ND ND ND ND ND
09-Apr-12 1.0 1.0 ND ND ND ND ND ND
15-Oct-12 1.0 1.0 ND ND ND ND ND ND
15-Apr-13 1.0 1.0 1.4 B 1.3 B 1.6 B 1.4 B 1.5 B 1.6
07-Oct-13 1.0 1.0 ND ND ND ND ND ND
28-Apr-14 1.0 1.0 ND ND ND ND ND ND
13-Oct-14 1.0 1.0 ND ND ND ND ND ND
08-Apr-15 0.5 1.0 ND ND ND ND ND ND
26-Oct-15 0.5 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 3 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Cadmium Apr-93 NR 1 <2 2.1 <2 <2 <2 NA
Sep-93 NR 1 <2 <2 <2 <2 <2 NA
Apr-94 NR 1 <2 4 <2 <2 <2 NA
Oct-94 NR 1 1.8 ND 2.7 1 ND NA
Apr-95 NR 1 ND ND 1 ND ND NA
Nov-95 NR 1 2 1.8 1.5 ND ND NA
May-96 NR 1 ND 2 2 ND ND ND
Nov-96 NR 1 ND 2 1 ND ND ND
Mar-97 NR 1 ND 3 ND 1 ND ND
Sep-97 NR 1 ND 3 ND 2 ND ND
Mar-98 NR 1 ND 3 ND ND ND ND
Oct-94 NR 1 1.8 ND 2.7 1 ND NS
Sep-98 NR 1 ND 3 ND(1)1 ND ND
Mar-99 NR 1 ND 3(1)3 ND ND ND
Sep-99 NR 1 ND 1.7 ND ND ND ND
Apr-00 NR 1 ND ND ND ND ND ND
Sep-00 NR 1 ND ND ND ND ND ND
Mar-01 NR 1 ND ND ND 1.8 1.1 ND
Oct-01 NR 1 ND ND ND ND ND ND
Apr-02 NR 1 ND ND ND ND ND ND
Nov-02 NR 1 ND ND ND(1)ND ND ND
May-03 NR 1 ND ND ND ND ND ND
Nov-03 NR 1 ND ND ND ND ND ND
May-04 NR 1 ND ND ND ND ND ND
Nov-04 NR 1 1 ND ND ND ND ND
May-05 NR 1 2 1(1)2 ND ND ND
Nov-05 NR 1 ND 2 ND ND ND ND
29-Jun-06 NR 1 ND 3 ND ND ND ND
20-Dec-06 NR 1 ND ND ND ND ND 1.7
28-Jun-07 0.2 1.0 0.8 J 1.2 0.4 J (0.4 J)ND ND ND
NC 2L = 1.75 µg/L (10/23/07)27-Dec-07 0.2 1.0 ND ND ND (ND)ND ND ND
NC 2B = 2 µg/L (05/01/07)28-Apr-08 0.2 1.0 ND 0.8 J ND (ND)ND 0.2 J ND
08-Dec-08 0.2 1.0 0.9 J 0.8 J ND (ND)ND ND ND
24-Jun-09 0.2 1.0 0.3 B 0.7 (0.3 B)B 0.2 B 0.2 B 0.3 B 0.5 J
15-Dec-09 0.2 1.0 ND ND ND (ND)ND ND ND
NC 2L = 2 µg/L (01/01/10)22-Jun-10 0.2 1.0 2.1 1.8 (1.4)0.2 J ND ND ND
02-Nov-10 0.2 1.0 1.4 1.1 0.3 (0.4 J)J ND 0.4 J ND
11-Apr-11 0.50 1.0 ND ND ND ND ND ND
17-Oct-11 1.0 1.0 ND ND ND ND ND ND
09-Apr-12 1.0 1.0 ND ND ND ND ND ND
15-Oct-12 1.0 1.0 ND ND ND ND ND ND
15-Apr-13 1.0 1.0 ND ND ND ND ND ND
07-Oct-13 1.0 1.0 ND ND ND ND ND ND
28-Apr-14 1.0 1.0 ND ND ND ND ND ND
13-Oct-14 1.0 1.0 ND ND ND ND ND ND
08-Apr-15 0.5 1.0 ND ND 1.1 ND ND ND
26-Oct-15 0.5 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 4 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Chromium Apr-93 NR 40 <40 <40 <40 <20 <20 NA
Sep-93 NR 20 <20 <20 <20 <20 <20 NA
Apr-94 NR 20 41 <20 <20 <10 <10 NA
Oct-94 NR 10 ND ND ND ND ND NA
Apr-95 NR 10 ND ND ND ND ND NA
Nov-95 NR 10 ND ND ND 20 12 NA
May-96 NR 10 ND ND ND ND ND ND
Nov-96 NR 10 ND ND ND ND ND ND
Mar-97 NR 10 ND ND ND ND ND ND
Sep-97 NR 10 ND ND ND ND ND ND
Mar-98 NR 10 ND ND ND ND ND ND
Sep-98 NR 10 ND 13 ND ND ND ND
Mar-99 NR 10 ND ND ND ND ND ND
Sep-99 NR 10 ND 11 ND ND ND ND
Apr-00 NR 10 ND ND ND ND ND ND
Sep-00 NR 10 ND ND ND ND ND ND
Mar-01 NR 10 ND ND ND ND ND ND
Oct-01 NR 10 ND ND ND ND ND ND
Apr-02 NR 10 ND ND ND ND ND ND
Nov-02 NR 10 ND ND ND ND ND ND
May-03 NR 10 ND ND ND ND ND ND
Nov-03 NR 10 ND ND ND ND ND ND
May-04 NR 10 ND ND ND ND ND ND
Nov-04 NR 10 ND ND ND ND ND ND
May-05 NR 10 ND ND ND ND ND ND
Nov-05 NR 10 ND ND ND ND ND ND
29-Jun-06 NR 10 ND ND ND ND ND ND
20-Dec-06 NR 10 ND ND ND ND ND ND
28-Jun-07 0.7 10.0 1.7 J 4.8 J 9.3 J (7.9 J)ND 1.1 J ND
NC 2L = 50 µg/L (10/23/07)27-Dec-07 0.7 10.0 1.9 J 6.0 J 2.3 (3.3 J)J ND ND ND
NC 2B = 50 µg/L (05/01/07)28-Apr-08 0.7 10.0 2.7 J 7.3 J 3.0 (8.8 J)J ND ND ND
08-Dec-08 0.7 10.0 1.7 J 7.3 J 2.5 (2.5 J)J ND ND ND
24-Jun-09 0.7 10.0 2.2 J 4.8 (5.3 J)J 2.1 J 1.5 J ND ND
15-Dec-09 0.7 10.0 1.3 J 6.4 J 1.4 (1.5 J)J ND 1.2 J ND
NC 2L = 10 µg/L (01/01/10)22-Jun-10 0.7 10.0 ND 5.0 (4.3 J)J 3.2 J ND ND ND
02-Nov-10 0.7 10.0 1.0 J 3.3 J 1.8 (1.6 J)J ND ND ND
11-Apr-11 0.40 10.0 ND 0.61 J 0.96 J 0.66 J 0.44 J ND
17-Oct-11 5.0 10.0 ND ND ND ND ND ND
09-Apr-12 5.0 10.0 ND ND ND ND ND ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND
15-Apr-13 5.0 10.0 ND ND ND ND ND ND
07-Oct-13 5.0 10.0 ND ND ND ND ND ND
28-Apr-14 5.0 10.0 ND ND ND ND ND ND
13-Oct-14 5.0 10.0 ND ND ND ND ND ND
08-Apr-15 2.5 10.0 ND ND ND ND ND ND
26-Oct-15 2.5 10.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 5 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Cobalt Apr-93 NR 10 NS NS NS NS NS NA
Sep-93 NR 10 NS NS NS NS NS NA
Apr-94 NR 10 NS NS NS NS NS NA
Oct-94 NR 10 ND 47 105 ND ND NA
Apr-95 NR 10 ND 46 115 ND ND NA
Nov-95 NR 10 13 54 49 ND ND NA
May-96 NR 10 ND 60 46 ND ND ND
Nov-96 NR 10 ND 60 71 ND ND ND
Mar-97 NR 10 ND 64 29 ND ND ND
Sep-97 NR 10 ND 54 75 ND ND ND
Mar-98 NR 10 10 67 21 ND ND ND
Sep-98 NR 10 ND 76 77(75)ND ND ND
Mar-99 NR 10 14 65(65)45 ND ND ND
Sep-99 NR 10 ND 71 50 51 ND ND
Apr-00 NR 10 12 60(59)45 ND ND ND
Sep-00 NR 10 ND 72 59 ND ND ND
Mar-01 NR 10 12 71 34(34)ND ND ND
Oct-01 NR 10 ND 65 76(75)ND ND ND
Apr-02 NR 10 ND 63 64(63)ND ND ND
Nov-02 NR 10 ND 56 17(18)ND ND ND
May-03 NR 10 ND 78(80)31 ND ND ND
Nov-03 NR 10 ND 67 47(52)ND ND ND
May-04 NR 10 ND 54(54)59 ND ND ND
Nov-04 NR 10 ND 55(54)35 ND ND ND
May-05 NR 10 ND 53(50)44 ND ND ND
Nov-05 NR 10 ND 40 44(42)ND ND ND
29-Jun-06 NR 10 ND 50 57 ND ND ND
20-Dec-06 NR 10 ND ND ND ND ND ND
28-Jun-07 0.7 10.0 5.3 B 52.2 64.6 (66.1)ND ND 1.3
GWPS = 70 µg/L (10/23/07)27-Dec-07 0.7 10.0 4.1 J 47.8 26.5 (26.3)ND ND ND
NC 2B = NE µg/L (05/01/07)28-Apr-08 0.7 10.0 11.3 50.0 34.8 (46.8)0.7 B ND 1.5 J
08-Dec-08 0.7 10.0 9.0 J 50.0 30.1 (30.3)ND ND ND
24-Jun-09 0.7 10.0 13.4 52.0 (50.8)24.5 0.8 J ND ND
15-Dec-09 0.7 10.0 17.1 46.0 9.6 (9.2 J)J 0.8 J ND ND
22-Jun-10 0.7 10.0 16.7 56.4 (55.3)48.9 1.2 J ND ND
GWPS = 1 µg/L (10/1/10)02-Nov-10 0.7 10.0 21.3 44.3 13.1 (12.0)ND 0.9 J ND
11-Apr-11 0.60 10.0 48.2 52.6 24.2 ND ND ND
17-Oct-11 5.0 10.0 26.8 41.7 45.5 ND ND ND
09-Apr-12 5.0 10.0 46.1 34.3 19.6 ND ND ND
15-Oct-12 5.0 10.0 32.1 42.2 24.6 ND ND ND
15-Apr-13 5.0 10.0 92.6 57.0 14.9 ND ND ND
07-Oct-13 5.0 10.0 107 76.3 34.8 6.3 J 7.4 J ND
28-Apr-14 5.0 10.0 100 61.1 22 ND ND ND
13-Oct-14 5.0 10.0 24.8 52.6 48.7 ND ND ND
08-Apr-15 2.5 10.0 71.1 27.7 25.2 ND ND ND
26-Oct-15 2.5 10.0 59.2 32.4 25.3 ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 6 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Copper Apr-93 NR 200 23 43 21 <10 <10 NA
Sep-93 NR 200 <10 <10 <10 <10 <10 NA
Apr-94 NR 200 <10 10 72 <5 <5 NA
Oct-94 NR 200 ND ND ND ND ND NA
Apr-95 NR 200 ND ND ND ND ND NA
Nov-95 NR 200 ND ND ND ND ND NA
May-96 NR 200 ND ND ND ND ND ND
Nov-96 NR 200 ND ND ND ND ND ND
Mar-97 NR 200 ND ND ND ND ND ND
Sep-97 NR 200 ND ND ND ND ND ND
Mar-98 NR 200 ND ND ND ND ND ND
Sep-98 NR 200 ND ND ND ND ND ND
Mar-99 NR 200 ND ND ND ND ND ND
Sep-99 NR 200 ND ND ND ND ND ND
Apr-00 NR 200 ND ND ND ND ND ND
Sep-00 NR 200 ND ND ND ND ND ND
Mar-01 NR 200 ND ND ND ND ND ND
Oct-01 NR 200 ND ND ND ND ND ND
Apr-02 NR 200 ND ND ND ND ND ND
Nov-02 NR 200 ND ND ND ND ND ND
May-03 NR 200 ND ND ND ND ND ND
Nov-03 NR 200 ND ND ND ND ND ND
May-04 NR 200 ND ND ND ND ND ND
Nov-04 NR 200 ND ND ND ND ND ND
May-05 NR 200 ND ND ND ND ND ND
Nov-05 NR 200 ND ND ND ND ND ND
29-Jun-06 NR 200 ND ND ND ND ND ND
20-Dec-06 NR 10 12 ND ND ND ND ND
28-Jun-07 2.0 10.0 6.9 B 6.0 B 7.1 B (6.1 B)5.8 B 6.3 B 5.2 J
NC 2L = 1,000 µg/L (10/23/07)27-Dec-07 2.0 10.0 ND 10.0 1.3 (ND)J ND ND ND
NC 2B = 7 µg/L (05/01/07)28-Apr-08 2.0 10.0 ND 3.8 B 1.3 (2.4 B)B 3.2 B ND 2.0 J
08-Dec-08 2.0 10.0 ND 3.8 J ND (ND)ND ND ND
24-Jun-09 2.0 10.0 ND 4.3 (3.8 J)J 3.5 J 2.2 J ND ND
15-Dec-09 2.0 10.0 ND 4.2 J ND (ND)ND ND ND
NC 2L = 1,000 µg/L (01/01/10)22-Jun-10 2.0 10.0 ND 6.4 (3.6 J)J 1.7 J 1.8 J 1.7 J ND
02-Nov-10 2.0 10.0 ND ND ND (ND)ND ND 5.4 J
11-Apr-11 0.30 10.0 0.45 B 0.55 B 0.81 B 0.69 B 0.67 B 0.30 J
17-Oct-11 5.0 10.0 ND ND ND ND ND ND
09-Apr-12 5.0 10.0 5.3 J ND ND ND ND ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND
15-Apr-13 5.0 10.0 ND ND ND ND ND ND
07-Oct-13 5.0 10.0 ND ND ND ND 5.1 J ND
28-Apr-14 5.0 10.0 ND ND ND ND ND ND
13-Oct-14 5.0 10.0 ND ND ND ND ND ND
08-Apr-15 2.5 10.0 7.4 B 2.9 B ND 3.4 B 2.6 B 2.7 J
26-Oct-15 2.5 10.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 7 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Lead Apr-93 NR 10 <5 67 14 <5 <5 NA
Sep-93 NR 10 <5 30 8.8 <5 <5 NA
Apr-94 NR 10 <5 10 15 <5 <5 NA
Oct-94 NR 10 ND ND ND ND ND NA
Apr-95 NR 10 ND ND 18 ND ND NA
Nov-95 NR 10 ND 17 11 ND ND NA
May-96 NR 10 ND 16 11 ND ND ND
Nov-96 NR 10 ND 15 ND ND ND ND
Mar-97 NR 10 ND ND ND ND ND ND
Sep-97 NR 10 ND 16 ND ND ND ND
Mar-98 NR 10 ND 20 22 ND ND ND
Sep-98 NR 10 ND 20 ND ND ND ND
Mar-99 NR 10 ND 10(ND)ND ND ND ND
Sep-99 NR 10 ND 14 ND ND ND ND
Apr-00 NR 10 ND ND ND ND ND ND
Sep-00 NR 10 ND ND ND ND ND ND
Mar-01 NR 10 ND ND ND ND ND ND
Oct-01 NR 10 ND ND ND ND ND ND
Apr-02 NR 10 ND ND ND ND ND ND
Nov-02 NR 10 ND ND ND ND ND ND
May-03 NR 10 ND 10(12)ND ND ND ND
Nov-03 NR 10 ND ND ND ND ND ND
May-04 NR 10 ND ND ND ND ND ND
Nov-04 NR 10 ND ND ND ND ND ND
May-05 NR 10 ND ND ND ND ND ND
Nov-05 NR 10 ND ND ND ND ND ND
29-Jun-06 NR 10 ND ND ND ND ND ND
20-Dec-06 NR 10 ND ND ND ND ND ND
28-Jun-07 2.0 10.0 14.7 9.6 J 6.0 J (3.7 J)3.0 J ND ND
NC 2L = 15 µg/L (10/23/07)27-Dec-07 2.0 10.0 ND 3.5 B ND (ND)ND 2.8 B 2.1 J
NC 2B = 25 µg/L (05/01/07)28-Apr-08 2.0 10.0 ND 6.6 B ND (2.8 B)2.7 B 3.2 B 2.5 J
08-Dec-08 2.0 10.0 4.1 B 6.6 B 2.1 (2.6 B)B ND 2.7 B 2.8 J
24-Jun-09 2.0 10.0 4.0 J 4.6 (6.0 J)J 5.4 J 3.6 J ND ND
15-Dec-09 2.0 10.0 ND 4.6 J ND (ND)4.0 J ND ND
22-Jun-10 2.0 10.0 6.4 J 7.1 (4.0 J)J 1.7 J 3.2 J ND ND
02-Nov-10 2.0 10.0 2.8 J ND ND (ND)ND ND ND
11-Apr-11 4.0 10.0 ND ND ND ND ND ND
17-Oct-11 5.0 10.0 ND ND ND ND ND ND
09-Apr-12 5.0 10.0 ND 7.0 J ND ND ND ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND
15-Apr-13 5.0 10.0 ND ND ND ND ND ND
07-Oct-13 5.0 10.0 ND ND ND ND ND ND
28-Apr-14 5.0 10.0 ND ND ND ND ND ND
13-Oct-14 5.0 10.0 ND ND ND ND ND ND
08-Apr-15 2.5 10.0 2.6 J ND ND ND ND ND
26-Oct-15 2.5 10.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 8 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Nickel Apr-93 NR 50 NS NS NS NS NS NA
Sep-93 NR 50 NS NS NS NS NS NA
Apr-94 NR 50 NS NS NS NS NS NA
Oct-94 NR 50 ND ND ND ND ND NA
Apr-95 NR 50 ND ND ND ND ND NA
Nov-95 NR 50 ND ND ND ND ND NA
May-96 NR 50 ND ND ND ND ND ND
Nov-96 NR 50 ND ND ND ND ND ND
Mar-97 NR 50 ND ND ND ND ND ND
Sep-97 NR 50 ND ND ND ND ND ND
Mar-98 NR 50 ND ND ND ND ND ND
Sep-98 NR 50 ND ND ND ND ND ND
Mar-99 NR 50 ND ND 63 ND ND ND
Sep-99 NR 50 ND ND ND ND ND ND
Apr-00 NR 50 ND ND ND ND ND ND
Sep-00 NR 50 ND ND ND ND ND ND
Mar-01 NR 50 ND ND ND ND ND ND
Oct-01 NR 50 ND ND ND ND ND ND
Apr-02 NR 50 ND ND ND ND ND ND
Nov-02 NR 50 ND ND ND ND ND ND
May-03 NR 50 ND ND ND ND ND ND
Nov-03 NR 50 ND ND ND ND ND ND
May-04 NR 50 ND ND ND ND ND ND
Nov-04 NR 50 ND ND ND ND ND ND
May-05 NR 50 ND ND ND ND ND ND
Nov-05 NR 50 ND ND ND ND ND ND
29-Jun-06 NR 50 ND ND ND ND ND ND
20-Dec-06 NR 50 ND ND ND ND ND ND
28-Jun-07 0.6 50.0 1.9 B 13.4 B 9.2 (5.7 B)B 3.5 B 1.9 B 6.0 J
NC 2L = 100 µg/L (10/23/07)27-Dec-07 0.6 50.0 1.5 J 12.5 J 2.4 (1.7 J)J ND ND ND
NC 2B = 88 µg/L (05/01/07)28-Apr-08 0.6 50.0 2.0 B 14.9 B 1.9 (13.8 B)B 1.1 B ND 5.0 J
08-Dec-08 0.6 50.0 ND 14.9 B 17.7 (3.0 B)B 1.5 B 1.5 B 4.3 J
24-Jun-09 0.6 50.0 1.7 B 15.4 (15.3 J)J 1.8 B ND ND 2.4 J
15-Dec-09 0.6 50.0 ND 10.5 J ND (ND)50.0 ND ND
22-Jun-10 0.6 50.0 ND 12.8 (12.6 J)J ND ND ND ND
02-Nov-10 0.6 50.0 2.3 J 12.1 J 2.0 (1.7 J)J 0.8 J 0.8 J ND
11-Apr-11 1.7 50.0 ND 9.4 B ND ND ND 4.4 J
17-Oct-11 5.0 50.0 ND 9.7 J ND ND ND ND
09-Apr-12 5.0 50.0 ND 8.5 J ND ND ND ND
15-Oct-12 5.0 50.0 ND 10.7 J ND ND ND ND
15-Apr-13 5.0 50.0 ND 9.0 J ND ND ND ND
07-Oct-13 5.0 50.0 ND 8.1 J ND ND ND ND
28-Apr-14 5.0 50.0 ND 7.5 J ND ND ND ND
13-Oct-14 5.0 50.0 ND 12.7 J ND ND ND ND
08-Apr-15 2.5 50.0 3.0 J 8.6 J ND ND ND ND
26-Oct-15 2.5 50.0 ND 7.2 J ND ND ND ND
Selenium 24-Jun-09 6.3 10.0 ND ND (ND)ND 6.4 J ND ND
NC 2B = 5 µg/L (05/01/07)15-Dec-09 6.3 10.0 ND ND ND (ND)ND ND 7.4 J
NC 2L = 20 µg/L (01/01/10)22-Jun-10 6.3 10.0 ND ND (ND)ND ND ND ND
02-Nov-10 6.3 10.0 ND ND ND (ND)ND ND ND
11-Apr-11 3.8 10.0 ND ND ND ND ND ND
17-Oct-11 10.0 10.0 ND ND ND ND ND ND
09-Apr-12 10.0 10.0 ND ND ND ND ND ND
15-Oct-12 10.0 10.0 ND ND ND ND ND ND
15-Apr-13 10.0 10.0 ND ND ND ND ND ND
07-Oct-13 10.0 10.0 ND ND ND ND ND ND
28-Apr-14 10.0 10.0 ND ND ND ND ND ND
13-Oct-14 10.0 10.0 ND ND ND ND ND ND
08-Apr-15 5.0 10.0 ND ND ND ND ND ND
26-Oct-15 5.0 10.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 9 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Silver 27-Dec-07 1.1 10.0 2.6 B ND 1.3 (ND)B ND ND 1.1 J
NC 2L = 17.5 µg/L (10/23/07)28-Apr-08 1.1 10.0 ND ND ND (ND)ND ND ND
NC 2B = 0.06 µg/L (05/01/07)08-Dec-08 1.1 10.0 ND ND 1.5 (1.6 J)J ND ND ND
24-Jun-09 1.1 10.0 ND ND (4.1 J)ND 2.0 J ND ND
15-Dec-09 1.1 10.0 ND ND 1.8 (5.3B)B 5.9 B 1.7 B 1.6 J
NC 2L = 20 µg/L (01/01/10)22-Jun-10 1.1 10.0 ND ND (ND)1.8 J ND ND ND
02-Nov-10 1.1 10.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.10 10.0 ND ND ND 0.18 B 0.24 B 0.21 J
17-Oct-11 5.0 10.0 ND ND ND ND ND ND
09-Apr-12 5.0 10.0 ND ND ND ND ND ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND
15-Apr-13 5.0 10.0 ND ND ND ND ND ND
07-Oct-13 5.0 10.0 ND ND ND ND ND ND
28-Apr-14 5.0 10.0 ND ND ND ND ND ND
13-Oct-14 5.0 10.0 ND ND ND ND ND ND
08-Apr-15 2.5 10.0 ND ND ND ND ND ND
26-Oct-15 2.5 10.0 ND ND ND ND ND ND
Thallium 28-Apr-08 2.7 5.5 ND ND ND ND 3.3 J ND
GWPS = 0.28 µg/L (10/23/07)08-Dec-08 2.7 5.5 ND ND ND (ND)ND ND ND
NC 2B = NE (05/01/07)24-Jun-09 2.7 5.5 ND ND (ND)ND ND ND ND
15-Dec-09 2.7 5.5 ND ND ND (ND)ND ND ND
22-Jun-10 2.7 5.5 ND ND (ND)ND ND ND ND
GWPS = 0.2 µg/L (10/1/10)02-Nov-10 2.7 5.5 ND ND ND (ND)ND ND ND
11-Apr-11 3.0 5.5 ND ND ND ND ND ND
17-Oct-11 5.4 5.5 ND ND ND ND ND ND
09-Apr-12 5.4 5.5 ND ND ND ND ND ND
15-Oct-12 5.4 5.5 ND ND ND 6.4 ND ND
15-Apr-13 5.4 5.5 ND ND ND ND ND ND
07-Oct-13 5.4 5.5 ND ND ND ND ND ND
28-Apr-14 5.4 5.5 ND ND ND ND ND ND
13-Oct-14 5.4 5.5 ND ND ND ND ND ND
08-Apr-15 5.0 5.5 ND ND ND ND ND ND
26-Oct-15 5.0 5.5 ND ND ND ND ND ND
Vanadium 27-Dec-07 0.40 25.0 0.7 J 0.9 J ND (ND)ND ND ND
GWPS = 3.5 µg/L (10/23/07)28-Apr-08 0.4 25.0 ND 1.4 J ND (ND)ND ND ND
NC 2B = NE (05/01/07)08-Dec-08 0.4 25.0 3.3 J 1.4 J ND (ND)ND ND ND
24-Jun-09 0.4 25.0 4.2 J 1.4 (5.9 J)J ND ND ND ND
15-Dec-09 0.4 25.0 1.4 B 0.5 B 0.8 (ND)B ND ND 0.9 J
22-Jun-10 0.4 25.0 ND ND (ND)ND ND ND ND
GWPS = 0.3 µg/L (10/1/10)02-Nov-10 0.4 25.0 1.4 J 0.9 J ND (ND)ND ND ND
11-Apr-11 0.20 25.0 ND ND ND ND 0.23 J ND
17-Oct-11 5.0 25.0 ND ND ND ND ND ND
09-Apr-12 5.0 25.0 ND ND ND ND ND ND
15-Oct-12 5.0 25.0 ND ND ND ND ND ND
15-Apr-13 5.0 25.0 ND ND ND ND ND ND
07-Oct-13 5.0 25.0 ND ND ND ND ND ND
28-Apr-14 5.0 25.0 ND ND ND ND ND ND
13-Oct-14 5.0 25.0 ND ND ND ND ND ND
08-Apr-15 2.5 25.0 4.8 J 7.4 J 4.0 J ND ND ND
26-Oct-15 2.5 25.0 ND 6.2 J 4.2 J ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 10 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Zinc Apr-93 NR 50 27 140 335 27 14 NA
Sep-93 NR 50 20 41 84 <10 29 NA
Apr-94 NR 50 <20 51 133 <10 48 NA
Oct-94 NR 50 ND ND ND ND ND NA
Apr-95 NR 50 ND 52 74 112 ND NA
Nov-95 NR 50 68 174 98 ND ND NA
May-96 NR 50 125 198 70 98 ND ND
Nov-96 NR 50 84 92 72 56 92 ND
Mar-97 NR 50 55 B 86 B 72 B 54 B 82 B 56
Sep-97 NR 50 122 199 145 343 162 ND
Mar-98 NR 50 ND 349 110 ND ND ND
Sep-98 NR 50 ND 183 ND ND ND ND
Mar-99 NR 50 ND ND ND ND ND ND
Sep-99 NR 50 ND 185 ND ND ND ND
Apr-00 NR 50 ND ND ND ND ND ND
Sep-00 NR 50 ND ND ND ND ND ND
Mar-01 NR 50 ND ND ND ND ND ND
Oct-01 NR 50 ND 152 ND ND ND ND
Apr-02 NR 50 ND ND ND ND ND ND
Nov-02 NR 50 ND 52 ND ND ND ND
May-03 NR 50 ND ND(69)ND ND ND ND
Nov-03 NR 50 ND ND ND ND ND ND
May-04 NR 50 ND ND ND ND ND ND
Nov-04 NR 50 52 ND ND ND ND ND
May-05 NR 50 ND ND ND ND ND ND
Nov-05 NR 50 ND 55 ND ND ND ND
29-Jun-06 NR 50 ND ND ND ND ND ND
20-Dec-06 NR 10 ND 28(27)ND ND ND ND
28-Jun-07 2.7 10.0 32.3 38.0 50.7 (32.6)22.3 27.8 ND
NC 2L = 1,050 µg/L (10/23/07)27-Dec-07 2.7 10.0 20.9 B 51.6 17.9 (15.2 B)B 9.2 B 24.4 B 9.8 J
NC 2B = 50 µg/L (05/01/07)28-Apr-08 2.7 10.0 41.5 46.6 79.9 (68.6)64.1 20.3 ND
08-Dec-08 2.7 10.0 ND 46.6 B ND (ND)ND ND 19.8
24-Jun-09 2.7 10.0 10.2 B 161 (114)B 10.3 B ND 19.5 B 83.3
15-Dec-09 2.7 10.0 9.8 B 7.93 B ND (ND)ND ND 26.5
NC 2L = 1,000 µg/L (01/01/10)22-Jun-10 2.7 10.0 9.9 B 25.0 (16.4 B)B 10.6 B 8.2 B 8.8 B 7.8 J
02-Nov-10 2.7 10.0 11.1 B 25.6 B 9.6 (3.8 B)B 4.8 B 5.1 B 15.1
11-Apr-11 0.40 10.0 4.0 B 32.8 B 4.4 B ND 2.1 B 22.5
17-Oct-11 10.0 10.0 ND 131 ND ND ND ND
09-Apr-12 10.0 10.0 ND 59.1 ND ND ND ND
15-Oct-12 10.0 10.0 ND 71.4 ND ND ND ND
15-Apr-13 10.0 10.0 ND 42.9 ND ND ND ND
07-Oct-13 10.0 10.0 ND 20.2 13.1 17.3 20.9 ND
28-Apr-14 10.0 10.0 ND ND ND ND ND ND
13-Oct-14 10.0 10.0 ND ND ND ND ND ND
08-Apr-15 5.0 10.0 8.8 J 14.2 ND ND ND ND
26-Oct-15 5.0 10.0 ND 70.1 ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 11 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Organic Compounds
Acetone Apr-95 NR 100 ND ND ND ND ND ND
Oct-95 NR 100 ND ND ND ND ND ND
Apr-96 NR 100 ND ND ND ND ND ND
Nov-96 NR 100 ND ND ND ND ND ND
Mar-97 NR 100 ND ND ND ND ND ND
Sep-97 NR 100 ND ND ND ND ND ND
Mar-98 NR 100 ND ND ND ND ND ND
Sep-98 NR 100 ND ND ND ND ND ND
Mar-99 NR 100 ND ND ND ND ND ND
Oct-99 NR 100 ND ND ND ND ND ND
Apr-00 NR 100 ND 137(160)ND ND ND ND
Sep-00 NR 100 ND ND ND ND ND ND
Mar-01 NR 100 ND ND ND ND ND ND
Oct-01 NR 100 ND 156 ND ND ND ND
Apr-02 NR 100 ND ND ND ND ND ND
Nov-02 NR 100 ND ND ND ND ND ND
May-03 NR 100 ND ND ND ND ND ND
Nov-03 NR 100 ND ND ND ND ND ND
May-04 NR 100 ND ND ND ND ND ND
Nov-04 NR 100 ND ND ND ND ND ND
May-05 NR 100 ND ND ND ND ND ND
Nov-05 NR 100 ND ND ND ND ND ND
29-Jun-06 NR 100 ND ND ND ND ND ND
20-Dec-06 NR 100 ND ND ND ND ND ND
28-Jun-07 1.2 100 ND ND ND ND ND ND
NC 2L = 700 µg/L (10/23/07)27-Dec-07 1.2 100 2.7 B 2.8 B ND (2.4 B)2.9 B 2.8 B 2.6 J
NC 2B = NE (05/01/07)28-Apr-08 1.2 100 11.0 J ND ND (ND)ND ND ND
08-Dec-08 1.2 100 1.3 J ND ND (ND)ND ND ND
24-Jun-09 1.2 100 ND ND (ND)ND ND ND ND
15-Dec-09 1.2 100 ND ND ND (ND)ND ND ND
NC 2L = 6,000 µg/L (01/01/10)22-Jun-10 1.2 100 ND ND (ND)ND ND ND ND
02-Nov-10 1.2 100 ND ND ND (ND)ND ND ND
11-Apr-11 2.2 100 ND ND ND ND ND ND
17-Oct-11 2.2 100 2.5 B ND ND 2.6 B 2.3 B 2.2 J
09-Apr-12 2.2 100 ND ND ND ND ND 6.0 J
15-Oct-12 10.0 100 ND ND ND ND ND ND
15-Apr-13 10.0 100 ND ND ND ND ND 70.2 J
07-Oct-13 10.0 100 ND ND ND ND ND ND
28-Apr-14 10.0 100 ND ND ND ND ND ND
13-Oct-14 10.0 100 ND ND ND ND ND ND
08-Apr-15 10.0 100 ND ND ND ND ND ND
26-Oct-15 10.0 100 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 12 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Benzene Sep-93 NR 5 ND ND ND ND ND ND
Oct-94 NR 5 8 ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 ND ND ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 21 ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 5.4 ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 3.3 J ND ND ND ND ND
28-Jun-07 0.1 1.0 3.4 0.5 J 0.7 J (0.7 J)ND ND ND
NC 2L = 1 µg/L (10/23/07)27-Dec-07 0.1 1.0 2.3 0.4 J ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 1.0 2.7 ND ND (ND)ND ND ND
08-Dec-08 0.1 1.0 2.1 ND ND (ND)ND ND ND
24-Jun-09 0.1 1.0 0.9 J 0.3 (ND)J ND ND ND ND
15-Dec-09 0.1 1.0 2.0 0.2 J ND (ND)ND ND ND
22-Jun-10 0.1 1.0 1.7 0.8 (0.7 J) J 0.2 J ND ND ND
02-Nov-10 0.1 1.0 1.3 ND ND (ND)ND ND ND
11-Apr-11 0.25 1.0 2.3 0.43 J 0.42 J ND ND ND
17-Oct-11 0.25 1.0 2.0 0.44 J 0.44 J ND ND ND
09-Apr-12 0.25 1.0 2.2 ND ND ND ND ND
15-Oct-12 0.25 1.0 2.4 ND ND ND ND ND
15-Apr-13 0.25 1.0 2.0 0.62 J ND ND ND ND
07-Oct-13 0.25 1.0 ND 0.88 J 0.33 J ND ND ND
28-Apr-14 0.25 1.0 2.5 0.99 J ND ND ND ND
13-Oct-14 0.25 1.0 2.3 0.63 J 0.49 J ND ND ND
08-Apr-15 0.25 1.0 2.2 ND ND ND ND ND
26-Oct-15 0.25 1.0 2.2 ND 0.39 J ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 13 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Carbon Disulfide Sep-93 NR 100 ND ND ND ND ND ND
Oct-94 NR 100 ND ND ND ND ND ND
Apr-95 NR 100 ND ND ND ND ND ND
Nov-95 NR 100 ND ND ND ND ND ND
May-96 NR 100 ND ND ND ND ND ND
Nov-96 NR 100 ND ND ND ND ND ND
Mar-97 NR 100 ND 14.9 ND ND ND ND
Sep-97 NR 100 ND ND ND ND ND ND
Mar-98 NR 100 ND ND ND ND ND ND
Sep-98 NR 100 ND ND ND ND ND ND
Mar-99 NR 100 ND ND ND ND ND ND
Sep-99 NR 100 ND ND ND ND ND ND
Apr-00 NR 100 ND ND ND ND ND ND
Sep-00 NR 100 ND ND ND ND ND ND
Mar-01 NR 100 ND ND ND ND ND ND
Oct-01 NR 100 ND ND ND ND ND ND
Apr-02 NR 100 ND ND ND ND ND ND
Nov-02 NR 100 ND ND ND ND ND ND
May-03 NR 100 ND ND ND ND ND ND
Nov-03 NR 100 ND ND ND ND ND ND
May-04 NR 100 ND ND ND ND ND ND
Nov-04 NR 100 ND ND ND ND ND ND
May-05 NR 100 ND ND ND ND ND ND
Nov-05 NR 100 ND ND ND ND ND ND
29-Jun-06 NR 100 ND ND ND ND ND ND
20-Dec-06 NR 100 ND ND ND ND ND ND
28-Jun-07 0.5 100 22.7 J 9.8 J 25.4 J (1.9 J)ND 1.1 J ND
NC 2L = 700 µg/L (10/23/07)27-Dec-07 0.5 100 2.9 J 3.0 J ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.5 100 ND 4.0 J ND (5.3 J)ND ND ND
08-Dec-08 0.5 100 7.4 J 0.7 J ND (ND)ND ND ND
24-Jun-09 0.5 100 ND ND (ND)ND ND ND ND
15-Dec-09 0.5 100 ND 1.6 J ND (ND)ND ND ND
22-Jun-10 0.5 100 ND ND (ND)ND ND ND ND
02-Nov-10 0.5 100 ND ND ND (ND)ND ND ND
11-Apr-11 1.2 100 ND ND ND ND ND ND
17-Oct-11 1.2 100 ND ND ND ND ND ND
09-Apr-12 1.2 100 ND ND ND ND ND ND
15-Oct-12 1.2 100 ND ND ND ND ND ND
15-Apr-13 1.2 100 ND ND ND ND ND ND
07-Oct-13 1.2 100 ND ND ND ND ND ND
28-Apr-14 1.2 100 ND ND ND ND ND ND
13-Oct-14 1.2 100 ND ND ND ND ND ND
08-Apr-15 1.2 100 ND ND ND ND ND ND
26-Oct-15 1.2 100 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 14 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Chlorobenzene Sep-93 NR 5 ND ND ND ND ND ND
Oct-94 NR 5 ND ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 ND ND ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND 5.0(5.6)ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND 1.7 J (1.5 J)ND ND ND ND
28-Jun-07 0.1 3.0 ND 2.1 J ND ND ND ND
NC 2L = 50 µg/L (10/23/07)27-Dec-07 0.1 3.0 0.4 J 1.7 J ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 3.0 0.5 J 1.0 J ND (0.9 J)ND ND ND
08-Dec-08 0.1 3.0 0.3 J ND ND (ND)ND ND ND
24-Jun-09 0.1 3.0 ND 2.3 (2.0 J)J ND ND ND ND
15-Dec-09 0.1 3.0 ND 1.1 J ND (ND)ND ND ND
22-Jun-10 0.1 3.0 ND 2.4 (2.4 J)J ND ND ND ND
02-Nov-10 0.1 3.0 ND 1.1 J ND (ND)ND ND ND
11-Apr-11 0.23 3.0 0.31 J 2.4 J 0.46 J ND ND ND
17-Oct-11 0.23 3.0 0.33 J 2.1 J 0.47 J ND ND ND
09-Apr-12 0.23 3.0 0.32 B 0.91 B 0.24 B ND ND 0.30 J
15-Oct-12 0.23 3.0 0.29 J 1.6 J 0.28 J ND ND ND
15-Apr-13 0.23 3.0 0.29 J 2.5 J ND ND ND ND
07-Oct-13 0.23 3.0 0.26 J 2.8 J 0.26 J ND ND ND
28-Apr-14 0.23 3.0 0.35 J 2.8 J ND ND ND ND
13-Oct-14 0.23 3.0 0.25 J 2.7 J 0.24 J ND ND ND
08-Apr-15 0.23 3.0 0.29 J 0.80 J ND ND ND ND
26-Oct-15 0.23 3.0 0.29 J 0.96 J ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 15 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Chloroethane Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 10 ND ND ND ND ND ND
Apr-95 NR 10 ND ND ND ND ND ND
Nov-95 NR 10 ND ND ND ND ND ND
May-96 NR 10 ND ND ND ND ND ND
Nov-96 NR 10 ND ND ND ND ND ND
Mar-97 NR 10 17 ND ND ND ND ND
Sep-97 NR 10 36 ND ND ND ND ND
Mar-98 NR 10 28 ND ND ND ND ND
Sep-98 NR 10 26 ND ND ND ND ND
Mar-99 NR 10 25 ND ND ND ND ND
Sep-99 NR 10 27 ND ND ND ND ND
Apr-00 NR 10 22 ND ND ND ND ND
Sep-00 NR 10 ND ND ND ND ND ND
Mar-01 NR 10 23 ND ND ND ND ND
Oct-01 NR 10 40 ND ND ND ND ND
Apr-02 NR 10 16 ND ND ND ND ND
Nov-02 NR 10 ND ND ND ND ND ND
May-03 NR 10 ND ND ND ND ND ND
Nov-03 NR 10 17 ND ND ND ND ND
May-04 NR 10 14 ND ND ND ND ND
Nov-04 NR 10 ND ND ND ND ND ND
May-05 NR 10 ND ND ND ND ND ND
Nov-05 NR 10 ND ND ND ND ND ND
29-Jun-06 NR 10 ND ND ND ND ND ND
20-Dec-06 NR 10 8.4 J ND ND ND ND ND
28-Jun-07 0.1 10.0 54.2 10.8 3.0 J (3.2 J)ND ND ND
NC 2L = 2,800 µg/L (10/23/07)27-Dec-07 0.1 10.0 5.3 J 1.9 J 0.4 (0.3 J)J ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 10.0 5.8 J 0.9 J ND (0.7 J)ND ND ND
08-Dec-08 0.1 10.0 5.9 J ND 0.3 (0.3 J)J ND ND ND
24-Jun-09 0.1 10.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.1 10.0 4.3 J 0.9 J ND (ND)ND ND ND
NC 2L = 3,000 µg/L (01/01/10)22-Jun-10 0.1 10.0 4.9 J 2.1 (1.9 J)J 0.3 J ND ND ND
02-Nov-10 0.1 10.0 2.5 J 0.4 J ND (ND)ND ND ND
11-Apr-11 0.54 10.0 3.2 J 0.99 J ND ND ND ND
17-Oct-11 0.54 10.0 3.0 J 0.89 J ND ND ND ND
09-Apr-12 0.54 10.0 3.4 J ND ND ND ND ND
15-Oct-12 0.54 10.0 3.8 J 0.62 J ND ND ND ND
15-Apr-13 0.54 10.0 5.0 J ND ND ND ND ND
07-Oct-13 0.54 10.0 4.2 J 0.80 J ND ND ND ND
28-Apr-14 0.54 10.0 4.5 J 0.82 J ND ND ND ND
13-Oct-14 0.54 10.0 ND ND ND ND ND ND
08-Apr-15 0.54 10.0 0.74 J ND ND ND ND ND
26-Oct-15 0.54 10.0 3.4 J ND ND ND ND ND
Chloromethane 17-Oct-11 0.11 1.0 0.11 J 0.12 J ND ND ND ND
NC 2L = 3 µg/L (01/01/10)09-Apr-12 0.11 1.0 ND ND ND ND ND ND
NC 2B = NE (05/01/07)15-Oct-12 0.11 1.0 ND ND ND ND ND ND
15-Apr-13 0.11 1.0 ND ND ND ND ND ND
07-Oct-13 0.11 1.0 ND ND ND ND ND ND
28-Apr-14 0.11 1.0 ND ND ND ND ND ND
13-Oct-14 0.11 1.0 0.17 J ND ND ND ND ND
08-Apr-15 0.11 1.0 ND ND ND ND ND ND
26-Oct-15 0.11 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 16 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
1,2-Dichlorobenzene Sep-93 NR 5 ND ND ND ND ND ND
Oct-94 NR 5 ND ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 ND ND ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND 5.0(5.3)ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND ND ND ND ND ND
28-Jun-07 0.1 5.0 ND 1.3 J ND ND ND ND
NC 2L = 24 µg/L (10/23/07)27-Dec-07 0.1 5.0 ND 1.1 J ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 5.0 ND 0.5 J ND (0.5 J)ND ND ND
08-Dec-08 0.1 5.0 ND ND ND (ND)ND ND ND
24-Jun-09 0.1 5.0 ND 0.5 (0.4 J)J ND ND ND ND
15-Dec-09 0.1 5.0 ND 0.7 J ND (ND)ND ND ND
NC 2L = 20 µg/L (01/01/10)22-Jun-10 0.1 5.0 ND 1.7 (1.7 J)J ND ND ND ND
02-Nov-10 0.1 5.0 ND 0.6 J ND (ND)ND ND ND
11-Apr-11 0.30 5.0 ND 1.1 J ND ND ND ND
17-Oct-11 0.30 5.0 ND 1.1 J ND ND ND ND
09-Apr-12 0.30 5.0 ND 0.43 J ND ND ND ND
15-Oct-12 0.30 5.0 ND 0.99 J ND ND ND ND
15-Apr-13 0.30 5.0 ND 0.65 J ND ND ND ND
07-Oct-13 0.30 5.0 ND 1.3 J ND ND ND ND
28-Apr-14 0.30 5.0 ND 1.2 J ND ND ND ND
13-Oct-14 0.30 5.0 ND 1.2 J ND ND ND ND
08-Apr-15 0.30 5.0 ND ND ND ND ND ND
26-Oct-15 0.30 5.0 ND 0.42 J ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 17 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
1,4-Dichlorobenzene Sep-93 NR NR NS NS NS NS NS NA
Oct-94 NR 5 ND 10 14 ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 5 16 ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND 5 ND ND ND
Mar-97 NR 5 ND 5 ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND 6.8 ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND 7.3 ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND 5.4(5.5)ND ND ND ND
Nov-03 NR 5 ND 7.5 ND ND ND ND
May-04 NR 5 ND 9.5(5.0)ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 6.5 5.0(6.3)6.5 ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND 6.4 5.7 ND ND ND
20-Dec-06 NR 5 4.6 J 4.3 J (3.8 J)4.2 J ND ND ND
28-Jun-07 0.1 1.0 3.8 5.5 4.7 (5.2)ND ND ND
NC 2L = 1.4 µg/L (10/23/07)27-Dec-07 0.1 1.0 4.6 5.1 1.9 (1.8)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 1.0 5.2 2.2 2.7 (2.2)ND ND ND
08-Dec-08 0.1 1.0 5.0 1.1 1.8 (1.8)ND ND ND
24-Jun-09 0.1 1.0 2.1 2.6 (2.2)1.1 ND ND ND
15-Dec-09 0.1 1.0 2.7 3.3 ND (ND)ND ND ND
NC 2L = 6 µg/L (01/01/10)22-Jun-10 0.1 1.0 1.9 8.0 (7.8)2.4 ND ND ND
02-Nov-10 0.1 1.0 2.2 3.3 0.6 (0.6 J)J ND ND ND
11-Apr-11 0.33 1.0 ND ND ND ND ND ND
17-Oct-11 0.33 1.0 3.3 7.1 4.1 ND ND ND
09-Apr-12 0.33 1.0 2.5 2.6 2.4 ND ND ND
15-Oct-12 0.33 1.0 1.8 5.3 2.0 ND ND ND
15-Apr-13 0.33 1.0 3.3 4.9 1.7 ND ND ND
07-Oct-13 0.33 1.0 2.5 8.5 4.7 ND ND ND
28-Apr-14 0.33 1.0 3.3 8.2 4.0 ND ND ND
13-Oct-14 0.33 1.0 2.1 8.9 8.4 ND ND ND
08-Apr-15 0.33 1.0 3.0 2.4 4.4 ND ND ND
26-Oct-15 0.33 1.0 2.4 3.3 5.2 ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 18 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
1,1-Dichloroethane Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 5 35 22 ND ND ND ND
Apr-95 NR 5 15 10 ND ND ND ND
Nov-95 NR 5 14 9 ND ND ND ND
May-96 NR 5 11 ND ND ND ND ND
Nov-96 NR 5 11 6 ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 9 ND ND ND ND ND
Mar-98 NR 5 5 ND ND ND ND ND
Sep-98 NR 5 5 ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 5.7 ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 5.7 ND ND ND ND ND
May-04 NR 5 6.3 ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 1.6 J ND ND ND ND ND
28-Jun-07 0.2 5.0 2.5 J ND 0.8 J (0.9 J)ND ND ND
NC 2L = 70 µg/L (10/23/07)27-Dec-07 0.2 5.0 1.3 J 0.3 J 0.5 (0.5 J)J ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.2 5.0 1.5 J ND 0.7 (ND)J ND ND ND
08-Dec-08 0.2 5.0 1.3 J 0.3 J 0.5 (0.6 J)J ND ND ND
24-Jun-09 0.2 5.0 0.7 J ND ( ND)ND ND ND ND
15-Dec-09 0.2 5.0 1.6 J ND ND (ND)ND ND ND
NC 2L = 6 µg/L (01/01/10)22-Jun-10 0.2 5.0 ND 0.4 (0.4 J)J 0.3 J ND ND ND
02-Nov-10 0.2 5.0 0.7 J ND ND (ND)ND ND ND
11-Apr-11 0.32 5.0 ND ND 0.57 J ND ND ND
17-Oct-11 0.32 5.0 1.2 J ND 0.57 J ND ND ND
09-Apr-12 0.32 5.0 1.6 J ND ND ND ND ND
15-Oct-12 0.32 5.0 1.9 J ND ND ND ND ND
15-Apr-13 0.32 5.0 0.69 J ND ND ND ND ND
07-Oct-13 0.32 5.0 1.1 J ND ND ND ND ND
28-Apr-14 0.32 5.0 0.82 J ND ND ND ND ND
13-Oct-14 0.32 5.0 1.3 J ND 0.34 J ND ND ND
08-Apr-15 0.32 5.0 0.93 J ND ND ND ND ND
26-Oct-15 0.32 5.0 0.99 J ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 19 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Cis-1,2-Dichloroethene Oct-94 NR 5 12 14 11 ND ND ND
Apr-95 NR 5 6 ND ND ND ND ND
Nov-95 NR 5 7 ND ND ND ND ND
May-96 NR 5 8 5 ND ND ND ND
Nov-96 NR 5 7 ND ND ND ND ND
Mar-97 NR 5 9 7 ND ND ND ND
Sep-97 NR 5 9 7 ND ND ND ND
Mar-98 NR 5 10 8 ND ND ND ND
Sep-98 NR 5 9 7 ND ND ND ND
Mar-99 NR 5 12 6(8)ND ND ND ND
Sep-99 NR 5 16 9.2 ND ND ND ND
Apr-00 NR 5 13 ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 18 ND ND ND ND ND
Oct-01 NR 5 24 12 ND ND ND ND
Apr-02 NR 5 18 ND ND ND ND ND
Nov-02 NR 5 23 ND ND ND ND ND
May-03 NR 5 7.9 5.6(6.7)ND ND ND ND
Nov-03 NR 5 10 7.8 ND ND ND ND
May-04 NR 5 12 6.5(5.3)ND ND ND ND
Nov-04 NR 5 11 ND ND ND ND ND
May-05 NR 5 8.2 5.7(7.3)ND ND ND ND
Nov-05 NR 5 14 7.4 ND ND ND ND
29-Jun-06 NR 5 10(10)ND ND ND ND ND
20-Dec-06 NR 5 17 4.4 J(4.1 J)2.1 J ND ND ND
28-Jun-07 0.1 5.0 16.1 6.2 3.0 J (3.2 J)ND ND ND
NC 2L = 70 µg/L (10/23/07)27-Dec-07 0.1 5.0 11.9 5.3 1.8 (1.6 J)J ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 5.0 13.0 2.4 J 1.9 (2.2 J)J ND ND ND
08-Dec-08 0.1 5.0 10.9 1.0 J 1.6 ( 1.5 J)J ND ND ND
24-Jun-09 0.1 5.0 5.2 2.0 (1.7 J)J 0.6 J ND ND ND
15-Dec-09 0.1 5.0 8.7 3.0 J ND (0.3 J)ND ND ND
22-Jun-10 0.1 5.0 8.0 6.4 (6.2)1.2 J ND ND ND
02-Nov-10 0.1 5.0 6.6 2.3 J 0.4 (0.4 J)J ND ND ND
11-Apr-11 0.19 5.0 10.8 4.5 J 2.0 J ND ND ND
17-Oct-11 0.19 5.0 9.7 5.1 2.6 J ND ND ND
09-Apr-12 0.19 5.0 11.2 1.8 J 1.3 J ND ND ND
15-Oct-12 0.19 5.0 11.1 3.8 J 1.3 J ND ND ND
15-Apr-13 0.19 5.0 8.5 2.6 J 0.89 J ND ND ND
07-Oct-13 0.19 5.0 9.3 4.9 J 1.8 J ND ND ND
28-Apr-14 0.19 5.0 8.3 3.6 J 1.1 J ND ND ND
13-Oct-14 0.19 5.0 9.4 4.3 J 1.8 J ND ND ND
08-Apr-15 0.19 5.0 9.2 1.3 J 1.1 J ND ND ND
26-Oct-15 0.19 5.0 7.8 1.5 J 1.2 J ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 20 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Methylene Chloride Sep-93 NR NR 40 ND 23 ND ND ND
(Dichloromethane)Oct-94 NR 10 98 ND 32 ND ND ND
Apr-95 NR 10 36 ND 11 ND ND ND
Nov-95 NR 10 13 ND ND ND ND ND
May-96 NR 10 22 ND ND ND ND ND
Nov-96 NR 10 ND ND ND ND ND ND
Mar-97 NR 10 15 ND ND ND ND ND
Sep-97 NR 10 27 ND ND ND ND ND
Mar-98 NR 10 21 ND ND ND ND ND
Sep-98 NR 10 17 ND ND ND ND ND
Mar-99 NR 10 15 ND ND ND ND ND
Sep-99 NR 10 16 ND ND ND ND ND
Apr-00 NR 10 12 ND ND ND ND ND
Sep-00 NR 10 ND ND ND ND ND ND
Mar-01 NR 10 17 ND ND ND ND ND
Oct-01 NR 10 17 ND ND ND ND ND
Apr-02 NR 10 13 ND ND ND ND ND
Nov-02 NR 10 ND ND ND ND ND ND
May-03 NR 10 ND ND ND ND ND ND
Nov-03 NR 10 17 ND ND ND ND ND
May-04 NR 10 16 ND ND ND ND ND
Nov-04 NR 10 ND ND ND ND ND ND
May-05 NR 10 ND ND ND ND ND ND
Nov-05 NR 10 ND ND ND ND ND ND
29-Jun-06 NR 10 ND ND ND ND ND ND
20-Dec-06 NR 5 ND 1.4 J (ND)ND ND ND ND
28-Jun-07 0.6 1.0 ND ND ND ND ND ND
NC 2L = 4.6 µg/L (10/23/07)27-Dec-07 0.6 1.0 2.3 B ND ND (ND)ND ND 0.7 J
NC 2B = NE (05/01/07)28-Apr-08 0.6 1.0 1.8 ND ND (ND)ND ND ND
08-Dec-08 0.6 1.0 1.4 ND ND (ND)ND ND ND
24-Jun-09 0.6 1.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.6 1.0 ND ND ND (ND)ND ND ND
NC 2L = 5 µg/L (01/01/10)22-Jun-10 0.6 1.0 ND ND (ND)ND ND ND ND
02-Nov-10 0.6 1.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.97 1.0 ND ND ND ND ND ND
17-Oct-11 0.97 1.0 ND ND ND ND ND ND
09-Apr-12 0.97 1.0 ND ND ND ND ND ND
15-Oct-12 0.97 1.0 ND ND ND ND ND ND
15-Apr-13 0.97 1.0 ND ND ND ND ND ND
07-Oct-13 0.97 1.0 ND ND ND ND ND 1.4
28-Apr-14 0.97 1.0 ND ND ND ND ND ND
13-Oct-14 0.97 1.0 ND ND ND ND ND 1.3
08-Apr-15 0.97 1.0 ND ND ND ND ND ND
26-Oct-15 0.97 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 21 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Tetrachloroethene Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 5 5 ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 6 ND ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
26-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND ND ND ND ND ND
28-Jun-07 0.2 1.0 0.9 J ND ND ND ND ND
NC 2L = 0.7 µg/L (10/23/07)27-Dec-07 0.2 1.0 0.3 J ND ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.2 1.0 0.4 J ND ND (ND)ND ND ND
08-Dec-08 0.2 1.0 ND ND ND (ND)ND ND ND
24-Jun-09 0.2 1.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.2 1.0 0.4 J ND ND (ND)ND ND ND
22-Jun-10 0.2 1.0 0.4 J ND (ND)ND ND ND ND
02-Nov-10 0.2 1.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.46 1.0 0.75 J ND ND ND ND ND
17-Oct-11 0.46 1.0 0.59 J ND ND ND ND ND
09-Apr-12 0.46 1.0 0.70 J ND ND ND ND ND
15-Oct-12 0.46 1.0 0.67 J ND ND ND ND ND
15-Apr-13 0.46 1.0 ND ND ND ND ND ND
07-Oct-13 0.46 1.0 0.57 J ND ND ND ND ND
28-Apr-14 0.46 1.0 ND ND ND ND ND ND
13-Oct-14 0.46 1.0 0.54 J ND ND ND ND ND
08-Apr-15 0.46 1.0 ND ND ND ND ND ND
26-Oct-15 0.46 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 22 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Toluene Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 5 ND ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 ND 57 ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
DUP NR 5 NS NS ND NS NS NS
Mar-99 NR 5 ND ND ND ND ND ND
DUP NR 5 NS ND NS NS NS NS
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND 23 ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND 10(6.9)ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND ND ND ND ND ND
28-Jun-07 0.3 1.0 ND ND ND ND ND ND
NC 2L = 1,000 µg/L (10/23/07)27-Dec-07 0.3 1.0 ND ND ND (ND)ND ND ND
NC 2B = 11 µg/L (05/01/07)28-Apr-08 0.3 1.0 ND ND ND (ND)ND ND ND
08-Dec-08 0.3 1.0 ND ND ND (ND)ND ND ND
24-Jun-09 0.3 1.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.3 1.0 ND ND ND (ND)ND ND ND
NC 2L = 600 µg/L (01/01/10)22-Jun-10 0.3 1.0 ND ND (ND)ND ND ND ND
02-Nov-10 0.3 1.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.26 1.0 ND ND ND ND ND ND
17-Oct-11 0.26 1.0 ND ND ND ND ND ND
09-Apr-12 0.26 1.0 ND ND ND ND ND ND
15-Oct-12 0.26 1.0 ND ND ND ND ND ND
15-Apr-13 0.26 1.0 ND ND ND ND ND ND
07-Oct-13 0.26 1.0 ND ND ND ND ND ND
28-Apr-14 0.26 1.0 ND ND ND ND ND ND
13-Oct-14 0.26 1.0 ND ND ND ND ND ND
08-Apr-15 0.26 1.0 ND ND ND ND ND ND
26-Oct-15 0.26 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 23 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
1,1,1-Trichloroethane Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 5 6 ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 ND ND ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
26-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND ND ND ND ND ND
28-Jun-07 0.1 1.0 ND ND ND ND ND ND
NC 2L = 200 µg/L (10/23/07)27-Dec-07 0.1 1.0 ND ND ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 1.0 ND ND ND (ND)ND ND ND
08-Dec-08 0.1 1.0 ND ND ND (ND)ND ND ND
24-Jun-09 0.1 1.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.1 1.0 ND ND ND (ND)ND ND ND
22-Jun-10 0.1 1.0 ND ND (ND)ND ND ND ND
02-Nov-10 0.1 1.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.48 1.0 ND ND ND ND ND ND
17-Oct-11 0.48 1.0 ND ND ND ND ND ND
09-Apr-12 0.48 1.0 ND ND ND ND ND ND
15-Oct-12 0.48 1.0 ND ND ND ND ND ND
15-Apr-13 0.48 1.0 ND ND ND ND ND ND
07-Oct-13 0.48 1.0 ND ND ND ND ND ND
28-Apr-14 0.48 1.0 ND ND ND ND ND ND
13-Oct-14 0.48 1.0 ND ND ND ND ND ND
08-Apr-15 0.48 1.0 ND ND ND ND ND ND
26-Oct-15 0.48 1.0 ND ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 24 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Trichloroethene Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 5 ND ND ND ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 9 8 ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 6 ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND ND ND ND ND ND
28-Jun-07 0.1 1.0 1.5 ND ND ND ND ND
NC 2L = 2.8 µg/L (10/23/07)27-Dec-07 0.1 1.0 0.7 J ND ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 1.0 0.7 J ND ND (ND)ND ND ND
08-Dec-08 0.1 1.0 0.6 J ND ND (ND)ND ND ND
24-Jun-09 0.1 1.0 0.4 J ND (ND)ND ND ND ND
15-Dec-09 0.1 1.0 0.8 J ND ND (ND)ND ND ND
NC 2L = 3µg/L (01/01/10)22-Jun-10 0.1 1.0 0.7 J ND (ND)ND ND ND ND
02-Nov-10 0.1 1.0 0.5 J ND ND (ND)ND ND ND
11-Apr-11 0.47 1.0 1.0 ND ND ND ND ND
17-Oct-11 0.47 1.0 0.79 J ND ND ND ND ND
09-Apr-12 0.47 1.0 1.1 ND ND ND ND ND
15-Oct-12 0.47 1.0 1.3 ND ND ND ND ND
15-Apr-13 0.47 1.0 0.63 J ND ND ND ND ND
07-Oct-13 0.47 1.0 0.81 J ND ND ND ND ND
28-Apr-14 0.47 1.0 0.87 J ND ND ND ND ND
13-Oct-14 0.47 1.0 1.0 ND ND ND ND ND
08-Apr-15 0.47 1.0 0.68 J ND ND ND ND ND
26-Oct-15 0.47 1.0 0.81 J ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 25 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Vinyl Acetate 27-Dec-07 0.2 50.0 11.9 J ND ND (ND)ND ND ND
GWPS = 7,000 µg/L (10/23/07)28-Apr-08 0.2 50.0 ND ND ND (ND)ND ND ND
NC 2B = NE (05/01/07)08-Dec-08 0.2 50.0 ND ND ND (ND)ND ND ND
24-Jun-09 0.2 50.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.2 50.0 ND ND ND (ND)ND ND ND
22-Jun-10 0.2 50.0 ND ND (ND)ND ND ND ND
GWPS = 88 µg/L (10/1/10)02-Nov-10 0.2 50.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.35 50.0 ND ND ND ND ND ND
17-Oct-11 0.35 50.0 ND ND ND ND ND ND
09-Apr-12 0.35 50.0 ND ND ND ND ND ND
15-Oct-12 0.35 50.0 ND ND ND ND ND ND
15-Apr-13 0.35 50.0 ND ND ND ND ND ND
07-Oct-13 0.35 50.0 ND ND ND ND ND ND
28-Apr-14 0.35 50.0 ND ND ND ND ND ND
13-Oct-14 0.35 50.0 ND ND ND ND ND ND
08-Apr-15 0.35 50.0 ND ND ND ND ND ND
26-Oct-15 0.35 50.0 ND ND ND ND ND ND
Vinyl Chloride 28-Jun-07 0.1 1.0 1.9 0.5 J ND ND ND ND
NC 2L = 0.015 µg/L (10/23/07)27-Dec-07 0.1 1.0 0.8 J 0.3 J ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.1 1.0 ND ND ND (ND)ND ND ND
08-Dec-08 0.1 1.0 1.3 ND ND (ND)ND ND ND
24-Jun-09 0.1 1.0 0.4 J ND (ND)ND ND ND ND
15-Dec-09 0.1 1.0 0.8 J ND ND (ND)ND ND ND
NC 2L = 0.03 µg/L (01/01/10)22-Jun-10 0.1 1.0 ND ND (ND)ND ND ND ND
02-Nov-10 0.1 1.0 0.6 J ND ND (ND)ND ND ND
11-Apr-11 0.62 1.0 0.92 J ND ND ND ND ND
17-Oct-11 0.62 1.0 1.0 ND ND ND ND ND
09-Apr-12 0.62 1.0 1.6 ND ND ND ND ND
15-Oct-12 0.62 1.0 1.7 ND ND ND ND ND
15-Apr-13 0.62 1.0 1.4 ND ND ND ND ND
07-Oct-13 0.62 1.0 1.7 ND ND ND ND ND
28-Apr-14 0.62 1.0 1.4 ND ND ND ND ND
13-Oct-14 0.62 1.0 1.6 ND ND ND ND ND
08-Apr-15 0.62 1.0 1.9 ND ND ND ND ND
26-Oct-15 0.62 1.0 1.7 ND ND ND ND ND
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 26 of 27 Joyce Engineering
TABLE 1
Summary of Historically Detected Constituents
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 Upstream Downstream Blanks
Xylene (Total)Sep-93 NR NR ND ND ND ND ND ND
Oct-94 NR 5 7 ND 6 ND ND ND
Apr-95 NR 5 ND ND ND ND ND ND
Nov-95 NR 5 6 ND ND ND ND ND
May-96 NR 5 ND ND ND ND ND ND
Nov-96 NR 5 ND ND ND ND ND ND
Mar-97 NR 5 ND ND ND ND ND ND
Sep-97 NR 5 ND ND ND ND ND ND
Mar-98 NR 5 ND ND ND ND ND ND
Sep-98 NR 5 ND ND ND ND ND ND
Mar-99 NR 5 ND ND ND ND ND ND
Sep-99 NR 5 ND ND ND ND ND ND
Apr-00 NR 5 ND ND ND ND ND ND
Sep-00 NR 5 ND ND ND ND ND ND
Mar-01 NR 5 ND ND ND ND ND ND
Oct-01 NR 5 ND ND ND ND ND ND
Apr-02 NR 5 ND ND ND ND ND ND
Nov-02 NR 5 ND ND ND ND ND ND
May-03 NR 5 ND ND ND ND ND ND
Nov-03 NR 5 ND ND ND ND ND ND
May-04 NR 5 ND ND ND ND ND ND
Nov-04 NR 5 ND ND ND ND ND ND
May-05 NR 5 ND ND ND ND ND ND
Nov-05 NR 5 ND ND ND ND ND ND
29-Jun-06 NR 5 ND ND ND ND ND ND
20-Dec-06 NR 5 ND ND ND ND ND ND
28-Jun-07 0.3 4.0 ND ND ND ND ND ND
NC 2L = 530 µg/L (10/23/07)27-Dec-07 0.3 4.0 ND ND ND (ND)ND ND ND
NC 2B = NE (05/01/07)28-Apr-08 0.3 4.0 ND ND ND (ND)ND ND ND
08-Dec-08 0.3 4.0 ND ND ND (ND)ND ND ND
24-Jun-09 0.3 4.0 ND ND (ND)ND ND ND ND
15-Dec-09 0.3 5.0 ND ND ND (ND)ND ND ND
NC 2L = 300 µg/L (01/01/10)22-Jun-10 0.3 5.0 ND ND (ND)ND ND ND ND
02-Nov-10 0.3 5.0 ND ND ND (ND)ND ND ND
11-Apr-11 0.66 2.0 ND ND ND ND ND ND
17-Oct-11 0.66 2.0 ND ND ND ND ND ND
09-Apr-12 0.66 2.0 ND ND ND ND ND ND
15-Oct-12 0.66 5.0 ND ND ND ND ND ND
15-Apr-13 0.66 5.0 ND ND ND ND ND ND
07-Oct-13 0.66 5.0 ND ND ND ND ND ND
28-Apr-14 0.66 5.0 ND ND ND ND ND ND
13-Oct-14 0.66 5.0 ND ND ND ND ND ND
08-Apr-15 0.66 5.0 ND ND ND ND ND ND
26-Oct-15 0.66 5.0 ND ND ND ND ND ND
Notes:
All concentrations are reported in micrograms per liter (mg/L).
Values shown in parentheses are from duplicate samples.
MW = Groundwater monitoring well.
DL = Laboratory detection limit.
QL = Laboratory reporting limit ( NC SWSL {or lower} From June 2007 to present).
B = Reported detect considered to represent blank contamination.
NS = Not sampled.
NR = Not reported.
NA = Not available.
NC 2L = North Carolina's groundwater quality Standard established under 15A NCAC 2L, .0202.
J = Estimate concetrations.
GWPS = Groundwater Protection Standards.
NC 2B = North Carolina Surface Water Standard.
Boldvalues are above the NC 2L, GWPS, or NC 2B.
NE = Not established.
Wilkes County Dan Johnson Landfill
Permit No. 97-02 page 27 of 27 Joyce Engineering
TABLE 2
Summary of Historical Groundwater Elevations
Location MW-1 MW-2 MW-3
TOC Elevation 1199.50 1188.00 1188.00
Well Depth 60.12 40.08 64.00
Apr-13 1167.85 1159.08 1178.50
Oct-13 1170.00 1156.20 1178.10
Apr-14 1167.60 1159.70 1178.50
Oct-14 1166.22 1156.17 1177.70
Apr-15 1167.41 1156.45 1177.94
Oct-15 1166.75 1155.55 1177.65
Notes:
TOC= Top of casing
Wilkes County Roaring River Landfill
Permit No. 97-04 Joyce Engineering

Figure

Drawing

Appendices
Appendix 1 Laboratory Analytical Reports and Field Data Logs
Appendix 2 Summary of Detections, Exceedances, and Field Parameters
Appendix 3 Horizontal Groundwater Flow Velocities

Appendix 1
Laboratory Analytical Reports and Field Data Logs
#=CL#
November 06, 2015
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92273639
92273639
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
WILKES-DAN JOHNSON 356.1501.12
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on October 28, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Lab ID Sample ID Matrix Date Collected Date Received
92273639001 9702-MW1 Water 10/26/15 10:23 10/28/15 10:10
92273639002 9702-MW2 Water 10/26/15 11:15 10/28/15 10:10
92273639003 9702-MW3 Water 10/26/15 10:50 10/28/15 10:10
92273639004 9702-UPSTREAM Water 10/26/15 11:20 10/28/15 10:10
92273639005 9702-DOWNSTREAM Water 10/26/15 10:47 10/28/15 10:10
92273639006 9702-FIELD BLANK Water 10/26/15 11:30 10/28/15 10:10
92273639007 9702-TRIP BLANK Water 10/26/15 08:00 10/28/15 10:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92273639001 9702-MW1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92273639002 9702-MW2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92273639003 9702-MW3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92273639004 9702-UPSTREAM EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92273639005 9702-DOWNSTREAM EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92273639006 9702-FIELD BLANK EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92273639007 9702-TRIP BLANK EPA 8260 50 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92273639001 9702-MW1
Barium 34.5J ug/L 11/05/15 17:44500EPA 6010
Cobalt 59.2 ug/L 11/05/15 17:4450.0EPA 6010
Benzene 2.2 ug/L 11/01/15 07:021.0EPA 8260
Chlorobenzene 0.29J ug/L 11/01/15 07:023.0EPA 8260
Chloroethane 3.4J ug/L 11/01/15 07:0210.0EPA 8260
1,4-Dichlorobenzene 2.4 ug/L 11/01/15 07:021.0EPA 8260
1,1-Dichloroethane 0.99J ug/L 11/01/15 07:025.0EPA 8260
cis-1,2-Dichloroethene 7.8 ug/L 11/01/15 07:025.0EPA 8260
Trichloroethene 0.81J ug/L 11/01/15 07:021.0EPA 8260
Vinyl chloride 1.7 ug/L 11/01/15 07:021.0EPA 8260
92273639002 9702-MW2
Barium 92.9J ug/L 11/05/15 01:44100EPA 6010
Cobalt 32.4 ug/L 11/05/15 01:4410.0EPA 6010
Nickel 7.2J ug/L 11/05/15 01:4450.0EPA 6010
Vanadium 6.2J ug/L 11/05/15 01:4425.0EPA 6010
Zinc 70.1 ug/L 11/05/15 01:4410.0EPA 6010
Chlorobenzene 0.96J ug/L 11/01/15 07:183.0EPA 8260
1,2-Dichlorobenzene 0.42J ug/L 11/01/15 07:185.0EPA 8260
1,4-Dichlorobenzene 3.3 ug/L 11/01/15 07:181.0EPA 8260
cis-1,2-Dichloroethene 1.5J ug/L 11/01/15 07:185.0EPA 8260
92273639003 9702-MW3
Barium 104 ug/L 11/05/15 01:47100EPA 6010
Cobalt 25.3 ug/L 11/05/15 01:4710.0EPA 6010
Vanadium 4.2J ug/L 11/05/15 01:4725.0EPA 6010
Benzene 0.39J ug/L 11/01/15 07:351.0EPA 8260
1,4-Dichlorobenzene 5.2 ug/L 11/01/15 07:351.0EPA 8260
cis-1,2-Dichloroethene 1.2J ug/L 11/01/15 07:355.0EPA 8260
92273639004 9702-UPSTREAM
Barium 13.0J ug/L 11/05/15 01:50100EPA 6010
92273639005 9702-DOWNSTREAM
Barium 14.2J ug/L 11/05/15 01:53100EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-MW1 Lab ID:92273639001 Collected:10/26/15 10:23 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/05/15 17:44 7440-36-010/29/15 20:0030.0 19.0 5
Arsenic ND ug/L 11/05/15 17:44 7440-38-210/29/15 20:0050.0 12.5 5
Barium 34.5J ug/L 11/05/15 17:44 7440-39-310/29/15 20:0050012.5 5
Beryllium ND ug/L 11/05/15 17:44 7440-41-710/29/15 20:005.0 2.5 5
Cadmium ND ug/L 11/05/15 17:44 7440-43-910/29/15 20:005.0 2.5 5
Chromium ND ug/L 11/05/15 17:44 7440-47-310/29/15 20:0050.0 12.5 5
Cobalt 59.2 ug/L 11/05/15 17:44 7440-48-410/29/15 20:0050.0 12.5 5
Copper ND ug/L 11/05/15 17:44 7440-50-810/29/15 20:0050.0 12.5 5
Lead ND ug/L 11/05/15 17:44 7439-92-110/29/15 20:0050.0 12.5 5
Nickel ND ug/L 11/05/15 17:44 7440-02-010/29/15 20:0025012.5 5
Selenium ND ug/L 11/05/15 17:44 7782-49-210/29/15 20:0050.0 25.0 5
Silver ND ug/L 11/05/15 17:44 7440-22-410/29/15 20:0050.0 12.5 5
Thallium ND ug/L 11/05/15 17:44 7440-28-010/29/15 20:0027.5 25.0 5
Vanadium ND ug/L 11/05/15 17:44 7440-62-210/29/15 20:0012512.5 5
Zinc ND ug/L 11/05/15 17:44 7440-66-610/29/15 20:0050.0 25.0 5
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 07:02 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 07:02 107-13-12001.9 1
Benzene 2.2 ug/L 11/01/15 07:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 07:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 07:02 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 07:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 07:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 07:02 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 07:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 07:02 56-23-51.0 0.25 1
Chlorobenzene 0.29J ug/L 11/01/15 07:02 108-90-73.0 0.23 1
Chloroethane 3.4J ug/L 11/01/15 07:02 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 07:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 07:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 07:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 07:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 07:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 07:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/01/15 07:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.4 ug/L 11/01/15 07:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 07:02 110-57-61001.0 1
1,1-Dichloroethane 0.99J ug/L 11/01/15 07:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 07:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 07:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.8 ug/L 11/01/15 07:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 07:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 07:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 07:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 07:02 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-MW1 Lab ID:92273639001 Collected:10/26/15 10:23 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/01/15 07:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 07:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 07:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 07:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 07:02 108-10-11000.33 1
Styrene ND ug/L 11/01/15 07:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 07:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 07:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 07:02 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 07:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 07:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 07:02 79-00-51.0 0.29 1
Trichloroethene 0.81J ug/L 11/01/15 07:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 07:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 07:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 07:02 108-05-450.0 0.35 1
Vinyl chloride 1.7 ug/L 11/01/15 07:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/01/15 07:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %11/01/15 07:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/01/15 07:02 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 07:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-MW2 Lab ID:92273639002 Collected:10/26/15 11:15 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/05/15 01:44 7440-36-010/29/15 20:006.0 3.8 1
Arsenic ND ug/L 11/05/15 01:44 7440-38-210/29/15 20:0010.0 2.5 1
Barium 92.9J ug/L 11/05/15 01:44 7440-39-310/29/15 20:001002.5 1
Beryllium ND ug/L 11/05/15 01:44 7440-41-710/29/15 20:001.0 0.50 1
Cadmium ND ug/L 11/05/15 01:44 7440-43-910/29/15 20:001.0 0.50 1
Chromium ND ug/L 11/05/15 01:44 7440-47-310/29/15 20:0010.0 2.5 1
Cobalt 32.4 ug/L 11/05/15 01:44 7440-48-410/29/15 20:0010.0 2.5 1
Copper ND ug/L 11/05/15 01:44 7440-50-810/29/15 20:0010.0 2.5 1
Lead ND ug/L 11/05/15 01:44 7439-92-110/29/15 20:0010.0 2.5 1
Nickel 7.2J ug/L 11/05/15 01:44 7440-02-010/29/15 20:0050.0 2.5 1
Selenium ND ug/L 11/05/15 01:44 7782-49-210/29/15 20:0010.0 5.0 1
Silver ND ug/L 11/05/15 01:44 7440-22-410/29/15 20:0010.0 2.5 1
Thallium ND ug/L 11/05/15 01:44 7440-28-010/29/15 20:005.5 5.0 1
Vanadium 6.2J ug/L 11/05/15 01:44 7440-62-210/29/15 20:0025.0 2.5 1
Zinc 70.1 ug/L 11/05/15 01:44 7440-66-610/29/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 07:18 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 07:18 107-13-12001.9 1
Benzene ND ug/L 11/01/15 07:18 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 07:18 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 07:18 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 07:18 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 07:18 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 07:18 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 07:18 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 07:18 56-23-51.0 0.25 1
Chlorobenzene 0.96J ug/L 11/01/15 07:18 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/01/15 07:18 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 07:18 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 07:18 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 07:18 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 07:18 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 07:18 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 07:18 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.42J ug/L 11/01/15 07:18 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.3 ug/L 11/01/15 07:18 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 07:18 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/01/15 07:18 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 07:18 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 07:18 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.5J ug/L 11/01/15 07:18 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 07:18 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 07:18 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 07:18 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 07:18 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-MW2 Lab ID:92273639002 Collected:10/26/15 11:15 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/01/15 07:18 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 07:18 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 07:18 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 07:18 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 07:18 108-10-11000.33 1
Styrene ND ug/L 11/01/15 07:18 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 07:18 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 07:18 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 07:18 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 07:18 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 07:18 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 07:18 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/01/15 07:18 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 07:18 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 07:18 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 07:18 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/01/15 07:18 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/01/15 07:18 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %11/01/15 07:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/01/15 07:18 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 07:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-MW3 Lab ID:92273639003 Collected:10/26/15 10:50 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/05/15 01:47 7440-36-010/29/15 20:006.0 3.8 1
Arsenic ND ug/L 11/05/15 01:47 7440-38-210/29/15 20:0010.0 2.5 1
Barium 104 ug/L 11/05/15 01:47 7440-39-310/29/15 20:001002.5 1
Beryllium ND ug/L 11/05/15 01:47 7440-41-710/29/15 20:001.0 0.50 1
Cadmium ND ug/L 11/05/15 01:47 7440-43-910/29/15 20:001.0 0.50 1
Chromium ND ug/L 11/05/15 01:47 7440-47-310/29/15 20:0010.0 2.5 1
Cobalt 25.3 ug/L 11/05/15 01:47 7440-48-410/29/15 20:0010.0 2.5 1
Copper ND ug/L 11/05/15 01:47 7440-50-810/29/15 20:0010.0 2.5 1
Lead ND ug/L 11/05/15 01:47 7439-92-110/29/15 20:0010.0 2.5 1
Nickel ND ug/L 11/05/15 01:47 7440-02-010/29/15 20:0050.0 2.5 1
Selenium ND ug/L 11/05/15 01:47 7782-49-210/29/15 20:0010.0 5.0 1
Silver ND ug/L 11/05/15 01:47 7440-22-410/29/15 20:0010.0 2.5 1
Thallium ND ug/L 11/05/15 01:47 7440-28-010/29/15 20:005.5 5.0 1
Vanadium 4.2J ug/L 11/05/15 01:47 7440-62-210/29/15 20:0025.0 2.5 1
Zinc ND ug/L 11/05/15 01:47 7440-66-610/29/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 07:35 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 07:35 107-13-12001.9 1
Benzene 0.39J ug/L 11/01/15 07:35 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 07:35 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 07:35 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 07:35 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 07:35 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 07:35 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 07:35 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 07:35 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/01/15 07:35 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/01/15 07:35 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 07:35 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 07:35 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 07:35 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 07:35 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 07:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 07:35 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/01/15 07:35 95-50-15.0 0.30 1
1,4-Dichlorobenzene 5.2 ug/L 11/01/15 07:35 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 07:35 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/01/15 07:35 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 07:35 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 07:35 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.2J ug/L 11/01/15 07:35 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 07:35 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 07:35 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 07:35 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 07:35 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-MW3 Lab ID:92273639003 Collected:10/26/15 10:50 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/01/15 07:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 07:35 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 07:35 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 07:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 07:35 108-10-11000.33 1
Styrene ND ug/L 11/01/15 07:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 07:35 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 07:35 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 07:35 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 07:35 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 07:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 07:35 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/01/15 07:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 07:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 07:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 07:35 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/01/15 07:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/01/15 07:35 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %11/01/15 07:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/01/15 07:35 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 07:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-UPSTREAM Lab ID:92273639004 Collected:10/26/15 11:20 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/05/15 01:50 7440-36-010/29/15 20:006.0 3.8 1
Arsenic ND ug/L 11/05/15 01:50 7440-38-210/29/15 20:0010.0 2.5 1
Barium 13.0J ug/L 11/05/15 01:50 7440-39-310/29/15 20:001002.5 1
Beryllium ND ug/L 11/05/15 01:50 7440-41-710/29/15 20:001.0 0.50 1
Cadmium ND ug/L 11/05/15 01:50 7440-43-910/29/15 20:001.0 0.50 1
Chromium ND ug/L 11/05/15 01:50 7440-47-310/29/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/05/15 01:50 7440-48-410/29/15 20:0010.0 2.5 1
Copper ND ug/L 11/05/15 01:50 7440-50-810/29/15 20:0010.0 2.5 1
Lead ND ug/L 11/05/15 01:50 7439-92-110/29/15 20:0010.0 2.5 1
Nickel ND ug/L 11/05/15 01:50 7440-02-010/29/15 20:0050.0 2.5 1
Selenium ND ug/L 11/05/15 01:50 7782-49-210/29/15 20:0010.0 5.0 1
Silver ND ug/L 11/05/15 01:50 7440-22-410/29/15 20:0010.0 2.5 1
Thallium ND ug/L 11/05/15 01:50 7440-28-010/29/15 20:005.5 5.0 1
Vanadium ND ug/L 11/05/15 01:50 7440-62-210/29/15 20:0025.0 2.5 1
Zinc ND ug/L 11/05/15 01:50 7440-66-610/29/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 07:52 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 07:52 107-13-12001.9 1
Benzene ND ug/L 11/01/15 07:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 07:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 07:52 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 07:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 07:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 07:52 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 07:52 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 07:52 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/01/15 07:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/01/15 07:52 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 07:52 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 07:52 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 07:52 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 07:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 07:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 07:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/01/15 07:52 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/01/15 07:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 07:52 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/01/15 07:52 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 07:52 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 07:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/01/15 07:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 07:52 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 07:52 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 07:52 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 07:52 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-UPSTREAM Lab ID:92273639004 Collected:10/26/15 11:20 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/01/15 07:52 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 07:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 07:52 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 07:52 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 07:52 108-10-11000.33 1
Styrene ND ug/L 11/01/15 07:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 07:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 07:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 07:52 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 07:52 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 07:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 07:52 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/01/15 07:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 07:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 07:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 07:52 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/01/15 07:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/01/15 07:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %11/01/15 07:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/01/15 07:52 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 07:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-DOWNSTREAM Lab ID:92273639005 Collected:10/26/15 10:47 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/05/15 01:53 7440-36-010/29/15 20:006.0 3.8 1
Arsenic ND ug/L 11/05/15 01:53 7440-38-210/29/15 20:0010.0 2.5 1
Barium 14.2J ug/L 11/05/15 01:53 7440-39-310/29/15 20:001002.5 1
Beryllium ND ug/L 11/05/15 01:53 7440-41-710/29/15 20:001.0 0.50 1
Cadmium ND ug/L 11/05/15 01:53 7440-43-910/29/15 20:001.0 0.50 1
Chromium ND ug/L 11/05/15 01:53 7440-47-310/29/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/05/15 01:53 7440-48-410/29/15 20:0010.0 2.5 1
Copper ND ug/L 11/05/15 01:53 7440-50-810/29/15 20:0010.0 2.5 1
Lead ND ug/L 11/05/15 01:53 7439-92-110/29/15 20:0010.0 2.5 1
Nickel ND ug/L 11/05/15 01:53 7440-02-010/29/15 20:0050.0 2.5 1
Selenium ND ug/L 11/05/15 01:53 7782-49-210/29/15 20:0010.0 5.0 1
Silver ND ug/L 11/05/15 01:53 7440-22-410/29/15 20:0010.0 2.5 1
Thallium ND ug/L 11/05/15 01:53 7440-28-010/29/15 20:005.5 5.0 1
Vanadium ND ug/L 11/05/15 01:53 7440-62-210/29/15 20:0025.0 2.5 1
Zinc ND ug/L 11/05/15 01:53 7440-66-610/29/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 08:09 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 08:09 107-13-12001.9 1
Benzene ND ug/L 11/01/15 08:09 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 08:09 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 08:09 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 08:09 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 08:09 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 08:09 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 08:09 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 08:09 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/01/15 08:09 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/01/15 08:09 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 08:09 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 08:09 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 08:09 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 08:09 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 08:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 08:09 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/01/15 08:09 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/01/15 08:09 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 08:09 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/01/15 08:09 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 08:09 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 08:09 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/01/15 08:09 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 08:09 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 08:09 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 08:09 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 08:09 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-DOWNSTREAM Lab ID:92273639005 Collected:10/26/15 10:47 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/01/15 08:09 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 08:09 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 08:09 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 08:09 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 08:09 108-10-11000.33 1
Styrene ND ug/L 11/01/15 08:09 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 08:09 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 08:09 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 08:09 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 08:09 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 08:09 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 08:09 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/01/15 08:09 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 08:09 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 08:09 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 08:09 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/01/15 08:09 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/01/15 08:09 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %11/01/15 08:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/01/15 08:09 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 08:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-FIELD BLANK Lab ID:92273639006 Collected:10/26/15 11:30 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/05/15 01:56 7440-36-010/29/15 20:006.0 3.8 1
Arsenic ND ug/L 11/05/15 01:56 7440-38-210/29/15 20:0010.0 2.5 1
Barium ND ug/L 11/05/15 01:56 7440-39-310/29/15 20:001002.5 1
Beryllium ND ug/L 11/05/15 01:56 7440-41-710/29/15 20:001.0 0.50 1
Cadmium ND ug/L 11/05/15 01:56 7440-43-910/29/15 20:001.0 0.50 1
Chromium ND ug/L 11/05/15 01:56 7440-47-310/29/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/05/15 01:56 7440-48-410/29/15 20:0010.0 2.5 1
Copper ND ug/L 11/05/15 01:56 7440-50-810/29/15 20:0010.0 2.5 1
Lead ND ug/L 11/05/15 01:56 7439-92-110/29/15 20:0010.0 2.5 1
Nickel ND ug/L 11/05/15 01:56 7440-02-010/29/15 20:0050.0 2.5 1
Selenium ND ug/L 11/05/15 01:56 7782-49-210/29/15 20:0010.0 5.0 1
Silver ND ug/L 11/05/15 01:56 7440-22-410/29/15 20:0010.0 2.5 1
Thallium ND ug/L 11/05/15 01:56 7440-28-010/29/15 20:005.5 5.0 1
Vanadium ND ug/L 11/05/15 01:56 7440-62-210/29/15 20:0025.0 2.5 1
Zinc ND ug/L 11/05/15 01:56 7440-66-610/29/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 08:26 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 08:26 107-13-12001.9 1
Benzene ND ug/L 11/01/15 08:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 08:26 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 08:26 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 08:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 08:26 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 08:26 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 08:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 08:26 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/01/15 08:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/01/15 08:26 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 08:26 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 08:26 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 08:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 08:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 08:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 08:26 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/01/15 08:26 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/01/15 08:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 08:26 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/01/15 08:26 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 08:26 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 08:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/01/15 08:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 08:26 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 08:26 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 08:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 08:26 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-FIELD BLANK Lab ID:92273639006 Collected:10/26/15 11:30 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/01/15 08:26 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 08:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 08:26 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 08:26 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 08:26 108-10-11000.33 1
Styrene ND ug/L 11/01/15 08:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 08:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 08:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 08:26 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 08:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 08:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 08:26 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/01/15 08:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 08:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 08:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 08:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/01/15 08:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/01/15 08:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %11/01/15 08:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/01/15 08:26 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 08:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-TRIP BLANK Lab ID:92273639007 Collected:10/26/15 08:00 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/01/15 08:42 67-64-110010.0 1
Acrylonitrile ND ug/L 11/01/15 08:42 107-13-12001.9 1
Benzene ND ug/L 11/01/15 08:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/01/15 08:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/01/15 08:42 75-27-41.0 0.18 1
Bromoform ND ug/L 11/01/15 08:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/01/15 08:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/01/15 08:42 78-93-31000.96 1
Carbon disulfide ND ug/L 11/01/15 08:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/01/15 08:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/01/15 08:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/01/15 08:42 75-00-310.0 0.54 1
Chloroform ND ug/L 11/01/15 08:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/01/15 08:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/15 08:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/01/15 08:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/15 08:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/01/15 08:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/01/15 08:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/01/15 08:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/01/15 08:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/01/15 08:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/01/15 08:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/01/15 08:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/01/15 08:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/01/15 08:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/01/15 08:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/01/15 08:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/01/15 08:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 11/01/15 08:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/01/15 08:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/01/15 08:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/01/15 08:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/01/15 08:42 108-10-11000.33 1
Styrene ND ug/L 11/01/15 08:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/15 08:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/15 08:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/01/15 08:42 127-18-41.0 0.46 1
Toluene ND ug/L 11/01/15 08:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/01/15 08:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/01/15 08:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/01/15 08:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/01/15 08:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/01/15 08:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/01/15 08:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/01/15 08:42 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
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Page 18 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Sample:9702-TRIP BLANK Lab ID:92273639007 Collected:10/26/15 08:00 Received:10/28/15 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 11/01/15 08:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %11/01/15 08:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/01/15 08:42 17060-07-070-130 1
Toluene-d8 (S)99 %11/01/15 08:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19926
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92273639001, 92273639002, 92273639003, 92273639004, 92273639005, 92273639006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1595304
Associated Lab Samples:92273639001, 92273639002, 92273639003, 92273639004, 92273639005, 92273639006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 11/05/15 00:303.8
Arsenic ug/L ND 10.0 11/05/15 00:302.5
Barium ug/L ND 100 11/05/15 00:302.5
Beryllium ug/L ND 1.0 11/05/15 00:300.50
Cadmium ug/L ND 1.0 11/05/15 00:300.50
Chromium ug/L ND 10.0 11/05/15 00:302.5
Cobalt ug/L ND 10.0 11/05/15 00:302.5
Copper ug/L ND 10.0 11/05/15 00:302.5
Lead ug/L ND 10.0 11/05/15 00:302.5
Nickel ug/L ND 50.0 11/05/15 00:302.5
Selenium ug/L ND 10.0 11/05/15 00:305.0
Silver ug/L ND 10.0 11/05/15 00:302.5
Thallium ug/L ND 5.5 11/05/15 00:305.0
Vanadium ug/L ND 25.0 11/05/15 00:302.5
Zinc ug/L ND 10.0 11/05/15 00:305.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1595305LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 442500 88 80-120
Arsenic ug/L 452500 90 80-120
Barium ug/L 426500 85 80-120
Beryllium ug/L 412500 82 80-120
Cadmium ug/L 444500 89 80-120
Chromium ug/L 443500 89 80-120
Cobalt ug/L 453500 91 80-120
Copper ug/L 446500 89 80-120
Lead ug/L 455500 91 80-120
Nickel ug/L 440500 88 80-120
Selenium ug/L 448500 90 80-120
Silver ug/L 218250 87 80-120
Thallium ug/L 473500 95 80-120
Vanadium ug/L 436500 87 80-120
Zinc ug/L 463500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
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Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1595306MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92273406006
1595307
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 87 75-12588 1 25500ND435441
Arsenic ug/L 500 89 75-12590 1 25500ND444449
Barium ug/L 500 85 75-12584 2 2550031.4 457 450
Beryllium ug/L 500 83 75-12581 2 25500ND414404
Cadmium ug/L 500 88 75-12588 0 25500ND439440
Chromium ug/L 500 88 75-12586 2 25500ND441431
Cobalt ug/L 500 89 75-12589 0 25500ND447446
Copper ug/L 500 89 75-12589 0 25500ND445444
Lead ug/L 500 90 75-12589 0 25500ND449447
Nickel ug/L 500 87 75-12587 0 25500ND437435
Selenium ug/L 500 88 75-12589 1 25500ND438444
Silver ug/L 250 86 75-12584 1 25250ND215212
Thallium ug/L 500 93 75-12593 0 25500ND465465
Vanadium ug/L 500 87 75-12585 3 25500ND436425
Zinc ug/L 500 92 75-12590 2 25500ND466458
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
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[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34087
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92273639001, 92273639002, 92273639003, 92273639004, 92273639005, 92273639006, 92273639007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1596344
Associated Lab Samples:92273639001, 92273639002, 92273639003, 92273639004, 92273639005, 92273639006, 92273639007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 11/01/15 00:300.33
1,1,1-Trichloroethane ug/L ND 1.0 11/01/15 00:300.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 11/01/15 00:300.40
1,1,2-Trichloroethane ug/L ND 1.0 11/01/15 00:300.29
1,1-Dichloroethane ug/L ND 5.0 11/01/15 00:300.32
1,1-Dichloroethene ug/L ND 5.0 11/01/15 00:300.56
1,2,3-Trichloropropane ug/L ND 1.0 11/01/15 00:300.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 11/01/15 00:302.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/01/15 00:300.27
1,2-Dichlorobenzene ug/L ND 5.0 11/01/15 00:300.30
1,2-Dichloroethane ug/L ND 1.0 11/01/15 00:300.24
1,2-Dichloropropane ug/L ND 1.0 11/01/15 00:300.27
1,4-Dichlorobenzene ug/L ND 1.0 11/01/15 00:300.33
2-Butanone (MEK)ug/L ND 100 11/01/15 00:300.96
2-Hexanone ug/L ND 50.0 11/01/15 00:300.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 11/01/15 00:300.33
Acetone ug/L ND 100 11/01/15 00:3010.0
Acrylonitrile ug/L ND 200 11/01/15 00:301.9
Benzene ug/L ND 1.0 11/01/15 00:300.25
Bromochloromethane ug/L ND 3.0 11/01/15 00:300.17
Bromodichloromethane ug/L ND 1.0 11/01/15 00:300.18
Bromoform ug/L ND 3.0 11/01/15 00:300.26
Bromomethane ug/L ND 10.0 11/01/15 00:300.29
Carbon disulfide ug/L ND 100 11/01/15 00:301.2
Carbon tetrachloride ug/L ND 1.0 11/01/15 00:300.25
Chlorobenzene ug/L ND 3.0 11/01/15 00:300.23
Chloroethane ug/L ND 10.0 11/01/15 00:300.54
Chloroform ug/L ND 5.0 11/01/15 00:300.14
Chloromethane ug/L ND 1.0 11/01/15 00:300.11
cis-1,2-Dichloroethene ug/L ND 5.0 11/01/15 00:300.19
cis-1,3-Dichloropropene ug/L ND 1.0 11/01/15 00:300.13
Dibromochloromethane ug/L ND 3.0 11/01/15 00:300.21
Dibromomethane ug/L ND 10.0 11/01/15 00:300.21
Ethylbenzene ug/L ND 1.0 11/01/15 00:300.30
Iodomethane ug/L ND 10.0 11/01/15 00:300.32
Methylene Chloride ug/L ND 1.0 11/01/15 00:300.97
Styrene ug/L ND 1.0 11/01/15 00:300.26
Tetrachloroethene ug/L ND 1.0 11/01/15 00:300.46
Toluene ug/L ND 1.0 11/01/15 00:300.26
trans-1,2-Dichloroethene ug/L ND 5.0 11/01/15 00:300.49
trans-1,3-Dichloropropene ug/L ND 1.0 11/01/15 00:300.26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1596344
Associated Lab Samples:92273639001, 92273639002, 92273639003, 92273639004, 92273639005, 92273639006, 92273639007
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 11/01/15 00:301.0
Trichloroethene ug/L ND 1.0 11/01/15 00:300.47
Trichlorofluoromethane ug/L ND 1.0 11/01/15 00:300.20
Vinyl acetate ug/L ND 50.0 11/01/15 00:300.35
Vinyl chloride ug/L ND 1.0 11/01/15 00:300.62
Xylene (Total)ug/L ND 5.0 11/01/15 00:300.66
1,2-Dichloroethane-d4 (S)%101 70-130 11/01/15 00:30
4-Bromofluorobenzene (S)%100 70-130 11/01/15 00:30
Toluene-d8 (S)%101 70-130 11/01/15 00:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1596345LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.050 100 80-125
1,1,1-Trichloroethane ug/L 53.250 106 71-129
1,1,2,2-Tetrachloroethane ug/L 50.950 102 79-124
1,1,2-Trichloroethane ug/L 48.250 96 85-125
1,1-Dichloroethane ug/L 52.350 105 73-126
1,1-Dichloroethene ug/L 55.250 110 66-135
1,2,3-Trichloropropane ug/L 49.150 98 75-130
1,2-Dibromo-3-chloropropane ug/L 50.450 101 71-133
1,2-Dibromoethane (EDB)ug/L 50.750 101 83-124
1,2-Dichlorobenzene ug/L 50.750 101 80-133
1,2-Dichloroethane ug/L 45.950 92 67-128
1,2-Dichloropropane ug/L 49.850 100 75-132
1,4-Dichlorobenzene ug/L 49.550 99 78-130
2-Butanone (MEK)ug/L 98.6J100 99 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 72-135
Acetone ug/L 97.6J100 98 48-146
Acrylonitrile ug/L 253250 101 40-160
Benzene ug/L 51.350 103 80-125
Bromochloromethane ug/L 53.050 106 71-125
Bromodichloromethane ug/L 52.650 105 78-124
Bromoform ug/L 50.250 100 71-128
Bromomethane ug/L 48.950 98 40-160
Carbon disulfide ug/L 53.4J50 107 50-160
Carbon tetrachloride ug/L 54.150 108 69-131
Chlorobenzene ug/L 49.150 98 81-122
Chloroethane ug/L 48.650 97 39-148
Chloroform ug/L 51.750 103 73-127
Chloromethane ug/L 50.650 101 44-146
cis-1,2-Dichloroethene ug/L 50.150 100 74-124
cis-1,3-Dichloropropene ug/L 50.650 101 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
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Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1596345LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 51.850 104 78-125
Dibromomethane ug/L 49.950 100 82-120
Ethylbenzene ug/L 50.350 101 79-121
Iodomethane ug/L 102100 102 39-154
Methylene Chloride ug/L 54.550 109 64-133
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 50.550 101 78-122
Toluene ug/L 50.650 101 80-121
trans-1,2-Dichloroethene ug/L 52.050 104 71-127
trans-1,3-Dichloropropene ug/L 50.450 101 69-141
trans-1,4-Dichloro-2-butene ug/L 61.0J50 122 40-160
Trichloroethene ug/L 48.650 97 78-122
Trichlorofluoromethane ug/L 52.850 106 53-137
Vinyl acetate ug/L 104100 104 40-160
Vinyl chloride ug/L 59.450 119 58-137
Xylene (Total)ug/L 151150 101 81-126
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1596346MATRIX SPIKE SAMPLE:
MSSpike
Result
92273348002
1,1,1,2-Tetrachloroethane ug/L 21.020 105 70-130ND
1,1,1-Trichloroethane ug/L 24.320 121 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.720 108 70-130ND
1,1,2-Trichloroethane ug/L 20.620 103 70-130ND
1,1-Dichloroethane ug/L 23.620 118 70-130ND
1,1-Dichloroethene ug/L 25.720 128 70-166ND
1,2,3-Trichloropropane ug/L 20.720 104 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.520 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.320 107 70-130ND
1,2-Dichlorobenzene ug/L 21.920 109 70-130ND
1,2-Dichloroethane ug/L 20.020 99 70-130ND
1,2-Dichloropropane ug/L 21.620 108 70-130ND
1,4-Dichlorobenzene ug/L 21.820 109 70-130ND
2-Butanone (MEK)ug/L 43.4J40 108 70-130ND
2-Hexanone ug/L 44.3J40 111 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.6J40 109 70-130ND
Acetone ug/L 48.6J40 115 70-130ND
Acrylonitrile ug/L 109J100 109 70-130ND
Benzene ug/L 22.620 113 70-148ND
Bromochloromethane ug/L 23.620 118 70-130ND
Bromodichloromethane ug/L 21.720 109 70-130ND
Bromoform ug/L 18.920 95 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
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Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1596346MATRIX SPIKE SAMPLE:
MSSpike
Result
92273348002
Bromomethane ug/L 19.920 99 70-130ND
Carbon disulfide ug/L 23.8J20 119 70-130ND
Carbon tetrachloride ug/L 23.920 119 70-130ND
Chlorobenzene ug/L 21.920 109 70-146ND
Chloroethane ug/L 23.520 118 70-130ND
Chloroform ug/L 23.020 115 70-130ND
Chloromethane ug/L 24.220 121 70-130ND
cis-1,2-Dichloroethene ug/L 22.520 112 70-130ND
cis-1,3-Dichloropropene ug/L 20.220 101 70-130ND
Dibromochloromethane ug/L 20.720 103 70-130ND
Dibromomethane ug/L 21.120 106 70-130ND
Ethylbenzene ug/L 22.320 112 70-130ND
Iodomethane ug/L 41.140 103 70-130ND
Methylene Chloride ug/L 23.120 115 70-130ND
Styrene ug/L 20.420 102 70-130ND
Tetrachloroethene ug/L 22.820 114 70-130ND
Toluene ug/L 21.920 110 70-155ND
trans-1,2-Dichloroethene ug/L 23.620 118 70-130ND
trans-1,3-Dichloropropene ug/L 19.720 99 70-130ND
trans-1,4-Dichloro-2-butene ug/L 16.9J20 85 70-130ND
Trichloroethene ug/L 21.520 107 69-151ND
Trichlorofluoromethane ug/L 25.320 126 70-130ND
Vinyl acetate ug/L 37.5J40 94 70-130ND
Vinyl chloride ug/L 27.4 M12013770-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92273348003
1596347SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
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Page 25 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92273348003
1596347SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%100 1101
4-Bromofluorobenzene (S)%98 199
Toluene-d8 (S)%99 1100
REPORT OF LABORATORY ANALYSIS
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Page 26 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92273639
WILKES-DAN JOHNSON 356.1501.12
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92273639001 MPRP/19926 ICP/179689702-MW1 EPA 3010 EPA 6010
92273639002 MPRP/19926 ICP/179689702-MW2 EPA 3010 EPA 6010
92273639003 MPRP/19926 ICP/179689702-MW3 EPA 3010 EPA 6010
92273639004 MPRP/19926 ICP/179689702-UPSTREAM EPA 3010 EPA 6010
92273639005 MPRP/19926 ICP/179689702-DOWNSTREAM EPA 3010 EPA 6010
92273639006 MPRP/19926 ICP/179689702-FIELD BLANK EPA 3010 EPA 6010
92273639001 MSV/340879702-MW1 EPA 8260
92273639002 MSV/340879702-MW2 EPA 8260
92273639003 MSV/340879702-MW3 EPA 8260
92273639004 MSV/340879702-UPSTREAM EPA 8260
92273639005 MSV/340879702-DOWNSTREAM EPA 8260
92273639006 MSV/340879702-FIELD BLANK EPA 8260
92273639007 MSV/340879702-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/06/2015 03:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 30
Page 29 of 30
Page 30 of 30

Appendix 2
Summary of Detections, Exceedances, and Field Parameters
Summary of Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
9702-MW1 pH 5.15 S.U.10/26/2015
9702-MW1 Temperature 14.8 C˚10/26/2015
9702-MW1 Conductivity 252 µS 10/26/2015
9702-MW1 Turbidity 10.3 NTU 10/26/2015
9702-MW1 Static Water Level 32.75 ft 10/26/2015
9702-MW1 Well Depth 60.12 ft 10/26/2015
9702-MW2 pH 5.38 S.U.10/26/2015
9702-MW2 Temperature 13.6 C˚10/26/2015
9702-MW2 Conductivity 399 µS 10/26/2015
9702-MW2 Turbidity 8.36 NTU 10/26/2015
9702-MW2 Static Water Level 32.45 ft 10/26/2015
9702-MW2 Well Depth 40.08 ft 10/26/2015
9702-MW3 pH 4.65 S.U.10/26/2015
9702-MW3 Temperature 14.4 C˚10/26/2015
9702-MW3 Conductivity 212 µS 10/26/2015
9702-MW3 Turbidity 4.1 NTU 10/26/2015
9702-MW3 Static Water Level 10.35 ft 10/26/2015
9702-MW3 Well Depth 29.43 ft 10/26/2015
9702-Upstream pH 7 S.U.10/26/2015
9702-Upstream Temperature 13.7 C˚10/26/2015
9702-Upstream Conductivity 52 µS 10/26/2015
9702-Upstream Turbidity 7.69 NTU 10/26/2015
9702-Downstream pH 5.23 S.U.10/26/2015
9702-Downstream Temperature 13.8 C˚10/26/2015
9702-Downstream Conductivity 61 µS 10/26/2015
9702-Downstream Turbidity 6.36 NTU 10/26/2015
NOTES:C˚= degrees Centigrade
S.U.= Standard Units
µS = microsemens
NTU = Nephelometric Turbidity Units
ft = Feet
Wilkes Co. Dan Johnson Landfill
Permit No. 97-02 Joyce Engineering
Summary of Detections
WELL ID PARAMETER RESULT UNITS SWSL DATE
9702-MW1 Cobalt 59.2 µg/L 10 10/26/2015
9702-MW1 1,4-Dichlorobenzene 2.4 µg/L 1 10/26/2015
9702-MW1 Benzene 2.2 µg/L 1 10/26/2015
9702-MW1 Vinyl chloride 1.7 µg/L 1 10/26/2015
9702-MW1 cis-1,2-Dichloroethene 7.8 µg/L 5 10/26/2015
9702-MW2 Cobalt 32.4 µg/L 10 10/26/2015
9702-MW2 Zinc 70.1 µg/L 10 10/26/2015
9702-MW2 1,4-Dichlorobenzene 3.3 µg/L 1 10/26/2015
9702-MW3 Barium 104 µg/L 100 10/26/2015
9702-MW3 Cobalt 25.3 µg/L 10 10/26/2015
9702-MW3 1,4-Dichlorobenzene 5.2 µg/L 1 10/26/2015
NOTES:All Results in micorgrams per liter (µg/L)
SWSL = NC Soild Waste Section Reporting Limit
Wilkes Co. Dan Johnson Landfill
Permit No. 97-02 Page 1 of 1 Joyce Engineering
Summary of Exceedances
WELL ID PARAMETER RESULT UNITS SWSL NC2L/*GWPS GPS DATE
9702-MW1 Cobalt 59.2 µg/L 10 1*1 10/26/2015
9702-MW1 Benzene 2.2 µg/L 1 1 1 10/26/2015
9702-MW1 Vinyl chloride 1.7 µg/L 1 0.03 0.03 10/26/2015
9702-MW2 Cobalt 32.4 µg/L 10 1*1 10/26/2015
9702-MW3 Cobalt 25.2 µg/L 10 1*1 10/26/2015
NOTES:All Results in micorgrams per liter (µg/L)
SWSL = NC Soild Waste Section Reporting Limit
NC2L = NC Groundwater Standard from 15A NCAC 2L.0202
GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L)
GPS = Groundwater Protection Standard as defined by 15A NCAC 13B.1634(g)
Wilkes Co. Dan Johnson Landfill
Permit No. 97-02 Joyce Engineering

Appendix 3
Horizontal Groundwater Flow Velocities
Horizontal Groundwater Flow Velocities
Date of Water Table Measurements: October 26, 2015
SEGMENT HORIZ.HYDRAULIC EFFECTIVE LINEAR
FLOW BEGIN & END GRADIENT CONDUCTIVITY POROSITY VELOCITY
DIRECTION GW ELEVATION i K n e V
(feet-AMSL)(ft/ft) (ft/day)(ft/year)
1,170
1,150
1,180
1,150
Average 0.0423 Average 53.10
Notes:
Linear flow velocity: V = Ki/n e (modified Darcy equation).
Hydraulic conductivity (K ) is based on slug test from Wilkes County Roaring River Landfill.
Effective porosity (n e ) is based on data for the Wilkes County Roaring River Landfill.
Refer to Drawing 1 for flow line segments.
FLOW LINE
SEGMENT
SEGMENT
LENGTH
(feet)
48.51
i 1 435 W 0.0460 0.16 57.69
0.16
5.50E-01
5.50E-01i2776SE0.0387
Wilkes County Dan Johnson Landfill
Permit # 97-02 Joyce Engineering