SW_F_6403-CDLF-2000_11-05-2014_RM_GW

1 1 1 1 2 B R A N D I N G I R O N P LA C E , W E N D E L L, N C 2 7 5 9 1
919-3 6 6-3 6 6 3 O ff i c e ● 9 1 9 -995-0 3 6 3 C e l l ● b b o u t i n p g @ b e l l s o u t h . n e t

December 17, 2014

Ms. Jaclynne Drummond
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Solid Waste Section
P. O. Box 27687
Raleigh, NC 27611-7687

RE: Report of Results
Semi-Annual Groundwater and Surface Water Monitoring: November 2014
Nash County C&D Landfill
Nashville, Nash County, NC
Permit # 64-03

Dear Ms. Drummond:

This report presents the results of semi-annual groundwater and surface water quality monitoring
conducted at the C&D landfill site referenced above (Figure 1) in November 2014. The scope of work
performed included sampling and laboratory analysis of groundwater samples from six on-site monitoring
wells (MW-1 through MW-6) and surface water samples from two on-site locations (SW-3 and SW-4).
The groundwater and surface water samples were collected in accordance with the NCDENR, Division of
Waste Management (DWM), Solid Waste Section (SWS) Groundwater Monitoring Guidance Document
and the facility Water Quality Monitoring Plan. The sampling and data collection methods, as well as the
current and historical results of field and laboratory testing of the water samples, are presented in the
following sections.

1.0 POTENTIOMETRIC PATTERN AND GROUNDWATER FLOW

Groundwater levels were gauged in the site groundwater monitoring wells on November 5, 2014 as part
of the site monitoring. Depths to groundwater were measured using an electronic water-level meter that
was thoroughly decontaminated between wells with a non-phosphate soap and water wash followed in
order by multiple rinses with distilled water, an isopropyl alcohol rinse, and multiple distilled water
rinses. Depth-to-water measurements were made after the wells were opened for a sufficient period of
time to allow water levels to equilibrate with atmospheric pressure. The locations of the site monitoring
wells are depicted in Figure 2. Groundwater elevation data collected at the monitoring wells on
November 5, 2014 are presented in Table 1. The depth to groundwater across the site measured relative
to the top of the PVC casing of the Type II groundwater-monitoring wells on November 5, 2014, ranged
from 19.54 feet (MW-2) to 41.65 feet (MW-5), which is consistent with the surface topography. It is
– 2 – December 17, 2014
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919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
noted, however, that the depths to groundwater measured in November 2014 were significantly lower
than those measured in May 2014.

A water-table elevation contour map that was developed based on the November 5, 2014 groundwater-
gauging data for the Type II monitoring wells is presented as Figure 3. The pattern of the water-table
contours indicates that the horizontal component of shallow groundwater flow at the site is generally to
the northeast, which is consistent with the surface topography and drainage features at the site. The
delineated direction of shallow groundwater flow is also consistent with previous estimates of
groundwater flow direction at the site. The hydraulic gradient of the water table, based on the data
depicted in Figure 3, is approximately 0.028 ft/ft.

2.0 RESULTS OF GROUNDWATER AND SURFACE WATER SAMPLING AND ANALYSIS

Groundwater samples were collected from the site monitoring wells and surface water samples were
collected from two on-site locations on November 5 and 6, 2014 for laboratory analysis to monitor the
quality of groundwater and surface water at the site. It is noted that monitoring well MW-1 serves as the
up gradient, background well for the facility, and monitoring wells MW-2 through MW-6 serve as the
down gradient monitoring wells. The groundwater and surface water samples were collected and handled
in accordance with the sampling protocols included in the site Water Quality Monitoring Plan as well as
the SWS Groundwater Monitoring Guidance Document. Prior to groundwater sampling, monitoring
wells MW-1, MW-2, MW-3 and MW-6, were purged of stagnant water using pre-cleaned Teflon-
lined disposable polyethylene tubing connected to a peristaltic pump under low flow (≤ 200
ml/min) conditions. Monitoring wells MW-4 and MW-5 were purged and sampled using
disposable, bottom-loading PVC bailers. Surface water samples were collected directly into sample
containers by direct submersion in the stream. All reusable sampling equipment was properly
decontaminated between sampling locations with a non-phosphate soap and water wash, followed by
multiple rinses with distilled water. New disposable nitrile or latex gloves were worn during all sampling
activities. Disposable sampling equipment/material (e.g., disposable bailers, gloves, etc.) was discarded
after each use.

During purging, measurements were made in the field of the pH, temperature, specific conductance and
turbidity of the groundwater collected from the monitoring wells, in accordance with SWS requirements.
The results of the field analyses of these parameters are presented in Table 1. Copies of Groundwater
Sampling Forms containing pertinent information recorded in the field during purging and sampling at
each groundwater monitoring well are presented in Appendix A. The results of the field-measured water-
quality parameters indicate that the values measured in groundwater collected from the site monitoring
wells were generally within the applicable stabilization criteria with the exception of turbidity, which was
slightly elevated (>10 NTUs) at monitoring wells MW-4 and MW-5 (see Groundwater Sampling Forms).
Groundwater at the site is slightly acidic based on the pH values measured in the field (4.88 to 5.40).
Specific conductance values ranged from 36 (MW-3 and MW-5) to 70 (MW-4) S/cm and turbidity
– 3 – December 17, 2014
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919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
values ranged from 4.7 (MW-2) to 12.6 (MW-4) NTUs. It is noted that groundwater in monitoring wells
MW-4 and MW-5 was allowed to recover and settle for approximately 24 hours before the final turbidity
of the groundwater samples were measured and the samples collected.

Surface water samples were collected from two locations at the site (SW-3 and SW-4). The sampling
locations are depicted in Figure 2. SW-3 is located approximately 1,200-feet southeast (downstream) of
the C&D Landfill along Pig Basket Creek. SW-4 is located upstream where Pig Basket Creek runs under
a bridge at State Road 1411. All surface water samples were collected directly into sample containers by
direct submersion in the stream in accordance with the protocol presented in the SWS Groundwater
Monitoring Guidance Document.

All groundwater and surface water samples were analyzed at a North Carolina-certified laboratory for
Appendix I volatile organic compounds (VOCs) by SW 846 Method 8260 and the 8 RCRA metals by
EPA 6000/7000 series methods. Summarized results of laboratory analyses for groundwater and surface
water samples collected from the site in November 2014 are presented in Table 2. Summarized historical
groundwater and surface water quality data (from 2006 to present) for the site are presented in Table 3.
Copies of the original laboratory reports are included in Appendix B.

The laboratory analytical results for the surface water samples collected from the site in November 2014
indicate that no low levels of acetone were reported in samples SW-3 and SW-4 (5.3 µg/L and 6.2 µg/L,
respectively) which were well below the 15A NCAC 2L groundwater quality standard (6,000 µg/L) and
the 15A NCAC 2B surface water quality standard (2,000 µg/L for fresh water aquatic life). No other
VOCs were detected in either sample. Low levels of barium, chromium and lead were reported in both of
the surface water samples. It is noted that none of the reported concentrations of these metals in the
surface water samples exceed the corresponding 15A NCAC 2B surface water quality standards or the
15A NCAC 2L .0202 groundwater quality standards.

The laboratory analytical results for the groundwater samples collected from the site monitoring wells in
May 2014 indicate that trace levels of acetone and trichlorofluoromethane were reported in the
groundwater samples collected from MW-4 and MW-5, and a trace level of tetrahydrofuran was reported
in the groundwater sample collected from MW-4. In addition, a trace level of methylene chloride was
reported in the groundwater sample collected from background monitoring well MW-1 (1 µg/l). It is
noted that methylene chloride was also detected in the trip blank at a concentration of 1.7 µg/L, indicating
that the detection of methylene chloride in MW-1 may be the result of laboratory contamination. None of
the reported concentrations of these volatile organic constituents exceeds the corresponding 15A NCAC
2L .0202 groundwater quality standards. No other Appendix I VOCs were reported in any of the
groundwater samples.

The results of the metals analyses of the groundwater samples indicate that barium, cadmium and
chromium were reported in all of the samples, and lead was reported in four of the samples. Arsenic,
mercury, selenium and silver were not detected in any of the groundwater samples. None of the reported
– 4 – December 17, 2014
1 1 1 1 2 B R A N D I N G I R O N P LA C E , W E N D E L L, N C 2 7 5 9 1
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
concentrations of RCRA metals in the groundwater samples exceed the corresponding 15A NCAC 2L
.0202 groundwater quality standards.

3.0 CONCLUSIONS AND RECOMMENDATIONS

The results of the November 2014 groundwater and surface water quality monitoring conducted at the
Nash County C&D Landfill are generally consistent with the results of previous monitoring conducted at
the site. No volatile organic compounds or RCRA metals were reported in any of the groundwater or
surface water samples at concentrations that exceed the corresponding 15A NCAC 2L .0202 groundwater
quality standards or 15A NCAC 2B surface water quality standards.

If you have any questions or require further assistance regarding this report, please call me at 919-995-
0363. The next water quality monitoring event for the Nash County C&D Landfill is scheduled for May
2015.

Sincerely,
Brian S. Boutin, P.G.
Consulting Geologist

Cc: Mr. William W. Hill, Health Director, Nash County Health Department
Mr. Matthew Richardson, Nash County Landfill
Vance Moore, Garrett & Moore, Inc.
1
9
6
1
9
8
2
0
0
2
0
2
2
0
4
2
0
6
2
0
8
2
1
0
2
1
2
2
1
4
2
1
6
2
1
8
(221.04)
(216.54)
(207.45)(195.91)
(195.63)
(195.54)
MW-1 41.1 2.0 244.07 23.03 221.04 17.8 4.88 56 5.9
MW-2 37.2 2.0 236.08 19.54 216.54 17.6 5.27 48 4.7
MW-3 37.1 2.0 231.36 23.91 207.45 16.8 4.76 36 4.9
MW-4 41.8 2.0 229.51 33.60 195.91 16.2 5.07 70 12.6
MW-5 51.2 2.0 237.28 41.65 195.63 16.3 5.40 36 12.2
MW-6 41.9 2.0 221.09 25.55 195.54 17.0 4.99 30 6.9
Notes:MSL = Mean Sea Level
BTOC = Below Top of Casing
S.C. = Specific Conductance
ntu = Nephelometric Turbidity Units
Monitoring well construction data taken from October-December 2006 Sampling Event Monitoring Report prepared by Withers & Ravenel.
pH
Well
Identity
Well Diameter
(Inches)
Field Parameters
Turbidity
(ntu)
Top of Casing
Elevation
(ft. MSL)
Groundwater
Elevation
(ft. MSL)
Depth to
Groundwater
(ft. BTOC)
Well Depth
(Feet BGS)
Table 1
Permit # 64-03
Monitoring Well and Groundwater Data
Nash County C&D Landfill
Nashville, Nash County, North Carolina
November 5 and 6, 2014
Temp. Co S.C.
umhos/cm
ORGANIC CONSTITUENTS GWP Std NCAC 2L STD
(ug/L)(ug/L)(ug/L)
Acetone 5.3 6.2 ND ND ND 6.7 6 ND NE 6000
Acrylonitrile ND ND ND ND ND ND ND ND NE NE
Benzene ND ND ND ND ND ND ND ND NE 1
Bromochloromethane ND ND ND ND ND ND ND ND 0.6 NE
Bromodichloromethane ND ND ND ND ND ND ND ND NE 0.6
Bromoform (Tribromoethane)ND ND ND ND ND ND ND ND NE 4
Bromomethane (Methyl Bromide)ND ND ND ND ND ND ND ND NE 10
2-Butanone (MEK), (Methyl Ethyl Ketone)ND ND ND ND ND ND ND ND NE 4000
Carbon Disulfide ND ND ND ND ND ND ND ND NE 700
Carbon Tetrachloride ND ND ND ND ND ND ND ND NE 0.3
Chlorobenzene ND ND ND ND ND ND ND ND NE 50
Chloroethane (Ethyl Chloride)ND ND ND ND ND ND ND ND NE 3000
Chloroform (Trichloromethane)ND ND ND ND ND ND ND ND NE 70
1,2-Dibromo-3-Chloropropane (DBCP)ND ND ND ND ND ND ND ND NE 0.04
Dibromochloromethane (Chlorodibromomethane)ND ND ND ND ND ND ND ND 0.41 0.4
1,2,-Dibromoethane (Ethylene Dibromide)ND ND ND ND ND ND ND ND NE 0.02
Dibromomethane (Methylene Bromide)ND ND ND ND ND ND ND ND 5.5 NE
1,2-Dichlorobenzene (O-Dichlorobenzene)ND ND ND ND ND ND ND ND NE 20
1,3-Dichlorobenzene (M-Dichlorobenzene)ND ND ND ND ND ND ND ND NE 200
1,4-Dichlorobenzene (P-Dichlorobenzene)ND ND ND ND ND ND ND ND NE 6
Trans-1,4-Dichloro-2-butene ND ND ND ND ND ND ND ND NE NE
1,1-Dichloroethane ND ND ND ND ND ND ND ND NE 6
1,2-Dichloroethane (Ethylene Dichloride)ND ND ND ND ND ND ND ND NE 0.4
1,1-Dichloroethene (Vinylidene Chloride)ND ND ND ND ND ND ND ND NE 7
1,2-Dichloroethene (cis and trans isomers)ND ND ND ND ND ND ND ND 60 70
Dichlorofluoromethane (Freon-12; Halon)ND ND ND ND ND ND ND ND NE 1000
1,2-Dichloropropane (Propylene Dichloride)ND ND ND ND ND ND ND ND NE 0.6
1,1-Dichloropropene ND ND ND ND ND ND ND ND NE NE
1,3-Dichloropropene (cis and trans isomers)ND ND ND ND ND ND ND ND NE 0.4
Ethylbenzene ND ND ND ND ND ND ND ND NE 600
Iodomethane (Methyl Iodide)ND ND ND ND ND ND ND ND NE NE
2-Hexanone (Methyl Butyl Ketone)ND ND ND ND ND ND ND ND NE 40
Methyl Chloride (Chloromethane)ND ND 1 ND ND ND ND ND NE 3
Methylene Chloride (Dichloromethane)ND ND ND ND ND ND ND ND NE 5
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone)ND ND ND ND ND ND ND ND 560 NE
Styrene ND ND ND ND ND ND ND ND NE 70
1,1,1,2-Tetrachloroethane ND ND ND ND ND ND ND ND 1 NE
1,1,2,2-Tetrachloroethane ND ND ND ND ND ND ND ND 0.18 0.2
Tetrachloroethene (Tetrachloroethylene), (PCE)ND ND ND ND ND ND ND ND NE 0.7
Tetrahydrofuran ND ND ND ND ND 8.7 J ND ND NE NE
Toluene ND ND ND ND ND ND ND ND NE 600
1,1,1-Trichloroethane (Methylchloroform)ND ND ND ND ND ND ND ND NE 200
1,1,2-Trichloroethane ND ND ND ND ND ND ND ND 0.6 NE
Trichloroethene (Trichloroethylene), (TCE)ND ND ND ND ND ND ND ND NE 3
Trichlorofluoromethane (CFC-11) ND ND ND ND ND 2.6 2.9 ND NE 2000
1,2,3-Trichloropropane ND ND ND ND ND ND ND ND NE 0.005
Vinyl Acetate ND ND ND ND ND ND ND ND 88 NE
Vinyl Chloride ND ND ND ND ND ND ND ND NE 0.03
Total Xylenes ND ND ND ND ND ND ND ND NE 500
INORGANIC CONSTITUENTS GWP Std NCAC 2L STD
(in ug/L)(ug/L)(ug/L)
Arsenic ND ND ND ND ND ND ND ND NE 10
Barium 22.0 24.0 39.0 12.0 26.0 40.0 8.7 12.0 NE 700
Cadmium ND ND 0.37 J 0.47 J 0.22 J 0.44 J 0.10 J 0.13 J NE 2
Chromium 0.40 J 0.90 J 0.52 J 0.59 J 0.51 J 0.41 J 0.38 J 1.60 NE 10
Lead 0.38 J 0.39 J 0.25 J 0.20 J ND 5.1 2.3 ND NE 15
Mercury ND ND ND ND ND ND ND ND NE 1
Selenium ND ND ND ND ND ND ND ND NE 20
Silver ND ND ND ND ND ND ND ND NE 20
Notes:
Values in boldface exceed the corresponding 15A NCAC 2L .0202 groundwater quality standard for Class GA groundwater.NE - No standard established.
NCAC 2L STD = North Carolina Groundwater Standard established in Title 15A of North Carolina Administrative Code Subchapter 2L GWP - Solid Waste Section Groundwater Protection Standard
J = Estimated value above laboratory method detection limit and below SWSL or reporting limit.
B = Analyte found in associated field and/or laboratory blank.
SWSL = Solid Waste Section Limit
ND = None detected above laboratory method detection limit.
Laboratory Analytical Results for Surface Water and Groundwater Samples
Permit # 64-03
MW-1 MW-2 MW-6
NS = Not Sampled, No sample exists for this sampling period
Table 2
SW-3 SW-4 MW-4 MW-5
Nash County C&D Landfill, Nashville, North Carolina
MW-3
November 5 and 6, 2014
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/5/2014
Well No:MW-1
Arsenic 10 ND 3.8 J ND ND 1.92 J ND ND ND ND 0.98 J 0.2 J ND ND 0.43 J ND ND ND
Barium 700 32.00 55.3 JB 32.3 JB 47.6 J 43.1 JB 22.1 J 39.8 JB 31.00 25.00 43.00 27.00 58.00 28.00 15.00 34.00 43.00 39.00
Cadmium 2 ND 4.7 JB ND 0.18 J ND ND ND 0.36 J 3.40 0.44 J 0.78 J 0.49 J 0.22 J 0.076 J 0.091 J 0.085 J 0.37 J
Chromium 10 ND 4.95 JB 3.87 JB 1.42 JB 5.9 JB ND 3.89 J 0.6 J 0.55 J 1.5 J 2.1 B ND 0.78 J ND ND ND 0.52 J
Lead 15 ND 10.9 B 4.85 JB ND 8.22 JB 4.96 J ND ND ND 0.5 J 0.2 J 0.53 J 0.17 J 0.15 J 0.37 J 0.11 J 0.25 J
Mercury 1 ND 0.084 JB ND NA NA ND ND ND ND ND 0.039 JB ND ND ND ND ND ND
Selenium 20 ND 1.44 JB ND ND 8.16 J ND ND ND ND 0.81 J ND 0.85 JB 0.62 J ND ND ND ND
Silver 20 ND ND 3.17 JB ND 4.74 JB 1.65 JB ND ND ND 0.37 J ND 0.22 J ND ND ND ND ND
Ethylbenzene 600 ND 0.72 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.00
Toluene 600 ND 0.63 JB ND 0.18 J ND ND ND ND ND 1.20 ND ND ND ND ND ND ND
Total Xylenes 500 ND 1.16 J ND 0.41 J ND ND ND ND ND 1 J ND ND ND ND ND ND ND
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/5/2014
Well No:MW-2
Arsenic 10 ND ND 10.00 ND ND ND ND ND ND 0.89 J ND ND 0.15 J 1.10 0.5 J ND ND
Barium 700 11.00 25.4 JB 430 B 13.1 J 20.3 JB 15 J 157 B 26.00 11.00 12.00 21.00 15.00 8.80 8.60 9.50 15.00 12.00
Cadmium 2 ND 4.26 JB 0.16 J ND 0.32 J ND ND 0.25 J 1.20 0.59 J 0.4 J 5.30 0.54 J 0.31 J 0.23 J 0.22 J 0.47 J
Chromium 10 ND 3.64 JB 59.2 B 1.73 JB 4 JB 2.98 J 17.00 1.6 J 054 J 1.6 J 2.1 B ND 0.2 J ND ND ND 0.59 J
Lead 15 ND 14.5 B 47 B ND ND 4.86 J 18.10 0.98 J 0.31 J 0.9 J 0.86 J 0.52 J 0.36 J 3.50 0.42 J 0.15 J 0.20 J
Mercury 1 ND 0.084 JB ND NA NA ND ND ND ND ND 0.038 JB ND ND ND ND ND ND
Selenium 20 ND 17 JB 50.00 ND ND ND 6.79 J 3.3 J 0.23 J 1.30 ND 0.72 JB 0.6 J 0.46 J ND ND ND
Silver 20 ND ND 2.34 JB 1.07 JB 4.65 JB 1.83 JB ND ND ND 0.32 J ND 0.12 J ND 0.062 J ND ND ND
Ethylbenzene 600 ND ND ND ND 0.29 J ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride 5 ND ND 0.41 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ND 0.53 JB ND 0.107 J 1.08 ND ND ND 1.00 1.00 ND ND ND ND ND ND ND
Total Xylenes 500 ND ND ND 0.36 J 1.79 J ND ND ND 0.83 J 0.52 J ND ND ND ND ND ND ND
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/5/2014
Well No:MW-3
Arsenic 10 ND 4.02 J 10.00 ND 4.02 J ND ND ND ND 0.2 J 0.14 J ND ND ND ND ND ND
Barium 700 22.00 31.2 JB 445 B 24 J 58 JB 17.7 J 46.4 JB 27.00 34.00 28.00 27.00 28.00 29.00 26.00 32.00 37.00 26.00
Cadmium 2 ND 0.00608 JB 0.33 J ND ND ND ND ND ND ND ND 0.54 J ND 0.093 J 0.69 J 0.077 J 0.22 J
Chromium 10 ND 3.9 JB 72 B 2.49 JB 6.66 JB 1.34 J 3.9 J ND 1.00 1.3 J 2.5 B ND 1.00 ND 0.32 J ND 0.51 J
Lead 15 ND 1.19 B 83.5 B ND 7.79 JB 5.94 J 7.76 J 0.62 J 0.79 J 0.48 J 0.23 J 0.19 J 0.4 J ND 0.39 J 0.075 J ND
Mercury 1 ND 0.083 JB ND NA NA ND ND ND ND ND 0.032 JB ND ND ND ND ND ND
Selenium 20 ND 16.6 JB 98.50 ND ND ND ND ND ND 0.89 J ND 0.78 JB 0.45 J ND 0.19 J ND ND
Silver 20 ND ND ND 0.89 JB 3.74 JB 1.74 JB ND ND ND 0.1 J 0.072 J ND ND 0.022 J ND ND ND
Methylene Chloride 5 ND ND 0.26 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ND ND ND 0.19 J ND ND ND ND ND ND ND ND ND ND ND ND ND
Total Xylenes 500 ND ND ND 0.44 J ND ND ND ND ND ND ND ND ND ND ND ND ND
Table 3
Historical Summary of Constituent Detections
Nash County C&D Landfill
Nash County, North Carolina
Permit # 64-03
Page 1 of 3
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/6/2014
Well No:MW-4
Arsenic 10 25.00 0.01 ND ND 4.93 J ND ND ND 0.31 J 0.49 J 1.20 0.96 J 0.18 J 0.53 J 0.57 J 0.61 J ND
Barium 700 390.00 144 B 29.6 JB 37.4 J 44.3 JB 34.4 J 37.1 JB 54.00 41.00 37.00 35.00 57.00 27.00 37.00 71.00 51.00 40.00
Cadmium 2 ND 5.28 JB ND 0.27 J ND ND ND ND 0.34 J 0.48 J 0.48 J 0.13 0.25 J 0.43 J 0.33 J 0.56 J 0.44 J
Chromium 10 17.00 11 B 3.48 JB 2.5 JB 5.26 JB 3.72 J 1.85 J 0.59 J 0.56 J 1.2 J 2.9 B 0.36 J 0.62 J ND 0.00 0.13 J 0.41 J
Lead 15 160.00 70.5 B 3.93 JB 6.38 J 8.27 JB 19.90 8.94 J 6.60 6.60 6.40 5.20 25.00 2.10 11.00 30.00 12.00 5.10
Mercury 1 ND 0.106 JB ND NA NA ND ND ND 0.25 0.033 J 0.18 JB ND ND ND ND ND ND
Selenium 20 ND 15 JB ND ND ND ND ND 3 J 0.34 J 0.8 J ND 1.9 B 0.49 J ND ND ND ND
Silver 20 ND ND 3.50 JB 1.84 JB 4.4 JB 2.22 JB ND ND 0.094 J 0.072 J 0.25 J 0.65 J 0.1 J 0.11 J 0.045 J 0.16 J ND
Acetone 6000 ND ND ND ND ND ND ND ND ND ND 7.1 B 70.00 ND ND ND ND 6.70
Chloroform 70 ND ND ND ND ND 0.13 J ND ND ND ND ND ND ND ND ND ND ND
Chloroethane 3000 ND ND ND ND ND ND ND ND ND ND ND 0.31 J ND ND ND ND ND
1,1,-Dichloroethane 0.4 ND ND ND ND ND 0.12 J ND ND ND ND ND ND ND ND ND ND ND
Cis-1,2-Dichloroethene 70 ND ND 0.25 J 0.2 J 0.18 J 0.17 J 0.29 J ND ND ND ND ND ND ND ND ND ND
Dichlorofluoromethane 1000 ND ND ND ND ND ND ND 2.20 ND ND ND ND ND ND ND ND ND
Methylene Chloride 5 ND 0.52 JB 1.07 JB ND 0.74 J 0.65 J ND ND 1.00 0.6 J 0.64 JB 0.36 J 0.68 J 0.81 J ND ND ND
Tetrachloroethene 0.7 ND ND 0.21 J 0.41 J 0.24 J 0.43 J ND ND ND ND ND 0.36 J ND ND ND ND ND
Tetrahydrofuran NE NA NA NA NA NA NA NA NA 23.00 12.00 15.00 9.9 J 14.00 14.00 17.00 6.4 J 8.7 J
Trichloroethene 3 ND ND 0.29 J 0.19 J 0.25 J 0.19 J ND ND ND ND ND 0.75 J ND ND ND ND ND
Trichlorofluoromethane 2100 ND 3.81 12.30 8.75 8.55 8.08 6.40 4.60 8.50 3.80 3.30 3.10 4.50 2.00 3.40 1.60 2.60
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/6/2014
Well No:MW-5
Arsenic 10 ND 0.01 4.38 J ND 2.28 J ND ND ND ND ND 0.38 J ND 0.36 J 0.49 J ND ND ND
Barium 700 7.4 J 233 B 83.2 JB 54.7 J 7.67 JB 14.2 J 5.65 JB 14.00 42.00 8.60 11.00 54.00 7.90 7.60 22.00 8.80 8.70
Cadmium 2 0.3 J 5.05 JB ND 2.4 J 0.14 J ND ND ND ND ND ND 0.28 J ND 0.42 J 0.38 J 0.089 J 0.10 J
Chromium 10 ND 11.5 B 10.5 B 6.92 JB 8.68 JB 3.63 J 5.36 J 1.2 J 2.40 1.1 J 1.6 JB 0.19 J 1.40 ND ND ND 0.38 J
Lead 15 ND 147 B 83.2 B 46.30 81.3 B 27.30 48.00 8.30 41.00 3.60 3.20 43.00 2.90 1.00 21.00 2.20 2.30
Mercury 1 ND 0.107 JB ND NA NA ND ND ND ND ND 0.037 JB ND ND ND ND ND ND
Selenium 20 ND 13.9 JB 10.00 12.1 B 13.30 ND 4.32 J ND ND 0.92 J ND 0.58 J 0.5 J ND 0.15 J ND ND
Silver 20 ND 0.99 J 3.39 JB 1.72 JB 4.65 JB 1.67 JB ND ND ND ND ND 0.17 J ND ND ND ND ND
Acetone 6000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6.00
Chloroform 70 ND 0.32 J 0.34 J 0.17 J 0.28 J ND 0.21 J ND ND ND ND ND ND ND ND ND ND
Trichlorofluoromethane 2100 ND 1.18 J 0.28 J 0.59 J ND ND ND ND ND ND 0.76 1.20 1.40 ND 1.70 1.70 2.90
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/5/2014
Well No:MW-6
Arsenic 10 ND 2.78 J ND ND 2.81 J ND ND ND ND 1.00 0.34 J 0.14 J ND 0.72 J 0.47 J ND ND
Barium 700 14.00 22.5 JB 28.5 JB 10.5 J 31.3 JB ND 24.7 JB 16.00 18.00 13.00 16.00 16.00 11.00 13.00 12.00 32.00 12.00
Cadmium 2 ND 5.01 JB ND 0.56 J 0.61 J ND ND 0.47 J 0.66 J 0.6 J 1.20 0.2 J 0.34 J 0.1 J 0.066 J 0.14 J 0.13 J
Chromium 10 ND 5.09 JB 14.1 B 3.56 JB 6.78 JB 2.53 J 3.12 J 2.1 J 1.50 2.20 3 B 0.34 J 2.50 0.8 J 0.71 J 1.70 1.60
Lead 15 ND 8.66 JB 7.95 JB ND 7.2 JB ND ND ND 0.43 J 0.26 J 0.4 J 0.17 J 0.19 J ND 0.3 J 0.14 J ND
Mercury 1 ND 0.083 JB ND NA NA ND ND ND ND ND 0.034 JB ND ND ND ND ND ND
Selenium 20 ND 14 JB ND ND ND ND ND ND ND 0.5 J ND 0.6 JB 0.00 ND 0.28 J ND ND
Silver 20 ND ND 3.04 JB ND 4.37 JB 1.85 JB ND ND ND ND 0.087 J 0.063 J 0.62 J 0.031 J ND ND ND
Ethylbenzene 600 ND ND ND ND 0.23 J ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ND ND ND 0.21 J 0.84 J ND ND ND 0.87 J 1.60 ND ND ND ND ND ND ND
Total Xylenes 500 ND ND ND 0.41 J 1.57 J ND ND ND 0.75 J 1.8 J ND ND ND ND ND ND ND
Page 2 of 3
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/6/2014
Sample No:SW-3
Arsenic 10 ND 3.36 J ND ND 3.02 J ND ND ND 0.65 J 1.90 0.79 J 0.97 J 0.46 J 1.20 0.77 J 0.72 J ND
Barium 700 29.00 34.2 JB 38.2 JB 29.7 J 46.9 JB 29.5 J 47.5 JB 34.00 34.00 41.00 31.00 41.00 23.00 24.00 32.00 33.00 22.00
Cadmium 2 ND 4.59 JB ND ND ND 1.20 ND ND ND 1.30 ND ND ND ND ND 0.26 J ND
Chromium 10 ND 4.55 JB 3.87 JB 3.41 JB 4.88 JB 2.9 J 1.76 J ND 0.56 J 1.8 J 2.1 B ND 0.75 J ND ND 0.87 J 0.40 J
Lead 15 ND 15.2 B 7.40 JB 5.79 J 4.06 JB 6.58 J ND 0.73 J 0.93 J 2.50 0.69 J 1.30 0.54 J 0.83 J 0.8 J 1.70 0.38 J
Mercury 1 ND 0.083 JB ND NA NA ND ND ND ND ND 0.04 JB ND ND ND ND ND ND
Selenium 20 ND 12.4 JB ND ND ND ND ND 4.8 J 0.27 J 1.20 ND 0.77 JB 0.6 J ND ND 0.40 J ND
Silver 20 ND ND 3.17 JB 1.21 JB 4.65 JB 1.6 JB ND ND ND ND ND 0.064 J ND 0.024 J ND ND ND
Acetone 6000 ND ND 5 J 4.46 J ND 3.83 ND ND ND ND 4.5 JB 3.4 J ND ND ND ND 5.30
Sampling Date:NCAC 2L STD 11/1/2006 5/17/2007 11/6/2007 5/7/2008 11/21/2008 5/6/2009 11/18/2009 5/6/2010 11/19/2010 5/10/2011 11/14/2011 5/3/2012 11/9/2012 5/9/2013 10/31/2013 5/1/2014 11/6/2014
Sample No:SW-4
Arsenic 10 ND 3.09 J ND ND ND ND ND ND 0.65 J 2.00 0.6 J 0.68 J 0.87 J 1.50 0.42 J 0.65 J ND
Barium 700 29.00 43.7 JB 42.5 JB 39.1 J 47.1 JB 26.3 J 43.8 JB 37.00 34.00 42.00 28.00 37.00 21.00 20.00 54.00 33.00 24.00
Cadmium 2 ND 4.49 JB ND ND ND ND ND ND ND 0.22 J 0.36 J ND ND 0.045 J ND 0.055 J ND
Chromium 10 ND 4.04 JB 4.88 JB 3.25 JB 3.74 JB 2.44 J 3.02 J ND 0.64 J 2.30 2.1 B ND 0.77 J ND ND 0.58 J 0.90 J
Lead 15 ND 12.7 B 5.71 JB 4.71 J 3.95 JB ND ND 0.81 J 0.79 J 2.10 0.65 J 1.40 0.42 J 1.10 1.20 1.60 0.39 J
Mercury 1 ND 0.087 JB ND NA NA ND ND ND ND ND 0.039 JB ND ND ND ND ND ND
Selenium 20 ND 17.9 JB ND ND ND ND ND 3.6 J 0.23 J 1.20 ND 0.98 JB 0.83 J 0.71 J 0.31 J 0.19 J ND
Silver 20 ND ND 3.29 JB 1.26 JB 4.93 JB 1.41 JB ND ND ND ND ND 1.2 J ND ND ND ND ND
Acetone 6000 ND ND ND 2.6 J ND 3.48 ND ND ND ND 3.8 JB 4 J ND ND ND ND 6.20
All results in µg/lNCAC 2L STD = North Carolina Groundwater Standard established in Title 15A of North Carolina Administrative Code Subchapter 2L
NCAC 2L STD and Laboratory Results are in mg/L
ND - Not Detected above the Laboratory Reporting Limit NE - Not Established
J = Estimated value above laboratory MDL and below SWSL or reporting limit.B = Analyte found in associated field and/or laboratory blank.
Laboratory results in bold exceed NCAC 2L STD NA = Not analyzed
Page 3 of 3

1 1 1 1 2 B R A N D I N G I R O N P LA C E , W E N D E L L, N C 2 7 5 9 1
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
APPENDIX A

Groundwater Sampling Forms

1 1 1 1 2 B R A N D I N G I R O N P LA C E , W E N D E L L, N C 2 7 5 9 1
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
APPENDIX B

Laboratory Reports
And
Chain-of-Custody Records

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
11/25/2014
Nautilus Geologic Consulting, PLLC
Brian S. Boutin
11112 Branding Iron Place
Wendell, NC 27591
Project: Nash County C&D Landfill
Project No.: 64-03
Lab Submittal Date: 11/07/2014
Prism Work Order: 4110128
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Methylene Chloride is present in the Trip Blank that was prepared at the laboratory. The Methylene
Chloride present in the client sample (6403-MW1) is possible lab contamination.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
H1 Analysis within hold time from preserved vial.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 28
Sample Receipt Summary
11/25/2014
Prism Work Order: 4110128
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
4110128-01 11/06/146403-Trip Blank 11/07/14Water
4110128-02 11/05/146403-MW1 11/07/14Water
4110128-03 11/05/146403-MW2 11/07/14Water
4110128-04 11/05/146403-MW3 11/07/14Water
4110128-05 11/05/146403-MW6 11/07/14Water
4110128-06 11/06/146403-MW4 11/07/14Water
4110128-07 11/06/146403-MW5 11/07/14Water
4110128-08 11/06/146403-SW3 11/07/14Water
4110128-09 11/06/146403-SW4 11/07/14Water
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 28
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 4110128
11/25/2014
Summary of Detections
1.7 ug/L4110128-01 6403-Trip Blank Methylene Chloride 8260B
39 ug/L4110128-02 6403-MW1 Barium 6020A
0.37 J ug/L4110128-02 6403-MW1 Cadmium 6020A
0.52 J ug/L4110128-02 6403-MW1 Chromium 6020A
0.25 J ug/L4110128-02 6403-MW1 Lead 6020A
1.0 ug/L4110128-02 6403-MW1 Methylene Chloride 8260B
12 ug/L4110128-03 6403-MW2 Barium 6020A
0.47 J ug/L4110128-03 6403-MW2 Cadmium 6020A
0.59 J ug/L4110128-03 6403-MW2 Chromium 6020A
0.20 J ug/L4110128-03 6403-MW2 Lead 6020A
26 ug/L4110128-04 6403-MW3 Barium 6020A
0.22 J ug/L4110128-04 6403-MW3 Cadmium 6020A
0.51 J ug/L4110128-04 6403-MW3 Chromium 6020A
12 ug/L4110128-05 6403-MW6 Barium 6020A
0.13 J ug/L4110128-05 6403-MW6 Cadmium 6020A
1.6 ug/L4110128-05 6403-MW6 Chromium 6020A
40 ug/L4110128-06 6403-MW4 Barium 6020A
0.44 J ug/L4110128-06 6403-MW4 Cadmium 6020A
0.41 J ug/L4110128-06 6403-MW4 Chromium 6020A
5.1 ug/L4110128-06 6403-MW4 Lead 6020A
6.7 ug/L4110128-06 6403-MW4 Acetone 8260B
8.7 J ug/L4110128-06 6403-MW4 Tetrahydrofuran 8260B
2.6 ug/L4110128-06 6403-MW4 Trichlorofluoromethane 8260B
8.7 ug/L4110128-07 6403-MW5 Barium 6020A
0.10 J ug/L4110128-07 6403-MW5 Cadmium 6020A
0.38 J ug/L4110128-07 6403-MW5 Chromium 6020A
2.3 ug/L4110128-07 6403-MW5 Lead 6020A
6.0 ug/L4110128-07 6403-MW5 Acetone 8260B
2.9 ug/L4110128-07 6403-MW5 Trichlorofluoromethane 8260B
22 ug/L4110128-08 6403-SW3 Barium 6020A
0.40 J ug/L4110128-08 6403-SW3 Chromium 6020A
0.38 J ug/L4110128-08 6403-SW3 Lead 6020A
5.3 ug/L4110128-08 6403-SW3 Acetone 8260B
24 ug/L4110128-09 6403-SW4 Barium 6020A
0.90 J ug/L4110128-09 6403-SW4 Chromium 6020A
0.39 J ug/L4110128-09 6403-SW4 Lead 6020A
6.2 ug/L4110128-09 6403-SW4 Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-Trip Blank
Prism Sample ID: 4110128-01
Prism Work Order: 4110128
Time Collected: 11/06/14 00:00
Time Submitted: 11/07/14 08:40
64-03
Volatile Organic Compounds by GC/MS
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018611.0 11/12/14 16:47 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018612.0 11/12/14 16:47 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.0681,4-Dichlorobenzene
BRL 8260B P4K018615.0 11/12/14 16:47 CGPug/L 0.62Acetone
BRL 8260B P4K018612011/12/14 16:47 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.072Benzene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018611.0 11/12/14 16:47 CGPug/L 0.27Bromoform
BRL 8260B P4K018611.0 11/12/14 16:47 CGPug/L 0.47Bromomethane
BRL 8260B P4K018615.0 11/12/14 16:47 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.13Chloroethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.089Chloroform
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.11Chloromethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018611.0 11/12/14 16:47 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018615.0 11/12/14 16:47 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P4K018615.0 11/12/14 16:47 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018615.0 11/12/14 16:47 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018615.0 11/12/14 16:47 CGPug/L 0.12Methyl Isobutyl Ketone
1.7 8260B P4K018611.0 11/12/14 16:47 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.046o-Xylene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.047Styrene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018611011/12/14 16:47 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.042Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-Trip Blank
Prism Sample ID: 4110128-01
Prism Work Order: 4110128
Time Collected: 11/06/14 00:00
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018611011/12/14 16:47 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018612.0 11/12/14 16:47 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018610.50 11/12/14 16:47 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018613.0 11/12/14 16:47 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124104 %4-Bromofluorobenzene
75-129105 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW1
Prism Sample ID: 4110128-02
Prism Work Order: 4110128
Time Collected: 11/05/14 12:00
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:30 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/12/14 23:40 BGMug/L 0.62Arsenic
39 6020A P4K014815.0 11/12/14 23:40 BGMug/L 0.50Barium
0.37 6020A P4K014811.0 11/12/14 23:40 BGMJug/L 0.074Cadmium
0.52 6020A P4K014811.0 11/12/14 23:40 BGMJug/L 0.26Chromium
0.25 6020A P4K014811.0 11/12/14 23:40 BGMJug/L 0.18Lead
BRL 6020A P4K014811.0 11/12/14 23:40 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/12/14 23:40 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS H1
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018411.0 11/13/14 16:55 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018412.0 11/13/14 16:55 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.0681,4-Dichlorobenzene
BRL 8260B P4K018415.0 11/13/14 16:55 CGPug/L 0.62Acetone
BRL 8260B P4K018412011/13/14 16:55 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.072Benzene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018411.0 11/13/14 16:55 CGPug/L 0.27Bromoform
BRL 8260B P4K018411.0 11/13/14 16:55 CGPug/L 0.47Bromomethane
BRL 8260B P4K018415.0 11/13/14 16:55 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.13Chloroethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.089Chloroform
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.11Chloromethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018411.0 11/13/14 16:55 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018415.0 11/13/14 16:55 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW1
Prism Sample ID: 4110128-02
Prism Work Order: 4110128
Time Collected: 11/05/14 12:00
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018415.0 11/13/14 16:55 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018415.0 11/13/14 16:55 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018415.0 11/13/14 16:55 CGPug/L 0.12Methyl Isobutyl Ketone
1.0 8260B P4K018411.0 11/13/14 16:55 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.046o-Xylene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.047Styrene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018411011/13/14 16:55 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.042Toluene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018411011/13/14 16:55 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018412.0 11/13/14 16:55 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018410.50 11/13/14 16:55 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018413.0 11/13/14 16:55 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124105 %4-Bromofluorobenzene
75-129106 %Dibromofluoromethane
77-123103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW2
Prism Sample ID: 4110128-03
Prism Work Order: 4110128
Time Collected: 11/05/14 12:55
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:33 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/12/14 23:43 BGMug/L 0.62Arsenic
12 6020A P4K014815.0 11/12/14 23:43 BGMug/L 0.50Barium
0.47 6020A P4K014811.0 11/12/14 23:43 BGMJug/L 0.074Cadmium
0.59 6020A P4K014811.0 11/12/14 23:43 BGMJug/L 0.26Chromium
0.20 6020A P4K014811.0 11/12/14 23:43 BGMJug/L 0.18Lead
BRL 6020A P4K014811.0 11/12/14 23:43 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/12/14 23:43 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS H1
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018411.0 11/13/14 17:20 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018412.0 11/13/14 17:20 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.0681,4-Dichlorobenzene
BRL 8260B P4K018415.0 11/13/14 17:20 CGPug/L 0.62Acetone
BRL 8260B P4K018412011/13/14 17:20 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.072Benzene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018411.0 11/13/14 17:20 CGPug/L 0.27Bromoform
BRL 8260B P4K018411.0 11/13/14 17:20 CGPug/L 0.47Bromomethane
BRL 8260B P4K018415.0 11/13/14 17:20 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.13Chloroethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.089Chloroform
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.11Chloromethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018411.0 11/13/14 17:20 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018415.0 11/13/14 17:20 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW2
Prism Sample ID: 4110128-03
Prism Work Order: 4110128
Time Collected: 11/05/14 12:55
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018415.0 11/13/14 17:20 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018415.0 11/13/14 17:20 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018415.0 11/13/14 17:20 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018411.0 11/13/14 17:20 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.046o-Xylene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.047Styrene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018411011/13/14 17:20 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.042Toluene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018411011/13/14 17:20 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018412.0 11/13/14 17:20 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018410.50 11/13/14 17:20 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018413.0 11/13/14 17:20 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124106 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW3
Prism Sample ID: 4110128-04
Prism Work Order: 4110128
Time Collected: 11/05/14 13:45
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:37 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/12/14 23:47 BGMug/L 0.62Arsenic
26 6020A P4K014815.0 11/12/14 23:47 BGMug/L 0.50Barium
0.22 6020A P4K014811.0 11/12/14 23:47 BGMJug/L 0.074Cadmium
0.51 6020A P4K014811.0 11/12/14 23:47 BGMJug/L 0.26Chromium
BRL 6020A P4K014811.0 11/12/14 23:47 BGMug/L 0.18Lead
BRL 6020A P4K014811.0 11/12/14 23:47 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/12/14 23:47 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS H1
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018411.0 11/13/14 17:46 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018412.0 11/13/14 17:46 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.0681,4-Dichlorobenzene
BRL 8260B P4K018415.0 11/13/14 17:46 CGPug/L 0.62Acetone
BRL 8260B P4K018412011/13/14 17:46 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.072Benzene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018411.0 11/13/14 17:46 CGPug/L 0.27Bromoform
BRL 8260B P4K018411.0 11/13/14 17:46 CGPug/L 0.47Bromomethane
BRL 8260B P4K018415.0 11/13/14 17:46 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.13Chloroethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.089Chloroform
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.11Chloromethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018411.0 11/13/14 17:46 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018415.0 11/13/14 17:46 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW3
Prism Sample ID: 4110128-04
Prism Work Order: 4110128
Time Collected: 11/05/14 13:45
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018415.0 11/13/14 17:46 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018415.0 11/13/14 17:46 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018415.0 11/13/14 17:46 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018411.0 11/13/14 17:46 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.046o-Xylene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.047Styrene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018411011/13/14 17:46 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.042Toluene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018411011/13/14 17:46 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018412.0 11/13/14 17:46 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018410.50 11/13/14 17:46 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018413.0 11/13/14 17:46 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124105 %4-Bromofluorobenzene
75-129105 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW6
Prism Sample ID: 4110128-05
Prism Work Order: 4110128
Time Collected: 11/05/14 15:55
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:41 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/12/14 23:50 BGMug/L 0.62Arsenic
12 6020A P4K014815.0 11/12/14 23:50 BGMug/L 0.50Barium
0.13 6020A P4K014811.0 11/12/14 23:50 BGMJug/L 0.074Cadmium
1.6 6020A P4K014811.0 11/12/14 23:50 BGMug/L 0.26Chromium
BRL 6020A P4K014811.0 11/12/14 23:50 BGMug/L 0.18Lead
BRL 6020A P4K014811.0 11/12/14 23:50 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/12/14 23:50 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS H1
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018411.0 11/13/14 18:11 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018412.0 11/13/14 18:11 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.0681,4-Dichlorobenzene
BRL 8260B P4K018415.0 11/13/14 18:11 CGPug/L 0.62Acetone
BRL 8260B P4K018412011/13/14 18:11 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.072Benzene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018411.0 11/13/14 18:11 CGPug/L 0.27Bromoform
BRL 8260B P4K018411.0 11/13/14 18:11 CGPug/L 0.47Bromomethane
BRL 8260B P4K018415.0 11/13/14 18:11 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.13Chloroethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.089Chloroform
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.11Chloromethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018411.0 11/13/14 18:11 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018415.0 11/13/14 18:11 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW6
Prism Sample ID: 4110128-05
Prism Work Order: 4110128
Time Collected: 11/05/14 15:55
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018415.0 11/13/14 18:11 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018415.0 11/13/14 18:11 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018415.0 11/13/14 18:11 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018411.0 11/13/14 18:11 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.046o-Xylene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.047Styrene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018411011/13/14 18:11 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.042Toluene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018411011/13/14 18:11 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018412.0 11/13/14 18:11 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018410.50 11/13/14 18:11 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018413.0 11/13/14 18:11 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124105 %4-Bromofluorobenzene
75-129105 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW4
Prism Sample ID: 4110128-06
Prism Work Order: 4110128
Time Collected: 11/06/14 10:20
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:45 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/13/14 0:02 BGMug/L 0.62Arsenic
40 6020A P4K014815.0 11/13/14 0:02 BGMug/L 0.50Barium
0.44 6020A P4K014811.0 11/13/14 0:02 BGMJug/L 0.074Cadmium
0.41 6020A P4K014811.0 11/13/14 0:02 BGMJug/L 0.26Chromium
5.1 6020A P4K014811.0 11/13/14 0:02 BGMug/L 0.18Lead
BRL 6020A P4K014811.0 11/13/14 0:02 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/13/14 0:02 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018611.0 11/12/14 19:46 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018612.0 11/12/14 19:46 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.0681,4-Dichlorobenzene
6.7 8260B P4K018615.0 11/12/14 19:46 CGPug/L 0.62Acetone
BRL 8260B P4K018612011/12/14 19:46 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.072Benzene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018611.0 11/12/14 19:46 CGPug/L 0.27Bromoform
BRL 8260B P4K018611.0 11/12/14 19:46 CGPug/L 0.47Bromomethane
BRL 8260B P4K018615.0 11/12/14 19:46 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.13Chloroethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.089Chloroform
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.11Chloromethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018611.0 11/12/14 19:46 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018615.0 11/12/14 19:46 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW4
Prism Sample ID: 4110128-06
Prism Work Order: 4110128
Time Collected: 11/06/14 10:20
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018615.0 11/12/14 19:46 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018615.0 11/12/14 19:46 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018615.0 11/12/14 19:46 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018611.0 11/12/14 19:46 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.046o-Xylene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.047Styrene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.069Tetrachloroethylene
8.7 8260B P4K018611011/12/14 19:46 CGPJug/L 1.5Tetrahydrofuran
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.042Toluene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018611011/12/14 19:46 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.054Trichloroethylene
2.6 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018612.0 11/12/14 19:46 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018610.50 11/12/14 19:46 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018613.0 11/12/14 19:46 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124104 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-123104 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW5
Prism Sample ID: 4110128-07
Prism Work Order: 4110128
Time Collected: 11/06/14 10:35
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:49 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/13/14 0:05 BGMug/L 0.62Arsenic
8.7 6020A P4K014815.0 11/13/14 0:05 BGMug/L 0.50Barium
0.10 6020A P4K014811.0 11/13/14 0:05 BGMJug/L 0.074Cadmium
0.38 6020A P4K014811.0 11/13/14 0:05 BGMJug/L 0.26Chromium
2.3 6020A P4K014811.0 11/13/14 0:05 BGMug/L 0.18Lead
BRL 6020A P4K014811.0 11/13/14 0:05 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/13/14 0:05 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018611.0 11/12/14 20:11 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018612.0 11/12/14 20:11 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.0681,4-Dichlorobenzene
6.0 8260B P4K018615.0 11/12/14 20:11 CGPug/L 0.62Acetone
BRL 8260B P4K018612011/12/14 20:11 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.072Benzene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018611.0 11/12/14 20:11 CGPug/L 0.27Bromoform
BRL 8260B P4K018611.0 11/12/14 20:11 CGPug/L 0.47Bromomethane
BRL 8260B P4K018615.0 11/12/14 20:11 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.13Chloroethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.089Chloroform
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.11Chloromethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018611.0 11/12/14 20:11 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018615.0 11/12/14 20:11 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-MW5
Prism Sample ID: 4110128-07
Prism Work Order: 4110128
Time Collected: 11/06/14 10:35
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018615.0 11/12/14 20:11 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018615.0 11/12/14 20:11 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018615.0 11/12/14 20:11 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018611.0 11/12/14 20:11 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.046o-Xylene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.047Styrene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018611011/12/14 20:11 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.042Toluene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018611011/12/14 20:11 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.054Trichloroethylene
2.9 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018612.0 11/12/14 20:11 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018610.50 11/12/14 20:11 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018613.0 11/12/14 20:11 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124104 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-SW3
Prism Sample ID: 4110128-08
Prism Work Order: 4110128
Time Collected: 11/06/14 09:50
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:52 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/13/14 0:09 BGMug/L 0.62Arsenic
22 6020A P4K014815.0 11/13/14 0:09 BGMug/L 0.50Barium
BRL 6020A P4K014811.0 11/13/14 0:09 BGMug/L 0.074Cadmium
0.40 6020A P4K014811.0 11/13/14 0:09 BGMJug/L 0.26Chromium
0.38 6020A P4K014811.0 11/13/14 0:09 BGMJug/L 0.18Lead
BRL 6020A P4K014811.0 11/13/14 0:09 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/13/14 0:09 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018611.0 11/12/14 20:37 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018612.0 11/12/14 20:37 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.0681,4-Dichlorobenzene
5.3 8260B P4K018615.0 11/12/14 20:37 CGPug/L 0.62Acetone
BRL 8260B P4K018612011/12/14 20:37 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.072Benzene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018611.0 11/12/14 20:37 CGPug/L 0.27Bromoform
BRL 8260B P4K018611.0 11/12/14 20:37 CGPug/L 0.47Bromomethane
BRL 8260B P4K018615.0 11/12/14 20:37 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.13Chloroethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.089Chloroform
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.11Chloromethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018611.0 11/12/14 20:37 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018615.0 11/12/14 20:37 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-SW3
Prism Sample ID: 4110128-08
Prism Work Order: 4110128
Time Collected: 11/06/14 09:50
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018615.0 11/12/14 20:37 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018615.0 11/12/14 20:37 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018615.0 11/12/14 20:37 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018611.0 11/12/14 20:37 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.046o-Xylene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.047Styrene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018611011/12/14 20:37 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.042Toluene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018611011/12/14 20:37 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018612.0 11/12/14 20:37 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018610.50 11/12/14 20:37 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018613.0 11/12/14 20:37 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124106 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-SW4
Prism Sample ID: 4110128-09
Prism Work Order: 4110128
Time Collected: 11/06/14 10:05
Time Submitted: 11/07/14 08:40
64-03
Total Metals
BRL 7470A P4K019610.20 11/14/14 10:56 BGMug/L 0.012Mercury
BRL 6020A P4K014811.0 11/13/14 0:12 BGMug/L 0.62Arsenic
24 6020A P4K014815.0 11/13/14 0:12 BGMug/L 0.50Barium
BRL 6020A P4K014811.0 11/13/14 0:12 BGMug/L 0.074Cadmium
0.90 6020A P4K014811.0 11/13/14 0:12 BGMJug/L 0.26Chromium
0.39 6020A P4K014811.0 11/13/14 0:12 BGMJug/L 0.18Lead
BRL 6020A P4K014811.0 11/13/14 0:12 BGMug/L 0.73Selenium
BRL 6020A P4K014811.0 11/13/14 0:12 BGMug/L 0.040Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.151,1,1,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.0631,1,1-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.0711,1,2,2-Tetrachloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.171,1,2-Trichloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.0961,1-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.0781,1-Dichloroethylene
BRL 8260B P4K018611.0 11/12/14 21:02 CGPug/L 0.0811,2,3-Trichloropropane
BRL 8260B P4K018612.0 11/12/14 21:02 CGPug/L 0.591,2-Dibromo-3-chloropropane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.141,2-Dibromoethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.141,2-Dichloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.131,2-Dichloropropane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.0681,4-Dichlorobenzene
6.2 8260B P4K018615.0 11/12/14 21:02 CGPug/L 0.62Acetone
BRL 8260B P4K018612011/12/14 21:02 CGPug/L 0.86Acrylonitrile
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.072Benzene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.13Bromochloromethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.062Bromodichloromethane
BRL 8260B P4K018611.0 11/12/14 21:02 CGPug/L 0.27Bromoform
BRL 8260B P4K018611.0 11/12/14 21:02 CGPug/L 0.47Bromomethane
BRL 8260B P4K018615.0 11/12/14 21:02 CGPug/L 1.4Carbon disulfide
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.12Carbon Tetrachloride
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.061Chlorobenzene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.13Chloroethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.089Chloroform
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.11Chloromethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.076cis-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.10cis-1,3-Dichloropropylene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.30Dibromochloromethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.13Dibromomethane
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.067Ethylbenzene
BRL 8260B P4K018611.0 11/12/14 21:02 CGPug/L 0.081m,p-Xylenes
BRL 8260B P4K018615.0 11/12/14 21:02 CGPug/L 0.19Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 28
Laboratory Report
11/25/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID: 6403-SW4
Prism Sample ID: 4110128-09
Prism Work Order: 4110128
Time Collected: 11/06/14 10:05
Time Submitted: 11/07/14 08:40
64-03
BRL 8260B P4K018615.0 11/12/14 21:02 CGPug/L 0.90Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P4K018615.0 11/12/14 21:02 CGPug/L 0.45Methyl Iodide
BRL 8260B P4K018615.0 11/12/14 21:02 CGPug/L 0.12Methyl Isobutyl Ketone
BRL 8260B P4K018611.0 11/12/14 21:02 CGPug/L 0.44Methylene Chloride
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.046o-Xylene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.047Styrene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.069Tetrachloroethylene
BRL 8260B P4K018611011/12/14 21:02 CGPug/L 1.5Tetrahydrofuran
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.042Toluene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.12trans-1,2-Dichloroethylene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.043trans-1,3-Dichloropropylene
BRL 8260B P4K018611011/12/14 21:02 CGPug/L 0.51trans-1,4-Dichloro-2-butene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.054Trichloroethylene
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.088Trichlorofluoromethane
BRL 8260B P4K018612.0 11/12/14 21:02 CGPug/L 0.10Vinyl acetate
BRL 8260B P4K018610.50 11/12/14 21:02 CGPug/L 0.16Vinyl chloride
BRL 8260B P4K018613.0 11/12/14 21:02 CGPug/L 0.13Xylenes, total
Surrogate Recovery Control Limits
80-124105 %4-Bromofluorobenzene
75-129105 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 28
11/25/14
Level II QC Report
11112 Branding Iron Place Project No: 64-03
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 4110128
Time Submitted: 11/7/2014 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4K0184 - 5030B
Blank (P4K0184-BLK1)Prepared & Analyzed: 11/13/14
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 28
11/25/14
Level II QC Report
11112 Branding Iron Place Project No: 64-03
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 4110128
Time Submitted: 11/7/2014 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4K0184 - 5030B
Blank (P4K0184-BLK1)Prepared & Analyzed: 11/13/14
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10552.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10853.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10452.0
LCS (P4K0184-BS1)Prepared & Analyzed: 11/13/14
1,1-Dichloroethylene ug/L22.5 0.50 20.00 70-154112
Benzene ug/L22.1 0.50 20.00 77-128110
Chlorobenzene ug/L22.0 0.50 20.00 78-119110
Tetrahydrofuran ug/L22.1 10 20.00 70-130111
Toluene ug/L22.2 0.50 20.00 76-131111
Trichloroethylene ug/L21.9 0.50 20.00 77-133109
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10452.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10552.4
ug/L 50.00 77-123Surrogate: Toluene-d8 10552.3
LCS Dup (P4K0184-BSD1)Prepared & Analyzed: 11/13/14
1,1-Dichloroethylene ug/L21.4 0.50 20.00 2070-154107 5
Benzene ug/L21.4 0.50 20.00 2077-128107 3
Chlorobenzene ug/L21.1 0.50 20.00 2078-119105 4
Tetrahydrofuran ug/L21.2 10 20.00 2070-130106 4
Toluene ug/L21.2 0.50 20.00 2076-131106 5
Trichloroethylene ug/L20.6 0.50 20.00 2077-133103 6
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10451.9
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10451.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10452.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 28
11/25/14
Level II QC Report
11112 Branding Iron Place Project No: 64-03
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 4110128
Time Submitted: 11/7/2014 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4K0186 - 5030B
Blank (P4K0186-BLK1)Prepared & Analyzed: 11/12/14
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 28
11/25/14
Level II QC Report
11112 Branding Iron Place Project No: 64-03
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 4110128
Time Submitted: 11/7/2014 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4K0186 - 5030B
Blank (P4K0186-BLK1)Prepared & Analyzed: 11/12/14
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10854.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10652.9
ug/L 50.00 77-123Surrogate: Toluene-d8 10251.2
LCS (P4K0186-BS1)Prepared & Analyzed: 11/12/14
1,1-Dichloroethylene ug/L23.5 0.50 20.00 70-154118
Benzene ug/L21.2 0.50 20.00 77-128106
Chlorobenzene ug/L20.7 0.50 20.00 78-119104
Tetrahydrofuran ug/L21.0 10 20.00 70-130105
Toluene ug/L21.0 0.50 20.00 76-131105
Trichloroethylene ug/L21.4 0.50 20.00 77-133107
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10251.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.6
ug/L 50.00 77-123Surrogate: Toluene-d8 10351.4
LCS Dup (P4K0186-BSD1)Prepared & Analyzed: 11/12/14
1,1-Dichloroethylene ug/L22.3 0.50 20.00 2070-154112 5
Benzene ug/L20.4 0.50 20.00 2077-128102 4
Chlorobenzene ug/L20.3 0.50 20.00 2078-119102 2
Tetrahydrofuran ug/L21.4 10 20.00 2070-130107 2
Toluene ug/L20.3 0.50 20.00 2076-131102 3
Trichloroethylene ug/L20.6 0.50 20.00 2077-133103 4
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10251.2
ug/L 50.00 77-123Surrogate: Toluene-d8 10150.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 28
11/25/14
Level II QC Report
11112 Branding Iron Place Project No: 64-03
Project: Nash County C&D LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 4110128
Time Submitted: 11/7/2014 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P4K0148 - 3005A
Blank (P4K0148-BLK1)Prepared: 11/11/14 Analyzed: 11/12/14
Arsenic ug/LBRL1.0
Barium ug/L0.779 5.0 J
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Lead ug/LBRL1.0
Selenium ug/LBRL1.0
Silver ug/LBRL1.0
LCS (P4K0148-BS1)Prepared: 11/11/14 Analyzed: 11/12/14
Arsenic ug/L96.6 1.0 100.0 80-12097
Barium ug/L97.0 5.0 100.0 80-12097
Cadmium ug/L94.4 1.0 100.0 80-12094
Chromium ug/L1001.0 100.0 80-120100
Lead ug/L92.7 1.0 100.0 80-12093
Selenium ug/L88.0 1.0 100.0 80-12088
Silver ug/L96.5 1.0 100.0 80-12097
Batch P4K0196 - 7470A
Blank (P4K0196-BLK1)Prepared: 11/13/14 Analyzed: 11/14/14
Mercury ug/LBRL0.20
LCS (P4K0196-BS1)Prepared: 11/13/14 Analyzed: 11/14/14
Mercury ug/L7.73 0.20 9.375 80-12082
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 28
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P4K01484110128-02 11/11/14 8:0550 50mL mL
P4K01484110128-03 11/11/14 8:0550 50mL mL
P4K01484110128-04 11/11/14 8:0550 50mL mL
P4K01484110128-05 11/11/14 8:0550 50mL mL
P4K01484110128-06 11/11/14 8:0550 50mL mL
P4K01484110128-07 11/11/14 8:0550 50mL mL
P4K01484110128-08 11/11/14 8:0550 50mL mL
P4K01484110128-09 11/11/14 8:0550 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P4K01964110128-02 11/13/14 9:0520 30mL mL
P4K01964110128-03 11/13/14 9:0520 30mL mL
P4K01964110128-04 11/13/14 9:0520 30mL mL
P4K01964110128-05 11/13/14 9:0520 30mL mL
P4K01964110128-06 11/13/14 9:0520 30mL mL
P4K01964110128-07 11/13/14 9:0520 30mL mL
P4K01964110128-08 11/13/14 9:0520 30mL mL
P4K01964110128-09 11/13/14 9:0520 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P4K01864110128-01 11/12/14 14:3010 10mL mL
P4K01844110128-02 11/13/14 8:5910 10mL mL
P4K01844110128-03 11/13/14 8:5910 10mL mL
P4K01844110128-04 11/13/14 8:5910 10mL mL
P4K01844110128-05 11/13/14 8:5910 10mL mL
P4K01864110128-06 11/12/14 14:3010 10mL mL
P4K01864110128-07 11/12/14 14:3010 10mL mL
P4K01864110128-08 11/12/14 14:3010 10mL mL
P4K01864110128-09 11/12/14 14:3010 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 28
Page 28 of 28