SW_F_8602-MSWLF-1983_10-01-2014_RM_GW.pdf

Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
May 2014
SWS Facility Permit Number: 86-02
Semi-Annual Water Quality Monitoring Report
Prepared for
Submitted: October 1, 2014
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G14032.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

UIC Permit Number:WI0400176

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Groundwater Samples Page 3
Groundwater Characterization Page 3
Findings Page 3
Closing Page 4
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards Figure 2
Total Cumulative VOC Concentrations Pre/Post Injection Comparison Figure 3
Bromide Tracer Concentrations Time Series Graph and Table Figure 4
TABLES
Sampling and Analysis Summary Table 1
Detections that Attain or are Above SWSL or 2L Standard Table 2
Field Parameter Data Summary Table 3
Hydrologic Properties at Monitoring Wells Table 4
MNA Parameter Data Summary Table 5
APPENDIX
Laboratory Analysis Report and Chains of Custody Appendix A
October 1, 2014
Mr. Thomas Slusser, P.G.
Aquifer Protection Section-Underground Injection Control Program
Division of Water Quality
North Carolina Department of Environment and Natural Resources
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Semi-Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 27030
SWS Permit No. 86-02
UIC Permit No. WI0400176
MESCO Project No. G14032.0
Event Date(s) May 27-29, 2014
Dear Mr. Slusser:
Introduction
Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to
present this brief Semi-Annual Water Quality Report that details a water quality monitoring event performed at the
Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02)
on May 27-29, 2014. The Injection Well Permit Application and Well Permit No. WI0400176 (4/15/13) requires
that Surry County provide this report to the Underground Injection Control (UIC) program on a semi-annual basis.
Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to
persist in levels above 2L Standards at seven wells that monitor the uppermost aquifer downgradient of five
injection points. However, total VOC concentrations have decreased at all locations compared to their respective
baseline averages established during the five events prior to the first injection event performed in November 2011.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill
the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January 1, 1999.
The MSWLF was closed with a low permeability cohesive soil cap per the Transition Plan. The top portion of the
southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed
with another cohesive soil cap in accordance with the Closure Plan.
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (5/6/11) with the goal to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below 2L Standards.
On November 2-3, 2011 an EOS-water emulsion with sodium bromide tracer was injected into three wells ( IW-2,
IW-3 and IW-5). Injection was attempted into IW-1 during this same event but due to the tightness of the formation
an insignificant amount (< 3 gallons of slurry) entered the uppermost aquifer. For all intents and purposes IW-1
injection did not occur nor ever will be able to in the future. Monitoring of wells downgradient of this location will
continue to be monitored semi-annually as required by the NC Solid Waste Section (SWS). Any observed changes
in geochemistry downgradient of IW-1 is not attributed to the unsuccessful injection event. Details of the premier
injection event are provided in the Injection Event Record dated November 4, 2010.

On October 24-25, 2012 similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 in
fulfillment of Phase 2 of Corrective Action. Details of the second injection events is provided in the Injection Event
Record submitted January 10, 2013.
The UIC Injection Well Permit was renewed on April 15, 2013 which reduced monitoring frequency from
quarterly to semi-annually and the prescribed constituents listed in the approved application was also reduced
and vague.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. This is the seventh post-injection water quality monitoring event with previous events performed on
February 9, 2012, May 30, 2012, August 20, 2012, October 23, 2012, May 29, 2013, October 29,2014. Previous
event reports have already been submitted to the UIC and SWS.
This report contains sampling procedures, field and laboratory results, groundwater characterization, and findings.
A potentiometric map of the uppermost aquifer, time-series graphs of select constituents, a table of detections
compared to Standards, field data results table, groundwater flow directions/rates table and laboratory analytical
data results are also enclosed.
Sampling Procedure
MESCO personnel performed this sampling event targeting the parameters outlined in the Water Quality Sampling
and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10,
2013. Monitored locations were consistent with the renewed Well Permit (4/15/13).
Groundwater samples were collected and analyzed from fourteen wells which includes MW-3R, MW-7, MW-9,
MW-12S, MW-13, MW-14, MW-16, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23 and upgradient
background well MW-1. Additionally, water within all six injection wells were measured and visually evaluated in
an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the
viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2.
Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling
and Analysis Plan which was submitted with the Corrective Action Plan (CAP) revision 2 dated December 10, 2010.
The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low-flow pumping methodology or bailing was utilized to adequately purge the wells a minimum of three well
volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed
into laboratory-prepared, pre-preserved containers via a new disposable polyethylene bailer. Samples were kept on
ice, and transported within hold-times to a NC-certified laboratory under proper chain of custody (C-O-C) protocols.
Field Parameter Data
Field parameters recorded included depth to water, pH, specific conductance, temperature, dissolved oxygen (DO),
oxidation reduction potential (ORP), total dissolved solids (TDS) and turbidity. A summary of the field parameter
data since injection is presented in Table 3.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory
analysis. Groundwater samples were analyzed for all the parameters requested by the SWS which includes
constituents listed in Appendix I of 40 CFR 258 plus select monitored natural attenuation parameters (MNA) at
select locations. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed select samples for the
bromide tracer. A sampling and analysis table summarizing the locations, target parameters and laboratory methods
is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (MDL),
which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-O-Cs
are presented in Appendix A.
2
Groundwater Samples
The wells with Appendix I VOCs detected in concentrations in exceedance of their respective 2L Standard during
this event include MW-9 (1,4-dichlorobenzene, benzene, vinyl chloride), MW-13 (1,2-DCA), MW-14 (PCE), MW-
15 (PCE, TCE, 1,2-DCA, 1,1-DCA, benzene, vinyl chloride), MW-16 (1,4-dichlorobenzene, 1,2-DCP, 1,2-DCA,
benzene, vinyl chloride), MW-21 (1,2-DCA, 1,1-DCA) and MW-22 (1,2-DCA). Although not regulatory applicable
the only constituents detected above the EPA established maximum contaminant levels (MCLs) or primary
“Drinking Water Standards” were vinyl chloride (MW-9, MW-16) and 1,1-dichloroethene (MW-15). Table 2
summarizes constituents detected in groundwater samples in concentrations above the current SWSL or North
Carolina Groundwater Standards (2L). MNA data presented in Table 5 continues to indicate that favorable
geochemical conditions exist for continued natural attenuation.
A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard
during this event is presented on Figure 2.
Groundwater Characterization
A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the May
2014 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's
equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water-bearing zones
in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable
but consistent compared to historical observations.
Findings
The laboratory results indicate that dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue
to be detected in groundwater samples collected from seven wells. All VOCs detected in concentrations above the
2L Standard during this event remain within their own respective historically identified range. Total cumulative
VOC concentrations were lower during this event compared to their own respective five event averages established
prior to injection in all locations as shown on Figure 3.
Evaluation of the injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) continues to indicate that a considerable
amount of residual organic substrate remain in each of these wells rendering them unsuitable for representative
water quality analysis. The viscosity of the water in the injection wells precludes sample collection as either a
bailer would not descend or the check valve failed.
In an attempt to track migration of injectants bromide was targeted at MW-3R, MW-13, MW-14, MW-15, MW-16,
MW-21 and background well MW-1. MW-16, located 86 feet downgradient of IW-3, is the only location
exhibiting tracer levels which may potentially indicate injectant communication. Based on the average linear
velocity rates of IW-3 and MW-16 reported since injection the injectant was expected to reach MW-16 in May 2012.
Bromide concentrations exhibited a consistent increasing trend in MW-16 the first year following injection then has
decreased the last year (Figure 4). Calculations performed following injection indicates that reported levels of
bromide injected was insufficient to provide clear evidence of migration within the uppermost aquifer.
3
Closing
Water quality monitoring is planned to continue with the next event scheduled for October 2014. No further
injections are planned at this time but if they do Permit conditions will be met including giving the UIC advance
notice prior to installation or injection of any additional well(s).
If you have any questions or comments regarding this report, please contact us at [phone] or by email at
[e-mail].
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
Jonathan Pfohl
Environmental Specialist
Enclosures
cc: Mr. Dennis Bledsoe
Surry County
Ms. Jaclynne Drummond (Electronic Copy Only)
SWS-Compliance Branch
Ms. Shuying Wang (Electronic Copy Only)
UIC
4
Figures
Topographic Map with Site Location
FIGURE 1
Surry County Closed Unlined C&D and Closed Unlined MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat:36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48 Closed Unlined C&D Landfill
Closed Unlined Sanitary Landfill
01 1 MILE
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 3
October 22, 2009 – May 28, 2014
Well ID
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 20.50 -48.62 -70 Downward
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 81.50 -43.44 -35 Downward
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 0.00 -14.32 -100 No Trend
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 27.90 -17.24 -38 Downward
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100 No Trend
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15 96.13 63.89 55.00 78.10 64.06 71.44 58.99 -12.45 -17 No Trend
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
Oct
2009
(ug/L)
May
2010
(ug/L)
Oct
2010
(ug/L)
May
2011
(ug/L)
Oct
2011
(ug/L)
Average of
first Five
Corrective
Action
Events
(ug/L)
May
2014
(ug/L)
Difference
(ug/L)
Difference
(%)
Statistical Trend*
Between Oct
2009-May 2014
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
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Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 4
Bromide Tracer Concentrations Time Series Graph and Table
February 9, 2012 – May 28, 2014
Date MW-16
2/9/2012 0.0380 (j)
5/30/2012 0.1300 (j)
8/20/2012 0.2600 (j)
10/23/2012 0.2800 (j)
5/30/2013 0.1400 (j)
10/31/2013 0.1100 (j)
5/28/2014 0.2200 (j)
(j) = The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
* = May 25, 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 ft/yr) since injection occurred.
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Bromide Tracer Levels in MW-16
Located 87 feet Downgradient of IW-3 which was Injected on November 2, 2011
MW-16
Date
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Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Table 1
Sampling and Analysis Summary
May 27-29, 2014
MNA Field Parameter Tracer
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IW-1 E x
MW-1 x x x x x x x x x x x x x x x x x x x x
IW-2 E x
MW-3R x x x x x x x x x
IW-3 E x
IW-4 E x
IW-5 E x
MW-7 x x x x x x x x x x x x x x x x x x x
IW-6 E x
MW-9 x x x x x x x x x x x x x x x x x x
MW-12S x x x x x x x x x
MW-13 x x x x x x x x x x
MW-14 x x x x x x x x x x x x x x x x x x x x
MW-15 x x x x x x x x x x x x x x x x x x x x
MW-16 x x x x x x x x x x x x
MW-17 x x x x x x x x x
MW-18 x x x x x x x x x
MW-19 x x x x x x x x x x
MW-20 x x x x x x x x x
MW-21 x x x x x x x x x x x x x x x x x x x x
MW-22 x x x x x x x x x x
MW-23 x x x x x x x x x
EB x x
FB x x
TB x
App. I App. II
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App I & II = Appendix I & II List from current 40 CFR 258
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2
Table 2
Detections in Water Samples above SWSL or 2L Standards
May 27-29, 2014
Result Unit
MW-7 5/28/14 2.7 0.33 1 6 75
MW-7 Antimony, total 5/28/14 9.8 5 6 NE 8.4
MW-7 5/28/14 5.7 0.23 3 50 100
MW-7 Cobalt, total 5/28/14 77.3 5 10 NE 7.3
MW-9 5/28/14 6.6 0.33 1 6 75 0.6
MW-9 Benzene 5/28/14 3.3 0.25 1 1 5 2.3
MW-9 5/28/14 5.7 0.19 5 70 70
MW-9 Cobalt, total 5/28/14 140 5 10 NE 70
MW-9 Vinyl chloride 5/28/14 10.8 0.62 1 0.03 5 10.77
MW-13 5/28/14 0.47 j 0.12 1 0.4 5 0.07
MW-13 5/28/14 19.3 0.19 5 70 70
MW-13 5/28/14 1.2 0.47 1 3 5
MW-14 5/28/14 0.89 j 0.46 1 0.7 5 0.19
MW-15 5/28/14 14.2 0.32 5 6 7 8.2
MW-15 5/28/14 0.58 j 0.12 1 0.4 5 0.18
MW-15 5/28/14 3.6 0.33 1 6 75
MW-15 Benzene 5/28/14 2.3 0.25 1 1 5 1.3
MW-15 5/28/14 35.2 0.19 5 70 70
MW-15 5/28/14 0.74 j 0.46 1 0.7 5 0.04
MW-15 5/28/14 3.6 0.47 1 3 5 0.6
MW-15 Vinyl chloride 5/28/14 1.9 0.62 1 0.03 5 1.87
MW-16 5/28/14 2.4 0.12 1 0.4 5 2
MW-16 5/28/14 3.2 0.27 1 0.6 5 2.6
MW-16 5/28/14 15 0.33 1 6 75 9
MW-16 Antimony, total 5/28/14 15.9 5 6 NE 14.5
MW-16 Barium, total 5/28/14 117 5 100 2000 2000
MW-16 Benzene 5/28/14 1.8 0.25 1 1 5 0.8
MW-16 5/28/14 5.8 0.23 3 50 100
MW-16 5/28/14 46.6 0.19 5 70 70
MW-16 Cobalt, total 5/28/14 325 5 10 NE 255
MW-16 Thallium, total 5/28/14 9.5 5.4 5.5 2 9.22
MW-16 Vinyl chloride 5/28/14 6.7 0.62 1 0.03 5 6.67
MW-16 Zinc, total 5/28/14 13.5 10 10 1000 5000
MW-17 Cobalt, total 5/28/14 44.3 5 10 NE
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 MCL 5
2L
Exceedance
Amount
1,4-Dichlorobenzene ug/L
ug/L
Chlorobenzene ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
1,2-Dichloroethane ug/L
cis-1,2-Dichloroethene ug/L
Trichloroethene ug/L
Tetrachloroethene ug/L
1,1-Dichloroethane ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
ug/L
1,2-Dichloroethane ug/L
1,2-Dichloropropane ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 2 of 2
Result Unit
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 MCL 5
2L
Exceedance
Amount
MW-19 Vanadium, total 5/27/14 6.4 j 5 25 NE 2.9
MW-19 Zinc, total 5/27/14 10.1 10 10 1000 5000
MW-20 Cobalt, total 5/27/14 14.2 5 10 NE
MW-21 5/28/14 6.3 0.32 5 6 7 0.3
MW-21 5/28/14 0.42 j 0.12 1 0.4 5 0.02
MW-21 5/28/14 20.1 0.19 5 70 70
MW-21 5/28/14 1.5 0.47 1 3 5
MW-22 5/28/14 0.51 j 0.12 1 0.4 5 0.11
MW-22 5/28/14 2.4 0.33 1 6 75
MW-22 Cobalt, total 5/28/14 37.3 5 10 NE
EB Methylene Chloride 5/29/14 1 j 0.97 1 4.6 5
j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
ug/L
ug/L
ug/L
1,1-Dichloroethane ug/L
1,2-Dichloroethane ug/L
cis-1,2-Dichloroethene ug/L
Trichloroethene ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
1 Table contains Appendix I constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 MCL = Maximum Contaminant Level (“Drinking Water Standard”) not applicable regulatory Standard but shown for comparison purposes
BOLD = Concentration > 2L, or 2B Standard
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Table 3
Field Parameter Data Summary
May 27-28, 2014
Parameter Temp. ORP DO pH TDS Turbidity
Units C mg/L SU mg/L Visual or NTU
MW-1 24.80 1109.55 1134.35 14.8 201 2.3 6.03 300 140 16.2
IW-2 39.61 1029.25 1068.86 NR NR NR NR NR NR >1000
MW-3R 30.95 986.55 1017.50 15.2 119 0.5 7.82 200 90 Clear
IW-3 40.77 979.80 1020.57 NR NR NR NR NR NR >1000
IW-4 33.94 992.32 1026.26 NR NR NR NR NR NR >1000
IW-5 39.94 1040.24 1080.18 NR NR NR NR NR NR >1000
MW-6 22.38 1045.29 1067.67 13.9 -23 1.1 6.35 500 240 Slight
MW-7 11.81 1061.69 1073.50 14.6 201 2.6 5.43 330 160 18.1
IW-6 40.98 1047.47 1088.45 NR NR NR NR NR NR >1000
MW-9 32.99 1061.08 1094.07 15.9 30 0.1 6.27 480 240 13.1
MW-12S 13.38 1012.42 1025.80 14.0 60 3.3 7.26 410 200 Clear
MW-12D 0.00 1027.05 1027.05 14.1 -91 1.4 7.35 160 120 Clear
MW-13 25.23 983.25 1008.48 14.6 206 2.3 5.30 250 120 Clear
MW-14 35.39 983.41 1018.80 14.3 21 2.2 5.26 100 50 20.1
MW-15 51.12 1024.84 1075.96 14.8 27 0.4 5.32 140 70 >1000
MW-16 25.69 973.85 999.54 16.0 82 0.6 5.74 520 250 Clear
MW-17 8.39 957.04 965.43 13.1 78 1.4 6.05 310 150 Clear
MW-18 9.17 973.83 983.00 13.0 191 6.3 5.81 30 10 Slight
MW-19 9.84 936.43 946.27 13.1 273 3.0 5.52 50 30 Slight
MW-20 19.41 1062.78 1082.19 13.4 201 1.2 5.38 80 40 Clear
MW-21 5.44 959.92 965.36 13.7 203 1.9 5.01 210 100 163
MW-22 5.22 948.18 953.40 16.4 233 4.1 5.83 280 140 Clear
MW-23 7.39 947.92 955.31 14.7 211 4.3 6.98 100 40 Clear
Minimum 0.00 936.43 946.27 13.0 -91 0.1 5.01 30 10 13.10
Average 23.21 1006.27 1029.48 14.4 124 2.2 6.04 247 122 Slight
Maximum 51.12 1109.55 1134.35 16.4 273 6.3 7.82 520 250 >1000
NR = No reading attempted
Depth to
Water*
Water
Elevation
TOC
Elevation
Specific
Conductance
ft (btoc) ft (amsl) ft (amsl)mV umhos/cm
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Table 4
May 27-28, 2014
(cm/second)(%) (feet/feet) (feet/year)
MW-1 4.30E-05 15 0.083 25 S18W 24.80 1109.55 Clay
IW-2 4.30E-05 15 0.024 7 S76E 39.61 1029.25 Clay
MW-7 8.10E-04 15 0.319 1,785 N84W 11.81 1061.69 PWR/Fractured Rock
IW-6 4.40E-04 15 0.113 342 S14E 40.98 1047.47 PWR/Fractured Rock
MW-9 1.90E-04 15 0.038 50 S53E 32.99 1061.08 Sandy Silt
MW-13 2.06E-04 23 0.063 59 S36E 25.23 983.25
MW-18 2.04E-03 15 0.117 S39E 9.17 973.83
MW-19 1.10E-03 3 0.093 3,519 S14W 9.84 936.43 PWR
MW-21 1.28E-03 3 0.033 1,453 S55E 5.44 959.92
MW-22 9.88E-04 15 0.120 821 S29W 5.22 948.18
MW-23 3.04E-04 15 0.154 324 S40E 7.39 947.92 Sandy Silt
Minimum 4.30E-05 3 0.024 7 - 5.22 936.43 -
Average 6.77E-04 14 0.105 838 - 19.32 1005.32 -
Maximum 2.04E-03 23 0.319 3,519 - 40.98 1109.55 -
MW-3R 2.40E-04 5 40.77 976.73 Fractured Rock
IW-3 2.40E-05 5 0.028 14 S40W 30.95 989.62 Fractured Rock
IW-4 1.10E-04 5 0.205 466 S41E 33.94 992.32 Fractured Rock
IW-5 1.50E-05 5 0.161 50 S63W 39.94 1040.24 Fractured Rock
MW-6 1.90E-05 5 0.191 75 S80W 22.38 1045.29 Fractured Rock
MW-12S 3 0.104 S04W 13.38 1012.42 Fractured Rock
MW-12D 1.30E-06 5 0.00 1027.05 Fractured Rock
MW-14 7.45E-03 3 0.305 78,438 S72E 35.39 983.41 Fractured Rock
MW-15 7.21E-05 3 0.190 473 S06W 51.12 1024.84 Fractured Rock
MW-16 2.82E-05 3 0.157 152 S40W 25.69 973.85 Fractured Rock
MW-17 2.94E-04 3 0.102 1,031 S64W 8.39 957.04 Rock
MW-20 1.92E-04 3 0.107 707 S03E 19.41 1062.78 Rock
Minimum 1.30E-06 3 0.028 14 - 0.00 957.04 -
Average 7.68E-04 4 0.155 371 - 26.78 1007.13 -
Maximum 7.45E-03 5 0.305 1,031 - 51.12 1062.78 -
NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Wells screened entirely in rock were not utilized for flow directions/gradients.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
na = Not available/applicable
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average
Linear
Velocity Rate
Flow
Direction
Groundwater
Depth
Groundwater
Potentiometric
Elevation
Screened Interval
Lithology(feet btoc) (feet amsl)
Saprolite
na Saprolite
Saprolite/PWR
Saprolite
na na na
na na
na na na
Hydrologic gradient from water levels recorded on May 27-28, 2014.
Average Linear Velocity (Q) is defined by modified Darcy's equation:
K= hydraulic conductivity
ne= effective porosity
dh= head difference
dl= horizontal distance
dl
dh
n
KQ
e
-=
Surry County Closed C&D and CLosed MSWLF, Mt. Airy Page 1 of 1
Table 5
MNA Parameter Data Summary
May 28, 2014
Parameters Method MDL* Units
MW-1 MW-7 MW-9 MW-14 MW-15 MW-21
5/28/14 5/28/14 5/28/14 5/28/14 5/28/14 5/28/14
VFA – Acetic Acid AM23G NS NS NS NS NS NS NS
AM23G NS NS NS NS NS NS NS
VFA – Lactic Acid AM23G NS NS NS NS NS NS NS
AM23G NS NS NS NS NS NS NS
AM23G NS NS NS NS NS NS NS
Hydrogen AM20GAX NS NS NS NS NS NS NS
Methane RSK175 400 <400 93500 1570 <400
AM20GAX NS NS NS NS NS NS NS
Ethane AM20GAX NS NS NS NS NS NS NS
CO2-Dissolved Field HACH Kit NS mg/L NS NS NS NS NS NS
Alkalinity SM 2320B 1000 81500 79100 112000 32400 44000 34500
Sulfate EPA 300.0 2000 7940 6570 <2000 2210 <2000 <2000
Sulfide SM 4500-S2D 100 <100 <100 <100 <100 <100 <100
Chloride SM 4500-Cl-E 1000 3270 2710 1890 27600
TOC SM 5310B 1000 2960 13900 8070 5660 10700
COD SM 5220D 25000 <25000 35000 33000 <25000 <25000 <25000
BOD SM5210B NS NS NS NS NS NS NS
Iron EPA 6010 50 167 <50 44900 245 2640 <50
Nitrate EPA 353.2 <20 NS NS NS NS NS NS
Temperature Field Instrument 0 C 14.8 2.6 15.9 14.3 14.8 13.7
ORP Field Instrument -900 201 201 30 21 27 203
DO Field Instrument 0 mg/L 2.3 2.6 0.8 2.2 0.4 1.9
pH Field Instrument 0 SU 6.03 5.43 6.27 5.26 5.32 5.01
Specific Conductance Field Instrument 0 us/cm 300 330 480 100 140 210
Turbidity Field Instrument 0 NTU 16.2 18.1 13.1 20.1 >1000 163
Notes:
MDL* = Lab Method Detection Limit or lowest field measurement possible.
Constituents detected below quantifiable limits are shown as < MDL value.
>100 = CO2 Concentration exceeds maximum capability of method used.
NS = Not Sampled
ug/L
VFA – Butyric Acid ug/L
ug/L
VFA – Propionic Acid ug/L
VFA – Pyruvic Acid ug/L
nM
ug/L 1530000 21 957000 21
Ethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L 28800 2 45100 5
ug/L 8670 5
ug/L
ug/L
ug/L
ug/L
mV
5 Indicates dilution factor used
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
June 12, 2014
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92203121
92203121
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Surry Closed-Mt. Airy (UIC)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between May 28, 2014
and May 29, 2014. The results relate only to the samples included in this report. Results reported
herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 73
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 73
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Lab ID Sample ID Matrix Date Collected Date Received
92203121001 MW-12S Water 05/27/14 14:35 05/28/14 17:00
92203121002 MW-18 Water 05/27/14 13:30 05/28/14 17:00
92203121003 MW-19 Water 05/27/14 15:10 05/28/14 17:00
92203121004 MW-23 Water 05/27/14 16:00 05/28/14 17:00
92203121005 MW-1 Water 05/28/14 08:05 05/29/14 15:20
92203121006 MW-7 Water 05/28/14 12:00 05/29/14 15:20
92203121007 MW-15 Water 05/28/14 09:45 05/29/14 15:20
92203121008 MW-21 Water 05/28/14 13:40 05/29/14 15:20
92203121009 MW-9 Water 05/28/14 11:35 05/29/14 15:20
92203121010 MW-14 Water 05/28/14 10:15 05/29/14 15:20
92203121011 MW-3R Water 05/28/14 08:40 05/29/14 15:20
92203121012 MW-13 Water 05/28/14 11:00 05/29/14 15:20
92203121013 MW-17 Water 05/28/14 15:10 05/29/14 15:20
92203121014 MW-20 Water 05/27/14 06:05 05/29/14 15:20
92203121015 MW-16 Water 05/28/14 09:10 05/29/14 15:20
92203121016 MW-22 Water 05/28/14 14:35 05/29/14 15:20
92203121017 MW-19 Water 05/27/14 15:10 05/29/14 15:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 73
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92203121001 MW-12S EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CMCK
92203121002 MW-18 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CMCK
92203121003 MW-19 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CMCK
92203121004 MW-23 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CMCK
92203121005 MW-1 EPA 6010 16 PASI-AJMW
EPA 8260 51 PASI-CNU1
SM 2320B 1 PASI-AMDW
SM 4500-S2D 1 PASI-ASAE
EPA 300.0 1 PASI-ASAE
SM 4500-Cl-E 1 PASI-ASMW
SM 4500-CN-E 1 PASI-AJDA
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-ASAE
92203121006 MW-7 EPA 6010 16 PASI-AJMW
EPA 8260 51 PASI-CNU1
SM 2320B 1 PASI-AMDW
SM 4500-S2D 1 PASI-ASAE
EPA 300.0 1 PASI-ASAE
SM 4500-Cl-E 1 PASI-ASMW
SM 4500-CN-E 1 PASI-AJDA
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-ASAE
92203121007 MW-15 EPA 6010 16 PASI-AJMW
EPA 8260 51 PASI-CNU1
SM 2320B 1 PASI-AMDW
SM 4500-S2D 1 PASI-ASAE
EPA 300.0 1 PASI-ASAE
SM 4500-Cl-E 1 PASI-ASMW
SM 4500-CN-E 1 PASI-AJDA
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-ASAE
92203121008 MW-21 EPA 6010 16 PASI-AJMW
EPA 8260 51 PASI-CNU1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 73
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2320B 1 PASI-AMDW
SM 4500-S2D 1 PASI-ASAE
EPA 300.0 1 PASI-ASAE
SM 4500-Cl-E 1 PASI-ASMW
SM 4500-CN-E 1 PASI-AJDA
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-ASAE
92203121009 MW-9 EPA 6010 16 PASI-AJMW
EPA 8260 51 PASI-CNU1
SM 2320B 1 PASI-AMDW
SM 4500-S2D 1 PASI-ASAE
EPA 300.0 1 PASI-ASAE
SM 4500-Cl-E 1 PASI-ASMW
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-ASAE
92203121010 MW-14 EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 51 PASI-CNU1
SM 2320B 1 PASI-AMDW
SM 4500-S2D 1 PASI-ASAE
EPA 300.0 1 PASI-ASAE
SM 4500-Cl-E 1 PASI-ASMW
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-ASAE
92203121011 MW-3R EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CNU1
92203121012 MW-13 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CNU1
92203121013 MW-17 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CNU1
92203121014 MW-20 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CNU1
92203121015 MW-16 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CNU1
SM 4500-CN-E 1 PASI-AJDA
92203121016 MW-22 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CNU1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 73
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-CN-E 1 PASI-AJDA
92203121017 MW-19 SM 4500-CN-E 1 PASI-AJDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-12S Lab ID: 92203121001 Collected: 05/27/14 14:35 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 05/30/14 19:59 7440-36-005/29/14 15:556.0 5.0 1
Arsenic ND ug/L 05/30/14 19:59 7440-38-205/29/14 15:5510.0 5.0 1
Barium 22.4J ug/L 05/30/14 19:59 7440-39-305/29/14 15:55100 5.0 1
Beryllium ND ug/L 05/30/14 19:59 7440-41-705/29/14 15:551.0 1.0 1
Cadmium ND ug/L 05/30/14 19:59 7440-43-905/29/14 15:551.0 1.0 1
Chromium ND ug/L 05/30/14 19:59 7440-47-305/29/14 15:5510.0 5.0 1
Cobalt ND ug/L 05/30/14 19:59 7440-48-405/29/14 15:5510.0 5.0 1
Copper ND ug/L 05/30/14 19:59 7440-50-805/29/14 15:5510.0 5.0 1
Lead ND ug/L 05/30/14 19:59 7439-92-105/29/14 15:5510.0 5.0 1
Nickel ND ug/L 05/30/14 19:59 7440-02-005/29/14 15:5550.0 5.0 1
Selenium ND ug/L 05/30/14 19:59 7782-49-205/29/14 15:5510.0 10.0 1
Silver ND ug/L 05/30/14 19:59 7440-22-405/29/14 15:5510.0 5.0 1
Thallium ND ug/L 05/30/14 19:59 7440-28-005/29/14 15:555.5 5.4 1
Vanadium ND ug/L 05/30/14 19:59 7440-62-205/29/14 15:5525.0 5.0 1
Zinc ND ug/L 05/30/14 19:59 7440-66-605/29/14 15:5510.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/29/14 23:52 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/29/14 23:52 107-13-1200 1.9 1
Benzene ND ug/L 05/29/14 23:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/29/14 23:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/29/14 23:52 75-27-41.0 0.18 1
Bromoform ND ug/L 05/29/14 23:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/29/14 23:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/29/14 23:52 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/29/14 23:52 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/29/14 23:52 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/29/14 23:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/29/14 23:52 75-00-310.0 0.54 1
Chloroform ND ug/L 05/29/14 23:52 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/29/14 23:52 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/29/14 23:52 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/29/14 23:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/29/14 23:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/29/14 23:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/29/14 23:52 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/29/14 23:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/29/14 23:52 110-57-6100 1.0 1
1,1-Dichloroethane 0.64J ug/L 05/29/14 23:52 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/29/14 23:52 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/29/14 23:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.59J ug/L 05/29/14 23:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/29/14 23:52 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/29/14 23:52 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/29/14 23:52 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/29/14 23:52 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-12S Lab ID: 92203121001 Collected: 05/27/14 14:35 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/29/14 23:52 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/29/14 23:52 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/29/14 23:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/29/14 23:52 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/29/14 23:52 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/29/14 23:52 108-10-1100 0.33 1
Styrene ND ug/L 05/29/14 23:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/29/14 23:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/29/14 23:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/29/14 23:52 127-18-41.0 0.46 1
Toluene ND ug/L 05/29/14 23:52 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/29/14 23:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/29/14 23:52 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/29/14 23:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/29/14 23:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/29/14 23:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/29/14 23:52 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/29/14 23:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/29/14 23:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %05/29/14 23:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/29/14 23:52 17060-07-070-130 1
Toluene-d8 (S)97 %05/29/14 23:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-18 Lab ID: 92203121002 Collected: 05/27/14 13:30 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 05/30/14 20:02 7440-36-005/29/14 15:556.0 5.0 1
Arsenic ND ug/L 05/30/14 20:02 7440-38-205/29/14 15:5510.0 5.0 1
Barium 11.7J ug/L 05/30/14 20:02 7440-39-305/29/14 15:55100 5.0 1
Beryllium ND ug/L 05/30/14 20:02 7440-41-705/29/14 15:551.0 1.0 1
Cadmium ND ug/L 05/30/14 20:02 7440-43-905/29/14 15:551.0 1.0 1
Chromium ND ug/L 05/30/14 20:02 7440-47-305/29/14 15:5510.0 5.0 1
Cobalt ND ug/L 05/30/14 20:02 7440-48-405/29/14 15:5510.0 5.0 1
Copper ND ug/L 05/30/14 20:02 7440-50-805/29/14 15:5510.0 5.0 1
Lead ND ug/L 05/30/14 20:02 7439-92-105/29/14 15:5510.0 5.0 1
Nickel ND ug/L 05/30/14 20:02 7440-02-005/29/14 15:5550.0 5.0 1
Selenium ND ug/L 05/30/14 20:02 7782-49-205/29/14 15:5510.0 10.0 1
Silver ND ug/L 05/30/14 20:02 7440-22-405/29/14 15:5510.0 5.0 1
Thallium ND ug/L 05/30/14 20:02 7440-28-005/29/14 15:555.5 5.4 1
Vanadium ND ug/L 05/30/14 20:02 7440-62-205/29/14 15:5525.0 5.0 1
Zinc ND ug/L 05/30/14 20:02 7440-66-605/29/14 15:5510.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/30/14 00:08 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/30/14 00:08 107-13-1200 1.9 1
Benzene ND ug/L 05/30/14 00:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/30/14 00:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/30/14 00:08 75-27-41.0 0.18 1
Bromoform ND ug/L 05/30/14 00:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/30/14 00:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/30/14 00:08 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/30/14 00:08 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/30/14 00:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/30/14 00:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/30/14 00:08 75-00-310.0 0.54 1
Chloroform ND ug/L 05/30/14 00:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/30/14 00:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/30/14 00:08 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/30/14 00:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/30/14 00:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/30/14 00:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/30/14 00:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/30/14 00:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/30/14 00:08 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 05/30/14 00:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/30/14 00:08 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/30/14 00:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/30/14 00:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/30/14 00:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/30/14 00:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/30/14 00:08 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/30/14 00:08 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-18 Lab ID: 92203121002 Collected: 05/27/14 13:30 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/30/14 00:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/30/14 00:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/30/14 00:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/30/14 00:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/30/14 00:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/30/14 00:08 108-10-1100 0.33 1
Styrene ND ug/L 05/30/14 00:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/30/14 00:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/30/14 00:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/30/14 00:08 127-18-41.0 0.46 1
Toluene ND ug/L 05/30/14 00:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/30/14 00:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/30/14 00:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/30/14 00:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/30/14 00:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/30/14 00:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/30/14 00:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/30/14 00:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/30/14 00:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %05/30/14 00:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %05/30/14 00:08 17060-07-070-130 1
Toluene-d8 (S)97 %05/30/14 00:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-19 Lab ID: 92203121003 Collected: 05/27/14 15:10 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 05/30/14 20:14 7440-36-005/29/14 15:556.0 5.0 1
Arsenic ND ug/L 05/30/14 20:14 7440-38-205/29/14 15:5510.0 5.0 1
Barium 54.8J ug/L 05/30/14 20:14 7440-39-305/29/14 15:55100 5.0 1
Beryllium ND ug/L 05/30/14 20:14 7440-41-705/29/14 15:551.0 1.0 1
Cadmium ND ug/L 05/30/14 20:14 7440-43-905/29/14 15:551.0 1.0 1
Chromium ND ug/L 05/30/14 20:14 7440-47-305/29/14 15:5510.0 5.0 1
Cobalt ND ug/L 05/30/14 20:14 7440-48-405/29/14 15:5510.0 5.0 1
Copper ND ug/L 05/30/14 20:14 7440-50-805/29/14 15:5510.0 5.0 1
Lead ND ug/L 05/30/14 20:14 7439-92-105/29/14 15:5510.0 5.0 1
Nickel ND ug/L 05/30/14 20:14 7440-02-005/29/14 15:5550.0 5.0 1
Selenium ND ug/L 05/30/14 20:14 7782-49-205/29/14 15:5510.0 10.0 1
Silver ND ug/L 05/30/14 20:14 7440-22-405/29/14 15:5510.0 5.0 1
Thallium ND ug/L 05/30/14 20:14 7440-28-005/29/14 15:555.5 5.4 1
Vanadium 6.4J ug/L 05/30/14 20:14 7440-62-205/29/14 15:5525.0 5.0 1
Zinc 10.1 ug/L 05/30/14 20:14 7440-66-605/29/14 15:5510.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/30/14 00:25 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/30/14 00:25 107-13-1200 1.9 1
Benzene ND ug/L 05/30/14 00:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/30/14 00:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/30/14 00:25 75-27-41.0 0.18 1
Bromoform ND ug/L 05/30/14 00:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/30/14 00:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/30/14 00:25 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/30/14 00:25 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/30/14 00:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/30/14 00:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/30/14 00:25 75-00-310.0 0.54 1
Chloroform ND ug/L 05/30/14 00:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/30/14 00:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/30/14 00:25 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/30/14 00:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/30/14 00:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/30/14 00:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/30/14 00:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/30/14 00:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/30/14 00:25 110-57-6100 1.0 1
1,1-Dichloroethane 2.3J ug/L 05/30/14 00:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/30/14 00:25 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/30/14 00:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 3.1J ug/L 05/30/14 00:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/30/14 00:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/30/14 00:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/30/14 00:25 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/30/14 00:25 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-19 Lab ID: 92203121003 Collected: 05/27/14 15:10 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/30/14 00:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/30/14 00:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/30/14 00:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/30/14 00:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/30/14 00:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/30/14 00:25 108-10-1100 0.33 1
Styrene ND ug/L 05/30/14 00:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/30/14 00:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/30/14 00:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/30/14 00:25 127-18-41.0 0.46 1
Toluene ND ug/L 05/30/14 00:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/30/14 00:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/30/14 00:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/30/14 00:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/30/14 00:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/30/14 00:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/30/14 00:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/30/14 00:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/30/14 00:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %05/30/14 00:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %05/30/14 00:25 17060-07-070-130 1
Toluene-d8 (S)98 %05/30/14 00:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-23 Lab ID: 92203121004 Collected: 05/27/14 16:00 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 05/30/14 20:17 7440-36-005/29/14 15:556.0 5.0 1
Arsenic ND ug/L 05/30/14 20:17 7440-38-205/29/14 15:5510.0 5.0 1
Barium 39.8J ug/L 05/30/14 20:17 7440-39-305/29/14 15:55100 5.0 1
Beryllium ND ug/L 05/30/14 20:17 7440-41-705/29/14 15:551.0 1.0 1
Cadmium ND ug/L 05/30/14 20:17 7440-43-905/29/14 15:551.0 1.0 1
Chromium ND ug/L 05/30/14 20:17 7440-47-305/29/14 15:5510.0 5.0 1
Cobalt ND ug/L 05/30/14 20:17 7440-48-405/29/14 15:5510.0 5.0 1
Copper ND ug/L 05/30/14 20:17 7440-50-805/29/14 15:5510.0 5.0 1
Lead ND ug/L 05/30/14 20:17 7439-92-105/29/14 15:5510.0 5.0 1
Nickel ND ug/L 05/30/14 20:17 7440-02-005/29/14 15:5550.0 5.0 1
Selenium ND ug/L 05/30/14 20:17 7782-49-205/29/14 15:5510.0 10.0 1
Silver ND ug/L 05/30/14 20:17 7440-22-405/29/14 15:5510.0 5.0 1
Thallium ND ug/L 05/30/14 20:17 7440-28-005/29/14 15:555.5 5.4 1
Vanadium ND ug/L 05/30/14 20:17 7440-62-205/29/14 15:5525.0 5.0 1
Zinc ND ug/L 05/30/14 20:17 7440-66-605/29/14 15:5510.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/30/14 00:41 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/30/14 00:41 107-13-1200 1.9 1
Benzene ND ug/L 05/30/14 00:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/30/14 00:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/30/14 00:41 75-27-41.0 0.18 1
Bromoform ND ug/L 05/30/14 00:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/30/14 00:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/30/14 00:41 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/30/14 00:41 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/30/14 00:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/30/14 00:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/30/14 00:41 75-00-310.0 0.54 1
Chloroform ND ug/L 05/30/14 00:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/30/14 00:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/30/14 00:41 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/30/14 00:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/30/14 00:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/30/14 00:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/30/14 00:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/30/14 00:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/30/14 00:41 110-57-6100 1.0 1
1,1-Dichloroethane 1.1J ug/L 05/30/14 00:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/30/14 00:41 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/30/14 00:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.0J ug/L 05/30/14 00:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/30/14 00:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/30/14 00:41 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/30/14 00:41 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/30/14 00:41 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-23 Lab ID: 92203121004 Collected: 05/27/14 16:00 Received: 05/28/14 17:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/30/14 00:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/30/14 00:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/30/14 00:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/30/14 00:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/30/14 00:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/30/14 00:41 108-10-1100 0.33 1
Styrene ND ug/L 05/30/14 00:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/30/14 00:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/30/14 00:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/30/14 00:41 127-18-41.0 0.46 1
Toluene ND ug/L 05/30/14 00:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/30/14 00:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/30/14 00:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/30/14 00:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/30/14 00:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/30/14 00:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/30/14 00:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/30/14 00:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/30/14 00:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %05/30/14 00:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %05/30/14 00:41 17060-07-070-130 1
Toluene-d8 (S)98 %05/30/14 00:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-1 Lab ID: 92203121005 Collected: 05/28/14 08:05 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:08 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:08 7440-38-206/03/14 12:3010.0 5.0 1
Barium 19.2J ug/L 06/04/14 20:08 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:08 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:08 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:08 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt ND ug/L 06/04/14 20:08 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:08 7440-50-806/03/14 12:3010.0 5.0 1
Iron 167J ug/L 06/04/14 20:08 7439-89-606/03/14 12:30300 50.0 1
Lead ND ug/L 06/04/14 20:08 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:08 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:08 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:08 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:08 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:08 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:08 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 03:44 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 03:44 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 03:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 03:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 03:44 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 03:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 03:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 03:44 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 03:44 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 03:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/31/14 03:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 03:44 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 03:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 03:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 03:44 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 03:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 03:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 03:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 03:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/31/14 03:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 03:44 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 05/31/14 03:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/14 03:44 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 03:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/31/14 03:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 03:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 03:44 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 03:44 142-28-91.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-1 Lab ID: 92203121005 Collected: 05/28/14 08:05 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/L 05/31/14 03:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 03:44 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 03:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 03:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 03:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 03:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 03:44 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 03:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 03:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 03:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 03:44 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 03:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 03:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 03:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 03:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 03:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 03:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 03:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 03:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 03:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/14 03:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %05/31/14 03:44 17060-07-070-130 1
Toluene-d8 (S)99 %05/31/14 03:44 2037-26-570-130 1
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 81500 ug/L 06/03/14 14:005000 1000 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/03/14 15:47 18496-25-81000 100 1
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate 7940J ug/L 06/03/14 07:53 14808-79-8250000 2000 1
4500 Chloride Analytical Method: SM 4500-Cl-E
Chloride 3270 ug/L 06/11/14 18:00 16887-00-61000 1000 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND ug/L 06/09/14 11:11 57-12-510.0 5.0 1
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND ug/L 06/10/14 13:4025000 25000 1
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 2960 ug/L 06/05/14 20:23 7440-44-01000 1000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-7 Lab ID: 92203121006 Collected: 05/28/14 12:00 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 9.8 ug/L 06/04/14 20:11 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:11 7440-38-206/03/14 12:3010.0 5.0 1
Barium 71.9J ug/L 06/04/14 20:11 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:11 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:11 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:11 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 77.3 ug/L 06/04/14 20:11 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:11 7440-50-806/03/14 12:3010.0 5.0 1
Iron ND ug/L 06/04/14 20:11 7439-89-606/03/14 12:30300 50.0 1
Lead ND ug/L 06/04/14 20:11 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:11 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:11 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:11 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:11 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:11 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:11 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 03:59 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 03:59 107-13-1200 1.9 1
Benzene 0.72J ug/L 05/31/14 03:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 03:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 03:59 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 03:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 03:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 03:59 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 03:59 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 03:59 56-23-51.0 0.25 1
Chlorobenzene 5.7 ug/L 05/31/14 03:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 03:59 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 03:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 03:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 03:59 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 03:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 03:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 03:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 03:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.7 ug/L 05/31/14 03:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 03:59 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 05/31/14 03:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/14 03:59 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 03:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.38J ug/L 05/31/14 03:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 03:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 03:59 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 03:59 142-28-91.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-7 Lab ID: 92203121006 Collected: 05/28/14 12:00 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/L 05/31/14 03:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 03:59 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 03:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 03:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 03:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 03:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 03:59 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 03:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 03:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 03:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 03:59 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 03:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 03:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 03:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 03:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 03:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 03:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 03:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 03:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 03:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/31/14 03:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/31/14 03:59 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 03:59 2037-26-570-130 1
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 79100 ug/L 06/03/14 14:115000 1000 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/03/14 15:47 18496-25-81000 100 1
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate 6570J ug/L 06/03/14 08:06 14808-79-8250000 2000 1
4500 Chloride Analytical Method: SM 4500-Cl-E
Chloride 28800 ug/L 06/11/14 18:00 16887-00-62000 2000 2
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide 5.6J ug/L 06/09/14 11:12 57-12-510.0 5.0 1
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 35000 ug/L 06/10/14 13:4025000 25000 1
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 13900 ug/L 06/06/14 00:16 7440-44-0 M11000 1000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-15 Lab ID: 92203121007 Collected: 05/28/14 09:45 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:15 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:15 7440-38-206/03/14 12:3010.0 5.0 1
Barium 37.5J ug/L 06/04/14 20:15 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:15 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:15 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:15 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt ND ug/L 06/04/14 20:15 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:15 7440-50-806/03/14 12:3010.0 5.0 1
Iron 2640 ug/L 06/04/14 20:15 7439-89-606/03/14 12:30300 50.0 1
Lead ND ug/L 06/04/14 20:15 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:15 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:15 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:15 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:15 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:15 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:15 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 04:15 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 04:15 107-13-1200 1.9 1
Benzene 2.3 ug/L 05/31/14 04:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 04:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 04:15 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 04:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 04:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 04:15 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 04:15 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 04:15 56-23-51.0 0.25 1
Chlorobenzene 2.3J ug/L 05/31/14 04:15 108-90-73.0 0.23 1
Chloroethane 0.65J ug/L 05/31/14 04:15 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 04:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 04:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 04:15 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 04:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 04:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 04:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 04:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.6 ug/L 05/31/14 04:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 04:15 110-57-6100 1.0 1
1,1-Dichloroethane 14.2 ug/L 05/31/14 04:15 75-34-35.0 0.32 1
1,2-Dichloroethane 0.58J ug/L 05/31/14 04:15 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 04:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 35.2 ug/L 05/31/14 04:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 04:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 04:15 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 04:15 142-28-91.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-15 Lab ID: 92203121007 Collected: 05/28/14 09:45 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/L 05/31/14 04:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 04:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 04:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 04:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 04:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 04:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 04:15 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 04:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 04:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 04:15 79-34-53.0 0.40 1
Tetrachloroethene 0.74J ug/L 05/31/14 04:15 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 04:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 04:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 04:15 79-00-51.0 0.29 1
Trichloroethene 3.6 ug/L 05/31/14 04:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 04:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 04:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 04:15 108-05-450.0 0.35 1
Vinyl chloride 1.9 ug/L 05/31/14 04:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 04:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/14 04:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/31/14 04:15 17060-07-070-130 1
Toluene-d8 (S)99 %05/31/14 04:15 2037-26-570-130 1
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 44000 ug/L 06/03/14 14:235000 1000 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/03/14 15:47 18496-25-81000 100 1
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate ND ug/L 06/05/14 20:33 14808-79-8250000 2000 1
4500 Chloride Analytical Method: SM 4500-Cl-E
Chloride 1890 ug/L 06/11/14 18:01 16887-00-61000 1000 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND ug/L 06/09/14 11:14 57-12-510.0 5.0 1
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND ug/L 06/10/14 13:4025000 25000 1
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 8670 ug/L 06/06/14 10:13 7440-44-05000 5000 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-21 Lab ID: 92203121008 Collected: 05/28/14 13:40 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:18 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:18 7440-38-206/03/14 12:3010.0 5.0 1
Barium 53.4J ug/L 06/04/14 20:18 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:18 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:18 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:18 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 5.1J ug/L 06/04/14 20:18 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:18 7440-50-806/03/14 12:3010.0 5.0 1
Iron ND ug/L 06/04/14 20:18 7439-89-606/03/14 12:30300 50.0 1
Lead ND ug/L 06/04/14 20:18 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:18 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:18 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:18 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:18 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:18 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:18 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 04:31 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 04:31 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 04:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 04:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 04:31 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 04:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 04:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 04:31 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 04:31 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 04:31 56-23-51.0 0.25 1
Chlorobenzene 0.36J ug/L 05/31/14 04:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 04:31 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 04:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 04:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 04:31 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 04:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 04:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 04:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 04:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.75J ug/L 05/31/14 04:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 04:31 110-57-6100 1.0 1
1,1-Dichloroethane 6.3 ug/L 05/31/14 04:31 75-34-35.0 0.32 1
1,2-Dichloroethane 0.42J ug/L 05/31/14 04:31 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 04:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 20.1 ug/L 05/31/14 04:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 04:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 04:31 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 04:31 142-28-91.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-21 Lab ID: 92203121008 Collected: 05/28/14 13:40 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/L 05/31/14 04:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 04:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 04:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 04:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 04:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 04:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 04:31 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 04:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 04:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 04:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 04:31 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 04:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 04:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 04:31 79-00-51.0 0.29 1
Trichloroethene 1.5 ug/L 05/31/14 04:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 04:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 04:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 04:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 04:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 04:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %05/31/14 04:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/31/14 04:31 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 04:31 2037-26-570-130 1
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 34500 ug/L 06/03/14 14:545000 1000 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/03/14 15:47 18496-25-81000 100 1
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate ND ug/L 06/05/14 20:47 14808-79-8250000 2000 1
4500 Chloride Analytical Method: SM 4500-Cl-E
Chloride 27600 ug/L 06/11/14 18:02 16887-00-61000 1000 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND ug/L 06/09/14 11:17 57-12-510.0 5.0 1
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND ug/L 06/10/14 13:4025000 25000 1
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 10700 ug/L 06/06/14 00:53 7440-44-01000 1000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-9 Lab ID: 92203121009 Collected: 05/28/14 11:35 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:21 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:21 7440-38-206/03/14 12:3010.0 5.0 1
Barium 59.2J ug/L 06/04/14 20:21 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:21 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:21 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:21 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 140 ug/L 06/04/14 20:21 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:21 7440-50-806/03/14 12:3010.0 5.0 1
Iron 44900 ug/L 06/04/14 20:21 7439-89-606/03/14 12:30300 50.0 1
Lead ND ug/L 06/04/14 20:21 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:21 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:21 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:21 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:21 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:21 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:21 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 04:46 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 04:46 107-13-1200 1.9 1
Benzene 3.3 ug/L 05/31/14 04:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 04:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 04:46 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 04:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 04:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 04:46 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 04:46 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 04:46 56-23-51.0 0.25 1
Chlorobenzene 2.4J ug/L 05/31/14 04:46 108-90-73.0 0.23 1
Chloroethane 1.9J ug/L 05/31/14 04:46 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 04:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 04:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 04:46 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 04:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 04:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 04:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene 2.1J ug/L 05/31/14 04:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene 6.6 ug/L 05/31/14 04:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 04:46 110-57-6100 1.0 1
1,1-Dichloroethane 2.7J ug/L 05/31/14 04:46 75-34-35.0 0.32 1
1,2-Dichloroethane 0.23J ug/L 05/31/14 04:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 04:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 5.7 ug/L 05/31/14 04:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 04:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 04:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 04:46 142-28-91.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-9 Lab ID: 92203121009 Collected: 05/28/14 11:35 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/L 05/31/14 04:46 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 04:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 04:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 04:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 04:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 04:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 04:46 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 04:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 04:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 04:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 04:46 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 04:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 04:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 04:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 04:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 04:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 04:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 04:46 108-05-450.0 0.35 1
Vinyl chloride 10.8 ug/L 05/31/14 04:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 04:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/31/14 04:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/31/14 04:46 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 04:46 2037-26-570-130 1
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 112000 ug/L 06/03/14 15:285000 1000 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/03/14 15:53 18496-25-81000 100 1
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate ND ug/L 06/05/14 21:00 14808-79-8250000 2000 1
4500 Chloride Analytical Method: SM 4500-Cl-E
Chloride 45100 ug/L 06/11/14 18:02 16887-00-65000 5000 5
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 33000 ug/L 06/10/14 13:4025000 25000 1
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 8070 ug/L 06/06/14 01:04 7440-44-01000 1000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-14 Lab ID: 92203121010 Collected: 05/28/14 10:15 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:24 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:24 7440-38-206/03/14 12:3010.0 5.0 1
Barium 22.4J ug/L 06/04/14 20:24 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:24 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:24 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:24 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt ND ug/L 06/04/14 20:24 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:24 7440-50-806/03/14 12:3010.0 5.0 1
Iron 245J ug/L 06/04/14 20:24 7439-89-606/03/14 12:30300 50.0 1
Lead ND ug/L 06/04/14 20:24 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:24 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:24 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:24 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:24 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:24 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:24 7440-66-606/03/14 12:3010.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury 0.14J ug/L 06/03/14 18:41 7439-97-606/02/14 19:450.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 05:02 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 05:02 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 05:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 05:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 05:02 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 05:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 05:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 05:02 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 05:02 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 05:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/31/14 05:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 05:02 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 05:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 05:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 05:02 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 05:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 05:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 05:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 05:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/31/14 05:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 05:02 110-57-6100 1.0 1
1,1-Dichloroethane 3.6J ug/L 05/31/14 05:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/14 05:02 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 05:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.8J ug/L 05/31/14 05:02 156-59-25.0 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-14 Lab ID: 92203121010 Collected: 05/28/14 10:15 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,2-Dichloroethene ND ug/L 05/31/14 05:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 05:02 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 05:02 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/31/14 05:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 05:02 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 05:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 05:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 05:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 05:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 05:02 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 05:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 05:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 05:02 79-34-53.0 0.40 1
Tetrachloroethene 0.89J ug/L 05/31/14 05:02 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 05:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 05:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 05:02 79-00-51.0 0.29 1
Trichloroethene 0.77J ug/L 05/31/14 05:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 05:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 05:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 05:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 05:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 05:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/31/14 05:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/31/14 05:02 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 05:02 2037-26-570-130 1
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 32400 ug/L 06/03/14 15:415000 1000 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/03/14 15:53 18496-25-81000 100 1
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate 2210J ug/L 06/05/14 21:41 14808-79-8250000 2000 1
4500 Chloride Analytical Method: SM 4500-Cl-E
Chloride 2710 ug/L 06/11/14 18:04 16887-00-61000 1000 1
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND ug/L 06/10/14 13:4025000 25000 1
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 5660 ug/L 06/06/14 01:53 7440-44-01000 1000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-3R Lab ID: 92203121011 Collected: 05/28/14 08:40 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:27 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:27 7440-38-206/03/14 12:3010.0 5.0 1
Barium 6.1J ug/L 06/04/14 20:27 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:27 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:27 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:27 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt ND ug/L 06/04/14 20:27 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:27 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:27 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:27 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:27 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:27 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:27 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:27 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:27 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 05:17 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 05:17 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 05:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 05:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 05:17 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 05:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 05:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 05:17 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 05:17 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 05:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/31/14 05:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 05:17 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 05:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 05:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 05:17 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 05:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 05:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 05:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 05:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/31/14 05:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 05:17 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 05/31/14 05:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/14 05:17 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 05:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/31/14 05:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 05:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 05:17 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 05:17 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/31/14 05:17 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-3R Lab ID: 92203121011 Collected: 05/28/14 08:40 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/31/14 05:17 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 05:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 05:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 05:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 05:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 05:17 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 05:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 05:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 05:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 05:17 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 05:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 05:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 05:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 05:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 05:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 05:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 05:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 05:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 05:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/31/14 05:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %05/31/14 05:17 17060-07-070-130 1
Toluene-d8 (S)99 %05/31/14 05:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-13 Lab ID: 92203121012 Collected: 05/28/14 11:00 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:31 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:31 7440-38-206/03/14 12:3010.0 5.0 1
Barium 55.7J ug/L 06/04/14 20:31 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:31 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:31 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:31 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 7.4J ug/L 06/04/14 20:31 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:31 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:31 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:31 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:31 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:31 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:31 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:31 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:31 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 05:33 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 05:33 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 05:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 05:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 05:33 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 05:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 05:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 05:33 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 05:33 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 05:33 56-23-51.0 0.25 1
Chlorobenzene 0.24J ug/L 05/31/14 05:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 05:33 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 05:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 05:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 05:33 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 05:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 05:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 05:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 05:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.51J ug/L 05/31/14 05:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 05:33 110-57-6100 1.0 1
1,1-Dichloroethane 4.4J ug/L 05/31/14 05:33 75-34-35.0 0.32 1
1,2-Dichloroethane 0.47J ug/L 05/31/14 05:33 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 05:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 19.3 ug/L 05/31/14 05:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 05:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 05:33 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 05:33 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/31/14 05:33 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-13 Lab ID: 92203121012 Collected: 05/28/14 11:00 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/31/14 05:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 05:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 05:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 05:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 05:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 05:33 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 05:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 05:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 05:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 05:33 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 05:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 05:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 05:33 79-00-51.0 0.29 1
Trichloroethene 1.2 ug/L 05/31/14 05:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 05:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 05:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 05:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 05:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 05:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/14 05:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/31/14 05:33 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 05:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-17 Lab ID: 92203121013 Collected: 05/28/14 15:10 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 5.5J ug/L 06/04/14 20:34 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:34 7440-38-206/03/14 12:3010.0 5.0 1
Barium 57.8J ug/L 06/04/14 20:34 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:34 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:34 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:34 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 44.3 ug/L 06/04/14 20:34 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:34 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:34 7439-92-106/03/14 12:3010.0 5.0 1
Nickel 8.9J ug/L 06/04/14 20:34 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:34 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:34 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:34 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:34 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:34 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 05:49 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 05:49 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 05:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 05:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 05:49 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 05:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 05:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 05:49 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 05:49 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 05:49 56-23-51.0 0.25 1
Chlorobenzene 0.29J ug/L 05/31/14 05:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 05:49 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 05:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 05:49 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 05:49 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 05:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 05:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 05:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 05:49 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.44J ug/L 05/31/14 05:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 05:49 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 05/31/14 05:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/14 05:49 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 05:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.55J ug/L 05/31/14 05:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 05:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 05:49 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 05:49 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/31/14 05:49 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-17 Lab ID: 92203121013 Collected: 05/28/14 15:10 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/31/14 05:49 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 05:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 05:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 05:49 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 05:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 05:49 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 05:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 05:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 05:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 05:49 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 05:49 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 05:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 05:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 05:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 05:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 05:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 05:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 05:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 05:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/14 05:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/31/14 05:49 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 05:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-20 Lab ID: 92203121014 Collected: 05/27/14 06:05 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:37 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:37 7440-38-206/03/14 12:3010.0 5.0 1
Barium 23.4J ug/L 06/04/14 20:37 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:37 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:37 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:37 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 14.2 ug/L 06/04/14 20:37 7440-48-406/03/14 12:3010.0 5.0 1
Copper 7.8J ug/L 06/04/14 20:37 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:37 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:37 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:37 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:37 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:37 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:37 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:37 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 06:35 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 06:35 107-13-1200 1.9 1
Benzene ND ug/L 05/31/14 06:35 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 06:35 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 06:35 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 06:35 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 06:35 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 06:35 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 06:35 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 06:35 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/31/14 06:35 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 06:35 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 06:35 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 06:35 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 06:35 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 06:35 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 06:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 06:35 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/14 06:35 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/31/14 06:35 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 06:35 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 05/31/14 06:35 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/14 06:35 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 06:35 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.78J ug/L 05/31/14 06:35 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 06:35 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 06:35 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 06:35 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/31/14 06:35 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-20 Lab ID: 92203121014 Collected: 05/27/14 06:05 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/31/14 06:35 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 06:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 06:35 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 06:35 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 06:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 06:35 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 06:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 06:35 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 06:35 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 06:35 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 06:35 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 06:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 06:35 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 06:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 06:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 06:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 06:35 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 06:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 06:35 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/14 06:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/31/14 06:35 17060-07-070-130 1
Toluene-d8 (S)99 %05/31/14 06:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-16 Lab ID: 92203121015 Collected: 05/28/14 09:10 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony 15.9 ug/L 06/04/14 20:49 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:49 7440-38-206/03/14 12:3010.0 5.0 1
Barium 117 ug/L 06/04/14 20:49 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:49 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:49 7440-43-906/03/14 12:301.0 1.0 1
Chromium 8.9J ug/L 06/04/14 20:49 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 325 ug/L 06/04/14 20:49 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:49 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:49 7439-92-106/03/14 12:3010.0 5.0 1
Nickel 18.8J ug/L 06/04/14 20:49 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:49 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:49 7440-22-406/03/14 12:3010.0 5.0 1
Thallium 9.5 ug/L 06/04/14 20:49 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:49 7440-62-206/03/14 12:3025.0 5.0 1
Zinc 13.5 ug/L 06/04/14 20:49 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 06:04 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 06:04 107-13-1200 1.9 1
Benzene 1.8 ug/L 05/31/14 06:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 06:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 06:04 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 06:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 06:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 06:04 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 06:04 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 06:04 56-23-51.0 0.25 1
Chlorobenzene 5.8 ug/L 05/31/14 06:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 06:04 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 06:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 06:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 06:04 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 06:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 06:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 06:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.8J ug/L 05/31/14 06:04 95-50-15.0 0.30 1
1,3-Dichlorobenzene 0.29J ug/L 05/31/14 06:04 541-73-15.0 0.24 1
1,4-Dichlorobenzene 15.0 ug/L 05/31/14 06:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 06:04 110-57-6100 1.0 1
1,1-Dichloroethane 2.8J ug/L 05/31/14 06:04 75-34-35.0 0.32 1
1,2-Dichloroethane 2.4 ug/L 05/31/14 06:04 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 06:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 46.6 ug/L 05/31/14 06:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 06:04 156-60-55.0 0.49 1
1,2-Dichloropropane 3.2 ug/L 05/31/14 06:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 06:04 142-28-91.0 0.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-16 Lab ID: 92203121015 Collected: 05/28/14 09:10 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/L 05/31/14 06:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/14 06:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 06:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 06:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 06:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 06:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 06:04 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 06:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 06:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 06:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 06:04 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 06:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 06:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 06:04 79-00-51.0 0.29 1
Trichloroethene 0.89J ug/L 05/31/14 06:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 06:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 06:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 06:04 108-05-450.0 0.35 1
Vinyl chloride 6.7 ug/L 05/31/14 06:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 06:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/14 06:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/31/14 06:04 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 06:04 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide 11.0 ug/L 06/09/14 11:18 57-12-510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-22 Lab ID: 92203121016 Collected: 05/28/14 14:35 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:53 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:53 7440-38-206/03/14 12:3010.0 5.0 1
Barium 65.2J ug/L 06/04/14 20:53 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:53 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:53 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:53 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt 37.3 ug/L 06/04/14 20:53 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:53 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:53 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:53 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:53 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:53 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:53 7440-28-006/03/14 12:305.5 5.4 1
Vanadium ND ug/L 06/04/14 20:53 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:53 7440-66-606/03/14 12:3010.0 10.0 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 05/31/14 06:51 67-64-1100 10.0 1
Acrylonitrile ND ug/L 05/31/14 06:51 107-13-1200 1.9 1
Benzene 0.42J ug/L 05/31/14 06:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/14 06:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/14 06:51 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/14 06:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/14 06:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/14 06:51 78-93-3100 0.96 1
Carbon disulfide ND ug/L 05/31/14 06:51 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 05/31/14 06:51 56-23-51.0 0.25 1
Chlorobenzene 0.97J ug/L 05/31/14 06:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/14 06:51 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/14 06:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/14 06:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/14 06:51 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 05/31/14 06:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/14 06:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/14 06:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.35J ug/L 05/31/14 06:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.4 ug/L 05/31/14 06:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/14 06:51 110-57-6100 1.0 1
1,1-Dichloroethane 1.4J ug/L 05/31/14 06:51 75-34-35.0 0.32 1
1,2-Dichloroethane 0.51J ug/L 05/31/14 06:51 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 05/31/14 06:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 3.2J ug/L 05/31/14 06:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/14 06:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/14 06:51 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/14 06:51 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 05/31/14 06:51 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
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Page 37 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-22 Lab ID: 92203121016 Collected: 05/28/14 14:35 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 05/31/14 06:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/14 06:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/31/14 06:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/14 06:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/31/14 06:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/14 06:51 108-10-1100 0.33 1
Styrene ND ug/L 05/31/14 06:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/14 06:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/14 06:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/14 06:51 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/14 06:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/31/14 06:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/14 06:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/14 06:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/14 06:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/14 06:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/14 06:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/14 06:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/14 06:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/31/14 06:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/31/14 06:51 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/14 06:51 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND ug/L 06/09/14 11:19 57-12-510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
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[phone]
Page 38 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Sample: MW-19 Lab ID: 92203121017 Collected: 05/27/14 15:10 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND ug/L 06/09/14 10:40 57-12-510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6689
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples: 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1212169
Associated Lab Samples:92203121010
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 06/03/14 18:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1212170LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.72.5 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212171MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121010
1212172
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 101 75-125100 0 252.50.14J 2.7 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16067
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1208932
Associated Lab Samples:92203121001, 92203121002, 92203121003, 92203121004
Matrix: Water
Analyzed
Antimony ug/L ND 6.0 05/30/14 19:41
Arsenic ug/L ND 10.0 05/30/14 19:41
Barium ug/L ND 100 05/30/14 19:41
Beryllium ug/L ND 1.0 05/30/14 19:41
Cadmium ug/L ND 1.0 05/30/14 19:41
Chromium ug/L ND 10.0 05/30/14 19:41
Cobalt ug/L ND 10.0 05/30/14 19:41
Copper ug/L ND 10.0 05/30/14 19:41
Lead ug/L ND 10.0 05/30/14 19:41
Nickel ug/L ND 50.0 05/30/14 19:41
Selenium ug/L ND 10.0 05/30/14 19:41
Silver ug/L ND 10.0 05/30/14 19:41
Thallium ug/L ND 5.5 05/30/14 19:41
Vanadium ug/L ND 25.0 05/30/14 19:41
Zinc ug/L ND 10.0 05/30/14 19:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1208933LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 492500 98 80-120
Arsenic ug/L 467500 93 80-120
Barium ug/L 483500 97 80-120
Beryllium ug/L 451500 90 80-120
Cadmium ug/L 466500 93 80-120
Chromium ug/L 465500 93 80-120
Cobalt ug/L 480500 96 80-120
Copper ug/L 466500 93 80-120
Lead ug/L 475500 95 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 480500 96 80-120
Silver ug/L 234250 93 80-120
Thallium ug/L 458500 92 80-120
Vanadium ug/L 457500 91 80-120
Zinc ug/L 457500 91 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1208934MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203116001
1208935
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-125102 0 25500ND507 509
Arsenic ug/L 500 96 75-12597 1 25500ND480 485
Barium ug/L 500 98 75-12599 2 255006.1J 494 501
Beryllium ug/L 500 92 75-12594 2 25500ND461 469
Cadmium ug/L 500 95 75-12596 1 25500ND477 481
Chromium ug/L 500 94 75-12597 2 25500ND472 484
Cobalt ug/L 500 96 75-12598 2 25500ND482 490
Copper ug/L 500 96 75-12597 1 25500ND478 485
Lead ug/L 500 95 75-12597 2 25500ND476 485
Nickel ug/L 500 93 75-12595 2 25500ND467 475
Selenium ug/L 500 97 75-12599 1 25500ND487 493
Silver ug/L 250 95 75-12596 1 25250ND238 241
Thallium ug/L 500 93 75-12594 2 25500ND465 472
Vanadium ug/L 500 93 75-12596 2 25500ND467 478
Zinc ug/L 500 92 75-12594 2 25500ND460 471
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16107
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011,
92203121012, 92203121013, 92203121014, 92203121015, 92203121016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1212519
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011,
92203121012, 92203121013, 92203121014, 92203121015, 92203121016
Matrix: Water
Analyzed
Antimony ug/L ND 6.0 06/04/14 19:28
Arsenic ug/L ND 10.0 06/04/14 19:28
Barium ug/L ND 100 06/04/14 19:28
Beryllium ug/L ND 1.0 06/04/14 19:28
Cadmium ug/L ND 1.0 06/04/14 19:28
Chromium ug/L ND 10.0 06/04/14 19:28
Cobalt ug/L ND 10.0 06/04/14 19:28
Copper ug/L ND 10.0 06/04/14 19:28
Iron ug/L ND 300 06/04/14 19:28
Lead ug/L ND 10.0 06/04/14 19:28
Nickel ug/L ND 50.0 06/04/14 19:28
Selenium ug/L ND 10.0 06/04/14 19:28
Silver ug/L ND 10.0 06/04/14 19:28
Thallium ug/L ND 5.5 06/04/14 19:28
Vanadium ug/L ND 25.0 06/04/14 19:28
Zinc ug/L ND 10.0 06/04/14 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1212520LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 497500 99 80-120
Arsenic ug/L 477500 95 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 479500 96 80-120
Cadmium ug/L 480500 96 80-120
Chromium ug/L 486500 97 80-120
Cobalt ug/L 495500 99 80-120
Copper ug/L 494500 99 80-120
Iron ug/L 47005000 94 80-120
Lead ug/L 497500 99 80-120
Nickel ug/L 478500 96 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 242250 97 80-120
Thallium ug/L 469500 94 80-120
Vanadium ug/L 480500 96 80-120
Zinc ug/L 478500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212521MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203332001
1212522
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 95 75-12597 2 25500ND474 483
Arsenic ug/L 500 91 75-12594 3 25500ND456 468
Barium ug/L 500 94 75-12598 4 2550022.5J 490 511
Beryllium ug/L 500 91 75-12594 4 25500ND454 471
Cadmium ug/L 500 91 75-12593 2 25500ND456 467
Chromium ug/L 500 92 75-12595 3 25500ND462 476
Cobalt ug/L 500 93 75-12596 3 25500ND464 480
Copper ug/L 500 95 75-12596 1 25500ND475 480
Iron ug/L 5000 89 75-12593 4 255000178J4630 4800
Lead ug/L 500 93 75-12596 3 25500ND465 478
Nickel ug/L 500 91 75-12593 3 25500ND453 467
Selenium ug/L 500 93 75-12596 2 25500ND467 479
Silver ug/L 250 91 75-12594 3 25250ND229 235
Thallium ug/L 500 89 75-12592 3 25500ND446 459
Vanadium ug/L 500 91 75-12594 3 25500ND457 472
Zinc ug/L 500 91 75-12593 2 25500ND457 467
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/26995
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1209031
Associated Lab Samples:92203121001, 92203121002, 92203121003, 92203121004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/29/14 15:03
1,1,1-Trichloroethane ug/L ND 1.0 05/29/14 15:03
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/29/14 15:03
1,1,2-Trichloroethane ug/L ND 1.0 05/29/14 15:03
1,1-Dichloroethane ug/L ND 5.0 05/29/14 15:03
1,1-Dichloroethene ug/L ND 5.0 05/29/14 15:03
1,2,3-Trichloropropane ug/L ND 1.0 05/29/14 15:03
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/29/14 15:03
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/29/14 15:03
1,2-Dichlorobenzene ug/L ND 5.0 05/29/14 15:03
1,2-Dichloroethane ug/L ND 1.0 05/29/14 15:03
1,2-Dichloropropane ug/L ND 1.0 05/29/14 15:03
1,3-Dichloropropane ug/L ND 1.0 05/29/14 15:03
1,4-Dichlorobenzene ug/L ND 1.0 05/29/14 15:03
2-Butanone (MEK)ug/L ND 100 05/29/14 15:03
2-Hexanone ug/L ND 50.0 05/29/14 15:03
4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/29/14 15:03
Acetone ug/L ND 100 05/29/14 15:03
Acrylonitrile ug/L ND 200 05/29/14 15:03
Benzene ug/L ND 1.0 05/29/14 15:03
Bromochloromethane ug/L ND 3.0 05/29/14 15:03
Bromodichloromethane ug/L ND 1.0 05/29/14 15:03
Bromoform ug/L ND 3.0 05/29/14 15:03
Bromomethane ug/L ND 10.0 05/29/14 15:03
Carbon disulfide ug/L ND 100 05/29/14 15:03
Carbon tetrachloride ug/L ND 1.0 05/29/14 15:03
Chlorobenzene ug/L ND 3.0 05/29/14 15:03
Chloroethane ug/L ND 10.0 05/29/14 15:03
Chloroform ug/L ND 5.0 05/29/14 15:03
Chloromethane ug/L ND 1.0 05/29/14 15:03
cis-1,2-Dichloroethene ug/L ND 5.0 05/29/14 15:03
cis-1,3-Dichloropropene ug/L ND 1.0 05/29/14 15:03
Dibromochloromethane ug/L ND 3.0 05/29/14 15:03
Dibromomethane ug/L ND 10.0 05/29/14 15:03
Ethylbenzene ug/L ND 1.0 05/29/14 15:03
Iodomethane ug/L ND 10.0 05/29/14 15:03
Methylene Chloride ug/L ND 1.0 05/29/14 15:03
Styrene ug/L ND 1.0 05/29/14 15:03
Tetrachloroethene ug/L ND 1.0 05/29/14 15:03
Toluene ug/L ND 1.0 05/29/14 15:03
trans-1,2-Dichloroethene ug/L ND 5.0 05/29/14 15:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 45 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1209031
Associated Lab Samples:92203121001, 92203121002, 92203121003, 92203121004
Matrix: Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 05/29/14 15:03
trans-1,4-Dichloro-2-butene ug/L ND 100 05/29/14 15:03
Trichloroethene ug/L ND 1.0 05/29/14 15:03
Trichlorofluoromethane ug/L ND 1.0 05/29/14 15:03
Vinyl acetate ug/L ND 50.0 05/29/14 15:03
Vinyl chloride ug/L ND 1.0 05/29/14 15:03
Xylene (Total)ug/L ND 5.0 05/29/14 15:03
1,2-Dichloroethane-d4 (S)%92 70-130 05/29/14 15:03
4-Bromofluorobenzene (S)%95 70-130 05/29/14 15:03
Toluene-d8 (S)%97 70-130 05/29/14 15:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1209032LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.650 101 70-130
1,1,1-Trichloroethane ug/L 48.150 96 70-130
1,1,2,2-Tetrachloroethane ug/L 51.350 103 70-130
1,1,2-Trichloroethane ug/L 50.650 101 70-130
1,1-Dichloroethane ug/L 47.050 94 70-130
1,1-Dichloroethene ug/L 47.050 94 70-132
1,2,3-Trichloropropane ug/L 48.150 96 70-130
1,2-Dibromo-3-chloropropane ug/L 48.250 96 70-130
1,2-Dibromoethane (EDB)ug/L 49.150 98 70-130
1,2-Dichlorobenzene ug/L 50.050 100 70-130
1,2-Dichloroethane ug/L 48.850 98 70-130
1,2-Dichloropropane ug/L 49.650 99 70-130
1,3-Dichloropropane ug/L 49.850 100 70-130
1,4-Dichlorobenzene ug/L 49.150 98 70-130
2-Butanone (MEK)ug/L 87.7J100 88 70-145
2-Hexanone ug/L 97.1100 97 70-144
4-Methyl-2-pentanone (MIBK) ug/L 91.7J100 92 70-140
Acetone ug/L 94.0J100 94 50-175
Acrylonitrile ug/L 237250 95 70-143
Benzene ug/L 54.150 108 70-130
Bromochloromethane ug/L 49.050 98 70-130
Bromodichloromethane ug/L 48.650 97 70-130
Bromoform ug/L 49.250 98 70-130
Bromomethane ug/L 32.250 64 54-130
Carbon disulfide ug/L 49.9J50 100 70-131
Carbon tetrachloride ug/L 46.050 92 70-132
Chlorobenzene ug/L 47.450 95 70-130
Chloroethane ug/L 42.450 85 64-134
Chloroform ug/L 48.750 97 70-130
Chloromethane ug/L 34.350 69 64-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 46 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1209032LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.050 96 70-131
cis-1,3-Dichloropropene ug/L 51.250 102 70-130
Dibromochloromethane ug/L 47.850 96 70-130
Dibromomethane ug/L 47.150 94 70-131
Ethylbenzene ug/L 48.150 96 70-130
Iodomethane ug/L 27.5 L010027 49-180
Methylene Chloride ug/L 48.150 96 63-130
Styrene ug/L 52.250 104 70-130
Tetrachloroethene ug/L 48.750 97 70-130
Toluene ug/L 49.750 99 70-130
trans-1,2-Dichloroethene ug/L 47.450 95 70-130
trans-1,3-Dichloropropene ug/L 49.050 98 70-132
trans-1,4-Dichloro-2-butene ug/L 46.6J50 93 70-141
Trichloroethene ug/L 52.250 104 70-130
Trichlorofluoromethane ug/L 40.250 80 62-133
Vinyl acetate ug/L 100100 100 66-157
Vinyl chloride ug/L 54.950 110 69-130
Xylene (Total)ug/L 147150 98 70-130
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27034
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011,
92203121012, 92203121013, 92203121014, 92203121015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1210761
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011,
92203121012, 92203121013, 92203121014, 92203121015
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/14 01:23
1,1,1-Trichloroethane ug/L ND 1.0 05/31/14 01:23
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/14 01:23
1,1,2-Trichloroethane ug/L ND 1.0 05/31/14 01:23
1,1-Dichloroethane ug/L ND 5.0 05/31/14 01:23
1,1-Dichloroethene ug/L ND 5.0 05/31/14 01:23
1,2,3-Trichloropropane ug/L ND 1.0 05/31/14 01:23
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/14 01:23
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/31/14 01:23
1,2-Dichlorobenzene ug/L ND 5.0 05/31/14 01:23
1,2-Dichloroethane ug/L ND 1.0 05/31/14 01:23
1,2-Dichloropropane ug/L ND 1.0 05/31/14 01:23
1,3-Dichlorobenzene ug/L ND 5.0 05/31/14 01:23
1,3-Dichloropropane ug/L ND 1.0 05/31/14 01:23
1,4-Dichlorobenzene ug/L ND 1.0 05/31/14 01:23
2-Butanone (MEK)ug/L ND 100 05/31/14 01:23
2-Hexanone ug/L ND 50.0 05/31/14 01:23
4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/31/14 01:23
Acetone ug/L ND 100 05/31/14 01:23
Acrylonitrile ug/L ND 200 05/31/14 01:23
Benzene ug/L ND 1.0 05/31/14 01:23
Bromochloromethane ug/L ND 3.0 05/31/14 01:23
Bromodichloromethane ug/L ND 1.0 05/31/14 01:23
Bromoform ug/L ND 3.0 05/31/14 01:23
Bromomethane ug/L ND 10.0 05/31/14 01:23
Carbon disulfide ug/L ND 100 05/31/14 01:23
Carbon tetrachloride ug/L ND 1.0 05/31/14 01:23
Chlorobenzene ug/L ND 3.0 05/31/14 01:23
Chloroethane ug/L ND 10.0 05/31/14 01:23
Chloroform ug/L ND 5.0 05/31/14 01:23
Chloromethane ug/L ND 1.0 05/31/14 01:23
cis-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23
cis-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23
Dibromochloromethane ug/L ND 3.0 05/31/14 01:23
Dibromomethane ug/L ND 10.0 05/31/14 01:23
Ethylbenzene ug/L ND 1.0 05/31/14 01:23
Iodomethane ug/L ND 10.0 05/31/14 01:23
Methylene Chloride ug/L ND 1.0 05/31/14 01:23
Styrene ug/L ND 1.0 05/31/14 01:23
Tetrachloroethene ug/L ND 1.0 05/31/14 01:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1210761
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011,
92203121012, 92203121013, 92203121014, 92203121015
Matrix: Water
Analyzed
Toluene ug/L ND 1.0 05/31/14 01:23
trans-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23
trans-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23
trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/14 01:23
Trichloroethene ug/L ND 1.0 05/31/14 01:23
Trichlorofluoromethane ug/L ND 1.0 05/31/14 01:23
Vinyl acetate ug/L ND 50.0 05/31/14 01:23
Vinyl chloride ug/L ND 1.0 05/31/14 01:23
Xylene (Total)ug/L ND 5.0 05/31/14 01:23
1,2-Dichloroethane-d4 (S)%97 70-130 05/31/14 01:23
4-Bromofluorobenzene (S)%99 70-130 05/31/14 01:23
Toluene-d8 (S)%100 70-130 05/31/14 01:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1210762LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.350 93 70-130
1,1,1-Trichloroethane ug/L 47.250 94 70-130
1,1,2,2-Tetrachloroethane ug/L 48.150 96 70-130
1,1,2-Trichloroethane ug/L 49.650 99 70-130
1,1-Dichloroethane ug/L 44.550 89 70-130
1,1-Dichloroethene ug/L 50.350 101 70-132
1,2,3-Trichloropropane ug/L 50.050 100 70-130
1,2-Dibromo-3-chloropropane ug/L 49.950 100 70-130
1,2-Dibromoethane (EDB)ug/L 48.150 96 70-130
1,2-Dichlorobenzene ug/L 48.450 97 70-130
1,2-Dichloroethane ug/L 47.150 94 70-130
1,2-Dichloropropane ug/L 47.350 95 70-130
1,3-Dichlorobenzene ug/L 47.450 95 70-130
1,3-Dichloropropane ug/L 47.350 95 70-130
1,4-Dichlorobenzene ug/L 46.950 94 70-130
2-Butanone (MEK)ug/L 99.9J100 100 70-145
2-Hexanone ug/L 98.5100 99 70-144
4-Methyl-2-pentanone (MIBK) ug/L 107100 107 70-140
Acetone ug/L 96.9J100 97 50-175
Acrylonitrile ug/L 247250 99 70-143
Benzene ug/L 48.850 98 70-130
Bromochloromethane ug/L 49.050 98 70-130
Bromodichloromethane ug/L 46.350 93 70-130
Bromoform ug/L 48.650 97 70-130
Bromomethane ug/L 46.250 92 54-130
Carbon disulfide ug/L 48.0J50 96 70-131
Carbon tetrachloride ug/L 52.450 105 70-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1210762LABORATORY CONTROL SAMPLE:
LCSSpike
Chlorobenzene ug/L 45.450 91 70-130
Chloroethane ug/L 51.750 103 64-134
Chloroform ug/L 47.150 94 70-130
Chloromethane ug/L 47.750 95 64-130
cis-1,2-Dichloroethene ug/L 47.450 95 70-131
cis-1,3-Dichloropropene ug/L 47.250 94 70-130
Dibromochloromethane ug/L 45.650 91 70-130
Dibromomethane ug/L 48.250 96 70-131
Ethylbenzene ug/L 45.450 91 70-130
Iodomethane ug/L 95.0100 95 49-180
Methylene Chloride ug/L 50.850 102 63-130
Styrene ug/L 48.750 97 70-130
Tetrachloroethene ug/L 49.550 99 70-130
Toluene ug/L 47.850 96 70-130
trans-1,2-Dichloroethene ug/L 48.350 97 70-130
trans-1,3-Dichloropropene ug/L 47.550 95 70-132
trans-1,4-Dichloro-2-butene ug/L 49.6J50 99 70-141
Trichloroethene ug/L 48.050 96 70-130
Trichlorofluoromethane ug/L 55.650 111 62-133
Vinyl acetate ug/L 99.1100 99 66-157
Vinyl chloride ug/L 60.450 121 69-130
Xylene (Total)ug/L 139150 93 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1211546MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203116003
1211547
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 112 70-166121 7 3050ND56.2 60.5
Benzene ug/L 50 103 70-148112 8 30500.42J 52.0 56.3
Chlorobenzene ug/L 50 96 70-146103 7 30500.38J 48.3 51.7
Toluene ug/L 50 97 70-155104 7 3050ND48.5 52.1
Trichloroethene ug/L 50 108 69-151115 7 3050ND54.1 57.7
1,2-Dichloroethane-d4 (S) %99 70-130100
4-Bromofluorobenzene (S) %100 70-130101
Toluene-d8 (S)%101 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27035
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92203121016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1210768
Associated Lab Samples:92203121016
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/14 01:07
1,1,1-Trichloroethane ug/L ND 1.0 05/31/14 01:07
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/14 01:07
1,1,2-Trichloroethane ug/L ND 1.0 05/31/14 01:07
1,1-Dichloroethane ug/L ND 5.0 05/31/14 01:07
1,1-Dichloroethene ug/L ND 5.0 05/31/14 01:07
1,2,3-Trichloropropane ug/L ND 1.0 05/31/14 01:07
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/14 01:07
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/31/14 01:07
1,2-Dichlorobenzene ug/L ND 5.0 05/31/14 01:07
1,2-Dichloroethane ug/L ND 1.0 05/31/14 01:07
1,2-Dichloropropane ug/L ND 1.0 05/31/14 01:07
1,3-Dichloropropane ug/L ND 1.0 05/31/14 01:07
1,4-Dichlorobenzene ug/L ND 1.0 05/31/14 01:07
2-Butanone (MEK)ug/L ND 100 05/31/14 01:07
2-Hexanone ug/L ND 50.0 05/31/14 01:07
4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/31/14 01:07
Acetone ug/L ND 100 05/31/14 01:07
Acrylonitrile ug/L ND 200 05/31/14 01:07
Benzene ug/L ND 1.0 05/31/14 01:07
Bromochloromethane ug/L ND 3.0 05/31/14 01:07
Bromodichloromethane ug/L ND 1.0 05/31/14 01:07
Bromoform ug/L ND 3.0 05/31/14 01:07
Bromomethane ug/L ND 10.0 05/31/14 01:07
Carbon disulfide ug/L ND 100 05/31/14 01:07
Carbon tetrachloride ug/L ND 1.0 05/31/14 01:07
Chlorobenzene ug/L ND 3.0 05/31/14 01:07
Chloroethane ug/L ND 10.0 05/31/14 01:07
Chloroform ug/L ND 5.0 05/31/14 01:07
Chloromethane ug/L ND 1.0 05/31/14 01:07
cis-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:07
cis-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:07
Dibromochloromethane ug/L ND 3.0 05/31/14 01:07
Dibromomethane ug/L ND 10.0 05/31/14 01:07
Ethylbenzene ug/L ND 1.0 05/31/14 01:07
Iodomethane ug/L ND 10.0 05/31/14 01:07
Methylene Chloride ug/L ND 1.0 05/31/14 01:07
Styrene ug/L ND 1.0 05/31/14 01:07
Tetrachloroethene ug/L ND 1.0 05/31/14 01:07
Toluene ug/L ND 1.0 05/31/14 01:07
trans-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1210768
Associated Lab Samples:92203121016
Matrix: Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:07
trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/14 01:07
Trichloroethene ug/L ND 1.0 05/31/14 01:07
Trichlorofluoromethane ug/L ND 1.0 05/31/14 01:07
Vinyl acetate ug/L ND 50.0 05/31/14 01:07
Vinyl chloride ug/L ND 1.0 05/31/14 01:07
Xylene (Total)ug/L ND 5.0 05/31/14 01:07
1,2-Dichloroethane-d4 (S)%98 70-130 05/31/14 01:07
4-Bromofluorobenzene (S)%99 70-130 05/31/14 01:07
Toluene-d8 (S)%99 70-130 05/31/14 01:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1210769LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.250 94 70-130
1,1,1-Trichloroethane ug/L 48.650 97 70-130
1,1,2,2-Tetrachloroethane ug/L 46.250 92 70-130
1,1,2-Trichloroethane ug/L 48.150 96 70-130
1,1-Dichloroethane ug/L 46.050 92 70-130
1,1-Dichloroethene ug/L 52.650 105 70-132
1,2,3-Trichloropropane ug/L 48.150 96 70-130
1,2-Dibromo-3-chloropropane ug/L 48.750 97 70-130
1,2-Dibromoethane (EDB)ug/L 47.650 95 70-130
1,2-Dichlorobenzene ug/L 49.050 98 70-130
1,2-Dichloroethane ug/L 48.050 96 70-130
1,2-Dichloropropane ug/L 47.950 96 70-130
1,3-Dichloropropane ug/L 47.250 94 70-130
1,4-Dichlorobenzene ug/L 47.750 95 70-130
2-Butanone (MEK)ug/L 93.1J100 93 70-145
2-Hexanone ug/L 90.0100 90 70-144
4-Methyl-2-pentanone (MIBK) ug/L 96.8J100 97 70-140
Acetone ug/L 92.8J100 93 50-175
Acrylonitrile ug/L 238250 95 70-143
Benzene ug/L 50.050 100 70-130
Bromochloromethane ug/L 49.550 99 70-130
Bromodichloromethane ug/L 47.250 94 70-130
Bromoform ug/L 47.650 95 70-130
Bromomethane ug/L 45.850 92 54-130
Carbon disulfide ug/L 49.6J50 99 70-131
Carbon tetrachloride ug/L 54.650 109 70-132
Chlorobenzene ug/L 46.150 92 70-130
Chloroethane ug/L 53.350 107 64-134
Chloroform ug/L 46.650 93 70-130
Chloromethane ug/L 49.350 99 64-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1210769LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.250 96 70-131
cis-1,3-Dichloropropene ug/L 47.550 95 70-130
Dibromochloromethane ug/L 45.950 92 70-130
Dibromomethane ug/L 47.950 96 70-131
Ethylbenzene ug/L 46.550 93 70-130
Iodomethane ug/L 92.1100 92 49-180
Methylene Chloride ug/L 50.350 101 63-130
Styrene ug/L 49.050 98 70-130
Tetrachloroethene ug/L 50.650 101 70-130
Toluene ug/L 48.450 97 70-130
trans-1,2-Dichloroethene ug/L 50.350 101 70-130
trans-1,3-Dichloropropene ug/L 46.650 93 70-132
trans-1,4-Dichloro-2-butene ug/L 45.9J50 92 70-141
Trichloroethene ug/L 49.750 99 70-130
Trichlorofluoromethane ug/L 59.150 118 62-133
Vinyl acetate ug/L 96.7100 97 66-157
Vinyl chloride ug/L 62.650 125 69-130
Xylene (Total)ug/L 141150 94 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1211548MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121016
1211549
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 119 70-166143 19 3050ND59.4 71.6
Benzene ug/L 50 109 70-148134 21 30500.42J 54.7 67.4
Chlorobenzene ug/L 50 100 70-146124 20 30500.97J 51.1 62.7
Toluene ug/L 50 102 70-155125 20 3050ND50.8 62.4
Trichloroethene ug/L 50 113 69-151138 20 3050ND56.4 69.1
1,2-Dichloroethane-d4 (S) %100 70-130100
4-Bromofluorobenzene (S) %100 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/31334
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1212368
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010
Matrix: Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 06/03/14 11:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1212369LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4760050000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203313010
1212371
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500007075-12570 0 2050000163
mg/L 198000 198000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212372MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121008
1212373
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 94 75-12592 1 20500003450081400 80400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/31323
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1211984
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008
Matrix: Water
Analyzed
Sulfide ug/L ND 1000 06/03/14 15:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211985LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 508J500 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1211988MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203023007
1211989
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15006275-12562 0 20500ND309J 309J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212570MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203023002
1212571
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 97 75-12597 0 20500ND484J 484J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/31324
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples: 92203121009, 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1211998
Associated Lab Samples:92203121009, 92203121010
Matrix: Water
Analyzed
Sulfide ug/L ND 1000 06/03/14 15:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211999LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 512J500 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212002MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203346002
1212003
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 99 75-12599 0 20500ND493J 493J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212481MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203313004
1212482
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 77 75-12577 0 20500ND385J 385J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19162
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples: 92203121005, 92203121006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1210885
Associated Lab Samples:92203121005, 92203121006
Matrix: Water
Analyzed
Sulfate ug/L ND 250000 06/03/14 01:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1210886LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19100J20000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1210887MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203023012
1210888
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M6200007390-11044 6 20200008520099900J 93900J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1210889MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203263009
1210890
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M12000012590-110123 1 202000013.2
mg/L 38200J 37800J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19211
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples: 92203121007, 92203121008, 92203121009, 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1214099
Associated Lab Samples:92203121007, 92203121008, 92203121009, 92203121010
Matrix: Water
Analyzed
Sulfate ug/L ND 250000 06/05/14 18:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1214100LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19200J20000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1214101MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203770001
1214102
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M62000062390-110646 0 20200002030
mg/L
2150000
J
2160000
J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1214103MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203346005
1214104
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 103 90-110103 0 20200007.8
mg/L 28300J 28400J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19280
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1219158
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008, 92203121009
Matrix: Water
Analyzed
Chloride ug/L ND 1000 06/11/14 17:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219159LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2050020000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219160MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203236001
1219161
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 20000 93 75-12592 0 20200002.2
mg/L 20800 20700
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219162MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203313012
1219163
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M1200005075-12551 0 202000036.7
mg/L 46700 46900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19281
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples: 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1219164
Associated Lab Samples:92203121010
Matrix: Water
Analyzed
Chloride ug/L ND 1000 06/11/14 18:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219165LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2040020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219166MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121010
1219167
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 20000 95 75-12596 0 2020000271021800 21900
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219168MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203397002
1219169
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 20000 99 75-12597 1 202000017.7
mg/L 37600 37100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19243
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples: 92203121017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1216407
Associated Lab Samples:92203121017
Matrix: Water
Analyzed
Cyanide ug/L ND 10.0 06/09/14 10:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1216408LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 107100 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216409MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203836001
1216410
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 108 75-125110 1 20100ND110 112
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216411MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203023009
1216412
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 110 75-125108 1 20100ND111 109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19244
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121015, 92203121016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1216413
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008, 92203121015, 92203121016
Matrix: Water
Analyzed
Cyanide ug/L ND 10.0 06/09/14 10:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1216414LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 110100 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216415MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203313004
1216416
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L R110010675-12586 21 20100ND108 87.2
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216417MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121007
1216418
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 87 75-12588 1 20100ND89.6 90.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19250
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1216637
Associated Lab Samples:92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010
Matrix: Water
Analyzed
Chemical Oxygen Demand ug/L ND 25000 06/10/14 13:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1216638LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 745000750000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216639MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204031002
1216640
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 102 75-125102 0 2075000076.0
mg/L 841000 843000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216641MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121008
1216642
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 97 75-12597 0 20750000ND728000 731000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19200
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples: 92203121005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1213002
Associated Lab Samples:92203121005
Matrix: Water
Analyzed
Total Organic Carbon ug/L ND 1000 06/05/14 14:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1213003LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2460025000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1213004MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203708001
1213005
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 107 75-125107 0 20250002.0
mg/L 28700 28700
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1213006MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203155012
1213007
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 97 75-12597 0 20250002.4
mg/L 26800 26800
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19212
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples: 92203121006, 92203121007, 92203121008, 92203121009, 92203121010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1214105
Associated Lab Samples:92203121006, 92203121007, 92203121008, 92203121009, 92203121010
Matrix: Water
Analyzed
Total Organic Carbon ug/L ND 1000 06/05/14 20:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1214106LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2480025000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1214107MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203814001
1214108
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 99 75-12599 0 2025000ND24800 24800
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1214109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121006
1214110
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250007375-12573 0 20250001390032100 32000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 73
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 73
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92203121001 MPRP/16067 ICP/14532MW-12S EPA 3010 EPA 6010
92203121002 MPRP/16067 ICP/14532MW-18 EPA 3010 EPA 6010
92203121003 MPRP/16067 ICP/14532MW-19 EPA 3010 EPA 6010
92203121004 MPRP/16067 ICP/14532MW-23 EPA 3010 EPA 6010
92203121005 MPRP/16107 ICP/14568MW-1 EPA 3010 EPA 6010
92203121006 MPRP/16107 ICP/14568MW-7 EPA 3010 EPA 6010
92203121007 MPRP/16107 ICP/14568MW-15 EPA 3010 EPA 6010
92203121008 MPRP/16107 ICP/14568MW-21 EPA 3010 EPA 6010
92203121009 MPRP/16107 ICP/14568MW-9 EPA 3010 EPA 6010
92203121010 MPRP/16107 ICP/14568MW-14 EPA 3010 EPA 6010
92203121011 MPRP/16107 ICP/14568MW-3R EPA 3010 EPA 6010
92203121012 MPRP/16107 ICP/14568MW-13 EPA 3010 EPA 6010
92203121013 MPRP/16107 ICP/14568MW-17 EPA 3010 EPA 6010
92203121014 MPRP/16107 ICP/14568MW-20 EPA 3010 EPA 6010
92203121015 MPRP/16107 ICP/14568MW-16 EPA 3010 EPA 6010
92203121016 MPRP/16107 ICP/14568MW-22 EPA 3010 EPA 6010
92203121010 MERP/6689 MERC/6449MW-14 EPA 7470 EPA 7470
92203121001 MSV/26995MW-12S EPA 8260
92203121002 MSV/26995MW-18 EPA 8260
92203121003 MSV/26995MW-19 EPA 8260
92203121004 MSV/26995MW-23 EPA 8260
92203121005 MSV/27034MW-1 EPA 8260
92203121006 MSV/27034MW-7 EPA 8260
92203121007 MSV/27034MW-15 EPA 8260
92203121008 MSV/27034MW-21 EPA 8260
92203121009 MSV/27034MW-9 EPA 8260
92203121010 MSV/27034MW-14 EPA 8260
92203121011 MSV/27034MW-3R EPA 8260
92203121012 MSV/27034MW-13 EPA 8260
92203121013 MSV/27034MW-17 EPA 8260
92203121014 MSV/27034MW-20 EPA 8260
92203121015 MSV/27034MW-16 EPA 8260
92203121016 MSV/27035MW-22 EPA 8260
92203121005 WET/31334MW-1 SM 2320B
92203121006 WET/31334MW-7 SM 2320B
92203121007 WET/31334MW-15 SM 2320B
92203121008 WET/31334MW-21 SM 2320B
92203121009 WET/31334MW-9 SM 2320B
92203121010 WET/31334MW-14 SM 2320B
92203121005 WET/31323MW-1 SM 4500-S2D
92203121006 WET/31323MW-7 SM 4500-S2D
92203121007 WET/31323MW-15 SM 4500-S2D
92203121008 WET/31323MW-21 SM 4500-S2D
92203121009 WET/31324MW-9 SM 4500-S2D
92203121010 WET/31324MW-14 SM 4500-S2D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
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Page 67 of 73
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92203121
Surry Closed-Mt. Airy (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92203121005 WETA/19162MW-1 EPA 300.0
92203121006 WETA/19162MW-7 EPA 300.0
92203121007 WETA/19211MW-15 EPA 300.0
92203121008 WETA/19211MW-21 EPA 300.0
92203121009 WETA/19211MW-9 EPA 300.0
92203121010 WETA/19211MW-14 EPA 300.0
92203121005 WETA/19280MW-1 SM 4500-Cl-E
92203121006 WETA/19280MW-7 SM 4500-Cl-E
92203121007 WETA/19280MW-15 SM 4500-Cl-E
92203121008 WETA/19280MW-21 SM 4500-Cl-E
92203121009 WETA/19280MW-9 SM 4500-Cl-E
92203121010 WETA/19281MW-14 SM 4500-Cl-E
92203121005 WETA/19244MW-1 SM 4500-CN-E
92203121006 WETA/19244MW-7 SM 4500-CN-E
92203121007 WETA/19244MW-15 SM 4500-CN-E
92203121008 WETA/19244MW-21 SM 4500-CN-E
92203121015 WETA/19244MW-16 SM 4500-CN-E
92203121016 WETA/19244MW-22 SM 4500-CN-E
92203121017 WETA/19243MW-19 SM 4500-CN-E
92203121005 WETA/19250MW-1 SM 5220D
92203121006 WETA/19250MW-7 SM 5220D
92203121007 WETA/19250MW-15 SM 5220D
92203121008 WETA/19250MW-21 SM 5220D
92203121009 WETA/19250MW-9 SM 5220D
92203121010 WETA/19250MW-14 SM 5220D
92203121005 WETA/19200MW-1 SM 5310B
92203121006 WETA/19212MW-7 SM 5310B
92203121007 WETA/19212MW-15 SM 5310B
92203121008 WETA/19212MW-21 SM 5310B
92203121009 WETA/19212MW-9 SM 5310B
92203121010 WETA/19212MW-14 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2014 08:20 AM
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[phone]
Page 68 of 73
Page 69 of 73
Page 70 of 73
Page 71 of 73
Page 72 of 73
Page 73 of 73
#=CL#
June 10, 2014
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92203466
92203466
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92203466
SURRY BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92203466001 EB Water 05/29/14 14:20 05/29/14 15:20
92203466002 FB Water 05/29/14 14:30 05/29/14 15:20
92203466003 TB Water 05/29/14 00:00 05/29/14 15:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92203466
SURRY BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92203466001 EB EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 51 PASI-CGAW
SM 4500-S2D 1 PASI-ASAE
SM 4500-CN-E 1 PASI-AJDA
92203466002 FB EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 51 PASI-CGAW
92203466003 TB EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Sample: EB Lab ID: 92203466001 Collected: 05/29/14 14:20 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:56 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:56 7440-38-206/03/14 12:3010.0 5.0 1
Barium ND ug/L 06/04/14 20:56 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:56 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:56 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:56 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt ND ug/L 06/04/14 20:56 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:56 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:56 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:56 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:56 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:56 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:56 7440-28-006/03/14 12:305.5 5.4 1
Tin ND ug/L 06/04/14 20:56 7440-31-506/03/14 12:30100 5.0 1
Vanadium ND ug/L 06/04/14 20:56 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:56 7440-66-606/03/14 12:3010.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 06/03/14 19:05 7439-97-606/02/14 19:450.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 06/01/14 18:14 67-64-1100 10.0 1
Acrylonitrile ND ug/L 06/01/14 18:14 107-13-1200 1.9 1
Benzene ND ug/L 06/01/14 18:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/01/14 18:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/01/14 18:14 75-27-41.0 0.18 1
Bromoform ND ug/L 06/01/14 18:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/01/14 18:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/01/14 18:14 78-93-3100 0.96 1
Carbon disulfide ND ug/L 06/01/14 18:14 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 06/01/14 18:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/01/14 18:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/01/14 18:14 75-00-310.0 0.54 1
Chloroform ND ug/L 06/01/14 18:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/01/14 18:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/01/14 18:14 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 06/01/14 18:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/01/14 18:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/01/14 18:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/01/14 18:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/01/14 18:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/01/14 18:14 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 06/01/14 18:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/01/14 18:14 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/01/14 18:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/01/14 18:14 156-59-25.0 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
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Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Sample: EB Lab ID: 92203466001 Collected: 05/29/14 14:20 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,2-Dichloroethene ND ug/L 06/01/14 18:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/01/14 18:14 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/01/14 18:14 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/01/14 18:14 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/01/14 18:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/01/14 18:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/01/14 18:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/01/14 18:14 74-88-410.0 0.32 1
Methylene Chloride 1.0 ug/L 06/01/14 18:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/01/14 18:14 108-10-1100 0.33 1
Styrene ND ug/L 06/01/14 18:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/01/14 18:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/01/14 18:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/01/14 18:14 127-18-41.0 0.46 1
Toluene ND ug/L 06/01/14 18:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/01/14 18:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/01/14 18:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/01/14 18:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/01/14 18:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/01/14 18:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/01/14 18:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/01/14 18:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/01/14 18:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/01/14 18:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/01/14 18:14 17060-07-070-130 1
Toluene-d8 (S)97 %06/01/14 18:14 2037-26-570-130 1
4500S2D Sulfide Water Analytical Method: SM 4500-S2D
Sulfide ND ug/L 06/04/14 13:25 18496-25-81000 100 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND ug/L 06/09/14 11:31 57-12-510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
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9800 Kincey Ave. Suite 100
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Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Sample: FB Lab ID: 92203466002 Collected: 05/29/14 14:30 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 06/04/14 20:59 7440-36-006/03/14 12:306.0 5.0 1
Arsenic ND ug/L 06/04/14 20:59 7440-38-206/03/14 12:3010.0 5.0 1
Barium ND ug/L 06/04/14 20:59 7440-39-306/03/14 12:30100 5.0 1
Beryllium ND ug/L 06/04/14 20:59 7440-41-706/03/14 12:301.0 1.0 1
Cadmium ND ug/L 06/04/14 20:59 7440-43-906/03/14 12:301.0 1.0 1
Chromium ND ug/L 06/04/14 20:59 7440-47-306/03/14 12:3010.0 5.0 1
Cobalt ND ug/L 06/04/14 20:59 7440-48-406/03/14 12:3010.0 5.0 1
Copper ND ug/L 06/04/14 20:59 7440-50-806/03/14 12:3010.0 5.0 1
Lead ND ug/L 06/04/14 20:59 7439-92-106/03/14 12:3010.0 5.0 1
Nickel ND ug/L 06/04/14 20:59 7440-02-006/03/14 12:3050.0 5.0 1
Selenium ND ug/L 06/04/14 20:59 7782-49-206/03/14 12:3010.0 10.0 1
Silver ND ug/L 06/04/14 20:59 7440-22-406/03/14 12:3010.0 5.0 1
Thallium ND ug/L 06/04/14 20:59 7440-28-006/03/14 12:305.5 5.4 1
Tin ND ug/L 06/04/14 20:59 7440-31-506/03/14 12:30100 5.0 1
Vanadium ND ug/L 06/04/14 20:59 7440-62-206/03/14 12:3025.0 5.0 1
Zinc ND ug/L 06/04/14 20:59 7440-66-606/03/14 12:3010.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 06/03/14 19:08 7439-97-606/02/14 19:450.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 06/01/14 18:30 67-64-1100 10.0 1
Acrylonitrile ND ug/L 06/01/14 18:30 107-13-1200 1.9 1
Benzene ND ug/L 06/01/14 18:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/01/14 18:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/01/14 18:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/01/14 18:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/01/14 18:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/01/14 18:30 78-93-3100 0.96 1
Carbon disulfide ND ug/L 06/01/14 18:30 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 06/01/14 18:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/01/14 18:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/01/14 18:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/01/14 18:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/01/14 18:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/01/14 18:30 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 06/01/14 18:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/01/14 18:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/01/14 18:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/01/14 18:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/01/14 18:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/01/14 18:30 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 06/01/14 18:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/01/14 18:30 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/01/14 18:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/01/14 18:30 156-59-25.0 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Sample: FB Lab ID: 92203466002 Collected: 05/29/14 14:30 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,2-Dichloroethene ND ug/L 06/01/14 18:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/01/14 18:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/01/14 18:30 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/01/14 18:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/01/14 18:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/01/14 18:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/01/14 18:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/01/14 18:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/01/14 18:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/01/14 18:30 108-10-1100 0.33 1
Styrene ND ug/L 06/01/14 18:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/01/14 18:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/01/14 18:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/01/14 18:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/01/14 18:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/01/14 18:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/01/14 18:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/01/14 18:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/01/14 18:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/01/14 18:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/01/14 18:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/01/14 18:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/01/14 18:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/01/14 18:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %06/01/14 18:30 17060-07-070-130 1
Toluene-d8 (S)97 %06/01/14 18:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
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[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Sample: TB Lab ID: 92203466003 Collected: 05/29/14 00:00 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 06/01/14 18:46 67-64-1100 10.0 1
Acrylonitrile ND ug/L 06/01/14 18:46 107-13-1200 1.9 1
Benzene ND ug/L 06/01/14 18:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/01/14 18:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/01/14 18:46 75-27-41.0 0.18 1
Bromoform ND ug/L 06/01/14 18:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/01/14 18:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/01/14 18:46 78-93-3100 0.96 1
Carbon disulfide ND ug/L 06/01/14 18:46 75-15-0100 1.2 1
Carbon tetrachloride ND ug/L 06/01/14 18:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/01/14 18:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/01/14 18:46 75-00-310.0 0.54 1
Chloroform ND ug/L 06/01/14 18:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/01/14 18:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/01/14 18:46 96-12-813.0 2.5 1
Dibromochloromethane ND ug/L 06/01/14 18:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/01/14 18:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/01/14 18:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/01/14 18:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/01/14 18:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/01/14 18:46 110-57-6100 1.0 1
1,1-Dichloroethane ND ug/L 06/01/14 18:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/01/14 18:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/01/14 18:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/01/14 18:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/01/14 18:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/01/14 18:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/01/14 18:46 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/01/14 18:46 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/01/14 18:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/01/14 18:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/01/14 18:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/01/14 18:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/01/14 18:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/01/14 18:46 108-10-1100 0.33 1
Styrene ND ug/L 06/01/14 18:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/01/14 18:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/01/14 18:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/01/14 18:46 127-18-41.0 0.46 1
Toluene ND ug/L 06/01/14 18:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/01/14 18:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/01/14 18:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/01/14 18:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/01/14 18:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/01/14 18:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/01/14 18:46 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
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Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203466
SURRY BLANKS
Sample: TB Lab ID: 92203466003 Collected: 05/29/14 00:00 Received: 05/29/14 15:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Vinyl chloride ND ug/L 06/01/14 18:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/01/14 18:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %06/01/14 18:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %06/01/14 18:46 17060-07-070-130 1
Toluene-d8 (S)97 %06/01/14 18:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6689
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples: 92203466001, 92203466002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1212169
Associated Lab Samples:92203466001, 92203466002
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 06/03/14 18:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1212170LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.72.5 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212171MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203121010
1212172
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 101 75-125100 0 252.50.14J 2.7 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16107
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples: 92203466001, 92203466002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1212519
Associated Lab Samples:92203466001, 92203466002
Matrix: Water
Analyzed
Antimony ug/L ND 6.0 06/04/14 19:28
Arsenic ug/L ND 10.0 06/04/14 19:28
Barium ug/L ND 100 06/04/14 19:28
Beryllium ug/L ND 1.0 06/04/14 19:28
Cadmium ug/L ND 1.0 06/04/14 19:28
Chromium ug/L ND 10.0 06/04/14 19:28
Cobalt ug/L ND 10.0 06/04/14 19:28
Copper ug/L ND 10.0 06/04/14 19:28
Lead ug/L ND 10.0 06/04/14 19:28
Nickel ug/L ND 50.0 06/04/14 19:28
Selenium ug/L ND 10.0 06/04/14 19:28
Silver ug/L ND 10.0 06/04/14 19:28
Thallium ug/L ND 5.5 06/04/14 19:28
Tin ug/L ND 100 06/04/14 19:28
Vanadium ug/L ND 25.0 06/04/14 19:28
Zinc ug/L ND 10.0 06/04/14 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1212520LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 497500 99 80-120
Arsenic ug/L 477500 95 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 479500 96 80-120
Cadmium ug/L 480500 96 80-120
Chromium ug/L 486500 97 80-120
Cobalt ug/L 495500 99 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 497500 99 80-120
Nickel ug/L 478500 96 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 242250 97 80-120
Thallium ug/L 469500 94 80-120
Tin ug/L 496500 99 80-120
Vanadium ug/L 480500 96 80-120
Zinc ug/L 478500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212521MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203332001
1212522
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 95 75-12597 2 25500ND474 483
Arsenic ug/L 500 91 75-12594 3 25500ND456 468
Barium ug/L 500 94 75-12598 4 2550022.5J 490 511
Beryllium ug/L 500 91 75-12594 4 25500ND454 471
Cadmium ug/L 500 91 75-12593 2 25500ND456 467
Chromium ug/L 500 92 75-12595 3 25500ND462 476
Cobalt ug/L 500 93 75-12596 3 25500ND464 480
Copper ug/L 500 95 75-12596 1 25500ND475 480
Lead ug/L 500 93 75-12596 3 25500ND465 478
Nickel ug/L 500 91 75-12593 3 25500ND453 467
Selenium ug/L 500 93 75-12596 2 25500ND467 479
Silver ug/L 250 91 75-12594 3 25250ND229 235
Thallium ug/L 500 89 75-12592 3 25500ND446 459
Tin ug/L 500 93 75-12596 3 25500ND468 481
Vanadium ug/L 500 91 75-12594 3 25500ND457 472
Zinc ug/L 500 91 75-12593 2 25500ND457 467
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27045
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92203466001, 92203466002, 92203466003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1211358
Associated Lab Samples:92203466001, 92203466002, 92203466003
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/01/14 13:23
1,1,1-Trichloroethane ug/L ND 1.0 06/01/14 13:23
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/01/14 13:23
1,1,2-Trichloroethane ug/L ND 1.0 06/01/14 13:23
1,1-Dichloroethane ug/L ND 5.0 06/01/14 13:23
1,1-Dichloroethene ug/L ND 5.0 06/01/14 13:23
1,2,3-Trichloropropane ug/L ND 1.0 06/01/14 13:23
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/01/14 13:23
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/01/14 13:23
1,2-Dichlorobenzene ug/L ND 5.0 06/01/14 13:23
1,2-Dichloroethane ug/L ND 1.0 06/01/14 13:23
1,2-Dichloropropane ug/L ND 1.0 06/01/14 13:23
1,3-Dichloropropane ug/L ND 1.0 06/01/14 13:23
1,4-Dichlorobenzene ug/L ND 1.0 06/01/14 13:23
2-Butanone (MEK)ug/L ND 100 06/01/14 13:23
2-Hexanone ug/L ND 50.0 06/01/14 13:23
4-Methyl-2-pentanone (MIBK) ug/L ND 100 06/01/14 13:23
Acetone ug/L ND 100 06/01/14 13:23
Acrylonitrile ug/L ND 200 06/01/14 13:23
Benzene ug/L ND 1.0 06/01/14 13:23
Bromochloromethane ug/L ND 3.0 06/01/14 13:23
Bromodichloromethane ug/L ND 1.0 06/01/14 13:23
Bromoform ug/L ND 3.0 06/01/14 13:23
Bromomethane ug/L ND 10.0 06/01/14 13:23
Carbon disulfide ug/L ND 100 06/01/14 13:23
Carbon tetrachloride ug/L ND 1.0 06/01/14 13:23
Chlorobenzene ug/L ND 3.0 06/01/14 13:23
Chloroethane ug/L ND 10.0 06/01/14 13:23
Chloroform ug/L ND 5.0 06/01/14 13:23
Chloromethane ug/L ND 1.0 06/01/14 13:23
cis-1,2-Dichloroethene ug/L ND 5.0 06/01/14 13:23
cis-1,3-Dichloropropene ug/L ND 1.0 06/01/14 13:23
Dibromochloromethane ug/L ND 3.0 06/01/14 13:23
Dibromomethane ug/L ND 10.0 06/01/14 13:23
Ethylbenzene ug/L ND 1.0 06/01/14 13:23
Iodomethane ug/L ND 10.0 06/01/14 13:23
Methylene Chloride ug/L ND 1.0 06/01/14 13:23
Styrene ug/L ND 1.0 06/01/14 13:23
Tetrachloroethene ug/L ND 1.0 06/01/14 13:23
Toluene ug/L ND 1.0 06/01/14 13:23
trans-1,2-Dichloroethene ug/L ND 5.0 06/01/14 13:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1211358
Associated Lab Samples:92203466001, 92203466002, 92203466003
Matrix: Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 06/01/14 13:23
trans-1,4-Dichloro-2-butene ug/L ND 100 06/01/14 13:23
Trichloroethene ug/L ND 1.0 06/01/14 13:23
Trichlorofluoromethane ug/L ND 1.0 06/01/14 13:23
Vinyl acetate ug/L ND 50.0 06/01/14 13:23
Vinyl chloride ug/L ND 1.0 06/01/14 13:23
Xylene (Total)ug/L ND 5.0 06/01/14 13:23
1,2-Dichloroethane-d4 (S)%99 70-130 06/01/14 13:23
4-Bromofluorobenzene (S)%101 70-130 06/01/14 13:23
Toluene-d8 (S)%96 70-130 06/01/14 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211359LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 59.350 119 70-130
1,1,1-Trichloroethane ug/L 53.550 107 70-130
1,1,2,2-Tetrachloroethane ug/L 53.750 107 70-130
1,1,2-Trichloroethane ug/L 54.350 109 70-130
1,1-Dichloroethane ug/L 49.450 99 70-130
1,1-Dichloroethene ug/L 49.450 99 70-132
1,2,3-Trichloropropane ug/L 53.250 106 70-130
1,2-Dibromo-3-chloropropane ug/L 48.450 97 70-130
1,2-Dibromoethane (EDB)ug/L 54.650 109 70-130
1,2-Dichlorobenzene ug/L 53.650 107 70-130
1,2-Dichloroethane ug/L 54.850 110 70-130
1,2-Dichloropropane ug/L 51.750 103 70-130
1,3-Dichloropropane ug/L 53.050 106 70-130
1,4-Dichlorobenzene ug/L 52.650 105 70-130
2-Butanone (MEK)ug/L 89.3J100 89 70-145
2-Hexanone ug/L 99.7100 100 70-144
4-Methyl-2-pentanone (MIBK) ug/L 99.1J100 99 70-140
Acetone ug/L 95.5J100 96 50-175
Acrylonitrile ug/L 250250 100 70-143
Benzene ug/L 55.150 110 70-130
Bromochloromethane ug/L 54.450 109 70-130
Bromodichloromethane ug/L 56.450 113 70-130
Bromoform ug/L 53.150 106 70-130
Bromomethane ug/L 54.250 108 54-130
Carbon disulfide ug/L 50.9J50 102 70-131
Carbon tetrachloride ug/L 56.950 114 70-132
Chlorobenzene ug/L 51.450 103 70-130
Chloroethane ug/L 40.950 82 64-134
Chloroform ug/L 52.350 105 70-130
Chloromethane ug/L 48.650 97 64-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
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[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211359LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 49.950 100 70-131
cis-1,3-Dichloropropene ug/L 55.650 111 70-130
Dibromochloromethane ug/L 51.350 103 70-130
Dibromomethane ug/L 54.450 109 70-131
Ethylbenzene ug/L 50.050 100 70-130
Iodomethane ug/L 120100 120 49-180
Methylene Chloride ug/L 52.450 105 63-130
Styrene ug/L 54.150 108 70-130
Tetrachloroethene ug/L 54.750 109 70-130
Toluene ug/L 51.650 103 70-130
trans-1,2-Dichloroethene ug/L 50.550 101 70-130
trans-1,3-Dichloropropene ug/L 55.450 111 70-132
trans-1,4-Dichloro-2-butene ug/L 56.7J50 113 70-141
Trichloroethene ug/L 56.850 114 70-130
Trichlorofluoromethane ug/L 48.250 96 62-133
Vinyl acetate ug/L 108100 108 66-157
Vinyl chloride ug/L 57.150 114 69-130
Xylene (Total)ug/L 152150 102 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1211566MATRIX SPIKE SAMPLE:
MSSpike
Result
92203468011
1,1,1,2-Tetrachloroethane ug/L 66.7 M050133 70-130ND
1,1,1-Trichloroethane ug/L 64.750 129 70-130ND
1,1,2,2-Tetrachloroethane ug/L 59.250 118 70-130ND
1,1,2-Trichloroethane ug/L 61.250 122 70-130ND
1,1-Dichloroethane ug/L 58.750 117 70-130ND
1,1-Dichloroethene ug/L 61.350 123 70-166ND
1,2,3-Trichloropropane ug/L 58.950 118 70-130ND
1,2-Dibromo-3-chloropropane ug/L 49.350 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 59.950 120 70-130ND
1,2-Dichlorobenzene ug/L 59.650 119 70-130ND
1,2-Dichloroethane ug/L 64.050 128 70-130ND
1,2-Dichloropropane ug/L 59.550 119 70-130ND
1,3-Dichloropropane ug/L 57.850 116 70-130ND
1,4-Dichlorobenzene ug/L 59.550 119 70-130ND
2-Butanone (MEK)ug/L 98.5J100 99 70-130ND
2-Hexanone ug/L 110100 110 70-130ND
4-Methyl-2-pentanone (MIBK) ug/L 109100 109 70-130ND
Acetone ug/L 105100 103 70-130ND
Acrylonitrile ug/L 284250 114 70-130ND
Benzene ug/L 64.850 130 70-148ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1211566MATRIX SPIKE SAMPLE:
MSSpike
Result
92203468011
Bromochloromethane ug/L 62.550 125 70-130ND
Bromodichloromethane ug/L 64.450 129 70-130ND
Bromoform ug/L 55.850 112 70-130ND
Bromomethane ug/L 65.5 M050131 70-130ND
Carbon disulfide ug/L 60.5J50 121 70-130ND
Carbon tetrachloride ug/L 69.6 M050139 70-130ND
Chlorobenzene ug/L 58.250 116 70-146ND
Chloroethane ug/L 44.450 89 70-130ND
Chloroform ug/L 61.350 123 70-130ND
Chloromethane ug/L 58.150 116 70-130ND
cis-1,2-Dichloroethene ug/L 59.750 119 70-130ND
cis-1,3-Dichloropropene ug/L 61.950 124 70-130ND
Dibromochloromethane ug/L 56.050 112 70-130ND
Dibromomethane ug/L 61.550 123 70-130ND
Ethylbenzene ug/L 57.050 114 70-130ND
Iodomethane ug/L 149 M0100149 70-130ND
Methylene Chloride ug/L 61.450 123 70-130ND
Styrene ug/L 61.350 123 70-130ND
Tetrachloroethene ug/L 63.550 127 70-130ND
Toluene ug/L 60.350 121 70-155ND
trans-1,2-Dichloroethene ug/L 61.450 123 70-130ND
trans-1,3-Dichloropropene ug/L 61.950 124 70-130ND
trans-1,4-Dichloro-2-butene ug/L 61.8J50 124 70-130ND
Trichloroethene ug/L 66.550 133 69-151ND
Trichlorofluoromethane ug/L 63.150 126 70-130ND
Vinyl acetate ug/L 121100 121 70-130ND
Vinyl chloride ug/L 71.7 M050143 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203468012
1211567SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203468012
1211567SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK) ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%102 1103
4-Bromofluorobenzene (S)%100 199
Toluene-d8 (S)%96 096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/31341
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples: 92203466001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1213017
Associated Lab Samples:92203466001
Matrix: Water
Analyzed
Sulfide ug/L ND 1000 06/04/14 13:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1213018LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 516J500 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1213019MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203023014
1213020
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 75-125100 0 20500ND499J 499J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203466
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/19245
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples: 92203466001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1216419
Associated Lab Samples:92203466001
Matrix: Water
Analyzed
Cyanide ug/L ND 10.0 06/09/14 11:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1216420LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 93.4100 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216421MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203385006
1216422
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 92 75-12590 2 20100ND94.1 92.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1216423MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204279003
1216424
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 89 75-12588 1 20100ND90.7 89.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92203466
SURRY BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92203466
SURRY BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92203466001 MPRP/16107 ICP/14568EBEPA 3010 EPA 6010
92203466002 MPRP/16107 ICP/14568FBEPA 3010 EPA 6010
92203466001 MERP/6689 MERC/6449EBEPA 7470 EPA 7470
92203466002 MERP/6689 MERC/6449FBEPA 7470 EPA 7470
92203466001 MSV/27045EBEPA 8260
92203466002 MSV/27045FBEPA 8260
92203466003 MSV/27045TBEPA 8260
92203466001 WET/31341EBSM 4500-S2D
92203466001 WETA/19245EBSM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/10/2014 07:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 24
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