SW_F_4403-MSWLF-1982_06-30-2014_EA_C.pdf

BUNNELL-LAMMONS ENGINEERING, INC.
GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS

REPORT OF GROUNDWATER ASSESSMENT:
MONITORING WELL MW-23D

CLOSED FRANCIS FARM LANDFILL
HAYWOOD COUNTY, NORTH CAROLINA

PERMIT NUMBER 44-03

PREPARED FOR:

HAYWOOD COUNTY SOLID WASTE MANAGEMENT DEPARTMENT
CLYDE, NORTH CAROLINA

PREPARED BY:

BUNNELL-LAMMONS ENGINEERING, INC.
GREENVILLE, SOUTH CAROLINA
ASHEVILLE, NORTH CAROLINA

JUNE 30, 2014

BLE PROJECT NUMBER J13-1957-39

BUNNELL-LAMMONS ENGINEERING, INC.
GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS

6004 PONDERS COURT PHONE [phone]
GREENVILLE, SOUTH CAROLINA 29615 FAX [phone]

June 30, 2014

North Carolina Department of Environment and Natural Resources
Division of Waste Management – Solid Waste Section
1646 Mail Service Center
Raleigh, NC 27699-1646

Attention: Ms. Elizabeth S. Werner
Hydrogeologist

Subject: Report of Groundwater Assessment: Monitoring Well MW-23D
Closed Francis Farm Landfill
Haywood County, North Carolina
BLE Project Number J13-1957-39
Permit Number 44-03

Dear Ms. Werner:

As authorized by Haywood County’s acceptance of our Proposal Number P13-0179 dated August
20, 2013 and on behalf of Haywood County, Bunnell-Lammons Engineering, Inc. (BLE) has
performed the required well installation services at the subject site. The purpose of the work was to
install, sample, and prepare a report as part of a fourth phase of an approved assessment monitoring
plan for the subject site. The enclosed report describes the work performed, documents the well
installation as required, and provides recommendations for the next phase of the project.

BACKGROUND INFORMATION

The following project information was obtained from documents provided by Haywood County and
from site data (in BLE’s project records) from our current services proposal with Haywood County.

Haywood County owns and maintains the Francis Farm Landfill which is currently closed (Figure 1).
McGill Associates, P.A. (McGill) has been retained by Haywood County to provide engineering
services related to the post-closure care of the landfill. BLE has been retained by Haywood County
(since 2007) to provide semi-annual statistical analysis and reporting services for groundwater and
surface water sampling conducted by Pace Analytical Services, Inc. (Pace).

We understand that Municipal Engineering Services Company, PA [(MESCO), former consultant for
Haywood County] submitted a Groundwater Assessment Monitoring Plan (dated August 11, 2004) to
the North Carolina Division of Waste Management (DWM) on behalf of Haywood County. The DWM
reviewed the plan and Mr. Larry Rose issued a letter (dated August 23, 2004) to Haywood County
requesting additional information and a proposed schedule for implementation of the plan. Haywood
County responded with a letter to the DWM on October 14, 2004 requesting additional time to
“negotiate with the property owner of the adjacent property before we commit to a schedule.” No
further correspondence is present in the records until September 11, 2009 when the DWM issued a
letter to Haywood County requesting a response and schedule (due by approximately November 16,

Report of Groundwater Assessment: Monitoring Wells MW-23D June 30, 2014
Closed Francis Farm Landfill - Haywood County, North Carolina BLE Project Number J13-1957-39

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2009).

Haywood County retained McGill to assist with the preparation of a letter responding to the DWM
request. McGill subsequently retained BLE to evaluate the 2004 groundwater assessment plan and
provide technical information to be used in future correspondence between Haywood County and the
DWM.

As part of our assigned task, BLE issued a letter to McGill titled Comments on the Proposed 2004
Groundwater Assessment Monitoring Plan, Closed Francis Farm Landfill dated November 9, 2009
(BLE Project Number J09-1957-11). The letter stated that “Based on the limited data available in the
MESCO plan we are unable to provide a technical rationale for the proposed well locations. We believe
that some modification of the plan is necessary based on our evaluation of recently collected data.” A
date of December 31, 2009 was proposed as the due date for a submittal of a revised groundwater
elevation contour map and proposed well location plan (with a proposed well depth table) to the DWM.

BLE submitted the aforementioned information to the DWM on December 30, 2009. The DWM
subsequently issued a letter to Haywood County dated February 19, 2010 which conditionally approved
the proposed well locations, depths, and assessment plan revisions. As part of the approval, the DWM
requested that Haywood County prepare and submit a milestone schedule to the DWM for completion
of the assessment.

Our Mr. Alexander, P.G. and Mr. Jeff Bishop, P.E. of McGill attended a meeting with Mr. David Cotton
and Mr. Marty Stamey of Haywood County on February 23, 2010. Haywood County requested that we
submit a proposal to McGill to prepare the milestone schedule letter and to install and sample ten (10)
proposed groundwater monitoring wells designated MW-6 through MW-15. These activities are the
initial phase of the required groundwater assessment (assessment monitoring program) for the subject
site.

BLE prepared a proposal (BLE Proposal Number P09-0817, dated March 2, 2010) for the required work
which was subsequently approved by McGill on behalf of Haywood County. As part of the work, BLE
prepared a letter titled Milestone Schedule for the Groundwater Assessment -- Closed Francis Farm
Landfill dated May 26, 2010. The schedule was subsequently approved by the DWM.

The approved schedule included the installation of the 10 wells (MW-6 through MW-15) in the summer
of 2010 with sampling and analysis in February 2011. The subject services were performed and a data
submittal of the findings was prepared and submitted to the DWM (Groundwater Assessment Data
Submittal dated May 12, 2011) in accordance with the notification requirements of NCAC Title 15A
13B .1634 (g).

On June 10, 2011, BLE submitted a document to the DWM titled Proposed Groundwater Sampling
Matrix for August 2011 (BLE Project Number J10-1957-14). The document provided an evaluation
of the laboratory data from the February 2011 sampling event and provided a recommended sampling
matrix for the August 2011 groundwater sampling event. The matrix was subsequently approved by
the DWM in a letter dated June 27, 2011 (Doc ID No. 14252).

BLE prepared and submitted a report to Haywood County titled Report of Groundwater Assessment:
Groundwater Monitoring Wells MW-6 through MW-15 dated July 20, 2011 (BLE Project Number
J10-1957-14) to document the installation of the new wells and assessment results. The report

Report of Groundwater Assessment: Monitoring Wells MW-23D June 30, 2014
Closed Francis Farm Landfill - Haywood County, North Carolina BLE Project Number J13-1957-39

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included a recommendation for the installation of six (6) additional groundwater monitoring wells to
be designated MW-16 through MW-21. The DWM responded with a letter dated August 29, 2011
(Doc ID No. 15046) which approved the proposed well locations.

As part of the on-going groundwater assessment at the facility, Haywood County conducted a public
meeting to discuss the status of the groundwater assessment and to identify property owners and
residents near the landfill which have or had water supply wells on their properties. Several property
owners were identified, six of which signed authorization forms that allowed Haywood County
access to their wells for sampling. Water supply well sampling was conducted in August 2011.
These activities were performed by Haywood County as a pro-active measure and are in compliance
with the requirements of NCAC Title 15A 13B .1634 (g) and NCAC Title 15A 13B .1635 (c). The
results were documented in a report titled Report of Water Supply Well Sampling – August 2011
dated September 21, 2011 (BLE Project Number J11-1957-24). The results indicated that the release
of volatile organic compounds from the landfill had not impacted the water supply wells which were
tested.

On November 23, 2011 BLE submitted a document to the DWM titled Proposed Groundwater
Sampling Matrix for February 2012 (BLE Project Number J11-1957-24). The document provided
an evaluation of the laboratory data from the August 2011 sampling event and provided a
recommended sampling matrix for the February 2012 groundwater sampling event. The matrix was
subsequently approved by the DWM in a letter dated December 5, 2011 (Doc ID No. 15707). The
approved matrix included the entire monitoring well system including monitoring wells MW-16
through MW-21 which were installed in October 2011.

Monitoring wells MW-16 through MW-21 were installed in October of 2011 and were sampled as
part of the approved sampling matrix in February and August of 2012. These tasks were the second
phase of assessment at the facility. BLE prepared and submitted a report to Haywood County titled
Report of Groundwater Assessment: Groundwater Monitoring Wells MW-16 through MW-21 dated
September 10, 2012 (BLE Project Number J11-1957-25) to document the installation of the new
wells and assessment results. The report included a recommendation for the installation of eight (8)
additional groundwater monitoring wells to be designated MW-14D, MW-16D, MW-19D, MW-
20D, MW-22 through MW-25. The DWM responded with a letter dated September 21, 2012 (Doc
ID No. 17288) which approved the proposed well locations and assessment plan.

Monitoring wells MW-14D, MW-16D, MW-19D, MW-20D, MW-22 through MW-25 were installed
in December 2012 and were sampled as part of the approved sampling matrix in February 2013.
These tasks were the third phase of assessment at the facility. BLE prepared and submitted a report
to Haywood County titled Report of Groundwater Assessment: Groundwater Monitoring Wells MW-
14D, MW-16D, MW-19D, MW-20D, MW-22 through MW-25 dated July 10, 2013 (BLE Project
Number J12-1957-34) to document the installation of the new wells and assessment results. The
report included a recommendation for the installation of one (1) additional groundwater monitoring
well to be designated MW-23D. The DWM responded with a letter dated August 15, 2013 (Doc ID
No. 19536) which approved the proposed well location and assessment plan.

As part of the fourth phase of assessment, documented herein, one additional monitoring well MW-
23D was installed in September/October 2013, and was sampled in February 2014. Additionally,
the surface water monitoring locations for the subject site were relocated and sampled in accordance

Report of Groundwater Assessment: Monitoring Wells MW-23D June 30, 2014
Closed Francis Farm Landfill - Haywood County, North Carolina BLE Project Number J13-1957-39

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with the approved assessment plan. This report describes the work performed, documents the well
installation as required, and provides recommendations for the next phase of the project.

SCOPE OF SERVICES PERFORMED

The required tasks for this assessment included the installation, development, and sampling of one
groundwater monitoring well. The well location was located via a hand-held GPS unit and/or by
visually referencing existing landmarks prior to arrival of our drill crew.

Groundwater monitoring well installation was performed by North Carolina-licensed drillers retained
by BLE (North Carolina Registration #3290-A) in general accordance with North Carolina Well
Construction Standards Rule 15A NCAC 2C, .0113.

Groundwater Monitoring Well Installation, Development, and Survey

BLE mobilized an ATV-mounted CME-750 drill rig and truck-mounted Schramm drill rig to install
monitoring well MW-23D via hollow stem auger and downhole air hammer from September 30, 2013
to October 1, 2013. The as-built well location is shown on Figure 2.

The actual well installation location and depth was dependent on site conditions and the well was drilled
and installed in general accordance with the approved assessment plan. The well drilling and
installation procedures are included in Appendices A and B. The well included a surface completion
consisting of a 3 by 3 foot by 4-inch thick concrete pad with a lockable well cap and steel flush mount
cover. North Carolina well construction record (Form GW-1) is included in Appendix C. A well log
prepared by BLE is included in Appendix D and well construction data are summarized on Table 1.
The groundwater levels on Table 1 were measured by Pace on February 19, 2014 as noted on the table.

BLE provided well development services for the newly installed monitoring well. The monitoring well
was developed to remove fine particles from the sand pack around the well screen. The well
development consisted of the following:

1. Place a pump or bailer in the monitoring well;
2. Purge the well; and
3. Intermittently surge the well with a surge block.

Groundwater turbidity was measured periodically during well development using a Hach 2100Q
Portable Turbidity Meter, or equivalent. Well development logs are included in Appendix E.

The location and elevation of groundwater monitoring well MW-23D was surveyed by a North
Carolina registered land surveyor provided by McGill under direct contract with Haywood County.
The survey data was provided in digital format to BLE by McGill and was used to prepare Figure 2
and the well construction summary on Table 1.

Report of Groundwater Assessment: Monitoring Wells MW-23D June 30, 2014
Closed Francis Farm Landfill - Haywood County, North Carolina BLE Project Number J13-1957-39

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Groundwater Sampling and Analysis

Haywood County is conducting an ongoing groundwater assessment at the subject site in compliance
with the Assessment Monitoring Program rules. As part of the assessment, groundwater monitoring
well MW-23D was installed at the site to supplement the previously existing thirty (30) groundwater
monitoring wells (MW-1, MW-1A, MW-2A, MW-3A, MW-4 through MW-25, MW-14D, MW-
16D, MW-19D, and MW-20D). These wells (except MW-1; which is typically dry) were sampled
by Pace in February 2014 during a routine semi-annual groundwater monitoring event.

The wells were sampled in accordance with the approved matrix. The matrix includes the Appendix
II volatile organic compounds by EPA Method 8260, the Appendix II total metals by EPA Methods
6010 and 7470, pesticides by EPA Method 8081, and cyanide by Standard Method SM 4500-CN-E.
Groundwater levels were obtained (by Pace) from the new and previously existing monitoring wells
and a potentiometric surface map was prepared by BLE (Figure 2). A well construction and water level
summary table has been prepared by BLE (Table 1).

A summary of the February 2014 sampling data is shown on Tables 2 through 4. Please note that
the summary tables also include the results from the February 2011 through the August 2013 event
for reference. The proposed sampling matrix for August 2014 is included as Table 5. Our rationale
for the proposed sampling matrix is discussed below. The laboratory analytical data for the February
2014 sampling event is included in Appendix F. The data is also summarized/displayed on Figures 3
& 4.

RESULTS, CONCLUSIONS, AND RECOMMENDATIONS

The compounds detected in the groundwater in February 2014 are similar to those detected in February
2011 through August 2013. Surface water sampling results from the 4 new sampling locations did not
detect concentrations of VOCs, pesticides, cyanide, or mercury. Only concentrations of naturally
occurring metals were detected in the surface water.

As stated in our report dated July 10, 2013, we have reevaluated the historical data to determine if
adjustments should be made to the sampling matrix. Based on our review we have modified the matrix
(Tables 5A and 5B) to eliminate sampling and analysis for parameters with a history of non-detects.
Those changes include the elimination of mercury analysis for both groundwater and surface water.
No other changes are recommended for the surface water matrix (Table 5B). Additional changes to
the groundwater matrix include removal of pesticides from 20 of the wells and removal of cyanide
analysis from 19 of the wells (Table 5A). The proposed modifications to the matrix are in general
compliance with NCAC Title 15A 13B .1634 (b).

Report of Groundwater Assessment: Monitoring Wells MW-23D June 30, 2014
Closed Francis Farm Landfill - Haywood County, North Carolina BLE Project Number J13-1957-39

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Plan for Assessment -- Groundwater

In summary, the results indicate that the extent of the plume has been significantly defined.
Therefore, it appears that additional assessment will not be required to characterize the nature and
extent of the release as required in NCAC Title 15A 13B .1634 (g)(1)(A).

The preliminary findings were discussed in a meeting between Mr. Stephen King and Mr. David
Francis of Haywood County, Mr. Dave Pasko and Mr. Mark Cathey of McGill, and Andrew Alexander
of BLE on April 24, 2014 at the Haywood County offices. Based on these data, Haywood County,
McGill, and BLE have begun planning to meet the requirements for an Assessment of Corrective
Measures (ACM) in accordance with NCAC Title 15A 13B .1635. The ACM will be initiated after
receiving DWM approval of this report.

Plan for Assessment – Surface Water

The DWM approved a new surface water monitoring locations starting in August 2013. The locations
are specified below.

Location ID Upstream or
Downstream
Surface Water Property Owner
US-1 Upstream Ratcliffe Cove Branch Betty F. Lewis
DS-1 Downstream Ratcliffe Cove Branch Betty F. Lewis
DS-2 Downstream Ratcliffe Cove Branch Betty F. Lewis
DS-3 Downstream Ratcliffe Cove Branch Haywood County Schools

The surface water sampling locations should remain as specified above. We recommend that sampling
and analysis should be performed in accordance with the matrix (Table 5B) starting in August 2014.
Furthermore we recommend that the proposed surface water sampling plan be reevaluated after the
data from the August 2014 becomes available.

Report of Groundwater Assessment: Monitoring Wells MW-23D June 30, 2014
Closed Francis Farm Landfill - Haywood County, North Carolina BLE Project Number J13-1957-39

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CLOSING

We appreciate the opportunity to work with Haywood County, McGill, and the DWM on this project.
We request that the DWM review and approve the status of the assessment of the extent of the plume,
the revised sampling matrix, and authorize initiation of the ACM. If the DWM has any questions or
comments, please contact us at [phone].

Sincerely,
BUNNELL-LAMMONS ENGINEERING, INC.

Andrew W. Alexander, P.G., RSM Mark S. Preddy, P.G.
Senior Hydrogeologist Senior Hydrogeologist
Registered, NC No. 1475 Registered, NC No. 1043

cc: Mr. Stephen King – Haywood County
Mr. David Francis – Haywood County
Mr. Mark Cathey, P.E. – McGill Associates
Ms. Andrea Keller – NCDENR Asheville (CD Only)

Attachments: Tables 1 through 5
Figures 1 through 8
Appendices A through F

e:\awa\active projects\mcgill\haywood county lf\1957-39 fflf mw-23d\report of mw-23d install and assessment\fflf
groundwater assessment 1957-39 ble.docx

TABLES
Table 1
Groundwater Monitoring Well Construction and Groundwater Elevation Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J13-1957-39
February 19, 2014
Well Northing Easting Meas. Pt.Gnd. Surface *Depth to Depth to Water Total Borehole Screen Well Well Top of Rock Top of
Well Location (feet)(feet)Elevation Elevation Water (bgs)Water (bmp)Elevation Depth (bgs)Depth (bgs)Type Monitors Depth (bgs)Rock Elev.
MW-1 On-Site 662,529.13 822,317.14 2,666.59 2,663.72 >33.13 >36 <2630.59 UK UK -UK UK -UK UK UK UK UK
MW-1A On-Site 662,590.73 822,083.15 2,690.88 2,687.97 41.98 44.89 2,645.99 UK UK -UK UK -UK UK UK UK UK
MW-2A On-Site 662,347.08 822,814.69 2,643.78 2,640.98 20.00 22.80 2,620.98 27.0 12.0 -27.0 2,629.0 -2,614.0 II PWR/BR 18.0 2,623.0
MW-3A On-Site 661,921.62 823,026.22 2,674.29 2,671.59 33.10 35.80 2,638.49 UK UK -UK UK -UK UK UK UK UK
MW-4 On-Site 661,420.29 822,245.39 2,789.47 2,786.88 65.96 68.55 2,720.92 UK UK -UK UK -UK UK UK UK UK
MW-5 On-Site 661,286.31 822,167.91 2,797.08 2,797.37 71.71 71.42 2,725.66 94.0 73.1 -88.1 2,724.3 -2,709.3 II PWR 89.0 2,708.4
Groundwater Monitoring Wells MW-6 through MW-25 Installed by BLE
MW-6 Off-Site 662,941.12 822,167.78 2,612.63 2,613.03 6.07 5.67 2,606.96 12.5 2.3 -12.3 2,610.7 -2,600.7 II Res/Collv 12.5 2,600.5
MW-7 Off-Site 662,800.72 822,584.39 2,621.33 2,621.48 6.43 6.28 2,615.05 24.0 4.0 -19.0 2,617.5 -2,602.5 II Collv/Allv NE NE
MW-8 Off-Site 662,619.60 822,989.68 2,620.05 2,620.25 3.96 3.76 2,616.29 19.0 3.0 -13.0 2,617.3 -2,607.3 II Alluvial NE NE
MW-9 Off-Site 662,309.84 823,295.25 2,618.67 2,619.19 1.89 1.37 2,617.30 19.0 2.0 -12.0 2,617.2 -2,607.2 II Alluvial NE NE
MW-10 Off-Site 661,947.33 823,365.59 2,623.60 2,623.96 2.08 1.72 2,621.88 15.0 2.0 -12.0 2,622.0 -2,612.0 II Alluvial NE NE
MW-11 On-Site 661,509.39 822,572.73 2,756.22 2,756.46 77.13 76.89 2,679.33 100.0 70.8 -85.8 2,685.7 -2,670.7 II BR 71.0 2,685.5
MW-12 Off-Site 661,078.94 822,142.39 2,803.11 2,800.28 67.12 69.95 2,733.16 90.0 64.8 -79.8 2,735.5 -2,720.5 II BR 64.0 2,736.3
MW-13 On-Site 661,377.43 821,791.88 2,799.14 2,799.51 81.59 81.22 2,717.92 127.0 74.0 -89.0 2,725.5 -2,710.5 II PWR/BR 81.0 2,718.5
MW-14 On-Site 661,894.81 821,755.37 2,770.34 2,770.64 85.00 84.70 2,685.64 120.0 93.8 -108.8 2,676.8 -2,661.8 II BR 33.0 2,737.6
MW-14D On-Site 661,878.59 821,754.85 2,771.63 2,772.05 145.15 144.73 2,626.90 250.5 202.0 -212.0 2,570.0 -2,560.0 II BR 41.0 2,731.0
MW-15 On-Site 662,338.59 821,896.86 2,719.57 2,716.89 79.14 81.82 2,637.75 163.0 75.8 -90.8 2,641.1 -2,626.1 II BR 19.0 2,697.9
MW-16 Off-Site 661,203.62 821,457.75 2,716.16 2,716.29 52.82 52.69 2,663.47 70.0 54.8 -69.8 2,661.5 -2,646.5 II PWR/BR 63.0 2,653.3
MW-16D Off-Site 661,192.49 821,467.73 2,716.28 2,716.57 72.26 71.97 2,644.31 150.0 116.0 -126.0 2,600.6 -2,590.6 II BR 81.0 2,635.6
MW-17 Off-Site 661,739.15 821,178.09 2,664.77 2,665.07 48.22 47.92 2,616.85 73.0 49.8 -64.8 2,615.3 -2,600.3 II PWR/BR 63.0 2,602.1
MW-18 Off-Site 662,150.91 821,256.31 2,620.91 2,620.93 24.30 24.28 2,596.63 41.0 25.8 -40.8 2,595.1 -2,580.1 II BR 22.0 2,598.9
MW-19 Off-Site 662,965.29 822,624.55 2,615.08 2,615.29 6.54 6.33 2,608.75 21.0 5.5 -20.5 2,609.8 -2,594.8 II Allv/Res NE NE
MW-19D Off-Site 662,952.84 822,617.92 2,615.33 2,615.62 6.14 5.85 2,609.48 59.0 53.9 -58.9 2,561.7 -2,556.7 II PWR NE NE
MW-20 Off-Site 661,973.29 823,503.41 2,621.94 2,622.13 1.61 1.42 2,620.52 15.5 5.3 -15.3 2,616.8 -2,606.8 II Alluvial NE NE
MW-20D Off-Site 661,973.43 823,494.68 2,621.94 2,622.12 0.28 0.10 2,621.84 69.0 60.0 -65.0 2,562.1 -2,557.1 II PWR NE NE
MW-21 Off-Site 661,424.40 823,203.28 2,658.37 2,658.72 20.14 19.79 2,638.58 36.0 18.8 -33.8 2,639.9 -2,624.9 II Residuum NE NE
MW-22 Off-Site 661,046.30 820,724.07 2,599.86 2,600.00 1.21 1.08 2,598.78 25.0 4.0 -24.0 2,596.0 -2,576.0 II Alluvial NE NE
MW-23 Off-Site 663,169.77 822,719.36 2,611.43 2,611.63 0.91 0.72 2,610.71 24.0 3.8 -23.8 2,607.8 -2,587.8 II Alluvial NE NE
MW-23D Off-Site 663,182.53 822,725.71 2,611.52 2,611.75 2.28 2.05 2,609.47 62.0 53.0 -58.0 2,558.8 -2,553.8 III BR 37.0 2,574.8
MW-24 Off-Site 662,019.81 823,641.42 2,625.80 2,626.04 3.44 3.20 2,622.60 35.0 7.5 -27.5 2,618.5 -2,598.5 II Collv/PWR/BR 15.0 2,611.0
MW-25 Off-Site 661,488.76 822,382.32 2,756.31 2,756.67 48.65 48.29 2,708.02 259.5 249.3 -259.3 2,507.4 -2,497.4 II BR 62.0 2,694.7
Notes:
All survey data provided by McGill Associates, all units in feet.Measuring Point Elevation is top of casing BR & PWR = Bedrock & Partially Weathered Rock
*DTW from bgs values have been calculated from survey data provided by McGill Associates.II = Type II well Res = Residuum
All values shown to the nearest 0.1-ft have been rounded.III = Type III well Collv = Colluvium
Water levels measured on 8/19-26/13 by Pace NE = Not encountered Allv = Alluvium
MW-1, -1A, -2A, -3A, -4, -5 installed by others. MW-6 through MW-25 installed by BLE.UK = Unknown, information is not available NP = Well Not Present at Time of Measurement
Screen
Elevation
Table 1 GWM of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: IAI
Table 2A
Volatile Organic Compounds (VOC) February 2011 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-24
Sampled by Pace on February 22, 2011 (Pace Projects 9288391 & 9288386)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
Acetone mg/l 2.2 25 6000 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 2.3 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9
Benzene mg/l 0.25 1 1 <0.25 <0.25 <0.25 15.5 5.1 <0.25 0.72 <0.25 <0.25 <0.25 <0.25 <0.25 5.3 1.3 0.42
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 1.2
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 1.8 <0.23 <0.23 <0.23 <0.23 <0.23 0.93 <0.23 <0.23 <0.23 <0.23 <0.23 0.61 1.6 <0.23
Chloroethane mg/l 0.54 1 3000 1.5 <0.54 7.3 3.1 4 <0.54 1.3 <0.54 <0.54 <0.54 <0.54 <0.54 1.3 1.3 <0.54
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 0.26
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.3 1 20 <0.3 <0.3 1.1 <0.3 <0.3 <0.3 1.4 <0.3 <0.3 0.33 4.2 <0.3 <0.3 104 3.3
1,4-Dichlorobenzene mg/l 0.33 1 6 <0.33 7 1.2 4.7 1.3 <0.33 1.7 <0.33 <0.33 <0.33 1.4 <0.33 5.9 21.4 0.8
trans-1,4-Dichloro-2-butene mg/l 1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.2 1.4 17.5 31.9 12.9 <0.32 4.4 <0.32 0.34 3.1 7.5 <0.32 4.8 1.5 1
1,2-Dichloroethane mg/l 0.12 1 0.4 <0.12 <0.12 2.8 2 <0.12 <0.12 3 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 1 5.6 1.6 34.6 14.4 <0.19 2.7 <0.19 0.55 2.3 10.9 <0.19 17.3 32.5 8.9
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 0.58 <0.27 <0.27 <0.27 0.46 <0.27 <0.27 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l 0.12 1 70 NT NT NT NT NT <0.12 0.31 <0.12 <0.12 <0.12 0.31 <0.12 0.67 0.34 0.24
Ethylbenzene mg/l 0.3 1 600 <0.3 <0.3 <0.3 1.7 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 2 5 <0.97 <0.97 <0.97 46.6 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.4 1 0.2 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 6.7 5.6 <0.46 <0.46 <0.46 <0.46 0.85 0.53 <0.46 2.2 <0.46 <0.46
Toluene mg/l 0.26 1 600 <0.26 <0.26 <0.26 11.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 7 4.8 <0.47 <0.47 <0.47 <0.47 0.55 0.53 <0.47 1.7 <0.47 <0.47
Trichlorofluoromethane mg/l 0.2 1 2000 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 0.79 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 8.4 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 4.2 2.3 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 8.8 <0.23 <0.23
Dichlorodifluoromethane mg/l 0.21 1 1000 NT NT NT NT NT <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 5.5 14.0 31.5 177.8 50.4 ND 19.3 ND 0.9 7.1 25.8 ND 49.4 163.9 16.1
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on February 22, 2011
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2A Feb 11 VOCs of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: MLT/TZS
Table 2B
Volatile Organic Compounds (VOC) August 2011 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-24
Sampled by Pace on August 23, 2011 (Pace Project 92100967)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
Acetone mg/l 2.2 25 6000 <2.2 4.4 4.1 7.9 3.7 <2.2 2.5 <2.2 <2.2 <2.2 <2.2 <2.2 2.6 2.5 <2.2
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9
Benzene mg/l 0.25 1 1 0.28 0.61 0.3 16.9 4.2 <0.25 0.79 <0.25 <0.25 <0.25 <0.25 <0.25 4.4 1.2 0.39
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 2.6 0.59 0.73 0.61 <0.23 <0.23 0.93 <0.23 <0.23 <0.23 <0.23 <0.23 0.45 1.7 <0.23
Chloroethane mg/l 0.54 1 3000 2.2 2.5 <0.54 2.7 2.9 <0.54 1.2 <0.54 <0.54 <0.54 <0.54 <0.54 1.2 1.6 <0.54
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.3 1 20 0.43 1.3 0.7 <0.3 <0.3 <0.3 1.5 <0.3 <0.3 <0.3 4 <0.3 <0.3 97.1 2.8
1,4-Dichlorobenzene mg/l 0.33 1 6 0.37 7.3 0.96 5.1 1.1 <0.33 1.6 <0.33 <0.33 <0.33 1.5 <0.33 5.6 21.7 0.69
trans-1,4-Dichloro-2-butene mg/l 1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.4 1.7 14.7 33.2 9.6 <0.32 4.6 <0.32 1.5 2.8 9.6 <0.32 4.3 1.3 0.82
1,2-Dichloroethane mg/l 0.12 1 0.4 0.97 <0.12 2.1 2 0.23 <0.12 3.2 <0.12 0.12 <0.12 0.27 <0.12 0.36 <0.12 <0.12
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 0.64 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 1 4 2.4 36.7 11.5 <0.19 3.6 0.2 2.3 2.1 10.1 <0.19 15.8 31.1 7.7
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 0.33 0.34 0.36 0.57 <0.27 <0.27 0.58 <0.27 <0.27 <0.27 0.42 <0.27 0.38 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l 0.12 1 70 0.13 0.44 0.43 1.7 0.17 <0.12 0.29 <0.12 <0.12 <0.12 0.12 <0.12 0.61 0.42 0.25
Ethylbenzene mg/l 0.3 1 600 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 2 5 <0.97 <0.97 <0.97 48.5 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.4 1 0.2 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 7.5 4.6 <0.46 <0.46 <0.46 1.2 0.85 1 <0.46 1.7 <0.46 <0.46
Toluene mg/l 0.26 1 600 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 7.9 3.7 <0.47 <0.47 <0.47 <0.47 0.51 0.86 <0.47 1.5 <0.47 <0.47
Trichlorofluoromethane mg/l 0.2 1 2000 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 <0.62 0.66 0.96 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 4.9 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 2.8 1.9 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 7.7 <0.23 <0.23
Dichlorodifluoromethane mg/l 0.21 1 1000 <0.21 <0.21 <0.21 0.99 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 9.7 23.2 27.4 181.6 44.0 ND 20.8 0.2 5.1 6.3 27.9 ND 46.6 158.6 12.7
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on August 23, 2011
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2B Aug 11 2B VOCs of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: TZS
Table 2C
Volatile Organic Compounds (VOC) February 2012 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-25
Sampled by Pace on February 21-22, 2012 (Pace Projects 92112617 & 92112760)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21
Acetone mg/l 2.2 25 6000 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9
Benzene mg/l 0.25 1 1 <0.25 0.65 <0.25 16.9 3.9 <0.25 0.68 <0.25 <0.25 <0.25 <0.25 <0.25 5.0 1.3 0.43 <0.25 <0.25 <0.25 0.39 <0.25 <0.25
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 2.5 0.27 0.44 0.53 <0.23 <0.23 0.88 <0.23 <0.23 <0.23 <0.23 <0.23 0.55 1.5 <0.23 <0.23 <0.23 <0.23 0.5 <0.23 <0.23
Chloroethane mg/l 0.54 1 3000 1.7 <0.54 3.7 1.7 2.3 <0.54 0.87 <0.54 <0.54 <0.54 <0.54 <0.54 1.2 1.2 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.3 1 20 0.48 <0.3 0.56 <0.3 <0.3 <0.3 1.6 <0.3 <0.3 0.65 5 <0.3 <0.3 75.9 4.0 <0.3 <0.3 <0.3 0.94 <0.3 <0.3
1,4-Dichlorobenzene mg/l 0.33 1 6 0.42 3.1 0.61 4.9 0.99 <0.33 1.6 <0.33 <0.33 <0.33 1.6 <0.33 6.0 18.7 0.79 <0.33 <0.33 <0.33 0.99 <0.33 <0.33
trans-1,4-Dichloro-2-butene mg/l 1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.2 0.63 8.4 30.1 8.1 <0.32 3.0 <0.32 <0.32 2.1 8.5 <0.32 4.7 0.88 0.88 1.8 <0.32 <0.32 3.4 0.46 <0.32
1,2-Dichloroethane mg/l 0.12 1 0.4 0.86 <0.12 0.71 1.7 <0.12 <0.12 2.2 <0.12 <0.12 <0.12 0.15 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 3.2 <0.12 <0.12
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 0.57 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 0.78 4.6 0.8 33.1 10.2 <0.19 2.4 <0.19 <0.19 1.7 10.6 <0.19 18.4 20.7 9.0 1.5 <0.19 <0.19 1.3 <0.19 <0.19
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 <0.27 <0.27 <0.27 0.47 <0.27 <0.27 0.42 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 0.51 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l 0.12 1 70 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Ethylbenzene mg/l 0.3 1 600 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 2 5 <0.97 <0.97 <0.97 32.6 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.4 1 0.2 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 5.9 3.7 <0.46 <0.46 <0.46 <0.46 0.89 0.93 <0.46 1.6 <0.46 <0.46 0.82 <0.46 <0.46 <0.46 <0.46 <0.46
Toluene mg/l 0.26 1 600 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 7.3 3.6 <0.47 <0.47 <0.47 <0.47 0.50 <0.47 <0.47 1.6 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47
Trichlorofluoromethane mg/l 0.2 1 2000 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 3.8 3.8
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 0.65 <0.62 0.78 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 0.74 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 4.9 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 1.7 0.52 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 7.7 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23
Dichlorodifluoromethane mg/l 0.21 1 1000 <0.21 <0.21 <0.21 0.7 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 7.9 9.9 15.2 143.9 33.3 ND 13.7 ND ND 5.8 26.8 ND 47.5 120.2 15.1 4.1 ND ND 11.2 4.3 3.8
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on February 21-22, 2012
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2C Feb 12 VOCs of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: TZS
Table 2D
Volatile Organic Compounds (VOC) August 2012 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-25
Sampled by Pace on August 27-29, 2012 (Pace Project #92129364)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21
Acetone mg/l 2.2 25 6000 <2.2 2.6 <2.2 4.1 <2.2 <2.2 2.9 3.7 3.5 <2.2 2.2 <2.2 2.4 <2.2 3.8 <2.2 <2.2 <2.2 <2.2 <2.2 <2.2
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9
Benzene mg/l 0.25 1 1 0.32 0.65 <0.25 15.6 3.3 <0.25 0.64 <0.25 <0.25 <0.25 0.36 <0.25 4.4 1.1 <0.25 <0.25 <0.25 <0.25 0.33 <0.25 <0.25
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 2.3 0.66 0.64 0.53 <0.23 <0.23 0.82 <0.23 <0.23 <0.23 <0.23 <0.23 0.44 1.4 <0.23 <0.23 <0.23 <0.23 0.57 <0.23 <0.23
Chloroethane mg/l 0.54 1 3000 0.73 <0.54 1.8 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.3 1 20 0.57 1.8 0.62 <0.3 <0.3 <0.3 1.6 <0.3 <0.3 <0.3 5.9 <0.3 <0.3 70.7 4.4 <0.3 <0.3 <0.3 1.2 <0.3 <0.3
1,4-Dichlorobenzene mg/l 0.33 1 6 <0.33 8.6 0.88 5 0.87 <0.33 1.4 <0.33 <0.33 <0.33 1.8 <0.33 5.6 17.5 0.74 <0.33 <0.33 <0.33 1.3 <0.33 <0.33
trans-1,4-Dichloro-2-butene mg/l 1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.3 1.5 15.2 26.5 7.4 <0.32 2.6 <0.32 0.91 1.8 6.8 <0.32 3.3 0.76 0.68 1.6 <0.32 <0.32 4.5 0.42 <0.32
1,2-Dichloroethane mg/l 0.12 1 0.4 0.96 0.36 2.1 1.4 <0.12 <0.12 1.7 <0.12 <0.12 <0.12 0.26 <0.12 0.23 <0.12 <0.12 <0.12 <0.12 <0.12 3.9 <0.12 <0.12
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 0.99 2.8 2.6 30.5 8 <0.19 2.2 <0.19 1.6 1.3 15.1 <0.19 13.9 22.8 5.3 1.2 <0.19 <0.19 1.3 <0.19 <0.19
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 0.58 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l 0.12 1 70 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Ethylbenzene mg/l 0.3 1 600 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 <0.3
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 1 5 <0.97 <0.97 <0.97 16.8 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.4 1 0.2 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 5.8 3.7 <0.46 <0.46 <0.46 0.86 0.66 0.98 <0.46 1.5 <0.46 <0.46 0.75 <0.46 <0.46 <0.46 <0.46 <0.46
Toluene mg/l 0.26 1 600 <0.26 <0.26 0.38 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 7 3.4 <0.47 <0.47 <0.47 <0.47 <0.47 1.1 <0.47 1.3 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47
Trichlorofluoromethane mg/l 0.2 1 2000 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 <0.62 0.78 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 4.2 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 1.1 0.29 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 6.7 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23
Dichlorodifluoromethane mg/l 0.21 1 1000 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 7.2 19.0 25.0 118.5 27.0 ND 13.9 3.7 6.9 3.8 34.5 ND 39.8 114.3 14.9 3.6 ND ND 13.7 0.4 ND
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on August 27-29, 2012
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2D Aug 12 VOCsof FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by : BPN
Checked by: PJVH
Table 2E
Volatile Organic Compounds (VOC) February 2013 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J12-1957-34
Sampled by Pace on February 18-21, 2013 (Pace Projects #92148500 & 92148504)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Acetone mg/l 10.0 25 6000 <10.0 14.6 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9
Benzene mg/l 0.25 1 1 <0.25 0.45 0.39 17.1 4.1 <0.25 0.65 <0.25 <0.25 <0.25 0.46 <0.25 3.5 1.2 <0.25 0.84 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 9.5 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 3.9
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 3.1 <0.23 0.34 0.56 <0.23 <0.23 1.1 <0.23 <0.23 <0.23 <0.23 <0.23 0.36 1.5 <0.23 0.28 <0.23 <0.23 <0.23 <0.23 0.53 2.3 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23
Chloroethane mg/l 0.54 1 3000 2.1 <0.54 2.7 1.3 2.4 <0.54 1.3 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 2.1 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.30 1 20 0.76 0.33 0.53 <0.30 <0.30 <0.30 2.2 <0.30 <0.30 <0.30 5.9 <0.30 <0.30 76.7 5.9 9.2 <0.30 <0.30 <0.30 <0.30 1.1 3.2 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30
1,3-Dichlorobenzene mg/l 0.24 1 200 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 0.40 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24
1,4-Dichlorobenzene mg/l 0.33 1 6 0.53 2.2 0.49 5.6 1.1 <0.33 1.9 <0.33 <0.33 <0.33 1.6 <0.33 5.2 18.1 1.1 1.6 <0.33 <0.33 <0.33 <0.33 1.1 2.7 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
trans-1,4-Dichloro-2-butene mg/l 1.0 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.4 0.52 7.0 27.5 7.9 <0.32 2.9 <0.32 0.52 1.8 5.7 <0.32 2.7 0.76 <0.32 0.76 0.58 1.1 <0.32 <0.32 3.6 3.4 <0.32 0.97 <0.32 <0.32 <0.32 <0.32 3.1
1,2-Dichloroethane mg/l 0.12 1 0.4 <0.12 <0.12 0.63 1.6 <0.12 <0.12 2.2 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 3.0 3.7 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 0.5 1.6 <0.19 31.4 10.4 <0.19 2.6 <0.19 0.81 1.6 17.3 <0.19 14.2 20.6 1.5 10.6 0.39 0.63 <0.19 <0.19 1.1 0.78 <0.19 0.86 <0.19 <0.19 <0.19 <0.19 2.0
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 0.86 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l NT NT 70 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Ethylbenzene mg/l 0.3 1 600 <0.30 <0.30 <0.30 0.46 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 1 5 <0.97 <0.97 <0.97 21.4 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 2.4
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Naphthalene mg/l 0.24 1 6 0.91 <0.24 <0.24 5.2 0.82 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.40 1 0.2 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 5.8 4.4 <0.46 <0.46 <0.46 <0.46 0.60 0.69 <0.46 0.78 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Toluene mg/l 0.26 1 600 <0.26 <0.26 <0.26 1.3 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 0.32 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 6.1 3.3 <0.47 <0.47 <0.47 <0.47 <0.47 0.82 <0.47 0.67 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47
Trichlorofluoromethane mg/l 0.20 1 2000 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 5.6 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 1.9 0.76 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 2.8 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23
Dichlorodifluoromethane mg/l 0.21 1 1000 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 9.3 19.7 12.1 132.8 35.2 ND 14.9 ND 1.3 4.0 32.5 ND 30.2 119.3 18.3 23.3 1.0 1.7 ND ND 10.4 19.0 ND 1.8 ND ND ND ND 11.4
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on February 18-21, 2013
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2E Feb 13 VOCs of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: SJN/PJVH
Checked by: AWA/IAI
Table 2F
Volatile Organic Compounds (VOC) August 2013 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J12-1957-34
Sampled by Pace on August 20-26, 2013 (Pace Project #92169299)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Acetone mg/l 10.0 25 6000 <10.0 <10.0 <10.0 <10.0 13.7 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 20.6
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9
Benzene mg/l 0.25 1 1 0.45 0.93 0.50 15.7 3.7 <0.25 0.64 <0.25 <0.25 <0.25 <0.25 <0.25 3.8 1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 0.37 0.52 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 8.6
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 4.3 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 5.8
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 3.8 0.40 0.42 0.65 <0.23 <0.23 1.2 <0.23 <0.23 <0.23 <0.23 <0.23 0.72 1.8 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 0.67 2.3 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 0.46
Chloroethane mg/l 0.54 1 3000 2.3 <0.54 5.7 <0.54 2.1 <0.54 1.5 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 2.8 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 2.4
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 2.3 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.30 1 20 0.97 0.47 0.57 <0.30 <0.30 <0.30 2.6 <0.30 <0.30 0.33 4.2 <0.30 <0.30 78.6 2.3 8.2 <0.30 <0.30 <0.30 <0.30 1.2 3.4 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 0.33
1,3-Dichlorobenzene mg/l 0.24 1 200 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 0.43 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24
1,4-Dichlorobenzene mg/l 0.33 1 6 0.65 5.7 0.82 6.2 1.1 <0.33 2.2 <0.33 <0.33 <0.33 1.5 <0.33 6.4 20.7 0.49 1.1 <0.33 <0.33 <0.33 <0.33 1.2 3.0 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 3.9
trans-1,4-Dichloro-2-butene mg/l 1.0 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.3 0.56 7.9 20.8 7.8 <0.32 2.6 <0.32 0.80 1.5 6.6 <0.32 2.1 0.71 <0.32 0.58 <0.32 1.1 <0.32 <0.32 2.8 2.7 0.68 0.99 <0.32 <0.32 <0.32 <0.32 16.3
1,2-Dichloroethane mg/l 0.12 1 0.4 1.2 <0.12 0.77 1.5 <0.12 <0.12 1.9 <0.12 <0.12 <0.12 0.29 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 2.5 3.0 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 0.99
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 0.38 5.1 2.0 25.8 8.6 <0.19 1.8 <0.19 1.1 1.4 17.2 <0.19 11.3 18.1 0.76 4.5 <0.19 0.77 <0.19 <0.19 1.1 0.55 0.32 0.89 <0.19 <0.19 <0.19 <0.19 23.2
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 0.31 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 0.64 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l NT NT 70 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Ethylbenzene mg/l 0.3 1 600 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 1 5 <0.97 <0.97 <0.97 40.6 2.9 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 28.3
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Naphthalene mg/l 0.24 1 6 <0.24 <0.24 <0.24 5.8 0.56 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 0.48 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 7.7
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.40 1 0.2 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 5.9 4.4 <0.46 <0.46 <0.46 0.70 0.68 1.0 <0.46 0.97 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 3.3
Toluene mg/l 0.26 1 600 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 0.43
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 6.0 3.8 <0.47 <0.47 <0.47 <0.47 <0.47 1.1 <0.47 0.94 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 3.7
Trichlorofluoromethane mg/l 0.20 1 2000 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 5.7 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 1.9 0.60 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 4.7 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 0.55
Dichlorodifluoromethane mg/l 0.21 1 1000 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 11.4 13.8 18.7 136.6 49.3 ND 14.4 ND 2.6 3.9 31.9 ND 31.4 121.3 7.9 14.4 2.3 1.9 ND ND 9.8 18.9 1.0 1.9 ND ND ND ND 126.6
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on August 20-26, 2013
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2F Aug 13 VOCs of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: PJVH
Checked by: RAD
Table 2G
Volatile Organic Compounds (VOC) February 2014 Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J13-1957-39
Sampled by Pace on February 20-26, 2014 (Pace Project 92190605, 92190677, 92191006 & 92191140)
COMPOUND UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-23D MW-24 MW-25
Acetone mg/l 10.0 25 6000 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0
Acrylonitrile mg/l 1.9 10 NE <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.9 <1.10 <1.9 <1.9
Benzene mg/l 0.25 1 1 0.36 0.86 0.34 16.5 4.4 <0.25 0.72 <0.25 <0.25 <0.25 0.28 <0.25 3.6 1.3 <0.25 0.26 <0.25 <0.25 <0.25 <0.25 0.73 0.54 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 5.7
Bromochloromethane mg/l 0.17 1 NE <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Bromodichloromethane mg/l 0.18 1 0.6 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18 <0.18
Bromoform mg/l 0.26 1 4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Carbon Disulfide mg/l 1.2 2 700 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 1.2 <1.2 <1.2 <1.2 <1.3 <1.2 1.2
Bromomethane (Methylbromide)mg/l 0.29 2 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Carbon tetrachloride mg/l 0.25 1 0.3 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene (mono)mg/l 0.23 1 50 2.5 0.29 <0.23 0.61 <0.23 <0.23 1.2 <0.23 <0.23 <0.23 <0.23 <0.23 0.57 1.5 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 1.8 2.0 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 0.39
Chloroethane mg/l 0.54 1 3000 1.2 0.94 1.1 0.78 1.4 <0.54 1.2 <0.54 <0.54 <0.54 <0.54 <0.54 0.57 1.0 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 1.7 1.6 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54
Chloroform mg/l 0.14 1 70 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 1.4 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14 <0.14
Chloromethane (Methylchloride)mg/l 0.11 1 3 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11
Dibromochloromethane mg/l 0.21 1 0.4 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dibromo-3-chloropropane; DBCP mg/l 2.5 5 0.04 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.6 <2.5 <2.5
1,2-Dibromoethane; Ethylene dibromide mg/l 0.27 1 0.02 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
Dibromomethane mg/l 0.21 1 NE <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,2-Dichlorobenzene mg/l 0.30 1 20 1.0 0.43 <0.30 <0.30 <0.30 <0.30 2.8 <0.30 <0.30 <0.30 3.3 <0.30 <0.30 70.5 1.6 7.2 <0.30 <0.30 <0.30 <0.30 3.1 3.3 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30
1,3-Dichlorobenzene mg/l 0.24 1 200 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 0.42 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24
1,4-Dichlorobenzene mg/l 0.33 1 6 0.49 4.0 <0.33 6.1 1.4 <0.33 2.3 <0.33 <0.33 <0.33 1.0 <0.33 7.3 18.0 0.36 0.72 <0.33 <0.33 <0.33 <0.33 2.8 2.5 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 2.8
trans-1,4-Dichloro-2-butene mg/l 1.0 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.1 <1.0 <1.0
1,1-Dichloroethane mg/l 0.32 1 6 1.2 0.46 3.2 21.2 6.8 <0.32 2.3 <0.32 0.72 1.1 5.2 <0.32 1.7 0.68 <0.32 0.54 <0.32 1.2 <0.32 <0.32 3.4 2.3 0.67 1.1 <0.32 <0.32 <0.32 <0.32 <0.32 8.7
1,2-Dichloroethane mg/l 0.12 1 0.4 0.99 <0.12 <0.12 1.7 0.25 <0.12 1.7 <0.12 <0.12 <0.12 <0.12 <0.12 0.25 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 3.0 2.6 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 0.87
1,1-Dichloroethene (-ethylene)mg/l 0.56 1 7 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56
cis-1,2-Dichloroethene (-ethylene)mg/l 0.19 1 70 0.67 2.8 0.59 27.6 10.2 <0.19 1.6 <0.19 1.0 1.2 14.8 <0.19 10.9 15.1 0.68 3.7 <0.19 0.82 <0.19 <0.19 1.9 0.58 0.35 0.96 <0.19 <0.19 <0.19 <0.19 <0.19 14.1
trans-1,2-Dichloroethene (-ylene)mg/l 0.49 1 100 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49
1,2-Dichloropropane mg/l 0.27 1 0.6 0.31 <0.27 <0.27 0.48 <0.27 <0.27 0.53 <0.27 <0.27 <0.27 0.31 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 0.79 0.71 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
cis-1,3-Dichloropropene (-propylene)mg/l 0.13 1 0.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
trans-1,3-Dichloropropene (-propylene)mg/l 0.26 1 0.4 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Diisopropyl ether (Isopropyl ether)mg/l NT NT 70 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Ethylbenzene mg/l 0.3 1 600 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30
2-Hexanone mg/l 0.46 5 NE <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Iodomethane mg/l 0.32 5 NE <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.32
Dichloromethane (Methylene chloride)mg/l 0.97 1 5 <0.97 <0.97 <0.97 34.1 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97
2-Butanone (Methyl ethyl ketone)mg/l 0.96 5 4000 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96 <0.96
4-Methyl-2-Pentanone mg/l 0.33 5 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
Naphthalene mg/l 0.24 1 6 <0.24 <0.24 <0.24 6.5 0.80 1.6 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 1.0 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 8.9
Styrene mg/l 0.26 1 70 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1,2-Tetrachloroethane mg/l 0.33 1 NE <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33 <0.33
1,1,2,2-Tetrachloroethane mg/l 0.40 1 0.2 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40
Tetrachloroethene (-ethylene)mg/l 0.46 1 0.7 <0.46 <0.46 <0.46 6.0 5.1 <0.46 <0.46 <0.46 0.65 0.54 1.1 <0.46 1.2 <0.46 <0.46 <0.46 <0.46 0.62 <0.46 <0.46 <0.46 <0.46 <0.46 0.52 <0.46 <0.46 <0.46 <0.46 <0.46 1.3
Toluene mg/l 0.26 1 600 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
1,1,1-Trichloroethane mg/l 0.48 1 200 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48
1,1,2-Trichloroethane mg/l 0.29 1 NE <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29 <0.29
Trichloroethene (-ethylene)mg/l 0.47 1 3 <0.47 <0.47 <0.47 6.0 4.1 <0.47 <0.47 <0.47 <0.47 <0.47 1.2 <0.47 0.98 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 1.9
Trichlorofluoromethane mg/l 0.20 1 2000 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20
1,2,3-Trichloropropane mg/l 0.41 1 0.005 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41
Vinyl acetate mg/l 0.35 2 NE <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35 <0.35
Vinyl chloride mg/l 0.62 1 0.03 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
M&P Xylene mg/l 0.66 2 500 <0.66 <0.66 <0.66 4.6 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66 <0.66
O Xylene mg/l 0.23 1 500 <0.23 <0.23 <0.23 1.8 0.52 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23 <0.23
Dichlorodifluoromethane mg/l 0.21 1 1000 <0.21 <0.21 <0.21 0.58 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Total VOCs mg/l NE NE NE 8.7 9.8 5.2 134.6 35.0 1.6 14.4 ND 2.4 2.8 27.2 ND 28.1 108.5 2.6 12.4 1.4 2.6 ND ND 19.2 16.1 1.0 3.8 ND ND ND ND ND 45.9
Notes:
MDL = Laboratory Method Detection Limit NT = Not Tested
RL = Laboratory Report Limit NE = Not Established; North Carolina has not established a MCL
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable Shaded cells indicate exceedance of MCL.
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on August 20-26, 2013
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).Analysis by EPA Method 8260
Table 2G Feb 14 VOCs of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: PJVH
Checked by: RAD
Table 3A (2011)
Pesticides, Herbicides, & Cyanide
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-25
Sampled by Pace on February 22, 2011 (Pace Project 9288391)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Pesticides -- Heptachlor EPA 8081 mg/l 0.0015 0.01 0.008 NT NT NT NT NT <0.0015 <0.0015 <0.0015 <0.0015 <0.0015 0.079 <0.0015 <0.0015 <0.0015 NP <0.0015 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- Methoxychlor EPA 8081 mg/l *V*0.01 40 NT NT NT NT NT <0.0071 <0.0072 <0.0072 <0.0071 <0.0072 <0.0071 <0.0072 <0.0071 <0.0070 NP <0.0071 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- Endosulfan sulfate EPA 8081 mg/l *V*0.01 40 NT NT NT NT NT <0.00061 <0.00061 <0.00062 <0.00061 <0.00061 <0.00061 <0.00061 <0.00061 <0.00060 NP <0.00061 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- beta-BHC EPA 8081 mg/l *V*0.01 0.02 NT NT NT NT NT <0.00051 <0.00051 <0.00052 <0.00051 <0.00051 <0.00051 <0.00051 <0.00051 <0.00050 NP <0.00050 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l 0.0002 0.01 0.03 NT NT NT NT NT <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 0.027 NP <0.0002 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- All Other EPA 8081 mg/l NA NA NA NT NT NT NT NT ND ND ND ND ND ND ND ND ND NP ND NP NP NP NP NP NP NP NP NP NP NP NP NP
Herbicides -- Silvex EPA 8151 mg/l 0.049 2 50 NT NT NT NT NT <0.049 0.078 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 NP <0.049 NP NP NP NP NP NP NP NP NP NP NP NP NP
Herbicides -- All Other EPA 8151 mg/l NA NA NA NT NT NT NT NT ND ND ND ND ND ND ND ND ND NP ND NP NP NP NP NP NP NP NP NP NP NP NP NP
Cyanide SM 4500-CN-E mg/l 0.005 0.005 0.07 NT NT NT NT NT <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.0067 NP 0.0086 NP NP NP NP NP NP NP NP NP NP NP NP NP
Sampled by Pace on August 23, 2011 (Pace Project 92100967)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-21 MW-21 MW-22 MW-23 MW-24 MW-21
Pesticides -- Heptachlor EPA 8081 mg/l *V**V*0.008 <0.054 <0.052 <0.056 <0.054 <0.053 <0.054 <0.057 <0.057 <0.059 <0.062 <0.054 <0.053 <0.050 <0.050 NP <0.057 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- Methoxychlor EPA 8081 mg/l *V**V*40 <0.16 <0.16 <0.17 <0.16 <0.16 <0.16 <0.17 <0.17 <0.18 <0.19 <0.16 <0.16 <0.15 0.15 NP <0.17 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- Endosulfan sulfate EPA 8081 mg/l *V**V*40 <0.054 <0.052 <0.056 <0.054 <0.053 <0.054 <0.057 <0.057 <0.059 <0.062 <0.054 <0.053 <0.050 0.062 NP <0.057 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- beta-BHC EPA 8081 mg/l *V**V*0.02 <0.054 0.13 <0.056 <0.054 <0.053 <0.054 <0.057 <0.057 <0.059 <0.062 <0.054 <0.053 <0.050 <0.050 NP <0.057 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l *V**V*0.03 <0.054 <0.052 <0.056 <0.054 <0.053 <0.054 <0.057 <0.057 <0.059 <0.062 0.27 <0.053 <0.050 <0.050 NP <0.057 NP NP NP NP NP NP NP NP NP NP NP NP NP
Pesticides -- All Other EPA 8081 mg/l NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND NP ND NP NP NP NP NP NP NP NP NP NP NP NP NP
Herbicides -- Silvex EPA 8151 mg/l 0.049 0.19 50 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 <0.049 NP <0.049 NP NP NP NP NP NP NP NP NP NP NP NP NP
Herbicides -- All Other EPA 8151 mg/l NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND NP ND NP NP NP NP NP NP NP NP NP NP NP NP NP
Cyanide SM 4500-CN-E mg/l 0.005 0.005 0.07 <0.005 0.0092 0.0052 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NP <0.005 NP NP NP NP NP NP NP NP NP NP NP NP NP
Notes:
MDL = Laboratory Method Detection Limit *V* = The laboratory report varies the MDL and RL from sample to sample
RL = Laboratory Report Limit NP = Not Present at the time of sampling
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NA = Not Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.NT = Not Tested
Shaded cells indicate exceedance of MCL.NE = Not Established; North Carolina has not established a MCL
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).ND = Not Detected
Samples collected by Pace on dates specifed above
Table 3A PestHerbs (2011) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: TZS
Table 3B (2012)
Pesticides, Herbicides, & Cyanide
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-25
Sampled by Pace on February 21-22, 2012 (Pace Projects 92112617 & 92112760)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Pesticides -- 4,4'-DDT EPA 8081 mg/l <0.050 <0.050 0.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.072 0.054 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- Heptachlor EPA 8081 mg/l <0.050 <0.050 0.008 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- Methoxychlor EPA 8081 mg/l <0.15 <0.15 40 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 NP <0.15 <0.15 NP <0.15 <0.15 <0.15 NP <0.15 NP <0.15 NP NP NP NP
Pesticides -- Endosulfan sulfate EPA 8081 mg/l <0.050 <0.050 40 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 0.061 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- beta-BHC EPA 8081 mg/l <0.050 <0.050 0.02 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l <0.050 <0.050 0.03 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.28 <0.050 <0.050 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 0.056 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- All Other EPA 8081 mg/l NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND NP ND ND NP ND ND ND NP ND NP ND NP NP NP NP
Herbicides -- Silvex EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NP NT NT NP NT NT NT NP NT NP NT NP NP NP NP
Herbicides -- All Other EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NP NT NT NP NT NT NT NP NT NP NT NP NP NP NP
Cyanide SM 4500-CN-E mg/l 0.005 0.005 0.07 <0.005 0.0057 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NP <0.005 <0.005 NP <0.005 <0.005 <0.005 NP <0.005 NP <0.005 NP NP NP NP
Sampled by Pace on August 27-29, 2012 (Pace Project #92129364)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Pesticides -- 4,4'-DDT EPA 8081 mg/l *V**V*0.1 <0.050 <0.2 <0.050 <0.2 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.2 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- Heptachlor EPA 8081 mg/l *V**V*0.008 <0.050 <0.2 <0.050 <0.2 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.2 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- Methoxychlor EPA 8081 mg/l *V**V*40 <0.15 <0.6 <0.15 <0.6 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.6 <0.15 NP <0.15 <0.15 NP <0.15 <0.15 <0.15 NP <0.15 NP <0.15 NP NP NP NP
Pesticides -- Endosulfan sulfate EPA 8081 mg/l *V**V*40 <0.050 <0.2 <0.050 <0.2 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.2 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- beta-BHC EPA 8081 mg/l *V**V*0.02 <0.050 <0.2 <0.050 <0.2 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.2 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 <0.050 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l *V**V*0.03 <0.050 <0.2 <0.050 <0.2 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.2 <0.050 NP <0.050 <0.050 NP <0.050 <0.050 0.084 NP <0.050 NP <0.050 NP NP NP NP
Pesticides -- All Other EPA 8081 mg/l NA NA NA ND ND ND ND ND ND ND ND 0.056 ND ND ND ND ND NP ND ND NP ND ND 0.15 NP ND NP ND NP NP NP NP
Herbicides -- Silvex EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NP NT NT NP NT NT NT NP NT NP NT NP NP NP NP
Herbicides -- All Other EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NP NT NT NP NT NT NT NP NT NP NT NP NP NP NP
Cyanide SM 4500-CN-E mg/l 0.005 0.005 0.07 0.0053 0.0057 <0.005 <0.005 0.0057 0.0052 0.0055 0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NP <0.005 <0.005 NP <0.005 <0.005 <0.005 NP <0.005 NP <0.005 NP NP NP NP
Notes:
MDL = Laboratory Method Detection Limit *V* = The laboratory report varies the MDL and RL from sample to sample
RL = Laboratory Report Limit NP = Not Present at the time of sampling
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NA = Not Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.NT = Not Tested
Shaded cells indicate exceedance of MCL.NE = Not Established; North Carolina has not established a MCL
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).ND = Not Detected
Samples collected by Pace on dates specifed above
Table 3B PestHerbs (2012) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA/BPN
Checked by: TZS/PJVH
Table 3C (2013)
Pesticides, Herbicides, & Cyanide
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J12-1957-34
Sampled by Pace on February 18-21, 2013 (Pace Project 92148500 & 92148504)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Pesticides -- 4,4'-DDT EPA 8081 mg/l 0.05 0.05 0.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- Heptachlor EPA 8081 mg/l 0.05 0.05 0.008 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- Methoxychlor EPA 8081 mg/l 0.15 0.15 40 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15
Pesticides -- Endosulfan sulfate EPA 8081 mg/l 0.05 0.05 40 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- alpha-BHC EPA 8081 mg/l 0.05 0.05 0.02 <0.050 <0.050 <0.050 0.054 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- beta-BHC EPA 8081 mg/l 0.05 0.05 0.02 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l 0.05 0.05 0.03 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.051 <0.050 <0.050 <0.050 0.21 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.061 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- All Other EPA 8081 mg/l NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Herbicides -- Silvex EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Herbicides -- All Other EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Cyanide SM 4500-CN-E mg/l 0.005 0.005 0.07 <0.005 0.0064 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.0053 <0.005 0.0056 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
Sampled by Pace on August 20-26, 2013 (Pace Project #92169299)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Pesticides -- 4,4'-DDT EPA 8081 mg/l 0.05 0.05 0.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- Heptachlor EPA 8081 mg/l 0.05 0.05 0.008 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- Methoxychlor EPA 8081 mg/l 0.15 0.15 40 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15
Pesticides -- Endosulfan sulfate EPA 8081 mg/l 0.05 0.05 40 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- beta-BHC EPA 8081 mg/l 0.05 0.05 0.02 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l 0.05 0.05 0.03 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.10
Pesticides -- All Other EPA 8081 mg/l NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Herbicides -- Silvex EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Herbicides -- All Other EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Cyanide SM 4500-CN-E mg/l 0.0050 0.0050 0.07 <0.005 0.0060 0.0063 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.0057 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
Notes:
MDL = Laboratory Method Detection Limit
RL = Laboratory Report Limit NA = Not Applicable
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NT = Not Tested
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.NE = Not Established; North Carolina has not established a MCL
Shaded cells indicate exceedance of MCL.ND = Not Detected
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).
Samples collected by Pace on dates specifed above
Table 3C PestHerbs (2013) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: PJVH
Checked by: RAD
Table 3D (2014)
Pesticides, Herbicides, & Cyanide
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J13-1957-39
Sampled by Pace on February 20-26, 2014 (Pace Project 92190605, 92190677, 92191006 & 92191140)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-23D MW-24 MW-25
Pesticides -- 4,4'-DDT EPA 8081 mg/l 0.05 0.05 0.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- Heptachlor EPA 8081 mg/l 0.05 0.05 0.008 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.07
Pesticides -- Methoxychlor EPA 8081 mg/l 0.15 0.15 40 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 <0.15
Pesticides -- Endosulfan sulfate EPA 8081 mg/l 0.05 0.05 40 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- alpha-BHC EPA 8081 mg/l 0.05 0.05 0.02 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- beta-BHC EPA 8081 mg/l 0.05 0.05 0.02 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l 0.05 0.05 0.03 <0.050 <0.050 <0.050 0.13 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.22
Pesticides -- All Other EPA 8081 mg/l NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Herbicides -- Silvex EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Herbicides -- All Other EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Cyanide SM 4500-CN-E mg/l 0.005 0.005 0.07 <0.005 <0.005 0.0084 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.0052 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.006 <0.005 <0.005
Sampled by Pace on August TBD, 2014 (Pace Project TBD)
CLASS -- COMPOUND Method UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-23D MW-24 MW-25
Pesticides -- 4,4'-DDT EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Pesticides -- Heptachlor EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Pesticides -- Methoxychlor EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Pesticides -- Endosulfan sulfate EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Pesticides -- beta-BHC EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Pesticides -- gamma-BHC (Lindane)EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Pesticides -- All Other EPA 8081 mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Herbicides -- Silvex EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Herbicides -- All Other EPA 8151 mg/l NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Cyanide SM 4500-CN-E mg/l DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Notes:
MDL = Laboratory Method Detection Limit
RL = Laboratory Report Limit NA = Not Applicable
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NT = Not Tested
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.NE = Not Established; North Carolina has not established a MCL
Shaded cells indicate exceedance of MCL.ND = Not Detected
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).DP = Data Pending
Samples collected by Pace on dates specifed above
Table 3 PestHerbs (2014) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: PJVH
Checked by: RAD
Table 4A (2011)
Total & Dissolved Metals Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-25
Sampled by Pace on February 22, 2011 (Pace Projects 9288391 & 9288386)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 5.1 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Arsenic (As)mg/l 2.7 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 5.8 <5.0 5.3 <5.0 <5.0 <5.0 NP 3.9 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Barium (Ba)mg/l 0.2 5 700 171 191 241 163 237 54 213 72.8 1190 193 138 197 977 309 NP 68.7 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Beryllium (Be)mg/l 0.1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.19 <1.0 3.6 0.51 <1.0 <1.0 <1.0 <1.0 NP <1.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Cadmium (Cd)mg/l 0.5 1 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Chromium (Cr)mg/l 0.4 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 2.5 3.7 6.3 161 17.6 1.7 8.1 1.8 3.7 NP 2.4 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Cobalt (Co)mg/l 0.6 5 NE 10.5 55.5 110 13.5 16.8 1.3 5.4 <5.0 40.5 5.2 9.4 9.8 3.2 6.1 NP 2.6 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Copper (Cu)mg/l 0.3 5 1,000 <5.0 <5.0 5.1 <5.0 155 1.1 2.4 2.3 64.3 10.7 <5.0 3.2 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Lead (Pb)mg/l 4 5 15 <5.0 <5.0 <5.0 <5.0 7.2 <5.0 <5.0 <5.0 16.2 6.3 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Mercury (Hg)mg/l 0.1 0.2 1 NT NT NT NT NT <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 NP <0.20 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Nickel (Ni)mg/l 1.7 5 100 <5.0 <5.0 39 5 5.4 8 <5.0 4.2 97.3 8.4 <5.0 7.6 15.9 7.5 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Selenium (Se)mg/l 3.8 10 20 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 NP <10.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Silver (Ag)mg/l 0.1 5 20 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 0.11 <5.0 <5.0 <5.0 0.34 <5.0 0.37 0.12 NP 0.45 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Thallium (Tl)mg/l 3 5.4 NE <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 4.3 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 NP <5.4 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Vanadium (V)mg/l 0.2 5 NE <5.0 <5.0 <5.0 6.1 <5.0 2.6 4.3 5.6 205 22.8 <5.0 7.8 <5.0 0.38 NP 0.73 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Zinc (Zn)mg/l 0.4 10 1,000 <10.0 <10.0 <10.0 30.7 90.4 5.1 19.8 7.7 162 36.7 10.3 26.5 0.71 16 NP 5.6 NP NP NP NP NP NP NP NP NP NP NP NP NP
Sampled by Pace on August 23, 2011 (Pace Project 92100967)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Arsenic (As)mg/l 2.7 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 8.7 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Arsenic (As)mg/l 2.7 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 5.6 <5.0 5.5 6.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Barium (Ba)mg/l 0.2 5 700 189 189 214 133 280 66.8 1640 76.4 202 71.9 104 191 972 284 NP 57.7 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Barium (Ba)mg/l 0.2 5 700 174 150 132 120 208 33.9 161 62.2 47.4 51.6 88.1 136 902 240 NP 49.9 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Beryllium (Be)mg/l 0.1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Beryllium (Be)mg/l 0.1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Cadmium (Cd)mg/l 0.5 1 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Cadmium (Cd)mg/l 0.5 1 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Chromium (Cr)mg/l 0.4 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 105 <5.0 19.3 <5.0 <5.0 8.3 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Chromium (Cr)mg/l 0.4 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Cobalt (Co)mg/l 0.6 5 NE 8.9 45.4 51.9 6.8 9.7 <5.0 43.1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Cobalt (Co)mg/l 0.6 5 NE 8.3 44.4 44.1 5.6 7.9 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Copper (Cu)mg/l 0.3 5 1,000 <5.0 <5.0 7.9 <5.0 7.3 <5.0 125 <5.0 7.9 <5.0 7.5 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Copper (Cu)mg/l 0.3 5 1,000 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Lead (Pb)mg/l 4 5 15 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 37.2 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Lead (Pb)mg/l 4 5 15 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Mercury (Hg)mg/l 0.1 0.2 1 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NP NT NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Mercury (Hg)mg/l 0.1 0.2 1 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NP NT NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Nickel (Ni)mg/l 1.7 5 100 <5.0 5.7 11.6 8.2 7.4 5.5 62.1 <5.0 10.9 <5.0 5.2 7.7 20.1 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Nickel (Ni)mg/l 1.7 5 100 <5.0 6.4 7.9 8.7 6.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 21.1 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Selenium (Se)mg/l 0.1 10 20 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 NP <10.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Selenium (Se)mg/l 3.8 10 20 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 NP <10.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Silver (Ag)mg/l 0.1 5 20 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Silver (Ag)mg/l 0.1 5 20 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Thallium (Tl)mg/l 3 5.4 NE <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 NP <5.4 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Thallium (Tl)mg/l 3 10 NE <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 NP <10.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Vanadium (V)mg/l 0.2 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 185 <5.0 23.1 <5.0 <5.0 8.1 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Vanadium (V)mg/l 0.2 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Total Zinc (Zn)mg/l 0.4 10 1,000 <10.0 <10.0 59.2 <10.0 16.9 <10.0 283 <10.0 15.9 <10.0 50.6 <10.0 <10.0 21.0 NP <10.0 NP NP NP NP NP NP NP NP NP NP NP NP NP
Dissolved Zinc (Zn)mg/l 0.4 10 1,000 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 15.8 <10.0 <10.0 17.8 NP 52.7 NP NP NP NP NP NP NP NP NP NP NP NP NP
Notes:
MDL = Laboratory Method Detection Limit NP = Not Present at the time of sampling
RL = Laboratory Report Limit NT = Not Tested
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NE = Not Established; North Carolina has not established a MCL
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on dates specifed above
Shaded cells indicate exceedance of MCL.Analysis by EPA Methods 6010 & 7470
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).
Table 4A Metals (2011) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: TZS
Table 4B (2012)
Total Metals Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J11-1957-25
Sampled by Pace on February 21-22, 2012 (Pace Projects 92112617 & 92112760)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP <5.0 NP <5.0 NP NP NP NP
Total Arsenic (As)mg/l 2.7 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 3.1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP <5.0 NP <5.0 NP NP NP NP
Total Barium (Ba)mg/l 0.2 5 700 222 266 175 134 214 48.7 207 62.7 126 102 90.2 196 970 237 NP 49.9 249 NP 93.5 135 141 NP 80.3 NP 56.3 NP NP NP NP
Total Beryllium (Be)mg/l 0.1 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.20 0.25 0.28 <1.0 0.18 <1.0 <1.0 NP <1.0 <1.0 NP <1.0 <1.0 <1.0 NP <1.0 NP <1.0 NP NP NP NP
Total Cadmium (Cd)mg/l 0.5 1 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 <1.0 NP <1.0 <1.0 <1.0 NP <1.0 NP <1.0 NP NP NP NP
Total Chromium (Cr)mg/l 0.4 5 10 2.5 1.2 1.8 1.2 0.91 3.7 5.2 6.9 10.6 6.2 0.85 11.1 3.3 2.5 NP 0.78 5.7 NP <5.0 7.3 <5.0 NP 6.4 NP <5.0 NP NP NP NP
Total Cobalt (Co)mg/l 0.6 5 NE 10.1 30.9 54.0 5.7 5.8 0.90 1.6 1.6 <5.0 <5.0 2.3 2.1 5.5 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP <5.0 NP <5.0 NP NP NP NP
Total Copper (Cu)mg/l 0.3 5 1,000 4.0 1.1 2.4 2.0 1.9 2.3 3.9 5.7 6.9 4.2 1.5 8.3 2.0 2.7 NP 1.4 6.8 NP <5.0 5.4 <5.0 NP 7.4 NP <5.0 NP NP NP NP
Total Lead (Pb)mg/l 4 5 15 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP <5.0 NP <5.0 NP NP NP NP
Total Mercury (Hg)mg/l 0.1 0.2 1 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 NP <0.20 <0.20 NP <0.20 <0.20 <0.20 NP <0.20 NP <0.20 NP NP NP NP
Total Nickel (Ni)mg/l 1.7 5 100 <5.0 <5.0 11.0 9.2 4.8 3.3 <5.0 2.1 5.0 2.0 3.2 9.6 24.6 5.2 NP <5.0 <5.0 NP <5.0 6.2 <5.0 NP 5.9 NP <5.0 NP NP NP NP
Total Selenium (Se)mg/l 3.8 10 20 <10.0 4.5 2.8 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 0.18 1.5 2.6 <10.0 0.66 NP <10.0 <10.0 NP <10.0 <10.0 <10.0 NP <10.0 NP <10.0 NP NP NP NP
Total Silver (Ag)mg/l 0.1 5 20 1.9 2.0 2.5 1.4 1.4 1.2 1.4 1.3 0.28 0.24 1.5 1.4 1.7 1.7 NP 1.8 <5.0 NP <5.0 <5.0 <5.0 NP <5.0 NP <5.0 NP NP NP NP
Total Thallium (Tl)mg/l 3 5.4 NE <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 4.3 <5.4 <5.4 <5.4 NP <5.4 <5.4 NP <5.4 <5.4 <5.4 NP <5.4 NP <5.4 NP NP NP NP
Total Vanadium (V)mg/l 0.2 5 NE 0.84 <5.0 <5.0 1.5 1.4 3.9 4.9 8.8 12.5 8.6 1.2 14.1 5.0 1.1 NP 1.2 11.0 NP <5.0 9.8 6.1 NP 7.6 NP <5.0 NP NP NP NP
Total Zinc (Zn)mg/l 0.4 10 1,000 16.7 8.7 10.5 9.2 8.2 10.4 16.7 16.8 23.1 31.8 8.2 10.9 11.0 143 NP 5.0 21.4 NP 12.4 17.2 24.3 NP 26.9 NP 15.3 NP NP NP NP
Sampled by Pace on August 27-29, 2012 (Pace Project #92129364)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP <5.0 NP <5.0 NP NP NP NP
Total Arsenic (As)mg/l 2.7 5 10 3.1 3.5 5.3 4.5 2.8 <5.0 3.1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP 11.2 NP <5.0 NP NP NP NP
Total Barium (Ba)mg/l 0.2 5 700 174 283 232 151 289 42.8 224 67.4 106 110 106 335 931 237 NP 64 184 NP 96.2 83.7 137 NP 615 NP 51 NP NP NP NP
Total Beryllium (Be)mg/l 0.1 1 NE <1.0 0.13 0.19 <1.0 0.37 <1.0 0.15 <1.0 0.22 0.25 <1.0 0.56 <1.0 <1.0 NP <1.0 0.12 NP 0.14 0.18 0.11 NP 1.1 NP 0.18 NP NP NP NP
Total Cadmium (Cd)mg/l 0.5 1 2 <1.0 <1.0 0.72 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NP <1.0 <1.0 NP <1.0 <1.0 <1.0 NP 0.88 NP <1.0 NP NP NP NP
Total Chromium (Cr)mg/l 0.4 5 10 <5.0 6.2 5.5 0.56 7.1 6.1 9.7 3.4 7.9 6.5 0.55 40.2 0.48 <5.0 NP <5.0 0.92 NP 2.3 0.81 2.2 NP 56.3 0.4 2.4 NP NP NP NP
Total Cobalt (Co)mg/l 0.6 5 NE 8.5 40.0 104.0 9.6 17.3 1.40 5.1 1.1 1.6 1.6 4.1 11.7 15.8 2.8 NP 0.91 1.6 NP 1.2 1.4 2.2 NP 21.4 NP 1.4 NP NP NP NP
Total Copper (Cu)mg/l 0.3 5 1,000 0.92 5.6 9.2 1.6 16.2 0.65 5.6 1.4 3.9 5 1.5 17.3 0.86 0.74 NP 1.2 2.7 NP 1.7 1.2 2.5 NP 78.5 NP 1.6 NP NP NP NP
Total Lead (Pb)mg/l 4 5 15 <5.0 <5.0 5.4 <5.0 4.6 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 9.2 <5.0 <5.0 NP <5.0 <5.0 NP <5.0 <5.0 <5.0 NP 13.3 NP <5.0 NP NP NP NP
Total Mercury (Hg)mg/l 0.1 0.2 1 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 NP <0.20 <0.20 NP <0.20 <0.20 0.11 NP <0.20 NP <0.20 NP NP NP NP
Total Nickel (Ni)mg/l 1.7 5 100 <5.0 13.3 23.0 10.3 9.2 3.9 5.5 <5.0 5.0 3.1 4.0 22.3 34.9 2.5 NP <5.0 <5.0 NP <5.0 1.9 <5.0 NP 60.8 NP <5.0 NP NP NP NP
Total Selenium (Se)mg/l 0.1 10 20 0.33 1.1 0.93 <10.0 <10.0 <10.0 <10.0 1.9 <10.0 <10.0 <10.0 1.5 <10.0 <10.0 NP <10.0 <10.0 NP 0.97 <10.0 <10.0 NP 2.8 NP <10.0 NP NP NP NP
Total Silver (Ag)mg/l 0.1 5 20 0.67 0.98 0.86 0.34 0.44 <5.0 <5.0 <5.0 <5.0 <5.0 0.45 0.18 0.56 0.27 NP 0.65 0.32 NP 0.24 0.23 0.2 NP 0.11 NP <5.0 NP NP NP NP
Total Thallium (Tl)mg/l 3 5.4 NE <5.4 <5.4 <5.4 3.8 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 NP <5.4 <5.4 NP <5.4 <5.4 <5.4 NP <5.4 NP <5.4 NP NP NP NP
Total Vanadium (V)mg/l 0.2 5 NE <5.0 8.1 5.9 2.4 14.7 1.2 9.9 3.4 10.6 10 1.7 49.0 1.1 0.2 NP 1.3 5.5 NP 4.2 2.7 3.4 NP 86.2 NP 2.7 NP NP NP NP
Total Zinc (Zn)mg/l 0.4 10 1,000 7.0 28.0 194 1.7 12.7 37.8 20.3 14.5 10.4 19.5 2.0 21.0 10.8 12.4 NP <10.0 2.2 NP 2.3 <10.0 13.6 NP 198 NP 11.7 NP NP NP NP
Notes:
MDL = Laboratory Method Detection Limit NP = Not Present at the time of sampling
RL = Laboratory Report Limit NT = Not Tested
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NE = Not Established; North Carolina has not established a MCL
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on dates specifed above
Shaded cells indicate exceedance of MCL.Analysis by EPA Methods 6010 & 7470
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).
Table 4B Metals (2012) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA/BPN
Checked by: TZS/PJVH
Table 4C (2013)
Total Metals Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J12-1957-34
Sampled by Pace on February 18-21, 2013 (Pace Projects 92148500 & 92148504)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Arsenic (As)mg/l 2.7 10 10 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 3.2 <10.0 3.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 7.2 <10.0 <10.0
Total Barium (Ba)mg/l 0.20 5 700 267 221 172 128 229 16.2 200 41.3 75.7 86.0 95.5 216 815 238 34.6 42.6 118 56.1 65.6 91.5 131 265 100 54.5 45.6 103 1470 31.6 64.6
Total Beryllium (Be)mg/l 0.10 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.1 <1.0 <1.0 0.12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.14 <1.0 0.12 <1.0 2.5 <1.0 <1.0
Total Cadmium (Cd)mg/l 0.50 1 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.4 <1.0 <1.0
Total Chromium (Cr)mg/l 0.40 5 10 <5.0 <5.0 <5.0 <5.0 1.5 0.44 3.9 4.9 2.9 3.6 <5.0 16.0 0.51 1.9 <5.0 <5.0 <5.0 6.0 1.7 2.6 3.0 <1.0 7.0 <1.0 1.9 <1.0 292 <1.0 51.4
Total Cobalt (Co)mg/l 0.60 5 NE 26.1 49.7 84.3 6.0 14.8 <5.0 <5.0 <5.0 <5.0 0.61 4.3 7.0 20.7 6.2 <5.0 0.97 0.72 <5.0 0.61 2.1 1.0 <5.0 3.2 <5.0 1.6 <5.0 72.7 <5.0 <5.0
Total Copper (Cu)mg/l 0.30 5 1,000 1.6 3.8 12.8 1.4 7.3 <5.0 <5.0 0.89 0.64 1.9 1.7 9.0 0.96 2.4 <5.0 1.4 1.5 <5.0 1.8 2.7 <5.0 <5.0 8.8 <5.0 0.5 <5.0 207 <5.0 12.3
Total Lead (Pb)mg/l 4.0 5 15 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 5.4 <5.0 <5.0
Total Mercury (Hg)mg/l 0.10 0.2 1 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20
Total Nickel (Ni)mg/l 1.7 5 100 2.4 2.6 11.9 <5.0 6.0 <5.0 2.0 2.2 1.9 2.1 2.7 11.3 36.5 2.0 <5.0 <5.0 <5.0 <5.0 <5.0 2.8 2.7 6.6 8.4 <5.0 <5.0 <5.0 104 <5.0 18.5
Total Selenium (Se)mg/l 0.10 10 20 1.4 4.2 6.8 2.5 1.3 <10.0 3.5 2.3 3.4 <10.0 <10.0 0.84 <10.0 <10.0 <10.0 <10.0 3.1 <10.0 2.5 4.7 1.1 <10.0 2.2 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0
Total Silver (Ag)mg/l 0.10 5 20 <5.0 <5.0 <5.0 0.52 0.59 <5.0 0.63 0.39 <5.0 0.45 0.68 0.44 0.68 0.71 <5.0 0.70 0.55 <5.0 0.63 0.57 0.59 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Thallium (Tl)mg/l 3.0 5.4 NE <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4
Total Vanadium (V)mg/l 0.20 5 NE <5.0 <5.0 <5.0 <5.0 4.1 0.55 2.7 5.3 3.0 4.9 <5.0 20.8 0.85 0.61 6.2 <5.0 0.88 <5.0 1.0 2.9 3.5 <5.0 10.6 5.1 1.3 <5.0 393 <5.0 24.5
Total Zinc (Zn)mg/l 0.40 10 1,000 123 25.7 14.2 24.0 11.5 19.5 9.2 20.2 5.9 7.8 9.9 13.6 5.6 13.7 <10.0 3.3 7.1 <10.0 4.9 12.4 5.6 <10.0 24.8 21.4 7.6 <10.0 195 <10.0 39.2
Sampled by Pace on August 20-26, 2013 (Pace Project #92169299)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5.0 NE <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6 <2.6
Total Arsenic (As)mg/l 2.7 10.0 10 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 2.8 <2.7 <2.7 <2.7 <2.7 3.8 <2.7 3.2 3.1 <2.7 <2.7 <2.7 3.2 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 <2.7 4.2
Total Barium (Ba)mg/l 0.20 5.0 700 264 259 149 163 255 23.7 204 50.7 79.8 77.5 111 207 854 281 30.9 45.1 97.1 36.4 48.8 135 112 264 58.9 253 49.6 96.6 283 42.0 106
Total Beryllium (Be)mg/l 0.10 1.0 NE <0.10 <0.10 <0.10 <0.10 <0.10 0.36 0.34 0.34 0.45 0.40 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.34 0.44 0.38 0.44 1.1 0.40 0.44 0.47 0.39 <0.10
Total Cadmium (Cd)mg/l 0.50 1.0 2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
Total Chromium (Cr)mg/l 0.40 5.0 10 <0.40 <0.40 <0.40 1.3 2.8 0.64 3.7 3.5 3.7 2.0 <0.40 6.0 1.4 9.9 0.76 <0.40 0.58 2.1 2.9 6.6 0.95 3.9 3.1 23.8 2.8 3.5 40.6 2.1 151
Total Cobalt (Co)mg/l 0.60 5.0 NE 52.6 155 90.7 11.9 26.6 0.80 3.0 1.4 2.8 1.8 5.3 5.8 16.9 19.5 <0.6 1.6 1.2 1.7 0.7 7.4 2.5 13.3 4.6 23.7 2.8 5.4 22.0 2.1 <0.6
Total Copper (Cu)mg/l 0.30 5.0 1,000 2.4 0.44 0.99 1.0 8.4 <0.3 1.9 1.2 1.6 1.4 2.1 6.3 0.88 8.1 0.36 0.59 <0.3 1.4 <0.3 5.6 0.36 1.9 3.8 28.0 1.7 0.77 25.9 1.1 3.3
Total Lead (Pb)mg/l 4.0 5.0 15 <4.0 4.1 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 <4.0 5.7 <4.0 <4.0 <4.0 <4.0 <4.0
Total Mercury (Hg)mg/l 0.10 0.2 1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
Total Nickel (Ni)mg/l 1.70 5.0 100 <1.7 <1.7 4.4 10.1 8.1 <1.7 <1.7 <1.7 <1.7 <1.7 2.5 5.1 32.2 7.9 <1.7 <1.7 <1.7 <1.7 <1.7 6.3 <1.7 6.2 3.3 11.7 <1.7 2.6 14.3 <1.7 <1.7
Total Selenium (Se)mg/l 0.10 10.0 20 3.1 4.0 <0.1 <0.1 0.43 <0.1 3.7 3.4 <0.1 <0.1 5.2 3.5 <0.1 <0.1 <0.1 <0.1 0.44 <0.1 <0.1 <0.1 4.1 <0.1 <0.1 0.54 <0.1 <0.1 <0.1 <0.1 6.4
Total Silver (Ag)mg/l 0.10 5.0 20 <0.10 <0.10 <0.10 <0.10 0.21 0.61 0.85 0.38 0.62 0.67 0.31 0.12 0.40 0.54 0.23 0.15 <0.10 <0.10 <0.10 <0.10 0.56 1.4 0.47 0.54 0.51 0.51 0.62 0.41 1.8
Total Thallium (Tl)mg/l 3.0 5.4 NE <3.0 <3.0 <3.0 <3.0 <3.0 5.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 3.6 <3.0 <3.0 <3.0 <3.0
Total Vanadium (V)mg/l 0.20 5.0 NE <0.20 <0.20 <0.20 1.1 2.7 1.3 3.6 3.3 6.0 3.7 <0.20 6.8 6.6 14.8 2.1 0.37 1.6 1.8 1.4 8.8 2.0 4.0 5.8 37.2 4.4 4.0 67.9 3.3 <0.20
Total Zinc (Zn)mg/l 0.40 10.0 1,000 14.8 5.4 7.3 7.3 29.0 34.3 10.8 14.1 11.6 17.1 7.0 11.0 12.8 37.6 5.8 3.6 6.5 5.9 5.1 21.8 22.1 102 45.0 129 11.4 25.5 102 34.7 12.1
Notes:
MDL = Laboratory Method Detection Limit NP = Not Present at the time of sampling
RL = Laboratory Report Limit NT = Not Tested
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NE = Not Established; North Carolina has not established a MCL
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on dates specifed above
Shaded cells indicate exceedance of MCL.Analysis by EPA Methods 6010 & 7470
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).
Table 4C Metals (2013) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: PJVH
Checked by: RAD
Table 4D (2014)
Total Metals Data
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J13-1957-39
Sampled by Pace on February 20-26, 2014 (Pace Project 92190605, 92190677, 92191006 & 92191140)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-23D MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Arsenic (As)mg/l 2.7 10 10 <10.0 9.3 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0
Total Barium (Ba)mg/l 0.20 5 700 215 253 159 149 210 16.8 214 13.0 92.5 97.3 85.3 185 823 240 42.4 40.1 176 38.6 48.8 80.1 183 278 32.5 109 122 74.7 86.9 70.8 42.8 19.2
Total Beryllium (Be)mg/l 0.10 1 NE <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
Total Cadmium (Cd)mg/l 0.50 1 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
Total Chromium (Cr)mg/l 0.40 5 10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 6.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 10.8 11.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Cobalt (Co)mg/l 0.60 5 NE 18.3 36.6 48.8 8.5 6.9 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 11.9 <5.0 <5.0 <5.0 5.6 <5.0 <5.0 <5.0 10.2 13.9 <5.0 <5.0 6.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Copper (Cu)mg/l 0.30 5 1,000 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 10.8 8.3 <5.0 <5.0 <5.0 <5.0 <5.0
Total Lead (Pb)mg/l 4.0 5 15 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Mercury (Hg)mg/l 0.10 0.2 1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
Total Nickel (Ni)mg/l 1.7 5 100 <5.0 <5.0 6.2 8.1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 8.0 28.6 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 6.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Selenium (Se)mg/l 0.10 10 20 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0
Total Silver (Ag)mg/l 0.10 5 20 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
Total Thallium (Tl)mg/l 3.0 5.4 NE <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 6.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4 <5.4
Total Vanadium (V)mg/l 0.20 5 NE <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 6.5 7.6 <5.0 7.4 6.2 <5.0 <5.0 <5.0 12.8 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 15.8 16.5 <5.0 5.3 <5.0 <5.0 9.2
Total Zinc (Zn)mg/l 0.40 10 1,000 <10.0 <10.0 19.2 <10.0 <10.0 <10.0 54.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 14.0 <10.0 <10.0 <10.0 12.5 <10.0 <10.0 42.2 22.2 35.2 <10.0 <10.0 13.8 <10.0
Sampled by Pace on August TBD, 2014 (Pace Project TBD)
TEST UNITS MDL RL MCL MW-1A MW-2A MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-14D MW-15 MW-16 MW-16D MW-17 MW-18 MW-19 MW-19D MW-20 MW-20D MW-21 MW-22 MW-23 MW-23D MW-24 MW-25
Total Antimony (Sb)mg/l 2.6 5.0 NE DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Arsenic (As)mg/l 2.7 10.0 10 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Barium (Ba)mg/l 0.20 5.0 700 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Beryllium (Be)mg/l 0.10 1.0 NE DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Cadmium (Cd)mg/l 0.50 1.0 2 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Chromium (Cr)mg/l 0.40 5.0 10 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Cobalt (Co)mg/l 0.60 5.0 NE DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Copper (Cu)mg/l 0.30 5.0 1,000 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Lead (Pb)mg/l 4.0 5.0 15 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Mercury (Hg)mg/l 0.10 0.2 1 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Nickel (Ni)mg/l 1.70 5.0 100 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Selenium (Se)mg/l 0.10 10.0 20 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Silver (Ag)mg/l 0.10 5.0 20 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Thallium (Tl)mg/l 3.0 5.4 NE DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Vanadium (V)mg/l 0.20 5.0 NE DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Total Zinc (Zn)mg/l 0.40 10.0 1,000 DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP DP
Notes:
MDL = Laboratory Method Detection Limit NP = Not Present at the time of sampling
RL = Laboratory Report Limit NT = Not Tested
MCL = Maximum Contaminant Level, as established in the NCDENR Classifications of Water Quality Standards Applicable NE = Not Established; North Carolina has not established a MCL
to Groundwaters of North Carolina, Section 15A NCAC 2L.202.Samples collected by Pace on dates specifed above
Shaded cells indicate exceedance of MCL.Analysis by EPA Methods 6010 & 7470
Refer to the laboratory data sheets for detected concentrations which are J values (estimated values above MDL but below RL).DP = Data Pending
Table 4D Metals (2014) of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: PJVH
Checked by: RAD
Table 5A
Groundwater Sampling Matrix
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J13-1957-39
Lat. North Long. West App II VOCs SVOCs App I Total Metals Dissolved Metals Pesticides Herbicides PCBs Sulfide Cyanide
Well (dd)(dd)EPA 8260 EPA 8270 EPA 6010 EPA 6010/7470 EPA 8081 EPA 8151 EPA 8082 SM 4500-S2D SM 4500-CN-E
MW-1 35.505892476 82.958166600 No No No No No No No No No
MW-1A 35.506035959 82.958960455 Yes No Yes No No No No No Yes
MW-2A 35.505447169 82.956471743 Yes No Yes No Yes No No No Yes
MW-3A 35.504302294 82.955704601 Yes No Yes No No No No No Yes
MW-4 35.502840483 82.958258973 Yes No Yes No Yes No No No No
MW-5 35.502464177 82.958501150 Yes No Yes No No No No No Yes
MW-6 35.507007166 82.958723254 Yes No Yes No No No No No Yes
MW-7 35.506667347 82.957305699 Yes No Yes No Yes No No No Yes
MW-8 35.506214483 82.955920712 Yes No Yes No No No No No Yes
MW-9 35.505397531 82.954853325 Yes No Yes No Yes No No No No
MW-10 35.504410017 82.954568656 Yes No Yes No No No No No No
MW-11 35.503120939 82.957171928 Yes No Yes No Yes No No No Yes
MW-12 35.501892082 82.958559051 Yes No Yes No No No No No No
MW-13 35.502673138 82.959775795 Yes No Yes No Yes No No No Yes
MW-14 35.504089518 82.959967696 Yes No Yes No Yes No No No Yes
MW-14D 35.504044931 82.959967268 Yes No Yes No No No No No No
MW-15 35.505323343 82.959552125 Yes No Yes No No No No No Yes
MW-16 35.502159358 82.960874268 Yes No Yes No No No No No No
MW-16D 35.502129896 82.960839270 Yes No Yes No No No No No No
MW-17 35.503598911 82.961884951 Yes No Yes No No No No No No
MW-18 35.504737902 82.961677540 Yes No Yes No No No No No No
MW-19 35.507123544 82.957192901 Yes No Yes No Yes No No No No
MW-19D 35.507088639 82.957213494 Yes No Yes No Yes No No No No
MW-20 35.504496365 82.954109418 Yes No Yes No No No No No No
MW-20D 35.504495795 82.954138746 Yes No Yes No No No No No No
MW-21 35.502956636 82.955043604 Yes No Yes No No No No No No
MW-22 35.501647029 82.963316321 Yes No Yes No No No No No No
MW-23 35.507695290 82.956901959 Yes No Yes No No No No No No
MW-23D 35.507731029 82.956882336 Yes No Yes No No No No No No
MW-24 35.504639177 82.953652291 Yes No Yes No No No No No No
MW-25 35.503043453 82.957808429 Yes No Yes No Yes No No No No
Notes:
(1) MW-1 is typically dry and cannot be sampled
(2) VOCs = Volatile Organic Compounds (Appendix II List)
(3) SVOCs = Semi-Volatile Organic Compounds
(4) Total metals includes 15 metals (excludes mercury)
(5) EPA or SM #### = Environmental Protection Agency or Standard Method analysis method code
(6) GPS coordinates converted from N&E survey data provided by McGill Associates
(7) dd - decimal degrees
Table 5A GW Matrix of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: MSP
Table 5B
Surface Water Sampling Matrix
Closed Francis Farm Landfill
Haywood County, North Carolina
Permit Number 44-03
BLE Project No. J13-1957-39
Lat. North Long. West App II VOCs App I Total Metals Pesticides Cyanide pH Sp. Cond.Temp.
Location (dd)(dd)EPA 8260 EPA 6010 EPA 8081 SM 4500-CN-E Field Field Field
US-1 35.50145 82.95387 Yes Yes Yes Yes Yes Yes Yes
DS-1 35.50449 82.95406 Yes Yes Yes Yes Yes Yes Yes
DS-2 35.50726 82.95746 Yes Yes Yes Yes Yes Yes Yes
DS-3 35.50513 82.96319 Yes Yes Yes Yes Yes Yes Yes
Notes:
(1) VOCs = Volatile Organic Compounds (Appendix II List)
(2) Total metals includes 15 metals (excludes mercury)
(3) EPA or SM #### = Environmental Protection Agency or Standard Method analysis method code
(4) GPS coordinates measured by BLE via hand-held GPS receiver on January 16, 2014
(5) dd - decimal degrees
Table 5B SW Matrix of FFLF Assessment Tables Feb 2014 1957-39.xlsx
Prepared by: AWA
Checked by: MSP

FIGURES
R
A
C
C
O
O
N

C
R
E
E
K
R
A
C
C
O
O
N

C
R
E
E
K
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
UNNAMED TRIBUTARY
BL
A
N
T
O
N

B
R
A
N
C
H
RATCLIFFE

C
O
V
E

B
R
A
N
C
H
MM-10
MM-11
MM-12
SM-1a
SM-1c
SM-1b
SM-3
MM-7
MM-9
MM-3
MM-13
MM-2
MM-5
MM-4
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
(

F
L
O
W
)
(FL
O
W

)
( FLOW)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
2621.84
MM-5
SM-1a
SM-2
MM-8
MM-1
MM-6
MW-3A
2638.49
MW-3A
MW-4
MW-5
MW-25
MW-1A
*
*
*
*
2621.88
MW-2A
MW-1
R
A
C
C
O
O
N

C
R
E
E
K
R
A
C
C
O
O
N

C
R
E
E
K
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
UNNAMED TRIBUTARY
BL
A
N
T
O
N

B
R
A
N
C
H

RATCLIFFE

C
O
V
E

B
R
A
N
C
H
SM-2
MM-8
MM-1
MM-10
MM-11
MM-12
SM-1a
SM-1c
SM-1b
SM-3
MM-7
MM-6
MM-9
MM-3
MM-13
MM-2
MM-5
MM-4
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
(

F
L
O
W
)
(FL
O
W

)
( FLOW)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
8.7
MW-1
MW-3A
MW-4
MW-5
MM-5
SM-1a
MW-1A
MW-1
MW-2A
MW-4
MW-5
MW-25
MW-1A
R
A
C
C
O
O
N

C
R
E
E
K
R
A
C
C
O
O
N

C
R
E
E
K
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
UNNAMED TRIBUTARY
BL
A
N
T
O
N

B
R
A
N
C
H

RATCLIFFE

C
O
V
E

B
R
A
N
C
H
SM-2
MM-8
MM-1
MM-10
MM-11
MM-12
SM-1a
SM-1c
SM-1b
SM-3
MM-7
MM-6
MM-9
MM-3
MM-13
MM-2
MM-5
MM-4
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
(

F
L
O
W
)
(FL
O
W

)
( FLOW)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
8.7
MW-1
MW-2A
MW-3A
MW-4
MW-5
MM-5
SM-1a
MW-25
MW-1A
DRY
R
A
C
C
O
O
N

C
R
E
E
K
R
A
C
C
O
O
N

C
R
E
E
K
RATC
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
UNNAMED TRIBUTARY
BL
A
N
T
O
N

B
R
A
N
C
H

RATCLIFFE

C
O
V
E

B
R
A
N
C
H
SM-2
MM-8
MM-1
MM-10
MM-11
MM-12
SM-1a
SM-1c
SM-1b
SM-3
MM-7
MM-6
MM-9
MM-3
MM-13
MM-2
MM-5
MM-4
R
A
T
C
L
I
F
F
E

C
O
V
E

B
R
A
N
C
H
(

F
L
O
W
)
(FL
O
W

)
( FLOW)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
(

F
L
O
W
)
MW-1A
MW-1
MW-3A
MW-5
MM-5
SM-1a
MW-25
MW-2A
MW-4
WA
S
T
E

L
I
M
I
T
S
WA
S
T
E

L
I
M
I
T
S
EXISTING GROUND SURFACE
COVE BRANCH
RATCLIFFE
WA
S
T
E

L
I
M
I
T
S
WA
S
T
E

L
I
M
I
T
S
EXISTING GROUND SURFACE
RACOON CREEK
U.S. HIGHWAY 23 BUSINESS
ASHEVILLE ROAD
RATCLIFFE COVE
BRANCH
WA
S
T
E

L
I
M
I
T
S
WA
S
T
E

L
I
M
I
T
S
EXISTING GROUND SURFACE
RATCLIFFE COVE BRANCH
U.S. HIGHWAY 23 BUSINESS
ASHEVILLE ROAD
RACOON
CREEK

APPENDICES

APPENDIX A

DRILLING PROCEDURES

Air Hammer Drilling

Air drilled borings were advanced through unconsolidated and consolidated materials using a downhole
air hammer and compressed air to remove the soil and rock cuttings. The pneumatic drill hammer
rapidly strikes the soil or rock while the drill pipe is slowly rotated. The drill hammers are typically
constructed of alloy steel with tungsten-carbide inserts that provide the chipping or cutting surfaces. An
in-line air filter is attached to the air compressor on the rig to remove oil from the air and to prevent oil
contamination in the borehole.

Representative portions of the soil samples were placed in glass jars or plastic bags. The samples were
examined by a geologist to verify the technician’s and/or driller’s field classifications and Soil Boring
Records were prepared. Soil borings were advanced to their required termination depths for monitoring
well installation.
Hollow Stem Auger Drilling

Soil borings were advanced by mechanically twisting a continuous flight of steel augers into the soil.
Soil sampling was performed by collecting samples of the auger cuttings or split spoon samplers, as
needed.

General

To help prevent cross-contamination between borings, all downhole drilling equipment was steam
cleaned prior to drilling each boring.

APPENDIX B

WELL INSTALLATION PROCEDURES

Type II Monitoring Well

Type II groundwater monitoring wells consist of 2-inch Schedule 40 polyvinyl chloride (PVC) casing
with flush-threaded joints installed in the borehole. The bottom section of each well consists of a
manufactured well screen with 0.01-inch wide machined slots. The well screen was installed to the
approximate termination depth of the borehole.

Type III Monitoring Well

Type III groundwater monitoring wells consist of 6-inch or larger Schedule 40 PVC casing installed to
the top of rock and grouted to the surface. A 2-inch Schedule 40 PVC well riser casing with flush-
threaded joints is installed in the outer casing. The bottom section of each well consists of a
manufactured well screen with 0.01-inch wide machined slots. The well screen is installed to the
approximate termination depth of the borehole or to intercept water bearing fractures.

General

A washed sand filter pack was emplaced around the outside of the pipe from the bottom of the well
casing to from one to five feet above the top of the well screen. The sand filter pack was used to stabilize
the formation and to help yield a less turbid groundwater sample.

A one-foot thick (minimum) bentonite seal was installed on top of the sand filter pack to seal the
monitoring well at the desired level. The well annulus was then grouted to the surface with a cement
grout mixture. A lockable PVC cap and a protective steel cover were placed over each well.

APPENDIX C

DWR WELL CONSTRUCTION RECORD GW-1 FORM
FOR GROUNDWATER MONITORING WELLS
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:

APPENDIX D

WELL CONSTRUCTION AND BORING LOGS
4-inches of TOPSOIL/GRASS
Brown, micaceous, silty, fine to medium SAND -
(alluvium)
Very moist COBBLE layer - (alluvium)
Gray-brown, moist, very micaceous, silty, fine to
medium SAND - (alluvium)
Brown, moist, micaceous, silty, fine to medium SAND
- (alluvium)
PARTIALLY WEATHERED ROCK which sampled as
brown, micaceous, silty, fine to medium SAND
ROCK which sampled as grayish-brown, micaceous,
silty, fine to medium SAND
ND
ND
ND
SURFACE COMPLETION
Flush-mount secured with an
8-inch diameter steel bolted
manhole cover in a 3' x 3' x 4"
concrete pad
Top of PVC casing elev. = 2,611.52
feet
Ground surface elev. = 2,611.75
feet
Northing = 663,182.5348'
Easting = 822,725.7136'
6-inch outer casing set to 37.0 feet
Grout, 0 to 46.7 feet
Borehole diameter 0 to 37 feet,
8-inches
DESCRIPTION
PI
D

(
p
p
m
)
RE
A
D
I
N
G
MONITOR WELL INSTALLATION
DETAILS
SOIL
TYPE
SA
M
P
L
E
S
LOCATION:
DRILLER:
DRILLING METHOD:
2610
2605
2600
2595
2590
2585
2580
2575
CAVING>
GROUNDWATER MONITORING WELL NO. MW-23D
Sheet 1 of 2
10-1-13
DEPTH TO - WATER> INITIAL:
CLIENT:
PROJECT NO.:
END:Haywood County
Waynesville, North Carolina
Landprobe, M. King
ELEVATION/
DEPTH (FT)
5
10
15
20
25
30
35
PROJECT:
CME 750; 8-inch OD hollow stem auger, Schramm T450S; 6-inch air hammer
J13-1957-39
AFTER 24 HOURS:2.8
GROUNDWATER MONITORING WELL NO. MW-23D
START:9-30-13
2611.75ELEVATION:
B. NisbethLOGGED BY:
Francis Farm Landfill
EN
V
_
W
E
L
L
_
O
N
L
Y
_
P
I
D

1
9
5
7
-
3
9
.
G
P
J

6
/
3
0
/
1
4
ROCK which sampled as grayish-brown, micaceous,
silty, fine to medium SAND
Water bearing fracture at 55 feet
Water bearing fracture at 59 feet
Boring terminated at 62.0 feet. Groundwater
encountered at 2.8 feet after 24 hours.
Grout, 0 to 46.7 feet
Bentonite seal, 46.7 to 50.5 feet
Filter pack, sand 50.5 to 62.0 feet
2-inch diameter, 0.010-inch slotted
Schedule 40 PVC well screen, 53.0
to 58.0 feet
Pipe cap
Total well depth, 58.2 feet
Borehole diameter 37 to 62 feet,
6-inches
DESCRIPTION
PI
D

(
p
p
m
)
RE
A
D
I
N
G
MONITOR WELL INSTALLATION
DETAILS
SOIL
TYPE
SA
M
P
L
E
S
LOCATION:
DRILLER:
DRILLING METHOD:
2570
2565
2560
2555
2550
2545
2540
2535
CAVING>
GROUNDWATER MONITORING WELL NO. MW-23D
Sheet 2 of 2
10-1-13
DEPTH TO - WATER> INITIAL:
CLIENT:
PROJECT NO.:
END:Haywood County
Waynesville, North Carolina
Landprobe, M. King
ELEVATION/
DEPTH (FT)
45
50
55
60
65
70
75
PROJECT:
CME 750; 8-inch OD hollow stem auger, Schramm T450S; 6-inch air hammer
J13-1957-39
AFTER 24 HOURS:2.8
GROUNDWATER MONITORING WELL NO. MW-23D
START:9-30-13
2611.75ELEVATION:
B. NisbethLOGGED BY:
Francis Farm Landfill
EN
V
_
W
E
L
L
_
O
N
L
Y
_
P
I
D

1
9
5
7
-
3
9
.
G
P
J

6
/
3
0
/
1
4

APPENDIX E

MONITORING WELL DEVELOPMENT LOGS
MONITORING WELL DEVELOPMENT LOG
DATE 1/16/2014 TOTAL WELL DEPTH (TWD); TOP OF CASING =58.00 1/100 ft
PERSONNEL BPN DEPTH TO GROUND WATER (DGW) =1.14 1/100 ft
SITE Francis Farm Landfill LENGTH OF WATER COLUMN (LWC) = TWD - DGW =56.86 1/100 ft
JOB #1957-39 1 CASING VOLUME (CV) = LWC x 0.17 =9.7 gallons
WELL ID MW-23D
WEATHER Clear TOTAL VOLUME OF WATER REMOVED =220.0 gallons
AIR TEMP.20°F - 32°F METHOD OF WELL DEVELOPMENT =Pump
TIME VOLUME PURGED WATER pH Eh SPECIF. COND.TURBIDITY SAND CONTENT Remarks
(gallons)TEMP (°C)(units)(umho/cm)NTU (%)
935 0.0 10.2 8.02 129.2 1000+Surged Initially
942 10 12.7 7.70 102.3 1000+
950 20 12.8 7.32 102.6 1000+
1000 30 13.5 7.16 103.0 1000+
1010 40 13.1 6.99 95.9 83.2
1020 50 13.7 6.92 96.1 25.7 Surged @ 50 gallons
1042 60 13.7 6.90 95.4 1000+
1052 70 13.6 6.75 99.5 1000+
1102 80 13.5 6.75 96.4 95.4
1112 90 13.8 6.65 95.5 21
1122 100.0 13.7 6.65 96.4 18.1 Surged @ 100 gallons
1145 120.0 13.6 6.65 95.8 429
1205 140.0 12.5 6.70 96.1 9.21
1225 160.0 13.3 6.72 95.6 9.61
1245 180.0 13.0 6.60 95.8 4.25
1305 200.0 13.3 6.60 97.7 5.15
1325 220.0 13.1 6.62 97.0 4.88 Stopped @ 220 gallons
Prepared by: BPN
Checked by: AWA

APPENDIX F

LABORATORY ANALYTICAL DATA
#=CL#
March 19, 2014
LIMS USE: FR - STEPHEN KING
LIMS OBJECT ID: 92190605
92190605
Project:
Pace Project No.:
RE:
Mr. Stephen King
Haywood Co. Solid Waste
278 Recycle Rd.
Clyde, NC 28721
Haywood FFLF MWs
Dear Mr. King:
Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
cc:Andy Alexander, BLE
Mr. Stephen King, Haywood Co. Solid Waste
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 71
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 71
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Lab ID Sample ID Matrix Date Collected Date Received
92190605001 MW-6 Water 02/20/14 15:40 02/21/14 09:35
92190605002 MW-7 Water 02/20/14 15:55 02/21/14 09:35
92190605003 MW-8 Water 02/20/14 16:40 02/21/14 09:35
92190605004 MW-9 Water 02/20/14 17:05 02/21/14 09:35
92190605005 MW-10 Water 02/20/14 17:25 02/21/14 09:35
92190605006 MW-19 Water 02/20/14 16:10 02/21/14 09:35
92190605007 MW-19D Water 02/20/14 16:20 02/21/14 09:35
92190605008 MW-20 Water 02/20/14 17:40 02/21/14 09:35
92190605009 MW-20D Water 02/20/14 17:55 02/21/14 09:35
92190605010 MW-21 Water 02/20/14 14:40 02/21/14 09:35
92190605011 MW-24 Water 02/20/14 15:00 02/21/14 09:35
92190605012 US-1 Water 02/20/14 14:15 02/21/14 09:35
92190605013 DS-1 Water 02/20/14 12:45 02/21/14 09:35
92190605014 DS-2 Water 02/20/14 16:30 02/21/14 09:35
92190605015 DS-3 Water 02/20/14 18:30 02/21/14 09:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92190605001 MW-6 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605002 MW-7 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605003 MW-8 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605004 MW-9 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605005 MW-10 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605006 MW-19 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605007 MW-19D EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605008 MW-20 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605009 MW-20D EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605010 MW-21 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605011 MW-24 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605012 US-1 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605013 DS-1 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605014 DS-2 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190605015 DS-3 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-CN-E 1 PASI-AJDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-6 Lab ID:92190605001 Collected:02/20/14 15:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:291
Collected Date 02/20/14 03/12/14 16:291
Collected Time 15:40 03/12/14 16:291
Field pH 5.8 Std. Units 03/12/14 16:290.10 0.10 1
Field Temperature 11.3 deg C 03/12/14 16:290.50 0.50 1
Field Specific Conductance >4 umhos/cm 03/12/14 16:291.0 1.0 1
Turbidity 3.30 NTU 03/12/14 16:291.0 1.0 1
Odor NONE 03/12/14 16:291
Appearance CLEAR 03/12/14 16:291
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 17:03 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 17:03 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 17:03 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 17:03 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 17:03 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 17:03 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 17:03 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 17:03 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 17:03 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 17:03 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 17:03 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 17:03 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 17:03 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 17:03 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 17:03 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 17:03 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 17:03 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 17:03 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 17:03 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 17:03 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 17:03 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 17:03 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %03/07/14 17:03 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)66 %03/07/14 17:03 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/24/14 23:27 7440-36-002/22/14 08:455.0 5.0 1
Arsenic ND ug/L 02/24/14 23:27 7440-38-202/22/14 08:4510.0 5.0 1
Barium 16.8 ug/L 02/24/14 23:27 7440-39-302/22/14 08:455.0 5.0 1
Beryllium ND ug/L 02/24/14 23:27 7440-41-702/22/14 08:451.0 1.0 1
Cadmium ND ug/L 02/24/14 23:27 7440-43-902/22/14 08:451.0 1.0 1
Chromium ND ug/L 02/24/14 23:27 7440-47-302/22/14 08:455.0 5.0 1
Cobalt ND ug/L 02/24/14 23:27 7440-48-402/22/14 08:455.0 5.0 1
Copper ND ug/L 02/24/14 23:27 7440-50-802/22/14 08:455.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-6 Lab ID:92190605001 Collected:02/20/14 15:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/24/14 23:27 7439-92-102/22/14 08:455.0 5.0 1
Nickel ND ug/L 02/24/14 23:27 7440-02-002/22/14 08:455.0 5.0 1
Selenium ND ug/L 02/24/14 23:27 7782-49-202/22/14 08:4510.0 10.0 1
Silver ND ug/L 02/24/14 23:27 7440-22-402/22/14 08:455.0 5.0 1
Thallium ND ug/L 02/24/14 23:27 7440-28-002/22/14 08:455.4 5.4 1
Vanadium ND ug/L 02/24/14 23:27 7440-62-202/22/14 08:455.0 5.0 1
Zinc ND ug/L 02/24/14 23:27 7440-66-602/22/14 08:4510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:33 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 06:54 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 06:54 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 06:54 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 06:54 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 06:54 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 06:54 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 06:54 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 06:54 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 06:54 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 06:54 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 06:54 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 06:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 06:54 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 06:54 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 06:54 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 06:54 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 06:54 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 06:54 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 06:54 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 06:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 06:54 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 06:54 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 06:54 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 06:54 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 06:54 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 06:54 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 06:54 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 06:54 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 06:54 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 06:54 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 06:54 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 06:54 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 06:54 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 06:54 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-6 Lab ID:92190605001 Collected:02/20/14 15:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 06:54 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 06:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 06:54 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 06:54 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 06:54 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 06:54 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 06:54 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 06:54 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 06:54 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 06:54 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 06:54 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 06:54 108-10-15.0 0.33 1
Naphthalene 1.6 ug/L 02/24/14 06:54 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 06:54 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 06:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 06:54 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 06:54 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 06:54 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 06:54 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 06:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 06:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 06:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 06:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 06:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 06:54 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 06:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 06:54 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 06:54 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 06:54 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/24/14 06:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/24/14 06:54 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 06:54 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 12:51 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-7 Lab ID:92190605002 Collected:02/20/14 15:55 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:371
Collected Date 02/20/14 03/12/14 16:371
Collected Time 15:55 03/12/14 16:371
Field pH 5.9 Std. Units 03/12/14 16:370.10 0.10 1
Field Temperature 12.5 deg C 03/12/14 16:370.50 0.50 1
Field Specific Conductance 383 umhos/cm 03/12/14 16:371.0 1.0 1
Turbidity 4.60 NTU 03/12/14 16:371.0 1.0 1
Odor NONE 03/12/14 16:371
Appearance CLEAR 03/12/14 16:371
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 17:21 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 17:21 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 17:21 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 17:21 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 17:21 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 17:21 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 17:21 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 17:21 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 17:21 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 17:21 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 17:21 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 17:21 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 17:21 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 17:21 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 17:21 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 17:21 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 17:21 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 17:21 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 17:21 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 17:21 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 17:21 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 17:21 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)75 %03/07/14 17:21 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)81 %03/07/14 17:21 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/24/14 23:42 7440-36-002/22/14 08:455.0 5.0 1
Arsenic ND ug/L 02/24/14 23:42 7440-38-202/22/14 08:4510.0 5.0 1
Barium 214 ug/L 02/24/14 23:42 7440-39-302/22/14 08:455.0 5.0 1
Beryllium ND ug/L 02/24/14 23:42 7440-41-702/22/14 08:451.0 1.0 1
Cadmium ND ug/L 02/24/14 23:42 7440-43-902/22/14 08:451.0 1.0 1
Chromium ND ug/L 02/24/14 23:42 7440-47-302/22/14 08:455.0 5.0 1
Cobalt ND ug/L 02/24/14 23:42 7440-48-402/22/14 08:455.0 5.0 1
Copper ND ug/L 02/24/14 23:42 7440-50-802/22/14 08:455.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-7 Lab ID:92190605002 Collected:02/20/14 15:55 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/24/14 23:42 7439-92-102/22/14 08:455.0 5.0 1
Nickel ND ug/L 02/24/14 23:42 7440-02-002/22/14 08:455.0 5.0 1
Selenium ND ug/L 02/24/14 23:42 7782-49-202/22/14 08:4510.0 10.0 1
Silver ND ug/L 02/24/14 23:42 7440-22-402/22/14 08:455.0 5.0 1
Thallium ND ug/L 02/24/14 23:42 7440-28-002/22/14 08:455.4 5.4 1
Vanadium ND ug/L 02/24/14 23:42 7440-62-202/22/14 08:455.0 5.0 1
Zinc 54.0 ug/L 02/24/14 23:42 7440-66-602/22/14 08:4510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:35 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 07:09 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 07:09 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 07:09 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 07:09 107-05-12.0 1.5 1
Benzene 0.72J ug/L 02/24/14 07:09 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 07:09 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 07:09 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 07:09 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 07:09 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 07:09 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 07:09 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 07:09 56-23-51.0 0.25 1
Chlorobenzene 1.2 ug/L 02/24/14 07:09 108-90-71.0 0.23 1
Chloroethane 1.2 ug/L 02/24/14 07:09 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 07:09 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 07:09 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 07:09 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 07:09 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 07:09 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 07:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 07:09 74-95-31.0 0.21 1
1,2-Dichlorobenzene 2.8 ug/L 02/24/14 07:09 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 07:09 541-73-11.0 0.24 1
1,4-Dichlorobenzene 2.3 ug/L 02/24/14 07:09 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 07:09 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 07:09 75-71-81.0 0.21 1
1,1-Dichloroethane 2.3 ug/L 02/24/14 07:09 75-34-31.0 0.32 1
1,2-Dichloroethane 1.7 ug/L 02/24/14 07:09 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 07:09 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 1.6 ug/L 02/24/14 07:09 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 07:09 156-60-51.0 0.49 1
1,2-Dichloropropane 0.53J ug/L 02/24/14 07:09 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 07:09 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 07:09 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-7 Lab ID:92190605002 Collected:02/20/14 15:55 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 07:09 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 07:09 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 07:09 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 07:09 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 07:09 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 07:09 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 07:09 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 07:09 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 07:09 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 07:09 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 07:09 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 07:09 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 07:09 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 07:09 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 07:09 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 07:09 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 07:09 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 07:09 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 07:09 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 07:09 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 07:09 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 07:09 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 07:09 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 07:09 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 07:09 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 07:09 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 07:09 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 07:09 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 07:09 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 07:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/24/14 07:09 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 07:09 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 12:51 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-8 Lab ID:92190605003 Collected:02/20/14 16:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:331
Collected Date 02/20/14 03/12/14 16:331
Collected Time 16:40 03/12/14 16:331
Field pH 6.3 Std. Units 03/12/14 16:330.10 0.10 1
Field Temperature 10.5 deg C 03/12/14 16:330.50 0.50 1
Field Specific Conductance 208 umhos/cm 03/12/14 16:331.0 1.0 1
Turbidity 2.87 NTU 03/12/14 16:331.0 1.0 1
Odor NONE 03/12/14 16:331
Appearance CLEAR 03/12/14 16:331
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 17:38 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 17:38 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 17:38 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 17:38 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 17:38 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 17:38 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 17:38 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 17:38 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 17:38 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 17:38 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 17:38 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 17:38 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 17:38 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 17:38 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 17:38 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 17:38 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 17:38 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 17:38 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 17:38 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 17:38 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 17:38 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 17:38 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)67 %03/07/14 17:38 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)72 %03/07/14 17:38 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 22:22 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 22:22 7440-38-202/26/14 11:3510.0 5.0 1
Barium 13.0 ug/L 02/27/14 22:22 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 22:22 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 22:22 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 22:22 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 22:22 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 22:22 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-8 Lab ID:92190605003 Collected:02/20/14 16:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 22:22 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 22:22 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 22:22 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 22:22 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 22:22 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 22:22 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 22:22 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:38 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 07:25 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 07:25 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 07:25 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 07:25 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 07:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 07:25 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 07:25 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 07:25 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 07:25 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 07:25 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 07:25 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 07:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 07:25 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 07:25 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 07:25 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 07:25 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 07:25 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 07:25 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 07:25 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 07:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 07:25 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 07:25 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 07:25 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 07:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 07:25 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 07:25 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 07:25 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 07:25 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 07:25 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 07:25 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 07:25 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 07:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 07:25 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 07:25 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-8 Lab ID:92190605003 Collected:02/20/14 16:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 07:25 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 07:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 07:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 07:25 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 07:25 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 07:25 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 07:25 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 07:25 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 07:25 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 07:25 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 07:25 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 07:25 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 07:25 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 07:25 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 07:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 07:25 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 07:25 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 07:25 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 07:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 07:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 07:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 07:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 07:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 07:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 07:25 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 07:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 07:25 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 07:25 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 07:25 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 07:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/24/14 07:25 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 07:25 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 12:56 57-12-5 M10.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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Page 15 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-9 Lab ID:92190605004 Collected:02/20/14 17:05 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:381
Collected Date 02/20/14 03/12/14 16:381
Collected Time 17:05 03/12/14 16:381
Field pH 5.9 Std. Units 03/12/14 16:380.10 0.10 1
Field Temperature 11.4 deg C 03/12/14 16:380.50 0.50 1
Field Specific Conductance 115 umhos/cm 03/12/14 16:381.0 1.0 1
Turbidity 3.70 NTU 03/12/14 16:381.0 1.0 1
Odor NONE 03/12/14 16:381
Appearance CLEAR 03/12/14 16:381
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 17:56 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 17:56 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 17:56 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 17:56 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 17:56 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 17:56 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 17:56 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 17:56 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 17:56 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 17:56 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 17:56 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 17:56 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 17:56 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 17:56 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 17:56 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 17:56 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 17:56 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 17:56 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 17:56 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 17:56 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 17:56 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 17:56 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)71 %03/07/14 17:56 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)71 %03/07/14 17:56 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 22:33 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 22:33 7440-38-202/26/14 11:3510.0 5.0 1
Barium 92.5 ug/L 02/27/14 22:33 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 22:33 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 22:33 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 22:33 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 22:33 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 22:33 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-9 Lab ID:92190605004 Collected:02/20/14 17:05 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 22:33 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 22:33 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 22:33 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 22:33 7440-22-402/26/14 11:355.0 5.0 1
Thallium 6.4 ug/L 02/27/14 22:33 7440-28-002/26/14 11:355.4 5.4 1
Vanadium 6.5 ug/L 02/27/14 22:33 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 22:33 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:40 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 07:41 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 07:41 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 07:41 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 07:41 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 07:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 07:41 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 07:41 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 07:41 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 07:41 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 07:41 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 07:41 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 07:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 07:41 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 07:41 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 07:41 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 07:41 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 07:41 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 07:41 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 07:41 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 07:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 07:41 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 07:41 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 07:41 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 07:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 07:41 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 07:41 75-71-81.0 0.21 1
1,1-Dichloroethane 0.72J ug/L 02/24/14 07:41 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 07:41 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 07:41 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 1.0 ug/L 02/24/14 07:41 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 07:41 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 07:41 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 07:41 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 07:41 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-9 Lab ID:92190605004 Collected:02/20/14 17:05 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 07:41 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 07:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 07:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 07:41 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 07:41 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 07:41 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 07:41 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 07:41 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 07:41 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 07:41 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 07:41 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 07:41 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 07:41 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 07:41 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 07:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 07:41 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 07:41 79-34-51.0 0.40 1
Tetrachloroethene 0.65J ug/L 02/24/14 07:41 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 07:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 07:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 07:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 07:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 07:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 07:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 07:41 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 07:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 07:41 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 07:41 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 07:41 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 07:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/24/14 07:41 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 07:41 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 12:58 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-10 Lab ID:92190605005 Collected:02/20/14 17:25 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:401
Collected Date 02/20/14 03/12/14 16:401
Collected Time 17:25 03/12/14 16:401
Field pH 5.5 Std. Units 03/12/14 16:400.10 0.10 1
Field Temperature 11.6 deg C 03/12/14 16:400.50 0.50 1
Field Specific Conductance 62 umhos/cm 03/12/14 16:401.0 1.0 1
Turbidity 67 NTU 03/12/14 16:401.0 1.0 1
Odor NONE 03/12/14 16:401
Appearance OPAQUE 03/12/14 16:401
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 18:13 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 18:13 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 18:13 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 18:13 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 18:13 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 18:13 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 18:13 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 18:13 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 18:13 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 18:13 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 18:13 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 18:13 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 18:13 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 18:13 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 18:13 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 18:13 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 18:13 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 18:13 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 18:13 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 18:13 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 18:13 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 18:13 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)78 %03/07/14 18:13 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)65 %03/07/14 18:13 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 22:36 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 22:36 7440-38-202/26/14 11:3510.0 5.0 1
Barium 97.3 ug/L 02/27/14 22:36 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 22:36 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 22:36 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 22:36 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 22:36 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 22:36 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-10 Lab ID:92190605005 Collected:02/20/14 17:25 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 22:36 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 22:36 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 22:36 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 22:36 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 22:36 7440-28-002/26/14 11:355.4 5.4 1
Vanadium 7.6 ug/L 02/27/14 22:36 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 22:36 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:43 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 07:56 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 07:56 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 07:56 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 07:56 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 07:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 07:56 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 07:56 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 07:56 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 07:56 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 07:56 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 07:56 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 07:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 07:56 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 07:56 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 07:56 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 07:56 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 07:56 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 07:56 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 07:56 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 07:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 07:56 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 07:56 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 07:56 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 07:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 07:56 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 07:56 75-71-81.0 0.21 1
1,1-Dichloroethane 1.1 ug/L 02/24/14 07:56 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 07:56 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 07:56 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 1.2 ug/L 02/24/14 07:56 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 07:56 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 07:56 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 07:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 07:56 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-10 Lab ID:92190605005 Collected:02/20/14 17:25 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 07:56 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 07:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 07:56 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 07:56 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 07:56 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 07:56 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 07:56 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 07:56 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 07:56 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 07:56 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 07:56 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 07:56 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 07:56 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 07:56 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 07:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 07:56 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 07:56 79-34-51.0 0.40 1
Tetrachloroethene 0.54J ug/L 02/24/14 07:56 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 07:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 07:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 07:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 07:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 07:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 07:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 07:56 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 07:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 07:56 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 07:56 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 07:56 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)96 %02/24/14 07:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/24/14 07:56 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 07:56 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 12:59 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-19 Lab ID:92190605006 Collected:02/20/14 16:10 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:411
Collected Date 02/20/14 03/12/14 16:411
Collected Time 16:10 03/12/14 16:411
Field pH 5.8 Std. Units 03/12/14 16:410.10 0.10 1
Field Temperature 13.6 deg C 03/12/14 16:410.50 0.50 1
Field Specific Conductance 440 umhos/cm 03/12/14 16:411.0 1.0 1
Turbidity 2.22 NTU 03/12/14 16:411.0 1.0 1
Odor NONE 03/12/14 16:411
Appearance CLEAR 03/12/14 16:411
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 19:06 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 19:06 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 19:06 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 19:06 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 19:06 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 19:06 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 19:06 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 19:06 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 19:06 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 19:06 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 19:06 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 19:06 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 19:06 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 19:06 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 19:06 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 19:06 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 19:06 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 19:06 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 19:06 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 19:06 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 19:06 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 19:06 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)62 %03/07/14 19:06 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)84 %03/07/14 19:06 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 22:39 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 22:39 7440-38-202/26/14 11:3510.0 5.0 1
Barium 183 ug/L 02/27/14 22:39 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 22:39 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 22:39 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 22:39 7440-47-302/26/14 11:355.0 5.0 1
Cobalt 10.2 ug/L 02/27/14 22:39 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 22:39 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-19 Lab ID:92190605006 Collected:02/20/14 16:10 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 22:39 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 22:39 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 22:39 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 22:39 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 22:39 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 22:39 7440-62-202/26/14 11:355.0 5.0 1
Zinc 12.5 ug/L 02/27/14 22:39 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:46 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 08:12 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 08:12 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 08:12 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 08:12 107-05-12.0 1.5 1
Benzene 0.73J ug/L 02/24/14 08:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 08:12 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 08:12 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 08:12 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 08:12 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 08:12 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 08:12 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 08:12 56-23-51.0 0.25 1
Chlorobenzene 1.8 ug/L 02/24/14 08:12 108-90-71.0 0.23 1
Chloroethane 1.7 ug/L 02/24/14 08:12 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 08:12 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 08:12 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 08:12 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 08:12 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 08:12 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 08:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 08:12 74-95-31.0 0.21 1
1,2-Dichlorobenzene 3.1 ug/L 02/24/14 08:12 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 08:12 541-73-11.0 0.24 1
1,4-Dichlorobenzene 2.8 ug/L 02/24/14 08:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 08:12 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 08:12 75-71-81.0 0.21 1
1,1-Dichloroethane 3.4 ug/L 02/24/14 08:12 75-34-31.0 0.32 1
1,2-Dichloroethane 3.0 ug/L 02/24/14 08:12 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 08:12 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 1.9 ug/L 02/24/14 08:12 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 08:12 156-60-51.0 0.49 1
1,2-Dichloropropane 0.79J ug/L 02/24/14 08:12 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 08:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 08:12 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-19 Lab ID:92190605006 Collected:02/20/14 16:10 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 08:12 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 08:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 08:12 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 08:12 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 08:12 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 08:12 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 08:12 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 08:12 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 08:12 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 08:12 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 08:12 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 08:12 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 08:12 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 08:12 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 08:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 08:12 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 08:12 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 08:12 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 08:12 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 08:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 08:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 08:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 08:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 08:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 08:12 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 08:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 08:12 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 08:12 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 08:12 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/24/14 08:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/24/14 08:12 17060-07-070-130 1
Toluene-d8 (S)97 %02/24/14 08:12 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:00 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-19D Lab ID:92190605007 Collected:02/20/14 16:20 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:421
Collected Date 02/20/14 03/12/14 16:421
Collected Time 16:20 03/12/14 16:421
Field pH 6.1 Std. Units 03/12/14 16:420.10 0.10 1
Field Temperature 12.8 deg C 03/12/14 16:420.50 0.50 1
Field Specific Conductance 639 umhos/cm 03/12/14 16:421.0 1.0 1
Turbidity 3.12 NTU 03/12/14 16:421.0 1.0 1
Odor NONE 03/12/14 16:421
Appearance CLEAR 03/12/14 16:421
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 19:23 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 19:23 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 19:23 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 19:23 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 19:23 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 19:23 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 19:23 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 19:23 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 19:23 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 19:23 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 19:23 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 19:23 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 19:23 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 19:23 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 19:23 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 19:23 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 19:23 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 19:23 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 19:23 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 19:23 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 19:23 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 19:23 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)61 %03/07/14 19:23 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)101 %03/07/14 19:23 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 22:53 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 22:53 7440-38-202/26/14 11:3510.0 5.0 1
Barium 278 ug/L 02/27/14 22:53 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 22:53 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 22:53 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 22:53 7440-47-302/26/14 11:355.0 5.0 1
Cobalt 13.9 ug/L 02/27/14 22:53 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 22:53 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-19D Lab ID:92190605007 Collected:02/20/14 16:20 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 22:53 7439-92-102/26/14 11:355.0 5.0 1
Nickel 6.5 ug/L 02/27/14 22:53 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 22:53 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 22:53 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 22:53 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 22:53 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 22:53 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/24/14 19:48 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 08:27 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 08:27 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 08:27 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 08:27 107-05-12.0 1.5 1
Benzene 0.54J ug/L 02/24/14 08:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 08:27 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 08:27 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 08:27 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 08:27 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 08:27 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 08:27 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 08:27 56-23-51.0 0.25 1
Chlorobenzene 2.0 ug/L 02/24/14 08:27 108-90-71.0 0.23 1
Chloroethane 1.6 ug/L 02/24/14 08:27 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 08:27 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 08:27 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 08:27 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 08:27 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 08:27 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 08:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 08:27 74-95-31.0 0.21 1
1,2-Dichlorobenzene 3.3 ug/L 02/24/14 08:27 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 08:27 541-73-11.0 0.24 1
1,4-Dichlorobenzene 2.5 ug/L 02/24/14 08:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 08:27 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 08:27 75-71-81.0 0.21 1
1,1-Dichloroethane 2.3 ug/L 02/24/14 08:27 75-34-31.0 0.32 1
1,2-Dichloroethane 2.6 ug/L 02/24/14 08:27 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 08:27 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.58J ug/L 02/24/14 08:27 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 08:27 156-60-51.0 0.49 1
1,2-Dichloropropane 0.71J ug/L 02/24/14 08:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 08:27 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 08:27 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-19D Lab ID:92190605007 Collected:02/20/14 16:20 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 08:27 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 08:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 08:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 08:27 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 08:27 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 08:27 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 08:27 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 08:27 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 08:27 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 08:27 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 08:27 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 08:27 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 08:27 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 08:27 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 08:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 08:27 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 08:27 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 08:27 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 08:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 08:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 08:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 08:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 08:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 08:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 08:27 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 08:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 08:27 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 08:27 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 08:27 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 08:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/24/14 08:27 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 08:27 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:01 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-20 Lab ID:92190605008 Collected:02/20/14 17:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:421
Collected Date 02/20/14 03/12/14 16:421
Collected Time 17:40 03/12/14 16:421
Field pH 6.3 Std. Units 03/12/14 16:420.10 0.10 1
Field Temperature 13.4 deg C 03/12/14 16:420.50 0.50 1
Field Specific Conductance 61 umhos/cm 03/12/14 16:421.0 1.0 1
Turbidity 3.38 NTU 03/12/14 16:421.0 1.0 1
Odor NONE 03/12/14 16:421
Appearance CLEAR 03/12/14 16:421
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 19:41 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 19:41 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 19:41 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 19:41 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 19:41 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 19:41 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 19:41 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 19:41 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 19:41 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 19:41 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 19:41 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 19:41 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 19:41 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 19:41 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 19:41 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 19:41 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 19:41 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 19:41 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 19:41 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 19:41 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 19:41 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 19:41 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)70 %03/07/14 19:41 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)65 %03/07/14 19:41 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 22:56 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 22:56 7440-38-202/26/14 11:3510.0 5.0 1
Barium 32.5 ug/L 02/27/14 22:56 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 22:56 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 22:56 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 22:56 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 22:56 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 22:56 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-20 Lab ID:92190605008 Collected:02/20/14 17:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 22:56 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 22:56 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 22:56 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 22:56 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 22:56 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 22:56 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 22:56 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/25/14 15:47 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 08:43 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 08:43 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 08:43 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 08:43 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 08:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 08:43 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 08:43 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 08:43 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 08:43 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 08:43 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 08:43 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 08:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 08:43 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 08:43 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 08:43 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 08:43 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 08:43 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 08:43 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 08:43 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 08:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 08:43 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 08:43 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 08:43 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 08:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 08:43 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 08:43 75-71-81.0 0.21 1
1,1-Dichloroethane 0.67J ug/L 02/24/14 08:43 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 08:43 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 08:43 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.35J ug/L 02/24/14 08:43 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 08:43 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 08:43 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 08:43 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 08:43 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-20 Lab ID:92190605008 Collected:02/20/14 17:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 08:43 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 08:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 08:43 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 08:43 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 08:43 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 08:43 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 08:43 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 08:43 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 08:43 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 08:43 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 08:43 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 08:43 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 08:43 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 08:43 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 08:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 08:43 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 08:43 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 08:43 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 08:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 08:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 08:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 08:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 08:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 08:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 08:43 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 08:43 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 08:43 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 08:43 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 08:43 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/24/14 08:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/24/14 08:43 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 08:43 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:02 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-20D Lab ID:92190605009 Collected:02/20/14 17:55 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:441
Collected Date 02/20/14 03/12/14 16:441
Collected Time 17:55 03/12/14 16:441
Field pH 6.6 Std. Units 03/12/14 16:440.10 0.10 1
Field Temperature 12.0 deg C 03/12/14 16:440.50 0.50 1
Field Specific Conductance 91 umhos/cm 03/12/14 16:441.0 1.0 1
Turbidity 55 NTU 03/12/14 16:441.0 1.0 1
Odor NONE 03/12/14 16:441
Appearance CLOUDY 03/12/14 16:441
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 19:58 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 19:58 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 19:58 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 19:58 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 19:58 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 19:58 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 19:58 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 19:58 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 19:58 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 19:58 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 19:58 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 19:58 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 19:58 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 19:58 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 19:58 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 19:58 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 19:58 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 19:58 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 19:58 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 19:58 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 19:58 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 19:58 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)65 %03/07/14 19:58 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)57 %03/07/14 19:58 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:00 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:00 7440-38-202/26/14 11:3510.0 5.0 1
Barium 109 ug/L 02/27/14 23:00 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:00 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:00 7440-43-902/26/14 11:351.0 1.0 1
Chromium 10.8 ug/L 02/27/14 23:00 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:00 7440-48-402/26/14 11:355.0 5.0 1
Copper 10.8 ug/L 02/27/14 23:00 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-20D Lab ID:92190605009 Collected:02/20/14 17:55 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:00 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:00 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:00 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:00 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:00 7440-28-002/26/14 11:355.4 5.4 1
Vanadium 15.8 ug/L 02/27/14 23:00 7440-62-202/26/14 11:355.0 5.0 1
Zinc 42.2 ug/L 02/27/14 23:00 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/25/14 15:50 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 08:59 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 08:59 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 08:59 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 08:59 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 08:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 08:59 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 08:59 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 08:59 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 08:59 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 08:59 78-93-35.0 0.96 1
Carbon disulfide 1.2J ug/L 02/24/14 08:59 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 08:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 08:59 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 08:59 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 08:59 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 08:59 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 08:59 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 08:59 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 08:59 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 08:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 08:59 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 08:59 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 08:59 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 08:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 08:59 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 08:59 75-71-81.0 0.21 1
1,1-Dichloroethane 1.1 ug/L 02/24/14 08:59 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 08:59 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 08:59 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.96J ug/L 02/24/14 08:59 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 08:59 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 08:59 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 08:59 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 08:59 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-20D Lab ID:92190605009 Collected:02/20/14 17:55 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 08:59 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 08:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 08:59 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 08:59 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 08:59 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 08:59 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 08:59 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 08:59 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 08:59 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 08:59 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 08:59 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 08:59 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 08:59 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 08:59 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 08:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 08:59 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 08:59 79-34-51.0 0.40 1
Tetrachloroethene 0.52J ug/L 02/24/14 08:59 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 08:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 08:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 08:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 08:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 08:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 08:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 08:59 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 08:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 08:59 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 08:59 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 08:59 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 08:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/24/14 08:59 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 08:59 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:04 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-21 Lab ID:92190605010 Collected:02/20/14 14:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:441
Collected Date 02/20/14 03/12/14 16:441
Collected Time 14:40 03/12/14 16:441
Field pH 5.4 Std. Units 03/12/14 16:440.10 0.10 1
Field Temperature 14.1 deg C 03/12/14 16:440.50 0.50 1
Field Specific Conductance 18 umhos/cm 03/12/14 16:441.0 1.0 1
Turbidity 100 NTU 03/12/14 16:441.0 1.0 1
Odor NONE 03/12/14 16:441
Appearance OPAQUE 03/12/14 16:441
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 20:16 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 20:16 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 20:16 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 20:16 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 20:16 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 20:16 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 20:16 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 20:16 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 20:16 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 20:16 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 20:16 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 20:16 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 20:16 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 20:16 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 20:16 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 20:16 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 20:16 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 20:16 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 20:16 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 20:16 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 20:16 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 20:16 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)67 %03/07/14 20:16 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)71 %03/07/14 20:16 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:03 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:03 7440-38-202/26/14 11:3510.0 5.0 1
Barium 122 ug/L 02/27/14 23:03 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:03 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:03 7440-43-902/26/14 11:351.0 1.0 1
Chromium 11.0 ug/L 02/27/14 23:03 7440-47-302/26/14 11:355.0 5.0 1
Cobalt 6.0 ug/L 02/27/14 23:03 7440-48-402/26/14 11:355.0 5.0 1
Copper 8.3 ug/L 02/27/14 23:03 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-21 Lab ID:92190605010 Collected:02/20/14 14:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:03 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:03 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:03 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:03 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:03 7440-28-002/26/14 11:355.4 5.4 1
Vanadium 16.5 ug/L 02/27/14 23:03 7440-62-202/26/14 11:355.0 5.0 1
Zinc 22.2 ug/L 02/27/14 23:03 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/25/14 15:52 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 09:14 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 09:14 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 09:14 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 09:14 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 09:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 09:14 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 09:14 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 09:14 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 09:14 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 09:14 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 09:14 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 09:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 09:14 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 09:14 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 09:14 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 09:14 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 09:14 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 09:14 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 09:14 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 09:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 09:14 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 09:14 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 09:14 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 09:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 09:14 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 09:14 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 09:14 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 09:14 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 09:14 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 09:14 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 09:14 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 09:14 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 09:14 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 09:14 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-21 Lab ID:92190605010 Collected:02/20/14 14:40 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 09:14 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 09:14 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 09:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 09:14 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 09:14 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 09:14 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 09:14 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 09:14 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 09:14 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 09:14 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 09:14 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 09:14 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 09:14 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 09:14 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 09:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 09:14 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 09:14 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 09:14 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 09:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 09:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 09:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 09:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 09:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 09:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 09:14 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 09:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 09:14 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 09:14 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 09:14 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 09:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/24/14 09:14 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 09:14 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:05 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-24 Lab ID:92190605011 Collected:02/20/14 15:00 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:461
Collected Date 02/20/14 03/12/14 16:461
Collected Time 13:00 03/12/14 16:461
Field pH 6.1 Std. Units 03/12/14 16:460.10 0.10 1
Field Temperature 12.5 deg C 03/12/14 16:460.50 0.50 1
Field Specific Conductance 55 umhos/cm 03/12/14 16:461.0 1.0 1
Turbidity 4.20 NTU 03/12/14 16:461.0 1.0 1
Odor NONE 03/12/14 16:461
Appearance CLEAR 03/12/14 16:461
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 20:33 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 20:33 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 20:33 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 20:33 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 20:33 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 20:33 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 20:33 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 20:33 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 20:33 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 20:33 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 20:33 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 20:33 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 20:33 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 20:33 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 20:33 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 20:33 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 20:33 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 20:33 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 20:33 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 20:33 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 20:33 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 20:33 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)70 %03/07/14 20:33 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)73 %03/07/14 20:33 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:06 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:06 7440-38-202/26/14 11:3510.0 5.0 1
Barium 42.8 ug/L 02/27/14 23:06 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:06 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:06 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:06 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:06 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:06 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-24 Lab ID:92190605011 Collected:02/20/14 15:00 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:06 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:06 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:06 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:06 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:06 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:06 7440-62-202/26/14 11:355.0 5.0 1
Zinc 13.8 ug/L 02/27/14 23:06 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/25/14 15:55 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 09:30 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 09:30 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 09:30 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 09:30 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 09:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 09:30 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 09:30 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 09:30 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 09:30 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 09:30 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 09:30 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 09:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 09:30 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 09:30 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 09:30 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 09:30 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 09:30 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 09:30 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 09:30 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 09:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 09:30 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 09:30 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 09:30 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 09:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 09:30 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 09:30 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 09:30 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 09:30 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 09:30 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 09:30 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 09:30 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 09:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 09:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 09:30 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:MW-24 Lab ID:92190605011 Collected:02/20/14 15:00 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/24/14 09:30 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 09:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/24/14 09:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 09:30 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 09:30 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 09:30 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 09:30 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 09:30 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 09:30 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 09:30 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 09:30 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 09:30 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 09:30 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 09:30 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 09:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 09:30 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 09:30 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 09:30 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 09:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 09:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 09:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 09:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 09:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 09:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 09:30 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 09:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 09:30 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 09:30 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 09:30 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/24/14 09:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/24/14 09:30 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 09:30 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:06 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:US-1 Lab ID:92190605012 Collected:02/20/14 14:15 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:461
Collected Date 02/20/14 03/12/14 16:461
Collected Time 14:15 03/12/14 16:461
Field pH 6.6 Std. Units 03/12/14 16:460.10 0.10 1
Field Temperature 12.2 deg C 03/12/14 16:460.50 0.50 1
Field Specific Conductance 68 umhos/cm 03/12/14 16:461.0 1.0 1
Turbidity 4.61 NTU 03/12/14 16:461.0 1.0 1
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 20:51 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 20:51 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 20:51 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 20:51 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 20:51 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 20:51 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 20:51 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 20:51 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 20:51 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 20:51 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 20:51 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 20:51 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 20:51 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 20:51 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 20:51 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 20:51 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 20:51 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 20:51 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 20:51 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 20:51 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 20:51 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 20:51 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)65 %03/07/14 20:51 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)71 %03/07/14 20:51 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:09 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:09 7440-38-202/26/14 11:3510.0 5.0 1
Barium 39.6 ug/L 02/27/14 23:09 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:09 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:09 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:09 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:09 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:09 7440-50-802/26/14 11:355.0 5.0 1
Lead ND ug/L 02/27/14 23:09 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:09 7440-02-002/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:US-1 Lab ID:92190605012 Collected:02/20/14 14:15 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Selenium ND ug/L 02/27/14 23:09 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:09 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:09 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:09 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:09 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:12 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 09:46 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 09:46 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 09:46 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 09:46 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 09:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 09:46 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 09:46 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 09:46 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 09:46 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 09:46 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 09:46 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 09:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 09:46 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 09:46 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 09:46 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 09:46 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 09:46 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 09:46 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 09:46 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 09:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 09:46 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 09:46 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 09:46 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 09:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 09:46 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 09:46 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 09:46 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 09:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 09:46 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 09:46 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 09:46 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 09:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 09:46 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 09:46 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 02/24/14 09:46 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 09:46 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:US-1 Lab ID:92190605012 Collected:02/20/14 14:15 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 02/24/14 09:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 09:46 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 09:46 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 09:46 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 09:46 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 09:46 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 09:46 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 09:46 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 09:46 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 09:46 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 09:46 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 09:46 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 09:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 09:46 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 09:46 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 09:46 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 09:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 09:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 09:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 09:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 09:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 09:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 09:46 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 09:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 09:46 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 09:46 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 09:46 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/24/14 09:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/24/14 09:46 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 09:46 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:07 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-1 Lab ID:92190605013 Collected:02/20/14 12:45 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:471
Collected Date 02/20/14 03/12/14 16:471
Collected Time 12:45 03/12/14 16:471
Field pH 7.1 Std. Units 03/12/14 16:470.10 0.10 1
Field Temperature 13.2 deg C 03/12/14 16:470.50 0.50 1
Field Specific Conductance 54 umhos/cm 03/12/14 16:471.0 1.0 1
Turbidity 3.41 NTU 03/12/14 16:471.0 1.0 1
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 21:08 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 21:08 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 21:08 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 21:08 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 21:08 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 21:08 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 21:08 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 21:08 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 21:08 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 21:08 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 21:08 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 21:08 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 21:08 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 21:08 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 21:08 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 21:08 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 21:08 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 21:08 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 21:08 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 21:08 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 21:08 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 21:08 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)66 %03/07/14 21:08 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)72 %03/07/14 21:08 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:12 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:12 7440-38-202/26/14 11:3510.0 5.0 1
Barium 40.6 ug/L 02/27/14 23:12 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:12 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:12 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:12 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:12 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:12 7440-50-802/26/14 11:355.0 5.0 1
Lead ND ug/L 02/27/14 23:12 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:12 7440-02-002/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-1 Lab ID:92190605013 Collected:02/20/14 12:45 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Selenium ND ug/L 02/27/14 23:12 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:12 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:12 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:12 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:12 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:20 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 10:01 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 10:01 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 10:01 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 10:01 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 10:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 10:01 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 10:01 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 10:01 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 10:01 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 10:01 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 10:01 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 10:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 10:01 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 10:01 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 10:01 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 10:01 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 10:01 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 10:01 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 10:01 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 10:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 10:01 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 10:01 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 10:01 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 10:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 10:01 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 10:01 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 10:01 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 10:01 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 10:01 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 10:01 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 10:01 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 10:01 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 10:01 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 10:01 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 02/24/14 10:01 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 10:01 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-1 Lab ID:92190605013 Collected:02/20/14 12:45 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 02/24/14 10:01 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 10:01 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 10:01 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 10:01 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 10:01 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 10:01 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 10:01 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 10:01 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 10:01 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 10:01 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 10:01 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 10:01 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 10:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 10:01 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 10:01 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 10:01 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 10:01 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 10:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 10:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 10:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 10:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 10:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 10:01 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 10:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 10:01 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 10:01 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 10:01 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 10:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/24/14 10:01 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 10:01 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:08 57-12-5 M10.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 45 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-2 Lab ID:92190605014 Collected:02/20/14 16:30 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:471
Collected Date 02/20/14 03/12/14 16:471
Collected Time 16:30 03/12/14 16:471
Field pH 7.3 Std. Units 03/12/14 16:470.10 0.10 1
Field Temperature 11.9 deg C 03/12/14 16:470.50 0.50 1
Field Specific Conductance 74 umhos/cm 03/12/14 16:471.0 1.0 1
Turbidity 4.38 NTU 03/12/14 16:471.0 1.0 1
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 21:26 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 21:26 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 21:26 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 21:26 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 21:26 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 21:26 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 21:26 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 21:26 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 21:26 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 21:26 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 21:26 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 21:26 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 21:26 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 21:26 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 21:26 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 21:26 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 21:26 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 21:26 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 21:26 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 21:26 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 21:26 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 21:26 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)60 %03/07/14 21:26 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)66 %03/07/14 21:26 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:16 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:16 7440-38-202/26/14 11:3510.0 5.0 1
Barium 43.8 ug/L 02/27/14 23:16 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:16 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:16 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:16 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:16 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:16 7440-50-802/26/14 11:355.0 5.0 1
Lead ND ug/L 02/27/14 23:16 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:16 7440-02-002/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 46 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-2 Lab ID:92190605014 Collected:02/20/14 16:30 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Selenium ND ug/L 02/27/14 23:16 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:16 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:16 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:16 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:16 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:22 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 10:17 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 10:17 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 10:17 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 10:17 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 10:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 10:17 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 10:17 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 10:17 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 10:17 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 10:17 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 10:17 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 10:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 10:17 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 10:17 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 10:17 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 10:17 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 10:17 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 10:17 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 10:17 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 10:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 10:17 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 10:17 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 10:17 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 10:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 10:17 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 10:17 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 10:17 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 10:17 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 10:17 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 10:17 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 10:17 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 10:17 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 10:17 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 10:17 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 02/24/14 10:17 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 10:17 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 47 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-2 Lab ID:92190605014 Collected:02/20/14 16:30 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 02/24/14 10:17 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 10:17 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 10:17 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 10:17 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 10:17 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 10:17 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 10:17 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 10:17 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 10:17 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 10:17 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 10:17 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 10:17 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 10:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 10:17 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 10:17 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 10:17 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 10:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 10:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 10:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 10:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 10:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 10:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 10:17 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 10:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 10:17 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 10:17 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 10:17 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)96 %02/24/14 10:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/24/14 10:17 17060-07-070-130 1
Toluene-d8 (S)96 %02/24/14 10:17 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:10 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 48 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-3 Lab ID:92190605015 Collected:02/20/14 18:30 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:481
Collected Date 02/20/14 03/12/14 16:481
Collected Time 18:30 03/12/14 16:481
Field pH 7.1 Std. Units 03/12/14 16:480.10 0.10 1
Field Temperature 12.3 deg C 03/12/14 16:480.50 0.50 1
Field Specific Conductance 80 umhos/cm 03/12/14 16:481.0 1.0 1
Turbidity 4.92 NTU 03/12/14 16:481.0 1.0 1
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 22:36 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 22:36 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 22:36 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 22:36 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 22:36 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 22:36 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 22:36 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 22:36 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 22:36 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 22:36 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 22:36 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 22:36 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 22:36 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 22:36 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 22:36 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 22:36 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 22:36 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 22:36 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 22:36 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 22:36 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 22:36 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 22:36 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)64 %03/07/14 22:36 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)64 %03/07/14 22:36 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:19 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:19 7440-38-202/26/14 11:3510.0 5.0 1
Barium 46.6 ug/L 02/27/14 23:19 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:19 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:19 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:19 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:19 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:19 7440-50-802/26/14 11:355.0 5.0 1
Lead ND ug/L 02/27/14 23:19 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:19 7440-02-002/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 49 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-3 Lab ID:92190605015 Collected:02/20/14 18:30 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Selenium ND ug/L 02/27/14 23:19 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:19 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:19 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:19 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:19 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:25 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/24/14 10:32 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/24/14 10:32 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/24/14 10:32 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/24/14 10:32 107-05-12.0 1.5 1
Benzene ND ug/L 02/24/14 10:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/24/14 10:32 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/24/14 10:32 75-27-41.0 0.18 1
Bromoform ND ug/L 02/24/14 10:32 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/24/14 10:32 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/24/14 10:32 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/24/14 10:32 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/24/14 10:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/24/14 10:32 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/24/14 10:32 75-00-31.0 0.54 1
Chloroform ND ug/L 02/24/14 10:32 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/24/14 10:32 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/24/14 10:32 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/14 10:32 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/24/14 10:32 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/14 10:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/24/14 10:32 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/24/14 10:32 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/24/14 10:32 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/24/14 10:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/24/14 10:32 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/24/14 10:32 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/24/14 10:32 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/24/14 10:32 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/24/14 10:32 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/24/14 10:32 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/24/14 10:32 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/24/14 10:32 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/24/14 10:32 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/24/14 10:32 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 02/24/14 10:32 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/24/14 10:32 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 50 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Sample:DS-3 Lab ID:92190605015 Collected:02/20/14 18:30 Received:02/21/14 09:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
trans-1,3-Dichloropropene ND ug/L 02/24/14 10:32 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/24/14 10:32 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/24/14 10:32 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/24/14 10:32 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/24/14 10:32 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/24/14 10:32 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/24/14 10:32 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/24/14 10:32 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/24/14 10:32 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/24/14 10:32 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/24/14 10:32 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/24/14 10:32 107-12-020.0 3.6 1
Styrene ND ug/L 02/24/14 10:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/14 10:32 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/14 10:32 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/24/14 10:32 127-18-41.0 0.46 1
Toluene ND ug/L 02/24/14 10:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/24/14 10:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/24/14 10:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/24/14 10:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/24/14 10:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/24/14 10:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/24/14 10:32 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/24/14 10:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/24/14 10:32 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/24/14 10:32 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/24/14 10:32 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %02/24/14 10:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/24/14 10:32 17060-07-070-130 1
Toluene-d8 (S)95 %02/24/14 10:32 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:11 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 51 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6212
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143175
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 02/24/14 18:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143176LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143177MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92188563001
1143178
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 103 75-12593 10 252.5ND 2.6 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 52 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6213
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92190605012, 92190605013, 92190605014, 92190605015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143179
Associated Lab Samples:92190605012, 92190605013, 92190605014, 92190605015
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 02/28/14 20:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143180LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 3.02.5 118 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143181MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605012
1143182
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 119 75-125119 0 252.5ND 3.0 3.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 53 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15293
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92190605001, 92190605002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143216
Associated Lab Samples:92190605001, 92190605002
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 02/24/14 21:46
Arsenic ug/L ND 10.0 02/24/14 21:46
Barium ug/L ND 5.0 02/24/14 21:46
Beryllium ug/L 0.12J 1.0 02/24/14 21:46
Cadmium ug/L ND 1.0 02/24/14 21:46
Chromium ug/L ND 5.0 02/24/14 21:46
Cobalt ug/L ND 5.0 02/24/14 21:46
Copper ug/L 0.30J 5.0 02/24/14 21:46
Lead ug/L ND 5.0 02/24/14 21:46
Nickel ug/L 1.8J 5.0 02/24/14 21:46
Selenium ug/L ND 10.0 02/24/14 21:46
Silver ug/L 0.58J 5.0 02/24/14 21:46
Thallium ug/L ND 5.4 02/24/14 21:46
Vanadium ug/L 0.28J 5.0 02/24/14 21:46
Zinc ug/L ND 10.0 02/24/14 21:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143217LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 497500 99 80-120
Arsenic ug/L 484500 97 80-120
Barium ug/L 500500 100 80-120
Beryllium ug/L 512500 102 80-120
Cadmium ug/L 509500 102 80-120
Chromium ug/L 530500 106 80-120
Cobalt ug/L 516500 103 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 500500 100 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 497500 99 80-120
Silver ug/L 248250 99 80-120
Thallium ug/L 492500 98 80-120
Vanadium ug/L 509500 102 80-120
Zinc ug/L 502500 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143218MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190532001
1143219
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-125100 2 25500ND496504
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 54 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143218MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190532001
1143219
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 97 75-12598 1 25500ND486492
Barium ug/L 500 98 75-12599 2 2550036.5 524 532
Beryllium ug/L 500 102 75-125103 1 25500ND508515
Cadmium ug/L 500 99 75-125101 1 25500ND496503
Chromium ug/L 500 104 75-125106 1 25500ND524531
Cobalt ug/L 500 101 75-125102 1 25500ND505511
Copper ug/L 500 98 75-125100 1 25500ND493500
Lead ug/L 500 97 75-12599 2 25500ND483493
Nickel ug/L 500 98 75-125100 2 2550036.9J 528 536
Selenium ug/L 500 97 75-125100 2 25500ND490501
Silver ug/L 250 97 75-12599 1 25250ND244247
Thallium ug/L 500 96 75-12596 1 25500ND483486
Vanadium ug/L 500 100 75-125102 1 25500ND502509
Zinc ug/L 500 98 75-125100 1 25500ND494501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 55 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15308
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92190605003, 92190605004, 92190605005, 92190605006, 92190605007, 92190605008, 92190605009,
92190605010, 92190605011, 92190605012, 92190605013, 92190605014, 92190605015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1145455
Associated Lab Samples:92190605003, 92190605004, 92190605005, 92190605006, 92190605007, 92190605008, 92190605009,
92190605010, 92190605011, 92190605012, 92190605013, 92190605014, 92190605015
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 02/27/14 22:15
Arsenic ug/L ND 10.0 02/27/14 22:15
Barium ug/L ND 5.0 02/27/14 22:15
Beryllium ug/L 0.19J 1.0 02/27/14 22:15
Cadmium ug/L ND 1.0 02/27/14 22:15
Chromium ug/L ND 5.0 02/27/14 22:15
Cobalt ug/L ND 5.0 02/27/14 22:15
Copper ug/L ND 5.0 02/27/14 22:15
Lead ug/L ND 5.0 02/27/14 22:15
Nickel ug/L ND 5.0 02/27/14 22:15
Selenium ug/L 3.5J 10.0 02/27/14 22:15
Silver ug/L 0.42J 5.0 02/27/14 22:15
Thallium ug/L ND 5.4 02/27/14 22:15
Vanadium ug/L 1.0J 5.0 02/27/14 22:15
Zinc ug/L ND 10.0 02/27/14 22:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1145456LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 473500 95 80-120
Barium ug/L 481500 96 80-120
Beryllium ug/L 476500 95 80-120
Cadmium ug/L 473500 95 80-120
Chromium ug/L 484500 97 80-120
Cobalt ug/L 475500 95 80-120
Copper ug/L 485500 97 80-120
Lead ug/L 470500 94 80-120
Nickel ug/L 473500 95 80-120
Selenium ug/L 472500 94 80-120
Silver ug/L 241250 96 80-120
Thallium ug/L 471500 94 80-120
Vanadium ug/L 495500 99 80-120
Zinc ug/L 464500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 56 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1145457MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605003
1145458
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-12599 0 25500ND496496
Arsenic ug/L 500 96 75-12595 1 25500ND480475
Barium ug/L 500 95 75-12594 1 2550013.0 487 484
Beryllium ug/L 500 94 75-12594 0 25500ND469469
Cadmium ug/L 500 93 75-12593 0 25500ND466467
Chromium ug/L 500 96 75-12596 0 25500ND483482
Cobalt ug/L 500 93 75-12593 0 25500ND468468
Copper ug/L 500 97 75-12596 1 25500ND485482
Lead ug/L 500 93 75-12592 1 25500ND465462
Nickel ug/L 500 93 75-12593 0 25500ND465465
Selenium ug/L 500 95 75-12595 1 25500ND479476
Silver ug/L 250 96 75-12596 0 25250ND241240
Thallium ug/L 500 91 75-12592 0 25500ND461463
Vanadium ug/L 500 99 75-12599 0 25500ND497495
Zinc ug/L 500 92 75-12593 0 25500ND464465
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 57 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25872
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011, 92190605012, 92190605013, 92190605014,
92190605015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143610
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011, 92190605012, 92190605013, 92190605014,
92190605015
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/24/14 01:42
1,1,1-Trichloroethane ug/L ND 1.0 02/24/14 01:42
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/24/14 01:42
1,1,2-Trichloroethane ug/L ND 1.0 02/24/14 01:42
1,1-Dichloroethane ug/L ND 1.0 02/24/14 01:42
1,1-Dichloroethene ug/L ND 1.0 02/24/14 01:42
1,1-Dichloropropene ug/L ND 1.0 02/24/14 01:42
1,2,3-Trichloropropane ug/L ND 1.0 02/24/14 01:42
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/24/14 01:42
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/24/14 01:42
1,2-Dichlorobenzene ug/L ND 1.0 02/24/14 01:42
1,2-Dichloroethane ug/L ND 1.0 02/24/14 01:42
1,2-Dichloropropane ug/L ND 1.0 02/24/14 01:42
1,3-Dichlorobenzene ug/L ND 1.0 02/24/14 01:42
1,3-Dichloropropane ug/L ND 1.0 02/24/14 01:42
1,4-Dichlorobenzene ug/L ND 1.0 02/24/14 01:42
2,2-Dichloropropane ug/L ND 1.0 02/24/14 01:42
2-Butanone (MEK)ug/L ND 5.0 02/24/14 01:42
2-Hexanone ug/L ND 5.0 02/24/14 01:42
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/24/14 01:42
Acetone ug/L ND 25.0 02/24/14 01:42
Acetonitrile ug/L ND 50.0 02/24/14 01:42
Acrylonitrile ug/L ND 10.0 02/24/14 01:42
Allyl chloride ug/L ND 2.0 02/24/14 01:42
Benzene ug/L ND 1.0 02/24/14 01:42
Bromochloromethane ug/L ND 1.0 02/24/14 01:42
Bromodichloromethane ug/L ND 1.0 02/24/14 01:42
Bromoform ug/L ND 1.0 02/24/14 01:42
Bromomethane ug/L ND 2.0 02/24/14 01:42
Carbon disulfide ug/L ND 2.0 02/24/14 01:42
Carbon tetrachloride ug/L ND 1.0 02/24/14 01:42
Chlorobenzene ug/L ND 1.0 02/24/14 01:42
Chloroethane ug/L ND 1.0 02/24/14 01:42
Chloroform ug/L ND 1.0 02/24/14 01:42
Chloromethane ug/L ND 1.0 02/24/14 01:42
Chloroprene ug/L ND 5.0 02/24/14 01:42
cis-1,2-Dichloroethene ug/L ND 1.0 02/24/14 01:42
cis-1,3-Dichloropropene ug/L ND 1.0 02/24/14 01:42
Dibromochloromethane ug/L ND 1.0 02/24/14 01:42
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 58 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143610
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011, 92190605012, 92190605013, 92190605014,
92190605015
Matrix:Water
Analyzed
Dibromomethane ug/L ND 1.0 02/24/14 01:42
Dichlorodifluoromethane ug/L ND 1.0 02/24/14 01:42
Ethyl methacrylate ug/L ND 1.0 02/24/14 01:42
Ethylbenzene ug/L ND 1.0 02/24/14 01:42
Iodomethane ug/L ND 5.0 02/24/14 01:42
Isobutanol ug/L ND 100 02/24/14 01:42
m&p-Xylene ug/L ND 2.0 02/24/14 01:42
Methacrylonitrile ug/L ND 10.0 02/24/14 01:42
Methyl methacrylate ug/L ND 2.0 02/24/14 01:42
Methylene Chloride ug/L ND 1.0 02/24/14 01:42
Naphthalene ug/L ND 1.0 02/24/14 01:42
o-Xylene ug/L ND 1.0 02/24/14 01:42
Propionitrile ug/L ND 20.0 02/24/14 01:42
Styrene ug/L ND 1.0 02/24/14 01:42
Tetrachloroethene ug/L ND 1.0 02/24/14 01:42
Toluene ug/L ND 1.0 02/24/14 01:42
trans-1,2-Dichloroethene ug/L ND 1.0 02/24/14 01:42
trans-1,3-Dichloropropene ug/L ND 1.0 02/24/14 01:42
trans-1,4-Dichloro-2-butene ug/L ND 1.0 02/24/14 01:42
Trichloroethene ug/L ND 1.0 02/24/14 01:42
Trichlorofluoromethane ug/L ND 1.0 02/24/14 01:42
Vinyl acetate ug/L ND 2.0 02/24/14 01:42
Vinyl chloride ug/L ND 1.0 02/24/14 01:42
Xylene (Total)ug/L ND 2.0 02/24/14 01:42
1,2-Dichloroethane-d4 (S)%99 70-130 02/24/14 01:42
4-Bromofluorobenzene (S)%99 70-130 02/24/14 01:42
Toluene-d8 (S)%96 70-130 02/24/14 01:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143611LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.050 102 70-130
1,1,1-Trichloroethane ug/L 45.650 91 70-130
1,1,2,2-Tetrachloroethane ug/L 50.350 101 70-130
1,1,2-Trichloroethane ug/L 49.350 99 70-130
1,1-Dichloroethane ug/L 43.050 86 70-130
1,1-Dichloroethene ug/L 41.250 82 70-132
1,1-Dichloropropene ug/L 44.550 89 70-130
1,2,3-Trichloropropane ug/L 50.050 100 70-130
1,2-Dibromo-3-chloropropane ug/L 54.750 109 70-130
1,2-Dibromoethane (EDB)ug/L 50.650 101 70-130
1,2-Dichlorobenzene ug/L 52.150 104 70-130
1,2-Dichloroethane ug/L 44.750 89 70-130
1,2-Dichloropropane ug/L 46.750 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 59 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143611LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 50.250 100 70-130
1,3-Dichloropropane ug/L 50.950 102 70-130
1,4-Dichlorobenzene ug/L 50.950 102 70-130
2,2-Dichloropropane ug/L 41.350 83 58-145
2-Butanone (MEK)ug/L 88.9100 89 70-145
2-Hexanone ug/L 99.9100 100 70-144
4-Methyl-2-pentanone (MIBK)ug/L 97.3100 97 70-140
Acetone ug/L 84.8100 85 50-175
Acetonitrile ug/L 415500 83 70-130
Acrylonitrile ug/L 210250 84 70-143
Allyl chloride ug/L 39.850 80 70-130
Benzene ug/L 48.550 97 70-130
Bromochloromethane ug/L 44.250 88 70-130
Bromodichloromethane ug/L 49.050 98 70-130
Bromoform ug/L 51.950 104 70-130
Bromomethane ug/L 47.050 94 54-130
Carbon disulfide ug/L 41.950 84 70-131
Carbon tetrachloride ug/L 51.750 103 70-132
Chlorobenzene ug/L 49.750 99 70-130
Chloroethane ug/L 40.450 81 64-134
Chloroform ug/L 44.450 89 70-130
Chloromethane ug/L 40.450 81 64-130
Chloroprene ug/L 45.950 92 70-130
cis-1,2-Dichloroethene ug/L 41.850 84 70-131
cis-1,3-Dichloropropene ug/L 46.450 93 70-130
Dibromochloromethane ug/L 52.150 104 70-130
Dibromomethane ug/L 49.150 98 70-131
Dichlorodifluoromethane ug/L 42.950 86 56-130
Ethyl methacrylate ug/L 50.250 100 70-130
Ethylbenzene ug/L 49.950 100 70-130
Iodomethane ug/L 84.0100 84 49-180
Isobutanol ug/L 8611000 86 70-130
m&p-Xylene ug/L 103100 103 70-130
Methacrylonitrile ug/L 445500 89 70-130
Methyl methacrylate ug/L 48.450 97 70-130
Methylene Chloride ug/L 41.150 82 63-130
Naphthalene ug/L 54.250 108 70-138
o-Xylene ug/L 50.750 101 70-130
Propionitrile ug/L 437500 87 70-130
Styrene ug/L 51.550 103 70-130
Tetrachloroethene ug/L 51.350 103 70-130
Toluene ug/L 48.150 96 70-130
trans-1,2-Dichloroethene ug/L 41.250 82 70-130
trans-1,3-Dichloropropene ug/L 48.350 97 70-132
trans-1,4-Dichloro-2-butene ug/L 53.750 107 70-141
Trichloroethene ug/L 47.650 95 70-130
Trichlorofluoromethane ug/L 45.050 90 62-133
Vinyl acetate ug/L 84.1100 84 66-157
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 60 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143611LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl chloride ug/L 43.850 88 69-130
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143612MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605015
1143613
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 92 70-16689 3 3050ND46.0 44.7
Benzene ug/L 50 103 70-148101 2 3050ND51.3 50.3
Chlorobenzene ug/L 50 105 70-146105 0 3050ND52.7 52.7
Toluene ug/L 50 99 70-15597 2 3050ND49.3 48.3
Trichloroethene ug/L 50 108 69-151106 1 3050ND53.9 53.1
1,2-Dichloroethane-d4 (S)%101 70-130102
4-Bromofluorobenzene (S)%96 70-13098
Toluene-d8 (S)%96 70-13095
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 61 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26098
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011, 92190605012, 92190605013, 92190605014,
92190605015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1144739
Associated Lab Samples:92190605001, 92190605002, 92190605003, 92190605004, 92190605005, 92190605006, 92190605007,
92190605008, 92190605009, 92190605010, 92190605011, 92190605012, 92190605013, 92190605014,
92190605015
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 03/07/14 16:28
4,4'-DDE ug/L ND 0.050 03/07/14 16:28
4,4'-DDT ug/L ND 0.050 03/07/14 16:28
Aldrin ug/L ND 0.050 03/07/14 16:28
alpha-BHC ug/L ND 0.050 03/07/14 16:28
beta-BHC ug/L ND 0.050 03/07/14 16:28
Chlordane (Technical)ug/L ND 0.20 03/07/14 16:28
delta-BHC ug/L ND 0.050 03/07/14 16:28
Dieldrin ug/L ND 0.050 03/07/14 16:28
Endosulfan I ug/L ND 0.050 03/07/14 16:28
Endosulfan II ug/L ND 0.050 03/07/14 16:28
Endosulfan sulfate ug/L ND 0.050 03/07/14 16:28
Endrin ug/L ND 0.050 03/07/14 16:28
Endrin aldehyde ug/L ND 0.050 03/07/14 16:28
Endrin ketone ug/L ND 0.050 03/07/14 16:28
gamma-BHC (Lindane)ug/L ND 0.050 03/07/14 16:28
Heptachlor ug/L ND 0.050 03/07/14 16:28
Heptachlor epoxide ug/L ND 0.050 03/07/14 16:28
Hexachlorobenzene ug/L ND 0.050 03/07/14 16:28
Methoxychlor ug/L ND 0.15 03/07/14 16:28
Mirex ug/L ND 0.15 03/07/14 16:28
Toxaphene ug/L ND 0.20 03/07/14 16:28
Decachlorobiphenyl (S)%75 20-130 03/07/14 16:28
Tetrachloro-m-xylene (S)%74 20-130 03/07/14 16:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144740LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.19.25 79 20-150
4,4'-DDE ug/L 0.18.25 72 20-150
4,4'-DDT ug/L 0.19.25 77 20-150
Aldrin ug/L 0.12.25 50 20-150
alpha-BHC ug/L 0.19.25 76 20-150
beta-BHC ug/L 0.20.25 79 20-150
delta-BHC ug/L 0.20.25 81 20-150
Dieldrin ug/L 0.18.25 74 20-150
Endosulfan I ug/L 0.20.25 80 20-150
Endosulfan II ug/L 0.20.25 80 20-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 62 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144740LABORATORY CONTROL SAMPLE:
LCSSpike
Endosulfan sulfate ug/L 0.21.25 83 20-150
Endrin ug/L 0.22.25 88 20-150
Endrin aldehyde ug/L 0.19.25 76 20-150
Endrin ketone ug/L 0.21.25 84 20-150
gamma-BHC (Lindane)ug/L 0.19.25 76 20-150
Heptachlor ug/L 0.14.25 55 20-150
Heptachlor epoxide ug/L 0.20.25 81 20-150
Hexachlorobenzene ug/L 0.16.25 66 20-150
Methoxychlor ug/L 0.59.74 80 20-150
Mirex ug/L 0.61.74 82 20-150
Decachlorobiphenyl (S)%80 20-130
Tetrachloro-m-xylene (S)%77 20-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1144741MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605005
1144742
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4,4'-DDD ug/L .25 55 20-15074 29 30.25ND 0.14 0.18
4,4'-DDE ug/L .25 65 20-15077 17 30.25ND 0.16 0.19
4,4'-DDT ug/L .25 68 20-15084 22 30.25ND 0.17 0.21
Aldrin ug/L .25 49 20-15063 27 30.25ND 0.12 0.16
alpha-BHC ug/L .25 79 20-15076 4 30.25ND 0.20 0.19
beta-BHC ug/L .25 80 20-15077 4 30.25ND 0.20 0.19
delta-BHC ug/L .25 83 20-15081 3 30.25ND 0.21 0.20
Dieldrin ug/L .25 47 20-15063 28 30.25ND 0.12 0.16
Endosulfan I ug/L .25 57 20-15069 20 30.25ND 0.14 0.17
Endosulfan II ug/L .25 48 20-15062 25 30.25ND 0.12 0.15
Endosulfan sulfate ug/L .25 57 20-15069 18 30.25ND 0.14 0.17
Endrin ug/L .25 62 20-15079 24 30.25ND 0.15 0.20
Endrin aldehyde ug/L .25 74 20-15076 3 30.25ND 0.18 0.19
Endrin ketone ug/L .25 70 20-15077 10 30.25ND 0.17 0.19
gamma-BHC (Lindane)ug/L .25 79 20-15076 4 30.25ND 0.20 0.19
Heptachlor ug/L .25 47 20-15063 28 30.25ND 0.12 0.15
Heptachlor epoxide ug/L .25 62 20-15071 14 30.25ND 0.15 0.18
Hexachlorobenzene ug/L .25 57 20-15062 9 30.25ND 0.14 0.15
Methoxychlor ug/L .74 59 20-15074 22 30.74ND 0.44 0.55
Mirex ug/L .74 81 20-15080 0 30.74ND 0.60 0.60
Decachlorobiphenyl (S)%63 20-13061
Tetrachloro-m-xylene (S)%79 20-13080
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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Page 63 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/18216
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92190605001, 92190605002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148505
Associated Lab Samples:92190605001, 92190605002
Matrix:Water
Analyzed
Cyanide mg/L ND 0.0050 03/02/14 12:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148506LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.10.1 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148507MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190408004
1148508
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 122 75-125120 2 20.1ND 0.12 0.12
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148509MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190666002
1148510
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L M1,R1.1 62 75-12517 116 20.1ND 0.062 0.017
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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Page 64 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/18217
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92190605003, 92190605004, 92190605005, 92190605006, 92190605007, 92190605008, 92190605009,
92190605010, 92190605011, 92190605012, 92190605013, 92190605014, 92190605015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148511
Associated Lab Samples:92190605003, 92190605004, 92190605005, 92190605006, 92190605007, 92190605008, 92190605009,
92190605010, 92190605011, 92190605012, 92190605013, 92190605014, 92190605015
Matrix:Water
Analyzed
Cyanide mg/L ND 0.0050 03/02/14 12:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148512LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.10.1 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148513MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605003
1148514
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L M1.1 127 75-125127 0 20.1ND 0.13 0.13
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148515MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605013
1148516
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L M1.1 126 75-125125 1 20.1ND 0.13 0.13
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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Page 65 of 71
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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[phone]
Page 66 of 71
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190605001 FLD/MW-6
92190605002 FLD/MW-7
92190605003 FLD/MW-8
92190605004 FLD/MW-9
92190605005 FLD/MW-10
92190605006 FLD/MW-19
92190605007 FLD/MW-19D
92190605008 FLD/MW-20
92190605009 FLD/MW-20D
92190605010 FLD/MW-21
92190605011 FLD/MW-24
92190605012 FLD/US-1
92190605013 FLD/DS-1
92190605014 FLD/DS-2
92190605015 FLD/DS-3
92190605001 OEXT/26098 GCSV/16861MW-6 EPA 3510 EPA 8081
92190605002 OEXT/26098 GCSV/16861MW-7 EPA 3510 EPA 8081
92190605003 OEXT/26098 GCSV/16861MW-8 EPA 3510 EPA 8081
92190605004 OEXT/26098 GCSV/16861MW-9 EPA 3510 EPA 8081
92190605005 OEXT/26098 GCSV/16861MW-10 EPA 3510 EPA 8081
92190605006 OEXT/26098 GCSV/16861MW-19 EPA 3510 EPA 8081
92190605007 OEXT/26098 GCSV/16861MW-19D EPA 3510 EPA 8081
92190605008 OEXT/26098 GCSV/16861MW-20 EPA 3510 EPA 8081
92190605009 OEXT/26098 GCSV/16861MW-20D EPA 3510 EPA 8081
92190605010 OEXT/26098 GCSV/16861MW-21 EPA 3510 EPA 8081
92190605011 OEXT/26098 GCSV/16861MW-24 EPA 3510 EPA 8081
92190605012 OEXT/26098 GCSV/16861US-1 EPA 3510 EPA 8081
92190605013 OEXT/26098 GCSV/16861DS-1 EPA 3510 EPA 8081
92190605014 OEXT/26098 GCSV/16861DS-2 EPA 3510 EPA 8081
92190605015 OEXT/26098 GCSV/16861DS-3 EPA 3510 EPA 8081
92190605001 MPRP/15293 ICP/13873MW-6 EPA 3010 EPA 6010
92190605002 MPRP/15293 ICP/13873MW-7 EPA 3010 EPA 6010
92190605003 MPRP/15308 ICP/13890MW-8 EPA 3010 EPA 6010
92190605004 MPRP/15308 ICP/13890MW-9 EPA 3010 EPA 6010
92190605005 MPRP/15308 ICP/13890MW-10 EPA 3010 EPA 6010
92190605006 MPRP/15308 ICP/13890MW-19 EPA 3010 EPA 6010
92190605007 MPRP/15308 ICP/13890MW-19D EPA 3010 EPA 6010
92190605008 MPRP/15308 ICP/13890MW-20 EPA 3010 EPA 6010
92190605009 MPRP/15308 ICP/13890MW-20D EPA 3010 EPA 6010
92190605010 MPRP/15308 ICP/13890MW-21 EPA 3010 EPA 6010
92190605011 MPRP/15308 ICP/13890MW-24 EPA 3010 EPA 6010
92190605012 MPRP/15308 ICP/13890US-1 EPA 3010 EPA 6010
92190605013 MPRP/15308 ICP/13890DS-1 EPA 3010 EPA 6010
92190605014 MPRP/15308 ICP/13890DS-2 EPA 3010 EPA 6010
92190605015 MPRP/15308 ICP/13890DS-3 EPA 3010 EPA 6010
92190605001 MERP/6212 MERC/5994MW-6 EPA 7470 EPA 7470
92190605002 MERP/6212 MERC/5994MW-7 EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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Asheville, NC 28804
[phone]
Page 67 of 71
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190605
Haywood FFLF MWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190605003 MERP/6212 MERC/5994MW-8 EPA 7470 EPA 7470
92190605004 MERP/6212 MERC/5994MW-9 EPA 7470 EPA 7470
92190605005 MERP/6212 MERC/5994MW-10 EPA 7470 EPA 7470
92190605006 MERP/6212 MERC/5994MW-19 EPA 7470 EPA 7470
92190605007 MERP/6212 MERC/5994MW-19D EPA 7470 EPA 7470
92190605008 MERP/6212 MERC/5994MW-20 EPA 7470 EPA 7470
92190605009 MERP/6212 MERC/5994MW-20D EPA 7470 EPA 7470
92190605010 MERP/6212 MERC/5994MW-21 EPA 7470 EPA 7470
92190605011 MERP/6212 MERC/5994MW-24 EPA 7470 EPA 7470
92190605012 MERP/6213 MERC/5995US-1 EPA 7470 EPA 7470
92190605013 MERP/6213 MERC/5995DS-1 EPA 7470 EPA 7470
92190605014 MERP/6213 MERC/5995DS-2 EPA 7470 EPA 7470
92190605015 MERP/6213 MERC/5995DS-3 EPA 7470 EPA 7470
92190605001 MSV/25872MW-6 EPA 8260
92190605002 MSV/25872MW-7 EPA 8260
92190605003 MSV/25872MW-8 EPA 8260
92190605004 MSV/25872MW-9 EPA 8260
92190605005 MSV/25872MW-10 EPA 8260
92190605006 MSV/25872MW-19 EPA 8260
92190605007 MSV/25872MW-19D EPA 8260
92190605008 MSV/25872MW-20 EPA 8260
92190605009 MSV/25872MW-20D EPA 8260
92190605010 MSV/25872MW-21 EPA 8260
92190605011 MSV/25872MW-24 EPA 8260
92190605012 MSV/25872US-1 EPA 8260
92190605013 MSV/25872DS-1 EPA 8260
92190605014 MSV/25872DS-2 EPA 8260
92190605015 MSV/25872DS-3 EPA 8260
92190605001 WETA/18216MW-6 SM 4500-CN-E
92190605002 WETA/18216MW-7 SM 4500-CN-E
92190605003 WETA/18217MW-8 SM 4500-CN-E
92190605004 WETA/18217MW-9 SM 4500-CN-E
92190605005 WETA/18217MW-10 SM 4500-CN-E
92190605006 WETA/18217MW-19 SM 4500-CN-E
92190605007 WETA/18217MW-19D SM 4500-CN-E
92190605008 WETA/18217MW-20 SM 4500-CN-E
92190605009 WETA/18217MW-20D SM 4500-CN-E
92190605010 WETA/18217MW-21 SM 4500-CN-E
92190605011 WETA/18217MW-24 SM 4500-CN-E
92190605012 WETA/18217US-1 SM 4500-CN-E
92190605013 WETA/18217DS-1 SM 4500-CN-E
92190605014 WETA/18217DS-2 SM 4500-CN-E
92190605015 WETA/18217DS-3 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:44 PM
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[phone]
Page 68 of 71
Page 69 of 71
Page 70 of 71
Page 71 of 71
#=CL#
March 19, 2014
LIMS USE: FR - STEPHEN KING
LIMS OBJECT ID: 92190677
92190677
Project:
Pace Project No.:
RE:
Mr. Stephen King
Haywood Co. Solid Waste
278 Recycle Rd.
Clyde, NC 28721
FRANCIS FARM LF
Dear Mr. King:
Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
cc:Andy Alexander, BLE
Mr. Stephen King, Haywood Co. Solid Waste
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 34
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Lab ID Sample ID Matrix Date Collected Date Received
92190677001 MW-1A Water 02/21/14 14:40 02/21/14 16:05
92190677002 MW-4 Water 02/21/14 15:00 02/21/14 16:05
92190677003 MW-18 Water 02/21/14 14:15 02/21/14 16:05
92190677004 MW-23 Water 02/21/14 11:55 02/21/14 16:05
92190677005 MW-23D Water 02/21/14 12:10 02/21/14 16:05
REPORT OF LABORATORY ANALYSIS
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Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92190677001 MW-1A EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190677002 MW-4 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190677003 MW-18 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190677004 MW-23 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92190677005 MW-23D EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-1A Lab ID:92190677001 Collected:02/21/14 14:40 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:031
Collected Date 02/21/14 03/12/14 16:031
Collected Time 14:40 03/12/14 16:031
Field pH 6.2 Std. Units 03/12/14 16:030.10 0.10 1
Field Temperature 14.1 deg C 03/12/14 16:030.50 0.50 1
Field Specific Conductance 485 umhos/cm 03/12/14 16:031.0 1.0 1
Turbidity 3.36 NTU 03/12/14 16:031.0 1.0 1
Odor O&G 03/12/14 16:031
Appearance CLEAR 03/12/14 16:031
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 22:53 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 22:53 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 22:53 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 22:53 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 22:53 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 22:53 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 22:53 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 22:53 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 22:53 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 22:53 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 22:53 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 22:53 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 22:53 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 22:53 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 22:53 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 22:53 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 22:53 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 22:53 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 22:53 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 22:53 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 22:53 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 22:53 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)44 %03/07/14 22:53 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)92 %03/07/14 22:53 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:22 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:22 7440-38-202/26/14 11:3510.0 5.0 1
Barium 215 ug/L 02/27/14 23:22 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:22 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:22 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:22 7440-47-302/26/14 11:355.0 5.0 1
Cobalt 18.3 ug/L 02/27/14 23:22 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:22 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-1A Lab ID:92190677001 Collected:02/21/14 14:40 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:22 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:22 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:22 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:22 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:22 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:22 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:22 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:28 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 23:08 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 23:08 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 23:08 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 23:08 107-05-12.0 1.5 1
Benzene 0.36J ug/L 02/28/14 23:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 23:08 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 23:08 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 23:08 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 23:08 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 23:08 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 23:08 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 23:08 56-23-51.0 0.25 1
Chlorobenzene 2.5 ug/L 02/28/14 23:08 108-90-71.0 0.23 1
Chloroethane 1.2 ug/L 02/28/14 23:08 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 23:08 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 23:08 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 23:08 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 23:08 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 23:08 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 23:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 23:08 74-95-31.0 0.21 1
1,2-Dichlorobenzene 1.0J ug/L 02/28/14 23:08 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 23:08 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.49J ug/L 02/28/14 23:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 23:08 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 23:08 75-71-81.0 0.21 1
1,1-Dichloroethane 1.2 ug/L 02/28/14 23:08 75-34-31.0 0.32 1
1,2-Dichloroethane 0.99J ug/L 02/28/14 23:08 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 23:08 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.67J ug/L 02/28/14 23:08 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 23:08 156-60-51.0 0.49 1
1,2-Dichloropropane 0.31J ug/L 02/28/14 23:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 23:08 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 23:08 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-1A Lab ID:92190677001 Collected:02/21/14 14:40 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 23:08 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 23:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 23:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 23:08 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 23:08 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 23:08 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 23:08 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 23:08 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 23:08 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 23:08 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 23:08 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 23:08 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 23:08 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 23:08 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 23:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 23:08 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 23:08 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 23:08 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 23:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 23:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 23:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 23:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 23:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 23:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 23:08 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 23:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 23:08 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 23:08 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 23:08 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %02/28/14 23:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 23:08 17060-07-070-130 1
Toluene-d8 (S)100 %02/28/14 23:08 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:20 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-4 Lab ID:92190677002 Collected:02/21/14 15:00 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:051
Collected Date 02/21/14 03/12/14 16:051
Collected Time 15:00 03/12/14 16:051
Field pH 5.5 Std. Units 03/12/14 16:050.10 0.10 1
Field Temperature 13.6 deg C 03/12/14 16:050.50 0.50 1
Field Specific Conductance 222 umhos/cm 03/12/14 16:051.0 1.0 1
Turbidity 3.69 NTU 03/12/14 16:051.0 1.0 1
Odor O&G 03/12/14 16:051
Appearance CLEAR 03/12/14 16:051
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 23:11 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 23:11 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 23:11 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 23:11 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)0.13 ug/L 03/07/14 23:11 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 23:11 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 23:11 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 23:11 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 23:11 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 23:11 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 23:11 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 23:11 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 23:11 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 23:11 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 23:11 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 23:11 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 23:11 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 23:11 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 23:11 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 23:11 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 23:11 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 23:11 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)46 %03/07/14 23:11 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)52 %03/07/14 23:11 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:36 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:36 7440-38-202/26/14 11:3510.0 5.0 1
Barium 149 ug/L 02/27/14 23:36 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:36 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:36 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:36 7440-47-302/26/14 11:355.0 5.0 1
Cobalt 8.5 ug/L 02/27/14 23:36 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:36 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-4 Lab ID:92190677002 Collected:02/21/14 15:00 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:36 7439-92-102/26/14 11:355.0 5.0 1
Nickel 8.1 ug/L 02/27/14 23:36 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:36 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:36 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:36 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:36 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:36 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/27/14 17:48 7439-97-602/24/14 20:000.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 23:23 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 23:23 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 23:23 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 23:23 107-05-12.0 1.5 1
Benzene 16.5 ug/L 02/28/14 23:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 23:23 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 23:23 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 23:23 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 23:23 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 23:23 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 23:23 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 23:23 56-23-51.0 0.25 1
Chlorobenzene 0.61J ug/L 02/28/14 23:23 108-90-71.0 0.23 1
Chloroethane 0.78J ug/L 02/28/14 23:23 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 23:23 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 23:23 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 23:23 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 23:23 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 23:23 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 23:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 23:23 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 23:23 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 23:23 541-73-11.0 0.24 1
1,4-Dichlorobenzene 6.1 ug/L 02/28/14 23:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 23:23 110-57-61.0 1.0 1
Dichlorodifluoromethane 0.58J ug/L 02/28/14 23:23 75-71-81.0 0.21 1
1,1-Dichloroethane 21.2 ug/L 02/28/14 23:23 75-34-31.0 0.32 1
1,2-Dichloroethane 1.7 ug/L 02/28/14 23:23 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 23:23 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 27.6 ug/L 02/28/14 23:23 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 23:23 156-60-51.0 0.49 1
1,2-Dichloropropane 0.48J ug/L 02/28/14 23:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 23:23 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 23:23 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-4 Lab ID:92190677002 Collected:02/21/14 15:00 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 23:23 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 23:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 23:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 23:23 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 23:23 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 23:23 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 23:23 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 23:23 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 23:23 126-98-710.0 0.93 1
Methylene Chloride 34.1 ug/L 02/28/14 23:23 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 23:23 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 23:23 108-10-15.0 0.33 1
Naphthalene 6.5 ug/L 02/28/14 23:23 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 23:23 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 23:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 23:23 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 23:23 79-34-51.0 0.40 1
Tetrachloroethene 6.0 ug/L 02/28/14 23:23 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 23:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 23:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 23:23 79-00-51.0 0.29 1
Trichloroethene 6.0 ug/L 02/28/14 23:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 23:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 23:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 23:23 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 23:23 75-01-41.0 0.62 1
Xylene (Total)6.3 ug/L 02/28/14 23:23 1330-20-72.0 0.66 1
m&p-Xylene 4.6 ug/L 02/28/14 23:23 179601-23-12.0 0.66 1
o-Xylene 1.8 ug/L 02/28/14 23:23 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %02/28/14 23:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 23:23 17060-07-070-130 1
Toluene-d8 (S)99 %02/28/14 23:23 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:21 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-18 Lab ID:92190677003 Collected:02/21/14 14:15 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:061
Collected Date 02/21/14 03/12/14 16:061
Collected Time 14:15 03/12/14 16:061
Field pH 5.9 Std. Units 03/12/14 16:060.10 0.10 1
Field Temperature 14.0 deg C 03/12/14 16:060.50 0.50 1
Field Specific Conductance 60 umhos/cm 03/12/14 16:061.0 1.0 1
Turbidity 6.54 NTU 03/12/14 16:061.0 1.0 1
Odor NONE 03/12/14 16:061
Appearance CLEAR 03/12/14 16:061
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 23:28 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 23:28 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 23:28 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 23:28 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 23:28 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 23:28 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 23:28 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 23:28 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 23:28 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 23:28 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 23:28 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 23:28 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 23:28 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 23:28 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 23:28 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 23:28 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 23:28 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 23:28 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 23:28 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 23:28 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 23:28 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 23:28 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)60 %03/07/14 23:28 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)58 %03/07/14 23:28 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:40 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:40 7440-38-202/26/14 11:3510.0 5.0 1
Barium 80.1 ug/L 02/27/14 23:40 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:40 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:40 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:40 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:40 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:40 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-18 Lab ID:92190677003 Collected:02/21/14 14:15 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:40 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:40 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:40 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:40 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:40 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:40 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:40 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:30 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 23:39 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 23:39 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 23:39 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 23:39 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 23:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 23:39 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 23:39 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 23:39 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 23:39 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 23:39 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 23:39 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 23:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 23:39 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 23:39 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 23:39 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 23:39 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 23:39 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 23:39 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 23:39 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 23:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 23:39 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 23:39 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 23:39 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 23:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 23:39 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 23:39 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 23:39 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 23:39 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 23:39 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 23:39 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 23:39 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 23:39 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 23:39 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 23:39 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-18 Lab ID:92190677003 Collected:02/21/14 14:15 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 23:39 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 23:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 23:39 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 23:39 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 23:39 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 23:39 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 23:39 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 23:39 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 23:39 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 23:39 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 23:39 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 23:39 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 23:39 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 23:39 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 23:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 23:39 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 23:39 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 23:39 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 23:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 23:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 23:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 23:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 23:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 23:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 23:39 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 23:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 23:39 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 23:39 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 23:39 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 23:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 23:39 17060-07-070-130 1
Toluene-d8 (S)99 %02/28/14 23:39 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:22 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-23 Lab ID:92190677004 Collected:02/21/14 11:55 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:081
Collected Date 02/21/14 03/12/14 16:081
Collected Time 11:55 03/12/14 16:081
Field pH 5.8 Std. Units 03/12/14 16:080.10 0.10 1
Field Temperature 11.0 deg C 03/12/14 16:080.50 0.50 1
Field Specific Conductance 87 umhos/cm 03/12/14 16:081.0 1.0 1
Turbidity 2.28 NTU 03/12/14 16:081.0 1.0 1
Odor NONE 03/12/14 16:081
Appearance CLEAR 03/12/14 16:081
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/07/14 23:46 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/07/14 23:46 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/07/14 23:46 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/07/14 23:46 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/07/14 23:46 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/07/14 23:46 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/07/14 23:46 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/07/14 23:46 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/07/14 23:46 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/07/14 23:46 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/07/14 23:46 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/07/14 23:46 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/07/14 23:46 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/07/14 23:46 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/07/14 23:46 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/07/14 23:46 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/07/14 23:46 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/07/14 23:46 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/07/14 23:46 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/07/14 23:46 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/07/14 23:46 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/07/14 23:46 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)68 %03/07/14 23:46 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)69 %03/07/14 23:46 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:43 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:43 7440-38-202/26/14 11:3510.0 5.0 1
Barium 86.9 ug/L 02/27/14 23:43 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:43 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:43 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:43 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:43 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:43 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-23 Lab ID:92190677004 Collected:02/21/14 11:55 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:43 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:43 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:43 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:43 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:43 7440-28-002/26/14 11:355.4 5.4 1
Vanadium 5.3 ug/L 02/27/14 23:43 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:43 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:38 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 23:55 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 23:55 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 23:55 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 23:55 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 23:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 23:55 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 23:55 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 23:55 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 23:55 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 23:55 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 23:55 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 23:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 23:55 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 23:55 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 23:55 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 23:55 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 23:55 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 23:55 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 23:55 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 23:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 23:55 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 23:55 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 23:55 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 23:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 23:55 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 23:55 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 23:55 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 23:55 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 23:55 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 23:55 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 23:55 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 23:55 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 23:55 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 23:55 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-23 Lab ID:92190677004 Collected:02/21/14 11:55 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 23:55 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 23:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 23:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 23:55 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 23:55 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 23:55 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 23:55 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 23:55 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 23:55 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 23:55 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 23:55 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 23:55 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 23:55 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 23:55 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 23:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 23:55 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 23:55 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 23:55 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 23:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 23:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 23:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 23:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 23:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 23:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 23:55 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 23:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 23:55 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 23:55 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 23:55 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/28/14 23:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/28/14 23:55 17060-07-070-130 1
Toluene-d8 (S)99 %02/28/14 23:55 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:23 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
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Page 16 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-23D Lab ID:92190677005 Collected:02/21/14 12:10 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:091
Collected Date 02/21/14 03/12/14 16:091
Collected Time 12:10 03/12/14 16:091
Field pH 6.8 Std. Units 03/12/14 16:090.10 0.10 1
Field Temperature 10.3 deg C 03/12/14 16:090.50 0.50 1
Field Specific Conductance 124 umhos/cm 03/12/14 16:091.0 1.0 1
Turbidity 206 NTU 03/12/14 16:091.0 1.0 1
Odor NONE 03/12/14 16:091
Appearance CLEAR 03/12/14 16:091
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/08/14 00:03 309-00-202/25/14 14:300.050 0.050 1
alpha-BHC ND ug/L 03/08/14 00:03 319-84-602/25/14 14:300.050 0.050 1
beta-BHC ND ug/L 03/08/14 00:03 319-85-702/25/14 14:300.050 0.050 1
delta-BHC ND ug/L 03/08/14 00:03 319-86-802/25/14 14:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/08/14 00:03 58-89-902/25/14 14:300.050 0.050 1
Chlordane (Technical)ND ug/L 03/08/14 00:03 57-74-902/25/14 14:300.20 0.20 1
4,4'-DDD ND ug/L 03/08/14 00:03 72-54-802/25/14 14:300.050 0.050 1
4,4'-DDE ND ug/L 03/08/14 00:03 72-55-902/25/14 14:300.050 0.050 1
4,4'-DDT ND ug/L 03/08/14 00:03 50-29-302/25/14 14:300.050 0.050 1
Dieldrin ND ug/L 03/08/14 00:03 60-57-102/25/14 14:300.050 0.050 1
Endosulfan I ND ug/L 03/08/14 00:03 959-98-802/25/14 14:300.050 0.050 1
Endosulfan II ND ug/L 03/08/14 00:03 33213-65-902/25/14 14:300.050 0.050 1
Endosulfan sulfate ND ug/L 03/08/14 00:03 1031-07-802/25/14 14:300.050 0.050 1
Endrin ND ug/L 03/08/14 00:03 72-20-802/25/14 14:300.050 0.050 1
Endrin aldehyde ND ug/L 03/08/14 00:03 7421-93-402/25/14 14:300.050 0.050 1
Endrin ketone ND ug/L 03/08/14 00:03 53494-70-502/25/14 14:300.050 0.050 1
Heptachlor ND ug/L 03/08/14 00:03 76-44-802/25/14 14:300.050 0.050 1
Heptachlor epoxide ND ug/L 03/08/14 00:03 1024-57-302/25/14 14:300.050 0.050 1
Hexachlorobenzene ND ug/L 03/08/14 00:03 118-74-102/25/14 14:300.050 0.050 1
Methoxychlor ND ug/L 03/08/14 00:03 72-43-502/25/14 14:300.15 0.15 1
Mirex ND ug/L 03/08/14 00:03 2385-85-502/25/14 14:300.15 0.15 1
Toxaphene ND ug/L 03/08/14 00:03 8001-35-202/25/14 14:300.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)53 %03/08/14 00:03 877-09-802/25/14 14:3020-130 1
Decachlorobiphenyl (S)61 %03/08/14 00:03 2051-24-302/25/14 14:3020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/27/14 23:47 7440-36-002/26/14 11:355.0 5.0 1
Arsenic ND ug/L 02/27/14 23:47 7440-38-202/26/14 11:3510.0 5.0 1
Barium 70.8 ug/L 02/27/14 23:47 7440-39-302/26/14 11:355.0 5.0 1
Beryllium ND ug/L 02/27/14 23:47 7440-41-702/26/14 11:351.0 1.0 1
Cadmium ND ug/L 02/27/14 23:47 7440-43-902/26/14 11:351.0 1.0 1
Chromium ND ug/L 02/27/14 23:47 7440-47-302/26/14 11:355.0 5.0 1
Cobalt ND ug/L 02/27/14 23:47 7440-48-402/26/14 11:355.0 5.0 1
Copper ND ug/L 02/27/14 23:47 7440-50-802/26/14 11:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
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[phone]
Page 17 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-23D Lab ID:92190677005 Collected:02/21/14 12:10 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/27/14 23:47 7439-92-102/26/14 11:355.0 5.0 1
Nickel ND ug/L 02/27/14 23:47 7440-02-002/26/14 11:355.0 5.0 1
Selenium ND ug/L 02/27/14 23:47 7782-49-202/26/14 11:3510.0 10.0 1
Silver ND ug/L 02/27/14 23:47 7440-22-402/26/14 11:355.0 5.0 1
Thallium ND ug/L 02/27/14 23:47 7440-28-002/26/14 11:355.4 5.4 1
Vanadium ND ug/L 02/27/14 23:47 7440-62-202/26/14 11:355.0 5.0 1
Zinc ND ug/L 02/27/14 23:47 7440-66-602/26/14 11:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 02/28/14 20:41 7439-97-602/21/14 20:500.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 03/01/14 00:10 67-64-125.0 10.0 1
Acetonitrile ND ug/L 03/01/14 00:10 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 03/01/14 00:10 107-13-110.0 1.9 1
Allyl chloride ND ug/L 03/01/14 00:10 107-05-12.0 1.5 1
Benzene ND ug/L 03/01/14 00:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 03/01/14 00:10 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/01/14 00:10 75-27-41.0 0.18 1
Bromoform ND ug/L 03/01/14 00:10 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/01/14 00:10 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/01/14 00:10 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 03/01/14 00:10 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 03/01/14 00:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/01/14 00:10 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/01/14 00:10 75-00-31.0 0.54 1
Chloroform ND ug/L 03/01/14 00:10 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/01/14 00:10 74-87-31.0 0.11 1
Chloroprene ND ug/L 03/01/14 00:10 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 03/01/14 00:10 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 03/01/14 00:10 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/01/14 00:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/01/14 00:10 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/01/14 00:10 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/01/14 00:10 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/01/14 00:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 03/01/14 00:10 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 03/01/14 00:10 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/01/14 00:10 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/01/14 00:10 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/01/14 00:10 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/01/14 00:10 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/01/14 00:10 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/01/14 00:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/01/14 00:10 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/01/14 00:10 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Sample:MW-23D Lab ID:92190677005 Collected:02/21/14 12:10 Received:02/21/14 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 03/01/14 00:10 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/01/14 00:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/01/14 00:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 03/01/14 00:10 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 03/01/14 00:10 97-63-21.0 0.20 1
2-Hexanone ND ug/L 03/01/14 00:10 591-78-65.0 0.46 1
Iodomethane ND ug/L 03/01/14 00:10 74-88-45.0 0.32 1
Isobutanol ND ug/L 03/01/14 00:10 78-83-110035.0 1
Methacrylonitrile ND ug/L 03/01/14 00:10 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 03/01/14 00:10 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 03/01/14 00:10 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/01/14 00:10 108-10-15.0 0.33 1
Naphthalene ND ug/L 03/01/14 00:10 91-20-31.0 0.24 1
Propionitrile ND ug/L 03/01/14 00:10 107-12-020.0 3.6 1
Styrene ND ug/L 03/01/14 00:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/01/14 00:10 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/01/14 00:10 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/01/14 00:10 127-18-41.0 0.46 1
Toluene ND ug/L 03/01/14 00:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 03/01/14 00:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/01/14 00:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/01/14 00:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/01/14 00:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/01/14 00:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/01/14 00:10 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/01/14 00:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/01/14 00:10 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/01/14 00:10 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/01/14 00:10 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %03/01/14 00:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/01/14 00:10 17060-07-070-130 1
Toluene-d8 (S)99 %03/01/14 00:10 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/02/14 13:25 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6213
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92190677001, 92190677003, 92190677004, 92190677005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143179
Associated Lab Samples:92190677001, 92190677003, 92190677004, 92190677005
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 02/28/14 20:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143180LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 3.02.5 118 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143181MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605012
1143182
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 119 75-125119 0 252.5ND 3.0 3.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6221
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92190677002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1144161
Associated Lab Samples:92190677002
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 02/27/14 16:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144162LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1144163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190424001
1144164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 96 75-125102 7 252.5ND 2.4 2.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15308
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1145455
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 02/27/14 22:15
Arsenic ug/L ND 10.0 02/27/14 22:15
Barium ug/L ND 5.0 02/27/14 22:15
Beryllium ug/L 0.19J 1.0 02/27/14 22:15
Cadmium ug/L ND 1.0 02/27/14 22:15
Chromium ug/L ND 5.0 02/27/14 22:15
Cobalt ug/L ND 5.0 02/27/14 22:15
Copper ug/L ND 5.0 02/27/14 22:15
Lead ug/L ND 5.0 02/27/14 22:15
Nickel ug/L ND 5.0 02/27/14 22:15
Selenium ug/L 3.5J 10.0 02/27/14 22:15
Silver ug/L 0.42J 5.0 02/27/14 22:15
Thallium ug/L ND 5.4 02/27/14 22:15
Vanadium ug/L 1.0J 5.0 02/27/14 22:15
Zinc ug/L ND 10.0 02/27/14 22:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1145456LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 473500 95 80-120
Barium ug/L 481500 96 80-120
Beryllium ug/L 476500 95 80-120
Cadmium ug/L 473500 95 80-120
Chromium ug/L 484500 97 80-120
Cobalt ug/L 475500 95 80-120
Copper ug/L 485500 97 80-120
Lead ug/L 470500 94 80-120
Nickel ug/L 473500 95 80-120
Selenium ug/L 472500 94 80-120
Silver ug/L 241250 96 80-120
Thallium ug/L 471500 94 80-120
Vanadium ug/L 495500 99 80-120
Zinc ug/L 464500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1145457MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605003
1145458
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-12599 0 25500ND496496
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1145457MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605003
1145458
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 96 75-12595 1 25500ND480475
Barium ug/L 500 95 75-12594 1 2550013.0 487 484
Beryllium ug/L 500 94 75-12594 0 25500ND469469
Cadmium ug/L 500 93 75-12593 0 25500ND466467
Chromium ug/L 500 96 75-12596 0 25500ND483482
Cobalt ug/L 500 93 75-12593 0 25500ND468468
Copper ug/L 500 97 75-12596 1 25500ND485482
Lead ug/L 500 93 75-12592 1 25500ND465462
Nickel ug/L 500 93 75-12593 0 25500ND465465
Selenium ug/L 500 95 75-12595 1 25500ND479476
Silver ug/L 250 96 75-12596 0 25250ND241240
Thallium ug/L 500 91 75-12592 0 25500ND461463
Vanadium ug/L 500 99 75-12599 0 25500ND497495
Zinc ug/L 500 92 75-12593 0 25500ND464465
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25913
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1146094
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/28/14 20:48
1,1,1-Trichloroethane ug/L ND 1.0 02/28/14 20:48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/28/14 20:48
1,1,2-Trichloroethane ug/L ND 1.0 02/28/14 20:48
1,1-Dichloroethane ug/L ND 1.0 02/28/14 20:48
1,1-Dichloroethene ug/L ND 1.0 02/28/14 20:48
1,1-Dichloropropene ug/L ND 1.0 02/28/14 20:48
1,2,3-Trichloropropane ug/L ND 1.0 02/28/14 20:48
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/28/14 20:48
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/28/14 20:48
1,2-Dichlorobenzene ug/L ND 1.0 02/28/14 20:48
1,2-Dichloroethane ug/L 0.45J 1.0 02/28/14 20:48
1,2-Dichloropropane ug/L ND 1.0 02/28/14 20:48
1,3-Dichlorobenzene ug/L ND 1.0 02/28/14 20:48
1,3-Dichloropropane ug/L ND 1.0 02/28/14 20:48
1,4-Dichlorobenzene ug/L ND 1.0 02/28/14 20:48
2,2-Dichloropropane ug/L ND 1.0 02/28/14 20:48
2-Butanone (MEK)ug/L ND 5.0 02/28/14 20:48
2-Hexanone ug/L ND 5.0 02/28/14 20:48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/28/14 20:48
Acetone ug/L ND 25.0 02/28/14 20:48
Acetonitrile ug/L ND 50.0 02/28/14 20:48
Acrylonitrile ug/L ND 10.0 02/28/14 20:48
Allyl chloride ug/L ND 2.0 02/28/14 20:48
Benzene ug/L ND 1.0 02/28/14 20:48
Bromochloromethane ug/L ND 1.0 02/28/14 20:48
Bromodichloromethane ug/L ND 1.0 02/28/14 20:48
Bromoform ug/L ND 1.0 02/28/14 20:48
Bromomethane ug/L ND 2.0 02/28/14 20:48
Carbon disulfide ug/L ND 2.0 02/28/14 20:48
Carbon tetrachloride ug/L ND 1.0 02/28/14 20:48
Chlorobenzene ug/L ND 1.0 02/28/14 20:48
Chloroethane ug/L ND 1.0 02/28/14 20:48
Chloroform ug/L ND 1.0 02/28/14 20:48
Chloromethane ug/L ND 1.0 02/28/14 20:48
Chloroprene ug/L ND 5.0 02/28/14 20:48
cis-1,2-Dichloroethene ug/L ND 1.0 02/28/14 20:48
cis-1,3-Dichloropropene ug/L ND 1.0 02/28/14 20:48
Dibromochloromethane ug/L ND 1.0 02/28/14 20:48
Dibromomethane ug/L ND 1.0 02/28/14 20:48
Dichlorodifluoromethane ug/L ND 1.0 02/28/14 20:48
Ethyl methacrylate ug/L ND 1.0 02/28/14 20:48
Ethylbenzene ug/L ND 1.0 02/28/14 20:48
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:45 PM
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Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1146094
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Matrix:Water
Analyzed
Iodomethane ug/L ND 5.0 02/28/14 20:48
Isobutanol ug/L ND 100 02/28/14 20:48
m&p-Xylene ug/L ND 2.0 02/28/14 20:48
Methacrylonitrile ug/L ND 10.0 02/28/14 20:48
Methyl methacrylate ug/L ND 2.0 02/28/14 20:48
Methylene Chloride ug/L ND 1.0 02/28/14 20:48
Naphthalene ug/L ND 1.0 02/28/14 20:48
o-Xylene ug/L ND 1.0 02/28/14 20:48
Propionitrile ug/L ND 20.0 02/28/14 20:48
Styrene ug/L ND 1.0 02/28/14 20:48
Tetrachloroethene ug/L ND 1.0 02/28/14 20:48
Toluene ug/L ND 1.0 02/28/14 20:48
trans-1,2-Dichloroethene ug/L ND 1.0 02/28/14 20:48
trans-1,3-Dichloropropene ug/L ND 1.0 02/28/14 20:48
trans-1,4-Dichloro-2-butene ug/L ND 1.0 02/28/14 20:48
Trichloroethene ug/L ND 1.0 02/28/14 20:48
Trichlorofluoromethane ug/L ND 1.0 02/28/14 20:48
Vinyl acetate ug/L ND 2.0 02/28/14 20:48
Vinyl chloride ug/L ND 1.0 02/28/14 20:48
Xylene (Total)ug/L ND 2.0 02/28/14 20:48
1,2-Dichloroethane-d4 (S)%101 70-130 02/28/14 20:48
4-Bromofluorobenzene (S)%101 70-130 02/28/14 20:48
Toluene-d8 (S)%100 70-130 02/28/14 20:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1146095LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.050 106 70-130
1,1,1-Trichloroethane ug/L 52.650 105 70-130
1,1,2,2-Tetrachloroethane ug/L 52.050 104 70-130
1,1,2-Trichloroethane ug/L 52.850 106 70-130
1,1-Dichloroethane ug/L 51.750 103 70-130
1,1-Dichloroethene ug/L 50.850 102 70-132
1,1-Dichloropropene ug/L 54.550 109 70-130
1,2,3-Trichloropropane ug/L 53.650 107 70-130
1,2-Dibromo-3-chloropropane ug/L 51.250 102 70-130
1,2-Dibromoethane (EDB)ug/L 53.350 107 70-130
1,2-Dichlorobenzene ug/L 52.850 106 70-130
1,2-Dichloroethane ug/L 50.650 101 70-130
1,2-Dichloropropane ug/L 52.550 105 70-130
1,3-Dichlorobenzene ug/L 51.350 103 70-130
1,3-Dichloropropane ug/L 52.650 105 70-130
1,4-Dichlorobenzene ug/L 52.150 104 70-130
2,2-Dichloropropane ug/L 56.150 112 58-145
2-Butanone (MEK)ug/L 101100 101 70-145
REPORT OF LABORATORY ANALYSIS
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Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1146095LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 105100 105 70-144
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 70-140
Acetone ug/L 95.8100 96 50-175
Acetonitrile ug/L 501500 100 70-130
Acrylonitrile ug/L 257250 103 70-143
Allyl chloride ug/L 50.050 100 70-130
Benzene ug/L 53.350 107 70-130
Bromochloromethane ug/L 52.850 106 70-130
Bromodichloromethane ug/L 52.350 105 70-130
Bromoform ug/L 55.050 110 70-130
Bromomethane ug/L 46.850 94 54-130
Carbon disulfide ug/L 52.850 106 70-131
Carbon tetrachloride ug/L 52.650 105 70-132
Chlorobenzene ug/L 52.350 105 70-130
Chloroethane ug/L 48.850 98 64-134
Chloroform ug/L 51.750 103 70-130
Chloromethane ug/L 49.150 98 64-130
Chloroprene ug/L 53.650 107 70-130
cis-1,2-Dichloroethene ug/L 51.150 102 70-131
cis-1,3-Dichloropropene ug/L 53.750 107 70-130
Dibromochloromethane ug/L 53.250 106 70-130
Dibromomethane ug/L 52.550 105 70-131
Dichlorodifluoromethane ug/L 53.850 108 56-130
Ethyl methacrylate ug/L 52.150 104 70-130
Ethylbenzene ug/L 51.750 103 70-130
Iodomethane ug/L 99.8100 100 49-180
Isobutanol ug/L 10701000 107 70-130
m&p-Xylene ug/L 107100 107 70-130
Methacrylonitrile ug/L 524500 105 70-130
Methyl methacrylate ug/L 52.550 105 70-130
Methylene Chloride ug/L 49.050 98 63-130
Naphthalene ug/L 52.450 105 70-138
o-Xylene ug/L 53.850 108 70-130
Propionitrile ug/L 531500 106 70-130
Styrene ug/L 54.950 110 70-130
Tetrachloroethene ug/L 53.150 106 70-130
Toluene ug/L 52.050 104 70-130
trans-1,2-Dichloroethene ug/L 51.250 102 70-130
trans-1,3-Dichloropropene ug/L 54.150 108 70-132
trans-1,4-Dichloro-2-butene ug/L 53.550 107 70-141
Trichloroethene ug/L 51.850 104 70-130
Trichlorofluoromethane ug/L 50.750 101 62-133
Vinyl acetate ug/L 109100 109 66-157
Vinyl chloride ug/L 53.850 108 69-130
Xylene (Total)ug/L 161150 107 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1146096MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190677005
1146097
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 109 70-166108 1 3050ND54.3 54.0
Benzene ug/L 50 112 70-148110 1 3050ND55.8 55.2
Chlorobenzene ug/L 50 110 70-146108 2 3050ND55.0 53.9
Toluene ug/L 50 107 70-155104 2 3050ND53.3 52.1
Trichloroethene ug/L 50 115 69-151114 2 3050ND57.7 56.8
1,2-Dichloroethane-d4 (S)%97 70-13099
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26098
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1144739
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 03/07/14 16:28
4,4'-DDE ug/L ND 0.050 03/07/14 16:28
4,4'-DDT ug/L ND 0.050 03/07/14 16:28
Aldrin ug/L ND 0.050 03/07/14 16:28
alpha-BHC ug/L ND 0.050 03/07/14 16:28
beta-BHC ug/L ND 0.050 03/07/14 16:28
Chlordane (Technical)ug/L ND 0.20 03/07/14 16:28
delta-BHC ug/L ND 0.050 03/07/14 16:28
Dieldrin ug/L ND 0.050 03/07/14 16:28
Endosulfan I ug/L ND 0.050 03/07/14 16:28
Endosulfan II ug/L ND 0.050 03/07/14 16:28
Endosulfan sulfate ug/L ND 0.050 03/07/14 16:28
Endrin ug/L ND 0.050 03/07/14 16:28
Endrin aldehyde ug/L ND 0.050 03/07/14 16:28
Endrin ketone ug/L ND 0.050 03/07/14 16:28
gamma-BHC (Lindane)ug/L ND 0.050 03/07/14 16:28
Heptachlor ug/L ND 0.050 03/07/14 16:28
Heptachlor epoxide ug/L ND 0.050 03/07/14 16:28
Hexachlorobenzene ug/L ND 0.050 03/07/14 16:28
Methoxychlor ug/L ND 0.15 03/07/14 16:28
Mirex ug/L ND 0.15 03/07/14 16:28
Toxaphene ug/L ND 0.20 03/07/14 16:28
Decachlorobiphenyl (S)%75 20-130 03/07/14 16:28
Tetrachloro-m-xylene (S)%74 20-130 03/07/14 16:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144740LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.19.25 79 20-150
4,4'-DDE ug/L 0.18.25 72 20-150
4,4'-DDT ug/L 0.19.25 77 20-150
Aldrin ug/L 0.12.25 50 20-150
alpha-BHC ug/L 0.19.25 76 20-150
beta-BHC ug/L 0.20.25 79 20-150
delta-BHC ug/L 0.20.25 81 20-150
Dieldrin ug/L 0.18.25 74 20-150
Endosulfan I ug/L 0.20.25 80 20-150
Endosulfan II ug/L 0.20.25 80 20-150
Endosulfan sulfate ug/L 0.21.25 83 20-150
Endrin ug/L 0.22.25 88 20-150
Endrin aldehyde ug/L 0.19.25 76 20-150
REPORT OF LABORATORY ANALYSIS
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Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144740LABORATORY CONTROL SAMPLE:
LCSSpike
Endrin ketone ug/L 0.21.25 84 20-150
gamma-BHC (Lindane)ug/L 0.19.25 76 20-150
Heptachlor ug/L 0.14.25 55 20-150
Heptachlor epoxide ug/L 0.20.25 81 20-150
Hexachlorobenzene ug/L 0.16.25 66 20-150
Methoxychlor ug/L 0.59.74 80 20-150
Mirex ug/L 0.61.74 82 20-150
Decachlorobiphenyl (S)%80 20-130
Tetrachloro-m-xylene (S)%77 20-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1144741MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190605005
1144742
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4,4'-DDD ug/L .25 55 20-15074 29 30.25ND 0.14 0.18
4,4'-DDE ug/L .25 65 20-15077 17 30.25ND 0.16 0.19
4,4'-DDT ug/L .25 68 20-15084 22 30.25ND 0.17 0.21
Aldrin ug/L .25 49 20-15063 27 30.25ND 0.12 0.16
alpha-BHC ug/L .25 79 20-15076 4 30.25ND 0.20 0.19
beta-BHC ug/L .25 80 20-15077 4 30.25ND 0.20 0.19
delta-BHC ug/L .25 83 20-15081 3 30.25ND 0.21 0.20
Dieldrin ug/L .25 47 20-15063 28 30.25ND 0.12 0.16
Endosulfan I ug/L .25 57 20-15069 20 30.25ND 0.14 0.17
Endosulfan II ug/L .25 48 20-15062 25 30.25ND 0.12 0.15
Endosulfan sulfate ug/L .25 57 20-15069 18 30.25ND 0.14 0.17
Endrin ug/L .25 62 20-15079 24 30.25ND 0.15 0.20
Endrin aldehyde ug/L .25 74 20-15076 3 30.25ND 0.18 0.19
Endrin ketone ug/L .25 70 20-15077 10 30.25ND 0.17 0.19
gamma-BHC (Lindane)ug/L .25 79 20-15076 4 30.25ND 0.20 0.19
Heptachlor ug/L .25 47 20-15063 28 30.25ND 0.12 0.15
Heptachlor epoxide ug/L .25 62 20-15071 14 30.25ND 0.15 0.18
Hexachlorobenzene ug/L .25 57 20-15062 9 30.25ND 0.14 0.15
Methoxychlor ug/L .74 59 20-15074 22 30.74ND 0.44 0.55
Mirex ug/L .74 81 20-15080 0 30.74ND 0.60 0.60
Decachlorobiphenyl (S)%63 20-13061
Tetrachloro-m-xylene (S)%79 20-13080
REPORT OF LABORATORY ANALYSIS
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Page 29 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/18218
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148517
Associated Lab Samples:92190677001, 92190677002, 92190677003, 92190677004, 92190677005
Matrix:Water
Analyzed
Cyanide mg/L ND 0.0050 03/02/14 13:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148518LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.10.1 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148519MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190643005
1148520
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 107 75-125105 2 20.10.011 0.12 0.12
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148521MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190034008
1148522
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 111 75-125112 1 20.1ND 0.11 0.12
REPORT OF LABORATORY ANALYSIS
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Page 30 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 31 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190677
FRANCIS FARM LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190677001 FLD/MW-1A
92190677002 FLD/MW-4
92190677003 FLD/MW-18
92190677004 FLD/MW-23
92190677005 FLD/MW-23D
92190677001 OEXT/26098 GCSV/16861MW-1A EPA 3510 EPA 8081
92190677002 OEXT/26098 GCSV/16861MW-4 EPA 3510 EPA 8081
92190677003 OEXT/26098 GCSV/16861MW-18 EPA 3510 EPA 8081
92190677004 OEXT/26098 GCSV/16861MW-23 EPA 3510 EPA 8081
92190677005 OEXT/26098 GCSV/16861MW-23D EPA 3510 EPA 8081
92190677001 MPRP/15308 ICP/13890MW-1A EPA 3010 EPA 6010
92190677002 MPRP/15308 ICP/13890MW-4 EPA 3010 EPA 6010
92190677003 MPRP/15308 ICP/13890MW-18 EPA 3010 EPA 6010
92190677004 MPRP/15308 ICP/13890MW-23 EPA 3010 EPA 6010
92190677005 MPRP/15308 ICP/13890MW-23D EPA 3010 EPA 6010
92190677001 MERP/6213 MERC/5995MW-1A EPA 7470 EPA 7470
92190677002 MERP/6221 MERC/6001MW-4 EPA 7470 EPA 7470
92190677003 MERP/6213 MERC/5995MW-18 EPA 7470 EPA 7470
92190677004 MERP/6213 MERC/5995MW-23 EPA 7470 EPA 7470
92190677005 MERP/6213 MERC/5995MW-23D EPA 7470 EPA 7470
92190677001 MSV/25913MW-1A EPA 8260
92190677002 MSV/25913MW-4 EPA 8260
92190677003 MSV/25913MW-18 EPA 8260
92190677004 MSV/25913MW-23 EPA 8260
92190677005 MSV/25913MW-23D EPA 8260
92190677001 WETA/18218MW-1A SM 4500-CN-E
92190677002 WETA/18218MW-4 SM 4500-CN-E
92190677003 WETA/18218MW-18 SM 4500-CN-E
92190677004 WETA/18218MW-23 SM 4500-CN-E
92190677005 WETA/18218MW-23D SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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Page 32 of 34
Page 33 of 34
Page 34 of 34
#=CL#
March 19, 2014
LIMS USE: FR - STEPHEN KING
LIMS OBJECT ID: 92191006
92191006
Project:
Pace Project No.:
RE:
Mr. Stephen King
Haywood Co. Solid Waste
278 Recycle Rd.
Clyde, NC 28721
FRANCIS FARM LF
Dear Mr. King:
Enclosed are the analytical results for sample(s) received by the laboratory on February 25, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
cc:Andy Alexander, BLE
Mr. Stephen King, Haywood Co. Solid Waste
REPORT OF LABORATORY ANALYSIS
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Page 1 of 50
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 50
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Lab ID Sample ID Matrix Date Collected Date Received
92191006001 MW-11 Water 02/25/14 13:20 02/25/14 16:15
92191006002 MW-13 Water 02/25/14 12:15 02/25/14 16:15
92191006003 MW-14 Water 02/25/14 12:40 02/25/14 16:15
92191006004 MW-14D Water 02/25/14 12:55 02/25/14 16:15
92191006005 MW-15 Water 02/25/14 11:30 02/25/14 16:15
92191006006 MW-16 Water 02/25/14 10:50 02/25/14 16:15
92191006007 MW-16D Water 02/25/14 11:05 02/25/14 16:15
92191006008 MW-17 Water 02/25/14 10:30 02/25/14 16:15
92191006009 MW-22 Water 02/25/14 10:10 02/25/14 16:15
92191006010 MW-25 Water 02/25/14 13:35 02/25/14 16:15
REPORT OF LABORATORY ANALYSIS
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Page 3 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92191006001 MW-11 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006002 MW-13 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006003 MW-14 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006004 MW-14D EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006005 MW-15 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006006 MW-16 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006007 MW-16D EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006008 MW-17 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006009 MW-22 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191006010 MW-25 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-AJMW
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-11 Lab ID:92191006001 Collected:02/25/14 13:20 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:111
Collected Date 02/25/14 03/12/14 16:111
Collected Time 13:20 03/12/14 16:111
Field pH 6.4 Std. Units 03/12/14 16:110.10 0.10 1
Field Temperature 15.0 deg C 03/12/14 16:110.50 0.50 1
Field Specific Conductance 617 umhos/cm 03/12/14 16:111.0 1.0 1
Turbidity 2.87 NTU 03/12/14 16:111.0 1.0 1
Odor O&G 03/12/14 16:111
Appearance CLEAR 03/12/14 16:111
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/04/14 23:28 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/04/14 23:28 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/04/14 23:28 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/04/14 23:28 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/04/14 23:28 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/04/14 23:28 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/04/14 23:28 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/04/14 23:28 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/04/14 23:28 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/04/14 23:28 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/04/14 23:28 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/04/14 23:28 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/04/14 23:28 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/04/14 23:28 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/04/14 23:28 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/04/14 23:28 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/04/14 23:28 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/04/14 23:28 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/04/14 23:28 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/04/14 23:28 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/04/14 23:28 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/04/14 23:28 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)92 %03/04/14 23:28 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)72 %03/04/14 23:28 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 06:56 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 06:56 7440-38-202/27/14 10:3510.0 5.0 1
Barium 85.3 ug/L 02/28/14 06:56 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 06:56 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 06:56 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 06:56 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 06:56 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 06:56 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-11 Lab ID:92191006001 Collected:02/25/14 13:20 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 06:56 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 06:56 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 06:56 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 06:56 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 06:56 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 06:56 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 06:56 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:27 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 08:11 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 08:11 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 08:11 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 08:11 107-05-12.0 1.5 1
Benzene 0.28J ug/L 02/28/14 08:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 08:11 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 08:11 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 08:11 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 08:11 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 08:11 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 08:11 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 08:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 08:11 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 08:11 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 08:11 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 08:11 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 08:11 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 08:11 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 08:11 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 08:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 08:11 74-95-31.0 0.21 1
1,2-Dichlorobenzene 3.3 ug/L 02/28/14 08:11 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 08:11 541-73-11.0 0.24 1
1,4-Dichlorobenzene 1.0 ug/L 02/28/14 08:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 08:11 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 08:11 75-71-81.0 0.21 1
1,1-Dichloroethane 5.2 ug/L 02/28/14 08:11 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 08:11 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 08:11 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 14.8 ug/L 02/28/14 08:11 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 08:11 156-60-51.0 0.49 1
1,2-Dichloropropane 0.31J ug/L 02/28/14 08:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 08:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 08:11 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-11 Lab ID:92191006001 Collected:02/25/14 13:20 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 08:11 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 08:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 08:11 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 08:11 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 08:11 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 08:11 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 08:11 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 08:11 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 08:11 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 08:11 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 08:11 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 08:11 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 08:11 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 08:11 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 08:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 08:11 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 08:11 79-34-51.0 0.40 1
Tetrachloroethene 1.1 ug/L 02/28/14 08:11 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 08:11 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 08:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 08:11 79-00-51.0 0.29 1
Trichloroethene 1.2 ug/L 02/28/14 08:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 08:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 08:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 08:11 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 08:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 08:11 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 08:11 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 08:11 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 08:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 08:11 17060-07-070-130 1
Toluene-d8 (S)97 %02/28/14 08:11 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide 0.0052 mg/L 03/07/14 16:06 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-13 Lab ID:92191006002 Collected:02/25/14 12:15 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:131
Collected Date 02/25/14 03/12/14 16:131
Collected Time 12:15 03/12/14 16:131
Field pH 6.1 Std. Units 03/12/14 16:130.10 0.10 1
Field Temperature 15.8 deg C 03/12/14 16:130.50 0.50 1
Field Specific Conductance 478 umhos/cm 03/12/14 16:131.0 1.0 1
Turbidity 1.99 NTU 03/12/14 16:131.0 1.0 1
Odor SLIGHT 03/12/14 16:131
Appearance CLEAR 03/12/14 16:131
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/04/14 23:46 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/04/14 23:46 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/04/14 23:46 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/04/14 23:46 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/04/14 23:46 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/04/14 23:46 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/04/14 23:46 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/04/14 23:46 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/04/14 23:46 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/04/14 23:46 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/04/14 23:46 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/04/14 23:46 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/04/14 23:46 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/04/14 23:46 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/04/14 23:46 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/04/14 23:46 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/04/14 23:46 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/04/14 23:46 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/04/14 23:46 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/04/14 23:46 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/04/14 23:46 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/04/14 23:46 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %03/04/14 23:46 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)88 %03/04/14 23:46 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 06:59 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 06:59 7440-38-202/27/14 10:3510.0 5.0 1
Barium 823 ug/L 02/28/14 06:59 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 06:59 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 06:59 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 06:59 7440-47-302/27/14 10:355.0 5.0 1
Cobalt 11.9 ug/L 02/28/14 06:59 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 06:59 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-13 Lab ID:92191006002 Collected:02/25/14 12:15 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 06:59 7439-92-102/27/14 10:355.0 5.0 1
Nickel 28.6 ug/L 02/28/14 06:59 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 06:59 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 06:59 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 06:59 7440-28-002/27/14 10:355.4 5.4 1
Vanadium 6.2 ug/L 02/28/14 06:59 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 06:59 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:34 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 08:26 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 08:26 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 08:26 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 08:26 107-05-12.0 1.5 1
Benzene 3.6 ug/L 02/28/14 08:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 08:26 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 08:26 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 08:26 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 08:26 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 08:26 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 08:26 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 08:26 56-23-51.0 0.25 1
Chlorobenzene 0.57J ug/L 02/28/14 08:26 108-90-71.0 0.23 1
Chloroethane 0.57J ug/L 02/28/14 08:26 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 08:26 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 08:26 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 08:26 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 08:26 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 08:26 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 08:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 08:26 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 08:26 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 08:26 541-73-11.0 0.24 1
1,4-Dichlorobenzene 7.3 ug/L 02/28/14 08:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 08:26 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 08:26 75-71-81.0 0.21 1
1,1-Dichloroethane 1.7 ug/L 02/28/14 08:26 75-34-31.0 0.32 1
1,2-Dichloroethane 0.25J ug/L 02/28/14 08:26 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 08:26 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 10.9 ug/L 02/28/14 08:26 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 08:26 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 08:26 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 08:26 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 08:26 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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Page 10 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-13 Lab ID:92191006002 Collected:02/25/14 12:15 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 08:26 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 08:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 08:26 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 08:26 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 08:26 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 08:26 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 08:26 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 08:26 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 08:26 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 08:26 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 08:26 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 08:26 108-10-15.0 0.33 1
Naphthalene 1.0 ug/L 02/28/14 08:26 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 08:26 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 08:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 08:26 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 08:26 79-34-51.0 0.40 1
Tetrachloroethene 1.2 ug/L 02/28/14 08:26 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 08:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 08:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 08:26 79-00-51.0 0.29 1
Trichloroethene 0.98J ug/L 02/28/14 08:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 08:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 08:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 08:26 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 08:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 08:26 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 08:26 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 08:26 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %02/28/14 08:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 08:26 17060-07-070-130 1
Toluene-d8 (S)97 %02/28/14 08:26 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:07 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
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Page 11 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-14 Lab ID:92191006003 Collected:02/25/14 12:40 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:141
Collected Date 02/25/14 03/12/14 16:141
Collected Time 12:40 03/12/14 16:141
Field pH 6.3 Std. Units 03/12/14 16:140.10 0.10 1
Field Temperature 13.0 deg C 03/12/14 16:140.50 0.50 1
Field Specific Conductance 742 umhos/cm 03/12/14 16:141.0 1.0 1
Turbidity 4.88 NTU 03/12/14 16:141.0 1.0 1
Odor NONE 03/12/14 16:141
Appearance CLEAR 03/12/14 16:141
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 00:03 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 00:03 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 00:03 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 00:03 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 00:03 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 00:03 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 00:03 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 00:03 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 00:03 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 00:03 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 00:03 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 00:03 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 00:03 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 00:03 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 00:03 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 00:03 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 00:03 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 00:03 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 00:03 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 00:03 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 00:03 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 00:03 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %03/05/14 00:03 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)92 %03/05/14 00:03 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:02 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:02 7440-38-202/27/14 10:3510.0 5.0 1
Barium 240 ug/L 02/28/14 07:02 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:02 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:02 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:02 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:02 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:02 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-14 Lab ID:92191006003 Collected:02/25/14 12:40 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:02 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:02 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:02 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:02 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:02 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 07:02 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 07:02 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:37 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 08:42 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 08:42 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 08:42 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 08:42 107-05-12.0 1.5 1
Benzene 1.3 ug/L 02/28/14 08:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 08:42 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 08:42 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 08:42 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 08:42 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 08:42 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 08:42 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 08:42 56-23-51.0 0.25 1
Chlorobenzene 1.5 ug/L 02/28/14 08:42 108-90-71.0 0.23 1
Chloroethane 1.0 ug/L 02/28/14 08:42 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 08:42 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 08:42 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 08:42 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 08:42 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 08:42 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 08:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 08:42 74-95-31.0 0.21 1
1,2-Dichlorobenzene 70.5 ug/L 02/28/14 08:42 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.42J ug/L 02/28/14 08:42 541-73-11.0 0.24 1
1,4-Dichlorobenzene 18.0 ug/L 02/28/14 08:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 08:42 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 08:42 75-71-81.0 0.21 1
1,1-Dichloroethane 0.68J ug/L 02/28/14 08:42 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 08:42 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 08:42 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 15.1 ug/L 02/28/14 08:42 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 08:42 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 08:42 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 08:42 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 08:42 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-14 Lab ID:92191006003 Collected:02/25/14 12:40 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 08:42 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 08:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 08:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 08:42 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 08:42 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 08:42 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 08:42 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 08:42 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 08:42 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 08:42 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 08:42 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 08:42 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 08:42 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 08:42 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 08:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 08:42 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 08:42 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 08:42 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 08:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 08:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 08:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 08:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 08:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 08:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 08:42 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 08:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 08:42 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 08:42 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 08:42 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/28/14 08:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 08:42 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 08:42 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:08 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-14D Lab ID:92191006004 Collected:02/25/14 12:55 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:161
Collected Date 02/25/14 03/12/14 16:161
Collected Time 12:55 03/12/14 16:161
Field pH 9.6 Std. Units 03/12/14 16:160.10 0.10 1
Field Temperature 13.1 deg C 03/12/14 16:160.50 0.50 1
Field Specific Conductance 214 umhos/cm 03/12/14 16:161.0 1.0 1
Turbidity 4.27 NTU 03/12/14 16:161.0 1.0 1
Odor SLIGHT 03/12/14 16:161
Appearance CLEAR 03/12/14 16:161
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 00:21 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 00:21 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 00:21 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 00:21 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 00:21 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 00:21 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 00:21 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 00:21 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 00:21 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 00:21 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 00:21 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 00:21 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 00:21 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 00:21 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 00:21 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 00:21 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 00:21 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 00:21 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 00:21 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 00:21 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 00:21 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 00:21 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)57 %03/05/14 00:21 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)60 %03/05/14 00:21 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:15 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:15 7440-38-202/27/14 10:3510.0 5.0 1
Barium 42.4 ug/L 02/28/14 07:15 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:15 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:15 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:15 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:15 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:15 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-14D Lab ID:92191006004 Collected:02/25/14 12:55 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:15 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:15 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:15 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:15 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:15 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 07:15 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 07:15 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:40 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 08:58 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 08:58 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 08:58 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 08:58 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 08:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 08:58 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 08:58 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 08:58 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 08:58 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 08:58 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 08:58 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 08:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 08:58 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 08:58 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 08:58 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 08:58 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 08:58 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 08:58 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 08:58 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 08:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 08:58 74-95-31.0 0.21 1
1,2-Dichlorobenzene 1.6 ug/L 02/28/14 08:58 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 08:58 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.36J ug/L 02/28/14 08:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 08:58 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 08:58 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 08:58 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 08:58 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 08:58 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.68J ug/L 02/28/14 08:58 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 08:58 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 08:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 08:58 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 08:58 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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Page 16 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-14D Lab ID:92191006004 Collected:02/25/14 12:55 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 08:58 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 08:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 08:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 08:58 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 08:58 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 08:58 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 08:58 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 08:58 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 08:58 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 08:58 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 08:58 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 08:58 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 08:58 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 08:58 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 08:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 08:58 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 08:58 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 08:58 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 08:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 08:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 08:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 08:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 08:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 08:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 08:58 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 08:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 08:58 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 08:58 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 08:58 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/28/14 08:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 08:58 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 08:58 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:08 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
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Page 17 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-15 Lab ID:92191006005 Collected:02/25/14 11:30 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:171
Collected Date 02/25/14 03/12/14 16:171
Collected Time 11:30 03/12/14 16:171
Field pH 7.4 Std. Units 03/12/14 16:170.10 0.10 1
Field Temperature 13.2 deg C 03/12/14 16:170.50 0.50 1
Field Specific Conductance 701 umhos/cm 03/12/14 16:171.0 1.0 1
Turbidity 3.29 NTU 03/12/14 16:171.0 1.0 1
Odor NONE 03/12/14 16:171
Appearance CLEAR 03/12/14 16:171
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 00:38 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 00:38 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 00:38 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 00:38 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 00:38 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 00:38 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 00:38 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 00:38 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 00:38 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 00:38 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 00:38 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 00:38 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 00:38 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 00:38 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 00:38 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 00:38 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 00:38 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 00:38 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 00:38 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 00:38 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 00:38 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 00:38 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %03/05/14 00:38 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)86 %03/05/14 00:38 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:18 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:18 7440-38-202/27/14 10:3510.0 5.0 1
Barium 40.1 ug/L 02/28/14 07:18 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:18 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:18 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:18 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:18 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:18 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-15 Lab ID:92191006005 Collected:02/25/14 11:30 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:18 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:18 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:18 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:18 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:18 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 07:18 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 07:18 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:42 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 09:13 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 09:13 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 09:13 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 09:13 107-05-12.0 1.5 1
Benzene 0.26J ug/L 02/28/14 09:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 09:13 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 09:13 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 09:13 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 09:13 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 09:13 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 09:13 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 09:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 09:13 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 09:13 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 09:13 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 09:13 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 09:13 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 09:13 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 09:13 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 09:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 09:13 74-95-31.0 0.21 1
1,2-Dichlorobenzene 7.2 ug/L 02/28/14 09:13 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 09:13 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.72J ug/L 02/28/14 09:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 09:13 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 09:13 75-71-81.0 0.21 1
1,1-Dichloroethane 0.54J ug/L 02/28/14 09:13 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 09:13 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 09:13 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 3.7 ug/L 02/28/14 09:13 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 09:13 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 09:13 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 09:13 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 09:13 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-15 Lab ID:92191006005 Collected:02/25/14 11:30 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 09:13 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 09:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 09:13 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 09:13 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 09:13 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 09:13 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 09:13 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 09:13 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 09:13 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 09:13 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 09:13 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 09:13 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 09:13 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 09:13 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 09:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 09:13 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 09:13 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 09:13 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 09:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 09:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 09:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 09:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 09:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 09:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 09:13 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 09:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 09:13 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 09:13 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 09:13 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 09:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 09:13 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 09:13 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:11 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-16 Lab ID:92191006006 Collected:02/25/14 10:50 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:181
Collected Date 02/25/14 03/12/14 16:181
Collected Time 10:50 03/12/14 16:181
Field pH 6.1 Std. Units 03/12/14 16:180.10 0.10 1
Field Temperature 11.3 deg C 03/12/14 16:180.50 0.50 1
Field Specific Conductance 89 umhos/cm 03/12/14 16:181.0 1.0 1
Turbidity 15.8 NTU 03/12/14 16:181.0 1.0 1
Odor NONE 03/12/14 16:181
Appearance CLOUDY 03/12/14 16:181
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 00:56 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 00:56 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 00:56 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 00:56 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 00:56 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 00:56 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 00:56 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 00:56 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 00:56 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 00:56 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 00:56 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 00:56 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 00:56 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 00:56 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 00:56 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 00:56 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 00:56 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 00:56 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 00:56 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 00:56 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 00:56 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 00:56 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)70 %03/05/14 00:56 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)62 %03/05/14 00:56 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:22 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:22 7440-38-202/27/14 10:3510.0 5.0 1
Barium 176 ug/L 02/28/14 07:22 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:22 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:22 7440-43-902/27/14 10:351.0 1.0 1
Chromium 5.6 ug/L 02/28/14 07:22 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:22 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:22 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-16 Lab ID:92191006006 Collected:02/25/14 10:50 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:22 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:22 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:22 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:22 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:22 7440-28-002/27/14 10:355.4 5.4 1
Vanadium 12.8 ug/L 02/28/14 07:22 7440-62-202/27/14 10:355.0 5.0 1
Zinc 14.0 ug/L 02/28/14 07:22 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:45 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 09:29 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 09:29 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 09:29 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 09:29 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 09:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 09:29 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 09:29 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 09:29 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 09:29 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 09:29 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 09:29 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 09:29 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 09:29 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 09:29 75-00-31.0 0.54 1
Chloroform 1.4 ug/L 02/28/14 09:29 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 09:29 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 09:29 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 09:29 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 09:29 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 09:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 09:29 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 09:29 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 09:29 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 09:29 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 09:29 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 09:29 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 09:29 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 09:29 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 09:29 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 09:29 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 09:29 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 09:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 09:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 09:29 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-16 Lab ID:92191006006 Collected:02/25/14 10:50 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 09:29 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 09:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 09:29 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 09:29 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 09:29 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 09:29 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 09:29 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 09:29 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 09:29 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 09:29 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 09:29 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 09:29 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 09:29 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 09:29 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 09:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 09:29 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 09:29 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 09:29 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 09:29 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 09:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 09:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 09:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 09:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 09:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 09:29 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 09:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 09:29 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 09:29 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 09:29 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 09:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 09:29 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 09:29 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:12 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-16D Lab ID:92191006007 Collected:02/25/14 11:05 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:181
Collected Date 02/25/14 03/12/14 16:181
Collected Time 11:05 03/12/14 16:181
Field pH 7.2 Std. Units 03/12/14 16:180.10 0.10 1
Field Temperature 11.8 deg C 03/12/14 16:180.50 0.50 1
Field Specific Conductance 186 umhos/cm 03/12/14 16:181.0 1.0 1
Turbidity 6.71 NTU 03/12/14 16:181.0 1.0 1
Odor NONE 03/12/14 16:181
Appearance CLEAR 03/12/14 16:181
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 01:13 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 01:13 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 01:13 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 01:13 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 01:13 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 01:13 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 01:13 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 01:13 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 01:13 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 01:13 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 01:13 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 01:13 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 01:13 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 01:13 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 01:13 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 01:13 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 01:13 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 01:13 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 01:13 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 01:13 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 01:13 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 01:13 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)67 %03/05/14 01:13 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)54 %03/05/14 01:13 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:25 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:25 7440-38-202/27/14 10:3510.0 5.0 1
Barium 38.6 ug/L 02/28/14 07:25 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:25 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:25 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:25 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:25 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:25 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-16D Lab ID:92191006007 Collected:02/25/14 11:05 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:25 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:25 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:25 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:25 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:25 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 07:25 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 07:25 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:53 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 09:45 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 09:45 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 09:45 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 09:45 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 09:45 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 09:45 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 09:45 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 09:45 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 09:45 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 09:45 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 09:45 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 09:45 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 09:45 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 09:45 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 09:45 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 09:45 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 09:45 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 09:45 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 09:45 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 09:45 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 09:45 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 09:45 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 09:45 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 09:45 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 09:45 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 09:45 75-71-81.0 0.21 1
1,1-Dichloroethane 1.2 ug/L 02/28/14 09:45 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 09:45 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 09:45 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.82J ug/L 02/28/14 09:45 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 09:45 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 09:45 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 09:45 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 09:45 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-16D Lab ID:92191006007 Collected:02/25/14 11:05 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 09:45 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 09:45 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 09:45 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 09:45 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 09:45 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 09:45 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 09:45 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 09:45 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 09:45 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 09:45 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 09:45 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 09:45 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 09:45 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 09:45 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 09:45 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 09:45 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 09:45 79-34-51.0 0.40 1
Tetrachloroethene 0.62J ug/L 02/28/14 09:45 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 09:45 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 09:45 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 09:45 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 09:45 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 09:45 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 09:45 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 09:45 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 09:45 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 09:45 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 09:45 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 09:45 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 09:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/28/14 09:45 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 09:45 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:13 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-17 Lab ID:92191006008 Collected:02/25/14 10:30 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:201
Collected Date 02/25/14 03/12/14 16:201
Collected Time 10:30 03/12/14 16:201
Field pH 6.0 Std. Units 03/12/14 16:200.10 0.10 1
Field Temperature 11.6 deg C 03/12/14 16:200.50 0.50 1
Field Specific Conductance 77 umhos/cm 03/12/14 16:201.0 1.0 1
Turbidity 2.96 NTU 03/12/14 16:201.0 1.0 1
Odor NONE 03/12/14 16:201
Appearance CLEAR 03/12/14 16:201
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 03:16 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 03:16 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 03:16 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 03:16 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 03:16 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 03:16 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 03:16 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 03:16 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 03:16 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 03:16 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 03:16 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 03:16 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 03:16 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 03:16 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 03:16 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 03:16 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 03:16 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 03:16 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 03:16 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 03:16 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 03:16 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 03:16 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)68 %03/05/14 03:16 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)45 %03/05/14 03:16 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:28 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:28 7440-38-202/27/14 10:3510.0 5.0 1
Barium 48.8 ug/L 02/28/14 07:28 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:28 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:28 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:28 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:28 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:28 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-17 Lab ID:92191006008 Collected:02/25/14 10:30 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:28 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:28 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:28 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:28 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:28 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 07:28 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 07:28 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:56 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 10:00 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 10:00 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 10:00 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 10:00 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 10:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 10:00 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 10:00 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 10:00 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 10:00 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 10:00 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 10:00 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 10:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 10:00 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 10:00 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 10:00 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 10:00 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 10:00 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 10:00 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 10:00 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 10:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 10:00 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 10:00 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 10:00 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 10:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 10:00 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 10:00 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 10:00 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 10:00 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 10:00 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 10:00 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 10:00 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 10:00 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 10:00 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 10:00 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-17 Lab ID:92191006008 Collected:02/25/14 10:30 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 10:00 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 10:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 10:00 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 10:00 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 10:00 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 10:00 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 10:00 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 10:00 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 10:00 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 10:00 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 10:00 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 10:00 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 10:00 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 10:00 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 10:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 10:00 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 10:00 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 10:00 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 10:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 10:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 10:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 10:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 10:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 10:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 10:00 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 10:00 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 10:00 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 10:00 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 10:00 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 10:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 10:00 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 10:00 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:14 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-22 Lab ID:92191006009 Collected:02/25/14 10:10 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:211
Collected Date 02/25/14 03/12/14 16:211
Collected Time 10:10 03/12/14 16:211
Field pH 5.8 Std. Units 03/12/14 16:210.10 0.10 1
Field Temperature 7.8 deg C 03/12/14 16:210.50 0.50 1
Field Specific Conductance 72 umhos/cm 03/12/14 16:211.0 1.0 1
Turbidity 5.59 NTU 03/12/14 16:211.0 1.0 1
Odor NONE 03/12/14 16:211
Appearance CLEAR 03/12/14 16:211
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 03:33 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 03:33 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 03:33 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 03:33 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/05/14 03:33 58-89-902/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 03:33 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 03:33 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 03:33 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 03:33 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 03:33 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 03:33 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 03:33 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 03:33 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 03:33 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 03:33 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 03:33 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor ND ug/L 03/05/14 03:33 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 03:33 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 03:33 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 03:33 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 03:33 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 03:33 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)59 %03/05/14 03:33 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)70 %03/05/14 03:33 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:31 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:31 7440-38-202/27/14 10:3510.0 5.0 1
Barium 74.7 ug/L 02/28/14 07:31 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:31 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:31 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:31 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:31 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:31 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-22 Lab ID:92191006009 Collected:02/25/14 10:10 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:31 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:31 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:31 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:31 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:31 7440-28-002/27/14 10:355.4 5.4 1
Vanadium ND ug/L 02/28/14 07:31 7440-62-202/27/14 10:355.0 5.0 1
Zinc 35.2 ug/L 02/28/14 07:31 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 15:58 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 10:16 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 10:16 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 10:16 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 10:16 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 10:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 10:16 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 10:16 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 10:16 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 10:16 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 10:16 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 10:16 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 10:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 10:16 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 10:16 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 10:16 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 10:16 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 10:16 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 10:16 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 10:16 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 10:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 10:16 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 10:16 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 10:16 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 10:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 10:16 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 10:16 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 10:16 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 10:16 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 10:16 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 10:16 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 10:16 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 10:16 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 10:16 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 10:16 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-22 Lab ID:92191006009 Collected:02/25/14 10:10 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 10:16 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 10:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 10:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 10:16 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 10:16 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 10:16 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 10:16 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 10:16 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 10:16 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 10:16 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 10:16 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 10:16 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 10:16 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 10:16 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 10:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 10:16 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 10:16 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 10:16 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 10:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 10:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 10:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 10:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 10:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 10:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 10:16 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 10:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 10:16 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 10:16 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 10:16 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 10:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 10:16 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 10:16 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:16 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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Page 32 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-25 Lab ID:92191006010 Collected:02/25/14 13:35 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 16:221
Collected Date 02/25/14 03/12/14 16:221
Collected Time 13:35 03/12/14 16:221
Field pH 10.15 Std. Units 03/12/14 16:220.10 0.10 1
Field Temperature 14.8 deg C 03/12/14 16:220.50 0.50 1
Field Specific Conductance 663 umhos/cm 03/12/14 16:221.0 1.0 1
Turbidity 4.56 NTU 03/12/14 16:221.0 1.0 1
Odor SLIGHT 03/12/14 16:221
Appearance CLEAR 03/12/14 16:221
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/05/14 03:51 309-00-202/26/14 09:100.050 0.050 1
alpha-BHC ND ug/L 03/05/14 03:51 319-84-602/26/14 09:100.050 0.050 1
beta-BHC ND ug/L 03/05/14 03:51 319-85-702/26/14 09:100.050 0.050 1
delta-BHC ND ug/L 03/05/14 03:51 319-86-802/26/14 09:100.050 0.050 1
gamma-BHC (Lindane)0.22 ug/L 03/05/14 03:51 58-89-9 C202/26/14 09:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/05/14 03:51 57-74-902/26/14 09:100.20 0.20 1
4,4'-DDD ND ug/L 03/05/14 03:51 72-54-802/26/14 09:100.050 0.050 1
4,4'-DDE ND ug/L 03/05/14 03:51 72-55-902/26/14 09:100.050 0.050 1
4,4'-DDT ND ug/L 03/05/14 03:51 50-29-302/26/14 09:100.050 0.050 1
Dieldrin ND ug/L 03/05/14 03:51 60-57-102/26/14 09:100.050 0.050 1
Endosulfan I ND ug/L 03/05/14 03:51 959-98-802/26/14 09:100.050 0.050 1
Endosulfan II ND ug/L 03/05/14 03:51 33213-65-902/26/14 09:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/05/14 03:51 1031-07-802/26/14 09:100.050 0.050 1
Endrin ND ug/L 03/05/14 03:51 72-20-802/26/14 09:100.050 0.050 1
Endrin aldehyde ND ug/L 03/05/14 03:51 7421-93-402/26/14 09:100.050 0.050 1
Endrin ketone ND ug/L 03/05/14 03:51 53494-70-502/26/14 09:100.050 0.050 1
Heptachlor 0.070 ug/L 03/05/14 03:51 76-44-802/26/14 09:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/05/14 03:51 1024-57-302/26/14 09:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/05/14 03:51 118-74-102/26/14 09:100.050 0.050 1
Methoxychlor ND ug/L 03/05/14 03:51 72-43-502/26/14 09:100.15 0.15 1
Mirex ND ug/L 03/05/14 03:51 2385-85-502/26/14 09:100.15 0.15 1
Toxaphene ND ug/L 03/05/14 03:51 8001-35-202/26/14 09:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)44 %03/05/14 03:51 877-09-802/26/14 09:1020-130 1
Decachlorobiphenyl (S)44 %03/05/14 03:51 2051-24-302/26/14 09:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 02/28/14 07:35 7440-36-002/27/14 10:355.0 5.0 1
Arsenic ND ug/L 02/28/14 07:35 7440-38-202/27/14 10:3510.0 5.0 1
Barium 19.2 ug/L 02/28/14 07:35 7440-39-302/27/14 10:355.0 5.0 1
Beryllium ND ug/L 02/28/14 07:35 7440-41-702/27/14 10:351.0 1.0 1
Cadmium ND ug/L 02/28/14 07:35 7440-43-902/27/14 10:351.0 1.0 1
Chromium ND ug/L 02/28/14 07:35 7440-47-302/27/14 10:355.0 5.0 1
Cobalt ND ug/L 02/28/14 07:35 7440-48-402/27/14 10:355.0 5.0 1
Copper ND ug/L 02/28/14 07:35 7440-50-802/27/14 10:355.0 5.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
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Asheville, NC 28804
[phone]
Page 33 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-25 Lab ID:92191006010 Collected:02/25/14 13:35 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 02/28/14 07:35 7439-92-102/27/14 10:355.0 5.0 1
Nickel ND ug/L 02/28/14 07:35 7440-02-002/27/14 10:355.0 5.0 1
Selenium ND ug/L 02/28/14 07:35 7782-49-202/27/14 10:3510.0 10.0 1
Silver ND ug/L 02/28/14 07:35 7440-22-402/27/14 10:355.0 5.0 1
Thallium ND ug/L 02/28/14 07:35 7440-28-002/27/14 10:355.4 5.4 1
Vanadium 9.2 ug/L 02/28/14 07:35 7440-62-202/27/14 10:355.0 5.0 1
Zinc ND ug/L 02/28/14 07:35 7440-66-602/27/14 10:3510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/07/14 16:01 7439-97-602/26/14 20:350.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 10:32 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 10:32 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 10:32 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 10:32 107-05-12.0 1.5 1
Benzene 5.7 ug/L 02/28/14 10:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 10:32 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 10:32 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 10:32 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 10:32 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 10:32 78-93-35.0 0.96 1
Carbon disulfide 1.2J ug/L 02/28/14 10:32 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 10:32 56-23-51.0 0.25 1
Chlorobenzene 0.39J ug/L 02/28/14 10:32 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 10:32 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 10:32 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 10:32 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 10:32 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 10:32 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 10:32 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 10:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 10:32 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 10:32 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 10:32 541-73-11.0 0.24 1
1,4-Dichlorobenzene 2.8 ug/L 02/28/14 10:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 10:32 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 10:32 75-71-81.0 0.21 1
1,1-Dichloroethane 8.7 ug/L 02/28/14 10:32 75-34-31.0 0.32 1
1,2-Dichloroethane 0.87J ug/L 02/28/14 10:32 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 10:32 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 14.1 ug/L 02/28/14 10:32 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 10:32 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 10:32 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 10:32 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 10:32 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Sample:MW-25 Lab ID:92191006010 Collected:02/25/14 13:35 Received:02/25/14 16:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 10:32 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 10:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 10:32 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 10:32 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 10:32 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 10:32 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 10:32 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 10:32 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 10:32 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 10:32 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 10:32 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 10:32 108-10-15.0 0.33 1
Naphthalene 8.9 ug/L 02/28/14 10:32 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 10:32 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 10:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 10:32 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 10:32 79-34-51.0 0.40 1
Tetrachloroethene 1.3 ug/L 02/28/14 10:32 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 10:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 10:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 10:32 79-00-51.0 0.29 1
Trichloroethene 1.9 ug/L 02/28/14 10:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 10:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 10:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 10:32 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 10:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 10:32 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 10:32 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 10:32 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 10:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/28/14 10:32 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 10:32 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/07/14 16:17 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6237
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1146240
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 03/07/14 15:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1146241LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1146242MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191006001
1146243
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 93 75-12592 1 252.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15322
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1146556
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 02/28/14 06:10
Arsenic ug/L ND 10.0 02/28/14 06:10
Barium ug/L ND 5.0 02/28/14 06:10
Beryllium ug/L 0.47J 1.0 02/28/14 06:10
Cadmium ug/L ND 1.0 02/28/14 06:10
Chromium ug/L ND 5.0 02/28/14 06:10
Cobalt ug/L ND 5.0 02/28/14 06:10
Copper ug/L ND 5.0 02/28/14 06:10
Lead ug/L ND 5.0 02/28/14 06:10
Nickel ug/L ND 5.0 02/28/14 06:10
Selenium ug/L ND 10.0 02/28/14 06:10
Silver ug/L 0.83J 5.0 02/28/14 06:10
Thallium ug/L 3.5J 5.4 02/28/14 06:10
Vanadium ug/L 0.73J 5.0 02/28/14 06:10
Zinc ug/L ND 10.0 02/28/14 06:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1146557LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 472500 94 80-120
Arsenic ug/L 454500 91 80-120
Barium ug/L 459500 92 80-120
Beryllium ug/L 453500 91 80-120
Cadmium ug/L 454500 91 80-120
Chromium ug/L 478500 96 80-120
Cobalt ug/L 452500 90 80-120
Copper ug/L 458500 92 80-120
Lead ug/L 445500 89 80-120
Nickel ug/L 458500 92 80-120
Selenium ug/L 449500 90 80-120
Silver ug/L 239250 96 80-120
Thallium ug/L 444500 89 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 446500 89 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1146558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190693010
1146559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12593 1 25500ND471467
Arsenic ug/L 500 90 75-12589 1 25500ND454451
Barium ug/L 500 92 75-12591 1 2550024.4J 484 478
Beryllium ug/L 500 91 75-12590 1 25500ND458453
Cadmium ug/L 500 91 75-12590 1 25500ND455450
Chromium ug/L 500 96 75-12596 1 25500ND482479
Cobalt ug/L 500 91 75-12589 1 25500ND454448
Copper ug/L 500 92 75-12591 2 255007.2J 469 462
Lead ug/L 500 89 75-12588 1 25500ND443439
Nickel ug/L 500 92 75-12591 1 25500ND458453
Selenium ug/L 500 88 75-12588 1 25500ND443439
Silver ug/L 250 96 75-12595 0 25250ND240239
Thallium ug/L 500 89 75-12588 1 25500ND449443
Vanadium ug/L 500 95 75-12593 2 25500ND476468
Zinc ug/L 500 90 75-12589 1 2550030.9 480 475
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25928
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147362
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/28/14 07:55
1,1,1-Trichloroethane ug/L ND 1.0 02/28/14 07:55
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/28/14 07:55
1,1,2-Trichloroethane ug/L ND 1.0 02/28/14 07:55
1,1-Dichloroethane ug/L ND 1.0 02/28/14 07:55
1,1-Dichloroethene ug/L ND 1.0 02/28/14 07:55
1,1-Dichloropropene ug/L ND 1.0 02/28/14 07:55
1,2,3-Trichloropropane ug/L ND 1.0 02/28/14 07:55
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/28/14 07:55
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/28/14 07:55
1,2-Dichlorobenzene ug/L ND 1.0 02/28/14 07:55
1,2-Dichloroethane ug/L ND 1.0 02/28/14 07:55
1,2-Dichloropropane ug/L ND 1.0 02/28/14 07:55
1,3-Dichlorobenzene ug/L ND 1.0 02/28/14 07:55
1,3-Dichloropropane ug/L ND 1.0 02/28/14 07:55
1,4-Dichlorobenzene ug/L ND 1.0 02/28/14 07:55
2,2-Dichloropropane ug/L ND 1.0 02/28/14 07:55
2-Butanone (MEK)ug/L ND 5.0 02/28/14 07:55
2-Hexanone ug/L ND 5.0 02/28/14 07:55
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/28/14 07:55
Acetone ug/L ND 25.0 02/28/14 07:55
Acetonitrile ug/L ND 50.0 02/28/14 07:55
Acrylonitrile ug/L ND 10.0 02/28/14 07:55
Allyl chloride ug/L ND 2.0 02/28/14 07:55
Benzene ug/L ND 1.0 02/28/14 07:55
Bromochloromethane ug/L ND 1.0 02/28/14 07:55
Bromodichloromethane ug/L ND 1.0 02/28/14 07:55
Bromoform ug/L ND 1.0 02/28/14 07:55
Bromomethane ug/L ND 2.0 02/28/14 07:55
Carbon disulfide ug/L ND 2.0 02/28/14 07:55
Carbon tetrachloride ug/L ND 1.0 02/28/14 07:55
Chlorobenzene ug/L ND 1.0 02/28/14 07:55
Chloroethane ug/L ND 1.0 02/28/14 07:55
Chloroform ug/L ND 1.0 02/28/14 07:55
Chloromethane ug/L ND 1.0 02/28/14 07:55
Chloroprene ug/L ND 5.0 02/28/14 07:55
cis-1,2-Dichloroethene ug/L ND 1.0 02/28/14 07:55
cis-1,3-Dichloropropene ug/L ND 1.0 02/28/14 07:55
Dibromochloromethane ug/L ND 1.0 02/28/14 07:55
Dibromomethane ug/L ND 1.0 02/28/14 07:55
Dichlorodifluoromethane ug/L ND 1.0 02/28/14 07:55
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147362
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Matrix:Water
Analyzed
Ethyl methacrylate ug/L ND 1.0 02/28/14 07:55
Ethylbenzene ug/L ND 1.0 02/28/14 07:55
Iodomethane ug/L ND 5.0 02/28/14 07:55
Isobutanol ug/L ND 100 02/28/14 07:55
m&p-Xylene ug/L ND 2.0 02/28/14 07:55
Methacrylonitrile ug/L ND 10.0 02/28/14 07:55
Methyl methacrylate ug/L ND 2.0 02/28/14 07:55
Methylene Chloride ug/L ND 1.0 02/28/14 07:55
Naphthalene ug/L ND 1.0 02/28/14 07:55
o-Xylene ug/L ND 1.0 02/28/14 07:55
Propionitrile ug/L ND 20.0 02/28/14 07:55
Styrene ug/L ND 1.0 02/28/14 07:55
Tetrachloroethene ug/L ND 1.0 02/28/14 07:55
Toluene ug/L ND 1.0 02/28/14 07:55
trans-1,2-Dichloroethene ug/L ND 1.0 02/28/14 07:55
trans-1,3-Dichloropropene ug/L ND 1.0 02/28/14 07:55
trans-1,4-Dichloro-2-butene ug/L ND 1.0 02/28/14 07:55
Trichloroethene ug/L ND 1.0 02/28/14 07:55
Trichlorofluoromethane ug/L ND 1.0 02/28/14 07:55
Vinyl acetate ug/L ND 2.0 02/28/14 07:55
Vinyl chloride ug/L ND 1.0 02/28/14 07:55
Xylene (Total)ug/L ND 2.0 02/28/14 07:55
1,2-Dichloroethane-d4 (S)%102 70-130 02/28/14 07:55
4-Bromofluorobenzene (S)%100 70-130 02/28/14 07:55
Toluene-d8 (S)%97 70-130 02/28/14 07:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147363LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 70-130
1,1,1-Trichloroethane ug/L 47.550 95 70-130
1,1,2,2-Tetrachloroethane ug/L 50.350 101 70-130
1,1,2-Trichloroethane ug/L 48.450 97 70-130
1,1-Dichloroethane ug/L 41.850 84 70-130
1,1-Dichloroethene ug/L 39.450 79 70-132
1,1-Dichloropropene ug/L 45.250 90 70-130
1,2,3-Trichloropropane ug/L 53.450 107 70-130
1,2-Dibromo-3-chloropropane ug/L 59.450 119 70-130
1,2-Dibromoethane (EDB)ug/L 50.150 100 70-130
1,2-Dichlorobenzene ug/L 50.450 101 70-130
1,2-Dichloroethane ug/L 44.150 88 70-130
1,2-Dichloropropane ug/L 44.950 90 70-130
1,3-Dichlorobenzene ug/L 49.050 98 70-130
1,3-Dichloropropane ug/L 48.150 96 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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Page 40 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147363LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 50.050 100 70-130
2,2-Dichloropropane ug/L 40.950 82 58-145
2-Butanone (MEK)ug/L 83.6100 84 70-145
2-Hexanone ug/L 94.6100 95 70-144
4-Methyl-2-pentanone (MIBK)ug/L 91.1100 91 70-140
Acetone ug/L 83.1100 83 50-175
Acetonitrile ug/L 376500 75 70-130
Acrylonitrile ug/L 192250 77 70-143
Allyl chloride ug/L 35.850 72 70-130
Benzene ug/L 49.750 99 70-130
Bromochloromethane ug/L 42.450 85 70-130
Bromodichloromethane ug/L 48.450 97 70-130
Bromoform ug/L 52.450 105 70-130
Bromomethane ug/L 45.950 92 54-130
Carbon disulfide ug/L 40.850 82 70-131
Carbon tetrachloride ug/L 54.550 109 70-132
Chlorobenzene ug/L 49.950 100 70-130
Chloroethane ug/L 38.450 77 64-134
Chloroform ug/L 45.450 91 70-130
Chloromethane ug/L 36.250 72 64-130
Chloroprene ug/L 44.250 88 70-130
cis-1,2-Dichloroethene ug/L 41.650 83 70-131
cis-1,3-Dichloropropene ug/L 44.550 89 70-130
Dibromochloromethane ug/L 49.950 100 70-130
Dibromomethane ug/L 48.550 97 70-131
Dichlorodifluoromethane ug/L 44.850 90 56-130
Ethyl methacrylate ug/L 45.350 91 70-130
Ethylbenzene ug/L 52.650 105 70-130
Iodomethane ug/L 80.3100 80 49-180
Isobutanol ug/L 8101000 81 70-130
m&p-Xylene ug/L 108100 108 70-130
Methacrylonitrile ug/L 409500 82 70-130
Methyl methacrylate ug/L 47.850 96 70-130
Methylene Chloride ug/L 37.250 74 63-130
Naphthalene ug/L 67.750 135 70-138
o-Xylene ug/L 51.450 103 70-130
Propionitrile ug/L 416500 83 70-130
Styrene ug/L 50.750 101 70-130
Tetrachloroethene ug/L 55.650 111 70-130
Toluene ug/L 50.750 101 70-130
trans-1,2-Dichloroethene ug/L 40.650 81 70-130
trans-1,3-Dichloropropene ug/L 46.850 94 70-132
trans-1,4-Dichloro-2-butene ug/L 48.950 98 70-141
Trichloroethene ug/L 50.450 101 70-130
Trichlorofluoromethane ug/L 44.850 90 62-133
Vinyl acetate ug/L 75.5100 76 66-157
Vinyl chloride ug/L 40.150 80 69-130
Xylene (Total)ug/L 159150 106 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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[phone]
Page 41 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147363LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147364MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191006003
1147365
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 104 70-166106 2 3050ND52.1 53.0
Benzene ug/L 50 108 70-148112 3 30501.3 55.5 57.2
Chlorobenzene ug/L 50 107 70-146110 3 30501.5 55.1 56.7
Toluene ug/L 50 103 70-155107 4 3050ND51.8 53.6
Trichloroethene ug/L 50 113 69-151115 3 3050ND56.5 57.9
1,2-Dichloroethane-d4 (S)%96 70-13095
4-Bromofluorobenzene (S)%99 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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Page 42 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26118
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1145343
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 03/05/14 01:48
4,4'-DDE ug/L ND 0.050 03/05/14 01:48
4,4'-DDT ug/L ND 0.050 03/05/14 01:48
Aldrin ug/L ND 0.050 03/05/14 01:48
alpha-BHC ug/L ND 0.050 03/05/14 01:48
beta-BHC ug/L ND 0.050 03/05/14 01:48
Chlordane (Technical)ug/L ND 0.20 03/05/14 01:48
delta-BHC ug/L ND 0.050 03/05/14 01:48
Dieldrin ug/L ND 0.050 03/05/14 01:48
Endosulfan I ug/L ND 0.050 03/05/14 01:48
Endosulfan II ug/L ND 0.050 03/05/14 01:48
Endosulfan sulfate ug/L ND 0.050 03/05/14 01:48
Endrin ug/L ND 0.050 03/05/14 01:48
Endrin aldehyde ug/L ND 0.050 03/05/14 01:48
Endrin ketone ug/L ND 0.050 03/05/14 01:48
gamma-BHC (Lindane)ug/L ND 0.050 03/05/14 01:48
Heptachlor ug/L ND 0.050 03/05/14 01:48
Heptachlor epoxide ug/L ND 0.050 03/05/14 01:48
Hexachlorobenzene ug/L ND 0.050 03/05/14 01:48
Methoxychlor ug/L ND 0.15 03/05/14 01:48
Mirex ug/L ND 0.15 03/05/14 01:48
Toxaphene ug/L ND 0.20 03/05/14 01:48
Decachlorobiphenyl (S)%74 20-130 03/05/14 01:48
Tetrachloro-m-xylene (S)%74 20-130 03/05/14 01:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1145344LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.22.25 89 20-150
4,4'-DDE ug/L 0.21.25 85 20-150
4,4'-DDT ug/L 0.22.25 88 20-150
Aldrin ug/L 0.16.25 66 20-150
alpha-BHC ug/L 0.19.25 78 20-150
beta-BHC ug/L 0.20.25 81 20-150
delta-BHC ug/L 0.21.25 84 20-150
Dieldrin ug/L 0.20.25 81 20-150
Endosulfan I ug/L 0.21.25 86 20-150
Endosulfan II ug/L 0.21.25 85 20-150
Endosulfan sulfate ug/L 0.22.25 87 20-150
Endrin ug/L 0.24.25 97 20-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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[phone]
Page 43 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1145344LABORATORY CONTROL SAMPLE:
LCSSpike
Endrin aldehyde ug/L 0.20.25 80 20-150
Endrin ketone ug/L 0.22.25 89 20-150
gamma-BHC (Lindane)ug/L 0.20.25 79 20-150
Heptachlor ug/L 0.17.25 70 20-150
Heptachlor epoxide ug/L 0.21.25 84 20-150
Hexachlorobenzene ug/L 0.18.25 72 20-150
Methoxychlor ug/L 0.66.74 89 20-150
Mirex ug/L 0.62.74 84 20-150
Decachlorobiphenyl (S)%77 20-130
Tetrachloro-m-xylene (S)%72 20-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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Asheville, NC 28804
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/18273
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1152329
Associated Lab Samples:92191006001, 92191006002, 92191006003, 92191006004, 92191006005, 92191006006, 92191006007,
92191006008, 92191006009, 92191006010
Matrix:Water
Analyzed
Cyanide mg/L ND 0.0050 03/07/14 15:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1152330LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.11.1 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1152331MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191656001
1152332
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 108 75-125107 1 20.10.0097 0.12 0.12
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1152333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191006008
1152334
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 119 75-125118 1 20.1ND 0.12 0.12
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
Pace Analytical Services, Inc.
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[phone]
Page 45 of 50
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Relative percent difference between results from each column was greater than 40%. The lower of the two results was
reported.C2
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
[phone]
Page 46 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92191006001 FLD/MW-11
92191006002 FLD/MW-13
92191006003 FLD/MW-14
92191006004 FLD/MW-14D
92191006005 FLD/MW-15
92191006006 FLD/MW-16
92191006007 FLD/MW-16D
92191006008 FLD/MW-17
92191006009 FLD/MW-22
92191006010 FLD/MW-25
92191006001 OEXT/26118 GCSV/16828MW-11 EPA 3510 EPA 8081
92191006002 OEXT/26118 GCSV/16828MW-13 EPA 3510 EPA 8081
92191006003 OEXT/26118 GCSV/16828MW-14 EPA 3510 EPA 8081
92191006004 OEXT/26118 GCSV/16828MW-14D EPA 3510 EPA 8081
92191006005 OEXT/26118 GCSV/16828MW-15 EPA 3510 EPA 8081
92191006006 OEXT/26118 GCSV/16828MW-16 EPA 3510 EPA 8081
92191006007 OEXT/26118 GCSV/16828MW-16D EPA 3510 EPA 8081
92191006008 OEXT/26118 GCSV/16828MW-17 EPA 3510 EPA 8081
92191006009 OEXT/26118 GCSV/16828MW-22 EPA 3510 EPA 8081
92191006010 OEXT/26118 GCSV/16828MW-25 EPA 3510 EPA 8081
92191006001 MPRP/15322 ICP/13904MW-11 EPA 3010 EPA 6010
92191006002 MPRP/15322 ICP/13904MW-13 EPA 3010 EPA 6010
92191006003 MPRP/15322 ICP/13904MW-14 EPA 3010 EPA 6010
92191006004 MPRP/15322 ICP/13904MW-14D EPA 3010 EPA 6010
92191006005 MPRP/15322 ICP/13904MW-15 EPA 3010 EPA 6010
92191006006 MPRP/15322 ICP/13904MW-16 EPA 3010 EPA 6010
92191006007 MPRP/15322 ICP/13904MW-16D EPA 3010 EPA 6010
92191006008 MPRP/15322 ICP/13904MW-17 EPA 3010 EPA 6010
92191006009 MPRP/15322 ICP/13904MW-22 EPA 3010 EPA 6010
92191006010 MPRP/15322 ICP/13904MW-25 EPA 3010 EPA 6010
92191006001 MERP/6237 MERC/6018MW-11 EPA 7470 EPA 7470
92191006002 MERP/6237 MERC/6018MW-13 EPA 7470 EPA 7470
92191006003 MERP/6237 MERC/6018MW-14 EPA 7470 EPA 7470
92191006004 MERP/6237 MERC/6018MW-14D EPA 7470 EPA 7470
92191006005 MERP/6237 MERC/6018MW-15 EPA 7470 EPA 7470
92191006006 MERP/6237 MERC/6018MW-16 EPA 7470 EPA 7470
92191006007 MERP/6237 MERC/6018MW-16D EPA 7470 EPA 7470
92191006008 MERP/6237 MERC/6018MW-17 EPA 7470 EPA 7470
92191006009 MERP/6237 MERC/6018MW-22 EPA 7470 EPA 7470
92191006010 MERP/6237 MERC/6018MW-25 EPA 7470 EPA 7470
92191006001 MSV/25928MW-11 EPA 8260
92191006002 MSV/25928MW-13 EPA 8260
92191006003 MSV/25928MW-14 EPA 8260
92191006004 MSV/25928MW-14D EPA 8260
92191006005 MSV/25928MW-15 EPA 8260
92191006006 MSV/25928MW-16 EPA 8260
92191006007 MSV/25928MW-16D EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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Asheville, NC 28804
[phone]
Page 47 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92191006
FRANCIS FARM LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92191006008 MSV/25928MW-17 EPA 8260
92191006009 MSV/25928MW-22 EPA 8260
92191006010 MSV/25928MW-25 EPA 8260
92191006001 WETA/18273MW-11 SM 4500-CN-E
92191006002 WETA/18273MW-13 SM 4500-CN-E
92191006003 WETA/18273MW-14 SM 4500-CN-E
92191006004 WETA/18273MW-14D SM 4500-CN-E
92191006005 WETA/18273MW-15 SM 4500-CN-E
92191006006 WETA/18273MW-16 SM 4500-CN-E
92191006007 WETA/18273MW-16D SM 4500-CN-E
92191006008 WETA/18273MW-17 SM 4500-CN-E
92191006009 WETA/18273MW-22 SM 4500-CN-E
92191006010 WETA/18273MW-25 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:51 PM
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[phone]
Page 48 of 50
Page 49 of 50
Page 50 of 50
#=CL#
March 19, 2014
LIMS USE: FR - STEPHEN KING
LIMS OBJECT ID: 92191140
92191140
Project:
Pace Project No.:
RE:
Mr. Stephen King
Haywood Co. Solid Waste
278 Recycle Rd.
Clyde, NC 28721
FRANCIS FARM LF
Dear Mr. King:
Enclosed are the analytical results for sample(s) received by the laboratory on February 26, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
cc:Andy Alexander, BLE
Mr. Stephen King, Haywood Co. Solid Waste
REPORT OF LABORATORY ANALYSIS
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Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 35
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Lab ID Sample ID Matrix Date Collected Date Received
92191140001 MW-2A Water 02/26/14 10:45 02/26/14 13:30
92191140002 MW-3A Water 02/26/14 11:15 02/26/14 13:30
92191140003 MW-5 Water 02/26/14 11:55 02/26/14 13:30
92191140004 MW-12 Water 02/26/14 12:25 02/26/14 13:30
92191140005 TRIP BLANK Water 02/20/14 00:00 02/26/14 13:30
92191140006 EQUIP BLK Water 02/20/14 00:00 02/26/14 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92191140001 MW-2A EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191140002 MW-3A EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191140003 MW-5 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191140004 MW-12 EPA 8081 24 PASI-CNU1
EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
SM 4500-CN-E 1 PASI-AJDA
92191140005 TRIP BLANK EPA 8260 66 PASI-CMCK
92191140006 EQUIP BLK EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AMTS
EPA 8260 66 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-2A Lab ID:92191140001 Collected:02/26/14 10:45 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 15:101
Collected Date 02/26/14 03/12/14 15:101
Collected Time 10:45 03/12/14 15:101
Field pH 6.2 Std. Units 03/12/14 15:100.10 0.10 1
Field Temperature 12.5 deg C 03/12/14 15:100.50 0.50 1
Field Specific Conductance 514 umhos/cm 03/12/14 15:101.0 1.0 1
Turbidity 1.75 NTU 03/12/14 15:101.0 1.0 1
Odor O&G 03/12/14 15:101
Appearance CLEAR 03/12/14 15:101
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/08/14 23:45 309-00-203/02/14 16:100.050 0.050 1
alpha-BHC ND ug/L 03/08/14 23:45 319-84-603/02/14 16:100.050 0.050 1
beta-BHC ND ug/L 03/08/14 23:45 319-85-703/02/14 16:100.050 0.050 1
delta-BHC ND ug/L 03/08/14 23:45 319-86-803/02/14 16:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/08/14 23:45 58-89-903/02/14 16:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/08/14 23:45 57-74-903/02/14 16:100.20 0.20 1
4,4'-DDD ND ug/L 03/08/14 23:45 72-54-803/02/14 16:100.050 0.050 1
4,4'-DDE ND ug/L 03/08/14 23:45 72-55-903/02/14 16:100.050 0.050 1
4,4'-DDT ND ug/L 03/08/14 23:45 50-29-303/02/14 16:100.050 0.050 1
Dieldrin ND ug/L 03/08/14 23:45 60-57-103/02/14 16:100.050 0.050 1
Endosulfan I ND ug/L 03/08/14 23:45 959-98-803/02/14 16:100.050 0.050 1
Endosulfan II ND ug/L 03/08/14 23:45 33213-65-903/02/14 16:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/08/14 23:45 1031-07-803/02/14 16:100.050 0.050 1
Endrin ND ug/L 03/08/14 23:45 72-20-803/02/14 16:100.050 0.050 1
Endrin aldehyde ND ug/L 03/08/14 23:45 7421-93-403/02/14 16:100.050 0.050 1
Endrin ketone ND ug/L 03/08/14 23:45 53494-70-503/02/14 16:100.050 0.050 1
Heptachlor ND ug/L 03/08/14 23:45 76-44-803/02/14 16:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/08/14 23:45 1024-57-303/02/14 16:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/08/14 23:45 118-74-103/02/14 16:100.050 0.050 1
Methoxychlor ND ug/L 03/08/14 23:45 72-43-503/02/14 16:100.15 0.15 1
Mirex ND ug/L 03/08/14 23:45 2385-85-503/02/14 16:100.15 0.15 1
Toxaphene ND ug/L 03/08/14 23:45 8001-35-203/02/14 16:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)74 %03/08/14 23:45 877-09-803/02/14 16:1020-130 1
Decachlorobiphenyl (S)101 %03/08/14 23:45 2051-24-303/02/14 16:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 03/01/14 02:02 7440-36-002/28/14 09:055.0 5.0 1
Arsenic 9.3J ug/L 03/01/14 02:02 7440-38-202/28/14 09:0510.0 5.0 1
Barium 253 ug/L 03/01/14 02:02 7440-39-302/28/14 09:055.0 5.0 1
Beryllium ND ug/L 03/01/14 02:02 7440-41-702/28/14 09:051.0 1.0 1
Cadmium ND ug/L 03/01/14 02:02 7440-43-902/28/14 09:051.0 1.0 1
Chromium ND ug/L 03/01/14 02:02 7440-47-302/28/14 09:055.0 5.0 1
Cobalt 36.6 ug/L 03/01/14 02:02 7440-48-402/28/14 09:055.0 5.0 1
Copper ND ug/L 03/01/14 02:02 7440-50-802/28/14 09:055.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-2A Lab ID:92191140001 Collected:02/26/14 10:45 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 03/01/14 02:02 7439-92-102/28/14 09:055.0 5.0 1
Nickel ND ug/L 03/01/14 02:02 7440-02-002/28/14 09:055.0 5.0 1
Selenium ND ug/L 03/01/14 02:02 7782-49-202/28/14 09:0510.0 10.0 1
Silver ND ug/L 03/01/14 02:02 7440-22-402/28/14 09:055.0 5.0 1
Thallium ND ug/L 03/01/14 02:02 7440-28-002/28/14 09:055.4 5.4 1
Vanadium ND ug/L 03/01/14 02:02 7440-62-202/28/14 09:055.0 5.0 1
Zinc ND ug/L 03/01/14 02:02 7440-66-602/28/14 09:0510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/04/14 16:08 7439-97-602/27/14 18:150.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 10:47 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 10:47 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 10:47 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 10:47 107-05-12.0 1.5 1
Benzene 0.86J ug/L 02/28/14 10:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 10:47 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 10:47 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 10:47 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 10:47 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 10:47 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 10:47 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 10:47 56-23-51.0 0.25 1
Chlorobenzene 0.29J ug/L 02/28/14 10:47 108-90-71.0 0.23 1
Chloroethane 0.94J ug/L 02/28/14 10:47 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 10:47 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 10:47 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 10:47 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 10:47 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 10:47 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 10:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 10:47 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.43J ug/L 02/28/14 10:47 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 10:47 541-73-11.0 0.24 1
1,4-Dichlorobenzene 4.0 ug/L 02/28/14 10:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 10:47 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 10:47 75-71-81.0 0.21 1
1,1-Dichloroethane 0.46J ug/L 02/28/14 10:47 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 10:47 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 10:47 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 2.8 ug/L 02/28/14 10:47 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 10:47 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 10:47 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 10:47 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 10:47 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-2A Lab ID:92191140001 Collected:02/26/14 10:45 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 10:47 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 10:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 10:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 10:47 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 10:47 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 10:47 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 10:47 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 10:47 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 10:47 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 10:47 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 10:47 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 10:47 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 10:47 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 10:47 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 10:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 10:47 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 10:47 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 10:47 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 10:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 10:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 10:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 10:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 10:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 10:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 10:47 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 10:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 10:47 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 10:47 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 10:47 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %02/28/14 10:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 10:47 17060-07-070-130 1
Toluene-d8 (S)97 %02/28/14 10:47 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/10/14 13:35 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-3A Lab ID:92191140002 Collected:02/26/14 11:15 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 15:121
Collected Date 02/26/14 03/12/14 15:121
Collected Time 11:15 03/12/14 15:121
Field pH 6.2 Std. Units 03/12/14 15:120.10 0.10 1
Field Temperature 12.3 deg C 03/12/14 15:120.50 0.50 1
Field Specific Conductance 299 umhos/cm 03/12/14 15:121.0 1.0 1
Turbidity 1.25 NTU 03/12/14 15:121.0 1.0 1
Odor O&G 03/12/14 15:121
Appearance CLEAR 03/12/14 15:121
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/09/14 00:03 309-00-203/02/14 16:100.050 0.050 1
alpha-BHC ND ug/L 03/09/14 00:03 319-84-603/02/14 16:100.050 0.050 1
beta-BHC ND ug/L 03/09/14 00:03 319-85-703/02/14 16:100.050 0.050 1
delta-BHC ND ug/L 03/09/14 00:03 319-86-803/02/14 16:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/09/14 00:03 58-89-903/02/14 16:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/09/14 00:03 57-74-903/02/14 16:100.20 0.20 1
4,4'-DDD ND ug/L 03/09/14 00:03 72-54-803/02/14 16:100.050 0.050 1
4,4'-DDE ND ug/L 03/09/14 00:03 72-55-903/02/14 16:100.050 0.050 1
4,4'-DDT ND ug/L 03/09/14 00:03 50-29-303/02/14 16:100.050 0.050 1
Dieldrin ND ug/L 03/09/14 00:03 60-57-103/02/14 16:100.050 0.050 1
Endosulfan I ND ug/L 03/09/14 00:03 959-98-803/02/14 16:100.050 0.050 1
Endosulfan II ND ug/L 03/09/14 00:03 33213-65-903/02/14 16:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/09/14 00:03 1031-07-803/02/14 16:100.050 0.050 1
Endrin ND ug/L 03/09/14 00:03 72-20-803/02/14 16:100.050 0.050 1
Endrin aldehyde ND ug/L 03/09/14 00:03 7421-93-403/02/14 16:100.050 0.050 1
Endrin ketone ND ug/L 03/09/14 00:03 53494-70-503/02/14 16:100.050 0.050 1
Heptachlor ND ug/L 03/09/14 00:03 76-44-803/02/14 16:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/09/14 00:03 1024-57-303/02/14 16:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/09/14 00:03 118-74-103/02/14 16:100.050 0.050 1
Methoxychlor ND ug/L 03/09/14 00:03 72-43-503/02/14 16:100.15 0.15 1
Mirex ND ug/L 03/09/14 00:03 2385-85-503/02/14 16:100.15 0.15 1
Toxaphene ND ug/L 03/09/14 00:03 8001-35-203/02/14 16:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)64 %03/09/14 00:03 877-09-803/02/14 16:1020-130 1
Decachlorobiphenyl (S)86 %03/09/14 00:03 2051-24-303/02/14 16:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 03/01/14 02:06 7440-36-002/28/14 09:055.0 5.0 1
Arsenic ND ug/L 03/01/14 02:06 7440-38-202/28/14 09:0510.0 5.0 1
Barium 159 ug/L 03/01/14 02:06 7440-39-302/28/14 09:055.0 5.0 1
Beryllium ND ug/L 03/01/14 02:06 7440-41-702/28/14 09:051.0 1.0 1
Cadmium ND ug/L 03/01/14 02:06 7440-43-902/28/14 09:051.0 1.0 1
Chromium ND ug/L 03/01/14 02:06 7440-47-302/28/14 09:055.0 5.0 1
Cobalt 48.8 ug/L 03/01/14 02:06 7440-48-402/28/14 09:055.0 5.0 1
Copper ND ug/L 03/01/14 02:06 7440-50-802/28/14 09:055.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-3A Lab ID:92191140002 Collected:02/26/14 11:15 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 03/01/14 02:06 7439-92-102/28/14 09:055.0 5.0 1
Nickel 6.2 ug/L 03/01/14 02:06 7440-02-002/28/14 09:055.0 5.0 1
Selenium ND ug/L 03/01/14 02:06 7782-49-202/28/14 09:0510.0 10.0 1
Silver ND ug/L 03/01/14 02:06 7440-22-402/28/14 09:055.0 5.0 1
Thallium ND ug/L 03/01/14 02:06 7440-28-002/28/14 09:055.4 5.4 1
Vanadium ND ug/L 03/01/14 02:06 7440-62-202/28/14 09:055.0 5.0 1
Zinc 19.2 ug/L 03/01/14 02:06 7440-66-602/28/14 09:0510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/04/14 16:10 7439-97-602/27/14 18:150.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 11:03 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 11:03 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 11:03 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 11:03 107-05-12.0 1.5 1
Benzene 0.34J ug/L 02/28/14 11:03 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 11:03 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 11:03 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 11:03 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 11:03 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 11:03 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 11:03 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 11:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 11:03 108-90-71.0 0.23 1
Chloroethane 1.1 ug/L 02/28/14 11:03 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 11:03 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 11:03 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 11:03 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 11:03 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 11:03 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 11:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 11:03 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 11:03 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 11:03 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 11:03 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 11:03 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 11:03 75-71-81.0 0.21 1
1,1-Dichloroethane 3.2 ug/L 02/28/14 11:03 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 11:03 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 11:03 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.59J ug/L 02/28/14 11:03 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 11:03 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 11:03 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 11:03 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 11:03 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
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[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-3A Lab ID:92191140002 Collected:02/26/14 11:15 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 11:03 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 11:03 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 11:03 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 11:03 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 11:03 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 11:03 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 11:03 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 11:03 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 11:03 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 11:03 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 11:03 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 11:03 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 11:03 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 11:03 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 11:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 11:03 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 11:03 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 11:03 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 11:03 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 11:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 11:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 11:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 11:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 11:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 11:03 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 11:03 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 11:03 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 11:03 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 11:03 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/28/14 11:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/28/14 11:03 17060-07-070-130 1
Toluene-d8 (S)97 %02/28/14 11:03 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide 0.0084 mg/L 03/10/14 13:39 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
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2225 Riverside Dr.
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Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-5 Lab ID:92191140003 Collected:02/26/14 11:55 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 15:131
Collected Date 02/26/14 03/12/14 15:131
Collected Time 11:55 03/12/14 15:131
Field pH 5.8 Std. Units 03/12/14 15:130.10 0.10 1
Field Temperature 12.5 deg C 03/12/14 15:130.50 0.50 1
Field Specific Conductance 258 umhos/cm 03/12/14 15:131.0 1.0 1
Turbidity 1.42 NTU 03/12/14 15:131.0 1.0 1
Odor O&G 03/12/14 15:131
Appearance CLEAR 03/12/14 15:131
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/09/14 00:20 309-00-203/02/14 16:100.050 0.050 1
alpha-BHC ND ug/L 03/09/14 00:20 319-84-603/02/14 16:100.050 0.050 1
beta-BHC ND ug/L 03/09/14 00:20 319-85-703/02/14 16:100.050 0.050 1
delta-BHC ND ug/L 03/09/14 00:20 319-86-803/02/14 16:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/09/14 00:20 58-89-903/02/14 16:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/09/14 00:20 57-74-903/02/14 16:100.20 0.20 1
4,4'-DDD ND ug/L 03/09/14 00:20 72-54-803/02/14 16:100.050 0.050 1
4,4'-DDE ND ug/L 03/09/14 00:20 72-55-903/02/14 16:100.050 0.050 1
4,4'-DDT ND ug/L 03/09/14 00:20 50-29-303/02/14 16:100.050 0.050 1
Dieldrin ND ug/L 03/09/14 00:20 60-57-103/02/14 16:100.050 0.050 1
Endosulfan I ND ug/L 03/09/14 00:20 959-98-803/02/14 16:100.050 0.050 1
Endosulfan II ND ug/L 03/09/14 00:20 33213-65-903/02/14 16:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/09/14 00:20 1031-07-803/02/14 16:100.050 0.050 1
Endrin ND ug/L 03/09/14 00:20 72-20-803/02/14 16:100.050 0.050 1
Endrin aldehyde ND ug/L 03/09/14 00:20 7421-93-403/02/14 16:100.050 0.050 1
Endrin ketone ND ug/L 03/09/14 00:20 53494-70-503/02/14 16:100.050 0.050 1
Heptachlor ND ug/L 03/09/14 00:20 76-44-803/02/14 16:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/09/14 00:20 1024-57-303/02/14 16:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/09/14 00:20 118-74-103/02/14 16:100.050 0.050 1
Methoxychlor ND ug/L 03/09/14 00:20 72-43-503/02/14 16:100.15 0.15 1
Mirex ND ug/L 03/09/14 00:20 2385-85-503/02/14 16:100.15 0.15 1
Toxaphene ND ug/L 03/09/14 00:20 8001-35-203/02/14 16:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)65 %03/09/14 00:20 877-09-803/02/14 16:1020-130 1
Decachlorobiphenyl (S)68 %03/09/14 00:20 2051-24-303/02/14 16:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 03/01/14 02:19 7440-36-002/28/14 09:055.0 5.0 1
Arsenic ND ug/L 03/01/14 02:19 7440-38-202/28/14 09:0510.0 5.0 1
Barium 210 ug/L 03/01/14 02:19 7440-39-302/28/14 09:055.0 5.0 1
Beryllium ND ug/L 03/01/14 02:19 7440-41-702/28/14 09:051.0 1.0 1
Cadmium ND ug/L 03/01/14 02:19 7440-43-902/28/14 09:051.0 1.0 1
Chromium ND ug/L 03/01/14 02:19 7440-47-302/28/14 09:055.0 5.0 1
Cobalt 6.9 ug/L 03/01/14 02:19 7440-48-402/28/14 09:055.0 5.0 1
Copper ND ug/L 03/01/14 02:19 7440-50-802/28/14 09:055.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-5 Lab ID:92191140003 Collected:02/26/14 11:55 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 03/01/14 02:19 7439-92-102/28/14 09:055.0 5.0 1
Nickel ND ug/L 03/01/14 02:19 7440-02-002/28/14 09:055.0 5.0 1
Selenium ND ug/L 03/01/14 02:19 7782-49-202/28/14 09:0510.0 10.0 1
Silver ND ug/L 03/01/14 02:19 7440-22-402/28/14 09:055.0 5.0 1
Thallium ND ug/L 03/01/14 02:19 7440-28-002/28/14 09:055.4 5.4 1
Vanadium ND ug/L 03/01/14 02:19 7440-62-202/28/14 09:055.0 5.0 1
Zinc ND ug/L 03/01/14 02:19 7440-66-602/28/14 09:0510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/04/14 16:13 7439-97-602/27/14 18:150.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 11:19 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 11:19 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 11:19 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 11:19 107-05-12.0 1.5 1
Benzene 4.4 ug/L 02/28/14 11:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 11:19 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 11:19 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 11:19 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 11:19 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 11:19 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 11:19 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 11:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 11:19 108-90-71.0 0.23 1
Chloroethane 1.4 ug/L 02/28/14 11:19 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 11:19 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 11:19 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 11:19 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 11:19 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 11:19 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 11:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 11:19 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 11:19 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 11:19 541-73-11.0 0.24 1
1,4-Dichlorobenzene 1.4 ug/L 02/28/14 11:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 11:19 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 11:19 75-71-81.0 0.21 1
1,1-Dichloroethane 6.8 ug/L 02/28/14 11:19 75-34-31.0 0.32 1
1,2-Dichloroethane 0.25J ug/L 02/28/14 11:19 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 11:19 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 10.2 ug/L 02/28/14 11:19 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 11:19 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 11:19 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 11:19 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 11:19 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-5 Lab ID:92191140003 Collected:02/26/14 11:55 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 11:19 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 11:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 11:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 11:19 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 11:19 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 11:19 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 11:19 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 11:19 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 11:19 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 11:19 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 11:19 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 11:19 108-10-15.0 0.33 1
Naphthalene 0.80J ug/L 02/28/14 11:19 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 11:19 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 11:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 11:19 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 11:19 79-34-51.0 0.40 1
Tetrachloroethene 5.1 ug/L 02/28/14 11:19 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 11:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 11:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 11:19 79-00-51.0 0.29 1
Trichloroethene 4.1 ug/L 02/28/14 11:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 11:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 11:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 11:19 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 11:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 11:19 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 11:19 179601-23-12.0 0.66 1
o-Xylene 0.52J ug/L 02/28/14 11:19 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 11:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/28/14 11:19 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 11:19 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/10/14 13:42 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-12 Lab ID:92191140004 Collected:02/26/14 12:25 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Monitoring Well Data Analytical Method:
Collected By MPS 03/12/14 15:151
Collected Date 02/26/14 03/12/14 15:151
Collected Time 12:25 03/12/14 15:151
Field pH 6.6 Std. Units 03/12/14 15:150.10 0.10 1
Field Temperature 12.0 deg C 03/12/14 15:150.50 0.50 1
Field Specific Conductance 107 umhos/cm 03/12/14 15:151.0 1.0 1
Turbidity 9.20 NTU 03/12/14 15:151.0 1.0 1
Odor O&G 03/12/14 15:151
Appearance CLEAR 03/12/14 15:151
8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510
Aldrin ND ug/L 03/09/14 00:38 309-00-203/02/14 16:100.050 0.050 1
alpha-BHC ND ug/L 03/09/14 00:38 319-84-603/02/14 16:100.050 0.050 1
beta-BHC ND ug/L 03/09/14 00:38 319-85-703/02/14 16:100.050 0.050 1
delta-BHC ND ug/L 03/09/14 00:38 319-86-803/02/14 16:100.050 0.050 1
gamma-BHC (Lindane)ND ug/L 03/09/14 00:38 58-89-903/02/14 16:100.050 0.050 1
Chlordane (Technical)ND ug/L 03/09/14 00:38 57-74-903/02/14 16:100.20 0.20 1
4,4'-DDD ND ug/L 03/09/14 00:38 72-54-803/02/14 16:100.050 0.050 1
4,4'-DDE ND ug/L 03/09/14 00:38 72-55-903/02/14 16:100.050 0.050 1
4,4'-DDT ND ug/L 03/09/14 00:38 50-29-303/02/14 16:100.050 0.050 1
Dieldrin ND ug/L 03/09/14 00:38 60-57-103/02/14 16:100.050 0.050 1
Endosulfan I ND ug/L 03/09/14 00:38 959-98-803/02/14 16:100.050 0.050 1
Endosulfan II ND ug/L 03/09/14 00:38 33213-65-903/02/14 16:100.050 0.050 1
Endosulfan sulfate ND ug/L 03/09/14 00:38 1031-07-803/02/14 16:100.050 0.050 1
Endrin ND ug/L 03/09/14 00:38 72-20-803/02/14 16:100.050 0.050 1
Endrin aldehyde ND ug/L 03/09/14 00:38 7421-93-403/02/14 16:100.050 0.050 1
Endrin ketone ND ug/L 03/09/14 00:38 53494-70-503/02/14 16:100.050 0.050 1
Heptachlor ND ug/L 03/09/14 00:38 76-44-803/02/14 16:100.050 0.050 1
Heptachlor epoxide ND ug/L 03/09/14 00:38 1024-57-303/02/14 16:100.050 0.050 1
Hexachlorobenzene ND ug/L 03/09/14 00:38 118-74-103/02/14 16:100.050 0.050 1
Methoxychlor ND ug/L 03/09/14 00:38 72-43-503/02/14 16:100.15 0.15 1
Mirex ND ug/L 03/09/14 00:38 2385-85-503/02/14 16:100.15 0.15 1
Toxaphene ND ug/L 03/09/14 00:38 8001-35-203/02/14 16:100.20 0.20 1
Surrogates
Tetrachloro-m-xylene (S)66 %03/09/14 00:38 877-09-803/02/14 16:1020-130 1
Decachlorobiphenyl (S)58 %03/09/14 00:38 2051-24-303/02/14 16:1020-130 1
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 03/01/14 02:22 7440-36-002/28/14 09:055.0 5.0 1
Arsenic ND ug/L 03/01/14 02:22 7440-38-202/28/14 09:0510.0 5.0 1
Barium 185 ug/L 03/01/14 02:22 7440-39-302/28/14 09:055.0 5.0 1
Beryllium ND ug/L 03/01/14 02:22 7440-41-702/28/14 09:051.0 1.0 1
Cadmium ND ug/L 03/01/14 02:22 7440-43-902/28/14 09:051.0 1.0 1
Chromium 6.5 ug/L 03/01/14 02:22 7440-47-302/28/14 09:055.0 5.0 1
Cobalt ND ug/L 03/01/14 02:22 7440-48-402/28/14 09:055.0 5.0 1
Copper ND ug/L 03/01/14 02:22 7440-50-802/28/14 09:055.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-12 Lab ID:92191140004 Collected:02/26/14 12:25 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead ND ug/L 03/01/14 02:22 7439-92-102/28/14 09:055.0 5.0 1
Nickel 8.0 ug/L 03/01/14 02:22 7440-02-002/28/14 09:055.0 5.0 1
Selenium ND ug/L 03/01/14 02:22 7782-49-202/28/14 09:0510.0 10.0 1
Silver ND ug/L 03/01/14 02:22 7440-22-402/28/14 09:055.0 5.0 1
Thallium ND ug/L 03/01/14 02:22 7440-28-002/28/14 09:055.4 5.4 1
Vanadium 7.4 ug/L 03/01/14 02:22 7440-62-202/28/14 09:055.0 5.0 1
Zinc ND ug/L 03/01/14 02:22 7440-66-602/28/14 09:0510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/04/14 16:16 7439-97-602/27/14 18:150.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 11:34 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 11:34 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 11:34 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 11:34 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 11:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 11:34 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 11:34 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 11:34 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 11:34 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 11:34 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 11:34 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 11:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 11:34 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 11:34 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 11:34 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 11:34 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 11:34 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 11:34 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 11:34 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 11:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 11:34 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 11:34 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 11:34 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 11:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 11:34 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 11:34 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 11:34 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 11:34 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 11:34 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 11:34 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 11:34 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 11:34 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 11:34 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 11:34 594-20-71.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:MW-12 Lab ID:92191140004 Collected:02/26/14 12:25 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 02/28/14 11:34 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 11:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 11:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 11:34 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 11:34 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 11:34 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 11:34 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 11:34 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 11:34 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 11:34 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 11:34 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 11:34 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 11:34 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 11:34 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 11:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 11:34 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 11:34 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 11:34 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 11:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 11:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 11:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 11:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 11:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 11:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 11:34 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 11:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 11:34 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 11:34 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 11:34 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %02/28/14 11:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/28/14 11:34 17060-07-070-130 1
Toluene-d8 (S)96 %02/28/14 11:34 2037-26-570-130 1
4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 03/10/14 13:43 57-12-50.0050 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:TRIP BLANK Lab ID:92191140005 Collected:02/20/14 00:00 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 11:50 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 11:50 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 11:50 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 11:50 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 11:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 11:50 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 11:50 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 11:50 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 11:50 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 11:50 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 11:50 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 11:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 11:50 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 11:50 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 11:50 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 11:50 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 11:50 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 11:50 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 11:50 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 11:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 11:50 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 11:50 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 11:50 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 11:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 11:50 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 11:50 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 02/28/14 11:50 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 11:50 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 11:50 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 11:50 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 11:50 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 11:50 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 11:50 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 11:50 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 02/28/14 11:50 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 11:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 11:50 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 11:50 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 11:50 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 11:50 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 11:50 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 11:50 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 11:50 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 11:50 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 11:50 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 11:50 108-10-15.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:TRIP BLANK Lab ID:92191140005 Collected:02/20/14 00:00 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Naphthalene ND ug/L 02/28/14 11:50 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 11:50 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 11:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 11:50 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 11:50 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 11:50 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 11:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 11:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 11:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 11:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 11:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 11:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 11:50 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 11:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 11:50 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 11:50 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 11:50 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/28/14 11:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/28/14 11:50 17060-07-070-130 1
Toluene-d8 (S)97 %02/28/14 11:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:EQUIP BLK Lab ID:92191140006 Collected:02/20/14 00:00 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 03/01/14 02:26 7440-36-002/28/14 09:055.0 5.0 1
Arsenic ND ug/L 03/01/14 02:26 7440-38-202/28/14 09:0510.0 5.0 1
Barium ND ug/L 03/01/14 02:26 7440-39-302/28/14 09:055.0 5.0 1
Beryllium ND ug/L 03/01/14 02:26 7440-41-702/28/14 09:051.0 1.0 1
Cadmium ND ug/L 03/01/14 02:26 7440-43-902/28/14 09:051.0 1.0 1
Chromium ND ug/L 03/01/14 02:26 7440-47-302/28/14 09:055.0 5.0 1
Cobalt ND ug/L 03/01/14 02:26 7440-48-402/28/14 09:055.0 5.0 1
Copper ND ug/L 03/01/14 02:26 7440-50-802/28/14 09:055.0 5.0 1
Lead ND ug/L 03/01/14 02:26 7439-92-102/28/14 09:055.0 5.0 1
Nickel ND ug/L 03/01/14 02:26 7440-02-002/28/14 09:055.0 5.0 1
Selenium ND ug/L 03/01/14 02:26 7782-49-202/28/14 09:0510.0 10.0 1
Silver ND ug/L 03/01/14 02:26 7440-22-402/28/14 09:055.0 5.0 1
Thallium ND ug/L 03/01/14 02:26 7440-28-002/28/14 09:055.4 5.4 1
Vanadium ND ug/L 03/01/14 02:26 7440-62-202/28/14 09:055.0 5.0 1
Zinc ND ug/L 03/01/14 02:26 7440-66-602/28/14 09:0510.0 10.0 1
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 03/04/14 16:18 7439-97-602/27/14 18:150.20 0.10 1
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 02/28/14 12:05 67-64-125.0 10.0 1
Acetonitrile ND ug/L 02/28/14 12:05 75-05-850.0 2.2 1
Acrylonitrile ND ug/L 02/28/14 12:05 107-13-110.0 1.9 1
Allyl chloride ND ug/L 02/28/14 12:05 107-05-12.0 1.5 1
Benzene ND ug/L 02/28/14 12:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/28/14 12:05 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 02/28/14 12:05 75-27-41.0 0.18 1
Bromoform ND ug/L 02/28/14 12:05 75-25-21.0 0.26 1
Bromomethane ND ug/L 02/28/14 12:05 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 02/28/14 12:05 78-93-35.0 0.96 1
Carbon disulfide ND ug/L 02/28/14 12:05 75-15-02.0 1.2 1
Carbon tetrachloride ND ug/L 02/28/14 12:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/28/14 12:05 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/28/14 12:05 75-00-31.0 0.54 1
Chloroform ND ug/L 02/28/14 12:05 67-66-31.0 0.14 1
Chloromethane ND ug/L 02/28/14 12:05 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/28/14 12:05 126-99-85.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/14 12:05 96-12-85.0 2.5 1
Dibromochloromethane ND ug/L 02/28/14 12:05 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/14 12:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/28/14 12:05 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/28/14 12:05 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/28/14 12:05 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/28/14 12:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/28/14 12:05 110-57-61.0 1.0 1
Dichlorodifluoromethane ND ug/L 02/28/14 12:05 75-71-81.0 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Sample:EQUIP BLK Lab ID:92191140006 Collected:02/20/14 00:00 Received:02/26/14 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloroethane ND ug/L 02/28/14 12:05 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 02/28/14 12:05 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/28/14 12:05 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/28/14 12:05 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/28/14 12:05 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 02/28/14 12:05 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/28/14 12:05 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/28/14 12:05 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 02/28/14 12:05 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/28/14 12:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/28/14 12:05 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/28/14 12:05 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/28/14 12:05 97-63-21.0 0.20 1
2-Hexanone ND ug/L 02/28/14 12:05 591-78-65.0 0.46 1
Iodomethane ND ug/L 02/28/14 12:05 74-88-45.0 0.32 1
Isobutanol ND ug/L 02/28/14 12:05 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/28/14 12:05 126-98-710.0 0.93 1
Methylene Chloride ND ug/L 02/28/14 12:05 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 02/28/14 12:05 80-62-62.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/28/14 12:05 108-10-15.0 0.33 1
Naphthalene ND ug/L 02/28/14 12:05 91-20-31.0 0.24 1
Propionitrile ND ug/L 02/28/14 12:05 107-12-020.0 3.6 1
Styrene ND ug/L 02/28/14 12:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/14 12:05 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/14 12:05 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 02/28/14 12:05 127-18-41.0 0.46 1
Toluene ND ug/L 02/28/14 12:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/28/14 12:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/28/14 12:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/28/14 12:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/28/14 12:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/28/14 12:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/28/14 12:05 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 02/28/14 12:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/28/14 12:05 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 02/28/14 12:05 179601-23-12.0 0.66 1
o-Xylene ND ug/L 02/28/14 12:05 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/28/14 12:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/28/14 12:05 17060-07-070-130 1
Toluene-d8 (S)97 %02/28/14 12:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6244
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147366
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140006
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 03/04/14 15:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147367LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147368MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191224002
1147369
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 80 75-12576 4 252.5ND 2.0 1.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15331
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147586
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140006
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 03/01/14 01:40
Arsenic ug/L ND 10.0 03/01/14 01:40
Barium ug/L ND 5.0 03/01/14 01:40
Beryllium ug/L 0.18J 1.0 03/01/14 01:40
Cadmium ug/L ND 1.0 03/01/14 01:40
Chromium ug/L ND 5.0 03/01/14 01:40
Cobalt ug/L ND 5.0 03/01/14 01:40
Copper ug/L ND 5.0 03/01/14 01:40
Lead ug/L ND 5.0 03/01/14 01:40
Nickel ug/L ND 5.0 03/01/14 01:40
Selenium ug/L 1.0J 10.0 03/01/14 01:40
Silver ug/L 0.35J 5.0 03/01/14 01:40
Thallium ug/L ND 5.4 03/01/14 01:40
Vanadium ug/L 0.68J 5.0 03/01/14 01:40
Zinc ug/L 0.98J 10.0 03/01/14 01:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147587LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 492500 98 80-120
Arsenic ug/L 458500 92 80-120
Barium ug/L 476500 95 80-120
Beryllium ug/L 474500 95 80-120
Cadmium ug/L 484500 97 80-120
Chromium ug/L 483500 97 80-120
Cobalt ug/L 472500 94 80-120
Copper ug/L 475500 95 80-120
Lead ug/L 475500 95 80-120
Nickel ug/L 484500 97 80-120
Selenium ug/L 455500 91 80-120
Silver ug/L 238250 95 80-120
Thallium ug/L 455500 91 80-120
Vanadium ug/L 488500 98 80-120
Zinc ug/L 473500 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147588MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190918006
1147589
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12596 2 25500ND489479
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147588MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190918006
1147589
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 94 75-12591 3 25500ND469454
Barium ug/L 500 97 75-12595 2 2550030.8 517 506
Beryllium ug/L 500 97 75-12595 2 25500ND485475
Cadmium ug/L 500 98 75-12596 2 25500ND489479
Chromium ug/L 500 98 75-12597 2 25500ND496488
Cobalt ug/L 500 95 75-12594 2 25500ND478470
Copper ug/L 500 98 75-12596 2 25500ND489479
Lead ug/L 500 94 75-12592 2 25500ND474465
Nickel ug/L 500 97 75-12596 1 25500ND488481
Selenium ug/L 500 92 75-12591 2 25500ND463456
Silver ug/L 250 96 75-12595 2 25250ND241237
Thallium ug/L 500 91 75-12590 2 25500ND459451
Vanadium ug/L 500 99 75-12597 2 255007.0 504 493
Zinc ug/L 500 96 75-12594 2 25500ND483475
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25928
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140005, 92191140006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147362
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140005, 92191140006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/28/14 07:55
1,1,1-Trichloroethane ug/L ND 1.0 02/28/14 07:55
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/28/14 07:55
1,1,2-Trichloroethane ug/L ND 1.0 02/28/14 07:55
1,1-Dichloroethane ug/L ND 1.0 02/28/14 07:55
1,1-Dichloroethene ug/L ND 1.0 02/28/14 07:55
1,1-Dichloropropene ug/L ND 1.0 02/28/14 07:55
1,2,3-Trichloropropane ug/L ND 1.0 02/28/14 07:55
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/28/14 07:55
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/28/14 07:55
1,2-Dichlorobenzene ug/L ND 1.0 02/28/14 07:55
1,2-Dichloroethane ug/L ND 1.0 02/28/14 07:55
1,2-Dichloropropane ug/L ND 1.0 02/28/14 07:55
1,3-Dichlorobenzene ug/L ND 1.0 02/28/14 07:55
1,3-Dichloropropane ug/L ND 1.0 02/28/14 07:55
1,4-Dichlorobenzene ug/L ND 1.0 02/28/14 07:55
2,2-Dichloropropane ug/L ND 1.0 02/28/14 07:55
2-Butanone (MEK)ug/L ND 5.0 02/28/14 07:55
2-Hexanone ug/L ND 5.0 02/28/14 07:55
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/28/14 07:55
Acetone ug/L ND 25.0 02/28/14 07:55
Acetonitrile ug/L ND 50.0 02/28/14 07:55
Acrylonitrile ug/L ND 10.0 02/28/14 07:55
Allyl chloride ug/L ND 2.0 02/28/14 07:55
Benzene ug/L ND 1.0 02/28/14 07:55
Bromochloromethane ug/L ND 1.0 02/28/14 07:55
Bromodichloromethane ug/L ND 1.0 02/28/14 07:55
Bromoform ug/L ND 1.0 02/28/14 07:55
Bromomethane ug/L ND 2.0 02/28/14 07:55
Carbon disulfide ug/L ND 2.0 02/28/14 07:55
Carbon tetrachloride ug/L ND 1.0 02/28/14 07:55
Chlorobenzene ug/L ND 1.0 02/28/14 07:55
Chloroethane ug/L ND 1.0 02/28/14 07:55
Chloroform ug/L ND 1.0 02/28/14 07:55
Chloromethane ug/L ND 1.0 02/28/14 07:55
Chloroprene ug/L ND 5.0 02/28/14 07:55
cis-1,2-Dichloroethene ug/L ND 1.0 02/28/14 07:55
cis-1,3-Dichloropropene ug/L ND 1.0 02/28/14 07:55
Dibromochloromethane ug/L ND 1.0 02/28/14 07:55
Dibromomethane ug/L ND 1.0 02/28/14 07:55
Dichlorodifluoromethane ug/L ND 1.0 02/28/14 07:55
Ethyl methacrylate ug/L ND 1.0 02/28/14 07:55
Ethylbenzene ug/L ND 1.0 02/28/14 07:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1147362
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004, 92191140005, 92191140006
Matrix:Water
Analyzed
Iodomethane ug/L ND 5.0 02/28/14 07:55
Isobutanol ug/L ND 100 02/28/14 07:55
m&p-Xylene ug/L ND 2.0 02/28/14 07:55
Methacrylonitrile ug/L ND 10.0 02/28/14 07:55
Methyl methacrylate ug/L ND 2.0 02/28/14 07:55
Methylene Chloride ug/L ND 1.0 02/28/14 07:55
Naphthalene ug/L ND 1.0 02/28/14 07:55
o-Xylene ug/L ND 1.0 02/28/14 07:55
Propionitrile ug/L ND 20.0 02/28/14 07:55
Styrene ug/L ND 1.0 02/28/14 07:55
Tetrachloroethene ug/L ND 1.0 02/28/14 07:55
Toluene ug/L ND 1.0 02/28/14 07:55
trans-1,2-Dichloroethene ug/L ND 1.0 02/28/14 07:55
trans-1,3-Dichloropropene ug/L ND 1.0 02/28/14 07:55
trans-1,4-Dichloro-2-butene ug/L ND 1.0 02/28/14 07:55
Trichloroethene ug/L ND 1.0 02/28/14 07:55
Trichlorofluoromethane ug/L ND 1.0 02/28/14 07:55
Vinyl acetate ug/L ND 2.0 02/28/14 07:55
Vinyl chloride ug/L ND 1.0 02/28/14 07:55
Xylene (Total)ug/L ND 2.0 02/28/14 07:55
1,2-Dichloroethane-d4 (S)%102 70-130 02/28/14 07:55
4-Bromofluorobenzene (S)%100 70-130 02/28/14 07:55
Toluene-d8 (S)%97 70-130 02/28/14 07:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147363LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 70-130
1,1,1-Trichloroethane ug/L 47.550 95 70-130
1,1,2,2-Tetrachloroethane ug/L 50.350 101 70-130
1,1,2-Trichloroethane ug/L 48.450 97 70-130
1,1-Dichloroethane ug/L 41.850 84 70-130
1,1-Dichloroethene ug/L 39.450 79 70-132
1,1-Dichloropropene ug/L 45.250 90 70-130
1,2,3-Trichloropropane ug/L 53.450 107 70-130
1,2-Dibromo-3-chloropropane ug/L 59.450 119 70-130
1,2-Dibromoethane (EDB)ug/L 50.150 100 70-130
1,2-Dichlorobenzene ug/L 50.450 101 70-130
1,2-Dichloroethane ug/L 44.150 88 70-130
1,2-Dichloropropane ug/L 44.950 90 70-130
1,3-Dichlorobenzene ug/L 49.050 98 70-130
1,3-Dichloropropane ug/L 48.150 96 70-130
1,4-Dichlorobenzene ug/L 50.050 100 70-130
2,2-Dichloropropane ug/L 40.950 82 58-145
2-Butanone (MEK)ug/L 83.6100 84 70-145
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1147363LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 94.6100 95 70-144
4-Methyl-2-pentanone (MIBK)ug/L 91.1100 91 70-140
Acetone ug/L 83.1100 83 50-175
Acetonitrile ug/L 376500 75 70-130
Acrylonitrile ug/L 192250 77 70-143
Allyl chloride ug/L 35.850 72 70-130
Benzene ug/L 49.750 99 70-130
Bromochloromethane ug/L 42.450 85 70-130
Bromodichloromethane ug/L 48.450 97 70-130
Bromoform ug/L 52.450 105 70-130
Bromomethane ug/L 45.950 92 54-130
Carbon disulfide ug/L 40.850 82 70-131
Carbon tetrachloride ug/L 54.550 109 70-132
Chlorobenzene ug/L 49.950 100 70-130
Chloroethane ug/L 38.450 77 64-134
Chloroform ug/L 45.450 91 70-130
Chloromethane ug/L 36.250 72 64-130
Chloroprene ug/L 44.250 88 70-130
cis-1,2-Dichloroethene ug/L 41.650 83 70-131
cis-1,3-Dichloropropene ug/L 44.550 89 70-130
Dibromochloromethane ug/L 49.950 100 70-130
Dibromomethane ug/L 48.550 97 70-131
Dichlorodifluoromethane ug/L 44.850 90 56-130
Ethyl methacrylate ug/L 45.350 91 70-130
Ethylbenzene ug/L 52.650 105 70-130
Iodomethane ug/L 80.3100 80 49-180
Isobutanol ug/L 8101000 81 70-130
m&p-Xylene ug/L 108100 108 70-130
Methacrylonitrile ug/L 409500 82 70-130
Methyl methacrylate ug/L 47.850 96 70-130
Methylene Chloride ug/L 37.250 74 63-130
Naphthalene ug/L 67.750 135 70-138
o-Xylene ug/L 51.450 103 70-130
Propionitrile ug/L 416500 83 70-130
Styrene ug/L 50.750 101 70-130
Tetrachloroethene ug/L 55.650 111 70-130
Toluene ug/L 50.750 101 70-130
trans-1,2-Dichloroethene ug/L 40.650 81 70-130
trans-1,3-Dichloropropene ug/L 46.850 94 70-132
trans-1,4-Dichloro-2-butene ug/L 48.950 98 70-141
Trichloroethene ug/L 50.450 101 70-130
Trichlorofluoromethane ug/L 44.850 90 62-133
Vinyl acetate ug/L 75.5100 76 66-157
Vinyl chloride ug/L 40.150 80 69-130
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1147364MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191006003
1147365
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 104 70-166106 2 3050ND52.1 53.0
Benzene ug/L 50 108 70-148112 3 30501.3 55.5 57.2
Chlorobenzene ug/L 50 107 70-146110 3 30501.5 55.1 56.7
Toluene ug/L 50 103 70-155107 4 3050ND51.8 53.6
Trichloroethene ug/L 50 113 69-151115 3 3050ND56.5 57.9
1,2-Dichloroethane-d4 (S)%96 70-13095
4-Bromofluorobenzene (S)%99 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26235
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1148793
Associated Lab Samples:92191140001, 92191140002, 92191140003, 92191140004
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 03/08/14 17:03
4,4'-DDE ug/L ND 0.050 03/08/14 17:03
4,4'-DDT ug/L ND 0.050 03/08/14 17:03
Aldrin ug/L ND 0.050 03/08/14 17:03
alpha-BHC ug/L ND 0.050 03/08/14 17:03
beta-BHC ug/L ND 0.050 03/08/14 17:03
Chlordane (Technical)ug/L ND 0.20 03/08/14 17:03
delta-BHC ug/L ND 0.050 03/08/14 17:03
Dieldrin ug/L ND 0.050 03/08/14 17:03
Endosulfan I ug/L ND 0.050 03/08/14 17:03
Endosulfan II ug/L ND 0.050 03/08/14 17:03
Endosulfan sulfate ug/L ND 0.050 03/08/14 17:03
Endrin ug/L ND 0.050 03/08/14 17:03
Endrin aldehyde ug/L ND 0.050 03/08/14 17:03
Endrin ketone ug/L ND 0.050 03/08/14 17:03
gamma-BHC (Lindane)ug/L ND 0.050 03/08/14 17:03
Heptachlor ug/L ND 0.050 03/08/14 17:03
Heptachlor epoxide ug/L ND 0.050 03/08/14 17:03
Hexachlorobenzene ug/L ND 0.050 03/08/14 17:03
Methoxychlor ug/L ND 0.15 03/08/14 17:03
Mirex ug/L ND 0.15 03/08/14 17:03
Toxaphene ug/L ND 0.20 03/08/14 17:03
Decachlorobiphenyl (S)%76 20-130 03/08/14 17:03
Tetrachloro-m-xylene (S)%74 20-130 03/08/14 17:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148794LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.26.25 104 20-150
4,4'-DDE ug/L 0.25.25 103 20-150
4,4'-DDT ug/L 0.27.25 108 20-150
Aldrin ug/L 0.20.25 81 20-150
alpha-BHC ug/L 0.23.25 94 20-150
beta-BHC ug/L 0.24.25 99 20-150
delta-BHC ug/L 0.25.25 100 20-150
Dieldrin ug/L 0.24.25 97 20-150
Endosulfan I ug/L 0.25.25 102 20-150
Endosulfan II ug/L 0.25.25 101 20-150
Endosulfan sulfate ug/L 0.25.25 103 20-150
Endrin ug/L 0.29.25 117 20-150
Endrin aldehyde ug/L 0.22.25 90 20-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1148794LABORATORY CONTROL SAMPLE:
LCSSpike
Endrin ketone ug/L 0.26.25 105 20-150
gamma-BHC (Lindane)ug/L 0.23.25 95 20-150
Heptachlor ug/L 0.20.25 82 20-150
Heptachlor epoxide ug/L 0.25.25 99 20-150
Hexachlorobenzene ug/L 0.18.25 74 20-150
Methoxychlor ug/L 0.76.74 103 20-150
Mirex ug/L 0.75.74 101 20-150
Decachlorobiphenyl (S)%90 20-130
Tetrachloro-m-xylene (S)%85 20-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1148795MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191476007
1148796
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4,4'-DDD ug/L .5 54 20-15052 3 30.5ND 0.27 0.26
4,4'-DDE ug/L .5 51 20-15050 3 30.5ND 0.25 0.25
4,4'-DDT ug/L .5 53 20-15052 4 30.5ND 0.26 0.26
Aldrin ug/L .5 45 20-15042 5 30.5ND 0.22 0.21
alpha-BHC ug/L .5 47 20-15045 5 30.5ND 0.23 0.22
beta-BHC ug/L .5 48 20-15049 2 30.5ND 0.24 0.24
delta-BHC ug/L .5 50 20-15049 3 30.5ND 0.25 0.24
Dieldrin ug/L .5 49 20-15046 8 30.5ND 0.24 0.23
Endosulfan I ug/L .5 54 20-15051 5 30.5ND 0.26 0.25
Endosulfan II ug/L .5 53 20-15051 3 30.5ND 0.26 0.25
Endosulfan sulfate ug/L .5 54 20-15053 3 30.5ND 0.27 0.26
Endrin ug/L .5 60 20-15057 5 30.5ND 0.30 0.28
Endrin aldehyde ug/L .5 47 20-15046 4 30.5ND 0.23 0.23
Endrin ketone ug/L .5 57 20-15055 3 30.5ND 0.28 0.27
gamma-BHC (Lindane)ug/L .5 48 20-15046 5 30.5ND 0.24 0.23
Heptachlor ug/L .5 46 20-15044 6 30.5ND 0.23 0.22
Heptachlor epoxide ug/L .5 60 20-15051 16 30.5ND 0.30 0.25
Hexachlorobenzene ug/L .5 44 20-15042 4 30.5ND 0.22 0.21
Methoxychlor ug/L 1.5 56 20-15054 3 301.5ND 0.83 0.81
Mirex ug/L 1.5 53 20-15051 3 301.5ND 0.78 0.76
Decachlorobiphenyl (S)%83 20-13067
Tetrachloro-m-xylene (S)%78 20-13060
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/18294
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92191140001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1153435
Associated Lab Samples:92191140001
Matrix:Water
Analyzed
Cyanide mg/L ND 0.0050 03/10/14 13:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1153436LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.10.1 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1153439MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191102002
1153440
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 118 75-125111 5 20.1ND 0.12 0.11
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1153463MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191394001
1153464
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 106 75-125108 2 20.15.5J
ug/L 0.11 0.11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/18295
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92191140002, 92191140003, 92191140004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1153441
Associated Lab Samples:92191140002, 92191140003, 92191140004
Matrix:Water
Analyzed
Cyanide mg/L ND 0.0050 03/10/14 13:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1153442LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.11.1 113 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1153443MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191140002
1153444
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 99 75-12591 7 20.10.0084 0.11 0.099
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1153445MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92191476008
1153446
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 124 75-125115 7 20.1ND 0.13 0.12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92191140
FRANCIS FARM LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92191140001 FLD/MW-2A
92191140002 FLD/MW-3A
92191140003 FLD/MW-5
92191140004 FLD/MW-12
92191140001 OEXT/26235 GCSV/16879MW-2A EPA 3510 EPA 8081
92191140002 OEXT/26235 GCSV/16879MW-3A EPA 3510 EPA 8081
92191140003 OEXT/26235 GCSV/16879MW-5 EPA 3510 EPA 8081
92191140004 OEXT/26235 GCSV/16879MW-12 EPA 3510 EPA 8081
92191140001 MPRP/15331 ICP/13910MW-2A EPA 3010 EPA 6010
92191140002 MPRP/15331 ICP/13910MW-3A EPA 3010 EPA 6010
92191140003 MPRP/15331 ICP/13910MW-5 EPA 3010 EPA 6010
92191140004 MPRP/15331 ICP/13910MW-12 EPA 3010 EPA 6010
92191140006 MPRP/15331 ICP/13910EQUIP BLK EPA 3010 EPA 6010
92191140001 MERP/6244 MERC/6022MW-2A EPA 7470 EPA 7470
92191140002 MERP/6244 MERC/6022MW-3A EPA 7470 EPA 7470
92191140003 MERP/6244 MERC/6022MW-5 EPA 7470 EPA 7470
92191140004 MERP/6244 MERC/6022MW-12 EPA 7470 EPA 7470
92191140006 MERP/6244 MERC/6022EQUIP BLK EPA 7470 EPA 7470
92191140001 MSV/25928MW-2A EPA 8260
92191140002 MSV/25928MW-3A EPA 8260
92191140003 MSV/25928MW-5 EPA 8260
92191140004 MSV/25928MW-12 EPA 8260
92191140005 MSV/25928TRIP BLANK EPA 8260
92191140006 MSV/25928EQUIP BLK EPA 8260
92191140001 WETA/18294MW-2A SM 4500-CN-E
92191140002 WETA/18295MW-3A SM 4500-CN-E
92191140003 WETA/18295MW-5 SM 4500-CN-E
92191140004 WETA/18295MW-12 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/19/2014 03:46 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 35
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