SW_F_5601-MSWLF-1980_02-27-2014_RM_GW_2

#=CL#
March 26, 2014
LIMS USE: FR - MIKE GLADDEN
LIMS OBJECT ID: 92191404
92191404
Project:
Pace Project No.:
RE:
Mr. Mike Gladden
McDowell County Landfill
10 East Court St.
Marion, NC 28752
LANDFILL MW
Dear Mr. Gladden:
Enclosed are the analytical results for sample(s) received by the laboratory on February 27, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92191404
LANDFILL MW
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92191404
LANDFILL MW
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92191404001 MW-1 EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92191404002 MW-2 EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92191404003 MW-3 EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92191404004 MW-4 EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
92191404005 TVL BLK EPA 8260 67 PASI-CMCK
92191404006 EQUIP BLK EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 67 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-1 Lab ID:92191404001 Collected:02/27/14 12:50 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Monitoring Well Data Analytical Method:
Collected By MPS 02/28/14 16:031
Collected Date 02/27/13 02/28/14 16:031
Collected Time 12:50 02/28/14 16:031
Field pH 4.9 Std. Units 02/28/14 16:030.10 1
Field Temperature 18.8 deg C 02/28/14 16:030.50 1
Static Water Level 18.52 feet 02/28/14 16:031
Field Specific Conductance 607 umhos/cm 02/28/14 16:031.0 1
Turbidity 2.23 NTU 02/28/14 16:031.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 5.02 ug/L 03/04/14 23:32 7440-36-002/28/14 09:055.0 1
Arsenic 10.02 ug/L 03/04/14 23:32 7440-38-202/28/14 09:0510.0 1
Barium 672 ug/L 03/04/14 23:32 7440-39-302/28/14 09:055.0 1
Beryllium 1.02 ug/L 03/04/14 23:32 7440-41-702/28/14 09:051.0 1
Cadmium 1.02 ug/L 03/04/14 23:32 7440-43-902/28/14 09:051.0 1
Chromium 5.02 ug/L 03/04/14 23:32 7440-47-302/28/14 09:055.0 1
Cobalt 5.2 ug/L 03/04/14 23:32 7440-48-402/28/14 09:055.0 1
Copper 5.02 ug/L 03/04/14 23:32 7440-50-802/28/14 09:055.0 1
Lead 5.02 ug/L 03/04/14 23:32 7439-92-102/28/14 09:055.0 1
Nickel 5.02 ug/L 03/04/14 23:32 7440-02-002/28/14 09:055.0 1
Selenium 10.02 ug/L 03/04/14 23:32 7782-49-202/28/14 09:0510.0 1
Silver 5.02 ug/L 03/04/14 23:32 7440-22-402/28/14 09:055.0 1
Thallium 5.42 ug/L 03/04/14 23:32 7440-28-002/28/14 09:055.4 1
Vanadium 5.02 ug/L 03/04/14 23:32 7440-62-202/28/14 09:055.0 1
Zinc 23.2 ug/L 03/04/14 23:32 7440-66-602/28/14 09:0510.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury 0.202 ug/L 03/06/14 20:01 7439-97-602/28/14 16:450.20 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 25.02 ug/L 03/02/14 23:23 67-64-125.0 1
Acrolein 10.02 ug/L 03/02/14 23:23 107-02-810.0 1
Acrylonitrile 10.02 ug/L 03/02/14 23:23 107-13-110.0 1
Allyl chloride 2.02 ug/L 03/02/14 23:23 107-05-12.0 1
Benzene 1.02 ug/L 03/02/14 23:23 71-43-21.0 1
Bromochloromethane 1.02 ug/L 03/02/14 23:23 74-97-51.0 1
Bromodichloromethane 1.02 ug/L 03/02/14 23:23 75-27-41.0 1
Bromoform 1.02 ug/L 03/02/14 23:23 75-25-21.0 1
Bromomethane 2.02 ug/L 03/02/14 23:23 74-83-92.0 1
2-Butanone (MEK)5.02 ug/L 03/02/14 23:23 78-93-35.0 1
Carbon disulfide 2.02 ug/L 03/02/14 23:23 75-15-02.0 1
Carbon tetrachloride 1.02 ug/L 03/02/14 23:23 56-23-51.0 1
Chlorobenzene 1.02 ug/L 03/02/14 23:23 108-90-71.0 1
Chloroethane 1.02 ug/L 03/02/14 23:23 75-00-31.0 1
Chloroform 1.02 ug/L 03/02/14 23:23 67-66-31.0 1
Chloromethane 1.02 ug/L 03/02/14 23:23 74-87-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-1 Lab ID:92191404001 Collected:02/27/14 12:50 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Cyclohexane 1.02 ug/L 03/02/14 23:23 110-82-71.0 1
1,2-Dibromo-3-chloropropane 5.02 ug/L 03/02/14 23:23 96-12-85.0 1
Dibromochloromethane 1.02 ug/L 03/02/14 23:23 124-48-11.0 1
1,2-Dibromoethane (EDB)1.02 ug/L 03/02/14 23:23 106-93-41.0 1
Dibromomethane 1.02 ug/L 03/02/14 23:23 74-95-31.0 1
1,2-Dichlorobenzene 1.02 ug/L 03/02/14 23:23 95-50-11.0 1
1,4-Dichlorobenzene 1.02 ug/L 03/02/14 23:23 106-46-71.0 1
trans-1,4-Dichloro-2-butene 1.02 ug/L 03/02/14 23:23 110-57-61.0 1
1,1-Dichloroethane 1.02 ug/L 03/02/14 23:23 75-34-31.0 1
1,2-Dichloroethane 1.02 ug/L 03/02/14 23:23 107-06-21.0 1
cis-1,2-Dichloroethene 1.02 ug/L 03/02/14 23:23 156-59-21.0 1
trans-1,2-Dichloroethene 1.02 ug/L 03/02/14 23:23 156-60-51.0 1
1,2-Dichloropropane 1.02 ug/L 03/02/14 23:23 78-87-51.0 1
1,3-Dichloropropane 1.02 ug/L 03/02/14 23:23 142-28-91.0 1
cis-1,3-Dichloropropene 1.02 ug/L 03/02/14 23:23 10061-01-51.0 1
trans-1,3-Dichloropropene 1.02 ug/L 03/02/14 23:23 10061-02-61.0 1
Diethyl ether (Ethyl ether)1.02 ug/L 03/02/14 23:23 60-29-71.0 1
Diisopropyl ether 1.02 ug/L 03/02/14 23:23 108-20-31.0 1
Ethyl acetate 20.02 ug/L 03/02/14 23:23 141-78-620.0 1
Ethylbenzene 1.02 ug/L 03/02/14 23:23 100-41-41.0 1
Ethyl methacrylate 1.02 ug/L 03/02/14 23:23 97-63-21.0 1
n-Hexane 1.02 ug/L 03/02/14 23:23 110-54-31.0 1
Iodomethane 5.02 ug/L 03/02/14 23:23 74-88-45.0 1
Isobutanol 1002 ug/L 03/02/14 23:23 78-83-11001
Methacrylonitrile 10.02 ug/L 03/02/14 23:23 126-98-710.0 1
Methyl acetate 10.02 ug/L 03/02/14 23:23 79-20-910.0 1
Methylcyclohexane 10.02 ug/L 03/02/14 23:23 108-87-210.0 1
Methylene Chloride 2.02 ug/L 03/02/14 23:23 75-09-22.0 1
Methyl methacrylate 2.02 ug/L 03/02/14 23:23 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)5.02 ug/L 03/02/14 23:23 108-10-15.0 1
Propionitrile 20.02 ug/L 03/02/14 23:23 107-12-020.0 1
Styrene 1.02 ug/L 03/02/14 23:23 100-42-51.0 1
1,1,1,2-Tetrachloroethane 1.02 ug/L 03/02/14 23:23 630-20-61.0 1
1,1,2,2-Tetrachloroethane 1.02 ug/L 03/02/14 23:23 79-34-51.0 1
Tetrachloroethene 1.02 ug/L 03/02/14 23:23 127-18-41.0 1
Tetrahydrofuran 10.02 ug/L 03/02/14 23:23 109-99-910.0 1
Toluene 1.02 ug/L 03/02/14 23:23 108-88-31.0 1
1,1,1-Trichloroethane 1.02 ug/L 03/02/14 23:23 71-55-61.0 1
1,1,2-Trichloroethane 1.02 ug/L 03/02/14 23:23 79-00-51.0 1
Trichloroethene 1.02 ug/L 03/02/14 23:23 79-01-61.0 1
Trichlorofluoromethane 1.02 ug/L 03/02/14 23:23 75-69-41.0 1
1,2,3-Trichloropropane 1.02 ug/L 03/02/14 23:23 96-18-41.0 1
1,2,3-Trimethylbenzene 1.02 ug/L 03/02/14 23:23 526-73-81.0 1
Vinyl acetate 2.02 ug/L 03/02/14 23:23 108-05-42.0 1
Vinyl chloride 1.02 ug/L 03/02/14 23:23 75-01-41.0 1
Xylene (Total)2.02 ug/L 03/02/14 23:23 1330-20-72.0 1
m&p-Xylene 2.02 ug/L 03/02/14 23:23 179601-23-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-1 Lab ID:92191404001 Collected:02/27/14 12:50 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
o-Xylene 1.02 ug/L 03/02/14 23:23 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %03/02/14 23:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %03/02/14 23:23 17060-07-070-130 1
Toluene-d8 (S)99 %03/02/14 23:23 2037-26-570-130 1
Sample:MW-2 Lab ID:92191404002 Collected:02/27/14 13:10 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Monitoring Well Data Analytical Method:
Collected By MPS 02/28/14 16:041
Collected Date 02/27/14 02/28/14 16:041
Collected Time 13:10 02/28/14 16:041
Field pH 6.1 Std. Units 02/28/14 16:040.10 1
Field Temperature 16.1 deg C 02/28/14 16:040.50 1
Static Water Level 37.57 feet 02/28/14 16:041
Field Specific Conductance 801 umhos/cm 02/28/14 16:041.0 1
Turbidity 3.70 NTU 02/28/14 16:041.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 5.02 ug/L 03/04/14 23:36 7440-36-002/28/14 09:055.0 1
Arsenic 10.02 ug/L 03/04/14 23:36 7440-38-202/28/14 09:0510.0 1
Barium 170 ug/L 03/04/14 23:36 7440-39-302/28/14 09:055.0 1
Beryllium 1.02 ug/L 03/04/14 23:36 7440-41-702/28/14 09:051.0 1
Cadmium 1.02 ug/L 03/04/14 23:36 7440-43-902/28/14 09:051.0 1
Chromium 5.02 ug/L 03/04/14 23:36 7440-47-302/28/14 09:055.0 1
Cobalt 52.6 ug/L 03/04/14 23:36 7440-48-402/28/14 09:055.0 1
Copper 5.02 ug/L 03/04/14 23:36 7440-50-802/28/14 09:055.0 1
Lead 5.02 ug/L 03/04/14 23:36 7439-92-102/28/14 09:055.0 1
Nickel 5.8 ug/L 03/04/14 23:36 7440-02-002/28/14 09:055.0 1
Selenium 10.02 ug/L 03/04/14 23:36 7782-49-202/28/14 09:0510.0 1
Silver 5.02 ug/L 03/04/14 23:36 7440-22-402/28/14 09:055.0 1
Thallium 5.42 ug/L 03/04/14 23:36 7440-28-002/28/14 09:055.4 1
Vanadium 5.02 ug/L 03/04/14 23:36 7440-62-202/28/14 09:055.0 1
Zinc 14.5 ug/L 03/04/14 23:36 7440-66-602/28/14 09:0510.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury 0.202 ug/L 03/06/14 20:03 7439-97-602/28/14 16:450.20 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 25.02 ug/L 03/02/14 23:38 67-64-125.0 1
Acrolein 10.02 ug/L 03/02/14 23:38 107-02-810.0 1
Acrylonitrile 10.02 ug/L 03/02/14 23:38 107-13-110.0 1
Allyl chloride 2.02 ug/L 03/02/14 23:38 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-2 Lab ID:92191404002 Collected:02/27/14 13:10 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Benzene 4.6 ug/L 03/02/14 23:38 71-43-21.0 1
Bromochloromethane 1.02 ug/L 03/02/14 23:38 74-97-51.0 1
Bromodichloromethane 1.02 ug/L 03/02/14 23:38 75-27-41.0 1
Bromoform 1.02 ug/L 03/02/14 23:38 75-25-21.0 1
Bromomethane 2.02 ug/L 03/02/14 23:38 74-83-92.0 1
2-Butanone (MEK)5.02 ug/L 03/02/14 23:38 78-93-35.0 1
Carbon disulfide 2.02 ug/L 03/02/14 23:38 75-15-02.0 1
Carbon tetrachloride 1.02 ug/L 03/02/14 23:38 56-23-51.0 1
Chlorobenzene 10.8 ug/L 03/02/14 23:38 108-90-71.0 1
Chloroethane 0.97J ug/L 03/02/14 23:38 75-00-31.0 1
Chloroform 1.02 ug/L 03/02/14 23:38 67-66-31.0 1
Chloromethane 1.02 ug/L 03/02/14 23:38 74-87-31.0 1
Cyclohexane 1.02 ug/L 03/02/14 23:38 110-82-71.0 1
1,2-Dibromo-3-chloropropane 5.02 ug/L 03/02/14 23:38 96-12-85.0 1
Dibromochloromethane 1.02 ug/L 03/02/14 23:38 124-48-11.0 1
1,2-Dibromoethane (EDB)1.02 ug/L 03/02/14 23:38 106-93-41.0 1
Dibromomethane 1.02 ug/L 03/02/14 23:38 74-95-31.0 1
1,2-Dichlorobenzene 3.0 ug/L 03/02/14 23:38 95-50-11.0 1
1,4-Dichlorobenzene 10.2 ug/L 03/02/14 23:38 106-46-71.0 1
trans-1,4-Dichloro-2-butene 1.02 ug/L 03/02/14 23:38 110-57-61.0 1
1,1-Dichloroethane 0.98J ug/L 03/02/14 23:38 75-34-31.0 1
1,2-Dichloroethane 1.02 ug/L 03/02/14 23:38 107-06-21.0 1
cis-1,2-Dichloroethene 33.6 ug/L 03/02/14 23:38 156-59-21.0 1
trans-1,2-Dichloroethene 1.02 ug/L 03/02/14 23:38 156-60-51.0 1
1,2-Dichloropropane 0.47J ug/L 03/02/14 23:38 78-87-51.0 1
1,3-Dichloropropane 1.02 ug/L 03/02/14 23:38 142-28-91.0 1
cis-1,3-Dichloropropene 1.02 ug/L 03/02/14 23:38 10061-01-51.0 1
trans-1,3-Dichloropropene 1.02 ug/L 03/02/14 23:38 10061-02-61.0 1
Diethyl ether (Ethyl ether)26.0 ug/L 03/02/14 23:38 60-29-71.0 1
Diisopropyl ether 1.3 ug/L 03/02/14 23:38 108-20-31.0 1
Ethyl acetate 20.02 ug/L 03/02/14 23:38 141-78-620.0 1
Ethylbenzene 0.43J ug/L 03/02/14 23:38 100-41-41.0 1
Ethyl methacrylate 1.02 ug/L 03/02/14 23:38 97-63-21.0 1
n-Hexane 1.02 ug/L 03/02/14 23:38 110-54-31.0 1
Iodomethane 5.02 ug/L 03/02/14 23:38 74-88-45.0 1
Isobutanol 1002 ug/L 03/02/14 23:38 78-83-11001
Methacrylonitrile 10.02 ug/L 03/02/14 23:38 126-98-710.0 1
Methyl acetate 10.02 ug/L 03/02/14 23:38 79-20-910.0 1
Methylcyclohexane 10.02 ug/L 03/02/14 23:38 108-87-210.0 1
Methylene Chloride 2.02 ug/L 03/02/14 23:38 75-09-22.0 1
Methyl methacrylate 2.02 ug/L 03/02/14 23:38 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)5.02 ug/L 03/02/14 23:38 108-10-15.0 1
Propionitrile 20.02 ug/L 03/02/14 23:38 107-12-020.0 1
Styrene 1.02 ug/L 03/02/14 23:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane 1.02 ug/L 03/02/14 23:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane 1.02 ug/L 03/02/14 23:38 79-34-51.0 1
Tetrachloroethene 1.02 ug/L 03/02/14 23:38 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-2 Lab ID:92191404002 Collected:02/27/14 13:10 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Tetrahydrofuran 123 ug/L 03/02/14 23:38 109-99-910.0 1
Toluene 0.46J ug/L 03/02/14 23:38 108-88-31.0 1
1,1,1-Trichloroethane 1.02 ug/L 03/02/14 23:38 71-55-61.0 1
1,1,2-Trichloroethane 1.02 ug/L 03/02/14 23:38 79-00-51.0 1
Trichloroethene 1.02 ug/L 03/02/14 23:38 79-01-61.0 1
Trichlorofluoromethane 1.02 ug/L 03/02/14 23:38 75-69-41.0 1
1,2,3-Trichloropropane 1.02 ug/L 03/02/14 23:38 96-18-41.0 1
1,2,3-Trimethylbenzene 1.02 ug/L 03/02/14 23:38 526-73-81.0 1
Vinyl acetate 2.02 ug/L 03/02/14 23:38 108-05-42.0 1
Vinyl chloride 2.2 ug/L 03/02/14 23:38 75-01-41.0 1
Xylene (Total)2.02 ug/L 03/02/14 23:38 1330-20-72.0 1
m&p-Xylene 1.1J ug/L 03/02/14 23:38 179601-23-12.0 1
o-Xylene 0.27J ug/L 03/02/14 23:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %03/02/14 23:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %03/02/14 23:38 17060-07-070-130 1
Toluene-d8 (S)99 %03/02/14 23:38 2037-26-570-130 1
Sample:MW-3 Lab ID:92191404003 Collected:02/27/14 12:25 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Monitoring Well Data Analytical Method:
Collected By MPS 02/28/14 16:051
Collected Date 02/27/14 02/28/14 16:051
Collected Time 12:25 02/28/14 16:051
Field pH 5.9 Std. Units 02/28/14 16:050.10 1
Field Temperature 14.2 deg C 02/28/14 16:050.50 1
Static Water Level 32.13 feet 02/28/14 16:051
Field Specific Conductance 525 umhos/cm 02/28/14 16:051.0 1
Turbidity 9.94 NTU 02/28/14 16:051.0 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 5.02 ug/L 03/04/14 23:40 7440-36-002/28/14 09:055.0 1
Arsenic 10.02 ug/L 03/04/14 23:40 7440-38-202/28/14 09:0510.0 1
Barium 2280 ug/L 03/04/14 23:40 7440-39-302/28/14 09:055.0 1
Beryllium 1.8 ug/L 03/04/14 23:40 7440-41-702/28/14 09:051.0 1
Cadmium 1.8 ug/L 03/04/14 23:40 7440-43-902/28/14 09:051.0 1
Chromium 5.02 ug/L 03/04/14 23:40 7440-47-302/28/14 09:055.0 1
Cobalt 220 ug/L 03/04/14 23:40 7440-48-402/28/14 09:055.0 1
Copper 5.02 ug/L 03/04/14 23:40 7440-50-802/28/14 09:055.0 1
Lead 5.02 ug/L 03/04/14 23:40 7439-92-102/28/14 09:055.0 1
Nickel 39.4 ug/L 03/04/14 23:40 7440-02-002/28/14 09:055.0 1
Selenium 10.02 ug/L 03/04/14 23:40 7782-49-202/28/14 09:0510.0 1
Silver 5.02 ug/L 03/04/14 23:40 7440-22-402/28/14 09:055.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
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Page 8 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-3 Lab ID:92191404003 Collected:02/27/14 12:25 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Thallium 5.42 ug/L 03/04/14 23:40 7440-28-002/28/14 09:055.4 1
Vanadium 5.02 ug/L 03/04/14 23:40 7440-62-202/28/14 09:055.0 1
Zinc 130 ug/L 03/04/14 23:40 7440-66-602/28/14 09:0510.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury 0.202 ug/L 03/06/14 20:06 7439-97-602/28/14 16:450.20 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 25.02 ug/L 03/02/14 23:54 67-64-125.0 1
Acrolein 10.02 ug/L 03/02/14 23:54 107-02-810.0 1
Acrylonitrile 10.02 ug/L 03/02/14 23:54 107-13-110.0 1
Allyl chloride 2.02 ug/L 03/02/14 23:54 107-05-12.0 1
Benzene 1.02 ug/L 03/02/14 23:54 71-43-21.0 1
Bromochloromethane 1.02 ug/L 03/02/14 23:54 74-97-51.0 1
Bromodichloromethane 1.02 ug/L 03/02/14 23:54 75-27-41.0 1
Bromoform 1.02 ug/L 03/02/14 23:54 75-25-21.0 1
Bromomethane 2.02 ug/L 03/02/14 23:54 74-83-92.0 1
2-Butanone (MEK)5.02 ug/L 03/02/14 23:54 78-93-35.0 1
Carbon disulfide 2.02 ug/L 03/02/14 23:54 75-15-02.0 1
Carbon tetrachloride 1.02 ug/L 03/02/14 23:54 56-23-51.0 1
Chlorobenzene 1.02 ug/L 03/02/14 23:54 108-90-71.0 1
Chloroethane 1.02 ug/L 03/02/14 23:54 75-00-31.0 1
Chloroform 1.02 ug/L 03/02/14 23:54 67-66-31.0 1
Chloromethane 1.02 ug/L 03/02/14 23:54 74-87-31.0 1
Cyclohexane 1.02 ug/L 03/02/14 23:54 110-82-71.0 1
1,2-Dibromo-3-chloropropane 5.02 ug/L 03/02/14 23:54 96-12-85.0 1
Dibromochloromethane 1.02 ug/L 03/02/14 23:54 124-48-11.0 1
1,2-Dibromoethane (EDB)1.02 ug/L 03/02/14 23:54 106-93-41.0 1
Dibromomethane 1.02 ug/L 03/02/14 23:54 74-95-31.0 1
1,2-Dichlorobenzene 1.02 ug/L 03/02/14 23:54 95-50-11.0 1
1,4-Dichlorobenzene 1.02 ug/L 03/02/14 23:54 106-46-71.0 1
trans-1,4-Dichloro-2-butene 1.02 ug/L 03/02/14 23:54 110-57-61.0 1
1,1-Dichloroethane 1.02 ug/L 03/02/14 23:54 75-34-31.0 1
1,2-Dichloroethane 1.02 ug/L 03/02/14 23:54 107-06-21.0 1
cis-1,2-Dichloroethene 1.02 ug/L 03/02/14 23:54 156-59-21.0 1
trans-1,2-Dichloroethene 1.02 ug/L 03/02/14 23:54 156-60-51.0 1
1,2-Dichloropropane 1.02 ug/L 03/02/14 23:54 78-87-51.0 1
1,3-Dichloropropane 1.02 ug/L 03/02/14 23:54 142-28-91.0 1
cis-1,3-Dichloropropene 1.02 ug/L 03/02/14 23:54 10061-01-51.0 1
trans-1,3-Dichloropropene 1.02 ug/L 03/02/14 23:54 10061-02-61.0 1
Diethyl ether (Ethyl ether)1.02 ug/L 03/02/14 23:54 60-29-71.0 1
Diisopropyl ether 1.02 ug/L 03/02/14 23:54 108-20-31.0 1
Ethyl acetate 20.02 ug/L 03/02/14 23:54 141-78-620.0 1
Ethylbenzene 1.02 ug/L 03/02/14 23:54 100-41-41.0 1
Ethyl methacrylate 1.02 ug/L 03/02/14 23:54 97-63-21.0 1
n-Hexane 1.02 ug/L 03/02/14 23:54 110-54-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-3 Lab ID:92191404003 Collected:02/27/14 12:25 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Iodomethane 5.02 ug/L 03/02/14 23:54 74-88-45.0 1
Isobutanol 1002 ug/L 03/02/14 23:54 78-83-11001
Methacrylonitrile 10.02 ug/L 03/02/14 23:54 126-98-710.0 1
Methyl acetate 10.02 ug/L 03/02/14 23:54 79-20-910.0 1
Methylcyclohexane 10.02 ug/L 03/02/14 23:54 108-87-210.0 1
Methylene Chloride 2.02 ug/L 03/02/14 23:54 75-09-22.0 1
Methyl methacrylate 2.02 ug/L 03/02/14 23:54 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)5.02 ug/L 03/02/14 23:54 108-10-15.0 1
Propionitrile 20.02 ug/L 03/02/14 23:54 107-12-020.0 1
Styrene 1.02 ug/L 03/02/14 23:54 100-42-51.0 1
1,1,1,2-Tetrachloroethane 1.02 ug/L 03/02/14 23:54 630-20-61.0 1
1,1,2,2-Tetrachloroethane 1.02 ug/L 03/02/14 23:54 79-34-51.0 1
Tetrachloroethene 1.02 ug/L 03/02/14 23:54 127-18-41.0 1
Tetrahydrofuran 10.02 ug/L 03/02/14 23:54 109-99-910.0 1
Toluene 1.02 ug/L 03/02/14 23:54 108-88-31.0 1
1,1,1-Trichloroethane 1.02 ug/L 03/02/14 23:54 71-55-61.0 1
1,1,2-Trichloroethane 1.02 ug/L 03/02/14 23:54 79-00-51.0 1
Trichloroethene 1.02 ug/L 03/02/14 23:54 79-01-61.0 1
Trichlorofluoromethane 0.71J ug/L 03/02/14 23:54 75-69-41.0 1
1,2,3-Trichloropropane 1.02 ug/L 03/02/14 23:54 96-18-41.0 1
1,2,3-Trimethylbenzene 1.02 ug/L 03/02/14 23:54 526-73-81.0 1
Vinyl acetate 2.02 ug/L 03/02/14 23:54 108-05-42.0 1
Vinyl chloride 1.02 ug/L 03/02/14 23:54 75-01-41.0 1
Xylene (Total)2.02 ug/L 03/02/14 23:54 1330-20-72.0 1
m&p-Xylene 2.02 ug/L 03/02/14 23:54 179601-23-12.0 1
o-Xylene 1.02 ug/L 03/02/14 23:54 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %03/02/14 23:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %03/02/14 23:54 17060-07-070-130 1
Toluene-d8 (S)99 %03/02/14 23:54 2037-26-570-130 1
Sample:MW-4 Lab ID:92191404004 Collected:02/27/14 12:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Monitoring Well Data Analytical Method:
Collected By MPS 02/28/14 16:051
Collected Date 02/27/14 02/28/14 16:051
Collected Time 12:00 02/28/14 16:051
Field pH 6.2 Std. Units 02/28/14 16:050.10 1
Field Temperature 12.0 deg C 02/28/14 16:050.50 1
Static Water Level 15.19 feet 02/28/14 16:051
Field Specific Conductance 78 umhos/cm 02/28/14 16:051.0 1
Turbidity >100 NTU 02/28/14 16:051.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-4 Lab ID:92191404004 Collected:02/27/14 12:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 5.02 ug/L 03/04/14 23:44 7440-36-002/28/14 09:055.0 1
Arsenic 5.8J ug/L 03/04/14 23:44 7440-38-202/28/14 09:0510.0 1
Barium 362 ug/L 03/04/14 23:44 7440-39-302/28/14 09:055.0 1
Beryllium 2.3 ug/L 03/04/14 23:44 7440-41-702/28/14 09:051.0 1
Cadmium 1.02 ug/L 03/04/14 23:44 7440-43-902/28/14 09:051.0 1
Chromium 9.8 ug/L 03/04/14 23:44 7440-47-302/28/14 09:055.0 1
Cobalt 33.3 ug/L 03/04/14 23:44 7440-48-402/28/14 09:055.0 1
Copper 13.0 ug/L 03/04/14 23:44 7440-50-802/28/14 09:055.0 1
Lead 15.4 ug/L 03/04/14 23:44 7439-92-102/28/14 09:055.0 1
Nickel 10.7 ug/L 03/04/14 23:44 7440-02-002/28/14 09:055.0 1
Selenium 10.02 ug/L 03/04/14 23:44 7782-49-202/28/14 09:0510.0 1
Silver 5.02 ug/L 03/04/14 23:44 7440-22-402/28/14 09:055.0 1
Thallium 5.42 ug/L 03/04/14 23:44 7440-28-002/28/14 09:055.4 1
Vanadium 109 ug/L 03/04/14 23:44 7440-62-202/28/14 09:055.0 1
Zinc 56.4 ug/L 03/04/14 23:44 7440-66-602/28/14 09:0510.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury 0.202 ug/L 03/06/14 20:14 7439-97-602/28/14 16:450.20 1
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 25.02 ug/L 03/03/14 00:10 67-64-125.0 1
Acrolein 10.02 ug/L 03/03/14 00:10 107-02-810.0 1
Acrylonitrile 10.02 ug/L 03/03/14 00:10 107-13-110.0 1
Allyl chloride 2.02 ug/L 03/03/14 00:10 107-05-12.0 1
Benzene 1.02 ug/L 03/03/14 00:10 71-43-21.0 1
Bromochloromethane 1.02 ug/L 03/03/14 00:10 74-97-51.0 1
Bromodichloromethane 1.02 ug/L 03/03/14 00:10 75-27-41.0 1
Bromoform 1.02 ug/L 03/03/14 00:10 75-25-21.0 1
Bromomethane 2.02 ug/L 03/03/14 00:10 74-83-92.0 1
2-Butanone (MEK)5.02 ug/L 03/03/14 00:10 78-93-35.0 1
Carbon disulfide 2.02 ug/L 03/03/14 00:10 75-15-02.0 1
Carbon tetrachloride 1.02 ug/L 03/03/14 00:10 56-23-51.0 1
Chlorobenzene 1.02 ug/L 03/03/14 00:10 108-90-71.0 1
Chloroethane 1.02 ug/L 03/03/14 00:10 75-00-31.0 1
Chloroform 1.02 ug/L 03/03/14 00:10 67-66-31.0 1
Chloromethane 1.02 ug/L 03/03/14 00:10 74-87-31.0 1
Cyclohexane 1.02 ug/L 03/03/14 00:10 110-82-71.0 1
1,2-Dibromo-3-chloropropane 5.02 ug/L 03/03/14 00:10 96-12-85.0 1
Dibromochloromethane 1.02 ug/L 03/03/14 00:10 124-48-11.0 1
1,2-Dibromoethane (EDB)1.02 ug/L 03/03/14 00:10 106-93-41.0 1
Dibromomethane 1.02 ug/L 03/03/14 00:10 74-95-31.0 1
1,2-Dichlorobenzene 1.02 ug/L 03/03/14 00:10 95-50-11.0 1
1,4-Dichlorobenzene 1.02 ug/L 03/03/14 00:10 106-46-71.0 1
trans-1,4-Dichloro-2-butene 1.02 ug/L 03/03/14 00:10 110-57-61.0 1
1,1-Dichloroethane 1.02 ug/L 03/03/14 00:10 75-34-31.0 1
1,2-Dichloroethane 1.02 ug/L 03/03/14 00:10 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:MW-4 Lab ID:92191404004 Collected:02/27/14 12:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
cis-1,2-Dichloroethene 1.02 ug/L 03/03/14 00:10 156-59-21.0 1
trans-1,2-Dichloroethene 1.02 ug/L 03/03/14 00:10 156-60-51.0 1
1,2-Dichloropropane 1.02 ug/L 03/03/14 00:10 78-87-51.0 1
1,3-Dichloropropane 1.02 ug/L 03/03/14 00:10 142-28-91.0 1
cis-1,3-Dichloropropene 1.02 ug/L 03/03/14 00:10 10061-01-51.0 1
trans-1,3-Dichloropropene 1.02 ug/L 03/03/14 00:10 10061-02-61.0 1
Diethyl ether (Ethyl ether)1.02 ug/L 03/03/14 00:10 60-29-71.0 1
Diisopropyl ether 1.02 ug/L 03/03/14 00:10 108-20-31.0 1
Ethyl acetate 20.02 ug/L 03/03/14 00:10 141-78-620.0 1
Ethylbenzene 1.02 ug/L 03/03/14 00:10 100-41-41.0 1
Ethyl methacrylate 1.02 ug/L 03/03/14 00:10 97-63-21.0 1
n-Hexane 1.02 ug/L 03/03/14 00:10 110-54-31.0 1
Iodomethane 5.02 ug/L 03/03/14 00:10 74-88-45.0 1
Isobutanol 1002 ug/L 03/03/14 00:10 78-83-11001
Methacrylonitrile 10.02 ug/L 03/03/14 00:10 126-98-710.0 1
Methyl acetate 10.02 ug/L 03/03/14 00:10 79-20-910.0 1
Methylcyclohexane 10.02 ug/L 03/03/14 00:10 108-87-210.0 1
Methylene Chloride 2.02 ug/L 03/03/14 00:10 75-09-22.0 1
Methyl methacrylate 2.02 ug/L 03/03/14 00:10 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)5.02 ug/L 03/03/14 00:10 108-10-15.0 1
Propionitrile 20.02 ug/L 03/03/14 00:10 107-12-020.0 1
Styrene 1.02 ug/L 03/03/14 00:10 100-42-51.0 1
1,1,1,2-Tetrachloroethane 1.02 ug/L 03/03/14 00:10 630-20-61.0 1
1,1,2,2-Tetrachloroethane 1.02 ug/L 03/03/14 00:10 79-34-51.0 1
Tetrachloroethene 1.02 ug/L 03/03/14 00:10 127-18-41.0 1
Tetrahydrofuran 10.02 ug/L 03/03/14 00:10 109-99-910.0 1
Toluene 1.02 ug/L 03/03/14 00:10 108-88-31.0 1
1,1,1-Trichloroethane 1.02 ug/L 03/03/14 00:10 71-55-61.0 1
1,1,2-Trichloroethane 1.02 ug/L 03/03/14 00:10 79-00-51.0 1
Trichloroethene 1.02 ug/L 03/03/14 00:10 79-01-61.0 1
Trichlorofluoromethane 1.02 ug/L 03/03/14 00:10 75-69-41.0 1
1,2,3-Trichloropropane 1.02 ug/L 03/03/14 00:10 96-18-41.0 1
1,2,3-Trimethylbenzene 1.02 ug/L 03/03/14 00:10 526-73-81.0 1
Vinyl acetate 2.02 ug/L 03/03/14 00:10 108-05-42.0 1
Vinyl chloride 1.02 ug/L 03/03/14 00:10 75-01-41.0 1
Xylene (Total)2.02 ug/L 03/03/14 00:10 1330-20-72.0 1
m&p-Xylene 2.02 ug/L 03/03/14 00:10 179601-23-12.0 1
o-Xylene 1.02 ug/L 03/03/14 00:10 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %03/03/14 00:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %03/03/14 00:10 17060-07-070-130 1
Toluene-d8 (S)100 %03/03/14 00:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:TVL BLK Lab ID:92191404005 Collected:02/27/14 00:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 25.02 ug/L 03/03/14 00:25 67-64-125.0 1
Acrolein 10.02 ug/L 03/03/14 00:25 107-02-810.0 1
Acrylonitrile 10.02 ug/L 03/03/14 00:25 107-13-110.0 1
Allyl chloride 2.02 ug/L 03/03/14 00:25 107-05-12.0 1
Benzene 1.02 ug/L 03/03/14 00:25 71-43-21.0 1
Bromochloromethane 1.02 ug/L 03/03/14 00:25 74-97-51.0 1
Bromodichloromethane 1.02 ug/L 03/03/14 00:25 75-27-41.0 1
Bromoform 1.02 ug/L 03/03/14 00:25 75-25-21.0 1
Bromomethane 2.02 ug/L 03/03/14 00:25 74-83-92.0 1
2-Butanone (MEK)5.02 ug/L 03/03/14 00:25 78-93-35.0 1
Carbon disulfide 2.02 ug/L 03/03/14 00:25 75-15-02.0 1
Carbon tetrachloride 1.02 ug/L 03/03/14 00:25 56-23-51.0 1
Chlorobenzene 1.02 ug/L 03/03/14 00:25 108-90-71.0 1
Chloroethane 1.02 ug/L 03/03/14 00:25 75-00-31.0 1
Chloroform 1.02 ug/L 03/03/14 00:25 67-66-31.0 1
Chloromethane 1.02 ug/L 03/03/14 00:25 74-87-31.0 1
Cyclohexane 1.02 ug/L 03/03/14 00:25 110-82-71.0 1
1,2-Dibromo-3-chloropropane 5.02 ug/L 03/03/14 00:25 96-12-85.0 1
Dibromochloromethane 1.02 ug/L 03/03/14 00:25 124-48-11.0 1
1,2-Dibromoethane (EDB)1.02 ug/L 03/03/14 00:25 106-93-41.0 1
Dibromomethane 1.02 ug/L 03/03/14 00:25 74-95-31.0 1
1,2-Dichlorobenzene 1.02 ug/L 03/03/14 00:25 95-50-11.0 1
1,4-Dichlorobenzene 1.02 ug/L 03/03/14 00:25 106-46-71.0 1
trans-1,4-Dichloro-2-butene 1.02 ug/L 03/03/14 00:25 110-57-61.0 1
1,1-Dichloroethane 1.02 ug/L 03/03/14 00:25 75-34-31.0 1
1,2-Dichloroethane 1.02 ug/L 03/03/14 00:25 107-06-21.0 1
cis-1,2-Dichloroethene 1.02 ug/L 03/03/14 00:25 156-59-21.0 1
trans-1,2-Dichloroethene 1.02 ug/L 03/03/14 00:25 156-60-51.0 1
1,2-Dichloropropane 1.02 ug/L 03/03/14 00:25 78-87-51.0 1
1,3-Dichloropropane 1.02 ug/L 03/03/14 00:25 142-28-91.0 1
cis-1,3-Dichloropropene 1.02 ug/L 03/03/14 00:25 10061-01-51.0 1
trans-1,3-Dichloropropene 1.02 ug/L 03/03/14 00:25 10061-02-61.0 1
Diethyl ether (Ethyl ether)1.02 ug/L 03/03/14 00:25 60-29-71.0 1
Diisopropyl ether 1.02 ug/L 03/03/14 00:25 108-20-31.0 1
Ethyl acetate 20.02 ug/L 03/03/14 00:25 141-78-620.0 1
Ethylbenzene 1.02 ug/L 03/03/14 00:25 100-41-41.0 1
Ethyl methacrylate 1.02 ug/L 03/03/14 00:25 97-63-21.0 1
n-Hexane 1.02 ug/L 03/03/14 00:25 110-54-31.0 1
Iodomethane 5.02 ug/L 03/03/14 00:25 74-88-45.0 1
Isobutanol 1002 ug/L 03/03/14 00:25 78-83-11001
Methacrylonitrile 10.02 ug/L 03/03/14 00:25 126-98-710.0 1
Methyl acetate 10.02 ug/L 03/03/14 00:25 79-20-910.0 1
Methylcyclohexane 10.02 ug/L 03/03/14 00:25 108-87-210.0 1
Methylene Chloride 2.02 ug/L 03/03/14 00:25 75-09-22.0 1
Methyl methacrylate 2.02 ug/L 03/03/14 00:25 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)5.02 ug/L 03/03/14 00:25 108-10-15.0 1
Propionitrile 20.02 ug/L 03/03/14 00:25 107-12-020.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:TVL BLK Lab ID:92191404005 Collected:02/27/14 00:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Styrene 1.02 ug/L 03/03/14 00:25 100-42-51.0 1
1,1,1,2-Tetrachloroethane 1.02 ug/L 03/03/14 00:25 630-20-61.0 1
1,1,2,2-Tetrachloroethane 1.02 ug/L 03/03/14 00:25 79-34-51.0 1
Tetrachloroethene 1.02 ug/L 03/03/14 00:25 127-18-41.0 1
Tetrahydrofuran 10.02 ug/L 03/03/14 00:25 109-99-910.0 1
Toluene 1.02 ug/L 03/03/14 00:25 108-88-31.0 1
1,1,1-Trichloroethane 1.02 ug/L 03/03/14 00:25 71-55-61.0 1
1,1,2-Trichloroethane 1.02 ug/L 03/03/14 00:25 79-00-51.0 1
Trichloroethene 1.02 ug/L 03/03/14 00:25 79-01-61.0 1
Trichlorofluoromethane 1.02 ug/L 03/03/14 00:25 75-69-41.0 1
1,2,3-Trichloropropane 1.02 ug/L 03/03/14 00:25 96-18-41.0 1
1,2,3-Trimethylbenzene 1.02 ug/L 03/03/14 00:25 526-73-81.0 1
Vinyl acetate 2.02 ug/L 03/03/14 00:25 108-05-42.0 1
Vinyl chloride 1.02 ug/L 03/03/14 00:25 75-01-41.0 1
Xylene (Total)2.02 ug/L 03/03/14 00:25 1330-20-72.0 1
m&p-Xylene 2.02 ug/L 03/03/14 00:25 179601-23-12.0 1
o-Xylene 1.02 ug/L 03/03/14 00:25 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %03/03/14 00:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %03/03/14 00:25 17060-07-070-130 1
Toluene-d8 (S)99 %03/03/14 00:25 2037-26-570-130 1
Sample:EQUIP BLK Lab ID:92191404006 Collected:02/27/14 00:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 5.02 ug/L 03/04/14 23:48 7440-36-002/28/14 09:055.0 1
Arsenic 10.02 ug/L 03/04/14 23:48 7440-38-202/28/14 09:0510.0 1
Barium 5.02 ug/L 03/04/14 23:48 7440-39-302/28/14 09:055.0 1
Beryllium 1.02 ug/L 03/04/14 23:48 7440-41-702/28/14 09:051.0 1
Cadmium 1.02 ug/L 03/04/14 23:48 7440-43-902/28/14 09:051.0 1
Chromium 5.02 ug/L 03/04/14 23:48 7440-47-302/28/14 09:055.0 1
Cobalt 5.02 ug/L 03/04/14 23:48 7440-48-402/28/14 09:055.0 1
Copper 5.02 ug/L 03/04/14 23:48 7440-50-802/28/14 09:055.0 1
Lead 5.02 ug/L 03/04/14 23:48 7439-92-102/28/14 09:055.0 1
Nickel 5.02 ug/L 03/04/14 23:48 7440-02-002/28/14 09:055.0 1
Selenium 10.02 ug/L 03/04/14 23:48 7782-49-202/28/14 09:0510.0 1
Silver 5.02 ug/L 03/04/14 23:48 7440-22-402/28/14 09:055.0 1
Thallium 5.42 ug/L 03/04/14 23:48 7440-28-002/28/14 09:055.4 1
Vanadium 5.02 ug/L 03/04/14 23:48 7440-62-202/28/14 09:055.0 1
Zinc 10.02 ug/L 03/04/14 23:48 7440-66-602/28/14 09:0510.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury 0.202 ug/L 03/06/14 20:17 7439-97-602/28/14 16:450.20 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 14 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:EQUIP BLK Lab ID:92191404006 Collected:02/27/14 00:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 25.02 ug/L 03/03/14 00:41 67-64-125.0 1
Acrolein 10.02 ug/L 03/03/14 00:41 107-02-810.0 1
Acrylonitrile 10.02 ug/L 03/03/14 00:41 107-13-110.0 1
Allyl chloride 2.02 ug/L 03/03/14 00:41 107-05-12.0 1
Benzene 1.02 ug/L 03/03/14 00:41 71-43-21.0 1
Bromochloromethane 1.02 ug/L 03/03/14 00:41 74-97-51.0 1
Bromodichloromethane 1.02 ug/L 03/03/14 00:41 75-27-41.0 1
Bromoform 1.02 ug/L 03/03/14 00:41 75-25-21.0 1
Bromomethane 2.02 ug/L 03/03/14 00:41 74-83-92.0 1
2-Butanone (MEK)5.02 ug/L 03/03/14 00:41 78-93-35.0 1
Carbon disulfide 2.02 ug/L 03/03/14 00:41 75-15-02.0 1
Carbon tetrachloride 1.02 ug/L 03/03/14 00:41 56-23-51.0 1
Chlorobenzene 1.02 ug/L 03/03/14 00:41 108-90-71.0 1
Chloroethane 1.02 ug/L 03/03/14 00:41 75-00-31.0 1
Chloroform 1.02 ug/L 03/03/14 00:41 67-66-31.0 1
Chloromethane 1.02 ug/L 03/03/14 00:41 74-87-31.0 1
Cyclohexane 1.02 ug/L 03/03/14 00:41 110-82-71.0 1
1,2-Dibromo-3-chloropropane 5.02 ug/L 03/03/14 00:41 96-12-85.0 1
Dibromochloromethane 1.02 ug/L 03/03/14 00:41 124-48-11.0 1
1,2-Dibromoethane (EDB)1.02 ug/L 03/03/14 00:41 106-93-41.0 1
Dibromomethane 1.02 ug/L 03/03/14 00:41 74-95-31.0 1
1,2-Dichlorobenzene 1.02 ug/L 03/03/14 00:41 95-50-11.0 1
1,4-Dichlorobenzene 1.02 ug/L 03/03/14 00:41 106-46-71.0 1
trans-1,4-Dichloro-2-butene 1.02 ug/L 03/03/14 00:41 110-57-61.0 1
1,1-Dichloroethane 1.02 ug/L 03/03/14 00:41 75-34-31.0 1
1,2-Dichloroethane 1.02 ug/L 03/03/14 00:41 107-06-21.0 1
cis-1,2-Dichloroethene 1.02 ug/L 03/03/14 00:41 156-59-21.0 1
trans-1,2-Dichloroethene 1.02 ug/L 03/03/14 00:41 156-60-51.0 1
1,2-Dichloropropane 1.02 ug/L 03/03/14 00:41 78-87-51.0 1
1,3-Dichloropropane 1.02 ug/L 03/03/14 00:41 142-28-91.0 1
cis-1,3-Dichloropropene 1.02 ug/L 03/03/14 00:41 10061-01-51.0 1
trans-1,3-Dichloropropene 1.02 ug/L 03/03/14 00:41 10061-02-61.0 1
Diethyl ether (Ethyl ether)1.02 ug/L 03/03/14 00:41 60-29-71.0 1
Diisopropyl ether 1.02 ug/L 03/03/14 00:41 108-20-31.0 1
Ethyl acetate 20.02 ug/L 03/03/14 00:41 141-78-620.0 1
Ethylbenzene 1.02 ug/L 03/03/14 00:41 100-41-41.0 1
Ethyl methacrylate 1.02 ug/L 03/03/14 00:41 97-63-21.0 1
n-Hexane 1.02 ug/L 03/03/14 00:41 110-54-31.0 1
Iodomethane 5.02 ug/L 03/03/14 00:41 74-88-45.0 1
Isobutanol 1002 ug/L 03/03/14 00:41 78-83-11001
Methacrylonitrile 10.02 ug/L 03/03/14 00:41 126-98-710.0 1
Methyl acetate 10.02 ug/L 03/03/14 00:41 79-20-910.0 1
Methylcyclohexane 10.02 ug/L 03/03/14 00:41 108-87-210.0 1
Methylene Chloride 2.02 ug/L 03/03/14 00:41 75-09-22.0 1
Methyl methacrylate 2.02 ug/L 03/03/14 00:41 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)5.02 ug/L 03/03/14 00:41 108-10-15.0 1
Propionitrile 20.02 ug/L 03/03/14 00:41 107-12-020.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 15 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191404
LANDFILL MW
Sample:EQUIP BLK Lab ID:92191404006 Collected:02/27/14 00:00 Received:02/27/14 16:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Styrene 1.02 ug/L 03/03/14 00:41 100-42-51.0 1
1,1,1,2-Tetrachloroethane 1.02 ug/L 03/03/14 00:41 630-20-61.0 1
1,1,2,2-Tetrachloroethane 1.02 ug/L 03/03/14 00:41 79-34-51.0 1
Tetrachloroethene 1.02 ug/L 03/03/14 00:41 127-18-41.0 1
Tetrahydrofuran 10.02 ug/L 03/03/14 00:41 109-99-910.0 1
Toluene 1.02 ug/L 03/03/14 00:41 108-88-31.0 1
1,1,1-Trichloroethane 1.02 ug/L 03/03/14 00:41 71-55-61.0 1
1,1,2-Trichloroethane 1.02 ug/L 03/03/14 00:41 79-00-51.0 1
Trichloroethene 1.02 ug/L 03/03/14 00:41 79-01-61.0 1
Trichlorofluoromethane 1.02 ug/L 03/03/14 00:41 75-69-41.0 1
1,2,3-Trichloropropane 1.02 ug/L 03/03/14 00:41 96-18-41.0 1
1,2,3-Trimethylbenzene 1.02 ug/L 03/03/14 00:41 526-73-81.0 1
Vinyl acetate 2.02 ug/L 03/03/14 00:41 108-05-42.0 1
Vinyl chloride 1.02 ug/L 03/03/14 00:41 75-01-41.0 1
Xylene (Total)2.02 ug/L 03/03/14 00:41 1330-20-72.0 1
m&p-Xylene 2.02 ug/L 03/03/14 00:41 179601-23-12.0 1
o-Xylene 1.02 ug/L 03/03/14 00:41 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %03/03/14 00:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %03/03/14 00:41 17060-07-070-130 1
Toluene-d8 (S)99 %03/03/14 00:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 16 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6249
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148154
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404006
Matrix:Water
Analyzed
Mercury ug/L 0.202 0.20 03/06/14 19:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148155LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148156MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191338001
1148157
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 105 75-125101 42.5<0.10 2.6 2.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 17 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15332
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147590
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404006
Matrix:Water
Analyzed
Antimony ug/L 5.02 5.0 03/04/14 22:42
Arsenic ug/L 10.02 10.0 03/04/14 22:42
Barium ug/L 5.02 5.0 03/04/14 22:42
Beryllium ug/L 1.02 1.0 03/04/14 22:42
Cadmium ug/L 1.02 1.0 03/04/14 22:42
Chromium ug/L 5.02 5.0 03/04/14 22:42
Cobalt ug/L 5.02 5.0 03/04/14 22:42
Copper ug/L 5.02 5.0 03/04/14 22:42
Lead ug/L 5.02 5.0 03/04/14 22:42
Nickel ug/L 5.02 5.0 03/04/14 22:42
Selenium ug/L 10.02 10.0 03/04/14 22:42
Silver ug/L 5.02 5.0 03/04/14 22:42
Thallium ug/L 5.42 5.4 03/04/14 22:42
Vanadium ug/L 5.02 5.0 03/04/14 22:42
Zinc ug/L 10.02 10.0 03/04/14 22:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147591LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 484500 97 80-120
Arsenic ug/L 462500 92 80-120
Barium ug/L 477500 95 80-120
Beryllium ug/L 476500 95 80-120
Cadmium ug/L 479500 96 80-120
Chromium ug/L 481500 96 80-120
Cobalt ug/L 480500 96 80-120
Copper ug/L 474500 95 80-120
Lead ug/L 479500 96 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 470500 94 80-120
Silver ug/L 240250 96 80-120
Thallium ug/L 461500 92 80-120
Vanadium ug/L 484500 97 80-120
Zinc ug/L 469500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147592MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191398001
1147593
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 89 75-12588 1500ND447442
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 18 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147592MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191398001
1147593
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 95 75-12594 1500ND476471
Barium ug/L 500 95 75-12593 150063.9J 538 530
Beryllium ug/L 500 96 75-12595 1500ND479473
Cadmium ug/L 500 94 75-12593 1500ND472467
Chromium ug/L 500 98 75-12597 150013.5 503 498
Cobalt ug/L 500 95 75-12593 150010.1 484 477
Copper ug/L 500 98 75-12597 150011.2 502 495
Lead ug/L 500 91 75-12590 1500ND458452
Nickel ug/L 500 94 75-12594 15007.3J 479 476
Selenium ug/L 500 95 75-12592 2500ND475464
Silver ug/L 250 96 75-12595 1250ND241238
Thallium ug/L 500 89 75-12588 1500ND443439
Vanadium ug/L 500 98 75-12596 250029.2 519 511
Zinc ug/L 500 95 75-12594 150015.0 489 484
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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[phone]
Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25955
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404005, 92191404006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148868
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404005, 92191404006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L 1.02 1.0 03/02/14 22:20
1,1,1-Trichloroethane ug/L 1.02 1.0 03/02/14 22:20
1,1,2,2-Tetrachloroethane ug/L 1.02 1.0 03/02/14 22:20
1,1,2-Trichloroethane ug/L 1.02 1.0 03/02/14 22:20
1,1-Dichloroethane ug/L 1.02 1.0 03/02/14 22:20
1,2,3-Trichloropropane ug/L 1.02 1.0 03/02/14 22:20
1,2,3-Trimethylbenzene ug/L 1.02 1.0 03/02/14 22:20
1,2-Dibromo-3-chloropropane ug/L 5.02 5.0 03/02/14 22:20
1,2-Dibromoethane (EDB)ug/L 1.02 1.0 03/02/14 22:20
1,2-Dichlorobenzene ug/L 1.02 1.0 03/02/14 22:20
1,2-Dichloroethane ug/L 1.02 1.0 03/02/14 22:20
1,2-Dichloropropane ug/L 1.02 1.0 03/02/14 22:20
1,3-Dichloropropane ug/L 1.02 1.0 03/02/14 22:20
1,4-Dichlorobenzene ug/L 1.02 1.0 03/02/14 22:20
2-Butanone (MEK)ug/L 5.02 5.0 03/02/14 22:20
4-Methyl-2-pentanone (MIBK)ug/L 5.02 5.0 03/02/14 22:20
Acetone ug/L 25.02 25.0 03/02/14 22:20
Acrolein ug/L 10.02 10.0 03/02/14 22:20
Acrylonitrile ug/L 10.02 10.0 03/02/14 22:20
Allyl chloride ug/L 2.02 2.0 03/02/14 22:20
Benzene ug/L 1.02 1.0 03/02/14 22:20
Bromochloromethane ug/L 1.02 1.0 03/02/14 22:20
Bromodichloromethane ug/L 1.02 1.0 03/02/14 22:20
Bromoform ug/L 1.02 1.0 03/02/14 22:20
Bromomethane ug/L 2.02 2.0 03/02/14 22:20
Carbon disulfide ug/L 2.02 2.0 03/02/14 22:20
Carbon tetrachloride ug/L 1.02 1.0 03/02/14 22:20
Chlorobenzene ug/L 1.02 1.0 03/02/14 22:20
Chloroethane ug/L 1.02 1.0 03/02/14 22:20
Chloroform ug/L 1.02 1.0 03/02/14 22:20
Chloromethane ug/L 1.02 1.0 03/02/14 22:20
cis-1,2-Dichloroethene ug/L 1.02 1.0 03/02/14 22:20
cis-1,3-Dichloropropene ug/L 1.02 1.0 03/02/14 22:20
Cyclohexane ug/L 1.02 1.0 03/02/14 22:20
Dibromochloromethane ug/L 1.02 1.0 03/02/14 22:20
Dibromomethane ug/L 1.02 1.0 03/02/14 22:20
Diethyl ether (Ethyl ether)ug/L 1.02 1.0 03/02/14 22:20
Diisopropyl ether ug/L 1.02 1.0 03/02/14 22:20
Ethyl acetate ug/L 20.02 20.0 03/02/14 22:20
Ethyl methacrylate ug/L 1.02 1.0 03/02/14 22:20
Ethylbenzene ug/L 1.02 1.0 03/02/14 22:20
Iodomethane ug/L 5.02 5.0 03/02/14 22:20
Isobutanol ug/L 1002 100 03/02/14 22:20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 20 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148868
Associated Lab Samples:92191404001, 92191404002, 92191404003, 92191404004, 92191404005, 92191404006
Matrix:Water
Analyzed
m&p-Xylene ug/L 2.02 2.0 03/02/14 22:20
Methacrylonitrile ug/L 10.02 10.0 03/02/14 22:20
Methyl acetate ug/L 10.02 10.0 03/02/14 22:20
Methyl methacrylate ug/L 2.02 2.0 03/02/14 22:20
Methylcyclohexane ug/L 10.02 10.0 03/02/14 22:20
Methylene Chloride ug/L 2.02 2.0 03/02/14 22:20
n-Hexane ug/L 1.02 1.0 03/02/14 22:20
o-Xylene ug/L 1.02 1.0 03/02/14 22:20
Propionitrile ug/L 20.02 20.0 03/02/14 22:20
Styrene ug/L 1.02 1.0 03/02/14 22:20
Tetrachloroethene ug/L 1.02 1.0 03/02/14 22:20
Tetrahydrofuran ug/L 10.02 10.0 03/02/14 22:20
Toluene ug/L 1.02 1.0 03/02/14 22:20
trans-1,2-Dichloroethene ug/L 1.02 1.0 03/02/14 22:20
trans-1,3-Dichloropropene ug/L 1.02 1.0 03/02/14 22:20
trans-1,4-Dichloro-2-butene ug/L 1.02 1.0 03/02/14 22:20
Trichloroethene ug/L 1.02 1.0 03/02/14 22:20
Trichlorofluoromethane ug/L 1.02 1.0 03/02/14 22:20
Vinyl acetate ug/L 2.02 2.0 03/02/14 22:20
Vinyl chloride ug/L 1.02 1.0 03/02/14 22:20
Xylene (Total)ug/L 2.02 2.0 03/02/14 22:20
1,2-Dichloroethane-d4 (S)%98 70-130 03/02/14 22:20
4-Bromofluorobenzene (S)%100 70-130 03/02/14 22:20
Toluene-d8 (S)%99 70-130 03/02/14 22:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148869LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.050 104 70-130
1,1,1-Trichloroethane ug/L 50.750 101 70-130
1,1,2,2-Tetrachloroethane ug/L 51.450 103 70-130
1,1,2-Trichloroethane ug/L 53.250 106 70-130
1,1-Dichloroethane ug/L 49.750 99 70-130
1,2,3-Trichloropropane ug/L 52.550 105 70-130
1,2,3-Trimethylbenzene ug/L 50.950 102 70-130
1,2-Dibromo-3-chloropropane ug/L 49.850 100 70-130
1,2-Dibromoethane (EDB)ug/L 52.550 105 70-130
1,2-Dichlorobenzene ug/L 52.250 104 70-130
1,2-Dichloroethane ug/L 48.750 97 70-130
1,2-Dichloropropane ug/L 52.350 105 70-130
1,3-Dichloropropane ug/L 52.650 105 70-130
1,4-Dichlorobenzene ug/L 51.750 103 70-130
2-Butanone (MEK)ug/L 103100 103 70-145
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-140
Acetone ug/L 91.1100 91 50-175
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
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Page 21 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148869LABORATORY CONTROL SAMPLE:
LCSSpike
Acrolein ug/L 235250 94 70-130
Acrylonitrile ug/L 250250 100 70-143
Allyl chloride ug/L 47.250 94 70-130
Benzene ug/L 52.350 105 70-130
Bromochloromethane ug/L 51.150 102 70-130
Bromodichloromethane ug/L 50.850 102 70-130
Bromoform ug/L 54.950 110 70-130
Bromomethane ug/L 46.050 92 54-130
Carbon disulfide ug/L 50.550 101 70-131
Carbon tetrachloride ug/L 51.750 103 70-132
Chlorobenzene ug/L 51.250 102 70-130
Chloroethane ug/L 47.550 95 64-134
Chloroform ug/L 49.850 100 70-130
Chloromethane ug/L 44.150 88 64-130
cis-1,2-Dichloroethene ug/L 48.850 98 70-131
cis-1,3-Dichloropropene ug/L 51.450 103 70-130
Cyclohexane ug/L 50.750 101 70-130
Dibromochloromethane ug/L 53.150 106 70-130
Dibromomethane ug/L 52.650 105 70-131
Diethyl ether (Ethyl ether)ug/L 52.050 104 70-130
Diisopropyl ether ug/L 50.850 102 70-130
Ethyl acetate ug/L 101100 101 70-130
Ethyl methacrylate ug/L 50.350 101 70-130
Ethylbenzene ug/L 50.550 101 70-130
Iodomethane ug/L 92.4100 92 49-180
Isobutanol ug/L 11001000 110 70-130
m&p-Xylene ug/L 105100 105 70-130
Methacrylonitrile ug/L 505500 101 70-130
Methyl acetate ug/L 46.450 93 70-130
Methyl methacrylate ug/L 52.850 106 70-130
Methylcyclohexane ug/L 52.350 105 70-130
Methylene Chloride ug/L 46.650 93 63-130
n-Hexane ug/L 49.750 99 70-130
o-Xylene ug/L 52.450 105 70-130
Propionitrile ug/L 517500 103 70-130
Styrene ug/L 54.150 108 70-130
Tetrachloroethene ug/L 52.050 104 70-130
Tetrahydrofuran ug/L 528500 106 70-130
Toluene ug/L 51.450 103 70-130
trans-1,2-Dichloroethene ug/L 48.550 97 70-130
trans-1,3-Dichloropropene ug/L 51.850 104 70-132
trans-1,4-Dichloro-2-butene ug/L 46.750 93 70-141
Trichloroethene ug/L 51.450 103 70-130
Trichlorofluoromethane ug/L 48.850 98 62-133
Vinyl acetate ug/L 97.9100 98 66-157
Vinyl chloride ug/L 51.850 104 69-130
Xylene (Total)ug/L 158150 105 70-130
1,2-Dichloroethane-d4 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191404
LANDFILL MW
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148869LABORATORY CONTROL SAMPLE:
LCSSpike
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 27
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92191404
LANDFILL MW
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 27
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92191404
LANDFILL MW
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92191404001 FLD/MW-1
92191404002 FLD/MW-2
92191404003 FLD/MW-3
92191404004 FLD/MW-4
92191404001 MPRP/15332 ICP/13911MW-1 EPA 3010 EPA 6010
92191404002 MPRP/15332 ICP/13911MW-2 EPA 3010 EPA 6010
92191404003 MPRP/15332 ICP/13911MW-3 EPA 3010 EPA 6010
92191404004 MPRP/15332 ICP/13911MW-4 EPA 3010 EPA 6010
92191404006 MPRP/15332 ICP/13911EQUIP BLK EPA 3010 EPA 6010
92191404001 MERP/6249 MERC/6033MW-1 EPA 7470 EPA 7470
92191404002 MERP/6249 MERC/6033MW-2 EPA 7470 EPA 7470
92191404003 MERP/6249 MERC/6033MW-3 EPA 7470 EPA 7470
92191404004 MERP/6249 MERC/6033MW-4 EPA 7470 EPA 7470
92191404006 MERP/6249 MERC/6033EQUIP BLK EPA 7470 EPA 7470
92191404001 MSV/25955MW-1 EPA 8260
92191404002 MSV/25955MW-2 EPA 8260
92191404003 MSV/25955MW-3 EPA 8260
92191404004 MSV/25955MW-4 EPA 8260
92191404005 MSV/25955TVL BLK EPA 8260
92191404006 MSV/25955EQUIP BLK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2014 08:31 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 27
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