SW_F_1901-MSWLF-1979_10-30-2014_RM_GW.pdf

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October 2014 Groundwater Monitoring Report

Chatham County Landfill
Pittsboro, North Carolina
NC Solid Waste Permit # 19-01

Prepared for:

Chatham County Environmental Quality Department
PO BOX 1550
Pittsboro, North Carolina 27312

December 2014

Prepared by:

© 2014 Smith Gardner, Inc.
This document is intended for the sole use of the client for which it was prepared and
for the purpose agreed upon by the client and Smith Gardner, Inc.

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Chatham County Landfill October 2014 Groundwater Monitoring Report
December 2014 Table of Contents Page i
Chatham County Landfill
Solid Waste Permit No. 19-01

October 2014 Water Quality Monitoring Report

Table of Contents
Page

1.0 INTRODUCTION ......................................................................................................... 1 
2.0 SITE GEOLOGY ........................................................................................................... 1 
3.0 SAMPLING LOCATIONS ............................................................................................. 1 
4.0 SAMPLING PROCEDURES ......................................................................................... 1 
5.0 FIELD & LABORATORY RESULTS .............................................................................. 2 
5.1 Field Results .............................................................................................................. 2 
5.2 Laboratory Analysis & Results ................................................................................. 2 
5.2.1 Inorganic Constituent Results ...................................................................... 2 
5.2.2 Organic Constituent Results ......................................................................... 3 
5.2.3 Surface Water Results .................................................................................. 3 
6.0 GROUNDWATER CHARACTERIZATION ...................................................................... 3 
7.0 CONCLUSIONS .......................................................................................................... 3 

FIGURES
Figure 1 Groundwater Potentiometric Map

TABLES
Table 1 Groundwater Elevations & Velocities
Table 2 Field Parameter Results
Table 3 Detected Inorganic Constituents
Table 4 Detected Organic Constituents
Table 5 Velocity and Conductivity Calculations

APPENDICES
Appendix A Monitoring Well Information
Appendix B Laboratory Analytical Report

Chatham County Landfill October 2014 Groundwater Monitoring Report
December 2014 Table of Contents Page ii

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Chatham County Landfill October 2014 Groundwater Monitoring Report
December 2014 Page 1
1.0 INTRODUCTION
The Chatham County Landfill located at 811 County Landfill Road in Pittsboro, North Carolina,
operating under Solid Waste Permit #19-01, is required to submit semi-annual groundwater
monitoring reports in accordance with 15A NCAC 13B.0544. This report presents the results
from the sampling conducted on October 30, 2014.

The Chatham County Landfill facility contains a closed MSW landfill, a scrap metal area, scrap
tire area, a yard-waste compost operation, the notified land clearing and inert debris (LCID)
landfill (N0069) and the household hazardous waste (HHW) collection facility (19-04). White
goods collections ceased at this facility in 2012. The MSW landfill is an approximately 80 acre
unlined facility that ceased operation in 1993 per Solid Waste Regulations and the post closure
conditions dated December 20, 1996.

This report includes a field procedure summary, summary tables, laboratory analyses and
groundwater characterization.
2.0 SITE GEOLOGY
According to the 1985 Geologic Map of North Carolina, the Chatham County Landfill is located in
Cambrian/Late Proterozoic age Felsic Metavolcanic Rock of the Charlotte Belt; defined as
metamorphosed dacite, rhyolitic flows and tuffs, light gray to greenish gray and generally
interbedded with mafic and intermediate metavolcanic rock, meta-argillite and metamudstone.
The Geology of the Carolinas1 describes the Charlotte Belt as ‘‘dominantly plutonic’’ mafic
gneisses, amphibolites, metagabbros and metavolcanic rock. Due to the abundance of post-
deformational plutions geologic structure is difficult to determine. Many Cambrian/Late
Proterozoic age plutons have a massive interior and only show foliation near their contacts.
3.0 SAMPLING LOCATIONS
The groundwater monitoring network consists of five wells (MW-1 through MW-5) positioned
around the landfill perimeter (Figure 1). Well depths range from 21 to 64 feet below ground
surface (bgs).

Two surface water sampling points (SW-1 and SW-2) are located up and downstream of the
landfill on Shoe Heel Creek, respectively. A trip blank (TB) was also submitted for quality
control purposes. . Available well records are presented in Appendix A.
4.0 SAMPLING PROCEDURES
Sampling procedures followed the protocols set forth in the North Carolina Water Quality
Monitoring Guidance Document for Solid Waste Facilities (North Carolina Department of
Environment and Natural Resources, Division of Waste Management). Each well was gauged to
determine groundwater depth and then purged three to five well volumes or until dry. Field

1 Horton, J. Wright, and Zullo, Victor, A., The Geology of the Carolinas, University of Tennessee Press, 1991.

Chatham County Landfill October 2014 Groundwater Monitoring Report
December 2014 Page 2
measurements for pH, specific conductivity, turbidity and temperature were recorded at each
well. Water table elevations are included in Table 1.

Samples were collected in laboratory prepared containers for the specified analytical
procedures. Sampling equipment was cleaned in accordance with Solid Waste regulation or
was used in sterilized form from the manufacturer. Groundwater samples were properly
preserved, placed on ice and transported to the laboratory facility within the specified hold
times for analysis.
5.0 FIELD & LABORATORY RESULTS
5.1 Field Results
Field parameters of pH, temperature, specific conductivity and turbidity were collected
by S+G personnel; data is presented in Table 2. Overall, October 2014 data is generally
consistent with previously recorded field measurements at the site; however, the
sample from MW-3 exceeded the instrument calibration for turbidity.
5.2 Laboratory Analysis & Results
Samples were transported to ESC Lab Sciences, Mount Juliet, TN, a North Carolina
certified laboratory (NC Certification No.: Env375). Laboratory analysis for sampled
locations included metals via EPA Test Method 6020A and Appendix I volatile organic
compounds (VOCs) via EPA Test Method 8260B.

Analytical results were compared to the NC DWM Solid Waste Section Quantitation
Limits (SWSLs), 15A NCAC 2L.0200 (2L Standard), SWS established Groundwater
Protection (GWP) Standards and Federal Maximum Contaminant Limits (MCL).
Constituents detected between the Method Detection Limit (MDL) and Report Detection
Limit (RDL) are denoted as ‘‘J’’ values by the laboratory. Values reported below the MDL
are considered non-detect.

The laboratory analytical report is included as Appendix B.
5.2.1 Inorganic Constituent Results
Five inorganic constituents were reported in samples at concentrations above
the 2L groundwater standard:

 cobalt (MW-1, MW-2, MW-3 and MW-4),
 chromium (MW-3),
 lead (MW-3),
 selenium (MW-3) and
 vanadium (MW-3 and MW-4).

Chatham County Landfill October 2014 Groundwater Monitoring Report
December 2014 Page 3
High sample turbidity, especially in the sample collected from MW-3, influenced
inorganic concentrations this event. Inorganic detections are summarized in
Table 3.
5.2.2 Organic Constituent Results
Two organic constituents were detected in samples above the 2L Standard:

 benzene (MW-2 and MW-4); and
 vinyl chloride (MW-4).

Organics analysis is consistent with historically reported detections. Organic
detections are summarized in Table 4.
5.2.3 Surface Water Results
Surface water sample results indicated no inorganic constituents were detected
above the 15a NCAC 2B.0200 criteria (2B Standards for Class C Waters). Organic
concentrations for SW-1 and SW-2 were either below MDLs or non-quantifiable
‘‘J’’-values. Surface water results are presented in Tables 3 and 4.
6.0 GROUNDWATER CHARACTERIZATION
A potentiometric surface map was prepared from groundwater elevations for this sampling
event. In general, groundwater is flowing east toward Shoe Heel Creek. This is consistent with
groundwater flow patterns previously reported for the site. The potentiometric surface map is
attached as Figure 1.

Groundwater flow velocities were calculated for monitoring wells MW-1 through MW-5 using
the equation:
V = Ki/n
Where: K = hydraulic conductivity
i = groundwater gradient
n = porosity

Groundwater flow velocities averaged 0.212 (ft/day). Calculated flow velocities are included in
Table 5.
7.0 CONCLUSIONS
Laboratory results indicated that water quality at the Chatham County Landfill is generally
consistent with reported historical detections. Metals detections are likely due to naturally
occurring conditions in conjunction with high sample turbidity levels that influence analytical
results. Flow direction remains consistent with reported historical observations. The facility
will continue semi-annual monitoring with the next event scheduled for May 2015.

Chatham County Landfill October 2014 Groundwater Monitoring Report
December 2014 Page 4

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FIGURE

October 2014 Groundwater Monitoring Report
Chatham County Landfill
Solid Waste Permit No. 19-01

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MW-1
GWE=470.30
TOC=481.73
DTW=11.43
MW-1A
MW-2
GWE=451.12
TOC=465.36
DTW=14.24
MW-2A
MW-3
GWE=456.48
TOC=465.85
DTW=9.37
MW-4
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TOC=522.84
DTW=47.41
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TOC=515.58
DTW=38.56
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October 2014 Groundwater Monitoring Report
Chatham County Landfill
Solid Waste Permit No. 19-01

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APPENDIX A
Monitoring Well Information
October 2014 Groundwater Monitoring Report
Chatham County Landfill
Solid Waste Permit No. 19-01

This page intentionally left blank.

APPENDIX B
Laboratory Analytical Results
October 2014 Groundwater Monitoring Reports
Chatham County Landfill
Solid Waste Permit No. 19-01

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12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Joan Smyth
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
Report Summary
Tuesday November 11, 2014
Report Number: L730897
Samples Received: 10/31/14
Client Project:
Description: Chatham 13-2
The analytical results in this report are based upon information suppliedby you, the client, and are for your exclusive use. If you have anyquestions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By: ____________________________________
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TN002
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-01
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-1
Project # :
Collected By :
Collection Date : 10/30/14 11:10
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony U 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic U 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 150 0.36 5.0 ug/l 6020 11/11/14 1
Beryllium U 0.12 2.0 ug/l 6020 11/11/14 1 1
Cadmium U 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 4.0 0.54 2.0 ug/l 6020 11/11/14 1
Copper 2.6 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 2.2 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead U 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 73. 0.35 2.0 ug/l 6020 11/11/14 1
Selenium 1.0 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver U 0.31 2.0 ug/l 6020 11/11/14 1
Thallium U 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 3.0 0.18 5.0 ug/l 6020 11/11/14 1
Zinc 3.5 2.6 25. ug/l 6020 11/11/14 1 10
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene U 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene 0.67 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/05/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene 1.1 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane 0.92 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene 0.40 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 2 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-01
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-1
Project # :
Collected By :
Collection Date : 10/30/14 11:10
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 97.9 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 94.2 % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 101. % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 3 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-02
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-2
Project # :
Collected By :
Collection Date : 10/30/14 11:24
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony U 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic 3.5 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 380 1.8 25. ug/l 6020 11/11/14 5
Beryllium 0.15 0.12 2.0 ug/l 6020 11/11/14 1 1
Cadmium U 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 1.0 0.54 2.0 ug/l 6020 11/11/14 1
Copper 1.6 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 6.9 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead 0.26 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 1.8 0.35 2.0 ug/l 6020 11/11/14 1
Selenium 0.73 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver U 0.31 2.0 ug/l 6020 11/11/14 1
Thallium U 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 3.5 0.18 5.0 ug/l 6020 11/11/14 1
Zinc 20. 2.6 25. ug/l 6020 11/11/14 1 10
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/06/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/06/14 1 200
Benzene 2.0 0.33 1.0 ug/l 8260B 11/06/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/06/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/06/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/06/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/06/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/06/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/06/14 1 1
Chlorobenzene 3.3 0.35 1.0 ug/l 8260B 11/06/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/06/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/06/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/06/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/06/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/06/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/06/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/06/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/06/14 1 5
1,4-Dichlorobenzene 0.92 0.27 1.0 ug/l 8260B 11/06/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/06/14 1 100
1,1-Dichloroethane U 0.26 1.0 ug/l 8260B 11/06/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/06/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/06/14 1 5
cis-1,2-Dichloroethene 2.0 0.26 1.0 ug/l 8260B 11/06/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/06/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 4 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-02
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-2
Project # :
Collected By :
Collection Date : 10/30/14 11:24
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/06/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/06/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/06/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/06/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/06/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/06/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/06/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/06/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/06/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/06/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/06/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/06/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/06/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/06/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/06/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/06/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/06/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/06/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/06/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/06/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/06/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/06/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/06/14 1
Surrogate Recovery
Toluene-d8 104. % Rec. 8260B 11/06/14 1
Dibromofluoromethane 111. % Rec. 8260B 11/06/14 1
4-Bromofluorobenzene 100. % Rec. 8260B 11/06/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 5 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-03
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-3
Project # :
Collected By :
Collection Date : 10/30/14 12:19
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony 0.24 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic 7.9 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 280 1.8 25. ug/l 6020 11/11/14 5
Beryllium 3.6 0.60 10. ug/l 6020 11/11/14 5 1
Cadmium 0.47 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 35. 2.7 10. ug/l 6020 11/11/14 5
Copper 22. 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 11. 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead 47. 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 8.1 0.35 2.0 ug/l 6020 11/11/14 1
Selenium 51. 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver 0.53 0.31 2.0 ug/l 6020 11/11/14 1
Thallium 0.31 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 51. 0.90 25. ug/l 6020 11/11/14 5
Zinc 290 13. 130 ug/l 6020 11/11/14 5 10
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene U 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/05/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene U 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane U 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene U 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 6 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-03
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-3
Project # :
Collected By :
Collection Date : 10/30/14 12:19
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 98.5 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 99.5 % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 97.4 % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 7 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-04
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-4
Project # :
Collected By :
Collection Date : 10/30/14 10:36
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony U 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic 5.9 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 62. 0.36 5.0 ug/l 6020 11/11/14 1
Beryllium U 0.12 2.0 ug/l 6020 11/11/14 1 1
Cadmium 0.17 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 1.6 0.54 2.0 ug/l 6020 11/11/14 1
Copper 2.7 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 14. 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead 2.0 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 2.7 0.35 2.0 ug/l 6020 11/11/14 1
Selenium 1.7 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver U 0.31 2.0 ug/l 6020 11/11/14 1
Thallium U 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 8.2 0.18 5.0 ug/l 6020 11/11/14 1
Zinc 36. 2.6 25. ug/l 6020 11/11/14 1 10
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene 1.3 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene 3.0 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane 2.7 0.45 5.0 ug/l 8260B 11/05/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene 2.0 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane 0.32 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene 1.1 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 8 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-04
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-4
Project # :
Collected By :
Collection Date : 10/30/14 10:36
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride 1.2 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran 1.9 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 97.7 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 99.1 % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 109. % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 9 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-05
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-5
Project # :
Collected By :
Collection Date : 10/30/14 10:23
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony U 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic 1.6 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 14. 0.36 5.0 ug/l 6020 11/11/14 1
Beryllium 0.33 0.12 2.0 ug/l 6020 11/11/14 1 1
Cadmium U 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 3.1 0.54 2.0 ug/l 6020 11/11/14 1
Copper 2.1 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 0.66 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead 4.2 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 5.4 0.35 2.0 ug/l 6020 11/11/14 1
Selenium 1.9 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver U 0.31 2.0 ug/l 6020 11/11/14 1
Thallium U 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 2.1 0.18 5.0 ug/l 6020 11/11/14 1
Zinc 16. 2.6 25. ug/l 6020 11/11/14 1 10
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene U 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/05/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene U 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane U 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene U 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 10 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-05
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : MW-5
Project # :
Collected By :
Collection Date : 10/30/14 10:23
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 93.3 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 101. % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 96.9 % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 11 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-06
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : SW-1
Project # :
Collected By :
Collection Date : 10/30/14 11:42
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony U 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic 0.54 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 39. 0.36 5.0 ug/l 6020 11/11/14 1
Beryllium U 0.12 2.0 ug/l 6020 11/11/14 1 1
Cadmium U 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 0.73 0.54 2.0 ug/l 6020 11/11/14 1
Copper 2.4 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 1.2 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead 0.37 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 1.0 0.35 2.0 ug/l 6020 11/11/14 1
Selenium 0.78 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver U 0.31 2.0 ug/l 6020 11/11/14 1
Thallium U 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 1.8 0.18 5.0 ug/l 6020 11/11/14 1
Zinc 4.5 2.6 25. ug/l 6020 11/11/14 1 10
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene U 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/05/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene U 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane U 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene U 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 12 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-06
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : SW-1
Project # :
Collected By :
Collection Date : 10/30/14 11:42
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 98.4 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 92.8 % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 110. % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 13 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-07
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : SW-2
Project # :
Collected By :
Collection Date : 10/30/14 12:03
Parameter Result MDL RDL Units Method Date Dil. SWSL
Antimony 0.22 0.21 2.0 ug/l 6020 11/11/14 1 6
Arsenic 0.64 0.25 2.0 ug/l 6020 11/11/14 1 10
Barium 43. 0.36 5.0 ug/l 6020 11/11/14 1
Beryllium U 0.12 2.0 ug/l 6020 11/11/14 1 1
Cadmium U 0.16 1.0 ug/l 6020 11/11/14 1 1
Chromium 0.76 0.54 2.0 ug/l 6020 11/11/14 1
Copper 1.2 0.52 5.0 ug/l 6020 11/11/14 1 10
Cobalt 1.7 0.26 2.0 ug/l 6020 11/11/14 1 10
Lead 0.42 0.24 2.0 ug/l 6020 11/11/14 1 10
Nickel 1.2 0.35 2.0 ug/l 6020 11/11/14 1
Selenium U 0.38 2.0 ug/l 6020 11/11/14 1 10
Silver U 0.31 2.0 ug/l 6020 11/11/14 1
Thallium U 0.19 2.0 ug/l 6020 11/11/14 1 5.5 Vanadium 1.6 0.18 5.0 ug/l 6020 11/11/14 1
Zinc 3.6 2.6 25. ug/l 6020 11/11/14 1 10
Volatile Organics
Acetone 10. 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene U 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/05/14 1 10
Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10 1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene U 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane U 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene U 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 14 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-07
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : SW-2
Project # :
Collected By :
Collection Date : 10/30/14 12:03
Parameter Result MDL RDL Units Method Date Dil. SWSL
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10
2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1 Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 97.8 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 93.1 % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 99.8 % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 15 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-08
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : TRIP BLANK
Project # :
Collected By :
Collection Date : 10/30/14 00:00
Parameter Result MDL RDL Units Method Date Dil. SWSL
Volatile Organics
Acetone U 10. 50. ug/l 8260B 11/05/14 1 100
Acrylonitrile U 1.9 10. ug/l 8260B 11/05/14 1 200
Benzene U 0.33 1.0 ug/l 8260B 11/05/14 1 1
Bromochloromethane U 0.52 1.0 ug/l 8260B 11/05/14 1 3
Bromodichloromethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Bromoform U 0.47 1.0 ug/l 8260B 11/05/14 1 3
Bromomethane U 0.87 5.0 ug/l 8260B 11/05/14 1 10
Carbon disulfide U 0.28 1.0 ug/l 8260B 11/05/14 1 100
Carbon tetrachloride U 0.38 1.0 ug/l 8260B 11/05/14 1 1
Chlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 3
Chlorodibromomethane U 0.33 1.0 ug/l 8260B 11/05/14 1 3
Chloroethane U 0.45 5.0 ug/l 8260B 11/05/14 1 10 Chloroform U 0.32 5.0 ug/l 8260B 11/05/14 1 5
Chloromethane U 0.28 2.5 ug/l 8260B 11/05/14 1 1
Dibromomethane U 0.35 1.0 ug/l 8260B 11/05/14 1 10
1,2-Dibromo-3-Chloropropane U 1.3 5.0 ug/l 8260B 11/05/14 1
1,2-Dibromoethane U 0.38 1.0 ug/l 8260B 11/05/14 1
1,2-Dichlorobenzene U 0.35 1.0 ug/l 8260B 11/05/14 1 5
1,4-Dichlorobenzene U 0.27 1.0 ug/l 8260B 11/05/14 1 1
trans-1,4-Dichloro-2-butene U 0.87 2.5 ug/l 8260B 11/05/14 1 100
1,1-Dichloroethane U 0.26 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloroethane U 0.36 1.0 ug/l 8260B 11/05/14 1 1
1,1-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
cis-1,2-Dichloroethene U 0.26 1.0 ug/l 8260B 11/05/14 1 5
trans-1,2-Dichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 5
1,2-Dichloropropane U 0.31 1.0 ug/l 8260B 11/05/14 1 1
cis-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
trans-1,3-Dichloropropene U 0.42 1.0 ug/l 8260B 11/05/14 1 1
Ethylbenzene U 0.38 1.0 ug/l 8260B 11/05/14 1 1
2-Hexanone U 3.8 10. ug/l 8260B 11/05/14 1 50
Iodomethane U 1.7 10. ug/l 8260B 11/05/14 1 10 2-Butanone (MEK) U 3.9 10. ug/l 8260B 11/05/14 1 100
Methylene Chloride U 1.0 5.0 ug/l 8260B 11/05/14 1 1
4-Methyl-2-pentanone (MIBK) U 2.1 10. ug/l 8260B 11/05/14 1 100
Styrene U 0.31 1.0 ug/l 8260B 11/05/14 1 1
1,1,1,2-Tetrachloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 5
1,1,2,2-Tetrachloroethane U 0.58 1.0 ug/l 8260B 11/05/14 1 3
Tetrachloroethene U 0.37 1.0 ug/l 8260B 11/05/14 1 1
Toluene U 0.78 5.0 ug/l 8260B 11/05/14 1 1
1,1,1-Trichloroethane U 0.32 1.0 ug/l 8260B 11/05/14 1 1
1,1,2-Trichloroethane U 0.38 1.0 ug/l 8260B 11/05/14 1 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 16 of 19
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Joan Smyth November 11, 2014
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
ESC Sample # : L730897-08
Date Received : October 31, 2014
Description : Chatham 13-2
Site ID : Sample ID : TRIP BLANK
Project # :
Collected By :
Collection Date : 10/30/14 00:00
Parameter Result MDL RDL Units Method Date Dil. SWSL
Trichloroethene U 0.40 1.0 ug/l 8260B 11/05/14 1 1
Trichlorofluoromethane U 1.2 5.0 ug/l 8260B 11/05/14 1 1
1,2,3-Trichloropropane U 0.81 2.5 ug/l 8260B 11/05/14 1 1
Vinyl acetate U 1.6 10. ug/l 8260B 11/05/14 1 50
Vinyl chloride U 0.26 1.0 ug/l 8260B 11/05/14 1 1
Xylenes, Total U 1.1 3.0 ug/l 8260B 11/05/14 1 5
Tetrahydrofuran U 1.8 5.0 ug/l 8260B 11/05/14 1
Surrogate Recovery
Toluene-d8 97.1 % Rec. 8260B 11/05/14 1
Dibromofluoromethane 99.3 % Rec. 8260B 11/05/14 1
4-Bromofluorobenzene 101. % Rec. 8260B 11/05/14 1
U = ND (Not Detected)
SWSL = Solid Waste Section Limit
MDL = Minimum Detection Limit = LOD = TRRP SDL
RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 11/11/14 13:19 Printed: 11/11/14 13:20
Page 17 of 19
Attachment AList of Analytes with QC Qualifiers
Sample Work Sample Run
Number Group Type Analyte ID Qualifier
________________ ___________ _______ ________________________________________ __________ __________
L730897-01 WG752320 SAMP Copper R3003699 J
WG752320 SAMP Selenium R3003699 JB
WG752320 SAMP Silver R3003699 J6
WG752320 SAMP Vanadium R3003699 J
WG752320 SAMP Zinc R3003699 J
WG752127 SAMP Chlorobenzene R3002530 J
WG752127 SAMP 1,1-Dichloroethane R3002530 J
WG752127 SAMP cis-1,2-Dichloroethene R3002530 J
WG752127 SAMP Vinyl chloride R3002530 J3
L730897-02 WG752320 SAMP Beryllium R3003699 J
WG752320 SAMP Chromium R3003699 J
WG752320 SAMP Copper R3003699 J WG752320 SAMP Lead R3003699 J
WG752320 SAMP Nickel R3003699 J
WG752320 SAMP Selenium R3003699 JB
WG752320 SAMP Vanadium R3003699 J
WG752320 SAMP Zinc R3003699 J
WG752903 SAMP 1,4-Dichlorobenzene R3002842 J
WG752903 SAMP Trichlorofluoromethane R3002842 J4
L730897-03 WG752320 SAMP Antimony R3003699 J
WG752320 SAMP Beryllium R3003699 J
WG752320 SAMP Cadmium R3003699 J
WG752320 SAMP Selenium R3003699 B
WG752320 SAMP Silver R3003699 J
WG752320 SAMP Thallium R3003699 J
L730897-04 WG752320 SAMP Cadmium R3003699 J
WG752320 SAMP Chromium R3003699 J
WG752320 SAMP Copper R3003699 J
WG752320 SAMP Lead R3003699 J
WG752320 SAMP Selenium R3003699 JB
WG752127 SAMP Chloroethane R3002530 J
WG752127 SAMP 1,1-Dichloroethane R3002530 J WG752127 SAMP Tetrahydrofuran R3002530 J
L730897-05 WG752320 SAMP Arsenic R3003699 J
WG752320 SAMP Beryllium R3003699 J
WG752320 SAMP Copper R3003699 J
WG752320 SAMP Cobalt R3003699 J
WG752320 SAMP Selenium R3003699 JB
WG752320 SAMP Vanadium R3003699 J
WG752320 SAMP Zinc R3003699 J
L730897-06 WG752320 SAMP Arsenic R3003699 J
WG752320 SAMP Chromium R3003699 J
WG752320 SAMP Copper R3003699 J
WG752320 SAMP Cobalt R3003699 J
WG752320 SAMP Lead R3003699 J
WG752320 SAMP Nickel R3003699 J
WG752320 SAMP Selenium R3003699 JB
WG752320 SAMP Vanadium R3003699 J
WG752320 SAMP Zinc R3003699 J
L730897-07 WG752320 SAMP Antimony R3003699 J
WG752320 SAMP Arsenic R3003699 J WG752320 SAMP Chromium R3003699 J
WG752320 SAMP Copper R3003699 J
WG752320 SAMP Cobalt R3003699 J
WG752320 SAMP Lead R3003699 J
WG752320 SAMP Nickel R3003699 J
WG752320 SAMP Vanadium R3003699 J
WG752320 SAMP Zinc R3003699 J
WG752127 SAMP Acetone R3002530 J
Page 18 of 19
Attachment BExplanation of QC Qualifier Codes
Qualifier Meaning
__________________ _______________________________________________________________________________
B (EPA) - The indicated compound was found in the associated method blank as
well as the laboratory sample.
J (EPA) - Estimated value below the lowest calibration point. Confidence
correlates with concentration.
J3 The associated batch QC was outside the established quality control range
for precision.
J4 The associated batch QC was outside the established quality control range
for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 19 of 19
Summary of Remarks For Samples Printed
11/11/14 at 13:20:21
TSR Signing Reports: 350
R5 - Desired TAT
MDL/RDL
Sample: L730897-01 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR
Sample: L730897-02 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR
Sample: L730897-03 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR
Sample: L730897-04 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR
Sample: L730897-05 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENRSample: L730897-06 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR
Sample: L730897-07 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR
Sample: L730897-08 Account: SMIGARNC Received: 10/31/14 09:00 Due Date: 11/07/14 00:00 RPT Date: 11/11/14 13:19
EDD = NCDENR