SW_F_5301-MSWLF-1981_05-12-2015_RM_GW.pdf

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone] F [phone]
May 14, 2015
Ms. Jaclynne Drummond
Compliance Hydrogeologist
NC Department of Environment and Natural Resources Division of Waste
Management - Solid Waste Section 1646 Mail Service Center
Raleigh, North Carolina 27699-1646
RE: First Semi-annual Groundwater Monitoring Report of 2015 Lee County Landfill,
Permit No. 53-01
Lee County, North Carolina
Dear Ms. Drummond:

On behalf of Lee County, East Coast Environmental, P.A. (ECE) is submitting the enclosed
First Semiannual Groundwater Monitoring Report of 2015 in electronic format. This
completes the first semiannual compliance monitoring event of 2015 for the closed Lee
County Landfill, Permit No. 53-01, as required by the North Carolina Division of Waste
Management, Solid Waste Section. Please contact me at [phone] if you have any
questions regarding this submittal.

Sincerely,

Thomas R. Will, North Carolina Licensed Geologist 1164
Project Manager
East Coast Environmental, P.A.

Enclosures
C: Joseph Cherry - Lee County, Solid Waste Superintendent

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone] F [phone]
FIRST SEMI-ANNUAL GROUNDWATER MONITORING
REPORT OF 2015
PREPARED FOR:
LEE COUNTY GENERAL SERVICES
805 S. FIFTH STREET SANFORD, NORTH CAROLINA 27330
LEE COUNTY LANDFILL PERMIT No. 53-01

Prepared by:

East Coast Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina
[phone]

First Semiannual Groundwater Monitoring Report of 2015
Lee County Landfill
Lee County, North Carolina

TABLE OF CONTENTS
1.0 INTRODUCTION ...................................................................................................................... 1
1.1 Site Information ......................................................................................................................... 1
1.2 Site Geology and Hydrogeology ................................................................................................ 1
1.3 Regulatory Status ....................................................................................................................... 1
2.0 FACILITY MONITORING PROGRAM ................................................................................ 1
2.1 Groundwater Monitoring Program .......................................................................................... 1
2.2 Surface Water Monitoring Program ........................................................................................ 2
3.0 FIELD WORK AND LABORATORY ANALYSIS ............................................................... 2
4.0 DATA ANALYSIS AND COMPARISONS TO STANDARDS ............................................ .4
5.0 CONCLUSION ........................................................................................................................... 4
6.0 REFERENCES ........................................................................................................................... 4

Tables
Table 1
Table 2
Table 3
Figures
Figure 1
Figure 2

Appendix
Summary of Detected Constituents
Summary of Groundwater Elevations
Summary of Well Construction Data

Site Location Map

Groundwater Hydraulic Gradient Map
Laboratory Analytical Report

1

East
1.0 INTRODUCTION
1.1 Site Information
The Lee County Landfill is a closed, unlined municipal solid waste (MSW) and
construction & demolition (C&D) landfill located on approximately 254.6 acres in Lee
County, NC, approximately 6.5 miles south of Sanford. The six MSW and one C&D waste
disposal areas comprise approximately 100.8 acres. The property boundary is indicated on
an excerpt from the 7.5 minutes USGS topographic map for Muchison & Sanford, North
Carolina (Figure 1). The MSW portion of the facility ceased accepting waste prior to
October 9, 1993, and a letter of closure was issued on December 20, 1996. The C&D
portion of the facility was issued a Permit to Operate on July 25, 1995 and ceased
accepting waste June 30, 2008.
1.2 Site Geology and Hydrogeology
The Lee County Landfill is located near the edge of the Coastal Plain Physiographic
Province. The facility is underlain by the Middendorf Fonnation consisting of sand,
sandstone, and mudstone. The Middendorf Formation is underlain by metavolcanic rocks
of the Eastern Slate Belt. The uppermost aquifer is unconfined. The groundwater level
measurements taken in April 2015 were used to construct the potentiometric surface
contours shown in Figure 2. Historical static water levels are provided in Table 1.
Groundwater flow at the site is generally to the southeast.
1.3 Regulatory Status
The Lee County Landfill is currently monitoring groundwater in accordance with criteria
set forth in Rule .0500 of the North Carolina Solid Waste Management Rules (NCSWMR)
for MSW landfills closed prior to October 9, 1993 and C&D landfills closed prior to July
1, 2008.

2.0 FACILITY MONITORING PROGRAM
2.1 Groundwater Monitoring Program
The current groundwater compliance monitoring network includes 6 monitoring wells. In
addition, there are 4 monitoring wells used only for water level measurements. These wells
are summarized below, along with their current monitoring program status. The locations
of the monitoring wells are shown on Figure 2.
Groundwater samples are collected semiannually in April and October. Samples are
analyzed for RCRA metals and the NC Appendix I list of volatile organic constituents
during the first and second semiannual events.

1

Monitoring Well Classification .Monitoring Program Total Depth From
TOC (ft)
MW-4 Observation Water Levels Only 19.00 MW-5 Compliance Detection (.0500) 19.50 MW-6 Compliance Detection (.0500) 40.40
MW-7 Observation Water Levels Only 22.17 MW-9 Compliance Detection (.0500) 22.85 MW-l0 Compliance Detection (.0500) 22.80 MW-l1 Observation Water Levels Only 22.75 MW-12 Compliance Detection (.0500) 13.30 MW-13 Observation Water Levels Only 24.25 MW-14 Compliance Detection (.0500) 18.25 *TOC = Top of casing.
2.2 Surface Water Monitoring Program
Surface water at the Lee County Landfill is monitored semiannually in conjunction with
the groundwater sampling events. Samples are collected from one surface water monitoring
point (SW-2). Samples are not collected from SW-l. The location of the surface water
monitoring point is shown on Figure 2.
Surface water samples will be collected and analyzed for RCRA metals and the NC
Appendix I list of volatile organic constituents during both semiannual monitoring events.
These surface water monitoring point are summarized below, along with their current
monitoring program status.

Surface Point Classification Monitoring Program
SW-l Not Monitored Surface Water
SW-2 Compliance Surface Water

3.0 FIELD WORK AND LABORATORY ANALYSIS
In order to detect potential releases of leachate and/or landfill gas migration in a timely
manner, a visual inspection program has been implemented at the Lee County Landfill.
This inspection program involves field personnel making the following observations:
Observation of stress induced on the biological community (e.g., dead or dying
vegetation),
Indications of leachate impact (e.g., seeps, impacted surface water), Observations of erosion; and Negative changes around the waste facility.

2

On April 24, 2015 ECE personnel visited the facility to purge and sample the facility's
monitoring wells MW-5, MW-6, MW-9, MW-10, MW-12, and MW-14. Prior to purging,
the depth to static water level was measured for all monitoring wells with an electronic
water level indicator, accurate to 0.01 foot. MW-4, MW-7, MW-11, and MW-13 were
measured for static water levels only.
Monitoring wells were purged and sampled using disposable bailers. Measurements of
temperature, pH, specific conductivity, and turbidity were recorded in the site specific log
book prior to purging, after each purge volume, and during sampling. Prior to sampling,
laboratory-supplied containers were prepared with the following information:
Monitoring well number (completed by field personnel),
Date and time of sample collection (completed by field personnel), Initials of sampling personnel (completed by field personnel), Project name and number (completed by the laboratory), Chemical preservative (completed by the laboratory); and
Requested chemical analysis (completed by the laboratory).
Groundwater samples from each monitoring well were collected directly from the
disposable bailers in the provided laboratory containers immediately after purging.
Immediately after collection, the samples were placed in a laboratory provided cooler and
chilled on ice.
Surface water samples are collected directly from stream flow, by lowering the prepared
sample containers into the stream flow with the opening facing into the current flow. Care
is taken not to overflow the sample containers (which could lead to preservative loss) and
avoid sample induced turbidity. At the time of sampling, surface water is also measured for
temperature, pH, specific conductivity, and turbidity. After sample collection, the samples
are placed in a laboratory provided cooler and chilled on ice.
The April 2015 groundwater and surface water samples were submitted to Environmental
Conservation Laboratories (ENCO) of Cary, North Carolina under chain-of-custody control
for analysis. As presented earlier, the groundwater samples were analyzed for RCRA
metals and the NC Appendix I list of volatile organic constituents. ECE requested a Level II
data report for the final laboratory report. The samples were received by the laboratory on
April 28, 2015 in good condition, properly preserved, and within analysis hold times.

In addition to samples collected for compliance monitoring at the Lee County Landfill, a
Field Blank was collected by ECE personnel as part of the April 2015 sampling event. Also,
a Trip Blank was prepared by the laboratory to accompany the volatile sampling containers
during shipment to and from the laboratory. The April 2015 Field Blank was analyzed for
RCRA metals and the NC Appendix I list of volatile organic constituents while the April
2015 Trip Blank was analyzed for the NCSWMR Appendix I volatile organic constituent
only.

3

4.0 DATA ANALYSIS AND COMPARISONS TO STANDARDS
Results from the April 2015 sampling event were received May 12, 2015 from ENCO and
are attached. Analytical results from monitoring wells were compared directly to the NC 2L
Groundwater Standards or Groundwater Protection Standards. Analytical results from the
surface water monitoring point are also compared to the NC 2B Surface Water Standards.
A summary of the April 2015 detected constituents can be found in Table 1. Two contaminants (benzene and barium) were detected in one groundwater monitoring well
(MW-12 at levels in excess of their maximum allowable concentrations in groundwater as
set forth in 15A NCAC 2L .0202.

5.0 CONCLUSIONS
Based on historical water quality data, constituents detected in groundwater and surface
water samples collected during the April 2015 monitoring event are consistent with
previous events. The Lee County Landfill will remain in Detection Monitoring and the next semiannual sampling event is scheduled for the October 2015.

6.0 REFERENCES
Brown, Philip M., Chief Geologist, 1985, Geologic Map of North Carolina, The North
Carolina Geologic Survey, scale 1:500,000.
North Carolina Department of Environment and Natural Resources, 1990-2011, Solid
Waste Management Regulations.
USEPA, 1986, RCRA Ground Water Monitoring Technical Enforcement Guidance
Document (TEGD).
USEPA, 1992, Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance, Chapter 2, July.

Second Semiannual Groundwater Monitoring Report of 2011. January 2012. Prepared by
Joyce Engineering

Second Semiannual Groundwater Monitoring Report of 2012. November 2012. Prepared
by East Coast Environmental, P.A.

First Semiannual Groundwater Monitoring Report of 2013. May 2013. Prepared by East
Coast Environmental, P.A.

Second Semiannual Groundwater Monitoring Report of 2014. November 2014. Prepared
by East Coast Environmental, P.A.

East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone] Fax: [phone]
Figure 1
Site Location Map
Lee County Landfill
331 Landfill Road
Lee County, North Carolina
Scale:Prep. By:Rev. By:Date:
1”=2000'CKC TRW 11/12/2012
N
Source: USGS 7.5 Minute Topographics: Sanford and Murchison, NC
E a s t C o a s t
E n v i r o n m e n t a l , P .A .
3 8 1 5 J u n c t i o n B o u l e v a r d
R a l e i g h , N o r t h C a r o l i n a 2 7 6 0 3
(9 1 9 ) 7 7 2 -0 2 6 8 F a x : (9 1 9 ) 7 7 2 -0 4 6 8
F i g u r e 2
G r o u n d w a t e r H y d r a u l i c G r a d i e n t M a p – 1 0 /2 1 /2 0 1 4
L e e C o u n t y L a n d f i l l
L a n d f i l l R o a d
L e e C o u n t y , N o r t h C a r o l i n a
S c a l e :
P r e p . B y :
R e v . B y :
D a t e :
1 ”=4 0 0 '
T R W
T R W
5 /1 2 /2 0 1 5
Figure 2
N
391.80
393.25
369.80
377.00
356.48
353.11
352.47
344.87
335.67
336.43
Directio
n of G
rou
nd
w
ater
Flo
w (4/2
4/20
15)
3 3 5
3 4 0
3 4 5
3 5 0
3 5 5360365370375
3 8 0390
3 9 0
3 8 5
3 8 5 3 8 0
3 7 5
3 7 0
3 6 5
3 6 0
3 5 5
3 5 0
3 4 5
3 4 0
3 3 5
TABLE 1

SUMMARY OF DETECTED CONSTITUENTS – GROUNDWATER

Analytical Method >

3050 3050 3050 3050 3050 8260 8260 8260 8260 8260 8260 8260 8260
Well
ID
Contaminant of Concern >
Ar
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Ba
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Ch
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1 -1
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2

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1,
4

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X
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Date
Collected
m/dd/yy
Sample
ID

MW-5 4/24/15 MW-5 ND 355 11.0 ND 12.5 ND ND ND ND ND ND ND ND
MW-6 4/24/15 MW-6 ND 78.3 1.78 ND ND ND ND ND ND ND ND ND ND
MW-9 4/24/15 MW-9 ND 160 ND ND 3.90 ND ND ND ND ND ND ND ND
MW-10 4/24/15 MW-10 ND 237 3.94 ND ND ND ND ND ND ND ND ND ND
MW-12 4/24/15 MW-12 ND 1,530 3.13 0.717 8.47 6.7 5.7 0.41 5.7 26 57 1.5 0.42
MW-14 4/24/15 MW-14 ND 170 3.43 ND 20.4 ND ND ND ND ND ND ND ND
SW-2 4/24/15 SW-2 ND 61.2 ND ND ND ND ND ND ND ND ND ND ND
Field
Blank
4/24/15 Field
Blank
ND ND ND ND ND ND ND ND ND ND ND ND ND
Trip
Blank
4/24/15 Trip
Blank
ND ND ND ND ND ND ND ND ND ND ND ND ND

2L Standard (ug/l) 10 700 10 2 15 1 6 20 6 50 3,000 NRS 1,000
Results are in ug/l
Bold results indicate exceedence of 2L Standards

TABLE 1 (Continued)

SUMMARY OF DETECTED CONSTITUENTS – GROUNDWATER

Analytical Method >

3050 3050 8260
Well
ID
Contaminant of Concern >
Se
l
e
n
i
u
m

Si
l
v
e
r

To
l
u
e
n
e

Date
Collected
m/dd/yy
Sample ID

MW-5 4/24/15 MW-5 ND ND ND
MW-6 4/24/15 MW-6 ND ND ND
MW-9 4/24/15 MW-9 ND ND ND
MW-10 4/24/15 MW-10 ND ND ND
MW-12 4/24/15 MW-12 ND ND ND
MW-14 4/24/15 MW-14 ND ND ND
SW-2 4/24/15 SW-2 ND ND ND
Field
Blank
4/24/15 Field
Blank
ND ND ND
Trip
Blank
4/24/15 Trip Blank ND ND ND

2L Standard (ug/l) 20 20 600
Results are in ug/l
Bold results indicate exceedence of 2L Standards

TABLE 2
SUMMARY OF HISTORICAL GROUNDWATER ELEVATIONS

Location MW-4 MW-5 MW-6 MW-7 MW-9 MW-1O MW-l1 MW-12 MW-13 MW-14
TOC Elevation 345.90 351.10 402. 10 360.30 384.20 377.00 399.60 337.40 363.93 358.61
Well Depth 19.00 19.50 40.40 22.17 22.85 22.80 22.75 13.30 24.25 18.25
24-Apr-09 336.60 NM 393.46 351.82 377.27 369.77 390.44 333.59 355.87 352.89
24-Nov-09 335.10 344.85 393.15 351.45 375.05 369.05 389.05 333.75 354.69 351.83
09-Apr-10 337.10 344.90 392.68 351. 75 376.44 369.67 390.30 333.85 355.98 352.91
04-0ct-10 330.59 344.55 392.16 349.24 374.82 367.84 388.54 332.98 353.38 350.52
15-Apr-11 NA NA NA NA NA NA NA NA NA NA
10-Oct-l1 DRY 341.64 391.18 347.76 370.56 363.44 383.59 328.87 348.94 347.68
18-Oct-12 331.62 344.35 392.48 349.73 374.91 367.55 387.62 332.50 353.19 350.71
17-Apr-13 335.45 344.80 392.55 351.87 375.92 369.61 389.65 333.62 356.24 352.48
21-Oct-14 332.65 344.00 392.70 349.85 375.38 367.42 386.42 333.35 353.81 351.07
24-Apr-15 336.43 344.87 393.25 352.47 377.00 369.80 391.80 335.67 356.48 353.11
Notes:
1. Water levels are measured from top of casing (TOC).
NM = Not monitored.
2. NA = Not available.
4. DRY = Monitoring well was dry.

TABLE 3

SUMMARY OF WELL CONSTRUCTION DATA

Well ID Date
Installed
Well
Diameter
(Inches)
Screened
Interval
(Feet below
TOC)
Bottom of
Well
(Feet below
TOC)
Top of
Casing
Elevation
(Feet Above
Sea Level )
Groundwater
Elevation
(4-24-15)
Depth to
Water
(4-24-15)
Longitude Latitude
MW-4 Unknown 2” 9.0 -19.0 19.00 345.90 336.43 9.47 35° 22’ 11.51” 79° 10’ 58.32”
MW-5 Unknown 2” 9.5-19.5 19.50 351.10 344.87 6.23 35° 21’ 56.71” 79° 11’ 15.67”
MW-6 Unknown 2” 20.4-40.4 40.40 402.10 393.25 8.85 35° 22’ 14.30” 79° 11’ 48.52”
MW-7 Unknown 2” 12.17-22.17 22.17 360.30 352.47 7.83 35° 22’ 02.59” 79° 11’ 23.29”
MW-9 Unknown 2” 12.85- 22.85 22.85 384.20 377.00 7.20 35° 22’ 09.06” 79° 11’ 35.51”
MW-10 Unknown 2” 12.80-22.80 22.80 377.00 369.80 7.20 35° 22’10.17” 79° 11’ 33.40”
MW-11 Unknown 2” 12.75-22.75 22.75 399.60 391.80 7.80 35° 22’ 28.02” 79° 11’ 22.30”
MW-12 Unknown 2” 3.30-13.30 13.30 337.40 335.67 1.73 35° 22’ 06.49” 79° 10’ 56.74”
MW-13 Unknown 2” 14.25-24.25 24.25 363.93 356.48 7.45 35° 21’ 58.82” 79° 11’ 28.49”
MW-14 Unknown 2” 8.25-18.25 18.25 358.61 353.11 5.50 35° 22’ 00.43” 79° 11’ 25.47”

Note: Installation dates and screen intervals will be confirmed prior to 10-2015 groundwater monitoring event.
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): C504926
Raleigh, NC 27603
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Lee County
Attn: Tom Will
East Coast Environmental (EA030)
3815 Junction Blvd.
Bill Scott
Project Manager
Tuesday, May 12, 2015
RE: Laboratory Results for
Dear Tom Will,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, April 28, 2015.
The total number of pages in this report, including this page is 48.
Page 1 of 48
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SAMPLE SUMMARY/LABORATORY CHRONICLE
5301-MW5 C504926-01 Sampled:04/24/15 12:20 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:24
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:00
EPA 8260B 05/08/15 05/06/15 11:02 5/6/2015 14:12
5301-MW6 C504926-02 Sampled:04/24/15 12:10 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:26
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:02
EPA 8260B 05/08/15 05/06/15 11:02 5/6/2015 14:42
5301-MW9 C504926-03 Sampled:04/24/15 09:45 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 10:39
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 12:27
EPA 8260B 05/08/15 05/06/15 11:02 5/6/2015 13:42
5301-MW10 C504926-04 Sampled:04/24/15 10:00 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:29
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:04
EPA 8260B 05/08/15 05/06/15 11:02 5/6/2015 15:11
5301-MW12 C504926-05 Sampled:04/24/15 11:15 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:39
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:07
5301-MW12 C504926-05RE1 Sampled:04/24/15 11:15 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 05/08/15 05/07/15 10:17 5/7/2015 14:46
5301-MW14 C504926-06 Sampled:04/24/15 12:00 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:42
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:09
EPA 8260B 05/08/15 05/06/15 11:20 5/7/2015 07:02
Page 2 of 48
Page 2 of 48
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5301-SW2 C504926-07 Sampled:04/24/15 12:30 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:55
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:15
EPA 8260B 05/08/15 05/06/15 11:20 5/7/2015 07:32
5301-Fieldblank C504926-08 Sampled:04/24/15 11:45 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 10/21/15 05/07/15 13:21 5/11/2015 11:58
EPA 7470A 05/22/15 05/11/15 11:25 5/12/2015 13:18
EPA 8260B 05/08/15 05/06/15 11:20 5/7/2015 08:02
5301-Tripblank C504926-09 Sampled:04/24/15 09:15 Received:04/28/15 11:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 05/08/15 05/06/15 11:20 5/7/2015 02:35
Page 3 of 48
Page 3 of 48
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW5 C504926-01
Flag NotesMDLNC SWSLMRLDF
355 ug/L EPA 6010C 10010.01.001Barium - Total
11.0 ug/L EPA 6010C 1010.01.401Chromium - Total
12.5 ug/L EPA 6010C 1010.03.101Lead - Total
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW6 C504926-02
Flag NotesMDLNC SWSLMRLDF
78.3 ug/L EPA 6010CJ 10010.01.001Barium - Total
1.78 ug/L EPA 6010CJ 1010.01.401Chromium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW9 C504926-03
Flag NotesMDLNC SWSLMRLDF
160 ug/L EPA 6010C 10010.01.001Barium - Total
3.90 ug/L EPA 6010CJ 1010.03.101Lead - Total
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW10 C504926-04
Flag NotesMDLNC SWSLMRLDF
237 ug/L EPA 6010C 10010.01.001Barium - Total
3.94 ug/L EPA 6010CJ 1010.01.401Chromium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW12 C504926-05
Flag NotesMDLNC SWSLMRLDF
1530 ug/L EPA 6010C 10010.01.001Barium - Total
0.717 ug/L EPA 6010CJ 11.000.3601Cadmium - Total
3.13 ug/L EPA 6010CJ 1010.01.401Chromium - Total
8.47 ug/L EPA 6010CJ 1010.03.101Lead - Total
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW12 C504926-05RE1
Flag NotesMDLNC SWSLMRLDF
5.7 ug/L EPA 8260B 51.00.1311,1-Dichloroethane
0.41 ug/L EPA 8260BJ 51.00.1911,2-Dichlorobenzene
5.7 ug/L EPA 8260B 11.00.1911,4-Dichlorobenzene
1.5 ug/L EPA 8260BJ 1005.01.312-Butanone
6.7 ug/L EPA 8260B 11.00.151Benzene
26 ug/L EPA 8260B 31.00.171Chlorobenzene
57 ug/L EPA 8260B 101.00.231Chloroethane
0.42 ug/L EPA 8260BJ NE1.00.0651o-Xylene
Analyte MethodUnitsResults
Lab ID:Client ID:5301-MW14 C504926-06
Flag NotesMDLNC SWSLMRLDF
170 ug/L EPA 6010C 10010.01.001Barium - Total
3.43 ug/L EPA 6010CJ 1010.01.401Chromium - Total
20.4 ug/L EPA 6010C 1010.03.101Lead - Total
Analyte MethodUnitsResults
Lab ID:Client ID:5301-SW2 C504926-07
Flag NotesMDLNC SWSLMRLDF
61.3 ug/L EPA 6010CJ 10010.01.001Barium - Total
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ANALYTICAL RESULTS
5301-MW5Description:Lab Sample ID:C504926-01 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:20 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/06/15 14:121,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/06/15 14:121,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/06/15 14:121,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/06/15 14:121,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 14:121,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/06/15 14:121,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 14:121,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 14:121,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/06/15 14:121,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/06/15 14:121,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/06/15 14:121,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/06/15 14:121,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/06/15 14:121,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/06/15 14:122-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/06/15 14:122-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/06/15 14:124-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/06/15 14:12Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/06/15 14:12Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/06/15 14:12Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 14:12Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/06/15 14:12Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 14:12Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/06/15 14:12Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/06/15 14:12Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/06/15 14:12Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 14:12Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 14:12Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/06/15 14:12Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/06/15 14:12Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 14:12cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/06/15 14:12cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/06/15 14:12Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 14:12Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/06/15 14:12Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 14:12Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/06/15 14:12m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/06/15 14:12Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 14:12o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/06/15 14:12Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/06/15 14:12Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 14:12Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 14:12trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 14:12trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 14:12trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/06/15 14:12Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 14:12Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/06/15 14:12Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/06/15 14:12Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
Page 5 of 48
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5301-MW5Description:Lab Sample ID:C504926-01 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:20 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/06/15 14:12Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13690 %MSZEPA 8260B 05/06/15 14:125E060124550.0 1
Dibromofluoromethane 67-129124 %MSZEPA 8260B 05/06/15 14:125E060126250.0 1
Toluene-d8 59-134100 %MSZEPA 8260B 05/06/15 14:125E060125050.0 1
Page 6 of 48
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5301-MW5Description:Lab Sample ID:C504926-01 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:20 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:00Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 7 of 48
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5301-MW5Description:Lab Sample ID:C504926-01 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:20 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:24Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:24Barium [7440-39-3] ^1 1.00 JDH10.0355 100
ug/L EPA 6010C 05/11/15 11:24Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 11:24Chromium [7440-47-3] ^1 1.40 JDH10.011.0 10
ug/L EPA 6010C 05/11/15 11:24Lead [7439-92-1] ^1 3.10 JDH10.012.5 10
ug/L EPA 6010C 05/11/15 11:24Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:24Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 48
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5301-MW6Description:Lab Sample ID:C504926-02 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:10 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/06/15 14:421,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/06/15 14:421,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/06/15 14:421,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/06/15 14:421,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 14:421,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/06/15 14:421,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 14:421,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 14:421,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/06/15 14:421,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/06/15 14:421,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/06/15 14:421,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/06/15 14:421,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/06/15 14:421,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/06/15 14:422-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/06/15 14:422-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/06/15 14:424-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/06/15 14:42Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/06/15 14:42Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/06/15 14:42Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 14:42Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/06/15 14:42Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 14:42Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/06/15 14:42Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/06/15 14:42Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/06/15 14:42Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 14:42Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 14:42Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/06/15 14:42Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/06/15 14:42Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 14:42cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/06/15 14:42cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/06/15 14:42Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 14:42Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/06/15 14:42Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 14:42Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/06/15 14:42m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/06/15 14:42Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 14:42o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/06/15 14:42Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/06/15 14:42Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 14:42Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 14:42trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 14:42trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 14:42trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/06/15 14:42Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 14:42Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/06/15 14:42Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/06/15 14:42Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/06/15 14:42Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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5301-MW6Description:Lab Sample ID:C504926-02 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:10 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13688 %MSZEPA 8260B 05/06/15 14:425E060124450.0 1
Dibromofluoromethane 67-129123 %MSZEPA 8260B 05/06/15 14:425E060126250.0 1
Toluene-d8 59-13497 %MSZEPA 8260B 05/06/15 14:425E060124950.0 1
Page 10 of 48
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5301-MW6Description:Lab Sample ID:C504926-02 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:10 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:02Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 11 of 48
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5301-MW6Description:Lab Sample ID:C504926-02 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:10 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:26Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:26Barium [7440-39-3] ^1 1.00 JDH10.078.3 J 100
ug/L EPA 6010C 05/11/15 11:26Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 11:26Chromium [7440-47-3] ^1 1.40 JDH10.01.78 J 10
ug/L EPA 6010C 05/11/15 11:26Lead [7439-92-1] ^1 3.10 JDH10.03.10 U 10
ug/L EPA 6010C 05/11/15 11:26Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:26Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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5301-MW9Description:Lab Sample ID:C504926-03 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 09:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/06/15 13:421,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/06/15 13:421,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/06/15 13:421,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/06/15 13:421,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 13:421,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/06/15 13:421,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 13:421,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 13:421,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/06/15 13:421,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/06/15 13:421,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/06/15 13:421,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/06/15 13:421,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/06/15 13:421,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/06/15 13:422-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/06/15 13:422-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/06/15 13:424-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/06/15 13:42Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/06/15 13:42Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/06/15 13:42Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 13:42Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/06/15 13:42Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 13:42Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/06/15 13:42Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/06/15 13:42Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/06/15 13:42Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 13:42Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 13:42Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/06/15 13:42Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/06/15 13:42Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 13:42cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/06/15 13:42cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/06/15 13:42Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 13:42Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/06/15 13:42Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 13:42Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/06/15 13:42m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/06/15 13:42Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 13:42o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/06/15 13:42Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/06/15 13:42Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 13:42Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 13:42trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 13:42trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 13:42trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/06/15 13:42Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 13:42Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/06/15 13:42Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/06/15 13:42Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/06/15 13:42Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Page 13 of 48
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www.encolabs.com
5301-MW9Description:Lab Sample ID:C504926-03 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 09:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MSZEPA 8260B 05/06/15 13:425E060124550.0 1
Dibromofluoromethane 67-129121 %MSZEPA 8260B 05/06/15 13:425E060126150.0 1
Toluene-d8 59-13499 %MSZEPA 8260B 05/06/15 13:425E060124950.0 1
Page 14 of 48
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www.encolabs.com
5301-MW9Description:Lab Sample ID:C504926-03 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 09:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 12:27Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 15 of 48
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www.encolabs.com
5301-MW9Description:Lab Sample ID:C504926-03 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 09:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 10:39Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 10:39Barium [7440-39-3] ^1 1.00 JDH10.0160 100
ug/L EPA 6010C 05/11/15 10:39Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 10:39Chromium [7440-47-3] ^1 1.40 JDH10.01.40 U 10
ug/L EPA 6010C 05/11/15 10:39Lead [7439-92-1] ^1 3.10 JDH10.03.90 J 10
ug/L EPA 6010C 05/11/15 10:39Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 10:39Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 16 of 48
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www.encolabs.com
5301-MW10Description:Lab Sample ID:C504926-04 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 10:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/06/15 15:111,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/06/15 15:111,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/06/15 15:111,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/06/15 15:111,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 15:111,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/06/15 15:111,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 15:111,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 15:111,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/06/15 15:111,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/06/15 15:111,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/06/15 15:111,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/06/15 15:111,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/06/15 15:111,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/06/15 15:112-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/06/15 15:112-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/06/15 15:114-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/06/15 15:11Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/06/15 15:11Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/06/15 15:11Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 15:11Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/06/15 15:11Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 15:11Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/06/15 15:11Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/06/15 15:11Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/06/15 15:11Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 15:11Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 15:11Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/06/15 15:11Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/06/15 15:11Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 15:11cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/06/15 15:11cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/06/15 15:11Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/06/15 15:11Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/06/15 15:11Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/06/15 15:11Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/06/15 15:11m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/06/15 15:11Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/06/15 15:11o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/06/15 15:11Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/06/15 15:11Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/06/15 15:11Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/06/15 15:11trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/06/15 15:11trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 15:11trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/06/15 15:11Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/06/15 15:11Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/06/15 15:11Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/06/15 15:11Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/06/15 15:11Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Page 17 of 48
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www.encolabs.com
5301-MW10Description:Lab Sample ID:C504926-04 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 10:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13690 %MSZEPA 8260B 05/06/15 15:115E060124550.0 1
Dibromofluoromethane 67-129125 %MSZEPA 8260B 05/06/15 15:115E060126250.0 1
Toluene-d8 59-134100 %MSZEPA 8260B 05/06/15 15:115E060125050.0 1
Page 18 of 48
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www.encolabs.com
5301-MW10Description:Lab Sample ID:C504926-04 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 10:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:04Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 19 of 48
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www.encolabs.com
5301-MW10Description:Lab Sample ID:C504926-04 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 10:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:29Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:29Barium [7440-39-3] ^1 1.00 JDH10.0237 100
ug/L EPA 6010C 05/11/15 11:29Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 11:29Chromium [7440-47-3] ^1 1.40 JDH10.03.94 J 10
ug/L EPA 6010C 05/11/15 11:29Lead [7439-92-1] ^1 3.10 JDH10.03.10 U 10
ug/L EPA 6010C 05/11/15 11:29Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:29Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 20 of 48
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www.encolabs.com
5301-MW12Description:Lab Sample ID:C504926-05 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:15 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/07/15 14:461,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/07/15 14:461,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/07/15 14:461,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/07/15 14:461,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 14:461,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.05.7 5
ug/L EPA 8260B 05/07/15 14:461,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 14:461,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 14:461,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/07/15 14:461,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/07/15 14:461,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.41 J 5
ug/L EPA 8260B 05/07/15 14:461,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/07/15 14:461,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/07/15 14:461,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.05.7 1
ug/L EPA 8260B 05/07/15 14:462-Butanone [78-93-3] ^1 1.3 MSZ5.01.5 J 100
ug/L EPA 8260B 05/07/15 14:462-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/07/15 14:464-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/07/15 14:46Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/07/15 14:46Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/07/15 14:46Benzene [71-43-2] ^1 0.15 MSZ1.06.7 1
ug/L EPA 8260B 05/07/15 14:46Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/07/15 14:46Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 14:46Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/07/15 14:46Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/07/15 14:46Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/07/15 14:46Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 14:46Chlorobenzene [108-90-7] ^1 0.17 MSZ1.026 3
ug/L EPA 8260B 05/07/15 14:46Chloroethane [75-00-3] ^1 0.23 MSZ1.057 10
ug/L EPA 8260B 05/07/15 14:46Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/07/15 14:46Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 14:46cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/07/15 14:46cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/07/15 14:46Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 14:46Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/07/15 14:46Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 14:46Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/07/15 14:46m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/07/15 14:46Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 14:46o-Xylene [95-47-6] ^1 0.065 MSZ1.00.42 J NE
ug/L EPA 8260B 05/07/15 14:46Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/07/15 14:46Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 14:46Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 14:46trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 14:46trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 14:46trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/07/15 14:46Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 14:46Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/07/15 14:46Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/07/15 14:46Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/07/15 14:46Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Page 21 of 48
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www.encolabs.com
5301-MW12Description:Lab Sample ID:C504926-05 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:15 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MSZEPA 8260B 05/07/15 14:465E070184450.0 1
Dibromofluoromethane 67-129121 %MSZEPA 8260B 05/07/15 14:465E070186050.0 1
Toluene-d8 59-134100 %MSZEPA 8260B 05/07/15 14:465E070185050.0 1
Page 22 of 48
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www.encolabs.com
5301-MW12Description:Lab Sample ID:C504926-05 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:15 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:07Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 23 of 48
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www.encolabs.com
5301-MW12Description:Lab Sample ID:C504926-05 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:15 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:39Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:39Barium [7440-39-3] ^1 1.00 JDH10.01530 100
ug/L EPA 6010C 05/11/15 11:39Cadmium [7440-43-9] ^1 0.360 JDH1.000.717 J 1
ug/L EPA 6010C 05/11/15 11:39Chromium [7440-47-3] ^1 1.40 JDH10.03.13 J 10
ug/L EPA 6010C 05/11/15 11:39Lead [7439-92-1] ^1 3.10 JDH10.08.47 J 10
ug/L EPA 6010C 05/11/15 11:39Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:39Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 24 of 48
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5301-MW14Description:Lab Sample ID:C504926-06 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/07/15 07:021,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/07/15 07:021,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/07/15 07:021,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/07/15 07:021,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 07:021,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/07/15 07:021,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 07:021,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 07:021,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/07/15 07:021,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/07/15 07:021,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/07/15 07:021,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/07/15 07:021,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/07/15 07:021,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/07/15 07:022-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/07/15 07:022-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/07/15 07:024-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/07/15 07:02Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/07/15 07:02Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/07/15 07:02Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 07:02Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/07/15 07:02Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 07:02Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/07/15 07:02Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/07/15 07:02Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/07/15 07:02Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 07:02Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 07:02Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/07/15 07:02Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/07/15 07:02Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 07:02cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/07/15 07:02cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/07/15 07:02Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 07:02Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/07/15 07:02Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 07:02Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/07/15 07:02m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/07/15 07:02Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 07:02o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/07/15 07:02Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/07/15 07:02Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 07:02Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 07:02trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 07:02trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 07:02trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/07/15 07:02Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 07:02Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/07/15 07:02Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/07/15 07:02Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/07/15 07:02Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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5301-MW14Description:Lab Sample ID:C504926-06 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MSZEPA 8260B 05/07/15 07:025E060154450.0 1
Dibromofluoromethane 67-129126 %MSZEPA 8260B 05/07/15 07:025E060156350.0 1
Toluene-d8 59-13498 %MSZEPA 8260B 05/07/15 07:025E060154950.0 1
Page 26 of 48
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www.encolabs.com
5301-MW14Description:Lab Sample ID:C504926-06 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:09Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 27 of 48
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www.encolabs.com
5301-MW14Description:Lab Sample ID:C504926-06 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:00 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:42Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:42Barium [7440-39-3] ^1 1.00 JDH10.0170 100
ug/L EPA 6010C 05/11/15 11:42Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 11:42Chromium [7440-47-3] ^1 1.40 JDH10.03.43 J 10
ug/L EPA 6010C 05/11/15 11:42Lead [7439-92-1] ^1 3.10 JDH10.020.4 10
ug/L EPA 6010C 05/11/15 11:42Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:42Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 28 of 48
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5301-SW2Description:Lab Sample ID:C504926-07 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:30 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/07/15 07:321,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/07/15 07:321,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/07/15 07:321,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/07/15 07:321,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 07:321,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/07/15 07:321,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 07:321,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 07:321,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/07/15 07:321,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/07/15 07:321,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/07/15 07:321,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/07/15 07:321,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/07/15 07:321,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/07/15 07:322-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/07/15 07:322-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/07/15 07:324-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/07/15 07:32Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/07/15 07:32Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/07/15 07:32Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 07:32Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/07/15 07:32Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 07:32Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/07/15 07:32Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/07/15 07:32Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/07/15 07:32Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 07:32Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 07:32Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/07/15 07:32Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/07/15 07:32Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 07:32cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/07/15 07:32cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/07/15 07:32Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 07:32Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/07/15 07:32Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 07:32Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/07/15 07:32m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/07/15 07:32Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 07:32o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/07/15 07:32Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/07/15 07:32Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 07:32Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 07:32trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 07:32trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 07:32trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/07/15 07:32Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 07:32Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/07/15 07:32Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/07/15 07:32Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/07/15 07:32Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Page 29 of 48
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5301-SW2Description:Lab Sample ID:C504926-07 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:30 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13688 %MSZEPA 8260B 05/07/15 07:325E060154450.0 1
Dibromofluoromethane 67-129124 %MSZEPA 8260B 05/07/15 07:325E060156250.0 1
Toluene-d8 59-13498 %MSZEPA 8260B 05/07/15 07:325E060154950.0 1
Page 30 of 48
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5301-SW2Description:Lab Sample ID:C504926-07 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:30 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:15Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 31 of 48
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5301-SW2Description:Lab Sample ID:C504926-07 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 12:30 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:55Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:55Barium [7440-39-3] ^1 1.00 JDH10.061.3 J 100
ug/L EPA 6010C 05/11/15 11:55Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 11:55Chromium [7440-47-3] ^1 1.40 JDH10.01.40 U 10
ug/L EPA 6010C 05/11/15 11:55Lead [7439-92-1] ^1 3.10 JDH10.03.10 U 10
ug/L EPA 6010C 05/11/15 11:55Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:55Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 32 of 48
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5301-FieldblankDescription:Lab Sample ID:C504926-08 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/07/15 08:021,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/07/15 08:021,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/07/15 08:021,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/07/15 08:021,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 08:021,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/07/15 08:021,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 08:021,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 08:021,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/07/15 08:021,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/07/15 08:021,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/07/15 08:021,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/07/15 08:021,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/07/15 08:021,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/07/15 08:022-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/07/15 08:022-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/07/15 08:024-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/07/15 08:02Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/07/15 08:02Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/07/15 08:02Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 08:02Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/07/15 08:02Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 08:02Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/07/15 08:02Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/07/15 08:02Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/07/15 08:02Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 08:02Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 08:02Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/07/15 08:02Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/07/15 08:02Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 08:02cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/07/15 08:02cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/07/15 08:02Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 08:02Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/07/15 08:02Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 08:02Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/07/15 08:02m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/07/15 08:02Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 08:02o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/07/15 08:02Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/07/15 08:02Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 08:02Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 08:02trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 08:02trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 08:02trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/07/15 08:02Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 08:02Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/07/15 08:02Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/07/15 08:02Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/07/15 08:02Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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5301-FieldblankDescription:Lab Sample ID:C504926-08 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MSZEPA 8260B 05/07/15 08:025E060154550.0 1
Dibromofluoromethane 67-129127 %MSZEPA 8260B 05/07/15 08:025E060156350.0 1
Toluene-d8 59-134102 %MSZEPA 8260B 05/07/15 08:025E060155150.0 1
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5301-FieldblankDescription:Lab Sample ID:C504926-08 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 05/12/15 13:18Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
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5301-FieldblankDescription:Lab Sample ID:C504926-08 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 11:45 Work Order:C504926
Lee CountyProject:Sampled By:Client
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6010C 05/11/15 11:58Arsenic [7440-38-2] ^1 6.80 JDH10.06.80 U 10
ug/L EPA 6010C 05/11/15 11:58Barium [7440-39-3] ^1 1.00 JDH10.01.00 U 100
ug/L EPA 6010C 05/11/15 11:58Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 05/11/15 11:58Chromium [7440-47-3] ^1 1.40 JDH10.01.40 U 10
ug/L EPA 6010C 05/11/15 11:58Lead [7439-92-1] ^1 3.10 JDH10.03.10 U 10
ug/L EPA 6010C 05/11/15 11:58Selenium [7782-49-2] ^1 5.00 JDH10.05.00 U 10
ug/L EPA 6010C 05/11/15 11:58Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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5301-TripblankDescription:Lab Sample ID:C504926-09 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 09:15 Work Order:C504926
Lee CountyProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/07/15 02:351,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 MSZ1.00.17 U 5
ug/L EPA 8260B 05/07/15 02:351,1,1-Trichloroethane [71-55-6] ^1 0.12 MSZ1.00.12 U 1
ug/L EPA 8260B 05/07/15 02:351,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 MSZ1.00.28 U 3
ug/L EPA 8260B 05/07/15 02:351,1,2-Trichloroethane [79-00-5] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 02:351,1-Dichloroethane [75-34-3] ^1 0.13 MSZ1.00.13 U 5
ug/L EPA 8260B 05/07/15 02:351,1-Dichloroethene [75-35-4] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 02:351,2,3-Trichloropropane [96-18-4] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 02:351,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 MSZ1.00.48 U 13
ug/L EPA 8260B 05/07/15 02:351,2-Dibromoethane [106-93-4] ^1 0.66 MSZ1.00.66 U 1
ug/L EPA 8260B 05/07/15 02:351,2-Dichlorobenzene [95-50-1] ^1 0.19 MSZ1.00.19 U 5
ug/L EPA 8260B 05/07/15 02:351,2-Dichloroethane [107-06-2] ^1 0.21 MSZ1.00.21 U 1
ug/L EPA 8260B 05/07/15 02:351,2-Dichloropropane [78-87-5] ^1 0.10 MSZ1.00.10 U 1
ug/L EPA 8260B 05/07/15 02:351,4-Dichlorobenzene [106-46-7] ^1 0.19 MSZ1.00.19 U 1
ug/L EPA 8260B 05/07/15 02:352-Butanone [78-93-3] ^1 1.3 MSZ5.01.3 U 100
ug/L EPA 8260B 05/07/15 02:352-Hexanone [591-78-6] ^1 0.88 MSZ5.00.88 U 50
ug/L EPA 8260B 05/07/15 02:354-Methyl-2-pentanone [108-10-1] ^1 1.1 MSZ5.01.1 U 100
ug/L EPA 8260B 05/07/15 02:35Acetone [67-64-1] ^1 1.2 MSZ5.01.2 U 100
ug/L EPA 8260B 05/07/15 02:35Acrylonitrile [107-13-1] ^1 3.5 MSZ103.5 U 200
ug/L EPA 8260B 05/07/15 02:35Benzene [71-43-2] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 02:35Bromochloromethane [74-97-5] ^1 0.48 MSZ1.00.48 U 3
ug/L EPA 8260B 05/07/15 02:35Bromodichloromethane [75-27-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 02:35Bromoform [75-25-2] ^1 0.22 MSZ1.00.22 U 3
ug/L EPA 8260B 05/07/15 02:35Bromomethane [74-83-9] ^1 0.14 MSZ1.00.14 U 10
ug/L EPA 8260B 05/07/15 02:35Carbon disulfide [75-15-0] ^1 1.5 MSZ5.01.5 U 100
ug/L EPA 8260B 05/07/15 02:35Carbon tetrachloride [56-23-5] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 02:35Chlorobenzene [108-90-7] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 02:35Chloroethane [75-00-3] ^1 0.23 MSZ1.00.23 U 10
ug/L EPA 8260B 05/07/15 02:35Chloroform [67-66-3] ^1 0.18 MSZ1.00.18 U 5
ug/L EPA 8260B 05/07/15 02:35Chloromethane [74-87-3] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 02:35cis-1,2-Dichloroethene [156-59-2] ^1 0.15 MSZ1.00.15 U 5
ug/L EPA 8260B 05/07/15 02:35cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 MSZ1.00.20 U 1
ug/L EPA 8260B 05/07/15 02:35Dibromochloromethane [124-48-1] ^1 0.17 MSZ1.00.17 U 3
ug/L EPA 8260B 05/07/15 02:35Dibromomethane [74-95-3] ^1 0.27 MSZ1.00.27 U 10
ug/L EPA 8260B 05/07/15 02:35Ethylbenzene [100-41-4] ^1 0.13 MSZ1.00.13 U 1
ug/L EPA 8260B 05/07/15 02:35Iodomethane [74-88-4] ^1 1.7 MSZ5.01.7 U 10
ug/L EPA 8260B 05/07/15 02:35m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 MSZ2.00.17 U NE
ug/L EPA 8260B 05/07/15 02:35Methylene chloride [75-09-2] ^1 0.23 MSZ1.00.23 U 1
ug/L EPA 8260B 05/07/15 02:35o-Xylene [95-47-6] ^1 0.065 MSZ1.00.065 U NE
ug/L EPA 8260B 05/07/15 02:35Styrene [100-42-5] ^1 0.11 MSZ1.00.11 U 1
ug/L EPA 8260B 05/07/15 02:35Tetrachloroethene [127-18-4] ^1 0.17 MSZ1.00.17 U 1
ug/L EPA 8260B 05/07/15 02:35Toluene [108-88-3] ^1 0.14 MSZ1.00.14 U 1
ug/L EPA 8260B 05/07/15 02:35trans-1,2-Dichloroethene [156-60-5] ^1 0.21 MSZ1.00.21 U 5
ug/L EPA 8260B 05/07/15 02:35trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 02:35trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 MSZ1.00.70 U 100
ug/L EPA 8260B 05/07/15 02:35Trichloroethene [79-01-6] ^1 0.15 MSZ1.00.15 U 1
ug/L EPA 8260B 05/07/15 02:35Trichlorofluoromethane [75-69-4] ^1 0.24 MSZ1.00.24 U 1
ug/L EPA 8260B 05/07/15 02:35Vinyl acetate [108-05-4] ^1 0.95 MSZ5.00.95 U 50
ug/L EPA 8260B 05/07/15 02:35Vinyl chloride [75-01-4] ^1 0.32 MSZ1.00.32 U 1
ug/L EPA 8260B 05/07/15 02:35Xylenes (Total) [1330-20-7] ^1 0.45 MSZ3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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5301-TripblankDescription:Lab Sample ID:C504926-09 04/28/15 11:30Received:
Matrix:Water Sampled:04/24/15 09:15 Work Order:C504926
Lee CountyProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MSZEPA 8260B 05/07/15 02:355E060154450.0 1
Dibromofluoromethane 67-129124 %MSZEPA 8260B 05/07/15 02:355E060156250.0 1
Toluene-d8 59-134101 %MSZEPA 8260B 05/07/15 02:355E060155150.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 5E06012 - EPA 5030B_MS
Prepared: 05/06/2015 11:02 Analyzed: 05/06/2015 11:14Blank (5E06012-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
Page 39 of 48
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 5E06012 - EPA 5030B_MS
Prepared: 05/06/2015 11:02 Analyzed: 05/06/2015 11:14Blank (5E06012-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9045
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12362
ug/L 50.0 59-134Surrogate: Toluene-d8 10050
Prepared: 05/06/2015 11:02 Analyzed: 05/06/2015 11:43LCS (5E06012-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13311523 1,1-Dichloroethene
ug/L1.0 20.0 81-13410922 Benzene
ug/L1.0 20.0 83-11710421 Chlorobenzene
ug/L1.0 20.0 71-1189118 Toluene
ug/L1.0 20.0 74-11910822 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12160
ug/L 50.0 59-134Surrogate: Toluene-d8 10050
Prepared: 05/06/2015 11:02 Analyzed: 05/06/2015 12:13Matrix Spike (5E06012-MS1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331310.21 U26 1,1-Dichloroethene
ug/L1.0 20.0 81-1341150.15 U23 Benzene
ug/L1.0 20.0 83-1171090.17 U22 Chlorobenzene
ug/L1.0 20.0 71-118980.14 U20 Toluene
ug/L1.0 20.0 74-1191140.15 U23 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12261
ug/L 50.0 59-134Surrogate: Toluene-d8 9949
Prepared: 05/06/2015 11:02 Analyzed: 05/06/2015 12:43Matrix Spike Dup (5E06012-MSD1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133128 20.21 U26 1,1-Dichloroethene
ug/L1.0 20.0 1781-134113 20.15 U23 Benzene
ug/L1.0 20.0 1683-117110 10.17 U22 Chlorobenzene
ug/L1.0 20.0 1771-11896 20.14 U19 Toluene
ug/L1.0 20.0 2274-119112 20.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12060
ug/L 50.0 59-134Surrogate: Toluene-d8 9849
Batch 5E06015 - EPA 5030B_MS
Prepared: 05/06/2015 11:20 Analyzed: 05/06/2015 23:37Blank (5E06015-BLK1)
Page 40 of 48
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 5E06015 - EPA 5030B_MS
Prepared: 05/06/2015 11:20 Analyzed: 05/06/2015 23:37Blank (5E06015-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
Page 41 of 48
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 5E06015 - EPA 5030B_MS
Prepared: 05/06/2015 11:20 Analyzed: 05/06/2015 23:37Blank (5E06015-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9045
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12663
ug/L 50.0 59-134Surrogate: Toluene-d8 9950
Prepared: 05/06/2015 11:20 Analyzed: 05/07/2015 00:07LCS (5E06015-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13311423 1,1-Dichloroethene
ug/L1.0 20.0 81-13410721 Benzene
ug/L1.0 20.0 83-11710220 Chlorobenzene
ug/L1.0 20.0 71-1188918 Toluene
ug/L1.0 20.0 74-11910421 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12462
ug/L 50.0 59-134Surrogate: Toluene-d8 10150
Prepared: 05/06/2015 11:20 Analyzed: 05/07/2015 00:36Matrix Spike (5E06015-MS1)
Source: C505325-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331180.21 U24 1,1-Dichloroethene
ug/L1.0 20.0 81-1341070.15 U21 Benzene
ug/L1.0 20.0 83-1171030.17 U21 Chlorobenzene
ug/L1.0 20.0 71-118910.14 U18 Toluene
ug/L1.0 20.0 74-1191050.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9346
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12261
ug/L 50.0 59-134Surrogate: Toluene-d8 10050
Prepared: 05/06/2015 11:20 Analyzed: 05/07/2015 01:06Matrix Spike Dup (5E06015-MSD1)
Source: C505325-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133112 50.21 U22 1,1-Dichloroethene
ug/L1.0 20.0 1781-134104 30.15 U21 Benzene
ug/L1.0 20.0 1683-117100 30.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-11888 30.14 U18 Toluene
ug/L1.0 20.0 2274-119102 30.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12161
ug/L 50.0 59-134Surrogate: Toluene-d8 10251
Batch 5E07018 - EPA 5030B_MS
Prepared: 05/07/2015 10:17 Analyzed: 05/07/2015 11:47Blank (5E07018-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 5E07018 - EPA 5030B_MS
Prepared: 05/07/2015 10:17 Analyzed: 05/07/2015 11:47Blank (5E07018-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 5E07018 - EPA 5030B_MS
Prepared: 05/07/2015 10:17 Analyzed: 05/07/2015 11:47Blank (5E07018-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8743
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12161
ug/L 50.0 59-134Surrogate: Toluene-d8 9949
Prepared: 05/07/2015 10:17 Analyzed: 05/07/2015 12:17LCS (5E07018-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310822 1,1-Dichloroethene
ug/L1.0 20.0 81-13410621 Benzene
ug/L1.0 20.0 83-11710220 Chlorobenzene
ug/L1.0 20.0 71-1189018 Toluene
ug/L1.0 20.0 74-11910521 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9045
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12160
ug/L 50.0 59-134Surrogate: Toluene-d8 10050
Prepared: 05/07/2015 10:17 Analyzed: 05/07/2015 12:46Matrix Spike (5E07018-MS1)
Source: C504152-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331210.21 U24 1,1-Dichloroethene
ug/L1.0 20.0 81-1341110.15 U22 Benzene
ug/L1.0 20.0 83-1171060.17 U21 Chlorobenzene
ug/L1.0 20.0 71-118930.14 U19 Toluene
ug/L1.0 20.0 74-1191100.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 12261
ug/L 50.0 59-134Surrogate: Toluene-d8 10251
Prepared: 05/07/2015 10:17 Analyzed: 05/07/2015 13:16Matrix Spike Dup (5E07018-MSD1)
Source: C504152-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133111 80.21 U22 1,1-Dichloroethene
ug/L1.0 20.0 1781-134105 60.15 U21 Benzene
ug/L1.0 20.0 1683-117101 50.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-11889 50.14 U18 Toluene
ug/L1.0 20.0 2274-119105 50.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9146
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11959
ug/L 50.0 59-134Surrogate: Toluene-d8 9849
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 5E11017 - EPA 7470A
Prepared: 05/11/2015 11:25 Analyzed: 05/12/2015 12:22Blank (5E11017-BLK1)
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QUALITY CONTROL
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 5E11017 - EPA 7470A
Prepared: 05/11/2015 11:25 Analyzed: 05/12/2015 12:22Blank (5E11017-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.2000.170 U Mercury
Prepared: 05/11/2015 11:25 Analyzed: 05/12/2015 12:24LCS (5E11017-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 80-1201115.54 Mercury
Prepared: 05/11/2015 11:25 Analyzed: 05/12/2015 12:29Matrix Spike (5E11017-MS1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 75-1251520.170 U7.61 QM-07Mercury
Prepared: 05/11/2015 11:25 Analyzed: 05/12/2015 12:31Matrix Spike Dup (5E11017-MSD1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 2575-125145 50.170 U7.23 QM-07Mercury
Prepared: 05/11/2015 11:25 Analyzed: 05/12/2015 12:33Post Spike (5E11017-PS1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 75-1251400.01607.02 QM-08Mercury
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 5E07038 - EPA 3005A
Prepared: 05/07/2015 13:21 Analyzed: 05/11/2015 10:29Blank (5E07038-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.03.10 U Lead
ug/L10.05.00 U Selenium
ug/L10.01.90 U Silver
Prepared: 05/07/2015 13:21 Analyzed: 05/11/2015 10:36LCS (5E07038-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12097194 Arsenic
ug/L10.0 200 80-12099198 Barium
ug/L1.00 20.0 80-1209919.8 Cadmium
ug/L10.0 200 80-12098195 Chromium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 5E07038 - EPA 3005A
Prepared: 05/07/2015 13:21 Analyzed: 05/11/2015 10:36LCS (5E07038-BS1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12098196 Lead
ug/L10.0 200 80-12092185 Selenium
ug/L10.0 200 80-12094188 Silver
Prepared: 05/07/2015 13:21 Analyzed: 05/11/2015 10:41Matrix Spike (5E07038-MS1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251096.80 U218 Arsenic
ug/L10.0 200 75-125109160379 Barium
ug/L1.00 20.0 75-1251110.360 U22.3 Cadmium
ug/L10.0 200 75-1251111.40 U222 Chromium
ug/L10.0 200 75-1251103.90223 Lead
ug/L10.0 200 75-1251085.00 U216 Selenium
ug/L10.0 200 75-1251051.90 U211 Silver
Prepared: 05/07/2015 13:21 Analyzed: 05/11/2015 10:44Matrix Spike Dup (5E07038-MSD1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125110 0.86.80 U220 Arsenic
ug/L10.0 200 2075-125108 0.6160376 Barium
ug/L1.00 20.0 2075-125111 0.30.360 U22.2 Cadmium
ug/L10.0 200 2075-125110 0.41.40 U221 Chromium
ug/L10.0 200 2075-125109 0.23.90223 Lead
ug/L10.0 200 2075-125109 15.00 U218 Selenium
ug/L10.0 200 2075-125105 0.61.90 U210 Silver
Prepared: 05/07/2015 13:21 Analyzed: 05/11/2015 10:46Post Spike (5E07038-PS1)
Source: C504926-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-1201080.006360.223 Arsenic
mg/L0.0100 0.200 80-1201070.1600.375 Barium
mg/L0.00100 0.0200 80-1201080.0003230.0219 Cadmium
mg/L0.0100 0.200 80-1201080.001260.218 Chromium
mg/L0.0100 0.200 80-1201110.003900.226 Lead
mg/L0.0100 0.200 80-1201090.001310.219 Selenium
mg/L0.0100 0.200 80-1201040.0008120.208 Silver
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
Post-digestion spike did not meet method requirements due to confirmed matrix effects
(dilution test).
QM-08
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