SW_F_8401-MSWLF-1999_03-26-2013_RM_GW.pdf

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TABLE OF CONTENTS
Page

1.0 BACKGROUND INFORMATION ...................................................................................... 1-1
1.1 ACTIVE C&D AND CLOSED MSWLF ..................................................................... 1-2
1.2 SUBTITLE D LINED MSWLF .................................................................................... 1-3
1.3 SAMPLING PLAN ....................................................................................................... 1-4
2.0 ACTIVE C&D AND CLOSED MSWLF .............................................................................. 2-1
2.1 SAMPLING AND CHEMICAL ANALYSES ............................................................. 2-1
2.2 GROUNDWATER AND SURFACE WATER SAMPLING ....................................... 2-1
2.2.1 Groundwater Flow Characteristics .................................................................... 2-1
2.2.2 Indicator Parameters .......................................................................................... 2-1
2.3 RESULTS OF CHEMICAL ANALYSES .................................................................... 2-2
3.0 SUBTITLE D LINED MSWLF ............................................................................................. 3-1
3.1 SAMPLING AND CHEMICAL ANALYSES ............................................................. 3-1
3.2 GROUNDWATER AND SURFACE WATER SAMPLING ....................................... 3-1
3.2.1 Groundwater Flow Characteristics .................................................................... 3-1
3.2.2 Indicator Parameters .......................................................................................... 3-2
3.3 RESULTS OF CHEMICAL ANALYSES .................................................................... 3-2
4.0 SUMMARY AND CONCLUSIONS ..................................................................................... 4-1

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FIGURES

Figure 1 Site Vicinity Map
Figure 2 Groundwater Contour Map – City of Albemarle Landfill

TABLES

Table 1 Summary of Groundwater Data
Table 2 Groundwater Flow Characteristics – Active C&D and Closed MSWLF
Table 3 Field-Tested Parameters – Active C&D and Closed MSWLF
Table 4 Analytical Inorganic Parameters for Groundwater Samples – January 2013
Table 5 Analytical Organic Parameters for Groundwater Samples – January 2013
Table 6 Monitored Natural Attenuation Parameters for Groundwater Samples –
January 2013
Table 7 Analytical Inorganic Parameters for Surface Water Samples – January 2013
Table 8 Groundwater Flow Characteristics – Subtitle D Lined MSWLF
Table 9 Field-Tested Parameters – Subtitle D Lined MSWLF

APPENDICES

Appendix A: Laboratory Report

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1.0 BACKGROUND INFORMATION

The City of Albemarle Landfill (DSWM [Division of Solid Waste Management] Permit #84-01) is
located on Stony Gap Road (SR 1720), in Stanly County, North Carolina (see Figure 1). Prior to
operating as a C&D Landfill, the site formerly operated as an unlined Municipal Solid Waste Landfill
(MSWLF) that consisted of two units. The first unit (Unit #1) was closed prior to October 1991 with a
24-inch final soil cover. The second unit (Unit #2) was closed with an 18-inch thick cohesive soil cap
with a permeability of 10-5 centimeters per second (cm/sec) and an 18-inch thick soil erosive layer prior to
June 1999 in accordance with the Transition Plan. The C&D Landfill is constructed and operating on top
of the Unit #1 MSWLF.

Adjacent to the C&D Landfill, across the unnamed tributary of Jacobs Creek, on the same contiguous
property is the active Subtitle D lined MSWLF. The lined MSWLF is comprised of two contiguous
phases (Phase 1 and 2) which are combined and treated as a single unit for continuity of the reporting to
the SWS. This active MSWLF also operates under DSWM Permit #84-01 and is also reported herein.

As specified within Solid Waste Management Rules as per Title 15A, Subchapter 13B, Rules .1630 -
.1637 of the North Carolina Administrative Code (15A NCAC 13B.1630 - .1637) this report contains
sampling procedures, field measurements, laboratory analytical results, characterization of the
groundwater and surface water, and findings from this sampling event. Tables of the hydrogeologic
properties of the underlying groundwater, field parameters, summary of the analytical results with
detections of those constituents exceeding the North Carolina Groundwater Standards (i.e., 15A NCAC
2L.0202) (NC 2L Groundwater Standards), potentiometric map, and quality assurance/quality control
data, are presented. Additionally the laboratory analytical reports with chains-of-custody (CoC) are
included in Appendix A.

The sampling programs for these two areas (i.e., Active C&D and closed MSWLF; and, the Subtitle D
lined MSWLF) are described in Sections 1.1 and 1.2, respectively. The sampling procedures are
described in Section 1.3.
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1.1 ACTIVE C&D AND CLOSED MSWLF
A groundwater monitoring system for the Active C&D and the closed MSWLF landfill has been installed
in accordance with Solid Waste Management Rules 15A NCAC 13B.1630 - .1637.

The site-specific Sampling and Analysis Plan (SAP) contains a combination of detection, assessment and
corrective action monitoring. Detection monitoring was performed on six monitoring wells (MW-4R,
MW-5R, MW-8D, MW-11, MW-24, and MW-25); one surface water sampling location (SW-7); and,
background monitoring well (MW-1). Corrective action monitoring was performed on six monitoring
wells (MW-2, MW-3, MW-6, MW-7, MW-9, and MW-10). An area downgradient of the Phase 1
Subtitle D lined MSWLF; and, between the unnamed tributary of Jacobs Creek and the Active C&D and
closed MSWLF around the Leachate Lagoon has been under assessment since July 2009. At a meeting
with SWS on July 14, 2009 a subset of monitoring wells were selected for assessment monitoring in this
area. Therefore, assessment monitoring was performed on Monitoring Wells MW-12, MW-13 and MW-
23 around the Leachate Lagoon. These monitoring well locations are shown on Figure 2.

Three surface water sampling locations monitor the unnamed tributary of Jacobs Creek (i.e., SW-1, SW-
6, and SW-7); with SW-1 upstream, SW-6 downstream, and SW-7 is located between these two locations
(i.e., SW-1 and SW-6). Since the unnamed tributary of Jacobs Creek passes between the closed MSWLF
and the Subtitle D lined MSWLF, these three surface water sampling locations are also included for the
SAP for the Subtitle D lined MSWLF (see Section 1.2). A fourth surface water sampling location (SW-5)
monitors surface water runoff from the closed MSWLF before the runoff enters into the unnamed
tributary of Jacobs Creek. These four surface water monitoring locations are shown on Figure 2.

Groundwater and surface water samples have been collected at this site on a semi-annual basis since
1994, in accordance with Solid Waste Management Rule 15A NCAC 13B.1633(b). As a condition of the
water quality monitoring program, semi-annual reports are required to be submitted to the North Carolina
Solid Waste Section (SWS). Shield Engineering, Inc. (Shield) of Charlotte, North Carolina performed
this sampling event on January 14 through 15, 2013 in accordance with the Sampling and Analysis Plan
(SAP) contained in the CAER dated July 1, 2011 for this site; and, the SWS Guidelines for Groundwater,
Soil, and Surface Water Sampling dated April 2008.

SWS Rule 15A NCAC 13B.1634(d)(2) requires that an Appendix I detection exceeding the NC 2L
Groundwater Standards within the groundwater at any of the monitoring wells be followed by re-
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sampling of “all wells of the approved detection monitoring system for the unit for all constituents listed
in the Appendix I and for those constituents in Appendix II that have been detected”. In the vicinity of
the leachate lagoon Appendix II sampling has been previously performed at Monitoring Wells MW-12,
MW-13, and MW-23. Hence, for this sampling event Appendix II sampling was again completed in these
three monitoring wells and reported to the SWS herein. Appendix I sampling was completed for the
remaining monitoring wells at this site.
1.2 SUBTITLE D LINED MSWLF
A groundwater monitoring system for the Subtitle D lined MSWLF landfill has been installed in
accordance with Solid Waste Management Rules as per Rules .1630 - .1637 of the North Carolina
Administrative Code (15A NCAC 13B.1630 - .1637).

Based on both the site-specific SAP and interaction with the SWS the water quality monitoring program
for this site consists of detection monitoring. Detection monitoring was performed on nine monitoring
wells (MW-14, MW-15, MW-16S, MW-16D, MW-17, MW-18, MW-22, MW-26, and MW-27); four
surface water sampling locations (SW-1, SW-2, SW-6, and SW-7); background monitoring well (MW-
19); and, a leachate sample (LEACHATE) from the collection lagoon.

The three surface water sampling locations that monitor the unnamed tributary of Jacobs Creek (i.e., SW-
1, SW-6, and SW-7) are located between the closed MSWLF (see Section 1.1) and the Subtitle D lined
MSWLF. Hence, these three surface water sampling locations are also included for the SAP for the
Subtitle D lined MSWLF. A fourth surface water sampling location (SW-2) monitors surface water
runoff in a drainage feature south from the Subtitle D lined MSWLF before the runoff enters into the
unnamed tributary of Jacobs Creek. These four surface water monitoring locations are shown on Figure
2.

Groundwater and surface water samples have been collected at this site on a semi-annual basis since this
MSWLF commenced operations in 1999. The groundwater and surface water sampling has been
conducted in accordance with Solid Waste Management Rule .1633(b) [15A NCAC 13B.1633(b)]. As a
condition of the water quality monitoring program, semi-annual reports are required to be submitted to
the North Carolina Solid Waste Section (SWS). Shield Engineering, Inc. (Shield) of Charlotte, North
Carolina performed this sampling event on January 16 through 17, 2013 in accordance with the Sampling
and Analysis Plan dated March 2, 2009 for this site; and, the SWS Guidelines for Groundwater, Soil, and
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Surface Water Sampling dated April 2008.
1.3 SAMPLING PLAN
Prior to the initiation of the data collection during this sampling event the function and integrity of each
of the monitoring locations was visually evaluated and inspected. Subsequently, the depth-to-
groundwater measurements were collected using an electronic water level meter at each of the monitoring
wells prior to the purging of the groundwater from the monitoring wells. Additionally, the dissolved
oxygen (DO) was measured in the monitoring well prior to the initiation of the well purging. The purging
of each of the monitoring wells was carried out using bailing with clean Teflon bailers. The well purging
was completed for a minimum of three well volumes or until the well was dry. During the well purging
field parameters of pH, specific conductivity, temperature, and oxidation-reduction potential (ORP) were
recorded for each monitoring well.

Shield personnel performed this sampling event utilizing portable monitoring methodology. Monitoring
locations were designated in the approved SAPs for both sites. Groundwater sampling and analysis were
performed at each of the two City of Albemarle sites in general accordance with the respective SAPs for
these sites, and other appropriate documents and agreements. The first 2013 semi-annual sampling event
for these two sites was performed in January 2013. The results of this sampling event are reported herein.

The samples were placed into laboratory prepared pre-preserved containers using a Teflon bailer.
Samples were collected based on likelihood of potential cross-contamination, kept on ice, and transported
to a North Carolina certified laboratory using proper Chain-of-Custody protocol within the specified hold
times for each of the required analyses.

The sampling was attempted at the Active C&D and closed MSWLF for the following:
 Appendix I list constituents and turbidity for Monitoring Wells MW-1, MW-2, MW-3, MW-4R,
MW-5R, MW-6, MW-7, MW-8D, MW-9, MW-10, MW-11, MW-24, and MW-25; and Surface
Water monitoring stations SW-1, SW-2, SW-5, and SW-7.
 Appendix II list constituents and turbidity for Monitoring Wells MW-12, MW-13, and MW-23
and Surface Water monitoring station SW-6.
 Monitored natural attenuation parameters for Monitoring Wells MW-1, MW-2, MW-3, MW-6,
MW-7, MW-9, and MW-10.

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The sampling was attempted at the Subtitle D lined MSWLF for the following:
 Appendix I list constituents for Monitoring Wells MW-14, MW-15, MW-16S, MW-16D, MW-
17, MW-18, MW-19, MW-22, MW-26, and MW-27; and, Surface Water monitoring stations
SW-1, SW-2, SW-6 and SW-7.

The sampling includes the collection of a leachate sample from the leachate lagoon for the Subtitle D
lined MSWLF for the following:
 Leachate for Biochemical Oxygen Demand (BOD), Chemical Oxygen Demand (COD), nitrate,
sulfate, phosphate, pH, Total Suspended Solids, and Appendix I metals and volatile constituents.

Quality control measures implemented during this sampling event included submittal and subsequent
blank quantification, equipment blank (EB), field blank (FB), and trip blank (TB).

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2.0 ACTIVE C&D AND CLOSED MSWLF

2.1 SAMPLING AND CHEMICAL ANALYSES
The function and integrity of each of the monitoring locations was visually evaluated and inspected prior
to the purging/sampling at the monitoring location. Subsequently, the depths to groundwater were
measured at the site monitoring wells prior to well purging and sampling and are presented in Section 2.2.
The sixteen wells identified in Section 1.1 were purged on the date listed below. Samples of groundwater
were collected from monitoring locations described in Section 1.1 and samples of surface water were
collected from the four surface water sampling locations (i.e., SW-1, SW-5, SW-6, and SW-7). Water
samples were collected in laboratory cleaned and laboratory furnished containers, preserved as
appropriate for the test method, and delivered to Environmental Conservation Laboratories (ENCO) in
Cary, North Carolina. Chain-of-custody protocol was followed.

The chemical analyses (i.e., Appendix I or Appendix II) performed on the samples of groundwater were
identified in Section 1.3 and the results of these analyses are presented in Section 2.3.
2.2 GROUNDWATER DEPTHS AND FIELD MEASUREMENTS
2.2.1 Groundwater Flow Characteristics

Depths to groundwater were measured at the site monitoring wells prior to well purging and sampling.
Groundwater elevations at the wells are listed in the attached Table 1, and were determined by subtracting
the depths to groundwater measured on January 14 through 16, 2013 from the surveyed (reference) top-
of-casing elevations.

A potentiometric map for the contiguous property, which includes both sites, is included in Figure 2. The
groundwater flow characteristics based on both the potentiometric map and the aquifer characteristics for
the monitoring system in January 2013, are presented in Table 2. The estimated groundwater flow
velocities for this site range from 0.3 (MW-8D) up to 120 (MW-10) feet per year (ft/yr), with an average
groundwater flow velocity of about 36 ft/yr.

2.2.2 Indicator Parameters

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The field parameters pH, temperature, DO, ORP, and specific conductivity were measured with calibrated
electronic meters. Field tested parameters are shown in Table 3. Specific conductivity values of the
groundwater samples for the monitoring wells ranged from 208 (MW-6) to 2504 (MW-10) micromhos
per centimeter (μmhos/cm). Values of groundwater pH for the monitoring wells ranged from 5.31 (MW-
2) to 7.02 (MW-10). The concentrations of dissolved oxygen ranged from 0.02 (MW-12) to 5.67 (MW-
5R) milligrams per liter (mg/L). Values of oxidation reduction potential (ORP) for the monitoring wells
ranged from 37.0 (MW-13 and MW-23) to 144.0 (MW-3) millivolts (mV).

Specific conductivity values for the surface water samples from the four sampling locations (i.e., SW-1,
SW-5 through SW-7) ranged from 134.5 (SW-1) to 356.4 (SW-5) micromhos per centimeter (μmhos/cm).
Values for the surface water pH for the four sampling locations ranged from 6.76 (SW-5) to 7.38 (SW-7).
Values of oxidation reduction potential (ORP) for the four surface water sampling locations ranged from
77.0 (SW-1) to 111.0 (SW-5) millivolts (mV).

2.3 RESULTS OF CHEMICAL ANALYSES

Results of analyses for inorganics in groundwater are listed in Table 4 and the organics in groundwater
are listed in Table 5. The results of the analyses for the partial list of monitored natural attenuation
parameters for the six (seven were attempted, however MW-1 was dry) selected corrective action
monitoring wells (i.e., MW-2, MW-3, MW-6, MW-7, MW-9, and MW-10) are shown in Table 6. Results
of analyses for inorganics in surface water are listed in Table 7. No organic constituents were detected in
the four surface water samples (see Appendix A).

Several inorganics exceeded the NC 2L Groundwater Standards (i.e., arsenic [MW-3, and MW-25],
cadmium [MW-7], chromium [MW-2, MW-11, MW-24, and MW-25], lead [MW-2 and MW-25], and
nickel [MW-2]). The Interim Maximum Allowable Concentration (IMAC) for cobalt was exceeded in all
of the sampled monitoring wells except Monitoring Well MW-9. The IMAC for vanadium was exceeded
in about half of the Monitoring Wells (i.e., MW-2, MW-3, MW-7, MW-9, MW-11, MW-12, MW-24, and
MW-25). Additionally, the IMAC for beryllium was exceeded in Monitoring Well MW-2.

Only those organic constituents that were detected in any one of the monitoring wells or in the leachate
sample were included in Table 5. Organic constituents were detected in eight of the 15 monitoring wells
sampled in January 2013. The remaining seven monitoring wells did not exhibit any organic constituents
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(i.e., MW-2, MW-4R, MW-5R, MW-10, MW-13, MW-24 and MW-25: - see Table 5). However, only
five of these monitoring wells (i.e., MW-7, MW-8D, MW-9, MW-11, and MW-23) had organic
constituent concentrations exceeding the NC 2L Groundwater Standards.

Tetrachloroethene was detected above the NC 2L Groundwater Standard of 0.7 mg/L in Monitoring Wells
MW-8D, and MW-9 at estimated concentrations of 0.97J and 0.98J μg/L, respectively. Vinyl chloride
was detected above the NC 2L Groundwater Standard of 0.03 μg/L in Monitoring Wells MW-11 and
MW-23 at concentrations of 2.2 and 1.8 μg/L, respectively. Two other organic constituent (1,1-
dichloroethane and benzene) were detected above the NC 2L Groundwater Standard, with one in each of
Monitoring Wells MW-11 and MW-7 (see Table 5), respectively.

Monitoring Wells MW-2, MW-6 and MW-7 are located along the western property boundary in an area
where the groundwater has been labeled as the West Plume due to the previous occurrence of organic
constituents at these wells. Similar to previous sampling events one VOC (benzene at 2.4 μg/L) exceeded
the NC 2L Groundwater Standard (1 μg/L) in Monitoring Well MW-7. Recently the City of Albemarle
purchased the adjacent 104-acre property beyond the western property boundary as a buffer for the active
C&D and closed MSWLF area of the site. This additional buffer is located beyond these monitoring
wells. Additionally, Monitoring Well MW-24 which is located immediately downgradient from
Monitoring Well MW-7, continued to exhibit no detections of organic constituents during this sampling
event. Hence, with the increased buffer zone in this area Monitoring Well MW-7 will no longer be a
compliance well in this area.

Also within the West Plume, no VOCs were detected at either Monitoring Well MW-2 or the
downgradient well (MW-25) during the January 2013 sampling event. Six VOCs (1,1-dichloroethane,
chlorobenzene, methylene chloride, tetrachloroethene, tetrahydrofuran, and trichlorofluormethane) were
detected in Monitoring Well MW-6, but without any exceedances of the NC 2L Groundwater Standards.
The two monitoring wells (MW-24 and 25) immediately downgradient from Monitoring Wells MW-2
and MW-7, did not exhibit any VOCs during this sampling event.

Monitoring Wells MW-3, MW-9, and MW-11 are located on the east side of the closed MSWLF area of
the site. Together these wells make up the East Plume due to previous occurrence of organic constituents
in these three monitoring wells. During this sampling event no exceedances of the NC 2L Groundwater
Standards were identified in the area of the East Plume at Monitoring Wells MW-3 or MW-10. One
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VOCs (tetrachloroethene) was measured above the NC 2L Groundwater Standard in Monitoring Well
MW-9. The monitoring wells in this area (i.e., MW-3, MW-9, and MW-10) will continue to be
monitored during subsequent sampling events.

Monitoring Well MW-8D is located upgradient from the active C&D and closed MSWLF area. This well
exhibited tetrachloroethene at an estimated concentration of 0.97 μg/L, above the NC 2L Groundwater
Standard of 0.7 μg/L. Estimated concentrations of tetrachloroethene have been reported at this well in
several previous sampling events.

In the area of the Leachate Lagoon Monitoring Well MW-12, which is located upgradient from the lagoon
(see Figure 2), exhibited one VOC (acetone), but no exceedances of the NC 2L Groundwater Standards.
Two monitoring wells are located on the downgradient side of the Leachate Lagoon (i.e., MW-13 and
MW-23; which are both located between the lagoon and the unnamed tributary of Jacobs Creek).
Monitoring Well MW-13 did not exhibit any VOCs. Monitoring Well MW-23 exhibited five VOCs, with
only one VOC above the NC 2L Groundwater Standards (i.e., vinyl chloride at 1.8 μg/L).

Due to the rains this winter the unnamed tributary of Jacobs Creek that passes through the property has
been flowing. Therefore surface water samples were collected during the January 2013 sampling event.
Only three inorganics (copper, nickel, and zinc) exceeded the 15A NCAC 2B.0202 surface water
standards (NC 2B surface water standards) (see Table 7). Each of these three inorganics exceeded the
surface water standards at Surface water Sampling Location SW-5 (see Figure 2). Five inorganics were
identified in the surface water sample collected at the upstream sampling location (SW-1) (see Table 7).
A comparison between the three surface water sampling locations located on the unnamed tributary of
Jacobs Creek (i.e., SW-1 [upstream], SW-7 [middle of the onsite stream reach] and SW-6 [downstream])
does indicate that for some inorganics, concentrations increase as the surface water flows through the site,
and then for several other inorganics the higher concentrations were found at the middle surface water
sampling station and then the downstream sample exhibited lower concentrations (barium, chromium, and
vanadium). The three inorganics (antimony, chromium, and copper) that were not found in the upstream
surface water sample, did exhibit traces in the other two downstream surface water samples (i.e., SW-7
and SW-6) collected from the unnamed tributary of Jacobs Creek (see Table 7).

Selected monitored natural attenuation (MNA) parameters were measured in the laboratory for selected
monitoring wells (i.e., MW-2, MW-3, MW-6, MW-7, MW-9 and MW-10). The results of the laboratory
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analyses for the MNA parameters are shown in Table 6. However, these particular MNA parameters are a
partial set of the complete suite of typical MNA parameters and as a result it is not possible to provide an
assessment of overall biodegradation for these wells. A comparison of these results to previous MNA
data sets does indicate ongoing degradation. In their letter dated July 11, 2011 the SWS has provided the
City of Albemarle a sequencing schedule for collecting the MNA parameters over the coming years. The
primary conclusion from these data is that natural degradation is continuing to breakdown the VOCs
within the subsurface.

The laboratory reports for these analyses are included in Appendix A.
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3.0 SUBTITLE D LINED MSWLF

3.1 SAMPLING AND CHEMICAL ANALYSES
The function and integrity of each of the monitoring locations was visually evaluated and inspected prior
to the purging/sampling at the monitoring location. Subsequently, the depths to groundwater were
measured at the site monitoring wells prior to well purging and sampling and are presented in Section 3.2.
The ten monitoring wells identified in Section 1.2 were purged on the date listed below. Samples of
groundwater were collected from monitoring locations described in Section 1.2 and samples of surface
water were collected from the four surface water sampling locations (i.e., SW-1, SW-2, SW-6, and SW-
7). Water samples were collected in laboratory cleaned and laboratory furnished containers, preserved as
appropriate for the test method, and delivered to Environmental Conservation Laboratories (ENCO) in
Cary, North Carolina. Chain-of-custody protocol was followed.

The chemical analyses (i.e., Appendix I) performed on the samples of groundwater were identified in
Section 1.3 and the results of these analyses are presented in Section 3.3.
3.2 GROUNDWATER DEPTHS AND FIELD MEASUREMENTS
3.2.1 Groundwater Flow Characteristics

Depths to groundwater were measured at the site monitoring wells prior to well purging and sampling.
Groundwater elevations at the wells are listed in the attached Table 1, and were determined by subtracting
the depths to groundwater measured on January 14 through 16, 2013 from the surveyed (reference) top-
of-casing elevations.

A potentiometric map for the contiguous property, which includes both sites, is included in Figure 2. The
groundwater flow characteristics based on both the potentiometric map and the aquifer characteristics for
the detection monitoring system in January 2013, are presented in Table 8. The estimated groundwater
flow velocities for this site range from 1 (MW-16S) up to 700 (MW-15) feet per year (ft/year), with an
average groundwater flow velocity of about 138 ft/year.

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3.2.2 Indicator Parameters

The field parameters pH, temperature, DO, ORP, and specific conductivity were measured with calibrated
electronic meters. Field tested parameters are shown in Table 9. Specific conductivity values of the
groundwater samples for the detection monitoring system wells ranged from 117.3 (MW-18) to 768
(MW-19) μmhos/cm. Values of groundwater pH for the detection wells ranged from 5.35 (MW-22) to
6.66 (MW-26). The concentrations of dissolved oxygen ranged from 0.16 (MW-16D) to 6.25 (MW-26)
mg/L. Values of ORP for the detection wells ranged from 13.0 (MW-15) to 182.0 (MW-26) mV.

Specific conductivity values for the surface water samples from the four sampling locations (i.e., SW-1,
SW-2, SW-6, and SW-7) ranged from 127.1 (SW-2) to 173.7 (SW-6) micromhos per centimeter
(μmhos/cm). Values for the surface water pH for the four sampling locations ranged from 7.05 (SW-1) to
7.40 (SW-2). Values of oxidation reduction potential (ORP) for the four surface water sampling locations
ranged from 77.0 (SW-1) to 110.0 (SW-7) millivolts (mV).
3.3 RESULTS OF CHEMICAL ANALYSES
Results of analyses for the inorganics in groundwater are listed in Table 4 and the organics in
groundwater are listed in Table 5.

None of the 15 Appendix I total metals analyzed were detected above the NC 2L Groundwater Standard.
Two metals (cobalt and vanadium) were detected above the North Carolina IMACs. Cobalt was found
above the IMAC (i.e., 0.001 mg/L) in nine of the ten monitoring wells around the Subtitle D lined
MSWLF with concentrations ranging from 0.00172J (MW-15) up to 0.0508 (MW-16D) mg/L.
Vanadium was detected above the IMAC in Monitoring Wells MW-14, MW-18, MW-22, MW-26, and
MW-27 with estimated concentrations ranging from 0.0016J (MW-22) up to 0.00804J (MW-26) mg/L.

No organic constituents were detected at the Subtitle D lined MSWLF site. All the ten monitoring wells
around the Subtitle D lined MSWLF did not exhibit any traces of organic constituents.

Due to the rains this winter the unnamed tributary of Jacobs Creek that passes through the property has
been flowing. The three surface water samples collected along the unnamed tributary of Jacobs Creek
were discussed in Section 2.3. The only other surface water sampling location in the vicinity of the
Subtitle D lined MSWLF site is SW-2. This surface water sampling location is located on a drainage
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feature south of the Subtitle D lined MSWLF that discharges to the unnamed tributary of Jacobs Creek
that flows through the site (see Figure 2). The surface water samples were collected during the January
2013 sampling event. Only one inorganic (copper) exceeded any of the respective NC 2B surface water
standards and traces of eight other inorganics were also identified at the surface water sampling location
SW-2. A comparison between the three surface water sampling locations located on the unnamed
tributary of Jacobs Creek (i.e., SW-1, SW-7, and SW-6) and SW-2 indicates that the same seven
inorganics that were identified along the unnamed tributary of Jacobs Creek were also present at SW-2.
In addition to these seven inorganics at SW-2, arsenic was also identified at SW-2.

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4.0 SUMMARY AND CONCLUSIONS

The sampling event reported herein includes the monitoring wells for each of the two landfill sites (except
for MW-1, which was dry) presented in Sections 1.1 and 1.2, and the leachate sample collected from the
leachate lagoon that receives flow from the Subtitle D lined MSWLF. Surface water samples were
collected from all of the five surface water sampling locations during the January 2013 sampling event.

The inorganic constituents identified at the two landfill sites that exceed either the NC 2L Groundwater
Standards or the IMACs are as follows:
Active C&D and closed MSWLF:
 Arsenic: MW-3, and MW-25
 Beryillium: MW-2
 Cadmium: MW-7
 Chromium: MW-2, MW-11, MW-24, and MW-25
 Cobalt: All thirteen monitoring wells (except MW-9)
 Lead: MW-2 and MW-25
 Nickel: MW-2
 Vanadium: MW-2, MW-3, MW-7, MW-9, MW-11, MW-12, MW-24, and MW-25
Subtitle D lined MSWLF:
 Cobalt: Nine of the ten monitoring wells, including background Monitoring Well MW-19
 Vanadium: MW-14, MW-18, MW-22, MW-26, and MW-27

One of the wells listed above is the background monitoring well (MW-19) for the Subtitle D lined
MSWLF. Additionally, another monitoring well listed once above (cobalt - MW-8D; see Figure 2) is
located upgradient from the Active C&D and closed MSWLF, and is not a compliance well.

The organic constituents identified at the landfill sites that exceed either the NC 2L Groundwater
Standards or the IMACs are as follows:

Active C&D and closed MSWLF:
City of Albemarle Landfill March 26, 2013
Report of Semi-Annual Sampling and Analysis – January 2013
Shield Project 1110192

4-2

The only organic constituents identified at the Active C&D and closed MSWLF Site that exceed the NC
2L Groundwater Standards are as follows:
 1,1-Dichloroethane in Monitoring Well MW-11;
 Benzene in Monitoring Well MW-7;
 Tetrachloroethene in Monitoring Wells MW-8D, and MW-9;
 Vinyl chloride in Monitoring Wells MW-11, and MW-23.

Organic constituents continue to be present within Monitoring Wells MW-6, and MW-7 in the West
Plume and generally lower than previous sampling events, and no organics were identified in Monitoring
Well MW-2 during the January 2013 sampling event. Better than previous sampling events, only one
VOC exceeding the NC 2L Groundwater Standards was identified in Monitoring Well MW-7. The
monitoring wells in this area (i.e., MW-2, MW-6, and MW-7) will continue to be monitored during
subsequent sampling events. The two monitoring wells (MW-24 and 25) immediately downgradient from
Monitoring Wells MW-2 and MW-7, did not exhibit any VOCs during this sampling event.

No exceedances of the NC 2L Groundwater Standards were identified in the area of the East Plume at
Monitoring Wells MW-3 or MW-10. Whereas, tetrachloroethene exceeded the NC 2L Groundwater
Standard in Monitoring Well MW-9. The monitoring wells in this area (i.e., MW-3, MW-9, and MW-10)
will continue to be monitored during subsequent sampling events.

Subtitle D lined MSWLF:
No organic constituents were detected at the Subtitle D lined MSWLF site as all the ten monitoring wells
around this site did not exhibit any traces of organic constituents.

The leachate sample collected from the leachate lagoon exhibited five organic constituents (see Table 5).
Seven inorganic constituents were also identified in the leachate sample (see Table 4).

The monitoring networks currently sampled around each of the two landfill sites owned and operated by
City of Albemarle are capable of detecting the migration of constituents for the landfill cells.
City of Albemarle Landfill - Report of Semi-Annual Sampling and Analysis - January 2013
Solid Waste Permit #8401
Shield Project 1110192
March 26, 2013
Monitoring
Well
Identification
Specific Conductivity
(μmhos/cm)pH (SU)Temperature
(oC)
Dissolved
Oxygen (mg/L)
Oxygen Reduction
Potential (mV)
MW-14 471.5 6.11 12.5 1.12 82.0
MW-15 480.6 6.18 13.1 1.08 13.0
MW-16S 556.0 6.56 12.3 4.01 81.0
MW-16D 387.5 5.86 12.6 0.16 89.0
MW-17 273.6 6.03 12.9 2.44 139.0
MW-18 117.3 5.89 13.3 0.98 118.0
MW-19 768 6.65 16.2 2.85 76.0
MW-22 371.2 5.35 13.7 0.62 157.0
MW-26 235.5 6.66 14.2 6.25 182.0
MW-27 443.5 5.75 14.8 0.49 100.0
SW-1 134.5 7.05 10.6 NM 77.0
SW-2 127.1 7.40 11.0 NM 107.0
SW-6 173.7 7.21 10.7 NM 108.0
SW-7 145.3 7.38 11.4 NM 110.0
NOTES:Prepared/Date: R. Sutley 2/12/13
1) μmhos/cm = micromhos per centimeter Checked/Date: J. D. Wallace 2/18/13
2) SU = Standard Units
3) oC = Degrees Celsius
4) mg/L = Milligrams per Liter
5) mV = Millivolts
CITY OF ALBEMARLE LANDFILL
STANLY COUNTY, NORTH CAROLINA
TABLE 9
FIELD-TESTED PARAMETERS - SUBTITLE D LINED MSWLF
MEASUREMENTS OF JANUARY 2013
Page 1 of 1
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Page 1 of 1
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MW
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Page 1 of 1
City of Albemarle Landfill - Report of Semi-Annual Sampling and Analysis - January 2013
Solid Waste Permit #8401
Shield Project 1110192
March 26, 2013
1,1-DCA 1,4-DCB Acetone Benzene
Chloro-
benzene
Chloro-
ethane
cis-1,2-
DCE
Ethyl-
benzen
e
Methylen
e
Chloride
Methyl
Ethyl
Ketone
Tetrachloro-
ethene
Tetrahydro-
furan
Trichloro-
ethene
Trichloro-
fluoromethane
Vinyl
Chloride Xylenes
SWSL 5 1 100 1 3 10 5 1 1.0 100 1 NE 1 1 1 5
NC 2L 6 6 6000 1 50 3000 70 600 5.0 4000.0 0.7 NE 3 2000 0.03 500
IMAC -- -- -- -- -- -- -- -- -- -- -- -- -- -- --
MW-1 (1)NS NS NS NS NS NS NS NS NS NS NS NA NS NS NS NS
MW-2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-3 3.8J 1.9 ND ND 8.2 ND 0.85J ND ND ND ND 2.9 0.82J ND ND ND
MW-4R ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-5R ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-6 2.3J ND ND ND 0.44J ND ND ND 1.5 ND 0.67J 2.1 ND 7.5 ND ND
MW-7 2.6J 2.8 ND 2.4 7.9 ND 1.6J ND ND ND 0.40J 2.5 ND ND ND ND
MW-8D ND ND ND ND ND ND ND ND ND ND 0.97J ND ND ND ND ND
MW-9 0.44J ND ND ND ND ND 0.55J ND ND ND 0.98J ND 0.72J ND ND ND
MW-10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-11 18 ND ND 0.87J ND 4.8J 5.8 ND ND ND ND ND ND ND 2.2 ND
MW-12 ND ND 4.6J ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-13 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-23 3.1J ND ND 0.87J ND 1.8J 17 ND ND ND ND ND ND ND 1.8 ND
MW-24 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-25 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-14 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-15 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-16S ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-16D ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-17 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-18 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-19 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-22 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-26 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
MW-27 ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND
LAGOON ND ND 46J 0.48J ND ND ND 0.42J ND 6.6J ND NA ND ND ND 2.9J
Trip Blank ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Field Blank ND ND ND ND ND ND ND ND 0.55J ND ND ND ND ND ND ND
Equip. Blank ND ND ND ND ND ND ND ND 0.54J ND ND ND ND ND ND ND
NOTES:
1) All data reported in Micrograms per Liter (g/L)DCA - Dichloroethane
2) SWSL= North Carolina Solid Waste Section Limits DCE - Dichloroethene3) NC 2L = North Carolina 2L Groundwater Standard as found in 15A NCAC 2L.0202 DCB - Dichlorobenzene
4) IMAC = Interim Maximum Allowable Concentrations established under 15A NCAC 2L .0202
5) NE = Not Established.6) ND = Not detected at or Above the Minimum Detection Level (MDL).Prepared/Date:
7) NS = Not Sampled (Dry)Checked/Date: 2/19/13
8) NA = Not Analyzed
9) J = Estimated value, see Laboratory Report.10) Bold = Result exceeds SWSL; Shading = Result exceeds NC 2L Groundwater Standard or IMAC. (1) Monitoring Well MW-1 was Dry
LEACHATE SAMPLE
J. D. Wallace
R. Sutley
QUALITY CONTROL/QUALITY ASSURANCE SAMPLES
2/15/2013
TABLE 5
ANALYTICAL ORGANIC PARAMETERS FOR GROUNDWATER SAMPLES - JANUARY 2013
CITY OF ALBEMARLE LANDFILL
SUBTITLE D LINED MSWLF
ACTIVE C&D AND CLOSED MSWLF
STANLY COUNTY, NORTH CAROLINA
Page 1 of 1
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March 26, 2013
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D

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D

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Page 1 of 1
City of Albemarle Landfill - Report of Semi-Annual Sampling and Analysis - January 2013
Solid Waste Permit #8401
Shield Project 1110192
March 26, 2013
Monitoring
Well
Identification
Specific Conductivity
(μmhos/cm)pH (SU)Temperature
(oC)
Dissolved
Oxygen (mg/L)
Oxygen Reduction
Potential (mV)
MW-1 Dry Dry Dry Dry Dry
MW-2 1507.0 5.31 15.6 0.11 69.0
MW-3 1217.0 6.77 14.4 0.16 144.0
MW-4R 281.1 6.00 15.4 0.12 111.0
MW-5R 549.0 6.77 14.3 5.67 76.0
MW-6 208 5.51 15.1 1.56 111.0
MW-7 1423 6.36 14.8 1.58 59.0
MW-8D 1058 6.51 16.0 2.36 67.0
MW-9 375.1 6.30 11.9 2.69 121.0
MW-10 2504 7.02 12.1 3.43 75.0
MW-11 492.9 6.26 13.9 2.25 88.0
MW-12 430.2 6.23 16.0 0.02 76.0
MW-13 566 6.70 14.0 1.46 37.0
MW-23 667 6.01 13.0 0.15 37.0
MW-24 441.2 6.18 14.7 1.14 101.0
MW-25 215.6 5.93 14.6 4.76 102.0
SW-1 134.5 7.05 10.6 NM 77.0
SW-5 356.4 6.76 11.2 NM 111.0
SW-6 173.7 7.21 10.7 NM 108.0
SW-7 145.3 7.38 11.4 NM 110.0
NOTES:Prepared/Date: R. Sutley 2/12/13
1) μmhos/cm = micromhos per centimeter Checked/Date: J.D. Wallace 2/18/13
2) SU = Standard Units
3) oC = Degrees Celsius
4) mg/L = Milligrams per Liter
5) mV = Millivolts
6) NM = Not Measured
CITY OF ALBEMARLE LANDFILL
STANLY COUNTY, NORTH CAROLINA
TABLE 3
FIELD-TESTED PARAMETERS - ACTIVE C&D AND CLOSED MSWLF
MEASUREMENTS OF JANUARY 2013
Page 1 of 1
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Page 1 of 1
City of Albemarle Landfill - Report of Semi-Annual Sampling and Analysis - January 2013
Solid Waste Permit #8401
Shield Project 1110192
March 26, 2013
Well TOC Ground Depth to Groundwater
Identifi- Elevation Elevation Groundwater Elevation
cation (Feet above (Feet above(Ft below TOC)(Ft above NGVD)
NGVD) NGVD)
MW-1 447.21 445.6 19.75 427.46
MW-2 431.85 429.9 16.10 415.75
MW-3 396.11 393.9 13.85 382.26
MW-4R 415.36 412.8 25.35 390.01
MW-5R 416.06 413.1 9.73 406.33
MW-6 439.63 437.7 28.59 411.04
MW-7 431.30 429.4 17.16 414.14
MW-8D 491.38 488.8 57.38 434.00
MW-9 392.64 389.1 6.84 385.80
MW-10 388.01 385.4 5.12 382.89
MW-11 386.78 384.4 7.02 379.76
MW-12 399.47 398.1 15.67 383.80
MW-13 388.52 385.7 9.25 379.27
MW-23 386.41 383.9 7.36 379.05
MW-24 432.19 429.2 17.55 414.64
MW-25 425.22 422.3 13.94 411.28
MW-14 383.55 380.8 4.65 378.90
MW-15 385.72 383.2 5.30 380.42
MW-16S 386.75 384.4 4.50 382.25
MW-16D 386.88 384.4 4.00 382.88
MW-17 396.47 393.5 7.79 388.68
MW-18 409.41 410.4 8.03 401.38
MW-19 452.34 450.8 26.10 426.24
MW-22 388.41 385.0 10.55 377.86
MW-26 413.98 411.0 33.37 380.61
MW-27 404.71 402.4 4.41 400.30
Notes:
1) GW = Groundwater Prepared/Date: R. Sutley 1/12/13
2) TOC = Top of Casing Checked/Date: J.D. Wallace 2/18/13
3) NM = Not Measured
4) GS = Ground Surface
5) NGVD = National Geodetic Vertical Datum
6) Depth to Groundwater Measured from Top of Well casing
TABLE 1
ACTIVE C&D AND CLOSED MSWLF
SUBTITLE D LINED MSWLF
1/14-16/2013
SUMMARY OF GROUNDWATER DATA
CITY OF ALBEMARLE LANDFILL
STANLY COUNTY, NORTH CAROLINA
Page 1 of 1
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): C300054
Charlotte, NC 28208
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 1110192, Project Name/Desc: Albemarle LF SWs
Attn: Danny Hefner
Shield Engineering, Inc. (SH007)
4301 Taggart Creek Road
Stephanie Franz
Project Manager
Thursday, January 24, 2013
RE: Laboratory Results for
Dear Danny Hefner,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, January 18, 2013.
The total number of pages in this report, including this page is 34.
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
8401-SW1 C300054-01 Sampled:01/17/13 11:30 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:44
EPA 6020A 07/16/13 01/18/13 12:41 1/23/2013 13:47
EPA 8260B 01/31/13 01/21/13 13:04 1/22/2013 02:35
SM 2130B 01/19/13 11:30 01/18/13 18:54 1/18/2013 18:54
8401-SW2 C300054-02 Sampled:01/17/13 13:00 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:46
EPA 6020A 07/16/13 01/18/13 12:41 1/23/2013 13:07
EPA 8260B 01/31/13 01/21/13 13:04 1/22/2013 03:04
SM 2130B 01/19/13 13:00 01/18/13 18:54 1/18/2013 18:54
8401-SW5 C300054-03 Sampled:01/17/13 11:45 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:48
EPA 6020A 07/16/13 01/18/13 12:41 1/23/2013 13:51
EPA 8260B 01/31/13 01/21/13 13:04 1/22/2013 03:34
SM 2130B 01/19/13 11:45 01/18/13 18:54 1/18/2013 18:54
8401-SW6 C300054-04 Sampled:01/17/13 13:20 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:50
EPA 6020A 07/16/13 01/18/13 12:41 1/23/2013 13:55
EPA 7470A 02/14/13 01/21/13 10:48 1/22/2013 17:02
EPA 8260B 01/31/13 01/21/13 13:04 1/22/2013 04:04
SM 2130B 01/19/13 13:20 01/18/13 18:54 1/18/2013 18:54
8401-SW7 C300054-05 Sampled:01/17/13 12:10 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:52
EPA 6020A 07/16/13 01/18/13 12:41 1/23/2013 13:59
EPA 8260B 01/31/13 01/21/13 13:04 1/22/2013 04:33
SM 2130B 01/19/13 12:10 01/18/13 18:54 1/18/2013 18:54
Page 2 of 34
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:8401-SW1 C300054-01
Flag NotesMDLNC SWSLMRLDF
19.8 ug/L EPA 6010CJ 10010.01.001Barium - Total
1.41 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
2.44 ug/L EPA 6010CJ 5010.01.801Nickel - Total
17 NTU SM 2130B NE1.00.501Turbidity
1.55 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
4.09 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-SW2 C300054-02
Flag NotesMDLNC SWSLMRLDF
0.977 ug/L EPA 6020AJ 62.000.2201Antimony - Total
3.31 ug/L EPA 6010CJ 1010.02.801Arsenic - Total
21.8 ug/L EPA 6010CJ 10010.01.001Barium - Total
3.22 ug/L EPA 6010CJ 1010.01.001Chromium - Total
2.47 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
4.35 ug/L EPA 6010CJ 1010.01.601Copper - Total
4.26 ug/L EPA 6010CJ 5010.01.801Nickel - Total
53 NTU SM 2130BD NE2.01.02Turbidity
7.68 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
9.47 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-SW5 C300054-03
Flag NotesMDLNC SWSLMRLDF
6.36 ug/L EPA 6020A 62.000.2201Antimony - Total
18.1 ug/L EPA 6010CJ 10010.01.001Barium - Total
0.208 ug/L EPA 6010CJ 11.000.1001Beryllium - Total
2.72 ug/L EPA 6010CJ 1010.01.001Chromium - Total
54.8 ug/L EPA 6010C 1010.01.101Cobalt - Total
76.9 ug/L EPA 6010C 1010.01.601Copper - Total
115 ug/L EPA 6010C 5010.01.801Nickel - Total
48 NTU SM 2130BD NE2.01.02Turbidity
2.01 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
115 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-SW6 C300054-04
Flag NotesMDLNC SWSLMRLDF
0.558 ug/L EPA 6020AJ 62.000.2201Antimony - Total
28.9 ug/L EPA 6010CJ 10010.01.001Barium - Total
4.93 ug/L EPA 6010CJ 1010.01.001Chromium - Total
4.15 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
10.5 ug/L EPA 6010C 1010.01.601Copper - Total
10.3 ug/L EPA 6010CJ 5010.01.801Nickel - Total
77 NTU SM 2130BD NE2.01.02Turbidity
5.84 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
19.0 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-SW7 C300054-05
Flag NotesMDLNC SWSLMRLDF
0.361 ug/L EPA 6020AJ 62.000.2201Antimony - Total
Page 3 of 34
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-SW7 C300054-05
Flag NotesMDLNC SWSLMRLDF
29.4 ug/L EPA 6010CJ 10010.01.001Barium - Total
5.39 ug/L EPA 6010CJ 1010.01.001Chromium - Total
3.61 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
5.75 ug/L EPA 6010CJ 1010.01.601Copper - Total
6.98 ug/L EPA 6010CJ 5010.01.801Nickel - Total
59 NTU SM 2130BD NE2.01.02Turbidity
6.26 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
11.7 ug/L EPA 6010C 1010.03.801Zinc - Total
Page 4 of 34
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ANALYTICAL RESULTS
8401-SW1Description:Lab Sample ID:C300054-01 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:30 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 02:351,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 02:351,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 02:351,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 02:351,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 02:351,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 02:351,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 02:351,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 02:351,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 02:351,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 02:351,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 02:351,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 02:351,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 02:351,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 02:352-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/22/13 02:352-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 02:354-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 02:35Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/22/13 02:35Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 02:35Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 02:35Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 02:35Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 02:35Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 02:35Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 02:35Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 02:35Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 02:35Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 02:35Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 02:35Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 02:35Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 02:35cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 02:35cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 02:35Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 02:35Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 02:35Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 02:35Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 02:35Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 02:35Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 02:35Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 02:35Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/22/13 02:35Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 02:35trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 02:35trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 02:35trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
Page 5 of 34
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8401-SW1Description:Lab Sample ID:C300054-01 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:30 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 02:35Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 02:35Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 02:35Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/22/13 02:35Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/22/13 02:35Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/22/13 02:353A210275450.0 1
Dibromofluoromethane 68-117106 %JKGEPA 8260B 01/22/13 02:353A210275350.0 1
Toluene-d8 67-127102 %JKGEPA 8260B 01/22/13 02:353A210275150.0 1
Page 6 of 34
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8401-SW1Description:Lab Sample ID:C300054-01 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:30 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 13:47Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/21/13 13:44Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:44Barium [7440-39-3] ^1 1.00 JDH10.019.8 J 100
ug/L EPA 6010C 01/21/13 13:44Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:44Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:44Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:44Cobalt [7440-48-4] ^1 1.10 JDH10.01.41 J 10
ug/L EPA 6010C 01/21/13 13:44Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:44Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:44Nickel [7440-02-0] ^1 1.80 JDH10.02.44 J 50
ug/L EPA 6010C 01/21/13 13:44Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:44Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 13:47Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:44Vanadium [7440-62-2] ^1 1.40 JDH10.01.55 J 25
ug/L EPA 6010C 01/21/13 13:44Zinc [7440-66-6] ^1 3.80 JDH10.04.09 J 10
Page 7 of 34
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8401-SW1Description:Lab Sample ID:C300054-01 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:30 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/18/13 18:54Turbidity [ECL-0177] ^1 0.50 JOC1.017 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 34
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8401-SW2Description:Lab Sample ID:C300054-02 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:00 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 03:041,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 03:041,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 03:041,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 03:041,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 03:041,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 03:041,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 03:041,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 03:041,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 03:041,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 03:041,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 03:041,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 03:041,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 03:041,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 03:042-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/22/13 03:042-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 03:044-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 03:04Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/22/13 03:04Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 03:04Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 03:04Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 03:04Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 03:04Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 03:04Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 03:04Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 03:04Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 03:04Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 03:04Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 03:04Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 03:04Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 03:04cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 03:04cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 03:04Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 03:04Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 03:04Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 03:04Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 03:04Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 03:04Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 03:04Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 03:04Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 03:04trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 03:04trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 03:04trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/22/13 03:04Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 03:04Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 03:04Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/22/13 03:04Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 9 of 34
www.encolabs.com
8401-SW2Description:Lab Sample ID:C300054-02 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:00 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 03:04Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122110 %JKGEPA 8260B 01/22/13 03:043A210275550.0 1
Dibromofluoromethane 68-117106 %JKGEPA 8260B 01/22/13 03:043A210275350.0 1
Toluene-d8 67-127105 %JKGEPA 8260B 01/22/13 03:043A210275250.0 1
Page 10 of 34
www.encolabs.com
8401-SW2Description:Lab Sample ID:C300054-02 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:00 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 13:07Antimony [7440-36-0] ^1 0.220 VLO2.000.977 J 6
ug/L EPA 6010C 01/21/13 13:46Arsenic [7440-38-2] ^1 2.80 JDH10.03.31 J 10
ug/L EPA 6010C 01/21/13 13:46Barium [7440-39-3] ^1 1.00 JDH10.021.8 J 100
ug/L EPA 6010C 01/21/13 13:46Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:46Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:46Chromium [7440-47-3] ^1 1.00 JDH10.03.22 J 10
ug/L EPA 6010C 01/21/13 13:46Cobalt [7440-48-4] ^1 1.10 JDH10.02.47 J 10
ug/L EPA 6010C 01/21/13 13:46Copper [7440-50-8] ^1 1.60 JDH10.04.35 J 10
ug/L EPA 6010C 01/21/13 13:46Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:46Nickel [7440-02-0] ^1 1.80 JDH10.04.26 J 50
ug/L EPA 6010C 01/21/13 13:46Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:46Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 13:07Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:46Vanadium [7440-62-2] ^1 1.40 JDH10.07.68 J 25
ug/L EPA 6010C 01/21/13 13:46Zinc [7440-66-6] ^1 3.80 JDH10.09.47 J 10
Page 11 of 34
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8401-SW2Description:Lab Sample ID:C300054-02 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:00 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/18/13 18:54Turbidity [ECL-0177] ^2 1.0 JOC2.053D NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 12 of 34
www.encolabs.com
8401-SW5Description:Lab Sample ID:C300054-03 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:45 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 03:341,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 03:341,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 03:341,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 03:341,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 03:341,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 03:341,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 03:341,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 03:341,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 03:341,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 03:341,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 03:341,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 03:341,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 03:341,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 03:342-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/22/13 03:342-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 03:344-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 03:34Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/22/13 03:34Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 03:34Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 03:34Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 03:34Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 03:34Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 03:34Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 03:34Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 03:34Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 03:34Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 03:34Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 03:34Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 03:34Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 03:34cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 03:34cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 03:34Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 03:34Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 03:34Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 03:34Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 03:34Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 03:34Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 03:34Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 03:34Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/22/13 03:34Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 03:34trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 03:34trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 03:34trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/22/13 03:34Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 03:34Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 03:34Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 13 of 34
www.encolabs.com
8401-SW5Description:Lab Sample ID:C300054-03 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:45 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 03:34Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/22/13 03:34Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/22/13 03:343A210275450.0 1
Dibromofluoromethane 68-117105 %JKGEPA 8260B 01/22/13 03:343A210275350.0 1
Toluene-d8 67-127107 %JKGEPA 8260B 01/22/13 03:343A210275350.0 1
Page 14 of 34
www.encolabs.com
8401-SW5Description:Lab Sample ID:C300054-03 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:45 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 13:51Antimony [7440-36-0] ^1 0.220 VLO2.006.36 6
ug/L EPA 6010C 01/21/13 13:48Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:48Barium [7440-39-3] ^1 1.00 JDH10.018.1 J 100
ug/L EPA 6010C 01/21/13 13:48Beryllium [7440-41-7] ^1 0.100 JDH1.000.208 J 1
ug/L EPA 6010C 01/21/13 13:48Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:48Chromium [7440-47-3] ^1 1.00 JDH10.02.72 J 10
ug/L EPA 6010C 01/21/13 13:48Cobalt [7440-48-4] ^1 1.10 JDH10.054.8 10
ug/L EPA 6010C 01/21/13 13:48Copper [7440-50-8] ^1 1.60 JDH10.076.9 10
ug/L EPA 6010C 01/21/13 13:48Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:48Nickel [7440-02-0] ^1 1.80 JDH10.0115 50
ug/L EPA 6010C 01/21/13 13:48Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:48Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 13:51Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:48Vanadium [7440-62-2] ^1 1.40 JDH10.02.01 J 25
ug/L EPA 6010C 01/21/13 13:48Zinc [7440-66-6] ^1 3.80 JDH10.0115 10
Page 15 of 34
www.encolabs.com
8401-SW5Description:Lab Sample ID:C300054-03 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:45 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/18/13 18:54Turbidity [ECL-0177] ^2 1.0 JOC2.048D NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 16 of 34
www.encolabs.com
8401-SW6Description:Lab Sample ID:C300054-04 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:20 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 04:041,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 04:041,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 04:041,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 04:041,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 04:041,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 04:041,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 04:041,1-Dichloropropene [563-58-6] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 04:041,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 04:041,2,4-Trichlorobenzene [120-82-1] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 04:041,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 04:041,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 04:041,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 04:041,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 04:041,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 04:041,3-Dichlorobenzene [541-73-1] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 04:041,3-Dichloropropane [142-28-9] ^1 0.16 JKG1.00.16 U 1
ug/L EPA 8260B 01/22/13 04:041,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 04:042,2-Dichloropropane [594-20-7] ^1 0.28 JKG1.00.28 U 15
ug/L EPA 8260B 01/22/13 04:042-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/22/13 04:042-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 04:043-Chloropropene [107-05-1] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/22/13 04:044-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 04:04Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/22/13 04:04Acetonitrile [75-05-8] ^1 5.0 JKG105.0 U 55
ug/L EPA 8260B 01/22/13 04:04Acrolein [107-02-8] ^1 4.0 JKG104.0 U 53
ug/L EPA 8260B 01/22/13 04:04Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 04:04Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 04:04Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 04:04Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 04:04Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 04:04Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 04:04Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 04:04Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 04:04Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 04:04Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 04:04Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 04:04Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 04:04Chloroprene [126-99-8] ^1 0.64 JKG1.00.64 U 20
ug/L EPA 8260B 01/22/13 04:04cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 04:04cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 04:04Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 04:04Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 04:04Dichlorodifluoromethane [75-71-8] ^1 0.20 JKG1.00.20 U 5
ug/L EPA 8260B 01/22/13 04:04Ethyl Methacrylate [97-63-2] ^1 0.38 JKG1.00.38 U 10
ug/L EPA 8260B 01/22/13 04:04Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 04:04Hexachlorobutadiene [87-68-3] ^1 0.22 JKG1.00.22 U 10
Page 17 of 34
www.encolabs.com
8401-SW6Description:Lab Sample ID:C300054-04 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:20 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 04:04Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 04:04Isobutyl alcohol [78-83-1] ^1 11 JKG5011U 100
ug/L EPA 8260B 01/22/13 04:04m,p-Xylenes [108-38-3/106-42-3] ^1 0.17 JKG2.00.17 U NE
ug/L EPA 8260B 01/22/13 04:04Methacrylonitrile [126-98-7] ^1 4.9 JKG104.9 U 100
ug/L EPA 8260B 01/22/13 04:04Methyl Methacrylate [80-62-6] ^1 0.51 JKG1.00.51 U 30
ug/L EPA 8260B 01/22/13 04:04Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 04:04Naphthalene [91-20-3] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/22/13 04:04o-Xylene [95-47-6] ^1 0.065 JKG1.00.065 U NE
ug/L EPA 8260B 01/22/13 04:04Propionitrile [107-12-0] ^1 5.0 JKG105.0 U 150
ug/L EPA 8260B 01/22/13 04:04Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 04:04Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 04:04Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/22/13 04:04Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 04:04trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 04:04trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 04:04trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/22/13 04:04Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 04:04Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 04:04Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/22/13 04:04Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/22/13 04:04Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122105 %JKGEPA 8260B 01/22/13 04:043A210275350.0 1
Dibromofluoromethane 68-117105 %JKGEPA 8260B 01/22/13 04:043A210275250.0 1
Toluene-d8 67-127103 %JKGEPA 8260B 01/22/13 04:043A210275250.0 1
Page 18 of 34
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8401-SW6Description:Lab Sample ID:C300054-04 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:20 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 01/22/13 17:02Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 19 of 34
www.encolabs.com
8401-SW6Description:Lab Sample ID:C300054-04 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:20 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 13:55Antimony [7440-36-0] ^1 0.220 VLO2.000.558 J 6
ug/L EPA 6010C 01/21/13 13:50Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:50Barium [7440-39-3] ^1 1.00 JDH10.028.9 J 100
ug/L EPA 6010C 01/21/13 13:50Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:50Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:50Chromium [7440-47-3] ^1 1.00 JDH10.04.93 J 10
ug/L EPA 6010C 01/21/13 13:50Cobalt [7440-48-4] ^1 1.10 JDH10.04.15 J 10
ug/L EPA 6010C 01/21/13 13:50Copper [7440-50-8] ^1 1.60 JDH10.010.5 10
ug/L EPA 6010C 01/21/13 13:50Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:50Nickel [7440-02-0] ^1 1.80 JDH10.010.3 J 50
ug/L EPA 6010C 01/21/13 13:50Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:50Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 13:55Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:50Tin [7440-31-5] ^1 2.10 JDH10.02.10 U 100
ug/L EPA 6010C 01/21/13 13:50Vanadium [7440-62-2] ^1 1.40 JDH10.05.84 J 25
ug/L EPA 6010C 01/21/13 13:50Zinc [7440-66-6] ^1 3.80 JDH10.019.0 10
Page 20 of 34
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8401-SW6Description:Lab Sample ID:C300054-04 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 13:20 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/18/13 18:54Turbidity [ECL-0177] ^2 1.0 JOC2.077D NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 21 of 34
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8401-SW7Description:Lab Sample ID:C300054-05 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 12:10 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 04:331,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 04:331,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 04:331,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 04:331,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 04:331,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 04:331,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 04:331,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 04:331,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 04:331,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 04:331,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 04:331,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 04:331,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 04:331,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 04:332-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/22/13 04:332-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 04:334-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 04:33Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/22/13 04:33Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 04:33Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 04:33Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 04:33Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 04:33Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 04:33Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 04:33Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 04:33Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 04:33Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 04:33Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 04:33Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 04:33Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 04:33cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 04:33cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 04:33Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 04:33Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 04:33Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 04:33Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 04:33Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 04:33Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 04:33Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 04:33Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/22/13 04:33Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 04:33trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 04:33trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 04:33trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/22/13 04:33Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 04:33Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 04:33Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 22 of 34
www.encolabs.com
8401-SW7Description:Lab Sample ID:C300054-05 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 12:10 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 04:33Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/22/13 04:33Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122110 %JKGEPA 8260B 01/22/13 04:333A210275550.0 1
Dibromofluoromethane 68-117109 %JKGEPA 8260B 01/22/13 04:333A210275450.0 1
Toluene-d8 67-127104 %JKGEPA 8260B 01/22/13 04:333A210275250.0 1
Page 23 of 34
www.encolabs.com
8401-SW7Description:Lab Sample ID:C300054-05 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 12:10 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 13:59Antimony [7440-36-0] ^1 0.220 VLO2.000.361 J 6
ug/L EPA 6010C 01/21/13 13:52Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:52Barium [7440-39-3] ^1 1.00 JDH10.029.4 J 100
ug/L EPA 6010C 01/21/13 13:52Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:52Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:52Chromium [7440-47-3] ^1 1.00 JDH10.05.39 J 10
ug/L EPA 6010C 01/21/13 13:52Cobalt [7440-48-4] ^1 1.10 JDH10.03.61 J 10
ug/L EPA 6010C 01/21/13 13:52Copper [7440-50-8] ^1 1.60 JDH10.05.75 J 10
ug/L EPA 6010C 01/21/13 13:52Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:52Nickel [7440-02-0] ^1 1.80 JDH10.06.98 J 50
ug/L EPA 6010C 01/21/13 13:52Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:52Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 13:59Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:52Vanadium [7440-62-2] ^1 1.40 JDH10.06.26 J 25
ug/L EPA 6010C 01/21/13 13:52Zinc [7440-66-6] ^1 3.80 JDH10.011.7 10
Page 24 of 34
www.encolabs.com
8401-SW7Description:Lab Sample ID:C300054-05 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 12:10 Work Order:C300054
Albemarle LF SWsProject:Sampled By:Danny Hefner / Joanna Harbison
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/18/13 18:54Turbidity [ECL-0177] ^2 1.0 JOC2.059D NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 25 of 34
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.15 U 1,1-Dichloropropene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.14 U 1,2,4-Trichlorobenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.15 U 1,3-Dichlorobenzene
ug/L1.00.16 U 1,3-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L1.00.28 U 2,2-Dichloropropane
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L1.00.11 U 3-Chloropropene
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L105.0 U Acetonitrile
ug/L104.0 U Acrolein
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.64 U Chloroprene
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.20 U Dichlorodifluoromethane
ug/L1.00.38 U Ethyl Methacrylate
ug/L1.00.13 U Ethylbenzene
ug/L1.00.22 U Hexachlorobutadiene
ug/L5.01.7 U Iodomethane
ug/L5011U Isobutyl alcohol
ug/L2.00.17 U m,p-Xylenes
Page 26 of 34
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L104.9 U Methacrylonitrile
ug/L1.00.51 U Methyl Methacrylate
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Naphthalene
ug/L1.00.065 U o-Xylene
ug/L105.0 U Propionitrile
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.80 U Tetrahydrofuran
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10753
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10452
ug/L 50.0 67-127Surrogate: Toluene-d8 10452
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:37LCS (3A21027-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310020 1,1-Dichloroethene
ug/L1.0 20.0 81-1349419 Benzene
ug/L1.0 20.0 83-11710421 Chlorobenzene
ug/L1.0 20.0 71-11810020 Toluene
ug/L1.0 20.0 74-1199419 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11357
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10753
ug/L 50.0 67-127Surrogate: Toluene-d8 10251
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:06Matrix Spike (3A21027-MS1)
Source: C300689-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331060.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-134960.15 U19 Benzene
ug/L1.0 20.0 83-1171080.17 U22 Chlorobenzene
ug/L1.0 20.0 71-1181050.14 U21 Toluene
ug/L1.0 20.0 74-1191040.15 U21 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10351
Page 27 of 34
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:35Matrix Spike Dup (3A21027-MSD1)
Source: C300689-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133100 60.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-13494 30.15 U19 Benzene
ug/L1.0 20.0 1683-117107 0.70.17 U21 Chlorobenzene
ug/L1.0 20.0 1771-118102 20.14 U20 Toluene
ug/L1.0 20.0 2274-119104 0.50.15 U21 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10352
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 3A21019 - EPA 7470A
Prepared: 01/21/2013 10:48 Analyzed: 01/22/2013 16:23Blank (3A21019-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.2000.170 U Mercury
Prepared: 01/21/2013 10:48 Analyzed: 01/22/2013 16:25LCS (3A21019-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 80-120924.62 Mercury
Prepared: 01/21/2013 10:48 Analyzed: 01/22/2013 16:29Matrix Spike (3A21019-MS1)
Source: C300031-04
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 75-125980.170 U4.88 Mercury
Prepared: 01/21/2013 10:48 Analyzed: 01/22/2013 16:32Matrix Spike Dup (3A21019-MSD1)
Source: C300031-04
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 2575-12596 20.170 U4.79 Mercury
Prepared: 01/21/2013 10:48 Analyzed: 01/22/2013 16:34Post Spike (3A21019-PS1)
Source: C300031-04
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 75-125860.06904.36 Mercury
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:38Blank (3A18017-BLK1)
Page 28 of 34
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:38Blank (3A18017-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.02.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.00 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.01.90 U Lead
ug/L10.01.80 U Nickel
ug/L10.04.50 U Selenium
ug/L10.01.90 U Silver
ug/L10.02.10 U Tin
ug/L10.01.40 U Vanadium
ug/L10.03.80 U Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:41LCS (3A18017-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-120106212 Arsenic
ug/L10.0 200 80-120106212 Barium
ug/L1.00 20.0 80-12010521.0 Beryllium
ug/L1.00 20.0 80-12011122.1 Cadmium
ug/L10.0 200 80-120105210 Chromium
ug/L10.0 200 80-120109219 Cobalt
ug/L10.0 200 80-120103206 Copper
ug/L10.0 200 80-120105211 Lead
ug/L10.0 200 80-120107214 Nickel
ug/L10.0 200 80-120107213 Selenium
ug/L10.0 200 80-120107214 Silver
ug/L10.0 200 80-120104209 Tin
ug/L10.0 200 80-120105209 Vanadium
ug/L10.0 200 80-120108216 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:46Matrix Spike (3A18017-MS1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251082.80 U216 Arsenic
ug/L10.0 200 75-12510616.1229 Barium
ug/L1.00 20.0 75-1251070.100 U21.4 Beryllium
ug/L1.00 20.0 75-1251050.360 U21.0 Cadmium
ug/L10.0 200 75-1251061.00 U212 Chromium
ug/L10.0 200 75-1251101.72223 Cobalt
ug/L10.0 200 75-1251051.60 U209 Copper
ug/L10.0 200 75-1251071.90 U214 Lead
ug/L10.0 200 75-1251061.80 U212 Nickel
ug/L10.0 200 75-1251074.50 U214 Selenium
ug/L10.0 200 75-1251091.90 U217 Silver
Page 29 of 34
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:46Matrix Spike (3A18017-MS1) Continued
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251092.16219 Tin
ug/L10.0 200 75-1251091.40 U217 Vanadium
ug/L10.0 200 75-1251063.80 U212 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:48Matrix Spike Dup (3A18017-MSD1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125107 12.80 U214 Arsenic
ug/L10.0 200 2075-125108 116.1232 Barium
ug/L1.00 20.0 2075-125112 50.100 U22.4 Beryllium
ug/L1.00 20.0 2075-125110 40.360 U22.0 Cadmium
ug/L10.0 200 2075-125110 31.00 U219 Chromium
ug/L10.0 200 2075-125111 0.21.72223 Cobalt
ug/L10.0 200 2075-125108 41.60 U217 Copper
ug/L10.0 200 2075-125107 0.21.90 U213 Lead
ug/L10.0 200 2075-125108 21.80 U217 Nickel
ug/L10.0 200 2075-125110 34.50 U220 Selenium
ug/L10.0 200 2075-125114 51.90 U228 Silver
ug/L10.0 200 2075-125109 0.62.16221 Tin
ug/L10.0 200 2075-125113 41.40 U225 Vanadium
ug/L10.0 200 2075-125108 23.80 U216 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:50Post Spike (3A18017-PS1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120101-0.002150.200 Arsenic
mg/L0.0100 0.200 80-1201000.01610.217 Barium
mg/L0.00100 0.0200 80-120102-5.42E-50.0204 Beryllium
mg/L0.00100 0.0200 80-120102-0.0003670.0201 Cadmium
mg/L0.0100 0.200 80-120101-0.0004260.202 Chromium
mg/L0.0100 0.200 80-1201040.001720.209 Cobalt
mg/L0.0100 0.200 80-120100-0.001080.199 Copper
mg/L0.0100 0.200 80-1201007.65E-50.200 Lead
mg/L0.0100 0.200 80-1201010.0006480.202 Nickel
mg/L0.0100 0.200 80-120105-0.009140.200 Selenium
mg/L0.0100 0.200 80-120105-0.0003190.210 Silver
mg/L0.0100 0.200 80-1201020.002160.206 Tin
mg/L0.0100 0.200 80-1201030.0005810.206 Vanadium
mg/L0.0100 0.200 80-1201060.003570.216 Zinc
Batch 3A18023 - EPA 3005A
Prepared: 01/18/2013 12:41 Analyzed: 01/23/2013 12:59Blank (3A18023-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18023 - EPA 3005A
Prepared: 01/18/2013 12:41 Analyzed: 01/23/2013 12:59Blank (3A18023-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.220 U Antimony
ug/L1.000.110 U Thallium
Prepared: 01/18/2013 12:41 Analyzed: 01/23/2013 13:03LCS (3A18023-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120105211 Antimony
ug/L1.00 200 80-120104208 Thallium
Prepared: 01/18/2013 12:41 Analyzed: 01/23/2013 13:11Matrix Spike (3A18023-MS1)
Source: C300054-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-125930.977186 Antimony
ug/L1.00 200 75-1251020.110 U204 Thallium
Prepared: 01/18/2013 12:41 Analyzed: 01/23/2013 13:15Matrix Spike Dup (3A18023-MSD1)
Source: C300054-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-12593 0.10.977187 Antimony
ug/L1.00 200 2075-125102 0.40.110 U205 Thallium
Prepared: 01/18/2013 12:41 Analyzed: 01/23/2013 13:19Post Spike (3A18023-PS1)
Source: C300054-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201090.977219 Antimony
ug/L1.00 200 80-1201020.0449204 Thallium
Classical Chemistry Parameters - Quality Control
Batch 3A18037 - NO PREP
Prepared & Analyzed: 01/18/2013 18:54Blank (3A18037-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.00.50 U Turbidity
Prepared & Analyzed: 01/18/2013 18:54LCS (3A18037-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.0 20.4 90-11010221 Turbidity
Prepared & Analyzed: 01/18/2013 18:54Duplicate (3A18037-DUP1)
Source: C300054-01
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A18037 - NO PREP
Prepared & Analyzed: 01/18/2013 18:54Duplicate (3A18037-DUP1) Continued
Source: C300054-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.0 2511717 Turbidity
Page 32 of 34
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
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Page 34 of 34
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): C300053
Charlotte, NC 28208
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 1110192, Project Name/Desc: Albemarle LF
Attn: Danny Hefner
Shield Engineering, Inc. (SH007)
4301 Taggart Creek Road
Stephanie Franz
Project Manager
Thursday, January 31, 2013
RE: Laboratory Results for
Dear Danny Hefner,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, January 18, 2013.
The total number of pages in this report, including this page is 56.
www.encolabs.com
PROJECT NARRATIVE
Date:31 January 2013
Client:Shield Engineering, Inc. (SH007)
Project:Albemarle LF
Lab ID:C300053
Overview
Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods
referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in
the QC Remarks section below.
Quality Control Samples
No Comments
Quality Control Remarks
The determination of pH is considered a field parameter, and as such, has a holding time of approximately 15 minutes. As
this time passed prior to receipt by ENCO, the analysis was conducted outside of holding time, and the result is appropriately
qualified (Q-flagged)
Other Comments
The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any
exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of
the report.
Released By:
Environmental Conservation Laboratories, Inc.
Stephanie Franz
Project Manager
Page 2 of 56
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SAMPLE SUMMARY/LABORATORY CHRONICLE
8401-MW14 C300053-01 Sampled:01/17/13 09:33 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:06
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:07
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 16:33
8401-MW15 C300053-02 Sampled:01/17/13 09:01 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 12:43
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:11
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 17:04
8401-MW16S C300053-03 Sampled:01/17/13 08:46 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:09
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:15
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 17:34
8401-MW16D C300053-04 Sampled:01/17/13 09:00 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:11
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:19
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 18:05
8401-MW17 C300053-05 Sampled:01/17/13 09:30 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:14
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:23
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 18:36
8401-MW18 C300053-06 Sampled:01/17/13 10:03 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:16
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:27
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 19:06
Page 3 of 56
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8401-MW19 C300053-07 Sampled:01/17/13 10:00 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:19
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:31
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 19:37
8401-MW22 C300053-08 Sampled:01/17/13 10:29 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:21
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:43
8401-MW22 C300053-08RE1 Sampled:01/17/13 10:29 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 01/31/13 01/22/13 07:18 1/23/2013 04:44
8401-MW26 C300053-09 Sampled:01/17/13 10:30 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:23
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:47
EPA 8260B 01/31/13 01/21/13 08:16 1/21/2013 20:37
8401-MW27 C300053-10 Sampled:01/17/13 10:57 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/16/13 01/18/13 11:40 1/21/2013 13:39
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:51
8401-MW27 C300053-10RE1 Sampled:01/17/13 10:57 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 01/31/13 01/22/13 07:18 1/23/2013 05:13
8401-LAGOON C300053-11 Sampled:01/17/13 11:17 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 353.2 01/19/13 11:17 01/18/13 16:28 1/18/2013 18:14
EPA 353.2 02/14/13 01/23/13 08:14 1/23/2013 12:31
EPA 353.2 10/13/15 01/28/13 17:03 1/28/2013 17:28
EPA 365.4 02/14/13 01/23/13 08:00 1/24/2013 12:07
EPA 6010C 07/16/13 01/18/13 11:40 1/23/2013 13:36
EPA 6020A 07/16/13 01/18/13 12:39 1/23/2013 12:55
EPA 8260B 01/31/13 01/21/13 13:04 1/22/2013 02:05
SM 2540D 01/24/13 01/24/13 09:51 1/24/2013 09:51
SM 5210B 01/19/13 11:17 01/18/13 17:58 1/18/2013 17:58
SM 5220D 02/14/13 01/21/13 10:50 1/21/2013 13:57
SM4500-H/B 01/17/13 11:31 01/18/13 16:41 1/18/2013 16:41
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8401-LAGOON C300053-11RE1 Sampled:01/17/13 11:17 Received:01/18/13 09:50Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/14/13 01/21/13 08:08 1/23/2013 17:52
Page 5 of 56
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW14 C300053-01
Flag NotesMDLNC SWSLMRLDF
3.14 ug/L EPA 6010CJ 10010.01.001Barium - Total
2.63 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
14.7 ug/L EPA 6010CJ 5010.01.801Nickel - Total
2.97 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
4.12 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW15 C300053-02
Flag NotesMDLNC SWSLMRLDF
16.1 ug/L EPA 6010CJ 10010.01.001Barium - Total
1.72 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW16S C300053-03
Flag NotesMDLNC SWSLMRLDF
0.255 ug/L EPA 6020AJ 62.000.2201Antimony - Total
4.08 ug/L EPA 6010CJ 10010.01.001Barium - Total
1.93 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
3.27 ug/L EPA 6010CJ 5010.01.801Nickel - Total
4.63 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW16D C300053-04
Flag NotesMDLNC SWSLMRLDF
0.440 ug/L EPA 6020AJ 62.000.2201Antimony - Total
39.2 ug/L EPA 6010CJ 10010.01.001Barium - Total
1.97 ug/L EPA 6010CJ 1010.01.001Chromium - Total
50.8 ug/L EPA 6010C 1010.01.101Cobalt - Total
10.1 ug/L EPA 6010C 1010.01.601Copper - Total
9.23 ug/L EPA 6010CJ 5010.01.801Nickel - Total
5.29 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW17 C300053-05
Flag NotesMDLNC SWSLMRLDF
0.296 ug/L EPA 6020AJ 62.000.2201Antimony - Total
8.51 ug/L EPA 6010CJ 10010.01.001Barium - Total
2.45 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
2.24 ug/L EPA 6010CJ 1010.01.601Copper - Total
1.98 ug/L EPA 6010CJ 5010.01.801Nickel - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW18 C300053-06
Flag NotesMDLNC SWSLMRLDF
4.33 ug/L EPA 6010CJ 1010.02.801Arsenic - Total
5.21 ug/L EPA 6010CJ 10010.01.001Barium - Total
3.00 ug/L EPA 6010CJ 5010.01.801Nickel - Total
1.76 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW19 C300053-07
Flag NotesMDLNC SWSLMRLDF
0.357 ug/L EPA 6020AJ 62.000.2201Antimony - Total
7.08 ug/L EPA 6010CJ 10010.01.001Barium - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW19 C300053-07
Flag NotesMDLNC SWSLMRLDF
4.21 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
7.33 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW22 C300053-08
Flag NotesMDLNC SWSLMRLDF
0.422 ug/L EPA 6020AJ 62.000.2201Antimony - Total
44.1 ug/L EPA 6010CJ 10010.01.001Barium - Total
36.8 ug/L EPA 6010C 1010.01.101Cobalt - Total
11.3 ug/L EPA 6010CJ 5010.01.801Nickel - Total
1.60 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
6.10 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW26 C300053-09
Flag NotesMDLNC SWSLMRLDF
0.274 ug/L EPA 6020AJ 62.000.2201Antimony - Total
18.6 ug/L EPA 6010CJ 10010.01.001Barium - Total
6.40 ug/L EPA 6010CJ 1010.01.001Chromium - Total
2.33 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
5.47 ug/L EPA 6010CJ 1010.01.601Copper - Total
12.5 ug/L EPA 6010CJ 5010.01.801Nickel - Total
8.04 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
14.0 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW27 C300053-10
Flag NotesMDLNC SWSLMRLDF
34.9 ug/L EPA 6010CJ 10010.01.001Barium - Total
19.9 ug/L EPA 6010C 1010.01.101Cobalt - Total
15.1 ug/L EPA 6010CJ 5010.01.801Nickel - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-LAGOON C300053-11
Flag NotesMDLNC SWSLMRLDF
6.6 ug/L EPA 8260BJ 1005.01.312-Butanone
46 ug/L EPA 8260BJ 1005.01.21Acetone
8.19 ug/L EPA 6010CJ 1010.02.801Arsenic - Total
85.1 ug/L EPA 6010CJ 10010.01.001Barium - Total
0.48 ug/L EPA 8260BJ 11.00.151Benzene
32000 ug/L SM 5210B NE200020001Biochemical Oxygen Demand
300000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
11.2 ug/L EPA 6010C 1010.01.001Chromium - Total
19.6 ug/L EPA 6010C 1010.01.101Cobalt - Total
0.42 ug/L EPA 8260BJ 11.00.131Ethylbenzene
31.1 ug/L EPA 6010CJ 5010.01.801Nickel - Total
1000 ug/L EPA 353.2J 10000100251Nitrate as N
1100 ug/L EPA 353.2 NE100251Nitrate/Nitrite as N
70 ug/L EPA 353.2J 10001003.01Nitrite as N
7.7 pH SM4500-H/B QNE1.01.01pH
240 ug/L EPA 365.4 NE100241Phosphorus
22000 ug/L SM 2540D NE100010001Total Suspended Solids
3.47 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
2.9 ug/L EPA 8260BJ 53.00.451Xylenes (Total)
18.3 ug/L EPA 6010C 1010.03.801Zinc - Total
Page 7 of 56
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-LAGOON C300053-11RE1
Flag NotesMDLNC SWSLMRLDF
170000 ug/L EPA 300.0JD 250000200001604Sulfate as SO4
Page 8 of 56
www.encolabs.com
ANALYTICAL RESULTS
8401-MW14Description:Lab Sample ID:C300053-01 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:33 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 16:331,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 16:331,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 16:331,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 16:331,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 16:331,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 16:331,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 16:331,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 16:331,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 16:331,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 16:331,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 16:331,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 16:331,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 16:331,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 16:332-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 16:332-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 16:334-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 16:33Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 16:33Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 16:33Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 16:33Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 16:33Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 16:33Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 16:33Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 16:33Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 16:33Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 16:33Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 16:33Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 16:33Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 16:33Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 16:33cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 16:33cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 16:33Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 16:33Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 16:33Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 16:33Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 16:33Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 16:33Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 16:33Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 16:33Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 16:33trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 16:33trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 16:33trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 16:33Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
Page 9 of 56
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8401-MW14Description:Lab Sample ID:C300053-01 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:33 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 16:33Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 16:33Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 16:33Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/21/13 16:33Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/21/13 16:333A210085350.0 1
Dibromofluoromethane 68-117105 %JKGEPA 8260B 01/21/13 16:333A210085350.0 1
Toluene-d8 67-127104 %JKGEPA 8260B 01/21/13 16:333A210085250.0 1
Page 10 of 56
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8401-MW14Description:Lab Sample ID:C300053-01 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:33 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:07Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/21/13 13:06Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:06Barium [7440-39-3] ^1 1.00 JDH10.03.14 J 100
ug/L EPA 6010C 01/21/13 13:06Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:06Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:06Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:06Cobalt [7440-48-4] ^1 1.10 JDH10.02.63 J 10
ug/L EPA 6010C 01/21/13 13:06Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:06Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:06Nickel [7440-02-0] ^1 1.80 JDH10.014.7 J 50
ug/L EPA 6010C 01/21/13 13:06Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:06Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:07Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:06Vanadium [7440-62-2] ^1 1.40 JDH10.02.97 J 25
ug/L EPA 6010C 01/21/13 13:06Zinc [7440-66-6] ^1 3.80 JDH10.04.12 J 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 56
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8401-MW15Description:Lab Sample ID:C300053-02 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:01 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 17:041,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 17:041,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 17:041,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 17:041,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 17:041,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 17:041,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 17:041,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 17:041,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 17:041,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 17:041,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 17:041,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 17:041,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 17:041,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 17:042-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 17:042-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 17:044-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 17:04Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 17:04Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 17:04Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 17:04Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 17:04Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 17:04Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 17:04Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 17:04Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 17:04Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 17:04Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 17:04Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 17:04Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 17:04Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 17:04cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 17:04cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 17:04Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 17:04Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 17:04Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 17:04Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 17:04Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 17:04Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 17:04Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 17:04Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 17:04trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 17:04trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 17:04trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 17:04Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 17:04Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 17:04Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 17:04Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 12 of 56
www.encolabs.com
8401-MW15Description:Lab Sample ID:C300053-02 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:01 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 17:04Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/21/13 17:043A210085350.0 1
Dibromofluoromethane 68-117110 %JKGEPA 8260B 01/21/13 17:043A210085550.0 1
Toluene-d8 67-127104 %JKGEPA 8260B 01/21/13 17:043A210085250.0 1
Page 13 of 56
www.encolabs.com
8401-MW15Description:Lab Sample ID:C300053-02 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:01 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:11Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/21/13 12:43Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 12:43Barium [7440-39-3] ^1 1.00 JDH10.016.1 J 100
ug/L EPA 6010C 01/21/13 12:43Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 12:43Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 12:43Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 12:43Cobalt [7440-48-4] ^1 1.10 JDH10.01.72 J 10
ug/L EPA 6010C 01/21/13 12:43Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 12:43Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 12:43Nickel [7440-02-0] ^1 1.80 JDH10.01.80 U 50
ug/L EPA 6010C 01/21/13 12:43Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 12:43Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:11Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 12:43Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/21/13 12:43Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 14 of 56
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8401-MW16SDescription:Lab Sample ID:C300053-03 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 08:46 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 17:341,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 17:341,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 17:341,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 17:341,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 17:341,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 17:341,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 17:341,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 17:341,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 17:341,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 17:341,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 17:341,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 17:341,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 17:341,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 17:342-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 17:342-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 17:344-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 17:34Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 17:34Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 17:34Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 17:34Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 17:34Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 17:34Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 17:34Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 17:34Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 17:34Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 17:34Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 17:34Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 17:34Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 17:34Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 17:34cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 17:34cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 17:34Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 17:34Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 17:34Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 17:34Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 17:34Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 17:34Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 17:34Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 17:34Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 17:34trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 17:34trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 17:34trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 17:34Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 17:34Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 17:34Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 17:34Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 15 of 56
www.encolabs.com
8401-MW16SDescription:Lab Sample ID:C300053-03 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 08:46 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 17:34Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122104 %JKGEPA 8260B 01/21/13 17:343A210085250.0 1
Dibromofluoromethane 68-117111 %JKGEPA 8260B 01/21/13 17:343A210085650.0 1
Toluene-d8 67-127106 %JKGEPA 8260B 01/21/13 17:343A210085350.0 1
Page 16 of 56
www.encolabs.com
8401-MW16SDescription:Lab Sample ID:C300053-03 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 08:46 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:15Antimony [7440-36-0] ^1 0.220 VLO2.000.255 J 6
ug/L EPA 6010C 01/21/13 13:09Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:09Barium [7440-39-3] ^1 1.00 JDH10.04.08 J 100
ug/L EPA 6010C 01/21/13 13:09Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:09Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:09Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:09Cobalt [7440-48-4] ^1 1.10 JDH10.01.93 J 10
ug/L EPA 6010C 01/21/13 13:09Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:09Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:09Nickel [7440-02-0] ^1 1.80 JDH10.03.27 J 50
ug/L EPA 6010C 01/21/13 13:09Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:09Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:15Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:09Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/21/13 13:09Zinc [7440-66-6] ^1 3.80 JDH10.04.63 J 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 17 of 56
www.encolabs.com
8401-MW16DDescription:Lab Sample ID:C300053-04 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:00 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 18:051,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 18:051,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 18:051,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 18:051,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 18:051,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 18:051,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 18:051,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 18:051,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 18:051,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 18:051,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 18:051,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 18:051,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 18:051,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 18:052-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 18:052-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 18:054-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 18:05Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 18:05Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 18:05Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 18:05Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 18:05Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 18:05Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 18:05Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 18:05Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 18:05Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 18:05Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 18:05Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 18:05Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 18:05Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 18:05cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 18:05cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 18:05Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 18:05Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 18:05Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 18:05Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 18:05Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 18:05Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 18:05Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 18:05Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 18:05trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 18:05trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 18:05trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 18:05Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 18:05Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 18:05Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 18:05Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 18 of 56
www.encolabs.com
8401-MW16DDescription:Lab Sample ID:C300053-04 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:00 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 18:05Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122105 %JKGEPA 8260B 01/21/13 18:053A210085350.0 1
Dibromofluoromethane 68-117109 %JKGEPA 8260B 01/21/13 18:053A210085550.0 1
Toluene-d8 67-127101 %JKGEPA 8260B 01/21/13 18:053A210085050.0 1
Page 19 of 56
www.encolabs.com
8401-MW16DDescription:Lab Sample ID:C300053-04 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:00 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:19Antimony [7440-36-0] ^1 0.220 VLO2.000.440 J 6
ug/L EPA 6010C 01/21/13 13:11Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:11Barium [7440-39-3] ^1 1.00 JDH10.039.2 J 100
ug/L EPA 6010C 01/21/13 13:11Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:11Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:11Chromium [7440-47-3] ^1 1.00 JDH10.01.97 J 10
ug/L EPA 6010C 01/21/13 13:11Cobalt [7440-48-4] ^1 1.10 JDH10.050.8 10
ug/L EPA 6010C 01/21/13 13:11Copper [7440-50-8] ^1 1.60 JDH10.010.1 10
ug/L EPA 6010C 01/21/13 13:11Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:11Nickel [7440-02-0] ^1 1.80 JDH10.09.23 J 50
ug/L EPA 6010C 01/21/13 13:11Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:11Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:19Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:11Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/21/13 13:11Zinc [7440-66-6] ^1 3.80 JDH10.05.29 J 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 20 of 56
www.encolabs.com
8401-MW17Description:Lab Sample ID:C300053-05 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:30 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 18:361,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 18:361,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 18:361,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 18:361,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 18:361,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 18:361,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 18:361,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 18:361,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 18:361,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 18:361,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 18:361,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 18:361,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 18:361,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 18:362-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 18:362-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 18:364-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 18:36Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 18:36Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 18:36Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 18:36Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 18:36Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 18:36Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 18:36Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 18:36Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 18:36Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 18:36Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 18:36Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 18:36Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 18:36Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 18:36cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 18:36cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 18:36Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 18:36Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 18:36Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 18:36Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 18:36Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 18:36Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 18:36Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 18:36Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 18:36trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 18:36trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 18:36trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 18:36Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 18:36Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 18:36Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 18:36Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 21 of 56
www.encolabs.com
8401-MW17Description:Lab Sample ID:C300053-05 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:30 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 18:36Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122105 %JKGEPA 8260B 01/21/13 18:363A210085350.0 1
Dibromofluoromethane 68-117107 %JKGEPA 8260B 01/21/13 18:363A210085450.0 1
Toluene-d8 67-127103 %JKGEPA 8260B 01/21/13 18:363A210085150.0 1
Page 22 of 56
www.encolabs.com
8401-MW17Description:Lab Sample ID:C300053-05 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 09:30 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:23Antimony [7440-36-0] ^1 0.220 VLO2.000.296 J 6
ug/L EPA 6010C 01/21/13 13:14Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:14Barium [7440-39-3] ^1 1.00 JDH10.08.51 J 100
ug/L EPA 6010C 01/21/13 13:14Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:14Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:14Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:14Cobalt [7440-48-4] ^1 1.10 JDH10.02.45 J 10
ug/L EPA 6010C 01/21/13 13:14Copper [7440-50-8] ^1 1.60 JDH10.02.24 J 10
ug/L EPA 6010C 01/21/13 13:14Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:14Nickel [7440-02-0] ^1 1.80 JDH10.01.98 J 50
ug/L EPA 6010C 01/21/13 13:14Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:14Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:23Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:14Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/21/13 13:14Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 23 of 56
www.encolabs.com
8401-MW18Description:Lab Sample ID:C300053-06 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:03 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 19:061,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 19:061,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 19:061,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 19:061,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 19:061,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 19:061,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 19:061,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 19:061,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 19:061,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 19:061,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 19:061,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 19:061,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 19:061,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 19:062-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 19:062-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 19:064-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 19:06Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 19:06Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 19:06Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 19:06Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 19:06Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 19:06Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 19:06Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 19:06Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 19:06Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 19:06Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 19:06Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 19:06Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 19:06Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 19:06cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 19:06cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 19:06Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 19:06Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 19:06Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 19:06Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 19:06Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 19:06Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 19:06Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 19:06Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 19:06trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 19:06trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 19:06trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 19:06Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 19:06Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 19:06Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 19:06Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 24 of 56
www.encolabs.com
8401-MW18Description:Lab Sample ID:C300053-06 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:03 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 19:06Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/21/13 19:063A210085450.0 1
Dibromofluoromethane 68-117108 %JKGEPA 8260B 01/21/13 19:063A210085450.0 1
Toluene-d8 67-127103 %JKGEPA 8260B 01/21/13 19:063A210085250.0 1
Page 25 of 56
www.encolabs.com
8401-MW18Description:Lab Sample ID:C300053-06 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:03 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:27Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/21/13 13:16Arsenic [7440-38-2] ^1 2.80 JDH10.04.33 J 10
ug/L EPA 6010C 01/21/13 13:16Barium [7440-39-3] ^1 1.00 JDH10.05.21 J 100
ug/L EPA 6010C 01/21/13 13:16Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:16Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:16Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:16Cobalt [7440-48-4] ^1 1.10 JDH10.01.10 U 10
ug/L EPA 6010C 01/21/13 13:16Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:16Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:16Nickel [7440-02-0] ^1 1.80 JDH10.03.00 J 50
ug/L EPA 6010C 01/21/13 13:16Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:16Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:27Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:16Vanadium [7440-62-2] ^1 1.40 JDH10.01.76 J 25
ug/L EPA 6010C 01/21/13 13:16Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 26 of 56
www.encolabs.com
8401-MW19Description:Lab Sample ID:C300053-07 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:00 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 19:371,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 19:371,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 19:371,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 19:371,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 19:371,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 19:371,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 19:371,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 19:371,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 19:371,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 19:371,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 19:371,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 19:371,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 19:371,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 19:372-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 19:372-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 19:374-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 19:37Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 19:37Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 19:37Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 19:37Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 19:37Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 19:37Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 19:37Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 19:37Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 19:37Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 19:37Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 19:37Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 19:37Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 19:37Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 19:37cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 19:37cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 19:37Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 19:37Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 19:37Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 19:37Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 19:37Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 19:37Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 19:37Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 19:37Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 19:37trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 19:37trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 19:37trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 19:37Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 19:37Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 19:37Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 19:37Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 27 of 56
www.encolabs.com
8401-MW19Description:Lab Sample ID:C300053-07 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:00 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 19:37Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122104 %JKGEPA 8260B 01/21/13 19:373A210085250.0 1
Dibromofluoromethane 68-117109 %JKGEPA 8260B 01/21/13 19:373A210085450.0 1
Toluene-d8 67-127102 %JKGEPA 8260B 01/21/13 19:373A210085150.0 1
Page 28 of 56
www.encolabs.com
8401-MW19Description:Lab Sample ID:C300053-07 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:00 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:31Antimony [7440-36-0] ^1 0.220 VLO2.000.357 J 6
ug/L EPA 6010C 01/21/13 13:19Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:19Barium [7440-39-3] ^1 1.00 JDH10.07.08 J 100
ug/L EPA 6010C 01/21/13 13:19Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:19Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:19Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:19Cobalt [7440-48-4] ^1 1.10 JDH10.04.21 J 10
ug/L EPA 6010C 01/21/13 13:19Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:19Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:19Nickel [7440-02-0] ^1 1.80 JDH10.01.80 U 50
ug/L EPA 6010C 01/21/13 13:19Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:19Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:31Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:19Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/21/13 13:19Zinc [7440-66-6] ^1 3.80 JDH10.07.33 J 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 29 of 56
www.encolabs.com
8401-MW22Description:Lab Sample ID:C300053-08 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:29 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/23/13 04:441,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/23/13 04:441,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/23/13 04:441,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/23/13 04:441,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/23/13 04:441,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/23/13 04:441,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/23/13 04:441,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/23/13 04:441,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/23/13 04:441,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/23/13 04:441,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/23/13 04:441,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/23/13 04:441,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/23/13 04:441,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/23/13 04:442-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/23/13 04:442-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/23/13 04:444-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/23/13 04:44Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/23/13 04:44Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/23/13 04:44Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/23/13 04:44Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/23/13 04:44Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/23/13 04:44Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/23/13 04:44Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/23/13 04:44Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/23/13 04:44Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/23/13 04:44Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/23/13 04:44Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/23/13 04:44Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/23/13 04:44Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/23/13 04:44cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/23/13 04:44cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/23/13 04:44Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/23/13 04:44Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/23/13 04:44Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/23/13 04:44Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/23/13 04:44Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/23/13 04:44Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/23/13 04:44Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/23/13 04:44Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/23/13 04:44trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/23/13 04:44trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/23/13 04:44trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/23/13 04:44Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/23/13 04:44Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/23/13 04:44Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/23/13 04:44Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 30 of 56
www.encolabs.com
8401-MW22Description:Lab Sample ID:C300053-08 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:29 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/23/13 04:44Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/23/13 04:443A220215350.0 1
Dibromofluoromethane 68-117108 %JKGEPA 8260B 01/23/13 04:443A220215450.0 1
Toluene-d8 67-127103 %JKGEPA 8260B 01/23/13 04:443A220215250.0 1
Page 31 of 56
www.encolabs.com
8401-MW22Description:Lab Sample ID:C300053-08 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:29 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:43Antimony [7440-36-0] ^1 0.220 VLO2.000.422 J 6
ug/L EPA 6010C 01/21/13 13:21Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:21Barium [7440-39-3] ^1 1.00 JDH10.044.1 J 100
ug/L EPA 6010C 01/21/13 13:21Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:21Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:21Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:21Cobalt [7440-48-4] ^1 1.10 JDH10.036.8 10
ug/L EPA 6010C 01/21/13 13:21Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:21Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:21Nickel [7440-02-0] ^1 1.80 JDH10.011.3 J 50
ug/L EPA 6010C 01/21/13 13:21Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:21Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:43Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:21Vanadium [7440-62-2] ^1 1.40 JDH10.01.60 J 25
ug/L EPA 6010C 01/21/13 13:21Zinc [7440-66-6] ^1 3.80 JDH10.06.10 J 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 32 of 56
www.encolabs.com
8401-MW26Description:Lab Sample ID:C300053-09 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:30 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 20:371,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/21/13 20:371,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/21/13 20:371,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/21/13 20:371,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 20:371,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/21/13 20:371,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 20:371,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 20:371,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/21/13 20:371,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/21/13 20:371,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/21/13 20:371,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/21/13 20:371,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/21/13 20:371,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/21/13 20:372-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/21/13 20:372-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/21/13 20:374-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/21/13 20:37Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/21/13 20:37Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/21/13 20:37Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 20:37Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/21/13 20:37Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 20:37Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/21/13 20:37Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/21/13 20:37Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/21/13 20:37Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 20:37Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 20:37Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/21/13 20:37Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/21/13 20:37Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 20:37cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/21/13 20:37cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/21/13 20:37Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/21/13 20:37Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/21/13 20:37Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/21/13 20:37Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/21/13 20:37Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/21/13 20:37Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/21/13 20:37Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/21/13 20:37Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/21/13 20:37trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/21/13 20:37trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 20:37trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/21/13 20:37Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/21/13 20:37Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/21/13 20:37Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/21/13 20:37Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 33 of 56
www.encolabs.com
8401-MW26Description:Lab Sample ID:C300053-09 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:30 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/21/13 20:37Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122105 %JKGEPA 8260B 01/21/13 20:373A210085350.0 1
Dibromofluoromethane 68-117107 %JKGEPA 8260B 01/21/13 20:373A210085450.0 1
Toluene-d8 67-127102 %JKGEPA 8260B 01/21/13 20:373A210085150.0 1
Page 34 of 56
www.encolabs.com
8401-MW26Description:Lab Sample ID:C300053-09 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:30 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:47Antimony [7440-36-0] ^1 0.220 VLO2.000.274 J 6
ug/L EPA 6010C 01/21/13 13:23Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:23Barium [7440-39-3] ^1 1.00 JDH10.018.6 J 100
ug/L EPA 6010C 01/21/13 13:23Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:23Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:23Chromium [7440-47-3] ^1 1.00 JDH10.06.40 J 10
ug/L EPA 6010C 01/21/13 13:23Cobalt [7440-48-4] ^1 1.10 JDH10.02.33 J 10
ug/L EPA 6010C 01/21/13 13:23Copper [7440-50-8] ^1 1.60 JDH10.05.47 J 10
ug/L EPA 6010C 01/21/13 13:23Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:23Nickel [7440-02-0] ^1 1.80 JDH10.012.5 J 50
ug/L EPA 6010C 01/21/13 13:23Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:23Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:47Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:23Vanadium [7440-62-2] ^1 1.40 JDH10.08.04 J 25
ug/L EPA 6010C 01/21/13 13:23Zinc [7440-66-6] ^1 3.80 JDH10.014.0 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 35 of 56
www.encolabs.com
8401-MW27Description:Lab Sample ID:C300053-10 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:57 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/23/13 05:131,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/23/13 05:131,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/23/13 05:131,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/23/13 05:131,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/23/13 05:131,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/23/13 05:131,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/23/13 05:131,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/23/13 05:131,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/23/13 05:131,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/23/13 05:131,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/23/13 05:131,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/23/13 05:131,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/23/13 05:131,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/23/13 05:132-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/23/13 05:132-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/23/13 05:134-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/23/13 05:13Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/23/13 05:13Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/23/13 05:13Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/23/13 05:13Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/23/13 05:13Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/23/13 05:13Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/23/13 05:13Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/23/13 05:13Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/23/13 05:13Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/23/13 05:13Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/23/13 05:13Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/23/13 05:13Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/23/13 05:13Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/23/13 05:13cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/23/13 05:13cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/23/13 05:13Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/23/13 05:13Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/23/13 05:13Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/23/13 05:13Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/23/13 05:13Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/23/13 05:13Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/23/13 05:13Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/23/13 05:13Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/23/13 05:13trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/23/13 05:13trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/23/13 05:13trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/23/13 05:13Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/23/13 05:13Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/23/13 05:13Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/23/13 05:13Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 36 of 56
www.encolabs.com
8401-MW27Description:Lab Sample ID:C300053-10 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:57 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/23/13 05:13Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/23/13 05:133A220215450.0 1
Dibromofluoromethane 68-117108 %JKGEPA 8260B 01/23/13 05:133A220215450.0 1
Toluene-d8 67-127104 %JKGEPA 8260B 01/23/13 05:133A220215250.0 1
Page 37 of 56
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8401-MW27Description:Lab Sample ID:C300053-10 01/18/13 09:50Received:
Matrix:Ground Water Sampled:01/17/13 10:57 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:51Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/21/13 13:39Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/21/13 13:39Barium [7440-39-3] ^1 1.00 JDH10.034.9 J 100
ug/L EPA 6010C 01/21/13 13:39Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/21/13 13:39Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:39Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/21/13 13:39Cobalt [7440-48-4] ^1 1.10 JDH10.019.9 10
ug/L EPA 6010C 01/21/13 13:39Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/21/13 13:39Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/21/13 13:39Nickel [7440-02-0] ^1 1.80 JDH10.015.1 J 50
ug/L EPA 6010C 01/21/13 13:39Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:39Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:51Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/21/13 13:39Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/21/13 13:39Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 38 of 56
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8401-LAGOONDescription:Lab Sample ID:C300053-11 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:17 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 02:051,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 02:051,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 02:051,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 02:051,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 02:051,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 02:051,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 02:051,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 02:051,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 02:051,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 02:051,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 02:051,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 02:051,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 02:051,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 02:052-Butanone [78-93-3] ^1 1.3 JKG5.06.6 J 100
ug/L EPA 8260B 01/22/13 02:052-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 02:054-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 02:05Acetone [67-64-1] ^1 1.2 JKG5.046J 100
ug/L EPA 8260B 01/22/13 02:05Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 02:05Benzene [71-43-2] ^1 0.15 JKG1.00.48 J 1
ug/L EPA 8260B 01/22/13 02:05Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 02:05Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 02:05Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 02:05Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 02:05Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 02:05Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 02:05Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 02:05Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 02:05Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 02:05Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 02:05cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 02:05cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 02:05Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 02:05Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 02:05Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.42 J 1
ug/L EPA 8260B 01/22/13 02:05Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 02:05Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 02:05Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 02:05Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 02:05Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 02:05trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 02:05trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 02:05trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/22/13 02:05Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 02:05Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 02:05Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/22/13 02:05Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
Page 39 of 56
www.encolabs.com
8401-LAGOONDescription:Lab Sample ID:C300053-11 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:17 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 02:05Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.02.9 J 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122107 %JKGEPA 8260B 01/22/13 02:053A210275450.0 1
Dibromofluoromethane 68-117106 %JKGEPA 8260B 01/22/13 02:053A210275350.0 1
Toluene-d8 67-127103 %JKGEPA 8260B 01/22/13 02:053A210275150.0 1
Page 40 of 56
www.encolabs.com
8401-LAGOONDescription:Lab Sample ID:C300053-11 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:17 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/23/13 12:55Antimony [7440-36-0] ^10 2.20 VLO20.02.20 UD 6
ug/L EPA 6010C 01/23/13 13:36Arsenic [7440-38-2] ^1 2.80 JDH10.08.19 J 10
ug/L EPA 6010C 01/23/13 13:36Barium [7440-39-3] ^1 1.00 JDH10.085.1 J 100
ug/L EPA 6010C 01/23/13 13:36Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/23/13 13:36Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/23/13 13:36Chromium [7440-47-3] ^1 1.00 JDH10.011.2 10
ug/L EPA 6010C 01/23/13 13:36Cobalt [7440-48-4] ^1 1.10 JDH10.019.6 10
ug/L EPA 6010C 01/23/13 13:36Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/23/13 13:36Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/23/13 13:36Nickel [7440-02-0] ^1 1.80 JDH10.031.1 J 50
ug/L EPA 6010C 01/23/13 13:36Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/23/13 13:36Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/23/13 12:55Thallium [7440-28-0] ^10 1.10 VLO10.01.10 UD 5.5
ug/L EPA 6010C 01/23/13 13:36Vanadium [7440-62-2] ^1 1.40 JDH10.03.47 J 25
ug/L EPA 6010C 01/23/13 13:36Zinc [7440-66-6] ^1 3.80 JDH10.018.3 10
Page 41 of 56
www.encolabs.com
8401-LAGOONDescription:Lab Sample ID:C300053-11 01/18/13 09:50Received:
Matrix:Surface Water Sampled:01/17/13 11:17 Work Order:C300053
Albemarle LFProject:Sampled By:Danny Hefner / Joanna Harbison
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5210B 01/18/13 17:58Biochemical Oxygen Demand
[ECL-0017] ^
1 2000 JOC200032000 NE
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC10000300000 NE
ug/L EPA 353.2 01/28/13 17:28Nitrate as N [14797-55-8] ^1 25 JCS1001000J 10000
ug/L EPA 353.2 01/23/13 12:31Nitrate/Nitrite as N [ECL-0010] ^1 25 AJB1001100 NE
ug/L EPA 353.2 01/18/13 18:14Nitrite as N [14797-65-0] ^1 3.0 AJB10070J 1000
pH SM4500-H/B 01/18/13 16:41pH [ECL-0062] ^1 1.0 MPL1.07.7 QNE
ug/L EPA 365.4 01/24/13 12:07Phosphorus [7723-14-0] ^1 24 JCS100240 NE
ug/L EPA 300.0 01/23/13 17:52Sulfate as SO4 [14808-79-8] ^4 160 AJB20000170000JD 250000
ug/L SM 2540D 01/24/13 09:51Total Suspended Solids [ECL-0169] ^1 1000 AJB100022000 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 42 of 56
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21008 - EPA 5030B_MS
Prepared: 01/21/2013 08:16 Analyzed: 01/21/2013 10:27Blank (3A21008-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10753
Page 43 of 56
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21008 - EPA 5030B_MS
Prepared: 01/21/2013 08:16 Analyzed: 01/21/2013 10:27Blank (3A21008-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10251
ug/L 50.0 67-127Surrogate: Toluene-d8 10352
Prepared: 01/21/2013 08:16 Analyzed: 01/21/2013 10:56LCS (3A21008-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1339319 1,1-Dichloroethene
ug/L1.0 20.0 81-1349018 Benzene
ug/L1.0 20.0 83-11710321 Chlorobenzene
ug/L1.0 20.0 71-11810020 Toluene
ug/L1.0 20.0 74-1199519 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10955
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10352
ug/L 50.0 67-127Surrogate: Toluene-d8 10553
Prepared: 01/21/2013 08:16 Analyzed: 01/21/2013 11:26Matrix Spike (3A21008-MS1)
Source: C300573-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331000.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 81-134960.15 U19 Benzene
ug/L1.0 20.0 83-1171070.17 U21 Chlorobenzene
ug/L1.0 20.0 71-1181040.14 U21 Toluene
ug/L1.0 20.0 74-119990.15 U20 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11055
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10352
ug/L 50.0 67-127Surrogate: Toluene-d8 10452
Prepared: 01/21/2013 08:16 Analyzed: 01/21/2013 11:55Matrix Spike Dup (3A21008-MSD1)
Source: C300573-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13392 90.21 U18 1,1-Dichloroethene
ug/L1.0 20.0 1781-13492 30.15 U18 Benzene
ug/L1.0 20.0 1683-117102 50.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-11897 70.14 U19 Toluene
ug/L1.0 20.0 2274-11994 60.15 U19 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10954
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10050
ug/L 50.0 67-127Surrogate: Toluene-d8 10351
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
Page 44 of 56
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10753
Page 45 of 56
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10452
ug/L 50.0 67-127Surrogate: Toluene-d8 10452
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:37LCS (3A21027-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310020 1,1-Dichloroethene
ug/L1.0 20.0 81-1349419 Benzene
ug/L1.0 20.0 83-11710421 Chlorobenzene
ug/L1.0 20.0 71-11810020 Toluene
ug/L1.0 20.0 74-1199419 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11357
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10753
ug/L 50.0 67-127Surrogate: Toluene-d8 10251
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:06Matrix Spike (3A21027-MS1)
Source: C300689-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331060.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-134960.15 U19 Benzene
ug/L1.0 20.0 83-1171080.17 U22 Chlorobenzene
ug/L1.0 20.0 71-1181050.14 U21 Toluene
ug/L1.0 20.0 74-1191040.15 U21 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10351
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:35Matrix Spike Dup (3A21027-MSD1)
Source: C300689-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133100 60.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-13494 30.15 U19 Benzene
ug/L1.0 20.0 1683-117107 0.70.17 U21 Chlorobenzene
ug/L1.0 20.0 1771-118102 20.14 U20 Toluene
ug/L1.0 20.0 2274-119104 0.50.15 U21 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10352
Batch 3A22021 - EPA 5030B_MS
Prepared: 01/22/2013 10:46 Analyzed: 01/23/2013 02:16Blank (3A22021-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
Page 46 of 56
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A22021 - EPA 5030B_MS
Prepared: 01/22/2013 10:46 Analyzed: 01/23/2013 02:16Blank (3A22021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10753
Page 47 of 56
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A22021 - EPA 5030B_MS
Prepared: 01/22/2013 10:46 Analyzed: 01/23/2013 02:16Blank (3A22021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10552
Prepared: 01/22/2013 10:46 Analyzed: 01/23/2013 02:46LCS (3A22021-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310321 1,1-Dichloroethene
ug/L1.0 20.0 81-1349519 Benzene
ug/L1.0 20.0 83-1179820 Chlorobenzene
ug/L1.0 20.0 71-1189619 Toluene
ug/L1.0 20.0 74-1199319 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10854
ug/L 50.0 67-127Surrogate: Toluene-d8 10452
Prepared: 01/22/2013 10:46 Analyzed: 01/23/2013 03:15Matrix Spike (3A22021-MS1)
Source: C300689-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133990.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 81-134920.15 U18 Benzene
ug/L1.0 20.0 83-1171010.17 U20 Chlorobenzene
ug/L1.0 20.0 71-118970.14 U19 Toluene
ug/L1.0 20.0 74-119910.15 U18 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10753
ug/L 50.0 67-127Surrogate: Toluene-d8 10251
Prepared: 01/22/2013 10:46 Analyzed: 01/23/2013 03:45Matrix Spike Dup (3A22021-MSD1)
Source: C300689-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13399 0.050.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-13494 10.15 U19 Benzene
ug/L1.0 20.0 1683-117101 0.20.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-11896 0.30.14 U19 Toluene
ug/L1.0 20.0 2274-11990 0.30.15 U18 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11155
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10251
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:38Blank (3A18017-BLK1)
Page 48 of 56
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:38Blank (3A18017-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.02.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.00 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.01.90 U Lead
ug/L10.01.80 U Nickel
ug/L10.04.50 U Selenium
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.03.80 U Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:41LCS (3A18017-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-120106212 Arsenic
ug/L10.0 200 80-120106212 Barium
ug/L1.00 20.0 80-12010521.0 Beryllium
ug/L1.00 20.0 80-12011122.1 Cadmium
ug/L10.0 200 80-120105210 Chromium
ug/L10.0 200 80-120109219 Cobalt
ug/L10.0 200 80-120103206 Copper
ug/L10.0 200 80-120105211 Lead
ug/L10.0 200 80-120107214 Nickel
ug/L10.0 200 80-120107213 Selenium
ug/L10.0 200 80-120107214 Silver
ug/L10.0 200 80-120105209 Vanadium
ug/L10.0 200 80-120108216 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:46Matrix Spike (3A18017-MS1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251082.80 U216 Arsenic
ug/L10.0 200 75-12510616.1229 Barium
ug/L1.00 20.0 75-1251070.100 U21.4 Beryllium
ug/L1.00 20.0 75-1251050.360 U21.0 Cadmium
ug/L10.0 200 75-1251061.00 U212 Chromium
ug/L10.0 200 75-1251101.72223 Cobalt
ug/L10.0 200 75-1251051.60 U209 Copper
ug/L10.0 200 75-1251071.90 U214 Lead
ug/L10.0 200 75-1251061.80 U212 Nickel
ug/L10.0 200 75-1251074.50 U214 Selenium
ug/L10.0 200 75-1251091.90 U217 Silver
ug/L10.0 200 75-1251091.40 U217 Vanadium
ug/L10.0 200 75-1251063.80 U212 Zinc
Page 49 of 56
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:48Matrix Spike Dup (3A18017-MSD1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125107 12.80 U214 Arsenic
ug/L10.0 200 2075-125108 116.1232 Barium
ug/L1.00 20.0 2075-125112 50.100 U22.4 Beryllium
ug/L1.00 20.0 2075-125110 40.360 U22.0 Cadmium
ug/L10.0 200 2075-125110 31.00 U219 Chromium
ug/L10.0 200 2075-125111 0.21.72223 Cobalt
ug/L10.0 200 2075-125108 41.60 U217 Copper
ug/L10.0 200 2075-125107 0.21.90 U213 Lead
ug/L10.0 200 2075-125108 21.80 U217 Nickel
ug/L10.0 200 2075-125110 34.50 U220 Selenium
ug/L10.0 200 2075-125114 51.90 U228 Silver
ug/L10.0 200 2075-125113 41.40 U225 Vanadium
ug/L10.0 200 2075-125108 23.80 U216 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:50Post Spike (3A18017-PS1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120101-0.002150.200 Arsenic
mg/L0.0100 0.200 80-1201000.01610.217 Barium
mg/L0.00100 0.0200 80-120102-5.42E-50.0204 Beryllium
mg/L0.00100 0.0200 80-120102-0.0003670.0201 Cadmium
mg/L0.0100 0.200 80-120101-0.0004260.202 Chromium
mg/L0.0100 0.200 80-1201040.001720.209 Cobalt
mg/L0.0100 0.200 80-120100-0.001080.199 Copper
mg/L0.0100 0.200 80-1201007.65E-50.200 Lead
mg/L0.0100 0.200 80-1201010.0006480.202 Nickel
mg/L0.0100 0.200 80-120105-0.009140.200 Selenium
mg/L0.0100 0.200 80-120105-0.0003190.210 Silver
mg/L0.0100 0.200 80-1201030.0005810.206 Vanadium
mg/L0.0100 0.200 80-1201060.003570.216 Zinc
Batch 3A18022 - EPA 3005A
Prepared: 01/18/2013 12:39 Analyzed: 01/23/2013 11:07Blank (3A18022-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.220 U Antimony
ug/L1.000.110 U Thallium
Prepared: 01/18/2013 12:39 Analyzed: 01/23/2013 11:11LCS (3A18022-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120101202 Antimony
ug/L1.00 200 80-120102205 Thallium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18022 - EPA 3005A
Prepared: 01/18/2013 12:39 Analyzed: 01/23/2013 11:19Matrix Spike (3A18022-MS1)
Source: C300032-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-125980.977197 Antimony
ug/L1.00 200 75-1251010.110 U201 Thallium
Prepared: 01/18/2013 12:39 Analyzed: 01/23/2013 11:23Matrix Spike Dup (3A18022-MSD1)
Source: C300032-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-12599 20.977200 Antimony
ug/L1.00 200 2075-125101 0.30.110 U202 Thallium
Prepared: 01/18/2013 12:39 Analyzed: 01/23/2013 11:27Post Spike (3A18022-PS1)
Source: C300032-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201050.977211 Antimony
ug/L1.00 200 80-1201040.0711207 Thallium
Classical Chemistry Parameters - Quality Control
Batch 3A18029 - NO PREP
Prepared & Analyzed: 01/18/2013 17:58Blank (3A18029-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L20002000U Biochemical Oxygen Demand
Prepared & Analyzed: 01/18/2013 17:58LCS (3A18029-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2000 198000 85-11594190000 Biochemical Oxygen Demand
Prepared & Analyzed: 01/18/2013 17:58Duplicate (3A18029-DUP1)
Source: C300053-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2000 2503200032000 Biochemical Oxygen Demand
Batch 3A18031 - NO PREP
Prepared & Analyzed: 01/18/2013 16:41LCS (3A18031-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
pH1.0 7.00 99-1011007.0 pH
Prepared & Analyzed: 01/18/2013 16:41Duplicate (3A18031-DUP1)
Source: C200160-01
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A18031 - NO PREP
Prepared & Analyzed: 01/18/2013 16:41Duplicate (3A18031-DUP1) Continued
Source: C200160-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
pH1.0 250.16.96.9 pH
Batch 3A18032 - NO PREP
Prepared: 01/18/2013 16:28 Analyzed: 01/18/2013 18:13Blank (3A18032-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1003.0 U Nitrite as N
Prepared: 01/18/2013 16:28 Analyzed: 01/18/2013 18:11LCS (3A18032-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.00 90-1101011.0 Nitrite as N
Prepared: 01/18/2013 16:28 Analyzed: 01/18/2013 18:14Matrix Spike (3A18032-MS1)
Source: C300053-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 1000 90-11095701000 Nitrite as N
Prepared: 01/18/2013 16:28 Analyzed: 01/18/2013 18:15Matrix Spike Dup (3A18032-MSD1)
Source: C300053-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 1000 1090-11096 0.6701000 Nitrite as N
Batch 3A21005 - NO PREP
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 02:31Blank (3A21005-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L500040U Sulfate as SO4
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 02:14LCS (3A21005-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 50000 90-1109447000 Sulfate as SO4
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 04:51Matrix Spike (3A21005-MS1)
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 90-1101125500077000 QM-05Sulfate as SO4
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 05:09Matrix Spike Dup (3A21005-MSD1)
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A21005 - NO PREP
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 05:09Matrix Spike Dup (3A21005-MSD1) Continued
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 1090-110118 15500078000 QM-05Sulfate as SO4
Batch 3A21014 - Same
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57Blank (3A21014-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000010000U Chemical Oxygen Demand
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57LCS (3A21014-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 90-110102510000 Chemical Oxygen Demand
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57Matrix Spike (3A21014-MS1)
Source: C212850-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 90-11010510000 U520000 Chemical Oxygen Demand
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57Matrix Spike Dup (3A21014-MSD1)
Source: C212850-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 1090-110106 110000 U530000 Chemical Oxygen Demand
Batch 3A22034 - Same
Prepared: 01/23/2013 08:00 Analyzed: 01/24/2013 11:15Blank (3A22034-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10024U Phosphorus
Prepared: 01/23/2013 08:00 Analyzed: 01/24/2013 11:17LCS (3A22034-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 1600 80-1201021600 Phosphorus
Prepared: 01/23/2013 08:00 Analyzed: 01/24/2013 11:20Matrix Spike (3A22034-MS1)
Source: C215728-02RE1
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L200 640 80-12013427003600D QM-05Phosphorus
Prepared: 01/23/2013 08:00 Analyzed: 01/24/2013 11:22Matrix Spike Dup (3A22034-MSD1)
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A22034 - Same
Prepared: 01/23/2013 08:00 Analyzed: 01/24/2013 11:22Matrix Spike Dup (3A22034-MSD1) Continued
Source: C215728-02RE1
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L200 640 2580-120109 527003400D Phosphorus
Batch 3A23006 - NO PREP
Prepared: 01/23/2013 08:14 Analyzed: 01/23/2013 12:22Blank (3A23006-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10025U Nitrate/Nitrite as N
Prepared: 01/23/2013 08:14 Analyzed: 01/23/2013 12:07LCS (3A23006-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.25 90-110951.2 Nitrate/Nitrite as N
Prepared: 01/23/2013 08:14 Analyzed: 01/23/2013 12:26Matrix Spike (3A23006-MS1)
Source: C215731-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000 5000 90-11084790012000 QM-05Nitrate/Nitrite as N
Prepared: 01/23/2013 08:14 Analyzed: 01/23/2013 12:28Matrix Spike Dup (3A23006-MSD1)
Source: C215731-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000 5000 1090-11091 3790012000 Nitrate/Nitrite as N
Batch 3A24003 - NO PREP
Prepared & Analyzed: 01/24/2013 08:45Blank (3A24003-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10001000U Total Suspended Solids
Prepared & Analyzed: 01/24/2013 08:45LCS (3A24003-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L1.0 100 80-120102100 Total Suspended Solids
Prepared & Analyzed: 01/24/2013 09:51Duplicate (3A24003-DUP1)
Source: C215563-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000 251000 U1000U Total Suspended Solids
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Analysis performed outside of method - specified holding time.Q
The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix
interference. The LCS and/or LCSD were within acceptance limits showing that the laboratory is
in control and the data is acceptable.
QM-05
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Page 56 of 56
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): C300052
Charlotte, NC 28208
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 1110192, Project Name/Desc: Albemarle Closed LF
Attn: Danny Hefner
Shield Engineering, Inc. (SH007)
4301 Taggart Creek Road
Stephanie Franz
Project Manager
Tuesday, January 29, 2013
RE: Laboratory Results for
Dear Danny Hefner,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, January 16, 2013.
The total number of pages in this report, including this page is 124.
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
8401-MW2 C300052-01 Sampled:01/15/13 11:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/21/13 08:08 1/23/2013 11:09
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 10:27
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 13:47
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:01
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 15:52
RSK-175 01/29/13 01/22/13 15:54 1/22/2013 17:22
SM 2130B 01/17/13 11:10 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-MW2 C300052-01RE2 Sampled:01/15/13 11:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/28/13 14:17 1/28/2013 22:27
8401-MW3 C300052-02 Sampled:01/15/13 09:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/21/13 08:08 1/23/2013 11:27
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 13:49
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 12:37
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 16:52
SM 2130B 01/17/13 09:10 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-MW3 C300052-02RE1 Sampled:01/15/13 09:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/21/13 08:08 1/23/2013 14:57
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 11:26
RSK-175 01/29/13 01/22/13 15:54 1/23/2013 10:26
8401-MW4R C300052-03 Sampled:01/15/13 11:40 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 13:54
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:05
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 17:22
Page 2 of 124
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8401-MW5R C300052-04 Sampled:01/15/13 11:43 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 13:57
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:17
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 17:51
8401-MW6 C300052-05 Sampled:01/15/13 11:13 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/21/13 08:08 1/23/2013 12:19
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 10:29
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 13:59
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:21
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 18:21
RSK-175 01/29/13 01/22/13 15:54 1/22/2013 17:54
SM 2130B 01/17/13 11:13 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-MW7 C300052-06 Sampled:01/15/13 10:50 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/21/13 08:08 1/23/2013 12:37
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:02
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:25
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 18:52
SM 2130B 01/17/13 10:50 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-MW7 C300052-06RE1 Sampled:01/15/13 10:50 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/21/13 08:08 1/23/2013 15:49
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 11:27
RSK-175 01/29/13 01/22/13 15:54 1/23/2013 10:42
8401-MW8D C300052-07 Sampled:01/15/13 10:11 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:04
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:29
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 19:22
Page 3 of 124
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8401-MW9 C300052-08 Sampled:01/15/13 09:33 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/28/13 14:17 1/28/2013 23:20
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 10:31
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:06
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:33
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 19:52
RSK-175 01/29/13 01/22/13 15:54 1/22/2013 18:27
SM 2130B 01/17/13 09:33 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-MW10 C300052-09 Sampled:01/15/13 09:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/28/13 14:17 1/28/2013 23:37
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:16
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:37
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 20:21
RSK-175 01/29/13 01/22/13 15:54 1/22/2013 18:43
SM 2130B 01/17/13 09:10 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-MW10 C300052-09RE1 Sampled:01/15/13 09:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 11:27
8401-MW10 C300052-09RE2 Sampled:01/15/13 09:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/28/13 14:17 1/29/2013 10:19
8401-MW11 C300052-10 Sampled:01/15/13 09:40 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:19
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:41
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 20:51
SM 2130B 01/17/13 09:40 01/16/13 16:05 1/16/2013 16:05
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8401-MW12 C300052-11 Sampled:01/15/13 12:00 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:21
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:45
EPA 7470A 02/12/13 01/17/13 16:08 1/18/2013 17:09
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 21:21
SM 2130B 01/17/13 12:00 01/16/13 16:05 1/16/2013 16:05
8401-MW13 C300052-12 Sampled:01/15/13 12:03 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:23
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:49
EPA 7470A 02/12/13 01/17/13 16:08 1/18/2013 17:11
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 21:51
SM 2130B 01/17/13 12:03 01/16/13 16:05 1/16/2013 16:05
8401-MW23 C300052-13 Sampled:01/15/13 12:30 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:26
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 13:53
EPA 7470A 02/12/13 01/17/13 16:08 1/18/2013 17:13
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 22:21
EPA 8270D 01/22/13 01/18/13 11:45 1/23/2013 17:1602/27/13
SM 2130B 01/17/13 12:30 01/16/13 16:05 1/16/2013 16:05
8401-MW24 C300052-14 Sampled:01/15/13 10:16 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/28/13 14:17 1/28/2013 23:55
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 10:33
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:33
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 14:05
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 22:50
RSK-175 01/29/13 01/22/13 15:54 1/22/2013 18:59
SM 2130B 01/17/13 10:16 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
Page 5 of 124
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8401-MW25 C300052-15 Sampled:01/15/13 10:41 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/12/13 01/28/13 14:17 1/29/2013 00:12
EPA 310.2 01/29/13 01/20/13 08:25 1/20/2013 10:35
EPA 353.2 10/11/15 01/21/13 12:29 1/21/2013 12:58
EPA 6010C 07/14/13 01/18/13 11:40 1/21/2013 13:01
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 14:09
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 23:21
RSK-175 01/29/13 01/22/13 15:54 1/22/2013 19:15
SM 2130B 01/17/13 10:41 01/16/13 16:05 1/16/2013 16:05
SM 5220D 02/12/13 01/21/13 10:50 1/21/2013 13:57
SM18 4500-S D 01/22/13 01/22/13 12:05 1/22/2013 12:39
SM18 5310B 02/12/13 01/21/13 11:00 1/21/2013 12:05
8401-Trip Blank C300052-16 Sampled:01/15/13 09:10 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 01/29/13 01/21/13 13:04 1/22/2013 01:36
8401-Bailer Blank C300052-17 Sampled:01/15/13 12:25 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:38
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 14:13
EPA 7470A 02/12/13 01/17/13 16:08 1/18/2013 17:15
EPA 8260B 01/29/13 01/18/13 09:48 1/18/2013 23:51
8401-Field Blank C300052-18 Sampled:01/15/13 12:35 Received:01/16/13 08:20Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010C 07/14/13 01/16/13 10:13 1/17/2013 14:40
EPA 6020A 07/14/13 01/16/13 10:16 1/18/2013 14:17
EPA 8260B 01/29/13 01/18/13 09:54 1/19/2013 11:45
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW2 C300052-01
Flag NotesMDLNC SWSLMRLDF
9.07 ug/L EPA 6010CJ 1010.02.801Arsenic - Total
171 ug/L EPA 6010C 10010.01.001Barium - Total
6.92 ug/L EPA 6010C 11.000.1001Beryllium - Total
190000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
42000 ug/L EPA 300.0B QB-01NE50004301Chloride
21.7 ug/L EPA 6010C 1010.01.001Chromium - Total
951 ug/L EPA 6010C 1010.01.101Cobalt - Total
70.0 ug/L EPA 6010C 1010.01.601Copper - Total
29300 ug/L EPA 6010C 30050.022.01Iron - Total
65.9 ug/L EPA 6010C 1010.01.901Lead - Total
0.00261 mg/L RSK-175 NE0.001000.0004301Methane
1050 ug/L EPA 6010C 5010.01.801Nickel - Total
96 ug/L EPA 353.2J 10000100251Nitrate as N
2.83 ug/L EPA 6010CJ 1010.01.901Silver - Total
54000 ug/L EPA 310.2 NE15000120001Total Alkalinity as CaCO3
7.5 mg/L SM18 5310B NE1.00.321Total Organic Carbon
4900 NTU SM 2130BD NE200100200Turbidity
38.6 ug/L EPA 6010C 2510.01.401Vanadium - Total
632 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW2 C300052-01RE2
Flag NotesMDLNC SWSLMRLDF
720000 ug/L EPA 300.0D 2500005000039010Sulfate as SO4
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW3 C300052-02
Flag NotesMDLNC SWSLMRLDF
3.8 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
1.9 ug/L EPA 8260B 11.00.1911,4-Dichlorobenzene
19.8 ug/L EPA 6010C 1010.02.801Arsenic - Total
22.9 ug/L EPA 6010CJ 10010.01.001Barium - Total
43000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
8.2 ug/L EPA 8260B 31.00.171Chlorobenzene
3.97 ug/L EPA 6010CJ 1010.01.001Chromium - Total
0.85 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
21.0 ug/L EPA 6010C 1010.01.101Cobalt - Total
28.3 ug/L EPA 6010C 1010.01.601Copper - Total
1860 ug/L EPA 6010C 30050.022.01Iron - Total
4.33 ug/L EPA 6010CJ 1010.01.901Lead - Total
4.00 ug/L EPA 6010CJ 5010.01.801Nickel - Total
23000 ug/L EPA 300.0J 2500005000401Sulfate as SO4
2.9 ug/L EPA 8260B NE1.00.801Tetrahydrofuran
6.4 mg/L SM18 5310B NE1.00.321Total Organic Carbon
0.82 ug/L EPA 8260BJ 11.00.151Trichloroethene
14 NTU SM 2130B NE1.00.501Turbidity
2.83 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
4.34 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW3 C300052-02RE1
Flag NotesMDLNC SWSLMRLDF
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW3 C300052-02RE1
Flag NotesMDLNC SWSLMRLDF
130000 ug/L EPA 300.0BD QB-01NE2000017004Chloride
0.235 mg/L RSK-175D NE0.01000.0043010Methane
440000 ug/L EPA 310.2D NE60000480004Total Alkalinity as CaCO3
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW4R C300052-03
Flag NotesMDLNC SWSLMRLDF
2.47 ug/L EPA 6010CJ 10010.01.001Barium - Total
1.04 ug/L EPA 6010CJ 1010.01.001Chromium - Total
2.31 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
6.52 ug/L EPA 6010CJ 5010.01.801Nickel - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW5R C300052-04
Flag NotesMDLNC SWSLMRLDF
8.55 ug/L EPA 6010CJ 10010.01.001Barium - Total
2.58 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW6 C300052-05
Flag NotesMDLNC SWSLMRLDF
2.3 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
13000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
14000 ug/L EPA 300.0B J-01NE50004301Chloride
0.44 ug/L EPA 8260BJ 31.00.171Chlorobenzene
1.20 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
114 ug/L EPA 6010CJ 30050.022.01Iron - Total
0.00121 mg/L RSK-175 NE0.001000.0004301Methane
1.5 ug/L EPA 8260B 11.00.231Methylene chloride
2.09 ug/L EPA 6010CJ 5010.01.801Nickel - Total
7200 ug/L EPA 353.2J 10000100251Nitrate as N
13000 ug/L EPA 300.0J 2500005000401Sulfate as SO4
0.67 ug/L EPA 8260BJ 11.00.171Tetrachloroethene
2.1 ug/L EPA 8260B NE1.00.801Tetrahydrofuran
30000 ug/L EPA 310.2 NE15000120001Total Alkalinity as CaCO3
2.8 mg/L SM18 5310B NE1.00.321Total Organic Carbon
7.5 ug/L EPA 8260B 11.00.241Trichlorofluoromethane
9.7 NTU SM 2130B NE1.00.501Turbidity
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW7 C300052-06
Flag NotesMDLNC SWSLMRLDF
2.6 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
2.8 ug/L EPA 8260B 11.00.1911,4-Dichlorobenzene
24.5 ug/L EPA 6010CJ 10010.01.001Barium - Total
2.4 ug/L EPA 8260B 11.00.151Benzene
2.33 ug/L EPA 6010C 11.000.3601Cadmium - Total
39000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
7.9 ug/L EPA 8260B 31.00.171Chlorobenzene
2.79 ug/L EPA 6010CJ 1010.01.001Chromium - Total
1.6 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
5.32 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
720 ug/L EPA 6010C 30050.022.01Iron - Total
6.55 ug/L EPA 6010CJ 5010.01.801Nickel - Total
6100 ug/L EPA 300.0J 2500005000401Sulfate as SO4
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW7 C300052-06
Flag NotesMDLNC SWSLMRLDF
0.40 ug/L EPA 8260BJ 11.00.171Tetrachloroethene
2.5 ug/L EPA 8260B NE1.00.801Tetrahydrofuran
7.7 mg/L SM18 5310B NE1.00.321Total Organic Carbon
6.25 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
7.25 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW7 C300052-06RE1
Flag NotesMDLNC SWSLMRLDF
160000 ug/L EPA 300.0BD QB-01NE2000017004Chloride
0.278 mg/L RSK-175D NE0.01000.0043010Methane
680000 ug/L EPA 310.2D NE60000480004Total Alkalinity as CaCO3
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW8D C300052-07
Flag NotesMDLNC SWSLMRLDF
9.19 ug/L EPA 6010CJ 10010.01.001Barium - Total
10.8 ug/L EPA 6010C 1010.01.101Cobalt - Total
2.39 ug/L EPA 6010CJ 5010.01.801Nickel - Total
0.97 ug/L EPA 8260BJ 11.00.171Tetrachloroethene
7.39 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW9 C300052-08
Flag NotesMDLNC SWSLMRLDF
0.44 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
7.19 ug/L EPA 6010CJ 10010.01.001Barium - Total
20000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
59000 ug/L EPA 300.0B QB-01NE50004301Chloride
2.38 ug/L EPA 6010CJ 1010.01.001Chromium - Total
0.55 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
630 ug/L EPA 6010C 30050.022.01Iron - Total
2.49 ug/L EPA 6010CJ 5010.01.801Nickel - Total
200 ug/L EPA 353.2J 10000100251Nitrate as N
15000 ug/L EPA 300.0J 2500005000401Sulfate as SO4
0.98 ug/L EPA 8260BJ 11.00.171Tetrachloroethene
41000 ug/L EPA 310.2 NE15000120001Total Alkalinity as CaCO3
1.3 mg/L SM18 5310B NE1.00.321Total Organic Carbon
0.72 ug/L EPA 8260BJ 11.00.151Trichloroethene
180 NTU SM 2130BD NE105.010Turbidity
3.25 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW10 C300052-09
Flag NotesMDLNC SWSLMRLDF
71.7 ug/L EPA 6010CJ 10010.01.001Barium - Total
72000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
1.41 ug/L EPA 6010CJ 1010.01.001Chromium - Total
1.95 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
42.5 ug/L EPA 6010CJ 30050.022.01Iron - Total
2.01 ug/L EPA 6010CJ 1010.01.901Lead - Total
16.3 ug/L EPA 6010CJ 5010.01.801Nickel - Total
37000 ug/L EPA 353.2 10000100251Nitrate as N
22000 ug/L EPA 300.0J 2500005000401Sulfate as SO4
9.6 mg/L SM18 5310B NE1.00.321Total Organic Carbon
Page 9 of 124
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW10 C300052-09
Flag NotesMDLNC SWSLMRLDF
3.1 NTU SM 2130B NE1.00.501Turbidity
3.87 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW10 C300052-09RE1
Flag NotesMDLNC SWSLMRLDF
340000 ug/L EPA 310.2D NE60000480004Total Alkalinity as CaCO3
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW10 C300052-09RE2
Flag NotesMDLNC SWSLMRLDF
470000 ug/L EPA 300.0BD QB-01NE50000430010Chloride
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW11 C300052-10
Flag NotesMDLNC SWSLMRLDF
18 ug/L EPA 8260B 51.00.1311,1-Dichloroethane
80.3 ug/L EPA 6010CJ 10010.01.001Barium - Total
0.87 ug/L EPA 8260BJ 11.00.151Benzene
4.8 ug/L EPA 8260BJ 101.00.231Chloroethane
30.6 ug/L EPA 6010C 1010.01.001Chromium - Total
5.8 ug/L EPA 8260B 51.00.151cis-1,2-Dichloroethene
9.74 ug/L EPA 6010CJ 1010.01.101Cobalt - Total
7.20 ug/L EPA 6010CJ 1010.01.601Copper - Total
68.4 ug/L EPA 6010C 5010.01.801Nickel - Total
28 NTU SM 2130B NE1.00.501Turbidity
16.4 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
2.2 ug/L EPA 8260B 11.00.321Vinyl chloride
12.5 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW12 C300052-11
Flag NotesMDLNC SWSLMRLDF
4.6 ug/L EPA 8260BJ 1005.01.21Acetone
3.27 ug/L EPA 6010CJ 1010.02.801Arsenic - Total
60.4 ug/L EPA 6010CJ 10010.01.001Barium - Total
3.58 ug/L EPA 6010CJ 1010.01.001Chromium - Total
43.5 ug/L EPA 6010C 1010.01.101Cobalt - Total
57.6 ug/L EPA 6010C 5010.01.801Nickel - Total
2.22 ug/L EPA 6010CJ 1010.01.901Silver - Total
3.96 ug/L EPA 6010CJ 10010.02.101Tin - Total
8.7 NTU SM 2130B NE1.00.501Turbidity
1.49 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
5.37 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW13 C300052-12
Flag NotesMDLNC SWSLMRLDF
36.1 ug/L EPA 6010CJ 10010.01.001Barium - Total
2.07 ug/L EPA 6010CJ 1010.01.001Chromium - Total
18.6 ug/L EPA 6010C 1010.01.101Cobalt - Total
5.65 ug/L EPA 6010CJ 10010.02.101Tin - Total
13 NTU SM 2130B NE1.00.501Turbidity
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW23 C300052-13
Flag NotesMDLNC SWSLMRLDF
Page 10 of 124
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW23 C300052-13
Flag NotesMDLNC SWSLMRLDF
3.1 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
49.7 ug/L EPA 6010CJ 10010.01.001Barium - Total
0.87 ug/L EPA 8260BJ 11.00.151Benzene
1.8 ug/L EPA 8260BJ 101.00.231Chloroethane
1.81 ug/L EPA 6010CJ 1010.01.001Chromium - Total
17 ug/L EPA 8260B 51.00.151cis-1,2-Dichloroethene
30.6 ug/L EPA 6010C 1010.01.101Cobalt - Total
12.8 ug/L EPA 6010CJ 5010.01.801Nickel - Total
5.28 ug/L EPA 6010CJ 10010.02.101Tin - Total
19 NTU SM 2130B NE1.00.501Turbidity
1.8 ug/L EPA 8260B 11.00.321Vinyl chloride
5.12 ug/L EPA 6010CJ 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW24 C300052-14
Flag NotesMDLNC SWSLMRLDF
41.3 ug/L EPA 6010CJ 10010.01.001Barium - Total
0.400 ug/L EPA 6010CJ 11.000.1001Beryllium - Total
59000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
64000 ug/L EPA 300.0B QB-01NE50004301Chloride
17.7 ug/L EPA 6010C 1010.01.001Chromium - Total
14.1 ug/L EPA 6010C 1010.01.101Cobalt - Total
34.3 ug/L EPA 6010C 1010.01.601Copper - Total
9550 ug/L EPA 6010C 30050.022.01Iron - Total
7.63 ug/L EPA 6010CJ 1010.01.901Lead - Total
14.4 ug/L EPA 6010CJ 5010.01.801Nickel - Total
70 ug/L EPA 353.2J 10000100251Nitrate as N
49000 ug/L EPA 300.0J 2500005000401Sulfate as SO4
66000 ug/L EPA 310.2 NE15000120001Total Alkalinity as CaCO3
4.6 mg/L SM18 5310B NE1.00.321Total Organic Carbon
320 NTU SM 2130BD NE105.010Turbidity
17.7 ug/L EPA 6010CJ 2510.01.401Vanadium - Total
32.9 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW25 C300052-15
Flag NotesMDLNC SWSLMRLDF
40.3 ug/L EPA 6010C 1010.02.801Arsenic - Total
301 ug/L EPA 6010C 10010.01.001Barium - Total
3.60 ug/L EPA 6010C 11.000.1001Beryllium - Total
110000 ug/L SM 5220D NE10000100001Chemical Oxygen Demand
17000 ug/L EPA 300.0B QB-01NE50004301Chloride
152 ug/L EPA 6010C 1010.01.001Chromium - Total
35.9 ug/L EPA 6010C 1010.01.101Cobalt - Total
99.4 ug/L EPA 6010C 1010.01.601Copper - Total
111000 ug/L EPA 6010C 30050.022.01Iron - Total
58.7 ug/L EPA 6010C 1010.01.901Lead - Total
95.3 ug/L EPA 6010C 5010.01.801Nickel - Total
1200 ug/L EPA 353.2J 10000100251Nitrate as N
3.76 ug/L EPA 6010CJ 1010.01.901Silver - Total
35000 ug/L EPA 300.0J 2500005000401Sulfate as SO4
17000 ug/L EPA 310.2 NE15000120001Total Alkalinity as CaCO3
7.6 mg/L SM18 5310B NE1.00.321Total Organic Carbon
Page 11 of 124
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Analyte MethodUnitsResults
Lab ID:Client ID:8401-MW25 C300052-15
Flag NotesMDLNC SWSLMRLDF
6400 NTU SM 2130BD NE200100200Turbidity
174 ug/L EPA 6010C 2510.01.401Vanadium - Total
172 ug/L EPA 6010C 1010.03.801Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:8401-Bailer Blank C300052-17
Flag NotesMDLNC SWSLMRLDF
1.14 ug/L EPA 6010CJ 10010.01.001Barium - Total
0.54 ug/L EPA 8260BJ 11.00.231Methylene chloride
Analyte MethodUnitsResults
Lab ID:Client ID:8401-Field Blank C300052-18
Flag NotesMDLNC SWSLMRLDF
0.55 ug/L EPA 8260BJ 11.00.231Methylene chloride
Page 12 of 124
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ANALYTICAL RESULTS
8401-MW2Description:Lab Sample ID:C300052-01 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 15:521,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 15:521,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 15:521,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 15:521,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 15:521,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 15:521,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 15:521,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 15:521,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 15:521,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 15:521,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 15:521,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 15:521,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 15:521,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 15:522-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 15:522-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 15:524-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 15:52Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 15:52Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 15:52Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 15:52Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 15:52Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 15:52Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 15:52Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 15:52Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 15:52Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 15:52Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 15:52Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 15:52Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 15:52Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 15:52cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 15:52cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 15:52Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 15:52Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 15:52Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 15:52Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 15:52Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 15:52Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 15:52Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 15:52Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 15:52Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 15:52trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 15:52trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 15:52trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
Page 13 of 124
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8401-MW2Description:Lab Sample ID:C300052-01 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 15:52Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 15:52Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 15:52Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/18/13 15:52Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 15:52Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12283 %JKGEPA 8260B 01/18/13 15:523A180114250.0 1
Dibromofluoromethane 68-11786 %JKGEPA 8260B 01/18/13 15:523A180114350.0 1
Toluene-d8 67-12787 %JKGEPA 8260B 01/18/13 15:523A180114350.0 1
Page 14 of 124
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8401-MW2Description:Lab Sample ID:C300052-01 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:01Antimony [7440-36-0] ^10 2.20 VLO20.02.20 UD R-016
ug/L EPA 6010C 01/17/13 13:47Arsenic [7440-38-2] ^1 2.80 JDH10.09.07 J 10
ug/L EPA 6010C 01/17/13 13:47Barium [7440-39-3] ^1 1.00 JDH10.0171 100
ug/L EPA 6010C 01/17/13 13:47Beryllium [7440-41-7] ^1 0.100 JDH1.006.92 1
ug/L EPA 6010C 01/17/13 13:47Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 13:47Chromium [7440-47-3] ^1 1.00 JDH10.021.7 10
ug/L EPA 6010C 01/17/13 13:47Cobalt [7440-48-4] ^1 1.10 JDH10.0951 10
ug/L EPA 6010C 01/17/13 13:47Copper [7440-50-8] ^1 1.60 JDH10.070.0 10
ug/L EPA 6010C 01/17/13 13:47Iron [7439-89-6] ^1 22.0 JDH50.029300 300
ug/L EPA 6010C 01/17/13 13:47Lead [7439-92-1] ^1 1.90 JDH10.065.9 10
ug/L EPA 6010C 01/17/13 13:47Nickel [7440-02-0] ^1 1.80 JDH10.01050 50
ug/L EPA 6010C 01/17/13 13:47Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 13:47Silver [7440-22-4] ^1 1.90 JDH10.02.83 J 10
ug/L EPA 6020A 01/18/13 13:01Thallium [7440-28-0] ^10 1.10 VLO10.01.10 UD R-015.5
ug/L EPA 6010C 01/17/13 13:47Vanadium [7440-62-2] ^1 1.40 JDH10.038.6 25
ug/L EPA 6010C 01/17/13 13:47Zinc [7440-66-6] ^1 3.80 JDH10.0632 10
Page 15 of 124
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8401-MW2Description:Lab Sample ID:C300052-01 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC10000190000 NE
ug/L EPA 300.0 01/23/13 11:09Chloride [16887-00-6] ^1 430 AJB500042000B QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS10096J 10000
ug/L EPA 300.0 01/28/13 22:27Sulfate as SO4 [14808-79-8] ^10 390 AJB50000720000D 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 10:27Total Alkalinity as CaCO3 [471-34-1] ^1 12000 JCS1500054000 NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^200 100 JOC2004900D NE
Page 16 of 124
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8401-MW2Description:Lab Sample ID:C300052-01 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.07.5 NE
Page 17 of 124
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8401-MW2Description:Lab Sample ID:C300052-01 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/22/13 17:22Methane [74-82-8]1 0.000430 GMB0.001000.00261 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 18 of 124
www.encolabs.com
8401-MW3Description:Lab Sample ID:C300052-02 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 16:521,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 16:521,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 16:521,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 16:521,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 16:521,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.03.8 J 5
ug/L EPA 8260B 01/18/13 16:521,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 16:521,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 16:521,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 16:521,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 16:521,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 16:521,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 16:521,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 16:521,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.01.9 1
ug/L EPA 8260B 01/18/13 16:522-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 16:522-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 16:524-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 16:52Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 16:52Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 16:52Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 16:52Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 16:52Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 16:52Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 16:52Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 16:52Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 16:52Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 16:52Chlorobenzene [108-90-7] ^1 0.17 JKG1.08.2 3
ug/L EPA 8260B 01/18/13 16:52Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 16:52Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 16:52Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 16:52cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.85 J 5
ug/L EPA 8260B 01/18/13 16:52cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 16:52Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 16:52Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 16:52Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 16:52Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 16:52Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 16:52Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 16:52Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 16:52Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.02.9 NE
ug/L EPA 8260B 01/18/13 16:52Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 16:52trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 16:52trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 16:52trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 16:52Trichloroethene [79-01-6] ^1 0.15 JKG1.00.82 J 1
ug/L EPA 8260B 01/18/13 16:52Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 16:52Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 19 of 124
www.encolabs.com
8401-MW3Description:Lab Sample ID:C300052-02 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 16:52Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 16:52Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12284 %JKGEPA 8260B 01/18/13 16:523A180114250.0 1
Dibromofluoromethane 68-11790 %JKGEPA 8260B 01/18/13 16:523A180114550.0 1
Toluene-d8 67-12789 %JKGEPA 8260B 01/18/13 16:523A180114450.0 1
Page 20 of 124
www.encolabs.com
8401-MW3Description:Lab Sample ID:C300052-02 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 12:37Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 13:49Arsenic [7440-38-2] ^1 2.80 JDH10.019.8 10
ug/L EPA 6010C 01/17/13 13:49Barium [7440-39-3] ^1 1.00 JDH10.022.9 J 100
ug/L EPA 6010C 01/17/13 13:49Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 13:49Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 13:49Chromium [7440-47-3] ^1 1.00 JDH10.03.97 J 10
ug/L EPA 6010C 01/17/13 13:49Cobalt [7440-48-4] ^1 1.10 JDH10.021.0 10
ug/L EPA 6010C 01/17/13 13:49Copper [7440-50-8] ^1 1.60 JDH10.028.3 10
ug/L EPA 6010C 01/17/13 13:49Iron [7439-89-6] ^1 22.0 JDH50.01860 300
ug/L EPA 6010C 01/17/13 13:49Lead [7439-92-1] ^1 1.90 JDH10.04.33 J 10
ug/L EPA 6010C 01/17/13 13:49Nickel [7440-02-0] ^1 1.80 JDH10.04.00 J 50
ug/L EPA 6010C 01/17/13 13:49Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 13:49Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 12:37Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 13:49Vanadium [7440-62-2] ^1 1.40 JDH10.02.83 J 25
ug/L EPA 6010C 01/17/13 13:49Zinc [7440-66-6] ^1 3.80 JDH10.04.34 J 10
Page 21 of 124
www.encolabs.com
8401-MW3Description:Lab Sample ID:C300052-02 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC1000043000 NE
ug/L EPA 300.0 01/23/13 14:57Chloride [16887-00-6] ^4 1700 AJB20000130000BD QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS10025U 10000
ug/L EPA 300.0 01/23/13 11:27Sulfate as SO4 [14808-79-8] ^1 40 AJB500023000J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 11:26Total Alkalinity as CaCO3 [471-34-1] ^4 48000 JCS60000440000D NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.014 NE
Page 22 of 124
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8401-MW3Description:Lab Sample ID:C300052-02 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.06.4 NE
Page 23 of 124
www.encolabs.com
8401-MW3Description:Lab Sample ID:C300052-02 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/23/13 10:26Methane [74-82-8]10 0.00430 GMB0.01000.235 D NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 24 of 124
www.encolabs.com
8401-MW4RDescription:Lab Sample ID:C300052-03 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 17:221,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 17:221,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 17:221,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 17:221,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 17:221,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 17:221,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 17:221,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 17:221,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 17:221,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 17:221,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 17:221,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 17:221,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 17:221,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 17:222-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 17:222-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 17:224-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 17:22Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 17:22Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 17:22Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 17:22Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 17:22Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 17:22Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 17:22Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 17:22Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 17:22Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 17:22Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 17:22Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 17:22Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 17:22Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 17:22cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 17:22cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 17:22Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 17:22Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 17:22Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 17:22Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 17:22Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 17:22Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 17:22Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 17:22Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 17:22Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 17:22trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 17:22trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 17:22trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 17:22Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 17:22Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 17:22Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 25 of 124
www.encolabs.com
8401-MW4RDescription:Lab Sample ID:C300052-03 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 17:22Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 17:22Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12286 %JKGEPA 8260B 01/18/13 17:223A180114350.0 1
Dibromofluoromethane 68-11791 %JKGEPA 8260B 01/18/13 17:223A180114650.0 1
Toluene-d8 67-12790 %JKGEPA 8260B 01/18/13 17:223A180114550.0 1
Page 26 of 124
www.encolabs.com
8401-MW4RDescription:Lab Sample ID:C300052-03 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:05Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 13:54Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 13:54Barium [7440-39-3] ^1 1.00 JDH10.02.47 J 100
ug/L EPA 6010C 01/17/13 13:54Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 13:54Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 13:54Chromium [7440-47-3] ^1 1.00 JDH10.01.04 J 10
ug/L EPA 6010C 01/17/13 13:54Cobalt [7440-48-4] ^1 1.10 JDH10.02.31 J 10
ug/L EPA 6010C 01/17/13 13:54Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 13:54Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 13:54Nickel [7440-02-0] ^1 1.80 JDH10.06.52 J 50
ug/L EPA 6010C 01/17/13 13:54Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 13:54Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:05Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 13:54Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 13:54Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 27 of 124
www.encolabs.com
8401-MW5RDescription:Lab Sample ID:C300052-04 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:43 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 17:511,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 17:511,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 17:511,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 17:511,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 17:511,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 17:511,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 17:511,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 17:511,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 17:511,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 17:511,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 17:511,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 17:511,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 17:511,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 17:512-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 17:512-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 17:514-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 17:51Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 17:51Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 17:51Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 17:51Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 17:51Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 17:51Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 17:51Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 17:51Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 17:51Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 17:51Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 17:51Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 17:51Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 17:51Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 17:51cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 17:51cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 17:51Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 17:51Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 17:51Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 17:51Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 17:51Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 17:51Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 17:51Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 17:51Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 17:51Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 17:51trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 17:51trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 17:51trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 17:51Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 17:51Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 17:51Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 28 of 124
www.encolabs.com
8401-MW5RDescription:Lab Sample ID:C300052-04 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:43 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 17:51Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 17:51Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12282 %JKGEPA 8260B 01/18/13 17:513A180114150.0 1
Dibromofluoromethane 68-11788 %JKGEPA 8260B 01/18/13 17:513A180114450.0 1
Toluene-d8 67-12789 %JKGEPA 8260B 01/18/13 17:513A180114450.0 1
Page 29 of 124
www.encolabs.com
8401-MW5RDescription:Lab Sample ID:C300052-04 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:43 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:17Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 13:57Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 13:57Barium [7440-39-3] ^1 1.00 JDH10.08.55 J 100
ug/L EPA 6010C 01/17/13 13:57Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 13:57Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 13:57Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/17/13 13:57Cobalt [7440-48-4] ^1 1.10 JDH10.02.58 J 10
ug/L EPA 6010C 01/17/13 13:57Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 13:57Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 13:57Nickel [7440-02-0] ^1 1.80 JDH10.01.80 U 50
ug/L EPA 6010C 01/17/13 13:57Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 13:57Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:17Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 13:57Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 13:57Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 30 of 124
www.encolabs.com
8401-MW6Description:Lab Sample ID:C300052-05 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:13 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 18:211,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 18:211,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 18:211,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 18:211,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 18:211,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.02.3 J 5
ug/L EPA 8260B 01/18/13 18:211,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 18:211,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 18:211,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 18:211,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 18:211,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 18:211,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 18:211,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 18:211,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 18:212-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 18:212-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 18:214-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 18:21Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 18:21Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 18:21Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 18:21Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 18:21Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 18:21Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 18:21Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 18:21Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 18:21Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 18:21Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.44 J 3
ug/L EPA 8260B 01/18/13 18:21Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 18:21Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 18:21Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 18:21cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 18:21cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 18:21Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 18:21Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 18:21Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 18:21Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 18:21Methylene chloride [75-09-2] ^1 0.23 JKG1.01.5 1
ug/L EPA 8260B 01/18/13 18:21Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 18:21Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.67 J 1
ug/L EPA 8260B 01/18/13 18:21Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.02.1 NE
ug/L EPA 8260B 01/18/13 18:21Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 18:21trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 18:21trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 18:21trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 18:21Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 18:21Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.07.5 1
ug/L EPA 8260B 01/18/13 18:21Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 31 of 124
www.encolabs.com
8401-MW6Description:Lab Sample ID:C300052-05 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:13 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 18:21Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 18:21Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12282 %JKGEPA 8260B 01/18/13 18:213A180114150.0 1
Dibromofluoromethane 68-11790 %JKGEPA 8260B 01/18/13 18:213A180114550.0 1
Toluene-d8 67-12788 %JKGEPA 8260B 01/18/13 18:213A180114450.0 1
Page 32 of 124
www.encolabs.com
8401-MW6Description:Lab Sample ID:C300052-05 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:13 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:21Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 13:59Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 13:59Barium [7440-39-3] ^1 1.00 JDH10.01.00 U 100
ug/L EPA 6010C 01/17/13 13:59Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 13:59Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 13:59Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/17/13 13:59Cobalt [7440-48-4] ^1 1.10 JDH10.01.20 J 10
ug/L EPA 6010C 01/17/13 13:59Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 13:59Iron [7439-89-6] ^1 22.0 JDH50.0114J 300
ug/L EPA 6010C 01/17/13 13:59Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 13:59Nickel [7440-02-0] ^1 1.80 JDH10.02.09 J 50
ug/L EPA 6010C 01/17/13 13:59Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 13:59Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:21Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 13:59Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 13:59Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
Page 33 of 124
www.encolabs.com
8401-MW6Description:Lab Sample ID:C300052-05 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:13 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC1000013000 NE
ug/L EPA 300.0 01/23/13 12:19Chloride [16887-00-6] ^1 430 AJB500014000B J-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS1007200J 10000
ug/L EPA 300.0 01/23/13 12:19Sulfate as SO4 [14808-79-8] ^1 40 AJB500013000J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 10:29Total Alkalinity as CaCO3 [471-34-1] ^1 12000 JCS1500030000 NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.09.7 NE
Page 34 of 124
www.encolabs.com
8401-MW6Description:Lab Sample ID:C300052-05 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:13 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.02.8 NE
Page 35 of 124
www.encolabs.com
8401-MW6Description:Lab Sample ID:C300052-05 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 11:13 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/22/13 17:54Methane [74-82-8]1 0.000430 GMB0.001000.00121 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 36 of 124
www.encolabs.com
8401-MW7Description:Lab Sample ID:C300052-06 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:50 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 18:521,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 18:521,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 18:521,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 18:521,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 18:521,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.02.6 J 5
ug/L EPA 8260B 01/18/13 18:521,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 18:521,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 18:521,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 18:521,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 18:521,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 18:521,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 18:521,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 18:521,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.02.8 1
ug/L EPA 8260B 01/18/13 18:522-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 18:522-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 18:524-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 18:52Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 18:52Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 18:52Benzene [71-43-2] ^1 0.15 JKG1.02.4 1
ug/L EPA 8260B 01/18/13 18:52Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 18:52Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 18:52Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 18:52Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 18:52Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 18:52Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 18:52Chlorobenzene [108-90-7] ^1 0.17 JKG1.07.9 3
ug/L EPA 8260B 01/18/13 18:52Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 18:52Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 18:52Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 18:52cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.01.6 J 5
ug/L EPA 8260B 01/18/13 18:52cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 18:52Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 18:52Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 18:52Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 18:52Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 18:52Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 18:52Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 18:52Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.40 J 1
ug/L EPA 8260B 01/18/13 18:52Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.02.5 NE
ug/L EPA 8260B 01/18/13 18:52Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 18:52trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 18:52trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 18:52trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 18:52Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 18:52Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 18:52Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 37 of 124
www.encolabs.com
8401-MW7Description:Lab Sample ID:C300052-06 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:50 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 18:52Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 18:52Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12282 %JKGEPA 8260B 01/18/13 18:523A180114150.0 1
Dibromofluoromethane 68-11788 %JKGEPA 8260B 01/18/13 18:523A180114450.0 1
Toluene-d8 67-12787 %JKGEPA 8260B 01/18/13 18:523A180114450.0 1
Page 38 of 124
www.encolabs.com
8401-MW7Description:Lab Sample ID:C300052-06 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:50 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:25Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:02Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:02Barium [7440-39-3] ^1 1.00 JDH10.024.5 J 100
ug/L EPA 6010C 01/17/13 14:02Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:02Cadmium [7440-43-9] ^1 0.360 JDH1.002.33 1
ug/L EPA 6010C 01/17/13 14:02Chromium [7440-47-3] ^1 1.00 JDH10.02.79 J 10
ug/L EPA 6010C 01/17/13 14:02Cobalt [7440-48-4] ^1 1.10 JDH10.05.32 J 10
ug/L EPA 6010C 01/17/13 14:02Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:02Iron [7439-89-6] ^1 22.0 JDH50.0720 300
ug/L EPA 6010C 01/17/13 14:02Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:02Nickel [7440-02-0] ^1 1.80 JDH10.06.55 J 50
ug/L EPA 6010C 01/17/13 14:02Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:02Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:25Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:02Vanadium [7440-62-2] ^1 1.40 JDH10.06.25 J 25
ug/L EPA 6010C 01/17/13 14:02Zinc [7440-66-6] ^1 3.80 JDH10.07.25 J 10
Page 39 of 124
www.encolabs.com
8401-MW7Description:Lab Sample ID:C300052-06 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:50 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC1000039000 NE
ug/L EPA 300.0 01/23/13 15:49Chloride [16887-00-6] ^4 1700 AJB20000160000BD QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS10025U 10000
ug/L EPA 300.0 01/23/13 12:37Sulfate as SO4 [14808-79-8] ^1 40 AJB50006100J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 11:27Total Alkalinity as CaCO3 [471-34-1] ^4 48000 JCS60000680000D NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.00.50 U NE
Page 40 of 124
www.encolabs.com
8401-MW7Description:Lab Sample ID:C300052-06 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:50 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.07.7 NE
Page 41 of 124
www.encolabs.com
8401-MW7Description:Lab Sample ID:C300052-06 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:50 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/23/13 10:42Methane [74-82-8]10 0.00430 GMB0.01000.278 D NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 42 of 124
www.encolabs.com
8401-MW8DDescription:Lab Sample ID:C300052-07 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:11 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 19:221,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 19:221,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 19:221,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 19:221,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 19:221,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 19:221,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 19:221,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 19:221,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 19:221,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 19:221,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 19:221,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 19:221,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 19:221,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 19:222-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 19:222-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 19:224-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 19:22Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 19:22Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 19:22Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 19:22Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 19:22Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 19:22Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 19:22Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 19:22Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 19:22Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 19:22Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 19:22Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 19:22Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 19:22Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 19:22cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 19:22cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 19:22Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 19:22Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 19:22Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 19:22Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 19:22Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 19:22Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 19:22Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.97 J 1
ug/L EPA 8260B 01/18/13 19:22Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 19:22Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 19:22trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 19:22trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 19:22trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 19:22Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 19:22Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 19:22Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 43 of 124
www.encolabs.com
8401-MW8DDescription:Lab Sample ID:C300052-07 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:11 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 19:22Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 19:22Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12283 %JKGEPA 8260B 01/18/13 19:223A180114150.0 1
Dibromofluoromethane 68-11788 %JKGEPA 8260B 01/18/13 19:223A180114450.0 1
Toluene-d8 67-12788 %JKGEPA 8260B 01/18/13 19:223A180114450.0 1
Page 44 of 124
www.encolabs.com
8401-MW8DDescription:Lab Sample ID:C300052-07 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:11 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:29Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:04Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:04Barium [7440-39-3] ^1 1.00 JDH10.09.19 J 100
ug/L EPA 6010C 01/17/13 14:04Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:04Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:04Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/17/13 14:04Cobalt [7440-48-4] ^1 1.10 JDH10.010.8 10
ug/L EPA 6010C 01/17/13 14:04Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:04Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:04Nickel [7440-02-0] ^1 1.80 JDH10.02.39 J 50
ug/L EPA 6010C 01/17/13 14:04Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:04Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:29Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:04Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 14:04Zinc [7440-66-6] ^1 3.80 JDH10.07.39 J 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 45 of 124
www.encolabs.com
8401-MW9Description:Lab Sample ID:C300052-08 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:33 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 19:521,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 19:521,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 19:521,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 19:521,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 19:521,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.44 J 5
ug/L EPA 8260B 01/18/13 19:521,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 19:521,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 19:521,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 19:521,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 19:521,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 19:521,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 19:521,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 19:521,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 19:522-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 19:522-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 19:524-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 19:52Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 19:52Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 19:52Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 19:52Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 19:52Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 19:52Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 19:52Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 19:52Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 19:52Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 19:52Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 19:52Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 19:52Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 19:52Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 19:52cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.55 J 5
ug/L EPA 8260B 01/18/13 19:52cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 19:52Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 19:52Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 19:52Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 19:52Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 19:52Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 19:52Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 19:52Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.98 J 1
ug/L EPA 8260B 01/18/13 19:52Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 19:52Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 19:52trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 19:52trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 19:52trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 19:52Trichloroethene [79-01-6] ^1 0.15 JKG1.00.72 J 1
ug/L EPA 8260B 01/18/13 19:52Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 19:52Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 46 of 124
www.encolabs.com
8401-MW9Description:Lab Sample ID:C300052-08 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:33 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 19:52Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 19:52Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12283 %JKGEPA 8260B 01/18/13 19:523A180114150.0 1
Dibromofluoromethane 68-11791 %JKGEPA 8260B 01/18/13 19:523A180114650.0 1
Toluene-d8 67-12788 %JKGEPA 8260B 01/18/13 19:523A180114450.0 1
Page 47 of 124
www.encolabs.com
8401-MW9Description:Lab Sample ID:C300052-08 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:33 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:33Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:06Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:06Barium [7440-39-3] ^1 1.00 JDH10.07.19 J 100
ug/L EPA 6010C 01/17/13 14:06Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:06Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:06Chromium [7440-47-3] ^1 1.00 JDH10.02.38 J 10
ug/L EPA 6010C 01/17/13 14:06Cobalt [7440-48-4] ^1 1.10 JDH10.01.10 U 10
ug/L EPA 6010C 01/17/13 14:06Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:06Iron [7439-89-6] ^1 22.0 JDH50.0630 300
ug/L EPA 6010C 01/17/13 14:06Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:06Nickel [7440-02-0] ^1 1.80 JDH10.02.49 J 50
ug/L EPA 6010C 01/17/13 14:06Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:06Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:33Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:06Vanadium [7440-62-2] ^1 1.40 JDH10.03.25 J 25
ug/L EPA 6010C 01/17/13 14:06Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
Page 48 of 124
www.encolabs.com
8401-MW9Description:Lab Sample ID:C300052-08 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:33 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC1000020000 NE
ug/L EPA 300.0 01/28/13 23:20Chloride [16887-00-6] ^1 430 AJB500059000B QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS100200J 10000
ug/L EPA 300.0 01/28/13 23:20Sulfate as SO4 [14808-79-8] ^1 40 AJB500015000J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 10:31Total Alkalinity as CaCO3 [471-34-1] ^1 12000 JCS1500041000 NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^10 5.0 JOC10180D NE
Page 49 of 124
www.encolabs.com
8401-MW9Description:Lab Sample ID:C300052-08 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:33 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.01.3 NE
Page 50 of 124
www.encolabs.com
8401-MW9Description:Lab Sample ID:C300052-08 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:33 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/22/13 18:27Methane [74-82-8]1 0.000430 GMB0.001000.000430 U NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 51 of 124
www.encolabs.com
8401-MW10Description:Lab Sample ID:C300052-09 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 20:211,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 20:211,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 20:211,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 20:211,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 20:211,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 20:211,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 20:211,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 20:211,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 20:211,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 20:211,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 20:211,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 20:211,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 20:211,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 20:212-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 20:212-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 20:214-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 20:21Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 20:21Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 20:21Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 20:21Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 20:21Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 20:21Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 20:21Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 20:21Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 20:21Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 20:21Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 20:21Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 20:21Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 20:21Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 20:21cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 20:21cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 20:21Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 20:21Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 20:21Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 20:21Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 20:21Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 20:21Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 20:21Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 20:21Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 20:21Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 20:21trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 20:21trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 20:21trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 20:21Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 20:21Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 20:21Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 52 of 124
www.encolabs.com
8401-MW10Description:Lab Sample ID:C300052-09 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 20:21Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 20:21Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12283 %JKGEPA 8260B 01/18/13 20:213A180114150.0 1
Dibromofluoromethane 68-11790 %JKGEPA 8260B 01/18/13 20:213A180114550.0 1
Toluene-d8 67-12789 %JKGEPA 8260B 01/18/13 20:213A180114450.0 1
Page 53 of 124
www.encolabs.com
8401-MW10Description:Lab Sample ID:C300052-09 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:37Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:16Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:16Barium [7440-39-3] ^1 1.00 JDH10.071.7 J 100
ug/L EPA 6010C 01/17/13 14:16Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:16Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:16Chromium [7440-47-3] ^1 1.00 JDH10.01.41 J 10
ug/L EPA 6010C 01/17/13 14:16Cobalt [7440-48-4] ^1 1.10 JDH10.01.95 J 10
ug/L EPA 6010C 01/17/13 14:16Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:16Iron [7439-89-6] ^1 22.0 JDH50.042.5 J 300
ug/L EPA 6010C 01/17/13 14:16Lead [7439-92-1] ^1 1.90 JDH10.02.01 J 10
ug/L EPA 6010C 01/17/13 14:16Nickel [7440-02-0] ^1 1.80 JDH10.016.3 J 50
ug/L EPA 6010C 01/17/13 14:16Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:16Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:37Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:16Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 14:16Zinc [7440-66-6] ^1 3.80 JDH10.03.87 J 10
Page 54 of 124
www.encolabs.com
8401-MW10Description:Lab Sample ID:C300052-09 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC1000072000 NE
ug/L EPA 300.0 01/29/13 10:19Chloride [16887-00-6] ^10 4300 AJB50000470000BD QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS10037000 10000
ug/L EPA 300.0 01/28/13 23:37Sulfate as SO4 [14808-79-8] ^1 40 AJB500022000J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 11:27Total Alkalinity as CaCO3 [471-34-1] ^4 48000 JCS60000340000D NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.03.1 NE
Page 55 of 124
www.encolabs.com
8401-MW10Description:Lab Sample ID:C300052-09 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.09.6 NE
Page 56 of 124
www.encolabs.com
8401-MW10Description:Lab Sample ID:C300052-09 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/22/13 18:43Methane [74-82-8]1 0.000430 GMB0.001000.000430 U NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 57 of 124
www.encolabs.com
8401-MW11Description:Lab Sample ID:C300052-10 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 20:511,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 20:511,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 20:511,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 20:511,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 20:511,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.018 5
ug/L EPA 8260B 01/18/13 20:511,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 20:511,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 20:511,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 20:511,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 20:511,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 20:511,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 20:511,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 20:511,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 20:512-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 20:512-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 20:514-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 20:51Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 20:51Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 20:51Benzene [71-43-2] ^1 0.15 JKG1.00.87 J 1
ug/L EPA 8260B 01/18/13 20:51Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 20:51Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 20:51Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 20:51Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 20:51Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 20:51Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 20:51Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 20:51Chloroethane [75-00-3] ^1 0.23 JKG1.04.8 J 10
ug/L EPA 8260B 01/18/13 20:51Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 20:51Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 20:51cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.05.8 5
ug/L EPA 8260B 01/18/13 20:51cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 20:51Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 20:51Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 20:51Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 20:51Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 20:51Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 20:51Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 20:51Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 20:51Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 20:51Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 20:51trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 20:51trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 20:51trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 20:51Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 20:51Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 20:51Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 58 of 124
www.encolabs.com
8401-MW11Description:Lab Sample ID:C300052-10 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 20:51Vinyl chloride [75-01-4] ^1 0.32 JKG1.02.2 1
ug/L EPA 8260B 01/18/13 20:51Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12285 %JKGEPA 8260B 01/18/13 20:513A180114350.0 1
Dibromofluoromethane 68-11792 %JKGEPA 8260B 01/18/13 20:513A180114650.0 1
Toluene-d8 67-12790 %JKGEPA 8260B 01/18/13 20:513A180114550.0 1
Page 59 of 124
www.encolabs.com
8401-MW11Description:Lab Sample ID:C300052-10 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:41Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:19Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:19Barium [7440-39-3] ^1 1.00 JDH10.080.3 J 100
ug/L EPA 6010C 01/17/13 14:19Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:19Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:19Chromium [7440-47-3] ^1 1.00 JDH10.030.6 10
ug/L EPA 6010C 01/17/13 14:19Cobalt [7440-48-4] ^1 1.10 JDH10.09.74 J 10
ug/L EPA 6010C 01/17/13 14:19Copper [7440-50-8] ^1 1.60 JDH10.07.20 J 10
ug/L EPA 6010C 01/17/13 14:19Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:19Nickel [7440-02-0] ^1 1.80 JDH10.068.4 50
ug/L EPA 6010C 01/17/13 14:19Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:19Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:41Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:19Vanadium [7440-62-2] ^1 1.40 JDH10.016.4 J 25
ug/L EPA 6010C 01/17/13 14:19Zinc [7440-66-6] ^1 3.80 JDH10.012.5 10
Page 60 of 124
www.encolabs.com
8401-MW11Description:Lab Sample ID:C300052-10 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:40 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.028 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 61 of 124
www.encolabs.com
8401-MW12Description:Lab Sample ID:C300052-11 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:00 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 21:211,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 21:211,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 21:211,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 21:211,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 21:211,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 21:211,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 21:211,1-Dichloropropene [563-58-6] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 21:211,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 21:211,2,4-Trichlorobenzene [120-82-1] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 21:211,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 21:211,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 21:211,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 21:211,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 21:211,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 21:211,3-Dichlorobenzene [541-73-1] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 21:211,3-Dichloropropane [142-28-9] ^1 0.16 JKG1.00.16 U 1
ug/L EPA 8260B 01/18/13 21:211,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 21:212,2-Dichloropropane [594-20-7] ^1 0.28 JKG1.00.28 U 15
ug/L EPA 8260B 01/18/13 21:212-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 21:212-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 21:213-Chloropropene [107-05-1] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/18/13 21:214-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 21:21Acetone [67-64-1] ^1 1.2 JKG5.04.6 J 100
ug/L EPA 8260B 01/18/13 21:21Acetonitrile [75-05-8] ^1 5.0 JKG105.0 U 55
ug/L EPA 8260B 01/18/13 21:21Acrolein [107-02-8] ^1 4.0 JKG104.0 U 53
ug/L EPA 8260B 01/18/13 21:21Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 21:21Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 21:21Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 21:21Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 21:21Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 21:21Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 21:21Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 21:21Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 21:21Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 21:21Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 21:21Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 21:21Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 21:21Chloroprene [126-99-8] ^1 0.64 JKG1.00.64 U 20
ug/L EPA 8260B 01/18/13 21:21cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 21:21cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 21:21Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 21:21Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 21:21Dichlorodifluoromethane [75-71-8] ^1 0.20 JKG1.00.20 U 5
ug/L EPA 8260B 01/18/13 21:21Ethyl Methacrylate [97-63-2] ^1 0.38 JKG1.00.38 U 10
ug/L EPA 8260B 01/18/13 21:21Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 21:21Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
Page 62 of 124
www.encolabs.com
8401-MW12Description:Lab Sample ID:C300052-11 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:00 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 21:21Isobutyl alcohol [78-83-1] ^1 11 JKG5011U 100
ug/L EPA 8260B 01/18/13 21:21Methacrylonitrile [126-98-7] ^1 4.9 JKG104.9 U 100
ug/L EPA 8260B 01/18/13 21:21Methyl Methacrylate [80-62-6] ^1 0.51 JKG1.00.51 U 30
ug/L EPA 8260B 01/18/13 21:21Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 21:21Naphthalene [91-20-3] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/18/13 21:21Propionitrile [107-12-0] ^1 5.0 JKG105.0 U 150
ug/L EPA 8260B 01/18/13 21:21Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 21:21Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 21:21Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 21:21Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 21:21trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 21:21trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 21:21trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 21:21Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 21:21Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 21:21Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/18/13 21:21Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 21:21Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12283 %JKGEPA 8260B 01/18/13 21:213A180114150.0 1
Dibromofluoromethane 68-11789 %JKGEPA 8260B 01/18/13 21:213A180114550.0 1
Toluene-d8 67-12789 %JKGEPA 8260B 01/18/13 21:213A180114550.0 1
Page 63 of 124
www.encolabs.com
8401-MW12Description:Lab Sample ID:C300052-11 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:00 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 01/18/13 17:09Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 64 of 124
www.encolabs.com
8401-MW12Description:Lab Sample ID:C300052-11 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:00 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:45Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:21Arsenic [7440-38-2] ^1 2.80 JDH10.03.27 J 10
ug/L EPA 6010C 01/17/13 14:21Barium [7440-39-3] ^1 1.00 JDH10.060.4 J 100
ug/L EPA 6010C 01/17/13 14:21Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:21Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:21Chromium [7440-47-3] ^1 1.00 JDH10.03.58 J 10
ug/L EPA 6010C 01/17/13 14:21Cobalt [7440-48-4] ^1 1.10 JDH10.043.5 10
ug/L EPA 6010C 01/17/13 14:21Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:21Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:21Nickel [7440-02-0] ^1 1.80 JDH10.057.6 50
ug/L EPA 6010C 01/17/13 14:21Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:21Silver [7440-22-4] ^1 1.90 JDH10.02.22 J 10
ug/L EPA 6020A 01/18/13 13:45Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:21Tin [7440-31-5] ^1 2.10 JDH10.03.96 J 100
ug/L EPA 6010C 01/17/13 14:21Vanadium [7440-62-2] ^1 1.40 JDH10.01.49 J 25
ug/L EPA 6010C 01/17/13 14:21Zinc [7440-66-6] ^1 3.80 JDH10.05.37 J 10
Page 65 of 124
www.encolabs.com
8401-MW12Description:Lab Sample ID:C300052-11 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:00 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.08.7 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 66 of 124
www.encolabs.com
8401-MW13Description:Lab Sample ID:C300052-12 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:03 Work Order:C300052
Albemarle Closed LFProject:Sampled By:
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 21:511,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 21:511,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 21:511,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 21:511,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 21:511,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 21:511,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 21:511,1-Dichloropropene [563-58-6] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 21:511,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 21:511,2,4-Trichlorobenzene [120-82-1] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 21:511,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 21:511,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 21:511,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 21:511,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 21:511,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 21:511,3-Dichlorobenzene [541-73-1] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 21:511,3-Dichloropropane [142-28-9] ^1 0.16 JKG1.00.16 U 1
ug/L EPA 8260B 01/18/13 21:511,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 21:512,2-Dichloropropane [594-20-7] ^1 0.28 JKG1.00.28 U 15
ug/L EPA 8260B 01/18/13 21:512-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 21:512-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 21:513-Chloropropene [107-05-1] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/18/13 21:514-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 21:51Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 21:51Acetonitrile [75-05-8] ^1 5.0 JKG105.0 U 55
ug/L EPA 8260B 01/18/13 21:51Acrolein [107-02-8] ^1 4.0 JKG104.0 U 53
ug/L EPA 8260B 01/18/13 21:51Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 21:51Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 21:51Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 21:51Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 21:51Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 21:51Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 21:51Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 21:51Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 21:51Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 21:51Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 21:51Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 21:51Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 21:51Chloroprene [126-99-8] ^1 0.64 JKG1.00.64 U 20
ug/L EPA 8260B 01/18/13 21:51cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 21:51cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 21:51Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 21:51Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 21:51Dichlorodifluoromethane [75-71-8] ^1 0.20 JKG1.00.20 U 5
ug/L EPA 8260B 01/18/13 21:51Ethyl Methacrylate [97-63-2] ^1 0.38 JKG1.00.38 U 10
ug/L EPA 8260B 01/18/13 21:51Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 21:51Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
Page 67 of 124
www.encolabs.com
8401-MW13Description:Lab Sample ID:C300052-12 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:03 Work Order:C300052
Albemarle Closed LFProject:Sampled By:
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 21:51Isobutyl alcohol [78-83-1] ^1 11 JKG5011U 100
ug/L EPA 8260B 01/18/13 21:51Methacrylonitrile [126-98-7] ^1 4.9 JKG104.9 U 100
ug/L EPA 8260B 01/18/13 21:51Methyl Methacrylate [80-62-6] ^1 0.51 JKG1.00.51 U 30
ug/L EPA 8260B 01/18/13 21:51Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 21:51Naphthalene [91-20-3] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/18/13 21:51Propionitrile [107-12-0] ^1 5.0 JKG105.0 U 150
ug/L EPA 8260B 01/18/13 21:51Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 21:51Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 21:51Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 21:51Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 21:51trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 21:51trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 21:51trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 21:51Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 21:51Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 21:51Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/18/13 21:51Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 21:51Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12281 %JKGEPA 8260B 01/18/13 21:513A180114150.0 1
Dibromofluoromethane 68-11788 %JKGEPA 8260B 01/18/13 21:513A180114450.0 1
Toluene-d8 67-12787 %JKGEPA 8260B 01/18/13 21:513A180114450.0 1
Page 68 of 124
www.encolabs.com
8401-MW13Description:Lab Sample ID:C300052-12 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:03 Work Order:C300052
Albemarle Closed LFProject:Sampled By:
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 01/18/13 17:11Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 69 of 124
www.encolabs.com
8401-MW13Description:Lab Sample ID:C300052-12 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:03 Work Order:C300052
Albemarle Closed LFProject:Sampled By:
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:49Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:23Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:23Barium [7440-39-3] ^1 1.00 JDH10.036.1 J 100
ug/L EPA 6010C 01/17/13 14:23Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:23Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:23Chromium [7440-47-3] ^1 1.00 JDH10.02.07 J 10
ug/L EPA 6010C 01/17/13 14:23Cobalt [7440-48-4] ^1 1.10 JDH10.018.6 10
ug/L EPA 6010C 01/17/13 14:23Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:23Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:23Nickel [7440-02-0] ^1 1.80 JDH10.01.80 U 50
ug/L EPA 6010C 01/17/13 14:23Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:23Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:49Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:23Tin [7440-31-5] ^1 2.10 JDH10.05.65 J 100
ug/L EPA 6010C 01/17/13 14:23Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 14:23Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
Page 70 of 124
www.encolabs.com
8401-MW13Description:Lab Sample ID:C300052-12 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:03 Work Order:C300052
Albemarle Closed LFProject:Sampled By:
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.013 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 71 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 22:211,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 22:211,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 22:211,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 22:211,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 22:211,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.03.1 J 5
ug/L EPA 8260B 01/18/13 22:211,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 22:211,1-Dichloropropene [563-58-6] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 22:211,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 22:211,2,4-Trichlorobenzene [120-82-1] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 22:211,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 22:211,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 22:211,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 22:211,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 22:211,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 22:211,3-Dichlorobenzene [541-73-1] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 22:211,3-Dichloropropane [142-28-9] ^1 0.16 JKG1.00.16 U 1
ug/L EPA 8260B 01/18/13 22:211,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 22:212,2-Dichloropropane [594-20-7] ^1 0.28 JKG1.00.28 U 15
ug/L EPA 8260B 01/18/13 22:212-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 22:212-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 22:213-Chloropropene [107-05-1] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/18/13 22:214-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 22:21Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 22:21Acetonitrile [75-05-8] ^1 5.0 JKG105.0 U 55
ug/L EPA 8260B 01/18/13 22:21Acrolein [107-02-8] ^1 4.0 JKG104.0 U 53
ug/L EPA 8260B 01/18/13 22:21Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 22:21Benzene [71-43-2] ^1 0.15 JKG1.00.87 J 1
ug/L EPA 8260B 01/18/13 22:21Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 22:21Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 22:21Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 22:21Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 22:21Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 22:21Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 22:21Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 22:21Chloroethane [75-00-3] ^1 0.23 JKG1.01.8 J 10
ug/L EPA 8260B 01/18/13 22:21Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 22:21Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 22:21Chloroprene [126-99-8] ^1 0.64 JKG1.00.64 U 20
ug/L EPA 8260B 01/18/13 22:21cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.017 5
ug/L EPA 8260B 01/18/13 22:21cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 22:21Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 22:21Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 22:21Dichlorodifluoromethane [75-71-8] ^1 0.20 JKG1.00.20 U 5
ug/L EPA 8260B 01/18/13 22:21Ethyl Methacrylate [97-63-2] ^1 0.38 JKG1.00.38 U 10
ug/L EPA 8260B 01/18/13 22:21Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 22:21Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
Page 72 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 22:21Isobutyl alcohol [78-83-1] ^1 11 JKG5011U 100
ug/L EPA 8260B 01/18/13 22:21Methacrylonitrile [126-98-7] ^1 4.9 JKG104.9 U 100
ug/L EPA 8260B 01/18/13 22:21Methyl Methacrylate [80-62-6] ^1 0.51 JKG1.00.51 U 30
ug/L EPA 8260B 01/18/13 22:21Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 22:21Naphthalene [91-20-3] ^1 0.11 JKG1.00.11 U 10
ug/L EPA 8260B 01/18/13 22:21Propionitrile [107-12-0] ^1 5.0 JKG105.0 U 150
ug/L EPA 8260B 01/18/13 22:21Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 22:21Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 22:21Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 22:21Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 22:21trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 22:21trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 22:21trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 22:21Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 22:21Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 22:21Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
ug/L EPA 8260B 01/18/13 22:21Vinyl chloride [75-01-4] ^1 0.32 JKG1.01.8 1
ug/L EPA 8260B 01/18/13 22:21Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12282 %JKGEPA 8260B 01/18/13 22:213A180114150.0 1
Dibromofluoromethane 68-11789 %JKGEPA 8260B 01/18/13 22:213A180114550.0 1
Toluene-d8 67-12788 %JKGEPA 8260B 01/18/13 22:213A180114450.0 1
Page 73 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8270D 01/23/13 17:321,2,4,5-Tetrachlorobenzene [95-94-3] ^1 2.0 DFM102.0 U 10
ug/L EPA 8270D 01/23/13 17:321,3,5-Trinitrobenzene [99-35-4] ^1 3.0 DFM103.0 U 10
ug/L EPA 8270D 01/23/13 17:321,3-Dinitrobenzene [99-65-0] ^1 1.9 DFM101.9 U 20
ug/L EPA 8270D 01/23/13 17:321,4-Naphthoquinone [130-15-4] ^1 2.5 DFM102.5 U 10
ug/L EPA 8270D 01/23/13 17:321,4-Phenylenediamine [106-50-3] ^1 4.0 DFM104.0 U 10
ug/L EPA 8270D 01/23/13 17:321-Naphthylamine [134-32-7] ^1 1.9 DFM101.9 U 10
ug/L EPA 8270D 01/23/13 17:322,3,4,6-Tetrachlorophenol [58-90-2] ^1 2.0 DFM102.0 U 10
ug/L EPA 8270D 01/23/13 17:322,4,5-Trichlorophenol [95-95-4] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:322,4,6-Trichlorophenol [88-06-2] ^1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:322,4-Dichlorophenol [120-83-2] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:322,4-Dimethylphenol [105-67-9] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:322,4-Dinitrophenol [51-28-5] ^1 2.6 DFM102.6 U 50
ug/L EPA 8270D 01/23/13 17:322,4-Dinitrotoluene [121-14-2] ^1 2.4 DFM102.4 U 10
ug/L EPA 8270D 01/23/13 17:322,6-Dichlorophenol [87-65-0] ^1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:322,6-Dinitrotoluene [606-20-2] ^1 1.5 DFM101.5 U 10
ug/L EPA 8270D 01/23/13 17:322-Acetylaminofluorene [53-96-3] ^1 2.5 DFM102.5 U 20
ug/L EPA 8270D 01/23/13 17:322-Chloronaphthalene [91-58-7] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:322-Chlorophenol [95-57-8] ^1 1.2 DFM101.2 U 10
ug/L EPA 8270D 01/23/13 17:322-Methyl-4,6-dinitrophenol [534-52-1] ^1 2.9 DFM102.9 U 50
ug/L EPA 8270D 01/23/13 17:322-Methylnaphthalene [91-57-6] ^1 1.5 DFM101.5 U 10
ug/L EPA 8270D 01/23/13 17:322-Methylphenol [95-48-7] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:322-Naphthylamine [91-59-8] ^1 3.0 DFM103.0 U 10
ug/L EPA 8270D 01/23/13 17:322-Nitroaniline [88-74-4] ^1 1.5 DFM101.5 U 50
ug/L EPA 8270D 01/23/13 17:322-Nitrophenol [88-75-5] ^1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:323 & 4-Methylphenol [108-39-4/106-44-5] ^1 1.6 DFM101.6 U 10
ug/L EPA 8270D 01/23/13 17:323,3'-Dichlorobenzidine [91-94-1] ^1 3.3 DFM103.3 U 20
ug/L EPA 8270D 01/23/13 17:323,3'-Dimethylbenzidine [119-93-7] ^1 2.2 DFM102.2 U 10
ug/L EPA 8270D 01/23/13 17:323-Methylcholanthrene [56-49-5] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:323-Nitroaniline [99-09-2] ^1 2.1 DFM102.1 U 50
ug/L EPA 8270D 01/23/13 17:324-Aminobiphenyl [92-67-1] ^1 2.1 DFM102.1 U 20
ug/L EPA 8270D 01/23/13 17:324-Bromophenyl-phenylether [101-55-3] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:324-Chloro-3-methylphenol [59-50-7] ^1 1.5 DFM101.5 U 20
ug/L EPA 8270D 01/23/13 17:324-Chloroaniline [106-47-8] ^1 1.2 DFM101.2 U 20
ug/L EPA 8270D 01/23/13 17:324-Chlorophenyl-phenylether [7005-72-3] ^1 1.6 DFM101.6 U 10
ug/L EPA 8270D 01/23/13 17:324-Nitroaniline [100-01-6] ^1 3.2 DFM103.2 U 20
ug/L EPA 8270D 01/23/13 17:324-Nitrophenol [100-02-7] ^1 2.0 DFM102.0 U 50
ug/L EPA 8270D 01/23/13 17:325-Nitro-o-toluidine [99-55-8] ^1 3.2 DFM103.2 U 10
ug/L EPA 8270D 01/23/13 17:327,12-Dimethylbenz(a)anthracene [57-97-6]
^
1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:32Acenaphthene [83-32-9] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Acenaphthylene [208-96-8] ^1 1.2 DFM101.2 U 10
ug/L EPA 8270D 01/23/13 17:32Acetophenone [98-86-2] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Anthracene [120-12-7] ^1 1.6 DFM101.6 U 10
ug/L EPA 8270D 01/23/13 17:32Benzo(a)anthracene [56-55-3] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Benzo(a)pyrene [50-32-8] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Benzo(b)fluoranthene [205-99-2] ^1 1.0 DFM101.0 U 10
Page 74 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8270D 01/23/13 17:32Benzo(g,h,i)perylene [191-24-2] ^1 2.4 DFM102.4 U 10
ug/L EPA 8270D 01/23/13 17:32Benzo(k)fluoranthene [207-08-9] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Benzyl alcohol [100-51-6] ^1 1.4 DFM101.4 U 20
ug/L EPA 8270D 01/23/13 17:32Bis(2-chloroethoxy)methane [111-91-1] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Bis(2-chloroethyl)ether [111-44-4] ^1 1.2 DFM101.2 U 10
ug/L EPA 8270D 01/23/13 17:32Bis(2-chloroisopropyl)ether [108-60-1] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Bis(2-ethylhexyl)phthalate [117-81-7] ^1 1.7 DFM5.01.7 U 15
ug/L EPA 8270D 01/23/13 17:32Butylbenzylphthalate [85-68-7] ^1 2.0 DFM102.0 U 10
ug/L EPA 8270D 01/23/13 17:32Chlorobenzilate [510-15-6] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:32Chrysene [218-01-9] ^1 2.0 DFM102.0 U 10
ug/L EPA 8270D 01/23/13 17:32Diallate [2303-16-4] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:32Dibenzo(a,h)anthracene [53-70-3] ^1 2.3 DFM102.3 U 10
ug/L EPA 8270D 01/23/13 17:32Dibenzofuran [132-64-9] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Diethylphthalate [84-66-2] ^1 2.1 DFM102.1 U 10
ug/L EPA 8270D 01/23/13 17:32Dimethoate [60-51-5] ^1 2.3 DFM102.3 U 20
ug/L EPA 8270D 01/23/13 17:32Dimethylphthalate [131-11-3] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Di-n-butylphthalate [84-74-2] ^1 1.5 DFM101.5 U 10
ug/L EPA 8270D 01/23/13 17:32Di-n-octylphthalate [117-84-0] ^1 3.1 DFM103.1 U 10
ug/L EPA 8270D 01/23/13 17:32Disulfoton [298-04-4] ^1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:32Ethyl methanesulfonate [62-50-0] ^1 1.2 DFM101.2 U 20
ug/L EPA 8270D 01/23/13 17:32Famphur [52-85-7] ^1 2.7 DFM102.7 U 20
ug/L EPA 8270D 01/23/13 17:32Fluoranthene [206-44-0] ^1 2.1 DFM102.1 U 10
ug/L EPA 8270D 01/23/13 17:32Fluorene [86-73-7] ^1 1.7 DFM101.7 U 10
ug/L EPA 8270D 01/23/13 17:32Hexachlorobenzene [118-74-1] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:32Hexachlorobutadiene [87-68-3] ^1 1.2 DFM101.2 U 10
ug/L EPA 8270D 01/23/13 17:32Hexachlorocyclopentadiene [77-47-4] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Hexachloroethane [67-72-1] ^1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:32Hexachloropropene [1888-71-7] ^1 1.7 DFM101.7 U 10
ug/L EPA 8270D 01/23/13 17:32Indeno(1,2,3-cd)pyrene [193-39-5] ^1 2.2 DFM102.2 U 10
ug/L EPA 8270D 01/23/13 17:32Isodrin [465-73-6] ^1 1.0 DFM101.0 U 20
ug/L EPA 8270D 01/23/13 17:32Isophorone [78-59-1] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Isosafrole [120-58-1] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:16Kepone [143-50-0] ^1 7.2 DFM207.2 U 20
ug/L EPA 8270D 01/23/13 17:32Methapyrilene [91-80-5] ^1 3.5 DFM103.5 U 100
ug/L EPA 8270D 01/23/13 17:32Methyl Methanesulfonate [66-27-3] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:32Methyl parathion [298-00-0] ^1 2.5 DFM102.5 U 10
ug/L EPA 8270D 01/23/13 17:32Nitrobenzene [98-95-3] ^1 1.2 DFM101.2 U 10
ug/L EPA 8270D 01/23/13 17:32N-Nitrosodiethylamine [55-18-5] ^1 1.3 DFM101.3 U 20
ug/L EPA 8270D 01/23/13 17:32N-Nitrosodimethylamine [62-75-9] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32N-Nitrosodi-n-butylamine [924-16-3] ^1 1.2 DFM101.2 U QV-0110
ug/L EPA 8270D 01/23/13 17:32N-Nitroso-di-n-propylamine [621-64-7] ^1 1.5 DFM101.5 U 10
ug/L EPA 8270D 01/23/13 17:32N-nitrosodiphenylamine/Diphenylamine
[86-30-6/122-39-4] ^
1 2.1 DFM102.1 U 10
ug/L EPA 8270D 01/23/13 17:32N-Nitrosomethylethylamine [10595-95-6] ^1 1.9 DFM101.9 U 10
ug/L EPA 8270D 01/23/13 17:32N-Nitrosopiperidine [100-75-4] ^1 1.1 DFM101.1 U 20
ug/L EPA 8270D 01/23/13 17:32N-Nitrosopyrrolidine [930-55-2] ^1 1.3 DFM101.3 U 10
Page 75 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8270D 01/23/13 17:32O,O,O-Triethyl phosphorothioate [126-68-1]
^
1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32o-Toluidine [95-53-4] ^1 1.1 DFM101.1 U 10
ug/L EPA 8270D 01/23/13 17:32Parathion [56-38-2] ^1 1.7 DFM101.7 U 10
ug/L EPA 8270D 01/23/13 17:32p-Dimethylaminoazobenzene [60-11-7] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Pentachlorobenzene [608-93-5] ^1 1.3 DFM101.3 U 10
ug/L EPA 8270D 01/23/13 17:32Pentachloronitrobenzene [82-68-8] ^1 1.0 DFM101.0 U 20
ug/L EPA 8270D 01/23/13 17:32Phenacetin [62-44-2] ^1 2.7 DFM102.7 U 20
ug/L EPA 8270D 01/23/13 17:32Phenanthrene [85-01-8] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Phenol [108-95-2] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Phorate [298-02-2] ^1 1.0 DFM101.0 U 10
ug/L EPA 8270D 01/23/13 17:32Pronamide [23950-58-5] ^1 1.4 DFM101.4 U 10
ug/L EPA 8270D 01/23/13 17:32Pyrene [129-00-0] ^1 2.1 DFM102.1 U 10
ug/L EPA 8270D 01/23/13 17:32Safrole [94-59-7] ^1 1.2 DFM101.2 U 10
ug/L EPA 8270D 01/23/13 17:32Thionazin [297-97-2] ^1 2.3 DFM102.3 U 20
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,6-Tribromophenol 10-17984 %DFMEPA 8270D 01/23/13 17:323A1702084100 1
2-Fluorobiphenyl 10-14991 %DFMEPA 8270D 01/23/13 17:323A170204550.0 1
2-Fluorophenol 10-11070 %DFMEPA 8270D 01/23/13 17:323A1702070100 1
Nitrobenzene-d5 10-14986 %DFMEPA 8270D 01/23/13 17:323A170204350.0 1
Phenol-d5 10-8865 %DFMEPA 8270D 01/23/13 17:323A1702065100 1
Terphenyl-d14 10-18891 %DFMEPA 8270D 01/23/13 17:323A170204650.0 1
Page 76 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 01/18/13 17:13Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 77 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 13:53Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:26Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:26Barium [7440-39-3] ^1 1.00 JDH10.049.7 J 100
ug/L EPA 6010C 01/17/13 14:26Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:26Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:26Chromium [7440-47-3] ^1 1.00 JDH10.01.81 J 10
ug/L EPA 6010C 01/17/13 14:26Cobalt [7440-48-4] ^1 1.10 JDH10.030.6 10
ug/L EPA 6010C 01/17/13 14:26Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:26Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:26Nickel [7440-02-0] ^1 1.80 JDH10.012.8 J 50
ug/L EPA 6010C 01/17/13 14:26Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:26Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 13:53Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:26Tin [7440-31-5] ^1 2.10 JDH10.05.28 J 100
ug/L EPA 6010C 01/17/13 14:26Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 14:26Zinc [7440-66-6] ^1 3.80 JDH10.05.12 J 10
Page 78 of 124
www.encolabs.com
8401-MW23Description:Lab Sample ID:C300052-13 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:30 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^1 0.50 JOC1.019 NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 79 of 124
www.encolabs.com
8401-MW24Description:Lab Sample ID:C300052-14 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:16 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 22:501,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 22:501,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 22:501,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 22:501,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 22:501,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 22:501,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 22:501,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 22:501,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 22:501,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 22:501,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 22:501,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 22:501,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 22:501,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 22:502-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 22:502-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 22:504-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 22:50Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 22:50Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 22:50Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 22:50Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 22:50Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 22:50Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 22:50Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 22:50Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 22:50Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 22:50Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 22:50Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 22:50Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 22:50Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 22:50cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 22:50cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 22:50Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 22:50Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 22:50Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 22:50Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 22:50Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 22:50Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 22:50Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 22:50Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 22:50Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 22:50trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 22:50trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 22:50trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 22:50Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 22:50Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 22:50Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 80 of 124
www.encolabs.com
8401-MW24Description:Lab Sample ID:C300052-14 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:16 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 22:50Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 22:50Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12282 %JKGEPA 8260B 01/18/13 22:503A180114150.0 1
Dibromofluoromethane 68-11787 %JKGEPA 8260B 01/18/13 22:503A180114450.0 1
Toluene-d8 67-12787 %JKGEPA 8260B 01/18/13 22:503A180114350.0 1
Page 81 of 124
www.encolabs.com
8401-MW24Description:Lab Sample ID:C300052-14 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:16 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 14:05Antimony [7440-36-0] ^10 2.20 VLO20.02.20 UD R-016
ug/L EPA 6010C 01/17/13 14:33Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:33Barium [7440-39-3] ^1 1.00 JDH10.041.3 J 100
ug/L EPA 6010C 01/17/13 14:33Beryllium [7440-41-7] ^1 0.100 JDH1.000.400 J 1
ug/L EPA 6010C 01/17/13 14:33Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:33Chromium [7440-47-3] ^1 1.00 JDH10.017.7 10
ug/L EPA 6010C 01/17/13 14:33Cobalt [7440-48-4] ^1 1.10 JDH10.014.1 10
ug/L EPA 6010C 01/17/13 14:33Copper [7440-50-8] ^1 1.60 JDH10.034.3 10
ug/L EPA 6010C 01/17/13 14:33Iron [7439-89-6] ^1 22.0 JDH50.09550 300
ug/L EPA 6010C 01/17/13 14:33Lead [7439-92-1] ^1 1.90 JDH10.07.63 J 10
ug/L EPA 6010C 01/17/13 14:33Nickel [7440-02-0] ^1 1.80 JDH10.014.4 J 50
ug/L EPA 6010C 01/17/13 14:33Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:33Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 14:05Thallium [7440-28-0] ^10 1.10 VLO10.01.10 UD R-015.5
ug/L EPA 6010C 01/17/13 14:33Vanadium [7440-62-2] ^1 1.40 JDH10.017.7 J 25
ug/L EPA 6010C 01/17/13 14:33Zinc [7440-66-6] ^1 3.80 JDH10.032.9 10
Page 82 of 124
www.encolabs.com
8401-MW24Description:Lab Sample ID:C300052-14 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:16 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC1000059000 NE
ug/L EPA 300.0 01/28/13 23:55Chloride [16887-00-6] ^1 430 AJB500064000B QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS10070J 10000
ug/L EPA 300.0 01/28/13 23:55Sulfate as SO4 [14808-79-8] ^1 40 AJB500049000J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 10:33Total Alkalinity as CaCO3 [471-34-1] ^1 12000 JCS1500066000 NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^10 5.0 JOC10320D NE
Page 83 of 124
www.encolabs.com
8401-MW24Description:Lab Sample ID:C300052-14 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:16 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.04.6 NE
Page 84 of 124
www.encolabs.com
8401-MW24Description:Lab Sample ID:C300052-14 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:16 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/22/13 18:59Methane [74-82-8]1 0.000430 GMB0.001000.000430 U NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 85 of 124
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8401-MW25Description:Lab Sample ID:C300052-15 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:41 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 23:211,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 23:211,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 23:211,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 23:211,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 23:211,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 23:211,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 23:211,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 23:211,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 23:211,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 23:211,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 23:211,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 23:211,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 23:211,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 23:212-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 23:212-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 23:214-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 23:21Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 23:21Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 23:21Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 23:21Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 23:21Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 23:21Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 23:21Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 23:21Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 23:21Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 23:21Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 23:21Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 23:21Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 23:21Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 23:21cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 23:21cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 23:21Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 23:21Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 23:21Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 23:21Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 23:21Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 23:21Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 23:21Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 23:21Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 23:21Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 23:21trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 23:21trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 23:21trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 23:21Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 23:21Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 23:21Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 86 of 124
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8401-MW25Description:Lab Sample ID:C300052-15 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:41 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 23:21Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 23:21Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12282 %JKGEPA 8260B 01/18/13 23:213A180114150.0 1
Dibromofluoromethane 68-11791 %JKGEPA 8260B 01/18/13 23:213A180114550.0 1
Toluene-d8 67-12787 %JKGEPA 8260B 01/18/13 23:213A180114450.0 1
Page 87 of 124
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8401-MW25Description:Lab Sample ID:C300052-15 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:41 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 14:09Antimony [7440-36-0] ^10 2.20 VLO20.02.20 UD R-016
ug/L EPA 6010C 01/21/13 13:01Arsenic [7440-38-2] ^1 2.80 JDH10.040.3 10
ug/L EPA 6010C 01/21/13 13:01Barium [7440-39-3] ^1 1.00 JDH10.0301 100
ug/L EPA 6010C 01/21/13 13:01Beryllium [7440-41-7] ^1 0.100 JDH1.003.60 1
ug/L EPA 6010C 01/21/13 13:01Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/21/13 13:01Chromium [7440-47-3] ^1 1.00 JDH10.0152 10
ug/L EPA 6010C 01/21/13 13:01Cobalt [7440-48-4] ^1 1.10 JDH10.035.9 10
ug/L EPA 6010C 01/21/13 13:01Copper [7440-50-8] ^1 1.60 JDH10.099.4 10
ug/L EPA 6010C 01/21/13 13:01Iron [7439-89-6] ^1 22.0 JDH50.0111000 300
ug/L EPA 6010C 01/21/13 13:01Lead [7439-92-1] ^1 1.90 JDH10.058.7 10
ug/L EPA 6010C 01/21/13 13:01Nickel [7440-02-0] ^1 1.80 JDH10.095.3 50
ug/L EPA 6010C 01/21/13 13:01Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/21/13 13:01Silver [7440-22-4] ^1 1.90 JDH10.03.76 J 10
ug/L EPA 6020A 01/18/13 14:09Thallium [7440-28-0] ^10 1.10 VLO10.01.10 UD R-015.5
ug/L EPA 6010C 01/21/13 13:01Vanadium [7440-62-2] ^1 1.40 JDH10.0174 25
ug/L EPA 6010C 01/21/13 13:01Zinc [7440-66-6] ^1 3.80 JDH10.0172 10
Page 88 of 124
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8401-MW25Description:Lab Sample ID:C300052-15 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:41 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5220D 01/21/13 13:57Chemical Oxygen Demand [ECL-0035]
^
1 10000 JOC10000110000 NE
ug/L EPA 300.0 01/29/13 00:12Chloride [16887-00-6] ^1 430 AJB500017000B QB-01NE
ug/L EPA 353.2 01/21/13 12:58Nitrate as N [14797-55-8] ^1 25 JCS1001200J 10000
ug/L EPA 300.0 01/29/13 00:12Sulfate as SO4 [14808-79-8] ^1 40 AJB500035000J 250000
ug/L SM18 4500-S D 01/22/13 12:39Sulfide [18496-25-8] ^1 10 JOC10010U 1000
ug/L EPA 310.2 01/20/13 10:35Total Alkalinity as CaCO3 [471-34-1] ^1 12000 JCS1500017000 NE
NTU SM 2130B 01/16/13 16:05Turbidity [ECL-0177] ^200 100 JOC2006400D NE
Page 89 of 124
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8401-MW25Description:Lab Sample ID:C300052-15 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:41 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L SM18 5310B 01/21/13 12:05Total Organic Carbon [ECL-0165] ^1 0.32 RSA1.07.6 NE
Page 90 of 124
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8401-MW25Description:Lab Sample ID:C300052-15 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 10:41 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Dissolved Gases by GC
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
mg/L RSK-175 01/22/13 19:15Methane [74-82-8]1 0.000430 GMB0.001000.000430 U NE
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 91 of 124
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8401-Trip BlankDescription:Lab Sample ID:C300052-16 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 01:361,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/22/13 01:361,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/22/13 01:361,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/22/13 01:361,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 01:361,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/22/13 01:361,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 01:361,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 01:361,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/22/13 01:361,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/22/13 01:361,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/22/13 01:361,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/22/13 01:361,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/22/13 01:361,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/22/13 01:362-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/22/13 01:362-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/22/13 01:364-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/22/13 01:36Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/22/13 01:36Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/22/13 01:36Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 01:36Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/22/13 01:36Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 01:36Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/22/13 01:36Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/22/13 01:36Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/22/13 01:36Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 01:36Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 01:36Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/22/13 01:36Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/22/13 01:36Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 01:36cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/22/13 01:36cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/22/13 01:36Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/22/13 01:36Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/22/13 01:36Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/22/13 01:36Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/22/13 01:36Methylene chloride [75-09-2] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/22/13 01:36Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/22/13 01:36Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/22/13 01:36Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/22/13 01:36Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/22/13 01:36trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/22/13 01:36trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 01:36trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/22/13 01:36Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/22/13 01:36Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/22/13 01:36Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 92 of 124
www.encolabs.com
8401-Trip BlankDescription:Lab Sample ID:C300052-16 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 09:10 Work Order:C300052
Albemarle Closed LFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/22/13 01:36Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/22/13 01:36Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-122105 %JKGEPA 8260B 01/22/13 01:363A210275350.0 1
Dibromofluoromethane 68-117105 %JKGEPA 8260B 01/22/13 01:363A210275350.0 1
Toluene-d8 67-127104 %JKGEPA 8260B 01/22/13 01:363A210275250.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 93 of 124
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8401-Bailer BlankDescription:Lab Sample ID:C300052-17 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:25 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 23:511,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/18/13 23:511,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/18/13 23:511,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/18/13 23:511,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 23:511,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/18/13 23:511,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 23:511,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/18/13 23:511,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/18/13 23:511,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/18/13 23:511,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/18/13 23:511,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/18/13 23:511,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/18/13 23:511,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/18/13 23:512-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/18/13 23:512-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/18/13 23:514-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/18/13 23:51Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/18/13 23:51Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/18/13 23:51Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 23:51Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/18/13 23:51Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 23:51Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/18/13 23:51Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/18/13 23:51Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/18/13 23:51Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 23:51Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 23:51Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/18/13 23:51Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/18/13 23:51Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 23:51cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/18/13 23:51cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/18/13 23:51Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/18/13 23:51Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/18/13 23:51Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/18/13 23:51Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/18/13 23:51Methylene chloride [75-09-2] ^1 0.23 JKG1.00.54 J 1
ug/L EPA 8260B 01/18/13 23:51Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/18/13 23:51Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/18/13 23:51Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/18/13 23:51Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/18/13 23:51trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/18/13 23:51trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 23:51trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/18/13 23:51Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/18/13 23:51Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/18/13 23:51Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 94 of 124
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8401-Bailer BlankDescription:Lab Sample ID:C300052-17 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:25 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/18/13 23:51Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/18/13 23:51Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12281 %JKGEPA 8260B 01/18/13 23:513A180114050.0 1
Dibromofluoromethane 68-11788 %JKGEPA 8260B 01/18/13 23:513A180114450.0 1
Toluene-d8 67-12786 %JKGEPA 8260B 01/18/13 23:513A180114350.0 1
Page 95 of 124
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8401-Bailer BlankDescription:Lab Sample ID:C300052-17 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:25 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 7470A 01/18/13 17:15Mercury [7439-97-6] ^1 0.170 T1D0.2000.170 U 0.2
Page 96 of 124
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8401-Bailer BlankDescription:Lab Sample ID:C300052-17 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:25 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 14:13Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:38Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:38Barium [7440-39-3] ^1 1.00 JDH10.01.14 J 100
ug/L EPA 6010C 01/17/13 14:38Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:38Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:38Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/17/13 14:38Cobalt [7440-48-4] ^1 1.10 JDH10.01.10 U 10
ug/L EPA 6010C 01/17/13 14:38Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:38Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:38Nickel [7440-02-0] ^1 1.80 JDH10.01.80 U 50
ug/L EPA 6010C 01/17/13 14:38Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:38Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 14:13Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:38Tin [7440-31-5] ^1 2.10 JDH10.02.10 U 100
ug/L EPA 6010C 01/17/13 14:38Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 14:38Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 97 of 124
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8401-Field BlankDescription:Lab Sample ID:C300052-18 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:35 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/19/13 11:451,1,1,2-Tetrachloroethane [630-20-6] ^1 0.17 JKG1.00.17 U 5
ug/L EPA 8260B 01/19/13 11:451,1,1-Trichloroethane [71-55-6] ^1 0.12 JKG1.00.12 U 1
ug/L EPA 8260B 01/19/13 11:451,1,2,2-Tetrachloroethane [79-34-5] ^1 0.28 JKG1.00.28 U 3
ug/L EPA 8260B 01/19/13 11:451,1,2-Trichloroethane [79-00-5] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/19/13 11:451,1-Dichloroethane [75-34-3] ^1 0.13 JKG1.00.13 U 5
ug/L EPA 8260B 01/19/13 11:451,1-Dichloroethene [75-35-4] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/19/13 11:451,2,3-Trichloropropane [96-18-4] ^1 0.23 JKG1.00.23 U 1
ug/L EPA 8260B 01/19/13 11:451,2-Dibromo-3-chloropropane [96-12-8] ^1 0.48 JKG1.00.48 U 13
ug/L EPA 8260B 01/19/13 11:451,2-Dibromoethane [106-93-4] ^1 0.66 JKG1.00.66 U 1
ug/L EPA 8260B 01/19/13 11:451,2-Dichlorobenzene [95-50-1] ^1 0.19 JKG1.00.19 U 5
ug/L EPA 8260B 01/19/13 11:451,2-Dichloroethane [107-06-2] ^1 0.21 JKG1.00.21 U 1
ug/L EPA 8260B 01/19/13 11:451,2-Dichloropropane [78-87-5] ^1 0.10 JKG1.00.10 U 1
ug/L EPA 8260B 01/19/13 11:451,4-Dichlorobenzene [106-46-7] ^1 0.19 JKG1.00.19 U 1
ug/L EPA 8260B 01/19/13 11:452-Butanone [78-93-3] ^1 1.3 JKG5.01.3 U 100
ug/L EPA 8260B 01/19/13 11:452-Hexanone [591-78-6] ^1 0.88 JKG5.00.88 U 50
ug/L EPA 8260B 01/19/13 11:454-Methyl-2-pentanone [108-10-1] ^1 1.1 JKG5.01.1 U 100
ug/L EPA 8260B 01/19/13 11:45Acetone [67-64-1] ^1 1.2 JKG5.01.2 U 100
ug/L EPA 8260B 01/19/13 11:45Acrylonitrile [107-13-1] ^1 3.5 JKG103.5 U 200
ug/L EPA 8260B 01/19/13 11:45Benzene [71-43-2] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/19/13 11:45Bromochloromethane [74-97-5] ^1 0.48 JKG1.00.48 U 3
ug/L EPA 8260B 01/19/13 11:45Bromodichloromethane [75-27-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/19/13 11:45Bromoform [75-25-2] ^1 0.22 JKG1.00.22 U 3
ug/L EPA 8260B 01/19/13 11:45Bromomethane [74-83-9] ^1 0.14 JKG1.00.14 U 10
ug/L EPA 8260B 01/19/13 11:45Carbon disulfide [75-15-0] ^1 1.5 JKG5.01.5 U 100
ug/L EPA 8260B 01/19/13 11:45Carbon tetrachloride [56-23-5] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/19/13 11:45Chlorobenzene [108-90-7] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/19/13 11:45Chloroethane [75-00-3] ^1 0.23 JKG1.00.23 U 10
ug/L EPA 8260B 01/19/13 11:45Chloroform [67-66-3] ^1 0.18 JKG1.00.18 U 5
ug/L EPA 8260B 01/19/13 11:45Chloromethane [74-87-3] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/19/13 11:45cis-1,2-Dichloroethene [156-59-2] ^1 0.15 JKG1.00.15 U 5
ug/L EPA 8260B 01/19/13 11:45cis-1,3-Dichloropropene [10061-01-5] ^1 0.20 JKG1.00.20 U 1
ug/L EPA 8260B 01/19/13 11:45Dibromochloromethane [124-48-1] ^1 0.17 JKG1.00.17 U 3
ug/L EPA 8260B 01/19/13 11:45Dibromomethane [74-95-3] ^1 0.27 JKG1.00.27 U 10
ug/L EPA 8260B 01/19/13 11:45Ethylbenzene [100-41-4] ^1 0.13 JKG1.00.13 U 1
ug/L EPA 8260B 01/19/13 11:45Iodomethane [74-88-4] ^1 1.7 JKG5.01.7 U 10
ug/L EPA 8260B 01/19/13 11:45Methylene chloride [75-09-2] ^1 0.23 JKG1.00.55 J 1
ug/L EPA 8260B 01/19/13 11:45Styrene [100-42-5] ^1 0.11 JKG1.00.11 U 1
ug/L EPA 8260B 01/19/13 11:45Tetrachloroethene [127-18-4] ^1 0.17 JKG1.00.17 U 1
ug/L EPA 8260B 01/19/13 11:45Tetrahydrofuran [109-99-9] ^1 0.80 JKG1.00.80 U NE
ug/L EPA 8260B 01/19/13 11:45Toluene [108-88-3] ^1 0.14 JKG1.00.14 U 1
ug/L EPA 8260B 01/19/13 11:45trans-1,2-Dichloroethene [156-60-5] ^1 0.21 JKG1.00.21 U 5
ug/L EPA 8260B 01/19/13 11:45trans-1,3-Dichloropropene [10061-02-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/19/13 11:45trans-1,4-Dichloro-2-butene [110-57-6] ^1 0.70 JKG1.00.70 U 100
ug/L EPA 8260B 01/19/13 11:45Trichloroethene [79-01-6] ^1 0.15 JKG1.00.15 U 1
ug/L EPA 8260B 01/19/13 11:45Trichlorofluoromethane [75-69-4] ^1 0.24 JKG1.00.24 U 1
ug/L EPA 8260B 01/19/13 11:45Vinyl acetate [108-05-4] ^1 0.95 JKG5.00.95 U 50
Page 98 of 124
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8401-Field BlankDescription:Lab Sample ID:C300052-18 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:35 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 01/19/13 11:45Vinyl chloride [75-01-4] ^1 0.32 JKG1.00.32 U 1
ug/L EPA 8260B 01/19/13 11:45Xylenes (Total) [1330-20-7] ^1 0.45 JKG3.00.45 U 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 51-12283 %JKGEPA 8260B 01/19/13 11:453A180124150.0 1
Dibromofluoromethane 68-11787 %JKGEPA 8260B 01/19/13 11:453A180124450.0 1
Toluene-d8 67-12790 %JKGEPA 8260B 01/19/13 11:453A180124550.0 1
Page 99 of 124
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8401-Field BlankDescription:Lab Sample ID:C300052-18 01/16/13 08:20Received:
Matrix:Ground Water Sampled:01/15/13 12:35 Work Order:C300052
Albemarle Closed LFProject:Sampled By:Joanna Harbison/Danny Hefner
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020A 01/18/13 14:17Antimony [7440-36-0] ^1 0.220 VLO2.000.220 U 6
ug/L EPA 6010C 01/17/13 14:40Arsenic [7440-38-2] ^1 2.80 JDH10.02.80 U 10
ug/L EPA 6010C 01/17/13 14:40Barium [7440-39-3] ^1 1.00 JDH10.01.00 U 100
ug/L EPA 6010C 01/17/13 14:40Beryllium [7440-41-7] ^1 0.100 JDH1.000.100 U 1
ug/L EPA 6010C 01/17/13 14:40Cadmium [7440-43-9] ^1 0.360 JDH1.000.360 U 1
ug/L EPA 6010C 01/17/13 14:40Chromium [7440-47-3] ^1 1.00 JDH10.01.00 U 10
ug/L EPA 6010C 01/17/13 14:40Cobalt [7440-48-4] ^1 1.10 JDH10.01.10 U 10
ug/L EPA 6010C 01/17/13 14:40Copper [7440-50-8] ^1 1.60 JDH10.01.60 U 10
ug/L EPA 6010C 01/17/13 14:40Lead [7439-92-1] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6010C 01/17/13 14:40Nickel [7440-02-0] ^1 1.80 JDH10.01.80 U 50
ug/L EPA 6010C 01/17/13 14:40Selenium [7782-49-2] ^1 4.50 JDH10.04.50 U 10
ug/L EPA 6010C 01/17/13 14:40Silver [7440-22-4] ^1 1.90 JDH10.01.90 U 10
ug/L EPA 6020A 01/18/13 14:17Thallium [7440-28-0] ^1 0.110 VLO1.000.110 U 5.5
ug/L EPA 6010C 01/17/13 14:40Vanadium [7440-62-2] ^1 1.40 JDH10.01.40 U 25
ug/L EPA 6010C 01/17/13 14:40Zinc [7440-66-6] ^1 3.80 JDH10.03.80 U 10
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 100 of 124
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A18011 - EPA 5030B_MS
Prepared: 01/18/2013 09:48 Analyzed: 01/18/2013 13:25Blank (3A18011-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.15 U 1,1-Dichloropropene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.14 U 1,2,4-Trichlorobenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.15 U 1,3-Dichlorobenzene
ug/L1.00.16 U 1,3-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L1.00.28 U 2,2-Dichloropropane
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L1.00.11 U 3-Chloropropene
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L105.0 U Acetonitrile
ug/L104.0 U Acrolein
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.64 U Chloroprene
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.20 U Dichlorodifluoromethane
ug/L1.00.38 U Ethyl Methacrylate
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L5011U Isobutyl alcohol
ug/L104.9 U Methacrylonitrile
ug/L1.00.51 U Methyl Methacrylate
Page 101 of 124
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A18011 - EPA 5030B_MS
Prepared: 01/18/2013 09:48 Analyzed: 01/18/2013 13:25Blank (3A18011-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Naphthalene
ug/L105.0 U Propionitrile
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.80 U Tetrahydrofuran
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8141
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8643
ug/L 50.0 67-127Surrogate: Toluene-d8 8643
Prepared: 01/18/2013 09:48 Analyzed: 01/18/2013 13:55LCS (3A18011-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13311323 1,1-Dichloroethene
ug/L1.0 20.0 81-13411022 Benzene
ug/L1.0 20.0 83-11710521 Chlorobenzene
ug/L1.0 20.0 71-11810120 Toluene
ug/L1.0 20.0 74-11910120 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8442
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8543
ug/L 50.0 67-127Surrogate: Toluene-d8 8944
Prepared: 01/18/2013 09:48 Analyzed: 01/18/2013 14:24Matrix Spike (3A18011-MS1)
Source: C300573-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331220.21 U24 1,1-Dichloroethene
ug/L1.0 20.0 81-1341150.15 U23 Benzene
ug/L1.0 20.0 83-1171080.17 U22 Chlorobenzene
ug/L1.0 20.0 71-1181070.14 U21 Toluene
ug/L1.0 20.0 74-1191150.15 U23 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8442
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8744
ug/L 50.0 67-127Surrogate: Toluene-d8 8844
Prepared: 01/18/2013 09:48 Analyzed: 01/18/2013 14:53Matrix Spike Dup (3A18011-MSD1)
Source: C300573-06
Page 102 of 124
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 3A18011 - EPA 5030B_MS
Prepared: 01/18/2013 09:48 Analyzed: 01/18/2013 14:53Matrix Spike Dup (3A18011-MSD1) Continued
Source: C300573-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133123 10.21 U25 1,1-Dichloroethene
ug/L1.0 20.0 1781-134117 10.15 U23 Benzene
ug/L1.0 20.0 1683-117107 0.80.17 U21 Chlorobenzene
ug/L1.0 20.0 1771-118105 20.14 U21 Toluene
ug/L1.0 20.0 2274-119118 30.15 U24 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8743
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8944
ug/L 50.0 67-127Surrogate: Toluene-d8 9246
Batch 3A18012 - EPA 5030B_MS
Prepared: 01/18/2013 09:54 Analyzed: 01/19/2013 01:50Blank (3A18012-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
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Batch 3A18012 - EPA 5030B_MS
Prepared: 01/18/2013 09:54 Analyzed: 01/19/2013 01:50Blank (3A18012-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.80 U Tetrahydrofuran
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8342
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 9045
ug/L 50.0 67-127Surrogate: Toluene-d8 8844
Prepared: 01/18/2013 09:54 Analyzed: 01/19/2013 02:20LCS (3A18012-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13312024 1,1-Dichloroethene
ug/L1.0 20.0 81-13411523 Benzene
ug/L1.0 20.0 83-11710521 Chlorobenzene
ug/L1.0 20.0 71-11810321 Toluene
ug/L1.0 20.0 74-11910521 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8241
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8844
ug/L 50.0 67-127Surrogate: Toluene-d8 8844
Prepared: 01/18/2013 09:54 Analyzed: 01/19/2013 02:50Matrix Spike (3A18012-MS1)
Source: C300573-07
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331210.21 U24 1,1-Dichloroethene
ug/L1.0 20.0 81-1341150.15 U23 Benzene
ug/L1.0 20.0 83-1171080.17 U22 Chlorobenzene
ug/L1.0 20.0 71-1181070.14 U21 Toluene
ug/L1.0 20.0 74-1191170.15 U23 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8643
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8844
ug/L 50.0 67-127Surrogate: Toluene-d8 9045
Prepared: 01/18/2013 09:54 Analyzed: 01/19/2013 03:20Matrix Spike Dup (3A18012-MSD1)
Source: C300573-07
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Volatile Organic Compounds by GCMS - Quality Control
Batch 3A18012 - EPA 5030B_MS
Prepared: 01/18/2013 09:54 Analyzed: 01/19/2013 03:20Matrix Spike Dup (3A18012-MSD1) Continued
Source: C300573-07
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133119 20.21 U24 1,1-Dichloroethene
ug/L1.0 20.0 1781-134111 40.15 U22 Benzene
ug/L1.0 20.0 1683-117104 40.17 U21 Chlorobenzene
ug/L1.0 20.0 1771-118101 50.14 U20 Toluene
ug/L1.0 20.0 2274-119108 80.15 U22 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 8542
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 8844
ug/L 50.0 67-127Surrogate: Toluene-d8 8844
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
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Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:07Blank (3A21027-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L1.00.23 U Methylene chloride
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.80 U Tetrahydrofuran
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 10753
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10452
ug/L 50.0 67-127Surrogate: Toluene-d8 10452
Prepared: 01/21/2013 13:04 Analyzed: 01/21/2013 23:37LCS (3A21027-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310020 1,1-Dichloroethene
ug/L1.0 20.0 81-1349419 Benzene
ug/L1.0 20.0 83-11710421 Chlorobenzene
ug/L1.0 20.0 71-11810020 Toluene
ug/L1.0 20.0 74-1199419 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11357
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10753
ug/L 50.0 67-127Surrogate: Toluene-d8 10251
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:06Matrix Spike (3A21027-MS1)
Source: C300689-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331060.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-134960.15 U19 Benzene
ug/L1.0 20.0 83-1171080.17 U22 Chlorobenzene
ug/L1.0 20.0 71-1181050.14 U21 Toluene
ug/L1.0 20.0 74-1191040.15 U21 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10351
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:35Matrix Spike Dup (3A21027-MSD1)
Source: C300689-06
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Volatile Organic Compounds by GCMS - Quality Control
Batch 3A21027 - EPA 5030B_MS
Prepared: 01/21/2013 13:04 Analyzed: 01/22/2013 00:35Matrix Spike Dup (3A21027-MSD1) Continued
Source: C300689-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133100 60.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-13494 30.15 U19 Benzene
ug/L1.0 20.0 1683-117107 0.70.17 U21 Chlorobenzene
ug/L1.0 20.0 1771-118102 20.14 U20 Toluene
ug/L1.0 20.0 2274-119104 0.50.15 U21 Trichloroethene
ug/L 50.0 51-122Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 68-117Surrogate: Dibromofluoromethane 10653
ug/L 50.0 67-127Surrogate: Toluene-d8 10352
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 3A17020 - EPA 3510C_MS
Prepared: 01/17/2013 18:15 Analyzed: 01/23/2013 16:32Blank (3A17020-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L102.0 U 1,2,4,5-Tetrachlorobenzene
ug/L103.0 U 1,3,5-Trinitrobenzene
ug/L101.9 U 1,3-Dinitrobenzene
ug/L102.5 U 1,4-Naphthoquinone
ug/L104.0 U 1,4-Phenylenediamine
ug/L101.9 U 1-Naphthylamine
ug/L102.0 U 2,3,4,6-Tetrachlorophenol
ug/L101.0 U 2,4,5-Trichlorophenol
ug/L101.1 U 2,4,6-Trichlorophenol
ug/L101.4 U 2,4-Dichlorophenol
ug/L101.3 U 2,4-Dimethylphenol
ug/L102.6 U 2,4-Dinitrophenol
ug/L102.4 U 2,4-Dinitrotoluene
ug/L101.1 U 2,6-Dichlorophenol
ug/L101.5 U 2,6-Dinitrotoluene
ug/L102.5 U 2-Acetylaminofluorene
ug/L101.0 U 2-Chloronaphthalene
ug/L101.2 U 2-Chlorophenol
ug/L102.9 U 2-Methyl-4,6-dinitrophenol
ug/L101.5 U 2-Methylnaphthalene
ug/L101.4 U 2-Methylphenol
ug/L103.0 U 2-Naphthylamine
ug/L101.5 U 2-Nitroaniline
ug/L101.1 U 2-Nitrophenol
ug/L101.6 U 3 & 4-Methylphenol
ug/L103.3 U 3,3'-Dichlorobenzidine
ug/L102.2 U 3,3'-Dimethylbenzidine
ug/L101.3 U 3-Methylcholanthrene
ug/L102.1 U 3-Nitroaniline
ug/L102.1 U 4-Aminobiphenyl
ug/L101.0 U 4-Bromophenyl-phenylether
ug/L101.5 U 4-Chloro-3-methylphenol
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Semivolatile Organic Compounds by GCMS - Quality Control
Batch 3A17020 - EPA 3510C_MS
Prepared: 01/17/2013 18:15 Analyzed: 01/23/2013 16:32Blank (3A17020-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L101.2 U 4-Chloroaniline
ug/L101.6 U 4-Chlorophenyl-phenylether
ug/L103.2 U 4-Nitroaniline
ug/L102.0 U 4-Nitrophenol
ug/L103.2 U 5-Nitro-o-toluidine
ug/L101.1 U 7,12-Dimethylbenz(a)anthracene
ug/L101.4 U Acenaphthene
ug/L101.2 U Acenaphthylene
ug/L101.3 U Acetophenone
ug/L101.6 U Anthracene
ug/L101.3 U Benzo(a)anthracene
ug/L101.3 U Benzo(a)pyrene
ug/L101.0 U Benzo(b)fluoranthene
ug/L102.4 U Benzo(g,h,i)perylene
ug/L101.3 U Benzo(k)fluoranthene
ug/L101.4 U Benzyl alcohol
ug/L101.4 U Bis(2-chloroethoxy)methane
ug/L101.2 U Bis(2-chloroethyl)ether
ug/L101.3 U Bis(2-chloroisopropyl)ether
ug/L5.01.7 U Bis(2-ethylhexyl)phthalate
ug/L102.0 U Butylbenzylphthalate
ug/L101.0 U Chlorobenzilate
ug/L102.0 U Chrysene
ug/L101.0 U Diallate
ug/L102.3 U Dibenzo(a,h)anthracene
ug/L101.4 U Dibenzofuran
ug/L102.1 U Diethylphthalate
ug/L102.3 U Dimethoate
ug/L101.4 U Dimethylphthalate
ug/L101.5 U Di-n-butylphthalate
ug/L103.1 U Di-n-octylphthalate
ug/L101.1 U Disulfoton
ug/L101.2 U Ethyl methanesulfonate
ug/L102.7 U Famphur
ug/L102.1 U Fluoranthene
ug/L101.7 U Fluorene
ug/L101.0 U Hexachlorobenzene
ug/L101.2 U Hexachlorobutadiene
ug/L101.3 U Hexachlorocyclopentadiene
ug/L101.1 U Hexachloroethane
ug/L101.7 U Hexachloropropene
ug/L102.2 U Indeno(1,2,3-cd)pyrene
ug/L101.0 U Isodrin
ug/L101.3 U Isophorone
ug/L101.3 U Isosafrole
ug/L207.2 U Kepone
ug/L103.5 U Methapyrilene
ug/L101.0 U Methyl Methanesulfonate
ug/L102.5 U Methyl parathion
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Semivolatile Organic Compounds by GCMS - Quality Control
Batch 3A17020 - EPA 3510C_MS
Prepared: 01/17/2013 18:15 Analyzed: 01/23/2013 16:32Blank (3A17020-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L101.2 U Nitrobenzene
ug/L101.3 U N-Nitrosodiethylamine
ug/L101.3 U N-Nitrosodimethylamine
ug/L101.2 U QV-01N-Nitrosodi-n-butylamine
ug/L101.5 U N-Nitroso-di-n-propylamine
ug/L102.1 U N-nitrosodiphenylamine/Diphenylamine
ug/L101.9 U N-Nitrosomethylethylamine
ug/L101.1 U N-Nitrosopiperidine
ug/L101.3 U N-Nitrosopyrrolidine
ug/L101.3 U O,O,O-Triethyl phosphorothioate
ug/L101.1 U o-Toluidine
ug/L101.7 U Parathion
ug/L101.4 U p-Dimethylaminoazobenzene
ug/L101.3 U Pentachlorobenzene
ug/L101.0 U Pentachloronitrobenzene
ug/L102.7 U Phenacetin
ug/L101.4 U Phenanthrene
ug/L101.4 U Phenol
ug/L101.0 U Phorate
ug/L101.4 U Pronamide
ug/L102.1 U Pyrene
ug/L101.2 U Safrole
ug/L102.3 U Thionazin
ug/L 100 10-179Surrogate: 2,4,6-Tribromophenol 8989
ug/L 50.0 10-149Surrogate: 2-Fluorobiphenyl 10050
ug/L 100 10-110Surrogate: 2-Fluorophenol 6969
ug/L 50.0 10-149Surrogate: Nitrobenzene-d5 9748
ug/L 100 10-88Surrogate: Phenol-d5 5555
ug/L 50.0 10-188Surrogate: Terphenyl-d14 10352
Prepared: 01/17/2013 18:15 Analyzed: 01/18/2013 13:59LCS (3A17020-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10 50.0 40-1097136 2-Chlorophenol
ug/L10 50.0 58-1217638 4-Chloro-3-methylphenol
ug/L10 50.0 33-1054321 4-Nitrophenol
ug/L10 50.0 39-1258342 Acenaphthene
ug/L10 50.0 48-1267940 N-Nitroso-di-n-propylamine
ug/L10 50.0 19-785125 Phenol
ug/L10 50.0 44-1377839 Pyrene
ug/L 100 10-179Surrogate: 2,4,6-Tribromophenol 8181
ug/L 50.0 10-149Surrogate: 2-Fluorobiphenyl 9346
ug/L 100 10-110Surrogate: 2-Fluorophenol 5959
ug/L 50.0 10-149Surrogate: Nitrobenzene-d5 8140
ug/L 100 10-88Surrogate: Phenol-d5 4646
ug/L 50.0 10-188Surrogate: Terphenyl-d14 8141
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Semivolatile Organic Compounds by GCMS - Quality Control
Batch 3A17020 - EPA 3510C_MS
Prepared: 01/17/2013 18:15 Analyzed: 01/18/2013 14:30Matrix Spike (3A17020-MS1)
Source: C300689-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10 50.0 40-109691.2 U34 2-Chlorophenol
ug/L10 50.0 58-121651.5 U33 4-Chloro-3-methylphenol
ug/L10 50.0 33-105382.0 U19 4-Nitrophenol
ug/L10 50.0 39-125801.4 U40 Acenaphthene
ug/L10 50.0 48-126761.5 U38 N-Nitroso-di-n-propylamine
ug/L10 50.0 19-78491.4 U24 Phenol
ug/L10 50.0 44-137772.1 U39 Pyrene
ug/L 100 10-179Surrogate: 2,4,6-Tribromophenol 6969
ug/L 50.0 10-149Surrogate: 2-Fluorobiphenyl 9447
ug/L 100 10-110Surrogate: 2-Fluorophenol 5757
ug/L 50.0 10-149Surrogate: Nitrobenzene-d5 7538
ug/L 100 10-88Surrogate: Phenol-d5 4242
ug/L 50.0 10-188Surrogate: Terphenyl-d14 7738
Prepared: 01/17/2013 18:15 Analyzed: 01/18/2013 15:01Matrix Spike Dup (3A17020-MSD1)
Source: C300689-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10 50.0 2240-10969 0.81.2 U35 2-Chlorophenol
ug/L10 50.0 2258-12174 131.5 U37 4-Chloro-3-methylphenol
ug/L10 50.0 2733-10544 152.0 U22 4-Nitrophenol
ug/L10 50.0 2539-12579 11.4 U39 Acenaphthene
ug/L10 50.0 2348-12674 11.5 U37 N-Nitroso-di-n-propylamine
ug/L10 50.0 1819-7850 21.4 U25 Phenol
ug/L10 50.0 2444-13774 42.1 U37 Pyrene
ug/L 100 10-179Surrogate: 2,4,6-Tribromophenol 7878
ug/L 50.0 10-149Surrogate: 2-Fluorobiphenyl 8341
ug/L 100 10-110Surrogate: 2-Fluorophenol 5555
ug/L 50.0 10-149Surrogate: Nitrobenzene-d5 7437
ug/L 100 10-88Surrogate: Phenol-d5 4343
ug/L 50.0 10-188Surrogate: Terphenyl-d14 7437
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 3A16016 - EPA 7470A
Prepared: 01/17/2013 16:08 Analyzed: 01/18/2013 16:20Blank (3A16016-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.2000.170 U Mercury
Prepared: 01/17/2013 16:08 Analyzed: 01/18/2013 16:22LCS (3A16016-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 80-1201105.52 Mercury
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Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 3A16016 - EPA 7470A
Prepared: 01/17/2013 16:08 Analyzed: 01/18/2013 16:30Matrix Spike (3A16016-MS1)
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 75-125810.170 U4.06 Mercury
Prepared: 01/17/2013 16:08 Analyzed: 01/18/2013 16:33Matrix Spike Dup (3A16016-MSD1)
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 2575-12573 100.170 U3.67 QM-07Mercury
Prepared: 01/17/2013 16:08 Analyzed: 01/18/2013 16:35Post Spike (3A16016-PS1)
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L0.200 5.00 75-12576-0.09103.72 Mercury
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A16018 - EPA 3005A
Prepared: 01/16/2013 10:13 Analyzed: 01/17/2013 13:22Blank (3A16018-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.02.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.00 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L50.022.0 U Iron
ug/L10.01.90 U Lead
ug/L10.01.80 U Nickel
ug/L10.04.50 U Selenium
ug/L10.01.90 U Silver
ug/L10.02.10 U Tin
ug/L10.01.40 U Vanadium
ug/L10.03.80 U Zinc
Prepared: 01/16/2013 10:13 Analyzed: 01/17/2013 13:25LCS (3A16018-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-120109218 Arsenic
ug/L10.0 200 80-120109217 Barium
ug/L1.00 20.0 80-12011122.2 Beryllium
ug/L1.00 20.0 80-12011222.3 Cadmium
ug/L10.0 200 80-120109218 Chromium
ug/L10.0 200 80-120112225 Cobalt
ug/L10.0 200 80-120108216 Copper
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Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A16018 - EPA 3005A
Prepared: 01/16/2013 10:13 Analyzed: 01/17/2013 13:25LCS (3A16018-BS1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L50.0 1000 80-1201111110 Iron
ug/L10.0 200 80-120111221 Lead
ug/L10.0 200 80-120108217 Nickel
ug/L10.0 200 80-120109218 Selenium
ug/L10.0 200 80-120114227 Silver
ug/L10.0 200 80-120108217 Tin
ug/L10.0 200 80-120111222 Vanadium
ug/L10.0 200 80-120107215 Zinc
Prepared: 01/16/2013 10:13 Analyzed: 01/17/2013 13:31Matrix Spike (3A16018-MS1)
Source: C215757-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251122.80 U223 Arsenic
ug/L10.0 200 75-12510829.5246 Barium
ug/L1.00 20.0 75-1251090.100 U21.8 Beryllium
ug/L1.00 20.0 75-1251110.360 U22.3 Cadmium
ug/L10.0 200 75-1251081.00 U216 Chromium
ug/L10.0 200 75-1251131.10 U225 Cobalt
ug/L10.0 200 75-1251071.60 U213 Copper
ug/L50.0 1000 75-12511139.71150 Iron
ug/L10.0 200 75-1251101.90 U220 Lead
ug/L10.0 200 75-1251081.80 U216 Nickel
ug/L10.0 200 75-1251104.50 U220 Selenium
ug/L10.0 200 75-1251101.90 U220 Silver
ug/L10.0 200 75-1251102.10 U220 Tin
ug/L10.0 200 75-1251101.41222 Vanadium
ug/L10.0 200 75-1251075.26219 Zinc
Prepared: 01/16/2013 10:13 Analyzed: 01/17/2013 13:33Matrix Spike Dup (3A16018-MSD1)
Source: C215757-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125112 0.012.80 U223 Arsenic
ug/L10.0 200 2075-125113 429.5256 Barium
ug/L1.00 20.0 2075-125116 60.100 U23.1 Beryllium
ug/L1.00 20.0 2075-125116 40.360 U23.2 Cadmium
ug/L10.0 200 2075-125113 51.00 U226 Chromium
ug/L10.0 200 2075-125116 31.10 U233 Cobalt
ug/L10.0 200 2075-125113 61.60 U226 Copper
ug/L50.0 1000 2075-125116 439.71200 Iron
ug/L10.0 200 2075-125113 31.90 U227 Lead
ug/L10.0 200 2075-125112 31.80 U223 Nickel
ug/L10.0 200 2075-125111 14.50 U222 Selenium
ug/L10.0 200 2075-125117 71.90 U235 Silver
ug/L10.0 200 2075-125114 42.10 U228 Tin
ug/L10.0 200 2075-125116 51.41234 Vanadium
ug/L10.0 200 2075-125111 45.26227 Zinc
Page 112 of 124
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A16018 - EPA 3005A
Prepared: 01/16/2013 10:13 Analyzed: 01/17/2013 13:43Post Spike (3A16018-PS1)
Source: C215757-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120104-0.001930.206 Arsenic
mg/L0.0100 0.200 80-1201040.02950.237 Barium
mg/L0.00100 0.0200 80-120108-4.78E-50.0216 Beryllium
mg/L0.00100 0.0200 80-1201070.0001650.0216 Cadmium
mg/L0.0100 0.200 80-1201050.0005860.211 Chromium
mg/L0.0100 0.200 80-1201080.0004680.215 Cobalt
mg/L0.0100 0.200 80-1201040.0006910.210 Copper
mg/L0.0500 1.00 80-1201070.03971.11 Iron
mg/L0.0100 0.200 80-120105-0.0007810.209 Lead
mg/L0.0100 0.200 80-1201040.001060.209 Nickel
mg/L0.0100 0.200 80-1201030.0004220.206 Selenium
mg/L0.0100 0.200 80-1201110.0008620.223 Silver
mg/L0.0100 0.200 80-1201040.001810.210 Tin
mg/L0.0100 0.200 80-1201080.001410.218 Vanadium
mg/L0.0100 0.200 80-1201030.005260.211 Zinc
Batch 3A16019 - EPA 3005A
Prepared: 01/16/2013 10:16 Analyzed: 01/18/2013 12:29Blank (3A16019-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.220 U Antimony
ug/L1.000.110 U Thallium
Prepared: 01/16/2013 10:16 Analyzed: 01/18/2013 12:33LCS (3A16019-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120100200 Antimony
ug/L1.00 200 80-120100200 Thallium
Prepared: 01/16/2013 10:16 Analyzed: 01/18/2013 12:41Matrix Spike (3A16019-MS1)
Source: C300052-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251000.220 U200 Antimony
ug/L1.00 200 75-125900.110 U180 Thallium
Prepared: 01/16/2013 10:16 Analyzed: 01/18/2013 12:45Matrix Spike Dup (3A16019-MSD1)
Source: C300052-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125100 0.20.220 U201 Antimony
ug/L1.00 200 2075-12590 0.40.110 U180 Thallium
Prepared: 01/16/2013 10:16 Analyzed: 01/18/2013 12:49Post Spike (3A16019-PS1)
Page 113 of 124
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A16019 - EPA 3005A
Prepared: 01/16/2013 10:16 Analyzed: 01/18/2013 12:49Post Spike (3A16019-PS1) Continued
Source: C300052-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201050.0802210 Antimony
ug/L1.00 200 80-120910.0751181 Thallium
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:38Blank (3A18017-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.02.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.00 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L50.022.0 U Iron
ug/L10.01.90 U Lead
ug/L10.01.80 U Nickel
ug/L10.04.50 U Selenium
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.03.80 U Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:41LCS (3A18017-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-120106212 Arsenic
ug/L10.0 200 80-120106212 Barium
ug/L1.00 20.0 80-12010521.0 Beryllium
ug/L1.00 20.0 80-12011122.1 Cadmium
ug/L10.0 200 80-120105210 Chromium
ug/L10.0 200 80-120109219 Cobalt
ug/L10.0 200 80-120103206 Copper
ug/L50.0 1000 80-1201071070 Iron
ug/L10.0 200 80-120105211 Lead
ug/L10.0 200 80-120107214 Nickel
ug/L10.0 200 80-120107213 Selenium
ug/L10.0 200 80-120107214 Silver
ug/L10.0 200 80-120105209 Vanadium
ug/L10.0 200 80-120108216 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:46Matrix Spike (3A18017-MS1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251082.80 U216 Arsenic
ug/L10.0 200 75-12510616.1229 Barium
Page 114 of 124
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:46Matrix Spike (3A18017-MS1) Continued
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00 20.0 75-1251070.100 U21.4 Beryllium
ug/L1.00 20.0 75-1251050.360 U21.0 Cadmium
ug/L10.0 200 75-1251061.00 U212 Chromium
ug/L10.0 200 75-1251101.72223 Cobalt
ug/L10.0 200 75-1251051.60 U209 Copper
ug/L50.0 1000 75-12594987010800 Iron
ug/L10.0 200 75-1251071.90 U214 Lead
ug/L10.0 200 75-1251061.80 U212 Nickel
ug/L10.0 200 75-1251074.50 U214 Selenium
ug/L10.0 200 75-1251091.90 U217 Silver
ug/L10.0 200 75-1251091.40 U217 Vanadium
ug/L10.0 200 75-1251063.80 U212 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:48Matrix Spike Dup (3A18017-MSD1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125107 12.80 U214 Arsenic
ug/L10.0 200 2075-125108 116.1232 Barium
ug/L1.00 20.0 2075-125112 50.100 U22.4 Beryllium
ug/L1.00 20.0 2075-125110 40.360 U22.0 Cadmium
ug/L10.0 200 2075-125110 31.00 U219 Chromium
ug/L10.0 200 2075-125111 0.21.72223 Cobalt
ug/L10.0 200 2075-125108 41.60 U217 Copper
ug/L50.0 1000 2075-125140 4987011300 QM-07Iron
ug/L10.0 200 2075-125107 0.21.90 U213 Lead
ug/L10.0 200 2075-125108 21.80 U217 Nickel
ug/L10.0 200 2075-125110 34.50 U220 Selenium
ug/L10.0 200 2075-125114 51.90 U228 Silver
ug/L10.0 200 2075-125113 41.40 U225 Vanadium
ug/L10.0 200 2075-125108 23.80 U216 Zinc
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:50Post Spike (3A18017-PS1)
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120101-0.002150.200 Arsenic
mg/L0.0100 0.200 80-1201000.01610.217 Barium
mg/L0.00100 0.0200 80-120102-5.42E-50.0204 Beryllium
mg/L0.00100 0.0200 80-120102-0.0003670.0201 Cadmium
mg/L0.0100 0.200 80-120101-0.0004260.202 Chromium
mg/L0.0100 0.200 80-1201040.001720.209 Cobalt
mg/L0.0100 0.200 80-120100-0.001080.199 Copper
mg/L0.0500 1.00 80-120599.8710.5 QM-08Iron
mg/L0.0100 0.200 80-1201007.65E-50.200 Lead
mg/L0.0100 0.200 80-1201010.0006480.202 Nickel
mg/L0.0100 0.200 80-120105-0.009140.200 Selenium
Page 115 of 124
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 3A18017 - EPA 3005A
Prepared: 01/18/2013 11:40 Analyzed: 01/21/2013 12:50Post Spike (3A18017-PS1) Continued
Source: C300053-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120105-0.0003190.210 Silver
mg/L0.0100 0.200 80-1201030.0005810.206 Vanadium
mg/L0.0100 0.200 80-1201060.003570.216 Zinc
Classical Chemistry Parameters - Quality Control
Batch 3A16029 - NO PREP
Prepared & Analyzed: 01/16/2013 16:05Blank (3A16029-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.00.50 U Turbidity
Prepared & Analyzed: 01/16/2013 16:05LCS (3A16029-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.0 20.4 90-11010121 Turbidity
Prepared & Analyzed: 01/16/2013 16:05Duplicate (3A16029-DUP1)
Source: C300052-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU200 25249005100D Turbidity
Batch 3A16033 - NO PREP
Prepared: 01/16/2013 17:00 Analyzed: 01/16/2013 17:46LCS (3A16033-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.00 90-110980.98 Nitrite as N
Prepared: 01/16/2013 17:00 Analyzed: 01/16/2013 17:51Matrix Spike (3A16033-MS1)
Source: C215983-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.00 90-110970.0140.98 Nitrite as N
Prepared: 01/16/2013 17:00 Analyzed: 01/16/2013 17:53Matrix Spike Dup (3A16033-MSD1)
Source: C215983-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.00 1090-110100 30.0141.0 Nitrite as N
Batch 3A18003 - NO PREP
Prepared: 01/18/2013 08:21 Analyzed: 01/18/2013 13:10LCS (3A18003-BS1)
Page 116 of 124
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A18003 - NO PREP
Prepared: 01/18/2013 08:21 Analyzed: 01/18/2013 13:10LCS (3A18003-BS1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.25 90-110981.2 Nitrate/Nitrite as N
Prepared: 01/18/2013 08:21 Analyzed: 01/18/2013 13:19Matrix Spike (3A18003-MS1)
Source: C214345-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 0.513 90-1101030.0330.56 Nitrate/Nitrite as N
Prepared: 01/18/2013 08:21 Analyzed: 01/18/2013 13:21Matrix Spike Dup (3A18003-MSD1)
Source: C214345-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 0.513 1090-11099 40.0330.54 Nitrate/Nitrite as N
Batch 3A20001 - NO PREP
Prepared: 01/20/2013 08:25 Analyzed: 01/20/2013 10:14Blank (3A20001-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1500012000U Total Alkalinity as CaCO3
Prepared: 01/20/2013 08:25 Analyzed: 01/20/2013 10:14LCS (3A20001-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L15000 100000 80-120100100000 Total Alkalinity as CaCO3
Prepared: 01/20/2013 08:25 Analyzed: 01/20/2013 10:16Matrix Spike (3A20001-MS1)
Source: C300436-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L15000 37800 80-12056180000200000 QM-05Total Alkalinity as CaCO3
Prepared: 01/20/2013 08:25 Analyzed: 01/20/2013 10:17Matrix Spike Dup (3A20001-MSD1)
Source: C300436-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L15000 37800 2580-12053 0.6180000200000 QM-05Total Alkalinity as CaCO3
Batch 3A21005 - NO PREP
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 02:31Blank (3A21005-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L50001400J Chloride
ug/L500040U Sulfate as SO4
Page 117 of 124
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A21005 - NO PREP
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 02:14LCS (3A21005-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 50000 90-1109648000B Chloride
ug/L5000 50000 90-1109447000 Sulfate as SO4
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 04:51Matrix Spike (3A21005-MS1)
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 90-1101106100083000B Chloride
ug/L5000 20000 90-1101125500077000 QM-05Sulfate as SO4
Prepared: 01/21/2013 08:08 Analyzed: 01/23/2013 05:09Matrix Spike Dup (3A21005-MSD1)
Source: C215848-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 1090-110116 16100084000B QM-05Chloride
ug/L5000 20000 1090-110118 15500078000 QM-05Sulfate as SO4
Batch 3A21014 - Same
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57Blank (3A21014-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000010000U Chemical Oxygen Demand
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57LCS (3A21014-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 90-110102510000 Chemical Oxygen Demand
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57Matrix Spike (3A21014-MS1)
Source: C212850-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 90-11010510000 U520000 Chemical Oxygen Demand
Prepared: 01/21/2013 10:50 Analyzed: 01/21/2013 13:57Matrix Spike Dup (3A21014-MSD1)
Source: C212850-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 1090-110106 110000 U530000 Chemical Oxygen Demand
Batch 3A22022 - NO PREP
Prepared: 01/22/2013 12:05 Analyzed: 01/22/2013 12:39Blank (3A22022-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
Page 118 of 124
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A22022 - NO PREP
Prepared: 01/22/2013 12:05 Analyzed: 01/22/2013 12:39Blank (3A22022-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10010U Sulfide
Prepared: 01/22/2013 12:05 Analyzed: 01/22/2013 12:39LCS (3A22022-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 0.401 80-1201030.41 Sulfide
Prepared: 01/22/2013 12:05 Analyzed: 01/22/2013 12:39Matrix Spike (3A22022-MS1)
Source: C300052-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 401 80-12010 U10U QM-05Sulfide
Prepared: 01/22/2013 12:05 Analyzed: 01/22/2013 12:39Matrix Spike Dup (3A22022-MSD1)
Source: C300052-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 401 2580-12010 U10U QM-05Sulfide
Batch 3A28033 - NO PREP
Prepared: 01/28/2013 14:17 Analyzed: 01/28/2013 19:32Blank (3A28033-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L50001400J Chloride
ug/L500040U Sulfate as SO4
Prepared: 01/28/2013 14:17 Analyzed: 01/28/2013 19:15LCS (3A28033-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 50000 90-1109548000B Chloride
ug/L5000 50000 90-1109346000 Sulfate as SO4
Prepared: 01/28/2013 14:17 Analyzed: 01/28/2013 21:35Matrix Spike (3A28033-MS1)
Source: C300036-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 90-11090860027000 Sulfate as SO4
Prepared: 01/28/2013 14:17 Analyzed: 01/29/2013 09:44Matrix Spike (3A28033-MS2)
Source: C300036-01RE1
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L25000 100000 90-11087370000460000B QM-05Chloride
Prepared: 01/28/2013 14:17 Analyzed: 01/28/2013 21:52Matrix Spike Dup (3A28033-MSD1)
Page 119 of 124
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A28033 - NO PREP
Prepared: 01/28/2013 14:17 Analyzed: 01/28/2013 21:52Matrix Spike Dup (3A28033-MSD1) Continued
Source: C300036-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 1090-11093 3860027000 Sulfate as SO4
Prepared: 01/28/2013 14:17 Analyzed: 01/29/2013 10:02Matrix Spike Dup (3A28033-MSD2)
Source: C300036-01RE1
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L25000 100000 1090-11086 0.2370000460000B QM-05Chloride
QUALITY CONTROL
Dissolved Gases by GC - Quality Control
Batch 3A22029 - Same
Prepared: 01/22/2013 15:54 Analyzed: 01/22/2013 16:34Blank (3A22029-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.001000.000430 U Methane
Prepared: 01/22/2013 15:54 Analyzed: 01/22/2013 16:50LCS (3A22029-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.00100 500 74-120105527 Methane
Prepared: 01/22/2013 15:54 Analyzed: 01/22/2013 17:06LCS Dup (3A22029-BSD1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.00100 500 1874-120106 0.7531 Methane
Prepared: 01/22/2013 15:54 Analyzed: 01/23/2013 11:30Duplicate (3A22029-DUP1)
Source: B300383-03RE1
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.500 30187.999.58 D Methane
QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A20004 - NO PREP
Prepared: 01/21/2013 11:00 Analyzed: 01/21/2013 12:05Blank (3A20004-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L1.00.32 U Total Organic Carbon
Prepared: 01/21/2013 11:00 Analyzed: 01/21/2013 12:05LCS (3A20004-BS1)
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 3A20004 - NO PREP
Prepared: 01/21/2013 11:00 Analyzed: 01/21/2013 12:05LCS (3A20004-BS1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L1.0 40.0 85-11510943 Total Organic Carbon
Prepared: 01/21/2013 11:00 Analyzed: 01/21/2013 12:05Matrix Spike (3A20004-MS1)
Source: A207168-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L1.0 40.0 85-1151112.947 Total Organic Carbon
Prepared: 01/21/2013 11:00 Analyzed: 01/21/2013 12:05Matrix Spike Dup (3A20004-MSD1)
Source: A207168-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L1.0 40.0 2185-115113 22.948 Total Organic Carbon
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Result is estimated due to positive results in the associated method blank.J-01
The method blank had a positive result for the analyte; however, the concentration in the
method blank is less than 10% of the sample result, which minimizes the impact of the
deviation.
QB-01
The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix
interference. The LCS and/or LCSD were within acceptance limits showing that the laboratory is
in control and the data is acceptable.
QM-05
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
Post-digestion spike did not meet method requirements due to confirmed matrix effects
(dilution test).
QM-08
The associated continuing calibration verification standard exhibited high bias; since the result is
ND, the impact on data quality is minimal.
QV-01
The Reporting Limit for this analyte has been raised to account for matrix interference.R-01
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