19053_Point_Five_Phase_I_ESA_20150604

TERRA~uest ...... .....,. ~--··· -·· ~-~ ENVIRONMENTAL CONSULTANTS, P.C.
LIMITED SITE ASSESSMENT REPORT
(PHASE I)
HASTY MART #23
501 N. BERI<ELEY BOULEVARD
GOLDSBORO, WAYNE COUNTY, NC
Latitude: 35.37485° N Longitude: 77.94542°W
Release Information:
Date Discovered: 12/23/14
Estimated Release Quantity: Unknown
Release Cause/Source: Commercial Underground Storage Tanks
UST Capacities: (1) 4,000-gallon gasoline, (4) 3,000-gallon gasoline,
and {1) 4,000-gallon diesel USTs
NCDWM-UST Incident No. 38538
NCDWM-UST Risk Ranking: PENDING
Facility ID No.: 0-005354
Current UST System Owner: Current Property Owner:
Wayne Oil Company, Inc.
1301 Wayne Memorial Drive
Goldsboro, NC 27534
Terraquest Project No. 07814
June 4, 2015
1 00 E. Ruffin Street • Mebane, North Carolina 27302
Telephone [phone] • Facsimile [phone]
www.terraquestpc.com
NORFAM, LLC
P.O. Box 10767
Goldsboro, NC 27532
CERTIFICATION FOR THE SUBMITTAL
OF AN ENVIRONMENTAL/ GEOLOGICAL ASSESSMENT
Attached is the Limited Site Assessment Report (Phase I) for:
Site Name:Hasty Mart #23
Address: 501 N. Berkeley Blvd.
City: Goldsboro State: NC
Responsible Party:
Address:
City:
Wayne Oil Company, Inc.
1301 Wayne Memorial Drive
Goldsboro State: NC
Property Owner: NORFAM, LLC
Address: P.O. Box 10767
City: Goldsboro State: NC
Zip Code: 27534
Zip Code: 27534
Zip Code: 27532
I, Michael J. Brown, a Licensed Geologist in the State of North Carolina for Terraquest
Environmental Consultants, P.C. do hereby certify that I am familiar with and have reviewed all
material including figures within this report and that to the best of my knowledge the data, site
assessments, figures, and other associated materials are correct and accurate. All work was
performed under my direct supervision. My seal and signature are affixed below. Additional
seals and/or signatures are also affixed below.
Terraquest Environmental Consultants, P.C. is licensed to practice geology in North Carolina.
The certification number of the corporation is C-291.
TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C.
Jordan T. Lerew
Environmental Technician
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
Michael J. Brown, P.G.
President
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
TABLE OF CONTENTS
1.0 INTRODUCTION ................................................................................................................... 1
2.0 SITE HISTORY ....................................................................................................................... 1
3.0 RISK CHARACTERIZATION AND RECEPTOR INFORMATION ................................................ 3
4.0 SITE GEOLOGY AND HYDROGEOLOGY ................................................................................ 5
5.0 SOIL INVESTIGATION ........................................................................................................... 6
6.0 GROUNDWATER INVESTIGATION ....................................................................................... 7
7.0 GROUNDWATER FLOW ....................................................................................................... 8
8.0 CONCLUSIONS AND RECOMMENDATIONS ......................................................................... 8
9.0 LIMITATIONS ....................................................................................................................... 9
REFERENCES .................................................................................................................................. 10
TABLES
1. Site History (UST System Information)
2. Surrounding Property Owners
3. Monitoring Well Construction Information
4. Summary of Soil Sampling Results
5. Summary of Groundwater Sampling Results
FIGURES
1. Site Location Map
2. Site Vicinity Map
3. Site Layout Map
4. Soil Sample Analytical Results Map
5. Groundwater Analytical Results Map
6. Potentiometric Surface Map (5/12/15)
APPENDICES
A. Environmental Acronyms and Technical Methods I Standard Procedures
B. Limited Site Assessment Risk Classification and Land Use Form
C. Well Construction Record and Boring Log
D. Analytical Report
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
ii
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
1.0 INTRODUCTION
Terraquest Environmental Consultants, P.C. has performed limited site assessment activities at
the Hasty Mart #23 facility located at 501 N Berkeley Blvd, Goldsboro, Wayne County, North
Carolina. The release was discovered by Mid-Atlantic Engineering and Environmental Solutions
(Mid-Atlantic) while conducting a Phase II Environmental Site Assessment for NORFAM, LLC on
the adjoining property located at 503 N. Berkeley Blvd. Analytical results for both soil and
groundwater indicated the presence of petroleum-type contamination; likely sourced from the
Hasty Mart #23 facility. A UST-61 24-Hour Release and UST Leak Reporting Form was submitted
to the NCDWM-UST Washington Regional Office (WRO) on September 26, 2014, by Mid-
Atlantic. On November 5, 2014, the NCDWM-UST issued an NORR requesting the completion of
a site check including line tightness tests. Tank tightness testing was also requested; however
soil sampling around the USTs was approved as a substitute by the NCDWM-UST. Results of
that site check have required the completion of this limited site assessment. This report has
been prepared to comply with those requirements set forth under Title 15A of the NCAC
Subchapter 2L Section .0405.
The site location is shown in Figure 1. The surrounding vicinity is shown in Figure 2. A site
layout map is included as Figure 3. Environmental Acronyms and Technical Methods and
Standard Procedures utilized by Terraquest personnel in this report and during the
groundwater sampling process are detailed in Appendix A.
2.0 SITE HISTORY
The Hasty Mart #23 property, located at 501 N. Berkeley Blvd. is owned by NORFAM, LLC and
leased by Wayne. According to the May 23, 1995 lease agreement, Wayne is the owner and
operator of any and all USTs on the property. One 4,000-gallon and four 3,000-gallon gasoline
USTs were installed on May 8, 1963. An additional 4,000-gallon diesel UST was installed on
May 2, 1985. Three non-commercial, non-registered USTs were identified to the rear of the
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
1
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
convenience store. Through conversations with Wayne representatives, half of the current
convenience store operated as an automobile mechanic shop, prior to the building's conversion
to its current layout. The USTs likely contained either heating oil and/or waste oil. Currently
the USTs are no longer in use, the fill ports have been cut to surface level, and filled with
concrete. It is unknown whether or not the USTs were pumped out prior to closure and
completely filled with concrete. A site history of the USTs located on the site is included as
Table 1. Current tank locations are shown on Figure 3. The site is currently operated as a retail
fuel facility.
On December 9, 2014, Terraquest advanced twenty-two (22) soil borings to investigate soil
quality around the current UST system (tanks, dispensers, product lines) and three orphan USTs
discovered to the rear of the convenience store. Samples were submitted for analysis per EPA
Method 8015 utilizing either the 5030 (gasoline) and/or 3550 (diesel) extraction methods
depending on the type of fuel stored. One soil sample from the orphan USTs was submitted for
analysis per EPA Methods 8260 for VOCs and 6010C for total lead and chromium. Soil boring
locations are depicted on Figure 4.
Analytical results of the collected soil samples revealed petroleum-type contaminant
concentrations exceeding regulatory levels at nineteen of the twenty-two soil sample locations.
Soil samples (B1 -B3) collected adjacent to the three orphan USTs contained TPH ORO
concentrations above the 10 mg/kg State Action Limit. The B1 soil sample also contained
concentrations of benzene (0.0062 mg/kg) and total chromium (5.59 mg/kg) which are above
their STG MSCCs (0.0056 mg/kg and 5.4 mg/kg, respectively). With the total chromium levels
exceeding STG MSCCs, the sample was analyzed per 7196A for total hexavalent chromium. The
reported concentration of this compound (1.18 mg/kg) does not exceed its STG MSCC. TPH
GRO and/or DRO violations were also reported for soil samples collected adjacent to the diesel
and gasoline USTs, along their associated product lines, and beneath two of four dispensers.
Soil analytical results are depicted along with soil boring locations on Figure 4.
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
2
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
With four potential source areas located on the property (gasoline USTs, diesel UST, orphan
USTs, and piping system}, Terraquest progressed to a Phase II LSA which included the
installation of a groundwater monitoring well at each potential source. Further information
regarding the Hasty Mart #23 site check can be found in the Site Check Report on file with the
NCDWM-UST Section, submitted by Terraquest on December 30, 2014.
3.0 RISK CHARACTERIZATION AND RECEPTOR INFORMATION
On May 12, 2015, in order to determine the risk classification of the site, Terraquest personnel
performed a reconnaissance of properties within a 1,500-foot radius of the source area. The
reconnaissance effort consisted of obtaining tax department and local zoning information on
properties and conducting door-to-door visits of certain properties within 1,500 feet of the
source area, in addition to collecting other pertinent information from the appropriate local
and state officials. Terraquest personnel inspected all properties within 1,500 feet of the site
and attempted to contact all of the property owners within 1,000 feet in person. Property
owners were questioned, if available, as to the source of their water and if any water supply
wells were located on their property. If owners/occupants were not home, a survey form was
left at their residence or forwarded to the property owners through the mail. In all cases,
Terraquest also conducted a visual survey of the property. A less detailed reconnaissance effort
was conducted for properties located 1,000 to 1,500 feet away from the site.
No water supply wells were identified within 1,500 feet of the source area. The site and
surrounding properties obtain water from the City of Goldsboro's municipal supply network.
Municipal water is sourced from the Neuse River. The site is not located within a wellhead
protection area. The site vicinity and surrounding properties are presented on Figure 2.
Surrounding property owners/occupants are detailed in Table 2.
As part of the reconnaissance effort, Terraquest also searched for any surface water bodies
within a 500-foot radius of the site. No surface water bodies were identified within this search
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
3
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
area. The nearest surface water body is an unnamed tributary of Stoney Creek located
approximately 900 feet to the north.
The site is located in the Coastal Plain Physiographic Province. The United State Geological
Survey Professional Paper 1401-1, "Hyrdrogeologic Framework of the North Carolina Coastal
Plain, Regional Aquifer-System Analysis," indicates the site is underlain by a phreatic aquifer
that is underlain by the Black Creek Aquifer of the Coastal Plain. Based upon a review of Plate 6
from the 1401-1 paper (the closest cross-section to the subject property), the release area does
overlie a recharge area for the Black Creek Aquifer, the shallowest aquifer believed to be
underlying the release area. According to the log of well 152 on Plate 6, the phreatic aquifer
begins at approximately 50 feet above mean sea level, infiltrates the Black Creek Aquifer below,
and is then confined from further vertical progression by the Upper Cape Fear Confining Unit
which begins at a depth of 25 feet above mean sea level. Interpretations from well 152 are
approximate given its distance of 4 miles from the site. This site is not located in a wellhead
protection area.
Land usage in the surrounding vicinity is a mixture of shopping center (SC) and general business
(GB) properties along N. Berkeley Blvd. Residential properties (R-6) are located outside of 500
feet to the northwest and southeast. The subject property is zoned shopping center (SC).
Zoning designations are depicted on Figure 2.
This site meets qualifications of Low Risk with an industrial/commercial land-use classification
according to the NCDWM-UST's Guidelines. This ranking stems from the absence of any active
sole source water supply wells within 1,000 feet of the source area, absence of any water
supply wells within 250 feet, and the absence of residential properties within 500 feet of the
release source. To help in the risk classification of this site, a completed Limited Site
Assessment Risk Classification and Land Use Form has been included as Appendix B.
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
4
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
The closest residence is located less than 700 feet to the southeast of the site. The closest
place of public assembly, excluding restaurants, is the Berkeley Mall located approximately 725
feet to the northeast of the site. The closest school is the Summit Christian Academy located
approximately 3,200 feet to the east of the site.
4.0 SITE GEOLOGY AND HYDROGEOLOGY
The site lies in the Black Creek Formation of the Coastal Plain physiographic province of North
Carolina. According to the Geologic Map of North Carolina (Brown, et. al, 1985), the site is
underlain by clay, gray to black, lignitic; contains thin beds and laminae of fine-grained
micaceous sand and thick lenses of cross-bedded sand.
Monitoring Well Installation
On May 12, 2015, Terraquest personnel supervised the installation of four Type II groundwater
monitoring wells (MW1 -MW4) in the vicinity of the potential source areas. All of the
monitoring wells were installed with hollow-stem augers using a Geoprobe Model 7728DT
drilling rig operated by an NC-licensed driller. All of the Type II wells were constructed with a
screen interval that brackets the water table. After the construction of each monitoring well,
Terraquest developed the wells to allow for the removal of fine sediment that might clog the
screened portion of each well. Construction details for these monitoring wells are listed in
Table 3. Well construction records and boring logs are included in Appendix C.
The following lithologies were encountered at the site during the advancement of soil borings
and installation of monitoring wells:
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
5
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
0'-8' below ground level (BGL):
SAND (SP)
Mostly dense poorly graded black sand with some clay. Soils become moist at 4
ft BGL
8' -13' BGL
SAND {SP)
Dense poorly graded tan/black sand, with some quartz gravel, and few clay.
Site topography is depicted in Figure 1. Monitoring well locations are shown on Figure 3.
Monitoring well construction information is provided in Table 3. Well construction records and
boring logs are included in Appendix C. The monitoring well installation protocol utilized by
Terraquest is detailed in the technical methods and standard procedures in Appendix A.
S.O SOIL INVESTIGATION
Prior to installation of monitoring wells MW1 -MW4, a soil boring was advanced at each
location to a depth of 5 ft BGL Soil samples from the 2' to 3' interval were collected, placed
into a sealable plastic bag, logged for lithology, and screened with a PID. The requested
laboratory analyses are as follows:
MW1 {2-3): 8260, 8270, VPH, EPH, Total Cr, & Total Hexavalent Cr.
MW2 {2-3): 8260, 8270, VPH, & EPH
MW3 {2-3): 8260 & VPH
MW4 {2-3): 8260 & VPH
Analytical results of soil samples collected during the LSA revealed STG MSCC violations from
the MW3 {2-3) and MW4 {2-3) soil samples for concentrations of benzene and total xylenes.
No STG MSCC violations were reported in the MW1 {2-3) and MW2 {2-3) soil samples. Soil
Phase I limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
6
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
analytical results are summarized on Table 4 and Figure 4. The analytical report is included in
Appendix D.
6.0 GROUNDWATER INVESTIGATION
On May 12, 2015, Terraquest personnel collected a groundwater sample from monitoring wells
MW1-MW4 using the standard sampling protocol detailed in Appendix A. Prior to sampling,
Terraquest purged the monitoring wells of at least three well volumes using a new disposable
bailer. The purge bailer was also used to retrieve a representative groundwater sample.
The collected groundwater samples from both sample events were placed in laboratory-
prepared sample containers, labeled, packed in ice, and shipped to a North Carolina-certified
laboratory for analysis prior to the expiration of the analytical method's hold time. Requested
laboratory analyses for each groundwater sample are as follows:
MW1: 62008, 625 8NA + 10 NTP, VPH, EPH, & Total Pb and Cr
MW2: 62008, 625 8NA + 10 NTP, VPH, & EPH
MW3: 62008, VPH, 504.1 targeting ED8, & Total Pb
MW4: 62008, VPH, 504.1 targeting ED8, & Total Pb
Analytical results of the groundwater samples collected from monitoring wells MW1-MW4 are
as follows:
>GCL: None
>2L Standards: MW2, MW3, and MW4
<2L Standards: MW1
The greatest levels of contamination were reported in the monitoring wells MW2 and MW3
groundwater samples. Monitoring well MW2 is located adjacent to the diesel UST and MW3 is
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
7
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
located to the east of the dispensers. To date, no overt release incident has been documented
near these portions of the UST system. Groundwater analytical results are summarized on
Table 5 and on Figure 5. The analytical report is included in Appendix D.
7.0 GROUNDWATER FLOW
Terraquest personnel surveyed the top of the well casing elevations for monitoring wells MW1
through MW4. Prior to purging and sampling any of the monitoring wells on May 12, 2015,
Terraquest personnel measured the depth to water in each monitoring well. Those
measurements were used in conjunction with established casing elevations to determine the
direction of groundwater flow. A review of the potentiometric surface map indicates
groundwater flow is directed toward the north-northeast. Figure 6 depicts the May 12, 2015
potentiometric surface map. The top of the well casing elevations and depth-to-water
measurements are summarized in Table 3.
8.0 CONCLUSIONS AND RECOMMENDATIONS
Terraquest performed various activities associated with the completion of a Phase I LSA.
Primary assessment efforts focused on determining potential receptors in the area as well as
determining onsite soil and groundwater quality; both critical steps in determining the risk
ranking of the site. Terraquest concludes:
• Analytical results of soil samples collected during the previously completed site check
revealed TPH concentrations above the State Action Limit in 19 out of 22 collected soil
samples. Analytical results of soil samples collected as part of this LSA revealed
contaminant concentrations above the STG MSCCs in two of the four samples. No
detected contaminant concentrations exceeded the Residential MSCCs.
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
8
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
• Analytical results of the collected groundwater samples revealed 2L Standard violations
in three out of the four monitoring wells, with the greatest levels of contamination
being observed at monitoring wells MW2 and MW3.
• No water supply wells were identified within 1,500 feet of the site. With the absence of
water supply wells within the search area and properties within the vicinity of the
release being commercial, the site should be ranked "Low" Risk with a
commercial/industrial land use classification. The release incident can be closed out.
• For site closure, a Notice of Residual Petroleum (NORP) will need to be completed due
to the presence of in situ soil contamination above the STG MSCCs and groundwater
contamination above the 2L Standards. The NORP would establish the location the
impacted soils and decree that if the soils were to be removed they would have to be
disposed of in an NCDWM-UST-approved manner. Also, the NORP would put a
restriction on any future groundwater use. Once a NORP is completed, a "Notice of No
Further Action" (NFA) letter will be issued for the release incident by the NCDWM-UST.
Once an NFA is issued, public notification will be completed and the monitoring wells at
the site will be abandoned in accordance with the Title 15A NCAC 2C regulations.
9.0 LIMITATIONS
This report is limited to the investigation of dissolved petroleum hydrocarbons, such as
gasoline, in groundwater and does not imply that other unforeseen adverse impacts to the
environment are not present at or around the site in question. In addition, subsurface
heterogeneities not identified during the current study may influence the migration of
groundwater or contaminants in unpredicted ways. The limited amount of sampling and
testing conducted during this study cannot practically reveal all subsurface heterogeneities.
Furthermore, the subsurface conditions, particularly groundwater flow, elevations, and water
quality, may vary through time. The opinions and conclusions determined in this report are in
accordance with industry-accepted geologic and hydrogeologic practices at this time and
location. No warranty is implied or intended.
Phase I Limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
9
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
REFERENCE
Brown, Philip M. et al. 1985. Geologic Map of North Carolina, 1: 500,000 Scale. North Carolina
Department of Natural Resources and Community Development.
North Carolina Administrative Code, Title 15A, Chapter 2, Subchapter 2L, Section .0202,
November 20, 1998, "Classifications and Water Quality Standards Applicable to the
Groundwaters of North Carolina".
North Carolina Department of Environment and Natural Resources, Division of Waste
Management UST Section, UST Section Guidelines for Assessment and Corrective Action
for UST Releases, August 1, 2012.
United State Geological Survey Professional Paper 1401-1, "Hyrdrogeologic Framework of the
North Carolina Coastal Plain, Regional Aquifer-System Analysis," Plate 6, 1996.
USGS 7.5-Minute Quadrangle Topographic Map, Northeast Goldsboro and Southeast
Goldsboro, North Carolina.
Wayne County Geographical information System Department.
Phase I limited Site Assessment
Sampling Event: May 12, 2015
Report Prepared: June 4, 2015
10
Wayne Oil Company, Inc.
Hasty Mart# 23
Goldsboro, NC
TABLES
Table 1 SITE HISTORY (UST SYSTEM INFORMATION)
Date: 5/29/15 Incident Name: Hasty Mart #23 Incident No. 38538 Facility ID No: 0-00S354
. . Capa~;lty
UST Product . . (Gallon's) Dimensions Date Installed Date Closed Release Discovered
T1 Gasoline 4,000 64" X 24' 5/8/63 Active Yes
T2 Gasoline 3,000 64" X 18' S/9/63 Active Yes
T3 Gasoline 3,000 64" X 18' 5/10/63 Active Yes
T4 Gasoline 3,000 64" X 18' 5/11/63 Active Yes
TS Gasoline 3,000 64" X 18' S/12/63 Active Yes
T6 Highway Diesel 4,000 92" X 10' 5/2/85 Active Yes
T7 Heating or Waste Oil 280 36" X 62" unknown Closed In Place Yes
T8 Heating or Waste Oil 280 36"x62" unknown Closed In Place Yes
T9 Heatlng or Waste Oil 500 4S.5" X 76" unknown Closed In Place Yes
Notes:
1. Information obtained from the North Carolina UST Database Records and field observations.
2.T=UST
Table 2 SURROUNDING PROPERTY OWNERS
Date: 5/29/15 Incident Name: Hasty Mart #23 Incident No.: 38538 Facilitv !0 No. 0-00S354
MapiO Tax Parcel Nu~~er _(PIN
Number Pioperty (A•mer Property Owner Address Property Address
1 P.O. Box 10767 503 N. Berkeley Blvd
3519434089 NORFAM, llC Goldsboro, NC 27532 Goldsboro, NC 27534
2 3S19432272 Norwood,CharlesSJr P.O. Box 10767 Cashwell Dr
Goldsboro, NC 27532 Goldsboro, NC 27534
3 3519421849 K2 Properties, LLC P.O. Box 167 435 N. Berkeley Blvd
Winston-Salem, NC 27102 Goldsboro, NC 27534
4 3519422648 Cook out Goldsboro, Inc 15 Laura ln 432 N. Berkeley Blvd
Thomasvi!fe, NC 27360 Goldsboro, NC 27534
5 3519424758 KS Associates, LLC 303 E Wacker Drive St 500 N. Berkeley Blvd
Chicaeo, ll60601 Goldsboro, NC 27534
SITE . 3519433021 NORFAM, LLC
. P.O. Box 10767 501 N. Ber_kele'y Blvd
GoldsbOro, NC 27532 Goldshoro, NC 27534
Notes:
1. Information gathered from field Interviews and Wayne County Geographic Information System.
2. MAP ID numbers corresoond with those disolaved on Figure 2.
=below ground surface
!Table: 4
loate: 5/29/15
. I ·. . ·.
I I
I I
·.
·.
.· I Method I. ; !1 .; ;
• Sa mole ID Date Collected Sa mole leoth
MW1 5/12/15 2'-
~-M~~n~_S.2~~~~4---y~~··-~-+o~_>"-~9
MW3 5712715 Z'--. u.071 0.015 .70£
MW4 S/IiJis 2'-3' 0.068 0.11 i,31)
Soil to · MSCC 0.0056 4.3 4.9 4.6
I MSCC 18 1,200 1,560 3,129
I MSCC 164 32,000 40.000 81.760
Notes:
1. All results in mg/kg =parts per million
12.' Boid denotes a' COffipo'u~'d detection. Sh~dingdenote~ a STG-MSCCvioiat'ion.
!3. <-denotes less than sample detection limit.
)4. Sample depths are in feet below ground level. Is. MSCC = Maximum Soil Contaminant Concentration
6. "J" =Indicates an estimated value
·.
.
.··
l···.l
.0055
0.02
0.091
350
3,100
7. "l" =The LCS data for this analytical batch was reported above the laboratory control limits.
8. "F" = RPD exceeded lab control limits.
9. "·"-Indicates analvte not tested per that method.
uc SOIL SAMPliNG RESULTS
Incident Name: Hasty Mart #23 Incident No.: 38538 Facility ID: I . I . . . ..... . I··'{ . . .·· . .
. . · . . • I .· ··._ .•.
.
I ; .· ;·· .; ; I ; ;··.·· .··. -~ . · ... ··· ~ ~-. ~-<
.
~ ~
. ..
~ ~ c c ~ ~ N N c c ~ ~ .0 .0 > > ~ ~ .., ..,
E E
i!= ~ ~-"' "' H' H'
~ ~
c " ~ '§
~ 6 ~ ~ e ~ a. ]-
5! ~ 6. :2
E ~ .E
E e
~ ~ .E u
~ e c ~ ~ -, j > m X ~ "'
~ • i3 • i3 • u 'jJ u ~ u ~ "' .., . ., m ~ m E m ~ ~ a. E ~ ~ a. i ~ ~ ~ ~
N n ~ u
. 1011 0.' 141 1 <0.000671 <0.0018 1 <0.00065 <10.9 <10.9 <21.7 5.36! 0.929 J
0.· 136 I<, I <0.0016 _, I <C.00057 0.0034 I <o.oos57 <( 5S7 <11.0 <11.0 0.746X <22.1 --
148 LF 0.
174 LF ).14
0.37 24
i=
4.3
).0019
).0022
3.3
0.058 11.9 -3.2 -
0.064 32.8 19 - -4.82 -
85 8.3 6s 541 S40 # 31 31
--
--
s.4 5.4
l.013 J.OM I<~~==~J~.OOB~22/,Z:-:j=J~J.O@c4~1~<rl.ruY~l7~R=±~:t~~:t~~~~~~~~~~==~~t:t:~~==~~==~~ l.015 o.015 1 o~ <0.0092 1-0.042
1.7 0.12 "'0:02 0.16 1.7 o:oo74
156 14,000 626 626 1,564 100 85 313 626 1.1 782 782 939 1.500 1,500 31.000 469 469 47 47
4,088 360,000 16,350 16,350 40,880 4,000 763 8,176 16,350 10 20,440 20,440 24,528 40,000 40,000 • 810,000 12,264 12,264 1,226 1,226
Table 5 SUMMARY OF GROUNDWATER SAMPLING RESULTS
Date: 5/29/15 Incident Name: Hast., Mart#23 Incident No. 38538 Facility 10 No.0~005354
I . .. •· I .
... . .. I···· . .. .. . .. . · . . I . . . . I
•• I .· ;! ; .
~
••••••••
I I I I ;;:. I
.. . ~ ~ ~ fu ~ ~ N > > w ;;: w . >e. <l <l <l <l ~ fu ~ fu fu m ~ m m ~ m ~ ro m ~ m ~ ro "' "' _: __ -~ ro z z z z w w w ~ ro ro
0 g 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m 0 0 0 0 I 0 0 .. 0 0
Arlalvtical Method ---0 ~--_ 0 0 0 0 0 0 0 0 0 :--~ ~ 0 ... ~ ~-·(;l --w );:· ~ <l ~· <l <l <l <l ~ M
N N N N N N N N l;j l;j N l;j N "' "' "' "' "' 0 0 0 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~
Contaminant of Concern
• • 0 0 • • • ~ ~ 0 0 0
Q • 0 0 0 • • 0 " " • • 0 % • • 0 • ] " " ~ 0 0 • • D D • £ 0 " " ~ ~ ~ ~ , 0 > > ~ E • ~ ~ ·~ ~ ~ ~ ~ ~ g ~ • ~ 0 0 ~ • ~ ~ >-~ ~ ~ ~ ~ .e-e c • • • e c 0 " ro >-~ ~ .e-e ~ 0 0 D ~ D • • E E ~ 0 ~ ~ ~ " <l E • 0 • 0 z. > ~ 0 • "" > > ~ " ~ <l N ,
0 • • >-~ 0 ~ e '5 ~ > ~ ·o E ~ ~ N "' m 0 N .E ~ 0 D X w ~ ~ , e e ~ ~ .. 0 " "' ~ M rl ~ rl u • >-.. ro 'Z i ~ 0 ~ ~ " :i ~ ~ rl e v , 0 ~ 1< &: ~-"' "' m • 0 ~ 15 ~ w m :c ~ N' m' " rl iil ~ !l Wei!ID Date Collected ro ~ "' ~ "' ~ 0. ~ u z c .-1 rl' rl 0. m u u u u u
MW1 5/12/15 <0.119 <0.0570 <0.0920 <0.298 <0.169 <0.0920 <0.352 <0.378 <0.0920 <0.172 <0.0980 <0.0890 <0.0540 <0.0940/<1.43 <0.0650 <0.103 <0.0870 <2.39 <1.31 <1.12 <2.39 <0.0150 <0.0150 <98.5 <98.5 <0:905 <98.5 -0.0979 <0.00330
MWl 5/12/15 36.4 9570 593 0 2,7000 <0.169 <0.0920 14.4 7.67 J 4.41 1.63 37.2 5.2 <0.0540 2380/70.1 119 7620 238 5.68J 3.86J 8,08J 37.5 207 2,700 <96.6 <96.6 2,140 <96.6 -
MW3 S/12/15 . 7360 4,6300 1,2700 6,6100 29 35.9 10.7 <0.378 4.41 0.320J 39.5 4.19 <0.0540 549 0/ ~ 1420 .··i,i90D 299 D --3,370 3,800 --2,950 <0.00612 <0.0330
MW4 5/12/15 5.77. <0.0570 8.37 22.85 3.19 1.08 <0.352 <0.378 <0.0920 <0.172 <0.0980 <0.0890 <0.0540 1.171i-1.12 2.72 <0.0870 ---19.9 35 --21.8 <0.00608 -<0.00330
2LStandard 1 600 600 500 20 70 6,000 4,000 70 70 70 25 0.7 6 70 400 400 100 1 30 40 400 700 700 10,000 200 200 0.02 10 15
GCL 5,000 260,000 84,500 85,500 20,000 70,000 6,000,000 4,000,000 8,500 70,000 25,000 11,700 700 6 000 30,000 28,500 25,000 100,000 1,000 12,500 NE NE NE NE NE NE NE so 10,000 15,000
Notes:
1. All results in IJ.g/L
2 .. B_()l?_denote_s a compound det~ction
3. Shading denotes·-a 2l Standard violation
4. <-denotes less than sample detection limit
5. NE-Not Established
6. "0" "'Indicates the samples were dlluted due to targets detected over the highest point of the caliration cuNe.
7. 'T-Indicates an estimated value
8. "-"-Not analyzed per this method.
FIGURES
MAP SOURCE: USGS 7.5 MINUTE TOPOGRAPHIC -NORTHEAST GOLDSBORO & SOUTHEAST GOLDSBORO, NC
GRAPHIC SCALE
0'
TERRA~uest -----======== =---iii :::::-.-. ; ,., ----iiiiiii£--~ ---~ ·---~ ENVIRONMENTAL CONSULTANTS, P.C.
2,000' 4,000'
SITE LOCATION MAP
'lAYNE OIL COMPANY, INC.
PROJECT NO. 07814
HASTY L'ART #23
501 N. BERKELEY BLVD
GOLDSBORO. WAYNE COUNlY, NC
DRAWN BY: JTL
SCALE: 1" • 2,000' CHECKED BY: VJB
DATE:
riGURE NO.
GOLDSBORO. NC
5/29/15
LEGEND /ZONING
GRAPHIC SCALE
G)CORRESPONDS TO MAP ID IN SURROUNDING
PROPERTY OWNERS TABLE
SC: SHOPPING CENTER
GB: GENERAL BUSINESS
R6: RESIDENTIAL
0&1: OFFICE & INSTITUTIONAL
o' 200' 400'
1" = 400'
SITE VICINITY MAP
HASTY MART 23 TERRAguest ---c:=s=•' ~ :;; .. __ zatf ~ ~ !!! a---=r:!
501 N. BERKELEY BLVD
GOLDSBORO, WAYNE COUNTY, NC
WAYNE OIL COMPANY, INC.
ENVIRONMENTAL CONSULTANTS, P.C. PROJECT NO. 05813 DRAWN BY: JTL DATE:
SCALE: 1" = 400' CHECKED BY: JRG FIGURE NO.
800'
GOLDSBORO, NC
5/29/15
2
\
\
\
DIESEL
PRODUCT
LINE
HASTY MART #23
GAS &
DIESE L
DISPENSER
FORMER AUTO
SERVICE STATION
~·
/
\
/ GAS \
P~OCUCT
LINt~
/
\
~
CATHODIC
PROTECTION
LINES
LEGEND
• TYPE II MONITORING WELL
UST LEGEND
T1: 4,000-GAL GASOLI NE
T2: 3,000-GAL GASOLINE
T3: 3 ,000-GAL GASOLINE
T4: 3 ,000-GAL GASOLINE
TS: 3,000-GAL GASOLINE
T6: 4,000-GAL DIESEL
T7: 280-GAL HEATI NG OIL/WASTE
T8: 280-GAL HEATING OIL/WASTE
T9 : 280-GAL HEATING OIL/WASTE
GRAPHIC~S.:....:C~AL~E--~
o· 10' 40'
OIL
OIL
OIL
u z
0 1.{)
gn~ m N Vl '-.. 0 1.{) _J
0 0 . 0 z
MW2
MW1
MW4
\
\
\
~ s Nul c•l Meflod :::
Con~tT'Jn1nt of Concern
i § ~ ~
<().CJOOH 0.0012
s 12 15 0.00079 0.0031
s 12 15 2'·3' 0.071 0.015
S 12 I S 2'-3' 0.063 0~1
Soli to roundh'JtcrMSCC 0.0056 4.3
~tt.lden~l MSCC 18 uoo
~
~ ~ !
<0.00()..l7
<O.OOC>-'1
0..90 0
uo
4.9
l,S60
HASTY MART #23
FORMER AUTO
SERVICE STATION
84 ~~?.?\, MW2~ ~ 85 \'
~ \'
0 :;! I X
~ !>
~ s ~ e:. ~ 0 < ::: :!!
,; ~ t f i 2 ~ 6 < ~ :c Q ! ~ g :. z 1l
<0.001609 <()CJOOS! <00011 <0.0591 <0.00625 <0.00625
0.002582 <0.00051 <0.00095 <00591 <0. SS7 <0.0557
4.70 D 0.0055 o.oo:n. 11.9 S.22
7.30 0.02 <0.0092 3U 8.99
4.6 0091 0.16 68 540
3,129 3SO 313 939 1,500
86 . \'
\' \~ /
~ e:. 0 < :!!
1 < q
f)
<10.9
<11.0
540
l,SOO
/ \'
5 e 0 .. :.
~ ~ < 0 ~
<10.9
<11.0
•
31,000
87 v~ . \
X ~ !> e 0 .. e:. ~ :. :.
g
i e e e .. .. ~ ~
<0.0020.! <21.7
0.746X <22.
3.2
U2
31 31
469 469
~-L ~ -~21
~ ~ §
~ "l E e 1 6 ] 6 ~ ! ~
S.l6J 0.929J
5.4 5.4
47 47
"---s'{ ?-'{-.<:::; \)s
\
\
\
,)
\
\ y
LEGEND
~ TY?E II MONITORING WELL
e SOIL BORING LOCATION
RESULTS <10 MG/KG TPH
AND/OR <STG MSCCs
e SOIL BORING LOCATION
RESU LTS >10 MG/KG TPH
AND/OR >STG MSCCs
SOIL BORINGS B 1 -B 1 7 WERE ADVANCED
DURING THE SITE CHECK.
SOIL BORINGS MW1 -MW4 WE RE ADVANCEC
DURING THE LSA.
ANALYTICAL RESULTS IN MG/KG.
INCLUDED TABLE SHOWS RESU LTS FOR BTEX,
MTBE. NAPHTHALENE, ALIPHATICS, AROMATICS,
AND CHROMIUM FOR LSA SOIL SAMPLES.
STG MSCC VIOLATIONS ARE SHADED.
SUMMARY OF ANALYTICAL RESULTS ARE IN
TABLE 4.
UST LEGEN D
T1: 4,000-GAL GASO LINE
T2 : 3,000-GAL GASO LINE
T3: 3,000-GAL GASO LINE
T4: 3,000-GAL GASO LINE
TS: 3,000-GAL GASO LINE
T6: 4,000-GAL DIESEL
T7: 280 -GAL HEATING OIL/WASTE OIL
T8: 280 -GAL HEATING OIL/WASTE OIL
T9: 280-GAL HEATING OIL/WASTE OIL
GRAPHIC SCALE
~ o· 10' 20' 40'
(/)
u z
~ or:= ~ ::J z ifJ n m ::J N 0 w '*'i:J u
0::: f-_J w o:::w z
__j <{ ~ >-<t: ::::!:0:::<{ u >-~:!;
u z
lf)
0 gs"":;;-m N Ul ......... 0 lf)
_J
0 <.:lei :z
w
0::: w ~ ';{ c;: 0
m _J
' f-
::::!: '
1-G ·a >-<{ z 0:::
__j I 0 <t: ~ m OUl Z lf)o. <{ ..JU ozt-+-.. o -__j
0
(/)
r: "" ~ z co <{ I'-~ 0
0 u
0
_J z
6 f-
w U
z '=5 ::J ~ ~ ~
cj a.: g
~ ...J :::> (/) z 0 (.)
~ z w ::iE z 0 0:: ~ w
(r6\
MW2.u~
"' "' "' "' "' 0 0 0 0 0 0 0 0 0 0
Anal leal Method N N N N N lD lD lD lD lD
Contaminant of Concern
., ~ § fii ., ., c ~ c c ., ., ., ..0 w ~ :::> > ~ 10! ~ .t:. ~ WeiiiD Date Coli ected "' .t: ::E
MW1 5/12/15 <0.119 <0.0570 <0.0920 <0.298 <0.169
MW2 5/12/15 36.4 957 D 593 D 2,700 D <0.169
MW3 5/12/15 736 D 4,630 D 1,270 D 6,610 D 29
MW4 5 12 15 5.77 <0.0570 8.37 22.85 3.19
2LStandard 1 600 600 500 20
GCL 5,000 260 000 84 500 85 500 20 000
HASTY MART #23
/ / _.
/ / 0 /' 0
/
~ "' "' N le. ~ "' "' "' 0 0 0 "' 0 0 0 "' N N N N lD lD lD lD
.,
~ .,
c ~ ., Ri ., ..0 fii £ > .t:. ., N £ a. c ~ ., ., ..
..0 E c Ri > ~ > £ a. .c:
.t:. ~ tl a. ~ ~ .. 0.. N' z C: .... -....
<0.0940/<1.43 <0.0650 <0.103 <1.31
238 D/70.1 119 762 D 3.86J
549 0/-142 D 1,190 D
1.17 J • 1.12 2.72
6 70 400 1
6 000 30 000 28 500 1000
FORMER AUTO
SERVICE STATION
/ ~ \\
\\
/\(
\\
:I: 0..
~ > 0.. w "' 0 "' <t N ::E lD
.,
ii Ri "' £ u .t:. . .,
a. .. .. .t:. c -~ > <( .t:. tl ~ ::E ~ ,.:,
<1.12 <0.0150
8.08J 207
3,370
19.9
30 400
12 500 NE
/
:I: 0.. > 0.. w 0 <t ::E
"' u ·p .. .c: -~ <(
N .... u en u
<0.0150
2,700
3,800
35
700
NE
/
/
:I: 0.. w
0.. w
0 <t ::E
"' u ·p .. .c: -~ <(
00 .... u en u
<98.5
<96.6
700
NE
\
\
:c 0.. w
0.. lU
0 <t ::E
"' u ·p .. .c: a. ~
lD 0 0.. ... u
<98.5
<96.6
10 000
NE
\
:I: ~ 0.. w 0 <t ::E
lj ·p .. E 0 ~
0 .... u f)
<0.005
2,140
2,950
21.8
200
NE
/
~W4
\
\
_.)
:I: 0.. w
0.. w .... 0 .; <t ::E 0 "'
"' u ·p .. E 0 ~
N N u ,.!, "' .... @ u
<98.5
<96.6
<0.00612
<0.00608
200 0.02
NE so
"' 0 .... 0 "'
E :::> .E
~ .c: u
0.0979
10
10 000
\
"' 0 .... 0 lD
"0 .. ~
\
~
<0.00330
<0.0330
<0.00330
15
15,000
LEGEND -+ TYPE II MONITORI NG WELL
ANALYTICAL RESULTS IN UG/L.
INCLUDED TABLE SHOWS COMPOUNDS WITH 2L
STANDARD VIOLATIONS, ALIP HATICS, AROMATICS,
EDB, AND METALS.
2L STANDARD VIOLATIONS ARE SHADED.
SUMMARY OF ANALYTICAL RESULTS ARE IN
TABLE 5.
UST LEGEND
T1 : 4,000-GAL GASOLINE
T2: 3,000-GAL GASOLINE
T3: 3,000-GAL GASOLINE
T4: 3,000-GAL GASOLINE
T5: 3,000-GAL GASOLINE
T6: 4,000-GAL DIESEL
T7: 280-GAL HEATING OIL/WASTE
T8: 280 -GAL HEATING OIL/WASTE
T9: 280 -GAL HEATING OIL/WASTE
GRAPHIC SCALE
~-I
a· 10' 20' 40'
OIL
OIL
OIL
Q_
<(
2
(J)
f-_j
:=l
(J) w
0::::
0:::: w
f-<(
3: 0 z
:=l
0
0::::
C)
u z
u z
0 cr 0 rn Vl
0
...J
........
l{)Ol
N ........
l{)
0 <.:>a
~ z <( n. ~ 0 u
...J
i5
z
rn -,
~
;;...:
CD
0 w :::.:: u w
:I: u
<t
o:J
" 0
0 z
1-u w -,
0 cr n.
...J 1--,
;;...: ro
z ~ 0:: 0
0 N
w ....1 <( u Vl
APPENDIX A
2l Standard
2B Standard
AFVR
AST
BGl
BTEX
C&D
CAP
CSA
EPA
EPH
ESA
GCl
lEl
lSA
IPE
MADEP
MNA
MMPE
MSCC
MSl
MSW
MTBE
NC
NCAC
NCDENR
NCDOT
NCDWM-SW
NCDWM-UST
NCDWQ
NORR
NORP
NOV
NPDES
OVM
PID
PlC
POE
POTW
RBCA
RP
SVE
STG
TA
TCC
Terraquest
TPH
UST
VOA
voc
VPH
XP
ENVIRONMENTAL ACRONYMS
Groundwater Standards under Title lSA NCAC 2l 0.0202(g)
Surface Water Standards under Title lSA NCAC 2B
Aggressive Fluid-Vapor Recovery
Aboveground Storage Tank
Below Ground level
Benzene, toluene, ethyl benzene, xylenes
Construction and Demolition
Corrective Action Plan
Comprehensive Site Assessment
Environmental Protection Agency
Extractable Petroleum Hydrocarbons
Environmental Site Assessment
Gross Contamination level
lower Explosive limit
Limited Site Assessment
di-lsopropyl Ether
Massachusetts Department of Environmental Protection
Monitored Natural Attenuation
Mobile Multi Phase Extraction
Maximum Soil Contaminant Concentration
Mean Sea level
Municipal Solid Waste
Methyl tertiary-Butyl Ether
North Carolina
NC Administrative Code
NC Department of Environment and Natural Resources
NC Department ofTransportation
NC Division of Waste Management's Solid Waste Section
NC Division of Waste Management's UST Section
NC Division of Water Quality
Notice of Regulatory Requirements
Notice of Residual Petroleum
Notice of Violation
National Pollutant Discharge Elimination System
Organic Vapor Meter
Photoionization Detector
Programmable logic Controller
Point of Entry (water treatment system)
Publicly Owned Treatment Works
Risk Based Corrective Action
Responsible Party
Soil Vapor Extraction
Soil to Groundwater (MSCC)
Task Authorization
Target Cleanup Concentrations
Terraquest Environmental Consultants, P.C.
Total Petroleum Hydrocarbon
Underground Storage Tank
Volatile Organic Analysis
Volatile Organic Compound
Volatile Petroleum Hydrocarbons
Explosion Proof
TECHNICAL METHODS/STANDARD PROCEDURES
Equipment Decontamination
All soil sampling equipment utilized during site assessment activities is decontaminated according
to standard and accepted protocol. Cleaning solutions range from clean potable water to acidic
solutions or organic solvents depending on the contaminants present at the site. Equipment
utilized at sites, such as hand augers, contaminated with petroleum hydrocarbons, is generally
decontaminated with a low-sudsing detergent such as Luiquinox® and triple rinsed with distilled
water. Larger equipment, such as drill rigs and associated tools, is steam cleaned. All
decontamination procedures are completed within an established decontamination area which is
located away from the active study area. Frequency of equipment decontamination depends on
the nature of work being performed, but in no case is decontamination performed less frequently
than once per test (i.e., soil boring, well installation, sample collection, etc.). Equipment blanks are
collected as a quality control measure when required by job specifications.
Soil Boring Installation
Soil borings are completed using hand-operated sampling tools, truck-mounted drills, or
Geoprobe® drilling rigs depending on the depth of sample collection and other site-specific
conditions. Hand operated stainless-steel bucket augers are utilized to collect soil samples at
regular intervals to determine site stratigraphy and to test for the presence of volatile organic
compounds. Samples retrieved from the hand auger are necessarily disturbed during the augering
process, but can provide accurate information on soil type and contaminant concentrations when
properly interpreted. Soil samples from hand augered borings are generally retrieved at one to
two foot intervals.
Truck-mounted or Geoprobe® drilling equipment is often utilized when sample retrieval depths
exceed twenty feet or subsurface conditions prevent utilization of hand augers (i.e., buried rocks,
wood, bricks or other materials occur in the subsurface). Truck-mounted drilling rigs usually
retrieve soil via a hollow-stem auger/split spoon collection method. Geoprobe® rigs usually
employ a Macro-Core® tube retrieval system.
Hollow stem augers provide relatively undisturbed 2-foot cores of soil samples. Soil samples are
generally collected at five foot intervals utilizing standard penetration test procedures as defined
by the American Society for Testing and Materials (ASTM) or are pushed to the desired depth using
the head ofthe drill rig. The standard penetration test involves driving a 2" outside diameter by 1-
3/8" inside diameter split-spoon sampler a minimum distance of one foot with a 340-lb. slide
hammer falling a distance of 30 inches.
A Geoprobe® rig is a hydraulically-powered soil probing machine. The probe utilizes static force
and percussion to advance a small diameter sampling device into the subsurface. The sampling
apparatus provides relatively undisturbed 5-foot cores of soil samples. Soil samples are collected
continuously. The Macro-Core® tube contains an inserted poly-vinyl chloride (PVC) liner which
retains the soil sample as the tube is driven into the ground. The Macro-Core® tube is
decontaminated between each 5-foot sample interval in a soil boring using a Liquinox and tap-
water mixture. A new PVC liner is used to collect soil from each sample interval in a soil boring.
Soil samples retrieved from the hollow-stem augers or Geoprobe are then carefully described
according to the Unified Soil Classification System. Soil descriptions are recorded on a soil
boring log.
Soil Sampling
Soils to be analyzed by a North Carolina-certified laboratory are prepared according to the
specified analytical method. Initially, soil samples are removed from the ground using either a
hand auger, backhoe bucket, spilt spoon auger, or a Macro-Core® sampling tube. During the
removal, care is taken to keep the disturbance of the soil structure to a minimum to reduce the
loss of contaminants. Once removed, the samples are placed in the proper sample container for
the specified analytical method. For samples collected for the MADEP VPH and 8260 method, a
Terra Core® sampler is used to collect three 5-gram allotments of soil. All three allotments are
placed in methanol-preserved 40 ml vials. Also, two 5-gram allotments of soil are placed into
sodium bisulfate-preserved 40 ml vials (5-gram each vial) forthe 8260 low concentration method.
A 250-ml glass jar of the sampled soil is also collected to provide moisture content information.
Soils sampled for MADEP EPH, EPA Methods 8270 and TPH 5030 and 3550 are placed in a 250-ml
glass jar. TPH 5030 samples are preserved in methanol similar to the 8260 analysis. Field
personnel wear new, disposable latex gloves during the collection of each sample.
The soil samples are labeled with the sample location, sample identification, date and time of
collection, and the analytical method. The samples are placed on ice, sent to a laboratory, and
analyzed before the expiration of an analytical method's prescribed holding time. Chain-of-
custody documentation is maintained for each sample collected in the field.
If the soil is being sampled for volatile or semi-volatile compounds, a portion of the collected soil is
placed in a sealable bag and screened for volatile organic vapors. Head screening procedures are
described in the following paragraph.
Headspace Screening
Collected soil samples are routinely tested for the presence of volatile organic compounds (VOCs).
After retrieval from the ground, a portion of a soil sample is placed in a sealable plastic bag. The
soil samples are then set aside for approximately five minutes so that volatile constituents present
in the sample can reach equilibrium concentrations with headspace gases in the bag. Once a
suitable time period has passed, the probe of the sampling instrument, typically an Organic Vapor
Monitor (OVM) or a Photo Ionization Meter (PID), is inserted into the bag and the relative
concentration of total VOCs is measured and permanently recorded in a field note book. VOC
concentrations are measured using either a Thermo Electron Corp.lnnova Series catalytic OVM or
an I on Science PhoCheck PI D. Both the OVM and PID instrumentation are periodically calibrated
according to the manufacturer's recommended procedures.
The OVM and PID are qualitative tools employed to detect and estimate the concentration of
organic or hydrocarbon vapors. A thin probe is inserted through a small break in the seal of a
bagged soil sample. For the OVM, an air sample from the headspace of the bag is drawn through
the probe into an internal chamber where the vapors are catalyzed. The concentration of the
VOCs is registered on a digital scale in parts per million (ppm). For the PID, an air sample from the
headspace of the bag is drawn across the face of a lamp causing the sample to emit photons, the
presence of which are converted into a VOC ppm reading that is displayed. Oxygen levels are field
calibrated prior to each use. VOC calibration occurs periodically depending upon use by using a
span gas of known concentration in a process recommended by the manufacturer.
Well Installation/Construction
Monitoring wells are installed using hand-operated sampling tools, a truck-mounted drill rig, or a
Geoprobe drilling rig depending on the depth of well and other site-specific conditions. All
monitoring wells are installed according to the requirements of 15A NCAC 2C-Well Construction
Standards. Specifically, individual monitoring wells are constructed of 2-inch diameter, schedule
40 PVC casing riser and screen. The screen interval is generally 10 to 15 feet of machine slotted
PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the
screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above
the top of the screen. A one to two foot-thick bentonite pellet seal is then placed above the filter
pack. The remainder of the well annulus is completely filled with a Portland (Type 1/11) cement
grout mixture. A protective outer steel manhole, locking cap, and concrete pad is installed for
each well.
Type II Monitoring Well Construction
Single-cased monitoring wells are generally used in delineation of groundwater quality within the
surficial aquifer. The wells are constructed of 2-inch diameter, schedule 40 PVC casing and screen.
The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010".
Only flush threaded joints are used. The annulus space around the screen is filled with washed
filter pack No.2 sand. The filter pack extends one to two feet above the top of the screen. A one
foot-thick bentonite pellet seal is then placed above the filter pack. The remainder of the well
annulus is completely filled with a Portland (Type 1/11} cement grout mixture. A protective outer
steel manhole, locking cap, and concrete pad are installed for each well.
Type Ill Monitoring Well Construction
Double-cased monitoring wells are used in the delineation of groundwater quality within a deeper
portion ofthe surficial aquifer or an additional aquifer (e.g. aquitard, bedrock). A four to six-inch
outer casing is installed through the surficial aquifer until a sufficient depth or until the deeper
aquifer is encountered. The casing is secured with a Portland-grout collar that is tremmied into
the annular spaced from the bottom of the bore hole to the surface. Once the grout has
sufficiently cured, the bore hole is continued through the bottom of the outer casing to a depth
approximately 15 -20 feet beneath the outer casing. The inner casing is constructed of 2-inch
diameter, schedule 40 PVC casing riser and screen. The screen interval is generally 5 to 10 feet of
machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus
space around the screen is filled with washed filter pack No.2 sand. The filter pack extends one to
two feet above the top ofthe screen. A one to two foot-thick bentonite pellet seal is then placed
above the filter pack. The remainder of the well annulus is completely filled with the same
Portland grout mixture used in the outer casing. A protective outer steel manhole, locking cap,
and concrete pad are installed for each well.
Well Development
Following installation of each well, surging and pumping or bailing techniques will be used to
remove fines from the screened interval. Groundwater is removed from each well until clear
water is retrieved or a noticeable reduction in the amount of silt is achieved. Purged groundwater
is disposed of in an environmentally safe manner.
Groundwater Sampling
Petroleum Sites
Groundwater samples are collected from temporary or permanent monitoring wells according to
established sampling protocol. When multiple monitoring wells or sampling points are sampled,
sampling is completed beginning with the least contaminated well to the most contaminated well,
if it is known. When permanent monitoring wells for petroleum sites are sampled, the well is
purged of a minimum of three well-bore volumes prior to sample collection in order to assure that
sampled water is representative of aquifer conditions. In temporary wells, the first water which
migrates into the open borehole is sampled. Samples from both temporary and permanent
monitoring wells are collected using individually wrapped disposable polyethylene bailers byfield
personnel wearing disposable latex gloves. Only one well is sampled with a given bailer in order to
prevent sample cross-contamination. During both well purging and sampling, proper protective
clothing and equipment is used and is dependent upon the type and level of contaminants
present. Also, field personnel change gloves between different samples to reduce the chance of
cross-contamination. Water samples are transferred from the bailer to laboratory-prepared
sampling containers using slow emptying devices to reduce the chance of contamination loss
through volatilization. Preservatives, such as acids, are added to samples directly after they are
collected if in-field preservation is necessary. The samples are labeled with the project name,
project number, sample identification, required analysis, and date and time of collection. The
samples are placed on ice, sent to a certified laboratory, and analyzed before the expiration of an
analytical method's prescribed holding time. Chain-of-custody documentation is maintained for
each sample collected in the field.
Other Groundwater Sampling Protocols
When required by state or federal regulations, low-flow groundwater sampling procedures are
instituted. Groundwater samples collected in low-flow situations are collected using a peristaltic
pump. A peristaltic pump is a type of positive displacement pump. The fluid is contained within a
flexible tube fitted inside a circular pump casing. A rotor with a number of rollers attached to the
external circumference compresses the flexible tube. As the rotor turns, the part of tube under
compression closes thus forcing the fluid to be pumped to move through the tube. Groundwater
parameters such as water level drawdown, pH, conductivity, dissolved oxygen (DO) and turbidity.
Pumping rate, drawdown, and the time or volume required to obtain stabilization of parameter
readings can be used as a future guide to purge the well. Measurements are collected at a pre-
pumping established interval (typically five to ten minutes). Once all or a majority of the
parameters have stabilized for three successive readings, stabilization has been achieved.ln lieu of
measuring all five parameters, a minimum subset would include pH, conductivity, and turbidity or
DO. Three successive readings should be within± 0.1 for pH,± 3% for conductivity, and± 10% for
turbidity and DO.
Upon parameter stabilization, sampling is initiated. Sampling flow rate is maintained at the estab-
lished purge rate or is adjusted slightly to minimize aeration, bubble formation, turbulent filling of
sample bottles, or loss of volatiles due to extended residence time in tubing. The same device used
for purging is used to collect the groundwater sample. Generally, volatile parameters are sampled
first. The sequence in which samples for inorganic parameters are collected is not determined
unless filtered (dissolved) samples are collected. Preservatives, such as acids, are added to samples
directly after they are collected if in-field preservation is necessary. The samples are labeled with
the project name, project number, sample identification, required analysis, and date and time of
collection. The samples are placed on ice, sent to a certified laboratory, and analyzed before the
expiration of an analytical method's prescribed holding time. Chain-of-custody documentation is
maintained for each sample collected in the field.
During both well purging and sampling, proper protective clothing and equipment is used and is
dependent upon the type and level of contaminants present. Also, field personnel change gloves
between different monitoring wells or sampling points to reduce the chance of cross-
contamination. When multiple monitoring wells or sampling points are sampled, sampling is
completed beginning with the least contaminated well to the most contaminated well, if it is
known.
Stockpile Sampling
The number of composite samples collected from a stockpile or a total quantity of excavated soil is
based upon the cubic yardage. One composite sample is collected for every 100 cubic yards of
contaminated soil excavated. The volume of a stockpile or total quantity of excavated soil is
calculated by approximating the general geometry of a stockpile or estimating the capacity of the
dump trucks used for hauling. If a stockpile is sampled, a grid pattern is laid out on the stockpile,
dividing the stockpile into segments of approximately 200 cubic yards. Two soil borings are
advanced within a grid and three soil samples are collected from each soil boring at various depths.
The six soil samples are mixed into a composite sample by a trained TerraQuest technician. If
truck loads are sampled, an aliquot sample is collected from the hauling trucks at a frequency
based upon the capacity of the hauling trucks.
Aliquots are gently mixed into a composite sample by a trained Terra Quest technician. Every effort
is made to minimize the loss of contaminants through volatilization. The com posited soil samples
are jarred in the appropriate laboratory-prepared containers, labeled with the sample location,
sample identification, date of collection, time of collection, the analytical method, and the
preservative. The samples are placed on ice, sent to a laboratory, and analyzed before the
expiration of an analytical method's prescribed holding time. Chain-of-custody documentation is
maintained for each sample collected in the field.
Surface Water Sampling
Surface water samples, specifically samples from creeks or streams, are collected from a
moving/flowing portion of the creek or stream to ensure that stagnant water is not collected. Field
personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a
loss of volatile contaminants which might have been contained in the creek's/stream's water.
Samples are collected by field personnel wearing disposable latex gloves. Field personnel change
gloves between different locations to reduce the chance of cross-contamination. Samples are
collected directly from the appropriate creek or stream location and placed into the appropriate
laboratory-prepared containers. Preservatives, such as acids, are added to samples directly after
they are collected if preservation is necessary. The samples are labeled with the project name,
project number, sample identification, required analysis, and date and time of collection. The
samples are cooled on ice to approximately four degrees centigrade, sent to a certified laboratory,
and analyzed before the expiration of an analytical method's prescribed holding time. Chain-of-
custody documentation is maintained for each sample collected in the field.
Potable Well Sampling
Groundwater samples from potable wells are collected from sampling points, typically spigots,
located in the closest proximity to the potable well pump house as possible. Prior to sample
collection, the water is run for a sufficient amount of time to purge the bladder tank and assure
that sampled water is representative of aquifer conditions. Once purged, the flow rate is reduced
and samples are placed in the appropriate laboratory prepared containers and the appropriate
acid preservatives are added if preservation of the sample is necessary. The samples are labeled
with the project name, project number, sample identification, required analysis, and date and time
of collection. The samples are placed on ice, sent to a laboratory, and analyzed before the
expiration of an analytical method's prescribed holding time. Chain-of-custody documentation is
maintained for each sample collected in the field.
Public Water Supply Line Sampling
Groundwater samples from public water supply lines are collected from sampling points, typically
spigots. To sample the spigot, the flow rate is reduced and samples are placed in the appropriate
laboratory prepared containers. The samples are labeled with the sample location, sample
identification, date of collection, time of collection, and required analytical method. The samples
are placed on ice, sent to a laboratory, and analyzed before the expiration of an analytical
method's prescribed holding time. Chain-of-custody documentation is maintained for each sample
collected in the field.
Air Sampling
Air samples are collected with the aide of a manually operated MityVac® pump manufactured by
Pristech, Inc. The air sampling process begins by connecting a length of rubber hose from the
MityVac® pump to the port to be sampled, or by hanging the hose inside of an emissions stack in
such a manner as to ensure no outside air causes dilution. Another length of hose is fixed to the
outlet port of the pump and is connected to a new Tedlar bag. Once the pump is hooked up, a
valve on the Tedlar collection bag is opened and air is manually forced into the bag by the pumping
action of sampling personnel.
Field Measurements
Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen
concentration of a particular groundwater sample are taken directly after a particular monitoring
well has been adequately purged. This ensures that the groundwater parameter data collected is
representative of the aquifer conditions at a given location. Once purging of the monitoring well is
complete, the decontaminated probe head and cord of the appropriate unit is lowered into the
required monitoring well. If the depth to water in a specific monitoring well is greater than the
length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate
monitoring well and a representative groundwater sample is retrieved. A slow pouring device is
fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable
plastic cup. Groundwater parameter data are then collected from the groundwater in the cup
using the required unit.
For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is
utilized. This unit is periodically calibrated and maintained in accordance with the unit's
operations manual by field personnel. Prior to data collection, the unit is properly decontaminated
to prevent cross-contamination. The unit is decontaminated between each sample. The
procedure used for sample measurement involves lowering the meter's probe into the new,
disposable cup containing the groundwater sample to be measured and slowly stirring the probe
to force groundwater across the probe's membrane. The measurements displayed by the meter
are then recorded.
For dissolved oxygen concentration measurements, a YSJ® Model 55 Handheld Dissolved Oxygen
System is utilized. This unit is periodically calibrated and maintained in accordance with the unit's
operations manual by field personnel. Prior to data collection, the unit is properly decontaminated
to prevent cross-contamination. The unit is decontaminated between each sample. The
procedure used for sample measurement involves adjusting the unit for the correct altitude where
the sampling will take place and adjusting the reported units desired. Once this is done, the unit's
probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to
force the groundwater across the probe's membrane. The measurements displayed by the unit
are then recorded.
For turbidity measurements, a Hach 2100P Portable Turbidity meter or equal equivalent is utilized.
The unit is calibrated prior to use in accordance with the unit's operations manual by field
personnel. Groundwater samples are collected in glass containers for measurement by the
instrument. The glass containers are washed with bottled-water between each measurement
collection. Once the sample is collected and inserted into the instrument, the measurements
displayed by the instrument are then recorded.
APPENDIX B
NCDWM-UST Release Incident Number: 38538
Hasty Mart #23-501 N. Berkeley Blvd, Goldsboro, NC
Limited Site Assessment Risk Classification and Land Use Form
Part I -Groundwater/Surface WaterN apor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including any use~·
non-drinking purposes? YES 0
If yes, explain.
2.
No water supply wells are located within1,500 feet of the source area.
Is a water supply well used for drinking water located within 1,000 feet of the source t:::\
of the discharge or release? YES~
No water supply wells are located within 1,500 feet of the source area.
3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial
cooling water, filling swimming pools) located within 250 feet of the source area o~
release or discharge? YES~
No water supply wells are located within 1,500 feet of the source area.
4. Does groundwater within 500 feet of the source area of the discharge or release have the
potential for future use in that there is no other source of water supply other tha~
groundwater? YES~
Explain
Municipal water is available to the site and the surrounding properties.
5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space or pose any serious tlueat to public he~
public safety, or the environment? YES NO
Explain.
No areas of potential vapor accumulation were noted on the subject property.
6. Are there any other factors that would cause the discharge or release to pose an imm~·
danger to public health, public safety, or the environment? YES NO
If yes, explain.
NCDWM-UST Release Incident Number: 38538
Hasty Mart #23-501 N. Berkeley Blvd, Goldsboro, NC
Intermediate Risl<
7. Is a surface water body located within 500 feet of the source area of the dischar~
release? YES~
8.
If yes, does the maximum groundwater contaminant concentration exceed the surface
water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of I 0?
Is the source area of the discharge or release
protection area as defined in 42 USC 300h-7( e)?
If yes, explain
located within a
YES/NO
designated wei~
YESt~
The NC Department of Environment and Natuml Resources does not have any
wellhead protection areas listed for the vicinity of the site on their website located at:
http :I !swap. dell. enr.state.nc.us!swap _ applviewer.lz tm.
9. Is the discharge or release located in the Coastal Plain physiographic region as designated
on a map entitled Geology of N01ih Carolina published by the Department in 19Q,
~0
If yes, is the source area of the discharge or release located in an area in which there is a
recharge to an unconfined or semi-confined deeper aquifer that is being used~~ Tbe
used as a source of drinking water? ~ 1'~ 0
If yes, explain.
The phreatic aquifer does not have a confining unit between it and the Black Creek
Aquifer. The City of Goldsboro derives its rb-inking water from the Neuse River and
not from this aquifer.
I 0. Do levels of groundwater contamination exceed the gross
established (see Table 7) by the Department?
See Table 5.
contamination levels YES~
Part II -Land Use
NCDWM-UST Release Incident Number: 38538
Hasty Mart #23-501 N. Berkeley Blvd, Goldsboro, NC
Property Containing Source Area of Discharge or Release
The questions below pertain to the property containing the source area of the release.
I. Does the prope1iy contain one or more primary or secondary residences (pennane~t ·
temporary)? YES 0
Explain.
The site is a fuel retail facility.
2. Does the prope1iy contain a school, daycare center, hospital, playground, park, recree·
area, church, nursing home, or other place of public assembly? YES NO
Explain.
The site is a fuel retail facility.
3. Does the prope1iy contain a commercial (e.g., retail, warehouse, office/business space,
etc.) Or industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) Enterprise, an inactive commercial oJ~l!al
enterprise, or is the land undeveloped? ~0
Explain.
The site is a fuel retail facility.
4. Do children visit the property?
Explain. ~0
Children can visit the property.
5. Is access to the property reliably restricted consistent with its use (e.g., by fences, sec~! ..
persmmel, or both)? YES 0
Explain.
There are 110 restrictions to accessing the property.
Do pavement, buildings, or other structures cap the contaminated soil?
Explain.
The property's asplutlt parking lot caps fill)' contaminated soil.
~0
If yes, what mechanisms are in place or can be put in place to ensure that the
contaminated soil will remain capped in the foreseeable future?
Maintenance of the parking lot.
NCDWM-UST Release Incident Number: 38538
Hasty Mart #23-501 N. Berkeley Blvd, Goldsboro, NC
6. What is the zoning status of the property?
SC: Shopping Center
7. Is the use of the property likely to change in the next 20 years?
Explain.
The site will likely remain a fuel retail facility and convenience store.
Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area within 1,500 feet of the source area of the discharge or
release (excludes property containing source area of the release):
I. What is the distance from the source area of the release to the nearest pnmary or
secondary residence (permanent or temporary)?
The closest residence is located approximately 700 feet to the southeast of the release.
2. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home, or other place
of public assembly?
The closest place of public assembly is Berkeley Mall located 725 feet to the northeast
of the release area.
3. What is the zoning status of properties in the surrounding area?
Properties along N. Berkeley Blvd are primarily Shopping Center (SC) and General
Business (GB). Residential properties (R6) are located outside of 500 feet to the
northwest ami southeast.
4. Briefly characterize the use and activities of the land in the surrounding area.
The site and surrounding properties along N. Berkeley Blvd. are commercial properties
and shopping centers. The area is highly developed.
APPENDIX C
WELL CONSTRUCTION RECORD
This fom1 can be used for single or multiple wells
l. Well Contractor Information:
NICK PERRY
Well Contractor Name
3329
NC Well Contractor Certification Number
Terraquest Environmental Consultants, P.C.
Company Name
2. Well Construction Permit#:
List aT/ applicable well pamils (i.e. County, Stale, Variana, lnjeclim~ elc.}
3, Well Use (check well use):
Water Supply Well:
DAgricultural DMunicipaVPublic
DGcothcrmal (Heating/Cooling Supply) DResidential Water Supply (single)
DindustrialiCommercia\ DResidential Water Supply (shared)
Dirrigation
Non-Water Supply Well:
0Monitoring DRccovery
Injection Well:
OAquifer Recharge DGroundwater Remediation
OAquifer Storage and Recovery DSaHnity Barrier
DAquifer Test DStomnvuter Drainage
DExperimental Technology DSubsidence Control
OGeothennal (Closed Loop) OTracer
DGeothem1al (Heating/Cooling Return) OOther (explain under #21 Remarks)
4. Date Well(s) Completed: 5/12/15 Wcii!D# MW1,MW2
Sa. Well Location:
Hasty Mart #23 0-005354
Facility/Owner Name Facility ID# (if applicable)
501 N. Berkeley Blvd., Goldsboro 27534
Physical Address, City, and Zip
Wayne 3519433021
County Parcel Identification No. (PIN)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one !at/long is suftlcient)
35.3748 N 77.9454 w
6. Is (are) the well(s): 0Permaneut or OTemporary
7. Is this a repair to an existing well: DYes or [)No
If this is a repair, jill out knownlfel! com/ruction informal ion and explain/he nature of/he
repair zmda #21 remarks sec/ion or on the backofthisform.
8. Number of wells constructed: _2~~---~~----
For multiple injation or non-water supply wells ONLY with th~ same constmc1io11, you can
submit one form.
9. Total well depth below land surface: ~2::.@.;=::,.1,3:,t====,-----•(ft.)
For multiple wells list off d~plhs if differen/ (example-3@200' and 2@100')
10. Static water le\'el below top of casing: _:5:_·_:8:_4.:.'.:•.:3.:..9::...;1_t _____ (ft.)
lf\\"alerlewl is abow casing, 11se "+"
11. Borehole diameter: 8.5" (in.)
12. Well construction method: Hollow Stem Auger
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATERSUPPLYWELLS ONLY:
13a. Yield (gpm) -------Method oftest: --------
ft. ft.
ft. ft.
~ ==·
ft. ft. In. I
16.1NNER <:ASING OR' UBIN,G!!!l ~
ft. ft. I~
ft. ft. In.
17.SCREI~
I». M1o Soh. 40 PVC 3' ft. 13' ft. 2in
ft. ft. In.
~1' ft. I I Pour
11' ft. 2' ft. ! Pour
ft. ft.
12' ft. 13' ft. ~Sand Pour
ft. ft.
~ ft.
~
4' ft. SAND
14' ft. 13' ft. ~clav
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
/1
II I
22. .I
tJ.! 5/13/15
~ac·t-~r Date
By signing this 102(( :uy certify tlmtth~ mdl(s) was (uw~) co/JS/ntcted in accordanc~
with 15A l\'CAC .0100 or 15A NCAC 02C .0200 Well Com/ruction Standard5 and that a
copy of this record has been prorhf~d to Ilk' ~rei/ Olr/li!r.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBi\IITTAL INSTUCI'lONS
24a. For All Wells: Submit this fonn within 30 days of completion of well
constmction to the following:
Division ofWater Resources, Information Processing Unit,
1617 Mail Sen ice Center, Raleigh, NC 27699Ml6J7
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this fonn within 30 days of completion of well
construction to the following:
Dh·ision ofWater Resources, Underground Injection Control Program,
1636 .Mail Senice Center, Raleigh, NC 27699M1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion of
Ll~3~b~.~D~i~si~n~fe:c~ti~o~n~ty~p~e::.========-~A~I~n~o~u~n~t:~========J well construction to the co\mty health department of the county where constructed.
Form OW· I North Carolina Department ofEm'ironment and Natural Resources-Division ofWater Resources Revised August2013
WELL CONSTRUCTION RECORD
This form can be used for single or multiple we !is
I. Well Contractor Information:
NICK PERRY
We!t Contractor Name
3329
NC Well Contractor Certification Number
Terraquest Environmental Consultants, P.C.
Company Name
2. 'Veil Constructionl1ermil #:
List all applicable ~ref! permits (i.e. Coumy, Slate, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
DAgricultural D:l\1unicipal!Public
DGeothermal (Heating/Cooling Supply) DResidential Water Supply (single)
Dindustrial/Commercial DResidential Water Supply (shared)
Oirrigation
Non-Water Supply \Vl.'ll:
0Monitoring DRI?1:0VCf)'
Injection Well:
DAquifer Recharge DGroundwater Remediation
DAquifer Storage and Recovery DSalinity Barrier
DAquifcr Test DStormwater Drainage
DExperimental Technology DSubsidence Control
DGeothcnnal (Closed Loop) DTracer
DGeothermal (Heating/Cooling Return) DOther (explain under #21 Remarks)
4. Date Wcll{s) Completed: 5/12/15 We!IID# MW3,MW4
Sa. Well Location:
Hasty Mart #23 0-005354
Facility/Owner Name Facility ID# (if applicable)
501 N. Berkeley Blvd., Goldsboro 27534
Physical Address, City, and Zip
Wayne 3519433021
County Parcelldentification No. (PIN)
5b. Latitude and Longitude in degrees/nlinutes/seconds or decimal degrees:
(if well field, one !at/long is sufficient)
35.3748 N 77.9454 w
6. Is (arc) the well{s): 12lPcrmanent or DTemporary
7. Is this a repair to an existing well: DYes or ~No
If this is a repair, fill out known \I" ell construction iJiformation and exploin tho! naturo! of the
repair under i:-21 rcmarh section or on/he backofthisform.
8. Number of wells constructed: 2
For multiple injection or non-water supp~l~y~,.~.d~I,~O~.~Vl7.~,.-,.~itl7,~,h~,~'"~'~"'~'~'~"~"='J/f:tiou, you can
submit one form.
9. Total well depth below land surface: 2@13' {ft.)
Far muftiple ll"clls list all depths ifdi}Jerenl (example-3@200' and 2@100')
10. Static water level below top of casing: _4_._5_6_'.:.,4_.4_0_' _____ (ft.)
If water lew/ is a bow casing, use "" "
11. Borehole diameter: ..:8:.:·.:5_" _____ (in.)
12. Well construction method: ,H,o,......llo_w.:.:__S.::..:te.:..m.:.:__..:A.:..u:.::g::..e.:..r _____ _
(i.e. auger. rOta!)', cable, direct push., etc_)
FOR WATERSUPPLYWELLS ONLY:
13a. Yield (gpm) _______ Method of test:--------
ft. ft.
ft. ft.
""'"' JRL fr
ft. ft. '"·
~ ~ r •. ft. '"·
ft. ft. '"·
3' ft. 13' ft. 2in '"· 0.010 Sch.40 PVC
ft. ft. '"· ~ft. 1' ft. Po;;
11' ft. 2' ft. Pour
ft. ft.
~2Sand '
12' ft. 113' "· Pour
"· "· ~"· ~ ;
14' "· SAND
14' "· 113' "· SAND. with clay
"· "· "· "·
ft. "· "· ft.
"· "·
I
22. .I v J 5/13/15
Sig"'""" .'C/ Date
By sigl/illg this form, I haeby certify that the 1ndl(s) was (uwe) com/meted in accordance
wilh 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Com/ruction Standards and that a
copy of this Ncord has been provided to the u-1!11 0\1"/la.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or we!!
construction details. You may also attach additional pages if necessary.
SUBMITTAL L'\'STUCTIONS
24a .. For All Wells: Submit this fonn within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
16171\lail Sen·ice Center, Ualeigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the fom1 to the address in
24a above, also submit a copy of this fonn within 30 days of completion of well
construction to the following:
Di\'ision of \Vater Resources, Underground Injection Control Program,
16361\lail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion of
13b. Disinfection type: Amount: well construction to the county health department of the county where I.:~~~~~~~:.C=======-~~~'-=========J constructed.
FormGW~l North Carolina Department ofEnvironment and Natural Resources-Division ofWater Resources Revised August2013
EN'IIRONUENTAL CONSULTANTS, P.C.
LEGEND
LOGS
FOR SOIL BORING
AND WELL COMPLETION
DIAGRAMS
GRAPHIC
SYMBOL
.....
• • --.A oA
mJ
~
r-8 L___j
LETTER
SYMBOL
GW
GP
GM
GC
sw
TYPICAL DESCRIPTION
Well-graded grovels, grovel-
sand mixtures.
Poorly-graded grovels, grovel-
sand mixtures.
Silty grovels, grovel-silt-sand
mixtures.
Clayey grovels, grovel-sand-cloy
mixtures.
Well-graded sands, gravelly sands.
GRAPHIC LETTER
SYMBOL SYMBOL [Ill] ML
~ CL
~ ~
/ /
/ / / /
////
////
OL
MH
CH
rn L_____j SP Poorly-groded sonds, grovelly-sonds. ~ OH
0. 0
_Q .
0-0-0 .-o
o, 0_' o/_
SM
sc
Silty sands, sand-silt mixtures .
Clayey sands, sand-cloy mixtures.
WELL COMPLETION SYMBOLS
~ l!lJ • Pl w
PORTLAND CEMENT
BENTONITE
WELL SAND
-'~ I /' ,, _,... ,,
-'~
I ,, _, .....
~ ,,
ClossiUcoUon symbol ond 1\Qmt (J(e bosed upon IM visvol-monuor procedures ~S<:ribed lri ASH,! Tesl Uetl'lod 0 2488.
BLOWS/FT. DENSITY
0-4 VERY LOOSE
5-10 LOOSE
11-30 MED. DENSE
31-SO DENSE
BLOWS/FT. CONSISTENC
0-2 VERY SOFT
3-4 SOFT
5-8 MEDIUM STIFF
9-1S STIFF
16-30 VERY STIFF
31+ HARD
COMPONENT %
MOSTLY
SOME
LITTLE
FEW
TRACE
50-100%
30-45%
15-25%
5-10%
<5%
TYPICAL DESCRIPTION
Inorganic silts and very fine
sands, silty or clayey fine sands
Inorganic cloys of low to
medium plasticity, gravelly cloys,
sandy clays, silty or leon cloys.
Organic silts and cloys.
Micaceous or silty soils.
Inorganic cloys of high plasticity.
Organic cloys, organic silts with
medium to high plasticity.
Saprolite with the soil
characteristics of o sand,
grovel, silt, or cloy.
Bedrock
BORING LOG/MONITORING WELL INSTALLATION DETAIL
Blow
Counts
5
10
Scale as shown; Hatch pattern denotes soil sample depth;
Solid denotes lab sample depth; Lithology hatch pattern legend is attached;
Well Construction
2" diameter Sch. 40 PVC; .010" slotted screen
Sand: no. 2 sand; Grout: poured portland; Bentonite: poured pellets
Finished with 8"~diameter metal bolt down manhole.
NA-Not Applicable; BGL -Below Ground Level
Boring Number:
MW1
Description
Densley packed, poorly graded black sand, with some clay.
Soils are saturated at 5 ft BGL.
Dense;lv packed, poorly graded tannish-black sand, with
some quartz gravel, and few clay. Soils are saturated.
Well Completed at 13ft BGL.
Site:
Hasty Mart #23
501 N. Berkeley Blvd.
Goldsboro, NC
Client:
Wayne Oil Company, Inc.
1301 Wayne Memorial Dr.
Goldsboro, NC
Project No.: 07814 1
BORING LOG/MONITORING WELL INSTALLATION DETAIL
Blow
Counts Feet
5
10
Scale as shown; Hatch pattern denotes soil sample depth;
Solid denotes lab sample depth; Lithology hatch pattern legend is attached;
Well Construction
2" diameter Sch. 40 PVC; .01 0" slotted screen
Sand: no. 2 sand; Grout: poured portland; Bentonite: poured pellets
Finished with 8"-diameter metal bolt down manhole.
NA-Not Applicable; BGL-Below Ground Level
Boring Number:
MW2
Description
De1nslr>v packed, poorly graded black sand, with some clay.
Soils are saturated at 5 It BGL.
De1nse·lv packed, poorly graded tannish-black sand, with
some quartz gravel, and few clay. Soils are saturated.
Well Completed at 13 ft BGL.
Site:
Hasty Mart #23 501 N. Berkeley Blvd.
Goldsboro, NC
Client:
Wayne Oil Company, Inc.
1301 Wayne Memorial Dr.
Goldsboro, NC
Project No.: 07814
BORING LOG/MONITORING WELL INSTALLATION DETAIL
Blow
Counts Feet
5
10
Scale as shown; Hatch pattern denotes soil sample depth;
Solid denotes lab sample depth; Lithology hatch pattern legend is attached;
Well Construction
2" diameter Sch. 40 PVC; .010" slotted screen
Sand: no. 2 sand; Grout: poured portland; Bentonite: poured pellets
Finished with 8"-diameter metal bolt down manhole.
NA-Not Applicable; BGL-Below Ground Level
Boring Number:
MW3
Description
Densley packed, poorly graded black sand, with some clay.
Soils are saturated at 5 It BGL.
De1nselvpacked, poorly graded tannish-black sand, with
some quartz gravel, and few clay. Soils are saturated.
Well Completed at 13 It BGL.
Site:
Hasty Mart #23 501 N. Berkeley Blvd.
Goldsboro, NC
Client:
Wayne Oil Company, Inc.
1301 Wayne Memorial Dr.
Goldsboro, NC
Project No.: 07814 1
BORING LOG/MONITORING WELL INSTALLATION DETAIL
Blow
Counts Feet
5
10
Scale as shown; Hatch pattern denotes soil sample depth;
Solid denotes lab sample depth; Lithology hatch pattern legend is attached;
Well Construction
2" diameter Sch. 40 PVC; .01 0" slotted screen
Sand: no. 2 sand; Grout: poured portland; Bentonite: poured pellets
Finished with 8"~diameter metal bolt down manhole.
NA-Not Applicable; BGL-Below Ground Level
Boring Number:
MW4
Description
De1nslew packed, poorly graded black sand, with some clay.
Soils are saturated at 5 It BGL.
Densely packed, poorly graded tannish-black sand, with
some quartz gravel, and few clay. Soils are saturated.
Well Completed at 13 It BGL.
Site:
Hasty Mart #23
501 N. Berkeley Blvd.
Goldsboro, NC
Client:
Wayne Oil Company, Inc.
1301 Wayne Memorial Dr. Goldsboro, NC
Project No.: 07814 1
APPENDIX D
Analytical Report 507823
for
Terraquest Environmental Consultants, P.C.
Project Manager: Mike Brown
Hasty Mart #23
28-MAY-15
Collected By: Client
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-14-18), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( Ll0-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (TI04704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Page 1 of96 Flnal1.000
28-MAY-15
Project Manager: Mike Brown
Terraquest Environmental Consultants, P .C.
I 00 E. Ruffin Street
Mebane, NC 27302
Reference: XENCO Report No(s): 507823
Hasty Mart #23
Project Address: NC
Mike Brown:
IJf
·~ ... .= ... .,.
We are reporting to you the results of the analyses petformed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 507823. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratmy ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data repmied in this Analytical Repmi are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without futiher notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 507823 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to retum to you any unused samples, extracts or solutions related to them if we
consider so necessmy (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
Debbie Simmons
Project Manager
Recipient of the Prestigious Small Business Administration Award of Excellence inl994.
Certified and approved by numerous States and Agencies.
A Small Busiuess and Minority Status Company that delivers SERVICE and QUALITY
Houston-Dallas-Odessa -San Antonio-Tampa-lakeland-Atlanta-Phoenix-Oklahoma-latin America
Page 2 of96 Final 1.000
Sample ld
MWl (2-3)
MW2 (2-3)
MW3 (2-3)
MW4 (2-3)
MW1
MW2
MW3
MW4
Sample Cross Reference 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix Date Collected Sample Depth Lab Sample Id
s 05-12-15 10:07 2-3ft 507823-001
s 05-12-15 10:49 2-3ft 507823-002
s 05-12-1511:29 2-3ft 507823-003
s 05-12-15 12:01 2-3ft 507823-004
w 05-12-15 15:24 507823-005
w 05-12-15 15:14 507823-006
w 05-12-15 15:30 507823-007
w 05-12-15 15:04 507823-008
Page 3 of96 Flnal1.000
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MSIMSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS&fSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for tills analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H TI1e LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were detennined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the 11N" and the "JU qualifier. The analysis indicates that the analyte is ''tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
1\-IDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit JVIQL Method Quantitation Limit LOQ Limit ofQuantitation
DL Method Detection Limit
NC Non~Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description)= Outside XENCO's scope ofNELAC accreditation
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston-DaUas-San Antonio· Atlanta· Midland/Odessa. Tampa/Lakeland-Phoenix-Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd, Dallas, TX 75220
5332 Blackbcny Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL33619
12600 West 1-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Page 4 of 96
Phone
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
Fa<
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
Final 1.000
Sample ld : MWl (2-3)
Lab Sample Id: 507823-001
Sample Depth : 2 - 3 ft
Hits Summary 507823
Terraquest Environmental Consultants, P.C.,
Hasty Mart #23
Mebane,NC
Matrix : Soil
Date Collected: 05.12.15 10.07
Date Received: 05.14.15 09.30
% Moisture : 8.93
Basis: Dry Weight
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Seq Number 968428 Date Prep: 05.17.15 10.14
Parameter
Acetone
Toluene
Sample Id : MWl (2-3)
Lab Sample Id: 507823-001
Sample Depth : 2 - 3 ft
Cas Number Result Units
67-64-1
108-88-3
0.041
0.0012
Matrix : Soil
mg/kg
mg/kg
Date Collected: 05.12.15 10.07
Date Received: 05.14.15 09.30
Analytical Method: Select Metals by SW-846 6010C
Seq Number 968286
Parameter
Chromium
Sample Id : MWl (2-3)
Lab Sample Id: 507823-001
Sample Depth : 2 - 3 ft
Cas Number Result Units
7440-47-3 5.36 mg/kg
Matrix : Soil
Date Collected: 05.12.15 10.07
Date Received: 05.14.15 09.30
Analytical Method: Chromium, Hexavalent by SW 7196A
Seq Number 968402
Parameter Cas Number Result Units
Chromium, Hexavalent 18540-29-9 0.929 mglkg
Page 5 of96
Analysis Date
05.17.15 14.52
05.17.15 14.52
Flag
%Moisture : 8.93
Basis : Dry Weight
Prep Method: SW3050B
Dil
Date Prep: 05.15.15 13.32
Analysis Date Flag Dil
05.17.1519.24 J
%Moisture: 18.22
Basis : Dry Weight
Analysis Date Flag Dil
05.17.15 10.00 J
Final1.000
Sample ld : MW2 (2-3)
Lab Sample ld : 507823-002
Sample Depth : 2 - 3 ft
Analytical Method : MADEP VPH
Seq Number 968507
Parameter
C9-C I 0 Aromatics
Hits Summary 507823
Terraquest Environmental Consultants, P.C.,
Hasty Mart #23
Mebane,NC
Matrix : Soil
Date Collected: 05.12.15 10.49
Date Received: 05.14.15 09.30
%Moisture: 11.37
Basis : Dry Weight
Prep Method: SW5030B
Date Prep: 05.19.15 09.10
Cas Number Result Units Analysis Date Flag Dil
HYDC9CIO 0.746 mglkg 05.19.15 13.36 X 50
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Seq Number 968428
Parameter
Acetone
Benzene
m,p-Xylenes
Tetrachloroethene
Toluene
Sample ld : MW3 (2-3)
Lab Sample ld : 507823-003
Sample Depth : 2 - 3 ft
Analytical Method : MADEP VPH
Seq Number 968507
Parameter
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-Cl 0 Aromatics
Cas Number Result Units
67-64-1 0.036 mgikg
71-43-2 0.00079 mgikg
179601-23-1 0.00206 mglkg
127-18-4 0.0034 mglkg
108-88-3 0.0031 mglkg
Matrix : Soil
Date Collected: 05.12.15 11.29
Date Received: 05.14.15 09.30
Cas Number
ALHYDRC5
ALHYDRC9
HYDC9CIO
Result
11.9
5.22
3.20
Page 6 of96
Units
mglkg
mglkg
mg/kg
Date Prep: 05.17.15 10.14
Analysis Date Flag Dil
05.17.15 15.18
05.17.15 15.18
05.17.15 15.18
05.17.15 15.18
05.17.15 15.18
%Moisture: 12.66
Basis : Dry Weight
Prep Method: SW5030B
Date Prep: 05.19.15 09.10
Analysis Date
05.19.1514.20
05.19.15 14.20
05.19.15 14.20
Final1.000
Flag Dil
50
50
50
Sample Id: MW3 (2-3)
Lab Sample Id : 507823-003
Sample Depth : 2 - 3 ft
Hits Summary 507823
Terraquest Environmental Consultants, P.C.,
Hasty Mart #23
Mebane,NC
Matrix : Soil
Date Collected: 05.12.15 11.29
Date Received: 05.14.15 09.30
%Moisture : 12.66
Basis : Dry Weight
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Seq Number 968474
Parameter Cas Number Result Units
1,2,4-Trimethylbenzene 95-63-6 1.0 mglkg
Ethyl benzene 100-41-4 0.90 mglkg
m,p-Xylenes 179601-23-1 3.9 mglkg
o-Xylene 95-47-6 0.80 mglkg
Analytical Method: VOCs by SW-846 8260B
Seq Number 968474
Parameter
I ,3,5-Trimethylbenzene
4-Isopropyltoluene
Acetone
Benzene
Isopropyl Ether
Isopropylbenzene
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butyl benzene
Toluene
Sample Id: MW4 (2-3)
Lab Sample Id : 507823-004
Sample Depth : 2 -3 ft
Analytical Method : MADEP VPH
Seq Number 968507
Parameter
C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
Cas Number Result Units
108-67-8 0.058 mglkg
99-87-6 0.0047 mglkg
67-64-1 0.10 mglkg
71-43-2 0.071 mglkg
108-20-3 0.0048 mglkg
98-82-8 0.013 mglkg
1634-04-4 0.0055 mglkg
91-20-3 0.0032 mglkg
104-51-8 0.0075 mglkg
103-65-1 0.040 mglkg
135-98-8 0.0019 mglkg
108-88-3 0.015 mglkg
Matrix : Soil
Date Collected: 05.12.15 12.01
Date Received: 05.14.15 09.30
Cas Number
ALHYDRC5
ALHYDRC9
HYDC9Cl0
Result
32.8
8.99
4.82
Page 7 of96
Units
mglkg
mglkg
mglkg
Date Prep: 05.18.15 13.26
Analysis Date Flag Dil
05.18.15 18.27 D 50
05.18.15 18.27 D 50
05.18.15 18.27 D 50
05.18.15 18.27 D 50
Prep Method: SW5035
Date Prep: 05.19.15 10.40
Analysis Date Flag Dil
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14 LF 1
05.19.15 21.14 I
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14
05.19.15 21.14
% Moisture : 11.16
Basis : Dry Weight
Prep Method: SW5030B
Date Prep: 05.19.15 09.10
Analysis Date
05.19.15 15.05
05.19.15 15.05
05.19.15 15.05
Flnal1.000
Flag Dil
50
50
50
Hits Summary 507823 Jif ·~ -~ ......
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix : Soil Sample Id: MW4 (2-3)
Lab Sample Id : 507823-004
Sample Depth : 2 -3 ft
Date Collected: 05.12.15 12.01
Date Received: 05.14.15 09.30
Analytical Method: VOCs by SW-846 8260B
Seq Number 968474
Parameter Cas Number Result Units
1,2,4-Trimethy1benzene 95-63-6 1.2 mglkg
Ethylbenzene 100-41-4 1.1 mglkg
m,p-Xylenes 179601-23-1 5.6 mglkg
a-Xylene 95-47-6 1.7 mglkg
Analytical Method: VOCs by SW-846 8260B
Seq Number 968474
Parameter Cas Number Result Units
l ,3,5-Trimethylbenzene 108-67-8 0.064 mglkg
4-Isopropyltoluene 99-87-6 O.Ql5 mglkg
Acetone 67-64-1 0.14 mglkg
Benzene 71-43-2 0.068 mglkg
Isopropyl Ether 108-20-3 0.0074 mglkg
Isopropylbenzene 98-82-8 O.Ql5 mglkg
Methyl tert -butyl ether 1634-04-4 0.020 mglkg
Methylene chloride 75-09-2 0.0026 mglkg
n-Butylbenzene 104-51-8 0.0082 mglkg
n-Propylbenzene 103-65-1 0.042 mglkg
sec-Butylbenzene 135-98-8 0.0022 mglkg
Toluene 108-88-3 0.11 mglkg
Sample Id : MWl
Lab Sample Id : 507823-005
Matrix : Ground Water
Date Collected: 05.12.15 15.24
Date Received: 05.14.15 09.30
Analytical Method : SVOCs by EPA 625 + I 0 TICs
Seq Number 968853
Parameter Cas Number Result Units
Trichloroacetic acid, hexadecyl es (TIC) TIC 5.92 ug/L
Analytical Method: Select Metals by SW-846 6010C
Seq Number 968525
Parameter Cas Number Result Units
Chromium 7440-47-3 0.0979 mg/1
Page 8 of 96
% Moisture : 11.16
Basis : Dry Weight
Prep Method: SW5035
Date Prep: 05.18.15 13.26
Analysis Date Flag Dil
05.18.15 18.52 D 50
05.18.15 18.52 D 50
05.18.15 18.52 D 50
05.18.15 18.52 D 50
Prep Method: SW5035
Date Prep: 05.19.15 10.40
Analysis Date Flag Dll
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39 LF
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39 J
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
%Moishue:
Prep Method: E625P
Date Prep: 05.19.15 14.00
Analysis Date Flag Dil
05.21.15 21.26 JN
Prep Method: SW3010A
Date Prep: 05.19.15 13.10
Analysis Date Flag Dil
05.20.15 12.12
Final1.000
Sample Id: MW2
Lab Sample Id : 507823-006
Analytical Method : MADEP VPH
Seq Number 968516
Parameter
C5-C8 Aliphatics
C9-C I 0 Aromatics
C9-Cl2 Aliphatics
Hits Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water %Moishtre:
Date Collected: 05.12.15 15.14
Date Received: 05.14.15 09.30
Prep Method: SW5030B
Date Prep: 05.19.15 09.10
Cas Number Result Units Analysis Date Flag Dil
ALHYDRC5 207 ug/L 05.19.15 18.47 I
HYDC9CIO 2140 ug/L 05.19.15 17.18 D 5
ALHYDRC9 2700 ug!L 05.19.15 17.18 D 5
Analytical Method : SVOCs by EPA 625 + I 0 TICs Prep Method: E625P
Seq Number 968853 Date Prep: 05.19.15 14.00
Parameter Cas Number Result Units Analysis Date Flag Dil
1-Methylnaphthalene + 90-12-0 3.86 ug/L 05.21.15 21.54 J
2,4-Dimethylphenol 105-67-9 5.68 ug/L 05.21.15 21.54 J
2-Methylnaphthalene 91-57-6 8.08 ug/L 05.21.15 21.54 J
3&4-Methylphenol 15831-10-4 37.5 ug/L 05.21.15 21.54
Naphthalene 91-20-3 70.1 ug/L 05.21.15 21.54
Benzene, 1,3,5-trimethy1-(TIC) TIC 235 ug/L 05.21.15 21.54 JN
Benzene, 1,2,4-trimethyl-(TIC) TIC 89.6 ug/L 05.21.15 21.54 JN
Benzene, 1,3-dimethyl-(TIC) TIC 358 ug/L 05.21.15 21.54 JN
Benzene, 1-ethy1-2-methy1-(TIC) TIC 183 ug/L 05.21.15 21.54 JN
Ethylbenzene (TIC) TIC 204 ug/L 05.21.15 21.54 JN
Benzene, 1,2,3-trimethyl-(TIC) TIC 74.6 ug!L 05.21.15 21.54 JN
unknown (TIC) TIC 56.0 ug/L 05.21.15 21.54 JN
Toluene (TIC) TIC 280 ug/L 05.21.15 21.54 JN
Indane (TIC) TIC 80.5 ug/L 05.21.15 21.54 JN
p-Xylene (TIC) TIC 545 ug/L 05.21.15 21.54 JN
Analytical Method : VOCs by GC/MS by SM6200B Prep Method: SM6200B_PREP
Seq Number 968479 Date Prep: 05.19.15 09.49
Parameter Cas Number Result Units Analysis Date Flag Dil
2-Butanone (MEK) 78-93-3 7.67 ug/L 05.19.15 17.51 J
4-Isopropyltoluene 99-87-6 5.20 ug/L 05.19.15 17.51
Acetone 67-64-1 14.4 ug/L 05.19.15 17.51
Benzene 71-43-2 36.4 ug/L 05.19.15 17.51
Chlorofonn 67-66-3 1.63 ug/L 05.19.15 17.51
lsopropy1benzene 98-82-8 37.2 ug/L 05.19.15 17.51
sec-Butyl benzene 135-98-8 4.41 ug/L 05.19.15 17.51
Page 9 of 96 Flnal1.000
Sample Id : MW2
Lab Sample Id : 507823-006
Hits Summary 507823
Terraquest Environmental Consultants, P .C.,
Hasty Mart #23
Mebane,NC
Matrix : Ground Water
Date Collected: 05.12.15 15.14
Date Received: 05.14.15 09.30
% Moishue:
JJf "~ -.!."'.'::. ......
Analytical Method : VOCs by GC/MS by SM6200B Prep Method: SM6200B]REP
Seq Number 968479 Date Prep: 05.20.15 05.59
Parameter Cas Number Result Units Analysis Date Flag Dil
1,2,4-Trimethylbenzene 95-63-6 762 ug!L 05.20.15 12.11 D 20
1,3 ,5-Trimethylbenzene 108-67-8 238 ug!L 05.20.15 12.11 D 20
Ethyl benzene 100-41-4 593 ug!L 05.20.15 12.11 D 20
Naphthalene 91-20-3 238 ug!L 05.20.15 12.11 D 20
n-Propylbenzene 103-65-1 119 ug!L 05.20.15 12.11 D 20
Toluene 108-88-3 957 ug!L 05.20.15 12.11 D 20
m,p-Xylenes 179601-23-1 1810 ug!L 05.20.15 12.11 D 20
o-Xylene 95-47-6 890 ug!L 05.20.15 12.11 D 20
Page 10 of 96 Final1.000
Sample Id: MW3
Lab Sample Id : 507823-007
Analytical Method : MADEP VPH
Seq Number 968516
Parameter
C5-C8 Aliphatics
C9-Cl0 Aromatics
C9-Cl2 Aliphatics
Hits Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water %Moisture:
Date Collected: 05.12.15 15.30
Date Received: 05.14.15 09.30
Prep Method: SW5030B
Date Prep: 05.19.15 09.10
Cas Number Result Units Analysis Date Flag Dil
ALHYDRC5 3370 ug/L 05.19.15 19.31 1
HYDC9C10 2950 ug/L 05.19.15 18.02 D 5
ALHYDRC9 3800 ug/L 05.19.15 18.02 D 5
Analytical Method : VOCs by GC/MS by SM6200B Prep Method: SM6200B_PREP
Seq Number 968479 Date Prep: 05.19.15 09.49
Parameter Cas Number Result Units Analysis Date Flag Dil
4-Isopropyltoluene 99-87-6 4.19 ug/L 05.19.15 17.24 1
Acetone 67-64-1 10.7 ug/L 05.19.15 17.24 1
Chloroform 67-66-3 0.320 ug/L 05.19.15 17.24 J 1
Isopropyl ether 108-20-3 35.9 ug/L 05.19.15 17.24 1
lsopropylbenzene 98-82-8 39.5 ug/L 05.19.15 17.24
Methyl tert-butyl ether (MTBE) 1634-04-4 29.0 ug/L 05.19.15 17.24
sec-Butyl benzene 135-98-8 4.41 ug/L 05.19.15 17.24
Analytical Method : VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Seq Number 968479 Date Prep: 05.20.15 05.59
Parameter Cas Number Result Units Analysis Date Flag Dil
1,2,4-Trimethylbenzene 95-63-6 1190 ug/L 05.20.15 11.31 D 20
1,3,5-Trimethylbenzene 108-67-8 299 ug/L 05.20.1511.31 D 20
Benzene 71-43-2 736 ug/L 05.20.15 11.31 D 20
Ethylbenzene 100-41-4 1270 ug/L 05.20.15 11.31 D 20
Naphthalene 91-20-3 549 ug/L 05.20.15 11.31 D 20
n-Propylbenzene 103-65-1 142 ug/L 05.20.15 11.31 D 20
Toluene 108-88-3 4630 ug/L 05.20.15 13.34 D 100
m,p-Xylenes 179601-23-1 4450 ug/L 05.20.15 13.34 D 100
a-Xylene 95-47-6 2160 ug/L 05.20.15 13.34 D 100
Page 11 of96 Final1.000
Sample Id : MW 4
Lab Sample Id : 507823-008
Analytical Method : MADEP VPH
Seq Number 968516
Parameter
C5-C8 Aliphatics
C9-Cl0 Aromatics
C9-C 12 Aliphatics
Hits Summary 507823
Terraquest Environmental Consultants, P.C.,
Hasty Matt #23
Mebane,NC
Matrix : Ground Water
Date Collected: 05.12.15 15.04
Date Received: 05.14.15 09.30
%Moisture:
Prep Method: SW5030B
Date Prep: 05.19.15 09.10
Cas Number
ALHYDRC5
HYDC9Cl0
ALHYDRC9
Result
19.9
21.8
35.0
Units
ug/L
ug/L
ug/L
Analysis Date
05.19.15 16.34
05.19.15 16.34
05.19.15 16.34
Flag Dil
Analytical Method : VOCs by GC!MS by SM6200B Prep Method: SM6200B PREP
Seq Number 968479 Date Prep: 05.19.15 09.49
Parameter Cas Number Result Units Analysis Date Flag Dll
1,2,4-Trimethy1benzene 95-63-6 2.72 ug/L 05.19.15 16.58
Benzene 71-43-2 5.77 ug/L 05.19.15 16.58
Ethylbenzene 100-41-4 8.37 ug/L 05.19.15 16.58
Isopropyl ether 108-20-3 1.08 ug/L 05.19.15 16.58
Methyl tert-buty1 ether (MTBE) 1634-04-4 3.19 ug!L 05.19.15 16.58
Naphthalene 91-20-3 1.17 ug!L 05.19.15 16.58 J
n-Propylbenzene 103-65-1 1.12 ug!L 05.19.15 16.58
m,p-X ylenes 179601-23-1 17.2 ug!L 05.19.15 16.58
o-Xylene 95-47-6 5.65 ug/L 05.19.15 16.58
Page 12 of96 Final1.000
Sample ld: 1\IWl (2-3)
lab Sample Id: 507823-001
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 IO.Q7
Date Receivcd:05.14.15 09.30
Sample Depth: 2 - 3 ft
Analytical Method: Select Metals by SW-846 60 I OC Prep Method: SW3050B
%Moisture: 8.93 Tech: 4099
Analyst: 4150 Date Prep: 05.15.15 13.32
Seq Number: 968286
Parameter Cas Number Result RL MDL
Chromium 7440-47-3 /5.36 5.49 0.0659
Analytical Method: Chromium, Hexavalent by SW 7196A
Tech: NSI
Analyst: NSI
Seq Number: 968402
Parameter
Chromium, Hexavalent
Analytical Method: MADEP EPH
Tech: lliG
Analyst: CLAR
Seq Number: 968290
Parameter
Cll-C22 Aromatics
C9-Cl8 Aliphatics
Cl9-C36 Aliphatics
Surrogate
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Cas Number Result RL MDL
18540-29-9 j 0.929 2.45 0.489
Date Prep: 05.14.15 16.05
Cas Number Result RL MDL
C1tC22 u 21.7 21.7
ALHYDRC9C II u 10.9 10.9
ALHYDRC19C: u 10.9 10.9
%
Cas Number Recovery Units
3386-33-2 55 %
84-15-t 52 %
321-60·8 87 %
Page 13 of96
Basis: Dry \Veight
Units Analysis Date Flag
mglkg 05.17.15 19.24 J
%Moisture: 18.22
Basis: Dry Weight
Units Analysis Date Flag
mglkg 05.17.15 10.00 J
Prep Method: SW3545
%Moisture: 8.93
Basis: Dry Weight
Units Analysis Date Flag
mglkg 05.19.1521.19 u
mglkg 05.20.15 02.05 u
mglkg 05.20.15 02.05 u
Limits Analysis Date Flag
40-140 05.20.15 02.05
40-140 05.19.15 21.19
40-140 05.19.15 21.19
Flnal1.000
Dll
Dil
Dil
Sample Id: MWl (2-3)
Lab Sample ld: 507823-001
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 I 0.07
Date Received:05.14.15 09.30
Sample Depth: 2 - 3 ft
Analytical Method: SVOCs by SW-846 8270D Prep Method: S\V3545
%Moisture: 8.93 Tech: JHG
Analyst: CLAR
Seq Number: 968618
Parameter
1 ,2 ,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Ch\orophenol
2-Methylnaphthalene
2-methylphenol
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4-chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (Phcnylamine, Aminoben:zene)
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Butyl Phthalate
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
Cas Number
120-82-1
95-50-1
541-73-1
106-46-7
95-95-4
88-06-2
120-83-2
105-67-9
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-74-4
88-75-5
15831-10-4
91-94-1
99-09-2
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-01-6
100-02-7
83-32-9
208-96-8
62-53-3
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
85-68-7
111-91-1
111-44-4
Date Prep:
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
05.19.15 15.40
RL
0.366
0.366
0,366
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.731
0.366
0.731
1.83
0.366
0.366
0.366
0.183
0.366
0.366
0.366
0.731
0.731
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.366
0.731
0.366
0.366
0.183
MDL
0.0647
0.0592
0.0578
0.0570
0.0673
0.0706
0.0464
0,0665
0.0589
0.0475
0.0665
0.0655
0.0559
0.0512
0.0490
0.0461
0.108
0.0534
0.0505
0.0636
0.0622
0.0523
0.0607
0.0695
0.0556
0.0450
0.0512
0.0622
0.0402
0.0541
0.0592
0.0538
0.0596
0.0603
0.0629
0.0578
0.0548
0.0439
0.0519
Page 14 of 96
Basis: Dry Weight
Units Analysis Date
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
mglkg 05.21.15 03.39
rug/kg 05.21.15 03.39
rug/kg 05.21.15 03.39
Flnai1.000
Flag
UXF
UXF
UF
UXF
u
ux
ux
u
u
u
ux
UF
UF
UF
u
UXF
UF
u
u
u
u
u
u
u
u
u
u
ux
UHF
u
u
u
u
u
u
u
u
UXF
UF
Dil
Certificate of Analytical Results 507823 Jif "u -~·-·
Terraquest Environmental Consultants, P .c., Mebane,NC
Hasty Mart #23
Sample Id: MWl (2-3) Matrix: Soil Date Received:05.14.15 09.30
Lab Sample Id: 507823-001 Date Collected: 05.12.15 10.07 Sample Depth: 2 - 3 ft
Analytical Method: SVOCs by SW-846 8270D Prep Method: SW3545
Tech: lliG %Moisture: 8.93
Analyst: CLAR Date Prep: 05.19.15 15.40 Basis: Dry Weight
Seq Number: 9686!8
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
bis(2-chloroisopropyl) ether 39638-32-9 u 0.366 0.0494 mg/kg 05.21.15 03.39 UF
bis(2-ethylhexyl) phthalate 117-81-7 u 0.366 0.0592 mg/kg 05.21.15 03.39 u
Chrysene 218-01-9 u 0.366 0.0486 mg/kg 05.21.15 03.39 u
Dibenz(a,h)Anthmcene 53-70-3 u 0.366 0.0709 mg/kg 05.21,15 03.39 u
Dibenzofuran 132-64-9 u 0.366 0.0468 mg/kg 05.21.15 03.39 u
Diethyl Phthalate 84-66-2 u 0.366 0.0589 mg/kg 05.21.15 03.39 u
Dimethyl Phthalate 131-11-3 u 0.366 0.0552 mg/kg 05.21.15 03.39 u
di-n-Butyl Phthalate 84-74-2 u 0.366 0.0673 rug/kg 05.21.15 03.39 u
di-n-Octyl Phthalate 117-84-0 u 0.366 0.0607 mg/kg 05.21.15 03.39 u
Fluoranthene 206-44-0 u 0.366 0.0475 mg/kg 05.21.15 03.39 u
Fluorene 86-73-7 u 0.366 0.0446 mg/kg 05.21.15 03.39 u
Hexachlorobenzene 118-74-1 u 0.366 0.0611 mg/kg 05.21.15 03.39 u
Hexachlorobutadiene 87-68-3 u 0.366 0.0406 rug/kg 05.21.15 03.39 UXF
Hexachlorocyclopentadiene 77-47-4 u 0.366 0.0629 mg/kg 05.21.15 03.39 u
Hexachloroethane 67-72-1 u 0.366 0.0567 mg/kg 05.21.15 03.39 UF
Indeno( 1 ,2,3 -c,d)Pyrene 193-39-5 u 0.366 0.0665 mg/kg 05.21.15 03.39 u
Isophorone 78-59-1 u 0.366 0.0377 mg/kg 05.21.15 03.39 u
Naphthalene 91-20-3 u 0.366 0.0585 rug/kg 05.21.15 03.39 UXF
Nitrobenzene 98-95-3 u 0.366 0.0651 mg/kg 05.21.!5 03.39 UF
N-Nitrosodi-n-Propylarnine 621-64-7 u 0.366 0.0523 mg/kg 05.21.!5 03.39 UF
N-Nitrosodiphenylamine 86-30-6 u 0.366 0.0768 mglkg 05.21.! 5 03.39 u
Pentachlorophenol 87-86-5 u 0.731 0.0662 mg/kg 05.21.15 03.39 u
Phenanthrene 85-01-8 u 0.366 0.0607 mg/kg 05.21.!5 03.39 u
Phenol 108-95-2 u 0.366 0.0512 mg/kg 05.21.15 03.39 u
Pyrene 129-00-0 u 0.366 0.0622 mg/kg 05.21.!5 03.39 u
Pyridine 110-86-1 u 0.366 0.0695 mg/kg 05.21.15 03.39 UF
% Surrogate Cas Number Reco\-'ery Units Limits Analysis Date Flag
2-Fluorophenol 367-12-4 41 % 25-121 05.21.15 03.39
Nitrobenzene-dS 4165-60-0 43 % 23-120 05.21.15 03.39
2-Fluorobiphenyl 321-60-8 44 % 30-115 05.21.15 03.39
2,4,6-Tribromophenol 118-79-6 50 % 19-122 05.21.15 03.39
Terphenyl-D 14 1718-51-0 52 % 18-137 05.21.15 03.39
Phenol-dS 4165-62-2 42 % 15-110 05.21.15 03.39
Page 15 of 96 Flnal1.000
Sample Id: MWI (2-3)
Lab Sample Id: 507823-001
Analytical Method: MADEP VPH
Tech: VBR
Analyst: ZHO
Seq Number: 968507
Parameter
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-C10 Aromatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 10.Q7
Date Prep: 05.19.15 09.10
Cas Number Result RL 1\IDL
ALHYDRC5C8 u 0.00625 0.00625
ALHYDRC9C1: u 0.00625 0.00625
HYDC9CIO u 0.00208 0.00208
%
Cas Number Recovery Units
615-59-8 Ill %
615-59-8 98 %
Page 16 of 96
Units
mglkg
mglkg
mglkg
Limits
70-130
70-130
Date Received:05.14.15 09.30
Sample Depth: 2 - 3 ft
Prep Method: SW5030B
%Moisture: 8.93
Basis: Dry Weight
Analysis Date Flag
05.19.15 12.52 u
05.19.1512.52 u
05.19.15 12.52 u
Analysis Date Flag
05.19.15 12.52
05.19.15 12.52
Final1.000
Dlt
50
50
50
Sample Id: MWl (2-3)
lab Sample Id: 507823-001
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 10.07
Date Received:05.14.15 09.30
Sample Depth: 2 -3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
%Moisture: 8.93 Tech: MWE
Analyst: ZHO
Seq Number: 968428
Parameter
l,l,l·Trichloroethane
1,1 ,2 ,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
I ,2 ,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2~Dichloropropane
2~Butanone (MEK)
2-Chlorotoluene
2~Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl~2-pentanone (MJBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chlorofonn
Chloromethane
cis-! ,2~Dichloroethene
Cas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
Date Prep;
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
0.041
u
u
u
u
u
u
u
u
u
u
u
u
u
05.17.15 10.14
RL
0.00084
0.0017
0.00084
0.00084
0.0017
0.00084
0.00084
0.0017
0.00084
0.00084
0.00084
0.0017
0.00084
0.00084
0.00084
0.00084
0.00084
0.00084
0.00084
0.0084
0.00084
0.0084
0.00084
0.00084
0.0084
0.0084
0.00084
0.00084
0.0017
0.00084
0.00084
0.0042
0.00084
0.00084
0.00084
0.0042
0.00084
0.0042
0.00084
MDL
0,00063
0.00099
0.00056
0.00067
0.00097
0.00045
0.00048
0.0014
0.00073
0,00060
0.00072
0.0011
0.00050
0.00078
0.00068
0.00083
0.00058
0.00057
0.00050
0.0019
0.00059
0.00094
0.00046
0.00067
0.0027
0.0058
0.00043
0.00071
0.00084
0.00042
0.00080
0.0021
0.00062
0.00048
0.00083
0.0020
0.00062
0.0019
0.00055
Page 17 of 96
Basis: Dry Weight
Units
mglkg
mglkg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
mglkg
mglkg
rug/kg
mglkg
mglkg
mglkg
mglkg
rug/kg
mglkg
mglkg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
mglkg
Analysis Date
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
05.17.1514.52
05.17.t5 14.52
05.17.15 14.52
05.17.15 14.52
05.17.15 14.52
Final 1.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DII
Certificate of Analytical Results 507823 Jif "~ -..!.~ ......
Terraquest Environmental Consultants, P.C., Mebane,NC
Hasty Mart #23
Sample Id: MWl (2-3) Matrix: Soil Date Receivcd:05.14.15 09.30
Lab Sample Id: 507823-001 Date Collected: 05.12.15 10,07 Sample Depth: 2 - 3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech: MWE %Moish1re: 8.93
Analyst: ZHO Date Prep: 05.17.15 10.14 Basis: Dry Weight
Seq Number: 968428
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis-1 ,3-Dichloropropene 10061-01-5 u 0.00084 0.00045 mglkg 05.17.15 14.52 u
Dichlorodifluoromethane 75-71-8 u 0.0017 0.00099 mglkg 05.17.15 14.52 u
Ethanol 64-17-5 u 0.042 0.023 mglkg 05.17.15 14.52 u
Ethylbenzene 100-41-4 u 0.00084 0.00047 mglkg 05.17.1514.52 u
Isopropyl Ether 108-20-3 u 0.0017 0.0011 mglkg 05.17.15 14.52 u
Isopropylbenzene 98-82-8 u 0.00084 0.00064 mglkg 05.17.15 14.52 u
m,p-Xylenes 179601-23-1 u 0,00167 0.00101 mglkg 05.17.15 14.52 u
Methyl tert-butyl ether 1634-04-4 u 0.0017 0.00058 mglkg 05.17.15 14.52 u
Methylene chloride 75-09-2 u 0.0042 0.0018 mglkg 05.17.15 14.52 u
Naphthalene 91-20-3 u 0.0017 0.0011 mglkg 05.17.15 14.52 u
n-Butylbenzene 104-51-8 u 0.00084 0.00074 mglkg 05.17.15 14.52 u
n-Propylbenzene 103-65-1 u 0.00084 0.00065 mglkg 05.17.15 14.52 u
a-Xylene 95-47-6 u 0.000837 0.000599 mglkg 05.17.15 14.52 u
sec-Butylbenzene 135-98-8 u 0.00084 0.00055 mglkg 05.17.15 14.52 u
Styrene 100-42-5 u 0.00084 0.00062 mglkg 05.17.15 14.52 u
tert-Butylbenzene 98-06-6 u 0.00084 0.00070 mglkg 05.17.15 14.52 u
Tetrachloroethene 127-18-4 u 0.0017 0.00087 mglkg 05.17.15 14.52 u
Toluene 108-88-3 0.0012 0.00084 0.00049 mglkg 05.17.15 14.52
tmns-1,2-Dichloroethene 156-60-5 u 0.00084 0.00065 mglkg 05.17.15 14.52 u
trans-1 ,3-Dichloropropene 10061-02-6 u 0.00084 0.00056 mglkg 05.17.15 14.52 u
Trichloroethene 79-01-6 u 0.00084 0.00059 mglkg 05.17.15 14.52 u
Trichlorofluoromethane 75-69-4 u 0.0042 0.0029 mglkg 05.17.15 14.52 u
Vinyl acetate 108-05-4 u 0.0042 0.00060 mglkg 05.17.15 14.52 u
Vinyl chloride 75-01-4 u 0.0042 0.0017 mglkg 05.17.15 14.52 u
% Surrogate Cas Number Recovery Units Limits Analysis Date Flag
1,2-Dlchloroethane-D4 17060-07-0 132 % 50-150 05.17.15 14.52
4-Bromofluorobenzene 460-00-4 99 % 57-158 05.17.15 14.52
Toluene-D8 2037-26-5 103 % 50-150 05.17.15 14.52
Page 18 of96 Flna11.000
Sample ld: MW2 (2-3)
Lab Sample Id: 507823-002
Analytical Method: MADEP EPH
Tech: JHG
Analyst: CLAR
Seq Number: 968290
Parameter
Cll-C22 Aromatics
C9-CI8 Aliphatics
Cl9-C36 Aliphatics
Surrogate
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 10.49
Date Prep: 05.14.15 16.05
Cas Number Result RL MDL
C11C22 u 22.1 22.1
ALHYDRC9Cll u 11.0 11.0
ALHYDRC19C: u 11.0 11.0
% Cas Number Reco\'Cry Units
3386-33-2 48 %
84-15-1 54 %
321-60-8 83 %
Page 19 of 96
Units
mglkg
mg/kg
mg/kg
Limits
40-140
40-140
40-140
Date Received:05.14.15 09.30
Sample Depth: 2-3 ft
Prep Method: SW3545
%Moisture: 11.37
Basis: Dry Weight
Analysis Date Flag
05.19.15 21.54 u
05.20.15 02.37 u
05.20.15 02.37 u
Analysis Date Flag
05.20.15 02.37
05.19.15 21.54
05.19.15 21.54
Fina\1.000
Dil
Sample Id: MW2 (2-3)
Lab Sample Id: 507823-002
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 10.49
Date Received:05.14.15 09.30
Sample Depth: 2 -3 fi
Analytical Method: SVOCs by SW-846 8270D Prep Method: SW3545
%Moisture: 11.37 Tech: JHG
Analyst: CLAR
Seq Number: 968618
Parameter
1,2,4-Trichlorobenzene
l ,2-Dichlorobenzene
I ,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4 ,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-mcthylphenol
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
3-Nitroani\ine
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4-chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (PhenylamiM, Aminob\!nzene)
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Butyl Phthalate
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
Cas Number
120-82-1
95-50·1
541-73-1
10646·7
95-95-4
88·06·2
120·83-2
105-67-9
t21-14-2
606·20·2
91-58-7
95-57·8
91-57·6
9548·7
88-74·4
88-75·5
15831-t0-4
91-94·1
99·09-2
534-52-t
101-55-3
59-50·7
106-47-8
7005·72-3
100·01·6
100·02-7
83-32-9
208-96-8
62-53·3
120-12-7
56·55-3
50·J2.8
205-99·2
191-24·2
207-08·9
65·85·0
85·68-7
111-91-1
111-44-4
Date Prep:
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
05.19.15 15.40
RL
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.370
0.739
0.370
0.739
1.85
0.370
0.370
0.370
0.185
0.370
0.370
0.370
0.739
0.739
0.370
0.370
0.370
0.370
0.370
0.370
0,370
0.370
0.370
0.739
0.370
0.370
O.t85
MDL
0.0654
0.0599
0.0584
0.0577
0.0680
0.0713
0.0469
0.0673
0.0595
0.0480
0.0673
0.0662
0.0565
0.0517
0.0495
0.0466
0.109
0.0540
0.0510
0.0643
0.0628
0.0528
0.0613
0.0702
0.0562
0.0455
0.0517
0.0628
0.0407
0.0547
0.0599
0.0543
0.0602
0.0610
0.0636
0.0584
0.0554
0.0443
0.0525
Page 20 of96
Basis: Dry Weight
Units Analysis Date
mg/kg 05.21.15 05.32
rug/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
rug/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
rug/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
rug/kg 05.21.15 05.32
mg/kg 05.2!.15 05.32
mg/kg 05.2l.l5 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
mg/kg 05.21.15 05.32
Flnal1.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
Dlt
Certificate of Analytical Results 507823 Jif .. ~ -~::. ......
Terraquest Environmental Consultants, P .c., Mebane,NC
Hasty Mart #23
Sample ld: MW2 (2-3) Matrix: Soil Date Received:05.14.15 09.30
Lab Sample Id: 507823-002 Date Collected: 05.12.15 10.49 Sample Depth: 2 - 3 ft
Analytical Method: SVOCs by SW-846 8270D Prep Method: SW3545
Tech: lliG %Moisture: 11.37
Analyst: CLAR Date Prep: 05.19.15 15.40 Basis: Dry Weight
Seq Number: 968618
Parameter Cas Number Result RL l\IDL Units Analysis Date Flag Dlt
bis(2-chloroisopropyl) ether 39638-32-9 u 0.370 0.0499 rug/kg 05.2!.l5 05.32 u
bis(2-ethylhexyl) phthalate 1!7-81-7 u 0.370 0.0599 rug/kg 05.2!.l5 05.32 u
Chrysene 218-01-9 u 0.370 0.0492 rug/kg 05.2!.l5 05.32 u
Dibenz(a,h)Anthracene 53-70-3 u 0.370 0.0717 rug/kg 05.2!.l5 05.32 u
Dibenzofuran 132-64-9 u 0.370 0.0473 rug/kg 05.2!.l5 05.32 u
Diethyl Phthalate 84-66-2 u 0.370 0.0595 rug/kg 05.21.15 05.32 u
Dimethyl Phthalate 131-ll-3 u 0.370 0.0558 rug/kg 05.2!.l5 05.32 u
di-n-Butyl Phthalate 84-74-2 u 0.370 0.0680 rug/kg 05.2!.l5 05.32 u
di-n-Octyl Phthalate 117-84-0 u 0.370 0.0613 rug/kg 05.21.15 05.32 u
Fluoranthene 206-44-0 u 0.370 0.0480 rug/kg 05.2!.l5 05.32 u
Fluorene 86-73-7 u 0.370 0.0451 rug/kg 05.21.15 05.32 u
Hexachlorobenzene 118-74-1 u 0.370 0.0617 rug/kg 05.21.15 05.32 u
Hexachlorobutadiene 87-68-3 u 0.370 0.0410 mg/kg 05.21.15 05.32 u
Hexachlorocyclopentadiene 77-47-4 u 0.370 0.0636 rug/kg 05.21.15 05.32 u
Hexachloroethane 67-72-1 u 0.370 0.0573 mg/kg 05.2!.l5 05.32 u
Indeno( 1 ,2,3-c,d)Pyrene 193-39-5 u 0.370 0.0673 mg/kg 05.21.15 05.32 u
Isophorone 78-59-1 u 0.370 0.0381 rug/kg 05.2!.l5 05.32 u
Naphthalene 91-20-3 u 0.370 0.0591 mglkg 05.2!.l5 05.32 u
Nitrobenzene 98-95-3 u 0.370 0.0658 rug/kg 05.21.15 05.32 u
N-Nitrosodi-n-Propylamine 62t-64-7 u 0.370 0.0528 mg/kg 05.21.15 05.32 u
N-Nitrosodiphenylamine 86-30-6 u 0.370 0.0776 mg/kg 05.21.15 05.32 u
Pentachlorophenol 87-86-5 u 0.739 0.0669 rug/kg 05.21.15 05.32 u
Phenanthrene 85-01-8 u 0.370 0.0613 mg/kg 05.21.15 05.32 u
Phenol 108-95-2 u 0.370 0.0517 mg/kg 05.21.15 05.32 u
Pyrene 129-00-0 u 0.370 0.0628 rug/kg 05.21.15 05.32 u
Pyridine I 10-86-1 u 0.370 0.0702 mg/kg 05.21.15 05.32 u
%
Surrogate Cas Number Recoyery Units Limits Analysis Date Flag
2-Fluorophenol 367-12-4 46 % 25-121 05.2!.15 05.32
Nitrobenzene-d5 4165-60-0 45 % 23-120 05.21.15 05.32
2-Fluorobiphenyl 321-60-8 47 % 30-115 05.2!.15 05.32
2,4,6-Tribromophenol 118-79-6 67 % 19-122 05.21.15 05.32
Terphenyl-D14 1718-51-0 64 % 18-137 05.2!.15 05.32
Phenol-d5 4165-62-2 49 % 15-110 05.2!.15 05.32
Page 21 of96 Final1.000
Sample Id: MW2 (2-3)
lab Sample Id: 507823-002
Analytical Method: MADEP VPH
Tech: VBR
Analyst: ZHO
Seq Number: 968507
Parameter
C5-C8 Aliphatics
C9-Ct2 Aliphatics
C9-C10 Aromatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 I 0.49
Date Prep: 05.19.15 09.10
Cas Number Result RL ~IDL
ALHYDRC5C8 u 0.00557 0.00557
ALHYDRC9CI: u 0.00557 0.00557
HYDC9CIO 0.746 0.00186 0.00186
% Cas Number Recovery Units
615-59-8 114 %
615-59-8 102 %
Page 22 of96
Units
mgfkg
mg/kg
mg/kg
Limits
70-130
70-130
Date Received:05.14.15 09.30
Sample Depth: 2 -3 ft
Prep Method: SW5030B
%Moisture: 11.37
Basis: Dry Weight
Analysis Date Flag
05.19.15 13.36 u
05.19.15 13.36 u
05.19.15 13.36 X
Analysis Date Flag
05.19.15 13.36
05.19.1513.36
Final1.000
Dll
50
50
50
Sample Id: MW2 (2-3)
lab Sample ld: 507823-002
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 10.49
Date Received:05.14.l5 09.30
Sample Depth: 2 -3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
%Moisture: 11.37 Tech: MWE
Analyst: ZHO
Seq Number: 968428
Parameter
1,1, l-Trichloroethane
1,1,2,2-Tetrachloroethane
1 ,1,2-Trichloroethane
1, 1-Dichloroethane
1 ,1-Dichloroethene
1 ,1-Dichloropropene
1 ,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1 ,2 ,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
l ,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromoch\oromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Cas Number
71-55·6
79-34·5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78·87-5
108-67-8
541-73-1
142-28-9
106-46·7
594-20-7
78-93-3
95-49-8
591-78·6
106-43-4
99·87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124·48-1
75-00-3
67-66-3
74·87-3
156-59-2
Date Prep: 05.17.15 10.14
Result RL
u 0.00073
u 0.0015
u 0.00073
u 0.00073
u 0.0015
u 0.00073
u 0.00073
u 0.0015
u 0.00073
u 0.00073
u 0.00073
u 0.0015
u 0.00073
u 0.00073
u 0.00073
u 0.00073
u 0.00073
u 0.00073
u 0.00073
u 0.0073
u 0.00073
u 0.0073
u 0.00073
u 0.00073
u 0.0073
0.036 0.0073
0.00079 0.00073
u 0.00073
u 0.0015
u 0.00073
u 0.00073
u 0.0036
u 0.00073
u 0.00073
u 0.00073
u 0.0036
u 0.00073
u 0.0036
u 0.00073
Page 23 of 96
MDL
0.00055
0.00087
0.00049
0.00058
0.00085
0.00039
0.00042
0.0012
0.00064
0.00052
0.00063
0.00094
0.00044
0.00068
0.00059
0.00073
0.00050
0.00050
0.00044
0.0017
0.00052
0.00082
0.00040
0.00058
0.0024
0.0050
0.00037
0.00062
0.00073
0.00037
0.00070
0.0018
0.00054
0.00042
0.00072
0.0018
0.00054
0.0017
0.00048
Basis: Dry Weight
Units Analysis Date
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.1515.18
mg./kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 t5.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
rug/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg 05.17.15 15.18
mg/kg
mgfkg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
05.17.15 15.18
05.17.15 15.18
05.17.15 15.18
05.17.15 15.t8
05.17.15 15.18
05.17.15 15.18
05.17.1515.18
05.17.15 t5.18
05.17.15 15.18
05.17.15 15.18
05.17.1515.18
05.17.15 15.18
05.17.15 15.18
05.17.15 15.18
Flna11.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Certificate of Analytical Results 507823 Jif "" -~'"~, .....
Terraquest Environmental Consultants, P.C., Mebane,NC
Hasty Mart #23
Sample Id: MW2 (2-3) Matrix: Soil Date Received:05.14.15 09.30
Lab Sample ld: 507823-002 Date Collected: 05.12.15 10.49 Sample Depth: 2 -3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech: MWE %Moisture: 11.37
Analyst: ZHO Date Prep: 05.17.15 10.14 Basis: Dry Weight
Seq Number: 968428
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis-1 ,3-Dichloropropene 10061-01-5 u 0.00073 0.00039 mglkg 05.17.15 15.!8 u
Dichlorodifluoromethane 75-71-8 u 0.0015 0.00086 mglkg 05.17.15 15.18 u
Ethanol 64-17-5 u 0.036 0.020 mglkg 05.!7.15 15.18 u
Ethylbenzene 100-41-4 u 0,00073 0.00041 mglkg 05.17.15 15.18 u
Isopropyl Ether 108-20-3 u 0.0015 0.00093 mglkg 05.17.15 15.18 u
Isopropylbenzene 98-82-8 u 0.00073 0.00055 mglkg 05.17.1515.18 u
m1p-Xylencs 179601-23-1 -0.00206 0.00146 0.000881 mglkg 05.!7.15 15.18
Methyl tert-butyl ether 1634-04-4 u 0.0015 0.00051 mglkg 05.17.15 15.18 u
Methylene chloride 75-09-2 u 0.0036 0.0016 mglkg 05.17.15 15.18 u
Naphthalene 91-20-3 u 0.0015 0.00095 mglkg 05.17.15 15.18 u
n-Butylbenzene 104-51-8 u 0.00073 0.00064 mglkg 05.17.15 15.18 u
n-Propylbenzene 103-65-1 u 0.00073 0.00057 mglkg 05.17.1515.18 u
a-Xylene 95-47-6 u 0.000729 0.000522 mglkg 05.17.15 15.18 u
sec-Butylbenzene 135-98-8 u 0.00073 0.00048 mglkg 05.17.15 15.18 u
Styrene 100-42-5 u 0.00073 0.00054 mglkg 05.17.15 15.18 u
tert-Butylbenzene 98-06-6 u 0.00073 0.00061 mglkg 05.17.15 15.18 u
Tetrachloroethene 127-18-4 0.0034 0.0015 0.00076 mglkg 05.17.15 15.18
Toluene 108-88-3 0.0031 0.00073 0.00043 mglkg 05.17.15 15.18
trans-! ,2-Dichloroethene 156-60-5 u 0.00073 0.00057 mglkg 05.17.15 15.18 u
trans-1,3-Dich loropropene 10061-02-6 u 0.00073 0.00049 mglkg 05.17.15 15.18 u
Trichloroethene 79-01-6 u 0.00073 0.00052 mglkg 05.17.15 15.18 u
Trichlorofluoromethane 75-69-4 u 0.0036 0.0026 mglkg 05.17.15 15.18 u
Vinyl acetate 108-05-4 u 0.0036 0.00053 mglkg 05.17.15 15.18 u
Vinyl chloride 75-01-4 u 0.0036 0.0015 mglkg 05.17.15 15.18 u
% Surrogate Cas Number Recovery Units Limits Analysis Date Flag
l ,2-Dichloroethane-D4 17060-07-0 130 % 50-150 05.17.15 15.18
4-Bromofluorobenzene 460-00-4 103 % 57-158 05.17.15 15.18
Toluene-DS 2037-26-5 !OJ % 50-150 05.17.15 15.18
Page 24 of96 Final1.000
Sample Jd: MW3 (2-3)
Lab Sample Id: 507823-003
Analytical Method: MADEP VPH
Tech: VBR
Analyst: ZHO
Seq Number: 968507
Parameter
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-C10 Aromatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 11.29
Date Prep: 05.19.15 09.10
Cas Number Result RL MDL
ALHYDRC5C8 11.9 0.00488 0.00488
ALHYDRC9C I; 5.22 0.00488 0.00488
HYDC9CIO 3.20 0.00163 0.00163
% Cas Number Reco\'cry Units
615-59-8 Ill %
615-59-8 95 %
Page 25 of 96
Units
mglkg
mglkg
mglkg
Limits
70-130
70-130
Date Received:05.14.15 09.30
Sample Depth: 2 - 3 ft
Prep Method: SW5030B
%Moisture: 12.66
Basis: Dry Weight
Analysis Date Flag
05.19.15 14.20
05.19.15 14.20
05.19.1514.20
Analysis Date Flag
05.19.1514.20
05.19.15 14.20
Flnal1.000
Dtl
50
50
50
Sample ld: MW3 (2-3)
Lab Sample Id: 507823-003
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 11.29
Date Received:05.14.15 09.30
Sample Depth: 2-3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
%Moisture: 12.66 Tech: ZHO
Analyst: ZHO
Seq Number: 968474
Parameter
I, 1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
l, 1-Dichloroethane
1, 1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1 ,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1 ,2,4-Tri methylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-TrimethyJbenzene
I ,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2~Dichloropropane
2~Butanone (MEK)
2~Chlorotoluene
2~Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1 ,2-Dichloroethene
Cas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50·1
107-06-2
78-87-5
108-67-8
541-73-1
142-28·9
106-46-7
594-20·7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83·9
56-23-5
108-90-7
124-48-1
75·00·3
67-66-3
74-87-3
156-59-2
Date Prep: 05.19.15 10.40
Result RL
u 0.00075
u 0.0015
u 0.00075
u 0.00075
u 0.0015
u 0.00075
u 0.00075
u 0.0015
u 0.00075
1.0 0.034
u 0.00075
u 0.0015
u 0.00075
u 0.00075
0.058 0.00075
u 0.00075
u 0.00075
u 0.00075
u 0.00075
u 0.0075
u 0.00075
u 0.0075
u 0.00075
0.0047 0.00075
u 0.0075
0.10 0.0075
0.071 0.00075
u 0.00075
u 0.0015
u 0.00075
u 0.00075
u 0.0037
u 0.00075
u 0.00075
u 0.00075
u 0.0037
u 0.00075
u 0.0037
u 0.00075
Page 26 of96
MDL
0.00056
0.00089
0.00050
0.00060
0.00087
0.00040
0.00043
0.0012
0.00065
0.625
0.00065
0.00097
0.00045
0.00070
0.00061
0.00075
0.00052
0.00051
0.00045
0.0017
0.00053
0.00085
0.00041
0.00060
0.0024
0.0052
0.00038
0.00064
0.00075
0.00038
0.00072
0.0018
0.00056
0.00043
0.00074
0.0018
0.00056
0.0017
0.00050
Basis: Dry \Veight
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Analysis Date
05.19.15 21.14
05.19.15 21.14
05.19.15 2!.14
05.19.15 2!.14
05.19.15 21.14
05.19.15 21.14
05.19.15 2!.14
05.19.15 21.14
05.19.15 21.14
05.18.15 18.27
05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.!5 21.14
mglkg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 21.14
mg/kg 05.19.15 2!.14
mg/kg 05.19.!5 21.14
Flnal1.000
Flag
u
u
u
UF
u
u
u
u
u
D
u
u
u
u
u
u
UH
u
UF
u
u
u
u
u
u
u
u
u
u
u
u
u
u
UF
u
Dil
50
1
Certificate of Analytical Results 507823 .a. NU -.!:'~ ......
Terraquest Environmental Consultants, P.C., Mebane,NC
Hasty Mart #23
Sample Id: l\IW3 (2-3) Matrix: Soil Date Received:05.14.15 09.30
Lab Sample ld: 507823-003 Date Collected: 05.12.15 11.29 Sample Depth: 2 -3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech: ZHO %Moisture: 12.66
Analyst: ZHO Date Prep: 05.19.15 10.40 Basis: Dry Weight
Seq Number: 968474
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis~ 1,3-Dichloropropene 10061-01-5 u 0.00075 0.00040 rng/kg 05.19.15 21.14 u
Dichlorodifluoromethane 75-71-8 u 0.0015 0.00088 rng!kg 05.19.15 21.14 u
Ethanol 64-17-5 u 0.037 0.021 mg/kg 05.19.15 21.14 UH
Ethylbenzene 100-41-4 0.90 0.034 0.019 rng/kg 05.18.15 18.27 D 50
lsopropyl Ether 108-20-3 0.0048 0.0015 0.00095 mg/kg 05.19.15 21.14 LF I
Isopropylbenzene 98-82-8 0.013 0.00075 0.00057 mg/kg 05.19.15 21.14 I
m,p-Xylenes 179601-23-1 3.9 0.068 0.041 mg/kg 05.18.15 18.27 D 50
Methyl tcrt-butyl ether 1634-04-4 0.0055 0.0015 0.00052 mg/kg 05.19.15 21.14
Methylene chloride 75-09-2 u 0.0037 0.0016 mg/kg 05.19.15 21.14 u
Naphthalene 91-20-3 0.0032 0.0015 0,00097 rng/kg 05.19.15 21.14
n-Butylbenzene 104-51-8 0.0075 0.00075 0.00066 mg/kg 05.19.15 21.14
n-Propylbenzene 103-65-1 0.040 0.00075 0.00059 mg/kg 05.19.1521.14
o-Xylene 95-47-6 0.80 0.034 0.024 rng!kg 05.18.15 18.27 D 50
scc-Butylbenzene 135-98-8 0.0019 0.00075 0.00049 rug/kg 05.19.15 21.14
Styrene !00-42-5 u 0.00075 0.00056 rng/kg 05.19.15 21.14 u
tert-Butylbenzene 98-06-6 u 0.00075 0.00062 mg!kg 05.19.15 21.14 u
Tetrachloroethene 127-18-4 u 0.0015 0.00078 mg/kg 05.19.15 21.14 u
Toluene 108-88-3 O.ol5 0.00075 0.00044 mg/kg 05.19.15 21.14
trans-1,2-Dichloroethene 156-60-5 u 0.00075 0.00058 mg/kg 05.19.15 21.14 u
trans-1 ,3-Dich loropropene I 0061-02-6 u 0.00075 0.00050 rng/kg 05.19.15 21.14 u
Trichloroethene 79-01-6 u 0.00075 0.00053 mg!kg 05.19.15 21.14 u
Trichlorofluoromethane 75-69-4 u 0.0037 0.0026 rug/kg 05.19.15 21.14 u
Vinyl acetate 108-05-4 u 0.0037 0.00054 rng/kg 05.19.15 21.14 u
Vinyl chloride 75-01-4 u 0.0037 0.0015 mg!kg 05.19.15 21.14 u
% Surrogate Cas Number Recovery Units Limits Analysis Date Flag
1 ,2·Dichloroethane·D4 17060-07-0 117 % 50-150 05.19.15 21.14
4-Bromofluorobenzene 460-00-4 114 % 57-158 05.19.15 21.14
Toluene-D8 2037-26-5 103 % 50-150 05.19.15 21.14
Page 27 of 96 Final 1.000
Sample Id: MW4 (2-3)
Lab Sample Id: 507823-004
Analytical Method: MADEP VPH
Tech: VBR
Analyst: ZHO
Seq Number: 968507
Parameter
C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Soil
Date Collected: 05.12.15 12.01
Date Prep: 05.19.15 09.10
Cas Number Result RL MDL
ALHYDRC5C8 32.8 0.00583 0.00583
ALHYDRC9C1: 8.99 0.00583 0.00583
HYDC9C10 4.82 0.00194 0.00194
% Cas Number Recovery Units
615-59-8 104 %
615-59-8 91 %
Page 28 of 96
Units
mglkg
mglkg
mglkg
Limits
70-130
70-130
Date Received:05.14.15 09.30
Sample Depth: 2 - 3 ft
Prep Method: SW5030B
%Moisture: 11.16
Basis: Dry Weight
Analysis Date Flag
05.19.15 15.05
05.19.15 15.05
05.19.15 15.05
Analysis Date Flag
05.19.15 15.05
05.19.15 15.05
Final1.000
Dil
50
50
50
Sample Id: MW4 (2-3)
Lab Sample Id: 507823-004
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Matt #23
Matrix: Soil
Date Collected: 05.12.15 12.01
Date Received:05.14.15 09.30
Sample Depth: 2 - 3 ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
% Moisture: 11.16 Tech: ZHO
Analyst: ZHO
Seq Number: 968474
Parameter
1,1,1-Trichloroethane
1,1 ,2 ,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
I, 1-Dichloropropene
1,2,3-Trichlorobenzene
l ,2,3-Trichloropropane
1,2.4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetmchloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1 ,2-Dichloroethene
Cas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120·82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108·67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49·8
591-78-6
106·43·4
99-87-6
108-10-1
67·64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
Date Prep: 05.19.15 10.40
Result RL
u 0.00071
u 0.0014
u 0.00071
u 0.00071
u 0.0014
u 0.00071
u 0.00071
u 0.0014
u 0.00071
1.2 0.040
u 0.00071
u 0.0014
u 0.00071
u 0.00071
0.064 0.00071
u 0.00071
u 0.00071
u 0.00071
u 0.00071
u 0.0071
u 0.00071
u 0.0071
u 0.00071
O.o15 0.00071
u 0.0071
0.14 0.0071
0.068 0.00071
u 0.00071
u 0.0014
u 0.00071
u 0.00071
u 0.0035
u 0.00071
u 0.00071
u 0.00071
u 0.0035
u 0.00071
u 0.0035
u 0.00071
Page 29 of 96
MDL
0.00053
0.00084
0.00047
0.00057
0.00082
0.00038
0.00041
0.0012
0.00062
0.029
0.00061
0.00091
0.00042
0.00066
0.00057
0.00070
0.00049
0.00048
0.00042
0.0016
0.00050
0.00080
0.00039
0.00056
0.0023
0.0049
0.00036
0.00060
0.00071
0.00035
0.00068
0.0017
0.00052
0.00041
0.00070
0.0017
0.00052
0.0016
0.00047
Basis: Dry 'Veight
Units
rug/kg
mg/kg
mg/kg
rug/kg
rug/kg
mg/kg
rug/kg
mg/kg
mg/kg
rug/kg
mg/kg
mg/kg
mg/kg
mg!kg
rug/kg
mg/kg
mg/kg
rug/kg
mg/kg
mg!kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rug/kg
mg/kg
mg/kg
mg/kg
mg!kg
mg!kg
mg/kg
mg/kg
rug/kg
mg/kg
mg/kg
mg!kg
mg/kg
mg!kg
Analysis Date
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.18.15 18.52
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
05.19.15 21.39
Final1.000
Flag
u
u
u
UF
u
u
u
u
u
D
u
u
u
u
u
u
UH
u
UF
u
u
u
u
u
u
u
u
u
u
u
u
u
u
UF
u
DH
50
Certificate of Analytical Results 507823 11:. "~ ... ~~ .......
Terraquest Environmental Consultants, P.C., Mebane,NC
Hasty Mmi #23
Sample Id: MW4(2-3) Matrix: Soil Date Received:05.14.15 09.30
Lab Sample Id: 507823-004 Date Collected: 05.12.15 t2.01 Sample Depth:2-3ft
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech: ZHO %Moisture: 11.16
Analyst: ZHO Date Prep: 05.19.15 10.40 Basis: Dry Weight
Seq Number: 968474
Parameter Cas Number Result RL l\IDL Units Analysis Date :Flag Dll
cis~ 1 ,3 ~Dichloropropene 10061-01-5 u 0.00071 0.00038 mgikg 05.19.15 21.39 u
Dichlorodifluoromethane 75-71-8 u 0.0014 0.00083 rug/kg 05.19.15 21.39 u
Ethanol 64-17-5 u 0.035 0.020 mglkg 05.19.15 21.39 UH
Ethylbenzene !00·41-4 1.1 0.040 0.022 mgikg 05.18.15 18.52 D 50
Isopropyl Ether 108-20·3 0.0074 0.0014 0.00090 rug/kg 05.19.t5 21.39 LF
Isopropylbenzene 98-82-8 O.otS 0.00071 0.00054 rug/kg 05.19.15 21.39
m,p-Xylenes 179601-23-1 5.6 0.079 0.048 mgikg 05.18.15 18.52 D 50
Methyl tert-butyl ether 1634-04-4 0.020 0.0014 0.00049 mgikg 05.19.15 21.39
Methylene chloride 75-09-2 0.0026 0.0035 0.0015 mglkg 05.19.15 21.39 J
Naphthalene 91-20-3 u 0.0014 0.00092 mglkg 05.19.15 21.39 u
n-Butylbenzene 104-51-8 0.0082 0.00071 0.00062 rug/kg 05.19.15 21.39
n-PropyJbenzene 103·65-1 0.042 0.00071 0.00055 rug/kg 05.19.15 21.39
o-Xylene 95-41·6 1.7 0.040 0.028 mgikg 05.18.15 18.52 D 50
sec-Butylbenzene 135-98-8 0.0022 0.00071 0.00046 rug/kg 05.19.15 21.39
Styrene 10042-5 u 0.00071 0.00052 mglkg 05.19.15 21.39 u
tert-Butylbenzene 98-06·6 u 0.00071 0.00059 mg/kg 05.19.15 21.39 u
Tetmchloroethene 127-18-4 u 0.0014 0.00073 mglkg 05.19.15 21.39 u
Toluene 108-88-3 0.11 0.00071 0.00042 mglkg 05.19.15 21.39
trans-1,2-Dichloroethene 156-60·5 u 0.00071 0.00055 mgikg 05.19.15 21.39 u
trans-1,3-Dichloropropene 10061-02-6 u 0.00071 0.00047 mglkg 05.19.15 21.39 u
Trichloroethene 79-01·6 u 0.0007t 0.00050 mglkg 05.19.15 21.39 u
Trichlorofluoromethane 75-69-4 u 0.0035 0.0025 mgikg 05.19.15 21.39 u
Vinyl acetate 108-05·4 u 0.0035 0.00051 mgikg 05.19.15 21.39 u
Vinyl chloride 15·014 u 0.0035 0.0014 mglkg 05.19.15 21.39 u
% Surrogate Cas Number Recovery Units Limits Analysis Date Flag
1,2-Dichloroethane-D4 17060·07-0 114 % 50-150 05.19.15 21.39
4-Bromofluorobenzene 460-00-4 t18 % 57-158 05.19.15 21.39
Toluene-DB 2037-26-5 103 % 50·150 05.19.15 21.39
Page 30 of96 Flnal1.000
Sample Id: MWl
lab Sample Id: 507823-005
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground \Vater
Date Collected: 05.12.15 15.24
Date Received:05.14.15 09.30
Analytical Method: Select Metals by SW-846 6010C Prep Method: SW30 I OA
%Moisture: Tech: 4099
Analyst: 4150
Seq Number: 968525
Parameter
Chromium
Lead
Analytical Method:
Tech: BRO
MADEPEPH
Analyst: CLAR
Seq Number: 968763
Parameter
Cll-C22 Aromatics
C9·Cl8 Aliphatics
C19-C36 Aliphatics
Surrogate
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Date Prep: 05.19.15 13.10
Cas Number Result RL MDL
(
7440-47-3 7o.o979 0.0500 0.000300
7439-92-1 u 0.0100 0.00330
Date Prep: 05.19.15 13.30
Cas Number Result RL MDL
Cl!C22 u 98.5 98.5
ALHYDRC9Cll u 98.5 98.5
ALHYDRC 19C: u 98.5 98.5
% Cas Number Recovery Units
3386-33-2 89 %
84-15-1 82 %
321-60-8 80 %
Page 31 of96
Units Analysis Date Flag
mg!L 05.20.15 12.12
mg!L 05.20.15 12.12 u
Prep Method: SW3510C
%Moisture:
Units Analysis Date Flag
ug!L 05.21.!5 20.36 u
ug/L 05.21.!5 03.28 u
ug!L 05.21.!5 03.28 u
Limits Analysis Date Flag
40-140 05.21.15 03.28
40-140 05.21.15 20.36
40-140 05.21.15 20.36
Flnal1.000
Jif. "~ -..= ......
Dil
Dil
Sample Id: MWl
Lab Sample Id: 507823-005
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.l4.15 09,30
Date Collected: 05.12.15 15.24
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: E625P
%Moisture: Tech: BRO
Analyst: CLAR
Seq Number: 968853
Parameter
1 ,2 ,4~ Trichlorobenzene
1 ,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1 ,3-Dinitrobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4.6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro·3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-.ch1oroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Cas Number
120-82-1
95-50-1
122-66-7
541-73-1
99-65-0
106-46-7
90-12-0
88-06-2
120-83-2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94-1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
t20-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
1t1-44-4
39638-32-9
117-81-7
85-68-7
Date Prep: 05.19.15 14.00
Result RL MDL
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Page 32 of96
9.39
9.39
9.39
9,39
47.0
9.39
9,39
9.39
9.39
9.39
18.8
9.39
9.39
9.39
9.39
9.39
18.8
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
18.8
9.39
9.39
9.39
9.39
9.39
9.39
1.34
1.72
4.47
1.98
18.8
1.51
1.31
1.54
1.67
!.53
6.68
1.21
1.72
1.12
1.88
1.83
2.39
3.64
1.31
1.99
2.05
2.90
1.27
2.26
1.34
1.39
1.89
1.78
1.69
1.85
1.85
2.54
2.08
1.15
1.17
1.67
1.16
1.13
1.71
Units
ugiL
ug!L
ugiL
ugiL
ug/L
ugiL
ugiL
ugiL
ug/L
ugiL
ugiL
ug/L
ugiL
ug/L
ugiL
ugiL
ug/L
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
11g/L
ugiL
ugiL
ugiL
ug/L
ugiL
ugiL
ug/L
ugiL
ugiL
ugiL
Analysis Date
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
05.21.15 21.26
Final1.000
Flag
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Sample Id: MWl
Lab Sample Id: 507823-005
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.24
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: E625P
%Moisture: Tech: BRO
Analyst: CLAR Date Prep: 05.19.15 14.00
Seq Number: 968853
Parameter Cas Number Result RL MDL Units Analysis Date Flag
Chrysene 218-01-9 u 9.39 1.96 ug/L 05.21.15 21.26 u
Dibenz(a,h)Anthracene 53-70-3 u 9.39 1.72 ug/L 05.2!.!5 21.26 u
Dibenzofuran 132-64-9 u 9.39 !.54 ug/L 05.2!.!5 21.26 u
Diethyl Phthalate 84-66-2 u 9.39 1.78 \!giL 05.2!.!5 21.26 u
Dimethyl Phthalate !31-ll-3 u 9.39 1.85 ug/L 05.2!.!5 21.26 u
di-n-Butyl Phthalate 84-74-2 u 9.39 !.95 ug/L 05.2!.!5 21.26 u
di-n-Octyl Phthalate !!7-84-0 u 9.39 1.30 ug/L 05.2!.!5 2!.26 u
Fluoranthene 206-44-0 u 9.39 1.70 ugfL 05.2!.!5 21.26 u
Fluorene 86-73-7 u 9.39 1.46 ug/L 05.2!.!5 21.26 u
Hexachlorobenzene !!8-74-l u 9.39 2.08 ug/L 05.2l.l5 21.26 u
Hexachlorobutadiene 87-68-3 u 9.39 1.67 ug/L 05.2l.l5 21.26 u
Hexachlorocyclopentadiene 77-47-4 u 9.39 1.76 ug/L 05.2l.l5 21.26 u
Hexachloroethane 67-72-l u 9.39 2.23 ug/L 05.2!.!5 21.26 u
Indeno(1,2,3-c,d)Pyrene 193-39-5 u 9.39 1.76 ug/L 05.2l.l5 21.26 u
Isophorone 78-59-1 u 9.39 1.32 ug/L 05.21.15 21.26 u
Naphthalene 91-20-3 u 9.39 !.43 ugfL 05.2!.!5 21.26 u
Nitrobenzene 98-95-3 u 9.39 1.40 ug/L 05.2l.l5 21.26 u
n-Nitrosodi-n-Propylamine 621-64-7 u 9.39 1.28 ug/L 05.2l.l5 2!.26 u
n-Nitrosodiphenylamine 86-30-6 u 9.39 2.35 ug/L 05.2!.!5 21.26 UH
Pentachlorophenol 87-86-5 u 9.39 2.12 ug/L 05.2l.l5 21.26 UH
Phenanthrene 85-01-8 u 9.39 !.92 ug/L 05.21.15 21.26 u
Phenol 108-95-2 u 9.39 1.65 ug/L 05.2l.l5 21.26 u
Pyrene 129-00-0 u 9.39 2.25 ug/L 05.2l.l5 2!.26 u
Trlchloroacetlc add, hexadecyl es (IIC) TIC 5.92 ugfL 05.2!.!5 21.26 JN
%
Surrogate Cas Number Recovery Units Limits Analysis Date Flag
2-Fluorobiphenyl 32!-60-8 71 % 44-!!7 05.2l.l5 21.26
2-Fluorophenol 367-12-4 64 % 30-100 05.2l.l5 2!.26
2,4,6-Tribromophenol 118-79-6 93 % 48-!!7 05.2l.l5 2!.26
Nitrobenzene-d5 4165-60-0 67 % 46-lll 05.2l.l5 2!.26
Phenol-d5 4165-62-2 68 % 50-200 05.21.15 21.26
Terphenyl-014 1718-51-0 87 % 46-126 05.2l.l5 21.26
Page 33 of 96 Final1.000
Dil
Sample ld: MWl
Lab Sample Id: 507823-005
Analytical Method: MADEP VPH
Tech: VBR
Analyst: ZHO
Seq Number: 968516
Parameter
C5-C8 Aliphatics
C9-CIO Aromatics
C9-Cl2 Aliphatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.l4.15 09.30
Date Collected: 05.12.15 15.24
Prep Method: SW5030B
%Moisture:
Date Prep: 05.19.15 09.10
Cas Number Result RL MDL Units Analysis Date Flag
ALHYDRC5C8 u 0.0150 0.0150 ug!L 05.19.15 15.49 u
HYDC9C10 u 0.00500 0.00500 ug!L 05.19.15 !5.49 u
ALHYDRC9C1: u 0.0150 0.0150 ug/L 05.!9.15 15.49 u
% Cas Number Recovery Units Limits Analysis Date Flag
615-59-8 105 % 70-130 05.!9.15 15.49
615-59-8 93 % 70-130 05.19.15 15.49
Page 34 of96 Final1.000
Dll
Sample Id: MWl
Lab Sample Id: 507823-005
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground \Vater Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.24
Analytical Method: VOCs by GC/MS by SM6200B Prep Me1hod: SM6200B _PREP
%Moisture: Tech: ZHO
Analyst: ZHO
Seq Number: 968479
Parameter
1,1, 1,2-Tetrachloroethane
1 ,1,1-Trichloroethane
1,1 ,2 ,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1,1-Dichloroethane
l ,1-Dichloroethene
1, 1-Dichloropropene
1,2,3-Trichlorobenzene
1 ,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1 ,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1 ,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chlorofonn
Chloromethane
Cas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
Date Prep: 05.19.15 09.49
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
RL
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
OAOO
0.500
0.500
OAOO
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Page 35 of 96
MDL
0.180
0.0760
O.o700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Units
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
Analysis Date
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.1514.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
05.19.15 14.38
Fina11.000
Flag
u
u
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
011
Sample Id: 1\1\Vl
Lab Sample ld: 507823-005
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.24
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Tech: ZHO %Moisture:
Analyst: ZHO Date Prep: 05.19.15 09.49
Seq Number: 968479
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis-1 ,2·Dichloroethene t56-59-2 u 0.500 0.114 ug!L 05.19.15 14.38 u
cis-I ,3-Dichloropropene 10061-01-5 u 1.00 0.100 ug!L 05.19.15 14.38 u
Dichlorodifluoromethane 75-71-8 u 1.00 0.0670 ug!L 05.19.15 14.38 u
Ethanol 64-17-5 u 50.0 3.00 ug!L 05.19.15 14.38 u
Ethylbenzene 100-41-4 u 0.500 0.0920 ug!L 05.19.15 14.38 u
Isopropyl ether 108-20-3 u 0.500 0.0920 ug!L 05.19.15 14.38 u
lsopropylbenzene 98-82-8 u 0.500 0.0980 ug!L 05.19.15 14.38 u
Methyl tert-butyl ether Qv1TBE) 1634-04-4 u 0.500 0.169 ug!L 05.19.15 14.38 u
Methylene Chloride 75-0~-2 u 0.500 0.190 ug!L 05.19.15 14.38 u
Naphthalene 91-20-3 u 2.00 0.0940 ug!L 05.19.1514.38 u
n-Butylbenzene 104-51-8 u 2.00 0.0600 ug!L 05.19.15 14.38 u
n-Propylbenzene 103-65-1 u 1.00 0.0650 ug!L 05.19.15 14.38 u
sec-Butylbenzene 135-98-8 u 0.500 0.0920 ug!L 05.19.15 14.38 u
Styrene 100-42-5 u 0.500 0.0740 ug!L 05.19.15 14.38 u
tert-Butylbenzene 98-06-6 u 0.500 0.0890 ug!L 05.19.1514.38 u
Tetmchloroethene (PCE) 127-18-4 u 0.500 0.0540 ug!L 05.19.15 14.38 u
Toluene 108-88-3 u 0.500 0.0570 ug!L 05.19.15 14.38 u
tmns-1 ,2-Dichloroethene 156-60-5 u 0.500 0.188 ug!L 05.19.15 14.38 u
trans-1 ,3 -Dichloropropene I006t-02-6 u 1.00 0.1 10 ug!L 05.19.15 14.38 u
Trichloroethene 79-01-6 u 0.500 0.139 ug!L 05.19.15 14.38 u
Trichlorofluoromethane 75-69-4 u 0.500 0.0540 ug!L 05.19.15 14.38 u
Vinyl Acetate 108-05-4 u 1.00 0.720 ug!L 05.19.15 14.38 u
Vinyl Chloride 75-01-4 u 0.500 0.0810 ug!L 05.19.15 14.38 u
m,p~Xylenes 179601-23-1 u 1.00 0.176 ug!L 05.19.15 14.38 u
o~Xylene 95-47-6 u 0.500 0.122 ug!L 05.19.15 14.38 u
% Surrogate Cas Number Reeoyery Units Limits Analysis Date Flag
1,2-Dichloroethane~D4 17060-07-0 105 % 65-126 05.19.1514.38
4-Bromofluorobenzene 460-00-4 108 % 86-111 05.19.1514.38
Toluene-D8 2037-26-5 101 % 83-116 05.19.15 14.38
Page 36 of96 Final1.000
Sample Id: MW2
Lab Sample Id: 507823-006
Analytical Method: MADEP EPH
Tech: BRO
Analyst: CLAR
Seq Number: 968763
Parameter
C11-C22 Aromatics
C9-C18 Aliphatics
Cl9-C36 Aliphatics
Surrogate
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water
Date Collected: 05.12.15 15.14
Date Received:05.14.15 09.30
Prep Method: SW3510C
%Moisture:
Date Prep: 05.19.15 13.30
Cas Number Result RL MDL Units Analysis Date Flag
C11C22 u 96.6 96.6 ug!L 05.21.15 21.1 t u
ALHYDRC9Cil u 96.6 96.6 ug!L 05.21.15 03.59 u
ALHYDRC19C: u 96.6 96.6 ug/L 05.21.15 03.59 u
% Cas Number Recovery Units Limits Analysis Date Flag
3386-33-2 82 % 40-140 05.21.15 03.59
84-15-1 97 % 40-140 05.21.15 21.11
321-60-8 85 % 40-140 05.21.15 21.11
Page 37 of 96 Flnal1.000
Dll
Sample Id: l\IW2
Lab Sample Id: 507823-006
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.14
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: E625P
%Moisture: Tech: BRO
Analyst: CLAR
Seq Number: 968853
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
I ,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
l ,3-Dinitrobenzene
1,4-Dichlorobenzene
1-1\lethylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-MethyJnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-I\Iethylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthmcene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluomnthene
Benzo{g,h,i)petylene
Benzo(k)fluomnthene
Benzoic Acid
Benzyl Alcohol
bis{2-chloroethoxy) methane
bis(2-chtoroethyl) ether
bis(2-chloroisopropyl) ether
bis{2-ethylhexyl) phthalate
Butyl benzyl phthalate
Cas Number
120-82-1
95-50-1
122-66-7
541-73-t
99-65-0
106-46-7
90-t2-0
88-06-2
120-83-2
t05-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
9t-94-t
534-52-1
tOI-55-3
59-50-7
!06-47-8
7005-72-3
t00-02-7
83-32-9
208-96-8
120-t2-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
llt-91-1
11!-44-4
39638-32-9
117-8t-7
85-68-7
Date Prep:
Result
u
u
u
u
u
u
I 3.86
u
u
j5.68
u
u
u
J 8.08
u
u
... 37.5
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
05.19.15 14.00
RL
9.39
9.39
9.39
9.39
47.0
9.39
9.39
9.39
9.39
9.39
18.8
9.39
9.39
9.39
9.39
9.39
t8.8
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
9.39
t8.8
9.39
9.39
9.39
9.39
9.39
9.39
MDL
!.34
1.72
4.47
!.98
18.8
1.51
1.31
!.54
1.67
1.53
6.68
!.21
!.72
l.t2
1.88
!.83
2.39
3.64
!.31
1.99
2.05
2.90
1.27
2.26
!.34
!.39
1.89
1.78
1.69
1.85
!.85
2.54
2.08
1.15
t.l7
1.67
1.!6
t.13
1.71
Page 38 of96
Units
ug/L
ug/L
ug/L
ug/L
ug/L
l'g/L
ug/L
ug/L
ug/L
l'g/L
l>g/L
ug/L
ug/L
l'g/L
l'g/L
ug/L
ugfL
l'g/L
ug/L
l>g/L
l'g/L
ug/L
ug/L
l'g/L
l'g/L
l'g/L
ug/L
l'g/L
l>g/L
l'g/L
ug/L
ug/L
l'g/L
l'g/L
ug/L
ug/L
l'g/L
ug/L
ug/L
Analysis Date
05.2l.t5 2!.54
05.2l.t5 2!.54
05.21.15 21.54
05.21.15 21.54
05.2l.t5 21.54
05.21.15 21.54
05.21.15 21.54
05.21.15 21.54
05.2l.t5 2!.54
05.21.15 21.54
05.2l.t5 2!.54
05.2l.t5 2!.54
05.21.15 21.54
05.2l.t5 21.54
05.21.15 21.54
05.21.15 21.54
05.2l.t5 21.54
05.21.15 21.54
05.21.15 21.54
05.2l.t5 2!.54
05.21.15 21.54
05.21.15 21.54
05.2l.t5 2!.54
05.21.15 21.54
05.21.15 21.54
05.2l.t 5 21.54
05.2l.t5 2!.54
05.2l.t5 2!.54
05.2l.t5 2!.54
05.2l.t5 21.54
05.2l.t5 21.54
05.2l.t5 21.54
05.2l.t5 21.54
05.21.15 2!.54
05.21.15 2!.54
05.2l.t5 2!.54
05.2l.t5 21.54
05.2l.t5 21.54
05.2l.t5 21.54
Final1.000
Flag
u
u
u
u
UH
u
J
u
u
J
u
u
u
J
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Certificate of Analytical Results 507823 Jif .. ~ -.!.."~ .......
Tenaquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Sample Id: MW2 Matrix: Ground \Vater Date Received:05.14.15 09.30
Lab Sample Jd: 507823-006 Date Collected: 05.12.15 15.14
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: E625P
Tech: BRO %Moisture:
Analyst: CLAR Date Prep: 05.19.15 14.00
Seq Number: 968853
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dll
Chrysene 218-01-9 u 9.39 1.96 ug/L 05.2l.l5 21.54 u
Dibenz(a,h)Anthracene 53-70-3 u 9.39 1.72 ug!L 05.2l.l5 21.54 u
Dibenzofuran 132-64-9 u 9.39 !.54 ug/L 05.2l.l5 21.54 u
Diethyl Phthalate 84-66-2 u 9.39 1.78 ug/L 05.2l.l5 21.54 u
Dimethyl Phthalate 131-11-3 u 9.39 1.85 ug/L 05.2l.l5 21.54 u
di-n-Butyl Phthalate 84-74-2 u 9.39 1.95 ug/L 05.2l.l5 21.54 u
di-n-Octyl Phthalate 117-84-0 u 9.39 1.30 ug/L 05.2l.l5 21.54 u
Fluornnthene 206-44-0 u 9.39 1.70 ug/L 05.2l.l5 21.54 u
Fluorene 86-73-7 u 9.39 1.46 ug/L 05.2l.l5 21.54 u
Hexachlorobenzene 118-74-1 u 9.39 2.08 ug/L 05.2l.l5 21.54 u
Hexachlorobutadiene 87-68-3 u 9.39 1.67 ug/L 05.2l.l5 21.54 u
Hexachlorocyclopentadiene 77-47-4 u 9.39 1.76 ug/L 05.2l.l5 21.54 u
Hexachloroethane 67-72-1 u 9.39 2.23 ug/L 05.2l.l5 21.54 u
Indeno(l,2,3-c,d)Pyrene I93-39-5 u 9.39 1.76 ug/L 05.2l.l5 21.54 u
Isophorone 78-59-1 u 9.39 1.32 ug/L 05.2l.l5 21.54 u
Naphthalene 91-20-3 t70.I 9.39 1.43 ug/L 05.2l.l5 21.54
Nitrobenzene 98-95-3 u 9.39 1.40 ug/L 05.2l.l5 21.54 u
n-Nitrosodi-n-Propylamine 621-64-7 u 9.39 1.28 ug/L 05.2l.l5 21.54 u
n-Nitrosodiphenylamine 86-30-6 u 9.39 2.35 ug/L 05.21.15 21.54 UH
Pentachlorophenol 87-86-5 u 9.39 2.12 ug/L 05.2l.l5 21.54 UH
Phenanthrene 85-01-8 u 9.39 1.92 ug/L 05.2!.15 21.54 u
Phenol 108-95-2 u 9.39 1.65 ug/L 05.2!.15 21.54 u
Pyrene 129-00-0 u 9.39 2.25 ug/L 05.2!.15 21.54 u
Benzene, 1,2,3-trlmethyl-(TIC) TIC 74.6 ug/L 05.2!.15 21.54 JN
Benzene, 1,2,4-trlmethyl-(II C) TIC 89.6 ug/L 05.2l.l5 21.54 JN
Benzene, 1,3,5-trimethyl-(TIC) TIC 235 ug/L 05.2!.15 21.54 JN
Benzene, 1,3-dimethyl-(TIC) TIC 358 ug/L 05.2!.15 21.54 JN
Benzene,1-ethyl-2-methyl-(TIC) TIC 183 ug/L 05.21.15 21.54 JN
Ethylbenzene (TIC) TIC 204 ug/L 05.21.15 21.54 JN
Indane (II C) TIC 80.5 ug/L 05.21.15 21.54 JN
Toluene (TIC) TIC 280 ug/L 05.2!.15 21.54 JN
p-Xylene (TIC) TIC 545 ug/L 05.2l.l5 21.54 JN
unknown (TIC) TIC 56.0 ug/L 05.21.15 21.54 JN
% Surrogate Cas Number Recoyery Units Limits Analysis Date Flag
2-Fluorobiphenyl 321-60-8 76 % 44-117 05.2l.l5 21.54
2-Fluorophenol 367-I2-4 67 % 30-100 05.21.15 21.54
2,4,6-Tribromophenol II8-79-6 96 % 48-117 05.2!.15 21.54
Nitrobenzene-d5 4I65-60-0 73 % 46-111 05.2!.15 21.54
Phenol-d5 4I65-62-2 72 % 50-200 05.2!.15 21.54
Page 39 of 96 Flnal1.000
Sample Id: MW2
Lab Sample Id: 507823-006
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.14
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: E625P
%Moisture: Tech: BRO
Analyst: CLAR
Seq Number: 968853
Surrogate
Terphenyl-014
Analytical Method:
Tech: VBR
Analyst: ZHO
MADEPVPH
Seq Number: 968516
Parameter
C5-C8 Allphatics
C9-C10 Aromatics
C9-Cl2 Allphatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Cas Number
ALHYDRC5C8
HYDC9Ct0
Date Prep: 05.19.15 14.00
Cas Number
1718-51-0
%
Recovery
86
Units
%
Date Prep: 05.19.15 09.10
Result RL MDL
I 207 0.0150 0.0150
12140 0.0250 0.0250
ALHYDRC9C1: j2700 0.0750 0.0750
%
Cas Number RecoYery Units
615-59-8 124 %
615-59-8 107 %
Page 40 of96
Limits
46-126
Units
ugiL
ug/L
ugiL
Limits
70-130
70-130
Analysis Date
05.21.15 21.54
Flag
Prep Method: SW5030B
%Moisture:
Analysis Date Flag
05.19.15 18.47
05.19.15 17.18 D
05.19.15 17.18 D
Analysis Date Flag
05.19.15 18.47
05.19.15 18.47
Final1.000
Dil
5
5
Sample Id: MW2
Lab Sample Id: 507823-006
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Matt #23
Matrix: Ground Water Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.14
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B_PREP
%Moisture: Tech:
Analyst:
ZHO
ZHO
Seq Number: 968479
Parameter
1,1,1,2-Tetrachloroethane
1,1 ,1-Trichloroethane
1,1 ,2,2-Tetrachloroethane
1,1,2-Trichloroethane
l ,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1 ,2,4-Trichlorobenzene
1,2 ,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
I ,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetmchloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Cas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
Date Prep: 05.19.15 09.49
Result RL MDL
u
u
u
u
u
u
u
u
u
u
\762
u
u
u
u
\. 238
u
u
u
u
,7,67
u
u
u
,s.2o
u
'-14.4
'36.4
u
u
u
u
u
u
u
u
u
'1.63
u
Page41 of96
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
10.0
1.00
0.500
0.500
0.500
10.0
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0,400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
2.06
0.180
0.0940
0.0900
0.122
1.74
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Units
ug/L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ugfL
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug/L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug/L
Analysis Date
05.19.15 17.51
05.19.1517.51
05.19.15 17.51
05.19.15 17.51
05.19.1517.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.1517.51
05.19.15 17.51
05.20.1512.11
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.20.15 12.11
05.19.15 17.51
05.19.1517.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
05.19.15 17.51
Ftnal1.000
Flag
u
u
u
u
u
u
u
u
UH
u
D
u
u
u
u
D
u
u
u
u
J
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
Dil
20
20
Certificate of Analytical Results 507823 Jif. .. ~
-.!:'::.,,., ..
Terraquest Environmental Consultants, P.C., Mebane,NC
Hasty Mart #23
Sample Id: MW2 Matrix: Ground \Vater Date Received:05.14.15 09.30
Lab Sample Id: 507823-006 Date Collected: 05.12.15 15.14
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Tech: ZHO %Moisture:
Analyst: ZHO Date Prep: 05.19.15 09.49
Seq Number: 968479
Parameter Cas Number Result RL MDL Units Analysis Date .Flag Dil
cis-1 ,2-Dichloroethene 156-59-2 u 0.500 0.114 ug!L 05.19.15 17.51 u
cis-1 ,3-Dichloropropene 10061-01-5 u 1.00 0.100 ug!L 05.19.15 17.51 u
Dichlorodifluoromethane 75-71-8 u 1.00 0.0670 ug/L 05.19.1517.51 u
Ethanol 64-17-5 u 50.0 3.00 ug!L 05.19.1517.51 u I
Ethylbenzene 100-41-4 -593 10.0 1.84 ug!L 05.20.15 12.11 D 20
Isopropyl ether 108-20-3 u 0.500 0.0920 ug!L 05.19.15 17.51 u
Jsopropylbenzene 98-82-8 -37.2 0.500 0.0980 ug!L 05.19.1517.51
Methyl tert-butyl ether (MfBE) 1634-04-4 u 0,500 0.169 ug!L 05.19.15 17.51 u
Methylene Chloride 75-09-2 u 0.500 0.190 ug!L 05.19.15 17.51 u
Naphthalene 91-20-3 -238 40.0 1.88 ug/L 05.20.15 12.11 D 20
n-Butylbenzene 104-51-8 u 2.00 0.0600 ug!L 05.19.15 17.51 u I
n-Propylbenzene 103-65-1 -119 20.0 1.30 ug!L 05.20.15 12.11 D 20
sec-Butylbenzene 135-98-8 _4,41 0.500 0.0920 ug!L 05.19.15 17.51
Styrene 100-42-5 u 0.500 0.0740 ug!L 05.19.15 17.51 u
tert-Butylbenzene 98-06-6 u 0.500 0.0890 ug!L 05.19.15 17.51 u
Tetrachloroethene (PCB) 127-18-4 u 0.500 0.0540 ug!L 05.19.15 17.51 u I
Toluene 108-88-3 -957 10.0 1.14 ug!L 05.20.15 12.11 D 20
trans-1 ,2-Dichloroethene 156-60-5 u 0.500 0.188 ug!L 05.19.1517.51 u
trans-1 ,3-Dichloropropene 10061-02-6 u 1.00 0.110 ug!L 05.19.15 17.51 u
Trichloroethene 79-01-6 u 0.500 0.139 ug!L 05.19.15 17.51 u
Trichlorofluoromethane 75-694 u 0.500 0.0540 ug!L 05.19.15 17.51 u
Vinyl Acetate 108-05-4 u 1.00 0.720 ug!L 05.19.1517.51 u
Vinyl Chloride 75-01-4 u 0.500 0.0810 ug!L 05.19.15 17.51 u
m,p·Xylenes 179601-23-1 -1810 20.0 3.52 ug!L 05.20.15 12.11 D 20
O·Xylene 95-47-6 ..... 890 10.0 2.44 l>g/L 05.20.15 12.11 D 20
%
Surrogate Cas Number Recovery Units Limits Analysis Date Flag
1 ,2·Dichloroethane· D4 17060-07-0 100 % 65-126 05.19.15 17.51
4-Bromofluorobenzene 460-00-4 109 % 86-111 05.19.15 17.51
Toluene-DS 2037-26-5 105 % 83-116 05.19.15 17.51
Page 42 of 96 Final 1.000
Sample Id: MW3
Lab Sample Id: 507823-007
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground \Vater Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.30
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
%Moisture: Tech: 4099
Analyst: 4150 Date Prep: 05.19.15 13.10
Seq Number: 968525
Parameter Cas Number Result RL MDL
Lead 7439-92-1 u 0.0100 0.00330
Ana1ytica1Method: EDB byEPA504.1
Tech: CLAR
Analyst: CLAR
Seq Number: 968570
Parameter
1,2-Dibromoethane (EDB)
Surrogate
4-Bromofluorobenzene
Analytical Method: MADEPVPH
Tech: VBR
Analyst: ZHO
Seq Number: 968516
Parameter
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 A1ipbatics
Surrogate
2,5-Dibromoto\uene
2,5-Dibromotoluene (Pill)
Date Prep: 05.20.15 10.35
Cas Number Result RL MDL
106-93-4 u 0.0510 0.00612
%
Cas Number RecoYery Units
460-00-4 109 %
Date Prep: 05.19.15 09.10
Cas Number Result RL MDL
ALHYDRC5C8 3370 0.0150 0.0150
HYDC9CIO 2950 0.0250 0.0250
ALHYDRC9CI: 3800 0.0750 0.0750
%
Cas Number RecoYery Units
615-59-8 149 %
615-59-8 133 %
Page 43 of 96
Units Analysis Date Flag
mg!L 05.20.15 12.14 u
Prep Method: E504.1P
%Moisture:
Units Analysis Date Flag
ug!L 05.20.15 19.48 u
Limits Analysis Date Flag
60-140 05.20.15 19.48
Prep Method: SW5030B
%Moisture:
Units Analysis Date Flag
ug!L 05.19.15 19.31
ug!L 05.19.15 18.02 D
ug!L 05.19.15 18.02 D
Limits Analysis Date Flag
70-130 05.19.15 19.31 ••
70-130 05.19.15 19.31 ..
Final1.000
Dil
Dil
Dil
5
5
Sample Id: MW3
Lab Sample ld: 507823-007
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground \Vater Date Received:05.14.15 09.30
Date Colleoted: 05.12.15 15.30
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
%Moisture: Tech: ZHO
Analyst: ZHO
Seq Number: 9684 79
Parameter
1,1,1,2-Tetrachloroethane
1,1, !-Trichloroethane
1,1 ,2,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1,1-Dichloroethane
1, 1-Dichloroethene
1,1 -Dichloropropene
1,2,3-Trichlorobenzene
l ,2,3-Trichloropropane
I ,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
l ,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
l ,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MJBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Cas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
Date Prep:
Result
u
u
v
v
u
v
u
u
v
v
'1190
v
u
u
v
'-299
u
v
u
v
v
u
u
v
'4.19
u
'10.7
'736
v
v
u
u
v
u
u
v
v
'-·0.320
v
05.19.15 09.49
RL
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
10.0
1.00
0.500
0.500
0.500
10.0
0.500
0.500
0.500
0.200
20.0
0.200
OAOO
0.500
0.500
OAOO
2.00
10.0
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
MDL
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
2.06
0.180
0.0940
0.0900
0.122
1.74
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
2.38
0.132
0.112
0.124
0.159
0.0970
0,0990
0.105
0.177
0.0420
0.172
0.0850
Page 44 of96
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analysis Date
05.19.1517.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.1517.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.1517.24
05.20.15 11.31
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.1517.24
05.20.15 11.31
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.1517.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.20.15 11.31
05.19.15 17.24
05.19.1517.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
05.19.15 17.24
Flnai1.000
Flag
u
u
v
v
u
u
v
u
UH
v
D
u
v
u
u
D
u
u
v
u
u
v
u
u
u
D
UH
u
v
u
u
v
v
u
u
J
u
Dil
20
20
20
Sample Id: MW3
Lab Sample Id: 507823-007
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground Water Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.30
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Tech: ZHO %Moisture:
Analyst: ZHO Date Prep: 05.19.15 09.49
Seq Number: 968479
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis~ 1 ,2~Dichloroethene 156-59-2 u 0.500 0.114 ug/L 05.19.15 17.24 u
cis-1 ,3-Dichloropropene 10061-01-5 u 1.00 0.100 ug/L 05.19.15 17.24 u
Dichlorodifluoromethane 75-71-8 u 1.00 0.0670 ug/L 05.19.15 17.24 u
Ethanol 64-17-5 u 50.0 3.00 ug/L 05.19.15 17.24 u
Ethylbenzene 100-41-4 ,-1270 10.0 1.84 \lg/L 05.20.15 I 1.31 D 20
Isopropyl ether 108-20-3 -35.9 0.500 0.0920 ug/L 05.19.15 17.24
Isopropylbenzene 98-82-8 -39.5 0.500 0.0980 ug/L 05.19.15 17.24
Methyl tert-butyl ether (MTBE} 1634-04-4 -29.0 0.500 0.169 ug/L 05.19.1517.24
Methylene Chloride 75-09-2 u 0.500 0.190 ug/L 05.19.15 17.24 u
Naphthalene 91-20-3 -549 40.0 1.88 ug/L 05.20.15 11.31 D 20
n-Butylbenzene 104-51-8 u 2.00 0.0600 ug/L 05.19.15 17.24 u
n-Propylbenzene 103-65-1 -142 20.0 1.30 ug/L 05.20.15 11.31 D 20
sec-Butylbenzene 135-98-8 -4.41 0.500 0.0920 ug/L 05.19.15 17.24
Styrene 100-42-5 u 0.500 0.0740 ug/L 05.19.15 17.24 u
tert-Butylbenzene 98-06-6 u 0.500 0.0890 ug/L 05.19.15 17.24 u
Tetrn.chloroethene (PCE) 127-18-4 u 0.500 0.0540 ug/L 05.19.15 17.24 u 1
Toluene 108-88-3 -4630 50.0 5.70 ug/L 05.20.15 13.34 D 100
trans-1 ,2-Dichloroethene 156-60-5 u 0.500 0.188 ug/L 05.19.15 17.24 u
trans-1 ,3-Dichloropropene 10061-02-6 u 1.00 0.110 ug/L 05.19.15 17.24 u
Trichloroethene 79-01-6 u 0.500 0.139 ug/L 05.19.15 17.24 u
Trichlorofluoromethane 75-69-4 u 0.500 0.0540 ug/L 05.19.15 17.24 u
Vinyl Acetate 108-05-4 u 1.00 0.720 ug/L 05.19.15 17.24 u
Vinyl Chloride 75-01-4 u 0.500 0.0810 ug/L 05.19.15 17.24 u
m,p-Xylenes 179601-23-1 ~4450 100 17.6 ug/L 05.20.15 13.34 D 100
o-Xylene 95-47-6 _2160 50.0 12.2 ug/L 05.20.15 13.34 D 100
%
Surrogate Cas Number Recovery Units Limits Analysis Date Flag
1,2-Dichloroethane-D4 17060-07-0 119 % 65-126 05.19.15 17.24
4-Bromofluorobenzene 460-00-4 105 % 86-111 05.19.15 17.24
Toluene-D8 2037-26-5 101 % 83-116 05.19.1517.24
Page 45 of 96 Final 1.000
Sample Id: .MW4
Lab Sample ld: 507823-008
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: Ground \Vater Date Received:05.14.15 09.30
Date Collected: 05.12.15 !5.Q4
Analytical Method: Lead by SW-846 60IOC Prep Method: SW30 I OA
%Moisture: Tech: 4099
Analyst: 4150 Date Prep: 05.19.15 13.10
Seq Number: 968525
Parameter Cas Number Result RL MDL
Lead 7439-92-1 u 0.0100 0.00330
Analytical Method: EDB by EPA 504.1
Tech: CLAR
Analyst: CLAR Date Prep: 05.20.15 10.35
Seq Number: 968570
Parameter Cas Number Result RL MDL
1,2~Dibromoethane (EDB) 106-93-4 u 0.0507 0.00608
% Surrogate Cas Number Recoyery Units
4~Bromofluorobenzene 460-00-4 103 %
Analytical Method: MADEPVPH
Tech: VBR
Analyst: ZHO Date Prep: 05.19.15 09.10
Seq Number: 968516
Parameter Cas Number Result RL MDL
cs~cs Aliphatics ALHYDRC5C8 19.9 0.0150 0.0150
C9-C10 Aromatics HYDC9C10 21.8 0.00500 0.00500
C9-Cl2 Aliphatics ALHYDRC9C1: 35.0 0.0150 0.0150
% Surrogate Cas Number Recoyery Units
2,5-Dibromotoluene 615-59-8 116 %
2,5-Dibromotoluene (PID) 615-59-8 99 %
Page 46 of96
Units
mg!L
Units
ug!L
Limits
60·140
Units
ug!L
ug!L
ug!L
Limits
70-130
70-130
Analysis Date Flag
05.20.15 12.16 u
Prep Method: E504.1P
%Moisture:
Analysis Date Flag
05.20.15 20.12 u
Analysis Date Flag
05.20.15 20.12
Prep Method: SW5030B
%Moisture:
Analysis Date Flag
05.19.15 16.34
05.19.15 16.34
05.19.15 16.34
Analysis Date Flag
05.19.15 16.34
05.19.15 16.34
F1nal1.000
Dil
Dll
Dil
Sample Id: MW4
Lab Sample Id: 507823-008
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Matt #23
Matrix: Ground \Vater
Date Collected: 05.12.15 15.o4
Date Received:05.14.15 09.30
Analytical Method: VOCs by GC!MS by SM6200B Prep Method: SM6200B _PREP
%Moisture: Teclt: ZHO
Analyst: ZHO
Seq Number: 968479
Parameter
1 , I, I ,2-T etmchloroethane
1,1,1-Trichloroethane
1,1 ,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1 ,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
I ,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Jsopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Cas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
Date Prep: 05.19.15 09.49
Result RL MDL
u
u
u
u
u
u
u
u
u
u
-2.72
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
-5.77
u
u
u
u
u
u
u
u
u
u
u
Page 47 of 96
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
OAOO
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Units
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ugiL
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ugiL
ug!L
ug!L
ugiL
ug!L
ugiL
ug!L
ug!L
ug!L
ug!L
ug!L
ugiL
ug!L
ug!L
ug!L
ug!L
Analysis Date
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.1516.58
05.19.15 16.58
05.19.15 16.58
05.19.1516.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.1516.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
05.19.15 16.58
Flnal1.000
Flag
u
u
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
UH
u
u
u
u
u
u
u
u
u
u
Dl!
Sample Id: MW4
Lab Sample Id: 507823-008
Certificate of Analytical Results 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Matt #23
Matrix: Ground \Vater Date Received:05.14.15 09.30
Date Collected: 05.12.15 15.04
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Tech: ZHO %Moisture:
Analyst: ZHO Date Prep: 05.19.15 09.49
Seq Number: 968479
Parameter Cas Number Result RL l\IDL Units Analysis Date Flag Dll
cis-I ,2-Dichloroethene 156-59-2 u 0.500 0.114 ug/L 05.19.15 16.58 u
cis-1 ,3-Dich \oropropene 10061-01-5 u 1.00 0.100 ug!L 05.19.15 16.58 u
Dichlorodifluoromethane 75-71-8 u 1.00 0.0670 ug!L 05.19.15 16.58 u
Ethanol 64-17-5 u 50.0 3.00 ug!L 05.19.15 16.58 u
Ethylbenzene 100-41-4 '--8.37 0.500 0.0920 ug!L 05.19.15 16.58
Isopropyl ether 108-20-3 -1.08 0.500 0.0920 ug!L 05.19.15 16.58
Isopropylbenzene 98-82-8 u 0.500 0.0980 ug!L 05.19.15 16.58 u
Methyl tert-butyl ether (l\lTBE) 1634-04-4 -3.19 0.500 0.169 ug/L 05.19.15 16.58
Methylene Chloride 75-09-2 u 0.500 0.190 ug!L 05.19.15 16.58 u
Naphthalene 91-20-3 -1.17 2.00 0.0940 ug!L 05.19.15 16.58 J
n-Butylbenzene 104-51-8 u 2.00 0.0600 ug!L 05.19.15 16.58 u
n-Propylbcnzene 103-65-1 '1.12 1.00 0.0650 ug!L 05.19.15 16.58
sec-Butylbenzene 135-98-8 u 0.500 0.0920 ug/L 05.19.15 16.58 u
Styrene 100-42-5 u 0.500 0.0740 ug!L 05.19.15 16.58 u
tert-Butylbenzene 98-06-6 u 0.500 0.0890 ug!L 05.19.15 16.58 u
Tetrachloroethene (PCB) 127-18-4 u 0.500 0.0540 ug!L 05.19.15 16.58 u
Toluene 108-88-3 u 0.500 0.0570 ug!L 05.19.1516.58 u
trans-1 ,2-Dichloroethene 156-60-5 u 0.500 0.188 ug!L 05.19.15 16.58 u
trans-I ,3 -Dichloropropene 10061-02-6 u 1.00 0.110 ug!L 05.19.15 16.58 u
Trichloroethene 79-01-6 u 0.500 0.139 ug!L 05.19.15 16.58 u
Trichlorofluoromethane 75-69-4 u 0.500 0.0540 ug!L 05.19.15 16.58 u
Vinyl Acetate 108-05-4 u 1.00 0.720 ug!L 05.19.15 16.58 u
Vinyl Chloride 75-01-4 u 0.500 0.0810 ug!L 05.19.15 16.58 u
m,p-Xylenes 179601-23-1 _17.2 1.00 0.176 ug!L 05.19.15 16.58
o-Xylene 95-47-6 -5.65 0.500 0.122 ug/L 05.19.15 16.58
% Surrogate Cas Number RecoYery Units Limits Analysis Date Flag
1,2-Dichloroethane-D4 17060-07-0 108 % 65-126 05.19.15 16.58
4-Bromofluorobcnzene 460-00-4 100 % 86-111 05.19.15 16.58
Toluene-D8 2037-26-5 99 % 83-116 05.19.15 16.58
Page 48 of98 Final1.000
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical Method: Percent Moisture by SM2540G
Seq Number: 968193 Matrix: Soil
Parent Sample Id:
Parameter
Percent Moisture
Analytical Method:
Seq Number:
MB Sample Id:
Parameter
Chromium
Analytical Method:
Seq Number:
MB Sample Id:
Parameter
Chromium
Lead
Analytical Method:
Seq Number:
Parent Sample Id:
Parameter
Chromium
Analytical Method:
Seq Number:
Parent Sample Id:
Parameter
Chromium
Lead
507823-001 MD Sample Id: 507823-001 D
Parent
Result
8.93
MD
Result
8.76
Select Metals by SW-846 6010C
968286 Matrix:
692613-1-BLK LCS Sample Id:
MB Spike LCS LCS
Result Amount Result %Rec
<0.0600 100 114 114
Select Metals by SW-846 6010C
968525 Matrix:
692750-1-BLK LCS Sample Id:
~m Spike LCS LCS
Result Amount Result %Rec
0.000900 1.00 1.01 101
<0.00330 1.00 0.998 100
Select Metals by SW-846 6010C
968286 Matrix:
507892-005 MD Sample Id:
Parent MD
Result Result
6.83 7.27
Select Metals by SW-846 6010C
968525 Matrix:
507850-001 MD Sample Id:
Parent MD
Result Result
0.00600 0.00590
<0.00330 <0.00330
Solid
692613-1-BKS
LCSD LCSD
Result %Rec
104 104
Water
692750-l-BKS
LCSD LCSD
Result %Rec
0.957 96
0.942 94
Soil
507892-005 D
Ground Water
507850-001 D
Page 49 of 96
Limits
75-125
Limits
80-120
80-120
%RPD RPD
Limit
2 20
Prep Method:
Date Prep:
Units
%
Analysis
Date
05.14.15 16:30
SW3050B
05.15.15
LCSD Sample Id: 692613-1-BSD
%RPD RPD Units Analysis
Limit Date
9 20 mglkg 05.17.1518:07
Prep Method: SW30!0A
Date Prep: 05.19.15
LCSD Sample Id: 692750-1-BSD
%RPD RPD Units Analysis
Limit Date
5 20 mg/L 05.20.1511:42
6 20 mg/L 05.20.15 I 1:42
Prep Method: SW3050B
Date Prep: 05.15.15
%RPD RPD Units Analysis
Limit Date
6 20 mglkg 05.17.1518:27
Prep Method: SW3010A
Date Prep: 05.19.15
%RPD RPD Units Analysis
Limit Date
2 20 mg/L 05.20.15 11:48
0 20 mg/L 05.20.15 11:48
Final1.000
Flag
Flag
Flag
Flag
Flag
J
u
QCSummary 507823
Terraquest Environmental Consultants, P .C.
Hasty Matt #23
Analytical.Method: Select Metals by SW-846 6010C
Seq Number: 968286 Matrix:
Parent Sample Id: 507892-005 MS Sample Id:
Parameter Parent Spike MS MS
Resu1t Amount Result %Rec
Chromium 6.83 94.3 112 112
Analytical ~Method: Select Metals by SW-846 6010C
Seq Number: 968525 Matrix:
Parent Sample Id: 507850·001 MS Sample Id:
Parameter Parent Spike MS MS
Result Amount Result %Rec
Chromium 0.00600 1.00 1.01 100
Lead <0.00330 1.00 0.964 96
Analytical Method: Chromium, Hexavalent by S\V 7196A
Seq Number: 968402 Matrix:
MB Sample Id: 968402-1-BLK LCS Sample Id:
Parameter ~m Spike LCS LCS
Result Amount Result %Rec
Chromium, Hexavalent <0.400 10.0 9.52 95
Analytical Method: Chromium, Hexavalent by SW 7196A
Seq Number: 968402
Parent Sample Id: 507373-001
Parameter
Chromium, Hexavalent
Parent
Result
0.792
Matrix:
MD Sample Id:
MD
Result
0.792
Analytical Method: Chromium, Hexavalent by S\V 7196A
Seq Number: 968402 Matrix:
Parent Sample Id: 507373-001 MS Sample Id:
Parameter Parent Spike MS MS
Result Amount Result %Rec
Chromium, Hexavalent 0.792 12.2 12.3 94
Soil
507892-005 s
MSD MSD
Result %Rec
97.1 107
Ground \Vater
507850-00 I S
MSD MSD
Result %Rec
1.02 101
0.968 97
Solid
968402-1-BKS
LCSD LCSD
Result %Rec
9.16 92
Soil
507373-001 D
Soil
507373-001 s
MSD MSD
Result %Rec
12.6 97
Page 50 of96
Limits
75-125
Limits
80·120
80·120
Limits
80-120
Limits
75-125
Prep Method: SW3050B
Date Prep: 05.15.15
MSD Sample Id: 507892-005 SD
%RPD RPD Units Analysis
Limit Date
14 20 mglkg 05.17.15 18:29
Prep Method: SW3010A
Date Prep: 05.19.15
MSD Sample Id: 507850-001 SD
%RPD RPD Units Analysis
Limit Date
20 mg/L 05.20.15 11:50
0 20 mg/L 05.20.15 11:50
LCSD Sample Id: 968402-1-BSD
%RPD RPD
Limit
4 20
%RPD RPD
Limit
0 20
Units
mglkg
Units
Analysis
Date
05.17.15 10;00
Analysis
Date
mglkg 05.17.15 10;00
MSD Sample Id: 507373-001 SD
%RPD RPD Units Analysis
Limit Date
2 20 mglkg 05.17.15 10:00
Final1.000
Flag
Flag
Flag
Flag
Flag
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical.Method: EDB by EPA 504.1 Prep Method: E504.1P
Seq Number: 968570 Matrix: \Vater Date Prep: 05.20.15
MB Sample Id: 692819-1-BLK LCS Sample Id: 692819-1-BKS LCSD Sample Id: 692819-1-BSD
Parameter ~m Spike LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
1,2~Dibromoethane (EDB) <0.00600 0.250 0.242 97 0.247 99 70-130 2 20 ug!L 05.20.15 19;00
Surrogate MB MB LCS LCS LCSD LCSD Limits Units Analysis
%Rec Flag %Rec Flag %Rec Flag Date
4-Bromofluorobenzene 100 104 105 60-140 % 05.20.15 19:00
Analytical Method: EDB by EPA 504.1 Prep Method: E504.1P
Seq Number: 968570 Matrix: Ground \Vater Date Prep: 05.20.15
Parent Sample Id: 507823-008 MS Sample Id: 507823-008 s MSD Sample Id: 507823-008 SD
Parameter Parent Spike MS MS MSD MSD Limits %RPD RPD Unlts Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
1,2-Dibromoethane (EDB) <0.00606 0.252 0.237 94 0.248 98 70-130 5 20 ug!L 05.20.15 20:37
Surrogate MS MS MSD MSD Limits Units Analysis
%Rec Flag %Rec Flag Date
4-Bromofluorobenzene 102 105 60-140 % 05.20.15 20:37
Analytical Method: MADEPEPH Prep Method: SW3545
Seq Number: 968290 Matrix: Solid Date Prep: 05.14.15
MB Sample Id: 692626-1-BLK LCS Sample Id: 692626-1-BKS LCSD Sample Id: 692626-1-BSD
Parameter MB Spike LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
Cll~C22 Aromatics <20.0 170 127 75 122 72 40-140 4 40 mg/kg 05.17.1506:03
C9~C18 Aliphatics <10.0 60.0 26.7 45 28.1 47 40-140 5 40 mg/kg 05.17.1505:51
C19~C36 Aliphatics <10.0 80.0 56.5 71 55.0 69 40-140 3 40 mg/kg 05.17.15 05:51
Surrogate MB MB LCS LCS LCSD LCSD Limits Units Analysis
%Rec Flag %Rec Flag %Rec Flag Date
l·Chlorooctadecane 58 62 59 40-140 % 05.17.15 05:51
o·Terphenyl 61 79 76 40-140 % 05.17.15 06:03
2~Fluorobiphenyl 80 86 86 40-140 % 05.17.15 06:03
Page 51 of 96 Final1.000
Analytical Method: MADEP EPH
Seq Number: 968763
MB Sampleld: 692958-l-BLK
Parameter MB
Result
Cll-C22 Aromatics <lOO
C9-Cl8 Aliphatics <100
C19-C36 Aliphatics <100
Surrogate MB
%Rec
1-Chlorooctadecane 81
o-Terphenyl 96
2-Fluorobiphenyl 85
Analyticall\tlethod: MADEPEPH
Seq Number: 968290
Parent Sample Id: 507470-006
Parameter Parent
Result
Cll-C22 Aromatics 373
C9-C18 Aliphatics 523
C19-C36 Aliphatics 548
Surrogate
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Matrix: "\Vater
LCS Sample ld: 692958-l-BKS
Spike LCS LCS LCSD LCSD
Amount Result %Rec Result %Rec
1700 1590 94 1690 99
600 333 56 305 51
800 884 Ill 845 !06
MB LCS LCS LCSD
Flag %Rec Flag %Rec
85 90
108 117
86 98
Matrix: Soil
MS Sample ld: 507470-006 s
Spike MS MS MSD MSD
Amount Result %Rec Result %Rec
190 742 194 588 115
67.2 948 632 695 260
89.6 856 344 698 170
MS MS 1\lSD
%Rec Flag %Rec
66 52
107 99
119 81
Page 52 of96
Limits
40-140
40-140
40-140
Prep Method: SW3510C
Date Prep: 05.19.15
LCSD Sampleld: 692958-1-BSD
%RPD RPD Units Analysis
Limit Date
6 40 ug!L 05.2l.15 19:26
9 40 ug!L 05.2l.l5 02:25
5 40 ug!L 05.21.15 02:25
LCSD Limits Units Analysis
Flag Date
40-140 % 05.21.15 02:25
40-140 % 05.21.15 19:26
40-140 % 05.21.15 19:26
Prep Method: SW3545
Date Prep: 05.14.15
MSD Sample ld: 507470-006 SD
Limits %RPD RPD Units Analysis
Limit Date
40-140 23 40 mglkg 05.17.15 10;36
40-140 31 40 mglkg 05.17.15 10:02
40-140 20 40 mglkg 05J7.15 10;02
MSD Limits Units Analysis
Flag Date
40-140 % 05.17.15 10:02
40-140 % 05.17.15 10;36
40-140 % 05.17.15 10;36
Flnal1.000
Flag
Flag
X
X
X
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method:
Seq Number:
SVOCs by EPA 625 + 10 TICs
968853
MB Sample Id: 692889-1-BLK
Parameter
I ,2 ,4-Trichlorobenzene
I ,2-Dichlorobenzene
I ,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofhran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(I,2,3-c,d)Pyrene
Isophorone
Naphthalene
l\IB Spike
Result Amount
<1.43
<1.83
<2.11
<20.1
<1.61
<1.40
<l.64
<1.78
<1.63
<7.11
<1.29
<1.83
<1.19
<2.00
<1.95
<2.55
<1.40
<2.12
<2.18
<3.09
<1.35
<2.41
<1.43
<1.48
<2.01
<1.90
<1.80
<1.97
<1.97
<2.71
<1.23
<1.25
<1.78
<1.24
6.50
<1.82
<2.09
<1.83
<1.64
<1.90
<1.97
<2.08
<1.38
<1.81
<1.56
<2.21
<1.78
<1.87
<2.38
<1.87
<1.41
<1.52
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
Hasty Mart #23
Matrix:
LCS Sample Id:
LCS LCS
Result %Rec
40.2
37.4
36.6
59.4
36.7
43.5
45.9
45.9
46.6
48.8
45.5
39.4
43.8
42.1
43.3
46.1
49.1
47.2
49.0
56.8
46.7
62.1
44.2
48.2
49.1
51.2
51.4
48.0
50.7
47.6
53.5
46.5
40.8
48.4
51.7
52.8
49.3
50.6
44.2
46.7
46.2
48.2
52.0
48.3
45.8
46.9
40.0
58.2
39.2
50.1
57.8
41.7
80
75
73
119
73
87
92
92
93
98
91
79
88
84
87
92
98
94
98
114
93
124
88
96
98
102
103
96
101
95
107
93
82
97
103
106
99
101
88
93
92
96
104
97
92
94
80
116
78
100
116
83
\Vater
692889-1-BKS
Page 53 of 96
Limits
44-142
32-129
65-135
45-110
20-124
25-175
37-144
39-135
32-119
0-191
60-118
36-120
45-105
40-110
29-182
30-110
10-181
53-127
22-147
15-110
25-158
0-132
47-145
33-145
27-133
33-143
17-163
24-159
0-219
11-162
30-110
33-184
12-158
36-166
8-158
0-152
17-168
0-227
55-105
0-114
0-112
1-118
0-107
26-137
59-121
0-152
24-116
41-125
40-113
0-171
21-196
21-133
Prep Method:
Date Prep:
Flnal1.000
SW3510C
05.19.15
Units
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ug/L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug/L
ug!L
ug/L
Analysis
Date
05.21.l5 19:04
05.21.l5 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19;04
05.2l.l5 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.l5 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.l5 19:04
05.21.l5 19:04
05.21.l5 19:04
05.21.15 19:04
05.21.15 19:04
05.2U5 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.2l.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
05.21.15 19:04
Flag
H
H
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical.Method: SVOCs by EPA 625 + 10 TICs Prep Method: SW3510C
Seq Number: 968853 Matrix: \Vater Date Prep: 05.19.15
MB Sample Jd: 692889-1-BLK LCS Sample Jd: 692889-1-BKS
Parameter l\IB Spike LCS LCS Limits Units Analysis Flag
Result Amount Result %Rec Date
Nitrobenzene <1.49 50.0 45.7 91 35-180 ug/L 05.21.15 19:04
n-Nitrosodi-n-Propylamine <1.36 50.0 49.2 98 !0-230 ug/L 05.21.15 19:04
n-Nitrosodiphenylamine <2.50 50.0 62.4 125 50-llO ug/L 05.21.15 19:04 H
Pentachlorophenol <2.26 50.0 46.3 93 14-76 ug!L 05.21.15 19:04 H
Phenanthrene <2.04 50.0 47.8 96 54-120 ug!L 05.21.15 19;04
Phenol <1.76 50.0 40.9 82 5-112 ug!L 05.21.15 19;04
Pyrene <2.40 50.0 52.1 !04 23-152 ug/L 05.21.15 19;04
Surrogate MB MB LCS LCS Limits Units Analysis
%Rec Flag %Rec Flag Date
2-Fluorobiphenyl 76 83 39-99 % 05.21.15 19:04
2-Fluorophenol 64 72 33-92 % 05.21.15 19:04
2,4,6-Tribromophenol 98 98 32-129 % 05.21.15 19:04
Nitrobenzene-d5 76 81 37-94 % 051l.IS 19;04
Phenol-dS 68 78 50-200 % 05.21.15 19:04
Terphenyl-Dl4 90 88 18-133 % 05.2l.l5 19:04
Page 54 of96 Final1.000
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: SVOCs by EPA 625 + 10 TICs
Seq Number: 968853
Parent Sample Id: 507860-013
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Parent Spike
Result Amount
<1.38
<1.77
<2.04
<19.4
<1.56
<1.35
<1.58
<1.72
<1.57
<6.87
<1.25
<1.77
<1.15
<1.93
<1.88
<2.46
<1.35
<2.05
<2.11
<2.99
<1.30
<2.33
<1.38
<1.43
<1.94
<1.84
<1.74
<1.90
<1.90
<2.62
<1.19
<1.21
<1.72
<1.20
2.52
<1.76
<2.02
<1.77
<1.58
<1.84
<1.90
<2.01
<1.33
<1.75
<1.51
<2.14
<1.72
<1.81
<2.30
<1.81
<1.36
<1.47
48.3
38.6
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
48.3
Hasty Mart #23
Matrix: Ground \Vater
MS Sample ld: 507860-013 S
Prep Method: SW3510C
Date Prep: 05.19.15
MSD Sample Jd: 507860-013 SD
MS MS
Result %Rec
MSD MSD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date
05.21.15 23:19
Flag
30.5
27.9
27.8
47.5
27.7
33.8
39.2
39.4
36.3
44.7
37.1
31.7
35.2
34.0
33.6
37.2
41.9
39.4
41.0
30.8
39.9
55.2
37.5
39.3
41.2
41.4
38.0
40.8
39.0
36.5
40.0
35.5
32.0
38.4
44.3
43.0
39.6
41.1
38.5
40.4
39.3
40.4
41.5
40.9
39.7
38.5
28.7
8.29
28.1
38.6
44.5
32.3
63
72
58
98
57
70
81
82
75
93
77
66
73
70
70
77
87
82
85
64
83
114
78
81
85
86
79
84
81
76
83
73
66
80
87
89
82
85
80
84
81
84
86
85
82
80
59
17
58
80
92
67
Page 55 of96
30.2
27.3
27.1
47.7
26.6
34.6
38.9
38.2
34.5
45.7
36.9
30.5
34.6
33.7
33.9
37.0
44.3
41.4
41.7
44.6
41.2
55.3
38.1
39.5
43.7
45.4
41.5
40.4
40.3
38.0
42.5
34.6
31.3
36.6
47.1
46.2
41.9
41.8
38.8
41.7
40.1
43.4
45.1
43.1
40.7
40.4
28.4
9.26
27.2
39.9
44.5
31.9
61 44-142
55 32-129
55 65-135
96 45-110
54 20-124
70 25-175
79 37-144
77 39-135
70 32-119
92 0-191
75 60-118
62 36-120
70 45-105
68 40-110
68 29-182
75 30-110
89 10-181
84 53-127
84 22-147
90 15-110
83 25-158
112 0-132
77 47-145
80 33-145
88 27-133
92 33-143
84 17-163
82 24-159
81 0-219
77 11-162
86 30-110
70 33-184
63 12-158
74 36-166
90 8-158
93 0-152
85 17-168
84 0-227
78 55-105
84 0-114
81 0-112
88 1-118
91 0-107
87 26-137
82 59-121
82 0-152
57 24-116
19 41-125
55 40-113
81 0-171
90 21-196
64 21-133
2
3
0
4
2
I
3
5
2
1
4
2
6
5
2
37
3
0
2
6
9
9
3
4
6
3
2
5
6
7
6
2
1
3
2
7
8
5
2
5
I
tl
3
3
0
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Flnal1.000
ug!L
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19 X
ug!L 05.21.15 23:19
ug!L 05,21.15 23:19
ug!L 052Ll523:19
ug!L 052Ll523:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.2l.l5 23:19
ug/L 05.21.15 23:19
ug/L 05.21.15 23:19
ug/L 05.21.15 23:19
ug!L 05.21.1523:19
ug!L 05.21.15 23:19
ug!L 05.2Ll5 23:19
ug!L 05.2U5 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19 F
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.2L15 23:19
ug!L 05.21.15 23:19
ug!L 05.2L15 23:19
ug!L 05.21.15 23:19
ug!L 05.2LI5 23:19
ug!L 05,21J5 23:19
ug!L 05,21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ugiL 05.21.15 23:19
ug!L 05.21.15 23:19
ugfL 05.21.15 23:19
ug!L 05.21.15 23:19
ug/L 05.2U5 23:19
ug!L 052U5 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.15 23:19
ug/L 05.21.15 23:19
ug/L 05.21.15 23:19 x
ug/L 05.21.15 23:19
ug!L 05.21.15 23:19
ug!L 05.21.l5 23:19
ug!L 05.21.15 23:19
QCSummary 507823
Terraquest Environmental Consultants, P .C.
Hasty Mart #23
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: SW3510C
Seq Number: 968853 Matrix: Ground 'Vater Date Prep: 05.19.15
Parent Sample Id: 507860-013 MS Sample Id: 507860-013 s MSD Sample Id: 507860-013 SD
Parameter Parent Spike MS MS MSD MSD Limits %RPD RPD Units Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
Nitrobenzene <1.44 48.3 37.3 77 36.2 73 35-180 3 30 ug/L 05.2l.l5 23:19
n-Nitrosodi-n-Propylamine <1.31 48.3 38.3 79 37.8 76 10-230 30 ug/L 05.21.15 23:19
n-Nitrosodiphenylamine <2.42 48.3 36.0 75 43.0 87 50-110 18 30 ug/L 05.21.15 23:19
Pentachlorophenol <2.18 48.3 43.1 89 44.4 90 14-76 3 30 ug/L 05.21.15 23:19 X
Phenanthrene <1.97 48.3 41.1 85 43.2 87 54-120 5 30 ug/L 05.21.15 23:19
Phenol <1.70 48.3 32.2 67 31.6 64 5-t 12 2 30 ug/L 05.21.15 23:19
Pyrene <2.32 48.3 42.7 88 46.8 95 23-152 9 30 ug/L 05.21.15 23:19
Surrogate MS MS MSD MSD Limits Units Analysis
%Rec Flag %Rec Flag Date
2-Fluorobiphenyl 74 71 39-99 % 05.21.15 23:19
2-Fluorophenol 57 53 33-92 % 05.21.15 23:19
2,4,6-Tr:ibromophcnol 90 90 32-129 % 05.21.15 23:19
Nitrobenzene-d5 69 66 37-94 % 05.21.15 23:19
Phenol-d5 66 62 50-200 % 05.21.15 23:19
Terphenyl-Dl4 76 83 18-133 % 05.21.15 23:19
Page 56 of96 Final 1.000
QC Summary 507823 Jif "~ ··~ -................
Terraquest Environmental Consultants, P.C.
Analytical Method:
Seq Number:
SVOCs by SW-846 8270D
968618
MB Sample Id: 692772-1-BLK
Parameter
1,2,4-Trlchlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-methylphenol
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4-<::hloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (Phenylamine, Aminobenzene)
Anthmcene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl Butyl Phthalate
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2--chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
I\m Spike
Result Amount
<0.0590
<0.0540
<0.0527
<0.0520
<0.0613
<0.0643
<0.0423
<0.0607
<0.0537
<0.0433
<0.0607
<0.0597
<0.0510
<0.0467
<0.0447
<0.0420
<0.0987
<0.0460
<0.0580
<0.0567
<0.0477
<0.0553
<0.0633
<0.0507
<0.0410
<0.0467
<0.0567
<0.0367
<0.0493
<0.0540
<0.0490
<0.0543
<0.0550
<0.0573
<0.0500
<0.0400
<0.0473
<0.0450
<0.0540
<0.0443
<0.0647
<0.0427
<0.0537
<0.0503
<0.0613
<0.0553
<0.0433
<0.0407
<0.0557
<0.0370
<0.0573
<0.0517
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
1.67
Hasty Mart #23
Matrix:
LCS Sample Id:
Solid
692772-1-BKS
Prep Method: SW3545
Date Prep: 05.19.15
LCSD Sample Id: 692772-1-BSD
LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis
Result %Rec Result %Rcc Limit
1.25
1.26
1.27
1.23
1.22
1.20
1.30
1.36
1.31
1.25
1.25
1.26
1.29
1.29
1.40
1.27
1.36
1.28
1.12
1.23
1.31
1.61
1.26
1.25
1.56
1.22
1.33
2.14
1.36
1.40
1.42
1.37
1.26
1.35
1.57
1.32
1.35
1.53
1.60
1.38
1.34
1.23
1.28
1.25
1.38
1.53
1.29
1.26
1.27
1.20
1.57
1.36
75
75
76
74
73
72
78
81
78
75
75
75
77
77
84
76
81
77
67
74
78
96
75
75
93
73
80
128
81
84
85
82
75
81
94
79
81
92
96
83
80
74
77
75
83
92
77
75
76
72
94
81
Page 57 of 96
1.23
1.26
1.28
1.24
1.16
1.19
1.31
1.36
1.28
1.25
1.26
1.27
1.31
1.28
1.38
1.23
1.37
1.28
1.12
1.23
1.28
1.61
1.26
1.23
1.51
1.24
1.32
2.16
1.34
1.35
1.37
1.30
1.23
1.29
1.48
1.34
1.31
1.55
1.54
1.30
1.26
1.22
1.27
1.25
1.32
1.47
1.26
1.26
1.26
1.19
1.59
1.35
74 35-129
75 38-122
77 38-120
74 37-121
69 40-135
71 39-139
78 36-135
81 38-133
77 48-131
75 42-136
75 32-138
76 38-125
78 36-126
77 37-128
83 30-133
74 33-142
82 38-126
77 41-135
67 30-146
74 37-140
77 40-134
96 34-124
75 41-131
74 46-132
90 21-152
74 37-131
79 39-129
129 33-117
80 39-139
81 44-135
82 43-153
78 40-153
74 40-153
77 33-156
89 43-145
80 30-129
78 33-127
93 25-124
92 46-145
78 42-135
75 41-155
73 39-132
76 45-131
75 43-132
79 43-142
88 34-166
75 41-138
75 41-131
75 36-142
71 35-129
95 16-106
81 36-121
2
0
5
I
1
0
2
0
2
I
3
0
0
0
2
0
0
2
3
2
I
4
4
5
2
5
6
2
3
1
4
6
6
1
0
4
4
2
0
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Final1.000
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
mg/kg
rug/kg
rug/kg
mglkg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rng/kg
rng/kg
rng/kg
rng/kg
rng/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rng/kg
rng/kg
rng/kg
rug/kg
rug/kg
rug/kg
rug/kg
rng/kg
rng/kg
rng/kg
rng/kg
rng/kg
rng/kg
rng/kg
rng/kg
rng/kg
Date
05.20.1523:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.1523:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.1523:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
05.20.15 23:12
Flag
H
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical ·Method: SVOCs by SW-846 8270D Prep Method: SW3545
Seq Number: 968618 Matrix: Solid Date Prep: 05.19.15
MB Sample Id: 692772-1-BLK LCS Sample ld: 692772-1-BKS LCSD Sample Jd: 692772-1-BSD
Parameter I'ID Spike LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
Indeno(1,2,3-c,d)Pyrene <0,0607 1.67 1.31 78 1.24 74 39-154 5 30 mglkg 05.20.15 23:12
Isophorone <0,0343 1.67 1.59 95 1.60 96 36-128 I 30 mglkg 05.20.15 23:12
Naphthalene <0.0533 1.67 1.27 76 1.26 75 35-128 30 mglkg 05.20.15 23:12
Nitrobenzene <0.0593 1.67 1.36 81 1.38 83 32-129 30 mglkg 05.20.15 23:12
N-Nitrosodi-n-Propylamine <0.0477 1.67 1.48 89 1.47 88 34-129 30 mglkg 05.20.15 23:12
N-Nitrosodiphenylamine <0.0700 1.67 1.72 103 1.71 102 27-155 30 mglkg 05.20.15 23:12
Pentachlorophenol <0.0603 1.67 1.04 62 1.05 63 14-148 30 mglkg 05.20.15 23:12
Phenanthrene <0.0553 1.67 1.32 79 1.30 78 37-139 2 30 mglkg 05.20.15 23:12
Phenol <0.0467 1.67 1.24 74 1.25 75 34-127 30 mglkg 05.20.15 23:12
Pyrene <0.0567 1.67 1.45 87 1.43 86 42-138 30 mglkg 05.20.15 23:12
Pyridine <0.0633 1.67 1.30 78 1.29 77 30-113 30 mglkg 05.20.15 23:12
Surrogate ~m ~m LCS LCS LCSD LCSD Limits Units Analysis
%Rec Flag %Rec Flag %Rec Flag Date
2-Fluorophenol 82 74 75 25-121 % 05.20.15 23:12
Nitrobenzene-d5 85 77 78 23-120 % 05.20.15 23:12
2-Fluorobiphenyl 81 72 72 30-115 % 05.20.15 23:12
2,4,6-Tribromophenol 87 80 80 19-122 % 05.20.15 23:12
Terphenyl-D14 90 78 77 18-137 % 05.20.1523:12
Phenol-d5 82 75 77 15-110 % 05.20.15 23:12
Page 58 of96 Fina11.000
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: SVOCs by SW-846 8270D
Seq Number: 968618
Parent Sample Id: 507823-001
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-methylphenol
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4.chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (Phenylamine, Aminobenzene)
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl Butyl Phthalate
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Parent
Result
<0.0642
<0.0588
<0.0573
<0.0566
<0.0667
<0.0700
<0.0461
<0.0660
<0.0584
<0.0472
<0.0660
<0.0649
<0.0555
<0.0508
<0.0486
<0.0457
<0.107
<0.0501
<0.0631
<0.0617
<0.0519
<0.0602
<0.0689
<0.0551
<0.0446
<0.0508
<0.0617
<0.0399
<0.0537
<0.0588
<0.0533
<0.0591
<0.0599
<0.0624
<0.0544
<0.0435
<0.0515
<0.0490
<0.0588
<0.0482
<0.0704
<0.0464
<0.0584
<0.0548
<0.0667
<0.0602
<0.0472
<0.0443
<0.0606
<0.0403
<0.0624
<0.0562
Spike
Amount
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
Hasty Mart #23
Matrix: Soil
MS Sample Jd: 507823-001 S
MS
Result
0.650
0.697
0.696
0.681
0.716
0.685
0.700
0.728
0.839
0.765
0.696
0.681
0.699
0.696
0.822
0.669
0.768
0.803
0.720
0.723
0.759
0.855
0.724
0.814
1.05
0.703
0.742
1.15
0.896
0.923
0.942
0.906
0.843
0.875
1.05
0.714
0.731
0.846
1.11
0.903
0.862
0.694
0.830
0.768
0.927
1.01
0.871
0.769
0.804
0.618
0.760
0.744
MS
%Rec
36
39
38
38
40
38
39
40
46
42
38
38
39
38
45
37
42
44
40
40
42
47
40
45
58
39
41
64
50
51
52
50
47
48
58
39
40
47
61
50
48
38
46
42
51
56
48
42
44
34
42
41
MSD
Result
0.436
0.455
0.458
0.440
0.688
0.598
0.517
0.542
0.877
0.732
0.519
0.456
0.489
0.509
0.798
0.432
0.561
0.839
0.827
0.758
0.682
0.636
0.673
0.912
1.18
0.594.
0.615
0.792
0.962
1.03
1.02
0.934
0.890
1.04
1.13
0.488
0.464
0.585
1.19
0.985
0.898
0.610
0.870
0.731
1.00
1.10
0.967
0.713
0.844
0.415
0.567
0.495
Page 59 of96
MSD Limits
%Rcc
24 31-100
25 27-97
25 25-96
24 27-94
38 33-110
33 35-111
28 33-103
30 28-109
48 35-122
40 35-119
29 32-108
25 25-102
27 22-104
28 27-104
44 20-128
24 30-104
31 30-111
46 22-117
45 3-130
42 38-115
37 26-116
35 4-104
37 34-114
50 28-117
65 12-137
33 31-lll
34 36-122
44 20-120
53 33-118
57 31-136
56 44-105
51 29-120
49 35-126
57 37-123
62 35-122
27 31-106
25 24-103
32 32-103
65 32-129
54 34-122
49 36-124
34 31-107
48 34-118
40 36-115
55 37-121
60 35-126
53 15-135
39 31-117
46 38-116
23 30-98
31 12-194
27 27-98
Prep Method: SW3545
Date Prep: 05.19.15
MSD Sample Id: 507823-001 SD
%RPD RPD
Limit
39 30
42 30
41 30
43 30
4 30
14 30
30 30
29 30
4 30
4 30
29 30
40 30
35 30
31 30
3 30
43 30
31 30
4 30
14 30
5 30
11 30
29 30
7 30
11 30
12 30
17 30
19 30
37 30
7 30
11 30
8 30
3 30
5 30
17 30
7 30
38 30
45 30
36 30
7 30
9 30
4 30
13 30
5 30
5 30
8 30
9 30
10 30
8 30
5 30
39 30
29 30
40 30
Final1.000
Units
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
Analysis
Date
05.21.15 04:07
05.2l.l5 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.2Ll5 04:07
05.2l.l5 04:07
05.2I.l5 04:07
05.2l.l5 04:07
05.2l.l5 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.2l.l5 04:07
05.2l.l5 04:07
05.21.15 04:07
05.21.15 04:07
05.2l.l5 04:07
05.21.15 04:07
05.21J5 04:07
05.21J5 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.l5 04:07
05.2l.15 04:07
05.2l.l5 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.2l.15 04:07
05.21.1504:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
Flag
XF
XF
F
XF
X
X
X
F
F
F
XF
F
X
F
XF
F
F
XF
F
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: SVOCs by SW-846 8270D
Seq Number: 968618
Parent Sample Id: 507823-001
Parameter
lndeno( l ,2 ,3~,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
N~Nitrosodi-n-Propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate
2-Fluorophenol
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terpheny1-Dl4
Phenol-d5
Parent Spike
Result Amount
<0.0660
<0.0374
<0.0580
<0.0646
<0.0519
<0.0762
<0.0657
<0.0602
<0.0508
<0.0617
<0.0689
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
1.81
Analytical Method: MADEP VPH
Seq Number: 968507
MB Sample Id: 692794-1-BLK
Parameter
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-C I 0 Aromatics
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
I\IB Spike
Result Amount
<0.000150
<0.000150
<0.0000500
~m
%Rec
120
107
0.150
0.150
0.0500
MB
Flag
Hasty Mart #23
Matrix: Soil
MS Sample Id: 507823-001 S
Prep Method: SW3545
Date Prep: 05.19.15
MSD Sample Id: 507823·001 SD
MS MS
Result %Rec
1\ISD l\ISD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date Flag
0.848
0.858
0.682
0.740
0.804
1.08
0.795
0.879
0.639
0.962
0.752
MS
%Rec
40
40
37
50
49
41
47
47
38
41
44
60
44
49
35
53
42
MS
Flag
0.897
0.666
0.466
0.489
0.587
1.11
0.909
0.942
0.525
1.08
0.520
Matrix: Solid
49 30-129
37 11-139
26 31-100
27 27-106
32 26-122
61 38-127
50 14-128
52 34-115
29 23-104
59 33-112
29 1-106
MSD
%Rec
23
23
25
47
47
25
MSD
Flag
"
LCS Sample Id: 692794-1-BKS
6
25
38
41
31
3
13
7
20
12
36
30
30
30
30
30
30
30
30
30
30
30
Limits
25-121
23-120
30·115
19-122
18-137
15-110
mglkg 05.2U5 04:07
mglkg 05.2Ll5 04:07
rug/kg 05.21.15 04:07 XF
mglkg 05.2LI5 04:07 F
mglkg 05.21.15 04:07 F
mglkg 05.21.15 04:07
mglkg 05.21.15 04:07
mglkg 05.2U5 04:07
mgfkg 05.2l.l5 04:07
mglkg 05.21.15 04:07
mg/kg 05.21.15 04:07 F
Units
%
%
%
%
%
%
Analysis
Date
05.21.15 04:07
05.2l.I5 04:07
05.21.15 04:07
05.21.15 04:07
05.21.15 04:07
05.2l.l5 04:07
Prep Method: SW5030B
Date Prep: 05.19.15
LCSD Sample Id: 692794-1-BSD
LCS LCS
Result %Rec
LCSD LCSD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date Flag
0.134
0.155
0.0501
LCS
%Rec
109
98
89
103
100
0.141
0.168
0.0524
LCS
Flag
Page 60 of 96
94 70-130
112 70-130
105 70-130
LCSD LCSD
%Rec Flag
117
104
5
8
4
25
25
25
Limits
70-130
70-130
Final 1.000
rug/kg 05.19.15 11:23
mg!kg 05.19.15 11:23
mgfkg 05.19.15 11:23
Units
%
%
Analysis
Date
05.19.15 11:23
05.19.15 11:23
Analytical Method: MADEP VPH
Seq Number:
MB Sample Id:
Parameter
C5·C8 Aliphatics
C9-CIO Aromatics
C9-C12 Aliphatics
Surrogate
2,5-Dibromotoluene
968516
692797-1-BLK
MB
Result
<0.0150
<0.00500
<0.0150
~m
%Rec
120
2,5-Dibromotoluene (PID) 107
Analyticall\Iethod: MADEPVPH
Seq Number: 968516
Parent Sample Id: 507823-005
Parameter Parent
Result
C5-C8 Aliphatics <0.0150
C9-C10 Aromatics <0.00500
C9-C12 Aliphatics <0.0150
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Analytical Method: MADEPVPH
Seq Number: 968507
Parent Sample Id: 507823-002
Parameter Parent
Result
C5-C8 Aliphatics <0.00557
C9-Cl2 Aliphatics <0.00557
C9-C10 Aromatics 0.746
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
QCSummary 507823
Terraquest Environmental Consultants, P .C.
Hasty Mart #23
Matrix: \Vater
LCS Sample Id: 692797-1-BKS
Spike LCS LCS LCSD LCSD
Amount Result %Rec Result %Rec
!50 134 89 141 94
50.0 50.1 100 52.4 105
!50 155 103 168 112
~m LCS LCS LCSD
Flag %Rcc Flag %Rec
109 117
98 104
Matrix: Ground Water
MS Sample Id: 507823-005 s
Spike MS MS MSD MSD
Amount Result %Rec Result %Rec
!50 122 81 127 85
50.0 44.4 89 48.7 97
!50 113 75 134 89
MS MS MSD
%Rec Flag %Rec
92 93
81 80
Matrix: Soil
MS Sample Id: 507823-002 s
Spike MS MS
Amount Result %Rec
5.57 3.98 71
5.57 5.50 99
1.86 1.97 66
MS MS
%Rec Flag
90
78
Page 61 of 96
Limits
70-130
70-130
70-130
Prep Method: SW5030B
Date Prep: 05.19.15
LCSD Sample Id: 692797-l-BSD
%RPD RPD Unlts Analysis
Limit Date
5 25 ug!L 05.19.15 11:23
4 25 ug!L 05.19.15 11:23
8 25 ug!L 05.19.15 l1:23
LCSD Limits Units Analysis
Flag Date
70-130 % 05.19.15 11:23
70-130 % 05.19.15 ll:23
Prep Method: SW5030B
Date Prep: 05.19.15
MSD Sample Id: 507823-005 SD
Limits %RPD RPD Units Analysis
Limit Date
70-130 4 25 ug!L 05.19.15 23:58
70-130 9 25 ug!L 05.19.15 23:58
70-130 17 25 ug/L 05.19.15 23:58
.1\ISD Limits Units Analysis
Flag Date
70-130 % 05.19.15 23:58
70-130 % 05.19.15 23:58
Prep Method: SW5030B
Date Prep: 05.19.15
Limits Units Analysis
Date
70-130 mglkg 05.19.15 22:28
70-130 mglkg 05.19.15 22:28
70-130 mglkg 05.19.15 22:28
Limits Units Analysis
Date
70-130 % 05.19.15 22:28
70-130 % 05.19.1522:28
Final1.000
Flag
Flag
Flag
X
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: VOCs by GCIMS by SM6200B
Seq Number: 968479
MB Sample Id: 692778-1-BLK
Parameter
1,1,1,2~Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
l, 1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzenc
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-lsopropyltoluene
4-Methyl-2-pentanone (MIDK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis·l ,2·Dichloroethene
cis·l ,3 -Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylhenzene
sec-Butylbenzene
1\.IB Spike
Result Amount
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
25,0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Hasty Mart #23
Matrix:
LCS Sample ld:
Water
692778-l-BKS
Prep Method: SM6200B _PREP
Date Prep: 05.19.15
LCSD Sample Id: 692778-1-BSD
LCS LCS
Result %Rec
LCSD LCSD Limits %RPD RPD
Result %Rcc Limit
Units Analysis
Date FJag
25.6
22.9
29.2
28.2
21.6
21.5
23.4
27.5
30.0
27.5
28.7
30.2
26.8
252
25.5
28.6
27.7
28.8
28,0
22.3
51.3
28.3
62.4
25.0
28.4
52.0
47.1
23.8
29.1
25.4
25,8
33.4
25.0
24.0
26.5
29.2
20.8
23.6
23.4
23.0
28.8
20.8
886
25.8
21.9
28.0
42.8
26.6
28.7
28.6
28.9
28.2
102
92
117
113
86
86
94
110
120
110
115
121
107
101
102
114
Ill
115
112
89
103
113
125
100
114
104
94
95
116
102
103
134
100
96
106
117
83
94
94
92
115
83
89
103
88
112
86
106
115
114
116
113
Page 62 of96
28.6
25.4
29.0
27.7
22.6
23.6
24.7
29.1
28.8
29.2
29.3
28.5
28.3
24.9
25.0
29.5
28.7
28.0
28.8
23.6
47.1
28.8
56.9
25.5
29.7
50.2
44.4
24.3
27.8
26.3
25.4
31.3
24.3
25.6
26.9
29.2
20.2
24.5
22.9
23.9
26.5
21.7
938
27.5
22.5
28.3
43.5
28.0
27.2
30.5
29.2
29.6
!14 75-127
!02 62-128
116 77-129
Ill 86-120
90 82-114
94 73-123
99 83-125
116 57-127
115 79-118
117 59-125
117 84-118
114 83-126
113 83-128
!00 56-133
!00 85-121
118 86-118
115 90-126
112 85-121
115 88-121
94 76-126
94 66-133
!15 80-128
114 70-130
!02 82-130
119 80-128
!00 74-129
89 51-143
97 81-123
Ill 84-114
105 89-127
102 79-129
125 73-140
97 53-143
!02 66-136
!08 88-118
117 73-139
81 70-123
98 72-118
92 65-125
96 85-125
!06 92-126
87 48-143
94 61-133
110 87-123
90 77-125
113 82-115
87 53-149
!12 75-119
!09 52-116
!22 83-130
117 84-122
!18 86-120
II
10
2
5
9
5
6
4
6
2
6
5
2
3
4
3
3
6
9
2
9
2
4
4
6
2
5
3
2
6
3
6
0
3
4
2
4
8
4
6
6
3
I
2
5
5
6
5
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Final 1.000
ug/L 05.19.15 ll:07
ug/L 05.19.15 11:07
ug/L 05.19.15 ll:07
ug!L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug!L 05.19.1511:07 H
ug!L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.1511:07
ug/L 05.19.15 11:07
ug!L 05.19.15 ll:07
ug!L 05.19.15 11:07
ug!L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug!L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.1511:07
llg/L 05.19.15 11:07
ug!L 05.19.15 11:07
ug/L 05.19.15 ll:07
ug!L 05.19.15 11:07
ug/L 05.19.15 II:07
ug/L 05.19.15 11:07 H
ug/L 05.19.15 11:07
ug/L 05.19.15ll:07
ug/L 05.19.15ll:07
ug!L 05.19.15 11:07
ug!L 05.19.15 ll:07
ug!L 05.19.15 11:07
ug!L 05.19.15 11:07
ug!L 05.19.15 11:07
ug!L 05.19.15 11:07
ug/L 05.19.15 11:07
ug!L 05.19.1511:07
ug!L 05.19.15 11:07
ug!L 05.19.15 11:07
ug!L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug!L 05.19.1511:07
ug/L 05.19.1511:07
ug/L 05.19.15 11:07
ug/L 05.19.15 11:07
ug!L 05.19.1511:07
ug!L 05.19.15 11:07
QCSummary 507823 Jif "" -.!:.=. .......
Terraquest Environmental Consultants, P.C.
Analytical Method: VOCs by GCiTIIS by SM6200B
Seq Number: 968479
MB Sample Jd: 692778-1-BLK
Parameter
Styrene
tert-Butylbenzene
Tetrachloroethene (PCB)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
a-Xylene
Surrogate
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
.MB Spike
Result Amount
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
MB
%Rec
94
105
100
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
~m
Flag
Analytical Method:
Seq Number:
VOCs by GC/MS by SM6200B
968541
MB Sample Jd:
Parameter
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylene-s
a-Xylene
Surrogate
1,2-Dichloroethane-04
4-Bromofluorobenzene
Toluene-DS
692812-1-BLK
MB Spike
Result Amount
<0.103 25.0
<0.0870 25.0
<0.119 25.0
<0.0920 25.0
<0.0940 25.0
<0.0650 25.0
<0.0570 25.0
<0.176 50.0
<0.122 25.0
I>m
%Rec
102
110
95
MB
Flag
Hasty Mart #23
Matrix:
LCS Sample Id:
LCS LCS
Result %Rec
27.6
27.8
26.0
26.0
20.7
30.2
23.7
24.3
25.7
23.5
52.7
25.7
LCS
%Rec
101
108
104
110
111
104
104
83
121
95
97
103
94
105
103
\Vater
692778-1-BKS
Prep Method: SM6200B _PREP
Date Prep: 05.19.15
LCSD Sample Id: 692778-1-BSD
LCSD LCSD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
LCS
Flag
27.8
29.0
28.1
27.4
21.9
28.9
24.3
24.6
25.2
23.4
55.6
28.0
111 85-123
116 79-126
112 64-131
110 89-116
88 78-118
116 86-127
97 82-119
98 46-144
101 58-141
94 76-122
111 90-125
112 86-119
LCSD LCSD
%Rec Flag
99
101
107
4
8
5
6
4
3
2
0
5
9
20
20
20
20
20
20
20
20
20
20
20
20
Limits
65-126
86-111
83-116
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
%
%
%
Analysis
Date
05.19.15 11:07
05.19.15 11:07
05.19.15 11:07
Matrix: \Vater
Prep Method: SM6200B _PREP
DatePrep: 05.20.15
LCS Sample ld: 692812-1-BKS LCSD Sample Jd: 692812-1-BSD
LCS LCS
Result %Rec
28.3 113
28.3 113
25.6 102
27.5 110
28.4 114
28.1 112
28.2 113
55.3 111
28.2 113
LCS
%Rec
98
98
107
LCSD LCSD Limits %RPD RPD
Result %Rec Limit
LCS
Flag
27.4 110 84-118 3 20
27.4 110 86-118 3 20
22.8 91 81-123 12 20
25.8 103 87-123 6 20
28.3 113 52-116 0 20
27.2 109 84-122 3 20
25.9 104 89-116 9 20
52.4 105 90-125 5 20
25.9 104 86-119 9 20
LCSD LCSD
%Rec Flag
102
100
103
Limits
65-126
86-111
83-116
Page 63 of 96 Final1.000
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
%
%
%
Analysis
Date
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
Analysis
Date
05.20.15 08:36
05.20.15 08:36
05.20.15 08:36
Flag
Flag
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: VOCs by GC/MS by SM6200B
Seq Number: 9684 79
Parent Sample Jd: 507716-003
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1 , I ,2 ,2-Tetrachloroethane
1,1,2-Trich\oroethane
1,1-Dichloroethane
1, 1-Dichloroethene
1,1-Dichloropropene
I ,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
I ,3-Dichloropropane
I ,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone {MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1 ,2-Dichloroethene
cis-1 ,3 -Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parent Spike
Result Amount
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Hasty Mart #23
Matrix:
MS Sample Jd:
Ground Water
507716-003 s
Prep Method: SM6200B _PREP
Date Prep: 05.19.15
MSD Sample Jd: 507716-003 SD
MS MS MSD MSD Limits %RPD RPD Units Analysis
Result %Rec Result %Rec Limit
21.3
18.1
27.2
26.1
18.3
18.4
18.7
23.6
27.8
23.6
25.1
27.5
23.4
21.6
22.2
25.0
24.2
27.0
24.3
17.1
49.1
25.0
57.3
22.1
25.1
49.4
41.4
19.8
25.9
19.2
22.1
30.5
19.2
18.0
22.7
25.6
17.1
18.4
18.5
18.9
25.5
15.1
780
22.2
19.6
25.6
37.0
17.6
25.0
24.6
26.0
24.8
85
72
109
104
73
74
75
94
Ill
94
100
110
94
86
89
100
97
108
97
68
98
100
115
88
100
99
83
79
104
77
88
122
77
72
91
102
68
74
74
76
102
60
78
89
78
102
74
70
100
98
104
99
Page 64 of 96
21.1
16.2
26.4
25.1
15.6
17.0
17.5
24.2
26.7
24.0
24.5
26.6
23.1
20.7
21.2
24.3
23.8
26.6
23.7
15.6
42.0
24.2
55.7
21.3
24.3
46.9
37.7
18.6
24.9
15.9
21.0
29.4
19.1
16.6
22.1
25.1
16.9
16.0
17.6
15.8
24.5
14.1
816
21.5
16.8
24.6
34.0
16.1
26.1
24.0
24.9
24.1
84 76-126
65 63-128
!06 79-133
100 82-126
62 77-120
68 67-123
70 76-126
97 41-136
107 77-125
96 41-132
98 53-141
106 82-130
92 83-128
83 59-134
85 79-125
97 69-125
95 83-126
!06 85-124
95 82-121
62 56-122
84 66-136
97 73-129
!II 63-140
85 76-129
97 73-126
94 71-140
75 47-138
74 70-135
!00 76-120
64 83-132
84 66-132
118 63-143
76 60-134
66 59-139
88 83-120
!00 68-140
68 67-125
64 72-120
70 59-128
63 80-125
98 74-122
56 48-138
82 55-140
86 70-140
67 77-125
98 75-117
68 51-155
64 75-119
104 34-135
96 73-128
100 75-125
96 77-122
11
3
4
16
8
7
3
4
2
2
3
4
5
3
2
I
3
9
16
3
3
4
3
5
9
6
4
19
5
4
I
8
3
2
14
5
18
4
7
5
3
15
4
8
9
4
2
4
3
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Final1.000
ug!L
ug!L
ug!L
ug/L
ug/L
ug/L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug/L
ug!L
ug/L
ug/L
ug!L
ug/L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ug/L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
Date
05.19.1520:11
05.19.1520:11
05.19.15 20:11
05.19.l520:ll
05.19.15 20:11
05.19.15 20:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:ll
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.1520:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:ll
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20: II
05.19.15 20:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:ll
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.1520:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.1520:11
05.19.15 20:11
05.19.15 20;ll
05.19.15 20:11
05.19.15 20:11
Flag
X
X
X
X
X
X
X
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: VOCs by GC/MS by SM6200B
Seq Number: 968479
Parent Sample Id:
Parameter
Styrene
tert·Butylbenzene
Tetrachloroethene (PCE)
Toluene
507716-003
trans-1 ,2-Dichloroethene
trans-1 ,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
a-Xylene
Surrogate
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Parent Spike
Result Amount
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
Analytical Method: VOCs by GC/MS by SM6200B
Seq Number: 968541
Parent Sample Id:
Parameter
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
a-Xylene
Surrogate
l,2-Dichloroethane·D4
4-Bromofluorobenzene
Toluene-D8
508042-002
Parent Splke
Result Amount
7.09
0.880
!.76
7.25
8.49
1.59
28.3
20.1
!3.4
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
Hasty Mart #23
Matrix:
MS Sample Jd:
MS MS
Result %Rec
23.2
24.7
22.6
22.7
16.8
27.6
19.6
19.3
23.9
19.0
45.3
2!.5
MS
%Rec
93
106
104
93
99
90
91
67
IIO
78
77
96
76
91
86
Matrix:
MS Sample Jd:
MS MS
Result %Rec
34.0
25.0
19.8
28.7
35.9
25.7
53.7
66.9
34.8
MS
%Rec
93
104
106
108
96
72
86
110
96
102
94
86
Ground Water
507716-003 s
Prep Method:
Date Prep:
MSD Sample Id:
SM6200B _PREP
05.19.15
507716-003 SD
l\ISD 1\ISD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date
05.19.1520:11
05.19.1520:11
05.19.1520:11
05.19.1520:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20:11
05.19.15 20: II
05.19.15 20:11
05.19.15 20:11
MS
Flag
22.5
24.0
2!.7
2!.8
15.0
26.5
18.9
19.2
19.0
18.4
43.8
2!.2
90 54-!37
96 74-124
87 57-!30
87 81-125
60 69-122
106 73-129
76 73-124
77 49-!39
76 57-134
74 70-!2!
88 65-151
85 58-148
MSD
%Rec
93
!09
104
MSD
Flag
Ground \Vater
508042-002 s
3
3
4
4
ll
4
4
23
3
3
20
20
20
20
20
20
20
20
20
20
20
20
Limits
65-126
86-111
83-ll6
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
%
%
%
Analysis
Date
05.19.15 20:11
05.19.1520:11
05.19.1520:11
Prep Method: SM6200B_PREP
Date Prep: 05.20.!5
MSD Sample Jd: 508042-002 SD
MSD 1\lSD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
MS
Flag
3!.7
23.1
18.9
27.0
36.3
23.7
50.3
62.6
33.7
98 53-141
89 69-125
69 70-135
79 70-140
Ill 34-135
88 75-!25
88 81-125
85 65-151
81 58-148
MSD
%Rec
95
109
104
MSD
Flag
7
8
5
6
I
8
7
7
3
20
20
20
20
20
20
20
20
20
Limits
65-126
86-111
83-ll6
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
%
%
%
Analysis
Date
05.20.15 15:05
05.20.15 15:05
05.20.15 15:05
Page 65 of96 Final1.000
Flag
X
F
Flag
X
QC Summary 507823
Terraquest Environmental Consultants, P.C.
Analytlcall\Iethod:
Seq Number:
VOCs by SW-846 8260B
968428
MB Sample Id: 692740-1-BLK
Parameter
1, 1, 1-Trichloroethane
I, I ,2,2-Tetrachloroethane
l, I ,2-Trich\oroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1 ,2,3-Trichloropropane
1 ,2,4-Trichlorobenzene
l ,2,4-Trimethylbenzene
1,2-Dibrornoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dich\oropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chloroto1uene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIDK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1 ,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl Ether
lsopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
a-Xylene
1\IB Spike
Result Amount
<0.00075
<0.0012
<0.00067
<0.00080
<0.0012
<0.00054
<0.00057
<0.0016
<0.00087
<0.00072
<0.00086
<0.0013
<0.00060
<0.00093
<0.00081
<0.0010
<0.00069
<0.00068
<0.00060
<0.0023
<0.00071
<0.0011
<0.00055
<0.00080
<0.0032
<0.0069
<0.00051
<0.00085
<0.0010
<0.00050
<0.00096
<0.0025
<0.00074
<0.00058
<0.00099
<0.0024
<0.00074
<0.0023
<0.00066
<0.00054
<0.0012
<0.028
<0.00057
<0.0013
<0.00076
<0.00121
<0.00069
<0.0022
0.0041
<0.00088
<0.00078
<0.000716
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.10
0.050
0.10
0.050
0.050
0.10
0.10
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
2.0
0.050
0.050
0.050
0.100
0.10
0.050
0.050
0.050
0.050
0.0500
Hasty Mart #23
Matrix:
LCS Sample Id:
Solid
692740-1-BKS
Prep Method:
Date Prep:
LCSD Sample Id:
SW5035
05.17.15
692740-1-BSD
LCS LCS
Result %Rec
LCSD LCSD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date
05.17.15 11:31
05.17.15 11:31
05.l7J5 11:31
05.17.15 ll:3l
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.15 11:31
05.17.15 li:Jl
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17J5 11:31
05.17.15 ll:Jl
05.17.15 11:31
05.17.1511:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.1511:31
05.17.1511:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.1511:31
05.17.1511:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.1511:31
05.17.15 11:31
05,17.1511:31
05.17.1511:31
0.054
0.048
0.047
0.048
0.051
0.056
0.052
0.050
0.052
0.055
0.049
0.050
0.047
0.047
0.054
0.053
0.050
0.057
0.053
0.10
0.053
0.11
0.054
0.052
0.11
0.10
0.049
0.049
0.048
0.048
0.050
0.051
0.053
0.048
0.049
0.052
0.049
0.045
0.049
0.046
0.047
2.1
0.052
0.048
0.050
0.105
0.098
0.046
0.060
0.053
0.054
0.0535
108
96
94
96
102
112
104
100
104
110
98
100
94
94
108
106
100
114
106
100
106
110
108
104
110
100
98
98
96
96
100
102
106
96
98
104
98
90
98
92
94
105
104
96
100
105
98
92
120
106
108
107
0.053
0.047
0.049
0.048
0.051
0.055
0.053
0.049
0.054
0.056
0.049
0.050
0.048
0.047
0.055
0.053
0.049
0.058
0.051
0.094
0.053
0.11
0.054
0.052
0.10
0.098
0.049
0.049
0.047
0.049
0.049
0.048
0.052
0.049
0.049
0.048
0.050
0.044
0.049
0.047
0.043
1.9
0.052
0.048
0.050
0.105
0.094
0.048
0.058
0.053
0.054
0.0528
Page 66 of96
106 61-140
94 68-124
98 79-117
96 72-125
102 78-126
110 73-134
106 75-135
98 63-124
108 73-136
112 77-132
98 81-118
100 80-124
96 59-131
94 81-122
110 74-138
106 83-125
98 81-120
116 83-118
102 54-152
94 61-127
106 78-133
110 61-138
108 78-134
104 60-144
100 65-125
98 60-130
98 79-122
98 72-122
94 73-120
98 76-126
98 56-125
96 61-137
104 60-142
98 86-115
98 74-118
96 57-148
100 71-120
88 49-147
98 78-121
94 80-123
86 34-145
95 58-125
104 83-133
96 80-122
100 64-140
105 82-133
94 68-125
96 67-136
116 58-123
106 64-146
108 79-140
106 79-133
2
2
4
0
0
2
2
2
4
2
0
0
2
0
2
0
2
2
4
6
0
0
0
0
10
2
0
0
2
2
2
6
2
2
0
8
2
2
0
2
9
10
0
0
0
0
4
4
3
0
0
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Final1.000
rug/kg
mglkg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
rug/kg
mglkg
mglkg
rug/kg
rug/kg
rug/kg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
mglkg
mglkg
mglkg
rug/kg
Flag
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analyticall\Iethod:
Seq Number:
VOCs by SW-846 8260B
968428
MB Sample Id: 692740-1-BLK
Parameter
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1 ,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Surrogate
1,2-Dichloroethane-04
4-Bromofluorobenzene
Toluene-DS
~m
Result
<0.00066
<0.00074
<0.00083
<0.0010
<0.00059
<0.00078
<0.00067
<0.00071
<0.0035
<0.00072
<0.0020
MB
%Rec
77
110
113
Spike
Amount
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
MB
Flag
Analytical Method: VOCs by SW-846 8260B
Seq Number: 968439
MB Sample ld: 692749-1-BLK
Parameter
1,2.4-Trimethylbenzene
Ethylbenzene
m,p-Xylenes
a-Xylene
Surrogate
1,2-Dichloroethane-04
4-Bromofluorobenzene
Toluene-DS
.rtm Spike
Result Amount
<0.00072
<0.00057
<0.00121
<0.000716
~m
%Rec
116
100
107
0.050
0.050
0.100
0.0500
~m
Flag
Hasty Mart #23
Matrix: Solid
LCS Sample Id: 692740-1-BKS
LCS
Result
0,056
0,047
0.049
0.056
0.049
0.052
0.047
0.053
0.052
0.045
0.050
LCS
%Rec
112
94
98
112
98
104
94
106
104
90
100
LCSD
Result
0.055
0.049
0.050
0.055
0.049
0.049
0.048
0.052
0.049
0.044
0.049
LCSD Limits
%Rec
110 75-137
98 82-128
100 61-137
110 72-140
98 85-120
98 76-126
96 78-115
104 71-128
98 51-154
88 72-124
98 67-138
Prep Method: SW5035
Date Prep: 05.17.15
LCSD Sample Id: 692740-1-BSD
%RPD
2
4
2
2
0
6
2
2
6
2
2
RPD
Limit
20
20
20
20
20
20
20
20
20
20
20
Units
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
Analysis
Date
05.17.l5ll:31
05.17.1511:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 11:31
05.17.15 ll:31
05.17.15 11:31
05.17.15 ll:31
05.17.15 11;31
LCS
%Rec
LCS
Flag
LCSD LCSD Limits Units Analysis
Date %Rec Flag
93
97
103
Matrix: Solid
LCS Sample Id: 692749-1-BKS
91
99
103
50-150
57-158
50-150
%
%
%
05.17.1511:31
05.17.15 11:31
05.17.1511:31
Prep Method: SW5035
Date Prep: 05.18.15
LCSD Sample Id: 692749-1-BSD
LCS LCS
Result %Rec
LCSD LCSD Limits %RPD RPD
Result %Rcc Limit
Units Analysis
Date
05.18.15 14:25
05.18.15 14:25
05.18.15 14:25
05.18.15 14:25
0.047
0.049
0.0981
0.0458
LCS
%Rec
98
100
102
94
98
98
92
0.047
0.048
0.0982
0.0443
LCS
Flag
Page 67 of96
94 77-132
96 83-133
98 82-133
89 79-133
LCSD LCSD
%Rec Flag
96
99
102
0
2
0
3
20
20
20
20
Limits
50-150
57-158
50-150
Final1.000
mglkg
mglkg
mglkg
mglkg
Units
%
%
%
Analysis
Date
05.18.15 14:25
05.18.15 14:25
05.18.15 14:25
Flag
Flag
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical ~'lethod:
Seq Number:
VOCs by SW-846 8260B
968474
MB Sample Id: 692757-1-BLK
Parameter
l,l,l-Trichloroethane
1,1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
I ,2,3-Trichloropropane
1 ,2,4-Trichloro benzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3 ,5-Trimethylbenzene
1,3-Dichlorobenzene
1 ,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MffiK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1 ,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Isopropyl Ether
Isopropylbenzene
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
1\ID Spike
Result Amount
<0,00075
<0.0012
<0.00067
<0.00080
<0.0012
<0.00054
<0.00057
<0.0016
<0.00087
<0.00086
<0.0013
<0.00060
<0.00093
<0.00081
<0.0010
<0.00069
<0.00068
<0.00060
<0.0023
<0.00071
<0.0011
<0.00055
<0.00080
<0.0032
<0.0069
<0,00051
<0.00085
<0.0010
<0,00050
<0.00096
<0.0025
<0.00074
<0.00058
<0.00099
<0.0024
<0.00074
<0.0023
<0.00066
<0.00054
<0.0012
<0.028
<0.0013
<0.00076
<0.00069
<0.0022
<0.0013
<0.00088
<0.00078
<0.00066
<0.00074
<0.00083
<0.0010
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0,050
0.050
0.050
0.050
0.050
0.050
0.050
0.10
0.050
0.10
0.050
0.050
0.10
0.10
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0,050
0.050
0.050
0.050
0.050
0.050
2.0
0.050
0.050
0.10
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
Hasty Mart #23
Matrix: Solid
LCS Sample Id: 692757-1-BKS
Prep Method: SW5035A
Date Prep: 05.19.15
LCSD Sample Id: 692757-1-BSD
LCS LCS
Result %Rec
LCSD LCSD Limits %RPD RPD
Result %Rec Limit
Units Analysis
Date
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.1511:35
05.19.15 11:35
05.19.15 11:35
05.19.1511:35
05.19.1511:35
05.19.15 11;35
05.19.15 11:35
05.19.15 ll:35
05.19.15 11:35
05.19.15 11:35
05.19.15 ll:35
05.19.15 11:35
05.19.1511:35
05.19.15 11:35
05.19.15 11:35
05.19.15 l1:35
05.19.15 11:35
05.19.15 I 1:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.1511:35
05.19.15 11:35
05.19.1511:35
05.19.15 11:35
05.19.15 ll:35
05.19.1511:35
05.19.15 Il:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 ll:35
05.19.15 ll:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.15 11:35
05.19.1511:35
05.19.15 11:35
0.053
0.045
0.046
0.039
0.051
0.053
0.048
0.048
0.050
0.047
0.050
0.051
0.044
0.054
0.051
0.048
0,064
0.055
0.074
0.051
0.11
0.054
0.050
0.11
0,12
0.047
0.048
0.045
0.050
0.048
0.051
0.053
0.048
0.049
0.050
0.050
0.036
0.047
0.045
0.039
2.8
0.037
0.048
0.11
0.050
0.052
0.052
0.052
0.053
0.048
0.047
0.058
106
90
92
78
102
106
96
96
100
94
100
102
88
108
102
96
128
110
74
102
110
108
100
110
120
94
96
90
100
96
102
106
96
98
100
100
72
94
90
78
140
74
96
110
100
104
104
104
106
96
94
116
0.056
0.046
0.050
0.051
0.057
0.056
0.052
0.051
0.053
0.052
0.053
0.054
0.048
0.057
0.055
0.051
0.065
0.056
0.10
0.054
0.11
0.056
0.054
0.11
0.13
0.050
0.051
0.052
0.053
0.051
0.053
0.056
0.052
0.053
0.053
0.052
0.048
0.052
0.048
O.D38
2.4
0.049
0.051
0.11
0.059
0.056
0.055
0.055
0.056
0.052
0.050
0.062
Page 68 of96
112 61-140
92 68-124
100 79-117
102 72-125
114 78-126
112 73-134
104 75-135
102 63-124
106 73-136
104 81-118
106 80-124
108 59-131
96 81-122
114 74-138
110 83-125
102 81-120
130 83-118
112 54-152
100 61-127
108 78-133
110 61-138
112 78-134
108 60-144
110 65-125
130 60-130
100 79-122
102 72-122
104 73-120
106 76-126
102 56-125
106 61-137
112 60-142
104 86-115
106 74-118
106 57-148
104 71-120
96 49-147
104 78-121
96 80-123
76 34-145
120 58-125
98 80-122
102 64-140
110 68-125
118 67-136
112 58-123
110 64-146
110 79-140
112 75-137
104 82-128
100 61-137
124 72-140
6
2
8
27
11
6
8
6
6
10
6
6
9
5
8
6
2
2
30
6
0
4
8
0
8
6
6
14
6
6
4
6
8
8
6
4
29
10
6
3
15
28
6
0
t7
7
6
6
6
8
6
7
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Final1.000
mg/kg
mg/kg
mg/kg
mg/kg
mglkg
mglkg
mglkg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
mglkg
mg/kg
mg/kg
mglkg
mg/kg
mg/kg
mglkg
mglkg
mg/kg
mglkg
mglkg
mg/kg
mglkg
mglkg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mglkg
mglkg
mg/kg
mglkg
mglkg
mg/kg
mglkg
mg/kg
mg/kg
Flag
F
H
F
F
H
LF
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035A
Seq Number: 968474 Matrix: Solid Date Prep: 05.19.15
MB Sample ld: 692757-1-BLK LCS Sample Id: 692757-1-BKS LCSD Sample Id: 692757-1-BSD
Parameter ~m Spike LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
Toluene <0.00059 0.050 0.047 94 0.050 100 85-120 6 20 mglkg 05.19.15 11:35
trans-1 ,2-Dichloroethene <0.00078 0.050 0.053 106 0.055 110 76-126 4 20 mglkg 05.19.15 11:35
trans-1 ,3-Dichloropropene <0.00067 0.050 0.048 96 0.051 102 78-115 6 20 mg/kg 05.19.15 11:35
Trichloroethene <0.00071 0.050 0.050 100 0.056 112 71-128 11 20 mglkg 05.19.15 11:35
Trichlorofluoromethane <0.0035 0.050 0.057 114 0.057 114 51-154 0 20 mglkg 05.19.15 11:35
Vinyl acetate <0.00072 0.050 0.044 88 0,047 94 72-124 7 20 mglkg 05.19.15 11:35
Vinyl chloride <0.0020 0.050 0.044 88 0.051 102 67-138 15 20 mg!kg 05.19.15 11:35
Surrogate ~m ~m LCS LCS LCSD LCSD Limits Units Analysis
%Rec Flag %Rec Flag %Rec Flag Date
1,2-Dichloroethane-D4 117 104 98 50-150 % 05.19.1511:35
4-Bromofluorobenzene 101 95 96 57-158 % 05.19.15 ll:35
Toluene-D8 100 100 100 50-150 % 05.19.15 11:35
Page 69 of96 Final1.000
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: VOCs by SW-846 8260B
Seq Number: 968428
Parent Sample Id: 507804-001
Parameter
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
l, 1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
I ,2-Dibromoethane (ED B)
1 ,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Ch\orotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl Ether
Isopropylbenzene
m,p-Xylene-s
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
a-Xylene
Parent
Result
<0.0012
<0.0018
<0.0010
<0.0012
<0.0018
<0.00083
<0.00088
<0.0025
<0.0013
<0.0011
<0.0013
<0.0020
<0.00091
<0.0014
<0.0012
<0.0015
<0.0011
<0.0010
<0.00092
<0.0035
<0.0011
<0.0017
<0.00085
<0.0012
<0.0050
<0.011
<0.00079
<0.0013
<0.0015
<0.00077
<0.0015
<0.0038
<0.0011
<0.00089
<0.0015
<0.0037
<0.0011
<0.0035
<0.0010
<0.00083
<0.0018
<0.043
<0.00087
<0.0019
<0.0012
<0.00185
<0.0011
<0.0033
0.0025
<0.0014
<0.0012
<0.00110
Spike
Amount
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.15
0.077
0.15
0.077
0.077
0.15
0.15
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
0.077
3.1
0.077
0.077
0.077
0.153
0.15
0.077
0.077
0.077
0.077
0.0766
Hasty Mart #23
Matrix: Soil
MS Sample Id: 507804-001 S
MS
Re.sult
0.068
0.067
0.073
0.067
0.063
0.061
0.062
O.o75
0.058
0.068
0.074
0.069
0.077
0.064
0.066
0.065
0.074
0.073
0.064
0.15
0.066
0.17
0.069
0.059
0.16
0.16
0.063
0.068
0.070
0.071
0.074
0.063
0.067
0.067
0.073
0.065
0.068
0.054
0.067
0.063
0.054
3.1
0.068
0.065
0.060
0.135
0.15
0.069
0.071
0.057
0.063
0.0702
MS
%Rec
88
87
95
87
82
79
81
97
75
88
96
90
100
83
86
84
96
95
83
100
86
ll3
90
77
107
107
82
88
91
92
96
82
87
87
95
84
88
70
87
82
70
100
88
84
78
88
100
90
89
74
82
92
MSD
Result
0.072
0.068
0.071
0.069
0.065
0.069
0.073
0.072
0.069
0.076
0.074
0.074
O.Q75
0.069
O.o75
0.073
0.074
0.081
0.066
0.14
0.073
0.16
O.o75
0.069
0.16
0.16
0.069
0.073
0.070
0.075
0.072
0.068
0.069
0.072
0.074
0.070
0.073
0.058
0.070
0.066
0.055
2.9
0.073
0.069
0.066
0.148
0.14
0.069
0.079
0.068
0.072
0.0748
Page 70 of 96
MSD Limits
%Rec
94 62-137
88 64-128
92 61-130
90 65-136
84 33-158
90 42-152
95 48-135
94 58-134
90 43-139
99 66-134
96 69-132
96 71-120
97 53-140
90 68-126
97 67-134
95 68-127
96 70-129
105 72-ll8
86 68-151
93 42-147
95 68-127
107 32-142
97 68-127
90 64-135
107 34-149
107 43-163
90 65-135
95 67-121
91 66-137
97 60-129
94 48-147
88 42-170
90 71-117
94 71-117
96 59-135
91 44-166
95 62-127
75 34-157
91 41-155
86 63-128
71 16-171
94 23-148
95 65-139
90 57-138
86 62-133
97 69-130
93 48-169
90 17-184
99 27-157
88 59-136
94 67-134
98 71-124
Prep Me1hod: SW5035
Date Prep: 05.17.15
MSD Sample Id: 507804-001 SD
%RPD
6
3
3
3
12
16
4
17
II
0
7
3
8
13
12
0
10
3
7
10
6
8
16
0
0
9
7
0
5
3
8
3
7
7
7
7
4
5
2
7
7
6
10
9
7
0
II
18
13
6
RPD
Limit
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Final 1.000
Units
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
mg!kg
Analysis
Date
05.17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
05.17.1516:58
05.17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
05.17.1516:58
05,17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
05.17.1516:58
05.17.1516:58
05.17.15 16:58
05.17.1516:58
05.17.1516:58
05.17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
05.17.1516:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.15 16:58
05.17.1516:58
Flag
QCSummary 507823 Jif ·~ ·-___ ....,.
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Seq Number: 968428 Matrix: Soil Date Prep: 05.17.15
Parent Sample Id: 507804-001 MS Sample Jd: 507804-001 s MSD Sample Id: 507804-001 SD
Parameter Parent Spike MS MS MSD MSD Limits %RPD RPD Units Analysis FJag Result Amount Result %Rec Result %Rec Limit Date
sec-Butylbenzene <0.0010 0.077 0.064 83 0.073 95 65-131 13 20 mglkg 05.17.15 16:58
Styrene <0.0011 0.077 0.068 88 0.071 92 50-143 4 20 mglkg 05.17.15 16:58
tert-Butylbenzene <0.0013 0.077 0.059 77 0.066 86 67-131 11 20 mglkg 05.17.15 16:58
Tetrachloroethene <0,0016 0.077 0,075 97 0.080 104 42-156 6 20 mglkg 05.17.15 16:58
Toluene <0.00090 0.077 0.063 82 0.069 90 13-188 9 20 mglkg 05.17.15 16:58
trans-1,2-Dichloroethene <0.0012 0.077 0.063 82 0.067 87 57-143 6 20 mglkg 05.17.15 16:58
trans-I ,3-Dichloropropene <0.0010 0.077 0.070 91 0.069 90 55-141 20 mglkg 05.17.1516:58
Trichloroethene <0.0011 0.077 0.069 90 0.071 92 39-150 3 20 mglkg 05.17.15 16:58
Trichlorofluoromethane <0,0054 0.077 0.068 88 0.066 86 34-179 3 20 mglkg 05.17.15 16:58
Vinyl acetate <0.0011 0.077 0.067 87 0.065 84 13-188 3 20 mglkg 05.17.15 16:58
Vinyl chloride <0.0031 0.077 0.059 77 0.065 84 40-161 10 20 mglkg 05.17.15 16:58
Surrogate MS MS 1\ISD MSD Limits Units Analysis
%Rec Flag %Rec Flag Date
1,2-Dichloroethane-D4 105 95 50-150 % 05.17.15 16:58
4-Bromofluorobenzene 96 99 57-158 % 05.17.15 16:58
Toluene-D8 99 102 50-150 % 05.17.15 16:58
Page 71 of96 Final1.000
QCSummary 507823
Terraquest Environmental Consultants, P.C.
Analytical Method: VOCs by SW-846 8260B
Seq Number: 968474
Parent Sample Id: 507650-007
Parameter
1,1, l ~Trichloroethane
1,1,2,2~Tetrachloroethane
1,1,2-Trichloroethane
1, 1-Dichloroethane
I, 1-Dichloroethene
I, 1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromoethane (EDB)
I ,2-Dichlorobenzene
1,2-Dichloroethane
1 ,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chlorofomt
Chloromethane
cis~ l ,2~Dichloroethene
cis~ 1 ,3 -Dichloropropene
Dichlorodifluoromethane
Ethanol
Isopropyl Ether
Jsopropylbenzene
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n~Butylbenzene
n~Propylbenzene
sec~Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Parent
Result
<0.00092
<0.0014
<0.00082
<0.00098
<0.0014
<0.00066
<0.00070
<0.0020
<0.0011
<0.0011
<0.0016
<0.00073
<0.0011
<0.00099
<0.0012
<0.00084
<0.00083
<0.00073
<0.0028
<0.00086
<0.0014
<0.00067
<0.00097
<0.0039
<0.0084
<0.00062
<0.0010
<0.0012
<0.00061
<0.0012
<0.0030
<0.00090
<0.00070
<0.0012
<0.0030
<0.00090
<0.0028
<0.00081
<0.00066
<0.0014
<0.034
<0.0015
<0.00092
<0.00084
0.031
<0.0016
<0.0011
<0.00095
<0.00080
<0.00090
<0.0010
<0.0013
Spike
Amount
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.12
0.061
0.12
0.061
0.061
0.12
0.12
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
2.4
0.061
0.061
0.12
0.061
0.061
0.061
0.061
0.061
0.061
0.061
0.061
Hasty Mart #23
Matrix: Soil
MS Sample Id: 507650-007 S
MS
Result
0.068
0.057
0.054
0.058
0.072
0.065
0.054
0.060
0.061
0.056
0.061
0.064
0.050
0.068
0.063
0.057
0.070
0.064
0.11
0.065
0.098
0.067
0.065
0.10
0.19
0.054
0.061
0.055
0.065
0.069
0.051
0.070
0.057
0.062
0.074
0.060
0.052
0.057
0.054
0.052
4.2
0.053
0.064
0.072
0.076
0.045
0.065
0.068
0.067
0.055
0.064
0.055
MS
%Rcc
Ill
93
89
95
118
107
89
98
100
92
100
105
82
Ill
!OJ
93
115
105
92
107
82
110
107
83
!58
89
100
90
107
11J
84
115
93
102
121
98
85
93
89
85
175
87
105
60
74
74
107
Ill
110
90
105
90
MSD
Result
0.052
0.061
0.058
0.051
0.055
0.060
0.054
0.060
0.057
0.060
0.057
0.054
0.054
0.062
0.058
0.060
0.065
0.046
0.12
0.059
0.13
0.060
0.058
0.13
0.12
0.052
0.056
0.054
0.054
0.060
0.039
0.051
0.054
0.057
0.050
0.054
0.045
0.056
0.054
O.oJ8
3.3
0.054
0.057
0.072
0.058
0.058
0.059
0.060
0.062
0.054
0.057
0.048
Page 72 of96
1\lSD Limits
%Rec
85 62-137
!00 64-128
95 61-130
84 65-136
90 33-158
98 42-152
89 48-135
98 58-134
93 43-139
98 69-132
93 71-120
89 53-140
89 68-126
102 67-134
95 68-127
98 70-129
!07 72-118
75 68-151
100 42-147
97 68-127
108 32-142
98 68-127
95 64-135
!08 34-149
!00 43-163
85 65-135
92 67-121
89 66-137
89 60-129
98 48-147
64 42-170
84 71-117
89 71-117
93 59-135
82 44-166
89 62-127
74 34-157
92 41-155
89 63-128
62 16-171
132 23-148
89 57-138
93 62-IJJ
60 48-169
44 17-184
95 27-157
97 59-136
98 67-134
102 65-131
89 50-143
93 67-131
79 42-156
Prep Method: SW5035A
DatePrep: 05.19.15
MSD Sample ld: 507650-007 SD
%RPD RPD
Limit
27 20
7 20
7 20
13 20
27 20
8 20
0 20
0 20
7 20
7 20
7 20
17 20
8 20
9 20
8 20
5 20
7 20
33 20
9 20
10 20
28 20
II 20
II 20
26 20
45 20
4 20
9 20
2 20
18 20
14 20
27 20
31 20
5 20
8 20
39 20
II 20
14 20
2 20
0 20
31 20
24 20
2 20
12 20
0 20
27 20
25 20
10 20
13 20
8 20
2 20
12 20
14 20
Final1.000
Units
m!l'kg
mg!kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
mglkg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
m!l'kg
Analysis
Date
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.1520:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.1520:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.1520:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.1520:23
05.19.1520:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20;23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.1520:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20;23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
05.19.1520:23
05.19.1520:23
05.19.15 20:23
05.19.15 20:23
05.19.15 20:23
Flag
F
F
F
F
F
F
F
F
F
F
XF
F
F
QCSummary 507823 Jit. .. ~ -~ -........ , .. ,,
Terraquest Environmental Consultants, P.C.
Hasty Mart #23
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035A
Seq Number: 968474 Matrix: Soil Date Prep: 05.19.15
Parent Sample Id: 507650-007 MS Sample Id: 507650-007 s MSD Sample Id: 507650-007 SD
Parameter Parent Spike MS MS MSD MSD Limits %RPD RPD Units Analysis Flag Result Amount Result %Rec Result %Rec Limit Date
Toluene <0.00072 0.061 0.055 90 0.051 84 13-188 8 20 mglkg 05.19.15 20:23
trans· 1 ,2·Dichloroethene <0.00095 0.061 0.071 116 0.054 89 57-143 27 20 mglkg 05.19.15 20:23 F
trans· 1 ,3-Dichloropropene <0.00082 0.061 0.055 90 0.052 85 55-141 6 20 mglkg 05.19.15 20:23
Trichloroethene <0.00086 0.061 0.062 102 0.055 90 39-150 12 20 mglkg 05.19.15 20:23
Trichlorofluoromethane <0.0043 0.061 O.OS5 139 0.052 85 34-179 48 20 mglkg 05.19.15 20:23 F
Vinyl acetate <0.00088 0.061 0.032 52 0.016 26 13-188 67 20 mglkg 05.19.15 20;23 F
Vinyl chloride <0.0024 0.061 0.065 107 0.054 89 40-161 18 20 mglkg 05.19.15 20;23
Surrogate MS MS MSD MSD Limits Units Analysis
%Rec Flag %Rec Flag Date
l,2-Dichloroethane-D4 110 93 50-150 % 05.19.15 20:23
4-Bromofluorobenzene 108 103 57-158 % 05.19.15 20:23
Toluene-D8 101 100 50-150 % 05.19.15 20:23
Page 73 of96 Final 1.000
Sample Id: 692613-1-BLK
Lab Sample ld: 692613-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Analytical Method: Select Metals by SW-846 6010C Prep Method: SW3050B
Tech: 4099
Analyst:
Seq Number:
Parameter
Chromium
4150
968286
Cas Number
7440-47-3
Date Prep: 05.15.15 13:32
Result RL
u 5.00
Page 74 of 96
MDL Units Analysis
Date
0.0600 rug/kg 05.17.15 18:06
Final1.000
Flag
u
Dil
Sample ld: 692626-1-BLK
Lab Sample Id: 692626-1-BLK
Analytical Method: l\IADEP EPH
Tech: IHG
Analyst: CLAR
Seq Number:
Parameter
C ll-C22 Aromatics
C9-Cl8 Aliphatics
Cl9-C36 Aliphatics
968290
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Prep Method: SW3545
Cas Number
Cl!C22
ALHYDRC9C1
ALHYDRC19C
Date Prep: 05.14.15 16:05
Result RL MDL
u 20.0
u 10.0
u 10.0
Page 75 of 96
Units Analysis Flag
Date
20.0 mglkg 05.17.15 05:29 u
10.0 mglkg 05.17.15 05:20 u
10.0 mglkg 05.17.15 05:20 u
Final 1.000
Jif. .. ~ ... ..= ......
DII
Sample Id: 692740-1-BLK
Lab Sample ld: 692740-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech: MWE
Analyst:
Seq Number:
Parameter
l, 1,1 ·Trichloroethane
ZHO
968428
1,1 ,2,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1 ,2,4-Trichlorobenzene
1 ,2 ,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chlorofonn
Chloromethane
cis·l ,2 ·Dichloroethene
cis· I ,3·Dich \oropropene
Cas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
DatePrep: 05.17.1510:14
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
RL
0.0010
0.0020
0.0010
0.0010
0.0020
0.0010
0.0010
0.0020
0.0010
0.0010
0.0010
0.0020
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.010
0.0010
0.010
0.0010
0.0010
0.010
0.010
0.0010
0.0010
0.0020
0.0010
0.0010
0.0050
0.0010
0.0010
0.0010
0.0050
0.0010
0.0050
0.0010
0.0010
Page 76 of96
~IDL
0.00075
0.0012
0.00067
0.00080
0.0012
0.00054
0.00057
0.0016
0.00087
0.00072
0.00086
0.0013
0.00060
0.00093
0.00081
0.00100
0.00069
0.00068
0.00060
0.0023
0.00071
0.0011
0.00055
0.00080
0.0032
0.0069
0.00051
0.00085
0.0010
0.00050
0.00096
0.0025
0.00074
0.00058
0.00099
0.0024
0.00074
0.0023
0.00066
0.00054
Units
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
rug/kg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
rug/kg
rug/kg
rug/kg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
Analysis
Date
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.1513:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.1513:12
05.17.15 13:12
05.17.15 13:12
05.17.1513:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.15 13:12
05.17.1513:12
05.17.15 13:12
05.17.1513:12
05.17.15 13:12
05.17.1513:12
05.17.1513:12
05.17.1513:12
Final1.000
.Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Sampleld: 692740-1-BLK Matrix: SOLID
Lab Sample Id: 692740-1-BLK
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech: MWE
Analyst: ZHO DatePrep: 05.17.1510:14
Seq Number: 968428
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Dichlorodifluoromethane 75-71-8 u 0.0020 0.0012 mglkg 05.17.1513:12 u
Ethanol 64-17-5 u 0.050 O.Q28 mglkg 05.17.15 13:12 u
Ethylbenzene 100-41-4 u 0.0010 0.00057 mglkg 05.17.1513:12 u
Isopropyl Ether 108-20-3 u 0.0020 0.0013 mglkg 05.17.15 13:12 u
Jsopropylbenzene 98-82-8 u 0.0010 0.00076 mglkg 05.17.1513:12 u
m,p-Xylenes 179601-23-1 u 0.00200 0.00121 mglkg 05.17.1513:12 u
Methyl tert-butyl ether 1634-04-4 u 0.0020 0.00069 mglkg 05.17.1513:12 u
Methylene chloride 75-09-2 u 0.0050 0.0022 mglkg 05.17.15 13:12 u
Naphthalene 91-20-3 0.0041 0.0020 0.0013 mglkg 05.17.15 13:12
n-Butylbenzene 104-51-8 u 0.0010 0.00088 mglkg 05.17.15 13:12 u
n-Propylbenzene 103-65-1 u 0.0010 0.00078 mglkg 05.17.1513:12 u
a-Xylene 95-47-6 u 0.00100 0.000716 mglkg 05.17.15 13:12 u
sec-Butylbenzene 135-98-8 u 0.0010 0.00066 mglkg 05.17.15 13:12 u
Styrene 100-42-5 u 0.0010 0.00074 mglkg 05.17.15 13:12 u
tert-Butylbenzene 98-06-6 u 0.0010 0.00083 mglkg 05.17.1513:12 u
Tetrachloroethene 127-18-4 u 0.0020 0.0010 mglkg 05.17.1513:12 u
Toluene 108-88-3 u 0.0010 0.00059 mglkg 05.17.1513:12 u
trans-1,2-Dichloroethene 156-60-5 u 0.0010 0.00078 mglkg 05.17.15 13:12 u
trans-1,3-Dichloropropene 1006HJ2-6 u 0.0010 0.00067 mglkg 05.17.1513:12 u
Trichloroethene 79-01-6 u 0.0010 0.00071 mglkg 05.17.1513:12 u
Trichlorofluoromethane 75-69-4 u 0.0050 0.0035 mglkg 05.17.1513:12 u
Vinyl acetate 108-05-4 u 0.0050 0.00072 mglkg 05.17.1513:12 u
Vinyl chloride 75-01-4 u 0.0050 0.0020 mglkg 05.17.1513:12 u
Page 77 of 96 Flnal1.000
Sampleld: 692749-1-BLK
Lab Sample ld: 692749-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035
Tech:
Analyst:
Seq Number:
Parameter
MWE
MWE
968439
1,2,4-Trimethylbenzene
Ethylbenzene
m,p-Xylenes
o-Xylene
Cas Number
95-63-6
100-41-4
179601-23-1
95-47-6
Date Prep: 05.18.15 13:26
Result RL MDL
u 0.0010 0.00072
u 0.0010 0,00057
u 0.00200 0.00121
u 0.00100 0.000716
Page 78 of 96
Units Analysis Flag
Date
mglkg 05.18.1516:31 u
mglkg 05.18.15 16:31 u
mglkg 05.18.15 16:31 u
mglkg 05.18.15 16:3t u
Final1.000
Dll
Sample Id: 692750-1-BLK
Lab Sample Id: 692750-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Analytical Method: Select Metals by SW-846 6010C Prep Method: SW3010A
Tech: 4099
Analyst:
Seq Number:
Parameter
Chromium
Lead
4150
968525
Cas Number
7440-47-3
7439-92-1
Date Prep: 05.19.15 13:10
Result RL MDL
0.000900 0.0500 0.000300
u 0.0100 0.00330
Page 79 of96
Units Analysis Flag
Date
mg/L 05.20.15 11:40 J
mg/L 05.20.15 11:40 u
Final 1.000
Dll
Sample Id: 692757-1-BLK
Lab Sample Id: 692757-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Matt #23
Matrix: SOLID
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035A
Tech: ZHO
Analyst: ZHO
Seq Number: 968474
Parameter
1, 1,1-Trichloroethane
1, 1 ,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
I ,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MJBK)
Acetone
Benzene
Bromobenzene
Bromochtoromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis~ 1 ,2-Dichloroethene
cis~ 1 ,3-Dichloropropene
Dichlorodifluoromethane
Cas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
106-934
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-434
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
75-71-8
Date Prep: 05.19.15 10:40
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
RL
0.0010
0.0020
0.0010
0.0010
0.0020
0.0010
0.0010
0.0020
0.0010
0.0010
0.0020
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.010
0.0010
0.010
0.0010
0.0010
0.010
0.010
0.0010
0.0010
0.0020
0.0010
0.0010
0.0050
0.0010
0.0010
0.0010
0.0050
0.0010
0.0050
0.0010
0.0010
0.0020
Page 80 of 96
MDL
0.00075
0.0012
0.00067
0.00080
0.0012
0.00054
0.00057
0.0016
0.00087
0.00086
0.0013
0.00060
0.00093
0.00081
0.00100
0.00069
0.00068
0.00060
0.0023
0.00071
0.0011
0.00055
0.00080
0.0032
0.0069
0.00051
0.00085
0.0010
0.00050
0.00096
0.0025
0.00074
0.00058
0.00099
0.0024
0.00074
0.0023
0.00066
0.00054
0.0012
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rug/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
rug/kg
rug/kg
rug/kg
rug/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rug/kg
rug/kg
rug/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Analysis
Date
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.1512:52
05.19.1512:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
05.19.15 12:52
F1na11.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Sample Id: 692757-1-BLK
Lab Sample ld: 692757-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Analytical Method: VOCs by SW-846 8260B Prep Method: SW5035A
Tech: ZHO
Analyst: ZHO DatePrep: 05.!9.1510:40
Seq Number: 968474
Parameter Cas Number Result RL MDL Units Analysis Flag
Date
Ethanol 64·17-5 u 0,050 0.028 mg!kg 05.19.15 12:52 u
Isopropyl Ether 108·20-3 u 0.0020 0.0013 mg!kg 05.19.15 12:52 u
Isopropylbenzene 98·82·8 u 0.0010 0.00076 mg!kg 05.19.15 12:52 u
Methyl tert-butyl ether 1634·044 u 0.0020 0.00069 mg!kg 05.19.15 12:52 u
Methylene chloride 75·09-2 u 0.0050 0.0022 mg!kg 05.19.15 12:52 u
Naphthalene 91-20-3 u 0.0020 0.0013 mg!kg 05.19.15 12:52 u
n-Butylbenzene 104-51-8 u 0.0010 0.00088 mg!kg 05.19.15 12:52 u
n-Propylbenzene 103·65-1 u 0.0010 0.00078 mg!kg 05.19.15 12:52 u
sec-Butylbenzene 135-98·8 u 0.0010 0.00066 mg!kg 05.19.15 12:52 u
Styrene 10042-5 u 0.0010 0.00074 mg!kg 05.19.15 12:52 u
tert-Butylbenzene 98·06·6 u 0.0010 0.00083 mg!kg 05.19.15 12:52 u
Tetrachloroethene 127·184 u 0.0020 0.0010 mg!kg 05.19.15 12:52 u
Toluene 108·88-3 u 0.0010 0.00059 mg!kg 05.19.15 12:52 u
trans-1, 2-Dich loroethene 156·60-5 u 0.0010 0.00078 mg!kg 05.19.1512:52 u
trans-! ,3 -Dichloropropene 10061-02-6 u 0.0010 0.00067 mg!kg 05.19.15 12:52 u
Trichloroethene 79·01-6 u 0.0010 0.00071 mg!kg 05.19.15 12:52 u
Trichlorofluoromethane 75·694 u 0.0050 0.0035 mg!kg 05.19.15 12:52 u
Vinyl acetate 108·054 u 0.0050 0.00072 mglkg 05.19.15 12:52 u
Vinyl chloride 75·014 u 0.0050 0.0020 mg!kg 05.19.15 12:52 u
Page 81 of96 Final 1.000
Dil
Sample Id: 692772-1-BLK
Lab Sample Id: 692772-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Analytical Method: SVOCs by SW-846 8270D Prep Method: SW3545
Tech: JHG
Analyst:
Seq Number:
Parameter
l,2,4~Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4.6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-methylphenol
2-Nitroaniline
CLAR
968618
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4~hloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (Phenylamine, Aminobenzene)
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Butyl Phthalate
bis(2-ch\oroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
Cas Number
120-82-1
95-50·1
541-73·1
10646·7
95-954
88·06·2
120·83-2
105·67-9
121-14-2
606-20-2
91-58-7
95-57·8
91-57-6
95·48-7
88·744
88·75-5
15831-10·4
91-94-1
99·09-2
534-52-1
101-55-3
59-50-7
106·47-8
7005-72-3
100·01-6
100·02-7
83·32-9
208·96·8
62-53-3
120-12-7
56-55·3
50·32-8
205·99-2
191-24-2
207-08-9
65·85-0
85·68·7
111-91-1
111-444
39638-32-9
Date Prep: 05.19.15 15:40
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
RL
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.667
0.333
0.667
1.67
0.333
0.333
0.333
0.167
0.333
0.333
0.333
0.667
0.667
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.333
0.667
0.333
0,333
0.167
0.333
Page 82 of 96
MDL
0.0590
0.0540
0.0527
0.0520
0.0613
0.0643
0.0423
0.0607
0.0537
0.0433
0.0607
0.0597
0.0510
0.0467
0.0447
0.0420
0.0987
0.0487
0.0460
0.0580
0.0567
0.0477
0.0553
0.0633
0.0507
0.0410
0,0467
0,0567
0.0367
0.0493
0.0540
0.0490
0.0543
0.0550
0.0573
0,0527
0.0500
0.0400
0.0473
0.0450
Units
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
mglkg
Analysis
Date
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.t5 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
05.20.15 22:43
Flnal1.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Sample Id: 692772-1-BLK Matrix: SOLID
Lab Sample Id: 692772-1-BLK
Analytical Method: SVOCs by SW-846 8270D Prep Method: SW3545
Tech: lliG
Analyst: CLAR Date Prep: 05.19.15 15:40
Seq Number: 968618
Parameter Cas Number Result RL MDL Units Analysis Flag Dll
Date
bis(2-ethylhexyl) phthalate 117-81-7 u 0.333 0.0540 mglkg 05.20.15 22:43 u
Chrysene 218-0t-9 u 0.333 0.0443 mglkg 05.20.15 22:43 u
Dibenz(a,h)Anthracene 53-70-3 u 0.333 0.0647 mglkg 05.20.15 22:43 u
Dibenzofuran 132-64'9 u 0.333 0.0427 mglkg 05.20.15 22:43 u
Diethyl Phthalate 84-66-2 u 0.333 0.0537 mglkg 05.20.15 22:43 u
Dimethyl Phthalate 131-tl-3 u 0.333 0.0503 mglkg 05.20.15 22:43 u
di-n-Butyl Phthalate 84-74-2 u 0.333 0.0613 mglkg 05.20.15 22:43 u
di-n-Octyl Phthalate 117-84-0 u 0.333 0.0553 mglkg 05.20.15 22:43 u
Fluoranthene 206-44-0 u 0.333 0.0433 mglkg 05.20.15 22:43 u
Fluorene 86-73-7 u 0.333 0.0407 mglkg 05.20.15 22:43 u
Hexachlorobenzene !18-74-1 u 0.333 0.0557 mglkg 05.20.15 22:43 u
Hexachlorobutadiene 87-68-3 u 0.333 0.0370 mglkg 05.20.15 22:43 u
Hexachlorocyclopentadiene 77-47-4 u 0.333 0.0573 mglkg 05.20.15 22:43 u
Hexachloroethane 67-72-1 u 0.333 0.0517 mglkg 05.20.15 22:43 u
Indeno(l,2,3-c,d)Pyrene 193-39-5 u 0.333 0.0607 mglkg 05.20.15 22:43 u
Isophorone 78-59-1 u 0.333 0.0343 mglkg 05.20.15 22:43 u
Naphthalene 91-20-3 u 0.333 0.0533 mglkg 05.20.15 22:43 u
Nitrobenzene 98-95-3 u 0.333 0.0593 mglkg 05.20.15 22:43 u
N-Nitrosodi-n-Propylamine 621-64-7 u 0.333 0.0477 mglkg 05.20.15 22:43 u
N-Nitrosodiphenylamine 86-30-6 u 0.333 0.0700 mglkg 05.20.15 22:43 u
Pentachlorophenol 87-86-5 u 0.667 0.0603 mglkg 05.20.15 22:43 u
Phenanthrene 85-01-8 u 0.333 0.0553 mglkg 05.20.15 22:43 u
Phenol 108-95-2 u 0.333 0.0467 mglkg 05.20.15 22:43 u
Pyrene 129-00-0 u 0.333 0.0567 mglkg 05.20.15 22:43 u
Pyridine I to-86-t u 0.333 0.0633 mglkg 05.20.15 22:43 u
Page 83 of96 Flnal1.000
Sample Id: 692778-1-BLK
Lab Sample ld: 692778-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Tech:
Analyst:
Seq Number:
Parameter
ZHO
MWE
968479
l, l, 1 ,2~Tetrachloroethane
l, 1,1 ~Trichloroethane
l, l ,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIDK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-l ,2-Dichloroethene
Cas Number
630-20-6
71-55·6
79-34-5
79·00·5
75-34-3
75-354
563-58-6
87-61-6
96-184
120-82-1
95-63-6
106-934
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
10646-7
594-20·7
78·93-3
9549-8
591-78-6
106-434
99-87-6
108-10-1
67·64-1
71-43·2
108-86-1
74-97-5
75-274
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
Date Prep: 05.19.15 09:49
Result RL
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Page 84 of96
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
OAOO
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
MDL
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analysis
Date
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53.
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.1512:53
05.19.1512:53
05.19.15 12:53
05.19.15 12:53
05.19.1512:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.1512:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
05.19.15 12:53
Fina\1.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Dil
Sample Id: 692778-1-BLK
Lab Sample Id: 692778-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B _PREP
Tech: ZHO
Analyst: MWE DatePrep: 05.19.1509:49
Seq Number: 968479
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
cis· I ,3 -Dichloropropene 10061-01-5 u 1.00 0.100 ug/L 05.19.15 12:53 u
Dichlorodifluoromethane 75-71-8 u 1.00 0.0670 ug/L 05.19.15 12:53 u
Ethanol 64-17-5 u 50.0 3.00 ug/L 05.19.15 12:53 u
Ethylbenzene 100-41-4 u 0.500 0.0920 ug/L 05.19.15 12:53 u
Isopropyl ether 108-20-3 u 0.500 0.0920 ug/L 05.19.15 12:53 u
lsopropylbenzene 98-82-8 u 0.500 0.0980 ug/L 05.19.15 12:53 u
Methyl tert-butyl ether (MTBE) 1634-04-4 u 0.500 0.169 ug/L 05.19.15 12:53 u
Methylene Chloride 75-09-2 u 0.500 0.190 ug/L 05.19.1512:53 u
Naphthalene 91-20-3 u 2.00 0.0940 ug/L 05.19.15 12:53 u
n-Butylbenzene 104-51-8 u 2.00 0.0600 ug/L 05.19.15 12:53 u
n-Propylbenzene 103-65-1 u 1.00 0.0650 ug/L 05.19.15 12:53 u
sec-Butylbenzene 135-98-8 u 0.500 0.0920 ug/L 05.19.15 12:53 u
Styrene 100-42-5 u 0.500 0.0740 ug/L 05.19.15 12:53 u
tert-Butylbenzene 98-06-6 u 0.500 0.0890 ug/L 05.19.15 12:53 u
Tetrachloroethene (PCE) 127-18-4 u 0.500 0.0540 ug/L 05.19.15 12:53 u
Toluene 108-88-3 u 0.500 0.0570 ug/L 05.19.15 12:53 u
trans-I ,2-Dichloroethene 156-60-5 u 0.500 0.188 ug/L 05.19.15 12:53 u
trans-1 ,3-Dichloropropene 10061-02-6 u 1.00 0.110 ug/L 05.19.15 12:53 u
Trichloroethene 79-01-6 u 0.500 0.139 ug/L 05.19.1512:53 u
Trichlorofluoromethane 75-69-4 u 0.500 0.0540 ug/L 05.19.15 12:53 u
Vinyl Acetate 108-05-4 u 1.00 0.720 ug/L 05.19.15 12:53 u
Vinyl Chloride 75-01-4 u 0.500 0.0810 ug/L 05.19.15 12:53 u
m,p-Xylenes 179601-23-1 u 1.00 0.176 ug/L 05.19.15 12:53 u
a-Xylene 95-47-6 u 0.500 0.122 ug/L 05.19.15 12:53 u
Page 85 of96 Final1.000
Sample ld: 692794-1-BLK
Lab Sample ld: 692794-1-BLK
Analytical Method: MADEP VPH
Tech:
Analyst:
Seq Number:
Parameter
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-C10 Aromatics
VBR
ZHO
968507
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Prep Method: SW5030B
Cas Number
'-LHYDRC5Cf
'-LHYDRC9Ct
HYDC9C10
Date Prep: 05.19.15 09:10
Result RL MDL
u 0.000150 0.000150
u 0.000150 0.000150
u 0.0000500 0.0000500
Page 86 of96
Units Analysis Flag
Date
mglkg 05.19.15 12:07 u
mglkg 05.19.15 12:07 u
mglkg 05.19.15 12:07 u
Final1.000
Dll
Sample ld: 692797-1-BLK
Lab Sample Id: 692797-1-BLK
Analytical Method: MADEP VPH
Tech: VBR
Analyst:
Seq Number:
Parameter
C5-C8 Aliphatics
C9-Cl0 Aromatics
C9-Cl2 Aliphatics
ZHO
968516
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Prep Method: SW5030B
Cas Number
ALHYDRCSC!
HYDC9CIO
ALHYDRC9CI
Date Prep: 05.19.15 09:10
Result RL MDL
u 0.0150 0.0150
u 0.00500 0.00500
u 0.0150 0.0150
Page 87 of 96
Units Analysis Flag
Date
ug!L 05.19.15 12:07 u
ug!L 05.19.15 12:07 u
ug!L 05.19.15 12:07 u
Flnal1.000
Dil
Sample Id: 692812-1-BLK
Lab Sample ld: 692812-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: \VATER
Analytical Method: VOCs by GCIMS by SM6200B Prep Method: SM6200B _PREP
Tech: ZHO
Analyst:
Seq Number:
Parameter
ZHO
968541
1 ,2,4~ Trimeth ylbenzene
I ,3,5~Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
n·Propylbenzene
Toluene
m,p·Xylenes
o·Xylene
Cas Number
95-63-6
108-67-8
71-43-2
100-41-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
Date Prep: 05.20.15 05:59
Result RL MDL Units Analysis Flag Dil
Date
u 0.500 0.103 ug!L 05.20.15 10:34 u
u 0.500 0.0870 ug!L 05.20.15 10:34 u
u 0.500 0.119 ug!L 05.20.15 10:34 u
u 0,500 0.0920 ug!L 05.20.15 10:34 u
u 2.00 0.0940 ug!L 05.20.15 10:34 u
u 1.00 0.0650 ug!L 05.20.15 10:34 u
u 0.500 0.0570 ug!L 05.20.15 10:34 u
u 1.00 0.176 ug!L 05.20.15 10:34 u
u 0.500 0.122 ug!L 05.20.15 10:34 u
Page 88 of96 Flnal1.000
Sampleld: 692819-1-BLK
Lab Sample Jd: 692819-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Analytical Method: EDB by EPA 504.1 Prep Method: E504.1P
Tech:
Analyst:
Seq Number:
Parameter
CLAR
CLAR
968570
1,2-Dibromoethane (EDB)
Cas Number
106-934
Date Prep: 05.20.15 10:35
Result RL
u 0.0500
Page 89 of96
MDL Units Analysis
Date
0.00600 ug!L 05.20.15 18:35
Flnal1.000
Flag
u
Dll
Sample Id: 692889-1-BLK
Lab Sample ld: 692889-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: SW3510C
Tech: BRO
Analyst:
Seq Number:
Parameter
CLAR
968853
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorohenzene
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene +
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthmcene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2·chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz(a,h)Anthracene
Cas Number
120-82-1
95-50-1
541-73-1
99-65-0
106·46-7
90·12-0
88-06-2
120·83·2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94·1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32·8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
111·44-4
39638-32-9
117-81-7
85-68-7
218-01-9
53·70·3
Date Prep: 05.19.15 14:00
Result RL MDL Units Analysis
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
6.50
u
u
u
Page 90 of96
10.0
10.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
1.43 ugiL
1.83 ugiL
2.11 ugiL
20.1 ugiL
1.61 ugiL
1.40 ugiL
1.64 ugiL
1.78 ugiL
1.63 ugiL
7.11 ugiL
1.29 ugiL
1.83 ugiL
1.19 ugiL
2.00 ugiL
1.95 ugiL
2.55 ugiL
3.88 ugiL
1.40 ugiL
2.12 ugiL
2.18 llg!L
3.09 ugiL
1.35 llg/L
2.41 ugiL
1.43 ugiL
1.48 ugiL
2.01 ug/L
1.90 ugiL
1.80 ugiL
1.97 ugiL
1.97 ugiL
2.71 ugiL
2.21 ugiL
1.23 ugiL
1.25 ugiL
1.78 ugiL
1.24 ugiL
1.20 ugiL
1.82 ugiL
2.09 ugiL
1.83 ugiL
Date
05.21.1518:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.1518:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
05.21.15 18:35
Flnal1.000
Flag
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
J
u
u
u
Dil
Sample ld: 692889-1-BLK
Lab Sample Id: 692889-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Analytical Method: SVOCs by EPA 625 + 10 TICs Prep Method: SW3510C
Tech: BRO
Analyst: CLAR Date Prep: 05.19.15 14:00
Seq Number: 968853
Parameter Cas Number Result RL MDL Units Analysis Flag
Date
Dibenzofuran 132-64-9 u 10.0 1.64 ug!L 05.21.15 18:35 u
Diethyl Phthalate 84-66-2 u 10.0 1.90 ug!L 05.21.15 18:35 u
Dimethyl Phthalate 131-ll-3 u 10.0 1.97 ug!L 05.21.15 18:35 u
di-n-Butyl Phthalate 84-74-2 u 10.0 2.08 ug!L 05.21.15 18:35 u
di-n-Octyl Phthalate 117-84-0 u 10.0 1.38 ug!L 05.21.15 18:35 u
Fluoranthene 206-44-0 u 10.0 1.81 ug!L 05.21.15 18:35 u
Fluorene 86-73-7 u 10.0 1.56 ug!L 05.21.15 18:35 u
Hexachlorobenzene ll8-74-1 u 10.0 2.21 ug!L 05.21.15 18:35 u
Hexachlorobutadiene 87-68-3 u 10.0 1.78 ug!L 05.21.15 18:35 u
Hexachlorocyclopentadiene 77-47-4 u 10.0 1.87 ug!L 05.21.15 18:35 u
Hexachloroethane 67-72-1 u 10.0 2.38 ug!L 05.21.1518:35 u
Indeno(1,2,3-c,d)Pyrene 193-39-5 u 10.0 1.87 ug!L 05.21.15 18:35 u
Isophorone 78-59-1 u 10.0 1.41 ug!L 05.21.15 18:35 u
Naphthalene 91-20-3 u 10.0 !.52 ug!L 05.21.15 18:35 u
Nitrobenzene 98-95-3 u 10.0 1.49 ug!L 05.21.15 18:35 u
n-Nitrosodi-n-Propylamine 621-64-7 u 10.0 1.36 ug/L 05.21.15 18:35 u
n-Nitrosodiphenylamine 86-30-6 u 10.0 2.50 ug/L 05.21.15 18:35 u
Pentachlorophenol 87-86-5 u 10.0 2.26 ug/L 05.21.1518:35 u
Phenanthrene 85-01-8 u 10.0 2.04 ug!L 05.21.15 18:35 u
Phenol 108-95-2 u 10.0 1.76 ug!L 05.21.15 18:35 u
Pyrene 129-00-0 u 10.0 2.40 ug!L 05.21.15 18:35 u
Page 91 of96 Fina11.000
Dil
Sample Id: 692958-1-BLK
Lab Sample ld: 692958-1-BLK
Analytical Method: MADEP EPH
Tech: BRO
Analyst:
Seq Number:
Parameter
Cll-C22 Aromatics
C9-Cl8 Aliphatics
Cl9-C36 Aliphatics
CLAR
968763
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: WATER
Prep Method: SW35IOC
Cas Number
CIIC22
'll.HYDRC9CI
'll.HYDRC19C
Date Prep: 05.19.1513:30
Result RL MDL
u 100 100
u 100 100
u 100 100
Page 92 of 96
Units Analysis Flag
Date
ug!L 05.21.15 18:51 u
ug!L 05.21.15 01:53 u
ug!L 05.21.15 01:53 u
Final 1.000
D!l
Sampleld: 968402-1-BLK
Lab Sample Id: 968402-1-BLK
Blank Summary 507823
Terraquest Environmental Consultants, P.C., Mebane, NC
Hasty Mart #23
Matrix: SOLID
Analytical Method: Chromium, Hexavalent by S\V 7196A Prep Method:
Tech: NSI
Analyst:
Seq Number:
Parameter
Chromium, Hexavalent
NSI
968402
Cas Number
18540-29-9
Date Prep:
Result RL
u 2.00
Page 93 of 96
1\IDL
OAOO
Units
mg/kg
Analysis
Date
05.17.1510:00
Final1.000
Flag Dil
u
X
xeNCO LABORATORIES
XENCO LABORATORIES
CHAIN OF CUSTODY
COCII tTL300600;-b Page---::+ of
6017 Fmancia! Drive, Norcross, GA 0071
Phone# [phone] Fax # (J70) 449-5477
Company Name: TerraquestEnvironmental Counsultams, P.C ~ye(s lllitialsn. emp: ~~ ;, a • J:/-' . . ' ; :; ji;:.'
lOOE.RuffinStreet Mebane,NC27302 CiiS!OdYseai(s):_· Y « L:ib#mx:oroerl# So~_$y~i:·
!Results Sent to: P.O.# (If reauired): IEmail address: ~Field CoDlJileiiiS I Lab Precautions:
FAX#: [phone] Contact Pbone #: 919-563-9091
Project Name (Site): Htbl-.. /tkti #23 Analysis Requested
Project Number (ID): ' Comalaer'l)pe:,
!Regulatory Program: .,_.,.,_.,.,..,_
~~;;~ Sampler(s): (printed)
-r.::. ,.,..In,., L££(!1../_ ~ .Qil!'~-~ J 'I.> ;, -~ ~ "1o .-e ~ ~~!""-~ :E-ll a " :> -<::) -~ ' Sample Collection "' "' ..o No. ot ~ ~ ~ ~ :of J1; ~ '::i' :-1
, SampleiD# Depth(Ft) Date/Time :!! ~ 5 ~ Containers ~ ~ ~ ~ ·~ ~ ~ ~ ~ ~ ~ u :J
I £
~ 1 llf\LtJ I fL.-7. 2 -;. .,/,., h~ 101:>4-S' IX t.. )( X X • x • X . a 2 IMWZ.. 1 2-3} -z-> r!YJ'? 5. I "II Xlx )( X
~ 3 lmw 1. (~-~I 2-., n'lq 5 I')( x • -1
4 ffiWl-1 C::z--:;l z-3 11.o' .s _ X _ i.. • x
slrr.w\ I I I l.1s:LUGwl lvl I LLx.lx.LLJXLx' IX
siM.wz.. 1 1 1 11s1--1_ lt..wl 1\(1 T l lxl xL_Llili
1 11'1\\,J :> l I I 153o lr.w I I X I I I I )(I I I I xI ·1 x I x
8 1 mw'-1 --11 T \t:;'o4 lt..J X )( -"X '-1 )( i 9
~ 10 r
0
1) Re · · -;;/_'f~ Date /'f"une I& 81· B)h-, '"~I'\...-.. 1 ~I Tune Delivered by: (Circle One) a /-~. LUJ r. .JIJ JJ '-"':::::::> ..... ,(..of-]) q. ,3·o FedExiUPS/Coarier/LabPickup/HaadiOther
!3) . "shedBy: Date/Time f4)ReceivedBy: Date/Tune TumaroundTime(businessdays)
iS) Relinquished By: Date /Tune 16) Received By: Date/Tune
TAT Starts when samples are ree'd by 2PM
_10 Days ;_5-7 Days; _3 Days
__2 Days; _1 Day; _Same Day
Matrix Guide: (W=Water) (DW = DriDkiDg Water) (GW = Grmmdwatel") ($W =Surface Water) (L =Liquid) (G = Oil) (S =Soil) (SD = SoDd) (SL =Sludge) (A= An-) (C =An-Cartridge)
Chemica!Pu:seatali<mCodes: l=HCL I 2=HNQ, I 3=H,S04 1 4=NaOH+NaAs0:t I S=NaOH+ZnAA: ti6=Na,J$,.0;, I 7=NaHSO,&MeOH/ 8=DIWater&MeOH
Container Type: VC=VJ81 (Oear); VA =Vial (Amber); GC=Giass (Oear); GA--Giass (Amber); P=Piastic: (HDPE); TB=Tedlar Bag; ES=EnCoreSampler; ZII=Zipl.., Bag; O=Other
r -
r·
·.·Tr-··
'1":~
~ g
~
I
§
'-l ~· j
~_r~=~ Paci<a~e. .
1 ~-US AtrJJIIf ..= 8047 7449 2250 -tr-
Dlt* -::-, -....
! ;._§ : .; .
,., .-~; ;, ; ~'>'lr'l ~::.-\ ;_;: ? ;·~~: r ,; ~:­. ,:: ·:<;.· t::; ~ _:; ~-;--.: ·;-:;·~-; ·:·~· i ...-_r.~.r,1~. ~ •,:..:•.,.._r,.~.~k·.r,~~'f 1 ,
""""' Wi sr.r ~ 1ffi I
___.... . ; (' Commlnv -fA( ( •_',,j,, /·'•1"" / ;"\-., q • "'.. :'\•\( \_~-'"-~·-· • -'" ,, . -, i [( ''+ i; ..... •. '
' '
FcdExFirsi:9Wmi;ltt o----.....,..,.....,..-..il~-....... ··~Dolinlyls......,
' oe-...... ~--::t:.... .
·· .•
' . . i
I
' ./ •• 1
r·~i··
. ~-t~~ ;
'• ·-~~=-l.'!,wmiobt I of.*.~.~"-;-_ ~ ........ ~...... ~~.MIIIIII:""·
""' r·;'-r f·/,_,, r ,.,., 1!/( ZIP J::Z?oZ s Pockagiog, ·--~-
.OK ... i
-i
z 'fourlldemo!SilllagRefatence
3 To -· .....
"""""" ......
·-. :~.
•:
:.:.,t.' ! •
WII-CtllmWI!O...,_oti!O.Zif'-......
...... Phone 7' ·' :_: .:.:.:~~. J::;.:o.:.;;)l,.'
-~~ 0 ----
uiii.._,;;.;;.--w .... -•• ~.,YM~....:
""' State ._,. ~· ZfP ·:_:;,.:(•?'] -:::-?;1:"'\ .,
: :; :i:'.':; ,::~.:::: :.:. .;.
L 8047 7449 .2:2®
•
0f«<Ex .......... o-.... D"""" ""'
6 Speciol-.gliiiiiDelfvertsu-Oplilms . 0 ........,~ -----···~ ' oQ.;a':!l•' --o"""-....,.,.._ ..... '",-:;-
DoeslfdnWptl'lfiatCOIIIIad&apowgo:adla
0~
0~~= ~·==--.
,---·--··· o...i.--aiiDabol. ···--·-···
·rtk. o"' · ov" ' 0""'"" Y"{"" ~-=:...... ~ ..,. ... , .. " --·--· ~=~:l=~:e-~--~::.~--0 """'-":""""'
-'~l!> ,_~.a.ac.t---__i.~OblliiAm:IJI. 0 ..... . Aca. Hq.,
l611!
l
I
' f; ~~~ l~.\ ~} ,,
i'''
) ·.·j~
,.. .. ~ ..... ·NIIII'I!JIIfUA.#S: • ··--· _____ ,...;.._ .... ~"·····--~·--.. --------··"""'-----~--~--->---·'-
'.
'
~
-.. •
;
XENCO Laboratories
Prelogin/Nonconformance Report-Sample Log-In
Client: Terraquest Environmental Consultants, F
Date/ Time Received: 05/14/2015 09:30:00 AM
Work Order#: 507823
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
Temperature Measuring device used : #61
#1 'Temperature of cooler(s)?
#2 'Shipping container in good condition?
#3 *Samples received on ice?
Sample Receipt Checklist
#4 'Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 'Custody Seals Signed and dated?
#7 'Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample Jabel(s)?
#12 Container Jabel(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples In proper container/ bottle?
#15 Samples properly preserved?
#16 Sample contalner(s) Intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (Jess than 1/4 inch bubble)?
#21 <2 for all samples preserved with HN03,HCL, H2S04? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAs02+NaOH, ZnAc+NaOH?
Comments
2.1
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
Yes
N/A
• Must be completed for after-hours delivery of samples prior to placing In the refrigerator
Analyst: Dl PH Device/lot#: 1016662-7
Checklist completed by: _V='-----n:===;;;:----
Dario Lagunas
Checklist reviewed by: ~ ~
Debbie Simmons
Page 96 of 96
Date: 05/14/2015
Date: 05/15/2015
Flnal1.000