SW_F_5601-MSWLF-1980_08-29-2013_RM_GW

#=CL#
September 13, 2013
LIMS USE: FR - MIKE GLADDEN
LIMS OBJECT ID: 92170518
92170518
Project:
Pace Project No.:
RE:
Mr. Mike Gladden
McDowell County Landfill
10 East Court St.
Marion, NC 28752
GWM August 2013
Dear Mr. Gladden:
Enclosed are the analytical results for sample(s) received by the laboratory on August 29, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92170518
GWM August 2013
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92170518
GWM August 2013
Lab ID Sample ID Matrix Date Collected Date Received
92170518001 MW-1 Water 08/28/13 12:30 08/29/13 08:30
92170518002 MW-2 Water 08/28/13 13:45 08/29/13 08:30
92170518003 MW-3 Water 08/28/13 12:55 08/29/13 08:30
92170518004 MW-4 Water 08/28/13 13:30 08/29/13 08:30
92170518005 TRAVEL BLANK Water 08/28/13 13:30 08/29/13 08:30
92170518006 EQUIP BLANK Water 08/28/13 00:00 08/29/13 08:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92170518
GWM August 2013
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92170518001 MW-1 EPA 6010 15 PASI-AJDA
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92170518002 MW-2 EPA 6010 15 PASI-AJDA
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92170518003 MW-3 EPA 6010 15 PASI-AJDA
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92170518004 MW-4 EPA 6010 15 PASI-AJDA
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92170518005 TRAVEL BLANK EPA 8260 67 PASI-CMCK
92170518006 EQUIP BLANK EPA 6010 15 PASI-AJDA
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-1 Lab ID:92170518001 Collected:08/28/13 12:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Monitoring Well Data Analytical Method:
Collected By MPS 09/11/13 12:171
Collected Date 8/28/13 09/11/13 12:171
Collected Time 12:30 09/11/13 12:171
Field pH 5.6 Std. Units 09/11/13 12:170.10 0.10 1
Field Temperature 16.7 deg C 09/11/13 12:170.50 0.50 1
Static Water Level 28.92 feet 09/11/13 12:171
Field Specific Conductance 39.5 umhos/cm 09/11/13 12:171.0 1.0 1
Turbidity 25 NTU 09/11/13 12:171.0 1.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 09/06/13 22:55 7440-36-009/04/13 08:555.0 5.0 1
Arsenic ND ug/L 09/06/13 22:55 7440-38-209/04/13 08:5510.0 5.0 1
Barium 77.7 ug/L 09/06/13 22:55 7440-39-309/04/13 08:555.0 5.0 1
Beryllium ND ug/L 09/06/13 22:55 7440-41-709/04/13 08:551.0 1.0 1
Cadmium ND ug/L 09/06/13 22:55 7440-43-909/04/13 08:551.0 1.0 1
Chromium ND ug/L 09/06/13 22:55 7440-47-309/04/13 08:555.0 5.0 1
Cobalt ND ug/L 09/06/13 22:55 7440-48-409/04/13 08:555.0 5.0 1
Copper ND ug/L 09/06/13 22:55 7440-50-809/04/13 08:555.0 5.0 1
Lead 5.1 ug/L 09/08/13 15:32 7439-92-109/04/13 08:555.0 5.0 1
Nickel ND ug/L 09/06/13 22:55 7440-02-009/04/13 08:555.0 5.0 1
Selenium ND ug/L 09/06/13 22:55 7782-49-209/04/13 08:5510.0 10.0 1
Silver ND ug/L 09/06/13 22:55 7440-22-409/04/13 08:555.0 5.0 1
Thallium ND ug/L 09/06/13 22:55 7440-28-009/04/13 08:555.4 5.4 1
Vanadium 22.2 ug/L 09/06/13 22:55 7440-62-209/04/13 08:555.0 5.0 1
Zinc 14.0 ug/L 09/06/13 22:55 7440-66-609/04/13 08:5510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 09/04/13 16:52 7439-97-608/30/13 15:250.20 0.10 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 09/04/13 21:24 67-64-125.0 10.0 1
Acrolein ND ug/L 09/04/13 21:24 107-02-810.0 1.6 1
Acrylonitrile ND ug/L 09/04/13 21:24 107-13-110.0 1.9 1
Allyl chloride ND ug/L 09/04/13 21:24 107-05-12.0 1.5 1
Benzene ND ug/L 09/04/13 21:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/04/13 21:24 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/04/13 21:24 75-27-41.0 0.18 1
Bromoform ND ug/L 09/04/13 21:24 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/04/13 21:24 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/04/13 21:24 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 09/04/13 21:24 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 09/04/13 21:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/04/13 21:24 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/04/13 21:24 75-00-31.0 0.54 1
Chloroform ND ug/L 09/04/13 21:24 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/04/13 21:24 74-87-31.0 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-1 Lab ID:92170518001 Collected:08/28/13 12:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Cyclohexane ND ug/L 09/04/13 21:24 110-82-71.0 0.36 1
Dibromochloromethane ND ug/L 09/04/13 21:24 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/04/13 21:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/04/13 21:24 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/04/13 21:24 95-50-11.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/04/13 21:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/04/13 21:24 110-57-61.0 1.0 1
1,1-Dichloroethane ND ug/L 09/04/13 21:24 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/04/13 21:24 107-06-21.0 0.12 1
cis-1,2-Dichloroethene ND ug/L 09/04/13 21:24 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/04/13 21:24 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/04/13 21:24 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/04/13 21:24 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 09/04/13 21:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/04/13 21:24 10061-02-61.0 0.26 1
Diethyl ether (Ethyl ether)ND ug/L 09/04/13 21:24 60-29-71.0 0.18 1
Diisopropyl ether ND ug/L 09/04/13 21:24 108-20-31.0 0.12 1
Ethyl acetate ND ug/L 09/04/13 21:24 141-78-620.0 0.48 1
Ethylbenzene ND ug/L 09/04/13 21:24 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/04/13 21:24 97-63-21.0 0.20 1
n-Hexane ND ug/L 09/04/13 21:24 110-54-31.0 0.55 1
Iodomethane ND ug/L 09/04/13 21:24 74-88-45.0 0.32 1
Isobutanol ND ug/L 09/04/13 21:24 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/04/13 21:24 126-98-710.0 0.93 1
Methyl acetate ND ug/L 09/04/13 21:24 79-20-910.0 0.82 1
Methylcyclohexane ND ug/L 09/04/13 21:24 108-87-210.0 1.9 1
Methylene Chloride ND ug/L 09/04/13 21:24 75-09-22.0 0.97 1
Methyl methacrylate ND ug/L 09/04/13 21:24 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/04/13 21:24 108-10-15.0 0.33 1
Propionitrile ND ug/L 09/04/13 21:24 107-12-020.0 3.6 1
Styrene ND ug/L 09/04/13 21:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/04/13 21:24 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/04/13 21:24 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/04/13 21:24 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/04/13 21:24 109-99-910.0 3.1 1
Toluene ND ug/L 09/04/13 21:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/04/13 21:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/04/13 21:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/04/13 21:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/04/13 21:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/04/13 21:24 96-18-41.0 0.41 1
1,2,3-Trimethylbenzene ND ug/L 09/04/13 21:24 526-73-81.0 0.090 1
Vinyl acetate ND ug/L 09/04/13 21:24 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/04/13 21:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/04/13 21:24 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 09/04/13 21:24 179601-23-12.0 0.66 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-1 Lab ID:92170518001 Collected:08/28/13 12:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
o-Xylene ND ug/L 09/04/13 21:24 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %09/04/13 21:24 460-00-470-130 1
Dibromofluoromethane (S)103 %09/04/13 21:24 1868-53-770-130 1
1,2-Dichloroethane-d4 (S)108 %09/04/13 21:24 17060-07-070-130 1
Toluene-d8 (S)93 %09/04/13 21:24 2037-26-570-130 1
Sample:MW-2 Lab ID:92170518002 Collected:08/28/13 13:45 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Monitoring Well Data Analytical Method:
Collected By MPS 09/11/13 12:231
Collected Date 8/28/13 09/11/13 12:231
Collected Time 13:45 09/11/13 12:231
Field pH 5.6 Std. Units 09/11/13 12:230.10 0.10 1
Field Temperature 17.8 deg C 09/11/13 12:230.50 0.50 1
Static Water Level 37.34 feet 09/11/13 12:231
Field Specific Conductance 790 umhos/cm 09/11/13 12:231.0 1.0 1
Turbidity 3.14 NTU 09/11/13 12:231.0 1.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 09/06/13 22:58 7440-36-009/04/13 08:555.0 5.0 1
Arsenic 6.2J ug/L 09/06/13 22:58 7440-38-209/04/13 08:5510.0 5.0 1
Barium 197 ug/L 09/06/13 22:58 7440-39-309/04/13 08:555.0 5.0 1
Beryllium ND ug/L 09/06/13 22:58 7440-41-709/04/13 08:551.0 1.0 1
Cadmium ND ug/L 09/06/13 22:58 7440-43-909/04/13 08:551.0 1.0 1
Chromium 5.7 ug/L 09/06/13 22:58 7440-47-309/04/13 08:555.0 5.0 1
Cobalt 29.4 ug/L 09/06/13 22:58 7440-48-409/04/13 08:555.0 5.0 1
Copper ND ug/L 09/06/13 22:58 7440-50-809/04/13 08:555.0 5.0 1
Lead 6.5 ug/L 09/08/13 15:35 7439-92-109/04/13 08:555.0 5.0 1
Nickel 10.5 ug/L 09/06/13 22:58 7440-02-009/04/13 08:555.0 5.0 1
Selenium ND ug/L 09/06/13 22:58 7782-49-209/04/13 08:5510.0 10.0 1
Silver ND ug/L 09/06/13 22:58 7440-22-409/04/13 08:555.0 5.0 1
Thallium ND ug/L 09/06/13 22:58 7440-28-009/04/13 08:555.4 5.4 1
Vanadium 16.4 ug/L 09/06/13 22:58 7440-62-209/04/13 08:555.0 5.0 1
Zinc 20.2 ug/L 09/06/13 22:58 7440-66-609/04/13 08:5510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 09/04/13 16:54 7439-97-608/30/13 15:250.20 0.10 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 28.5 ug/L 09/04/13 21:39 67-64-125.0 10.0 1
Acrolein ND ug/L 09/04/13 21:39 107-02-810.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-2 Lab ID:92170518002 Collected:08/28/13 13:45 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Acrylonitrile ND ug/L 09/04/13 21:39 107-13-110.0 1.9 1
Allyl chloride ND ug/L 09/04/13 21:39 107-05-12.0 1.5 1
Benzene 4.7 ug/L 09/04/13 21:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/04/13 21:39 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/04/13 21:39 75-27-41.0 0.18 1
Bromoform ND ug/L 09/04/13 21:39 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/04/13 21:39 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/04/13 21:39 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 09/04/13 21:39 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 09/04/13 21:39 56-23-51.0 0.25 1
Chlorobenzene 17.6 ug/L 09/04/13 21:39 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/04/13 21:39 75-00-31.0 0.54 1
Chloroform ND ug/L 09/04/13 21:39 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/04/13 21:39 74-87-31.0 0.11 1
Cyclohexane ND ug/L 09/04/13 21:39 110-82-71.0 0.36 1
Dibromochloromethane ND ug/L 09/04/13 21:39 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/04/13 21:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/04/13 21:39 74-95-31.0 0.21 1
1,2-Dichlorobenzene 2.6 ug/L 09/04/13 21:39 95-50-11.0 0.30 1
1,4-Dichlorobenzene 11.1 ug/L 09/04/13 21:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/04/13 21:39 110-57-61.0 1.0 1
1,1-Dichloroethane 0.89J ug/L 09/04/13 21:39 75-34-31.0 0.32 1
1,2-Dichloroethane 0.19J ug/L 09/04/13 21:39 107-06-21.0 0.12 1
cis-1,2-Dichloroethene 30.9 ug/L 09/04/13 21:39 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/04/13 21:39 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/04/13 21:39 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/04/13 21:39 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 09/04/13 21:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/04/13 21:39 10061-02-61.0 0.26 1
Diethyl ether (Ethyl ether)24.2 ug/L 09/04/13 21:39 60-29-71.0 0.18 1
Diisopropyl ether 1.1 ug/L 09/04/13 21:39 108-20-31.0 0.12 1
Ethyl acetate ND ug/L 09/04/13 21:39 141-78-620.0 0.48 1
Ethylbenzene 0.36J ug/L 09/04/13 21:39 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/04/13 21:39 97-63-21.0 0.20 1
n-Hexane ND ug/L 09/04/13 21:39 110-54-31.0 0.55 1
Iodomethane ND ug/L 09/04/13 21:39 74-88-45.0 0.32 1
Isobutanol ND ug/L 09/04/13 21:39 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/04/13 21:39 126-98-710.0 0.93 1
Methyl acetate ND ug/L 09/04/13 21:39 79-20-910.0 0.82 1
Methylcyclohexane ND ug/L 09/04/13 21:39 108-87-210.0 1.9 1
Methylene Chloride ND ug/L 09/04/13 21:39 75-09-22.0 0.97 1
Methyl methacrylate ND ug/L 09/04/13 21:39 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/04/13 21:39 108-10-15.0 0.33 1
Propionitrile ND ug/L 09/04/13 21:39 107-12-020.0 3.6 1
Styrene ND ug/L 09/04/13 21:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/04/13 21:39 630-20-61.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-2 Lab ID:92170518002 Collected:08/28/13 13:45 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
1,1,2,2-Tetrachloroethane ND ug/L 09/04/13 21:39 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/04/13 21:39 127-18-41.0 0.46 1
Tetrahydrofuran 120 ug/L 09/04/13 21:39 109-99-910.0 3.1 1
Toluene 0.38J ug/L 09/04/13 21:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/04/13 21:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/04/13 21:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/04/13 21:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/04/13 21:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/04/13 21:39 96-18-41.0 0.41 1
1,2,3-Trimethylbenzene 0.22J ug/L 09/04/13 21:39 526-73-81.0 0.090 1
Vinyl acetate ND ug/L 09/04/13 21:39 108-05-42.0 0.35 1
Vinyl chloride 2.1 ug/L 09/04/13 21:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/04/13 21:39 1330-20-72.0 0.66 1
m&p-Xylene 0.84J ug/L 09/04/13 21:39 179601-23-12.0 0.66 1
o-Xylene 0.28J ug/L 09/04/13 21:39 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %09/04/13 21:39 460-00-470-130 1
Dibromofluoromethane (S)102 %09/04/13 21:39 1868-53-770-130 1
1,2-Dichloroethane-d4 (S)105 %09/04/13 21:39 17060-07-070-130 1
Toluene-d8 (S)95 %09/04/13 21:39 2037-26-570-130 1
Sample:MW-3 Lab ID:92170518003 Collected:08/28/13 12:55 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Monitoring Well Data Analytical Method:
Collected By MPS 09/11/13 12:281
Collected Date 8/28/13 09/11/13 12:281
Collected Time 12:55 09/11/13 12:281
Field pH 5.8 Std. Units 09/11/13 12:280.10 0.10 1
Field Temperature 18.3 deg C 09/11/13 12:280.50 0.50 1
Static Water Level 31.33 feet 09/11/13 12:281
Field Specific Conductance 431.4 umhos/cm 09/11/13 12:281.0 1.0 1
Turbidity 9.09 NTU 09/11/13 12:281.0 1.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 09/06/13 23:02 7440-36-009/04/13 08:555.0 5.0 1
Arsenic ND ug/L 09/06/13 23:02 7440-38-209/04/13 08:5510.0 5.0 1
Barium 730 ug/L 09/06/13 23:02 7440-39-309/04/13 08:555.0 5.0 1
Beryllium ND ug/L 09/06/13 23:02 7440-41-709/04/13 08:551.0 1.0 1
Cadmium ND ug/L 09/06/13 23:02 7440-43-909/04/13 08:551.0 1.0 1
Chromium ND ug/L 09/06/13 23:02 7440-47-309/04/13 08:555.0 5.0 1
Cobalt 85.7 ug/L 09/06/13 23:02 7440-48-409/04/13 08:555.0 5.0 1
Copper ND ug/L 09/06/13 23:02 7440-50-809/04/13 08:555.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-3 Lab ID:92170518003 Collected:08/28/13 12:55 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 09/08/13 15:39 7439-92-109/04/13 08:555.0 5.0 1
Nickel 16.4 ug/L 09/06/13 23:02 7440-02-009/04/13 08:555.0 5.0 1
Selenium ND ug/L 09/06/13 23:02 7782-49-209/04/13 08:5510.0 10.0 1
Silver ND ug/L 09/06/13 23:02 7440-22-409/04/13 08:555.0 5.0 1
Thallium ND ug/L 09/06/13 23:02 7440-28-009/04/13 08:555.4 5.4 1
Vanadium 6.4 ug/L 09/06/13 23:02 7440-62-209/04/13 08:555.0 5.0 1
Zinc 56.1 ug/L 09/06/13 23:02 7440-66-609/04/13 08:5510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 09/04/13 16:57 7439-97-608/30/13 15:250.20 0.10 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 09/04/13 21:55 67-64-125.0 10.0 1
Acrolein ND ug/L 09/04/13 21:55 107-02-810.0 1.6 1
Acrylonitrile ND ug/L 09/04/13 21:55 107-13-110.0 1.9 1
Allyl chloride ND ug/L 09/04/13 21:55 107-05-12.0 1.5 1
Benzene ND ug/L 09/04/13 21:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/04/13 21:55 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/04/13 21:55 75-27-41.0 0.18 1
Bromoform ND ug/L 09/04/13 21:55 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/04/13 21:55 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/04/13 21:55 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 09/04/13 21:55 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 09/04/13 21:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/04/13 21:55 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/04/13 21:55 75-00-31.0 0.54 1
Chloroform ND ug/L 09/04/13 21:55 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/04/13 21:55 74-87-31.0 0.11 1
Cyclohexane ND ug/L 09/04/13 21:55 110-82-71.0 0.36 1
Dibromochloromethane ND ug/L 09/04/13 21:55 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/04/13 21:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/04/13 21:55 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/04/13 21:55 95-50-11.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/04/13 21:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/04/13 21:55 110-57-61.0 1.0 1
1,1-Dichloroethane ND ug/L 09/04/13 21:55 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/04/13 21:55 107-06-21.0 0.12 1
cis-1,2-Dichloroethene ND ug/L 09/04/13 21:55 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/04/13 21:55 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/04/13 21:55 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/04/13 21:55 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 09/04/13 21:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/04/13 21:55 10061-02-61.0 0.26 1
Diethyl ether (Ethyl ether)ND ug/L 09/04/13 21:55 60-29-71.0 0.18 1
Diisopropyl ether ND ug/L 09/04/13 21:55 108-20-31.0 0.12 1
Ethyl acetate ND ug/L 09/04/13 21:55 141-78-620.0 0.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-3 Lab ID:92170518003 Collected:08/28/13 12:55 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Ethylbenzene ND ug/L 09/04/13 21:55 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/04/13 21:55 97-63-21.0 0.20 1
n-Hexane ND ug/L 09/04/13 21:55 110-54-31.0 0.55 1
Iodomethane ND ug/L 09/04/13 21:55 74-88-45.0 0.32 1
Isobutanol ND ug/L 09/04/13 21:55 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/04/13 21:55 126-98-710.0 0.93 1
Methyl acetate ND ug/L 09/04/13 21:55 79-20-910.0 0.82 1
Methylcyclohexane ND ug/L 09/04/13 21:55 108-87-210.0 1.9 1
Methylene Chloride ND ug/L 09/04/13 21:55 75-09-22.0 0.97 1
Methyl methacrylate ND ug/L 09/04/13 21:55 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/04/13 21:55 108-10-15.0 0.33 1
Propionitrile ND ug/L 09/04/13 21:55 107-12-020.0 3.6 1
Styrene ND ug/L 09/04/13 21:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/04/13 21:55 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/04/13 21:55 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/04/13 21:55 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/04/13 21:55 109-99-910.0 3.1 1
Toluene ND ug/L 09/04/13 21:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/04/13 21:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/04/13 21:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/04/13 21:55 79-01-61.0 0.47 1
Trichlorofluoromethane 0.58J ug/L 09/04/13 21:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/04/13 21:55 96-18-41.0 0.41 1
1,2,3-Trimethylbenzene ND ug/L 09/04/13 21:55 526-73-81.0 0.090 1
Vinyl acetate ND ug/L 09/04/13 21:55 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/04/13 21:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/04/13 21:55 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 09/04/13 21:55 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/04/13 21:55 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %09/04/13 21:55 460-00-470-130 1
Dibromofluoromethane (S)98 %09/04/13 21:55 1868-53-770-130 1
1,2-Dichloroethane-d4 (S)107 %09/04/13 21:55 17060-07-070-130 1
Toluene-d8 (S)93 %09/04/13 21:55 2037-26-570-130 1
Sample:MW-4 Lab ID:92170518004 Collected:08/28/13 13:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Monitoring Well Data Analytical Method:
Collected By MPS 09/11/13 12:291
Collected Date 8/28/13 09/11/13 12:291
Collected Time 13:30 09/11/13 12:291
Field pH 4.6 Std. Units 09/11/13 12:290.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-4 Lab ID:92170518004 Collected:08/28/13 13:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Monitoring Well Data Analytical Method:
Field Temperature 21.1 deg C 09/11/13 12:290.50 0.50 1
Static Water Level 17.93 feet 09/11/13 12:291
Field Specific Conductance 677 umhos/cm 09/11/13 12:291.0 1.0 1
Turbidity 4.25 NTU 09/11/13 12:291.0 1.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 09/06/13 23:05 7440-36-009/04/13 08:555.0 5.0 1
Arsenic ND ug/L 09/06/13 23:05 7440-38-209/04/13 08:5510.0 5.0 1
Barium 834 ug/L 09/06/13 23:05 7440-39-309/04/13 08:555.0 5.0 1
Beryllium ND ug/L 09/06/13 23:05 7440-41-709/04/13 08:551.0 1.0 1
Cadmium ND ug/L 09/06/13 23:05 7440-43-909/04/13 08:551.0 1.0 1
Chromium ND ug/L 09/06/13 23:05 7440-47-309/04/13 08:555.0 5.0 1
Cobalt ND ug/L 09/06/13 23:05 7440-48-409/04/13 08:555.0 5.0 1
Copper ND ug/L 09/06/13 23:05 7440-50-809/04/13 08:555.0 5.0 1
Lead ND ug/L 09/08/13 15:42 7439-92-109/04/13 08:555.0 5.0 1
Nickel ND ug/L 09/06/13 23:05 7440-02-009/04/13 08:555.0 5.0 1
Selenium ND ug/L 09/06/13 23:05 7782-49-209/04/13 08:5510.0 10.0 1
Silver ND ug/L 09/06/13 23:05 7440-22-409/04/13 08:555.0 5.0 1
Thallium ND ug/L 09/06/13 23:05 7440-28-009/04/13 08:555.4 5.4 1
Vanadium ND ug/L 09/06/13 23:05 7440-62-209/04/13 08:555.0 5.0 1
Zinc 33.1 ug/L 09/06/13 23:05 7440-66-609/04/13 08:5510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 09/04/13 17:05 7439-97-608/30/13 15:250.20 0.10 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 09/04/13 22:11 67-64-125.0 10.0 1
Acrolein ND ug/L 09/04/13 22:11 107-02-810.0 1.6 1
Acrylonitrile ND ug/L 09/04/13 22:11 107-13-110.0 1.9 1
Allyl chloride ND ug/L 09/04/13 22:11 107-05-12.0 1.5 1
Benzene ND ug/L 09/04/13 22:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/04/13 22:11 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/04/13 22:11 75-27-41.0 0.18 1
Bromoform ND ug/L 09/04/13 22:11 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/04/13 22:11 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/04/13 22:11 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 09/04/13 22:11 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 09/04/13 22:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/04/13 22:11 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/04/13 22:11 75-00-31.0 0.54 1
Chloroform ND ug/L 09/04/13 22:11 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/04/13 22:11 74-87-31.0 0.11 1
Cyclohexane ND ug/L 09/04/13 22:11 110-82-71.0 0.36 1
Dibromochloromethane ND ug/L 09/04/13 22:11 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/04/13 22:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/04/13 22:11 74-95-31.0 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-4 Lab ID:92170518004 Collected:08/28/13 13:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene ND ug/L 09/04/13 22:11 95-50-11.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/04/13 22:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/04/13 22:11 110-57-61.0 1.0 1
1,1-Dichloroethane ND ug/L 09/04/13 22:11 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/04/13 22:11 107-06-21.0 0.12 1
cis-1,2-Dichloroethene ND ug/L 09/04/13 22:11 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/04/13 22:11 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/04/13 22:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/04/13 22:11 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 09/04/13 22:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/04/13 22:11 10061-02-61.0 0.26 1
Diethyl ether (Ethyl ether)ND ug/L 09/04/13 22:11 60-29-71.0 0.18 1
Diisopropyl ether ND ug/L 09/04/13 22:11 108-20-31.0 0.12 1
Ethyl acetate ND ug/L 09/04/13 22:11 141-78-620.0 0.48 1
Ethylbenzene ND ug/L 09/04/13 22:11 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/04/13 22:11 97-63-21.0 0.20 1
n-Hexane ND ug/L 09/04/13 22:11 110-54-31.0 0.55 1
Iodomethane ND ug/L 09/04/13 22:11 74-88-45.0 0.32 1
Isobutanol ND ug/L 09/04/13 22:11 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/04/13 22:11 126-98-710.0 0.93 1
Methyl acetate ND ug/L 09/04/13 22:11 79-20-910.0 0.82 1
Methylcyclohexane ND ug/L 09/04/13 22:11 108-87-210.0 1.9 1
Methylene Chloride ND ug/L 09/04/13 22:11 75-09-22.0 0.97 1
Methyl methacrylate ND ug/L 09/04/13 22:11 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/04/13 22:11 108-10-15.0 0.33 1
Propionitrile ND ug/L 09/04/13 22:11 107-12-020.0 3.6 1
Styrene ND ug/L 09/04/13 22:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/04/13 22:11 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/04/13 22:11 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/04/13 22:11 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/04/13 22:11 109-99-910.0 3.1 1
Toluene ND ug/L 09/04/13 22:11 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/04/13 22:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/04/13 22:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/04/13 22:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/04/13 22:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/04/13 22:11 96-18-41.0 0.41 1
1,2,3-Trimethylbenzene ND ug/L 09/04/13 22:11 526-73-81.0 0.090 1
Vinyl acetate ND ug/L 09/04/13 22:11 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/04/13 22:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/04/13 22:11 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 09/04/13 22:11 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/04/13 22:11 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %09/04/13 22:11 460-00-470-130 1
Dibromofluoromethane (S)101 %09/04/13 22:11 1868-53-770-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:MW-4 Lab ID:92170518004 Collected:08/28/13 13:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Surrogates
1,2-Dichloroethane-d4 (S)107 %09/04/13 22:11 17060-07-070-130 1
Toluene-d8 (S)95 %09/04/13 22:11 2037-26-570-130 1
Sample:TRAVEL BLANK Lab ID:92170518005 Collected:08/28/13 13:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 09/04/13 22:27 67-64-125.0 10.0 1
Acrolein ND ug/L 09/04/13 22:27 107-02-810.0 1.6 1
Acrylonitrile ND ug/L 09/04/13 22:27 107-13-110.0 1.9 1
Allyl chloride ND ug/L 09/04/13 22:27 107-05-12.0 1.5 1
Benzene ND ug/L 09/04/13 22:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/04/13 22:27 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/04/13 22:27 75-27-41.0 0.18 1
Bromoform ND ug/L 09/04/13 22:27 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/04/13 22:27 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/04/13 22:27 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 09/04/13 22:27 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 09/04/13 22:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/04/13 22:27 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/04/13 22:27 75-00-31.0 0.54 1
Chloroform ND ug/L 09/04/13 22:27 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/04/13 22:27 74-87-31.0 0.11 1
Cyclohexane ND ug/L 09/04/13 22:27 110-82-71.0 0.36 1
Dibromochloromethane ND ug/L 09/04/13 22:27 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/04/13 22:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/04/13 22:27 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/04/13 22:27 95-50-11.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/04/13 22:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/04/13 22:27 110-57-61.0 1.0 1
1,1-Dichloroethane ND ug/L 09/04/13 22:27 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/04/13 22:27 107-06-21.0 0.12 1
cis-1,2-Dichloroethene ND ug/L 09/04/13 22:27 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/04/13 22:27 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/04/13 22:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/04/13 22:27 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 09/04/13 22:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/04/13 22:27 10061-02-61.0 0.26 1
Diethyl ether (Ethyl ether)ND ug/L 09/04/13 22:27 60-29-71.0 0.18 1
Diisopropyl ether ND ug/L 09/04/13 22:27 108-20-31.0 0.12 1
Ethyl acetate ND ug/L 09/04/13 22:27 141-78-620.0 0.48 1
Ethylbenzene ND ug/L 09/04/13 22:27 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:TRAVEL BLANK Lab ID:92170518005 Collected:08/28/13 13:30 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Ethyl methacrylate ND ug/L 09/04/13 22:27 97-63-21.0 0.20 1
n-Hexane ND ug/L 09/04/13 22:27 110-54-31.0 0.55 1
Iodomethane ND ug/L 09/04/13 22:27 74-88-45.0 0.32 1
Isobutanol ND ug/L 09/04/13 22:27 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/04/13 22:27 126-98-710.0 0.93 1
Methyl acetate ND ug/L 09/04/13 22:27 79-20-910.0 0.82 1
Methylcyclohexane ND ug/L 09/04/13 22:27 108-87-210.0 1.9 1
Methylene Chloride ND ug/L 09/04/13 22:27 75-09-22.0 0.97 1
Methyl methacrylate ND ug/L 09/04/13 22:27 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/04/13 22:27 108-10-15.0 0.33 1
Propionitrile ND ug/L 09/04/13 22:27 107-12-020.0 3.6 1
Styrene ND ug/L 09/04/13 22:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/04/13 22:27 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/04/13 22:27 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/04/13 22:27 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/04/13 22:27 109-99-910.0 3.1 1
Toluene ND ug/L 09/04/13 22:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/04/13 22:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/04/13 22:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/04/13 22:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/04/13 22:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/04/13 22:27 96-18-41.0 0.41 1
1,2,3-Trimethylbenzene ND ug/L 09/04/13 22:27 526-73-81.0 0.090 1
Vinyl acetate ND ug/L 09/04/13 22:27 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/04/13 22:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/04/13 22:27 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 09/04/13 22:27 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/04/13 22:27 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %09/04/13 22:27 460-00-470-130 1
Dibromofluoromethane (S)103 %09/04/13 22:27 1868-53-770-130 1
1,2-Dichloroethane-d4 (S)109 %09/04/13 22:27 17060-07-070-130 1
Toluene-d8 (S)93 %09/04/13 22:27 2037-26-570-130 1
Sample:EQUIP BLANK Lab ID:92170518006 Collected:08/28/13 00:00 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 09/06/13 23:08 7440-36-009/04/13 08:555.0 5.0 1
Arsenic ND ug/L 09/06/13 23:08 7440-38-209/04/13 08:5510.0 5.0 1
Barium ND ug/L 09/06/13 23:08 7440-39-309/04/13 08:555.0 5.0 1
Beryllium ND ug/L 09/06/13 23:08 7440-41-709/04/13 08:551.0 1.0 1
Cadmium ND ug/L 09/06/13 23:08 7440-43-909/04/13 08:551.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:EQUIP BLANK Lab ID:92170518006 Collected:08/28/13 00:00 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 09/06/13 23:08 7440-47-309/04/13 08:555.0 5.0 1
Cobalt ND ug/L 09/06/13 23:08 7440-48-409/04/13 08:555.0 5.0 1
Copper ND ug/L 09/06/13 23:08 7440-50-809/04/13 08:555.0 5.0 1
Lead ND ug/L 09/08/13 15:45 7439-92-109/04/13 08:555.0 5.0 1
Nickel ND ug/L 09/06/13 23:08 7440-02-009/04/13 08:555.0 5.0 1
Selenium ND ug/L 09/06/13 23:08 7782-49-209/04/13 08:5510.0 10.0 1
Silver ND ug/L 09/06/13 23:08 7440-22-409/04/13 08:555.0 5.0 1
Thallium ND ug/L 09/06/13 23:08 7440-28-009/04/13 08:555.4 5.4 1
Vanadium ND ug/L 09/06/13 23:08 7440-62-209/04/13 08:555.0 5.0 1
Zinc ND ug/L 09/06/13 23:08 7440-66-609/04/13 08:5510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 09/04/13 17:08 7439-97-608/30/13 15:250.20 0.10 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 09/04/13 22:43 67-64-125.0 10.0 1
Acrolein ND ug/L 09/04/13 22:43 107-02-810.0 1.6 1
Acrylonitrile ND ug/L 09/04/13 22:43 107-13-110.0 1.9 1
Allyl chloride ND ug/L 09/04/13 22:43 107-05-12.0 1.5 1
Benzene ND ug/L 09/04/13 22:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/04/13 22:43 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/04/13 22:43 75-27-41.0 0.18 1
Bromoform ND ug/L 09/04/13 22:43 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/04/13 22:43 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/04/13 22:43 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 09/04/13 22:43 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 09/04/13 22:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/04/13 22:43 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/04/13 22:43 75-00-31.0 0.54 1
Chloroform ND ug/L 09/04/13 22:43 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/04/13 22:43 74-87-31.0 0.11 1
Cyclohexane ND ug/L 09/04/13 22:43 110-82-71.0 0.36 1
Dibromochloromethane ND ug/L 09/04/13 22:43 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/04/13 22:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/04/13 22:43 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/04/13 22:43 95-50-11.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/04/13 22:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/04/13 22:43 110-57-61.0 1.0 1
1,1-Dichloroethane ND ug/L 09/04/13 22:43 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/04/13 22:43 107-06-21.0 0.12 1
cis-1,2-Dichloroethene ND ug/L 09/04/13 22:43 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/04/13 22:43 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/04/13 22:43 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/04/13 22:43 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 09/04/13 22:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/04/13 22:43 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92170518
GWM August 2013
Sample:EQUIP BLANK Lab ID:92170518006 Collected:08/28/13 00:00 Received:08/29/13 08:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
8260 MSV Low Level Analytical Method: EPA 8260
Diethyl ether (Ethyl ether)ND ug/L 09/04/13 22:43 60-29-71.0 0.18 1
Diisopropyl ether ND ug/L 09/04/13 22:43 108-20-31.0 0.12 1
Ethyl acetate ND ug/L 09/04/13 22:43 141-78-620.0 0.48 1
Ethylbenzene ND ug/L 09/04/13 22:43 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/04/13 22:43 97-63-21.0 0.20 1
n-Hexane ND ug/L 09/04/13 22:43 110-54-31.0 0.55 1
Iodomethane ND ug/L 09/04/13 22:43 74-88-45.0 0.32 1
Isobutanol ND ug/L 09/04/13 22:43 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/04/13 22:43 126-98-710.0 0.93 1
Methyl acetate ND ug/L 09/04/13 22:43 79-20-910.0 0.82 1
Methylcyclohexane ND ug/L 09/04/13 22:43 108-87-210.0 1.9 1
Methylene Chloride ND ug/L 09/04/13 22:43 75-09-22.0 0.97 1
Methyl methacrylate ND ug/L 09/04/13 22:43 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/04/13 22:43 108-10-15.0 0.33 1
Propionitrile ND ug/L 09/04/13 22:43 107-12-020.0 3.6 1
Styrene ND ug/L 09/04/13 22:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/04/13 22:43 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/04/13 22:43 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/04/13 22:43 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/04/13 22:43 109-99-910.0 3.1 1
Toluene ND ug/L 09/04/13 22:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/04/13 22:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/04/13 22:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/04/13 22:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/04/13 22:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/04/13 22:43 96-18-41.0 0.41 1
1,2,3-Trimethylbenzene ND ug/L 09/04/13 22:43 526-73-81.0 0.090 1
Vinyl acetate ND ug/L 09/04/13 22:43 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/04/13 22:43 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/04/13 22:43 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 09/04/13 22:43 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/04/13 22:43 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %09/04/13 22:43 460-00-470-130 1
Dibromofluoromethane (S)98 %09/04/13 22:43 1868-53-770-130 1
1,2-Dichloroethane-d4 (S)108 %09/04/13 22:43 17060-07-070-130 1
Toluene-d8 (S)94 %09/04/13 22:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/5539
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1038662
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518006
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 09/04/13 16:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1038663LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.12.5 85 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1038664MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92170132001
1038665
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 84 75-12585 1 252.5ND 2.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/14119
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1040403
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518006
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 09/06/13 22:21
Arsenic ug/L ND 10.0 09/06/13 22:21
Barium ug/L ND 5.0 09/06/13 22:21
Beryllium ug/L ND 1.0 09/06/13 22:21
Cadmium ug/L ND 1.0 09/06/13 22:21
Chromium ug/L ND 5.0 09/06/13 22:21
Cobalt ug/L ND 5.0 09/06/13 22:21
Copper ug/L ND 5.0 09/06/13 22:21
Lead ug/L ND 5.0 09/06/13 22:21
Nickel ug/L ND 5.0 09/06/13 22:21
Selenium ug/L ND 10.0 09/06/13 22:21
Silver ug/L ND 5.0 09/06/13 22:21
Thallium ug/L ND 5.4 09/06/13 22:21
Vanadium ug/L ND 5.0 09/06/13 22:21
Zinc ug/L ND 10.0 09/06/13 22:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1040404LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 493500 99 80-120
Arsenic ug/L 485500 97 80-120
Barium ug/L 504500 101 80-120
Beryllium ug/L 501500 100 80-120
Cadmium ug/L 501500 100 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 495500 99 80-120
Copper ug/L 502500 100 80-120
Lead ug/L 492500 98 80-120
Nickel ug/L 511500 102 80-120
Selenium ug/L 498500 100 80-120
Silver ug/L 252250 101 80-120
Thallium ug/L 467500 93 80-120
Vanadium ug/L 514500 103 80-120
Zinc ug/L 505500 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1040405MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92170050010
1040406
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 100 75-12598 2 25500ND501492
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1040405MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92170050010
1040406
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 99 75-12598 1 25500ND496492
Barium ug/L 500 102 75-125100 2 2550033.3 544 534
Beryllium ug/L 500 102 75-125100 2 25500ND509500
Cadmium ug/L 500 100 75-12599 2 25500ND501493
Chromium ug/L 500 101 75-12599 2 25500ND506498
Cobalt ug/L 500 100 75-12598 2 25500ND499491
Copper ug/L 500 101 75-12599 2 25500ND503494
Lead ug/L 500 99 75-12597 2 25500ND496485
Nickel ug/L 500 102 75-125100 2 25500ND509500
Selenium ug/L 500 99 75-12598 1 25500ND498494
Silver ug/L 250 100 75-12599 2 25250ND250246
Thallium ug/L 500 95 75-12594 2 25500ND477470
Vanadium ug/L 500 104 75-125101 2 25500ND518506
Zinc ug/L 500 101 75-125100 1 25500ND516510
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/24129
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518005, 92170518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1040796
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518005, 92170518006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/04/13 18:14
1,1,1-Trichloroethane ug/L ND 1.0 09/04/13 18:14
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/04/13 18:14
1,1,2-Trichloroethane ug/L ND 1.0 09/04/13 18:14
1,1-Dichloroethane ug/L ND 1.0 09/04/13 18:14
1,2,3-Trichloropropane ug/L ND 1.0 09/04/13 18:14
1,2,3-Trimethylbenzene ug/L ND 1.0 09/04/13 18:14
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/04/13 18:14
1,2-Dichlorobenzene ug/L ND 1.0 09/04/13 18:14
1,2-Dichloroethane ug/L ND 1.0 09/04/13 18:14
1,2-Dichloropropane ug/L ND 1.0 09/04/13 18:14
1,3-Dichloropropane ug/L ND 1.0 09/04/13 18:14
1,4-Dichlorobenzene ug/L ND 1.0 09/04/13 18:14
2-Butanone (MEK)ug/L ND 5.0 09/04/13 18:14
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/04/13 18:14
Acetone ug/L ND 25.0 09/04/13 18:14
Acrolein ug/L ND 10.0 09/04/13 18:14
Acrylonitrile ug/L ND 10.0 09/04/13 18:14
Allyl chloride ug/L ND 2.0 09/04/13 18:14
Benzene ug/L ND 1.0 09/04/13 18:14
Bromochloromethane ug/L ND 1.0 09/04/13 18:14
Bromodichloromethane ug/L ND 1.0 09/04/13 18:14
Bromoform ug/L ND 1.0 09/04/13 18:14
Bromomethane ug/L ND 2.0 09/04/13 18:14
Carbon disulfide ug/L ND 2.0 09/04/13 18:14
Carbon tetrachloride ug/L ND 1.0 09/04/13 18:14
Chlorobenzene ug/L ND 1.0 09/04/13 18:14
Chloroethane ug/L ND 1.0 09/04/13 18:14
Chloroform ug/L ND 1.0 09/04/13 18:14
Chloromethane ug/L ND 1.0 09/04/13 18:14
cis-1,2-Dichloroethene ug/L ND 1.0 09/04/13 18:14
cis-1,3-Dichloropropene ug/L ND 1.0 09/04/13 18:14
Cyclohexane ug/L ND 1.0 09/04/13 18:14
Dibromochloromethane ug/L ND 1.0 09/04/13 18:14
Dibromomethane ug/L ND 1.0 09/04/13 18:14
Diethyl ether (Ethyl ether)ug/L ND 1.0 09/04/13 18:14
Diisopropyl ether ug/L ND 1.0 09/04/13 18:14
Ethyl acetate ug/L ND 20.0 09/04/13 18:14
Ethyl methacrylate ug/L ND 1.0 09/04/13 18:14
Ethylbenzene ug/L ND 1.0 09/04/13 18:14
Iodomethane ug/L ND 5.0 09/04/13 18:14
Isobutanol ug/L ND 100 09/04/13 18:14
m&p-Xylene ug/L ND 2.0 09/04/13 18:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1040796
Associated Lab Samples:92170518001, 92170518002, 92170518003, 92170518004, 92170518005, 92170518006
Matrix:Water
Analyzed
Methacrylonitrile ug/L ND 10.0 09/04/13 18:14
Methyl acetate ug/L ND 10.0 09/04/13 18:14
Methyl methacrylate ug/L ND 2.0 09/04/13 18:14
Methylcyclohexane ug/L ND 10.0 09/04/13 18:14
Methylene Chloride ug/L ND 2.0 09/04/13 18:14
n-Hexane ug/L ND 1.0 09/04/13 18:14
o-Xylene ug/L ND 1.0 09/04/13 18:14
Propionitrile ug/L ND 20.0 09/04/13 18:14
Styrene ug/L ND 1.0 09/04/13 18:14
Tetrachloroethene ug/L ND 1.0 09/04/13 18:14
Tetrahydrofuran ug/L ND 10.0 09/04/13 18:14
Toluene ug/L ND 1.0 09/04/13 18:14
trans-1,2-Dichloroethene ug/L ND 1.0 09/04/13 18:14
trans-1,3-Dichloropropene ug/L ND 1.0 09/04/13 18:14
trans-1,4-Dichloro-2-butene ug/L ND 1.0 09/04/13 18:14
Trichloroethene ug/L ND 1.0 09/04/13 18:14
Trichlorofluoromethane ug/L ND 1.0 09/04/13 18:14
Vinyl acetate ug/L ND 2.0 09/04/13 18:14
Vinyl chloride ug/L ND 1.0 09/04/13 18:14
Xylene (Total)ug/L ND 2.0 09/04/13 18:14
1,2-Dichloroethane-d4 (S)%101 70-130 09/04/13 18:14
4-Bromofluorobenzene (S)%99 70-130 09/04/13 18:14
Dibromofluoromethane (S)%99 70-130 09/04/13 18:14
Toluene-d8 (S)%93 70-130 09/04/13 18:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1040797LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.150 120 70-130
1,1,1-Trichloroethane ug/L 51.850 104 70-130
1,1,2,2-Tetrachloroethane ug/L 60.250 120 70-130
1,1,2-Trichloroethane ug/L 56.150 112 70-130
1,1-Dichloroethane ug/L 50.050 100 70-130
1,2,3-Trichloropropane ug/L 54.950 110 70-130
1,2,3-Trimethylbenzene ug/L 59.550 119 70-130
1,2-Dibromoethane (EDB)ug/L 59.650 119 70-130
1,2-Dichlorobenzene ug/L 64.750 129 70-130
1,2-Dichloroethane ug/L 51.950 104 70-130
1,2-Dichloropropane ug/L 50.150 100 70-130
1,3-Dichloropropane ug/L 56.550 113 70-130
1,4-Dichlorobenzene ug/L 63.250 126 70-130
2-Butanone (MEK)ug/L 105100 105 70-145
4-Methyl-2-pentanone (MIBK)ug/L 113100 113 70-140
Acetone ug/L 91.6100 92 50-175
Acrolein ug/L 255250 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1040797LABORATORY CONTROL SAMPLE:
LCSSpike
Acrylonitrile ug/L 239250 96 70-143
Allyl chloride ug/L 50.150 100 70-130
Benzene ug/L 53.750 107 70-130
Bromochloromethane ug/L 49.650 99 70-130
Bromodichloromethane ug/L 54.750 109 70-130
Bromoform ug/L 60.950 122 70-130
Bromomethane ug/L 53.550 107 54-130
Carbon disulfide ug/L 47.450 95 70-131
Carbon tetrachloride ug/L 52.550 105 70-132
Chlorobenzene ug/L 58.950 118 70-130
Chloroethane ug/L 48.850 98 64-134
Chloroform ug/L 52.850 106 70-130
Chloromethane ug/L 48.850 98 64-130
cis-1,2-Dichloroethene ug/L 49.350 99 70-131
cis-1,3-Dichloropropene ug/L 51.150 102 70-130
Cyclohexane ug/L 51.450 103 70-130
Dibromochloromethane ug/L 60.750 121 70-130
Dibromomethane ug/L 53.650 107 70-131
Diethyl ether (Ethyl ether)ug/L 49.250 98 70-130
Diisopropyl ether ug/L 51.950 104 70-130
Ethyl acetate ug/L 86.1100 86 70-130
Ethyl methacrylate ug/L 65.750 131 70-130
Ethylbenzene ug/L 57.050 114 70-130
Iodomethane ug/L 107100 107 49-180
Isobutanol ug/L 13901000 139 70-130
m&p-Xylene ug/L 117100 117 70-130
Methacrylonitrile ug/L 498500 100 70-130
Methyl acetate ug/L 49.650 99 70-130
Methyl methacrylate ug/L 50.750 101 70-130
Methylcyclohexane ug/L 53.450 107 70-130
Methylene Chloride ug/L 46.350 93 63-130
n-Hexane ug/L 47.450 95 70-130
o-Xylene ug/L 61.550 123 70-130
Propionitrile ug/L 514500 103 70-130
Styrene ug/L 60.450 121 70-130
Tetrachloroethene ug/L 59.250 118 70-130
Tetrahydrofuran ug/L 516500 103 70-130
Toluene ug/L 53.150 106 70-130
trans-1,2-Dichloroethene ug/L 48.950 98 70-130
trans-1,3-Dichloropropene ug/L 52.650 105 70-132
trans-1,4-Dichloro-2-butene ug/L 57.050 114 70-141
Trichloroethene ug/L 52.750 105 70-130
Trichlorofluoromethane ug/L 50.950 102 62-133
Vinyl acetate ug/L 112100 112 66-157
Vinyl chloride ug/L 45.850 92 69-130
Xylene (Total)ug/L 178150 119 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92170518
GWM August 2013
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1040797LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromofluoromethane (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1041938MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92170518004
1041939
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/L 50 113 70-148110 2 3050ND56.3 55.2
Chlorobenzene ug/L 50 125 70-146121 4 3050ND62.5 60.3
Toluene ug/L 50 126 70-155102 21 3050ND63.1 51.0
Trichloroethene ug/L 50 126 69-151114 10 3050ND63.1 57.2
1,2-Dichloroethane-d4 (S)%101 70-13099
4-Bromofluorobenzene (S)%90 70-130104
Dibromofluoromethane (S)%97 70-130107
Toluene-d8 (S)%107 70-13093
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92170518
GWM August 2013
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92170518
GWM August 2013
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92170518001 FLD/MW-1
92170518002 FLD/MW-2
92170518003 FLD/MW-3
92170518004 FLD/MW-4
92170518001 MPRP/14119 ICP/12854MW-1 EPA 3010 EPA 6010
92170518002 MPRP/14119 ICP/12854MW-2 EPA 3010 EPA 6010
92170518003 MPRP/14119 ICP/12854MW-3 EPA 3010 EPA 6010
92170518004 MPRP/14119 ICP/12854MW-4 EPA 3010 EPA 6010
92170518006 MPRP/14119 ICP/12854EQUIP BLANK EPA 3010 EPA 6010
92170518001 MERP/5539 MERC/5369MW-1 EPA 7470 EPA 7470
92170518002 MERP/5539 MERC/5369MW-2 EPA 7470 EPA 7470
92170518003 MERP/5539 MERC/5369MW-3 EPA 7470 EPA 7470
92170518004 MERP/5539 MERC/5369MW-4 EPA 7470 EPA 7470
92170518006 MERP/5539 MERC/5369EQUIP BLANK EPA 7470 EPA 7470
92170518001 MSV/24129MW-1 EPA 8260
92170518002 MSV/24129MW-2 EPA 8260
92170518003 MSV/24129MW-3 EPA 8260
92170518004 MSV/24129MW-4 EPA 8260
92170518005 MSV/24129TRAVEL BLANK EPA 8260
92170518006 MSV/24129EQUIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2013 01:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 28
Page 27 of 28
Page 28 of 28