19084_ West Stonewall Street_OAR_20151207

December 7, 2015

Ms. Linda Kaiser
Corporate Environmental Management
GSLH Charlotte Realty Holdings, LLC
6011 Connection Drive
Irving, Texas 75039

Re: PCB Assessment Summary Report
The Charlotte Observer Facility
600 South Tryon Street
Charlotte, North Carolina

Dear Ms. Kaiser:

On behalf of GSLH Charlotte Realty Holdings, LLC (GSLH), Cardno is pleased to submit a summary report of findings
for Polychlorinated Biphenyl (PCB) Assessment at the Charlotte Observer facility, which includes an office building, a
full basement with a tunnel, a warehouse, and parking lots. The Charlotte Observer Building, located at 600 South
Tryon Street, is a five-story office building with a basement and a basement tunnel that extends northwest below South
Church Street to the Charlotte Observer Warehouse. The warehouse is a one-story building located at 621 South
Poplar Street. The roof of the warehouse was in use as a parking deck.

The Charlotte Observer Building and warehouse were built in 1971, with the exception of the northeastern part of
the building located in the basement that was constructed prior to 1929 and the reel room (press area) in the
basement that was constructed in 1969. Numerous upgrades and renovations have occurred since the initial
development.

BACKGROUND

Based on the information provided in a previous Phase I Environmental Site Assessment (ESA), Cardno performed
an Initial Phase II ESA in which concrete, potential wastes, caulks, and glazes were analyzed for PCBs in July 2015.
Following the Initial Phase II ESA, Cardno completed additional PCB sampling during an Additional Phase II ESA
consisting of several separate sampling events in which caulk and similar materials were sampled and analyzed for
PCBs in September and October 2015. In conjunction with the additional caulk sampling, surface wipe samples of
non-porous materials (glass, metal, and polished stone) adjacent to caulk with elevated PCB content were collected
and analyzed in September and October 2015. Air sampling at the facility with analysis for PCBs was conducted in
October 2015.

PCB ASSESSMENT FINDINGS

Initial Phase II ESA

As part of the Initial Phase II ESA, the PCB data for caulks and glazes found impact in excess of Toxic Substance
Control Act (TSCA) standards for the majority of samples, on the interior and exterior of the main Charlotte
Observer building. Limited sampling was conducted for PCBs in caulk during the initial Phase II ESA. PCB
detections were also common across the concrete and waste data set, but the concentrations did not exceed 2.5
milligrams per kilogram (mg/kg) for any individual PCB homologue, or type of PCB. Aroclor 1016 and Aroclor 1254
were the two PCB homologues that were detected. The regulatory concentration for PCBs to be considered TSCA-
regulated waste is 50 mg/kg. Of the 15 caulk samples collected from various parts of the building, 13 of the samples
contained total PCBs in excess of the TSCA standard of 50 mg/kg. Concentrations of total PCBs in the samples in
excess of the TSCA standard ranged from 55 mg/kg up to 89,000 mg/kg.

Cardno
7606 Whitehall Executive Center Drive
Suite 800
Charlotte, NC 28273
Phone [phone]
Fax [phone]

www.cardno.com
The Charlotte Observer Facility
PCB Assessment Summary Report
December 7, 2015
Additional Phase II ESA
Caulk
Based on widespread PCB caulk findings during the initial Phase II ESA at concentrations above the TSCA 50
mg/kg limit in 13 of 15 samples, GSLH authorized testing of additional materials to confirm previous findings and
to assure that sufficient characterization of the various caulk and similar materials was conducted.
The first set of 20 additional caulk samples, collected on September 30 and October 1, 2015, included detections
in equivalent materials to some samples from the initial Phase II ESA and also identified additional materials. Six
of the 20 samples contained impact above the TSCA limit, and fourteen of the 20 samples had no detectable
impact or impact below the TSCA limit.
Further PCB Assessment
Cardno returned to the site on October 22, 2015, for confirmation caulk sampling of five materials; to sample porous
materials that were adjacent to caulk with elevated PCB impact in six locations; and to conduct 20 wipe samples
on non-porous surfaces near caulk with elevated PCB impact. A final sample of caulk was also collected on October
27, 2015. One additional material was found to contain impact above the TSCA limit and three additional samples
were found to confirm previous exceedances of TSCA limits.
In summary, of the total of 41 caulk samples, 23 samples, representing 19 separate materials, exceeded the TCSA
limit of 50 mg/kg for PCBs. Seven of the TSCA-positive caulk samples had had concentrations below 500 mg/kg
of PCBs, and the remaining 16 TSCA-positive samples exceeding 1,000 mg/kg. Nine samples had PCBs
exceeding 10,000 mg/kg, with the highest concentration at 89,000 mg/kg total PCBs. The majority of the TSCA-
regulated material consisted of window caulking or glaze and had a total estimated amount of approximately
250,000 linear feet, which includes an estimated 35,000 linear feet of assumed-positive materials from windows
and skylights that could not be accessed.
Two of the six porous materials adjacent to extensive amounts of caulk with elevated PCB content were found to
slightly exceed the TSCA limit (<100 mg/kg PCBs), and would be considered TSCA waste. A total of approximately
50,000 linear feet of porous materials adjacent to heavily impacted PCB caulk are estimated to have exceedances
of the TSCA limit of 50 mg/kg, and to be approximately a centimeter or less from the caulk. These materials include
pebble walls in the escalator area and the external pillars in the parking deck on the first level of the main Observer
building.
Cardno consulted the USEPA Question & Answer Manual (June 2014) for assessment of PCBs on non-porous
surfaces. The manual indicates regulatory requirements for disposal of non-porous materials that have impact
between 10 and 100 micrograms per 100 square centimeters (ug/100 cm2) as PCB-contaminated, in a similar
manner to detected PCBs below 50 mg/kg for solid materials. Surface concentrations below 10 ug/100cm2 do not
constitute TSCA-regulated materials according to the manual. Of 20 wipe samples, the following findings apply:
 No samples exceeded the 100 ug/100 cm2 limit that would potentially define the material as TSCA waste;
 Six samples contained PCBs between 10 and 100 ug/100 cm2; and
 Fourteen wipe samples were non-detect for PCBs or contained less than 10ug/100cm2 and would not be
regulated.
The six samples that would qualify as PCB-contaminated include a door frame in the basement area near a positive
caulk sample, escalator and stair railings on the second floor, a wall and railing near the escalators on the third
floor, and a newsroom door frame on the fourth floor. Floors were not tested, and because of constant cleaning,
relatively low potential for exceedances are assumed. Cardno has derived preliminary estimates that a total of
approximately 20,000 square feet of non-porous areas should be assumed to have PCBs between 10 and 100
ug/100 cm2.
Four homologues of PCBs were found in caulk, porous materials, or on surfaces at the site: Aroclor 1016, Aroclor
1254, Aroclor 1260, and Aroclor 1268. The majority of the detections, and each of the detections above the TSCA
limit, were Aroclor 1254 and Aroclor 1268.
The Charlotte Observer Facility
PCB Assessment Summary Report
December 7, 2015
PCB Air Assessment
Assessment of air quality for PCBs was conducted at the facility on October 23, 2015, and during a repeat sampling
of one location that had a pump failure on October 27, 2015. The analysis found detections of PCBs in air at the
facility. Except for the Occupational Safety and Health Administration Permissible Exposure Limits (OSHA PELs)
of 0.5 mg/m3 and 1 mg/m3, for Aroclor 1242 and Aroclor 1254, respectively, regulatory standards for air have not
been promulgated. None of the facility air samples had concentrations approaching the OSHA PELs.
The USEPA Regional Screening Levels (RSLs) are guidelines and indicate a limit for the Aroclor homologues in
Industrial Air of 0.021 micrograms per cubic meter (ug/m3). The air samples at the facility had detectable
concentrations of Aroclor 1248 in 10 of 11 samples. The sample from the warehouse had no detectable PCBs, and
the quality assurance blank also contained no detectable PCBs. Three locations – in the reel room and tunnel, in
the fourth floor imaging area, and in exterior air of the main Observer parking garage – contained PCBs at slightly
more than the EPA RSL (0.045 to 0.069 ug/m3). The remaining samples within the main observer building had
concentrations ranging from 0.14 to 0.77 ug/m3 and exceed the Industrial Air RSL by several times.
The difference between the Aroclors detected in facility building materials and the Aroclor detected in air have
several potential explanations, including that the source for the air impact may be from paint, electrical equipment
or other building materials that have not been sampled. The detections in air may also have segregated
components from caulk that have higher vapor pressures and thus vaporization potential, which produce and
apparent Aroclor 1248 signature. From an IH perspective, the detections point to possible separate air handling
for areas with no detection or low concentrations versus those that have elevated concentrations. The samples
with no detection appear to have a certain degree of isolation from impacted caulk. The former printing operation
does not appear to be a potential source because relatively low impact is present in the reel room and no detectable
impact is present in the warehouse areas. The imaging area on the fourth floor, also with relatively low detections,
may have HVAC isolation from the remainder of the building.
Recommendations

Prior to the anticipated demolition, Cardno recommends abatement by removal of PCB impacted materials. The
abatement will require that the work be performed in accordance with an EPA-approved PCB Management Plan. The
management of the PCBs, including abatement, monitoring, and disposal should be conducted by qualified and
properly trained contractors prior to demolition.

Cardno appreciates the opportunity to perform these services for GSLH and we look forward to working with you in
the future. If you have questions or comments regarding the information in this report, please contact the Cardno
Charlotte, North Carolina, office at [phone].

Sincerely,
Cardno

David A. Hunter, P.G. Kevin Headd, MS, MBA, CIH, PG, PMP, SAM
Principal Scientist Senior Industrial Hygienist

pc: Scott Carr, GSLH Charlotte Realty Holdings, LLC

Attachments

Attachment 1 Tables
Attachment 2 Figures
Attachment 3 Analytical Documentation
Attachment 4 Assumptions and Limitations

ATTACHMENT 1
TABLES
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EPA Method 8082 PCBs
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RCRA Metals
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8
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1
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0

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I
N
A
Adjacent
Porous Material
Sample
Additional
Caulk Sample Wipe Sample
Ar
o
c
l
o
r

1
0
1
6
Ar
o
c
l
o
r

1
2
5
4
Ar
o
c
l
o
r

1
2
6
0
Ar
o
c
l
o
r

1
2
6
8
C-1 C-17 & C-18 Window Glazing on floors 2 and 3 (Mail Room Window Glazing) 7/14/2015 40 64 104 50 30,000 lf
C-2 C-46 - PM Pillar Caulk (Mail Room Pillar) (Not including escalator system area) 7/15/2015 81,000 81,000 50 30,000 lf
C-3 Drywall/Wall Caulk (Mail Room) 7/15/2015 14,000 43,000 57,000 50 100 lf
C-4 C-42 - PM Caulk on Pebbly Walls (escalator system Area) 7/15/2015 89,000 89,000 50 15,000 lf
C-5 External Building Strip 7/15/2015 4.8 4.8 50 NA
C-6 W-4 External Parking Lot Window 7/15/2015 4,800 4,800 50 600 lf
C-7 C-36 - PM W-5 External Pillar Caulk (Parking Area) 7/23/2015 74,000 74,000 50 5,000 lf
C-8 C-20 & C-37 External Parking Lot Caulk 7/14/2015 9.8 55 36 100.8 50 1,000 lf
C-9 C-38 - PM C-22 & C-26 External Parking Lot Caulk (Entrance Wall) 7/14/2015 19,000 19,000 50 15,000 lf
C-10 C-40 Loading Dock Joints 7/14/2015 55 J 55 50 200 lf
C-11 Loading Dock Joints in Parking Lot 7/8/2015 9,200 9,200 50 1,000 lf
C-12 C-45 - PM External Warehouse Parking Lot Stone Wall 7/20/2015 990 6,100 7,090 50 5,000 lf
C-13 W-2 External Warehouse Window 7/15/2015 180 680 860 50 300 lf
C-14 W-1 External Warehouse Window Patch 7/17/2015 82 340 422 50 5 lf
C-15 External Warehouse Sidewalk 7/20/2015 8.3 5.1 13.4 50 NA
C-16 W-3 Tunnel Door Frame 9/30/2015 4,700 19,000 23,700 50 20 lf
C-17 C-1 & C18 Window Glazing on floors 2 and 3 (Mail Window Glazing) 9/30/2015 30 J 30 J 50 30,000 lf
C-18 C-1 & C-17 Window Glazing on floors 2 and 3 (Cafeteria Window Glazing) 9/30/2015 100 100 50 30,000 lf
C-19 External Building Strip 9/30/2015 50 NA
C-20 C-8 & C-37 External Parking Lot Caulk 9/30/2015 33 J 33 J 50 1,000 lf
C-21 Exterior Outer Pillar 9/30/2015 37J 50 NA
C-22 External Parking Lot Caulk (Parking Lot Wall) 9/30/2015 4,000 4,000 50 15,000 lf
C-23 Exterior Loading Dock Joints 9/30/2015 50 200 lf
C-24 C-41 - PM Exterior Building Joint at the Loading Dock 9/30/2015 7,000 21,000 28,000 50 1,000 lf
C-25 Exterior Parking Lot Tar Material 9/30/2015 50 NA
C-26 Exterior Sidewalk Caulk 9/30/2015 4,400 J 4,400 J 50 15,000 lf
C-27 Exterior Warehouse Wall Joint 9/30/2015 50 NA
C-28 Exterior Warehouse Wall Joint 9/30/2015 50 NA
C-29 Exterior Warehouse Window Frame 9/30/2015 50 NA
C-30 Exterior Warehouse Gray Parking Deck Surface 9/30/2015 50 NA
C-31 Exterior Warehouse Joint Parking Deck 9/30/2015 50 NA
C-32 Exterior Warehouse Joint Parking Deck 9/30/2015 50 NA
C-33 C-39 HVAC Black Caulk - on Floor 2 10/1/2015 74 J 74 J 50 1,000 lf
C-34 HVAC Black Caulk - on Floor 5 10/1/2015 45 J 45 J 50 NA
C-35 HVAC White Caulk - on Floor 5 10/1/2015 19 J 19 J 50 NA
C-36 - PM C-7 Adjacent Materials to External Pillar in Parking Deck 10/22/2015 34 44 78 50 10,000 lf
C-37 C-8 & C-20 External Parking Lot Caulk 10/22/2015 15 15 50 1,000 lf
C-38 - PM C-9 Adjacent Material to External Parking Lot Caulk (Entrance Wall) 10/22/2015 3.8 7.2 11 50 5,000 lf
C-39 C-33 Below (W-7) HVAC Black Caulk - on Floor 2 10/22/2015 160 160 50 1,000 lf
C-40 C-10 Loading Dock Joints 10/22/2015 50 200 lf
C-41 - PM C-24 Adjacent Wall Material Exterior Building Joint at the Loading Dock 10/22/2015 9.6 40 49.6 50 1,000 lf
C-42 - PM C-4 Adjacent to Central/Escalator Pebble Walls 10/22/2015 52 52 50 30,000 lf
C-43 C-44 Mail Room Window Frame Caulk 10/22/2015 8,800 J 24,000 32,800 J 50 30,000 lf
C-44 C-43 Mail Room Window Frame Caulk 10/22/2015 68,000 68,000 50 30,000 lf
C-45 - PM C-12 External Warehouse Parking Lot Stone Wall 10/22/2015 1.8 5.9 7.7 50 5,000 lf
C-46 - PM C-2 Adjacent Materials to Mail Room Pillar 10/22/2015 2.1 2.1 50 20,000 lf
C-47 - PM Visual Screen Around Loading Dock 10/22/2015 2.5 2.5 50 NA
PC-1 External Outer Pillar 10/27/2015 1,700 1,700 50 30,000 lf
W-1 C-14 External Warehouse Window Patch 10/22/2015 0.38 J 0.38 J 10 NA
W-2 C-13 External Warehouse Window 10/22/2015 0.32 J 0.32 J 10 NA
W-3 C-16 Tunnel Door Frame 10/22/2015 2.9 15 17.9 10 20 lf
W-4 C-6 External Wall/Window Frame 10/22/2015 1.2 5.2 6.4 10 NA
W-5 C-7 External Pillar 10/22/2015 0.38 J 0.38 J 10 NA
W-6 C-6 Interior Wall/Window Frame 10/22/2015 1.6 1.6 10 NA
W-7 C-39 Floor Below HVAC Black Caulk - on Floor 2 10/22/2015 1.4 0.98 2.38 10 NA
W-8 Second Floor Hall Windows 10/22/2015 0.64 0.64 10 NA
W-9 Second Floor Stairs Wall Window Frame 10/22/2015 23 95 118 10 24,000 sf
W-10 Second Floor Escalators Wall 10/22/2015 35 3.5 38.5 10 20,800 sf
W-11 Third Floor Escalator Wall 10/22/2015 92 92 10 20,800 sf
W-12 Third Floor Railing 10/22/2015 22 1.6 23.6 10 20,800 sf
W-13 Third Floor Window Frame 10/22/2015 1.4 1.4 2.8 10 NA
W-14 Third Floor Service Elevator 10/22/2015 1.2 0.25 J 1.45 J 10 NA
W-15 Third Floor Paper Shoot 10/22/2015 10 NA
W-16 Fourth Floor Newsroom Door Frame 10/22/2015 13 13 10 NA
W-17 Fourth Floor Imaging Window Frame 10/22/2015 10 NA
W-18 Basement Hall Window Frame 10/22/2015 10 NA
W-19 C-2 Mail Room Men's Restroom Window Frame 10/22/2015 0.79 0.79 10 NA
W-20 Front Entrance Revolving Door Frame 10/22/2015 10 NA
Notes:
1. All concentrations are reported in milligrams per kilogram (mg/kg), with the exception of the wipe samples which are reported in micrograms per ten square centimeters (µg/100 cm²).
2. Values in BOLD exceeds EPA TSCA Standard.
3. Aroclor compounds are PCBs.
4. TSCA = Toxic Substances Control Act
5. Blank spaces indicate no concentrations above detection limits. Detection limits are below the TSCA Standard of 50 mg/kg or 10 µg/100 cm².
TABLE 2
CAULK, ADJACENT POROUS MATERIAL, AND WIPE SAMPLE ANALYTICAL SUMMARY
PCB CONTENT
ADDITIONAL PHASE II ESA
CHARLOTTE OBSERVER FACILITY
600 SOUTH TRYON STREET
CHARLOTTE, NORTH CAROLINA
Sample ID
Location Cross-Reference
Sample Description Date
Sampled
EPA METHOD 8082A - PCBs
PC
B

T
o
t
a
l
EP
A

T
S
C
A

S
t
a
n
d
a
r
d
(S
e
e

N
o
t
e
s
)
Es
t
i
m
a
t
e
d

Q
u
a
n
t
i
t
y
Concentrations in mg/kg
INITIAL PHASE II ESA
ADDITIONAL PHASE II ESA
ADDITIONAL PCB ASSESSMENT - CAULK AND POROUS MATERIALS
ADDITIONAL PCB ASSESSMENT - WIPE SAMPLES Concentrations in µg/100 cm²
EPA METHOD
ETO10A - PCBs
Ar
o
c
l
o
r

1
2
4
8
PUF-1 Warehouse 10/23/2015 <0.0083 <0.0083 0.021
PUF-2 Reel Room & Tunnel 10/23/2015 0.049 0.049 0.021
PUF-3 Basement Copy Room 10/23/2015 0.14 0.14 0.021
PUF-4 First Floor Lobby 10/23/2015 0.65 0.65 0.021
PUF-5 First Floor Connection Center 10/23/2015 0.51 0.51 0.021
PUF-6 Third Floor Cafeteria 10/23/2015 0.55 0.55 0.021
PUF-7A Fourth Floor Newsroom 10/27/2015 0.41 0.41 0.021
PUF-8 Fifth Floor Main Hall 10/23/2015 0.37 0.37 0.021
PUF-9 Second Floor Escalator 10/23/2015 0.77 0.77 0.021
PUF-10 Fourth Floor Imaging 10/23/2015 0.069 0.069 0.021
PUF-11 Exterior 10/23/2015 0.045 0.045 0.021
Blank Blank (Opened and Closed On Site)
No Air Collected 10/23/2015 <0.0083 <0.0083 0.021
Notes:
1. Concentrations are in micrograms per cubic meter (µg/m³).
2. EPA = Environmental Protection Agency
3. Values in BOLD exceeds EPA Regional Screening Level.
4. Aroclor compounds are PCBs.
5. EPA = Environmental Protection Agency
6."<" indicates no concentrations above method detection limits.
7. PUF-7A was performed due to PUF-7 pump failures
8. No air collected in Blank.
TABLE 3
AIR SAMPLE ANALYTICAL SUMMARY
PCB CONTENT
ADDITIONAL PHASE II ESA
CHARLOTTE OBSERVER FACILITY
600 SOUTH TRYON STREET
Concentrations in µg/m³
ADDITIONAL PCB ASSESSMENT
CHARLOTTE, NORTH CAROLINA
Sample ID Sample Location Description
Date
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CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
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REFERENCE: USGS 7.5-MINUTE MAP, CHARLOTTE EAST,
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South Tryon Street
We
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C-
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76
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2
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5
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SU
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MAP – F IG 4 F
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(+
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76
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6

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(+
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(-
)
7606 Whitehall Executive Center Dr.
Suite 800
Charlotte, NC 28273
[phone]
PCB SURVEY
SAMPLE LOCATION MAP – FIG 4H
Map based on site plans provided by the Charlotte Observer
Charlotte Observer – Basement Tunnel
601 South Tryon Street- 621 South Poplar Street
Charlotte, North Carolina
W
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(+)
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West Stonewall StreetSouth Poplar Street
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C-
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C-27
C-
4
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W-
1
W-
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F
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(-
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(+
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(+
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(
+
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(-
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(
-
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(-
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(-
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(-
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(-
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(-
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(-
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(-)C-47(Along West St onewall Street)(-)
(-
)

ATTACHMENT 3
ANALYTICAL DOCUMENTATION
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
08/06/2015
Cardno - Charlotte
Steven Aldis
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Project: Charlotte Observer
Lab Submittal Date: 07/14/2015
Prism Work Order: 5070245
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Reactivity and Flashpoint analysis was subcontracted to GCAL. Laboratory report is attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 135
Data Qualifiers Key Reference:
A 0.6 g of the wipe was analyzed.
Aa Analyzed outside of hold time.
Ab LCS/LCSD result is below the control limits. CCV recovery within the limits. Analyte not detected in the sample down
to the MDL. No further action taken.
Ac Medium level analysis resulted in a BDL for Acetone. Straight run reported.
Ad Medium level analysis resulted in a detection below the reporting limit. The orginal 1x dilution is reported.
Ae Possible partial or weathered pattern. Results should be considered as estimated concentration.
Af Re-analysis. Recovery resulted in similar surrogate recoveries. Matrix interference suspected. Final run reported.
Ag Sample concentration exceeds solubility limit for this method. Result should be considered a minimum value.
Ah Sample was rerun at a 50x dilution with results below the reporting limit. Original 1x result has been reported.
Ai Samples ran under a passing CCV but ECV results are below established limits. Results should be considered
possible low bias.
Aj Samples ran under a passing CCV but ECV results are below established limits. Results should be considered
possible low bias. RPD value between the primary and secondary column is above range due to 1254 pattern
interference.
Ak Surrogate recovery below range due to sample matrix.
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
CVL CCV result is below the control limits. LCS recovery within the limits. Analyte not detected in the sample. No further
action taken.
D RPD value outside of the control limits.
DM Sample diluted and RL increased due to the matrix.
DO Surrogates diluted out.
E Estimated concentration above the calibration range
IH Internal standard response below the QC limit. Analyte reported with possible high bias.
IN Low Internal Standard response. Compound not detected. No further action taken.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
RL Increased RL because of the sample matrix.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 135
Sample Receipt Summary
08/06/2015
Prism Work Order: 5070245
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5070245-01 07/13/15PR1 07/14/15Solid
5070245-02 07/13/15PR2 07/14/15Solid
5070245-03 07/13/15PR3 07/14/15Solid
5070245-04 07/13/15PR4 07/14/15Solid
5070245-05 07/13/15PR5 07/14/15Solid
5070245-06 07/13/15PR6 07/14/15Solid
5070245-07 07/13/15PR7 07/14/15Solid
5070245-08 07/13/15PR8 07/14/15Solid
5070245-09 07/13/15IR1 07/14/15Solid
5070245-10 07/13/15IR2 07/14/15Solid
5070245-11 07/13/15PR-Pit 1 07/14/15Solid
5070245-12 07/13/15PR-Pit 2 07/14/15Solid
5070245-13 07/13/15PR-Pit 3 07/14/15Solid
5070245-14 07/13/15PR-Pit 4 07/14/15Solid
5070245-15 07/13/15IR-Pit 07/14/15Solid
5070245-16 07/13/15T-1 Totes 07/14/15Solid
5070245-17 07/13/15WO-1 07/14/15Solid
5070245-18 07/13/15E-1 07/14/15Solid
5070245-19 07/14/15PR-Oil 07/14/15Non-aqueous Liquid
5070245-20 07/14/15WO-Wase1 07/14/15Non-aqueous Liquid
5070245-21 07/14/15AG-1 07/14/15Wipe
5070245-22 07/14/15AG-2 07/14/15Wipe
Samples were received in good condition at 3.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 135
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5070245
08/06/2015
Summary of Detections
12 Aa pH Units5070245-01 PR1 Corrosivity-pH *9045D
1800 mg/kg dry5070245-01 PR1 Oil & Grease (HEM)*9071B
0.10 Ai mg/kg dry5070245-01 PR1 Aroclor 1254 8082A
4.2 mg/kg dry5070245-01 PR1 Arsenic *6010C
32 mg/kg dry5070245-01 PR1 Barium *6010C
14 mg/kg dry5070245-01 PR1 Chromium *6010C
11 mg/kg dry5070245-01 PR1 Lead *6010C
0.19 mg/kg dry5070245-01 PR1 Acetone 8260B
0.0036 J mg/kg dry5070245-01 PR1 Benzene 8260B
0.0033 J mg/kg dry5070245-01 PR1 m,p-Xylenes 8260B
0.0041 J mg/kg dry5070245-01 PR1 Methyl Isobutyl Ketone 8260B
0.027 mg/kg dry5070245-01 PR1 Naphthalene 8260B
0.0046 J mg/kg dry5070245-01 PR1 Toluene 8260B
0.0033 J mg/kg dry5070245-01 PR1 Xylenes, total 8260B
12 Aa pH Units5070245-02 PR2 Corrosivity-pH *9045D
520 mg/kg dry5070245-02 PR2 Oil & Grease (HEM)*9071B
0.067 Ai mg/kg dry5070245-02 PR2 Aroclor 1254 8082A
3.8 mg/kg dry5070245-02 PR2 Arsenic *6010C
140 mg/kg dry5070245-02 PR2 Barium *6010C
19 mg/kg dry5070245-02 PR2 Chromium *6010C
3.9 mg/kg dry5070245-02 PR2 Lead *6010C
0.11 mg/kg dry5070245-02 PR2 Acetone 8260B
0.042 J mg/kg dry5070245-02 PR2 Methyl Isobutyl Ketone 8260B
12 Aa pH Units5070245-03 PR3 Corrosivity-pH *9045D
15000 mg/kg dry5070245-03 PR3 Oil & Grease (HEM)*9071B
0.42 Ai mg/kg dry5070245-03 PR3 Aroclor 1254 8082A
4.5 mg/kg dry5070245-03 PR3 Arsenic *6010C
86 mg/kg dry5070245-03 PR3 Barium *6010C
20 mg/kg dry5070245-03 PR3 Chromium *6010C
12 mg/kg dry5070245-03 PR3 Lead *6010C
0.27 mg/kg dry5070245-03 PR3 Acetone 8260B
0.023 J mg/kg dry5070245-03 PR3 Methyl Butyl Ketone (2-Hexanone)8260B
0.015 J mg/kg dry5070245-03 PR3 Methyl Isobutyl Ketone 8260B
0.0085 LH mg/kg dry5070245-03 PR3 Styrene 8260B
12 Aa pH Units5070245-04 PR4 Corrosivity-pH *9045D
19000 mg/kg dry5070245-04 PR4 Oil & Grease (HEM)*9071B
1.3 Ae mg/kg dry5070245-04 PR4 Aroclor 1016 8082A
0.54 mg/kg dry5070245-04 PR4 Aroclor 1254 8082A
6.2 mg/kg dry5070245-04 PR4 Arsenic *6010C
99 mg/kg dry5070245-04 PR4 Barium *6010C
27 mg/kg dry5070245-04 PR4 Chromium *6010C
50 mg/kg dry5070245-04 PR4 Lead *6010C
0.0085 J mg/kg dry5070245-04 PR4 1,2,4-Trimethylbenzene 8260B
0.24 mg/kg dry5070245-04 PR4 Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 135
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5070245
08/06/2015
Summary of Detections
0.018 J mg/kg dry5070245-04 PR4 Methyl Isobutyl Ketone 8260B
12 Aa pH Units5070245-05 PR5 Corrosivity-pH *9045D
21000 mg/kg dry5070245-05 PR5 Oil & Grease (HEM)*9071B
0.19 Ai mg/kg dry5070245-05 PR5 Aroclor 1254 8082A
0.54 J mg/kg dry5070245-05 PR5 Naphthalene 8270D
5.4 mg/kg dry5070245-05 PR5 Arsenic *6010C
89 mg/kg dry5070245-05 PR5 Barium *6010C
29 mg/kg dry5070245-05 PR5 Chromium *6010C
88 mg/kg dry5070245-05 PR5 Lead *6010C
0.079 mg/kg dry5070245-05 PR5 1,2,4-Trimethylbenzene 8260B
0.030 J mg/kg dry5070245-05 PR5 1,3,5-Trimethylbenzene 8260B
0.78 mg/kg dry5070245-05 PR5 Acetone 8260B
0.061 J mg/kg dry5070245-05 PR5 m,p-Xylenes 8260B
0.11 J mg/kg dry5070245-05 PR5 Methyl Isobutyl Ketone 8260B
0.31 mg/kg dry5070245-05 PR5 Naphthalene 8260B
0.024 J mg/kg dry5070245-05 PR5 o-Xylene 8260B
0.034 J mg/kg dry5070245-05 PR5 Toluene 8260B
0.085 J mg/kg dry5070245-05 PR5 Xylenes, total 8260B
12 Aa pH Units5070245-06 PR6 Corrosivity-pH *9045D
18000 mg/kg dry5070245-06 PR6 Oil & Grease (HEM)*9071B
0.11 Ai mg/kg dry5070245-06 PR6 Aroclor 1254 8082A
7.7 mg/kg dry5070245-06 PR6 Arsenic *6010C
160 mg/kg dry5070245-06 PR6 Barium *6010C
25 mg/kg dry5070245-06 PR6 Chromium *6010C
15 mg/kg dry5070245-06 PR6 Lead *6010C
0.25 J mg/kg dry5070245-06 PR6 Acetone 8260B
0.020 J mg/kg dry5070245-06 PR6 Methyl Isobutyl Ketone 8260B
12 Aa pH Units5070245-07 PR7 Corrosivity-pH *9045D
15000 mg/kg dry5070245-07 PR7 Oil & Grease (HEM)*9071B
0.20 Ai mg/kg dry5070245-07 PR7 Aroclor 1254 8082A
0.89 J mg/kg dry5070245-07 PR7 Naphthalene 8270D
7.0 mg/kg dry5070245-07 PR7 Arsenic *6010C
75 mg/kg dry5070245-07 PR7 Barium *6010C
22 mg/kg dry5070245-07 PR7 Chromium *6010C
240 mg/kg dry5070245-07 PR7 Lead *6010C
0.029 mg/kg dry5070245-07 PR7 1,2,4-Trimethylbenzene 8260B
0.010 mg/kg dry5070245-07 PR7 1,3,5-Trimethylbenzene 8260B
0.0032 J mg/kg dry5070245-07 PR7 4-Isopropyltoluene 8260B
0.15 mg/kg dry5070245-07 PR7 Acetone 8260B
0.0049 J mg/kg dry5070245-07 PR7 Methyl Isobutyl Ketone 8260B
0.0045 J mg/kg dry5070245-07 PR7 n-Butylbenzene 8260B
0.0047 J mg/kg dry5070245-07 PR7 sec-Butylbenzene 8260B
5.0 mg/kg dry5070245-07 PR7 Naphthalene 8260B
12 Aa pH Units5070245-08 PR8 Corrosivity-pH *9045D
7100 mg/kg dry5070245-08 PR8 Oil & Grease (HEM)*9071B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 135
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5070245
08/06/2015
Summary of Detections
0.10 Ai mg/kg dry5070245-08 PR8 Aroclor 1254 8082A
1.6 J mg/kg dry5070245-08 PR8 Naphthalene 8270D
7.4 mg/kg dry5070245-08 PR8 Arsenic *6010C
78 mg/kg dry5070245-08 PR8 Barium *6010C
17 mg/kg dry5070245-08 PR8 Chromium *6010C
26 mg/kg dry5070245-08 PR8 Lead *6010C
0.012 mg/kg dry5070245-08 PR8 1,2,4-Trimethylbenzene 8260B
0.0040 J mg/kg dry5070245-08 PR8 1,3,5-Trimethylbenzene 8260B
0.086 mg/kg dry5070245-08 PR8 Acetone 8260B
0.0036 J mg/kg dry5070245-08 PR8 Methyl Isobutyl Ketone 8260B
0.0038 J mg/kg dry5070245-08 PR8 Toluene 8260B
2.9 mg/kg dry5070245-08 PR8 Naphthalene 8260B
12 Aa pH Units5070245-09 IR1 Corrosivity-pH *9045D
1600 mg/kg dry5070245-09 IR1 Oil & Grease (HEM)*9071B
17 Ai mg/kg dry5070245-09 IR1 Aroclor 1254 8082A
29 mg/kg dry5070245-09 IR1 Arsenic *6010C
54 mg/kg dry5070245-09 IR1 Barium *6010C
77 mg/kg dry5070245-09 IR1 Chromium *6010C
2.6 mg/kg dry5070245-09 IR1 Lead *6010C
0.17 mg/kg dry5070245-09 IR1 Acetone 8260B
0.038 J mg/kg dry5070245-09 IR1 Methyl Isobutyl Ketone 8260B
12 Aa pH Units5070245-10 IR2 Corrosivity-pH *9045D
3600 mg/kg dry5070245-10 IR2 Oil & Grease (HEM)*9071B
17 Ai mg/kg dry5070245-10 IR2 Aroclor 1254 8082A
0.11 J mg/kg dry5070245-10 IR2 Fluoranthene 8270D
0.12 J mg/kg dry5070245-10 IR2 Phenanthrene 8270D
0.45 mg/kg dry5070245-10 IR2 Pyrene 8270D
28 mg/kg dry5070245-10 IR2 Arsenic *6010C
46 mg/kg dry5070245-10 IR2 Barium *6010C
65 mg/kg dry5070245-10 IR2 Chromium *6010C
1.7 mg/kg dry5070245-10 IR2 Lead *6010C
0.018 mg/kg dry5070245-10 IR2 1,2,4-Trimethylbenzene 8260B
0.0066 J mg/kg dry5070245-10 IR2 1,3,5-Trimethylbenzene 8260B
0.14 mg/kg dry5070245-10 IR2 Acetone 8260B
0.015 J mg/kg dry5070245-10 IR2 m,p-Xylenes 8260B
0.014 J mg/kg dry5070245-10 IR2 Methyl Isobutyl Ketone 8260B
0.0087 J mg/kg dry5070245-10 IR2 Naphthalene 8260B
0.0068 J mg/kg dry5070245-10 IR2 o-Xylene 8260B
0.022 J mg/kg dry5070245-10 IR2 Xylenes, total 8260B
8.0 pH Units5070245-11 PR-Pit 1 Corrosivity-pH *9045D
230000 mg/kg dry5070245-11 PR-Pit 1 Oil & Grease (HEM)*9071B
0.69 Ai, J mg/kg dry5070245-11 PR-Pit 1 Aroclor 1254 8082A
0.16 mg/kg dry5070245-11 PR-Pit 1 Mercury *7471B
4.8 mg/kg dry5070245-11 PR-Pit 1 Arsenic *6010C
120 mg/kg dry5070245-11 PR-Pit 1 Barium *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 135
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5070245
08/06/2015
Summary of Detections
0.29 mg/kg dry5070245-11 PR-Pit 1 Cadmium *6010C
34 mg/kg dry5070245-11 PR-Pit 1 Chromium *6010C
68 mg/kg dry5070245-11 PR-Pit 1 Lead *6010C
0.0055 IH, J mg/kg dry5070245-11 PR-Pit 1 1,2,4-Trimethylbenzene 8260B
2.0 Ac, E mg/kg dry5070245-11 PR-Pit 1 Acetone 8260B
0.0043 J mg/kg dry5070245-11 PR-Pit 1 Benzene 8260B
0.010 J mg/kg dry5070245-11 PR-Pit 1 Methyl Butyl Ketone (2-Hexanone)8260B
0.045 J mg/kg dry5070245-11 PR-Pit 1 Methyl Isobutyl Ketone 8260B
0.0069 IH, J mg/kg dry5070245-11 PR-Pit 1 Naphthalene 8260B
0.011 mg/kg dry5070245-11 PR-Pit 1 Styrene 8260B
0.0096 J mg/kg dry5070245-11 PR-Pit 1 Toluene 8260B
7.6 pH Units5070245-12 PR-Pit 2 Corrosivity-pH *9045D
420000 mg/kg dry5070245-12 PR-Pit 2 Oil & Grease (HEM)*9071B
0.96 Aj mg/kg dry5070245-12 PR-Pit 2 Aroclor 1016 8082A
0.59 Ai mg/kg dry5070245-12 PR-Pit 2 Aroclor 1254 8082A
28 J mg/kg dry5070245-12 PR-Pit 2 1-Methylnaphthalene 8270D
17 J mg/kg dry5070245-12 PR-Pit 2 2-Methylnaphthalene 8270D
15 J mg/kg dry5070245-12 PR-Pit 2 Naphthalene 8270D
0.47 mg/kg dry5070245-12 PR-Pit 2 Mercury *7471B
2.8 mg/kg dry5070245-12 PR-Pit 2 Arsenic *6010C
160 mg/kg dry5070245-12 PR-Pit 2 Barium *6010C
2.4 mg/kg dry5070245-12 PR-Pit 2 Cadmium *6010C
24 mg/kg dry5070245-12 PR-Pit 2 Chromium *6010C
140 mg/kg dry5070245-12 PR-Pit 2 Lead *6010C
0.61 mg/kg dry5070245-12 PR-Pit 2 Silver *6010C
0.026 IH mg/kg dry5070245-12 PR-Pit 2 1,2,4-Trimethylbenzene 8260B
0.014 IH mg/kg dry5070245-12 PR-Pit 2 1,4-Dichlorobenzene 8260B
0.016 IH mg/kg dry5070245-12 PR-Pit 2 4-Isopropyltoluene 8260B
3.8 Ac, E mg/kg dry5070245-12 PR-Pit 2 Acetone 8260B
0.0054 J mg/kg dry5070245-12 PR-Pit 2 m,p-Xylenes 8260B
0.028 J mg/kg dry5070245-12 PR-Pit 2 Methyl Butyl Ketone (2-Hexanone)8260B
0.24 J mg/kg dry5070245-12 PR-Pit 2 Methyl Ethyl Ketone (2-Butanone)8260B
0.057 J mg/kg dry5070245-12 PR-Pit 2 Methyl Isobutyl Ketone 8260B
0.026 IH mg/kg dry5070245-12 PR-Pit 2 Naphthalene 8260B
0.0054 J mg/kg dry5070245-12 PR-Pit 2 Styrene 8260B
0.015 mg/kg dry5070245-12 PR-Pit 2 Toluene 8260B
0.0054 J mg/kg dry5070245-12 PR-Pit 2 Xylenes, total 8260B
7.0 pH Units5070245-13 PR-Pit 3 Corrosivity-pH *9045D
250000 mg/kg dry5070245-13 PR-Pit 3 Oil & Grease (HEM)*9071B
0.17 Aj mg/kg dry5070245-13 PR-Pit 3 Aroclor 1016 8082A
0.12 J, Ai mg/kg dry5070245-13 PR-Pit 3 Aroclor 1254 8082A
7.3 mg/kg dry5070245-13 PR-Pit 3 Arsenic *6010C
180 mg/kg dry5070245-13 PR-Pit 3 Barium *6010C
40 mg/kg dry5070245-13 PR-Pit 3 Chromium *6010C
22 mg/kg dry5070245-13 PR-Pit 3 Lead *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 135
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5070245
08/06/2015
Summary of Detections
0.64 mg/kg dry5070245-13 PR-Pit 3 Acetone 8260B
0.033 J mg/kg dry5070245-13 PR-Pit 3 Methyl Isobutyl Ketone 8260B
0.012 J mg/kg dry5070245-13 PR-Pit 3 Toluene 8260B
3.8 pH Units5070245-14 PR-Pit 4 Corrosivity-pH *9045D
250000 mg/kg dry5070245-14 PR-Pit 4 Oil & Grease (HEM)*9071B
5.5 mg/kg dry5070245-14 PR-Pit 4 Arsenic *6010C
130 mg/kg dry5070245-14 PR-Pit 4 Barium *6010C
37 mg/kg dry5070245-14 PR-Pit 4 Chromium *6010C
17 mg/kg dry5070245-14 PR-Pit 4 Lead *6010C
0.46 mg/kg dry5070245-14 PR-Pit 4 Acetone 8260B
0.0065 mg/kg dry5070245-14 PR-Pit 4 Benzene 8260B
0.030 J mg/kg dry5070245-14 PR-Pit 4 Methyl Butyl Ketone (2-Hexanone)8260B
0.010 J mg/kg dry5070245-14 PR-Pit 4 Methyl Isobutyl Ketone 8260B
0.0068 J mg/kg dry5070245-14 PR-Pit 4 Toluene 8260B
8.3 pH Units5070245-15 IR-Pit Corrosivity-pH *9045D
35000 mg/kg dry5070245-15 IR-Pit Oil & Grease (HEM)*9071B
0.48 Ai mg/kg dry5070245-15 IR-Pit Aroclor 1016 8082A
1.5 Ai mg/kg dry5070245-15 IR-Pit Aroclor 1254 8082A
43 J mg/kg dry5070245-15 IR-Pit 1-Methylnaphthalene 8270D
21 J mg/kg dry5070245-15 IR-Pit Naphthalene 8270D
100 DM mg/kg dry5070245-15 IR-Pit Arsenic *6010C
20 DM mg/kg dry5070245-15 IR-Pit Barium *6010C
79000 mg/kg dry5070245-15 IR-Pit Chromium *6010C
15 DM mg/kg dry5070245-15 IR-Pit Lead *6010C
0.0061 J mg/kg dry5070245-15 IR-Pit 1,4-Dichlorobenzene 8260B
4.0 Ah, E mg/kg dry5070245-15 IR-Pit Acetone 8260B
0.20 J mg/kg dry5070245-15 IR-Pit Methyl Ethyl Ketone (2-Butanone)8260B
0.10 J mg/kg dry5070245-15 IR-Pit Methyl Isobutyl Ketone 8260B
0.0068 LH, J mg/kg dry5070245-15 IR-Pit Styrene 8260B
8.1 pH Units5070245-16 T-1 Totes Corrosivity-pH *9045D
5400 mg/kg dry5070245-16 T-1 Totes Oil & Grease (HEM)*9071B
150 mg/kg dry5070245-16 T-1 Totes Barium *6010C
4.5 mg/kg dry5070245-16 T-1 Totes Chromium *6010C
5.4 E mg/kg dry5070245-16 T-1 Totes Acetone 8260B
0.012 mg/kg dry5070245-16 T-1 Totes Ethylbenzene 8260B
0.031 mg/kg dry5070245-16 T-1 Totes Isopropylbenzene (Cumene)8260B
0.017 J mg/kg dry5070245-16 T-1 Totes m,p-Xylenes 8260B
0.038 J mg/kg dry5070245-16 T-1 Totes Methyl Isobutyl Ketone 8260B
0.014 mg/kg dry5070245-16 T-1 Totes n-Propylbenzene 8260B
0.51 Ad, E mg/kg dry5070245-16 T-1 Totes Styrene 8260B
0.012 mg/kg dry5070245-16 T-1 Totes Toluene 8260B
0.017 J mg/kg dry5070245-16 T-1 Totes Xylenes, total 8260B
12 Aa pH Units5070245-17 WO-1 Corrosivity-pH *9045D
1700 mg/kg dry5070245-17 WO-1 Oil & Grease (HEM)*9071B
1.2 Ai mg/kg dry5070245-17 WO-1 Aroclor 1254 8082A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 135
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5070245
08/06/2015
Summary of Detections
13 mg/kg dry5070245-17 WO-1 Arsenic *6010C
30 mg/kg dry5070245-17 WO-1 Barium *6010C
18 mg/kg dry5070245-17 WO-1 Chromium *6010C
7.7 mg/kg dry5070245-17 WO-1 Lead *6010C
0.12 mg/kg dry5070245-17 WO-1 Acetone 8260B
0.0043 J mg/kg dry5070245-17 WO-1 Methyl Isobutyl Ketone 8260B
0.022 mg/kg dry5070245-17 WO-1 Naphthalene 8260B
12 Aa pH Units5070245-18 E-1 Corrosivity-pH *9045D
490 mg/kg dry5070245-18 E-1 Oil & Grease (HEM)*9071B
2.5 Aj mg/kg dry5070245-18 E-1 Aroclor 1016 8082A
1.6 Ai mg/kg dry5070245-18 E-1 Aroclor 1254 8082A
21 DM mg/kg dry5070245-18 E-1 Arsenic *6010C
56 DM mg/kg dry5070245-18 E-1 Barium *6010C
26 DM mg/kg dry5070245-18 E-1 Chromium *6010C
100 DM mg/kg dry5070245-18 E-1 Lead *6010C
0.11 mg/kg dry5070245-18 E-1 Acetone 8260B
0.0038 J mg/kg dry5070245-18 E-1 Methyl Isobutyl Ketone 8260B
7.9 Aa pH Units5070245-19 PR-Oil pH *9045D
1.5 mg/kg wet5070245-19 PR-Oil Barium *6010C
6.0 mg/kg wet5070245-19 PR-Oil Lead *6010C
2700 J mg/kg5070245-19 PR-Oil 1,2,4-Trimethylbenzene 8260B
7.4 Aa pH Units5070245-20 WO-Wase1 pH *9045D
1.7 mg/kg wet5070245-20 WO-Wase1 Barium *6010C
0.38 mg/kg wet5070245-20 WO-Wase1 Chromium *6010C
0.54 mg/kg wet5070245-20 WO-Wase1 Lead *6010C
10 pH Units5070245-21 AG-1 Corrosivity-pH *9045D
0.89 mg/kg wet5070245-21 AG-1 Chromium *6010C
11 mg/kg wet5070245-21 AG-1 Silver *6010C
8.4 pH Units5070245-22 AG-2 Corrosivity-pH *9045D
0.94 mg/kg wet5070245-22 AG-2 Barium *6010C
5.8 mg/kg wet5070245-22 AG-2 Chromium *6010C
800 Ag mg/kg wet5070245-22 AG-2 Silver *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR1
Prism Sample ID: 5070245-01
Prism Work Order: 5070245
Time Collected: 07/13/15 09:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
98.2 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
1800 *9071B P5G02421417/15/15 10:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.051 7/28/15 22:09 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 22:09 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 22:09 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.051 7/28/15 22:09 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.051 7/28/15 22:09 JMCAimg/kg dry 0.010Aroclor 1248
0.10 8082A P5G028410.051 7/28/15 22:09 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.051 7/28/15 22:09 JMCAimg/kg dry 0.0070Aroclor 1260
Surrogate Recovery Control Limits
36-18277 %Tetrachloro-m-xylene
34-18277 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.971-Methylnaphthalene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.812-Methylnaphthalene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.69Acenaphthene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.73Acenaphthylene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.81Anthracene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.66Benzo(a)anthracene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVCCVmg/kg dry 0.55Benzo(a)pyrene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVCCVmg/kg dry 0.59Benzo(b)fluoranthene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVCCVmg/kg dry 0.55Benzo(g,h,i)perylene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVCCVmg/kg dry 0.66Benzo(k)fluoranthene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.64Chrysene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVCCVmg/kg dry 0.61Dibenzo(a,h)anthracene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.64Fluoranthene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.72Fluorene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVCCVmg/kg dry 0.58Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.81Naphthalene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.66Phenanthrene
BRL 8270D P5G032955.0 8/3/15 12:01 JMVmg/kg dry 0.67Pyrene
Surrogate Recovery Control Limits
44-11576 %2-Fluorobiphenyl
37-12267 %Nitrobenzene-d5
54-12780 %Terphenyl-d14
Total Metals
BRL *7471B P5G027010.021 7/16/15 14:27 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR1
Prism Sample ID: 5070245-01
Prism Work Order: 5070245
Time Collected: 07/13/15 09:00
Time Submitted: 07/14/15 11:30
4.2 *6010C P5G029410.25 7/20/15 14:17 MWWmg/kg dry 0.035Arsenic
32 *6010C P5G029410.50 7/17/15 22:59 MWWmg/kg dry 0.095Barium
BRL *6010C P5G029410.25 7/17/15 22:59 MWWmg/kg dry 0.035Cadmium
14 *6010C P5G029410.25 7/20/15 14:17 MWWmg/kg dry 0.041Chromium
11 *6010C P5G029410.25 7/20/15 14:17 MWWmg/kg dry 0.038Lead
BRL *6010C P5G029410.50 7/17/15 22:59 MWWmg/kg dry 0.060Selenium
BRL *6010C P5G029410.25 7/17/15 22:59 MWWmg/kg dry 0.028Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCLHmg/kg dry 0.000531,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000311,1,1-Trichloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000441,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000571,1,2-Trichloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000351,1-Dichloropropylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000371,2,3-Trichlorobenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000821,2,3-Trichloropropane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000481,2,4-Trichlorobenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000491,2,4-Trimethylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000261,2-Dibromoethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000391,2-Dichloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000401,2-Dichloropropane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000491,3,5-Trimethylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000431,3-Dichlorobenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000321,3-Dichloropropane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000312,2-Dichloropropane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000332-Chlorotoluene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000394-Chlorotoluene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.000314-Isopropyltoluene
0.19 8260B P5G031810.065 7/18/15 12:51 MSCmg/kg dry 0.0016Acetone
0.0036 8260B P5G031810.0039 7/18/15 12:51 MSCJmg/kg dry 0.00038Benzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00054Bromobenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00036Bromochloromethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00036Bromodichloromethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00073Bromoform
BRL 8260B P5G031810.013 7/18/15 12:51 MSCmg/kg dry 0.00080Bromomethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00032Carbon Tetrachloride
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00034Chlorobenzene
BRL 8260B P5G031810.013 7/18/15 12:51 MSCmg/kg dry 0.00054Chloroethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00047Chloroform
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00043Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR1
Prism Sample ID: 5070245-01
Prism Work Order: 5070245
Time Collected: 07/13/15 09:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00029Dichlorodifluoromethane
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00025Ethylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCLHmg/kg dry 0.00038Isopropylbenzene (Cumene)
0.0033 8260B P5G031810.013 7/18/15 12:51 MSCJmg/kg dry 0.00060m,p-Xylenes
BRL 8260B P5G031810.065 7/18/15 12:51 MSCmg/kg dry 0.00058Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.13 7/18/15 12:51 MSCmg/kg dry 0.00058Methyl Ethyl Ketone (2-Butanone)
0.0041 8260B P5G031810.065 7/18/15 12:51 MSCJmg/kg dry 0.00055Methyl Isobutyl Ketone
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00036Methylene Chloride
BRL 8260B P5G031810.013 7/18/15 12:51 MSCmg/kg dry 0.00021Methyl-tert-Butyl Ether
0.027 8260B P5G031810.013 7/18/15 12:51 MSCmg/kg dry 0.00020Naphthalene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00033n-Butylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00038n-Propylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00027o-Xylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00031sec-Butylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCLHmg/kg dry 0.00039Styrene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00031Tetrachloroethylene
0.0046 8260B P5G031810.0065 7/18/15 12:51 MSCJmg/kg dry 0.00037Toluene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00039trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00034trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00042Trichloroethylene
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00042Trichlorofluoromethane
BRL 8260B P5G031810.032 7/18/15 12:51 MSCmg/kg dry 0.00089Vinyl acetate
BRL 8260B P5G031810.0065 7/18/15 12:51 MSCmg/kg dry 0.00031Vinyl chloride
0.0033 8260B P5G031810.019 7/18/15 12:51 MSCJmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13089 %4-Bromofluorobenzene
84-12363 %Dibromofluoromethane SR
76-12985 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR2
Prism Sample ID: 5070245-02
Prism Work Order: 5070245
Time Collected: 07/13/15 09:10
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
98.5 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
520 *9071B P5G02421417/15/15 10:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.051 7/28/15 22:21 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 22:21 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 22:21 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.051 7/28/15 22:21 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.051 7/28/15 22:21 JMCAimg/kg dry 0.010Aroclor 1248
0.067 8082A P5G028410.051 7/28/15 22:21 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.051 7/28/15 22:21 JMCAimg/kg dry 0.0070Aroclor 1260
Surrogate Recovery Control Limits
36-18281 %Tetrachloro-m-xylene
34-18276 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.321-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.24Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.27Anthracene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVCCVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVCCVmg/kg dry 0.19Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVCCVmg/kg dry 0.18Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.21Chrysene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVCCVmg/kg dry 0.20Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.21Fluoranthene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.24Fluorene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVCCVmg/kg dry 0.19Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.27Naphthalene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 12:23 JMVmg/kg dry 0.22Pyrene
Surrogate Recovery Control Limits
44-11563 %2-Fluorobiphenyl
37-12254 %Nitrobenzene-d5
54-12768 %Terphenyl-d14
Total Metals
BRL *7471B P5G027010.019 7/16/15 14:41 JABmg/kg dry 0.0012Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR2
Prism Sample ID: 5070245-02
Prism Work Order: 5070245
Time Collected: 07/13/15 09:10
Time Submitted: 07/14/15 11:30
3.8 *6010C P5G029410.25 7/20/15 14:43 MWWmg/kg dry 0.036Arsenic
140 *6010C P5G029410.50 7/17/15 23:29 MWWmg/kg dry 0.096Barium
BRL *6010C P5G029410.25 7/17/15 23:29 MWWmg/kg dry 0.036Cadmium
19 *6010C P5G029410.25 7/17/15 23:29 MWWmg/kg dry 0.041Chromium
3.9 *6010C P5G029410.25 7/20/15 14:43 MWWmg/kg dry 0.038Lead
BRL *6010C P5G029410.50 7/17/15 23:29 MWWmg/kg dry 0.060Selenium
BRL *6010C P5G029410.25 7/17/15 23:29 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCLHmg/kg dry 0.000731,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000431,1,1-Trichloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000601,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000791,1,2-Trichloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000251,1-Dichloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000391,1-Dichloroethylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000491,1-Dichloropropylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000511,2,3-Trichlorobenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00111,2,3-Trichloropropane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000661,2,4-Trichlorobenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000681,2,4-Trimethylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000361,2-Dibromoethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000421,2-Dichlorobenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000531,2-Dichloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000551,2-Dichloropropane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000671,3,5-Trimethylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000591,3-Dichlorobenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000451,3-Dichloropropane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000351,4-Dichlorobenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000422,2-Dichloropropane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000462-Chlorotoluene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000534-Chlorotoluene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.000434-Isopropyltoluene
0.11 8260B P5G031810.089 7/18/15 13:20 MSCmg/kg dry 0.0022Acetone
BRL 8260B P5G031810.0053 7/18/15 13:20 MSCmg/kg dry 0.00052Benzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00074Bromobenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00049Bromochloromethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00050Bromodichloromethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.0010Bromoform
BRL 8260B P5G031810.018 7/18/15 13:20 MSCmg/kg dry 0.0011Bromomethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00044Carbon Tetrachloride
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00047Chlorobenzene
BRL 8260B P5G031810.018 7/18/15 13:20 MSCmg/kg dry 0.00074Chloroethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00064Chloroform
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00060Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR2
Prism Sample ID: 5070245-02
Prism Work Order: 5070245
Time Collected: 07/13/15 09:10
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00038cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00030cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00037Dibromochloromethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00040Dichlorodifluoromethane
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00034Ethylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00036Isopropyl Ether
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCLHmg/kg dry 0.00053Isopropylbenzene (Cumene)
BRL 8260B P5G031810.018 7/18/15 13:20 MSCmg/kg dry 0.00082m,p-Xylenes
BRL 8260B P5G031810.089 7/18/15 13:20 MSCmg/kg dry 0.00080Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.18 7/18/15 13:20 MSCmg/kg dry 0.00080Methyl Ethyl Ketone (2-Butanone)
0.042 8260B P5G031810.089 7/18/15 13:20 MSCJmg/kg dry 0.00076Methyl Isobutyl Ketone
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00050Methylene Chloride
BRL 8260B P5G031810.018 7/18/15 13:20 MSCmg/kg dry 0.00028Methyl-tert-Butyl Ether
BRL 8260B P5G031810.018 7/18/15 13:20 MSCmg/kg dry 0.00028Naphthalene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00045n-Butylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00053n-Propylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00037o-Xylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00043sec-Butylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCLHmg/kg dry 0.00054Styrene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00030tert-Butylbenzene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00042Tetrachloroethylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00051Toluene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00053trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00047trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00058Trichloroethylene
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00058Trichlorofluoromethane
BRL 8260B P5G031810.045 7/18/15 13:20 MSCmg/kg dry 0.0012Vinyl acetate
BRL 8260B P5G031810.0089 7/18/15 13:20 MSCmg/kg dry 0.00043Vinyl chloride
BRL 8260B P5G031810.027 7/18/15 13:20 MSCmg/kg dry 0.0017Xylenes, total
Surrogate Recovery Control Limits
70-13087 %4-Bromofluorobenzene
84-12388 %Dibromofluoromethane
76-12985 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR3
Prism Sample ID: 5070245-03
Prism Work Order: 5070245
Time Collected: 07/13/15 09:20
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
98.1 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
15000 *9071B P5G02421417/15/15 10:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.051 7/28/15 22:33 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 22:33 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 22:33 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.051 7/28/15 22:33 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.051 7/28/15 22:33 JMCAimg/kg dry 0.010Aroclor 1248
0.42 8082A P5G028410.051 7/28/15 22:33 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.051 7/28/15 22:33 JMCAimg/kg dry 0.0070Aroclor 1260
Surrogate Recovery Control Limits
36-18280 %Tetrachloro-m-xylene
34-18261 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.321-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.24Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.27Anthracene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVCCVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVCCVmg/kg dry 0.19Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVCCVmg/kg dry 0.18Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.21Chrysene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVCCVmg/kg dry 0.20Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.21Fluoranthene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.24Fluorene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVCCVmg/kg dry 0.19Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.27Naphthalene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 10:53 JMVmg/kg dry 0.22Pyrene
Surrogate Recovery Control Limits
44-11542 %2-Fluorobiphenyl SR
37-12236 %Nitrobenzene-d5 SR
54-12743 %Terphenyl-d14 SR
Total Metals
BRL *7471B P5G027010.022 7/16/15 14:46 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR3
Prism Sample ID: 5070245-03
Prism Work Order: 5070245
Time Collected: 07/13/15 09:20
Time Submitted: 07/14/15 11:30
4.5 *6010C P5G029410.26 7/20/15 14:51 MWWmg/kg dry 0.037Arsenic
86 *6010C P5G029410.52 7/17/15 23:37 MWWmg/kg dry 0.10Barium
BRL *6010C P5G029410.26 7/17/15 23:37 MWWmg/kg dry 0.037Cadmium
20 *6010C P5G029410.26 7/17/15 23:37 MWWmg/kg dry 0.043Chromium
12 *6010C P5G029410.26 7/20/15 14:51 MWWmg/kg dry 0.040Lead
BRL *6010C P5G029410.52 7/17/15 23:37 MWWmg/kg dry 0.063Selenium
BRL *6010C P5G029410.26 7/17/15 23:37 MWWmg/kg dry 0.030Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCLHmg/kg dry 0.000481,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000281,1,1-Trichloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000521,1,2-Trichloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000321,1-Dichloropropylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000331,2,3-Trichlorobenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000751,2,3-Trichloropropane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000441,2,4-Trichlorobenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000361,2-Dichloropropane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000441,3,5-Trimethylbenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000354-Chlorotoluene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.000284-Isopropyltoluene
0.27 8260B P5G031810.059 7/18/15 13:48 MSCmg/kg dry 0.0014Acetone
BRL 8260B P5G031810.0035 7/18/15 13:48 MSCmg/kg dry 0.00034Benzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00049Bromobenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00032Bromochloromethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00067Bromoform
BRL 8260B P5G031810.012 7/18/15 13:48 MSCmg/kg dry 0.00072Bromomethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00031Chlorobenzene
BRL 8260B P5G031810.012 7/18/15 13:48 MSCmg/kg dry 0.00049Chloroethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00042Chloroform
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00039Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR3
Prism Sample ID: 5070245-03
Prism Work Order: 5070245
Time Collected: 07/13/15 09:20
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00027Dichlorodifluoromethane
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00022Ethylbenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00024Isopropyl Ether
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCLHmg/kg dry 0.00035Isopropylbenzene (Cumene)
BRL 8260B P5G031810.012 7/18/15 13:48 MSCmg/kg dry 0.00054m,p-Xylenes
0.023 8260B P5G031810.059 7/18/15 13:48 MSCJmg/kg dry 0.00053Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.12 7/18/15 13:48 MSCmg/kg dry 0.00053Methyl Ethyl Ketone (2-Butanone)
0.015 8260B P5G031810.059 7/18/15 13:48 MSCJmg/kg dry 0.00050Methyl Isobutyl Ketone
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00033Methylene Chloride
BRL 8260B P5G031810.012 7/18/15 13:48 MSCmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P5G031810.012 7/18/15 13:48 MSCmg/kg dry 0.00019Naphthalene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00030n-Butylbenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00035n-Propylbenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00024o-Xylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00028sec-Butylbenzene
0.0085 8260B P5G031810.0059 7/18/15 13:48 MSCLHmg/kg dry 0.00035Styrene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00028Tetrachloroethylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00034Toluene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00035trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00038Trichloroethylene
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P5G031810.029 7/18/15 13:48 MSCmg/kg dry 0.00080Vinyl acetate
BRL 8260B P5G031810.0059 7/18/15 13:48 MSCmg/kg dry 0.00028Vinyl chloride
BRL 8260B P5G031810.018 7/18/15 13:48 MSCmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-12385 %Dibromofluoromethane
76-12986 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR4
Prism Sample ID: 5070245-04
Prism Work Order: 5070245
Time Collected: 07/13/15 09:30
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
96.3 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
19000 *9071B P5G02421427/15/15 10:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
1.3 8082A P5H0043100.52 8/4/15 20:53 JMCAemg/kg dry 0.049Aroclor 1016
BRL 8082A P5H0043101.0 8/4/15 20:53 JMCmg/kg dry 0.42Aroclor 1221
BRL 8082A P5H0043101.0 8/4/15 20:53 JMCmg/kg dry 0.13Aroclor 1232
BRL 8082A P5H0043100.52 8/4/15 20:53 JMCmg/kg dry 0.14Aroclor 1242
BRL 8082A P5H0043100.52 8/4/15 20:53 JMCmg/kg dry 0.10Aroclor 1248
0.54 8082A P5H0043100.52 8/4/15 20:53 JMCmg/kg dry 0.13Aroclor 1254
BRL 8082A P5H0043100.52 8/4/15 20:53 JMCmg/kg dry 0.072Aroclor 1260
Surrogate Recovery Control Limits
36-18283 %Tetrachloro-m-xylene
34-18254 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.331-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.25Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.28Anthracene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVCCVmg/kg dry 0.19Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVCCVmg/kg dry 0.20Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVCCVmg/kg dry 0.19Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.22Chrysene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVCCVmg/kg dry 0.21Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.22Fluoranthene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.25Fluorene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVCCVmg/kg dry 0.20Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.28Naphthalene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 11:16 JMVmg/kg dry 0.23Pyrene
Surrogate Recovery Control Limits
44-11538 %2-Fluorobiphenyl SR
37-12234 %Nitrobenzene-d5 SR
54-12739 %Terphenyl-d14 SR
Total Metals
BRL *7471B P5G027010.021 7/16/15 14:51 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR4
Prism Sample ID: 5070245-04
Prism Work Order: 5070245
Time Collected: 07/13/15 09:30
Time Submitted: 07/14/15 11:30
6.2 *6010C P5G0294102.6 7/20/15 15:01 MWWmg/kg dry 0.38Arsenic
99 *6010C P5G0294105.3 7/20/15 15:01 MWWmg/kg dry 1.0Barium
BRL *6010C P5G029410.26 7/17/15 23:47 MWWmg/kg dry 0.037Cadmium
27 *6010C P5G0294102.6 7/20/15 15:01 MWWmg/kg dry 0.43Chromium
50 *6010C P5G0294102.6 7/20/15 15:01 MWWmg/kg dry 0.40Lead
BRL *6010C P5G029410.53 7/17/15 23:47 MWWmg/kg dry 0.063Selenium
BRL *6010C P5G029410.26 7/17/15 23:47 MWWmg/kg dry 0.030Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCLHmg/kg dry 0.000761,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000451,1,1-Trichloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000621,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000821,1,2-Trichloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000261,1-Dichloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000411,1-Dichloroethylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000501,1-Dichloropropylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000521,2,3-Trichlorobenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00121,2,3-Trichloropropane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000681,2,4-Trichlorobenzene
0.0085 8260B P5G031810.0092 7/18/15 14:17 MSCJmg/kg dry 0.000701,2,4-Trimethylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000371,2-Dibromoethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000431,2-Dichlorobenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000551,2-Dichloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000571,2-Dichloropropane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000701,3,5-Trimethylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000611,3-Dichlorobenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000461,3-Dichloropropane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000361,4-Dichlorobenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000442,2-Dichloropropane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000482-Chlorotoluene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000554-Chlorotoluene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.000444-Isopropyltoluene
0.24 8260B P5G031810.092 7/18/15 14:17 MSCmg/kg dry 0.0022Acetone
BRL 8260B P5G031810.0055 7/18/15 14:17 MSCmg/kg dry 0.00054Benzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00077Bromobenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00051Bromochloromethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00051Bromodichloromethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.0010Bromoform
BRL 8260B P5G031810.018 7/18/15 14:17 MSCmg/kg dry 0.0011Bromomethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00046Carbon Tetrachloride
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00049Chlorobenzene
BRL 8260B P5G031810.018 7/18/15 14:17 MSCmg/kg dry 0.00077Chloroethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00066Chloroform
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00062Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR4
Prism Sample ID: 5070245-04
Prism Work Order: 5070245
Time Collected: 07/13/15 09:30
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00039cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00031cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00038Dibromochloromethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00042Dichlorodifluoromethane
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00035Ethylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00038Isopropyl Ether
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCLHmg/kg dry 0.00055Isopropylbenzene (Cumene)
BRL 8260B P5G031810.018 7/18/15 14:17 MSCmg/kg dry 0.00085m,p-Xylenes
BRL 8260B P5G031810.092 7/18/15 14:17 MSCmg/kg dry 0.00083Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.18 7/18/15 14:17 MSCmg/kg dry 0.00083Methyl Ethyl Ketone (2-Butanone)
0.018 8260B P5G031810.092 7/18/15 14:17 MSCJmg/kg dry 0.00078Methyl Isobutyl Ketone
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00052Methylene Chloride
BRL 8260B P5G031810.018 7/18/15 14:17 MSCmg/kg dry 0.00029Methyl-tert-Butyl Ether
BRL 8260B P5G031810.018 7/18/15 14:17 MSCmg/kg dry 0.00029Naphthalene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00047n-Butylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00055n-Propylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00038o-Xylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00045sec-Butylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCLHmg/kg dry 0.00055Styrene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00031tert-Butylbenzene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00044Tetrachloroethylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00053Toluene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00055trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00048trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00060Trichloroethylene
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00059Trichlorofluoromethane
BRL 8260B P5G031810.046 7/18/15 14:17 MSCmg/kg dry 0.0013Vinyl acetate
BRL 8260B P5G031810.0092 7/18/15 14:17 MSCmg/kg dry 0.00045Vinyl chloride
BRL 8260B P5G031810.028 7/18/15 14:17 MSCmg/kg dry 0.0017Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
84-12388 %Dibromofluoromethane
76-12984 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR5
Prism Sample ID: 5070245-05
Prism Work Order: 5070245
Time Collected: 07/13/15 09:40
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.2 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
21000 *9071B P5G03371417/16/15 11:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.051 7/28/15 22:44 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 22:44 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 22:44 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.051 7/28/15 22:44 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.051 7/28/15 22:44 JMCAimg/kg dry 0.010Aroclor 1248
0.19 8082A P5G028410.051 7/28/15 22:44 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.051 7/28/15 22:44 JMCAimg/kg dry 0.0071Aroclor 1260
Surrogate Recovery Control Limits
36-18269 %Tetrachloro-m-xylene
34-18273 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.331-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.25Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.27Anthracene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVCCVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVCCVmg/kg dry 0.20Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVCCVmg/kg dry 0.19Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.21Chrysene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVCCVmg/kg dry 0.21Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.22Fluoranthene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.24Fluorene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVCCVmg/kg dry 0.19Indeno(1,2,3-cd)pyrene
0.54 8270D P5G032951.7 8/3/15 11:38 JMVJmg/kg dry 0.27Naphthalene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 11:38 JMVmg/kg dry 0.22Pyrene
Surrogate Recovery Control Limits
44-11545 %2-Fluorobiphenyl
37-12240 %Nitrobenzene-d5
54-12746 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.020 7/16/15 14:55 JABmg/kg dry 0.0013Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR5
Prism Sample ID: 5070245-05
Prism Work Order: 5070245
Time Collected: 07/13/15 09:40
Time Submitted: 07/14/15 11:30
5.4 *6010C P5G0294102.6 7/20/15 15:09 MWWmg/kg dry 0.37Arsenic
89 *6010C P5G0294105.1 7/20/15 15:09 MWWmg/kg dry 0.99Barium
BRL *6010C P5G029410.26 7/17/15 23:58 MWWmg/kg dry 0.036Cadmium
29 *6010C P5G0294102.6 7/20/15 15:09 MWWmg/kg dry 0.42Chromium
88 *6010C P5G0294102.6 7/20/15 15:09 MWWmg/kg dry 0.39Lead
BRL *6010C P5G029410.51 7/17/15 23:58 MWWmg/kg dry 0.062Selenium
BRL *6010C P5G029410.26 7/17/15 23:58 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.057 7/18/15 19:33 MSCLHmg/kg dry 0.00471,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00281,1,1-Trichloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00391,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00511,1,2-Trichloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00161,1-Dichloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00251,1-Dichloroethylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00311,1-Dichloropropylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00321,2,3-Trichlorobenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00731,2,3-Trichloropropane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00431,2,4-Trichlorobenzene
0.079 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00441,2,4-Trimethylbenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00231,2-Dibromoethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00271,2-Dichlorobenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00341,2-Dichloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00351,2-Dichloropropane
0.030 8260B P5G031810.057 7/18/15 19:33 MSCJmg/kg dry 0.00431,3,5-Trimethylbenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00381,3-Dichlorobenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00291,3-Dichloropropane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00231,4-Dichlorobenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00272,2-Dichloropropane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00302-Chlorotoluene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00344-Chlorotoluene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.00284-Isopropyltoluene
0.78 8260B P5G031810.57 7/18/15 19:33 MSCmg/kg dry 0.014Acetone
BRL 8260B P5G031810.034 7/18/15 19:33 MSCmg/kg dry 0.0033Benzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0048Bromobenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0031Bromochloromethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0032Bromodichloromethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0065Bromoform
BRL 8260B P5G031810.11 7/18/15 19:33 MSCmg/kg dry 0.0071Bromomethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0028Carbon Tetrachloride
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0030Chlorobenzene
BRL 8260B P5G031810.11 7/18/15 19:33 MSCmg/kg dry 0.0048Chloroethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0041Chloroform
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0038Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR5
Prism Sample ID: 5070245-05
Prism Work Order: 5070245
Time Collected: 07/13/15 09:40
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0024cis-1,2-Dichloroethylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0019cis-1,3-Dichloropropylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0024Dibromochloromethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0026Dichlorodifluoromethane
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0022Ethylbenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0023Isopropyl Ether
BRL 8260B P5G031810.057 7/18/15 19:33 MSCLHmg/kg dry 0.0034Isopropylbenzene (Cumene)
0.061 8260B P5G031810.11 7/18/15 19:33 MSCJmg/kg dry 0.0053m,p-Xylenes
BRL 8260B P5G031810.57 7/18/15 19:33 MSCmg/kg dry 0.0052Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031811.1 7/18/15 19:33 MSCmg/kg dry 0.0052Methyl Ethyl Ketone (2-Butanone)
0.11 8260B P5G031810.57 7/18/15 19:33 MSCJmg/kg dry 0.0049Methyl Isobutyl Ketone
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0032Methylene Chloride
BRL 8260B P5G031810.11 7/18/15 19:33 MSCmg/kg dry 0.0018Methyl-tert-Butyl Ether
0.31 8260B P5G031810.11 7/18/15 19:33 MSCmg/kg dry 0.0018Naphthalene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0029n-Butylbenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0034n-Propylbenzene
0.024 8260B P5G031810.057 7/18/15 19:33 MSCJmg/kg dry 0.0023o-Xylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0028sec-Butylbenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCLHmg/kg dry 0.0034Styrene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0019tert-Butylbenzene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0027Tetrachloroethylene
0.034 8260B P5G031810.057 7/18/15 19:33 MSCJmg/kg dry 0.0033Toluene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0034trans-1,2-Dichloroethylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0030trans-1,3-Dichloropropylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0037Trichloroethylene
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0037Trichlorofluoromethane
BRL 8260B P5G031810.29 7/18/15 19:33 MSCmg/kg dry 0.0078Vinyl acetate
BRL 8260B P5G031810.057 7/18/15 19:33 MSCmg/kg dry 0.0028Vinyl chloride
0.085 8260B P5G031810.17 7/18/15 19:33 MSCJmg/kg dry 0.011Xylenes, total
Surrogate Recovery Control Limits
70-13087 %4-Bromofluorobenzene
84-12379 %Dibromofluoromethane SR
76-12978 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR6
Prism Sample ID: 5070245-06
Prism Work Order: 5070245
Time Collected: 07/13/15 09:50
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.8 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
18000 *9071B P5G03371417/16/15 11:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.051 7/28/15 22:56 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 22:56 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 22:56 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.051 7/28/15 22:56 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.051 7/28/15 22:56 JMCAimg/kg dry 0.010Aroclor 1248
0.11 8082A P5G028410.051 7/28/15 22:56 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.051 7/28/15 22:56 JMCAimg/kg dry 0.0071Aroclor 1260
Surrogate Recovery Control Limits
36-18260 %Tetrachloro-m-xylene
34-18255 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.651-Methylnaphthalene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.542-Methylnaphthalene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.46Acenaphthene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.49Acenaphthylene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.54Anthracene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.44Benzo(a)anthracene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVCCVmg/kg dry 0.37Benzo(a)pyrene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVCCVmg/kg dry 0.39Benzo(b)fluoranthene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVCCVmg/kg dry 0.37Benzo(g,h,i)perylene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVCCVmg/kg dry 0.44Benzo(k)fluoranthene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.43Chrysene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVCCVmg/kg dry 0.41Dibenzo(a,h)anthracene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.43Fluoranthene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.48Fluorene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVCCVmg/kg dry 0.39Indeno(1,2,3-cd)pyrene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.54Naphthalene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.44Phenanthrene
BRL 8270D P5G0329103.4 8/3/15 12:46 JMVmg/kg dry 0.45Pyrene
Surrogate Recovery Control Limits
44-11544 %2-Fluorobiphenyl
37-12238 %Nitrobenzene-d5
54-12745 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.021 7/16/15 15:00 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR6
Prism Sample ID: 5070245-06
Prism Work Order: 5070245
Time Collected: 07/13/15 09:50
Time Submitted: 07/14/15 11:30
7.7 *6010C P5G029410.26 7/20/15 15:29 MWWmg/kg dry 0.037Arsenic
160 *6010C P5G029410.52 7/20/15 15:29 MWWmg/kg dry 0.099Barium
BRL *6010C P5G029410.26 7/18/15 0:20 MWWmg/kg dry 0.037Cadmium
25 *6010C P5G029410.26 7/20/15 15:29 MWWmg/kg dry 0.042Chromium
15 *6010C P5G029410.26 7/20/15 15:29 MWWmg/kg dry 0.039Lead
BRL *6010C P5G029410.52 7/18/15 0:20 MWWmg/kg dry 0.062Selenium
BRL *6010C P5G029410.26 7/18/15 0:20 MWWmg/kg dry 0.030Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.032 7/18/15 14:46 MSCLHmg/kg dry 0.00271,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00161,1,1-Trichloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00221,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00291,1,2-Trichloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.000901,1-Dichloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00141,1-Dichloroethylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00181,1-Dichloropropylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00181,2,3-Trichlorobenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00411,2,3-Trichloropropane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00241,2,4-Trichlorobenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00251,2,4-Trimethylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00131,2-Dibromoethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00151,2-Dichlorobenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00191,2-Dichloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00201,2-Dichloropropane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00241,3,5-Trimethylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00211,3-Dichlorobenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00161,3-Dichloropropane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00131,4-Dichlorobenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00152,2-Dichloropropane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00172-Chlorotoluene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00194-Chlorotoluene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.00164-Isopropyltoluene
0.25 8260B P5G031810.32 7/18/15 14:46 MSCJmg/kg dry 0.0079Acetone
BRL 8260B P5G031810.019 7/18/15 14:46 MSCmg/kg dry 0.0019Benzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0027Bromobenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0018Bromochloromethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0018Bromodichloromethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0037Bromoform
BRL 8260B P5G031810.065 7/18/15 14:46 MSCmg/kg dry 0.0040Bromomethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0016Carbon Tetrachloride
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0017Chlorobenzene
BRL 8260B P5G031810.065 7/18/15 14:46 MSCmg/kg dry 0.0027Chloroethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0023Chloroform
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0022Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR6
Prism Sample ID: 5070245-06
Prism Work Order: 5070245
Time Collected: 07/13/15 09:50
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0014cis-1,2-Dichloroethylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0011cis-1,3-Dichloropropylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0013Dibromochloromethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0015Dichlorodifluoromethane
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0012Ethylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0013Isopropyl Ether
BRL 8260B P5G031810.032 7/18/15 14:46 MSCLHmg/kg dry 0.0019Isopropylbenzene (Cumene)
BRL 8260B P5G031810.065 7/18/15 14:46 MSCmg/kg dry 0.0030m,p-Xylenes
BRL 8260B P5G031810.32 7/18/15 14:46 MSCmg/kg dry 0.0029Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.65 7/18/15 14:46 MSCmg/kg dry 0.0029Methyl Ethyl Ketone (2-Butanone)
0.020 8260B P5G031810.32 7/18/15 14:46 MSCJmg/kg dry 0.0028Methyl Isobutyl Ketone
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0018Methylene Chloride
BRL 8260B P5G031810.065 7/18/15 14:46 MSCmg/kg dry 0.0010Methyl-tert-Butyl Ether
BRL 8260B P5G031810.065 7/18/15 14:46 MSCmg/kg dry 0.0010Naphthalene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0017n-Butylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0019n-Propylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0013o-Xylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0016sec-Butylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCLHmg/kg dry 0.0019Styrene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0011tert-Butylbenzene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0015Tetrachloroethylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0019Toluene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0019trans-1,2-Dichloroethylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0017trans-1,3-Dichloropropylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0021Trichloroethylene
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0021Trichlorofluoromethane
BRL 8260B P5G031810.16 7/18/15 14:46 MSCmg/kg dry 0.0044Vinyl acetate
BRL 8260B P5G031810.032 7/18/15 14:46 MSCmg/kg dry 0.0016Vinyl chloride
BRL 8260B P5G031810.097 7/18/15 14:46 MSCmg/kg dry 0.0061Xylenes, total
Surrogate Recovery Control Limits
70-13089 %4-Bromofluorobenzene
84-12386 %Dibromofluoromethane
76-12983 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR7
Prism Sample ID: 5070245-07
Prism Work Order: 5070245
Time Collected: 07/13/15 10:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.0 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
15000 *9071B P5G03371417/16/15 11:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.052 7/28/15 23:08 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 23:08 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 23:08 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.052 7/28/15 23:08 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.052 7/28/15 23:08 JMCAimg/kg dry 0.010Aroclor 1248
0.20 8082A P5G028410.052 7/28/15 23:08 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.052 7/28/15 23:08 JMCAimg/kg dry 0.0071Aroclor 1260
Surrogate Recovery Control Limits
36-18258 %Tetrachloro-m-xylene
34-18263 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.331-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.25Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.27Anthracene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVCCVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVCCVmg/kg dry 0.20Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVCCVmg/kg dry 0.19Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.21Chrysene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVCCVmg/kg dry 0.21Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.22Fluoranthene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.24Fluorene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVCCVmg/kg dry 0.20Indeno(1,2,3-cd)pyrene
0.89 8270D P5G032951.7 8/3/15 13:08 JMVJmg/kg dry 0.27Naphthalene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 13:08 JMVmg/kg dry 0.23Pyrene
Surrogate Recovery Control Limits
44-11546 %2-Fluorobiphenyl
37-12239 %Nitrobenzene-d5
54-12748 %Terphenyl-d14 SR
Total Metals
BRL *7471B P5G027010.022 7/16/15 15:05 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR7
Prism Sample ID: 5070245-07
Prism Work Order: 5070245
Time Collected: 07/13/15 10:00
Time Submitted: 07/14/15 11:30
7.0 *6010C P5G029410.26 7/20/15 15:38 MWWmg/kg dry 0.037Arsenic
75 *6010C P5G029410.52 7/20/15 15:38 MWWmg/kg dry 0.10Barium
BRL *6010C P5G029410.26 7/18/15 0:30 MWWmg/kg dry 0.037Cadmium
22 *6010C P5G029410.26 7/20/15 15:38 MWWmg/kg dry 0.043Chromium
240 *6010C P5G029410.26 7/20/15 15:38 MWWmg/kg dry 0.040Lead
BRL *6010C P5G029410.52 7/18/15 0:30 MWWmg/kg dry 0.063Selenium
BRL *6010C P5G029410.26 7/18/15 0:30 MWWmg/kg dry 0.030Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCLHmg/kg dry 0.000521,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000561,1,2-Trichloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000801,2,3-Trichloropropane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000471,2,4-Trichlorobenzene
0.029 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000481,2,4-Trimethylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000391,2-Dichloropropane
0.010 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000421,3-Dichlorobenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.000374-Chlorotoluene
0.0032 8260B P5G031810.0063 7/18/15 15:14 MSCJmg/kg dry 0.000304-Isopropyltoluene
0.15 8260B P5G031810.063 7/18/15 15:14 MSCmg/kg dry 0.0015Acetone
BRL 8260B P5G031810.0038 7/18/15 15:14 MSCmg/kg dry 0.00036Benzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00052Bromobenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00034Bromochloromethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00071Bromoform
BRL 8260B P5G031810.013 7/18/15 15:14 MSCmg/kg dry 0.00077Bromomethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00033Chlorobenzene
BRL 8260B P5G031810.013 7/18/15 15:14 MSCmg/kg dry 0.00052Chloroethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00045Chloroform
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00042Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR7
Prism Sample ID: 5070245-07
Prism Work Order: 5070245
Time Collected: 07/13/15 10:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00024Ethylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCLHmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P5G031810.013 7/18/15 15:14 MSCmg/kg dry 0.00058m,p-Xylenes
BRL 8260B P5G031810.063 7/18/15 15:14 MSCmg/kg dry 0.00057Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.13 7/18/15 15:14 MSCmg/kg dry 0.00057Methyl Ethyl Ketone (2-Butanone)
0.0049 8260B P5G031810.063 7/18/15 15:14 MSCJmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00035Methylene Chloride
BRL 8260B P5G031810.013 7/18/15 15:14 MSCmg/kg dry 0.00020Methyl-tert-Butyl Ether
See 8260ML 8260B P5G031810.013 7/18/15 15:14 MSCmg/kg dry 0.00020Naphthalene
0.0045 8260B P5G031810.0063 7/18/15 15:14 MSCJmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00026o-Xylene
0.0047 8260B P5G031810.0063 7/18/15 15:14 MSCJmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCLHmg/kg dry 0.00038Styrene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00036Toluene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00041Trichloroethylene
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00041Trichlorofluoromethane
BRL 8260B P5G031810.031 7/18/15 15:14 MSCmg/kg dry 0.00086Vinyl acetate
BRL 8260B P5G031810.0063 7/18/15 15:14 MSCmg/kg dry 0.00030Vinyl chloride
BRL 8260B P5G031810.019 7/18/15 15:14 MSCmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13089 %4-Bromofluorobenzene
84-12368 %Dibromofluoromethane SR
76-12983 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
5.0 8260B P5G0389500.65 7/21/15 20:02 MSCmg/kg dry 0.049Naphthalene
Surrogate Recovery Control Limits
70-130167 %4-Bromofluorobenzene SR
70-13079 %Dibromofluoromethane
70-130149 %Toluene-d8 SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR8
Prism Sample ID: 5070245-08
Prism Work Order: 5070245
Time Collected: 07/13/15 10:10
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.5 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
7100 *9071B P5G03371417/16/15 11:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.051 7/28/15 23:19 JMCAimg/kg dry 0.0048Aroclor 1016
BRL 8082A P5G028410.10 7/28/15 23:19 JMCAimg/kg dry 0.041Aroclor 1221
BRL 8082A P5G028410.10 7/28/15 23:19 JMCAimg/kg dry 0.013Aroclor 1232
BRL 8082A P5G028410.051 7/28/15 23:19 JMCAimg/kg dry 0.014Aroclor 1242
BRL 8082A P5G028410.051 7/28/15 23:19 JMCAimg/kg dry 0.010Aroclor 1248
0.10 8082A P5G028410.051 7/28/15 23:19 JMCAimg/kg dry 0.013Aroclor 1254
BRL 8082A P5G028410.051 7/28/15 23:19 JMCAimg/kg dry 0.0071Aroclor 1260
Surrogate Recovery Control Limits
36-18253 %Tetrachloro-m-xylene
34-18253 %Decachlorobiphenyl
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.331-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.25Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.27Anthracene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVCCVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVCCVmg/kg dry 0.20Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVCCVmg/kg dry 0.19Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.21Chrysene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVCCVmg/kg dry 0.21Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.22Fluoranthene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.24Fluorene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVCCVmg/kg dry 0.19Indeno(1,2,3-cd)pyrene
1.6 8270D P5G032951.7 8/3/15 13:31 JMVJmg/kg dry 0.27Naphthalene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 13:31 JMVmg/kg dry 0.22Pyrene
Surrogate Recovery Control Limits
44-11554 %2-Fluorobiphenyl
37-12245 %Nitrobenzene-d5
54-12757 %Terphenyl-d14
Total Metals
BRL *7471B P5G027010.021 7/16/15 15:10 JABmg/kg dry 0.0013Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR8
Prism Sample ID: 5070245-08
Prism Work Order: 5070245
Time Collected: 07/13/15 10:10
Time Submitted: 07/14/15 11:30
7.4 *6010C P5G029410.26 7/20/15 15:47 MWWmg/kg dry 0.037Arsenic
78 *6010C P5G029410.51 7/20/15 15:47 MWWmg/kg dry 0.098Barium
BRL *6010C P5G029410.26 7/18/15 0:40 MWWmg/kg dry 0.036Cadmium
17 *6010C P5G029410.26 7/20/15 15:47 MWWmg/kg dry 0.042Chromium
26 *6010C P5G029410.26 7/20/15 15:47 MWWmg/kg dry 0.039Lead
BRL *6010C P5G029410.51 7/18/15 0:40 MWWmg/kg dry 0.061Selenium
BRL *6010C P5G029410.26 7/18/15 0:40 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCLHmg/kg dry 0.000661,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000391,1,1-Trichloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000541,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000711,1,2-Trichloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000221,1-Dichloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000351,1-Dichloroethylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000441,1-Dichloropropylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000461,2,3-Trichlorobenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00101,2,3-Trichloropropane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000601,2,4-Trichlorobenzene
0.012 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000611,2,4-Trimethylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000321,2-Dibromoethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000381,2-Dichlorobenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000481,2-Dichloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000501,2-Dichloropropane
0.0040 8260B P5G031810.0080 7/18/15 15:43 MSCJmg/kg dry 0.000611,3,5-Trimethylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000531,3-Dichlorobenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000401,3-Dichloropropane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000321,4-Dichlorobenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000382,2-Dichloropropane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000412-Chlorotoluene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000484-Chlorotoluene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.000394-Isopropyltoluene
0.086 8260B P5G031810.080 7/18/15 15:43 MSCmg/kg dry 0.0020Acetone
BRL 8260B P5G031810.0048 7/18/15 15:43 MSCmg/kg dry 0.00047Benzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00067Bromobenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00044Bromochloromethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00045Bromodichloromethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00091Bromoform
BRL 8260B P5G031810.016 7/18/15 15:43 MSCmg/kg dry 0.00099Bromomethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00040Carbon Tetrachloride
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00042Chlorobenzene
BRL 8260B P5G031810.016 7/18/15 15:43 MSCmg/kg dry 0.00067Chloroethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00058Chloroform
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00054Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR8
Prism Sample ID: 5070245-08
Prism Work Order: 5070245
Time Collected: 07/13/15 10:10
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00034cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00027cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00033Dibromochloromethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00036Dichlorodifluoromethane
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00031Ethylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00033Isopropyl Ether
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCLHmg/kg dry 0.00047Isopropylbenzene (Cumene)
BRL 8260B P5G031810.016 7/18/15 15:43 MSCmg/kg dry 0.00074m,p-Xylenes
BRL 8260B P5G031810.080 7/18/15 15:43 MSCmg/kg dry 0.00072Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.16 7/18/15 15:43 MSCmg/kg dry 0.00072Methyl Ethyl Ketone (2-Butanone)
0.0036 8260B P5G031810.080 7/18/15 15:43 MSCJmg/kg dry 0.00068Methyl Isobutyl Ketone
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00045Methylene Chloride
BRL 8260B P5G031810.016 7/18/15 15:43 MSCmg/kg dry 0.00026Methyl-tert-Butyl Ether
See 8260ML 8260B P5G031810.016 7/18/15 15:43 MSCmg/kg dry 0.00025Naphthalene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00041n-Butylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00048n-Propylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00033o-Xylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00039sec-Butylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCLHmg/kg dry 0.00048Styrene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00027tert-Butylbenzene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00038Tetrachloroethylene
0.0038 8260B P5G031810.0080 7/18/15 15:43 MSCJmg/kg dry 0.00046Toluene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00048trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00042trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00052Trichloroethylene
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00052Trichlorofluoromethane
BRL 8260B P5G031810.040 7/18/15 15:43 MSCmg/kg dry 0.0011Vinyl acetate
BRL 8260B P5G031810.0080 7/18/15 15:43 MSCmg/kg dry 0.00039Vinyl chloride
BRL 8260B P5G031810.024 7/18/15 15:43 MSCmg/kg dry 0.0015Xylenes, total
Surrogate Recovery Control Limits
70-13086 %4-Bromofluorobenzene
84-12370 %Dibromofluoromethane SR
76-12982 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
2.9 8260B P5G0389500.73 7/21/15 21:10 MSCmg/kg dry 0.056Naphthalene
Surrogate Recovery Control Limits
70-130157 %4-Bromofluorobenzene SR
70-13049 %Dibromofluoromethane SR
70-130141 %Toluene-d8 SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR1
Prism Sample ID: 5070245-09
Prism Work Order: 5070245
Time Collected: 07/13/15 10:20
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.3 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
1600 *9071B P5G03371417/16/15 11:20 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G02841005.1 7/28/15 23:31 JMCAimg/kg dry 0.48Aroclor 1016
BRL 8082A P5G0284100107/28/15 23:31 JMCAimg/kg dry 4.1Aroclor 1221
BRL 8082A P5G0284100107/28/15 23:31 JMCAimg/kg dry 1.3Aroclor 1232
BRL 8082A P5G02841005.1 7/28/15 23:31 JMCAimg/kg dry 1.4Aroclor 1242
BRL 8082A P5G02841005.1 7/28/15 23:31 JMCAimg/kg dry 1.0Aroclor 1248
17 8082A P5G02841005.1 7/28/15 23:31 JMCAimg/kg dry 1.3Aroclor 1254
BRL 8082A P5G02841005.1 7/28/15 23:31 JMCAimg/kg dry 0.71Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.651-Methylnaphthalene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.542-Methylnaphthalene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.46Acenaphthene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.49Acenaphthylene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.55Anthracene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.44Benzo(a)anthracene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVCCVmg/kg dry 0.37Benzo(a)pyrene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVCCVmg/kg dry 0.39Benzo(b)fluoranthene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVCCVmg/kg dry 0.37Benzo(g,h,i)perylene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVCCVmg/kg dry 0.45Benzo(k)fluoranthene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.43Chrysene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVCCVmg/kg dry 0.41Dibenzo(a,h)anthracene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.43Fluoranthene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.49Fluorene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVCCVmg/kg dry 0.39Indeno(1,2,3-cd)pyrene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.55Naphthalene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.44Phenanthrene
BRL 8270D P5G0329103.4 8/3/15 14:16 JMVmg/kg dry 0.45Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.021 7/16/15 15:14 JABmg/kg dry 0.0013Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR1
Prism Sample ID: 5070245-09
Prism Work Order: 5070245
Time Collected: 07/13/15 10:20
Time Submitted: 07/14/15 11:30
29 *6010C P5G0294102.6 7/20/15 15:55 MWWmg/kg dry 0.37Arsenic
54 *6010C P5G0294105.1 7/20/15 15:55 MWWmg/kg dry 0.99Barium
BRL *6010C P5G029410.26 7/18/15 0:50 MWWmg/kg dry 0.036Cadmium
77 *6010C P5G0294102.6 7/20/15 15:55 MWWmg/kg dry 0.42Chromium
2.6 *6010C P5G0294102.6 7/20/15 15:55 MWWmg/kg dry 0.39Lead
BRL *6010C P5G029410.51 7/18/15 0:50 MWWmg/kg dry 0.062Selenium
BRL *6010C P5G029410.26 7/18/15 0:50 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCLHmg/kg dry 0.000511,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000551,1,2-Trichloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000791,2,3-Trichloropropane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000461,2,4-Trichlorobenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000411,3-Dichlorobenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000374-Chlorotoluene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.000304-Isopropyltoluene
0.17 8260B P5G031810.062 7/18/15 16:12 MSCmg/kg dry 0.0015Acetone
BRL 8260B P5G031810.0037 7/18/15 16:12 MSCmg/kg dry 0.00036Benzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00051Bromobenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00034Bromochloromethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00070Bromoform
BRL 8260B P5G031810.012 7/18/15 16:12 MSCmg/kg dry 0.00076Bromomethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00033Chlorobenzene
BRL 8260B P5G031810.012 7/18/15 16:12 MSCmg/kg dry 0.00051Chloroethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00045Chloroform
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00041Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR1
Prism Sample ID: 5070245-09
Prism Work Order: 5070245
Time Collected: 07/13/15 10:20
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00024Ethylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCLHmg/kg dry 0.00036Isopropylbenzene (Cumene)
BRL 8260B P5G031810.012 7/18/15 16:12 MSCmg/kg dry 0.00057m,p-Xylenes
BRL 8260B P5G031810.062 7/18/15 16:12 MSCmg/kg dry 0.00056Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.12 7/18/15 16:12 MSCmg/kg dry 0.00056Methyl Ethyl Ketone (2-Butanone)
0.038 8260B P5G031810.062 7/18/15 16:12 MSCJmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00035Methylene Chloride
BRL 8260B P5G031810.012 7/18/15 16:12 MSCmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P5G031810.012 7/18/15 16:12 MSCmg/kg dry 0.00019Naphthalene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00031n-Butylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00025o-Xylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCLHmg/kg dry 0.00037Styrene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00035Toluene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00040Trichloroethylene
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00040Trichlorofluoromethane
BRL 8260B P5G031810.031 7/18/15 16:12 MSCmg/kg dry 0.00084Vinyl acetate
BRL 8260B P5G031810.0062 7/18/15 16:12 MSCmg/kg dry 0.00030Vinyl chloride
BRL 8260B P5G031810.018 7/18/15 16:12 MSCmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13087 %4-Bromofluorobenzene
84-12383 %Dibromofluoromethane SR
76-12983 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR2
Prism Sample ID: 5070245-10
Prism Work Order: 5070245
Time Collected: 07/13/15 10:30
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.7 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
3600 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G02841005.1 7/28/15 23:42 JMCAimg/kg dry 0.48Aroclor 1016
BRL 8082A P5G0284100107/28/15 23:42 JMCAimg/kg dry 4.1Aroclor 1221
BRL 8082A P5G0284100107/28/15 23:42 JMCAimg/kg dry 1.3Aroclor 1232
BRL 8082A P5G02841005.1 7/28/15 23:42 JMCAimg/kg dry 1.4Aroclor 1242
BRL 8082A P5G02841005.1 7/28/15 23:42 JMCAimg/kg dry 1.0Aroclor 1248
17 8082A P5G02841005.1 7/28/15 23:42 JMCAimg/kg dry 1.3Aroclor 1254
BRL 8082A P5G02841005.1 7/28/15 23:42 JMCAimg/kg dry 0.71Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.0651-Methylnaphthalene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.0542-Methylnaphthalene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.046Acenaphthene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.049Acenaphthylene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.054Anthracene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.044Benzo(a)anthracene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVCCVmg/kg dry 0.037Benzo(a)pyrene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVCCVmg/kg dry 0.039Benzo(b)fluoranthene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVCCVmg/kg dry 0.037Benzo(g,h,i)perylene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVCCVmg/kg dry 0.044Benzo(k)fluoranthene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.043Chrysene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVCCVmg/kg dry 0.041Dibenzo(a,h)anthracene
0.11 8270D P5G032910.34 8/3/15 17:18 JMVJmg/kg dry 0.043Fluoranthene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.049Fluorene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVCCVmg/kg dry 0.039Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.054Naphthalene
0.12 8270D P5G032910.34 8/3/15 17:18 JMVJmg/kg dry 0.044Phenanthrene
0.45 8270D P5G032910.34 8/3/15 17:18 JMVmg/kg dry 0.045Pyrene
Surrogate Recovery Control Limits
44-11550 %2-Fluorobiphenyl
37-12245 %Nitrobenzene-d5
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.022 7/16/15 15:19 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR2
Prism Sample ID: 5070245-10
Prism Work Order: 5070245
Time Collected: 07/13/15 10:30
Time Submitted: 07/14/15 11:30
28 *6010C P5G029410.25 7/20/15 16:03 MWWmg/kg dry 0.036Arsenic
46 *6010C P5G029410.51 7/20/15 16:03 MWWmg/kg dry 0.098Barium
BRL *6010C P5G029410.25 7/18/15 1:01 MWWmg/kg dry 0.036Cadmium
65 *6010C P5G029410.25 7/20/15 16:03 MWWmg/kg dry 0.042Chromium
1.7 *6010C P5G029410.25 7/20/15 16:03 MWWmg/kg dry 0.039Lead
BRL *6010C P5G029410.51 7/18/15 1:01 MWWmg/kg dry 0.061Selenium
BRL *6010C P5G029410.25 7/18/15 1:01 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.012 7/18/15 16:41 MSCLHmg/kg dry 0.000951,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000561,1,1-Trichloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000781,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00101,1,2-Trichloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000321,1-Dichloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000511,1-Dichloroethylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000631,1-Dichloropropylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000661,2,3-Trichlorobenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00151,2,3-Trichloropropane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000861,2,4-Trichlorobenzene
0.018 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000881,2,4-Trimethylbenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000471,2-Dibromoethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000541,2-Dichlorobenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000691,2-Dichloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000721,2-Dichloropropane
0.0066 8260B P5G031810.012 7/18/15 16:41 MSCJmg/kg dry 0.000881,3,5-Trimethylbenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000771,3-Dichlorobenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000581,3-Dichloropropane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000461,4-Dichlorobenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000552,2-Dichloropropane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000602-Chlorotoluene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000694-Chlorotoluene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.000564-Isopropyltoluene
0.14 8260B P5G031810.12 7/18/15 16:41 MSCmg/kg dry 0.0028Acetone
BRL 8260B P5G031810.0069 7/18/15 16:41 MSCmg/kg dry 0.00067Benzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00097Bromobenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00064Bromochloromethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00065Bromodichloromethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.0013Bromoform
BRL 8260B P5G031810.023 7/18/15 16:41 MSCmg/kg dry 0.0014Bromomethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00058Carbon Tetrachloride
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00061Chlorobenzene
BRL 8260B P5G031810.023 7/18/15 16:41 MSCmg/kg dry 0.00097Chloroethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00084Chloroform
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00078Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR2
Prism Sample ID: 5070245-10
Prism Work Order: 5070245
Time Collected: 07/13/15 10:30
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00049cis-1,2-Dichloroethylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00039cis-1,3-Dichloropropylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00048Dibromochloromethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00053Dichlorodifluoromethane
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00044Ethylbenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00047Isopropyl Ether
BRL 8260B P5G031810.012 7/18/15 16:41 MSCLHmg/kg dry 0.00069Isopropylbenzene (Cumene)
0.015 8260B P5G031810.023 7/18/15 16:41 MSCJmg/kg dry 0.0011m,p-Xylenes
BRL 8260B P5G031810.12 7/18/15 16:41 MSCmg/kg dry 0.0010Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.23 7/18/15 16:41 MSCmg/kg dry 0.0010Methyl Ethyl Ketone (2-Butanone)
0.014 8260B P5G031810.12 7/18/15 16:41 MSCJmg/kg dry 0.00099Methyl Isobutyl Ketone
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00065Methylene Chloride
BRL 8260B P5G031810.023 7/18/15 16:41 MSCmg/kg dry 0.00037Methyl-tert-Butyl Ether
0.0087 8260B P5G031810.023 7/18/15 16:41 MSCJmg/kg dry 0.00037Naphthalene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00059n-Butylbenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00069n-Propylbenzene
0.0068 8260B P5G031810.012 7/18/15 16:41 MSCJmg/kg dry 0.00047o-Xylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00056sec-Butylbenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCLHmg/kg dry 0.00070Styrene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00039tert-Butylbenzene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00055Tetrachloroethylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00066Toluene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00069trans-1,2-Dichloroethylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00061trans-1,3-Dichloropropylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00075Trichloroethylene
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00075Trichlorofluoromethane
BRL 8260B P5G031810.058 7/18/15 16:41 MSCmg/kg dry 0.0016Vinyl acetate
BRL 8260B P5G031810.012 7/18/15 16:41 MSCmg/kg dry 0.00056Vinyl chloride
0.022 8260B P5G031810.035 7/18/15 16:41 MSCJmg/kg dry 0.0022Xylenes, total
Surrogate Recovery Control Limits
70-13084 %4-Bromofluorobenzene
84-12378 %Dibromofluoromethane SR
76-12981 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 1
Prism Sample ID: 5070245-11
Prism Work Order: 5070245
Time Collected: 07/13/15 11:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.5 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
8.0 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
230000 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G0284101.3 7/28/15 23:54 JMCAimg/kg dry 0.12Aroclor 1016
BRL 8082A P5G0284102.6 7/28/15 23:54 JMCAimg/kg dry 1.0Aroclor 1221
BRL 8082A P5G0284102.6 7/28/15 23:54 JMCAimg/kg dry 0.33Aroclor 1232
BRL 8082A P5G0284101.3 7/28/15 23:54 JMCAimg/kg dry 0.34Aroclor 1242
BRL 8082A P5G0284101.3 7/28/15 23:54 JMCAimg/kg dry 0.26Aroclor 1248
0.69 8082A P5G0284101.3 7/28/15 23:54 JMCAi, J mg/kg dry 0.32Aroclor 1254
BRL 8082A P5G0284101.3 7/28/15 23:54 JMCAimg/kg dry 0.18Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 131-Methylnaphthalene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 112-Methylnaphthalene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 9.2Acenaphthene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 9.8Acenaphthylene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 11Anthracene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 8.9Benzo(a)anthracene
BRL 8270D P5G032920688/3/15 13:53 JMVCCVmg/kg dry 7.3Benzo(a)pyrene
BRL 8270D P5G032920688/3/15 13:53 JMVCCVmg/kg dry 7.9Benzo(b)fluoranthene
BRL 8270D P5G032920688/3/15 13:53 JMVCCVmg/kg dry 7.4Benzo(g,h,i)perylene
BRL 8270D P5G032920688/3/15 13:53 JMVCCVmg/kg dry 8.9Benzo(k)fluoranthene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 8.5Chrysene
BRL 8270D P5G032920688/3/15 13:53 JMVCCVmg/kg dry 8.2Dibenzo(a,h)anthracene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 8.6Fluoranthene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 9.7Fluorene
BRL 8270D P5G032920688/3/15 13:53 JMVCCVmg/kg dry 7.8Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 11Naphthalene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 8.8Phenanthrene
BRL 8270D P5G032920688/3/15 13:53 JMVmg/kg dry 9.0Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
0.16 *7471B P5G027010.022 7/16/15 15:33 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 1
Prism Sample ID: 5070245-11
Prism Work Order: 5070245
Time Collected: 07/13/15 11:00
Time Submitted: 07/14/15 11:30
4.8 *6010C P5G029410.25 7/20/15 16:12 MWWmg/kg dry 0.036Arsenic
120 *6010C P5G029410.50 7/20/15 16:12 MWWmg/kg dry 0.097Barium
0.29 *6010C P5G029410.25 7/20/15 16:12 MWWmg/kg dry 0.036Cadmium
34 *6010C P5G029410.25 7/20/15 16:12 MWWmg/kg dry 0.041Chromium
68 *6010C P5G029410.25 7/20/15 16:12 MWWmg/kg dry 0.038Lead
BRL *6010C P5G029410.50 7/18/15 1:11 MWWmg/kg dry 0.060Selenium
BRL *6010C P5G029410.25 7/18/15 1:11 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000861,1,1,2-Tetrachloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000501,1,1-Trichloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000701,1,2,2-Tetrachloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000921,1,2-Trichloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000291,1-Dichloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000461,1-Dichloroethylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000571,1-Dichloropropylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000591,2,3-Trichlorobenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00131,2,3-Trichloropropane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000781,2,4-Trichlorobenzene
0.0055 8260B P5G038510.010 7/22/15 4:33 MSCIH, J mg/kg dry 0.000801,2,4-Trimethylbenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000421,2-Dibromoethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000491,2-Dichlorobenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000621,2-Dichloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000651,2-Dichloropropane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000791,3,5-Trimethylbenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000691,3-Dichlorobenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000521,3-Dichloropropane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000411,4-Dichlorobenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.000502,2-Dichloropropane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000542-Chlorotoluene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000624-Chlorotoluene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.000504-Isopropyltoluene
2.0 8260B P5G038510.10 7/22/15 4:33 MSCAc, E mg/kg dry 0.0025Acetone
0.0043 8260B P5G038510.0063 7/22/15 4:33 MSCJmg/kg dry 0.00061Benzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00087Bromobenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00057Bromochloromethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00058Bromodichloromethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.0012Bromoform
BRL 8260B P5G038510.021 7/22/15 4:33 MSCmg/kg dry 0.0013Bromomethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00052Carbon Tetrachloride
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00055Chlorobenzene
BRL 8260B P5G038510.021 7/22/15 4:33 MSCmg/kg dry 0.00087Chloroethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00075Chloroform
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00070Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 1
Prism Sample ID: 5070245-11
Prism Work Order: 5070245
Time Collected: 07/13/15 11:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00044cis-1,2-Dichloroethylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00035cis-1,3-Dichloropropylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00043Dibromochloromethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00047Dichlorodifluoromethane
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00040Ethylbenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00043Isopropyl Ether
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00062Isopropylbenzene (Cumene)
BRL 8260B P5G038510.021 7/22/15 4:33 MSCmg/kg dry 0.00096m,p-Xylenes
0.010 8260B P5G038510.10 7/22/15 4:33 MSCJmg/kg dry 0.00094Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G038510.21 7/22/15 4:33 MSCmg/kg dry 0.00094Methyl Ethyl Ketone (2-Butanone)
0.045 8260B P5G038510.10 7/22/15 4:33 MSCJmg/kg dry 0.00089Methyl Isobutyl Ketone
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00059Methylene Chloride
BRL 8260B P5G038510.021 7/22/15 4:33 MSCmg/kg dry 0.00033Methyl-tert-Butyl Ether
0.0069 8260B P5G038510.021 7/22/15 4:33 MSCIH, J mg/kg dry 0.00033Naphthalene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00053n-Butylbenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00062n-Propylbenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00043o-Xylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00050sec-Butylbenzene
0.011 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00063Styrene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCINmg/kg dry 0.00035tert-Butylbenzene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00050Tetrachloroethylene
0.0096 8260B P5G038510.010 7/22/15 4:33 MSCJmg/kg dry 0.00060Toluene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00062trans-1,2-Dichloroethylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00055trans-1,3-Dichloropropylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00068Trichloroethylene
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00067Trichlorofluoromethane
BRL 8260B P5G038510.052 7/22/15 4:33 MSCmg/kg dry 0.0014Vinyl acetate
BRL 8260B P5G038510.010 7/22/15 4:33 MSCmg/kg dry 0.00050Vinyl chloride
BRL 8260B P5G038510.031 7/22/15 4:33 MSCmg/kg dry 0.0020Xylenes, total
Surrogate Recovery Control Limits
70-130234 %4-Bromofluorobenzene IN, SR
84-123116 %Dibromofluoromethane
76-129128 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 2
Prism Sample ID: 5070245-12
Prism Work Order: 5070245
Time Collected: 07/13/15 11:05
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.3 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
7.6 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
420000 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
0.96 8082A P5G028410.26 7/30/15 12:26 JMCAjmg/kg dry 0.024Aroclor 1016
BRL 8082A P5G028410.51 7/30/15 12:26 JMCAimg/kg dry 0.21Aroclor 1221
BRL 8082A P5G028410.51 7/30/15 12:26 JMCAimg/kg dry 0.067Aroclor 1232
BRL 8082A P5G028410.26 7/30/15 12:26 JMCAimg/kg dry 0.068Aroclor 1242
BRL 8082A P5G028410.26 7/30/15 12:26 JMCAimg/kg dry 0.051Aroclor 1248
0.59 8082A P5G028410.26 7/30/15 12:26 JMCAimg/kg dry 0.064Aroclor 1254
BRL 8082A P5G028410.26 7/30/15 12:26 JMCAimg/kg dry 0.035Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
28 8270D P5G032910348/3/15 14:41 JMVJmg/kg dry 6.51-Methylnaphthalene
17 8270D P5G032910348/3/15 14:41 JMVJmg/kg dry 5.42-Methylnaphthalene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.6Acenaphthene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.9Acenaphthylene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 5.5Anthracene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.4Benzo(a)anthracene
BRL 8270D P5G032910348/3/15 14:41 JMVCCVmg/kg dry 3.7Benzo(a)pyrene
BRL 8270D P5G032910348/3/15 14:41 JMVCCVmg/kg dry 3.9Benzo(b)fluoranthene
BRL 8270D P5G032910348/3/15 14:41 JMVCCVmg/kg dry 3.7Benzo(g,h,i)perylene
BRL 8270D P5G032910348/3/15 14:41 JMVCCVmg/kg dry 4.4Benzo(k)fluoranthene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.3Chrysene
BRL 8270D P5G032910348/3/15 14:41 JMVCCVmg/kg dry 4.1Dibenzo(a,h)anthracene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.3Fluoranthene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.9Fluorene
BRL 8270D P5G032910348/3/15 14:41 JMVCCVmg/kg dry 3.9Indeno(1,2,3-cd)pyrene
15 8270D P5G032910348/3/15 14:41 JMVJmg/kg dry 5.5Naphthalene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.4Phenanthrene
BRL 8270D P5G032910348/3/15 14:41 JMVmg/kg dry 4.5Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
0.47 *7471B P5G027010.020 7/16/15 15:38 JABmg/kg dry 0.0013Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 2
Prism Sample ID: 5070245-12
Prism Work Order: 5070245
Time Collected: 07/13/15 11:05
Time Submitted: 07/14/15 11:30
2.8 *6010C P5G029410.26 7/20/15 16:20 MWWmg/kg dry 0.037Arsenic
160 *6010C P5G029410.52 7/20/15 16:20 MWWmg/kg dry 0.10Barium
2.4 *6010C P5G029410.26 7/20/15 16:20 MWWmg/kg dry 0.037Cadmium
24 *6010C P5G029410.26 7/20/15 16:20 MWWmg/kg dry 0.043Chromium
140 *6010C P5G029410.26 7/20/15 16:20 MWWmg/kg dry 0.040Lead
BRL *6010C P5G029410.52 7/18/15 1:20 MWWmg/kg dry 0.063Selenium
0.61 *6010C P5G029410.26 7/18/15 1:20 MWWmg/kg dry 0.030Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00101,1,1,2-Tetrachloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000601,1,1-Trichloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000841,1,2,2-Tetrachloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00111,1,2-Trichloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000341,1-Dichloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000551,1-Dichloroethylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000681,1-Dichloropropylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000701,2,3-Trichlorobenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.00161,2,3-Trichloropropane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000921,2,4-Trichlorobenzene
0.026 8260B P5G038510.012 7/22/15 5:36 MSCIHmg/kg dry 0.000941,2,4-Trimethylbenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000501,2-Dibromoethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000581,2-Dichlorobenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000741,2-Dichloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000771,2-Dichloropropane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000931,3,5-Trimethylbenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000821,3-Dichlorobenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000621,3-Dichloropropane
0.014 8260B P5G038510.012 7/22/15 5:36 MSCIHmg/kg dry 0.000491,4-Dichlorobenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.000592,2-Dichloropropane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000642-Chlorotoluene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.000744-Chlorotoluene
0.016 8260B P5G038510.012 7/22/15 5:36 MSCIHmg/kg dry 0.000604-Isopropyltoluene
3.8 8260B P5G038510.12 7/22/15 5:36 MSCAc, E mg/kg dry 0.0030Acetone
BRL 8260B P5G038510.0074 7/22/15 5:36 MSCmg/kg dry 0.00072Benzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.0010Bromobenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00068Bromochloromethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00069Bromodichloromethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.0014Bromoform
BRL 8260B P5G038510.025 7/22/15 5:36 MSCmg/kg dry 0.0015Bromomethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00062Carbon Tetrachloride
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00065Chlorobenzene
BRL 8260B P5G038510.025 7/22/15 5:36 MSCmg/kg dry 0.0010Chloroethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00089Chloroform
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00083Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 2
Prism Sample ID: 5070245-12
Prism Work Order: 5070245
Time Collected: 07/13/15 11:05
Time Submitted: 07/14/15 11:30
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00053cis-1,2-Dichloroethylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00042cis-1,3-Dichloropropylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00051Dibromochloromethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00056Dichlorodifluoromethane
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00047Ethylbenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00050Isopropyl Ether
BRL 8260B P5G038510.012 7/22/15 5:36 MSCINmg/kg dry 0.00073Isopropylbenzene (Cumene)
0.0054 8260B P5G038510.025 7/22/15 5:36 MSCJmg/kg dry 0.0011m,p-Xylenes
0.028 8260B P5G038510.12 7/22/15 5:36 MSCJmg/kg dry 0.0011Methyl Butyl Ketone (2-Hexanone)
0.24 8260B P5G038510.25 7/22/15 5:36 MSCJmg/kg dry 0.0011Methyl Ethyl Ketone (2-Butanone)
0.057 8260B P5G038510.12 7/22/15 5:36 MSCJmg/kg dry 0.0011Methyl Isobutyl Ketone
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00069Methylene Chloride
BRL 8260B P5G038510.025 7/22/15 5:36 MSCmg/kg dry 0.00040Methyl-tert-Butyl Ether
0.026 8260B P5G038510.025 7/22/15 5:36 MSCIHmg/kg dry 0.00039Naphthalene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00063n-Butylbenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00073n-Propylbenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00051o-Xylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00060sec-Butylbenzene
0.0054 8260B P5G038510.012 7/22/15 5:36 MSCJmg/kg dry 0.00074Styrene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00042tert-Butylbenzene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00059Tetrachloroethylene
0.015 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00071Toluene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00074trans-1,2-Dichloroethylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00065trans-1,3-Dichloropropylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00080Trichloroethylene
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00080Trichlorofluoromethane
BRL 8260B P5G038510.062 7/22/15 5:36 MSCmg/kg dry 0.0017Vinyl acetate
BRL 8260B P5G038510.012 7/22/15 5:36 MSCmg/kg dry 0.00060Vinyl chloride
0.0054 8260B P5G038510.037 7/22/15 5:36 MSCJmg/kg dry 0.0023Xylenes, total
Surrogate Recovery Control Limits
70-130287 %4-Bromofluorobenzene IH, SR
84-123127 %Dibromofluoromethane SR
76-129155 %Toluene-d8 SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 3
Prism Sample ID: 5070245-13
Prism Work Order: 5070245
Time Collected: 07/13/15 11:10
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.3 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
7.0 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
250000 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
0.17 8082A P5G028410.13 7/30/15 12:37 JMCAjmg/kg dry 0.012Aroclor 1016
BRL 8082A P5G028410.26 7/30/15 12:37 JMCAimg/kg dry 0.10Aroclor 1221
BRL 8082A P5G028410.26 7/30/15 12:37 JMCAimg/kg dry 0.033Aroclor 1232
BRL 8082A P5G028410.13 7/30/15 12:37 JMCAimg/kg dry 0.034Aroclor 1242
BRL 8082A P5G028410.13 7/30/15 12:37 JMCAimg/kg dry 0.026Aroclor 1248
0.12 8082A P5G028410.13 7/30/15 12:37 JMCJ, Ai mg/kg dry 0.032Aroclor 1254
BRL 8082A P5G028410.13 7/30/15 12:37 JMCAimg/kg dry 0.018Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.651-Methylnaphthalene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.542-Methylnaphthalene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.46Acenaphthene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.49Acenaphthylene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.55Anthracene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.44Benzo(a)anthracene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVCCVmg/kg dry 0.37Benzo(a)pyrene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVCCVmg/kg dry 0.39Benzo(b)fluoranthene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVCCVmg/kg dry 0.37Benzo(g,h,i)perylene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVCCVmg/kg dry 0.44Benzo(k)fluoranthene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.43Chrysene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVCCVmg/kg dry 0.41Dibenzo(a,h)anthracene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.43Fluoranthene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.49Fluorene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVCCVmg/kg dry 0.39Indeno(1,2,3-cd)pyrene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.55Naphthalene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.44Phenanthrene
BRL 8270D P5G0329103.4 8/3/15 15:03 JMVmg/kg dry 0.45Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.020 7/16/15 15:43 JABmg/kg dry 0.0013Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 3
Prism Sample ID: 5070245-13
Prism Work Order: 5070245
Time Collected: 07/13/15 11:10
Time Submitted: 07/14/15 11:30
7.3 *6010C P5G029410.25 7/20/15 16:27 MWWmg/kg dry 0.036Arsenic
180 *6010C P5G029410.51 7/20/15 16:27 MWWmg/kg dry 0.098Barium
BRL *6010C P5G029410.25 7/18/15 1:40 MWWmg/kg dry 0.036Cadmium
40 *6010C P5G029410.25 7/20/15 16:27 MWWmg/kg dry 0.042Chromium
22 *6010C P5G029410.25 7/20/15 16:27 MWWmg/kg dry 0.039Lead
BRL *6010C P5G029410.51 7/18/15 1:40 MWWmg/kg dry 0.061Selenium
BRL *6010C P5G029410.25 7/18/15 1:40 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.023 7/18/15 18:07 MSCLHmg/kg dry 0.00191,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00111,1,1-Trichloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00151,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00201,1,2-Trichloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.000631,1-Dichloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00101,1-Dichloroethylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00121,1-Dichloropropylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00131,2,3-Trichlorobenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00291,2,3-Trichloropropane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00171,2,4-Trichlorobenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00171,2,4-Trimethylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.000911,2-Dibromoethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00111,2-Dichlorobenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00141,2-Dichloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00141,2-Dichloropropane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00171,3,5-Trimethylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00151,3-Dichlorobenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00111,3-Dichloropropane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.000901,4-Dichlorobenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00112,2-Dichloropropane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00122-Chlorotoluene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00144-Chlorotoluene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00114-Isopropyltoluene
0.64 8260B P5G031810.23 7/18/15 18:07 MSCmg/kg dry 0.0055Acetone
BRL 8260B P5G031810.014 7/18/15 18:07 MSCmg/kg dry 0.0013Benzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.0019Bromobenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0013Bromochloromethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0013Bromodichloromethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0026Bromoform
BRL 8260B P5G031810.045 7/18/15 18:07 MSCmg/kg dry 0.0028Bromomethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0011Carbon Tetrachloride
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0012Chlorobenzene
BRL 8260B P5G031810.045 7/18/15 18:07 MSCmg/kg dry 0.0019Chloroethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0016Chloroform
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0015Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 3
Prism Sample ID: 5070245-13
Prism Work Order: 5070245
Time Collected: 07/13/15 11:10
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00097cis-1,2-Dichloroethylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00076cis-1,3-Dichloropropylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00094Dibromochloromethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0010Dichlorodifluoromethane
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00087Ethylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00093Isopropyl Ether
BRL 8260B P5G031810.023 7/18/15 18:07 MSCIN, LH mg/kg dry 0.0013Isopropylbenzene (Cumene)
BRL 8260B P5G031810.045 7/18/15 18:07 MSCmg/kg dry 0.0021m,p-Xylenes
BRL 8260B P5G031810.23 7/18/15 18:07 MSCmg/kg dry 0.0021Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.45 7/18/15 18:07 MSCmg/kg dry 0.0021Methyl Ethyl Ketone (2-Butanone)
0.033 8260B P5G031810.23 7/18/15 18:07 MSCJmg/kg dry 0.0019Methyl Isobutyl Ketone
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0013Methylene Chloride
BRL 8260B P5G031810.045 7/18/15 18:07 MSCmg/kg dry 0.00073Methyl-tert-Butyl Ether
BRL 8260B P5G031810.045 7/18/15 18:07 MSCINmg/kg dry 0.00072Naphthalene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.0012n-Butylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.0014n-Propylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.00093o-Xylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.0011sec-Butylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCLHmg/kg dry 0.0014Styrene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCINmg/kg dry 0.00077tert-Butylbenzene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0011Tetrachloroethylene
0.012 8260B P5G031810.023 7/18/15 18:07 MSCJmg/kg dry 0.0013Toluene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0014trans-1,2-Dichloroethylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0012trans-1,3-Dichloropropylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0015Trichloroethylene
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0015Trichlorofluoromethane
BRL 8260B P5G031810.11 7/18/15 18:07 MSCmg/kg dry 0.0031Vinyl acetate
BRL 8260B P5G031810.023 7/18/15 18:07 MSCmg/kg dry 0.0011Vinyl chloride
BRL 8260B P5G031810.068 7/18/15 18:07 MSCmg/kg dry 0.0043Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene IN
84-12383 %Dibromofluoromethane SR
76-12981 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 4
Prism Sample ID: 5070245-14
Prism Work Order: 5070245
Time Collected: 07/13/15 11:30
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.5 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
3.8 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
250000 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028450.64 7/30/15 12:49 JMCAimg/kg dry 0.060Aroclor 1016
BRL 8082A P5G028451.3 7/30/15 12:49 JMCAimg/kg dry 0.51Aroclor 1221
BRL 8082A P5G028451.3 7/30/15 12:49 JMCAimg/kg dry 0.17Aroclor 1232
BRL 8082A P5G028450.64 7/30/15 12:49 JMCAimg/kg dry 0.17Aroclor 1242
BRL 8082A P5G028450.64 7/30/15 12:49 JMCAimg/kg dry 0.13Aroclor 1248
BRL 8082A P5G028450.64 7/30/15 12:49 JMCAimg/kg dry 0.16Aroclor 1254
BRL 8082A P5G028450.64 7/30/15 12:49 JMCAimg/kg dry 0.088Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 6.51-Methylnaphthalene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 5.42-Methylnaphthalene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.6Acenaphthene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.9Acenaphthylene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 5.5Anthracene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.4Benzo(a)anthracene
BRL 8270D P5G032910348/3/15 15:26 JMVCCVmg/kg dry 3.7Benzo(a)pyrene
BRL 8270D P5G032910348/3/15 15:26 JMVCCVmg/kg dry 3.9Benzo(b)fluoranthene
BRL 8270D P5G032910348/3/15 15:26 JMVCCVmg/kg dry 3.7Benzo(g,h,i)perylene
BRL 8270D P5G032910348/3/15 15:26 JMVCCVmg/kg dry 4.4Benzo(k)fluoranthene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.3Chrysene
BRL 8270D P5G032910348/3/15 15:26 JMVCCVmg/kg dry 4.1Dibenzo(a,h)anthracene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.3Fluoranthene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.9Fluorene
BRL 8270D P5G032910348/3/15 15:26 JMVCCVmg/kg dry 3.9Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 5.4Naphthalene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.4Phenanthrene
BRL 8270D P5G032910348/3/15 15:26 JMVmg/kg dry 4.5Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.021 7/16/15 15:47 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 4
Prism Sample ID: 5070245-14
Prism Work Order: 5070245
Time Collected: 07/13/15 11:30
Time Submitted: 07/14/15 11:30
5.5 *6010C P5G029410.26 7/20/15 16:35 MWWmg/kg dry 0.037Arsenic
130 *6010C P5G029410.52 7/20/15 16:35 MWWmg/kg dry 0.10Barium
BRL *6010C P5G029410.26 7/18/15 1:48 MWWmg/kg dry 0.037Cadmium
37 *6010C P5G029410.26 7/20/15 16:35 MWWmg/kg dry 0.043Chromium
17 *6010C P5G029410.26 7/20/15 16:35 MWWmg/kg dry 0.040Lead
BRL *6010C P5G029410.52 7/18/15 1:48 MWWmg/kg dry 0.063Selenium
BRL *6010C P5G029410.26 7/18/15 1:48 MWWmg/kg dry 0.030Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCLHmg/kg dry 0.000781,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000461,1,1-Trichloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000641,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000841,1,2-Trichloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000271,1-Dichloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000421,1-Dichloroethylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000521,1-Dichloropropylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000541,2,3-Trichlorobenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.00121,2,3-Trichloropropane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000711,2,4-Trichlorobenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000731,2,4-Trimethylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000381,2-Dibromoethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000451,2-Dichlorobenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000571,2-Dichloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000591,2-Dichloropropane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000721,3,5-Trimethylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000631,3-Dichlorobenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000481,3-Dichloropropane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000381,4-Dichlorobenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.000452,2-Dichloropropane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000492-Chlorotoluene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000574-Chlorotoluene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.000464-Isopropyltoluene
0.46 8260B P5G031810.095 7/18/15 18:36 MSCmg/kg dry 0.0023Acetone
0.0065 8260B P5G031810.0057 7/18/15 18:36 MSCmg/kg dry 0.00055Benzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.00080Bromobenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00052Bromochloromethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00053Bromodichloromethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.0011Bromoform
BRL 8260B P5G031810.019 7/18/15 18:36 MSCmg/kg dry 0.0012Bromomethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00047Carbon Tetrachloride
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00051Chlorobenzene
BRL 8260B P5G031810.019 7/18/15 18:36 MSCmg/kg dry 0.00080Chloroethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00069Chloroform
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00064Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: PR-Pit 4
Prism Sample ID: 5070245-14
Prism Work Order: 5070245
Time Collected: 07/13/15 11:30
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00041cis-1,2-Dichloroethylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00032cis-1,3-Dichloropropylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00039Dibromochloromethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00043Dichlorodifluoromethane
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00037Ethylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00039Isopropyl Ether
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCIN, LH mg/kg dry 0.00056Isopropylbenzene (Cumene)
BRL 8260B P5G031810.019 7/18/15 18:36 MSCmg/kg dry 0.00088m,p-Xylenes
0.030 8260B P5G031810.095 7/18/15 18:36 MSCJmg/kg dry 0.00086Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G031810.19 7/18/15 18:36 MSCmg/kg dry 0.00086Methyl Ethyl Ketone (2-Butanone)
0.010 8260B P5G031810.095 7/18/15 18:36 MSCJmg/kg dry 0.00081Methyl Isobutyl Ketone
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00054Methylene Chloride
BRL 8260B P5G031810.019 7/18/15 18:36 MSCmg/kg dry 0.00031Methyl-tert-Butyl Ether
BRL 8260B P5G031810.019 7/18/15 18:36 MSCINmg/kg dry 0.00030Naphthalene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.00049n-Butylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.00057n-Propylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00039o-Xylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.00046sec-Butylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCLHmg/kg dry 0.00057Styrene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCINmg/kg dry 0.00032tert-Butylbenzene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00045Tetrachloroethylene
0.0068 8260B P5G031810.0095 7/18/15 18:36 MSCJmg/kg dry 0.00055Toluene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00057trans-1,2-Dichloroethylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00050trans-1,3-Dichloropropylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00062Trichloroethylene
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00062Trichlorofluoromethane
BRL 8260B P5G031810.048 7/18/15 18:36 MSCmg/kg dry 0.0013Vinyl acetate
BRL 8260B P5G031810.0095 7/18/15 18:36 MSCmg/kg dry 0.00046Vinyl chloride
BRL 8260B P5G031810.029 7/18/15 18:36 MSCmg/kg dry 0.0018Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene IN
84-12384 %Dibromofluoromethane
76-12982 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR-Pit
Prism Sample ID: 5070245-15
Prism Work Order: 5070245
Time Collected: 07/13/15 11:40
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.6 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
8.3 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
35000 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
0.48 8082A P5G028450.26 7/30/15 13:01 JMCAimg/kg dry 0.024Aroclor 1016
BRL 8082A P5G028450.51 7/30/15 13:01 JMCAimg/kg dry 0.20Aroclor 1221
BRL 8082A P5G028450.51 7/30/15 13:01 JMCAimg/kg dry 0.066Aroclor 1232
BRL 8082A P5G028450.26 7/30/15 13:01 JMCAimg/kg dry 0.068Aroclor 1242
BRL 8082A P5G028450.26 7/30/15 13:01 JMCAimg/kg dry 0.051Aroclor 1248
1.5 8082A P5G028450.26 7/30/15 13:01 JMCAimg/kg dry 0.063Aroclor 1254
BRL 8082A P5G028450.26 7/30/15 13:01 JMCAimg/kg dry 0.035Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
43 8270D P5G032920688/3/15 15:48 JMVJmg/kg dry 131-Methylnaphthalene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 112-Methylnaphthalene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 9.2Acenaphthene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 9.8Acenaphthylene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 11Anthracene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 8.8Benzo(a)anthracene
BRL 8270D P5G032920688/3/15 15:48 JMVCCVmg/kg dry 7.3Benzo(a)pyrene
BRL 8270D P5G032920688/3/15 15:48 JMVCCVmg/kg dry 7.8Benzo(b)fluoranthene
BRL 8270D P5G032920688/3/15 15:48 JMVCCVmg/kg dry 7.4Benzo(g,h,i)perylene
BRL 8270D P5G032920688/3/15 15:48 JMVCCVmg/kg dry 8.9Benzo(k)fluoranthene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 8.5Chrysene
BRL 8270D P5G032920688/3/15 15:48 JMVCCVmg/kg dry 8.2Dibenzo(a,h)anthracene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 8.6Fluoranthene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 9.7Fluorene
BRL 8270D P5G032920688/3/15 15:48 JMVCCVmg/kg dry 7.8Indeno(1,2,3-cd)pyrene
21 8270D P5G032920688/3/15 15:48 JMVJmg/kg dry 11Naphthalene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 8.8Phenanthrene
BRL 8270D P5G032920688/3/15 15:48 JMVmg/kg dry 8.9Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-12244 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.021 7/16/15 15:52 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR-Pit
Prism Sample ID: 5070245-15
Prism Work Order: 5070245
Time Collected: 07/13/15 11:40
Time Submitted: 07/14/15 11:30
100 *6010C P5G0294102.6 7/20/15 16:55 MWWDMmg/kg dry 0.37Arsenic
20 *6010C P5G0294105.3 7/20/15 16:55 MWWDMmg/kg dry 1.0Barium
BRL *6010C P5G0294102.6 7/18/15 1:58 MWWDMmg/kg dry 0.37Cadmium
79000 *6010C P5G0294100267/20/15 17:03 MWWmg/kg dry 4.3Chromium
15 *6010C P5G0294102.6 7/20/15 16:55 MWWDMmg/kg dry 0.40Lead
BRL *6010C P5G0294105.3 7/18/15 1:58 MWWDMmg/kg dry 0.63Selenium
BRL *6010C P5G0294102.6 7/18/15 1:58 MWWDMmg/kg dry 0.30Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G031810.013 7/18/15 19:05 MSCLHmg/kg dry 0.00101,1,1,2-Tetrachloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000611,1,1-Trichloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000861,1,2,2-Tetrachloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00111,1,2-Trichloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000351,1-Dichloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000561,1-Dichloroethylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000691,1-Dichloropropylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000721,2,3-Trichlorobenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00161,2,3-Trichloropropane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000941,2,4-Trichlorobenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000971,2,4-Trimethylbenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000511,2-Dibromoethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000601,2-Dichlorobenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000761,2-Dichloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000791,2-Dichloropropane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000961,3,5-Trimethylbenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000841,3-Dichlorobenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000641,3-Dichloropropane
0.0061 8260B P5G031810.013 7/18/15 19:05 MSCJmg/kg dry 0.000501,4-Dichlorobenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000602,2-Dichloropropane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000652-Chlorotoluene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000764-Chlorotoluene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.000614-Isopropyltoluene
4.0 8260B P5G031810.13 7/18/15 19:05 MSCAh, E mg/kg dry 0.0031Acetone
BRL 8260B P5G031810.0076 7/18/15 19:05 MSCmg/kg dry 0.00074Benzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.0011Bromobenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00070Bromochloromethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00071Bromodichloromethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.0014Bromoform
BRL 8260B P5G031810.025 7/18/15 19:05 MSCmg/kg dry 0.0016Bromomethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00063Carbon Tetrachloride
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00067Chlorobenzene
BRL 8260B P5G031810.025 7/18/15 19:05 MSCmg/kg dry 0.0011Chloroethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00092Chloroform
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00085Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: IR-Pit
Prism Sample ID: 5070245-15
Prism Work Order: 5070245
Time Collected: 07/13/15 11:40
Time Submitted: 07/14/15 11:30
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00054cis-1,2-Dichloroethylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00043cis-1,3-Dichloropropylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00052Dibromochloromethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00058Dichlorodifluoromethane
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00049Ethylbenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00052Isopropyl Ether
BRL 8260B P5G031810.013 7/18/15 19:05 MSCLHmg/kg dry 0.00075Isopropylbenzene (Cumene)
BRL 8260B P5G031810.025 7/18/15 19:05 MSCmg/kg dry 0.0012m,p-Xylenes
BRL 8260B P5G031810.13 7/18/15 19:05 MSCmg/kg dry 0.0011Methyl Butyl Ketone (2-Hexanone)
0.20 8260B P5G031810.25 7/18/15 19:05 MSCJmg/kg dry 0.0011Methyl Ethyl Ketone (2-Butanone)
0.10 8260B P5G031810.13 7/18/15 19:05 MSCJmg/kg dry 0.0011Methyl Isobutyl Ketone
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00071Methylene Chloride
BRL 8260B P5G031810.025 7/18/15 19:05 MSCmg/kg dry 0.00041Methyl-tert-Butyl Ether
BRL 8260B P5G031810.025 7/18/15 19:05 MSCmg/kg dry 0.00040Naphthalene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00065n-Butylbenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00075n-Propylbenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00052o-Xylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00061sec-Butylbenzene
0.0068 8260B P5G031810.013 7/18/15 19:05 MSCLH, J mg/kg dry 0.00076Styrene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00043tert-Butylbenzene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00060Tetrachloroethylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00073Toluene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00076trans-1,2-Dichloroethylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00067trans-1,3-Dichloropropylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00082Trichloroethylene
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00082Trichlorofluoromethane
BRL 8260B P5G031810.063 7/18/15 19:05 MSCmg/kg dry 0.0017Vinyl acetate
BRL 8260B P5G031810.013 7/18/15 19:05 MSCmg/kg dry 0.00061Vinyl chloride
BRL 8260B P5G031810.038 7/18/15 19:05 MSCmg/kg dry 0.0024Xylenes, total
Surrogate Recovery Control Limits
70-13089 %4-Bromofluorobenzene
84-12383 %Dibromofluoromethane SR
76-12981 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: T-1 Totes
Prism Sample ID: 5070245-16
Prism Work Order: 5070245
Time Collected: 07/13/15 11:45
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
93.8 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
8.1 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
5400 *9071B P5G03371437/17/15 11:30 MJOmg/kg dry 14Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G028410.11 7/30/15 13:13 JMCAimg/kg dry 0.0099Aroclor 1016
BRL 8082A P5G028410.21 7/30/15 13:13 JMCAimg/kg dry 0.085Aroclor 1221
BRL 8082A P5G028410.21 7/30/15 13:13 JMCAimg/kg dry 0.027Aroclor 1232
BRL 8082A P5G028410.11 7/30/15 13:13 JMCAimg/kg dry 0.028Aroclor 1242
BRL 8082A P5G028410.11 7/30/15 13:13 JMCAimg/kg dry 0.021Aroclor 1248
BRL 8082A P5G028410.11 7/30/15 13:13 JMCAimg/kg dry 0.026Aroclor 1254
BRL 8082A P5G028410.11 7/30/15 13:13 JMCAimg/kg dry 0.015Aroclor 1260
Surrogate Recovery Control Limits
36-18231 %Tetrachloro-m-xylene Ak
34-18210 %Decachlorobiphenyl Ak
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 271-Methylnaphthalene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 222-Methylnaphthalene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 19Acenaphthene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 20Acenaphthylene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 23Anthracene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 18Benzo(a)anthracene
BRL 8270D P5G0329201408/3/15 16:11 JMVCCVmg/kg dry 15Benzo(a)pyrene
BRL 8270D P5G0329201408/3/15 16:11 JMVCCVmg/kg dry 16Benzo(b)fluoranthene
BRL 8270D P5G0329201408/3/15 16:11 JMVCCVmg/kg dry 15Benzo(g,h,i)perylene
BRL 8270D P5G0329201408/3/15 16:11 JMVCCVmg/kg dry 18Benzo(k)fluoranthene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 18Chrysene
BRL 8270D P5G0329201408/3/15 16:11 JMVCCVmg/kg dry 17Dibenzo(a,h)anthracene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 18Fluoranthene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 20Fluorene
BRL 8270D P5G0329201408/3/15 16:11 JMVCCVmg/kg dry 16Indeno(1,2,3-cd)pyrene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 22Naphthalene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 18Phenanthrene
BRL 8270D P5G0329201408/3/15 16:11 JMVmg/kg dry 18Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.022 7/16/15 15:57 JABmg/kg dry 0.0015Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: T-1 Totes
Prism Sample ID: 5070245-16
Prism Work Order: 5070245
Time Collected: 07/13/15 11:45
Time Submitted: 07/14/15 11:30
BRL *6010C P5G029410.27 7/18/15 2:04 MWWmg/kg dry 0.038Arsenic
150 *6010C P5G029410.54 7/20/15 17:16 MWWmg/kg dry 0.10Barium
BRL *6010C P5G029410.27 7/18/15 2:04 MWWmg/kg dry 0.038Cadmium
4.5 *6010C P5G029410.27 7/20/15 17:16 MWWmg/kg dry 0.044Chromium
BRL *6010C P5G029410.27 7/20/15 17:16 MWWmg/kg dry 0.041Lead
BRL *6010C P5G029410.54 7/18/15 2:04 MWWmg/kg dry 0.064Selenium
BRL *6010C P5G029410.27 7/18/15 2:04 MWWmg/kg dry 0.031Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000961,1,1,2-Tetrachloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000571,1,1-Trichloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000791,1,2,2-Tetrachloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00101,1,2-Trichloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000331,1-Dichloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000521,1-Dichloroethylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000641,1-Dichloropropylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000671,2,3-Trichlorobenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00151,2,3-Trichloropropane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000871,2,4-Trichlorobenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000901,2,4-Trimethylbenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000471,2-Dibromoethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000551,2-Dichlorobenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000701,2-Dichloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000731,2-Dichloropropane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000891,3,5-Trimethylbenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000781,3-Dichlorobenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000591,3-Dichloropropane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000461,4-Dichlorobenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000562,2-Dichloropropane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000612-Chlorotoluene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000704-Chlorotoluene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.000574-Isopropyltoluene
5.4 8260B P5G034710.12 7/20/15 23:21 cgpEmg/kg dry 0.0029Acetone
BRL 8260B P5G034710.0070 7/20/15 23:21 cgpmg/kg dry 0.00068Benzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00098Bromobenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00065Bromochloromethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00066Bromodichloromethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.0013Bromoform
BRL 8260B P5G034710.023 7/20/15 23:21 cgpmg/kg dry 0.0014Bromomethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00058Carbon Tetrachloride
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00062Chlorobenzene
BRL 8260B P5G034710.023 7/20/15 23:21 cgpmg/kg dry 0.00098Chloroethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00085Chloroform
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00079Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: T-1 Totes
Prism Sample ID: 5070245-16
Prism Work Order: 5070245
Time Collected: 07/13/15 11:45
Time Submitted: 07/14/15 11:30
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00050cis-1,2-Dichloroethylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00039cis-1,3-Dichloropropylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00048Dibromochloromethane
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00053Dichlorodifluoromethane
0.012 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00045Ethylbenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00048Isopropyl Ether
0.031 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00069Isopropylbenzene (Cumene)
0.017 8260B P5G034710.023 7/20/15 23:21 cgpJmg/kg dry 0.0011m,p-Xylenes
BRL 8260B P5G034710.12 7/20/15 23:21 cgpmg/kg dry 0.0011Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G034710.23 7/20/15 23:21 cgpmg/kg dry 0.0011Methyl Ethyl Ketone (2-Butanone)
0.038 8260B P5G034710.12 7/20/15 23:21 cgpJmg/kg dry 0.0010Methyl Isobutyl Ketone
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00066Methylene Chloride
BRL 8260B P5G034710.023 7/20/15 23:21 cgpmg/kg dry 0.00038Methyl-tert-Butyl Ether
BRL 8260B P5G034710.023 7/20/15 23:21 cgpmg/kg dry 0.00037Naphthalene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00060n-Butylbenzene
0.014 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00070n-Propylbenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00048o-Xylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00057sec-Butylbenzene
0.51 8260B P5G034710.012 7/20/15 23:21 cgpAd, E mg/kg dry 0.00071Styrene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00040tert-Butylbenzene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00056Tetrachloroethylene
0.012 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00067Toluene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00070trans-1,2-Dichloroethylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00062trans-1,3-Dichloropropylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00076Trichloroethylene
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00076Trichlorofluoromethane
BRL 8260B P5G034710.059 7/20/15 23:21 cgpAbmg/kg dry 0.0016Vinyl acetate
BRL 8260B P5G034710.012 7/20/15 23:21 cgpmg/kg dry 0.00057Vinyl chloride
0.017 8260B P5G034710.035 7/20/15 23:21 cgpJmg/kg dry 0.0022Xylenes, total
Surrogate Recovery Control Limits
70-130135 %4-Bromofluorobenzene SR
84-123107 %Dibromofluoromethane
76-129107 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: WO-1
Prism Sample ID: 5070245-17
Prism Work Order: 5070245
Time Collected: 07/13/15 12:45
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
97.8 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
1700 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G0284100.51 7/30/15 13:24 JMCAimg/kg dry 0.048Aroclor 1016
BRL 8082A P5G0284101.0 7/30/15 13:24 JMCAimg/kg dry 0.41Aroclor 1221
BRL 8082A P5G0284101.0 7/30/15 13:24 JMCAimg/kg dry 0.13Aroclor 1232
BRL 8082A P5G0284100.51 7/30/15 13:24 JMCAimg/kg dry 0.14Aroclor 1242
BRL 8082A P5G0284100.51 7/30/15 13:24 JMCAimg/kg dry 0.10Aroclor 1248
1.2 8082A P5G0284100.51 7/30/15 13:24 JMCAimg/kg dry 0.13Aroclor 1254
BRL 8082A P5G0284100.51 7/30/15 13:24 JMCAimg/kg dry 0.071Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.331-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.272-Methylnaphthalene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.23Acenaphthene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.24Acenaphthylene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.27Anthracene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.22Benzo(a)anthracene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVCCVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVCCVmg/kg dry 0.20Benzo(b)fluoranthene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVCCVmg/kg dry 0.19Benzo(g,h,i)perylene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVCCVmg/kg dry 0.22Benzo(k)fluoranthene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.21Chrysene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVCCVmg/kg dry 0.21Dibenzo(a,h)anthracene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.22Fluoranthene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.24Fluorene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVCCVmg/kg dry 0.19Indeno(1,2,3-cd)pyrene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.27Naphthalene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.22Phenanthrene
BRL 8270D P5G032951.7 8/3/15 16:33 JMVmg/kg dry 0.22Pyrene
Surrogate Recovery Control Limits
44-11566 %2-Fluorobiphenyl
37-12255 %Nitrobenzene-d5
54-12768 %Terphenyl-d14
Total Metals
BRL *7471B P5G027010.022 7/16/15 16:01 JABmg/kg dry 0.0014Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: WO-1
Prism Sample ID: 5070245-17
Prism Work Order: 5070245
Time Collected: 07/13/15 12:45
Time Submitted: 07/14/15 11:30
13 *6010C P5G029410.26 7/20/15 17:24 MWWmg/kg dry 0.037Arsenic
30 *6010C P5G029410.51 7/20/15 17:24 MWWmg/kg dry 0.099Barium
BRL *6010C P5G029410.26 7/18/15 2:12 MWWmg/kg dry 0.036Cadmium
18 *6010C P5G029410.26 7/20/15 17:24 MWWmg/kg dry 0.042Chromium
7.7 *6010C P5G029410.26 7/20/15 17:24 MWWmg/kg dry 0.039Lead
BRL *6010C P5G029410.51 7/18/15 2:12 MWWmg/kg dry 0.062Selenium
BRL *6010C P5G029410.26 7/18/15 2:12 MWWmg/kg dry 0.029Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000461,1,1,2-Tetrachloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000271,1,1-Trichloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000501,1,2-Trichloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000721,2,3-Trichloropropane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000431,2,4-Trimethylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000344-Chlorotoluene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.000274-Isopropyltoluene
0.12 8260B P5G034710.056 7/20/15 22:16 cgpmg/kg dry 0.0014Acetone
BRL 8260B P5G034710.0034 7/20/15 22:16 cgpmg/kg dry 0.00033Benzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00047Bromobenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00031Bromochloromethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00031Bromodichloromethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00064Bromoform
BRL 8260B P5G034710.011 7/20/15 22:16 cgpmg/kg dry 0.00069Bromomethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00030Chlorobenzene
BRL 8260B P5G034710.011 7/20/15 22:16 cgpmg/kg dry 0.00047Chloroethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00041Chloroform
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00038Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: WO-1
Prism Sample ID: 5070245-17
Prism Work Order: 5070245
Time Collected: 07/13/15 12:45
Time Submitted: 07/14/15 11:30
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00022Ethylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00033Isopropylbenzene (Cumene)
BRL 8260B P5G034710.011 7/20/15 22:16 cgpmg/kg dry 0.00052m,p-Xylenes
BRL 8260B P5G034710.056 7/20/15 22:16 cgpmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G034710.11 7/20/15 22:16 cgpmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)
0.0043 8260B P5G034710.056 7/20/15 22:16 cgpJmg/kg dry 0.00048Methyl Isobutyl Ketone
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00032Methylene Chloride
BRL 8260B P5G034710.011 7/20/15 22:16 cgpmg/kg dry 0.00018Methyl-tert-Butyl Ether
0.022 8260B P5G034710.011 7/20/15 22:16 cgpmg/kg dry 0.00018Naphthalene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00033n-Propylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00023o-Xylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00034Styrene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00032Toluene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00036Trichloroethylene
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00036Trichlorofluoromethane
BRL 8260B P5G034710.028 7/20/15 22:16 cgpAbmg/kg dry 0.00077Vinyl acetate
BRL 8260B P5G034710.0056 7/20/15 22:16 cgpmg/kg dry 0.00027Vinyl chloride
BRL 8260B P5G034710.017 7/20/15 22:16 cgpmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130118 %4-Bromofluorobenzene
84-12346 %Dibromofluoromethane SR
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: E-1
Prism Sample ID: 5070245-18
Prism Work Order: 5070245
Time Collected: 07/13/15 12:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
96.8 *SM2540 G P5G025310.100 7/15/15 15:31 ARC% by
Weight
0.100% Solids
12 *9045D P5G035817/20/15 15:30 EGCAapH UnitsCorrosivity-pH
Pass *1030 P5G041010.10 7/22/15 17:09 ARCmm/secIgnitability
490 *9071B P5G03371417/17/15 11:30 MJOmg/kg dry 13Oil & Grease (HEM)
Polychlorinated Biphenyls (PCBs) by GC/ECD
2.5 8082A P5G0284100.52 7/30/15 13:36 JMCAjmg/kg dry 0.049Aroclor 1016
BRL 8082A P5G0284101.0 7/30/15 13:36 JMCAimg/kg dry 0.41Aroclor 1221
BRL 8082A P5G0284101.0 7/30/15 13:36 JMCAimg/kg dry 0.13Aroclor 1232
BRL 8082A P5G0284100.52 7/30/15 13:36 JMCAimg/kg dry 0.14Aroclor 1242
BRL 8082A P5G0284100.52 7/30/15 13:36 JMCAimg/kg dry 0.10Aroclor 1248
1.6 8082A P5G0284100.52 7/30/15 13:36 JMCAimg/kg dry 0.13Aroclor 1254
BRL 8082A P5G0284100.52 7/30/15 13:36 JMCAimg/kg dry 0.071Aroclor 1260
Surrogate Recovery Control Limits
36-1820 %Tetrachloro-m-xylene DO
34-1820 %Decachlorobiphenyl DO
Semivolatile Organic Compounds by GC/MS RL
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 3.31-Methylnaphthalene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.72-Methylnaphthalene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.3Acenaphthene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.5Acenaphthylene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.7Anthracene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.2Benzo(a)anthracene
BRL 8270D P5G03295178/3/15 16:56 JMVCCVmg/kg dry 1.8Benzo(a)pyrene
BRL 8270D P5G03295178/3/15 16:56 JMVCCVmg/kg dry 2.0Benzo(b)fluoranthene
BRL 8270D P5G03295178/3/15 16:56 JMVCCVmg/kg dry 1.9Benzo(g,h,i)perylene
BRL 8270D P5G03295178/3/15 16:56 JMVCCVmg/kg dry 2.2Benzo(k)fluoranthene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.1Chrysene
BRL 8270D P5G03295178/3/15 16:56 JMVCCVmg/kg dry 2.1Dibenzo(a,h)anthracene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.2Fluoranthene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.4Fluorene
BRL 8270D P5G03295178/3/15 16:56 JMVCCVmg/kg dry 2.0Indeno(1,2,3-cd)pyrene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.7Naphthalene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.2Phenanthrene
BRL 8270D P5G03295178/3/15 16:56 JMVmg/kg dry 2.3Pyrene
Surrogate Recovery Control Limits
44-1150 %2-Fluorobiphenyl DO
37-1220 %Nitrobenzene-d5 DO
54-1270 %Terphenyl-d14 DO
Total Metals
BRL *7471B P5G027010.021 7/16/15 16:06 JABmg/kg dry 0.0013Mercury
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: E-1
Prism Sample ID: 5070245-18
Prism Work Order: 5070245
Time Collected: 07/13/15 12:00
Time Submitted: 07/14/15 11:30
21 *6010C P5G0294102.6 7/20/15 17:33 MWWDMmg/kg dry 0.37Arsenic
56 *6010C P5G0294105.2 7/20/15 17:33 MWWDMmg/kg dry 1.0Barium
BRL *6010C P5G029410.26 7/18/15 2:22 MWWmg/kg dry 0.037Cadmium
26 *6010C P5G0294102.6 7/20/15 17:33 MWWDMmg/kg dry 0.43Chromium
100 *6010C P5G0294102.6 7/20/15 17:33 MWWDMmg/kg dry 0.40Lead
BRL *6010C P5G0294105.2 7/20/15 17:33 MWWDMmg/kg dry 0.63Selenium
BRL *6010C P5G0294102.6 7/20/15 17:33 MWWmg/kg dry 0.30Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000741,1,1,2-Tetrachloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000441,1,1-Trichloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000611,1,2,2-Tetrachloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000801,1,2-Trichloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000251,1-Dichloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000401,1-Dichloroethylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000501,1-Dichloropropylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000511,2,3-Trichlorobenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00121,2,3-Trichloropropane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000671,2,4-Trichlorobenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000691,2,4-Trimethylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000361,2-Dibromoethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000431,2-Dichlorobenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000541,2-Dichloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000561,2-Dichloropropane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000681,3,5-Trimethylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000601,3-Dichlorobenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000451,3-Dichloropropane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000361,4-Dichlorobenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000432,2-Dichloropropane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000472-Chlorotoluene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000544-Chlorotoluene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.000444-Isopropyltoluene
0.11 8260B P5G034710.091 7/20/15 22:49 cgpmg/kg dry 0.0022Acetone
BRL 8260B P5G034710.0054 7/20/15 22:49 cgpmg/kg dry 0.00053Benzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00076Bromobenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00050Bromochloromethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00051Bromodichloromethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.0010Bromoform
BRL 8260B P5G034710.018 7/20/15 22:49 cgpmg/kg dry 0.0011Bromomethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00045Carbon Tetrachloride
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00048Chlorobenzene
BRL 8260B P5G034710.018 7/20/15 22:49 cgpmg/kg dry 0.00076Chloroethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00065Chloroform
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00061Chloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Solid
Client Sample ID: E-1
Prism Sample ID: 5070245-18
Prism Work Order: 5070245
Time Collected: 07/13/15 12:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00039cis-1,2-Dichloroethylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00030cis-1,3-Dichloropropylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00037Dibromochloromethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00041Dichlorodifluoromethane
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00035Ethylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00037Isopropyl Ether
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00054Isopropylbenzene (Cumene)
BRL 8260B P5G034710.018 7/20/15 22:49 cgpmg/kg dry 0.00084m,p-Xylenes
BRL 8260B P5G034710.091 7/20/15 22:49 cgpmg/kg dry 0.00082Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G034710.18 7/20/15 22:49 cgpmg/kg dry 0.00082Methyl Ethyl Ketone (2-Butanone)
0.0038 8260B P5G034710.091 7/20/15 22:49 cgpJmg/kg dry 0.00077Methyl Isobutyl Ketone
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00051Methylene Chloride
BRL 8260B P5G034710.018 7/20/15 22:49 cgpmg/kg dry 0.00029Methyl-tert-Butyl Ether
BRL 8260B P5G034710.018 7/20/15 22:49 cgpmg/kg dry 0.00029Naphthalene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00046n-Butylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00054n-Propylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00037o-Xylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00044sec-Butylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00055Styrene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00031tert-Butylbenzene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00043Tetrachloroethylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00052Toluene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00054trans-1,2-Dichloroethylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00048trans-1,3-Dichloropropylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00059Trichloroethylene
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00059Trichlorofluoromethane
BRL 8260B P5G034710.045 7/20/15 22:49 cgpAbmg/kg dry 0.0012Vinyl acetate
BRL 8260B P5G034710.0091 7/20/15 22:49 cgpmg/kg dry 0.00044Vinyl chloride
BRL 8260B P5G034710.027 7/20/15 22:49 cgpmg/kg dry 0.0017Xylenes, total
Surrogate Recovery Control Limits
70-130118 %4-Bromofluorobenzene
84-12398 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Non-aqueous Liquid
Client Sample ID: PR-Oil
Prism Sample ID: 5070245-19
Prism Work Order: 5070245
Time Collected: 07/14/15 09:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
7.9 *9045D P5G031517/17/15 11:50 EGCAapH UnitspH
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G031611.0 7/30/15 13:48 JMCmg/kg 0.50Aroclor 1016
BRL 8082A P5G031615.0 7/30/15 13:48 JMCmg/kg 2.5Aroclor 1221
BRL 8082A P5G031611.0 7/30/15 13:48 JMCmg/kg 0.50Aroclor 1232
BRL 8082A P5G031611.0 7/30/15 13:48 JMCmg/kg 0.50Aroclor 1242
BRL 8082A P5G031611.0 7/30/15 13:48 JMCmg/kg 0.50Aroclor 1248
BRL 8082A P5G031611.0 7/30/15 13:48 JMCmg/kg 0.50Aroclor 1254
BRL 8082A P5G031611.0 7/30/15 13:48 JMCmg/kg 0.50Aroclor 1260
Surrogate Recovery Control Limits
72-14790 %Tetrachloro-m-xylene
65-16012 %Decachlorobiphenyl Af
Total Metals
BRL *7471B P5G027110.021 7/16/15 16:53 JABmg/kg wet 0.0014Mercury
BRL *6010C P5G029510.25 7/20/15 13:49 MWWmg/kg wet 0.035Arsenic
1.5 *6010C P5G029510.49 7/20/15 13:49 MWWmg/kg wet 0.095Barium
BRL *6010C P5G029510.25 7/20/15 13:49 MWWmg/kg wet 0.035Cadmium
BRL *6010C P5G029510.25 7/20/15 13:49 MWWmg/kg wet 0.040Chromium
6.0 *6010C P5G029510.25 7/20/15 13:49 MWWmg/kg wet 0.037Lead
BRL *6010C P5G029510.49 7/20/15 13:49 MWWmg/kg wet 0.059Selenium
BRL *6010C P5G029510.25 7/20/15 13:49 MWWmg/kg wet 0.028Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 4101,1,1,2-Tetrachloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2401,1,1-Trichloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 3401,1,2,2-Tetrachloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 4401,1,2-Trichloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 1401,1-Dichloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2201,1-Dichloroethylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2701,1-Dichloropropylene
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 2801,2,3-Trichlorobenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 6401,2,3-Trichloropropane
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 3701,2,4-Trichlorobenzene
2700 8260B P5G04631000050007/24/15 21:07 cgpJmg/kg 3801,2,4-Trimethylbenzene
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 3701,2-Dibromo-3-chloropropane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2001,2-Dibromoethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2401,2-Dichlorobenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 3001,2-Dichloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 3101,2-Dichloropropane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 3801,3,5-Trimethylbenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 3301,3-Dichlorobenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2501,3-Dichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Non-aqueous Liquid
Client Sample ID: PR-Oil
Prism Sample ID: 5070245-19
Prism Work Order: 5070245
Time Collected: 07/14/15 09:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2001,4-Dichlorobenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2402,2-Dichloropropane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 9302-Chloroethyl Vinyl Ether
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2602-Chlorotoluene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 3004-Chlorotoluene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 2404-Isopropyltoluene
BRL 8260B P5G046310000200007/24/15 21:07 cgpmg/kg 1200Acetone
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 290Benzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 420Bromobenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 280Bromochloromethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 280Bromodichloromethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 570Bromoform
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 620Bromomethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpCVLmg/kg 240Carbon disulfide
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 250Carbon Tetrachloride
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 260Chlorobenzene
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 420Chloroethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 360Chloroform
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 340Chloromethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 210cis-1,2-Dichloroethylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 170cis-1,3-Dichloropropylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 210Dibromochloromethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 430Dibromomethane
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 230Dichlorodifluoromethane
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 190Ethylbenzene
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 400Hexachlorobutadiene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 200Isopropyl Ether
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 300Isopropylbenzene (Cumene)
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 460m,p-Xylenes
BRL 8260B P5G046310000200007/24/15 21:07 cgpmg/kg 450Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G046310000200007/24/15 21:07 cgpmg/kg 450Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5G046310000200007/24/15 21:07 cgpmg/kg 430Methyl Isobutyl Ketone
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 280Methylene Chloride
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 160Methyl-tert-Butyl Ether
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 160Naphthalene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 260n-Butylbenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 300n-Propylbenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 200o-Xylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 240sec-Butylbenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 300Styrene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 170tert-Butylbenzene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 240Tetrachloroethylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 290Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Non-aqueous Liquid
Client Sample ID: PR-Oil
Prism Sample ID: 5070245-19
Prism Work Order: 5070245
Time Collected: 07/14/15 09:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 300trans-1,2-Dichloroethylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 260trans-1,3-Dichloropropylene
BRL 8260B P5G04631000050007/24/15 21:07 cgpmg/kg 320Trichloroethylene
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 320Trichlorofluoromethane
BRL 8260B P5G046310000100007/24/15 21:07 cgpmg/kg 240Vinyl chloride
Surrogate Recovery Control Limits
70-1300 %4-Bromofluorobenzene DO
70-1300 %Dibromofluoromethane DO
70-1300 %Toluene-d8 DO
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Non-aqueous Liquid
Client Sample ID: WO-Wase1
Prism Sample ID: 5070245-20
Prism Work Order: 5070245
Time Collected: 07/14/15 09:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
7.4 *9045D P5G031517/17/15 11:50 EGCAapH UnitspH
Polychlorinated Biphenyls (PCBs) by GC/ECD
BRL 8082A P5G031611.0 7/30/15 13:59 JMCmg/kg 0.50Aroclor 1016
BRL 8082A P5G031615.0 7/30/15 13:59 JMCmg/kg 2.5Aroclor 1221
BRL 8082A P5G031611.0 7/30/15 13:59 JMCmg/kg 0.50Aroclor 1232
BRL 8082A P5G031611.0 7/30/15 13:59 JMCmg/kg 0.50Aroclor 1242
BRL 8082A P5G031611.0 7/30/15 13:59 JMCmg/kg 0.50Aroclor 1248
BRL 8082A P5G031611.0 7/30/15 13:59 JMCmg/kg 0.50Aroclor 1254
BRL 8082A P5G031611.0 7/30/15 13:59 JMCmg/kg 0.50Aroclor 1260
Surrogate Recovery Control Limits
72-14780 %Tetrachloro-m-xylene
65-16013 %Decachlorobiphenyl Af
Total Metals
BRL *7471B P5G027110.021 7/16/15 17:08 JABmg/kg wet 0.0014Mercury
BRL *6010C P5G029510.25 7/20/15 13:55 MWWmg/kg wet 0.035Arsenic
1.7 *6010C P5G029510.50 7/20/15 13:55 MWWmg/kg wet 0.095Barium
BRL *6010C P5G029510.25 7/20/15 13:55 MWWmg/kg wet 0.035Cadmium
0.38 *6010C P5G029510.25 7/20/15 13:55 MWWmg/kg wet 0.041Chromium
0.54 *6010C P5G029510.25 7/20/15 17:10 MWWmg/kg wet 0.038Lead
BRL *6010C P5G029510.50 7/20/15 17:10 MWWmg/kg wet 0.059Selenium
BRL *6010C P5G029510.25 7/20/15 13:55 MWWmg/kg wet 0.028Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 4101,1,1,2-Tetrachloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2401,1,1-Trichloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3401,1,2,2-Tetrachloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 4401,1,2-Trichloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 1401,1-Dichloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2201,1-Dichloroethylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2701,1-Dichloropropylene
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 2801,2,3-Trichlorobenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 6401,2,3-Trichloropropane
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 3701,2,4-Trichlorobenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3801,2,4-Trimethylbenzene
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 3701,2-Dibromo-3-chloropropane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2001,2-Dibromoethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2401,2-Dichlorobenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3001,2-Dichloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3101,2-Dichloropropane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3801,3,5-Trimethylbenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3301,3-Dichlorobenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2501,3-Dichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 67 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Non-aqueous Liquid
Client Sample ID: WO-Wase1
Prism Sample ID: 5070245-20
Prism Work Order: 5070245
Time Collected: 07/14/15 09:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2001,4-Dichlorobenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2402,2-Dichloropropane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 9302-Chloroethyl Vinyl Ether
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2602-Chlorotoluene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 3004-Chlorotoluene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 2404-Isopropyltoluene
BRL 8260B P5G046310000200007/24/15 22:15 cgpmg/kg 1200Acetone
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 290Benzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 420Bromobenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 280Bromochloromethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 280Bromodichloromethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 570Bromoform
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 620Bromomethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpCVLmg/kg 240Carbon disulfide
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 250Carbon Tetrachloride
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 260Chlorobenzene
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 420Chloroethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 360Chloroform
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 340Chloromethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 210cis-1,2-Dichloroethylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 170cis-1,3-Dichloropropylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 210Dibromochloromethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 430Dibromomethane
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 230Dichlorodifluoromethane
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 190Ethylbenzene
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 400Hexachlorobutadiene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 200Isopropyl Ether
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 300Isopropylbenzene (Cumene)
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 460m,p-Xylenes
BRL 8260B P5G046310000200007/24/15 22:15 cgpmg/kg 450Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5G046310000200007/24/15 22:15 cgpmg/kg 450Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5G046310000200007/24/15 22:15 cgpmg/kg 430Methyl Isobutyl Ketone
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 280Methylene Chloride
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 160Methyl-tert-Butyl Ether
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 160Naphthalene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 260n-Butylbenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 300n-Propylbenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 200o-Xylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 240sec-Butylbenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 300Styrene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 170tert-Butylbenzene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 240Tetrachloroethylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 290Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 68 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Non-aqueous Liquid
Client Sample ID: WO-Wase1
Prism Sample ID: 5070245-20
Prism Work Order: 5070245
Time Collected: 07/14/15 09:00
Time Submitted: 07/14/15 11:30
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 300trans-1,2-Dichloroethylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 260trans-1,3-Dichloropropylene
BRL 8260B P5G04631000050007/24/15 22:15 cgpmg/kg 320Trichloroethylene
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 320Trichlorofluoromethane
BRL 8260B P5G046310000100007/24/15 22:15 cgpmg/kg 240Vinyl chloride
Surrogate Recovery Control Limits
70-1300 %4-Bromofluorobenzene DO
70-1300 %Dibromofluoromethane DO
70-1300 %Toluene-d8 DO
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 69 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Wipe
Client Sample ID: AG-1
Prism Sample ID: 5070245-21
Prism Work Order: 5070245
Time Collected: 07/14/15 08:00
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
10 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Total Metals
BRL *7471B P5G027010.019 7/16/15 16:11 JABAmg/kg wet 0.0012Mercury
BRL *6010C P5G029410.25 7/18/15 2:33 MWWmg/kg wet 0.035Arsenic
BRL *6010C P5G029410.50 7/18/15 2:33 MWWmg/kg wet 0.095Barium
BRL *6010C P5G029410.25 7/18/15 2:33 MWWmg/kg wet 0.035Cadmium
0.89 *6010C P5G029410.25 7/20/15 17:41 MWWmg/kg wet 0.041Chromium
BRL *6010C P5G029410.25 7/18/15 2:33 MWWmg/kg wet 0.038Lead
BRL *6010C P5G029410.50 7/18/15 2:33 MWWmg/kg wet 0.059Selenium
11 *6010C P5G029410.25 7/20/15 17:41 MWWmg/kg wet 0.028Silver
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 70 of 135
Laboratory Report
08/06/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Wipe
Client Sample ID: AG-2
Prism Sample ID: 5070245-22
Prism Work Order: 5070245
Time Collected: 07/14/15 08:05
Time Submitted: 07/14/15 11:30
General Chemistry Parameters
8.4 *9045D P5G031017/17/15 11:50 EGCpH UnitsCorrosivity-pH
Total Metals
BRL *7471B P5G027010.019 7/16/15 16:16 JABAmg/kg wet 0.0012Mercury
BRL *6010C P5G029410.25 7/18/15 2:38 MWWmg/kg wet 0.036Arsenic
0.94 *6010C P5G029410.51 7/20/15 17:47 MWWmg/kg wet 0.097Barium
BRL *6010C P5G029410.25 7/18/15 2:38 MWWmg/kg wet 0.036Cadmium
5.8 *6010C P5G029410.25 7/20/15 17:47 MWWmg/kg wet 0.042Chromium
BRL *6010C P5G029410.25 7/18/15 2:38 MWWmg/kg wet 0.038Lead
BRL *6010C P5G029410.51 7/18/15 2:38 MWWmg/kg wet 0.061Selenium
800 *6010C P5G029450137/20/15 17:47 MWWAgmg/kg wet 1.5Silver
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 71 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0318 - 5035
Blank (P5G0318-BLK1)Prepared: 07/17/15 Analyzed: 07/18/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 72 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0318 - 5035
Blank (P5G0318-BLK1)Prepared: 07/17/15 Analyzed: 07/18/15
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 930.0463
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 900.0452
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 890.0447
LCS (P5G0318-BS1)Prepared: 07/17/15 Analyzed: 07/18/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0622 0.0050 0.05000 LH72-115124
1,1,1-Trichloroethane mg/kg wet0.0570 0.0050 0.05000 67-131114
1,1,2,2-Tetrachloroethane mg/kg wet0.0609 0.0050 0.05000 56-126122
1,1,2-Trichloroethane mg/kg wet0.0586 0.0050 0.05000 70-133117
1,1-Dichloroethane mg/kg wet0.0560 0.0050 0.05000 74-127112
1,1-Dichloroethylene mg/kg wet0.0596 0.0050 0.05000 67-149119
1,1-Dichloropropylene mg/kg wet0.0646 0.0050 0.05000 71-130129
1,2,3-Trichlorobenzene mg/kg wet0.0623 0.0050 0.05000 68-130125
1,2,3-Trichloropropane mg/kg wet0.0641 0.0050 0.05000 60-137128
1,2,4-Trichlorobenzene mg/kg wet0.0607 0.0050 0.05000 66-125121
1,2,4-Trimethylbenzene mg/kg wet0.0629 0.0050 0.05000 69-129126
1,2-Dibromoethane mg/kg wet0.0621 0.0050 0.05000 70-132124
1,2-Dichlorobenzene mg/kg wet0.0601 0.0050 0.05000 72-123120
1,2-Dichloroethane mg/kg wet0.0569 0.0050 0.05000 68-128114
1,2-Dichloropropane mg/kg wet0.0603 0.0050 0.05000 73-130121
1,3,5-Trimethylbenzene mg/kg wet0.0634 0.0050 0.05000 69-128127
1,3-Dichlorobenzene mg/kg wet0.0606 0.0050 0.05000 L171-120121
1,3-Dichloropropane mg/kg wet0.0612 0.0050 0.05000 75-124122
1,4-Dichlorobenzene mg/kg wet0.0586 0.0050 0.05000 71-123117
2,2-Dichloropropane mg/kg wet0.0553 0.0050 0.05000 50-142111
2-Chlorotoluene mg/kg wet0.0604 0.0050 0.05000 67-124121
4-Chlorotoluene mg/kg wet0.0610 0.0050 0.05000 71-126122
4-Isopropyltoluene mg/kg wet0.0642 0.0050 0.05000 68-129128
Acetone mg/kg wet0.118 0.050 0.1000 29-198118
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 73 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0318 - 5035
LCS (P5G0318-BS1)Prepared: 07/17/15 Analyzed: 07/18/15
Benzene mg/kg wet0.0603 0.0030 0.05000 74-127121
Bromobenzene mg/kg wet0.0598 0.0050 0.05000 73-125120
Bromochloromethane mg/kg wet0.0615 0.0050 0.05000 72-134123
Bromodichloromethane mg/kg wet0.0556 0.0050 0.05000 75-122111
Bromoform mg/kg wet0.0548 0.0050 0.05000 66-135110
Bromomethane mg/kg wet0.0615 0.010 0.05000 20-180123
Carbon Tetrachloride mg/kg wet0.0660 0.0050 0.05000 64-143132
Chlorobenzene mg/kg wet0.0598 0.0050 0.05000 L174-118120
Chloroethane mg/kg wet0.0618 0.010 0.05000 33-149124
Chloroform mg/kg wet0.0554 0.0050 0.05000 73-127111
Chloromethane mg/kg wet0.0580 0.0050 0.05000 45-143116
cis-1,2-Dichloroethylene mg/kg wet0.0578 0.0050 0.05000 76-134116
cis-1,3-Dichloropropylene mg/kg wet0.0598 0.0050 0.05000 71-125120
Dibromochloromethane mg/kg wet0.0568 0.0050 0.05000 73-122114
Dichlorodifluoromethane mg/kg wet0.0558 0.0050 0.05000 26-146112
Ethylbenzene mg/kg wet0.0610 0.0050 0.05000 74-128122
Isopropyl Ether mg/kg wet0.0550 0.0050 0.05000 59-159110
Isopropylbenzene (Cumene)mg/kg wet0.0681 0.0050 0.05000 LH68-126136
m,p-Xylenes mg/kg wet0.128 0.010 0.1000 L175-124128
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0678 0.050 0.05000 61-157136
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0562 0.10 0.05000 J63-149112
Methyl Isobutyl Ketone mg/kg wet0.0622 0.050 0.05000 57-162124
Methylene Chloride mg/kg wet0.0576 0.0050 0.05000 74-129115
Methyl-tert-Butyl Ether mg/kg wet0.0567 0.010 0.05000 70-130113
Naphthalene mg/kg wet0.0658 0.010 0.05000 57-157132
n-Butylbenzene mg/kg wet0.0639 0.0050 0.05000 65-135128
n-Propylbenzene mg/kg wet0.0643 0.0050 0.05000 67-130129
o-Xylene mg/kg wet0.0623 0.0050 0.05000 74-126125
sec-Butylbenzene mg/kg wet0.0679 0.0050 0.05000 L166-131136
Styrene mg/kg wet0.0646 0.0050 0.05000 LH77-121129
tert-Butylbenzene mg/kg wet0.0639 0.0050 0.05000 67-132128
Tetrachloroethylene mg/kg wet0.0584 0.0050 0.05000 68-130117
Toluene mg/kg wet0.0603 0.0050 0.05000 71-129121
trans-1,2-Dichloroethylene mg/kg wet0.0586 0.0050 0.05000 73-132117
trans-1,3-Dichloropropylene mg/kg wet0.0615 0.0050 0.05000 68-123123
Trichloroethylene mg/kg wet0.0596 0.0050 0.05000 75-133119
Trichlorofluoromethane mg/kg wet0.0590 0.0050 0.05000 44-146118
Vinyl acetate mg/kg wet0.0609 0.025 0.05000 85-161122
Vinyl chloride mg/kg wet0.0611 0.0050 0.05000 48-147122
Xylenes, total mg/kg wet0.190 0.015 0.1500 L174-126127
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 910.0454
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 910.0453
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 920.0460
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 74 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0318 - 5035
LCS Dup (P5G0318-BSD1)Prepared: 07/17/15 Analyzed: 07/18/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0596 0.0050 0.05000 20 LH72-115119 4
1,1,1-Trichloroethane mg/kg wet0.0526 0.0050 0.05000 2067-131105 8
1,1,2,2-Tetrachloroethane mg/kg wet0.0580 0.0050 0.05000 2056-126116 5
1,1,2-Trichloroethane mg/kg wet0.0563 0.0050 0.05000 2070-133113 4
1,1-Dichloroethane mg/kg wet0.0535 0.0050 0.05000 2074-127107 4
1,1-Dichloroethylene mg/kg wet0.0554 0.0050 0.05000 2067-149111 7
1,1-Dichloropropylene mg/kg wet0.0608 0.0050 0.05000 2071-130122 6
1,2,3-Trichlorobenzene mg/kg wet0.0591 0.0050 0.05000 2068-130118 5
1,2,3-Trichloropropane mg/kg wet0.0587 0.0050 0.05000 2060-137117 9
1,2,4-Trichlorobenzene mg/kg wet0.0570 0.0050 0.05000 2066-125114 6
1,2,4-Trimethylbenzene mg/kg wet0.0588 0.0050 0.05000 2069-129118 7
1,2-Dibromoethane mg/kg wet0.0599 0.0050 0.05000 2070-132120 4
1,2-Dichlorobenzene mg/kg wet0.0577 0.0050 0.05000 2072-123115 4
1,2-Dichloroethane mg/kg wet0.0554 0.0050 0.05000 2068-128111 3
1,2-Dichloropropane mg/kg wet0.0596 0.0050 0.05000 2073-130119 1
1,3,5-Trimethylbenzene mg/kg wet0.0594 0.0050 0.05000 2069-128119 6
1,3-Dichlorobenzene mg/kg wet0.0566 0.0050 0.05000 2071-120113 7
1,3-Dichloropropane mg/kg wet0.0594 0.0050 0.05000 2075-124119 3
1,4-Dichlorobenzene mg/kg wet0.0551 0.0050 0.05000 2071-123110 6
2,2-Dichloropropane mg/kg wet0.0526 0.0050 0.05000 2050-142105 5
2-Chlorotoluene mg/kg wet0.0584 0.0050 0.05000 2067-124117 3
4-Chlorotoluene mg/kg wet0.0575 0.0050 0.05000 2071-126115 6
4-Isopropyltoluene mg/kg wet0.0594 0.0050 0.05000 2068-129119 8
Acetone mg/kg wet0.108 0.050 0.1000 2029-198108 9
Benzene mg/kg wet0.0579 0.0030 0.05000 2074-127116 4
Bromobenzene mg/kg wet0.0564 0.0050 0.05000 2073-125113 6
Bromochloromethane mg/kg wet0.0610 0.0050 0.05000 2072-134122 0.9
Bromodichloromethane mg/kg wet0.0543 0.0050 0.05000 2075-122109 2
Bromoform mg/kg wet0.0527 0.0050 0.05000 2066-135105 4
Bromomethane mg/kg wet0.0570 0.010 0.05000 2020-180114 8
Carbon Tetrachloride mg/kg wet0.0603 0.0050 0.05000 2064-143121 9
Chlorobenzene mg/kg wet0.0570 0.0050 0.05000 2074-118114 5
Chloroethane mg/kg wet0.0573 0.010 0.05000 2033-149115 7
Chloroform mg/kg wet0.0531 0.0050 0.05000 2073-127106 4
Chloromethane mg/kg wet0.0538 0.0050 0.05000 2045-143108 7
cis-1,2-Dichloroethylene mg/kg wet0.0554 0.0050 0.05000 2076-134111 4
cis-1,3-Dichloropropylene mg/kg wet0.0586 0.0050 0.05000 2071-125117 2
Dibromochloromethane mg/kg wet0.0547 0.0050 0.05000 2073-122109 4
Dichlorodifluoromethane mg/kg wet0.0501 0.0050 0.05000 2026-146100 11
Ethylbenzene mg/kg wet0.0567 0.0050 0.05000 2074-128113 7
Isopropyl Ether mg/kg wet0.0537 0.0050 0.05000 2059-159107 2
Isopropylbenzene (Cumene)mg/kg wet0.0640 0.0050 0.05000 20 LH68-126128 6
m,p-Xylenes mg/kg wet0.119 0.010 0.1000 2075-124119 7
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0612 0.050 0.05000 2061-157122 10
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0525 0.10 0.05000 20 J63-149105 7
Methyl Isobutyl Ketone mg/kg wet0.0578 0.050 0.05000 2057-162116 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 75 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0318 - 5035
LCS Dup (P5G0318-BSD1)Prepared: 07/17/15 Analyzed: 07/18/15
Methylene Chloride mg/kg wet0.0559 0.0050 0.05000 2074-129112 3
Methyl-tert-Butyl Ether mg/kg wet0.0557 0.010 0.05000 2070-130111 2
Naphthalene mg/kg wet0.0623 0.010 0.05000 2057-157125 5
n-Butylbenzene mg/kg wet0.0584 0.0050 0.05000 2065-135117 9
n-Propylbenzene mg/kg wet0.0598 0.0050 0.05000 2067-130120 7
o-Xylene mg/kg wet0.0590 0.0050 0.05000 2074-126118 5
sec-Butylbenzene mg/kg wet0.0633 0.0050 0.05000 2066-131127 7
Styrene mg/kg wet0.0612 0.0050 0.05000 20 LH77-121122 5
tert-Butylbenzene mg/kg wet0.0600 0.0050 0.05000 2067-132120 6
Tetrachloroethylene mg/kg wet0.0537 0.0050 0.05000 2068-130107 8
Toluene mg/kg wet0.0576 0.0050 0.05000 2071-129115 5
trans-1,2-Dichloroethylene mg/kg wet0.0557 0.0050 0.05000 2073-132111 5
trans-1,3-Dichloropropylene mg/kg wet0.0610 0.0050 0.05000 2068-123122 0.9
Trichloroethylene mg/kg wet0.0563 0.0050 0.05000 2075-133113 6
Trichlorofluoromethane mg/kg wet0.0545 0.0050 0.05000 2044-146109 8
Vinyl acetate mg/kg wet0.0587 0.025 0.05000 2085-161117 4
Vinyl chloride mg/kg wet0.0554 0.0050 0.05000 2048-147111 10
Xylenes, total mg/kg wet0.178 0.015 0.1500 2074-126119 7
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 900.0448
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 920.0458
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 910.0456
Batch P5G0347 - 5035
Blank (P5G0347-BLK1)Prepared & Analyzed: 07/20/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 76 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0347 - 5035
Blank (P5G0347-BLK1)Prepared & Analyzed: 07/20/15
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1080.0542
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 970.0484
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 930.0466
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 77 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0347 - 5035
LCS (P5G0347-BS1)Prepared & Analyzed: 07/20/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0452 0.0050 0.05000 72-11590
1,1,1-Trichloroethane mg/kg wet0.0454 0.0050 0.05000 67-13191
1,1,2,2-Tetrachloroethane mg/kg wet0.0489 0.0050 0.05000 56-12698
1,1,2-Trichloroethane mg/kg wet0.0457 0.0050 0.05000 70-13391
1,1-Dichloroethane mg/kg wet0.0430 0.0050 0.05000 74-12786
1,1-Dichloroethylene mg/kg wet0.0465 0.0050 0.05000 67-14993
1,1-Dichloropropylene mg/kg wet0.0482 0.0050 0.05000 71-13096
1,2,3-Trichlorobenzene mg/kg wet0.0569 0.0050 0.05000 68-130114
1,2,3-Trichloropropane mg/kg wet0.0485 0.0050 0.05000 60-13797
1,2,4-Trichlorobenzene mg/kg wet0.0535 0.0050 0.05000 66-125107
1,2,4-Trimethylbenzene mg/kg wet0.0494 0.0050 0.05000 69-12999
1,2-Dibromoethane mg/kg wet0.0474 0.0050 0.05000 70-13295
1,2-Dichlorobenzene mg/kg wet0.0477 0.0050 0.05000 72-12395
1,2-Dichloroethane mg/kg wet0.0438 0.0050 0.05000 68-12888
1,2-Dichloropropane mg/kg wet0.0425 0.0050 0.05000 73-13085
1,3,5-Trimethylbenzene mg/kg wet0.0498 0.0050 0.05000 69-128100
1,3-Dichlorobenzene mg/kg wet0.0461 0.0050 0.05000 71-12092
1,3-Dichloropropane mg/kg wet0.0449 0.0050 0.05000 75-12490
1,4-Dichlorobenzene mg/kg wet0.0465 0.0050 0.05000 71-12393
2,2-Dichloropropane mg/kg wet0.0428 0.0050 0.05000 50-14286
2-Chlorotoluene mg/kg wet0.0477 0.0050 0.05000 67-12495
4-Chlorotoluene mg/kg wet0.0467 0.0050 0.05000 71-12693
4-Isopropyltoluene mg/kg wet0.0495 0.0050 0.05000 68-12999
Acetone mg/kg wet0.0911 0.050 0.1000 29-19891
Benzene mg/kg wet0.0474 0.0030 0.05000 74-12795
Bromobenzene mg/kg wet0.0472 0.0050 0.05000 73-12594
Bromochloromethane mg/kg wet0.0491 0.0050 0.05000 72-13498
Bromodichloromethane mg/kg wet0.0419 0.0050 0.05000 75-12284
Bromoform mg/kg wet0.0455 0.0050 0.05000 66-13591
Bromomethane mg/kg wet0.0424 0.010 0.05000 20-18085
Carbon Tetrachloride mg/kg wet0.0494 0.0050 0.05000 64-14399
Chlorobenzene mg/kg wet0.0466 0.0050 0.05000 74-11893
Chloroethane mg/kg wet0.0365 0.010 0.05000 33-14973
Chloroform mg/kg wet0.0421 0.0050 0.05000 73-12784
Chloromethane mg/kg wet0.0374 0.0050 0.05000 45-14375
cis-1,2-Dichloroethylene mg/kg wet0.0433 0.0050 0.05000 76-13487
cis-1,3-Dichloropropylene mg/kg wet0.0426 0.0050 0.05000 71-12585
Dibromochloromethane mg/kg wet0.0430 0.0050 0.05000 73-12286
Dichlorodifluoromethane mg/kg wet0.0388 0.0050 0.05000 26-14678
Ethylbenzene mg/kg wet0.0456 0.0050 0.05000 74-12891
Isopropyl Ether mg/kg wet0.0373 0.0050 0.05000 59-15975
Isopropylbenzene (Cumene)mg/kg wet0.0491 0.0050 0.05000 68-12698
m,p-Xylenes mg/kg wet0.0903 0.010 0.1000 75-12490
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0461 0.050 0.05000 J61-15792
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0494 0.10 0.05000 J63-14999
Methyl Isobutyl Ketone mg/kg wet0.0430 0.050 0.05000 J57-16286
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 78 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0347 - 5035
LCS (P5G0347-BS1)Prepared & Analyzed: 07/20/15
Methylene Chloride mg/kg wet0.0404 0.0050 0.05000 74-12981
Methyl-tert-Butyl Ether mg/kg wet0.0452 0.010 0.05000 70-13090
Naphthalene mg/kg wet0.0541 0.010 0.05000 57-157108
n-Butylbenzene mg/kg wet0.0496 0.0050 0.05000 65-13599
n-Propylbenzene mg/kg wet0.0502 0.0050 0.05000 67-130100
o-Xylene mg/kg wet0.0465 0.0050 0.05000 74-12693
sec-Butylbenzene mg/kg wet0.0492 0.0050 0.05000 66-13198
Styrene mg/kg wet0.0483 0.0050 0.05000 77-12197
tert-Butylbenzene mg/kg wet0.0481 0.0050 0.05000 67-13296
Tetrachloroethylene mg/kg wet0.0486 0.0050 0.05000 68-13097
Toluene mg/kg wet0.0474 0.0050 0.05000 71-12995
trans-1,2-Dichloroethylene mg/kg wet0.0452 0.0050 0.05000 73-13290
trans-1,3-Dichloropropylene mg/kg wet0.0459 0.0050 0.05000 68-12392
Trichloroethylene mg/kg wet0.0484 0.0050 0.05000 75-13397
Trichlorofluoromethane mg/kg wet0.0373 0.0050 0.05000 44-14675
Vinyl acetate mg/kg wet0.0401 0.025 0.05000 Ab85-16180
Vinyl chloride mg/kg wet0.0405 0.0050 0.05000 48-14781
Xylenes, total mg/kg wet0.137 0.015 0.1500 74-12691
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1040.0518
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 970.0488
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 950.0475
LCS Dup (P5G0347-BSD1)Prepared & Analyzed: 07/20/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0466 0.0050 0.05000 2072-11593 3
1,1,1-Trichloroethane mg/kg wet0.0430 0.0050 0.05000 2067-13186 5
1,1,2,2-Tetrachloroethane mg/kg wet0.0493 0.0050 0.05000 2056-12699 0.9
1,1,2-Trichloroethane mg/kg wet0.0466 0.0050 0.05000 2070-13393 2
1,1-Dichloroethane mg/kg wet0.0410 0.0050 0.05000 2074-12782 5
1,1-Dichloroethylene mg/kg wet0.0445 0.0050 0.05000 2067-14989 4
1,1-Dichloropropylene mg/kg wet0.0453 0.0050 0.05000 2071-13091 6
1,2,3-Trichlorobenzene mg/kg wet0.0565 0.0050 0.05000 2068-130113 0.7
1,2,3-Trichloropropane mg/kg wet0.0462 0.0050 0.05000 2060-13792 5
1,2,4-Trichlorobenzene mg/kg wet0.0531 0.0050 0.05000 2066-125106 0.7
1,2,4-Trimethylbenzene mg/kg wet0.0477 0.0050 0.05000 2069-12995 4
1,2-Dibromoethane mg/kg wet0.0500 0.0050 0.05000 2070-132100 5
1,2-Dichlorobenzene mg/kg wet0.0477 0.0050 0.05000 2072-12395 0.04
1,2-Dichloroethane mg/kg wet0.0432 0.0050 0.05000 2068-12886 1
1,2-Dichloropropane mg/kg wet0.0428 0.0050 0.05000 2073-13086 0.7
1,3,5-Trimethylbenzene mg/kg wet0.0494 0.0050 0.05000 2069-12899 0.7
1,3-Dichlorobenzene mg/kg wet0.0479 0.0050 0.05000 2071-12096 4
1,3-Dichloropropane mg/kg wet0.0439 0.0050 0.05000 2075-12488 2
1,4-Dichlorobenzene mg/kg wet0.0465 0.0050 0.05000 2071-12393 0.1
2,2-Dichloropropane mg/kg wet0.0428 0.0050 0.05000 2050-14286 0.09
2-Chlorotoluene mg/kg wet0.0480 0.0050 0.05000 2067-12496 0.6
4-Chlorotoluene mg/kg wet0.0475 0.0050 0.05000 2071-12695 2
4-Isopropyltoluene mg/kg wet0.0471 0.0050 0.05000 2068-12994 5
Acetone mg/kg wet0.0904 0.050 0.1000 2029-19890 0.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 79 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0347 - 5035
LCS Dup (P5G0347-BSD1)Prepared & Analyzed: 07/20/15
Benzene mg/kg wet0.0463 0.0030 0.05000 2074-12793 2
Bromobenzene mg/kg wet0.0460 0.0050 0.05000 2073-12592 3
Bromochloromethane mg/kg wet0.0503 0.0050 0.05000 2072-134101 2
Bromodichloromethane mg/kg wet0.0420 0.0050 0.05000 2075-12284 0.4
Bromoform mg/kg wet0.0465 0.0050 0.05000 2066-13593 2
Bromomethane mg/kg wet0.0442 0.010 0.05000 2020-18088 4
Carbon Tetrachloride mg/kg wet0.0476 0.0050 0.05000 2064-14395 4
Chlorobenzene mg/kg wet0.0465 0.0050 0.05000 2074-11893 0.2
Chloroethane mg/kg wet0.0338 0.010 0.05000 2033-14968 8
Chloroform mg/kg wet0.0428 0.0050 0.05000 2073-12786 2
Chloromethane mg/kg wet0.0368 0.0050 0.05000 2045-14374 2
cis-1,2-Dichloroethylene mg/kg wet0.0446 0.0050 0.05000 2076-13489 3
cis-1,3-Dichloropropylene mg/kg wet0.0442 0.0050 0.05000 2071-12588 4
Dibromochloromethane mg/kg wet0.0446 0.0050 0.05000 2073-12289 3
Dichlorodifluoromethane mg/kg wet0.0382 0.0050 0.05000 2026-14676 2
Ethylbenzene mg/kg wet0.0462 0.0050 0.05000 2074-12892 1
Isopropyl Ether mg/kg wet0.0357 0.0050 0.05000 2059-15971 4
Isopropylbenzene (Cumene)mg/kg wet0.0489 0.0050 0.05000 2068-12698 0.5
m,p-Xylenes mg/kg wet0.0918 0.010 0.1000 2075-12492 2
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0456 0.050 0.05000 20 J61-15791 1
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0498 0.10 0.05000 20 J63-149100 0.8
Methyl Isobutyl Ketone mg/kg wet0.0437 0.050 0.05000 20 J57-16287 1
Methylene Chloride mg/kg wet0.0404 0.0050 0.05000 2074-12981 0.07
Methyl-tert-Butyl Ether mg/kg wet0.0456 0.010 0.05000 2070-13091 0.9
Naphthalene mg/kg wet0.0534 0.010 0.05000 2057-157107 1
n-Butylbenzene mg/kg wet0.0470 0.0050 0.05000 2065-13594 6
n-Propylbenzene mg/kg wet0.0483 0.0050 0.05000 2067-13097 4
o-Xylene mg/kg wet0.0460 0.0050 0.05000 2074-12692 1
sec-Butylbenzene mg/kg wet0.0488 0.0050 0.05000 2066-13198 0.8
Styrene mg/kg wet0.0484 0.0050 0.05000 2077-12197 0.3
tert-Butylbenzene mg/kg wet0.0456 0.0050 0.05000 2067-13291 5
Tetrachloroethylene mg/kg wet0.0479 0.0050 0.05000 2068-13096 1
Toluene mg/kg wet0.0467 0.0050 0.05000 2071-12993 1
trans-1,2-Dichloroethylene mg/kg wet0.0437 0.0050 0.05000 2073-13287 3
trans-1,3-Dichloropropylene mg/kg wet0.0451 0.0050 0.05000 2068-12390 2
Trichloroethylene mg/kg wet0.0466 0.0050 0.05000 2075-13393 4
Trichlorofluoromethane mg/kg wet0.0348 0.0050 0.05000 2044-14670 7
Vinyl acetate mg/kg wet0.0395 0.025 0.05000 20 Ab85-16179 2
Vinyl chloride mg/kg wet0.0408 0.0050 0.05000 2048-14782 0.7
Xylenes, total mg/kg wet0.138 0.015 0.1500 2074-12692 0.8
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1010.0504
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 940.0470
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 970.0485
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 80 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0385 - 5035
Blank (P5G0385-BLK1)Prepared: 07/21/15 Analyzed: 07/22/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 81 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0385 - 5035
Blank (P5G0385-BLK1)Prepared: 07/21/15 Analyzed: 07/22/15
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1090.0545
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 970.0484
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1030.0515
LCS (P5G0385-BS1)Prepared: 07/21/15 Analyzed: 07/22/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0519 0.0050 0.05000 72-115104
1,1,1-Trichloroethane mg/kg wet0.0485 0.0050 0.05000 67-13197
1,1,2,2-Tetrachloroethane mg/kg wet0.0561 0.0050 0.05000 56-126112
1,1,2-Trichloroethane mg/kg wet0.0516 0.0050 0.05000 70-133103
1,1-Dichloroethane mg/kg wet0.0472 0.0050 0.05000 74-12794
1,1-Dichloroethylene mg/kg wet0.0515 0.0050 0.05000 67-149103
1,1-Dichloropropylene mg/kg wet0.0581 0.0050 0.05000 71-130116
1,2,3-Trichlorobenzene mg/kg wet0.0544 0.0050 0.05000 68-130109
1,2,3-Trichloropropane mg/kg wet0.0558 0.0050 0.05000 60-137112
1,2,4-Trichlorobenzene mg/kg wet0.0533 0.0050 0.05000 66-125107
1,2,4-Trimethylbenzene mg/kg wet0.0544 0.0050 0.05000 69-129109
1,2-Dibromoethane mg/kg wet0.0553 0.0050 0.05000 70-132111
1,2-Dichlorobenzene mg/kg wet0.0535 0.0050 0.05000 72-123107
1,2-Dichloroethane mg/kg wet0.0502 0.0050 0.05000 68-128100
1,2-Dichloropropane mg/kg wet0.0520 0.0050 0.05000 73-130104
1,3,5-Trimethylbenzene mg/kg wet0.0534 0.0050 0.05000 69-128107
1,3-Dichlorobenzene mg/kg wet0.0512 0.0050 0.05000 71-120102
1,3-Dichloropropane mg/kg wet0.0568 0.0050 0.05000 75-124114
1,4-Dichlorobenzene mg/kg wet0.0517 0.0050 0.05000 71-123103
2,2-Dichloropropane mg/kg wet0.0473 0.0050 0.05000 50-14295
2-Chlorotoluene mg/kg wet0.0500 0.0050 0.05000 67-124100
4-Chlorotoluene mg/kg wet0.0525 0.0050 0.05000 71-126105
4-Isopropyltoluene mg/kg wet0.0538 0.0050 0.05000 68-129108
Acetone mg/kg wet0.112 0.050 0.1000 29-198112
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 82 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0385 - 5035
LCS (P5G0385-BS1)Prepared: 07/21/15 Analyzed: 07/22/15
Benzene mg/kg wet0.0509 0.0030 0.05000 74-127102
Bromobenzene mg/kg wet0.0506 0.0050 0.05000 73-125101
Bromochloromethane mg/kg wet0.0546 0.0050 0.05000 72-134109
Bromodichloromethane mg/kg wet0.0472 0.0050 0.05000 75-12294
Bromoform mg/kg wet0.0525 0.0050 0.05000 66-135105
Bromomethane mg/kg wet0.0472 0.010 0.05000 20-18094
Carbon Tetrachloride mg/kg wet0.0540 0.0050 0.05000 64-143108
Chlorobenzene mg/kg wet0.0523 0.0050 0.05000 74-118105
Chloroethane mg/kg wet0.0453 0.010 0.05000 33-14991
Chloroform mg/kg wet0.0469 0.0050 0.05000 73-12794
Chloromethane mg/kg wet0.0454 0.0050 0.05000 45-14391
cis-1,2-Dichloroethylene mg/kg wet0.0486 0.0050 0.05000 76-13497
cis-1,3-Dichloropropylene mg/kg wet0.0518 0.0050 0.05000 71-125104
Dibromochloromethane mg/kg wet0.0515 0.0050 0.05000 73-122103
Dichlorodifluoromethane mg/kg wet0.0462 0.0050 0.05000 26-14692
Ethylbenzene mg/kg wet0.0527 0.0050 0.05000 74-128105
Isopropyl Ether mg/kg wet0.0473 0.0050 0.05000 59-15995
Isopropylbenzene (Cumene)mg/kg wet0.0582 0.0050 0.05000 68-126116
m,p-Xylenes mg/kg wet0.104 0.010 0.1000 75-124104
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0643 0.050 0.05000 61-157129
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0518 0.10 0.05000 J63-149104
Methyl Isobutyl Ketone mg/kg wet0.0579 0.050 0.05000 57-162116
Methylene Chloride mg/kg wet0.0478 0.0050 0.05000 74-12996
Methyl-tert-Butyl Ether mg/kg wet0.0523 0.010 0.05000 70-130105
Naphthalene mg/kg wet0.0588 0.010 0.05000 57-157118
n-Butylbenzene mg/kg wet0.0542 0.0050 0.05000 65-135108
n-Propylbenzene mg/kg wet0.0531 0.0050 0.05000 67-130106
o-Xylene mg/kg wet0.0522 0.0050 0.05000 74-126104
sec-Butylbenzene mg/kg wet0.0610 0.0050 0.05000 66-131122
Styrene mg/kg wet0.0540 0.0050 0.05000 77-121108
tert-Butylbenzene mg/kg wet0.0569 0.0050 0.05000 67-132114
Tetrachloroethylene mg/kg wet0.0528 0.0050 0.05000 68-130106
Toluene mg/kg wet0.0498 0.0050 0.05000 71-129100
trans-1,2-Dichloroethylene mg/kg wet0.0501 0.0050 0.05000 73-132100
trans-1,3-Dichloropropylene mg/kg wet0.0532 0.0050 0.05000 68-123106
Trichloroethylene mg/kg wet0.0526 0.0050 0.05000 75-133105
Trichlorofluoromethane mg/kg wet0.0552 0.0050 0.05000 44-146110
Vinyl acetate mg/kg wet0.0603 0.025 0.05000 85-161121
Vinyl chloride mg/kg wet0.0482 0.0050 0.05000 48-14796
Xylenes, total mg/kg wet0.156 0.015 0.1500 74-126104
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1030.0513
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 990.0493
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1000.0501
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 83 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0385 - 5035
LCS Dup (P5G0385-BSD1)Prepared: 07/21/15 Analyzed: 07/22/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0491 0.0050 0.05000 2072-11598 6
1,1,1-Trichloroethane mg/kg wet0.0452 0.0050 0.05000 2067-13190 7
1,1,2,2-Tetrachloroethane mg/kg wet0.0460 0.0050 0.05000 2056-12692 20
1,1,2-Trichloroethane mg/kg wet0.0467 0.0050 0.05000 2070-13393 10
1,1-Dichloroethane mg/kg wet0.0449 0.0050 0.05000 2074-12790 5
1,1-Dichloroethylene mg/kg wet0.0486 0.0050 0.05000 2067-14997 6
1,1-Dichloropropylene mg/kg wet0.0541 0.0050 0.05000 2071-130108 7
1,2,3-Trichlorobenzene mg/kg wet0.0496 0.0050 0.05000 2068-13099 9
1,2,3-Trichloropropane mg/kg wet0.0466 0.0050 0.05000 2060-13793 18
1,2,4-Trichlorobenzene mg/kg wet0.0489 0.0050 0.05000 2066-12598 9
1,2,4-Trimethylbenzene mg/kg wet0.0520 0.0050 0.05000 2069-129104 4
1,2-Dibromoethane mg/kg wet0.0493 0.0050 0.05000 2070-13299 12
1,2-Dichlorobenzene mg/kg wet0.0485 0.0050 0.05000 2072-12397 10
1,2-Dichloroethane mg/kg wet0.0462 0.0050 0.05000 2068-12892 8
1,2-Dichloropropane mg/kg wet0.0497 0.0050 0.05000 2073-13099 5
1,3,5-Trimethylbenzene mg/kg wet0.0511 0.0050 0.05000 2069-128102 4
1,3-Dichlorobenzene mg/kg wet0.0508 0.0050 0.05000 2071-120102 0.8
1,3-Dichloropropane mg/kg wet0.0502 0.0050 0.05000 2075-124100 12
1,4-Dichlorobenzene mg/kg wet0.0483 0.0050 0.05000 2071-12397 7
2,2-Dichloropropane mg/kg wet0.0455 0.0050 0.05000 2050-14291 4
2-Chlorotoluene mg/kg wet0.0486 0.0050 0.05000 2067-12497 3
4-Chlorotoluene mg/kg wet0.0482 0.0050 0.05000 2071-12696 8
4-Isopropyltoluene mg/kg wet0.0519 0.0050 0.05000 2068-129104 4
Acetone mg/kg wet0.0882 0.050 0.1000 20 D29-19888 24
Benzene mg/kg wet0.0495 0.0030 0.05000 2074-12799 3
Bromobenzene mg/kg wet0.0466 0.0050 0.05000 2073-12593 8
Bromochloromethane mg/kg wet0.0513 0.0050 0.05000 2072-134103 6
Bromodichloromethane mg/kg wet0.0450 0.0050 0.05000 2075-12290 5
Bromoform mg/kg wet0.0475 0.0050 0.05000 2066-13595 10
Bromomethane mg/kg wet0.0434 0.010 0.05000 2020-18087 8
Carbon Tetrachloride mg/kg wet0.0498 0.0050 0.05000 2064-143100 8
Chlorobenzene mg/kg wet0.0502 0.0050 0.05000 2074-118100 4
Chloroethane mg/kg wet0.0417 0.010 0.05000 2033-14983 8
Chloroform mg/kg wet0.0452 0.0050 0.05000 2073-12790 4
Chloromethane mg/kg wet0.0413 0.0050 0.05000 2045-14383 10
cis-1,2-Dichloroethylene mg/kg wet0.0471 0.0050 0.05000 2076-13494 3
cis-1,3-Dichloropropylene mg/kg wet0.0495 0.0050 0.05000 2071-12599 4
Dibromochloromethane mg/kg wet0.0467 0.0050 0.05000 2073-12293 10
Dichlorodifluoromethane mg/kg wet0.0432 0.0050 0.05000 2026-14686 7
Ethylbenzene mg/kg wet0.0504 0.0050 0.05000 2074-128101 5
Isopropyl Ether mg/kg wet0.0459 0.0050 0.05000 2059-15992 3
Isopropylbenzene (Cumene)mg/kg wet0.0570 0.0050 0.05000 2068-126114 2
m,p-Xylenes mg/kg wet0.0992 0.010 0.1000 2075-12499 4
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0498 0.050 0.05000 20 D, J61-157100 25
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0430 0.10 0.05000 20 J63-14986 19
Methyl Isobutyl Ketone mg/kg wet0.0452 0.050 0.05000 20 D, J57-16290 25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 84 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0385 - 5035
LCS Dup (P5G0385-BSD1)Prepared: 07/21/15 Analyzed: 07/22/15
Methylene Chloride mg/kg wet0.0450 0.0050 0.05000 2074-12990 6
Methyl-tert-Butyl Ether mg/kg wet0.0454 0.010 0.05000 2070-13091 14
Naphthalene mg/kg wet0.0511 0.010 0.05000 2057-157102 14
n-Butylbenzene mg/kg wet0.0505 0.0050 0.05000 2065-135101 7
n-Propylbenzene mg/kg wet0.0510 0.0050 0.05000 2067-130102 4
o-Xylene mg/kg wet0.0523 0.0050 0.05000 2074-126105 0.2
sec-Butylbenzene mg/kg wet0.0582 0.0050 0.05000 2066-131116 5
Styrene mg/kg wet0.0537 0.0050 0.05000 2077-121107 0.6
tert-Butylbenzene mg/kg wet0.0534 0.0050 0.05000 2067-132107 6
Tetrachloroethylene mg/kg wet0.0499 0.0050 0.05000 2068-130100 6
Toluene mg/kg wet0.0479 0.0050 0.05000 2071-12996 4
trans-1,2-Dichloroethylene mg/kg wet0.0481 0.0050 0.05000 2073-13296 4
trans-1,3-Dichloropropylene mg/kg wet0.0495 0.0050 0.05000 2068-12399 7
Trichloroethylene mg/kg wet0.0485 0.0050 0.05000 2075-13397 8
Trichlorofluoromethane mg/kg wet0.0507 0.0050 0.05000 2044-146101 9
Vinyl acetate mg/kg wet0.0541 0.025 0.05000 2085-161108 11
Vinyl chloride mg/kg wet0.0442 0.0050 0.05000 2048-14788 9
Xylenes, total mg/kg wet0.152 0.015 0.1500 2074-126101 3
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1000.0498
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 950.0476
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 970.0485
Batch P5G0463 - 3580A VMS
Blank (P5G0463-BLK1)Prepared & Analyzed: 07/24/15
1,1,1,2-Tetrachloroethane mg/kgBRL0.25
1,1,1-Trichloroethane mg/kgBRL0.25
1,1,2,2-Tetrachloroethane mg/kgBRL0.25
1,1,2-Trichloroethane mg/kgBRL0.25
1,1-Dichloroethane mg/kgBRL0.25
1,1-Dichloroethylene mg/kgBRL0.25
1,1-Dichloropropylene mg/kgBRL0.25
1,2,3-Trichlorobenzene mg/kgBRL0.50
1,2,3-Trichloropropane mg/kgBRL0.25
1,2,4-Trichlorobenzene mg/kgBRL0.50
1,2,4-Trimethylbenzene mg/kgBRL0.25
1,2-Dibromo-3-chloropropane mg/kgBRL0.50
1,2-Dibromoethane mg/kgBRL0.25
1,2-Dichlorobenzene mg/kgBRL0.25
1,2-Dichloroethane mg/kgBRL0.25
1,2-Dichloropropane mg/kgBRL0.25
1,3,5-Trimethylbenzene mg/kgBRL0.25
1,3-Dichlorobenzene mg/kgBRL0.25
1,3-Dichloropropane mg/kgBRL0.25
1,4-Dichlorobenzene mg/kgBRL0.25
2,2-Dichloropropane mg/kgBRL0.25
2-Chloroethyl Vinyl Ether mg/kgBRL0.25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 85 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0463 - 3580A VMS
Blank (P5G0463-BLK1)Prepared & Analyzed: 07/24/15
2-Chlorotoluene mg/kgBRL0.25
4-Chlorotoluene mg/kgBRL0.25
4-Isopropyltoluene mg/kgBRL0.25
Acetone mg/kgBRL1.0
Benzene mg/kgBRL0.25
Bromobenzene mg/kgBRL0.25
Bromochloromethane mg/kgBRL0.25
Bromodichloromethane mg/kgBRL0.25
Bromoform mg/kgBRL0.25
Bromomethane mg/kgBRL0.50
Carbon disulfide mg/kgBRL0.25
Carbon Tetrachloride mg/kgBRL0.25
Chlorobenzene mg/kgBRL0.25
Chloroethane mg/kgBRL0.50
Chloroform mg/kgBRL0.25
Chloromethane mg/kgBRL0.50
cis-1,2-Dichloroethylene mg/kgBRL0.25
cis-1,3-Dichloropropylene mg/kgBRL0.25
Dibromochloromethane mg/kgBRL0.25
Dibromomethane mg/kgBRL0.25
Dichlorodifluoromethane mg/kgBRL0.50
Ethylbenzene mg/kgBRL0.25
Hexachlorobutadiene mg/kgBRL0.50
Isopropyl Ether mg/kgBRL0.25
Isopropylbenzene (Cumene)mg/kgBRL0.25
m,p-Xylenes mg/kgBRL0.50
Methyl Butyl Ketone (2-Hexanone)mg/kgBRL1.0
Methyl Ethyl Ketone (2-Butanone)mg/kgBRL1.0
Methyl Isobutyl Ketone mg/kgBRL1.0
Methylene Chloride mg/kgBRL0.25
Methyl-tert-Butyl Ether mg/kgBRL0.25
Naphthalene mg/kgBRL0.50
n-Butylbenzene mg/kgBRL0.25
n-Propylbenzene mg/kgBRL0.25
o-Xylene mg/kgBRL0.25
sec-Butylbenzene mg/kgBRL0.25
Styrene mg/kgBRL0.25
tert-Butylbenzene mg/kgBRL0.25
Tetrachloroethylene mg/kgBRL0.25
Toluene mg/kgBRL0.25
trans-1,2-Dichloroethylene mg/kgBRL0.25
trans-1,3-Dichloropropylene mg/kgBRL0.25
Trichloroethylene mg/kgBRL0.25
Trichlorofluoromethane mg/kgBRL0.50
Vinyl chloride mg/kgBRL0.50
mg/kg 1.000 70-130Surrogate: 4-Bromofluorobenzene 960.956
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 86 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0463 - 3580A VMS
Blank (P5G0463-BLK1)Prepared & Analyzed: 07/24/15
mg/kg 1.000 70-130Surrogate: Dibromofluoromethane 970.970
mg/kg 1.000 70-130Surrogate: Toluene-d8 810.813
LCS (P5G0463-BS1)Prepared & Analyzed: 07/24/15
1,1,1,2-Tetrachloroethane mg/kg1.16 0.25 1.000 70-130116
1,1,1-Trichloroethane mg/kg1.15 0.25 1.000 70-130115
1,1,2,2-Tetrachloroethane mg/kg0.832 0.25 1.000 70-13083
1,1,2-Trichloroethane mg/kg0.953 0.25 1.000 70-13095
1,1-Dichloroethane mg/kg0.871 0.25 1.000 70-13087
1,1-Dichloroethylene mg/kg1.14 0.25 1.000 70-130114
1,1-Dichloropropylene mg/kg1.02 0.25 1.000 70-130102
1,2,3-Trichlorobenzene mg/kg1.07 0.50 1.000 70-130107
1,2,3-Trichloropropane mg/kg0.896 0.25 1.000 70-13090
1,2,4-Trichlorobenzene mg/kg1.03 0.50 1.000 70-130103
1,2,4-Trimethylbenzene mg/kg1.05 0.25 1.000 70-130105
1,2-Dibromo-3-chloropropane mg/kg1.06 0.50 1.000 70-130106
1,2-Dibromoethane mg/kg1.10 0.25 1.000 70-130110
1,2-Dichlorobenzene mg/kg1.09 0.25 1.000 70-130109
1,2-Dichloroethane mg/kg1.14 0.25 1.000 70-130114
1,2-Dichloropropane mg/kg0.855 0.25 1.000 70-13086
1,3,5-Trimethylbenzene mg/kg1.06 0.25 1.000 70-130106
1,3-Dichlorobenzene mg/kg1.08 0.25 1.000 70-130108
1,3-Dichloropropane mg/kg0.934 0.25 1.000 70-13093
1,4-Dichlorobenzene mg/kg1.10 0.25 1.000 70-130110
2,2-Dichloropropane mg/kg1.11 0.25 1.000 70-130111
2-Chloroethyl Vinyl Ether mg/kg0.792 0.25 1.000 70-13079
2-Chlorotoluene mg/kg1.03 0.25 1.000 70-130103
4-Chlorotoluene mg/kg1.03 0.25 1.000 70-130103
4-Isopropyltoluene mg/kg1.03 0.25 1.000 70-130103
Acetone mg/kg1.98 1.0 2.000 70-13099
Benzene mg/kg0.940 0.25 1.000 70-13094
Bromobenzene mg/kg1.04 0.25 1.000 70-130104
Bromochloromethane mg/kg1.07 0.25 1.000 70-130107
Bromodichloromethane mg/kg1.05 0.25 1.000 70-130105
Bromoform mg/kg1.07 0.25 1.000 70-130107
Bromomethane mg/kg1.16 0.50 1.000 70-130116
Carbon disulfide mg/kg0.740 0.25 1.000 70-13074
Carbon Tetrachloride mg/kg1.32 0.25 1.000 L170-130132
Chlorobenzene mg/kg1.05 0.25 1.000 70-130105
Chloroethane mg/kg0.955 0.50 1.000 70-13096
Chloroform mg/kg1.00 0.25 1.000 70-130100
Chloromethane mg/kg0.917 0.50 1.000 70-13092
cis-1,2-Dichloroethylene mg/kg0.978 0.25 1.000 70-13098
cis-1,3-Dichloropropylene mg/kg0.960 0.25 1.000 70-13096
Dibromochloromethane mg/kg1.07 0.25 1.000 70-130107
Dibromomethane mg/kg1.04 0.25 1.000 70-130104
Dichlorodifluoromethane mg/kg0.974 0.50 1.000 70-13097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 87 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0463 - 3580A VMS
LCS (P5G0463-BS1)Prepared & Analyzed: 07/24/15
Ethylbenzene mg/kg1.01 0.25 1.000 70-130101
Hexachlorobutadiene mg/kg1.15 0.50 1.000 70-130115
Isopropyl Ether mg/kg0.764 0.25 1.000 70-13076
Isopropylbenzene (Cumene)mg/kg1.04 0.25 1.000 70-130104
m,p-Xylenes mg/kg2.09 0.50 2.000 70-130104
Methyl Butyl Ketone (2-Hexanone)mg/kg0.794 1.0 1.000 J70-13079
Methyl Ethyl Ketone (2-Butanone)mg/kg0.744 1.0 1.000 J70-13074
Methyl Isobutyl Ketone mg/kg0.825 1.0 1.000 J70-13082
Methylene Chloride mg/kg0.944 0.25 1.000 70-13094
Methyl-tert-Butyl Ether mg/kg0.912 0.25 1.000 70-13091
Naphthalene mg/kg1.05 0.50 1.000 70-130105
n-Butylbenzene mg/kg0.968 0.25 1.000 70-13097
n-Propylbenzene mg/kg0.988 0.25 1.000 70-13099
o-Xylene mg/kg1.05 0.25 1.000 70-130105
sec-Butylbenzene mg/kg0.962 0.25 1.000 70-13096
Styrene mg/kg1.06 0.25 1.000 70-130106
tert-Butylbenzene mg/kg1.07 0.25 1.000 70-130107
Tetrachloroethylene mg/kg1.12 0.25 1.000 70-130112
Toluene mg/kg0.974 0.25 1.000 70-13097
trans-1,2-Dichloroethylene mg/kg0.991 0.25 1.000 70-13099
trans-1,3-Dichloropropylene mg/kg1.03 0.25 1.000 70-130103
Trichloroethylene mg/kg1.15 0.25 1.000 70-130115
Trichlorofluoromethane mg/kg1.19 0.50 1.000 70-130119
Vinyl chloride mg/kg0.958 0.50 1.000 70-13096
mg/kg 1.000 70-130Surrogate: 4-Bromofluorobenzene 990.993
mg/kg 1.000 70-130Surrogate: Dibromofluoromethane 1031.03
mg/kg 1.000 70-130Surrogate: Toluene-d8 930.926
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 88 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0463 - 3580A VMS
LCS Dup (P5G0463-BSD1)Prepared & Analyzed: 07/24/15
1,1,1,2-Tetrachloroethane mg/kg1.04 0.25 1.000 2070-130104 11
1,1,1-Trichloroethane mg/kg1.03 0.25 1.000 2070-130103 11
1,1,2,2-Tetrachloroethane mg/kg0.794 0.25 1.000 2070-13079 5
1,1,2-Trichloroethane mg/kg0.878 0.25 1.000 2070-13088 8
1,1-Dichloroethane mg/kg0.799 0.25 1.000 2070-13080 9
1,1-Dichloroethylene mg/kg1.03 0.25 1.000 2070-130103 10
1,1-Dichloropropylene mg/kg0.908 0.25 1.000 2070-13091 12
1,2,3-Trichlorobenzene mg/kg0.947 0.50 1.000 2070-13095 12
1,2,3-Trichloropropane mg/kg0.928 0.25 1.000 2070-13093 4
1,2,4-Trichlorobenzene mg/kg0.959 0.50 1.000 2070-13096 7
1,2,4-Trimethylbenzene mg/kg0.966 0.25 1.000 2070-13097 9
1,2-Dibromo-3-chloropropane mg/kg0.962 0.50 1.000 2070-13096 9
1,2-Dibromoethane mg/kg0.915 0.25 1.000 2070-13092 18
1,2-Dichlorobenzene mg/kg1.01 0.25 1.000 2070-130101 8
1,2-Dichloroethane mg/kg1.08 0.25 1.000 2070-130108 6
1,2-Dichloropropane mg/kg0.768 0.25 1.000 2070-13077 11
1,3,5-Trimethylbenzene mg/kg0.971 0.25 1.000 2070-13097 9
1,3-Dichlorobenzene mg/kg1.01 0.25 1.000 2070-130101 7
1,3-Dichloropropane mg/kg0.850 0.25 1.000 2070-13085 9
1,4-Dichlorobenzene mg/kg1.01 0.25 1.000 2070-130101 8
2,2-Dichloropropane mg/kg1.03 0.25 1.000 2070-130103 8
2-Chloroethyl Vinyl Ether mg/kg0.796 0.25 1.000 2070-13080 0.4
2-Chlorotoluene mg/kg0.953 0.25 1.000 2070-13095 7
4-Chlorotoluene mg/kg0.954 0.25 1.000 2070-13095 8
4-Isopropyltoluene mg/kg0.942 0.25 1.000 2070-13094 9
Acetone mg/kg1.82 1.0 2.000 2070-13091 8
Benzene mg/kg0.830 0.25 1.000 2070-13083 12
Bromobenzene mg/kg0.939 0.25 1.000 2070-13094 10
Bromochloromethane mg/kg1.01 0.25 1.000 2070-130101 5
Bromodichloromethane mg/kg0.944 0.25 1.000 2070-13094 11
Bromoform mg/kg0.964 0.25 1.000 2070-13096 11
Bromomethane mg/kg1.13 0.50 1.000 2070-130113 3
Carbon disulfide mg/kg0.686 0.25 1.000 20 L270-13069 8
Carbon Tetrachloride mg/kg1.14 0.25 1.000 2070-130114 14
Chlorobenzene mg/kg0.904 0.25 1.000 2070-13090 15
Chloroethane mg/kg0.846 0.50 1.000 2070-13085 12
Chloroform mg/kg0.942 0.25 1.000 2070-13094 6
Chloromethane mg/kg0.836 0.50 1.000 2070-13084 9
cis-1,2-Dichloroethylene mg/kg0.917 0.25 1.000 2070-13092 6
cis-1,3-Dichloropropylene mg/kg0.863 0.25 1.000 2070-13086 11
Dibromochloromethane mg/kg0.924 0.25 1.000 2070-13092 14
Dibromomethane mg/kg0.942 0.25 1.000 2070-13094 10
Dichlorodifluoromethane mg/kg0.858 0.50 1.000 2070-13086 13
Ethylbenzene mg/kg0.882 0.25 1.000 2070-13088 13
Hexachlorobutadiene mg/kg1.08 0.50 1.000 2070-130108 6
Isopropyl Ether mg/kg0.684 0.25 1.000 20 L270-13068 11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 89 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5G0463 - 3580A VMS
LCS Dup (P5G0463-BSD1)Prepared & Analyzed: 07/24/15
Isopropylbenzene (Cumene)mg/kg0.959 0.25 1.000 2070-13096 8
m,p-Xylenes mg/kg1.81 0.50 2.000 2070-13090 15
Methyl Butyl Ketone (2-Hexanone)mg/kg0.725 1.0 1.000 20 J70-13072 9
Methyl Ethyl Ketone (2-Butanone)mg/kg0.677 1.0 1.000 20 L2, J70-13068 9
Methyl Isobutyl Ketone mg/kg0.700 1.0 1.000 20 J70-13070 16
Methylene Chloride mg/kg0.848 0.25 1.000 2070-13085 11
Methyl-tert-Butyl Ether mg/kg0.867 0.25 1.000 2070-13087 5
Naphthalene mg/kg0.980 0.50 1.000 2070-13098 6
n-Butylbenzene mg/kg0.882 0.25 1.000 2070-13088 9
n-Propylbenzene mg/kg0.911 0.25 1.000 2070-13091 8
o-Xylene mg/kg0.910 0.25 1.000 2070-13091 15
sec-Butylbenzene mg/kg0.868 0.25 1.000 2070-13087 10
Styrene mg/kg0.918 0.25 1.000 2070-13092 15
tert-Butylbenzene mg/kg0.964 0.25 1.000 2070-13096 10
Tetrachloroethylene mg/kg0.977 0.25 1.000 2070-13098 14
Toluene mg/kg0.876 0.25 1.000 2070-13088 11
trans-1,2-Dichloroethylene mg/kg0.898 0.25 1.000 2070-13090 10
trans-1,3-Dichloropropylene mg/kg0.978 0.25 1.000 2070-13098 5
Trichloroethylene mg/kg1.00 0.25 1.000 2070-130100 14
Trichlorofluoromethane mg/kg1.07 0.50 1.000 2070-130107 10
Vinyl chloride mg/kg0.850 0.50 1.000 2070-13085 12
mg/kg 1.000 70-130Surrogate: 4-Bromofluorobenzene 950.954
mg/kg 1.000 70-130Surrogate: Dibromofluoromethane 990.986
mg/kg 1.000 70-130Surrogate: Toluene-d8 830.830
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 90 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P5G0389 - 5035
Blank (P5G0389-BLK1)Prepared & Analyzed: 07/21/15
Naphthalene mg/kg wetBRL0.50
Toluene mg/kg wetBRL0.25
mg/kg wet 1.000 70-130Surrogate: 4-Bromofluorobenzene 990.990
mg/kg wet 1.000 70-130Surrogate: Dibromofluoromethane 960.965
mg/kg wet 1.000 70-130Surrogate: Toluene-d8 840.838
LCS (P5G0389-BS1)Prepared & Analyzed: 07/21/15
Naphthalene mg/kg wet1.02 0.50 1.000 58-129102
Toluene mg/kg wet0.942 0.25 1.000 74-12294
mg/kg wet 1.000 70-130Surrogate: 4-Bromofluorobenzene 1001.00
mg/kg wet 1.000 70-130Surrogate: Dibromofluoromethane 1081.08
mg/kg wet 1.000 70-130Surrogate: Toluene-d8 880.882
LCS Dup (P5G0389-BSD1)Prepared & Analyzed: 07/21/15
Naphthalene mg/kg wet1.05 0.50 1.000 2058-129105 3
Toluene mg/kg wet0.901 0.25 1.000 2074-12290 4
mg/kg wet 1.000 70-130Surrogate: 4-Bromofluorobenzene 940.944
mg/kg wet 1.000 70-130Surrogate: Dibromofluoromethane 970.973
mg/kg wet 1.000 70-130Surrogate: Toluene-d8 860.860
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 91 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5G0329 - 3546
Blank (P5G0329-BLK1)Prepared: 07/20/15 Analyzed: 08/03/15
1-Methylnaphthalene mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 1.664 44-115Surrogate: 2-Fluorobiphenyl 711.18
mg/kg wet 1.664 37-122Surrogate: Nitrobenzene-d5 691.14
mg/kg wet 1.664 54-127Surrogate: Terphenyl-d14 781.30
LCS (P5G0329-BS1)Prepared: 07/20/15 Analyzed: 08/03/15
1-Methylnaphthalene mg/kg wet1.07 0.33 1.667 40-11964
2-Methylnaphthalene mg/kg wet1.08 0.33 1.667 38-12265
Acenaphthene mg/kg wet1.14 0.33 1.667 40-12368
Acenaphthylene mg/kg wet1.15 0.33 1.667 32-13269
Anthracene mg/kg wet1.24 0.33 1.667 47-12374
Benzo(a)anthracene mg/kg wet1.22 0.33 1.667 49-12673
Benzo(a)pyrene mg/kg wet1.43 0.33 1.667 45-12986
Benzo(b)fluoranthene mg/kg wet1.38 0.33 1.667 45-13283
Benzo(g,h,i)perylene mg/kg wet1.34 0.33 1.667 43-13480
Benzo(k)fluoranthene mg/kg wet1.38 0.33 1.667 47-13283
Chrysene mg/kg wet1.23 0.33 1.667 50-12474
Dibenzo(a,h)anthracene mg/kg wet1.34 0.33 1.667 45-13480
Fluoranthene mg/kg wet1.23 0.33 1.667 50-12774
Fluorene mg/kg wet1.20 0.33 1.667 43-12572
Indeno(1,2,3-cd)pyrene mg/kg wet1.73 0.33 1.667 45-133104
Naphthalene mg/kg wet1.07 0.33 1.667 35-12364
Phenanthrene mg/kg wet1.26 0.33 1.667 50-12175
Pyrene mg/kg wet1.25 0.33 1.667 47-12775
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 681.13
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 631.06
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 741.23
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 92 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5G0329 - 3546
LCS Dup (P5G0329-BSD1)Prepared: 07/20/15 Analyzed: 08/03/15
1-Methylnaphthalene mg/kg wet1.02 0.33 1.667 2040-11961 5
2-Methylnaphthalene mg/kg wet1.01 0.33 1.667 2038-12261 7
Acenaphthene mg/kg wet1.08 0.33 1.667 2040-12365 5
Acenaphthylene mg/kg wet1.09 0.33 1.667 2032-13266 5
Anthracene mg/kg wet1.23 0.33 1.667 2047-12374 0.9
Benzo(a)anthracene mg/kg wet1.25 0.33 1.667 2049-12675 3
Benzo(a)pyrene mg/kg wet1.47 0.33 1.667 2045-12988 3
Benzo(b)fluoranthene mg/kg wet1.40 0.33 1.667 2045-13284 2
Benzo(g,h,i)perylene mg/kg wet1.40 0.33 1.667 2043-13484 5
Benzo(k)fluoranthene mg/kg wet1.42 0.33 1.667 2047-13285 3
Chrysene mg/kg wet1.25 0.33 1.667 2050-12475 1
Dibenzo(a,h)anthracene mg/kg wet1.40 0.33 1.667 2045-13484 4
Fluoranthene mg/kg wet1.24 0.33 1.667 2050-12774 0.2
Fluorene mg/kg wet1.17 0.33 1.667 2043-12570 2
Indeno(1,2,3-cd)pyrene mg/kg wet1.79 0.33 1.667 2045-133107 3
Naphthalene mg/kg wet0.960 0.33 1.667 2035-12358 11
Phenanthrene mg/kg wet1.24 0.33 1.667 2050-12174 2
Pyrene mg/kg wet1.25 0.33 1.667 2047-12775 0.6
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 641.06
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 560.939
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 731.22
Matrix Spike (P5G0329-MS1)Prepared: 07/20/15 Analyzed: 08/03/15 Source: 5070245-17
1-Methylnaphthalene mg/kg dry1.87 0.34 1.704 BRL 40-119110
2-Methylnaphthalene mg/kg dry1.89 0.34 1.704 BRL 38-122111
Acenaphthene mg/kg dry1.87 0.34 1.704 BRL 40-123110
Acenaphthylene mg/kg dry1.87 0.34 1.704 BRL 32-132109
Anthracene mg/kg dry2.02 0.34 1.704 BRL 47-123119
Benzo(a)anthracene mg/kg dry1.73 0.34 1.704 BRL 49-126101
Benzo(a)pyrene mg/kg dry1.71 0.34 1.704 BRL 45-129101
Benzo(b)fluoranthene mg/kg dry1.67 0.34 1.704 BRL 45-13298
Benzo(g,h,i)perylene mg/kg dry1.63 0.34 1.704 BRL 43-13496
Benzo(k)fluoranthene mg/kg dry1.62 0.34 1.704 BRL 47-13295
Chrysene mg/kg dry1.76 0.34 1.704 BRL 50-124103
Dibenzo(a,h)anthracene mg/kg dry1.59 0.34 1.704 BRL 45-13493
Fluoranthene mg/kg dry2.08 0.34 1.704 BRL 50-127122
Fluorene mg/kg dry1.94 0.34 1.704 BRL 43-125114
Indeno(1,2,3-cd)pyrene mg/kg dry1.83 0.34 1.704 BRL 45-133107
Naphthalene mg/kg dry1.86 0.34 1.704 BRL 35-123109
Phenanthrene mg/kg dry2.47 0.34 1.704 BRL M50-121145
Pyrene mg/kg dry1.90 0.34 1.704 BRL 47-127111
mg/kg dry 1.704 44-115Surrogate: 2-Fluorobiphenyl 1101.87
mg/kg dry 1.704 37-122Surrogate: Nitrobenzene-d5 1081.84
mg/kg dry 1.704 54-127Surrogate: Terphenyl-d14 1021.75
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 93 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5G0329 - 3546
Matrix Spike Dup (P5G0329-MSD1)Prepared: 07/20/15 Analyzed: 08/03/15 Source: 5070245-17
1-Methylnaphthalene mg/kg dry1.63 0.34 1.704 BRL 2040-11996 14
2-Methylnaphthalene mg/kg dry1.73 0.34 1.704 BRL 2038-122101 9
Acenaphthene mg/kg dry1.60 0.34 1.704 BRL 2040-12394 16
Acenaphthylene mg/kg dry1.60 0.34 1.704 BRL 2032-13294 15
Anthracene mg/kg dry1.72 0.34 1.704 BRL 2047-123101 16
Benzo(a)anthracene mg/kg dry1.47 0.34 1.704 BRL 2049-12686 16
Benzo(a)pyrene mg/kg dry1.45 0.34 1.704 BRL 2045-12985 16
Benzo(b)fluoranthene mg/kg dry1.42 0.34 1.704 BRL 2045-13283 17
Benzo(g,h,i)perylene mg/kg dry1.37 0.34 1.704 BRL 2043-13481 17
Benzo(k)fluoranthene mg/kg dry1.34 0.34 1.704 BRL 2047-13279 18
Chrysene mg/kg dry1.50 0.34 1.704 BRL 2050-12488 16
Dibenzo(a,h)anthracene mg/kg dry1.34 0.34 1.704 BRL 2045-13478 17
Fluoranthene mg/kg dry1.75 0.34 1.704 BRL 2050-127102 18
Fluorene mg/kg dry1.62 0.34 1.704 BRL 2043-12595 18
Indeno(1,2,3-cd)pyrene mg/kg dry1.55 0.34 1.704 BRL 2045-13391 17
Naphthalene mg/kg dry1.61 0.34 1.704 BRL 2035-12395 14
Phenanthrene mg/kg dry2.07 0.34 1.704 BRL 2050-121121 18
Pyrene mg/kg dry1.62 0.34 1.704 BRL 2047-12795 16
mg/kg dry 1.704 44-115Surrogate: 2-Fluorobiphenyl 951.62
mg/kg dry 1.704 37-122Surrogate: Nitrobenzene-d5 941.61
mg/kg dry 1.704 54-127Surrogate: Terphenyl-d14 901.53
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 94 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P5G0284 - 3546
Blank (P5G0284-BLK1)Prepared: 07/16/15 Analyzed: 07/28/15
Aroclor 1016 mg/kg wetBRL0.050
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.050
Aroclor 1248 mg/kg wetBRL0.050
Aroclor 1254 mg/kg wetBRL0.050
Aroclor 1260 mg/kg wetBRL0.050
mg/kg wet 0.03333 36-182Surrogate: Tetrachloro-m-xylene 920.0308
mg/kg wet 0.03333 34-182Surrogate: Decachlorobiphenyl 990.0329
LCS (P5G0284-BS1)Prepared: 07/16/15 Analyzed: 07/28/15
Aroclor 1016 mg/kg wet0.342 0.050 0.3333 64-151103
Aroclor 1260 mg/kg wet0.304 0.050 0.3333 45-16691
mg/kg wet 0.03333 36-182Surrogate: Tetrachloro-m-xylene 950.0318
mg/kg wet 0.03333 34-182Surrogate: Decachlorobiphenyl 1050.0349
LCS Dup (P5G0284-BSD1)Prepared: 07/16/15 Analyzed: 07/28/15
Aroclor 1016 mg/kg wet0.334 0.050 0.3333 5064-151100 2
Aroclor 1260 mg/kg wet0.291 0.050 0.3333 5045-16687 5
mg/kg wet 0.03333 36-182Surrogate: Tetrachloro-m-xylene 930.0310
mg/kg wet 0.03333 34-182Surrogate: Decachlorobiphenyl 920.0308
Batch P5G0316 - 3580A
Blank (P5G0316-BLK1)Prepared: 07/20/15 Analyzed: 07/30/15
Aroclor 1016 mg/kgBRL1.0
Aroclor 1221 mg/kgBRL5.0
Aroclor 1232 mg/kgBRL1.0
Aroclor 1242 mg/kgBRL1.0
Aroclor 1248 mg/kgBRL1.0
Aroclor 1254 mg/kgBRL1.0
Aroclor 1260 mg/kgBRL1.0
mg/kg 2.000 72-147Surrogate: Tetrachloro-m-xylene 1082.16
mg/kg 2.000 65-160Surrogate: Decachlorobiphenyl 1032.05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 95 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P5H0043 - 3546
Blank (P5H0043-BLK1)Prepared & Analyzed: 08/04/15
Aroclor 1016 mg/kg wetBRL0.050
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.050
Aroclor 1248 mg/kg wetBRL0.050
Aroclor 1254 mg/kg wetBRL0.050
Aroclor 1260 mg/kg wetBRL0.050
mg/kg wet 0.03333 36-182Surrogate: Tetrachloro-m-xylene 690.0231
mg/kg wet 0.03333 34-182Surrogate: Decachlorobiphenyl 750.0251
LCS (P5H0043-BS1)Prepared & Analyzed: 08/04/15
Aroclor 1016 mg/kg wet0.325 0.050 0.3328 64-15198
Aroclor 1260 mg/kg wet0.325 0.050 0.3328 45-16698
mg/kg wet 0.03328 36-182Surrogate: Tetrachloro-m-xylene 730.0242
mg/kg wet 0.03328 34-182Surrogate: Decachlorobiphenyl 850.0284
LCS Dup (P5H0043-BSD1)Prepared & Analyzed: 08/04/15
Aroclor 1016 mg/kg wet0.333 0.050 0.3330 5064-151100 2
Aroclor 1260 mg/kg wet0.321 0.050 0.3330 5045-16696 1
mg/kg wet 0.03330 36-182Surrogate: Tetrachloro-m-xylene 780.0259
mg/kg wet 0.03330 34-182Surrogate: Decachlorobiphenyl 930.0310
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 96 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5G0270 - 7471B
Blank (P5G0270-BLK1)Prepared & Analyzed: 07/16/15
Mercury mg/kg wetBRL0.020
LCS (P5G0270-BS1)Prepared & Analyzed: 07/16/15
Mercury mg/kg wet0.452 0.020 0.4167 80-120109
Matrix Spike (P5G0270-MS1)Prepared & Analyzed: 07/16/15 Source: 5070245-01
Mercury mg/kg dry0.473 0.020 0.4245 BRL 80-120111
Matrix Spike Dup (P5G0270-MSD1)Prepared & Analyzed: 07/16/15 Source: 5070245-01
Mercury mg/kg dry0.485 0.020 0.4245 BRL 2080-120114 2
Batch P5G0271 - 7471B
Blank (P5G0271-BLK1)Prepared & Analyzed: 07/16/15
Mercury mg/kg wetBRL0.020
LCS (P5G0271-BS1)Prepared & Analyzed: 07/16/15
Mercury mg/kg wet0.464 0.020 0.4167 80-120111
Matrix Spike (P5G0271-MS1)Prepared & Analyzed: 07/16/15 Source: 5070245-19
Mercury mg/kg wet0.396 0.019 0.3906 BRL 80-120101
Matrix Spike Dup (P5G0271-MSD1)Prepared & Analyzed: 07/16/15 Source: 5070245-19
Mercury mg/kg wet0.448 0.021 0.4310 BRL 2080-120104 12
Batch P5G0294 - 3050B
Blank (P5G0294-BLK1)Prepared & Analyzed: 07/17/15
Arsenic mg/kg wetBRL0.25
Barium mg/kg wetBRL0.50
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wetBRL0.25
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL0.50
Silver mg/kg wetBRL0.25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 97 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5G0294 - 3050B
LCS (P5G0294-BS1)Prepared & Analyzed: 07/17/15
Arsenic mg/kg wet25.3 0.25 25.00 80-120101
Barium mg/kg wet26.5 0.50 25.00 80-120106
Cadmium mg/kg wet26.8 0.25 25.00 80-120107
Chromium mg/kg wet26.5 0.25 25.00 80-120106
Lead mg/kg wet26.0 0.25 25.00 80-120104
Selenium mg/kg wet24.9 0.50 25.00 80-120100
Silver mg/kg wet10.2 0.25 10.00 80-120102
Matrix Spike (P5G0294-MS1)Prepared & Analyzed: 07/17/15 Source: 5070245-01
Arsenic mg/kg dry29.2 0.26 25.86 4.22 75-12597
Barium mg/kg dry61.4 0.52 25.86 32.3 75-125113
Cadmium mg/kg dry20.9 0.26 25.86 BRL 75-12581
Chromium mg/kg dry36.9 0.26 25.86 14.3 75-12587
Lead mg/kg dry34.8 0.26 25.86 10.6 75-12594
Selenium mg/kg dry11.9 0.52 25.86 BRL 75-12546
Silver mg/kg dry9.44 0.26 10.34 BRL 75-12591
Matrix Spike Dup (P5G0294-MSD1)Prepared & Analyzed: 07/17/15 Source: 5070245-01
Arsenic mg/kg dry29.2 0.26 25.60 4.22 2075-12598 0.2
Barium mg/kg dry61.5 0.51 25.60 32.3 2075-125114 0.2
Cadmium mg/kg dry20.8 0.26 25.60 BRL 2075-12581 0.3
Chromium mg/kg dry36.7 0.26 25.60 14.3 2075-12588 0.4
Lead mg/kg dry33.2 0.26 25.60 10.6 2075-12589 5
Selenium mg/kg dry11.8 0.51 25.60 BRL 2075-12546 0.2
Silver mg/kg dry9.73 0.26 10.24 BRL 2075-12595 3
Post Spike (P5G0294-PS1)Prepared: 07/17/15 Analyzed: 07/18/15 Source: 5070245-01
Arsenic mg/L1.29 1.000 0.166 80-120112
Barium mg/L2.57 1.000 1.27 80-120130
Cadmium mg/L0.848 1.000 -0.00183 80-12085
Chromium mg/L1.59 1.000 0.560 80-120103
Lead mg/L1.39 1.000 0.415 80-12097
Selenium mg/L0.479 1.000 -0.426 80-12048
Silver mg/L0.443 0.4000 -0.0378 80-120111
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 98 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5G0295 - 3050B
Blank (P5G0295-BLK1)Prepared & Analyzed: 07/17/15
Arsenic mg/kg wetBRL0.25
Barium mg/kg wetBRL0.50
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wetBRL0.25
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL0.50
Silver mg/kg wetBRL0.25
LCS (P5G0295-BS1)Prepared & Analyzed: 07/17/15
Arsenic mg/kg wet25.8 0.25 25.00 80-120103
Barium mg/kg wet27.1 0.50 25.00 80-120109
Cadmium mg/kg wet27.3 0.25 25.00 80-120109
Chromium mg/kg wet27.1 0.25 25.00 80-120108
Lead mg/kg wet26.5 0.25 25.00 80-120106
Selenium mg/kg wet25.4 0.50 25.00 80-120102
Silver mg/kg wet10.4 0.25 10.00 80-120104
Matrix Spike (P5G0295-MS1)Prepared & Analyzed: 07/17/15 Source: 5070245-19
Arsenic mg/kg wet26.7 0.26 25.51 BRL 75-125105
Barium mg/kg wet30.0 0.51 25.51 1.49 75-125112
Cadmium mg/kg wet28.8 0.26 25.51 0.0411 75-125113
Chromium mg/kg wet28.7 0.26 25.51 0.140 75-125112
Lead mg/kg wet33.9 0.26 25.51 5.97 75-125110
Selenium mg/kg wet27.2 0.51 25.51 0.305 75-125105
Silver mg/kg wet11.0 0.26 10.20 BRL 75-125108
Matrix Spike Dup (P5G0295-MSD1)Prepared & Analyzed: 07/17/15 Source: 5070245-19
Arsenic mg/kg wet25.5 0.25 25.13 BRL 2075-125101 5
Barium mg/kg wet28.5 0.50 25.13 1.49 2075-125108 5
Cadmium mg/kg wet27.4 0.25 25.13 0.0411 2075-125109 5
Chromium mg/kg wet27.3 0.25 25.13 0.140 2075-125108 5
Lead mg/kg wet33.1 0.25 25.13 5.97 2075-125108 2
Selenium mg/kg wet26.0 0.50 25.13 0.305 2075-125102 4
Silver mg/kg wet10.5 0.25 10.05 BRL 2075-125104 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 99 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5G0295 - 3050B
Post Spike (P5G0295-PS1)Prepared & Analyzed: 07/17/15 Source: 5070245-19
Arsenic mg/L0.912 1.000 -0.00971 80-12091
Barium mg/L1.02 1.000 0.0595 80-12096
Cadmium mg/L0.974 1.000 0.00164 80-12097
Chromium mg/L0.971 1.000 0.00561 80-12097
Lead mg/L1.19 1.000 0.239 80-12095
Selenium mg/L0.942 1.000 0.0122 80-12093
Silver mg/L0.374 0.4000 0.000934 80-12093
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 100 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5G0242 - 9071B
Blank (P5G0242-BLK1)Prepared & Analyzed: 07/14/15
Oil & Grease (HEM)mg/kg wetBRL40
LCS (P5G0242-BS1)Prepared & Analyzed: 07/14/15
Oil & Grease (HEM)mg/kg wet2000 40 2000 80-120100
LCS Dup (P5G0242-BSD1)Prepared & Analyzed: 07/14/15
Oil & Grease (HEM)mg/kg wet2100 40 2000 2080-120105 5
Batch P5G0253 - Solids, Dry Weight
Blank (P5G0253-BLK1)Prepared & Analyzed: 07/15/15
% Solids % by Weight1000.100
Duplicate (P5G0253-DUP1)Prepared & Analyzed: 07/15/15 Source: 5070245-06
% Solids % by Weight96.0 0.100 97.8 202
Duplicate (P5G0253-DUP2)Prepared & Analyzed: 07/15/15 Source: 5070245-07
% Solids % by Weight96.9 0.100 97.0 200.1
Duplicate (P5G0253-DUP3)Prepared & Analyzed: 07/15/15 Source: 5070245-13
% Solids % by Weight97.3 0.100 97.3 200.01
Batch P5G0310 - NO PREP
LCS (P5G0310-BS1)Prepared & Analyzed: 07/17/15
Corrosivity-pH pH Units6.80 6.880 99-10199
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 101 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5G0310 - NO PREP
Duplicate (P5G0310-DUP1)Prepared & Analyzed: 07/17/15 Source: 5070245-13
Corrosivity-pH pH Units6.96 6.95 100.1
Batch P5G0315 - NO PREP
LCS (P5G0315-BS1)Prepared & Analyzed: 07/17/15
pH pH Units6.80 6.880 99-10199
Batch P5G0337 - 9071B
Blank (P5G0337-BLK1)Prepared & Analyzed: 07/16/15
Oil & Grease (HEM)mg/kg wetBRL40
LCS (P5G0337-BS1)Prepared & Analyzed: 07/16/15
Oil & Grease (HEM)mg/kg wet1820 40 2000 80-12091
LCS Dup (P5G0337-BSD1)Prepared & Analyzed: 07/16/15
Oil & Grease (HEM)mg/kg wet1840 40 2000 2080-12092 1
Matrix Spike (P5G0337-MS1)Prepared & Analyzed: 07/16/15 Source: 5070245-05
Oil & Grease (HEM)mg/kg dry2170041 2058 20700 M80-12048
Matrix Spike Dup (P5G0337-MSD1)Prepared & Analyzed: 07/16/15 Source: 5070245-05
Oil & Grease (HEM)mg/kg dry2240041 2058 20700 2080-12081 3
Batch P5G0358 - NO PREP
LCS (P5G0358-BS1)Prepared & Analyzed: 07/20/15
Corrosivity-pH pH Units6.81 6.880 99-10199
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 102 of 135
8/6/15
Level II QC Report
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5070245
Time Submitted: 7/14/2015 11:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5G0358 - NO PREP
Duplicate (P5G0358-DUP1)Prepared & Analyzed: 07/20/15 Source: 5070245-07
Corrosivity-pH pH Units12.2 12.2 100.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 103 of 135
Sample Extraction Data
Prep Method: 9071B
Lab Number Batch Date/TimeInitialFinal
P5G02425070245-01 07/15/15 10:2020 20g g
P5G02425070245-02 07/15/15 10:2020 20g g
P5G02425070245-03 07/15/15 10:2020 20g g
P5G02425070245-04 07/15/15 10:2020 20g g
P5G03375070245-05 07/16/15 11:2020 20g g
P5G03375070245-06 07/16/15 11:2020 20g g
P5G03375070245-07 07/16/15 11:2020 20g g
P5G03375070245-08 07/16/15 11:2020 20g g
P5G03375070245-09 07/16/15 11:2020 20g g
P5G03375070245-10 07/17/15 11:3020 20g g
P5G03375070245-11 07/17/15 11:3020 20g g
P5G03375070245-12 07/17/15 11:3020 20g g
P5G03375070245-13 07/17/15 11:3020 20g g
P5G03375070245-14 07/17/15 11:3020 20g g
P5G03375070245-15 07/17/15 11:3020 20g g
P5G03375070245-16 07/17/15 11:3020.03 20g g
P5G03375070245-17 07/17/15 11:3020 20g g
P5G03375070245-18 07/17/15 11:3020 20g g
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P5G02535070245-01 07/15/15 15:3130 30g g
P5G02535070245-02 07/15/15 15:3130 30g g
P5G02535070245-03 07/15/15 15:3130 30g g
P5G02535070245-04 07/15/15 15:3130 30g g
P5G02535070245-05 07/15/15 15:3130 30g g
P5G02535070245-06 07/15/15 15:3130 30g g
P5G02535070245-07 07/15/15 15:3130 30g g
P5G02535070245-08 07/15/15 15:3130 30g g
P5G02535070245-09 07/15/15 15:3130 30g g
P5G02535070245-10 07/15/15 15:3130 30g g
P5G02535070245-11 07/15/15 15:3130 30g g
P5G02535070245-12 07/15/15 15:3130 30g g
P5G02535070245-13 07/15/15 15:3130 30g g
P5G02535070245-14 07/15/15 15:3130 30g g
P5G02535070245-15 07/15/15 15:3130 30g g
P5G02535070245-16 07/15/15 15:3130 30g g
P5G02535070245-17 07/15/15 15:3130 30g g
P5G02535070245-18 07/15/15 15:3130 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5G02845070245-01 07/16/15 14:4530 10g mL
P5G02845070245-02 07/16/15 14:4530 10g mL
P5G02845070245-03 07/16/15 14:4530 10g mL
P5H00435070245-04 08/04/15 13:4530.02 10g mL
P5G02845070245-05 07/16/15 14:4530 10g mL
P5G02845070245-06 07/16/15 14:4530 10g mL
P5G02845070245-07 07/16/15 14:4530 10g mL
P5G02845070245-08 07/16/15 14:4530 10g mL
P5G02845070245-09 07/16/15 14:4530 10g mL
P5G02845070245-10 07/16/15 14:4530 10g mL
P5G02845070245-11 07/16/15 14:4530 25g mL
P5G02845070245-12 07/16/15 14:4515.02 25g mL
P5G02845070245-13 07/16/15 14:4530.04 25g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 104 of 135
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5G02845070245-14 07/16/15 14:4530.01 25g mL
P5G02845070245-15 07/16/15 14:4530.04 10g mL
P5G02845070245-16 07/16/15 14:4515.12 10g mL
P5G02845070245-17 07/16/15 14:4530 10g mL
P5G02845070245-18 07/16/15 14:4530.01 10g mL
Prep Method: 3580A
Lab Number Batch Date/TimeInitialFinal
P5G03165070245-19 07/20/15 16:000.5 10g mL
P5G03165070245-20 07/20/15 16:000.5 10g mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5G03295070245-01 07/20/15 9:1610 1g mL
P5G03295070245-02 07/20/15 9:1630.01 1g mL
P5G03295070245-03 07/20/15 9:1630.03 1g mL
P5G03295070245-04 07/20/15 9:1630.02 1g mL
P5G03295070245-05 07/20/15 9:1630.01 1g mL
P5G03295070245-06 07/20/15 9:1630 1g mL
P5G03295070245-07 07/20/15 9:1630.02 1g mL
P5G03295070245-08 07/20/15 9:1630.01 1g mL
P5G03295070245-09 07/20/15 9:1630 1g mL
P5G03295070245-10 07/20/15 9:1630 1g mL
P5G03295070245-11 07/20/15 9:1630 10g mL
P5G03295070245-12 07/20/15 9:1630.04 10g mL
P5G03295070245-13 07/20/15 9:1630 1g mL
P5G03295070245-14 07/20/15 9:1630.01 10g mL
P5G03295070245-15 07/20/15 9:1630.02 10g mL
P5G03295070245-16 07/20/15 9:1615.11 10g mL
P5G03295070245-17 07/20/15 9:1630 1g mL
P5G03295070245-18 07/20/15 9:1630.03 10g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P5G02945070245-01 07/17/15 8:502.05 50g mL
P5G02945070245-01 07/17/15 8:502.05 50g mL
P5G02945070245-02 07/17/15 8:502.02 50g mL
P5G02945070245-02 07/17/15 8:502.02 50g mL
P5G02945070245-03 07/17/15 8:501.95 50g mL
P5G02945070245-03 07/17/15 8:501.95 50g mL
P5G02945070245-04 07/17/15 8:501.97 50g mL
P5G02945070245-04 07/17/15 8:501.97 50g mL
P5G02945070245-05 07/17/15 8:502 50g mL
P5G02945070245-05 07/17/15 8:502 50g mL
P5G02945070245-06 07/17/15 8:501.98 50g mL
P5G02945070245-06 07/17/15 8:501.98 50g mL
P5G02945070245-07 07/17/15 8:501.97 50g mL
P5G02945070245-07 07/17/15 8:501.97 50g mL
P5G02945070245-08 07/17/15 8:502 50g mL
P5G02945070245-08 07/17/15 8:502 50g mL
P5G02945070245-09 07/17/15 8:502 50g mL
P5G02945070245-09 07/17/15 8:502 50g mL
P5G02945070245-10 07/17/15 8:502.01 50g mL
P5G02945070245-10 07/17/15 8:502.01 50g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 105 of 135
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P5G02945070245-11 07/17/15 8:502.04 50g mL
P5G02945070245-11 07/17/15 8:502.04 50g mL
P5G02945070245-12 07/17/15 8:501.96 50g mL
P5G02945070245-12 07/17/15 8:501.96 50g mL
P5G02945070245-13 07/17/15 8:502.02 50g mL
P5G02945070245-13 07/17/15 8:502.02 50g mL
P5G02945070245-14 07/17/15 8:501.96 50g mL
P5G02945070245-14 07/17/15 8:501.96 50g mL
P5G02945070245-15 07/17/15 8:501.95 50g mL
P5G02945070245-15 07/17/15 8:501.95 50g mL
P5G02945070245-15 07/17/15 8:501.95 50g mL
P5G02945070245-16 07/17/15 8:501.98 50g mL
P5G02945070245-16 07/17/15 8:501.98 50g mL
P5G02945070245-17 07/17/15 8:501.99 50g mL
P5G02945070245-17 07/17/15 8:501.99 50g mL
P5G02945070245-18 07/17/15 8:501.97 50g mL
P5G02945070245-18 07/17/15 8:501.97 50g mL
P5G02955070245-19 07/17/15 8:502.03 50g mL
P5G02955070245-20 07/17/15 8:502.02 50g mL
P5G02955070245-20 07/17/15 8:502.02 50g mL
P5G02945070245-21 07/17/15 8:502.02 50g mL
P5G02945070245-21 07/17/15 8:502.02 50g mL
P5G02945070245-22 07/17/15 8:501.97 50g mL
P5G02945070245-22 07/17/15 8:501.97 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P5G02705070245-01 07/16/15 10:400.58 50g mL
P5G02705070245-02 07/16/15 10:400.65 50g mL
P5G02705070245-03 07/16/15 10:400.56 50g mL
P5G02705070245-04 07/16/15 10:400.6 50g mL
P5G02705070245-05 07/16/15 10:400.62 50g mL
P5G02705070245-06 07/16/15 10:400.58 50g mL
P5G02705070245-07 07/16/15 10:400.57 50g mL
P5G02705070245-08 07/16/15 10:400.6 50g mL
P5G02705070245-09 07/16/15 10:400.6 50g mL
P5G02705070245-10 07/16/15 10:400.57 50g mL
P5G02705070245-11 07/16/15 10:400.57 50g mL
P5G02705070245-12 07/16/15 10:400.61 50g mL
P5G02705070245-13 07/16/15 10:400.63 50g mL
P5G02705070245-14 07/16/15 10:400.58 50g mL
P5G02705070245-15 07/16/15 10:400.58 50g mL
P5G02705070245-16 07/16/15 10:400.57 50g mL
P5G02705070245-17 07/16/15 10:400.55 50g mL
P5G02705070245-18 07/16/15 10:400.6 50g mL
P5G02715070245-19 07/16/15 10:400.56 50g mL
P5G02715070245-20 07/16/15 10:400.57 50g mL
P5G02705070245-21 07/16/15 10:400.64 50g mL
P5G02705070245-22 07/16/15 10:400.64 50g mL
Prep Method: 3580A VMS
Lab Number Batch Date/TimeInitialFinal
P5G04635070245-19 07/24/15 14:240.1 10g mL
P5G04635070245-20 07/24/15 14:240.1 10g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 106 of 135
Sample Extraction Data
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P5G03185070245-01 07/17/15 16:393.94 5g mL
P5G03185070245-02 07/17/15 16:392.85 5g mL
P5G03185070245-03 07/17/15 16:394.35 5g mL
P5G03185070245-04 07/17/15 16:392.82 5g mL
P5G03185070245-05 07/17/15 16:390.45 5g mL
P5G03185070245-06 07/17/15 16:390.79 5g mL
P5G03185070245-07 07/17/15 16:394.11 5g mL
P5G03185070245-08 07/17/15 16:393.2 5g mL
P5G03185070245-09 07/17/15 16:394.17 5g mL
P5G03185070245-10 07/17/15 16:392.21 5g mL
P5G03855070245-11 07/21/15 8:422.46 5g mL
P5G03855070245-12 07/21/15 8:422.08 5g mL
P5G03185070245-13 07/17/15 16:391.13 5g mL
P5G03185070245-14 07/17/15 16:392.69 5g mL
P5G03185070245-15 07/17/15 16:392.02 5g mL
P5G03475070245-16 07/20/15 9:592.27 5g mL
P5G03475070245-17 07/20/15 9:594.54 5g mL
P5G03475070245-18 07/20/15 9:592.85 5g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P5G03895070245-07 07/21/15 9:043.98 5g mL
P5G03895070245-08 07/21/15 9:043.49 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 107 of 135
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Analysis
5070245-01 Reactivity, Cyanide (Sub)
5070245-01 Reactivity, Sulfide (Sub)
5070245-02 Reactivity, Cyanide (Sub)
5070245-02 Reactivity, Sulfide (Sub)
5070245-03 Reactivity, Cyanide (Sub)
5070245-03 Reactivity, Sulfide (Sub)
5070245-04 Reactivity, Cyanide (Sub)
5070245-04 Reactivity, Sulfide (Sub)
5070245-05 Reactivity, Cyanide (Sub)
5070245-05 Reactivity, Sulfide (Sub)
5070245-06 Reactivity, Cyanide (Sub)
5070245-06 Reactivity, Sulfide (Sub)
5070245-07 Reactivity, Cyanide (Sub)
5070245-07 Reactivity, Sulfide (Sub)
5070245-08 Reactivity, Cyanide (Sub)
5070245-08 Reactivity, Sulfide (Sub)
5070245-09 Reactivity, Cyanide (Sub)
5070245-09 Reactivity, Sulfide (Sub)
5070245-10 Reactivity, Cyanide (Sub)
5070245-10 Reactivity, Sulfide (Sub)
5070245-11 Reactivity, Cyanide (Sub)
5070245-11 Reactivity, Sulfide (Sub)
5070245-12 Reactivity, Cyanide (Sub)
5070245-12 Reactivity, Sulfide (Sub)
5070245-13 Reactivity, Cyanide (Sub)
5070245-13 Reactivity, Sulfide (Sub)
5070245-14 Reactivity, Cyanide (Sub)
5070245-14 Reactivity, Sulfide (Sub)
5070245-15 Reactivity, Cyanide (Sub)
5070245-15 Reactivity, Sulfide (Sub)
5070245-16 Reactivity, Cyanide (Sub)
5070245-16 Reactivity, Sulfide (Sub)
5070245-17 Reactivity, Cyanide (Sub)
5070245-17 Reactivity, Sulfide (Sub)
5070245-18 Reactivity, Cyanide (Sub)
5070245-18 Reactivity, Sulfide (Sub)
5070245-19 Flash Point (Sub)
5070245-19 Reactivity, Cyanide (Sub)
5070245-19 Reactivity, Sulfide (Sub)
5070245-20 Flash Point (Sub)
5070245-20 Reactivity, Cyanide (Sub)
5070245-20 Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 108 of 135
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Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5100424
10/28/2015
34 mg/kg dry5100424-01 C-36 - PM Aroclor 1254 8082A
44 mg/kg dry5100424-01 C-36 - PM Aroclor 1260 8082A
15 mg/kg wet5100424-02 C-37 Aroclor 1254 8082A
3.8 mg/kg dry5100424-03 C-38 - PM Aroclor 1254 8082A
7.2 mg/kg dry5100424-03 C-38 - PM Aroclor 1268 8082A
160 mg/kg wet5100424-04 C-39 Aroclor 1254 8082A
9.6 mg/kg dry5100424-06 C-41 - PM Aroclor 1254 8082A
40 mg/kg dry5100424-06 C-41 - PM Aroclor 1268 8082A
52 mg/kg dry5100424-07 C-42 - PM Aroclor 1254 8082A
8800 J mg/kg wet5100424-08 C-43 Aroclor 1254 8082A
24000 mg/kg wet5100424-08 C-43 Aroclor 1268 8082A
68000 mg/kg wet5100424-09 C-44 Aroclor 1254 8082A
2.9 ug/Wipe5100424-10 W-3 Aroclor 1254 8082A
15 ug/Wipe5100424-10 W-3 Aroclor 1268 8082A
0.32 J ug/Wipe5100424-11 W-2 Aroclor 1268 8082A
0.38 J ug/Wipe5100424-12 W-1 Aroclor 1268 8082A
1.2 ug/Wipe5100424-13 W-4 Aroclor 1016 8082A
5.2 ug/Wipe5100424-13 W-4 Aroclor 1254 8082A
0.38 J ug/Wipe5100424-14 W-5 Aroclor 1254 8082A
1.6 ug/Wipe5100424-15 W-6 Aroclor 1254 8082A
1.4 ug/Wipe5100424-16 W-7 Aroclor 1016 8082A
0.98 ug/Wipe5100424-16 W-7 Aroclor 1254 8082A
0.64 ug/Wipe5100424-17 W-8 Aroclor 1254 8082A
23 ug/Wipe5100424-18 W-9 Aroclor 1254 8082A
95 ug/Wipe5100424-18 W-9 Aroclor 1268 8082A
35 ug/Wipe5100424-19 W-10 Aroclor 1254 8082A
3.5 Ab ug/Wipe5100424-19 W-10 Aroclor 1268 8082A
92 ug/Wipe5100424-20 W-11 Aroclor 1254 8082A
22 ug/Wipe5100424-21 W-12 Aroclor 1254 8082A
1.6 ug/Wipe5100424-21 W-12 Aroclor 1268 8082A
1.4 ug/Wipe5100424-22 W-13 Aroclor 1254 8082A
1.4 ug/Wipe5100424-22 W-13 Aroclor 1268 8082A
1.2 ug/Wipe5100424-23 W-14 Aroclor 1254 8082A
0.25 J ug/Wipe5100424-23 W-14 Aroclor 1268 8082A
13 ug/Wipe5100424-25 W-16 Aroclor 1254 8082A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 3 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Concrete
Client Sample ID: C-36 - PM
Prism Sample ID: 5100424-01
Prism Work Order: 5100424
Time Collected: 10/22/15 11:25
Time Submitted: 10/22/15 10:35
BRL 8082A P5J047910.30 10/26/15 16:43 JMCmg/kg dry 0.033Aroclor 1016
BRL 8082A P5J047910.61 10/26/15 16:43 JMCmg/kg dry 0.24Aroclor 1221
BRL 8082A P5J047910.61 10/26/15 16:43 JMCmg/kg dry 0.079Aroclor 1232
BRL 8082A P5J047910.30 10/26/15 16:43 JMCmg/kg dry 0.081Aroclor 1242
BRL 8082A P5J047910.30 10/26/15 16:43 JMCmg/kg dry 0.061Aroclor 1248
BRL 8082A P5J047910.30 10/26/15 16:43 JMCmg/kg dry 0.15Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 4 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Caulk
Client Sample ID: C-37
Prism Sample ID: 5100424-02
Prism Work Order: 5100424
Time Collected: 10/22/15 11:40
Time Submitted: 10/22/15 10:35
BRL 8082A P5J0479101410/27/15 21:57 JMCmg/kg wet 1.5Aroclor 1016
BRL 8082A P5J0479102810/27/15 21:57 JMCmg/kg wet 11Aroclor 1221
BRL 8082A P5J0479102810/27/15 21:57 JMCmg/kg wet 3.6Aroclor 1232
BRL 8082A P5J0479101410/27/15 21:57 JMCmg/kg wet 3.7Aroclor 1242
BRL 8082A P5J0479101410/27/15 21:57 JMCmg/kg wet 2.8Aroclor 1248
BRL 8082A P5J0479101410/27/15 21:57 JMCmg/kg wet 1.8Aroclor 1260
BRL 8082A P5J0479101410/27/15 21:57 JMCAmg/kg wet 7.0Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 5 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Concrete
Client Sample ID: C-38 - PM
Prism Sample ID: 5100424-03
Prism Work Order: 5100424
Time Collected: 10/22/15 11:50
Time Submitted: 10/22/15 10:35
BRL 8082A P5J047910.30 10/26/15 18:08 JMCmg/kg dry 0.033Aroclor 1016
BRL 8082A P5J047910.61 10/26/15 18:08 JMCmg/kg dry 0.24Aroclor 1221
BRL 8082A P5J047910.61 10/26/15 18:08 JMCmg/kg dry 0.079Aroclor 1232
BRL 8082A P5J047910.30 10/26/15 18:08 JMCmg/kg dry 0.081Aroclor 1242
BRL 8082A P5J047910.30 10/26/15 18:08 JMCmg/kg dry 0.061Aroclor 1248
BRL 8082A P5J047910.30 10/26/15 18:08 JMCmg/kg dry 0.038Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 6 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Caulk
Client Sample ID: C-39
Prism Sample ID: 5100424-04
Prism Work Order: 5100424
Time Collected: 10/22/15 13:26
Time Submitted: 10/22/15 10:35
BRL 8082A P5J047910015010/27/15 3:21 JMCmg/kg wet 16Aroclor 1016
BRL 8082A P5J047910030010/27/15 3:21 JMCmg/kg wet 120Aroclor 1221
BRL 8082A P5J047910030010/27/15 3:21 JMCmg/kg wet 39Aroclor 1232
BRL 8082A P5J047910015010/27/15 3:21 JMCmg/kg wet 40Aroclor 1242
BRL 8082A P5J047910015010/27/15 3:21 JMCmg/kg wet 30Aroclor 1248
BRL 8082A P5J047910015010/27/15 3:21 JMCmg/kg wet 19Aroclor 1260
BRL 8082A P5J047910015010/27/15 3:21 JMCmg/kg wet 74Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 7 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Caulk
Client Sample ID: C-40
Prism Sample ID: 5100424-05
Prism Work Order: 5100424
Time Collected: 10/22/15 13:55
Time Submitted: 10/22/15 10:35
RL
BRL 8082A P5J0479507410/27/15 16:49 JMCmg/kg wet 8.2Aroclor 1016
BRL 8082A P5J04795015010/27/15 16:49 JMCmg/kg wet 59Aroclor 1221
BRL 8082A P5J04795015010/27/15 16:49 JMCmg/kg wet 19Aroclor 1232
BRL 8082A P5J0479507410/27/15 16:49 JMCmg/kg wet 20Aroclor 1242
BRL 8082A P5J0479507410/27/15 16:49 JMCmg/kg wet 15Aroclor 1248
BRL 8082A P5J0479507410/27/15 16:49 JMCAmg/kg wet 18Aroclor 1254
BRL 8082A P5J0479507410/27/15 16:49 JMCmg/kg wet 9.4Aroclor 1260
BRL 8082A P5J0479507410/27/15 16:49 JMCAmg/kg wet 37Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 8 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Concrete
Client Sample ID: C-41 - PM
Prism Sample ID: 5100424-06
Prism Work Order: 5100424
Time Collected: 10/22/15 14:00
Time Submitted: 10/22/15 10:35
BRL 8082A P5J047910.30 10/27/15 4:46 JMCmg/kg dry 0.033Aroclor 1016
BRL 8082A P5J047910.60 10/27/15 4:46 JMCmg/kg dry 0.24Aroclor 1221
BRL 8082A P5J047910.60 10/27/15 4:46 JMCmg/kg dry 0.078Aroclor 1232
BRL 8082A P5J047910.30 10/27/15 4:46 JMCmg/kg dry 0.080Aroclor 1242
BRL 8082A P5J047910.30 10/27/15 4:46 JMCmg/kg dry 0.060Aroclor 1248
BRL 8082A P5J047910.30 10/27/15 4:46 JMCmg/kg dry 0.038Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 9 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Concrete
Client Sample ID: C-42 - PM
Prism Sample ID: 5100424-07
Prism Work Order: 5100424
Time Collected: 10/22/15 14:50
Time Submitted: 10/22/15 10:35
BRL 8082A P5J047910.30 10/27/15 5:28 JMCmg/kg dry 0.033Aroclor 1016
BRL 8082A P5J047910.60 10/27/15 5:28 JMCmg/kg dry 0.24Aroclor 1221
BRL 8082A P5J047910.60 10/27/15 5:28 JMCmg/kg dry 0.078Aroclor 1232
BRL 8082A P5J047910.30 10/27/15 5:28 JMCmg/kg dry 0.080Aroclor 1242
BRL 8082A P5J047910.30 10/27/15 5:28 JMCmg/kg dry 0.060Aroclor 1248
BRL 8082A P5J047910.30 10/27/15 5:28 JMCmg/kg dry 0.038Aroclor 1260
BRL 8082A P5J047910.30 10/27/15 5:28 JMCmg/kg dry 0.15Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 10 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Caulk
Client Sample ID: C-43
Prism Sample ID: 5100424-08
Prism Work Order: 5100424
Time Collected: 10/22/15 15:08
Time Submitted: 10/22/15 10:35
BRL 8082A P5J0479100001500010/26/15 21:41 JMCmg/kg wet 1600Aroclor 1016
BRL 8082A P5J0479100003000010/26/15 21:41 JMCmg/kg wet 12000Aroclor 1221
BRL 8082A P5J0479100003000010/26/15 21:41 JMCmg/kg wet 3900Aroclor 1232
BRL 8082A P5J0479100001500010/26/15 21:41 JMCmg/kg wet 4000Aroclor 1242
BRL 8082A P5J0479100001500010/26/15 21:41 JMCmg/kg wet 3000Aroclor 1248
BRL 8082A P5J0479100001500010/26/15 21:41 JMCmg/kg wet 1900Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 11 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Caulk
Client Sample ID: C-44
Prism Sample ID: 5100424-09
Prism Work Order: 5100424
Time Collected: 10/22/15 15:15
Time Submitted: 10/22/15 10:35
BRL 8082A P5J0479100001400010/26/15 22:23 JMCmg/kg wet 1600Aroclor 1016
BRL 8082A P5J0479100002900010/26/15 22:23 JMCmg/kg wet 11000Aroclor 1221
BRL 8082A P5J0479100002900010/26/15 22:23 JMCmg/kg wet 3700Aroclor 1232
BRL 8082A P5J0479100001400010/26/15 22:23 JMCmg/kg wet 3800Aroclor 1242
BRL 8082A P5J0479100001400010/26/15 22:23 JMCmg/kg wet 2900Aroclor 1248
BRL 8082A P5J0479100001400010/26/15 22:23 JMCmg/kg wet 1800Aroclor 1260
BRL 8082A P5J0479100001400010/26/15 22:23 JMCmg/kg wet 7100Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 12 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-3
Prism Sample ID: 5100424-10
Prism Work Order: 5100424
Time Collected: 10/22/15 11:06
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 15:12 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 15:12 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 15:12 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 15:12 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 15:12 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 15:12 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 13 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-2
Prism Sample ID: 5100424-11
Prism Work Order: 5100424
Time Collected: 10/22/15 10:44
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 15:54 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 15:54 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 15:54 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 15:54 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 15:54 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 15:54 JMCug/Wipe 0.12Aroclor 1254
BRL 8082A P5J045110.50 10/23/15 15:54 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 14 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-1
Prism Sample ID: 5100424-12
Prism Work Order: 5100424
Time Collected: 10/22/15 10:37
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 16:37 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 16:37 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 16:37 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 16:37 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 16:37 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 16:37 JMCug/Wipe 0.12Aroclor 1254
BRL 8082A P5J045110.50 10/23/15 16:37 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 15 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-4
Prism Sample ID: 5100424-13
Prism Work Order: 5100424
Time Collected: 10/22/15 11:17
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045111.0 10/23/15 17:19 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 17:19 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 17:19 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 17:19 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 17:19 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/23/15 17:19 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 16 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-5
Prism Sample ID: 5100424-14
Prism Work Order: 5100424
Time Collected: 10/22/15 11:23
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 18:02 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 18:02 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 18:02 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 18:02 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 18:02 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 18:02 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/23/15 18:02 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 17 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-6
Prism Sample ID: 5100424-15
Prism Work Order: 5100424
Time Collected: 10/22/15 13:09
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 18:44 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 18:44 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 18:44 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 18:44 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 18:44 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 18:44 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/23/15 18:44 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 18 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-7
Prism Sample ID: 5100424-16
Prism Work Order: 5100424
Time Collected: 10/22/15 13:28
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045111.0 10/23/15 19:27 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 19:27 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 19:27 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 19:27 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 19:27 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/23/15 19:27 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 19 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-8
Prism Sample ID: 5100424-17
Prism Work Order: 5100424
Time Collected: 10/22/15 13:45
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 20:09 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 20:09 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 20:09 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 20:09 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 20:09 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 20:09 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/23/15 20:09 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 20 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-9
Prism Sample ID: 5100424-18
Prism Work Order: 5100424
Time Collected: 10/22/15 14:10
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 20:51 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 20:51 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 20:51 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 20:51 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 20:51 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 20:51 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 21 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-10
Prism Sample ID: 5100424-19
Prism Work Order: 5100424
Time Collected: 10/22/15 14:15
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/23/15 21:34 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/23/15 21:34 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/23/15 21:34 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/23/15 21:34 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/23/15 21:34 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/23/15 21:34 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 22 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-11
Prism Sample ID: 5100424-20
Prism Work Order: 5100424
Time Collected: 10/22/15 14:35
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 0:23 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 0:23 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 0:23 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 0:23 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 0:23 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 0:23 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/24/15 0:23 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 23 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-12
Prism Sample ID: 5100424-21
Prism Work Order: 5100424
Time Collected: 10/22/15 14:58
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 1:06 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 1:06 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 1:06 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 1:06 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 1:06 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 1:06 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 24 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-13
Prism Sample ID: 5100424-22
Prism Work Order: 5100424
Time Collected: 10/22/15 15:18
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 1:48 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 1:48 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 1:48 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 1:48 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 1:48 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 1:48 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 25 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-14
Prism Sample ID: 5100424-23
Prism Work Order: 5100424
Time Collected: 10/22/15 15:21
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 2:30 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 2:30 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 2:30 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 2:30 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 2:30 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 2:30 JMCug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 26 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-15
Prism Sample ID: 5100424-24
Prism Work Order: 5100424
Time Collected: 10/22/15 15:24
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 3:13 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 3:13 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 3:13 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 3:13 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 3:13 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 3:13 JMCug/Wipe 0.12Aroclor 1254
BRL 8082A P5J045110.50 10/24/15 3:13 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/24/15 3:13 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 27 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-16
Prism Sample ID: 5100424-25
Prism Work Order: 5100424
Time Collected: 10/22/15 15:32
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 3:55 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 3:55 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 3:55 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 3:55 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 3:55 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 3:55 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/24/15 3:55 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 28 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-17
Prism Sample ID: 5100424-26
Prism Work Order: 5100424
Time Collected: 10/22/15 15:35
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 4:37 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 4:37 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 4:37 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 4:37 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 4:37 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 4:37 JMCug/Wipe 0.12Aroclor 1254
BRL 8082A P5J045110.50 10/24/15 4:37 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/24/15 4:37 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 29 of 37
10/28/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Sample Matrix: Wipe
Client Sample ID: W-18
Prism Sample ID: 5100424-27
Prism Work Order: 5100424
Time Collected: 10/22/15 15:40
Time Submitted: 10/22/15 10:35
BRL 8082A P5J045110.50 10/24/15 5:20 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J045111.0 10/24/15 5:20 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J045111.0 10/24/15 5:20 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J045110.50 10/24/15 5:20 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J045110.50 10/24/15 5:20 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J045110.50 10/24/15 5:20 JMCug/Wipe 0.12Aroclor 1254
BRL 8082A P5J045110.50 10/24/15 5:20 JMCug/Wipe 0.069Aroclor 1260
BRL 8082A P5J045110.50 10/24/15 5:20 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 30 of 37
10/28/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Prism Work Order: 5100424
Time Submitted: 10/22/2015 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared & Analyzed: 10/23/15
Aroclor 1016 ug/WipeBRL0.50
Aroclor 1221 ug/WipeBRL1.0
Aroclor 1232 ug/WipeBRL1.0
Aroclor 1242 ug/WipeBRL0.50
Aroclor 1248 ug/WipeBRL0.50
Aroclor 1254 ug/WipeBRL0.50
Aroclor 1260 ug/WipeBRL0.50
Aroclor 1268 ug/WipeBRL0.50
Prepared & Analyzed: 10/23/15
Aroclor 1016 ug/Wipe7.12 0.50 10.00 64-15171
Aroclor 1260 ug/Wipe6.38 0.50 10.00 45-16664
Prepared & Analyzed: 10/23/15
Aroclor 1016 ug/Wipe8.83 0.50 10.00 5064-15188 21
Aroclor 1260 ug/Wipe8.23 0.50 10.00 5045-16682 25
Prepared & Analyzed: 10/26/15
Aroclor 1016 mg/kg wetBRL0.050
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.050
Aroclor 1248 mg/kg wetBRL0.050
Aroclor 1254 mg/kg wetBRL0.050
Aroclor 1260 mg/kg wetBRL0.050
Aroclor 1268 mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 31 of 37
10/28/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Prism Work Order: 5100424
Time Submitted: 10/22/2015 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared & Analyzed: 10/26/15
Aroclor 1016 mg/kg wet0.320 0.050 0.3331 64-15196
Aroclor 1260 mg/kg wet0.275 0.050 0.3331 45-16682
Prepared & Analyzed: 10/26/15
Aroclor 1016 mg/kg wet0.328 0.050 0.3332 5064-15198 2
Aroclor 1260 mg/kg wet0.280 0.050 0.3332 5045-16684 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 32 of 37
10/28/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Dave Hunter
Prism Work Order: 5100424
Time Submitted: 10/22/2015 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared & Analyzed: 10/23/15
% Solids % by Weight1000.100
Prepared & Analyzed: 10/23/15
% Solids % by Weight99.3 0.100 99.4 200.01
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 33 of 37
P5J04535100424-01 10/23/15 10:593030gg
P5J04535100424-03 10/23/15 10:593030gg
P5J04535100424-06 10/23/15 10:593030gg
P5J04535100424-07 10/23/15 10:593030gg
P5J04515100424-10 10/23/15 9:15110WipemL
P5J04515100424-10 10/23/15 9:15110WipemL
P5J04515100424-11 10/23/15 9:15110WipemL
P5J04515100424-12 10/23/15 9:15110WipemL
P5J04515100424-13 10/23/15 9:15110WipemL
P5J04515100424-14 10/23/15 9:15110WipemL
P5J04515100424-15 10/23/15 9:15110WipemL
P5J04515100424-16 10/23/15 9:15110WipemL
P5J04515100424-17 10/23/15 9:15110WipemL
P5J04515100424-18 10/23/15 9:15110WipemL
P5J04515100424-18 10/23/15 9:15110WipemL
P5J04515100424-19 10/23/15 9:15110WipemL
P5J04515100424-19 10/23/15 9:15110WipemL
P5J04515100424-20 10/23/15 9:15110WipemL
P5J04515100424-20 10/23/15 9:15110WipemL
P5J04515100424-21 10/23/15 9:15110WipemL
P5J04515100424-21 10/23/15 9:15110WipemL
P5J04515100424-22 10/23/15 9:15110WipemL
P5J04515100424-23 10/23/15 9:15110WipemL
P5J04515100424-24 10/23/15 9:15110WipemL
P5J04515100424-25 10/23/15 9:15110WipemL
P5J04515100424-26 10/23/15 9:15110WipemL
P5J04515100424-27 10/23/15 9:15110WipemL
P5J04795100424-01 10/26/15 8:30510gmL
P5J04795100424-01 10/26/15 8:30510gmL
P5J04795100424-02 10/26/15 8:301.07 10g mL
P5J04795100424-02 10/26/15 8:301.07 10g mL
P5J04795100424-03 10/26/15 8:30510gmL
P5J04795100424-03 10/26/15 8:30510gmL
P5J04795100424-04 10/26/15 8:301.01 10g mL
P5J04795100424-05 10/26/15 8:301.01 10g mL
P5J04795100424-06 10/26/15 8:305.05 10g mL
P5J04795100424-06 10/26/15 8:305.05 10g mL
P5J04795100424-07 10/26/15 8:305.04 10g mL
P5J04795100424-07 10/26/15 8:305.04 10g mL
P5J04795100424-08 10/26/15 8:30110gmL
P5J04795100424-09 10/26/15 8:301.05 10g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 34 of 37
Page 35 of 37
Page 36 of 37
Page 37 of 37
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735 10/29/2015
Cardno - Charlotte
Steven Aldis
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Project: Charlotte Observer
Lab Submittal Date: 10/23/2015
Prism Work Order: 5100442
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
VP Laboratory Services
Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash
Project Manager
A The analyte was found at >1/2 the RL in the method blank, but not in the samples associated with this analytical
batch.
B Analyte is found in the associated blank at a concentration >1/2 RL.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 1 of 12
10/29/2015
Prism Work Order: 5100442
5100442-01 10/23/15C-45-PM 10/23/15Concrete
5100442-02 10/23/15W-19 10/23/15Caulk
5100442-03 10/23/15C-46-PM 10/23/15Concrete
5100442-04 10/23/15W-20 10/23/15Caulk
5100442-05 10/23/15C-47-PM 10/23/15Concrete
Samples were received in good condition at 5.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 2 of 12
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5100442
10/29/2015
1.8 mg/kg dry5100442-01 C-45-PM Aroclor 1254 8082A
5.9 mg/kg dry5100442-01 C-45-PM Aroclor 1268 8082A
0.79 ug/Wipe5100442-02 W-19 Aroclor 1254 8082A
0.30 J ug/Wipe5100442-02 W-19 Aroclor 1268 8082A
2.1 mg/kg dry5100442-03 C-46-PM Aroclor 1254 8082A
0.80 J mg/kg dry5100442-05 C-47-PM Aroclor 1254 8082A
2.5 mg/kg dry5100442-05 C-47-PM Aroclor 1268 8082A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 3 of 12
10/29/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Concrete
Client Sample ID: C-45-PM
Prism Sample ID: 5100442-01
Prism Work Order: 5100442
Time Collected: 10/23/15 10:57
Time Submitted: 10/23/15 14:40
BRL 8082A P5J047910.51 10/27/15 1:14 JMCmg/kg dry 0.056Aroclor 1016
BRL 8082A P5J047911.0 10/27/15 1:14 JMCmg/kg dry 0.41Aroclor 1221
BRL 8082A P5J047911.0 10/27/15 1:14 JMCmg/kg dry 0.13Aroclor 1232
BRL 8082A P5J047910.51 10/27/15 1:14 JMCmg/kg dry 0.14Aroclor 1242
BRL 8082A P5J047910.51 10/27/15 1:14 JMCmg/kg dry 0.10Aroclor 1248
BRL 8082A P5J047910.51 10/27/15 1:14 JMCmg/kg dry 0.064Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 4 of 12
10/29/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Caulk
Client Sample ID: W-19
Prism Sample ID: 5100442-02
Prism Work Order: 5100442
Time Collected: 10/23/15 13:27
Time Submitted: 10/23/15 14:40
BRL 8082A P5J046910.50 10/27/15 8:18 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J046911.0 10/27/15 8:18 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J046911.0 10/27/15 8:18 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J046910.50 10/27/15 8:18 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J046910.50 10/27/15 8:18 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J046910.50 10/27/15 8:18 JMCAug/Wipe 0.069Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 5 of 12
10/29/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Concrete
Client Sample ID: C-46-PM
Prism Sample ID: 5100442-03
Prism Work Order: 5100442
Time Collected: 10/23/15 13:34
Time Submitted: 10/23/15 14:40
BRL 8082A P5J047910.50 10/27/15 1:56 JMCmg/kg dry 0.055Aroclor 1016
BRL 8082A P5J047911.0 10/27/15 1:56 JMCmg/kg dry 0.40Aroclor 1221
BRL 8082A P5J047911.0 10/27/15 1:56 JMCmg/kg dry 0.13Aroclor 1232
BRL 8082A P5J047910.50 10/27/15 1:56 JMCmg/kg dry 0.13Aroclor 1242
BRL 8082A P5J047910.50 10/27/15 1:56 JMCmg/kg dry 0.10Aroclor 1248
BRL 8082A P5J047910.50 10/27/15 1:56 JMCmg/kg dry 0.063Aroclor 1260
BRL 8082A P5J047910.50 10/27/15 1:56 JMCmg/kg dry 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 6 of 12
10/29/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Caulk
Client Sample ID: W-20
Prism Sample ID: 5100442-04
Prism Work Order: 5100442
Time Collected: 10/23/15 13:45
Time Submitted: 10/23/15 14:40
BRL 8082A P5J046910.50 10/27/15 9:00 JMCug/Wipe 0.047Aroclor 1016
BRL 8082A P5J046911.0 10/27/15 9:00 JMCug/Wipe 0.40Aroclor 1221
BRL 8082A P5J046911.0 10/27/15 9:00 JMCug/Wipe 0.13Aroclor 1232
BRL 8082A P5J046910.50 10/27/15 9:00 JMCug/Wipe 0.13Aroclor 1242
BRL 8082A P5J046910.50 10/27/15 9:00 JMCug/Wipe 0.10Aroclor 1248
BRL 8082A P5J046910.50 10/27/15 9:00 JMCug/Wipe 0.12Aroclor 1254
BRL 8082A P5J046910.50 10/27/15 9:00 JMCAug/Wipe 0.069Aroclor 1260
BRL 8082A P5J046910.50 10/27/15 9:00 JMCug/Wipe 0.25Aroclor 1268
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 7 of 12
10/29/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Concrete
Client Sample ID: C-47-PM
Prism Sample ID: 5100442-05
Prism Work Order: 5100442
Time Collected: 10/23/15 14:02
Time Submitted: 10/23/15 14:40
BRL 8082A P5J047911.5 10/27/15 2:38 JMCmg/kg dry 0.17Aroclor 1016
BRL 8082A P5J047913.0 10/27/15 2:38 JMCmg/kg dry 1.2Aroclor 1221
BRL 8082A P5J047913.0 10/27/15 2:38 JMCmg/kg dry 0.39Aroclor 1232
BRL 8082A P5J047911.5 10/27/15 2:38 JMCmg/kg dry 0.40Aroclor 1242
BRL 8082A P5J047911.5 10/27/15 2:38 JMCmg/kg dry 0.30Aroclor 1248
BRL 8082A P5J047911.5 10/27/15 2:38 JMCmg/kg dry 0.19Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 8 of 12
10/29/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5100442
Time Submitted: 10/23/2015 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared: 10/26/15 Analyzed: 10/27/15
Aroclor 1016 ug/WipeBRL0.50
Aroclor 1221 ug/WipeBRL1.0
Aroclor 1232 ug/WipeBRL1.0
Aroclor 1242 ug/WipeBRL0.50
Aroclor 1248 ug/WipeBRL0.50
Aroclor 1254 ug/WipeBRL0.50
Aroclor 1260 ug/Wipe0.470 0.50 A, J
Aroclor 1268 ug/WipeBRL0.50
Prepared: 10/26/15 Analyzed: 10/27/15
Aroclor 1016 ug/Wipe6.77 0.50 10.00 64-15168
Aroclor 1260 ug/Wipe6.42 0.50 10.00 B45-16664
Prepared: 10/26/15 Analyzed: 10/27/15
Aroclor 1016 ug/Wipe6.54 0.50 10.00 5064-15165 3
Aroclor 1260 ug/Wipe6.01 0.50 10.00 50 B45-16660 7
Prepared & Analyzed: 10/26/15
Aroclor 1016 mg/kg wetBRL0.050
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.050
Aroclor 1248 mg/kg wetBRL0.050
Aroclor 1254 mg/kg wetBRL0.050
Aroclor 1260 mg/kg wetBRL0.050
Aroclor 1268 mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 9 of 12
10/29/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5100442
Time Submitted: 10/23/2015 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared & Analyzed: 10/26/15
Aroclor 1016 mg/kg wet0.320 0.050 0.3331 64-15196
Aroclor 1260 mg/kg wet0.275 0.050 0.3331 45-16682
Prepared & Analyzed: 10/26/15
Aroclor 1016 mg/kg wet0.328 0.050 0.3332 5064-15198 2
Aroclor 1260 mg/kg wet0.280 0.050 0.3332 5045-16684 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 10 of 12
10/29/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5100442
Time Submitted: 10/23/2015 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared & Analyzed: 10/26/15
% Solids % by Weight1000.100
P5J04855100442-01 10/26/15 13:003030gg
P5J04855100442-03 10/26/15 13:003030gg
P5J04855100442-05 10/26/15 13:003030gg
P5J04695100442-02 10/26/15 10:17110WipemL
P5J04695100442-04 10/26/15 10:17110WipemL
P5J04795100442-01 10/26/15 8:30310gmL
P5J04795100442-03 10/26/15 8:30310gmL
P5J04795100442-05 10/26/15 8:30110gmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 11 of 12
Page 12 of 12
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735 10/30/2015
Cardno - Charlotte
Steven Aldis
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Project: Charlotte Observer
Lab Submittal Date: 10/27/2015
Prism Work Order: 5100492
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Samples were received on wet ice at a temperature of 22.3 degrees C; however, samples were collected
and submitted to the laboratory immediately after sample collection.

Please call if you have any questions relating to this analytical report.
Respectfully,
VP Laboratory Services
Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash
Project Manager
DO Surrogates diluted out.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 1 of 6
10/30/2015
Prism Work Order: 5100492
5100492-01 10/27/15PC-1 10/27/15Caulk
Samples were received at 22.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 2 of 6
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5100492
10/30/2015
1700 mg/kg wet5100492-01 PC-1 Aroclor 1254 8082A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 3 of 6
10/30/2015
ResultParameter Batch
IDReport
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Sample Matrix: Caulk
Client Sample ID: PC-1
Prism Sample ID: 5100492-01
Prism Work Order: 5100492
Time Collected: 10/27/15 15:05
Time Submitted: 10/27/15 15:15
BRL 8082A P5J05221000150010/29/15 0:01 JMCmg/kg wet 160Aroclor 1016
BRL 8082A P5J05221000300010/29/15 0:01 JMCmg/kg wet 1200Aroclor 1221
BRL 8082A P5J05221000300010/29/15 0:01 JMCmg/kg wet 390Aroclor 1232
BRL 8082A P5J05221000150010/29/15 0:01 JMCmg/kg wet 400Aroclor 1242
BRL 8082A P5J05221000150010/29/15 0:01 JMCmg/kg wet 300Aroclor 1248
BRL 8082A P5J05221000150010/29/15 0:01 JMCmg/kg wet 190Aroclor 1260
Surrogate Recovery Control Limits
Tetrachloro-m-xylene
Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 4 of 6
10/30/15
7606 Whitehall Executive Center Drive, Suite 800
Project: Charlotte ObserverCardno - Charlotte
Charlotte, NC 28273
Attn: Steven Aldis
Prism Work Order: 5100492
Time Submitted: 10/27/2015 3:15:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Prepared & Analyzed: 10/28/15
Aroclor 1016 mg/kg wetBRL0.050
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.050
Aroclor 1248 mg/kg wetBRL0.050
Aroclor 1254 mg/kg wetBRL0.050
Aroclor 1260 mg/kg wetBRL0.050
Prepared & Analyzed: 10/28/15
Aroclor 1016 mg/kg wet0.290 0.050 0.3333 64-15187
Aroclor 1260 mg/kg wet0.243 0.050 0.3333 45-16673
Prepared & Analyzed: 10/28/15
Aroclor 1016 mg/kg wet0.293 0.050 0.3330 5064-15188 1
Aroclor 1260 mg/kg wet0.246 0.050 0.3330 5045-16674 1
P5J05225100492-01 10/28/15 8:20110gmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Page 5 of 6
Page 6 of 6
29-Oct-2015
Cardno
Dave Hunter
Dear Dave,
Re:Charlette Observer; 199GSG1501 Work Order:15101166
Fax:[phone]Tel:[phone]
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
ALS Environmental received 12 samples on 24-Oct-2015 for the analyses presented in the following
report.
Project Manager
Chris Gibson
Chris Gibson
Electronically approved by: Chris Gibson
The analytical data provided relates directly to the samples received by ALS Environmental and for only
the analyses requested.
QC sample results for this data met laboratory specifications. Any exceptions are noted in the Case
Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report
need to be reproduced, it should be reproduced in full unless written approval has been obtained from
ALS Laboratory Group. Samples will be disposed in 30 days unless storage arrangements are made.
The total number of pages in this report is 18.
If you have any questions regarding this report, please feel free to contact me.
Sincerely,
ADDRESS 4388 Glendale Milford Rd Cincinnati, Ohio 45242- | PHONE [phone] | FAX [phone]
ALS GROUP USA, CORP. Part of the ALS Group An ALS Limited Company
Date: 29-Oct-15ALS Environmental
Project:Charlette Observer; 199GSG1501
Client:Cardno
Work Order:15101166 Work Order Sample Summary
Lab Samp ID Client Sample ID Collection DateTag Number Date ReceivedMatrix Hold
15101166-01 PUF-1 Air 10/23/2015 10/24/2015
15101166-02 PUF-2 Air 10/23/2015 10/24/2015
15101166-03 PUF-3 Air 10/23/2015 10/24/2015
15101166-04 PUF-4 Air 10/23/2015 10/24/2015
15101166-05 PUF-5 Air 10/23/2015 10/24/2015
15101166-06 PUF-6 Air 10/23/2015 10/24/2015
15101166-07 PUF-7 Air 10/23/2015 10/24/2015
15101166-08 PUF-8 Air 10/23/2015 10/24/2015
15101166-09 PUF-9 Air 10/23/2015 10/24/2015
15101166-10 PUF-10 Air 10/23/2015 10/24/2015
15101166-11 PUF-11 Air 10/23/2015 10/24/2015
15101166-12 Blank Air 10/23/2015 10/24/2015
SS Page 1 of 1
Date: 29-Oct-15ALS Environmental
Project:Charlette Observer; 199GSG1501
Client:Cardno
Work Order:15101166 Case Narrative
The analytical data provided relates directly to the samples received by ALS Laboratory
Group and for only the analyses requested.
Results relate only to the items tested and are not blank corrected unless indicated.
QC sample results for this data met laboratory specifications. Any exceptions are noted in the
Case Narrative, or noted with qualifiers in the report or QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained from ALS Laboratory Group. Samples will be disposed in 30 days
unless storage arrangements are made.The sample condition upon receipt was acceptable
except where noted.
Compound identification is based upon retention time matching only. Any compound with a
similar retention time will interfere. In the prescence of mutliple aroclors with overlapping or
shared peaks, the dominant discernable pattern will be reported.
The pattern present in the PUFs is indicative of AR 1248 both in peak ratio and retention time.
CN Page 1 of 1
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-1
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-01
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015 12:57
Aroclor 1016 0.020ND <0.0000083
Aroclor 1221 0.020ND <0.0000083
Aroclor 1232 0.020ND <0.0000083
Aroclor 1242 0.020ND <0.0000083
Aroclor 1248 0.020ND <0.0000083
Aroclor 1254 0.020ND <0.0000083
Aroclor 1260 0.020ND <0.0000083
Aroclor 1262 0.020ND <0.0000083
Aroclor 1268 0.020ND <0.0000083
AR Page 1 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-2
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-02
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015 13:10
Aroclor 1016 0.020ND <0.0000083
Aroclor 1221 0.020ND <0.0000083
Aroclor 1232 0.020ND <0.0000083
Aroclor 1242 0.020ND <0.0000083
Aroclor 1248 0.0200.12 0.000049
Aroclor 1254 0.020ND <0.0000083
Aroclor 1260 0.020ND <0.0000083
Aroclor 1262 0.020ND <0.0000083
Aroclor 1268 0.020ND <0.0000083
AR Page 2 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-3
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-03
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015
Aroclor 1016 0.10ND <0.000042
Aroclor 1221 0.10ND <0.000042
Aroclor 1232 0.10ND <0.000042
Aroclor 1242 0.10ND <0.000042
Aroclor 1248 0.100.33 0.00014
Aroclor 1254 0.10ND <0.000042
Aroclor 1260 0.10ND <0.000042
Aroclor 1262 0.10ND <0.000042
Aroclor 1268 0.10ND <0.000042
AR Page 3 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-4
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-04
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015
Aroclor 1016 0.10ND <0.000042
Aroclor 1221 0.10ND <0.000042
Aroclor 1232 0.10ND <0.000042
Aroclor 1242 0.10ND <0.000042
Aroclor 1248 0.101.6 0.00065
Aroclor 1254 0.10ND <0.000042
Aroclor 1260 0.10ND <0.000042
Aroclor 1262 0.10ND <0.000042
Aroclor 1268 0.10ND <0.000042
AR Page 4 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-5
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-05
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015
Aroclor 1016 0.10ND <0.000042
Aroclor 1221 0.10ND <0.000042
Aroclor 1232 0.10ND <0.000042
Aroclor 1242 0.10ND <0.000042
Aroclor 1248 0.101.2 0.00051
Aroclor 1254 0.10ND <0.000042
Aroclor 1260 0.10ND <0.000042
Aroclor 1262 0.10ND <0.000042
Aroclor 1268 0.10ND <0.000042
AR Page 5 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-6
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-06
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015
Aroclor 1016 0.10ND <0.000042
Aroclor 1221 0.10ND <0.000042
Aroclor 1232 0.10ND <0.000042
Aroclor 1242 0.10ND <0.000042
Aroclor 1248 0.101.3 0.00055
Aroclor 1254 0.10ND <0.000042
Aroclor 1260 0.10ND <0.000042
Aroclor 1262 0.10ND <0.000042
Aroclor 1268 0.10ND <0.000042
AR Page 6 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-7
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-07
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015
Aroclor 1016 0.020ND <0.0000083
Aroclor 1221 0.020ND <0.0000083
Aroclor 1232 0.020ND <0.0000083
Aroclor 1242 0.020ND <0.0000083
Aroclor 1248 0.0200.18 0.000076
Aroclor 1254 0.020ND <0.0000083
Aroclor 1260 0.020ND <0.0000083
Aroclor 1262 0.020ND <0.0000083
Aroclor 1268 0.020ND <0.0000083
AR Page 7 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-8
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-08
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015
Aroclor 1016 0.10ND <0.000042
Aroclor 1221 0.10ND <0.000042
Aroclor 1232 0.10ND <0.000042
Aroclor 1242 0.10ND <0.000042
Aroclor 1248 0.100.89 0.00037
Aroclor 1254 0.10ND <0.000042
Aroclor 1260 0.10ND <0.000042
Aroclor 1262 0.10ND <0.000042
Aroclor 1268 0.10ND <0.000042
AR Page 8 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-9
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-09
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015 14:59
Aroclor 1016 0.10ND <0.000042
Aroclor 1221 0.10ND <0.000042
Aroclor 1232 0.10ND <0.000042
Aroclor 1242 0.10ND <0.000042
Aroclor 1248 0.101.8 0.00077
Aroclor 1254 0.10ND <0.000042
Aroclor 1260 0.10ND <0.000042
Aroclor 1262 0.10ND <0.000042
Aroclor 1268 0.10ND <0.000042
AR Page 9 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-10
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-10
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015 15:13
Aroclor 1016 0.020ND <0.0000083
Aroclor 1221 0.020ND <0.0000083
Aroclor 1232 0.020ND <0.0000083
Aroclor 1242 0.020ND <0.0000083
Aroclor 1248 0.0200.17 0.000069
Aroclor 1254 0.020ND <0.0000083
Aroclor 1260 0.020ND <0.0000083
Aroclor 1262 0.020ND <0.0000083
Aroclor 1268 0.020ND <0.0000083
AR Page 10 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:PUF-11
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-11
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015 15:27
Aroclor 1016 0.020ND <0.0000083
Aroclor 1221 0.020ND <0.0000083
Aroclor 1232 0.020ND <0.0000083
Aroclor 1242 0.020ND <0.0000083
Aroclor 1248 0.0200.11 0.000045
Aroclor 1254 0.020ND <0.0000083
Aroclor 1260 0.020ND <0.0000083
Aroclor 1262 0.020ND <0.0000083
Aroclor 1268 0.020ND <0.0000083
AR Page 11 of 12
Note:
Project:Charlette Observer; 199GSG1501
Sample ID:Blank
Collection Date:10/23/2015
Matrix:AIR
Analyses
Client:Cardno Work Order:15101166
Lab ID:15101166-12
ALS Environmental Date:29-Oct-15
Analytical Results
PCBS BY EPA TO-10 ETO10A Analyst:SADMethod:Air Volume (L):2400
µg/sample µg/sample mg/m3
Reporting LimitDate Analyzed:10/28/2015 15:40
Aroclor 1016 0.020ND <0.0000083
Aroclor 1221 0.020ND <0.0000083
Aroclor 1232 0.020ND <0.0000083
Aroclor 1242 0.020ND <0.0000083
Aroclor 1248 0.020ND <0.0000083
Aroclor 1254 0.020ND <0.0000083
Aroclor 1260 0.020ND <0.0000083
Aroclor 1262 0.020ND <0.0000083
Aroclor 1268 0.020ND <0.0000083
AR Page 12 of 12
Note:
Date: 29-Oct-15ALS Environmental
Project:Charlette Observer; 199GSG1501
Client:Cardno
Work Order:15101166 QC BATCH REPORT
Batch ID:2318 Instrument ID GC3 Method:ETO10A
Qual
RPD
Limit
Analysis Date:10/28/2015 12:16 PM
Prep Date:10/26/2015
Analyte Result %REC %RPD
Units:µg/sample
PQL
Client ID:SeqNo:1162542
MBLK
Run ID:GC3_151028A
SPK Val
SPK Ref
Value
RPD Ref
Value
Control
Limit
DF:1
Sample ID:MBLK-2318-2318
Aroclor 1016 0.10ND
Aroclor 1221 0.10ND
Aroclor 1232 0.10ND
Aroclor 1242 0.10ND
Aroclor 1248 0.10ND
Aroclor 1254 0.10ND
Aroclor 1260 0.10ND
Aroclor 1262 0.10ND
Aroclor 1268 0.10ND
000.25 Surr: Decachlorobiphenyl 79.8 41.6-11600.1995
000.25 Surr: Tetrachloro-m-xylene 85.4 45.7-11000.2135
Qual
RPD
Limit
Analysis Date:10/28/2015 12:30 PM
Prep Date:10/26/2015
Analyte Result %REC %RPD
Units:µg/sample
PQL
Client ID:SeqNo:1162543
LCS
Run ID:GC3_151028A
SPK Val
SPK Ref
Value
RPD Ref
Value
Control
Limit
DF:1
Sample ID:LCS-2318-2318
005Aroclor 1260 84.80.104.24
000.25 Surr: Decachlorobiphenyl 80.2 41.6-11600.2005
000.25 Surr: Tetrachloro-m-xylene 84.8 45.7-11000.212
The following samples were analyzed in this batch:15101166-
01A
15101166-
02A
15101166-
03A
15101166-
04A
15101166-
05A
15101166-
06A
15101166-
07A
15101166-
08A
QC Page: 1 of 1
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
ALS Environmental Date: 29-Oct-15
QUALIFIERS,
ACRONYMS, UNITSProject:Charlette Observer; 199GSG1501
Client:Cardno
WorkOrder:15101166
Units Reported Description
Qualifier Description
Acronym Description
µg/sample
Value exceeds Regulatory Limit*
Not accrediteda
Analyte detected in the associated Method Blank above the Reporting LimitB
Value above quantitation rangeE
Analyzed outside of Holding TimeH
Analyte detected below quantitation limitJ
Not offered for accreditationn
Not Detected at the Reporting LimitND
Sample amount is > 4 times amount spikedO
Dual Column results percent difference > 40%P
RPD above laboratory control limitR
Spike Recovery outside laboratory control limitsS
Analyzed but not detected above the MDLU
Method DuplicateDUP
EPA MethodE
Laboratory Control SampleLCS
Laboratory Control Sample DuplicateLCSD
Method BlankMBLK
Method Detection LimitMDL
Method Quantitation LimitMQL
Matrix SpikeMS
Matrix Spike DuplicateMSD
Post Digestion SpikePDS
Practical Quantitaion LimitPQL
Sample Detection LimitSDL
SW-846 MethodSW
QF Page 1 of 1
ALS Environmental
Sample Receipt Checklist
Client Name:CARDNO-CHARLOTTE
Work Order: 15101166
Date/Time Received:24-Oct-15 00:00
Received by:SMS
Checklist completed by
eSignature Date
Reviewed by:
DateeSignature
Matrices:
Carrier name: FedEx
Shipping container/cooler in good condition?Yes No Not Present
Custody seals intact on shipping container/cooler?Yes No Not Present
Custody seals intact on sample bottles?Yes No Not Present
Chain of custody present?Yes No
Chain of custody signed when relinquished and received?Yes No
Chain of custody agrees with sample labels?Yes No
Samples in proper container/bottle?Yes No
Sample containers intact?Yes No
Sufficient sample volume for indicated test?Yes No
All samples received within holding time?Yes No
Container/Temp Blank temperature in compliance?Yes No
Yes No No VOA vials submittedWater - VOA vials have zero headspace?
Water - pH acceptable upon receipt?Yes No N/A
Temperature(s)/Thermometer(s):19.0
Login Notes:
Cooler(s)/Kit(s):
24-Oct-15 26-Oct-15 Shawn Smythe Chris Gibson
pH adjusted?Yes No N/A
pH adjusted by:
CorrectiveAction:
Comments:
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
SRC Page 1 of 1
29-Oct-2015
Cardno
Dave Hunter
Dear Dave,
Re:Charlotte Observer; Project No.: 1996SC1501 Work Order:15101294
Fax:[phone]Tel:[phone]
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
ALS Environmental received 2 samples on 28-Oct-2015 11:07 AM for the analyses presented in the
following report.
Project Manager
Chris Gibson
Chris Gibson
Electronically approved by: Chris Gibson
The analytical data provided relates directly to the samples received by ALS Environmental and for only
the analyses requested.
QC sample results for this data met laboratory specifications. Any exceptions are noted in the Case
Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report
need to be reproduced, it should be reproduced in full unless written approval has been obtained from
ALS Laboratory Group. Samples will be disposed in 30 days unless storage arrangements are made.
The total number of pages in this report is 7.
If you have any questions regarding this report, please feel free to contact me.
Sincerely,
ADDRESS 4388 Glendale Milford Rd Cincinnati, Ohio 45242- | PHONE [phone] | FAX [phone]
ALS GROUP USA, CORP. Part of the ALS Group An ALS Limited Company
Date: 29-Oct-15ALS Environmental
Project:Charlotte Observer; Project No.: 1996SC1501
Client:Cardno
Work Order:15101294 Work Order Sample Summary
Lab Samp ID Client Sample ID Collection DateTag Number Date ReceivedMatrix Hold
15101294-01 PUF-7A Air 10/27/2015 10/28/2015 11:07
15101294-02 Blank Air 10/27/2015 10/28/2015 11:07
SS Page 1 of 1
Date: 29-Oct-15ALS Environmental
Project:Charlotte Observer; Project No.: 1996SC1501
Client:Cardno
Work Order:15101294 Case Narrative
The analytical data provided relates directly to the samples received by ALS Laboratory
Group and for only the analyses requested.
Results relate only to the items tested and are not blank corrected unless indicated.
QC sample results for this data met laboratory specifications. Any exceptions are noted in the
Case Narrative, or noted with qualifiers in the report or QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained from ALS Laboratory Group. Samples will be disposed in 30 days
unless storage arrangements are made.
Compound identification is based upon retention time matching only. Any compound with a
similar retention time will interfere. In the prescence of mutliple aroclors with overlapping or
shared peaks, the dominant discernable pattern will be reported.
CN Page 1 of 1
Project:Charlotte Observer; Project No.: 1996SC1501
Sample ID:PUF-7A
Collection Date:10/27/2015 Matrix:AIR
Analyses Result Qual Units Date Analyzed
Report
Limit
Client:Cardno
Work Order:15101294
Dilution
Factor
Lab ID:15101294-01
ALS Environmental Date:29-Oct-15
PCBS BY EPA TO-10 ETO10A Analyst:SADPrep Date:10/28/2015
Aroclor 1016 10/29/20150.020 µg/sample 1ND
Aroclor 1221 10/29/20150.020 µg/sample 1ND
Aroclor 1232 10/29/20150.020 µg/sample 1ND
Aroclor 1242 10/29/20150.020 µg/sample 1ND
Aroclor 1248 10/29/20150.020 µg/sample 11.0
Aroclor 1254 10/29/20150.020 µg/sample 1ND
Aroclor 1260 10/29/20150.020 µg/sample 1ND
Aroclor 1262 10/29/20150.020 µg/sample 1ND
Aroclor 1268 10/29/20150.020 µg/sample 1ND
Surr: Decachlorobiphenyl 10/29/201541.4-116 %REC 182.4
Surr: Tetrachloro-m-xylene 10/29/201545.7-110 %REC 194.0
AR Page 1 of 2
Note:
Project:Charlotte Observer; Project No.: 1996SC1501
Sample ID:Blank
Collection Date:10/27/2015 Matrix:AIR
Analyses Result Qual Units Date Analyzed
Report
Limit
Client:Cardno
Work Order:15101294
Dilution
Factor
Lab ID:15101294-02
ALS Environmental Date:29-Oct-15
PCBS BY EPA TO-10 ETO10A Analyst:SADPrep Date:10/28/2015
Aroclor 1016 10/29/20150.020 µg/sample 1ND
Aroclor 1221 10/29/20150.020 µg/sample 1ND
Aroclor 1232 10/29/20150.020 µg/sample 1ND
Aroclor 1242 10/29/20150.020 µg/sample 1ND
Aroclor 1248 10/29/20150.020 µg/sample 1ND
Aroclor 1254 10/29/20150.020 µg/sample 1ND
Aroclor 1260 10/29/20150.020 µg/sample 1ND
Aroclor 1262 10/29/20150.020 µg/sample 1ND
Aroclor 1268 10/29/20150.020 µg/sample 1ND
Surr: Decachlorobiphenyl 10/29/201541.4-116 %REC 170.9
Surr: Tetrachloro-m-xylene 10/29/201545.7-110 %REC 160.2
AR Page 2 of 2
Note:
ALS Environmental Date: 29-Oct-15
QUALIFIERS,
ACRONYMS, UNITSProject:Charlotte Observer; Project No.: 1996SC1501
Client:Cardno
WorkOrder:15101294
Units Reported Description
Qualifier Description
Acronym Description
µg/sample
Value exceeds Regulatory Limit*
Not accrediteda
Analyte detected in the associated Method Blank above the Reporting LimitB
Value above quantitation rangeE
Analyzed outside of Holding TimeH
Analyte detected below quantitation limitJ
Not offered for accreditationn
Not Detected at the Reporting LimitND
Sample amount is > 4 times amount spikedO
Dual Column results percent difference > 40%P
RPD above laboratory control limitR
Spike Recovery outside laboratory control limitsS
Analyzed but not detected above the MDLU
Method DuplicateDUP
EPA MethodE
Laboratory Control SampleLCS
Laboratory Control Sample DuplicateLCSD
Method BlankMBLK
Method Detection LimitMDL
Method Quantitation LimitMQL
Matrix SpikeMS
Matrix Spike DuplicateMSD
Post Digestion SpikePDS
Practical Quantitaion LimitPQL
Sample Detection LimitSDL
SW-846 MethodSW
QF Page 1 of 1
ALS Environmental
Sample Receipt Checklist
Client Name:CARDNO-CHARLOTTE
Work Order: 15101294
Date/Time Received:28-Oct-15 11:07
Received by: SNH
Checklist completed by
eSignature Date
Reviewed by:
DateeSignature
Matrices:
Carrier name: FedEx
Shipping container/cooler in good condition?Yes No Not Present
Custody seals intact on shipping container/cooler?Yes No Not Present
Custody seals intact on sample bottles?Yes No Not Present
Chain of custody present?Yes No
Chain of custody signed when relinquished and received?Yes No
Chain of custody agrees with sample labels?Yes No
Samples in proper container/bottle?Yes No
Sample containers intact?Yes No
Sufficient sample volume for indicated test?Yes No
All samples received within holding time?Yes No
Container/Temp Blank temperature in compliance?Yes No
Yes No No VOA vials submittedWater - VOA vials have zero headspace?
Water - pH acceptable upon receipt?Yes No N/A
Temperature(s)/Thermometer(s):
Login Notes:
Cooler(s)/Kit(s):
28-Oct-15 29-Oct-15 Jan Wilcox Chris Gibson
pH adjusted?Yes No N/A
pH adjusted by:
CorrectiveAction:
Comments:
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
SRC Page 1 of 1

ATTACHMENT 4
ASSUMPTIONS AND LIMITATIONS

The Charlotte Observer
PCB Assessment Summary Report
December 7, 2015

ASSUMPTIONS AND LIMITATIONS

The results, findings, conclusions, and recommendations expressed in this report are based only on
conditions that were noted during Cardno’s survey of the Charlotte Observer Building site at 600 South
Tryon Street in Charlotte, North Carolina. The site survey area includes a warehouse, with address 620 South
Poplar Street that is connected to the Charlotte Observer Building by a basement tunnel that crosses under
South Church Street. The site infrastructure was surveyed for PCBs in caulk or similar materials on July 13
and 14, September 30, October 1, 22, and 27, 2015. PCB samples were collected from air at the facility on
October 23 and 27, 2015, and PCBs were analyzed from waste materials, concrete floor slabs, and one
elevator hydraulic reservoir on July 13, 2015.

The selection of sample locations and frequency of sampling was based on Cardno’s observations and
the assumption that like materials in the same area are similar in content. PCBs may exist in areas or
materials that were not investigated or identified. Additional PCBs may also be present on site in
inaccessible or concealed spaces. If future maintenance/renovation/demolition activities make these
areas accessible, Cardno recommends that a thorough assessment of these spaces be conducted at that
time to identify and confirm the presence or absence of additional PCBs. Until then, such unidentified
materials that could contain PCBs should be treated as assumed PCBs in accordance with applicable
regulations.

The report is designed to aid the client in understanding the extent of PCB issues as they pertain to the
planned redevelopment of the site. Under no circumstances is the report to be utilized as a bidding
document or as a project specification document. The document does not have the components
required to serve as a PCB Management Plan. Contractors should rely on their own
determinations of quantities and actions necessary for proper abatement.

Our professional services have been performed, our findings obtained, and our conclusions and
recommendations prepared in accordance with customary principles and practices in the consulting fields of
environmental science and engineering. This statement is in lieu of other statements either expressed or
implied. This report does not warrant against future operations or conditions, nor does it warrant against
operations or conditions present of a type or at a location not investigated. Cardno ATC assumes no
responsibility for the investigation, remediation, abatement, or other potential liabilities associated with
environmental impact at, or from, the project site or structure, regardless of the date of occurrence.