19053_Point_Five_Contained_Out_20161118

1
Kady, Lebeed
From:Cooper, Harvi
Sent:Friday, November 18, 2016 2:44 PM
To:Tyburski, Jeff
Cc:Kady, Lebeed
Subject:FW: Goldsboro Berkeley Blvd. Contained Out Letter and Enclosures
Attachments:Berkeley Blvd Contained Out Certification 11172016.pdf; Berkeley Blvd Contained Out GW Data
09162016.pdf; Berkeley Blvd Contained Out Universal Treatment Std Table.pdf; Contained Out det for
Goldsboro BF site 111816.pdf
Hi Jeff, 
Attached are the contained‐out letter for the groundwater signed by Julie Woosley and the supporting documents you 
sent me yesterday. They will be scanned as one document for Laserfiche. Let me know when you get the analyticals for 
what remains in the frac tank after removal of the groundwater.  
Thanks, 
Harvi 

Harvi Cooper 
Environmental Chemist 
Hazardous Waste Section – Division of Waste Management 
NC Department of Environmental Quality  
P.O. Box 1848 
Pittsboro, NC 27312 
(919)642‐0098 office 
[e-mail] 
http://portal.ncdenr.org 

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed 
to third parties unless the content is exempt by statute or other regulation. 

From: Woosley, Julie  
Sent: Friday, November 18, 2016 2:26 PM 
To: Galantis, Kelly <[e-mail]> 
Cc: Cooper, Harvi <[e-mail]> 
Subject: FW: Goldsboro Contained Out Letter and Enclosures 

Kelly, 
Please have all four documents scanned into Laserfische as one document. Title and description to be based on the 
signed letter, which should be the first. The rest are supporting documents.  
Thanks, 
Julie 

From: Cooper, Harvi  
Sent: Thursday, November 17, 2016 4:24 PM 
2
To: Woosley, Julie <[e-mail]> 
Subject: Goldsboro Contained Out Letter and Enclosures 

Hi Julie, 
Jeff Tyburski completed the contained out form and submitted the associated table and analytical report for the 
contained out determination for the groundwater. I made a few additional revisions to the letter to address the 
enclosures. All 4 documents are attached. Let me know if you have any questions or further revisions. 
Thanks, 
Harvi 

Harvi Cooper 
Environmental Chemist 
Hazardous Waste Section – Division of Waste Management 
NC Department of Environmental Quality  
P.O. Box 1848 
Pittsboro, NC 27312 
(919)642‐0098 office 
[e-mail] 
http://portal.ncdenr.org 

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed 
to third parties unless the content is exempt by statute or other regulation. 

CERTIFICATION OF MEDIA MEETING NORTH CAROLINA "CONTAINED-OUT" LEVELS
(Any groundwater containing hazardous waste not meeting approved risk-based levels must be handled as if they were hazardous,
including hazardous waste manifesting. Groundwater with contaminant concentrations below these levels would be considered
non-hazardous waste but would require management through a publicly owned NPDES wastewater treatment facility POTW,
with documented approval.)
I. Location Information
Name of Site 501 & 503 North Berkeley Boulevard
EPA ID number (or Not Applicable) ... N~o""'t..,AwPw.P~Ji..i..calillh ... I.11<,,e _______________ _
If non-RCRA site, designate program with regulatory oversight NC Brownfields Program
County_\Y1.1..111a~y~n~e------------~
Street 501 & 503 North Berkeley Boulevard
City Goldsboro
Phone NA <Site under redevelopement}
(Area Code)
II. Groundwater Meeting Unrestricted Use Levels
State _N_c ______ Zip 27534
Description of groundwater (source of contamination, number of tanks).
Groundwater beneath the site has been impacted by an off-site release of dry-cleaning solvent from the former
Penny One-Hour Cleaners located at 433 N. Berkeley Boulevard, Goldsboro, NC. The Penny One-Hour Cleaners
£it.i is icfaHtifi.id as D£CA sit.i 96000:2.
III. Groundwater Meeting Levels for Treatment at a POT)Y
Description of groundwater (source of contamination, number of tanks, etc.)
An estimated 8,600-gallons of groundwater was pumped from and open construction excavation into a
20,000-gallon frac tank. Analysis of a water sample from the tank confirmed the presence of constituents likely
Associat.id with th.i dry cl.iaHiHg solv.iHt rnl.ias.i (aHalytical rnsHlts attach.id).
Quantity delivered: Volume in cubic yards, gallons, and/or weight in tons
Actual quantity to be determined upon delivery
Name of receiving POTW _.G.._o ... l...,d..,sh ... o ... r...,o._)Y....,.R..iS....._ __________________ _
NPDES Permit# _N .... c .... 0 .... 0_2_39._4 ... 9 _________ _
County_)Y1.1..111a~y~n~e------------------State...,N ..... c...._ ________ _
(page 1 of 2)
CERTIFICATION OF MEETING NORTH CAROLINA "CONTAINED-OUT"LEVELS
Physical (not mailing) address of POTW
Street 714 Arrington Brjdge Road
City Goldsboro State ... N ... C.....__ _____ Zip 27530
Phone [phone]
(Area Code)
IV. Analytical Information (Submit separate attachments for groundwater described in Sections II and Ill)
Attach laboratory analyses which should include:
• Name, address and phone number of the analytical laboratory.
• Information on the dilution factor.
• Total concentrations reported down to the method detection limits.
Attach comparison to "contained-out" level for management scenario:
• A spreadsheet of groundwater levels for each tank with comparison to the required "contained-out" level
for that scenario. Data sheets should be kept by the facility should any questions arise.
v. Hazardous by Characteristic
It was determined that none of the groundwater described above has hazardous characteristics:
By testing methodologies See attached
By generator knowledge D
Note: The Point Five Goldsboro, LLC is the Prospective Developer for the site under the NC Brownfields
Program and generated the water during construction dewatering during site redevelopment.
I hereby certify under penalty of law that the information contained in this document is accurate and that the
groundwater described either met unrestricted use levels or was delivered to the POTW above in the vehicle it
was placed in without mixing with any other solid waste. Any groundwater not meeting these criteria was
handled as hazardous waste, including hazardous waste manifesting to a TSD facility. Based on my inquiry of
the person or persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine and im · onment for 1~~
Signature of site manager/facility contact _.,,-ff /t / / ( (
Printed name and title of above person Jeffrey Tyburski, P,G, for Pojnt five Goldsboro, LLC
Phone [phone]
(Area Code)
The original of this signed certification must be sent to the project manager within the Division of Waste Management. A
copy of this signed certification must be retained at the facility (if applicable) for a minimum of three years.
(page 2 of 2)
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
09/16/2016
McAdams (John R.) Company, Inc.
Jeff Tyburski
2905 Meridian Pkwy
Durham, NC 27713
Project: Berkeley Brownfields
Lab Submittal Date: 09/09/2016
Prism Work Order: 6090167
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 39
Sample Receipt Summary
09/16/2016
Prism Work Order: 6090167
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6090167-01 09/07/16FRAC-1 09/09/16Water
6090167-02 09/07/16ROB-2A 09/09/16Solid
6090167-03 09/07/16ROB-2B 09/09/16Solid
6090167-04 09/07/16ROB-3A 09/09/16Solid
6090167-05 09/07/16ROB-3B 09/09/16Solid
6090167-06 09/07/16ROB-4A 09/09/16Solid
6090167-07 09/07/16ROB-4B 09/09/16Solid
Samples were received in good condition at 1.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 39
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6090167
09/16/2016
Summary of Detections
20 ug/L6090167-01 FRAC-1 Di-n-butyl phthalate 8270D
0.035 mg/L6090167-01 FRAC-1 Barium *6010D
0.0060 mg/L6090167-01 FRAC-1 Chromium *6010D
0.0052 mg/L6090167-01 FRAC-1 Lead *6010D
0.023 mg/L6090167-01 FRAC-1 Selenium *6010D
5.4 ug/L6090167-01 FRAC-1 Tetrachloroethylene 8260B
0.030 J mg/kg dry6090167-02 ROB-2A Acetone 8260B
0.031 J mg/kg dry6090167-03 ROB-2B Acetone 8260B
0.022 J mg/kg dry6090167-04 ROB-3A Acetone 8260B
0.021 J mg/kg dry6090167-05 ROB-3B Acetone 8260B
0.021 mg/kg dry6090167-05 ROB-3B Tetrachloroethylene 8260B
0.018 J mg/kg dry6090167-06 ROB-4A Acetone 8260B
0.0026 J mg/kg dry6090167-06 ROB-4A Tetrachloroethylene 8260B
0.018 J mg/kg dry6090167-07 ROB-4B Acetone 8260B
0.0027 J mg/kg dry6090167-07 ROB-4B Tetrachloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Water
Client Sample ID: FRAC-1
Prism Sample ID: 6090167-01
Prism Work Order: 6090167
Time Collected: 09/07/16 14:00
Time Submitted: 09/09/16 15:20
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.61,2-Dichlorobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.91,3-Dichlorobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.61,4-Dichlorobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.61-Methylnaphthalene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.62,4,5-Trichlorophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.82,4,6-Trichlorophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.62,4-Dichlorophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 3.42,4-Dimethylphenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.72,4-Dinitrophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.42,4-Dinitrotoluene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.12,6-Dinitrotoluene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.72-Chloronaphthalene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.92-Chlorophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.42-Methylnaphthalene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.82-Methylphenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.42-Nitroaniline
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.42-Nitrophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.43,3'-Dichlorobenzidine
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.53/4-Methylphenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.43-Nitroaniline
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.44-Chloro-3-methylphenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.44-Chloroaniline
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.34-Chlorophenyl phenyl ether
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 0.934-Nitroaniline
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 0.604-Nitrophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.8Acenaphthene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.0Acenaphthylene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.4Aniline
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Anthracene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.8Azobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Benzo(a)anthracene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Benzo(a)pyrene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.1Benzo(b)fluoranthene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Benzo(k)fluoranthene
BRL 8270D P6I018711009/15/16 20:27 JMVug/L 4.7Benzoic Acid
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.1Benzyl alcohol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.6bis(2-Chloroethoxy)methane
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.3Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Water
Client Sample ID: FRAC-1
Prism Sample ID: 6090167-01
Prism Work Order: 6090167
Time Collected: 09/07/16 14:00
Time Submitted: 09/09/16 15:20
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.0Bis(2-chloroisopropyl)ether
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Chrysene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.8Dibenzofuran
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 3.3Diethyl phthalate
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Dimethyl phthalate
20 8270D P6I01871109/15/16 20:27 JMVug/L 1.7Di-n-butyl phthalate
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.3Di-n-octyl phthalate
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.7Fluoranthene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.7Fluorene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.1Hexachlorobutadiene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.7Hexachlorocyclopentadiene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.7Hexachloroethane
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 3.9Indeno(1,2,3-cd)pyrene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.5Isophorone
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.6Naphthalene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.6Nitrobenzene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 2.2N-Nitroso-di-n-propylamine
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.3N-Nitrosodiphenylamine
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.2Pentachlorophenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.5Phenanthrene
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 0.98Phenol
BRL 8270D P6I01871109/15/16 20:27 JMVug/L 1.4Pyrene
Surrogate Recovery Control Limits
43-14078 %2,4,6-Tribromophenol
44-11967 %2-Fluorobiphenyl
19-11937 %2-Fluorophenol
44-12060 %Nitrobenzene-d5
11-5226 %Phenol-d5
50-13471 %Terphenyl-d14
Total Metals
BRL *7470A P6I023310.00020 9/15/16 13:02 JABmg/L 0.000030Mercury
BRL *6010D P6I017710.010 9/15/16 23:52 bgmmg/L 0.00070Arsenic
0.035 *6010D P6I017710.010 9/15/16 23:52 bgmmg/L 0.00070Barium
BRL *6010D P6I017710.0010 9/15/16 23:52 bgmmg/L 0.00010Cadmium
0.0060 *6010D P6I017710.0050 9/15/16 23:52 bgmmg/L 0.00060Chromium
0.0052 *6010D P6I017710.0050 9/15/16 23:52 bgmmg/L 0.0013Lead
0.023 *6010D P6I017710.020 9/15/16 23:52 bgmmg/L 0.0032Selenium
BRL *6010D P6I017710.0050 9/15/16 23:52 bgmmg/L 0.00020Silver
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Water
Client Sample ID: FRAC-1
Prism Sample ID: 6090167-01
Prism Work Order: 6090167
Time Collected: 09/07/16 14:00
Time Submitted: 09/09/16 15:20
Volatile Organic Compounds by GC/MS
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P6I025512.0 9/15/16 18:18 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P6I025512.0 9/15/16 18:18 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P6I025512.0 9/15/16 18:18 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P6I025515.0 9/15/16 18:18 KDMug/L 0.31Acetone
BRL 8260B P6I02551209/15/16 18:18 KDMug/L 0.20Acrolein
BRL 8260B P6I02551209/15/16 18:18 KDMug/L 0.20Acrylonitrile
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.048Benzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.057Bromobenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.14Bromochloromethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.062Bromodichloromethane
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.040Bromoform
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.18Bromomethane
BRL 8260B P6I025515.0 9/15/16 18:18 KDMug/L 0.075Carbon disulfide
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.062Chlorobenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.22Chloroethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.076Chloroform
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.079Chloromethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Water
Client Sample ID: FRAC-1
Prism Sample ID: 6090167-01
Prism Work Order: 6090167
Time Collected: 09/07/16 14:00
Time Submitted: 09/09/16 15:20
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.065Dibromomethane
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.061Ethylbenzene
BRL 8260B P6I025512.0 9/15/16 18:18 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.050Isopropyl Ether
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.12m,p-Xylenes
BRL 8260B P6I025515.0 9/15/16 18:18 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I025515.0 9/15/16 18:18 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I025515.0 9/15/16 18:18 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.083Methylene Chloride
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.19Naphthalene
BRL 8260B P6I025511.0 9/15/16 18:18 KDMug/L 0.076n-Butylbenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.087n-Propylbenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.044o-Xylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.047Styrene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.088tert-Butylbenzene
5.4 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.044Toluene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.078Trichloroethylene
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P6I025512.0 9/15/16 18:18 KDMug/L 0.060Vinyl acetate
BRL 8260B P6I025510.50 9/15/16 18:18 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-129105 %Dibromofluoromethane
77-12398 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-2A
Prism Sample ID: 6090167-02
Prism Work Order: 6090167
Time Collected: 09/07/16 13:00
Time Submitted: 09/09/16 15:20
General Chemistry Parameters
88.3 *SM2540 G P6I018510.100 9/12/16 15:51 JLB% by
Weight
0.100% Solids
Volatile Organic Compounds by GC/MS
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000501,1,1,2-Tetrachloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000541,1,2-Trichloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000781,2,3-Trichloropropane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000451,2,4-Trichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000364-Chlorotoluene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.000294-Isopropyltoluene
0.030 8260B P6I022110.061 9/15/16 14:40 ANGJmg/kg dry 0.0015Acetone
BRL 8260B P6I022110.0037 9/15/16 14:40 ANGmg/kg dry 0.00036Benzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00051Bromobenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00069Bromoform
BRL 8260B P6I022110.012 9/15/16 14:40 ANGmg/kg dry 0.00075Bromomethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00032Chlorobenzene
BRL 8260B P6I022110.012 9/15/16 14:40 ANGmg/kg dry 0.00051Chloroethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00044Chloroform
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00041Chloromethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00028Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-2A
Prism Sample ID: 6090167-02
Prism Work Order: 6090167
Time Collected: 09/07/16 13:00
Time Submitted: 09/09/16 15:20
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00023Ethylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00036Isopropylbenzene (Cumene)
BRL 8260B P6I022110.012 9/15/16 14:40 ANGmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P6I022110.061 9/15/16 14:40 ANGmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I022110.12 9/15/16 14:40 ANGmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I022110.061 9/15/16 14:40 ANGmg/kg dry 0.00052Methyl Isobutyl Ketone
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00034Methylene Chloride
BRL 8260B P6I022110.012 9/15/16 14:40 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6I022110.012 9/15/16 14:40 ANGmg/kg dry 0.00019Naphthalene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00031n-Butylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00036n-Propylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00025o-Xylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00037Styrene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00035Toluene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00040Trichloroethylene
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P6I022110.031 9/15/16 14:40 ANGmg/kg dry 0.00084Vinyl acetate
BRL 8260B P6I022110.0061 9/15/16 14:40 ANGmg/kg dry 0.00030Vinyl chloride
BRL 8260B P6I022110.018 9/15/16 14:40 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-2B
Prism Sample ID: 6090167-03
Prism Work Order: 6090167
Time Collected: 09/07/16 13:10
Time Submitted: 09/09/16 15:20
General Chemistry Parameters
78.3 *SM2540 G P6I018510.100 9/12/16 15:51 JLB% by
Weight
0.100% Solids
Volatile Organic Compounds by GC/MS
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000501,1,1,2-Tetrachloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000541,1,2-Trichloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000781,2,3-Trichloropropane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000451,2,4-Trichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000364-Chlorotoluene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.000294-Isopropyltoluene
0.031 8260B P6I022110.061 9/15/16 15:08 ANGJmg/kg dry 0.0015Acetone
BRL 8260B P6I022110.0037 9/15/16 15:08 ANGmg/kg dry 0.00036Benzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00051Bromobenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00069Bromoform
BRL 8260B P6I022110.012 9/15/16 15:08 ANGmg/kg dry 0.00075Bromomethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00032Chlorobenzene
BRL 8260B P6I022110.012 9/15/16 15:08 ANGmg/kg dry 0.00051Chloroethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00044Chloroform
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00041Chloromethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00028Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-2B
Prism Sample ID: 6090167-03
Prism Work Order: 6090167
Time Collected: 09/07/16 13:10
Time Submitted: 09/09/16 15:20
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00023Ethylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00036Isopropylbenzene (Cumene)
BRL 8260B P6I022110.012 9/15/16 15:08 ANGmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P6I022110.061 9/15/16 15:08 ANGmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I022110.12 9/15/16 15:08 ANGmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I022110.061 9/15/16 15:08 ANGmg/kg dry 0.00052Methyl Isobutyl Ketone
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00034Methylene Chloride
BRL 8260B P6I022110.012 9/15/16 15:08 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6I022110.012 9/15/16 15:08 ANGmg/kg dry 0.00019Naphthalene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00031n-Butylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00036n-Propylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00025o-Xylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00037Styrene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00035Toluene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00040Trichloroethylene
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P6I022110.031 9/15/16 15:08 ANGmg/kg dry 0.00084Vinyl acetate
BRL 8260B P6I022110.0061 9/15/16 15:08 ANGmg/kg dry 0.00030Vinyl chloride
BRL 8260B P6I022110.018 9/15/16 15:08 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-3A
Prism Sample ID: 6090167-04
Prism Work Order: 6090167
Time Collected: 09/07/16 13:20
Time Submitted: 09/09/16 15:20
General Chemistry Parameters
86.0 *SM2540 G P6I018510.100 9/12/16 15:51 JLB% by
Weight
0.100% Solids
Volatile Organic Compounds by GC/MS
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000401,1,1,2-Tetrachloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000231,1,1-Trichloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000331,1,2,2-Tetrachloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000431,1,2-Trichloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000131,1-Dichloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000211,1-Dichloroethylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000271,1-Dichloropropylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000271,2,3-Trichlorobenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000621,2,3-Trichloropropane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000361,2,4-Trichlorobenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000371,2,4-Trimethylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000191,2-Dibromoethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000231,2-Dichlorobenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000291,2-Dichloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000301,2-Dichloropropane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000371,3,5-Trimethylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000321,3-Dichlorobenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000241,3-Dichloropropane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000191,4-Dichlorobenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000232,2-Dichloropropane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000252-Chlorotoluene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000294-Chlorotoluene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.000234-Isopropyltoluene
0.022 8260B P6I022110.048 9/15/16 15:35 ANGJmg/kg dry 0.0012Acetone
BRL 8260B P6I022110.0029 9/15/16 15:35 ANGmg/kg dry 0.00028Benzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00040Bromobenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00027Bromochloromethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00027Bromodichloromethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00055Bromoform
BRL 8260B P6I022110.0097 9/15/16 15:35 ANGmg/kg dry 0.00060Bromomethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00024Carbon Tetrachloride
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00026Chlorobenzene
BRL 8260B P6I022110.0097 9/15/16 15:35 ANGmg/kg dry 0.00040Chloroethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00035Chloroform
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00033Chloromethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00021cis-1,2-Dichloroethylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00016cis-1,3-Dichloropropylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00020Dibromochloromethane
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00022Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-3A
Prism Sample ID: 6090167-04
Prism Work Order: 6090167
Time Collected: 09/07/16 13:20
Time Submitted: 09/09/16 15:20
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00019Ethylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00020Isopropyl Ether
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00029Isopropylbenzene (Cumene)
BRL 8260B P6I022110.0097 9/15/16 15:35 ANGmg/kg dry 0.00045m,p-Xylenes
BRL 8260B P6I022110.048 9/15/16 15:35 ANGmg/kg dry 0.00044Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I022110.097 9/15/16 15:35 ANGmg/kg dry 0.00044Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I022110.048 9/15/16 15:35 ANGmg/kg dry 0.00041Methyl Isobutyl Ketone
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00027Methylene Chloride
BRL 8260B P6I022110.0097 9/15/16 15:35 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether
BRL 8260B P6I022110.0097 9/15/16 15:35 ANGmg/kg dry 0.00015Naphthalene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00025n-Butylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00029n-Propylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00020o-Xylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00023sec-Butylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00029Styrene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00016tert-Butylbenzene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00023Tetrachloroethylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00028Toluene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00029trans-1,2-Dichloroethylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00025trans-1,3-Dichloropropylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00031Trichloroethylene
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00031Trichlorofluoromethane
BRL 8260B P6I022110.024 9/15/16 15:35 ANGmg/kg dry 0.00066Vinyl acetate
BRL 8260B P6I022110.0048 9/15/16 15:35 ANGmg/kg dry 0.00023Vinyl chloride
BRL 8260B P6I022110.015 9/15/16 15:35 ANGmg/kg dry 0.00091Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-3B
Prism Sample ID: 6090167-05
Prism Work Order: 6090167
Time Collected: 09/07/16 13:30
Time Submitted: 09/09/16 15:20
General Chemistry Parameters
85.5 *SM2540 G P6I018510.100 9/12/16 15:51 JLB% by
Weight
0.100% Solids
Volatile Organic Compounds by GC/MS
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000381,1,1,2-Tetrachloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000231,1,1-Trichloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000321,1,2,2-Tetrachloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000411,1,2-Trichloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000131,1-Dichloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000211,1-Dichloroethylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000261,1-Dichloropropylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000271,2,3-Trichlorobenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000601,2,3-Trichloropropane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000351,2,4-Trichlorobenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000361,2,4-Trimethylbenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000191,2-Dibromoethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000221,2-Dichlorobenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000281,2-Dichloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000291,2-Dichloropropane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000351,3,5-Trimethylbenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000311,3-Dichlorobenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000231,3-Dichloropropane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000181,4-Dichlorobenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000222,2-Dichloropropane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000242-Chlorotoluene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000284-Chlorotoluene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.000234-Isopropyltoluene
0.021 8260B P6I022110.047 9/15/16 16:03 ANGJmg/kg dry 0.0011Acetone
BRL 8260B P6I022110.0028 9/15/16 16:03 ANGmg/kg dry 0.00027Benzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00039Bromobenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00026Bromochloromethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00026Bromodichloromethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00053Bromoform
BRL 8260B P6I022110.0094 9/15/16 16:03 ANGmg/kg dry 0.00058Bromomethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00023Carbon Tetrachloride
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00025Chlorobenzene
BRL 8260B P6I022110.0094 9/15/16 16:03 ANGmg/kg dry 0.00039Chloroethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00034Chloroform
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00031Chloromethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00020cis-1,2-Dichloroethylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00016cis-1,3-Dichloropropylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00019Dibromochloromethane
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00021Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-3B
Prism Sample ID: 6090167-05
Prism Work Order: 6090167
Time Collected: 09/07/16 13:30
Time Submitted: 09/09/16 15:20
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00018Ethylbenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00019Isopropyl Ether
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00028Isopropylbenzene (Cumene)
BRL 8260B P6I022110.0094 9/15/16 16:03 ANGmg/kg dry 0.00043m,p-Xylenes
BRL 8260B P6I022110.047 9/15/16 16:03 ANGmg/kg dry 0.00042Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I022110.094 9/15/16 16:03 ANGmg/kg dry 0.00042Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I022110.047 9/15/16 16:03 ANGmg/kg dry 0.00040Methyl Isobutyl Ketone
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00026Methylene Chloride
BRL 8260B P6I022110.0094 9/15/16 16:03 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether
BRL 8260B P6I022110.0094 9/15/16 16:03 ANGmg/kg dry 0.00015Naphthalene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00024n-Butylbenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00028n-Propylbenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00019o-Xylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00023sec-Butylbenzene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00028Styrene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00016tert-Butylbenzene
0.021 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00022Tetrachloroethylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00027Toluene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00028trans-1,2-Dichloroethylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00025trans-1,3-Dichloropropylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00030Trichloroethylene
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00030Trichlorofluoromethane
BRL 8260B P6I022110.023 9/15/16 16:03 ANGmg/kg dry 0.00064Vinyl acetate
BRL 8260B P6I022110.0047 9/15/16 16:03 ANGmg/kg dry 0.00023Vinyl chloride
BRL 8260B P6I022110.014 9/15/16 16:03 ANGmg/kg dry 0.00088Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-4A
Prism Sample ID: 6090167-06
Prism Work Order: 6090167
Time Collected: 09/07/16 13:40
Time Submitted: 09/09/16 15:20
General Chemistry Parameters
84.4 *SM2540 G P6I018510.100 9/12/16 15:51 JLB% by
Weight
0.100% Solids
Volatile Organic Compounds by GC/MS
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000431,1,1,2-Tetrachloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000251,1,1-Trichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000351,1,2,2-Tetrachloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000471,1,2-Trichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000151,1-Dichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000231,1-Dichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000291,1-Dichloropropylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000301,2,3-Trichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000671,2,3-Trichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000391,2,4-Trichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000401,2,4-Trimethylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000211,2-Dibromoethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000251,2-Dichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000311,2-Dichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000331,2-Dichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000401,3,5-Trimethylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000351,3-Dichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000261,3-Dichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000211,4-Dichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000252,2-Dichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000272-Chlorotoluene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000314-Chlorotoluene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.000254-Isopropyltoluene
0.018 8260B P6I022110.052 9/15/16 16:31 ANGJmg/kg dry 0.0013Acetone
BRL 8260B P6I022110.0031 9/15/16 16:31 ANGmg/kg dry 0.00031Benzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00044Bromobenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00029Bromochloromethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00029Bromodichloromethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00060Bromoform
BRL 8260B P6I022110.010 9/15/16 16:31 ANGmg/kg dry 0.00065Bromomethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00026Carbon Tetrachloride
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00028Chlorobenzene
BRL 8260B P6I022110.010 9/15/16 16:31 ANGmg/kg dry 0.00044Chloroethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00038Chloroform
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00035Chloromethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00022cis-1,2-Dichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00018cis-1,3-Dichloropropylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00022Dibromochloromethane
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00024Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-4A
Prism Sample ID: 6090167-06
Prism Work Order: 6090167
Time Collected: 09/07/16 13:40
Time Submitted: 09/09/16 15:20
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00020Ethylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00021Isopropyl Ether
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00031Isopropylbenzene (Cumene)
BRL 8260B P6I022110.010 9/15/16 16:31 ANGmg/kg dry 0.00048m,p-Xylenes
BRL 8260B P6I022110.052 9/15/16 16:31 ANGmg/kg dry 0.00047Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I022110.10 9/15/16 16:31 ANGmg/kg dry 0.00047Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I022110.052 9/15/16 16:31 ANGmg/kg dry 0.00045Methyl Isobutyl Ketone
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00029Methylene Chloride
BRL 8260B P6I022110.010 9/15/16 16:31 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether
BRL 8260B P6I022110.010 9/15/16 16:31 ANGmg/kg dry 0.00017Naphthalene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00027n-Butylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00031n-Propylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00022o-Xylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00025sec-Butylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00032Styrene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00018tert-Butylbenzene
0.0026 8260B P6I022110.0052 9/15/16 16:31 ANGJmg/kg dry 0.00025Tetrachloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00030Toluene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00031trans-1,2-Dichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00028trans-1,3-Dichloropropylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00034Trichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00034Trichlorofluoromethane
BRL 8260B P6I022110.026 9/15/16 16:31 ANGmg/kg dry 0.00072Vinyl acetate
BRL 8260B P6I022110.0052 9/15/16 16:31 ANGmg/kg dry 0.00025Vinyl chloride
BRL 8260B P6I022110.016 9/15/16 16:31 ANGmg/kg dry 0.00098Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123112 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-4B
Prism Sample ID: 6090167-07
Prism Work Order: 6090167
Time Collected: 09/07/16 14:00
Time Submitted: 09/09/16 15:20
General Chemistry Parameters
86.0 *SM2540 G P6I018510.100 9/12/16 15:51 JLB% by
Weight
0.100% Solids
Volatile Organic Compounds by GC/MS
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000431,1,1,2-Tetrachloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000251,1,1-Trichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000351,1,2,2-Tetrachloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000461,1,2-Trichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000141,1-Dichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000231,1-Dichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000281,1-Dichloropropylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000291,2,3-Trichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000661,2,3-Trichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000391,2,4-Trichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000401,2,4-Trimethylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000211,2-Dibromoethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000241,2-Dichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000311,2-Dichloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000321,2-Dichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000391,3,5-Trimethylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000341,3-Dichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000261,3-Dichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000201,4-Dichlorobenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000252,2-Dichloropropane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000272-Chlorotoluene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000314-Chlorotoluene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.000254-Isopropyltoluene
0.018 8260B P6I022110.052 9/15/16 16:58 ANGJmg/kg dry 0.0013Acetone
BRL 8260B P6I022110.0031 9/15/16 16:58 ANGmg/kg dry 0.00030Benzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00043Bromobenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00028Bromochloromethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00029Bromodichloromethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00059Bromoform
BRL 8260B P6I022110.010 9/15/16 16:58 ANGmg/kg dry 0.00064Bromomethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00026Carbon Tetrachloride
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00027Chlorobenzene
BRL 8260B P6I022110.010 9/15/16 16:58 ANGmg/kg dry 0.00043Chloroethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00037Chloroform
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00035Chloromethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00022cis-1,2-Dichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00017cis-1,3-Dichloropropylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00021Dibromochloromethane
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00024Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 39
Laboratory Report
09/16/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Sample Matrix: Solid
Client Sample ID: ROB-4B
Prism Sample ID: 6090167-07
Prism Work Order: 6090167
Time Collected: 09/07/16 14:00
Time Submitted: 09/09/16 15:20
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00020Ethylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00021Isopropyl Ether
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00031Isopropylbenzene (Cumene)
BRL 8260B P6I022110.010 9/15/16 16:58 ANGmg/kg dry 0.00048m,p-Xylenes
BRL 8260B P6I022110.052 9/15/16 16:58 ANGmg/kg dry 0.00047Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6I022110.10 9/15/16 16:58 ANGmg/kg dry 0.00047Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6I022110.052 9/15/16 16:58 ANGmg/kg dry 0.00044Methyl Isobutyl Ketone
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00029Methylene Chloride
BRL 8260B P6I022110.010 9/15/16 16:58 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether
BRL 8260B P6I022110.010 9/15/16 16:58 ANGmg/kg dry 0.00016Naphthalene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00026n-Butylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00031n-Propylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00021o-Xylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00025sec-Butylbenzene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00031Styrene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00018tert-Butylbenzene
0.0027 8260B P6I022110.0052 9/15/16 16:58 ANGJmg/kg dry 0.00025Tetrachloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00030Toluene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00031trans-1,2-Dichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00027trans-1,3-Dichloropropylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00034Trichloroethylene
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00033Trichlorofluoromethane
BRL 8260B P6I022110.026 9/15/16 16:58 ANGmg/kg dry 0.00071Vinyl acetate
BRL 8260B P6I022110.0052 9/15/16 16:58 ANGmg/kg dry 0.00025Vinyl chloride
BRL 8260B P6I022110.016 9/15/16 16:58 ANGmg/kg dry 0.00097Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123112 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0221 - 5035
Blank (P6I0221-BLK1)Prepared: 09/14/16 Analyzed: 09/15/16
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0221 - 5035
Blank (P6I0221-BLK1)Prepared: 09/14/16 Analyzed: 09/15/16
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10753.6
ug/L 50.00 76-129Surrogate: Toluene-d8 9547.5
LCS (P6I0221-BS1)Prepared: 09/14/16 Analyzed: 09/15/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0520 0.0050 0.05000 72-115104
1,1,1-Trichloroethane mg/kg wet0.0586 0.0050 0.05000 67-131117
1,1,2,2-Tetrachloroethane mg/kg wet0.0431 0.0050 0.05000 56-12686
1,1,2-Trichloroethane mg/kg wet0.0442 0.0050 0.05000 70-13388
1,1-Dichloroethane mg/kg wet0.0493 0.0050 0.05000 74-12799
1,1-Dichloroethylene mg/kg wet0.0524 0.0050 0.05000 67-149105
1,1-Dichloropropylene mg/kg wet0.0479 0.0050 0.05000 71-13096
1,2,3-Trichlorobenzene mg/kg wet0.0543 0.0050 0.05000 68-130109
1,2,3-Trichloropropane mg/kg wet0.0473 0.0050 0.05000 60-13795
1,2,4-Trichlorobenzene mg/kg wet0.0519 0.0050 0.05000 66-125104
1,2,4-Trimethylbenzene mg/kg wet0.0513 0.0050 0.05000 69-129103
1,2-Dibromoethane mg/kg wet0.0520 0.0050 0.05000 70-132104
1,2-Dichlorobenzene mg/kg wet0.0498 0.0050 0.05000 72-123100
1,2-Dichloroethane mg/kg wet0.0579 0.0050 0.05000 68-128116
1,2-Dichloropropane mg/kg wet0.0432 0.0050 0.05000 73-13086
1,3,5-Trimethylbenzene mg/kg wet0.0508 0.0050 0.05000 69-128102
1,3-Dichlorobenzene mg/kg wet0.0489 0.0050 0.05000 71-12098
1,3-Dichloropropane mg/kg wet0.0436 0.0050 0.05000 75-12487
1,4-Dichlorobenzene mg/kg wet0.0475 0.0050 0.05000 71-12395
2,2-Dichloropropane mg/kg wet0.0585 0.0050 0.05000 50-142117
2-Chlorotoluene mg/kg wet0.0502 0.0050 0.05000 67-124100
4-Chlorotoluene mg/kg wet0.0506 0.0050 0.05000 71-126101
4-Isopropyltoluene mg/kg wet0.0508 0.0050 0.05000 68-129102
Acetone mg/kg wet0.109 0.050 0.1000 29-198109
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0221 - 5035
LCS (P6I0221-BS1)Prepared: 09/14/16 Analyzed: 09/15/16
Benzene mg/kg wet0.0464 0.0030 0.05000 74-12793
Bromobenzene mg/kg wet0.0481 0.0050 0.05000 73-12596
Bromochloromethane mg/kg wet0.0484 0.0050 0.05000 72-13497
Bromodichloromethane mg/kg wet0.0589 0.0050 0.05000 75-122118
Bromoform mg/kg wet0.0571 0.0050 0.05000 66-135114
Bromomethane mg/kg wet0.0678 0.010 0.05000 20-180136
Carbon Tetrachloride mg/kg wet0.0638 0.0050 0.05000 64-143128
Chlorobenzene mg/kg wet0.0480 0.0050 0.05000 74-11896
Chloroethane mg/kg wet0.0616 0.010 0.05000 33-149123
Chloroform mg/kg wet0.0532 0.0050 0.05000 73-127106
Chloromethane mg/kg wet0.0593 0.0050 0.05000 45-143119
cis-1,2-Dichloroethylene mg/kg wet0.0509 0.0050 0.05000 76-134102
cis-1,3-Dichloropropylene mg/kg wet0.0520 0.0050 0.05000 71-125104
Dibromochloromethane mg/kg wet0.0563 0.0050 0.05000 73-122113
Dichlorodifluoromethane mg/kg wet0.0725 0.0050 0.05000 26-146145
Ethylbenzene mg/kg wet0.0492 0.0050 0.05000 74-12898
Isopropyl Ether mg/kg wet0.0438 0.0050 0.05000 59-15988
Isopropylbenzene (Cumene)mg/kg wet0.0478 0.0050 0.05000 68-12696
m,p-Xylenes mg/kg wet0.0998 0.010 0.1000 75-124100
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0473 0.050 0.05000 J61-15795
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0456 0.10 0.05000 J63-14991
Methyl Isobutyl Ketone mg/kg wet0.0474 0.050 0.05000 J57-16295
Methylene Chloride mg/kg wet0.0466 0.0050 0.05000 74-12993
Methyl-tert-Butyl Ether mg/kg wet0.0515 0.010 0.05000 70-130103
Naphthalene mg/kg wet0.0513 0.010 0.05000 57-157103
n-Butylbenzene mg/kg wet0.0495 0.0050 0.05000 65-13599
n-Propylbenzene mg/kg wet0.0471 0.0050 0.05000 67-13094
o-Xylene mg/kg wet0.0492 0.0050 0.05000 74-12698
sec-Butylbenzene mg/kg wet0.0478 0.0050 0.05000 66-13196
Styrene mg/kg wet0.0498 0.0050 0.05000 77-121100
tert-Butylbenzene mg/kg wet0.0484 0.0050 0.05000 67-13297
Tetrachloroethylene mg/kg wet0.0500 0.0050 0.05000 68-130100
Toluene mg/kg wet0.0484 0.0050 0.05000 71-12997
trans-1,2-Dichloroethylene mg/kg wet0.0516 0.0050 0.05000 73-132103
trans-1,3-Dichloropropylene mg/kg wet0.0537 0.0050 0.05000 68-123107
Trichloroethylene mg/kg wet0.0495 0.0050 0.05000 75-13399
Trichlorofluoromethane mg/kg wet0.0762 0.0050 0.05000 L144-146152
Vinyl acetate mg/kg wet0.0574 0.025 0.05000 85-161115
Vinyl chloride mg/kg wet0.0572 0.0050 0.05000 48-147114
Xylenes, total mg/kg wet0.149 0.015 0.1500 74-12699
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10753.5
ug/L 50.00 76-129Surrogate: Toluene-d8 9447.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0221 - 5035
LCS Dup (P6I0221-BSD1)Prepared: 09/14/16 Analyzed: 09/15/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0497 0.0050 0.05000 2072-11599 5
1,1,1-Trichloroethane mg/kg wet0.0517 0.0050 0.05000 2067-131103 12
1,1,2,2-Tetrachloroethane mg/kg wet0.0408 0.0050 0.05000 2056-12682 5
1,1,2-Trichloroethane mg/kg wet0.0418 0.0050 0.05000 2070-13384 5
1,1-Dichloroethane mg/kg wet0.0458 0.0050 0.05000 2074-12792 7
1,1-Dichloroethylene mg/kg wet0.0463 0.0050 0.05000 2067-14993 12
1,1-Dichloropropylene mg/kg wet0.0428 0.0050 0.05000 2071-13086 11
1,2,3-Trichlorobenzene mg/kg wet0.0508 0.0050 0.05000 2068-130102 7
1,2,3-Trichloropropane mg/kg wet0.0444 0.0050 0.05000 2060-13789 6
1,2,4-Trichlorobenzene mg/kg wet0.0492 0.0050 0.05000 2066-12598 5
1,2,4-Trimethylbenzene mg/kg wet0.0462 0.0050 0.05000 2069-12992 10
1,2-Dibromoethane mg/kg wet0.0484 0.0050 0.05000 2070-13297 7
1,2-Dichlorobenzene mg/kg wet0.0460 0.0050 0.05000 2072-12392 8
1,2-Dichloroethane mg/kg wet0.0536 0.0050 0.05000 2068-128107 8
1,2-Dichloropropane mg/kg wet0.0410 0.0050 0.05000 2073-13082 5
1,3,5-Trimethylbenzene mg/kg wet0.0461 0.0050 0.05000 2069-12892 10
1,3-Dichlorobenzene mg/kg wet0.0448 0.0050 0.05000 2071-12090 9
1,3-Dichloropropane mg/kg wet0.0417 0.0050 0.05000 2075-12483 5
1,4-Dichlorobenzene mg/kg wet0.0431 0.0050 0.05000 2071-12386 10
2,2-Dichloropropane mg/kg wet0.0526 0.0050 0.05000 2050-142105 11
2-Chlorotoluene mg/kg wet0.0466 0.0050 0.05000 2067-12493 7
4-Chlorotoluene mg/kg wet0.0467 0.0050 0.05000 2071-12693 8
4-Isopropyltoluene mg/kg wet0.0467 0.0050 0.05000 2068-12993 8
Acetone mg/kg wet0.107 0.050 0.1000 2029-198107 2
Benzene mg/kg wet0.0424 0.0030 0.05000 2074-12785 9
Bromobenzene mg/kg wet0.0460 0.0050 0.05000 2073-12592 5
Bromochloromethane mg/kg wet0.0458 0.0050 0.05000 2072-13492 5
Bromodichloromethane mg/kg wet0.0539 0.0050 0.05000 2075-122108 9
Bromoform mg/kg wet0.0535 0.0050 0.05000 2066-135107 6
Bromomethane mg/kg wet0.0633 0.010 0.05000 2020-180127 7
Carbon Tetrachloride mg/kg wet0.0562 0.0050 0.05000 2064-143112 13
Chlorobenzene mg/kg wet0.0456 0.0050 0.05000 2074-11891 5
Chloroethane mg/kg wet0.0555 0.010 0.05000 2033-149111 10
Chloroform mg/kg wet0.0495 0.0050 0.05000 2073-12799 7
Chloromethane mg/kg wet0.0554 0.0050 0.05000 2045-143111 7
cis-1,2-Dichloroethylene mg/kg wet0.0468 0.0050 0.05000 2076-13494 8
cis-1,3-Dichloropropylene mg/kg wet0.0481 0.0050 0.05000 2071-12596 8
Dibromochloromethane mg/kg wet0.0524 0.0050 0.05000 2073-122105 7
Dichlorodifluoromethane mg/kg wet0.0661 0.0050 0.05000 2026-146132 9
Ethylbenzene mg/kg wet0.0454 0.0050 0.05000 2074-12891 8
Isopropyl Ether mg/kg wet0.0413 0.0050 0.05000 2059-15983 6
Isopropylbenzene (Cumene)mg/kg wet0.0434 0.0050 0.05000 2068-12687 10
m,p-Xylenes mg/kg wet0.0924 0.010 0.1000 2075-12492 8
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0453 0.050 0.05000 20 J61-15791 4
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0420 0.10 0.05000 20 J63-14984 8
Methyl Isobutyl Ketone mg/kg wet0.0449 0.050 0.05000 20 J57-16290 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0221 - 5035
LCS Dup (P6I0221-BSD1)Prepared: 09/14/16 Analyzed: 09/15/16
Methylene Chloride mg/kg wet0.0421 0.0050 0.05000 2074-12984 10
Methyl-tert-Butyl Ether mg/kg wet0.0480 0.010 0.05000 2070-13096 7
Naphthalene mg/kg wet0.0479 0.010 0.05000 2057-15796 7
n-Butylbenzene mg/kg wet0.0449 0.0050 0.05000 2065-13590 10
n-Propylbenzene mg/kg wet0.0430 0.0050 0.05000 2067-13086 9
o-Xylene mg/kg wet0.0452 0.0050 0.05000 2074-12690 8
sec-Butylbenzene mg/kg wet0.0429 0.0050 0.05000 2066-13186 11
Styrene mg/kg wet0.0478 0.0050 0.05000 2077-12196 4
tert-Butylbenzene mg/kg wet0.0439 0.0050 0.05000 2067-13288 10
Tetrachloroethylene mg/kg wet0.0442 0.0050 0.05000 2068-13088 12
Toluene mg/kg wet0.0436 0.0050 0.05000 2071-12987 10
trans-1,2-Dichloroethylene mg/kg wet0.0466 0.0050 0.05000 2073-13293 10
trans-1,3-Dichloropropylene mg/kg wet0.0496 0.0050 0.05000 2068-12399 8
Trichloroethylene mg/kg wet0.0452 0.0050 0.05000 2075-13390 9
Trichlorofluoromethane mg/kg wet0.0681 0.0050 0.05000 2044-146136 11
Vinyl acetate mg/kg wet0.0495 0.025 0.05000 2085-16199 15
Vinyl chloride mg/kg wet0.0534 0.0050 0.05000 2048-147107 7
Xylenes, total mg/kg wet0.138 0.015 0.1500 2074-12692 8
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.5
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10954.3
ug/L 50.00 76-129Surrogate: Toluene-d8 9648.2
Batch P6I0255 - 5030B
Blank (P6I0255-BLK1)Prepared & Analyzed: 09/15/16
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0255 - 5030B
Blank (P6I0255-BLK1)Prepared & Analyzed: 09/15/16
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0255 - 5030B
Blank (P6I0255-BLK1)Prepared & Analyzed: 09/15/16
Vinyl chloride ug/LBRL0.50
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10452.1
ug/L 50.00 77-123Surrogate: Toluene-d8 9949.5
LCS (P6I0255-BS1)Prepared & Analyzed: 09/15/16
1,1,1,2-Tetrachloroethane ug/L20.2 0.50 20.00 79-134101
1,1,1-Trichloroethane ug/L18.9 0.50 20.00 75-13694
1,1,2,2-Tetrachloroethane ug/L18.5 0.50 20.00 62-12792
1,1,2-Trichloroethane ug/L20.0 0.50 20.00 70-140100
1,1-Dichloroethane ug/L17.5 0.50 20.00 78-13087
1,1-Dichloroethylene ug/L18.7 0.50 20.00 70-15493
1,1-Dichloropropylene ug/L18.1 0.50 20.00 71-13691
1,2,3-Trichlorobenzene ug/L22.4 2.0 20.00 58-144112
1,2,3-Trichloropropane ug/L20.7 1.0 20.00 71-127104
1,2,4-Trichlorobenzene ug/L21.8 1.0 20.00 66-139109
1,2,4-Trimethylbenzene ug/L21.8 0.50 20.00 75-133109
1,2-Dibromo-3-chloropropane ug/L22.8 2.0 20.00 63-134114
1,2-Dibromoethane ug/L22.1 0.50 20.00 77-135110
1,2-Dichlorobenzene ug/L22.3 0.50 20.00 78-128112
1,2-Dichloroethane ug/L17.9 0.50 20.00 68-13189
1,2-Dichloropropane ug/L17.5 0.50 20.00 77-13088
1,3,5-Trimethylbenzene ug/L21.1 0.50 20.00 75-131105
1,3-Dichlorobenzene ug/L21.3 0.50 20.00 77-125106
1,3-Dichloropropane ug/L18.8 0.50 20.00 76-13294
1,4-Dichlorobenzene ug/L20.9 0.50 20.00 75-126104
2,2-Dichloropropane ug/L19.1 2.0 20.00 29-14996
2-Chlorotoluene ug/L20.6 0.50 20.00 74-126103
4-Chlorotoluene ug/L20.6 0.50 20.00 78-129103
4-Isopropyltoluene ug/L19.8 0.50 20.00 69-13299
Acetone ug/L36.5 5.0 40.00 40-16691
Acrolein ug/L38.1 20 40.00 70-13095
Acrylonitrile ug/L35.3 20 40.00 81-12788
Benzene ug/L19.1 0.50 20.00 77-12895
Bromobenzene ug/L19.9 0.50 20.00 78-129100
Bromochloromethane ug/L19.2 0.50 20.00 78-13596
Bromodichloromethane ug/L18.8 0.50 20.00 76-13894
Bromoform ug/L20.2 1.0 20.00 71-135101
Bromomethane ug/L15.3 1.0 20.00 41-16876
Carbon disulfide ug/L20.9 5.0 20.00 59-135105
Carbon Tetrachloride ug/L20.4 0.50 20.00 72-142102
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L18.9 0.50 20.00 57-14294
Chloroform ug/L18.0 0.50 20.00 77-13090
Chloromethane ug/L18.5 0.50 20.00 47-14592
cis-1,2-Dichloroethylene ug/L17.9 0.50 20.00 76-14189
cis-1,3-Dichloropropylene ug/L19.3 0.50 20.00 65-14096
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0255 - 5030B
LCS (P6I0255-BS1)Prepared & Analyzed: 09/15/16
Dibromochloromethane ug/L20.4 0.50 20.00 75-134102
Dibromomethane ug/L18.6 0.50 20.00 76-13893
Dichlorodifluoromethane ug/L21.7 1.0 20.00 28-163108
Ethylbenzene ug/L20.6 0.50 20.00 80-127103
Hexachlorobutadiene ug/L23.2 2.0 20.00 61-134116
Isopropyl Ether ug/L16.2 0.50 20.00 60-15481
Isopropylbenzene (Cumene)ug/L20.6 0.50 20.00 70-130103
m,p-Xylenes ug/L42.8 1.0 40.00 77-133107
Methyl Butyl Ketone (2-Hexanone)ug/L17.9 5.0 20.00 64-13790
Methyl Ethyl Ketone (2-Butanone)ug/L16.4 5.0 20.00 71-13482
Methyl Isobutyl Ketone ug/L17.9 5.0 20.00 69-13489
Methylene Chloride ug/L16.7 1.0 20.00 73-13184
Methyl-tert-Butyl Ether ug/L18.3 0.50 20.00 68-13592
Naphthalene ug/L21.2 1.0 20.00 64-136106
n-Butylbenzene ug/L20.7 1.0 20.00 68-134104
n-Propylbenzene ug/L20.3 0.50 20.00 72-132102
o-Xylene ug/L20.6 0.50 20.00 78-128103
sec-Butylbenzene ug/L19.2 0.50 20.00 71-13196
Styrene ug/L22.5 0.50 20.00 78-129113
tert-Butylbenzene ug/L20.4 0.50 20.00 70-132102
Tetrachloroethylene ug/L20.7 0.50 20.00 80-129104
Toluene ug/L19.8 0.50 20.00 76-13199
trans-1,2-Dichloroethylene ug/L17.7 0.50 20.00 76-13588
trans-1,3-Dichloropropylene ug/L19.1 0.50 20.00 67-14096
Trichloroethylene ug/L20.0 0.50 20.00 77-133100
Trichlorofluoromethane ug/L19.3 0.50 20.00 62-14897
Vinyl acetate ug/L11.0 2.0 20.00 34-16755
Vinyl chloride ug/L18.8 0.50 20.00 57-14194
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9648.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9849.2
ug/L 50.00 77-123Surrogate: Toluene-d8 10150.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0255 - 5030B
LCS Dup (P6I0255-BSD1)Prepared & Analyzed: 09/15/16
1,1,1,2-Tetrachloroethane ug/L20.0 0.50 20.00 2079-134100 1
1,1,1-Trichloroethane ug/L18.3 0.50 20.00 2075-13692 3
1,1,2,2-Tetrachloroethane ug/L18.8 0.50 20.00 2062-12794 2
1,1,2-Trichloroethane ug/L19.4 0.50 20.00 2070-14097 3
1,1-Dichloroethane ug/L17.2 0.50 20.00 2078-13086 1
1,1-Dichloroethylene ug/L17.6 0.50 20.00 2070-15488 6
1,1-Dichloropropylene ug/L17.4 0.50 20.00 2071-13687 4
1,2,3-Trichlorobenzene ug/L21.9 2.0 20.00 2058-144110 2
1,2,3-Trichloropropane ug/L20.0 1.0 20.00 2071-127100 3
1,2,4-Trichlorobenzene ug/L20.8 1.0 20.00 2066-139104 5
1,2,4-Trimethylbenzene ug/L20.6 0.50 20.00 2075-133103 5
1,2-Dibromo-3-chloropropane ug/L21.6 2.0 20.00 2063-134108 5
1,2-Dibromoethane ug/L22.2 0.50 20.00 2077-135111 0.5
1,2-Dichlorobenzene ug/L21.5 0.50 20.00 2078-128107 4
1,2-Dichloroethane ug/L18.0 0.50 20.00 2068-13190 0.7
1,2-Dichloropropane ug/L17.2 0.50 20.00 2077-13086 2
1,3,5-Trimethylbenzene ug/L20.0 0.50 20.00 2075-131100 5
1,3-Dichlorobenzene ug/L20.5 0.50 20.00 2077-125103 3
1,3-Dichloropropane ug/L18.3 0.50 20.00 2076-13292 3
1,4-Dichlorobenzene ug/L19.9 0.50 20.00 2075-126100 5
2,2-Dichloropropane ug/L18.6 2.0 20.00 2029-14993 3
2-Chlorotoluene ug/L19.7 0.50 20.00 2074-12699 4
4-Chlorotoluene ug/L20.2 0.50 20.00 2078-129101 2
4-Isopropyltoluene ug/L19.0 0.50 20.00 2069-13295 4
Acetone ug/L36.6 5.0 40.00 2040-16691 0.1
Acrolein ug/L36.3 20 40.00 2070-13091 5
Acrylonitrile ug/L34.8 20 40.00 2081-12787 1
Benzene ug/L18.4 0.50 20.00 2077-12892 3
Bromobenzene ug/L19.2 0.50 20.00 2078-12996 4
Bromochloromethane ug/L18.7 0.50 20.00 2078-13593 3
Bromodichloromethane ug/L18.5 0.50 20.00 2076-13892 2
Bromoform ug/L20.1 1.0 20.00 2071-135100 0.7
Bromomethane ug/L15.0 1.0 20.00 2041-16875 2
Carbon disulfide ug/L20.2 5.0 20.00 2059-135101 3
Carbon Tetrachloride ug/L20.1 0.50 20.00 2072-142101 1
Chlorobenzene ug/L20.4 0.50 20.00 2078-119102 1
Chloroethane ug/L18.5 0.50 20.00 2057-14292 2
Chloroform ug/L17.8 0.50 20.00 2077-13089 1
Chloromethane ug/L17.3 0.50 20.00 2047-14587 7
cis-1,2-Dichloroethylene ug/L17.5 0.50 20.00 2076-14187 2
cis-1,3-Dichloropropylene ug/L18.9 0.50 20.00 2065-14094 2
Dibromochloromethane ug/L20.4 0.50 20.00 2075-134102 0.1
Dibromomethane ug/L18.2 0.50 20.00 2076-13891 2
Dichlorodifluoromethane ug/L20.5 1.0 20.00 2028-163103 5
Ethylbenzene ug/L19.9 0.50 20.00 2080-127100 4
Hexachlorobutadiene ug/L21.5 2.0 20.00 2061-134108 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6I0255 - 5030B
LCS Dup (P6I0255-BSD1)Prepared & Analyzed: 09/15/16
Isopropyl Ether ug/L16.1 0.50 20.00 2060-15480 0.4
Isopropylbenzene (Cumene)ug/L19.9 0.50 20.00 2070-130100 3
m,p-Xylenes ug/L41.8 1.0 40.00 2077-133105 2
Methyl Butyl Ketone (2-Hexanone)ug/L17.5 5.0 20.00 2064-13788 2
Methyl Ethyl Ketone (2-Butanone)ug/L16.4 5.0 20.00 2071-13482 0.1
Methyl Isobutyl Ketone ug/L17.3 5.0 20.00 2069-13486 3
Methylene Chloride ug/L16.4 1.0 20.00 2073-13182 2
Methyl-tert-Butyl Ether ug/L17.9 0.50 20.00 2068-13590 2
Naphthalene ug/L20.6 1.0 20.00 2064-136103 3
n-Butylbenzene ug/L19.6 1.0 20.00 2068-13498 6
n-Propylbenzene ug/L19.4 0.50 20.00 2072-13297 4
o-Xylene ug/L20.0 0.50 20.00 2078-128100 3
sec-Butylbenzene ug/L18.1 0.50 20.00 2071-13191 6
Styrene ug/L22.1 0.50 20.00 2078-129111 2
tert-Butylbenzene ug/L19.7 0.50 20.00 2070-13298 3
Tetrachloroethylene ug/L20.2 0.50 20.00 2080-129101 3
Toluene ug/L19.2 0.50 20.00 2076-13196 3
trans-1,2-Dichloroethylene ug/L17.5 0.50 20.00 2076-13588 0.7
trans-1,3-Dichloropropylene ug/L18.8 0.50 20.00 2067-14094 2
Trichloroethylene ug/L19.4 0.50 20.00 2077-13397 3
Trichlorofluoromethane ug/L19.0 0.50 20.00 2062-14895 2
Vinyl acetate ug/L16.3 2.0 20.00 20 D34-16781 38
Vinyl chloride ug/L18.2 0.50 20.00 2057-14191 4
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9648.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 77-123Surrogate: Toluene-d8 10351.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6I0187 - 3510C MS
Blank (P6I0187-BLK1)Prepared: 09/13/16 Analyzed: 09/15/16
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1-Methylnaphthalene ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3'-Dichlorobenzidine ug/LBRL10
3/4-Methylphenol ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Aniline ug/LBRL10
Anthracene ug/LBRL10
Azobenzene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzoic Acid ug/LBRL100
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chrysene ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6I0187 - 3510C MS
Blank (P6I0187-BLK1)Prepared: 09/13/16 Analyzed: 09/15/16
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isophorone ug/LBRL10
Naphthalene ug/LBRL10
Nitrobenzene ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Pyrene ug/LBRL10
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 6867.7
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 6029.8
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 3636.3
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 5427.0
ug/L 100.0 11-52Surrogate: Phenol-d5 2424.4
ug/L 50.00 50-134Surrogate: Terphenyl-d14 6532.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6I0187 - 3510C MS
LCS (P6I0187-BS1)Prepared: 09/13/16 Analyzed: 09/15/16
1,2,4-Trichlorobenzene ug/L28.4 10 50.00 29-12657
1,2-Dichlorobenzene ug/L25.8 10 50.00 32-11152
1,3-Dichlorobenzene ug/L26.0 10 50.00 28-11052
1,4-Dichlorobenzene ug/L26.0 10 50.00 29-11252
1-Methylnaphthalene ug/L33.1 10 50.00 41-11966
2,4,5-Trichlorophenol ug/L36.4 10 50.00 53-12373
2,4,6-Trichlorophenol ug/L35.9 10 50.00 50-12572
2,4-Dichlorophenol ug/L32.7 10 50.00 47-12165
2,4-Dimethylphenol ug/L33.6 10 50.00 31-12467
2,4-Dinitrophenol ug/L16.4 10 50.00 23-14333
2,4-Dinitrotoluene ug/L39.0 10 50.00 57-12878
2,6-Dinitrotoluene ug/L38.4 10 50.00 57-12477
2-Chloronaphthalene ug/L42.0 10 50.00 40-11684
2-Chlorophenol ug/L30.0 10 50.00 38-11760
2-Methylnaphthalene ug/L33.2 10 50.00 40-12166
2-Methylphenol ug/L28.6 10 50.00 30-11757
2-Nitroaniline ug/L33.0 10 50.00 55-12766
2-Nitrophenol ug/L33.4 10 50.00 47-12367
3,3'-Dichlorobenzidine ug/L40.4 10 50.00 27-12981
3/4-Methylphenol ug/L27.2 10 50.00 29-11054
3-Nitroaniline ug/L33.2 10 50.00 41-12866
4,6-Dinitro-2-methylphenol ug/L25.2 10 50.00 44-13750
4-Bromophenyl phenyl ether ug/L35.5 10 50.00 55-12471
4-Chloro-3-methylphenol ug/L36.0 10 50.00 52-11972
4-Chloroaniline ug/L29.7 10 50.00 33-11759
4-Chlorophenyl phenyl ether ug/L35.1 10 50.00 53-12170
4-Nitroaniline ug/L31.9 10 50.00 45-13564
4-Nitrophenol ug/L19.6 10 50.00 10-7739
Acenaphthene ug/L36.3 10 50.00 47-12273
Acenaphthylene ug/L36.0 10 50.00 41-13072
Aniline ug/L22.5 10 50.00 12-19745
Anthracene ug/L38.0 10 50.00 57-12376
Azobenzene ug/L37.1 10 50.00 61-11674
Benzo(a)anthracene ug/L39.1 10 50.00 58-12578
Benzo(a)pyrene ug/L32.8 10 50.00 54-12866
Benzo(b)fluoranthene ug/L32.1 10 50.00 53-13164
Benzo(g,h,i)perylene ug/L32.4 10 50.00 50-13465
Benzo(k)fluoranthene ug/L33.2 10 50.00 57-12966
Benzoic Acid ug/LBRL100 50.00 L10-125
Benzyl alcohol ug/L28.2 10 50.00 31-11256
bis(2-Chloroethoxy)methane ug/L31.8 10 50.00 48-12064
Bis(2-Chloroethyl)ether ug/L30.9 10 50.00 43-11862
Bis(2-chloroisopropyl)ether ug/L30.7 10 50.00 37-13061
Bis(2-Ethylhexyl)phthalate ug/L39.6 10 50.00 55-13579
Butyl benzyl phthalate ug/L38.4 10 50.00 53-13477
Chrysene ug/L40.3 10 50.00 59-12381
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6I0187 - 3510C MS
LCS (P6I0187-BS1)Prepared: 09/13/16 Analyzed: 09/15/16
Dibenzo(a,h)anthracene ug/L32.2 10 50.00 51-13464
Dibenzofuran ug/L35.9 10 50.00 53-11872
Diethyl phthalate ug/L37.1 10 50.00 56-12574
Dimethyl phthalate ug/L35.9 10 50.00 45-12772
Di-n-butyl phthalate ug/L39.6 10 50.00 59-12779
Di-n-octyl phthalate ug/L33.2 10 50.00 51-14066
Fluoranthene ug/L38.2 10 50.00 57-12876
Fluorene ug/L37.5 10 50.00 52-12475
Hexachlorobenzene ug/L33.6 10 50.00 53-12567
Hexachlorobutadiene ug/L27.5 10 50.00 22-12455
Hexachlorocyclopentadiene ug/L27.3 10 50.00 32-11755
Hexachloroethane ug/L25.1 10 50.00 21-11550
Indeno(1,2,3-cd)pyrene ug/L34.0 10 50.00 52-13468
Isophorone ug/L35.3 10 50.00 42-12471
Naphthalene ug/L33.4 10 50.00 40-12167
Nitrobenzene ug/L33.7 10 50.00 45-12167
N-Nitroso-di-n-propylamine ug/L31.3 10 50.00 49-11963
N-Nitrosodiphenylamine ug/L36.2 10 50.00 51-12372
Pentachlorophenol ug/L18.2 10 50.00 35-13836
Phenanthrene ug/L38.4 10 50.00 59-12077
Phenol ug/L15.2 10 50.00 12-5830
Pyrene ug/L39.1 10 50.00 57-12678
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 7877.6
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 6834.0
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 4242.0
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6431.9
ug/L 100.0 11-52Surrogate: Phenol-d5 2828.4
ug/L 50.00 50-134Surrogate: Terphenyl-d14 6833.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6I0187 - 3510C MS
LCS Dup (P6I0187-BSD1)Prepared: 09/13/16 Analyzed: 09/15/16
1,2,4-Trichlorobenzene ug/L29.1 10 50.00 2029-12658 2
1,2-Dichlorobenzene ug/L27.4 10 50.00 2032-11155 6
1,3-Dichlorobenzene ug/L26.8 10 50.00 2028-11054 3
1,4-Dichlorobenzene ug/L27.0 10 50.00 2029-11254 4
1-Methylnaphthalene ug/L33.5 10 50.00 2041-11967 1
2,4,5-Trichlorophenol ug/L35.9 10 50.00 2053-12372 1
2,4,6-Trichlorophenol ug/L36.1 10 50.00 2050-12572 0.6
2,4-Dichlorophenol ug/L32.8 10 50.00 2047-12166 0.3
2,4-Dimethylphenol ug/L34.7 10 50.00 2031-12469 3
2,4-Dinitrophenol ug/L22.8 10 50.00 20 D23-14346 33
2,4-Dinitrotoluene ug/L38.9 10 50.00 2057-12878 0.3
2,6-Dinitrotoluene ug/L37.9 10 50.00 2057-12476 1
2-Chloronaphthalene ug/L42.4 10 50.00 2040-11685 1
2-Chlorophenol ug/L31.2 10 50.00 2038-11762 4
2-Methylnaphthalene ug/L32.8 10 50.00 2040-12166 1
2-Methylphenol ug/L29.3 10 50.00 2030-11759 3
2-Nitroaniline ug/L32.9 10 50.00 2055-12766 0.6
2-Nitrophenol ug/L33.6 10 50.00 2047-12367 0.7
3,3'-Dichlorobenzidine ug/L40.4 10 50.00 2027-12981 0.1
3/4-Methylphenol ug/L28.4 10 50.00 2029-11057 4
3-Nitroaniline ug/L33.1 10 50.00 2041-12866 0.3
4,6-Dinitro-2-methylphenol ug/L29.0 10 50.00 2044-13758 14
4-Bromophenyl phenyl ether ug/L34.6 10 50.00 2055-12469 3
4-Chloro-3-methylphenol ug/L35.5 10 50.00 2052-11971 1
4-Chloroaniline ug/L30.6 10 50.00 2033-11761 3
4-Chlorophenyl phenyl ether ug/L34.6 10 50.00 2053-12169 1
4-Nitroaniline ug/L31.7 10 50.00 2045-13563 0.8
4-Nitrophenol ug/L19.2 10 50.00 2010-7738 2
Acenaphthene ug/L36.6 10 50.00 2047-12273 0.7
Acenaphthylene ug/L36.7 10 50.00 2041-13073 2
Aniline ug/L25.8 10 50.00 2012-19752 14
Anthracene ug/L37.5 10 50.00 2057-12375 1
Azobenzene ug/L37.0 10 50.00 2061-11674 0.4
Benzo(a)anthracene ug/L39.2 10 50.00 2058-12578 0.3
Benzo(a)pyrene ug/L32.8 10 50.00 2054-12866 0.06
Benzo(b)fluoranthene ug/L32.3 10 50.00 2053-13165 0.8
Benzo(g,h,i)perylene ug/L32.3 10 50.00 2050-13465 0.4
Benzo(k)fluoranthene ug/L33.2 10 50.00 2057-12966 0.03
Benzoic Acid ug/LBRL100 50.00 20 L10-125
Benzyl alcohol ug/L29.0 10 50.00 2031-11258 3
bis(2-Chloroethoxy)methane ug/L32.6 10 50.00 2048-12065 2
Bis(2-Chloroethyl)ether ug/L32.2 10 50.00 2043-11864 4
Bis(2-chloroisopropyl)ether ug/L31.9 10 50.00 2037-13064 4
Bis(2-Ethylhexyl)phthalate ug/L39.3 10 50.00 2055-13579 0.6
Butyl benzyl phthalate ug/L38.8 10 50.00 2053-13478 1
Chrysene ug/L40.2 10 50.00 2059-12380 0.05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6I0187 - 3510C MS
LCS Dup (P6I0187-BSD1)Prepared: 09/13/16 Analyzed: 09/15/16
Dibenzo(a,h)anthracene ug/L32.2 10 50.00 2051-13464 0.2
Dibenzofuran ug/L36.2 10 50.00 2053-11872 1
Diethyl phthalate ug/L37.1 10 50.00 2056-12574 0.1
Dimethyl phthalate ug/L36.0 10 50.00 2045-12772 0.4
Di-n-butyl phthalate ug/L39.2 10 50.00 2059-12778 1
Di-n-octyl phthalate ug/L33.8 10 50.00 2051-14068 2
Fluoranthene ug/L38.0 10 50.00 2057-12876 0.6
Fluorene ug/L36.5 10 50.00 2052-12473 3
Hexachlorobenzene ug/L33.7 10 50.00 2053-12567 0.4
Hexachlorobutadiene ug/L28.3 10 50.00 2022-12457 3
Hexachlorocyclopentadiene ug/L28.4 10 50.00 2032-11757 4
Hexachloroethane ug/L27.1 10 50.00 2021-11554 8
Indeno(1,2,3-cd)pyrene ug/L33.6 10 50.00 2052-13467 1
Isophorone ug/L36.2 10 50.00 2042-12472 2
Naphthalene ug/L33.8 10 50.00 2040-12168 1
Nitrobenzene ug/L34.3 10 50.00 2045-12169 2
N-Nitroso-di-n-propylamine ug/L32.1 10 50.00 2049-11964 3
N-Nitrosodiphenylamine ug/L36.4 10 50.00 2051-12373 0.5
Pentachlorophenol ug/L24.3 10 50.00 20 D35-13849 29
Phenanthrene ug/L38.3 10 50.00 2059-12077 0.3
Phenol ug/L15.7 10 50.00 2012-5831 3
Pyrene ug/L38.6 10 50.00 2057-12677 1
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 7676.1
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 6934.5
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 4342.8
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6532.6
ug/L 100.0 11-52Surrogate: Phenol-d5 2828.4
ug/L 50.00 50-134Surrogate: Terphenyl-d14 6532.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6I0177 - 3010A
Blank (P6I0177-BLK1)Prepared: 09/13/16 Analyzed: 09/15/16
Arsenic mg/LBRL0.010
Barium mg/LBRL0.010
Cadmium mg/LBRL0.0010
Chromium mg/LBRL0.0050
Lead mg/LBRL0.0050
Selenium mg/LBRL0.020
Silver mg/LBRL0.0050
LCS (P6I0177-BS1)Prepared: 09/13/16 Analyzed: 09/15/16
Arsenic mg/L0.242 0.010 0.2500 80-12097
Barium mg/L0.250 0.010 0.2500 80-120100
Cadmium mg/L0.246 0.0010 0.2500 80-12098
Chromium mg/L0.246 0.0050 0.2500 80-12099
Lead mg/L0.251 0.0050 0.2500 80-120100
Selenium mg/L0.245 0.020 0.2500 80-12098
Silver mg/L0.100 0.0050 0.1000 80-120100
Matrix Spike (P6I0177-MS1)Prepared: 09/13/16 Analyzed: 09/16/16 Source: 6090167-01
Arsenic mg/L0.243 0.010 0.2500 BRL 75-12597
Barium mg/L0.288 0.010 0.2500 0.0353 75-125101
Cadmium mg/L0.241 0.0010 0.2500 BRL 75-12596
Chromium mg/L0.247 0.0050 0.2500 0.00604 75-12596
Lead mg/L0.252 0.0050 0.2500 0.00515 75-12599
Selenium mg/L0.261 0.020 0.2500 0.0229 75-12595
Silver mg/L0.0975 0.0050 0.1000 BRL 75-12598
Matrix Spike Dup (P6I0177-MSD1)Prepared: 09/13/16 Analyzed: 09/16/16 Source: 6090167-01
Arsenic mg/L0.248 0.010 0.2500 BRL 2075-12599 2
Barium mg/L0.295 0.010 0.2500 0.0353 2075-125104 2
Cadmium mg/L0.245 0.0010 0.2500 BRL 2075-12598 2
Chromium mg/L0.253 0.0050 0.2500 0.00604 2075-12599 2
Lead mg/L0.257 0.0050 0.2500 0.00515 2075-125101 2
Selenium mg/L0.262 0.020 0.2500 0.0229 2075-12596 0.4
Silver mg/L0.100 0.0050 0.1000 BRL 2075-125100 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6I0233 - 7470A
Blank (P6I0233-BLK1)Prepared & Analyzed: 09/15/16
Mercury mg/LBRL0.00020
LCS (P6I0233-BS1)Prepared & Analyzed: 09/15/16
Mercury mg/L0.0100 0.00020 0.009375 80-120107
Matrix Spike (P6I0233-MS1)Prepared & Analyzed: 09/15/16 Source: 6090167-01
Mercury mg/L0.00982 0.00020 0.009375 BRL 80-120105
Matrix Spike Dup (P6I0233-MSD1)Prepared & Analyzed: 09/15/16 Source: 6090167-01
Mercury mg/L0.00934 0.00020 0.009375 BRL 2080-120100 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 39
9/16/16
Level II QC Report
2905 Meridian Pkwy
Project: Berkeley BrownfieldsMcAdams (John R.) Company, Inc.
Durham, NC 27713
Attn: Jeff Tyburski
Prism Work Order: 6090167
Time Submitted: 9/9/2016 3:20:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P6I0185 - Solids, Dry Weight
Duplicate (P6I0185-DUP1)Prepared & Analyzed: 09/12/16 Source: 6090167-02
% Solids % by Weight88.3 0.100 88.3 200.07
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P6I01856090167-02 09/12/16 15:5130 30g g
P6I01856090167-03 09/12/16 15:5130 30g g
P6I01856090167-04 09/12/16 15:5130 30g g
P6I01856090167-05 09/12/16 15:5130 30g g
P6I01856090167-06 09/12/16 15:5130 30g g
P6I01856090167-07 09/12/16 15:5130 30g g
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P6I01876090167-01 09/13/16 12:201000 1mL mL
Prep Method: 3010A
Lab Number Batch Date/TimeInitialFinal
P6I01776090167-01 09/13/16 8:5550 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P6I02336090167-01 09/15/16 8:3020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P6I02556090167-01 09/15/16 8:2410 10mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6I02216090167-02 09/14/16 14:334.63 5g mL
P6I02216090167-03 09/14/16 14:335.23 5g mL
P6I02216090167-04 09/14/16 14:336.01 5g mL
P6I02216090167-05 09/14/16 14:336.25 5g mL
P6I02216090167-06 09/14/16 14:335.64 5g mL
P6I02216090167-07 09/14/16 14:335.61 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 39
Page 39 of 39
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Sample ID
FRAC-1
North Carolina
Groundwater Quality
Standard
Treatment Standards for
Hazardous Wastes Waste
Waters
Tetrachloroethylene 5.4 0.7 56
Selenium 0.023 0.02 0.82
Notes:
The table only includes constituents detected above applicable North Carolina Groundwater Quality Standards. See attached laboratory test report for a complete
listing of detected constituents
ug/L - Micrograms per Liter
mg/L - Milligrams per Liter
North Carolina Groundwater Quality Standard
https://ncdenr.s3.amazonaws.com/s3fs-public/documents/files/02L%20Groundwater%20Standards%20Table%205-21%202013_0.pdf
Treatment Standards for Hazardous Wastes
http://www.ecfr.gov/cgi-bin/text-idx?SID=29200eb8ab4207258a0b5698e5219360&mc=true&node=se40.29.268_140&rgn=div8
Metals mg/kg - EPA Method 6010D
Volatile Organic Compounds ug/L - EPA Method 8260D
SUMMARY OF LABORATORY TEST RESULTS - FRAC TANK WATER
GOLDSBORO, NORTH CAROLINA
Analyte
Regulatory Standards
510 & 503 BERKELEY BOULEVARD
PAT MCCRORY
DONALD R, V AN DER VAART
Waste Management
ENVIRONMENT Al QUAUTV
November 18, 2016
Mr. Jeffrey Tyburski, PG, RSM
2905 Meridian Parkway
Durham, NC 27713
Subject: Response to Contained-Out Determination Request
Dear Mr. Tyburski,
\·ureta;:r
MlCHAEl. SCOTT
Dh'<-'t
This letter is written in response to your email dated 10/13/2016 to provide a contained-out
determination for the contaminated groundwater removed from excavations at the Brownficlds
construction site at 501 and 503 North Berkeley Blvd., Goldsboro, Wayne County, NC. For
media contaminated with listed hazardous waste, contained-out determinations must be made on
a case-by-case basis by EPA or a RCRA authorized state regulatory agency, based on the
Contained-In Policy. The NC DEQ DWM Hazardous Waste Section is an authorized state
regulatory agency.
The two contaminants of concern in the groundwater in question are documented below
approved Land Disposal Restriction risk-based standard concentrations levels.
Tetrachloroethylene was documented in the groundwater at 5.4 ug!L and selenium was
documented at 23 ug/L. Documentation has been submitted that the Goldsboro Water
Reclamation Facility located at 714 Arrington Bridge Road, Goldsboro, has agreed to accept the
groundwater for treatment and disposal under their NPDES permit. Therefore, the groundwater
in question may be considered non-hazardous if managed through the Goldsboro publicly owned
treatment works facility. The Certification of Meeting NC Contained Out Levels and associated
supporting documents are enclosed.
Sincerely,
Julie S. Woosley, Chief
Hazardous Waste Section
cc: Harvi Cooper
Lebccd Kady
Central Files
Enclosures
Slate of N°orlh C'.,rnliDa Environmental Quali1y I W~1C \1,inxgement
1646 Mail Service Center I 217 West Jones Stn:et .Raleib-h, NC 27699-1646
919 707 8200 T
1
Kady, Lebeed
From:Cooper, Harvi
Sent:Friday, October 21, 2016 7:54 AM
To:Kady, Lebeed
Subject:RE: Goldsboro Site Update and Need Your Help
Hi Lebeed, 
After our discussion on Wednesday, I found where similar questions were posed to Julie by DSCA about a NC DOT 
project back in 2014 on this same issue. Below is part of the HWS response, including some general contained out 
options for groundwater contaminated with PCE or PCE and breakdown products. 

The sole purpose of this response is to address issues of managing water that is (i) removed from the ground for 
construction, maintenance, assessment or remediation and (ii) contains dry‐cleaning related PCE (or its breakdown 
products) that is assumed to have originated from a listed waste.  

Because this is considered a discarded commercial chemical product and is a listed waste (waste code U210), the 
Hazardous Waste Program is unable to provide flexibility and the waste generated from dewatering operations must be 
handled as follows. 

1. All waters collected from wells, excavations, trenches, or drains for reasons related to construction, maintenance, 
assessment or remediation, are to be containerized and tested. The samples should be analyzed for total concentrations 
and reported down to the method detection limits.  

2. Each container shall be tested for the suite(s) of compounds known or suspected to be present in the waters.  

3. Based on the analytical results, waters shall be managed as follows:  

a. Water must be managed as if it were hazardous waste if the levels are above 15A NCAC 2L standards:  
i. PCE is equal to or greater than 0.7 ug/L;   
ii. TCE is equal to or greater than 3 ug/L;   
iii. VC is equal to or greater than 0.03 ug/L.  

b. Water will have no management restrictions if all chemicals detected are below the lower of the applicable 15A NCAC 
2B standards, 15A NCAC 2L standards, or the Federal Maximum Contaminant Levels (MCLs). In this case, the 2B and 2L 
standards (above) are lower than the MCLs. 
i. PCE is less than 0.7 ug/L;   
ii. TCE is less than 2.5 ug/L;  
iii. VC is less than 0.025 ug/L. 

c. Alternately, develop site‐specific risk‐based standards for the project. The Hazardous Waste Section would be willing 
to review such standards for approval. Water with contaminant concentrations below approved risk‐based standard 
levels would be considered non‐hazardous waste but would require management through a publicly owned NPDES 
wastewater treatment facility, with documented approval. 

This looks like what we have here and I think we should be able to get some input from Sandy on site‐specific risk based 
standards for a conditional contained out determination if they can send the water to a WWTP. Please give me a call so 
we can discuss this sometime after 9:30.  
Thanks, 
2
Harvi 

Harvi Cooper 
Environmental Chemist 
Hazardous Waste Section – Division of Waste Management 
NC Department of Environmental Quality  
P.O. Box 1848 
Pittsboro, NC 27312 
(919)642‐0098 office 
[e-mail] 
http://portal.ncdenr.org 

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed 
to third parties unless the content is exempt by statute or other regulation. 

From: Kady, Lebeed  
Sent: Wednesday, October 19, 2016 2:40 PM 
To: Cooper, Harvi <[e-mail]> 
Subject: FW: Goldsboro Site Update and Need Your Help 

Harvey, 

As a follow‐up on our meeting today I am forwarding you Jeff Tyburski’s email concerning the 8,600 gallon of dewater 
with 5.4 ug/l of PCE. 

Thank you for your help 
Lebeed 

From: Tyburski, Jeff [mailto:[e-mail]]  
Sent: Thursday, October 13, 2016 10:17 AM 
To: Kady, Lebeed <[e-mail]> 
Subject: Goldsboro Site Update and Need Your Help 

Lebeed 

The Goldsboro site is progressing well. However, we have run into an issue where two restaurant tenants recently 
requested the installation of sub‐surface grease traps (two total). The installation of the grease traps encountered the 
water table. All soils below the water table were placed into a total of four (4) roll‐off boxes and sampled under the 
contained‐in policy as a precaution due to the known presence of a dry‐cleaning solvent groundwater plume from the 
nearby Penny Cleaners DSCA site. The excavation had to be dewatered to complete the work and the water 
(approximately 8,600‐gallons) was placed into a 20k gallon frac tank.  The sample results for the roll‐off boxes (ROB‐1 
through ROB‐4, “A” and “B” designations for the two samples per box per the contained‐in policy) indicate that the soil 
is non‐hazardous and plans are to ship it to a Subtitle D landfill. For the water in the frac tank, PCE showed up at a 
concentration of 5.4 ug/L. Available information from DSCA assessment reports suggest that the PCE is likely from the 
Penny Cleaners site. The other constituents detected in the water sample from the frac tank do not appear not to be 
associated with the dry‐cleaning solvent release. The lab results are attached. Note the REP‐1 sample is a composite of 
soil below the water table for additional analyses per the Subtitle D landfills requirements. 

3
For the PCE in water, the concentration of 5.4 ug/L is well below below the LDR of 0.056 mg/L (or 56.0 ug/L) – see 
below. Can this water be classified as non‐hazardous based on the use of the PCE LDR? Additionally, there is uncertainty 
if the detection is from virgin or spent solvent.  

This issue came up quickly and the site design/construction processes purposely avoided encountering groundwater up 
until this point. Your help and approval on how to manage this waste would certainly be appreciated as the cost to 
dispose of this much water as hazardous is very expensive (+ $40,000).  

Can you give me a call to discuss once you have read this? 

Sincerely, 

Jeff  

4

......................... ~···--........
F001, F001 , F002, F003, F004 andfor Acetone 67-64-1
F002, F005 solvent wastes that contain Benzene 71-43-2
F003, any combination of one or more of n-Buthyl alcohol 71-36-3
F004, the following spent solvents: Carbon disulfide 75-15-0
& acetone, benzene, n-butyl alcohol, Carbon tetrachloride 56-23-5
F005 carbon disulfide, carbon Chlorobenzene 108-
tetrachloride, chlorinated o-Cresol 90-7
fluorocarbons, chlorobenzene, m-Cresol (difficult to distinguish from 95-48-7
o-cresol, m-cresol, p-cresol, p-cresol) 108-
cyclohexanone, p-Cresol (difficult to distinguish from 39-4
o-dichlorobenzene, m-cresol)
2-ethoxyethanol, ethyl acetate, Cresol-mixed isomers (Cresylic acid) (sum 106-
ethyl benzene, ethyl ether, isobutyl of o-, m-, and p-cresol concentrations) 44-5
alcohol, methanol, methylene
chloride, methyl ethyl ketone, 1319-
methyl isobutyl ketone, 77-3
nitrobenzene, 2-nitropropane,
pyridine, tetrachloroethylene,
toluene, 1, 1, 1-trichloroethane,
1, 1,2-trichloroethane,
1, 1,2-tnchloro-1 ,2,2-trifluoroethane,
trichloroethylene,
trichlorofluoromethane, and/or
xylenes (except as specifically
noted in other subcategories]. See
further details of these listings in
§261 .31.
Cyclohexanone 108-
94-1
o-Dichlorobenzene 95-50-1
Ethyl acetate 141-
78-6
Ethyl benzene 100-
41-4
Ethyl ether 60-29-7
lsobutyl alcohol 78-83-1
Methanol 67-56-1
Methylene chloride 75-9-2
Methyl ethyl ketone 78-93-3
Methyl isobutyl ketone 108-
10-1
Nitrobenzene 98-95-3
Pyridine 110-
86-1
Tetrachloroethylene 127-
18-4
5
Jeffrey Tyburski, PG, RSM | Director of Environmental Services  
2905 Meridian Parkway | Durham, NC 27713 
Office: 919.361.5000 x 202 
Direct: 919.287.0732  
Mobile: [phone]  
McAdamsCo.com

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