HomeMy WebLinkAbout20074_E 7th Street_PRII_20160608
SUMMIT Engineering, Laboratory & Testing, Inc. 3575 Centre Circle
Fort Mill, South Carolina 29715
www.SUMMIT-companies.com Phone: (704) 504-1717
Fax: (704) 504-1125
June 8, 2016
Will Andrews
Proffitt Dixon Partners
1355 Greenwood Cliff, Suite 150
Charlotte, NC 28204
Subject: Limited Phase II Environmental Site Assessment
Proposed Charlotte Self-Storage
E. 7th Street Charlotte, Mecklenburg County, North Carolina
SUMMIT Project No. 3586.11
Dear Mr. Andrews:
SUMMIT ENGINEERING, LABRATORY & TESTING, INC. (SUMMIT) is pleased to submit the
following report of our Limited Phase II Environmental Site Assessment (ESA) of the Proposed
Charlotte Self-Storage property, located in Charlotte, Mecklenburg County, North Carolina
(Mecklenburg County Parcel ID: 08010175).
This report includes a description of the methodology of our investigation and a summary of our
findings and conclusions. If you have any questions regarding our assessment of the subject
property or our conclusions, please do not hesitate to call us at (704) 504-1717.
Sincerely,
SUMMIT
Patrick W. Lowery, LG Michael D. Zavislak, NRCC-EAC, CIH, PE
Senior Environmental Manager Environmental Department Manager
NC LG No: 2421
SUMMIT’s NC Engineering Firm License No. C-2530
LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT
PROPOSED CHARLOTTE SELF-STORAGE
CHARLOTTE
MECKLENBURG COUNTY
NORTH CAROLINA SUMMIT PROJECT NO. 3586.11
Prepared For:
Proffitt Dixon Partners
1355 Greenwood Cliff, Suite 150
Charlotte, NC 28204
Prepared By:
SUMMIT ENGINEERING, LABRATORY & TESTING, Inc.
3575 Centre Circle
Fort Mill, South Carolina 29715
704-504-1717
June 8, 2016
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina June 8, 2016
E:\Project Forms\Projects\3586.11 Charlote Self-Storage - Phase II\3586.11 Proposed Charlotte Self-Storage - Phase II ESA.doc i
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY ...................................................................................................... 1
2.0 INTRODUCTION .................................................................................................................... 2
2.1. PURPOSE .......................................................................................................................................... 2
2.2. SITE DESCRIPTION ........................................................................................................................ 2
2.3. ASSESSMENT HISTORY ................................................................................................................ 2
2.4. WORK PLAN OBJECTIVES ........................................................................................................... 3
3.0 PROPERTY SETTING ............................................................................................................ 4
3.1. TOPOGRAPHIC SETTING.............................................................................................................. 4
3.2. GEOLOGIC SETTING ..................................................................................................................... 4
3.3. HYDROLOGIC SETTING ............................................................................................................... 5
4.0 SUMMARY OF PHASE II ACTIVITIES................................................................................ 6
4.1. DRILLING ACTIVITES AND METHODS ..................................................................................... 6
4.2. SAMPLING ....................................................................................................................................... 7
4.3. PACKING AND SHIPMENT ........................................................................................................... 7
4.4. SAMPLING POINT ABANDONMENT ......................................................................................... 7
5.0 SUMMARY OF LABORATORY ANALYSIS ........................................................................ 8
6.0 FINDINGS & CONCLUSIONS .............................................................................................. 9
7.0 RECOMMENDATIONS ........................................................................................................ 10
8.0 QUALIFICATION OF REPORT ........................................................................................... 11
9.0 ADDITIONAL SERVICES .................................................................................................... 12
10.0 REFERENCES ....................................................................................................................... 13
APPENDICES
Appendix I: FIGURES
Appendix II: ANALYTICAL SUMMARY
Appendix III: ANALYTICAL RESULTS
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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1.0 EXECUTIVE SUMMARY
In summary, three (3) soil samples and two (2) groundwater samples were collected from locations
on-site identified to represent the highest potential for impact. TMW-1/SB-1 and TMW-2/SB-2
were completed along the sites northwestern boundary, adjacent to the approximate location of a
former dry cleaning and dye plant facility that operated from the 1920s to the 1960s when it was
destroyed by fire. TMW-3/SB-3 was collected adjacent to the southeastern boundary at a
downgradient location from TMW-1 and TMW-2. TMW-3 did not yield groundwater for collection
of a sample following installation. This sampling scope of services was completed to determine if
former historical use of the northwestern adjoining property and further upgradient properties had
impacted the subject site. All soil and groundwater samples were analyzed for the presence of
Volatile Organic Compounds (VOCs) by EPA method 8260.
Soils collected from SB-2 and groundwater collected from TMW-1 detected the presence of
Tetrachloroethene (PCE), above established regulatory standards. Acetone was detected within
soils from SB-1 and SB-3 below regulatory standards. Acetone is considered to be a result of the
breakdown of organic matter in soils and not an environmental condition. No other constituents
were identified above laboratory detection limits in all collected samples.
Based on the results of this assessment, SUMMIT concludes that the dry cleaning and dye plant
formerly located adjacent to the subject sites northwestern boundary has impacted the site soils and
groundwater.
Based on SUMMITs understanding of the intended use of the property, the presence of the
identified environmental conditions present at the site as result of an off-site source, should not
inhibit the planned development unless dewatering is required or additional soil impacts are
discovered. SUMMIT recommends the perspective purchaser of the property consult with counsel
or other entities to review the potential regulatory or finical liabilities related to the presence of
environmental conditions identified within this assessment. A copy of the Limited Phase II ESA
analysis and should be submitted to North Carolina Department of Environment Quality.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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2.0 INTRODUCTION
2.1. PURPOSE
SUMMIT was retained by Proffitt Dixon Partners to perform a Limited Phase II ESA of the
Proposed Charlotte Self-Storage in Charlotte, Mecklenburg County, North Carolina (Mecklenburg
County Tax ID: 08010175). The Limited Phase II ESA was requested in order to assess
environmental concerns identified in a Phase I ESA, performed by SUMMIT ELT, Inc, dated May
3, 2016. This report presents the results of our Limited Phase II ESA of the Proposed Charlotte
Self-Storage.
2.2. SITE DESCRIPTION
The subject site is located along eastern side of E. 7th Street, 300 feet south of its intersection with
N. McDowell Street in Charlotte, Mecklenburg County, North Carolina. The site is an irregular in
shaped 1.062 acre tract of undeveloped land in Charlotte, North Carolina. The site is partially
wooded and overgrown with brush. The site abuts US I-277 and various US I-277 on/off ramps to
the south. Sugar Creek is located beyond US I-277 to the south. Multiple stormwater structures are
located on the site, discharging stormwater through the site from up-gradient properties. The site is
currently serviced by municipal water and sewer service, electrical services, cable, telephone, etc.
Refer to the Site Plan shown in Figure 2 of Appendix I for the location of the subject property.
2.3. ASSESSMENT HISTORY
SUMMIT completed a Phase I ESA, dated May 3, 2016 for the subject site. The following
Recognized Environmental Conditions (RECs) were identified in the Phase I ESA:
• Historical review of the nearby and adjoining properties identified a dry cleaning
and dyeing plant facility located adjacent to the subject site in the 1929 through
1963 sanborn maps. Non-ASTM records confirmed the presence of Arrow
Laundry and Cleaners, and Rosenberg’s Laundry with the same physical addresses
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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as identified in the sanborn maps. Sanborn maps depict a “Solvent Tk” area at the
facility. The facility was depicted as destroyed by fire in the 1963 sanborn map.
The presence of the dry cleaning and dyeing facility located adjacent and up-
upgradient to the site represented an REC at the time of the Phase I ESA.
• Multiple historical dry cleaning facilities and gasoline filling stations were
identified as being located in close proximity and up-gradient to the subject site.
The historical use of up-gradient properties represented an REC at the time of the
Phase I ESA.
No other site specific or surrounding area assessment history is known at the time of this report.
2.4. WORK PLAN OBJECTIVES
SUMMIT proposed to perform a Limited Phase II ESA according to our understanding of the most
likely potential for impact, in general accordance with ASTM E1903, and in accordance with the
USEPA Field Branches Quality System and Technical Procedures Manual. The proposed scope of
services included the completion of three (3) soil borings and three (3) temporary monitoring wells
(TMW) in order to assess the soil and groundwater quality at the subject site. The proposed
sampling locations were placed in accessible locations and in areas that represented the highest
potential for on-site impacts. All samples collected f were scheduled to be relinquished to a NC
certified laboratory for analysis of Volatile Organic Compounds by EPA method 8260.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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3.0 PROPERTY SETTING
3.1. TOPOGRAPHIC SETTING
The United States Geological Survey (USGS) “Charlotte East” 7.5 minute topographic quadrangle
map was reviewed. According to the contour lines on the topographic map, the elevation of the
subject site ranges from approximately 660 feet to approximately 640 feet above Mean Sea Level
(MSL). The contour lines indicate the general direction of downward slope is to the southeast
towards Little Sugar Creek that flows south into Sugar Creek and then into the Catawba River near
Goat Island. Refer to Figure 1 in Appendix I of this report.
3.2. GEOLOGIC SETTING
The property is located in Mecklenburg County, North Carolina, which is located in the south
central Piedmont Physiographic Province. The Piedmont Province generally consists of well-
rounded hills and ridges which are dissected by a well-developed system of draws and streams. The
Piedmont Province is predominantly underlain by metamorphic rock (formed by heat, pressure
and/or chemical action) and igneous rock (formed directly from molten material) which were
initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks
deposited in the Piedmont Province during the Precambrian era were the host from the
metamorphism and were changed to gneiss and schist. The more recent Paleozoic era had periods
of igneous emplacement, with at least episodes of regional metamorphism resulting in the majority
of the rock types seen today.
The topography and relief of the Piedmont Province has developed from differential weathering of
the igneous and metamorphic rock. Ridges and hills have been developed on the more easily
weathered and erodible rock. Because of the continued chemical and physical weathering, the
rocks in the Piedmont Province are now generally covered with a mantle of soil that has weathered
in place from the parent bedrock. These soils vary in thickness and are referred to as residuum or
residual soils. The residuum is typically finer grained and has higher clay content near the surface
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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because of the advanced weathering. Similarly, the soils typically become coarser grained with
increasing depth because of decreased weathering. As the weathering decreases, the residual soils
generally retain the overall appearance, texture, gradation and foliations of the parent rock.
3.3. HYDROLOGIC SETTING
Based on a review of the United States Geological Survey (USGS) “Charlotte East” quadrangle
topographic map, inferred groundwater flow direction based on topography appears to be to the
southeast towards Little Sugar Creek. Refer to Figure 1 in Appendix I for a topographic map for the
subject property.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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4.0 SUMMARY OF PHASE II ACTIVITIES
4.1. DRILLING ACTIVITES AND METHODS
On May 25, 2016, SUMMIT personnel conducted the field activities scope of the Limited Phase II
ESA. The three (3) proposed temporary monitoring well (TMW) locations were placed in
accessible locations along the northwestern site boundary adjacent to the previously identified dry
cleaning and dying plant and near the southeastern boundary. Three (3) soil samples were collected
from the subsurface soils at each TMW location. The sampling locations can be viewed on the
attached Sampling Location Map, Figure 3, in appendix I.
SUMMIT utilized a hollow stem auger (HSA) drill rig to complete the soil borings and install the
temporary monitoring wells. At each sampling location the boring was advanced with HSA. Soils
were collected in 2 ft intervals utilizing a decontaminated split spoon sampler. The soil interval of
2-4 ft below ground surface (bgs) was selected for analysis for this assessment. Following the
collection of the soil sample, the boring was advanced into the groundwater table for collection of
groundwater samples. New 1 inch slotted well screen was inserted into the borehole with filter
pack sand added through the HSA drill string. The HSA drill string was removed and the temporary
well sampled utilizing a new disposable groundwater bailer. TMW-1 and TMW-2 were completed
to a depth of 30 ft bgs. TMW-3 was advanced to refusal depths 16 ft bgs. The bore hole was off-
set multiple times, encountering refusal on competent rock each time at depths of 16-18 ft bgs.
DTW was measured in each well prior to sampling. Each boring generally encountered six (6)
inches of surface material and subgrade followed by tan/orange fine to medium grained clayey sand
with mica to termination depths.
Upon completion of the drilling activities, the drilling equipment was decontaminated by the well
driller by use of a steam cleaner or Alconox and tap water wash, tap water rinse, isopropanol rinse
(sampling equipment), and deionized water rinse. Decontamination of the drilling equipment was
performed prior to starting drilling activities, and upon the completion of drilling activities at each
boring/well location.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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4.2. SAMPLING
Soils were collected in one (2) ft intervals to a depth of five (5) ft bgs at each location. The soil
intervals were field screened utilizing a PID and the interval displaying the highest reading was
planned for analysis. Additionally visual and olfactory observations were recorded for each
interval. No odors or staining was observed in SB-1 through SB-3. Additionally no PID readings
were recorded. Therefore, soils from the 2-4 ft bgs interval were collected for analysis of Volatile
Organic Compounds by EPA Method 8260B.
Groundwater was encountered in TMW-1 and TMW-2 at 24 ft and 25 ft bgs respectively.
Groundwater was not encountered within TMW-3 during this assessment. Groundwater samples
were collected utilizing new disposable bailers. Grab samples were collected in the laboratory
provided vials and jars. A copy of the analysis and chains of custody are included in Appendix III
of this report.
4.3. PACKING AND SHIPMENT
Upon securing the samples in laboratory provided containers, the vial and jar lids were tightly
fastened, and the jars encapsulated in shock-resistant plastic bags. The samples and ice were
double-bagged in large plastic bags, tied off with rubber bands, and packed into a cooler. The
samples were delivered to Shealy Environmental Services, Inc, in West Columbia, SC. The vials
and jars used for the collection of the samples at this site were prepared by Shealy, and were pre-
labeled and contained analyte-appropriate preservatives. A listing of the preservatives in the sample
containers utilized for the collection of the samples at this site are cataloged in the Chain-Of-
Custody record, attached in Appendix III of this report. The secured samples were relinquished to
laboratory on May 26, 2016 for laboratory analysis.
4.4. SAMPLING POINT ABANDONMENT
All boreholes were abandoned the same day by the certified well driller.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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5.0 SUMMARY OF LABORATORY ANALYSIS
All samples were relinquished to Shealy Environmental Services on May 26, 2016 for the prescribe
analysis. Table 1 in Appendix II of this report summarizes all detections. The analytical detections
are summarized below:
• Tetrachloroethene (PCE) was detected in soils collected from SB-2 at a concentration of
0.0065 mg/Kg, above the April 2016, North Carolina Inactive Hazardous Site Branch
(IHSB) Preliminary Soil Remediation Goal (PSRG) Protection to Groundwater standard of
0.005 mg/Kg. The detection in SB-2 was below the IHSB Residential PSRG concentration
of 16,200 mg/Kg.
• Acetone was detected in soils collected from SB-1 and SB-3 at concentrations of 0.091
mg/Kg and 0.058 mg/Kg respectively, below the NC IHSB Protection to Groundwater
PSRG of 24 mg/Kg. Acetone is likely present in the analysis due to a breakdown of organic
matter in the subsurface soils and is not considered an environmental impact at the time of
this report.
• Tetrachloroethene (PCE) was detected in groundwater collected from TMW-1 at a
concentration of 25 ug/L, above the North Carolina groundwater quality standard
concentration of 0.7 ug/L, established by 15A NCAC 2L regulations.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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6.0 FINDINGS & CONCLUSIONS
In summary, three (3) soil samples and two (2) groundwater samples were collected from locations
on-site identified to represent the highest potential for impact. TMW-1/SB-1 and TMW-2/SB-2
were completed along the sites northwestern boundary, adjacent to the approximate location of a
former dry cleaning and dye plant facility that operated from the 1920s to the 1960s when it was
destroyed by fire. TMW-3/SB-3 was collected adjacent to the southeastern boundary at a
downgradient location from TMW-1 and TMW-2. TMW-3 did not yield groundwater for collection
of a sample following installation. This sampling scope of services was completed to determine if
former historical use of the northwestern adjoining property and further upgradient properties had
impacted the subject site. All soil and groundwater samples were analyzed for the presence of
Volat ile Organic Compounds (VOCs) by EPA method 8260.
Soils collected from SB-2 and groundwater collected from TMW-1 detected the presence of
Tetrachloroethene (PCE), above established regulatory standards. Acetone was detected within
soils from SB-1 and SB-3 below regulatory standards. Acetone is considered to be a result of the
breakdown of organic matter in soils and not an environmental condition. No other constituents
were identified above laboratory detection limits in all collected samples.
Based on the results of this assessment, SUMMIT concludes that the dry cleaning and dye plant
formerly located adjacent to the subject sites northwestern boundary has impacted the site soils and
groundwater.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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7.0 RECOMMENDATIONS
Based on SUMMITs understanding of the intended use of the property, the presence of the
identified environmental conditions present at the site as result of an off-site source, should not
inhibit the planned development unless dewatering is required or additional soil impacts are
discovered. SUMMIT recommends the perspective purchaser of the property consult with counsel
or other entities to review the potential regulatory or finical liabilities related to the presence of
environmental conditions identified within this assessment. A copy of the Limited Phase II ESA
analysis and should be submitted to North Carolina Department of Environment Quality.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
E:\Project Forms\Projects\3586.11 Charlote Self-Storage - Phase II\3586.11 Proposed Charlotte Self-Storage - Phase II ESA.doc 11
8.0 QUALIFICATION OF REPORT
The Limited Phase II ESA was performed in general accordance with ASTM E1903, and in
accordance with the USEPA Field Branches Quality System and Technical Procedures Manual. The
findings detailed in this report are specific to the conditions in the immediate vicinity of the sample
locations for this particular project.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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9.0 ADDITIONAL SERVICES
This report does not include any environmental assessment of surface water, the determination of
wetlands, the determination of noise impact, the assessment of air quality, the identification of
cultural resources, or the identification of endangered species. These services are beyond the scope
of services of this limited sampling and analysis.
No additional services were provided.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina June 8, 2016
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10.0 REFERENCES
Phase I ESA Report, Charlotte Self-Storage, by SUMMIT ELT, Inc, dated May 3, 2016.
United States Geological Survey (USGS) 7.5 minute Topographic Map of the Charlotte East
topographic Quadrangle, Delorme 2002.
United States Department of Agriculture (USDA) Soil Conservation Service, Web Soil Survey
http://websoilsurvey.sc.egov.usda.gov/App/WebSoilSurvey.aspx
Mecklenburg County Polaris3 GIS –
http://polaris3g.mecklenburgcountync.gov/
EPA National Primary Drinking Water Regulations -
http://water.epa.gov/drink/contaminants/index.cfm
15A NCAC 2L Standards –
http://portal.ncdenr.org/web/wq/ps/csu/gwstandards
EPA Regional Screening Levels –
http://www.epa.gov/region9/superfund/prg/
North Carolina Maximum Soil Contaminant Concentrations –
http://portal.ncdenr.org/web/wm/ust/guidance
North Carolina Inactive Hazardous Site Branch, Preliminary Remediation Goals Table HTTPS://NCDENR.S3.AMAZONAWS.COM/S3FS-
PUBLIC/WASTE%20MANAGEMENT/DWM/SF/IHS/GUIDANCE/SOILTABLE%20APRIL%202016%20-FINAL-1PCB1.PDF
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina June 8, 2016
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APPENDIX I
FIGURES
Image Provided By EDR USGS Topographic Maps
Boundaries are approximate
TOPOGRAPHIC MAP
5/3/2016
Charlotte, North Carolina 28204
E 7th St
Charlotte Self-Storage
Source:Mecklenburg GIS Prepared By\Date:PL/06/16
Checked By\Date:MZ/06/16
Scale
Figure 2Charlotte, NC 28204
Site Location Map
NTS
Proffit Dixon Partners
Charlotte, NC
Proposed Charlotte Self-Storgae
E. 7th Street
1355 Greenwood Cliff, Suite 150
N
Subject Site
Source:Mecklenburg GIS Prepared By\Date:PL/06/16
Checked By\Date:MZ/06/16
Scale
Figure 2
1355 Greenwood Cliff, Suite 150 As Shown
Charlotte, NC 28204
Sampling Location Map
Proposed Charlotte Self-Storgae
E. 7th Street
Charlotte, NC
Proffit Dixon Partners
N
KEY
Groundwater Sample -TMW
Soil Sample
TMW-1/SB-1
TMW-2/BS-2
TMW-3/SB-3
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina June 8, 2016
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APPENDIX II
ANALYTICAL SUMMARY
Proposed Charlotte Self-Storage 6/8/2016
E. 7th Street SUMMIT Project #: 3586.11
Sample ID Collected Date Matrix Parameter Results Units
NC IHSB Protection of
Groundwater PSRGs
NC IHSB Residential
PSRGs
NC 2L Groundwater
Standards
SB-1 5/25/2016 Soil Acetone 0.091 mg/kg 24 12,200,000 -
SB-2 5/25/2016 Soil Tetrachloroethene 0.0065 mg/kg 0.005 16,200 -
SB-3 5/25/2016 Soil Acetone 0.085 mg/kg 24 12,200,000 -
TMW-1 5/25/2016 GW Tetrachloroethene 25 ug/L --0.7
TMW-2 5/25/2016 GW VOCs ND ug/L --NA
TMW-3 5/25/2016 NS NS NS ug/L --NS
Notes:
1) ND - Non Detect 4) Soil samples compared to April 2016 NC IHSB PSRG
2) NS - Not Sampled 5) Groundwater samples compared to NC 2L Standards
Table 1.0 Summary of Analytical Detections
3) Bolded items exceeded established regulatory concentrations.
Limited Phase II ESA – Proposed Charlotte Self-Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina June 8, 2016
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APPENDIX III
ANALYTICAL RESULTS
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Summit Engineering and Construction Services, Inc.
3575 Centre Circle
Fort Mill, SC 28715
Attention: Patrick Lowery
RE26007Lot Number:
3586.10Project Number:
Self StorageProject Name:
06/02/2016Date Completed:
Lucas Odom
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Summit Engineering and Construction Services, Inc.
Lot Number: RE26007
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
VOCs by GC/MS
Due to excessive sediment in sample -001, it has been analyzed at a 5X dilution.
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Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Summit Engineering and Construction Services, Inc.
Lot Number: RE26007
Sample Number Sample ID Matrix Date Sampled Date Received
001 05/25/2016 1130TMW-1 Aqueous 05/26/2016
002 05/25/2016 1300TMW-2 Aqueous 05/26/2016
003 05/25/2016 1110SB-1 Solid 05/26/2016
004 05/25/2016 1240SB-2 Solid 05/26/2016
005 05/25/2016 1330SB-3 Solid 05/26/2016
(5 samples)
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Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Summit Engineering and Construction Services, Inc.
Lot Number: RE26007
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 TMW-1 Aqueous Tetrachloroethene 8260B 25 ug/L 5
003 SB-1 Solid Acetone 8260B 91 ug/kg 9
004 SB-2 Solid Tetrachloroethene 8260B 6.5 ug/kg 11
005 SB-3 Solid Acetone 8260B 85 ug/kg 13
(4 detections)
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Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
TMW-1
RE26007-001
05/25/2016 1130
05/26/2016
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 5 05/28/2016 0357 ECP 14340
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L100
Benzene 71-43-2 8260B ND 1ug/L25
Bromodichloromethane 75-27-4 8260B ND 1ug/L25
Bromoform 75-25-2 8260B ND 1ug/L25
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L25
2-Butanone (MEK)78-93-3 8260B ND 1ug/L50
Carbon disulfide 75-15-0 8260B ND 1ug/L25
Carbon tetrachloride 56-23-5 8260B ND 1ug/L25
Chlorobenzene 108-90-7 8260B ND 1ug/L25
Chloroethane 75-00-3 8260B ND 1ug/L25
Chloroform 67-66-3 8260B ND 1ug/L25
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L25
Cyclohexane 110-82-7 8260B ND 1ug/L25
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L25
Dibromochloromethane 124-48-1 8260B ND 1ug/L25
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L25
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L25
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L25
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L25
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L25
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L25
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L25
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L25
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L25
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L25
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L25
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L25
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L25
Ethylbenzene 100-41-4 8260B ND 1ug/L25
2-Hexanone 591-78-6 8260B ND 1ug/L50
Isopropylbenzene 98-82-8 8260B ND 1ug/L25
Methyl acetate 79-20-9 8260B ND 1ug/L25
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L25
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L50
Methylcyclohexane 108-87-2 8260B ND 1ug/L25
Methylene chloride 75-09-2 8260B ND 1ug/L25
Styrene 100-42-5 8260B ND 1ug/L25
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L25
Tetrachloroethene 127-18-4 8260B 25 1ug/L25
Toluene 108-88-3 8260B ND 1ug/L25
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
TMW-1
RE26007-001
05/25/2016 1130
05/26/2016
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 5 05/28/2016 0357 ECP 14340
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L25
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L25
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L25
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L25
Trichloroethene 79-01-6 8260B ND 1ug/L25
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L25
Vinyl chloride 75-01-4 8260B ND 1ug/L10
Xylenes (total)1330-20-7 8260B ND 1ug/L25
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
TMW-2
RE26007-002
05/25/2016 1300
05/26/2016
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/28/2016 0420 ECP 14340
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L5.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L5.0
Bromoform 75-25-2 8260B ND 1ug/L5.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L5.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L5.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L5.0
Chlorobenzene 108-90-7 8260B ND 1ug/L5.0
Chloroethane 75-00-3 8260B ND 1ug/L5.0
Chloroform 67-66-3 8260B ND 1ug/L5.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L5.0
Cyclohexane 110-82-7 8260B ND 1ug/L5.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L5.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L5.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L5.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L5.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L5.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L5.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L5.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L5.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L5.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L5.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L5.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L5.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L5.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L5.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L5.0
Ethylbenzene 100-41-4 8260B ND 1ug/L5.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L5.0
Methyl acetate 79-20-9 8260B ND 1ug/L5.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L5.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L5.0
Styrene 100-42-5 8260B ND 1ug/L5.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L5.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L5.0
Toluene 108-88-3 8260B ND 1ug/L5.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
TMW-2
RE26007-002
05/25/2016 1300
05/26/2016
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/28/2016 0420 ECP 14340
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L5.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L5.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L5.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L5.0
Trichloroethene 79-01-6 8260B ND 1ug/L5.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L5.0
Vinyl chloride 75-01-4 8260B ND 1ug/L2.0
Xylenes (total)1330-20-7 8260B ND 1ug/L5.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 101 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1
RE26007-003
05/25/2016 1110
05/26/2016
Solid
% Solids:77.2 05/26/2016 2305
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 06/01/2016 1553 SES 14513 5.16
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B 91 1ug/kg25
Benzene 71-43-2 8260B ND 1ug/kg6.3
Bromodichloromethane 75-27-4 8260B ND 1ug/kg6.3
Bromoform 75-25-2 8260B ND 1ug/kg6.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg6.3
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg13
Carbon disulfide 75-15-0 8260B ND 1ug/kg6.3
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg6.3
Chlorobenzene 108-90-7 8260B ND 1ug/kg6.3
Chloroethane 75-00-3 8260B ND 1ug/kg6.3
Chloroform 67-66-3 8260B ND 1ug/kg6.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg6.3
Cyclohexane 110-82-7 8260B ND 1ug/kg6.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg6.3
Dibromochloromethane 124-48-1 8260B ND 1ug/kg6.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg6.3
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg6.3
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg6.3
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg6.3
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg6.3
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg6.3
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg6.3
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg6.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg6.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg6.3
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg6.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg6.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg6.3
Ethylbenzene 100-41-4 8260B ND 1ug/kg6.3
2-Hexanone 591-78-6 8260B ND 1ug/kg13
Isopropylbenzene 98-82-8 8260B ND 1ug/kg6.3
Methyl acetate 79-20-9 8260B ND 1ug/kg6.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg6.3
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg13
Methylcyclohexane 108-87-2 8260B ND 1ug/kg6.3
Methylene chloride 75-09-2 8260B ND 1ug/kg6.3
Styrene 100-42-5 8260B ND 1ug/kg6.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg6.3
Tetrachloroethene 127-18-4 8260B ND 1ug/kg6.3
Toluene 108-88-3 8260B ND 1ug/kg6.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1
RE26007-003
05/25/2016 1110
05/26/2016
Solid
% Solids:77.2 05/26/2016 2305
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 06/01/2016 1553 SES 14513 5.16
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg6.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg6.3
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg6.3
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg6.3
Trichloroethene 79-01-6 8260B ND 1ug/kg6.3
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg6.3
Vinyl chloride 75-01-4 8260B ND 1ug/kg6.3
Xylenes (total)1330-20-7 8260B ND 1ug/kg6.3
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 93 53-142
Bromofluorobenzene 100 47-138
Toluene-d8 102 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-2
RE26007-004
05/25/2016 1240
05/26/2016
Solid
% Solids:85.4 05/26/2016 2305
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 06/01/2016 1917 SES 14513 4.50
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 2ug/kg26
Benzene 71-43-2 8260B ND 2ug/kg6.5
Bromodichloromethane 75-27-4 8260B ND 2ug/kg6.5
Bromoform 75-25-2 8260B ND 2ug/kg6.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg6.5
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg13
Carbon disulfide 75-15-0 8260B ND 2ug/kg6.5
Carbon tetrachloride 56-23-5 8260B ND 2ug/kg6.5
Chlorobenzene 108-90-7 8260B ND 2ug/kg6.5
Chloroethane 75-00-3 8260B ND 2ug/kg6.5
Chloroform 67-66-3 8260B ND 2ug/kg6.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg6.5
Cyclohexane 110-82-7 8260B ND 2ug/kg6.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 2ug/kg6.5
Dibromochloromethane 124-48-1 8260B ND 2ug/kg6.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg6.5
1,2-Dichlorobenzene 95-50-1 8260B ND 2ug/kg6.5
1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg6.5
1,4-Dichlorobenzene 106-46-7 8260B ND 2ug/kg6.5
Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg6.5
1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg6.5
1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg6.5
1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg6.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg6.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg6.5
1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg6.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg6.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg6.5
Ethylbenzene 100-41-4 8260B ND 2ug/kg6.5
2-Hexanone 591-78-6 8260B ND 2ug/kg13
Isopropylbenzene 98-82-8 8260B ND 2ug/kg6.5
Methyl acetate 79-20-9 8260B ND 2ug/kg6.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 2ug/kg6.5
4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg13
Methylcyclohexane 108-87-2 8260B ND 2ug/kg6.5
Methylene chloride 75-09-2 8260B ND 2ug/kg6.5
Styrene 100-42-5 8260B ND 2ug/kg6.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg6.5
Tetrachloroethene 127-18-4 8260B 6.5 2ug/kg6.5
Toluene 108-88-3 8260B ND 2ug/kg6.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-2
RE26007-004
05/25/2016 1240
05/26/2016
Solid
% Solids:85.4 05/26/2016 2305
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 06/01/2016 1917 SES 14513 4.50
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 2ug/kg6.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg6.5
1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg6.5
1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg6.5
Trichloroethene 79-01-6 8260B ND 2ug/kg6.5
Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg6.5
Vinyl chloride 75-01-4 8260B ND 2ug/kg6.5
Xylenes (total)1330-20-7 8260B ND 2ug/kg6.5
AcceptanceRun 2
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 53-142
Bromofluorobenzene 85 47-138
Toluene-d8 107 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3
RE26007-005
05/25/2016 1330
05/26/2016
Solid
% Solids:86.5 05/26/2016 2305
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 06/01/2016 1701 SES 14513 6.18
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B 85 1ug/kg19
Benzene 71-43-2 8260B ND 1ug/kg4.7
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.7
Bromoform 75-25-2 8260B ND 1ug/kg4.7
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.7
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.4
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.7
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.7
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.7
Chloroethane 75-00-3 8260B ND 1ug/kg4.7
Chloroform 67-66-3 8260B ND 1ug/kg4.7
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.7
Cyclohexane 110-82-7 8260B ND 1ug/kg4.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.7
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.7
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.7
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.7
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.7
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.7
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.7
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.7
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.7
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.7
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.7
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.7
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.7
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.7
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.7
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.7
2-Hexanone 591-78-6 8260B ND 1ug/kg9.4
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.7
Methyl acetate 79-20-9 8260B ND 1ug/kg4.7
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.7
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.4
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.7
Methylene chloride 75-09-2 8260B ND 1ug/kg4.7
Styrene 100-42-5 8260B ND 1ug/kg4.7
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.7
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.7
Toluene 108-88-3 8260B ND 1ug/kg4.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 23
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Shealy Environmental Services, Inc.
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3
RE26007-005
05/25/2016 1330
05/26/2016
Solid
% Solids:86.5 05/26/2016 2305
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 06/01/2016 1701 SES 14513 6.18
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.7
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.7
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.7
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.7
Trichloroethene 79-01-6 8260B ND 1ug/kg4.7
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.7
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.7
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 53-142
Bromofluorobenzene 101 47-138
Toluene-d8 104 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 23
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Shealy Environmental Services, Inc.
QC Summary
Page: 15 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ14340-001
14340 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 05/27/2016 221620ug/L1
Benzene ND 05/27/2016 22165.0 ug/L1
Bromodichloromethane ND 05/27/2016 22165.0 ug/L1
Bromoform ND 05/27/2016 22165.0 ug/L1
Bromomethane (Methyl bromide)ND 05/27/2016 22165.0 ug/L1
2-Butanone (MEK)ND 05/27/2016 221610ug/L1
Carbon disulfide ND 05/27/2016 22165.0 ug/L1
Carbon tetrachloride ND 05/27/2016 22165.0 ug/L1
Chlorobenzene ND 05/27/2016 22165.0 ug/L1
Chloroethane ND 05/27/2016 22165.0 ug/L1
Chloroform ND 05/27/2016 22165.0 ug/L1
Chloromethane (Methyl chloride)ND 05/27/2016 22165.0 ug/L1
Cyclohexane ND 05/27/2016 22165.0 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 05/27/2016 22165.0 ug/L1
Dibromochloromethane ND 05/27/2016 22165.0 ug/L1
1,2-Dibromoethane (EDB)ND 05/27/2016 22165.0 ug/L1
1,4-Dichlorobenzene ND 05/27/2016 22165.0 ug/L1
1,3-Dichlorobenzene ND 05/27/2016 22165.0 ug/L1
1,2-Dichlorobenzene ND 05/27/2016 22165.0 ug/L1
Dichlorodifluoromethane ND 05/27/2016 22165.0 ug/L1
1,2-Dichloroethane ND 05/27/2016 22165.0 ug/L1
1,1-Dichloroethane ND 05/27/2016 22165.0 ug/L1
cis-1,2-Dichloroethene ND 05/27/2016 22165.0 ug/L1
trans-1,2-Dichloroethene ND 05/27/2016 22165.0 ug/L1
1,1-Dichloroethene ND 05/27/2016 22165.0 ug/L1
1,2-Dichloropropane ND 05/27/2016 22165.0 ug/L1
trans-1,3-Dichloropropene ND 05/27/2016 22165.0 ug/L1
cis-1,3-Dichloropropene ND 05/27/2016 22165.0 ug/L1
Ethylbenzene ND 05/27/2016 22165.0 ug/L1
2-Hexanone ND 05/27/2016 221610ug/L1
Isopropylbenzene ND 05/27/2016 22165.0 ug/L1
Methyl acetate ND 05/27/2016 22165.0 ug/L1
Methyl tertiary butyl ether (MTBE)ND 05/27/2016 22165.0 ug/L1
4-Methyl-2-pentanone ND 05/27/2016 221610ug/L1
Methylcyclohexane ND 05/27/2016 22165.0 ug/L1
Methylene chloride ND 05/27/2016 22165.0 ug/L1
Styrene ND 05/27/2016 22165.0 ug/L1
1,1,2,2-Tetrachloroethane ND 05/27/2016 22165.0 ug/L1
Tetrachloroethene ND 05/27/2016 22165.0 ug/L1
Toluene ND 05/27/2016 22165.0 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 05/27/2016 22165.0 ug/L1
1,2,4-Trichlorobenzene ND 05/27/2016 22165.0 ug/L1
1,1,2-Trichloroethane ND 05/27/2016 22165.0 ug/L1
1,1,1-Trichloroethane ND 05/27/2016 22165.0 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 16 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ14340-001
14340 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 05/27/2016 22165.0 ug/L1
Trichlorofluoromethane ND 05/27/2016 22165.0 ug/L1
Vinyl chloride ND 05/27/2016 22162.0 ug/L1
Xylenes (total)ND 05/27/2016 22165.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 17 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ14340-002
14340 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 89 05/27/2016 21078910060-1401
Benzene 46 05/27/2016 2107925070-1301
Bromodichloromethane 50 05/27/2016 21071015070-1301
Bromoform 52 05/27/2016 21071055070-1301
Bromomethane (Methyl bromide)43 05/27/2016 2107855060-1401
2-Butanone (MEK)100 05/27/2016 210710110060-1401
Carbon disulfide 39 05/27/2016 2107775060-1401
Carbon tetrachloride 45 05/27/2016 2107915070-1301
Chlorobenzene 53 05/27/2016 21071055070-1301
Chloroethane 45 05/27/2016 2107905060-1401
Chloroform 43 05/27/2016 2107855070-1301
Chloromethane (Methyl chloride)37 05/27/2016 2107755060-1401
Cyclohexane 38 05/27/2016 2107755070-1301
1,2-Dibromo-3-chloropropane (DBCP)54 05/27/2016 21071095070-1301
Dibromochloromethane 55 05/27/2016 21071095070-1301
1,2-Dibromoethane (EDB)55 05/27/2016 21071105070-1301
1,4-Dichlorobenzene 51 05/27/2016 21071035070-1301
1,3-Dichlorobenzene 54 05/27/2016 21071085070-1301
1,2-Dichlorobenzene 57 05/27/2016 21071135070-1301
Dichlorodifluoromethane 37 05/27/2016 2107745060-1401
1,2-Dichloroethane 48 05/27/2016 2107965070-1301
1,1-Dichloroethane 45 05/27/2016 2107895070-1301
cis-1,2-Dichloroethene 44 05/27/2016 2107885070-1301
trans-1,2-Dichloroethene 42 05/27/2016 2107845070-1301
1,1-Dichloroethene 42 05/27/2016 2107845070-1301
1,2-Dichloropropane 46 05/27/2016 2107935070-1301
trans-1,3-Dichloropropene 53 05/27/2016 21071065070-1301
cis-1,3-Dichloropropene 53 05/27/2016 21071065070-1301
Ethylbenzene 52 05/27/2016 21071045070-1301
2-Hexanone 110 05/27/2016 210711210060-1401
Isopropylbenzene 58 05/27/2016 21071165070-1301
Methyl acetate 43 05/27/2016 2107875060-1401
Methyl tertiary butyl ether (MTBE)43 05/27/2016 2107865070-1301
4-Methyl-2-pentanone 110 05/27/2016 210710910060-1401
Methylcyclohexane 49 05/27/2016 2107985070-1301
Methylene chloride 42 05/27/2016 2107845070-1301
Styrene 51 05/27/2016 21071015070-1301
1,1,2,2-Tetrachloroethane 52 05/27/2016 21071035070-1301
Tetrachloroethene 57 05/27/2016 21071145070-1301
Toluene 52 05/27/2016 21071035070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 43 05/27/2016 2107865070-1301
1,2,4-Trichlorobenzene 58 05/27/2016 21071165070-1301
1,1,2-Trichloroethane 50 05/27/2016 2107995070-1301
1,1,1-Trichloroethane 46 05/27/2016 2107915070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 18 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ14340-002
14340 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 49 05/27/2016 2107985070-1301
Trichlorofluoromethane 44 05/27/2016 2107885070-1301
Vinyl chloride 46 05/27/2016 2107915070-1301
Xylenes (total)110 05/27/2016 210711410070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 90 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 19 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ14513-001
14513 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 06/01/2016 113320ug/kg1
Benzene ND 06/01/2016 11335.0 ug/kg1
Bromodichloromethane ND 06/01/2016 11335.0 ug/kg1
Bromoform ND 06/01/2016 11335.0 ug/kg1
Bromomethane (Methyl bromide)ND 06/01/2016 11335.0 ug/kg1
2-Butanone (MEK)ND 06/01/2016 113310ug/kg1
Carbon disulfide ND 06/01/2016 11335.0 ug/kg1
Carbon tetrachloride ND 06/01/2016 11335.0 ug/kg1
Chlorobenzene ND 06/01/2016 11335.0 ug/kg1
Chloroethane ND 06/01/2016 11335.0 ug/kg1
Chloroform ND 06/01/2016 11335.0 ug/kg1
Chloromethane (Methyl chloride)ND 06/01/2016 11335.0 ug/kg1
Cyclohexane ND 06/01/2016 11335.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 06/01/2016 11335.0 ug/kg1
Dibromochloromethane ND 06/01/2016 11335.0 ug/kg1
1,2-Dibromoethane (EDB)ND 06/01/2016 11335.0 ug/kg1
1,4-Dichlorobenzene ND 06/01/2016 11335.0 ug/kg1
1,3-Dichlorobenzene ND 06/01/2016 11335.0 ug/kg1
1,2-Dichlorobenzene ND 06/01/2016 11335.0 ug/kg1
Dichlorodifluoromethane ND 06/01/2016 11335.0 ug/kg1
1,2-Dichloroethane ND 06/01/2016 11335.0 ug/kg1
1,1-Dichloroethane ND 06/01/2016 11335.0 ug/kg1
trans-1,2-Dichloroethene ND 06/01/2016 11335.0 ug/kg1
cis-1,2-Dichloroethene ND 06/01/2016 11335.0 ug/kg1
1,1-Dichloroethene ND 06/01/2016 11335.0 ug/kg1
1,2-Dichloropropane ND 06/01/2016 11335.0 ug/kg1
trans-1,3-Dichloropropene ND 06/01/2016 11335.0 ug/kg1
cis-1,3-Dichloropropene ND 06/01/2016 11335.0 ug/kg1
Ethylbenzene ND 06/01/2016 11335.0 ug/kg1
2-Hexanone ND 06/01/2016 113310ug/kg1
Isopropylbenzene ND 06/01/2016 11335.0 ug/kg1
Methyl acetate ND 06/01/2016 11335.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 06/01/2016 11335.0 ug/kg1
4-Methyl-2-pentanone ND 06/01/2016 113310ug/kg1
Methylcyclohexane ND 06/01/2016 11335.0 ug/kg1
Methylene chloride ND 06/01/2016 11335.0 ug/kg1
Styrene ND 06/01/2016 11335.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 06/01/2016 11335.0 ug/kg1
Tetrachloroethene ND 06/01/2016 11335.0 ug/kg1
Toluene ND 06/01/2016 11335.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 06/01/2016 11335.0 ug/kg1
1,2,4-Trichlorobenzene ND 06/01/2016 11335.0 ug/kg1
1,1,2-Trichloroethane ND 06/01/2016 11335.0 ug/kg1
1,1,1-Trichloroethane ND 06/01/2016 11335.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 20 of 23
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ14513-001
14513 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 06/01/2016 11335.0 ug/kg1
Trichlorofluoromethane ND 06/01/2016 11335.0 ug/kg1
Vinyl chloride ND 06/01/2016 11335.0 ug/kg1
Xylenes (total)ND 06/01/2016 11335.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 109 47-138
1,2-Dichloroethane-d4 95 53-142
Toluene-d8 101 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 21 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ14513-002
14513 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 110 06/01/2016 103310510060-1401
Benzene 46 06/01/2016 1033935069-1231
Bromodichloromethane 50 06/01/2016 10331015069-1211
Bromoform 45 06/01/2016 1033915061-1191
Bromomethane (Methyl bromide)47 06/01/2016 1033955010-1681
2-Butanone (MEK)110 06/01/2016 103311310057-1481
Carbon disulfide 46 06/01/2016 1033915058-1221
Carbon tetrachloride 52 06/01/2016 10331045058-1361
Chlorobenzene 48 06/01/2016 1033965059-1291
Chloroethane 50 06/01/2016 10331005060-1401
Chloroform 50 06/01/2016 10331005071-1251
Chloromethane (Methyl chloride)50 06/01/2016 10331015034-1341
Cyclohexane 49 06/01/2016 1033985053-1391
1,2-Dibromo-3-chloropropane (DBCP)45 06/01/2016 1033905055-1251
Dibromochloromethane 49 06/01/2016 1033995066-1191
1,2-Dibromoethane (EDB)49 06/01/2016 1033975074-1241
1,4-Dichlorobenzene 47 06/01/2016 1033935052-1331
1,3-Dichlorobenzene 48 06/01/2016 1033965051-1341
1,2-Dichlorobenzene 49 06/01/2016 1033995057-1311
Dichlorodifluoromethane 60 06/01/2016 10331215010-1571
1,2-Dichloroethane 49 06/01/2016 1033975067-1291
1,1-Dichloroethane 51 06/01/2016 10331025071-1271
trans-1,2-Dichloroethene 48 06/01/2016 1033965068-1311
cis-1,2-Dichloroethene 49 06/01/2016 1033995070-1221
1,1-Dichloroethene 48 06/01/2016 1033975069-1381
1,2-Dichloropropane 46 06/01/2016 1033925072-1241
trans-1,3-Dichloropropene 48 06/01/2016 1033955070-1241
cis-1,3-Dichloropropene 49 06/01/2016 1033995070-1261
Ethylbenzene 49 06/01/2016 1033975059-1281
2-Hexanone 96 06/01/2016 10339610054-1371
Isopropylbenzene 50 06/01/2016 1033995050-1361
Methyl acetate 52 06/01/2016 10331035059-1371
Methyl tertiary butyl ether (MTBE)47 06/01/2016 1033945070-1301
4-Methyl-2-pentanone 99 06/01/2016 10339910060-1341
Methylcyclohexane 51 06/01/2016 10331025041-1441
Methylene chloride 46 06/01/2016 1033925070-1301
Styrene 45 06/01/2016 1033905054-1361
1,1,2,2-Tetrachloroethane 45 06/01/2016 1033905069-1321
Tetrachloroethene 52 06/01/2016 10331045045-1501
Toluene 49 06/01/2016 1033975061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 49 06/01/2016 1033995049-1361
1,2,4-Trichlorobenzene 48 06/01/2016 1033965034-1451
1,1,2-Trichloroethane 48 06/01/2016 1033955055-1281
1,1,1-Trichloroethane 52 06/01/2016 10331045063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 23
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ14513-002
14513 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 49 06/01/2016 1033985062-1261
Trichlorofluoromethane 53 06/01/2016 10331075045-1381
Vinyl chloride 52 06/01/2016 10331045042-1321
Xylenes (total)100 06/01/2016 103310010058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 116 47-138
1,2-Dichloroethane-d4 88 53-142
Toluene-d8 103 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 23
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Shealy Environmental Services, Inc.
Chain of Custody
and
Miscellaneous Documents
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SHEALY ENVIRONMENTAL SERVICES, INC.
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