5802_MadisonCountyMSWLF_GWMonitoring_DIN27132_20151021

Prepared for
Madison County, North Carolina
Project Number 2313.1301

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Fall 2015 Semiannual
Water Quality Monitoring Report
Madison County Closed
Solid Waste Facility
Madison County, North Carolina
Permit No. 58-02
February 16, 2016

Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page iii
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx

Table of Contents
1.0 Introduction .................................................................................................................... 1
2.0 Methods ......................................................................................................................... 2
2.1 Groundwater Purging and Sampling Methods ..............................................................2
2.1.1 Monitoring Well Sampling Methods ..................................................................2
2.1.2 Domestic Well Sampling Methods ....................................................................3
2.1.3 Surface Water Sampling Methods ....................................................................3
2.2 Sample Handling, Documentation, and Analysis...........................................................3
3.0 Findings .......................................................................................................................... 4
3.1 Analytical Results ..........................................................................................................4
3.1.1 Groundwater Monitoring Wells .........................................................................4
3.1.2 Surface Water ...................................................................................................5
4.0 Site Hydrogeology ........................................................................................................... 7
5.0 Summary ........................................................................................................................ 8
5.1 Future Activities .............................................................................................................8
6.0 References ..................................................................................................................... 9

Figures
1. Site Location Map
2. Sample Location Map
Tables
1. Summary of Laboratory Analyses Performed on Samples
2. Summary of Detected Constituents
3. Solid Waste Section Limits Exceedances Notification
4. Water Quality Standards Exceedances Notification
Appendices
A. Sampling Logs and Equipment Documentation and Instrument Calibration Data Sheets
B. Reports of Laboratory Analysis and Chain-of-Custody Documentation
C. Environmental Monitoring Reporting Form and Electronic Submittal of Environmental Data
Deliverable 5802Oct2015 (Electronic Submittal Only)
Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 1
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
1.0 Introduction
The Madison County Solid Waste Department maintains a closed municipal solid waste landfill (Closed
Landfill) located near the intersection of US Highway 25/70 Bypass and Long Branch Road (State Route
1582) in Madison County, North Carolina. The general site location is presented on Figure 1.
The Closed Landfill is permitted by the North Carolina Department of Environmental Quality (DEQ), formerly
the Department of Environment and Natural Resources, Division of Waste Management (DWM) under Permit
No. 58-02, which requires semiannual monitoring of groundwater and surface water quality.
This report is being submitted in accordance with monitoring requirements for closed landfills as stipulated
in the DEQ DWM Permit No. 58-02 issued to the Madison County Solid Waste Department and with
regulations codified in the DEQ Solid Waste Management (SWM) Rules Title 15A, Subchapter 13B, Section
.1600, of the North Carolina Administrative Code (15A NCAC 13B.1600).
This report describes the second groundwater and surface water quality monitoring event performed in
2015.
The water quality monitoring network for the Closed Landfill consists of four compliance monitoring wells
(MW-01 OLD, MW-02 OLD, MW-03 OLD and MW-04 OLD), a background groundwater quality sampling
location (BG SPRING OLD), a domestic well sample (DW-01 OLD), and two surface water sample locations
SW-01 OLD (upstream) and SW-02 OLD (downstream) located along Profitt Branch (see Figure 2).

Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 2
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
2.0 Methods
Groundwater, surface water, and domestic well samples were collected at the Closed Landfill by Altamont
Environmental, Inc. (Altamont) personnel on October 21 and 22, 2015 (see Appendices A and B).
Approximate sample locations are depicted on Figure 2.
The water sample collected from background sampling location BG SPRING OLD is treated as a groundwater
sample for the following reasons:
 Groundwater does not discharge to the ground surface at the sampling point.
 Construction of the sample point is similar to that of a temporary monitoring well or piezometer, and
is located upslope and upgradient of a springhead.
 The sampling point is constructed of a polyvinyl chloride (PVC) casing extending below ground
surface and has a screened interval from which groundwater is collected and recharges.
2.1 Groundwater Purging and Sampling Methods
2.1.1 Monitoring Well Sampling Methods
2.1.1.1 Monitoring Wells MW-01 OLD, MW-02 OLD, and BG SPRING OLD
Prior to collecting groundwater samples from the monitoring wells, the static water level and the total well
depth was measured and recorded in order to calculate the well’s volume. At each sample location, an initial
round of field parameters consisting of pH, specific conductivity (SC), dissolved oxygen (DO), oxidation-
reduction potential (ORP), turbidity, and temperature was measured and recorded. Water-level
measurements and field parameters are included on the sampling logs (Appendix A). These wells were then
purged using a new disposable polyethylene bailer. As each consecutive well volume was removed with the
bailer, an additional round of groundwater parameters was recorded. Prior to sample collection, each well
was purged until a minimum of three well volumes were removed and field parameters stabilized, or until the
well had been bailed dry.
2.1.1.2 Monitoring Wells MW-03 OLD and MW-04 OLD
Prior to collecting groundwater samples from these monitoring wells, the static water level was measured
and recorded for each well. The monitoring wells were purged and sampled using low-flow techniques in
accordance with the procedures described in Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures, United States Environmental Protection Agency (EPA), Groundwater Issues (Puls and Barcelona
1996). During purging, pH, specific conductivity (SC), dissolved oxygen (DO), oxidation-reduction potential
(ORP), turbidity, and temperature were measured and recorded approximately every 3 minutes. Well purging
continued until these parameters stabilized for three consecutive readings. The required stabilization
criteria are as follows:
 pH values within +/- 0.1 pH unit
 SC values within +/- 3 percent
 Temperature, DO, and turbidity values within +/- 10 percent
 ORP values within +/- 10 millivolts
Following stabilization of these parameters, a groundwater sample was collected by a technician wearing a
new pair of non-reactive nitrile gloves. Each sample was placed into laboratory-supplied sample containers.
Low-flow sampling logs are included in Appendix A.
Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 3
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
2.1.2 Domestic Well Sampling Methods
Altamont personnel sampled one domestic well owned by Mrs. J.V. Edwards (DW-01) on October 21, 2015.
The well was purged and sampled using the dedicated pump existing in the well. Groundwater was accessed
from a spigot in the basement of Mrs. J. V. Edwards’s house because a spigot does not exist at the wellhead.
Altamont personnel recorded one round of field parameters initially at the start of the purge, and then one
round for every 10 gallons purged from the well. Prior to sample collection, a total of 30 gallons of water
were purged from the well. Field parameters are presented in Appendix A. A groundwater sample was
collected from the domestic well using laboratory-supplied sample containers by a technician wearing a new
pair of disposable nitrile gloves. The sample was identified as DW-01.
2.1.3 Surface Water Sampling Methods
Surface water samples SW-01 OLD and SW-02 OLD were collected at designated locations along Profitt
Branch, which flows adjacent to the southern site boundary in an east-to-west direction (Figure 2). The
surface water sample collected at the SW-01 OLD location is assumed to represent surface water quality
upstream of the Closed Landfill, while the surface water sample collected at the SW-02 OLD location is
assumed to represent surface water quality downstream of the Closed Landfill. One set of field parameters,
including temperature, pH, SC, DO, ORP, and turbidity, was measured and recorded at each surface water
sampling location prior to sample collection (Appendix A). One surface water sample was collected from each
sampling location using laboratory-supplied sample containers by a technician wearing a new pair of
disposable nitrile gloves.
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to water quality sampling at the Closed Landfill
sampling locations are provided on the sampling logs provided in Appendix A. Following sample collection,
groundwater and surface water samples were immediately placed on ice in sample coolers for transport to
TestAmerica Laboratories, Inc. (TestAmerica), a laboratory certified in North Carolina and located in
Nashville, Tennessee. Altamont submitted the water samples collected from the monitoring wells and the
surface water sampling locations to TestAmerica for analysis as follows:
 Appendix I volatile organic compounds (VOCs) using US Environmental Protection Agency (EPA)
Method 8260B
 Eight Resource Conservation and Recovery Act (RCRA) metals using EPA Methods 6010C and 7470A
A summary of laboratory analyses performed on samples is provided on Table 1. A trip blank, provided by the
laboratory for each day of sampling and stored in the sample cooler, was analyzed for Appendix I VOCs.
Proper chain-of-custody documentation procedures were followed during collection and transport of each
sample. The laboratory analytical reports and chain-of-custody documentation are included in Appendix B.
Water-level measurements and field parameters are included in Appendix A and in the Electronic Data
Deliverable (EDD) in Appendix C.
Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 4
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
3.0 Findings
3.1 Analytical Results
The field parameter data and laboratory analytical results for the groundwater, surface water, drinking water,
and trip blank samples collected at the Closed Landfill are included in Appendices A and B, respectively, in
hard copy, and also in Appendix C in the EDD format specified by the DEQ Solid Waste Section (SWS) of the
DWM (most recently updated on May 5,2010).
As stipulated in the DWM documents referenced above, non-detections were reported at the method
detection limit (MDL), and all concentrations exceeding the applicable laboratory-specific MDL were reported
and appropriately qualified (Tables 2, 3, and 4). The MDL is the minimum concentration of a substance that
can be measured and reported by a laboratory with 99 percent confidence that the analyte concentration is
greater than zero. All detections were compared to analyte-specific Solid Waste Section Limits (SWSLs)
established by the SWS. The SWSL is the lowest concentration of an analyte in a sample that can be
quantitatively determined with suitable precision and accuracy. If the reported concentration is above the
laboratory MDL and below the method reporting limit (MRL), the analytical result is qualified by the
laboratory as estimated, and is flagged with a “J” qualifier (J-flag). The MRL is the minimum concentration of
a target analyte that can be accurately determined by the referenced method and is listed in the “Report
Limit” (RL) column in the TestAmerica report of laboratory analysis (Appendix B). If the reported
concentration is greater than the laboratory MRL and less than the SWSL, the analytical result is qualified by
Altamont as estimated, and is flagged with a “J” qualifier (italicized J-flag).
Detected concentrations of analytes in groundwater and drinking water samples were compared to current
groundwater quality standards specified in 15A NCAC 2L .0202, and are referred to as 2L standards.
Detected concentrations of analytes in groundwater with no established 2L standard were compared to the
interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with
15A NCAC 02L .0202 [c]), if established. Detections of analytes in surface water samples were compared to
15A NCAC 2B .0200 surface water quality standards (2B standard). Concentrations below respective SWSLs
are not discussed in the text of this report unless they exceed their contaminant-specific 2L or 2B water
quality standard, as defined below.
Table 2 presents the summary of laboratory analytical results for detected constituents only. Table 3
presents all analytical results that were above the applicable SWSLs. Table 4 presents only the
concentrations of analytes detected in groundwater and/or surface water samples that exceeded their
respective 2L standards (including IMACs, if applicable) or 2B standards (surface water).
In the EDD (Appendix C), the identification of a well (“WELL ID”) consists of the name of the well prefaced by
the un-hyphenated permit number for the facility. For example, monitoring well MW-01 OLD is identified on
the tables as 5802-MW01OLD. In the tables, figures, and text of this report, however, the identification of a
well consists only of the name of the well and does not include the permit number for the facility.
3.1.1 Groundwater Monitoring Wells
The following sections summarize the results of laboratory and field parameter analyses of groundwater
samples.
3.1.1.1 RCRA Metals
Four metals (barium, chromium, lead, and selenium) were detected in groundwater samples collected from
one or more monitoring wells (Table 2). Three of these metals (barium, chromium, and lead) were detected
at concentrations greater than their respective SWSLs (Tables 2 and 3). The concentrations of barium
exceeded its 2L standard in the samples collected from monitoring wells MW-03 OLD and MW-04 OLD
Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 5
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
(Tables 2, 3, and 4). Chromium concentration exceeded the 2L standard in the sample collected from
monitoring wells BG SPRING OLD (Tables 2, 3, and 4). Lead concentrations exceeded the 2L standard in
samples collected from monitoring wells MW-03 OLD and BG SPRING OLD (Tables 2, 3, and 4). As noted on
Table 4, the metals that were detected could be naturally occurring.
3.1.1.2 Appendix I VOCs
Thirteen VOCs were detected in groundwater samples collected from one or more monitoring wells. Two
VOCs (1,4-dichlorobenzene and chlorobenzene) were detected in excess of their respective SWSLs in one or
more monitoring wells (Tables 2 and 3). Neither of these VOCs were detected at a concentration in excess of
the 2L standard. Although vinyl chloride was not detected at a level in excess of its SWSL, it did exceed its
applicable 2L standard in the sample collected from monitoring well MW-01 OLD (Table 4). Acetone was
detected in several monitoring well samples and also in both trip blanks. Methylene chloride was detected in
both trip blanks associated with this sampling event, but not in any of the groundwater samples. Acetone
and methylene chloride appear to be laboratory contaminants.
3.1.1.3 Field Parameters
The pH readings obtained on October 22, 2015 from all monitoring wells, except for MW-02 OLD, were
outside the range for pH (6.5 to 8.5 Standard Units [SU]) specified in 15A NCAC 02L .0202(c) (Tables 2 and
4).
The remaining parameters measured in the field have no established groundwater quality standards and are
therefore not discussed in this section.
3.1.2 Surface Water
The following sections summarize the results of laboratory and field parameter analyses of surface water
samples SW-01 OLD and SW-02 OLD.
3.1.2.1 RCRA Metals
One metal, barium, was detected above the MRL in both SW-01 OLD and SW-02 OLD (Table 2). These
concentrations were well below the applicable 2B standard.
3.1.2.2 Appendix I VOCs
There were no VOCs detected in the surface water samples. Acetone and methylene chloride were detected
in both trip blanks associated with these sampling events, but were not detected in either surface water
sample.
3.1.2.3 Field Parameters
The pH readings collected from both surface water sample locations were within the pH 2B standard range
established at 6.0 to 9.0 SU.
The turbidity measured in surface water samples were within the 2B standard of 50 NTUs established for
class C waters (Table 2).
Dissolved oxygen in both surface water samples were within the 2B standard of greater than 5.0 mg/L
(Table 2).
The remaining parameters measured in the field have no established surface water quality standards and
are therefore not discussed in this section.
Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 6
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
3.1.3 Drinking Water
The following sections summarize the results of laboratory and field parameter analyses of the drinking
water sample DW-01 OLD.
3.1.3.1 RCRA Metals
Three metals, barium, chromium, and lead were detected in DW-01 OLD (Table 2). Of these detections, only
barium and lead were detected above the MRL, and only barium exceeded the SWSL threshold. All metals
concentrations were well below applicable 2L standards.
3.1.3.2 Appendix I VOCs
One VOC, tetrahydrofuran, was detected in DW-01 OLD (Table 2). This was detected below the MRL of 10
µg/L. There is no 2L standard for groundwater established for this constituent in North Carolina.
3.1.3.3 Field Parameters
With the exception of pH, field parameter readings of dissolved oxygen, and turbidity were within 2L
standards established for groundwater (Table 2).

Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 7
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
4.0 Site Hydrogeology
Groundwater levels were measured in the four monitoring wells (MW-01 OLD, MW-02 OLD, MW-03 OLD, and
MW-04 OLD) at the Closed Landfill at depths of approximately 6.56 feet below ground surface (ft-bgs), 8.11
ft-bgs, 47.23 ft-bgs, and 48.07 ft-bgs, respectively (Appendix A).
Monitoring wells MW-03 OLD and MW-04 OLD are installed in bedrock east of the Edwards/Madison County
property line near the top of a ridge within the landfill parcel. Monitoring wells MW-01 OLD and MW-02 OLD
are located in topographic drainages and are screened in the water table aquifer. Locations of monitoring
wells at the site are not situated such that groundwater flow direction may be accurately calculated based
on data from these wells. However, within the unconsolidated soil, the shallow groundwater is interpreted to
generally flow in directions that mimic topography, which is generally southward toward Profitt Branch. The
site is situated on the southwest side of a knoll with an elevation of approximately 2,100 feet above mean
sea level and drains to Profitt Branch.

Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 8
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
5.0 Summary
Altamont completed the second semiannual water quality monitoring event of 2015 at the Madison County
Closed Solid Waste Landfill on October 21 and 22, 2015.
Tables 2, 3, and 4 of this report, sampling logs in Appendix A, TestAmerica Reports of Laboratory Analysis in
Appendix B, and the EDD spreadsheet in Appendix C provide detailed analytical results and field data related
to groundwater and surface water quality at the Closed Landfill.
5.1 Future Activities
Altamont has discussed the exceedances of applicable water quality standards with Madison County.
Altamont will continue to measure field parameters and collect water quality samples from groundwater and
surface water monitoring points associated with the Closed Landfill. Water quality samples will be submitted
to a North Carolina certified laboratory for analysis for RCRA metals and Appendix I VOCs on a semiannual
basis. The next sampling event is scheduled for April 2016.

Fall 2015 Semiannual Water Quality Monitoring Report February 16, 2016
Permit No. 58-02, Madison County, North Carolina Page 9
P:\Madison County\Reports\2015\Fall\5802-Closed\FINAL 5802Oct2015 Semiannual Water Quality Report.docx
6.0 References
DENR DWM Solid Waste Section (SWS). October 27, 2006. New Guidelines for Electronic Submittal of
Environmental Monitoring Data.
DENR DWM SWS. February 23, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding
New Guidelines for Electronic Submittal of Environmental Data.
Puls, R.W., and M. J. Barcelona. 1996. Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures,
U.S. Environmental Protection Agency, OSWER, EPA/540/S-95/504.

FIGURES

Site Location











1





¦
@A@A
@A
@A
@A
@A @A
@A








Profitt Bra
n
c
h
U
n
n
a
m
e
d

T
r
i
b
u
t
a
r
y
Unnamed Trib
u
t
a
r
y






















2055
204
5
20
6
5
2035
2025
2
0
7
5
2015
2005 2085
1
9
9
5
20
9
5
21052115
1985
21252135
1975
21452155
2165
1965
2175 2185
1955
2195
2205 2215
2225
2245
2235
2255
1945
2265
1935
2275
1925
2285
2295
2
3
0
5
1915
2315
2105
218
5
20
6
5 2145
203
5
2
0
7
5
2055
2085
21
4
5
2175
203
5
211
5
2115
2
1
2
5
21
3
5
2035
2035
2045
2125210
5
2115
2055
20
3
5
1975
2175














¦















@A 

TABLES

Table 1
Summary of Laboratory Analyses Performed on Samples
Madison County Closed Municipal Solid Waste Landfill, Madison County, North Carolina
GROUNDWATER SAMPLES
VOCs RCRA Metals
EPA 8260B EPA 6010C
EPA 7470A
58-02 MW-01 OLD 10/22/2015 X X
58-02 MW-02 OLD 10/22/2015 X X
58-02 MW-03 OLD 10/22/2015 X X
58-02 MW-04 OLD 10/22/2015 X X
58-02 BG SPRING OLD 10/22/2015 X X
58-02 DW-01 OLD 10/21/2015 X X
SURFACE WATER SAMPLES
VOCs RCRA Metals
EPA 8260B EPA 6010C
EPA 7470A
58-02 SW-1 OLD 10/21/2015 X X
58-02 SW-2 OLD 10/21/2015 X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
58-02 TRIP BLANK (DW)10/21/2015 X
58-02 TRIP BLANK (CLOSED)10/22/2015 X
Notes:
1. VOCs = volatile organic compounds.
2. VOCs analyses includes Appendix I constituents per 40 CFR Part 258.
FACILITY
PERMIT SAMPLE ID COLLECT DATE
FACILITY
PERMIT WELL ID COLLECT DATE
FACILITY
PERMIT SAMPLE ID COLLECT DATE
P:\Madison County\Analytical & Data\Water\2015\Fall\5802-Closed\Tables\5802Oct2015_Tables Page 1 of 1
Table 2
Summary of Detected Constituents
Madison County Closed Municipal Solid Waste Landfill, Madison County, North Carolina
Metals VOCs (Appendix I)Field Parameters
Lab Certification 387 387 5445 (pH only)
Lab Method EPA 6010C EPA 8260B
Parameter Barium Chromium Lead Selenium
1,1-
Dichloro-
ethane
1,2-
Dichloro-
benzene
1,2-
Dichloro-
propane
1,4-
Dichloro-
benzene
Acetone Benzene Chloro-
benzene
Chloro-
ethane
cis-1,2-
Dichloro-
ethene
Ethyl-
benzene
Methylene
Chloride
Tetra-
hydrofuran
Vinyl
Chloride
Xylene
(Total) pH Turbidity Dissolved
Oxygen
CAS Number 7440-39-3 7440-47-3 7439-92-1 7782-49-2 75-34-3 95-50-1 78-87-5 106-46-7 67-64-1 71-43-2 108-90-7 75-00-3 156-59-2 100-41-4 75-09-2 109-99-9 75-01-4 1330-20-7 SW320 SW330 7782-44-7
SWS ID 15 51 131 183 75 69 82 71 3 16 39 41 78 110 140 458 211 346 320 330 356
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU mg/L
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
MW-01 OLD 10/22/2015 395 4.90 J 11.0 5.00 U 0.674 J 0.281 J 0.311 J 3.12 2.66 U 0.603 J 1.77 J 0.810 J 1.97 J 0.190 U 0.220 U 0.820 U 0.324 J 0.580 U 6.33 124.6 3.18
MW-02 OLD 10/22/2015 46.7 J 3.00 U 4.80 J 5.00 U 0.612 J 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 0.220 U 0.820 U 0.180 U 0.580 U 6.80 31.38 7.28
MW-03 OLD 10/22/2015 887 3.00 U 15.8 5.70 J 0.240 U 0.190 U 0.250 U 2.69 3.04 J 0.749 J 3.98 0.865 J 0.210 U 0.210 J 0.220 U 0.820 U 0.180 U 1.21 J 6.32 24.51 0.41
MW-04 OLD 10/22/2015 872 3.00 U 8.40 J 5.80 J 0.540 J 0.190 U 0.250 U 0.878 J 5.65 J 0.354 J 1.72 J 0.576 J 0.841 J 0.357 J 0.220 U 2.37 J 0.180 U 2.26 J 6.25 4.75 2.77
BG SPRING OLD 10/22/2015 430 59.7 26.7 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 0.220 U 0.820 U 0.180 U 0.580 U 6.18 247.7 1.60
DW-01 OLD 10/21/2015 215 3.20 J 7.10 J 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 0.220 U 3.48 J 0.180 U 0.580 U 6.39 4.84 5.56
SW-01 OLD 10/21/2015 63.2 J 3.00 U 2.00 U 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 0.220 U 0.820 U 0.180 U 0.580 U 7.62 5.85 11.58
SW-02 OLD 10/21/2015 59.9 J 3.00 U 2.00 U 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 0.220 U 0.820 U 0.180 U 0.580 U 7.83 2.95 12.28
TRIP BLANK (DW)10/21/2015 NA NA NA NA 0.240 U 0.190 U 0.250 U 0.170 U 6.31 J 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 1.15 J 0.820 U 0.180 U 0.580 U NA NA NA
TRIP BLANK (CLOSED)10/22/2015 NA NA NA NA 0.240 U 0.190 U 0.250 U 0.170 U 10.2 J 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 1.45 J 0.820 U 0.180 U 0.580 U NA NA NA
MDL 5.00 3.00 2.00 5.00 0.240 0.190 0.250 0.170 2.66 0.200 0.180 0.360 0.210 0.190 0.220 0.820 0.180 0.580 NA NA NA
MRL 10.0 5.0 5.0 10.0 1.0 1.0 1.0 1.0 25.0 1.0 1.0 1.0 1.0 1.0 5.0 10.0 1.0 3.0 NA NA NE
SWSL 100 10 10 10 5 5 1 1 100 1 3 10 5 1 1 NE 1 5 NE NE NE
2L 700 10 15 20 6 20 0.6 6 6000 1 50 3,000 70 600 3 NE 0.03 500 6.5-8.5 NE NE
IMAC NE NE NE NE NE NE NE NE NE NE NE NE 60 NE NE NE NE NE NE NE NE
GWPS NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
2B 200,000 50 25 5 100 470 15 100 2000 51 140 NE 720 97 NE NE 2.4 600 6.0-9.0 50 > 5.0
Notes:
1.Only detected constituents are listed on this table. Please refer to the TestAmerica laboratory analysis reports for further details.
2."Lab Method" is the analytical method used to analyze the constituents.
3."CAS Number" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
4."SWS ID" is the Solid Waste Section Identification Number.
5."Units" are micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, and milligrams per liter (mg/L) for dissolved oxygen.
6."Collect Date" is the date on which the sample was collected in the field.
7."Result" is analytical data reported by the laboratory or field data collected by Altamont.
8."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
9."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method. MRL equals PQL values in the Pace Analytical Reports.
10."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
11."U" is a laboratory data qualifier used for parameters not detected at concentrations above MDL.
12."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL.
An italicized "J" qualifier is assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
13."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources,
Subchapter 2L - Groundwater Classifications and Standards," DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
14."GWPS" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DENR. Current standards were obtained from http://portal.ncdenr.org/web/sw/envmonitoringlist (last updated June 13, 2011).
GWPS is used only if 2L or IMAC standards are not established for specific constituent.
15."2B" indicates surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water and Wetland Standards,"
(last amended on May 1, 2007) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
16."NE" means Not Established. "NA" means Not Applicable.
17.Bold numbers indicate a detection. Shaded cells indicate result in exceedance of the 2L, IMAC, GWP, or 2B standard.
P:\Madison County\Analytical & Data\Water\2015\Fall\5802-Closed\Tables\5802Oct2015_Tables Page 1 of 1
Table 3
Solid Waste Section Limits Exceedances Notification
Madison County Closed Municipal Solid Waste Landfill, Madison County, North Carolina
FACILITY
PERMIT WELL ID CAS NUMBER SWS ID PARAMETER RESULT UNITS METHOD MDL MRL SWSL COLLECT DATE
58-02 MW-01 OLD 7440-39-3 15 Barium 395 ug/L EPA 6010 5.00 10.0 100 10/22/2015
58-02 MW-01 OLD 7439-92-1 131 Lead 11.0 ug/L EPA 6010 2.00 5.0 10 10/22/2015
58-02 MW-01 OLD 106-46-7 71 1,4-Dichlorobenzene 3.12 ug/L EPA 8260 0.170 1.0 1 10/22/2015
58-02 MW-03 OLD 7440-39-3 15 Barium 887 ug/L EPA 6010 5.00 10.0 100 10/22/2015
58-02 MW-03 OLD 7439-92-1 131 Lead 15.8 ug/L EPA 6010 2.00 5.0 10 10/22/2015
58-02 MW-03 OLD 106-46-7 71 1,4-Dichlorobenzene 2.69 ug/L EPA 8260 0.170 1.0 1 10/22/2015
58-02 MW-03 OLD 108-90-7 39 Chlorobenzene 3.98 ug/L EPA 8260 0.180 1.0 3 10/22/2015
58-02 MW-04 OLD 7440-39-3 15 Barium 872 ug/L EPA 6010 5.00 10.0 100 10/22/2015
58-02 BG SPRING OLD 7440-39-3 15 Barium 430 ug/L EPA 6010 5.00 10.0 100 10/22/2015
58-02 BG SPRING OLD 7440-47-3 51 Chromium 59.7 ug/L EPA 6010 3.00 5.0 10 10/22/2015
58-02 BG SPRING OLD 7439-92-1 51 Lead 26.7 ug/L EPA 6010 2.00 5.0 10 10/22/2015
58-02 DW-01 OLD 7440-47-4 51 Barium 215 ug/L EPA 6010 5.00 10.0 100 10/21/2015
58-02 TRIP BLANK (DW)75-09-2 140 Methylene Chloride 1.15 J ug/L EPA 6010 0.220 5.0 1 10/21/2015
58-02 TRIP BLANK (CLOSED)75-09-2 140 Methylene Chloride 1.45 J ug/L EPA 6010 0.220 5.0 1 10/22/2015
Notes:
1."CAS NUMBER" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
2."SWS ID" is the Solid Waste Section Identification Number.
3."RESULT" is the analytical data reported by the laboratory.
4."UNITS" are micrograms per liter (µg/L) for analytical results.
5."METHOD" is the analytical method used to analyze the constituents.
6."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence
that the analyte concentration is greater than zero.
7."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced
method.
8."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively
determined with suitable precision and accuracy.
9."COLLECT DATE" is the date on which the sample was collected in the field.
10.Shaded cells indicate result in exceedance of the applicable water quality standards ("2L", "IMAC", or "GWPS").
11."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards," DENR
(Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L rule.
12."GWPS" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DENR. Current standards were obtained from
portal.ncdenr.org/web/sw/envmonitoringlist (last updated June 13, 2011). GWPS is used only if 2L or IMAC standards are not established for the constituent.
P:\Madison County\Analytical & Data\Water\2015\Fall\5802-Closed\Tables\5802Oct2015_Tables Page 1 of 1
Table 4
Water Quality Standards Exceedances Notification
Madison County Closed Municipal Solid Waste Landfill, Madison County, North Carolina
FACILITY PERMIT WELL ID CAS
NUMBER SWS ID PARAMETER RESULT UNITS METHOD MDL MRL SWSL
WATER
QUALITY
STANDARD
COLLECT
DATE CAUSE AND SIGNIFICANCE
GROUNDWATER SAMPLES - 2L STANDARD, IMAC, OR GWPS
58-02 MW-01 OLD 75-01-4 211 Vinyl Chloride 0.324 J ug/L EPA 8260B 0.180 1.00 1 0.03 10/22/2015 Anthropogenic.
58-02 MW-01 OLD SW320 320 pH 6.33 SU NE NE 6.5-8.5 6.5-9.5 10/22/2015 Possibly naturally occuring.
58-02 MW-03 OLD 7440-39-3 15 Barium 887 ug/L EPA 6010C 5.00 10.0 100 700 10/22/2015
58-02 MW-03 OLD 7439-92-1 131 Lead 15.8 ug/L EPA 6010C 2.00 5.00 10 15 10/22/2015
58-02 MW-03 OLD SW320 320 pH 6.32 SU NE NE 6.5-8.5 6.5-9.5 10/22/2015
58-02 MW-04 OLD 7440-39-3 15 Barium 872 ug/L EPA 6010C 5.00 10.0 100 700 10/22/2015
58-02 MW-04 OLD SW320 320 pH 6.25 SU NE NE 6.5-8.5 6.5-9.5 10/22/2015
58-02 BG SPRING OLD 7440-47-3 51 Chromium 59.7 ug/L EPA 6010C 3.00 5.00 10 10 10/22/2015
58-02 BG SPRING OLD 7439-92-1 131 Lead 26.7 ug/L EPA 6010C 2.50 5.00 10 15 10/22/2015
58-02 BG SPRING OLD SW320 320 pH 6.18 SU NE NE NE 6.5-9.5 10/22/2015
58-02 DW-01 OLD SW320 320 pH 6.39 SU NE NE NE 6.5-9.5 10/21/2015 Likely naturally occurring.
Notes:
1."CAS NUMBER" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
2."SWS ID" is the Solid Waste Section Identification Number.
3."RESULT" is analytical data reported by the laboratory or field data collected by Altamont.
4."UNITS" are micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH and nephelometric turbidity units (NTU) for turbidity.
5."METHOD" is the analytical method used to analyze the constituents.
6."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte
concentration is greater than zero.
7."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
8."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable
precision and accuracy.
9."WATER QUALITY STANDARD" refers to the 2L standard or Interim Maximum Allowable Concentration (IMAC) for groundwater.
10."COLLECT DATE" is the date on which the sample was collected in the field.
11."NE" means not established.
12.Blank cell indicates that there is no relevant information associated with this cell.
13."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment
and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards," DENR (Amended April 1, 2013). The IMAC concentrations are listed in
Appendix #1 of the 2L rule.
14."2B" indicates surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water
and Wetland Standards," (last amended on May 1, 2007) or indicates National Criteria per EPA obtained from table current as of May 15, 2013.
15."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL.
An italicized "J" qualifier is assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
Possibly naturally occuring.
Possibly naturally occuring.
Possibly naturally occuring.
P:\Madison County\Analytical & Data\Water\2015\Fall\5802-Closed\Tables\5802Oct2015_Tables Page 1 of 1

APPENDICES

APPENDIX A

Sampling Logs and
Equipment Documentation
and Instrument Calibration Data Sheets

APPENDIX B

Reports of Laboratory Analysis
and Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-90188-1
Client Project/Site: Madison Co Closed Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
10/30/2015 1:05:22 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
TestAmerica Job ID: 490-90188-1
Page 2 of 28 TestAmerica Nashville10/30/2015
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
1
2
3
4
5
6
7
8
9
10
11
12
13
Sample Summary
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-90188-1 SW-01 OLD Water 10/21/15 14:00 10/22/15 10:10
490-90188-2 SW-02 OLD Water 10/21/15 14:20 10/22/15 10:10
490-90188-3 TripBlank Water 10/21/15 00:01 10/22/15 10:10
490-90188-4 DW-01 OLD Water 10/21/15 13:46 10/22/15 10:10
TestAmerica Nashville
Page 3 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90188-1
Project/Site: Madison Co Closed Landfill
Job ID: 490-90188-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-90188-1
Comments
No additional comments.
Receipt
The samples were received on 10/22/2015 10:10 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 4.7º C.
GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch
490-292542 recovered outside control limits for the following analytes: trans-1,2-Dichloroethene. These analytes were biased high in the
LCS and were not detected in the associated samples; therefore, the data have been reported.
Method(s) 8260B: Surrogate recovery was outside acceptance limits for the following matrix spike (MS) sample: (490-90102-D-1 MS). The
parent sample's surrogate recovery was within limits. The MS sample has been qualified and reported.
Method(s) 8260B: The preservative used in the sample containers provided is not compatible with one of the Method 8260 analytes
requested. The following samples was received preserved with hydrochloric acid: SW-01 OLD (490-90188-1), SW-02 OLD (490-90188-2),
TripBlank (490-90188-3), DW-01 OLD (490-90188-4) and (490-90102-C-1). The requested target analyte list includes Acrylonitrile that
degrades in an acidic medium.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 6010C: The continuing calibration verification (CCV) associated with batch 490-293404 recovered above the upper control limit
for chromium. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
The following samples are impacted: SW-01 OLD (490-90188-1) and SW-02 OLD (490-90188-2).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Definitions/Glossary
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Qualifiers
GC/MS VOA
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
X Surrogate is outside control limits
E Result exceeded calibration range.
F2 MS/MSD RPD exceeds control limits
*LCS or LCSD is outside acceptance limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-1Client Sample ID: SW-01 OLD
Matrix: WaterDate Collected: 10/21/15 14:00
Date Received: 10/22/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/24/15 09:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/24/15 09:32 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/24/15 09:32 1Benzene<0.200
1.00 0.150 ug/L 10/24/15 09:32 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/24/15 09:32 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/24/15 09:32 1Bromoform<0.290
1.00 0.350 ug/L 10/24/15 09:32 1Bromomethane<0.350
50.0 2.64 ug/L 10/24/15 09:32 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/24/15 09:32 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/24/15 09:32 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/24/15 09:32 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/24/15 09:32 1Chloroethane<0.360
1.00 0.230 ug/L 10/24/15 09:32 1Chloroform<0.230
1.00 0.360 ug/L 10/24/15 09:32 1Chloromethane<0.360
1.00 0.210 ug/L 10/24/15 09:32 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/24/15 09:32 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/24/15 09:32 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/24/15 09:32 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/24/15 09:32 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/24/15 09:32 1Dibromomethane<0.450
1.00 0.190 ug/L 10/24/15 09:32 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/24/15 09:32 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/24/15 09:32 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/24/15 09:32 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/24/15 09:32 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/24/15 09:32 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/24/15 09:32 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/24/15 09:32 12-Hexanone <1.28
10.0 1.50 ug/L 10/24/15 09:32 1Iodomethane<1.50
5.00 0.220 ug/L 10/24/15 09:32 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/24/15 09:32 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/24/15 09:32 1Styrene<0.280
1.00 0.150 ug/L 10/24/15 09:32 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/24/15 09:32 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/24/15 09:32 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/24/15 09:32 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/24/15 09:32 1Toluene<0.170
5.00 0.460 ug/L 10/24/15 09:32 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/24/15 09:32 1trans-1,2-Dichloroethene <0.230 *
1.00 0.170 ug/L 10/24/15 09:32 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/24/15 09:32 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/24/15 09:32 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/24/15 09:32 1Trichloroethene<0.200
1.00 0.210 ug/L 10/24/15 09:32 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/24/15 09:32 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/24/15 09:32 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/24/15 09:32 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/24/15 09:32 1Xylenes, Total <0.580
TestAmerica Nashville
Page 6 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-1Client Sample ID: SW-01 OLD
Matrix: WaterDate Collected: 10/21/15 14:00
Date Received: 10/22/15 10:10
4-Bromofluorobenzene (Surr)96 70-130 10/24/15 09:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 10/24/15 09:32 170-130
1,2-Dichloroethane-d4 (Surr)102 10/24/15 09:32 170-130
Toluene-d8 (Surr)102 10/24/15 09:32 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/24/15 14:24 10/27/15 20:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/24/15 14:24 10/27/15 20:16 1Barium63.2
1.00 0.500 ug/L 10/24/15 14:24 10/27/15 20:16 1Cadmium<0.500
5.00 3.00 ug/L 10/24/15 14:24 10/27/15 20:16 1Chromium<3.00 ^
5.00 2.00 ug/L 10/24/15 14:24 10/27/15 20:16 1Lead<2.00
10.0 5.00 ug/L 10/24/15 14:24 10/27/15 20:16 1Selenium<5.00
5.00 3.00 ug/L 10/24/15 14:24 10/27/15 20:16 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/26/15 11:43 10/27/15 17:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 7 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-2Client Sample ID: SW-02 OLD
Matrix: WaterDate Collected: 10/21/15 14:20
Date Received: 10/22/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/24/15 10:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/24/15 10:01 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/24/15 10:01 1Benzene<0.200
1.00 0.150 ug/L 10/24/15 10:01 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/24/15 10:01 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/24/15 10:01 1Bromoform<0.290
1.00 0.350 ug/L 10/24/15 10:01 1Bromomethane<0.350
50.0 2.64 ug/L 10/24/15 10:01 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/24/15 10:01 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/24/15 10:01 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/24/15 10:01 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/24/15 10:01 1Chloroethane<0.360
1.00 0.230 ug/L 10/24/15 10:01 1Chloroform<0.230
1.00 0.360 ug/L 10/24/15 10:01 1Chloromethane<0.360
1.00 0.210 ug/L 10/24/15 10:01 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/24/15 10:01 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/24/15 10:01 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/24/15 10:01 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/24/15 10:01 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/24/15 10:01 1Dibromomethane<0.450
1.00 0.190 ug/L 10/24/15 10:01 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/24/15 10:01 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/24/15 10:01 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/24/15 10:01 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/24/15 10:01 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/24/15 10:01 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/24/15 10:01 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/24/15 10:01 12-Hexanone <1.28
10.0 1.50 ug/L 10/24/15 10:01 1Iodomethane<1.50
5.00 0.220 ug/L 10/24/15 10:01 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/24/15 10:01 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/24/15 10:01 1Styrene<0.280
1.00 0.150 ug/L 10/24/15 10:01 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/24/15 10:01 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/24/15 10:01 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/24/15 10:01 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/24/15 10:01 1Toluene<0.170
5.00 0.460 ug/L 10/24/15 10:01 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/24/15 10:01 1trans-1,2-Dichloroethene <0.230 *
1.00 0.170 ug/L 10/24/15 10:01 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/24/15 10:01 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/24/15 10:01 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/24/15 10:01 1Trichloroethene<0.200
1.00 0.210 ug/L 10/24/15 10:01 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/24/15 10:01 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/24/15 10:01 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/24/15 10:01 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/24/15 10:01 1Xylenes, Total <0.580
TestAmerica Nashville
Page 8 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-2Client Sample ID: SW-02 OLD
Matrix: WaterDate Collected: 10/21/15 14:20
Date Received: 10/22/15 10:10
4-Bromofluorobenzene (Surr)97 70-130 10/24/15 10:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)97 10/24/15 10:01 170-130
1,2-Dichloroethane-d4 (Surr)86 10/24/15 10:01 170-130
Toluene-d8 (Surr)103 10/24/15 10:01 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/24/15 14:24 10/27/15 20:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/24/15 14:24 10/27/15 20:20 1Barium59.9
1.00 0.500 ug/L 10/24/15 14:24 10/27/15 20:20 1Cadmium<0.500
5.00 3.00 ug/L 10/24/15 14:24 10/27/15 20:20 1Chromium<3.00 ^
5.00 2.00 ug/L 10/24/15 14:24 10/27/15 20:20 1Lead<2.00
10.0 5.00 ug/L 10/24/15 14:24 10/27/15 20:20 1Selenium<5.00
5.00 3.00 ug/L 10/24/15 14:24 10/27/15 20:20 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/26/15 11:43 10/27/15 17:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 9 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-3Client Sample ID: TripBlank
Matrix: WaterDate Collected: 10/21/15 00:01
Date Received: 10/22/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 6.31 J 25.0 2.66 ug/L 10/24/15 05:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/24/15 05:17 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/24/15 05:17 1Benzene<0.200
1.00 0.150 ug/L 10/24/15 05:17 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/24/15 05:17 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/24/15 05:17 1Bromoform<0.290
1.00 0.350 ug/L 10/24/15 05:17 1Bromomethane<0.350
50.0 2.64 ug/L 10/24/15 05:17 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/24/15 05:17 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/24/15 05:17 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/24/15 05:17 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/24/15 05:17 1Chloroethane<0.360
1.00 0.230 ug/L 10/24/15 05:17 1Chloroform<0.230
1.00 0.360 ug/L 10/24/15 05:17 1Chloromethane<0.360
1.00 0.210 ug/L 10/24/15 05:17 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/24/15 05:17 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/24/15 05:17 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/24/15 05:17 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/24/15 05:17 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/24/15 05:17 1Dibromomethane<0.450
1.00 0.190 ug/L 10/24/15 05:17 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/24/15 05:17 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/24/15 05:17 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/24/15 05:17 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/24/15 05:17 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/24/15 05:17 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/24/15 05:17 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/24/15 05:17 12-Hexanone <1.28
10.0 1.50 ug/L 10/24/15 05:17 1Iodomethane<1.50
5.00 0.220 ug/L 10/24/15 05:17 1Methylene Chloride 1.15 J
10.0 0.810 ug/L 10/24/15 05:17 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/24/15 05:17 1Styrene<0.280
1.00 0.150 ug/L 10/24/15 05:17 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/24/15 05:17 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/24/15 05:17 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/24/15 05:17 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/24/15 05:17 1Toluene<0.170
5.00 0.460 ug/L 10/24/15 05:17 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/24/15 05:17 1trans-1,2-Dichloroethene <0.230 *
1.00 0.170 ug/L 10/24/15 05:17 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/24/15 05:17 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/24/15 05:17 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/24/15 05:17 1Trichloroethene<0.200
1.00 0.210 ug/L 10/24/15 05:17 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/24/15 05:17 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/24/15 05:17 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/24/15 05:17 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/24/15 05:17 1Xylenes, Total <0.580
TestAmerica Nashville
Page 10 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-3Client Sample ID: TripBlank
Matrix: WaterDate Collected: 10/21/15 00:01
Date Received: 10/22/15 10:10
4-Bromofluorobenzene (Surr)98 70-130 10/24/15 05:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)111 10/24/15 05:17 170-130
1,2-Dichloroethane-d4 (Surr)100 10/24/15 05:17 170-130
Toluene-d8 (Surr)103 10/24/15 05:17 170-130
TestAmerica Nashville
Page 11 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-4Client Sample ID: DW-01 OLD
Matrix: WaterDate Collected: 10/21/15 13:46
Date Received: 10/22/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/24/15 10:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/24/15 10:29 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/24/15 10:29 1Benzene<0.200
1.00 0.150 ug/L 10/24/15 10:29 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/24/15 10:29 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/24/15 10:29 1Bromoform<0.290
1.00 0.350 ug/L 10/24/15 10:29 1Bromomethane<0.350
50.0 2.64 ug/L 10/24/15 10:29 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/24/15 10:29 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/24/15 10:29 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/24/15 10:29 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/24/15 10:29 1Chloroethane<0.360
1.00 0.230 ug/L 10/24/15 10:29 1Chloroform<0.230
1.00 0.360 ug/L 10/24/15 10:29 1Chloromethane<0.360
1.00 0.210 ug/L 10/24/15 10:29 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/24/15 10:29 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/24/15 10:29 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/24/15 10:29 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/24/15 10:29 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/24/15 10:29 1Dibromomethane<0.450
1.00 0.190 ug/L 10/24/15 10:29 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/24/15 10:29 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/24/15 10:29 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/24/15 10:29 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/24/15 10:29 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/24/15 10:29 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/24/15 10:29 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/24/15 10:29 12-Hexanone <1.28
10.0 1.50 ug/L 10/24/15 10:29 1Iodomethane<1.50
5.00 0.220 ug/L 10/24/15 10:29 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/24/15 10:29 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/24/15 10:29 1Styrene<0.280
1.00 0.150 ug/L 10/24/15 10:29 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/24/15 10:29 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/24/15 10:29 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/24/15 10:29 1Tetrahydrofuran3.48 J
1.00 0.170 ug/L 10/24/15 10:29 1Toluene<0.170
5.00 0.460 ug/L 10/24/15 10:29 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/24/15 10:29 1trans-1,2-Dichloroethene <0.230 *
1.00 0.170 ug/L 10/24/15 10:29 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/24/15 10:29 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/24/15 10:29 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/24/15 10:29 1Trichloroethene<0.200
1.00 0.210 ug/L 10/24/15 10:29 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/24/15 10:29 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/24/15 10:29 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/24/15 10:29 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/24/15 10:29 1Xylenes, Total <0.580
TestAmerica Nashville
Page 12 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90188-4Client Sample ID: DW-01 OLD
Matrix: WaterDate Collected: 10/21/15 13:46
Date Received: 10/22/15 10:10
4-Bromofluorobenzene (Surr)98 70-130 10/24/15 10:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)116 10/24/15 10:29 170-130
1,2-Dichloroethane-d4 (Surr)107 10/24/15 10:29 170-130
Toluene-d8 (Surr)103 10/24/15 10:29 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/24/15 17:07 10/27/15 20:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/24/15 17:07 10/27/15 20:24 1Barium215
1.00 0.500 ug/L 10/24/15 17:07 10/27/15 20:24 1Cadmium<0.500
5.00 3.00 ug/L 10/24/15 17:07 10/28/15 13:58 1Chromium3.20 J
5.00 2.00 ug/L 10/24/15 17:07 10/27/15 20:24 1Lead7.10
10.0 5.00 ug/L 10/24/15 17:07 10/27/15 20:24 1Selenium<5.00
5.00 3.00 ug/L 10/24/15 17:07 10/27/15 20:24 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/26/15 11:43 10/27/15 17:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 13 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-292542/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/24/15 04:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 10/24/15 04:21 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/24/15 04:21 1Benzene
<0.150 0.1501.00 ug/L 10/24/15 04:21 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/24/15 04:21 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/24/15 04:21 1Bromoform
<0.350 0.3501.00 ug/L 10/24/15 04:21 1Bromomethane
<2.64 2.6450.0 ug/L 10/24/15 04:21 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/24/15 04:21 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/24/15 04:21 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/24/15 04:21 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/24/15 04:21 1Chloroethane
<0.230 0.2301.00 ug/L 10/24/15 04:21 1Chloroform
<0.360 0.3601.00 ug/L 10/24/15 04:21 1Chloromethane
<0.210 0.2101.00 ug/L 10/24/15 04:21 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/24/15 04:21 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/24/15 04:21 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/24/15 04:21 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/24/15 04:21 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/24/15 04:21 1Dibromomethane
<0.190 0.1901.00 ug/L 10/24/15 04:21 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/24/15 04:21 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/24/15 04:21 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/24/15 04:21 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/24/15 04:21 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/24/15 04:21 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/24/15 04:21 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/24/15 04:21 12-Hexanone
<1.50 1.5010.0 ug/L 10/24/15 04:21 1Iodomethane
<0.220 0.2205.00 ug/L 10/24/15 04:21 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/24/15 04:21 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/24/15 04:21 1Styrene
<0.150 0.1501.00 ug/L 10/24/15 04:21 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/24/15 04:21 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/24/15 04:21 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/24/15 04:21 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/24/15 04:21 1Toluene
<0.460 0.4605.00 ug/L 10/24/15 04:21 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/24/15 04:21 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/24/15 04:21 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/24/15 04:21 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/24/15 04:21 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/24/15 04:21 1Trichloroethene
<0.210 0.2101.00 ug/L 10/24/15 04:21 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/24/15 04:21 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/24/15 04:21 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/24/15 04:21 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/24/15 04:21 1Xylenes, Total
TestAmerica Nashville
Page 14 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-292542/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
4-Bromofluorobenzene (Surr)98 70-130 10/24/15 04:21 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
122 10/24/15 04:21 1Dibromofluoromethane (Surr)70-130
109 10/24/15 04:21 11,2-Dichloroethane-d4 (Surr)70-130
99 10/24/15 04:21 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-292542/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
Acetone 250 263.0 ug/L 105 54-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 664.8 ug/L 133 61-140
Benzene 50.0 46.92 ug/L 94 80-121
Bromochloromethane 50.0 58.13 ug/L 116 78-129
Bromodichloromethane 50.0 55.63 ug/L 111 75-129
Bromoform 50.0 53.62 E ug/L 107 46-145
Bromomethane 50.0 59.18 ug/L 118 41-150
2-Butanone (MEK)250 330.9 ug/L 132 62-133
Carbon disulfide 50.0 55.88 ug/L 112 77-126
Carbon tetrachloride 50.0 51.28 ug/L 103 64-147
Chlorobenzene 50.0 48.49 ug/L 97 80-120
Chloroethane 50.0 52.09 ug/L 104 72-120
Chloroform 50.0 54.38 ug/L 109 73-129
Chloromethane 50.0 51.58 ug/L 103 12-150
cis-1,2-Dichloroethene 50.0 62.59 ug/L 125 76-125
cis-1,3-Dichloropropene 50.0 54.19 ug/L 108 74-140
Dibromochloromethane 50.0 55.98 ug/L 112 69-133
1,2-Dibromo-3-Chloropropane 50.0 56.54 ug/L 113 54-125
1,2-Dibromoethane (EDB)50.0 51.41 ug/L 103 80-129
Dibromomethane 50.0 58.88 ug/L 118 71-125
1,2-Dichlorobenzene 50.0 50.97 ug/L 102 80-121
1,4-Dichlorobenzene 50.0 48.70 ug/L 97 80-120
1,1-Dichloroethane 50.0 57.95 ug/L 116 78-125
1,2-Dichloroethane 50.0 47.19 ug/L 94 77-121
1,1-Dichloroethene 50.0 54.84 ug/L 110 79-124
1,2-Dichloropropane 50.0 50.53 ug/L 101 75-120
Ethylbenzene 50.0 49.81 ug/L 100 80-130
2-Hexanone 250 268.2 ug/L 107 60-142
Iodomethane 50.0 60.38 ug/L 121 40-150
Methylene Chloride 50.0 56.36 ug/L 113 79-123
4-Methyl-2-pentanone (MIBK)250 276.7 ug/L 111 60-137
Styrene 50.0 51.40 ug/L 103 80-127
1,1,1,2-Tetrachloroethane 50.0 51.14 ug/L 102 74-135
1,1,2,2-Tetrachloroethane 50.0 52.35 ug/L 105 69-131
Tetrachloroethene 50.0 48.83 ug/L 98 80-126
Tetrahydrofuran 100 121.0 ug/L 121 51-124
Toluene 50.0 49.09 ug/L 98 80-126
trans-1,4-Dichloro-2-butene 50.0 52.07 ug/L 104 41-147
TestAmerica Nashville
Page 15 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-292542/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
trans-1,2-Dichloroethene 50.0 68.53 *ug/L 137 79-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
trans-1,3-Dichloropropene 50.0 54.13 ug/L 108 63-134
1,1,1-Trichloroethane 50.0 40.95 ug/L 82 78-135
1,1,2-Trichloroethane 50.0 51.93 ug/L 104 80-124
Trichloroethene 50.0 49.88 ug/L 100 80-123
Trichlorofluoromethane 50.0 60.48 ug/L 121 65-124
1,2,3-Trichloropropane 50.0 52.46 ug/L 105 70-131
Vinyl acetate 100 131.9 ug/L 132 54-139
Vinyl chloride 50.0 49.63 ug/L 99 68-120
Xylenes, Total 100 100.1 ug/L 100 80-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
82Dibromofluoromethane (Surr)70 -130
1021,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-90102-D-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
Acetone <2.66 F2 250 352.3 ug/L 141 45-141
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 516.1 ug/L 103 50-148
Benzene <0.200 50.0 46.35 ug/L 93 75-133
Bromochloromethane <0.150 F2 F1 50.0 75.56 F1 ug/L 151 67-139
Bromodichloromethane <0.170 50.0 54.82 ug/L 110 70-140
Bromoform <0.290 50.0 49.59 ug/L 99 42-147
Bromomethane <0.350 F1 50.0 88.17 F1 ug/L 176 16-163
2-Butanone (MEK)<2.64 F2 F1 250 515.9 F1 ug/L 206 50-138
Carbon disulfide <0.220 50.0 43.89 ug/L 88 48-152
Carbon tetrachloride <0.180 F2 50.0 61.92 ug/L 124 62-164
Chlorobenzene <0.180 50.0 48.75 ug/L 97 80-129
Chloroethane <0.360 F2 F1 50.0 84.94 F1 ug/L 170 58-137
Chloroform <0.230 F2 F1 50.0 80.98 F1 ug/L 162 66-138
Chloromethane <0.360 F2 50.0 83.11 ug/L 166 10-169
cis-1,2-Dichloroethene <0.210 F2 F1 50.0 75.07 F1 ug/L 150 68-138
cis-1,3-Dichloropropene <0.170 F2 F1 50.0 31.17 F1 ug/L 62 71-141
Dibromochloromethane <0.250 50.0 50.89 ug/L 102 66-140
1,2-Dibromo-3-Chloropropane <0.940 50.0 48.00 ug/L 96 52-126
1,2-Dibromoethane (EDB)<0.210 50.0 46.92 ug/L 94 75-137
Dibromomethane <0.450 50.0 54.47 ug/L 109 58-140
1,2-Dichlorobenzene <0.190 50.0 48.18 ug/L 96 79-128
1,4-Dichlorobenzene <0.170 50.0 46.32 ug/L 93 78-126
1,1-Dichloroethane <0.240 F2 F1 50.0 77.81 F1 ug/L 156 71-139
1,2-Dichloroethane <0.200 50.0 49.03 ug/L 98 64-136
1,1-Dichloroethene <0.250 F2 50.0 68.35 ug/L 137 70-142
1,2-Dichloropropane <0.250 F2 F1 50.0 46.49 ug/L 93 67-131
TestAmerica Nashville
Page 16 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-90102-D-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
Ethylbenzene <0.190 50.0 50.51 ug/L 101 79-139
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
2-Hexanone <1.28 250 243.3 ug/L 97 50-150
Iodomethane <1.50 F2 50.0 75.09 ug/L 150 34-191
Methylene Chloride <0.220 F2 50.0 67.53 ug/L 135 64-139
4-Methyl-2-pentanone (MIBK)<0.810 F2 250 132.7 ug/L 53 50-147
Styrene <0.280 50.0 50.05 ug/L 100 61-148
1,1,1,2-Tetrachloroethane <0.150 50.0 49.90 ug/L 100 73-141
1,1,2,2-Tetrachloroethane <0.190 50.0 46.37 ug/L 93 56-143
Tetrachloroethene <0.140 50.0 43.65 ug/L 87 72-145
Tetrahydrofuran <0.820 F2 F1 100 328.6 E F1 ug/L 329 34-133
Toluene <0.170 F2 F1 50.0 26.65 F1 ug/L 53 75-136
trans-1,4-Dichloro-2-butene <0.460 50.0 48.77 ug/L 98 29-156
trans-1,2-Dichloroethene <0.230 *50.0 60.02 ug/L 120 66-143
trans-1,3-Dichloropropene <0.170 F2 F1 50.0 28.52 F1 ug/L 57 59-135
1,1,1-Trichloroethane <0.190 F2 F1 50.0 88.94 F1 ug/L 178 76-149
1,1,2-Trichloroethane <0.190 F2 F1 50.0 27.10 F1 ug/L 54 74-134
Trichloroethene <0.200 F2 F1 50.0 53.21 ug/L 106 73-144
Trichlorofluoromethane <0.210 F1 50.0 69.84 F1 ug/L 140 58-139
1,2,3-Trichloropropane <0.230 50.0 48.14 ug/L 96 53-144
Vinyl acetate <1.71 F2 100 154.2 ug/L 154 37-154
Vinyl chloride <0.180 F2 F1 50.0 84.74 F1 ug/L 169 56-129
Xylenes, Total <0.580 100 101.1 ug/L 101 74-141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MS MS
Qualifier Limits%Recovery
168 XDibromofluoromethane (Surr)70 -130
1061,2-Dichloroethane-d4 (Surr)70 -130
53 XToluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-90102-E-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
Acetone <2.66 F2 250 266.4 F2 ug/L 107 45-141 28 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 552.1 ug/L 110 50-148 7 18
Benzene <0.200 50.0 49.56 ug/L 99 75-133 7 17
Bromochloromethane <0.150 F2 F1 50.0 51.17 F2 ug/L 102 67-139 38 17
Bromodichloromethane <0.170 50.0 52.78 ug/L 106 70-140 4 18
Bromoform <0.290 50.0 50.35 E ug/L 101 42-147 2 16
Bromomethane <0.350 F1 50.0 57.05 ug/L 114 16-163 43 50
2-Butanone (MEK)<2.64 F2 F1 250 260.2 F2 ug/L 104 50-138 66 19
Carbon disulfide <0.220 50.0 52.10 ug/L 104 48-152 17 21
Carbon tetrachloride <0.180 F2 50.0 38.35 F2 ug/L 77 62-164 47 19
Chlorobenzene <0.180 50.0 49.20 ug/L 98 80-129 1 14
Chloroethane <0.360 F2 F1 50.0 54.58 F2 ug/L 109 58-137 44 20
Chloroform <0.230 F2 F1 50.0 54.20 F2 ug/L 108 66-138 40 18
Chloromethane <0.360 F2 50.0 52.06 F2 ug/L 104 10-169 46 31
TestAmerica Nashville
Page 17 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-90102-E-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 292542
cis-1,2-Dichloroethene <0.210 F2 F1 50.0 52.80 F2 ug/L 106 68-138 35 17
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
cis-1,3-Dichloropropene <0.170 F2 F1 50.0 60.84 F2 ug/L 122 71-141 65 15
Dibromochloromethane <0.250 50.0 53.04 ug/L 106 66-140 4 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 48.16 ug/L 96 52-126 0 24
1,2-Dibromoethane (EDB)<0.210 50.0 49.09 ug/L 98 75-137 5 15
Dibromomethane <0.450 50.0 54.12 ug/L 108 58-140 1 16
1,2-Dichlorobenzene <0.190 50.0 48.85 ug/L 98 79-128 1 15
1,4-Dichlorobenzene <0.170 50.0 47.44 ug/L 95 78-126 2 15
1,1-Dichloroethane <0.240 F2 F1 50.0 50.75 F2 ug/L 101 71-139 42 17
1,2-Dichloroethane <0.200 50.0 45.08 ug/L 90 64-136 8 17
1,1-Dichloroethene <0.250 F2 50.0 56.63 F2 ug/L 113 70-142 19 17
1,2-Dichloropropane <0.250 F2 F1 50.0 30.76 F1 F2 ug/L 62 67-131 41 17
Ethylbenzene <0.190 50.0 50.98 ug/L 102 79-139 1 15
2-Hexanone <1.28 250 241.9 ug/L 97 50-150 1 15
Iodomethane <1.50 F2 50.0 52.82 F2 ug/L 106 34-191 35 23
Methylene Chloride <0.220 F2 50.0 51.14 F2 ug/L 102 64-139 28 17
4-Methyl-2-pentanone (MIBK)<0.810 F2 250 284.8 F2 ug/L 114 50-147 73 17
Styrene <0.280 50.0 51.35 ug/L 103 61-148 3 24
1,1,1,2-Tetrachloroethane <0.150 50.0 50.78 ug/L 102 73-141 2 16
1,1,2,2-Tetrachloroethane <0.190 50.0 48.02 ug/L 96 56-143 4 20
Tetrachloroethene <0.140 50.0 50.18 ug/L 100 72-145 14 16
Tetrahydrofuran <0.820 F2 F1 100 111.1 F2 ug/L 111 34-133 99 18
Toluene <0.170 F2 F1 50.0 50.10 F2 ug/L 100 75-136 61 15
trans-1,4-Dichloro-2-butene <0.460 50.0 50.85 ug/L 102 29-156 4 26
trans-1,2-Dichloroethene <0.230 *50.0 64.76 ug/L 130 66-143 8 16
trans-1,3-Dichloropropene <0.170 F2 F1 50.0 53.47 F2 ug/L 107 59-135 61 14
1,1,1-Trichloroethane <0.190 F2 F1 50.0 60.86 F2 ug/L 122 76-149 37 17
1,1,2-Trichloroethane <0.190 F2 F1 50.0 49.64 F2 ug/L 99 74-134 59 15
Trichloroethene <0.200 F2 F1 50.0 31.97 F1 F2 ug/L 64 73-144 50 17
Trichlorofluoromethane <0.210 F1 50.0 64.11 ug/L 128 58-139 9 18
1,2,3-Trichloropropane <0.230 50.0 49.09 ug/L 98 53-144 2 19
Vinyl acetate <1.71 F2 100 104.6 F2 ug/L 105 37-154 38 21
Vinyl chloride <0.180 F2 F1 50.0 55.37 F2 ug/L 111 56-129 42 17
Xylenes, Total <0.580 100 101.3 ug/L 101 74-141 0 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
MSD MSD
Qualifier Limits%Recovery
117Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
TestAmerica Nashville
Page 18 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 6010C - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-292695/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293404 Prep Batch: 292695
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/24/15 14:24 10/27/15 18:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<5.00 5.0010.0 ug/L 10/24/15 14:24 10/27/15 18:08 1Barium
<0.500 0.5001.00 ug/L 10/24/15 14:24 10/27/15 18:08 1Cadmium
<3.00 3.005.00 ug/L 10/24/15 14:24 10/27/15 18:08 1Chromium
<2.00 2.005.00 ug/L 10/24/15 14:24 10/27/15 18:08 1Lead
<5.00 5.0010.0 ug/L 10/24/15 14:24 10/27/15 18:08 1Selenium
<3.00 3.005.00 ug/L 10/24/15 14:24 10/27/15 18:08 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-292695/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293404 Prep Batch: 292695
Arsenic 50.0 48.20 ug/L 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2000 1997 ug/L 100 80-120
Cadmium 50.0 49.90 ug/L 100 80-120
Chromium 200 208.9 ug/L 104 80-120
Lead 50.0 49.60 ug/L 99 80-120
Selenium 50.0 47.00 ug/L 94 80-120
Silver 50.0 47.20 ug/L 94 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-292695/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293404 Prep Batch: 292695
Arsenic 50.0 46.00 ug/L 92 80-120 5 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Barium 2000 1968 ug/L 98 80-120 1 20
Cadmium 50.0 49.20 ug/L 98 80-120 1 20
Chromium 200 208.0 ug/L 104 80-120 0 20
Lead 50.0 49.40 ug/L 99 80-120 0 20
Selenium 50.0 48.00 ug/L 96 80-120 2 20
Silver 50.0 46.40 ug/L 93 80-120 2 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-90119-A-14-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293404 Prep Batch: 292695
Arsenic <8.60 50.0 50.80 ug/L 102 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 436 2000 2338 ug/L 95 75-125
Cadmium <0.500 50.0 48.50 ug/L 97 75-125
Chromium <3.00 200 196.8 ug/L 98 75-125
Lead <2.00 L F1 50.0 9.800 F1 ug/L 20 75-125
Selenium <5.00 50.0 48.10 ug/L 96 75-125
Silver <3.00 50.0 44.10 ug/L 88 75-125
TestAmerica Nashville
Page 19 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 6010C - Metals (ICP) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-90119-A-14-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293404 Prep Batch: 292695
Arsenic <8.60 50.0 55.30 ug/L 111 75-125 8 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 436 2000 2365 ug/L 96 75-125 1 20
Cadmium <0.500 50.0 49.10 ug/L 98 75-125 1 20
Chromium <3.00 200 200.7 ug/L 100 75-125 2 20
Lead <2.00 L F1 50.0 10.50 F1 ug/L 21 75-125 7 20
Selenium <5.00 50.0 44.80 ug/L 90 75-125 7 20
Silver <3.00 50.0 45.50 ug/L 91 75-125 3 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-292946/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293540 Prep Batch: 292946
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/26/15 11:43 10/27/15 16:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-292946/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293540 Prep Batch: 292946
Mercury 1.00 0.9276 ug/L 93 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-292946/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293540 Prep Batch: 292946
Mercury 1.00 0.8912 ug/L 89 80-120 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-89887-G-4-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293540 Prep Batch: 292946
Mercury <0.100 F1 1.00 0.4496 F1 ug/L 45 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-89887-G-4-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 293540 Prep Batch: 292946
Mercury <0.100 F1 1.00 0.4197 F1 ug/L 42 75-125 7 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
Page 20 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
GC/MS VOA
Analysis Batch: 292542
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-90102-D-1 MS Matrix Spike Total/NA
Water 8260B490-90102-E-1 MSD Matrix Spike Duplicate Total/NA
Water 8260B490-90188-1 SW-01 OLD Total/NA
Water 8260B490-90188-2 SW-02 OLD Total/NA
Water 8260B490-90188-3 TripBlank Total/NA
Water 8260B490-90188-4 DW-01 OLD Total/NA
Water 8260BLCS 490-292542/3 Lab Control Sample Total/NA
Water 8260BMB 490-292542/7 Method Blank Total/NA
Metals
Prep Batch: 292695
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-90119-A-14-C MS Matrix Spike Total/NA
Water 3010A490-90119-A-14-D MSD Matrix Spike Duplicate Total/NA
Water 3010A490-90188-1 SW-01 OLD Total/NA
Water 3010A490-90188-2 SW-02 OLD Total/NA
Water 3010A490-90188-4 DW-01 OLD Total/NA
Water 3010ALCS 490-292695/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-292695/3-A Lab Control Sample Dup Total/NA
Water 3010AMB 490-292695/1-A Method Blank Total/NA
Prep Batch: 292946
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-89887-G-4-C MS Matrix Spike Total/NA
Water 7470A490-89887-G-4-D MSD Matrix Spike Duplicate Total/NA
Water 7470A490-90188-1 SW-01 OLD Total/NA
Water 7470A490-90188-2 SW-02 OLD Total/NA
Water 7470A490-90188-4 DW-01 OLD Total/NA
Water 7470ALCS 490-292946/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-292946/3-A Lab Control Sample Dup Total/NA
Water 7470AMB 490-292946/1-A Method Blank Total/NA
Analysis Batch: 293404
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010C 292695490-90119-A-14-C MS Matrix Spike Total/NA
Water 6010C 292695490-90119-A-14-D MSD Matrix Spike Duplicate Total/NA
Water 6010C 292695490-90188-1 SW-01 OLD Total/NA
Water 6010C 292695490-90188-2 SW-02 OLD Total/NA
Water 6010C 292695490-90188-4 DW-01 OLD Total/NA
Water 6010C 292695LCS 490-292695/2-A Lab Control Sample Total/NA
Water 6010C 292695LCSD 490-292695/3-A Lab Control Sample Dup Total/NA
Water 6010C 292695MB 490-292695/1-A Method Blank Total/NA
Analysis Batch: 293540
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 292946490-89887-G-4-C MS Matrix Spike Total/NA
Water 7470A 292946490-89887-G-4-D MSD Matrix Spike Duplicate Total/NA
Water 7470A 292946490-90188-1 SW-01 OLD Total/NA
Water 7470A 292946490-90188-2 SW-02 OLD Total/NA
TestAmerica Nashville
Page 21 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Metals (Continued)
Analysis Batch: 293540 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 292946490-90188-4 DW-01 OLD Total/NA
Water 7470A 292946LCS 490-292946/2-A Lab Control Sample Total/NA
Water 7470A 292946LCSD 490-292946/3-A Lab Control Sample Dup Total/NA
Water 7470A 292946MB 490-292946/1-A Method Blank Total/NA
Analysis Batch: 293630
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010C 292695490-90188-4 DW-01 OLD Total/NA
TestAmerica Nashville
Page 22 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90188-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: SW-01 OLD Lab Sample ID: 490-90188-1
Matrix: WaterDate Collected: 10/21/15 14:00
Date Received: 10/22/15 10:10
Analysis 8260B RP10/24/15 09:321 TAL NSH292542
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 292695 10/24/15 14:24 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 293404 10/27/15 20:16 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 292946 10/26/15 11:43 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 293540 10/27/15 17:21 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SW-02 OLD Lab Sample ID: 490-90188-2
Matrix: WaterDate Collected: 10/21/15 14:20
Date Received: 10/22/15 10:10
Analysis 8260B RP10/24/15 10:011 TAL NSH292542
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 292695 10/24/15 14:24 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 293404 10/27/15 20:20 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 292946 10/26/15 11:43 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 293540 10/27/15 17:29 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: TripBlank Lab Sample ID: 490-90188-3
Matrix: WaterDate Collected: 10/21/15 00:01
Date Received: 10/22/15 10:10
Analysis 8260B RP10/24/15 05:171 TAL NSH292542
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Client Sample ID: DW-01 OLD Lab Sample ID: 490-90188-4
Matrix: WaterDate Collected: 10/21/15 13:46
Date Received: 10/22/15 10:10
Analysis 8260B RP10/24/15 10:291 TAL NSH292542
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 292695 10/24/15 17:07 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 293404 10/27/15 20:24 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 292695 10/24/15 17:07 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 293630 10/28/15 13:58 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 292946 10/26/15 11:43 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 293540 10/27/15 17:32 NJB TAL NSHTotal/NA 30 mL 30 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 23 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Method Summary
TestAmerica Job ID: 490-90188-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010CMetals (ICP)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 24 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90188-1
Project/Site: Madison Co Closed Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-15
TestAmerica Nashville
Page 25 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 26 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 27 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-90188-1
Login Number: 90188
Question Answer Comment
Creator: Vest, Laura E
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.4.7
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
Page 28 of 28 10/30/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-90364-1
Client Project/Site: Madison Co Closed Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
11/6/2015 3:15:59 PM
Heather Baker, Project Manager I
[phone]
[e-mail]
Designee for
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
TestAmerica Job ID: 490-90364-1
Page 2 of 35 TestAmerica Nashville11/6/2015
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
1
2
3
4
5
6
7
8
9
10
11
12
13
Sample Summary
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-90364-1 MW-01 Old Water 10/22/15 09:45 10/23/15 10:00
490-90364-2 MW-02 Old Water 10/22/15 12:50 10/23/15 10:00
490-90364-3 MW-03 Old Water 10/22/15 12:16 10/23/15 10:00
490-90364-4 MW-04 Old Water 10/22/15 11:16 10/23/15 10:00
490-90364-5 BG-Spring Old Water 10/22/15 13:29 10/23/15 10:00
490-90364-6 Trip Blank Water 10/22/15 01:01 10/23/15 10:00
TestAmerica Nashville
Page 3 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90364-1
Project/Site: Madison Co Closed Landfill
Job ID: 490-90364-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-90364-1
Comments
No additional comments.
Receipt
The samples were received on 10/23/2015 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 1.4º C.
GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch
490-294861 recovered outside control limits for the following analytes: Bromoform and Trichlorofluoromethane. These analytes were
biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.
Method(s) 8260B: The method blank for analytical batch 490-294861 contained Methylene Chloride above the method detection limit. This
target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not
performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Definitions/Glossary
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
*LCS or LCSD is outside acceptance limits.
F1 MS and/or MSD Recovery is outside acceptance limits.
B Compound was found in the blank and sample.
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-1Client Sample ID: MW-01 Old
Matrix: WaterDate Collected: 10/22/15 09:45
Date Received: 10/23/15 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 11/02/15 18:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 11/02/15 18:22 1Acrylonitrile<0.500
1.00 0.200 ug/L 11/02/15 18:22 1Benzene0.603 J
1.00 0.150 ug/L 11/02/15 18:22 1Bromochloromethane<0.150
1.00 0.170 ug/L 11/02/15 18:22 1Bromodichloromethane<0.170
1.00 0.290 ug/L 11/02/15 18:22 1Bromoform<0.290 * F2
1.00 0.350 ug/L 11/02/15 18:22 1Bromomethane<0.350
50.0 2.64 ug/L 11/02/15 18:22 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 11/02/15 18:22 1Carbon disulfide <0.220
1.00 0.180 ug/L 11/02/15 18:22 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 11/02/15 18:22 1Chlorobenzene1.77 F2
1.00 0.360 ug/L 11/02/15 18:22 1Chloroethane0.810 J
1.00 0.230 ug/L 11/02/15 18:22 1Chloroform<0.230
1.00 0.360 ug/L 11/02/15 18:22 1Chloromethane<0.360
1.00 0.210 ug/L 11/02/15 18:22 1cis-1,2-Dichloroethene 1.97
1.00 0.170 ug/L 11/02/15 18:22 1cis-1,3-Dichloropropene <0.170 F2
1.00 0.250 ug/L 11/02/15 18:22 1Dibromochloromethane<0.250 F2
10.0 0.940 ug/L 11/02/15 18:22 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 11/02/15 18:22 11,2-Dibromoethane (EDB)<0.210 F2
1.00 0.450 ug/L 11/02/15 18:22 1Dibromomethane<0.450
1.00 0.190 ug/L 11/02/15 18:22 11,2-Dichlorobenzene 0.281 J F2
1.00 0.170 ug/L 11/02/15 18:22 11,4-Dichlorobenzene 3.12 F2
1.00 0.240 ug/L 11/02/15 18:22 11,1-Dichloroethane 0.674 J
1.00 0.200 ug/L 11/02/15 18:22 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 11/02/15 18:22 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 11/02/15 18:22 11,2-Dichloropropane 0.311 J
1.00 0.190 ug/L 11/02/15 18:22 1Ethylbenzene<0.190 F2
10.0 1.28 ug/L 11/02/15 18:22 12-Hexanone <1.28 F2
10.0 1.50 ug/L 11/02/15 18:22 1Iodomethane<1.50
5.00 0.220 ug/L 11/02/15 18:22 1Methylene Chloride <0.220
10.0 0.810 ug/L 11/02/15 18:22 14-Methyl-2-pentanone (MIBK)<0.810 F2
1.00 0.280 ug/L 11/02/15 18:22 1Styrene<0.280
1.00 0.150 ug/L 11/02/15 18:22 11,1,1,2-Tetrachloroethane <0.150 F2
1.00 0.190 ug/L 11/02/15 18:22 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 11/02/15 18:22 1Tetrachloroethene<0.140 F2
10.0 0.820 ug/L 11/02/15 18:22 1Tetrahydrofuran<0.820 F2
1.00 0.170 ug/L 11/02/15 18:22 1Toluene<0.170 F2
5.00 0.460 ug/L 11/02/15 18:22 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 11/02/15 18:22 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 11/02/15 18:22 1trans-1,3-Dichloropropene <0.170 F2
1.00 0.190 ug/L 11/02/15 18:22 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 11/02/15 18:22 11,1,2-Trichloroethane <0.190 F2
1.00 0.200 ug/L 11/02/15 18:22 1Trichloroethene<0.200
1.00 0.210 ug/L 11/02/15 18:22 1Trichlorofluoromethane<0.210 * F1
1.00 0.230 ug/L 11/02/15 18:22 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 11/02/15 18:22 1Vinyl acetate <1.71 F2
1.00 0.180 ug/L 11/02/15 18:22 1Vinyl chloride 0.324 J
3.00 0.580 ug/L 11/02/15 18:22 1Xylenes, Total <0.580 F2
TestAmerica Nashville
Page 6 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-1Client Sample ID: MW-01 Old
Matrix: WaterDate Collected: 10/22/15 09:45
Date Received: 10/23/15 10:00
4-Bromofluorobenzene (Surr)99 70-130 11/02/15 18:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 11/02/15 18:22 170-130
1,2-Dichloroethane-d4 (Surr)99 11/02/15 18:22 170-130
Toluene-d8 (Surr)96 11/02/15 18:22 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/26/15 15:40 11/05/15 20:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:16 1Barium395
1.00 0.500 ug/L 10/26/15 15:40 11/05/15 20:16 1Cadmium<0.500
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:16 1Chromium4.90 J
5.00 2.00 ug/L 10/26/15 15:40 11/05/15 20:16 1Lead11.0
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:16 1Selenium<5.00
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:16 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:23 10/30/15 18:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 7 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-2Client Sample ID: MW-02 Old
Matrix: WaterDate Collected: 10/22/15 12:50
Date Received: 10/23/15 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 11/02/15 18:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 11/02/15 18:48 1Acrylonitrile<0.500
1.00 0.200 ug/L 11/02/15 18:48 1Benzene<0.200
1.00 0.150 ug/L 11/02/15 18:48 1Bromochloromethane<0.150
1.00 0.170 ug/L 11/02/15 18:48 1Bromodichloromethane<0.170
1.00 0.290 ug/L 11/02/15 18:48 1Bromoform<0.290 *
1.00 0.350 ug/L 11/02/15 18:48 1Bromomethane<0.350
50.0 2.64 ug/L 11/02/15 18:48 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 11/02/15 18:48 1Carbon disulfide <0.220
1.00 0.180 ug/L 11/02/15 18:48 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 11/02/15 18:48 1Chlorobenzene<0.180
1.00 0.360 ug/L 11/02/15 18:48 1Chloroethane<0.360
1.00 0.230 ug/L 11/02/15 18:48 1Chloroform<0.230
1.00 0.360 ug/L 11/02/15 18:48 1Chloromethane<0.360
1.00 0.210 ug/L 11/02/15 18:48 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 11/02/15 18:48 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 11/02/15 18:48 1Dibromochloromethane<0.250
10.0 0.940 ug/L 11/02/15 18:48 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 11/02/15 18:48 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 11/02/15 18:48 1Dibromomethane<0.450
1.00 0.190 ug/L 11/02/15 18:48 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 11/02/15 18:48 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 11/02/15 18:48 11,1-Dichloroethane 0.612 J
1.00 0.200 ug/L 11/02/15 18:48 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 11/02/15 18:48 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 11/02/15 18:48 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 11/02/15 18:48 1Ethylbenzene<0.190
10.0 1.28 ug/L 11/02/15 18:48 12-Hexanone <1.28
10.0 1.50 ug/L 11/02/15 18:48 1Iodomethane<1.50
5.00 0.220 ug/L 11/02/15 18:48 1Methylene Chloride <0.220
10.0 0.810 ug/L 11/02/15 18:48 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 11/02/15 18:48 1Styrene<0.280
1.00 0.150 ug/L 11/02/15 18:48 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 11/02/15 18:48 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 11/02/15 18:48 1Tetrachloroethene<0.140
10.0 0.820 ug/L 11/02/15 18:48 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 11/02/15 18:48 1Toluene<0.170
5.00 0.460 ug/L 11/02/15 18:48 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 11/02/15 18:48 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 11/02/15 18:48 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 11/02/15 18:48 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 11/02/15 18:48 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 11/02/15 18:48 1Trichloroethene<0.200
1.00 0.210 ug/L 11/02/15 18:48 1Trichlorofluoromethane<0.210 *
1.00 0.230 ug/L 11/02/15 18:48 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 11/02/15 18:48 1Vinyl acetate <1.71
1.00 0.180 ug/L 11/02/15 18:48 1Vinyl chloride <0.180
3.00 0.580 ug/L 11/02/15 18:48 1Xylenes, Total <0.580
TestAmerica Nashville
Page 8 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-2Client Sample ID: MW-02 Old
Matrix: WaterDate Collected: 10/22/15 12:50
Date Received: 10/23/15 10:00
4-Bromofluorobenzene (Surr)98 70-130 11/02/15 18:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 11/02/15 18:48 170-130
1,2-Dichloroethane-d4 (Surr)99 11/02/15 18:48 170-130
Toluene-d8 (Surr)95 11/02/15 18:48 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/26/15 15:40 11/05/15 20:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:20 1Barium46.7
1.00 0.500 ug/L 10/26/15 15:40 11/05/15 20:20 1Cadmium<0.500
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:20 1Chromium<3.00
5.00 2.00 ug/L 10/26/15 15:40 11/05/15 20:20 1Lead4.80 J
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:20 1Selenium<5.00
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:20 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:38 10/29/15 16:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 9 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-3Client Sample ID: MW-03 Old
Matrix: WaterDate Collected: 10/22/15 12:16
Date Received: 10/23/15 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 3.04 J 25.0 2.66 ug/L 11/02/15 19:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 11/02/15 19:14 1Acrylonitrile<0.500
1.00 0.200 ug/L 11/02/15 19:14 1Benzene0.749 J
1.00 0.150 ug/L 11/02/15 19:14 1Bromochloromethane<0.150
1.00 0.170 ug/L 11/02/15 19:14 1Bromodichloromethane<0.170
1.00 0.290 ug/L 11/02/15 19:14 1Bromoform<0.290 *
1.00 0.350 ug/L 11/02/15 19:14 1Bromomethane<0.350
50.0 2.64 ug/L 11/02/15 19:14 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 11/02/15 19:14 1Carbon disulfide <0.220
1.00 0.180 ug/L 11/02/15 19:14 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 11/02/15 19:14 1Chlorobenzene3.98
1.00 0.360 ug/L 11/02/15 19:14 1Chloroethane0.865 J
1.00 0.230 ug/L 11/02/15 19:14 1Chloroform<0.230
1.00 0.360 ug/L 11/02/15 19:14 1Chloromethane<0.360
1.00 0.210 ug/L 11/02/15 19:14 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 11/02/15 19:14 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 11/02/15 19:14 1Dibromochloromethane<0.250
10.0 0.940 ug/L 11/02/15 19:14 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 11/02/15 19:14 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 11/02/15 19:14 1Dibromomethane<0.450
1.00 0.190 ug/L 11/02/15 19:14 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 11/02/15 19:14 11,4-Dichlorobenzene 2.69
1.00 0.240 ug/L 11/02/15 19:14 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 11/02/15 19:14 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 11/02/15 19:14 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 11/02/15 19:14 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 11/02/15 19:14 1Ethylbenzene0.210 J
10.0 1.28 ug/L 11/02/15 19:14 12-Hexanone <1.28
10.0 1.50 ug/L 11/02/15 19:14 1Iodomethane<1.50
5.00 0.220 ug/L 11/02/15 19:14 1Methylene Chloride <0.220
10.0 0.810 ug/L 11/02/15 19:14 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 11/02/15 19:14 1Styrene<0.280
1.00 0.150 ug/L 11/02/15 19:14 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 11/02/15 19:14 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 11/02/15 19:14 1Tetrachloroethene<0.140
10.0 0.820 ug/L 11/02/15 19:14 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 11/02/15 19:14 1Toluene<0.170
5.00 0.460 ug/L 11/02/15 19:14 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 11/02/15 19:14 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 11/02/15 19:14 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 11/02/15 19:14 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 11/02/15 19:14 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 11/02/15 19:14 1Trichloroethene<0.200
1.00 0.210 ug/L 11/02/15 19:14 1Trichlorofluoromethane<0.210 *
1.00 0.230 ug/L 11/02/15 19:14 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 11/02/15 19:14 1Vinyl acetate <1.71
1.00 0.180 ug/L 11/02/15 19:14 1Vinyl chloride <0.180
3.00 0.580 ug/L 11/02/15 19:14 1Xylenes, Total 1.21 J
TestAmerica Nashville
Page 10 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-3Client Sample ID: MW-03 Old
Matrix: WaterDate Collected: 10/22/15 12:16
Date Received: 10/23/15 10:00
4-Bromofluorobenzene (Surr)99 70-130 11/02/15 19:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 11/02/15 19:14 170-130
1,2-Dichloroethane-d4 (Surr)100 11/02/15 19:14 170-130
Toluene-d8 (Surr)95 11/02/15 19:14 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/26/15 15:40 11/05/15 20:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:25 1Barium887
1.00 0.500 ug/L 10/26/15 15:40 11/05/15 20:25 1Cadmium<0.500
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:25 1Chromium<3.00
5.00 2.00 ug/L 10/26/15 15:40 11/05/15 20:25 1Lead15.8
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:25 1Selenium5.70 J
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:25 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:38 10/29/15 16:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 11 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-4Client Sample ID: MW-04 Old
Matrix: WaterDate Collected: 10/22/15 11:16
Date Received: 10/23/15 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.65 J 25.0 2.66 ug/L 11/02/15 19:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 11/02/15 19:41 1Acrylonitrile<0.500
1.00 0.200 ug/L 11/02/15 19:41 1Benzene0.354 J
1.00 0.150 ug/L 11/02/15 19:41 1Bromochloromethane<0.150
1.00 0.170 ug/L 11/02/15 19:41 1Bromodichloromethane<0.170
1.00 0.290 ug/L 11/02/15 19:41 1Bromoform<0.290 *
1.00 0.350 ug/L 11/02/15 19:41 1Bromomethane<0.350
50.0 2.64 ug/L 11/02/15 19:41 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 11/02/15 19:41 1Carbon disulfide <0.220
1.00 0.180 ug/L 11/02/15 19:41 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 11/02/15 19:41 1Chlorobenzene1.72
1.00 0.360 ug/L 11/02/15 19:41 1Chloroethane0.576 J
1.00 0.230 ug/L 11/02/15 19:41 1Chloroform<0.230
1.00 0.360 ug/L 11/02/15 19:41 1Chloromethane<0.360
1.00 0.210 ug/L 11/02/15 19:41 1cis-1,2-Dichloroethene 0.841 J
1.00 0.170 ug/L 11/02/15 19:41 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 11/02/15 19:41 1Dibromochloromethane<0.250
10.0 0.940 ug/L 11/02/15 19:41 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 11/02/15 19:41 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 11/02/15 19:41 1Dibromomethane<0.450
1.00 0.190 ug/L 11/02/15 19:41 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 11/02/15 19:41 11,4-Dichlorobenzene 0.878 J
1.00 0.240 ug/L 11/02/15 19:41 11,1-Dichloroethane 0.540 J
1.00 0.200 ug/L 11/02/15 19:41 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 11/02/15 19:41 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 11/02/15 19:41 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 11/02/15 19:41 1Ethylbenzene0.357 J
10.0 1.28 ug/L 11/02/15 19:41 12-Hexanone <1.28
10.0 1.50 ug/L 11/02/15 19:41 1Iodomethane<1.50
5.00 0.220 ug/L 11/02/15 19:41 1Methylene Chloride <0.220
10.0 0.810 ug/L 11/02/15 19:41 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 11/02/15 19:41 1Styrene<0.280
1.00 0.150 ug/L 11/02/15 19:41 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 11/02/15 19:41 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 11/02/15 19:41 1Tetrachloroethene<0.140
10.0 0.820 ug/L 11/02/15 19:41 1Tetrahydrofuran2.37 J
1.00 0.170 ug/L 11/02/15 19:41 1Toluene<0.170
5.00 0.460 ug/L 11/02/15 19:41 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 11/02/15 19:41 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 11/02/15 19:41 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 11/02/15 19:41 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 11/02/15 19:41 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 11/02/15 19:41 1Trichloroethene<0.200
1.00 0.210 ug/L 11/02/15 19:41 1Trichlorofluoromethane<0.210 *
1.00 0.230 ug/L 11/02/15 19:41 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 11/02/15 19:41 1Vinyl acetate <1.71
1.00 0.180 ug/L 11/02/15 19:41 1Vinyl chloride <0.180
3.00 0.580 ug/L 11/02/15 19:41 1Xylenes, Total 2.26 J
TestAmerica Nashville
Page 12 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-4Client Sample ID: MW-04 Old
Matrix: WaterDate Collected: 10/22/15 11:16
Date Received: 10/23/15 10:00
4-Bromofluorobenzene (Surr)100 70-130 11/02/15 19:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 11/02/15 19:41 170-130
1,2-Dichloroethane-d4 (Surr)99 11/02/15 19:41 170-130
Toluene-d8 (Surr)95 11/02/15 19:41 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/26/15 15:40 11/05/15 20:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:29 1Barium872
1.00 0.500 ug/L 10/26/15 15:40 11/05/15 20:29 1Cadmium<0.500
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:29 1Chromium<3.00
5.00 2.00 ug/L 10/26/15 15:40 11/05/15 20:29 1Lead8.40
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:29 1Selenium5.80 J
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:29 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:38 10/30/15 18:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 13 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-5Client Sample ID: BG-Spring Old
Matrix: WaterDate Collected: 10/22/15 13:29
Date Received: 10/23/15 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 11/02/15 20:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 11/02/15 20:08 1Acrylonitrile<0.500
1.00 0.200 ug/L 11/02/15 20:08 1Benzene<0.200
1.00 0.150 ug/L 11/02/15 20:08 1Bromochloromethane<0.150
1.00 0.170 ug/L 11/02/15 20:08 1Bromodichloromethane<0.170
1.00 0.290 ug/L 11/02/15 20:08 1Bromoform<0.290 *
1.00 0.350 ug/L 11/02/15 20:08 1Bromomethane<0.350
50.0 2.64 ug/L 11/02/15 20:08 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 11/02/15 20:08 1Carbon disulfide <0.220
1.00 0.180 ug/L 11/02/15 20:08 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 11/02/15 20:08 1Chlorobenzene<0.180
1.00 0.360 ug/L 11/02/15 20:08 1Chloroethane<0.360
1.00 0.230 ug/L 11/02/15 20:08 1Chloroform<0.230
1.00 0.360 ug/L 11/02/15 20:08 1Chloromethane<0.360
1.00 0.210 ug/L 11/02/15 20:08 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 11/02/15 20:08 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 11/02/15 20:08 1Dibromochloromethane<0.250
10.0 0.940 ug/L 11/02/15 20:08 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 11/02/15 20:08 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 11/02/15 20:08 1Dibromomethane<0.450
1.00 0.190 ug/L 11/02/15 20:08 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 11/02/15 20:08 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 11/02/15 20:08 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 11/02/15 20:08 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 11/02/15 20:08 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 11/02/15 20:08 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 11/02/15 20:08 1Ethylbenzene<0.190
10.0 1.28 ug/L 11/02/15 20:08 12-Hexanone <1.28
10.0 1.50 ug/L 11/02/15 20:08 1Iodomethane<1.50
5.00 0.220 ug/L 11/02/15 20:08 1Methylene Chloride <0.220
10.0 0.810 ug/L 11/02/15 20:08 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 11/02/15 20:08 1Styrene<0.280
1.00 0.150 ug/L 11/02/15 20:08 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 11/02/15 20:08 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 11/02/15 20:08 1Tetrachloroethene<0.140
10.0 0.820 ug/L 11/02/15 20:08 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 11/02/15 20:08 1Toluene<0.170
5.00 0.460 ug/L 11/02/15 20:08 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 11/02/15 20:08 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 11/02/15 20:08 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 11/02/15 20:08 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 11/02/15 20:08 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 11/02/15 20:08 1Trichloroethene<0.200
1.00 0.210 ug/L 11/02/15 20:08 1Trichlorofluoromethane<0.210 *
1.00 0.230 ug/L 11/02/15 20:08 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 11/02/15 20:08 1Vinyl acetate <1.71
1.00 0.180 ug/L 11/02/15 20:08 1Vinyl chloride <0.180
3.00 0.580 ug/L 11/02/15 20:08 1Xylenes, Total <0.580
TestAmerica Nashville
Page 14 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-5Client Sample ID: BG-Spring Old
Matrix: WaterDate Collected: 10/22/15 13:29
Date Received: 10/23/15 10:00
4-Bromofluorobenzene (Surr)100 70-130 11/02/15 20:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)97 11/02/15 20:08 170-130
1,2-Dichloroethane-d4 (Surr)98 11/02/15 20:08 170-130
Toluene-d8 (Surr)96 11/02/15 20:08 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/26/15 15:40 11/05/15 20:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:34 1Barium430
1.00 0.500 ug/L 10/26/15 15:40 11/05/15 20:34 1Cadmium<0.500
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:34 1Chromium59.7
5.00 2.00 ug/L 10/26/15 15:40 11/05/15 20:34 1Lead26.7
10.0 5.00 ug/L 10/26/15 15:40 11/05/15 20:34 1Selenium<5.00
5.00 3.00 ug/L 10/26/15 15:40 11/05/15 20:34 1Silver<3.00
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:38 10/30/15 18:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 15 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-6Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/22/15 01:01
Date Received: 10/23/15 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 10.2 J 25.0 2.66 ug/L 11/02/15 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 11/02/15 17:55 1Acrylonitrile<0.500
1.00 0.200 ug/L 11/02/15 17:55 1Benzene<0.200
1.00 0.150 ug/L 11/02/15 17:55 1Bromochloromethane<0.150
1.00 0.170 ug/L 11/02/15 17:55 1Bromodichloromethane<0.170
1.00 0.290 ug/L 11/02/15 17:55 1Bromoform<0.290 *
1.00 0.350 ug/L 11/02/15 17:55 1Bromomethane<0.350
50.0 2.64 ug/L 11/02/15 17:55 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 11/02/15 17:55 1Carbon disulfide <0.220
1.00 0.180 ug/L 11/02/15 17:55 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 11/02/15 17:55 1Chlorobenzene<0.180
1.00 0.360 ug/L 11/02/15 17:55 1Chloroethane<0.360
1.00 0.230 ug/L 11/02/15 17:55 1Chloroform<0.230
1.00 0.360 ug/L 11/02/15 17:55 1Chloromethane<0.360
1.00 0.210 ug/L 11/02/15 17:55 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 11/02/15 17:55 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 11/02/15 17:55 1Dibromochloromethane<0.250
10.0 0.940 ug/L 11/02/15 17:55 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 11/02/15 17:55 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 11/02/15 17:55 1Dibromomethane<0.450
1.00 0.190 ug/L 11/02/15 17:55 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 11/02/15 17:55 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 11/02/15 17:55 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 11/02/15 17:55 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 11/02/15 17:55 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 11/02/15 17:55 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 11/02/15 17:55 1Ethylbenzene<0.190
10.0 1.28 ug/L 11/02/15 17:55 12-Hexanone <1.28
10.0 1.50 ug/L 11/02/15 17:55 1Iodomethane<1.50
5.00 0.220 ug/L 11/02/15 17:55 1Methylene Chloride 1.45 J B
10.0 0.810 ug/L 11/02/15 17:55 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 11/02/15 17:55 1Styrene<0.280
1.00 0.150 ug/L 11/02/15 17:55 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 11/02/15 17:55 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 11/02/15 17:55 1Tetrachloroethene<0.140
10.0 0.820 ug/L 11/02/15 17:55 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 11/02/15 17:55 1Toluene<0.170
5.00 0.460 ug/L 11/02/15 17:55 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 11/02/15 17:55 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 11/02/15 17:55 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 11/02/15 17:55 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 11/02/15 17:55 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 11/02/15 17:55 1Trichloroethene<0.200
1.00 0.210 ug/L 11/02/15 17:55 1Trichlorofluoromethane<0.210 *
1.00 0.230 ug/L 11/02/15 17:55 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 11/02/15 17:55 1Vinyl acetate <1.71
1.00 0.180 ug/L 11/02/15 17:55 1Vinyl chloride <0.180
3.00 0.580 ug/L 11/02/15 17:55 1Xylenes, Total <0.580
TestAmerica Nashville
Page 16 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-90364-6Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/22/15 01:01
Date Received: 10/23/15 10:00
4-Bromofluorobenzene (Surr)99 70-130 11/02/15 17:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 11/02/15 17:55 170-130
1,2-Dichloroethane-d4 (Surr)99 11/02/15 17:55 170-130
Toluene-d8 (Surr)95 11/02/15 17:55 170-130
TestAmerica Nashville
Page 17 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-294861/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
RL MDL
Acetone <2.66 25.0 2.66 ug/L 11/02/15 14:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 11/02/15 14:21 1Acrylonitrile
<0.200 0.2001.00 ug/L 11/02/15 14:21 1Benzene
<0.150 0.1501.00 ug/L 11/02/15 14:21 1Bromochloromethane
<0.170 0.1701.00 ug/L 11/02/15 14:21 1Bromodichloromethane
<0.290 0.2901.00 ug/L 11/02/15 14:21 1Bromoform
<0.350 0.3501.00 ug/L 11/02/15 14:21 1Bromomethane
<2.64 2.6450.0 ug/L 11/02/15 14:21 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 11/02/15 14:21 1Carbon disulfide
<0.180 0.1801.00 ug/L 11/02/15 14:21 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 11/02/15 14:21 1Chlorobenzene
<0.360 0.3601.00 ug/L 11/02/15 14:21 1Chloroethane
<0.230 0.2301.00 ug/L 11/02/15 14:21 1Chloroform
<0.360 0.3601.00 ug/L 11/02/15 14:21 1Chloromethane
<0.210 0.2101.00 ug/L 11/02/15 14:21 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 11/02/15 14:21 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 11/02/15 14:21 1Dibromochloromethane
<0.940 0.94010.0 ug/L 11/02/15 14:21 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 11/02/15 14:21 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 11/02/15 14:21 1Dibromomethane
<0.190 0.1901.00 ug/L 11/02/15 14:21 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 11/02/15 14:21 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 11/02/15 14:21 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 11/02/15 14:21 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 11/02/15 14:21 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 11/02/15 14:21 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 11/02/15 14:21 1Ethylbenzene
<1.28 1.2810.0 ug/L 11/02/15 14:21 12-Hexanone
<1.50 1.5010.0 ug/L 11/02/15 14:21 1Iodomethane
0.3647 J 0.2205.00 ug/L 11/02/15 14:21 1Methylene Chloride
<0.810 0.81010.0 ug/L 11/02/15 14:21 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 11/02/15 14:21 1Styrene
<0.150 0.1501.00 ug/L 11/02/15 14:21 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 11/02/15 14:21 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 11/02/15 14:21 1Tetrachloroethene
<0.820 0.82010.0 ug/L 11/02/15 14:21 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 11/02/15 14:21 1Toluene
<0.460 0.4605.00 ug/L 11/02/15 14:21 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 11/02/15 14:21 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 11/02/15 14:21 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 11/02/15 14:21 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 11/02/15 14:21 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 11/02/15 14:21 1Trichloroethene
<0.210 0.2101.00 ug/L 11/02/15 14:21 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 11/02/15 14:21 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 11/02/15 14:21 1Vinyl acetate
<0.180 0.1801.00 ug/L 11/02/15 14:21 1Vinyl chloride
<0.580 0.5803.00 ug/L 11/02/15 14:21 1Xylenes, Total
TestAmerica Nashville
Page 18 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
4-Bromofluorobenzene (Surr)98 70-130 11/02/15 14:21 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 11/02/15 14:21 1Dibromofluoromethane (Surr)70-130
98 11/02/15 14:21 11,2-Dichloroethane-d4 (Surr)70-130
95 11/02/15 14:21 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-294861/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
Acetone 250 286.8 ug/L 115 54-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 545.2 ug/L 109 61-140
Benzene 50.0 55.29 ug/L 111 80-121
Bromochloromethane 50.0 54.04 ug/L 108 78-129
Bromodichloromethane 50.0 56.36 ug/L 113 75-129
Bromoform 50.0 69.92 ug/L 140 46-145
Bromomethane 50.0 58.42 ug/L 117 41-150
2-Butanone (MEK)250 303.9 ug/L 122 62-133
Carbon disulfide 50.0 53.95 ug/L 108 77-126
Carbon tetrachloride 50.0 58.74 ug/L 117 64-147
Chlorobenzene 50.0 53.55 ug/L 107 80-120
Chloroethane 50.0 56.53 ug/L 113 72-120
Chloroform 50.0 54.57 ug/L 109 73-129
Chloromethane 50.0 48.24 ug/L 96 12-150
cis-1,2-Dichloroethene 50.0 54.02 ug/L 108 76-125
cis-1,3-Dichloropropene 50.0 55.76 ug/L 112 74-140
Dibromochloromethane 50.0 59.01 ug/L 118 69-133
1,2-Dibromo-3-Chloropropane 50.0 53.59 ug/L 107 54-125
1,2-Dibromoethane (EDB)50.0 55.89 ug/L 112 80-129
Dibromomethane 50.0 54.40 ug/L 109 71-125
1,2-Dichlorobenzene 50.0 53.51 ug/L 107 80-121
1,4-Dichlorobenzene 50.0 51.94 ug/L 104 80-120
1,1-Dichloroethane 50.0 52.41 ug/L 105 78-125
1,2-Dichloroethane 50.0 52.92 ug/L 106 77-121
1,1-Dichloroethene 50.0 57.85 ug/L 116 79-124
1,2-Dichloropropane 50.0 53.00 ug/L 106 75-120
Ethylbenzene 50.0 55.10 ug/L 110 80-130
2-Hexanone 250 289.2 ug/L 116 60-142
Iodomethane 50.0 52.33 ug/L 105 40-150
Methylene Chloride 50.0 52.27 ug/L 105 79-123
4-Methyl-2-pentanone (MIBK)250 276.4 ug/L 111 60-137
Styrene 50.0 54.61 ug/L 109 80-127
1,1,1,2-Tetrachloroethane 50.0 56.93 ug/L 114 74-135
1,1,2,2-Tetrachloroethane 50.0 54.43 ug/L 109 69-131
Tetrachloroethene 50.0 54.60 ug/L 109 80-126
Tetrahydrofuran 100 110.2 ug/L 110 51-124
Toluene 50.0 54.65 ug/L 109 80-126
trans-1,4-Dichloro-2-butene 50.0 54.23 ug/L 108 41-147
trans-1,2-Dichloroethene 50.0 53.41 ug/L 107 79-126
trans-1,3-Dichloropropene 50.0 58.28 ug/L 117 63-134
1,1,1-Trichloroethane 50.0 56.47 ug/L 113 78-135
1,1,2-Trichloroethane 50.0 54.52 ug/L 109 80-124
Trichloroethene 50.0 55.04 ug/L 110 80-123
Trichlorofluoromethane 50.0 63.51 *ug/L 127 65-124
TestAmerica Nashville
Page 19 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-294861/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
1,2,3-Trichloropropane 50.0 53.06 ug/L 106 70-131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 100 123.1 ug/L 123 54-139
Vinyl chloride 50.0 55.11 ug/L 110 68-120
Xylenes, Total 100 107.6 ug/L 108 80-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-294861/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
Acetone 250 325.8 ug/L 130 54-145 13 21
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 574.0 ug/L 115 61-140 5 18
Benzene 50.0 56.81 ug/L 114 80-121 3 17
Bromochloromethane 50.0 56.15 ug/L 112 78-129 4 17
Bromodichloromethane 50.0 58.81 ug/L 118 75-129 4 18
Bromoform 50.0 73.52 *ug/L 147 46-145 5 16
Bromomethane 50.0 57.10 ug/L 114 41-150 2 50
2-Butanone (MEK)250 319.9 ug/L 128 62-133 5 19
Carbon disulfide 50.0 54.39 ug/L 109 77-126 1 21
Carbon tetrachloride 50.0 61.76 ug/L 124 64-147 5 19
Chlorobenzene 50.0 54.63 ug/L 109 80-120 2 14
Chloroethane 50.0 58.23 ug/L 116 72-120 3 20
Chloroform 50.0 56.20 ug/L 112 73-129 3 18
Chloromethane 50.0 48.32 ug/L 97 12-150 0 31
cis-1,2-Dichloroethene 50.0 56.02 ug/L 112 76-125 4 17
cis-1,3-Dichloropropene 50.0 57.57 ug/L 115 74-140 3 15
Dibromochloromethane 50.0 61.75 ug/L 124 69-133 5 15
1,2-Dibromo-3-Chloropropane 50.0 58.17 ug/L 116 54-125 8 24
1,2-Dibromoethane (EDB)50.0 58.59 ug/L 117 80-129 5 15
Dibromomethane 50.0 57.93 ug/L 116 71-125 6 16
1,2-Dichlorobenzene 50.0 55.69 ug/L 111 80-121 4 15
1,4-Dichlorobenzene 50.0 54.24 ug/L 108 80-120 4 15
1,1-Dichloroethane 50.0 55.84 ug/L 112 78-125 6 17
1,2-Dichloroethane 50.0 55.87 ug/L 112 77-121 5 17
1,1-Dichloroethene 50.0 58.30 ug/L 117 79-124 1 17
1,2-Dichloropropane 50.0 54.86 ug/L 110 75-120 3 17
Ethylbenzene 50.0 56.06 ug/L 112 80-130 2 15
2-Hexanone 250 309.0 ug/L 124 60-142 7 15
Iodomethane 50.0 53.40 ug/L 107 40-150 2 23
Methylene Chloride 50.0 54.17 ug/L 108 79-123 4 17
4-Methyl-2-pentanone (MIBK)250 294.9 ug/L 118 60-137 6 17
Styrene 50.0 56.27 ug/L 113 80-127 3 24
TestAmerica Nashville
Page 20 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-294861/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
1,1,1,2-Tetrachloroethane 50.0 58.46 ug/L 117 74-135 3 16
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 50.0 57.38 ug/L 115 69-131 5 20
Tetrachloroethene 50.0 55.34 ug/L 111 80-126 1 16
Tetrahydrofuran 100 112.9 ug/L 113 51-124 2 18
Toluene 50.0 55.96 ug/L 112 80-126 2 15
trans-1,4-Dichloro-2-butene 50.0 57.46 ug/L 115 41-147 6 26
trans-1,2-Dichloroethene 50.0 55.21 ug/L 110 79-126 3 16
trans-1,3-Dichloropropene 50.0 60.11 ug/L 120 63-134 3 14
1,1,1-Trichloroethane 50.0 57.77 ug/L 116 78-135 2 17
1,1,2-Trichloroethane 50.0 56.86 ug/L 114 80-124 4 15
Trichloroethene 50.0 56.29 ug/L 113 80-123 2 17
Trichlorofluoromethane 50.0 65.25 *ug/L 131 65-124 3 18
1,2,3-Trichloropropane 50.0 57.48 ug/L 115 70-131 8 19
Vinyl acetate 100 126.0 ug/L 126 54-139 2 21
Vinyl chloride 50.0 56.47 ug/L 113 68-120 2 17
Xylenes, Total 100 110.2 ug/L 110 80-132 2 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
96Toluene-d8 (Surr)70 -130
Client Sample ID: MW-01 OldLab Sample ID: 490-90364-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
Acetone <2.66 250 278.0 ug/L 111 45-141
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 495.8 ug/L 99 50-148
Benzene 0.603 J 50.0 56.96 ug/L 113 75-133
Bromochloromethane <0.150 50.0 54.89 ug/L 110 67-139
Bromodichloromethane <0.170 50.0 56.11 ug/L 112 70-140
Bromoform <0.290 * F2 50.0 66.42 ug/L 133 42-147
Bromomethane <0.350 50.0 62.44 ug/L 125 16-163
2-Butanone (MEK)<2.64 250 282.0 ug/L 113 50-138
Carbon disulfide <0.220 50.0 56.78 ug/L 114 48-152
Carbon tetrachloride <0.180 50.0 64.18 ug/L 128 62-164
Chlorobenzene 1.77 F2 50.0 56.01 ug/L 108 80-129
Chloroethane 0.810 J 50.0 59.56 ug/L 118 58-137
Chloroform <0.230 50.0 55.26 ug/L 111 66-138
Chloromethane <0.360 50.0 52.06 ug/L 104 10-169
cis-1,2-Dichloroethene 1.97 50.0 56.57 ug/L 109 68-138
cis-1,3-Dichloropropene <0.170 F2 50.0 54.95 ug/L 110 71-141
Dibromochloromethane <0.250 F2 50.0 58.54 ug/L 117 66-140
1,2-Dibromo-3-Chloropropane <0.940 50.0 51.60 ug/L 103 52-126
1,2-Dibromoethane (EDB)<0.210 F2 50.0 54.62 ug/L 109 75-137
Dibromomethane <0.450 50.0 55.43 ug/L 111 58-140
TestAmerica Nashville
Page 21 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-01 OldLab Sample ID: 490-90364-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
1,2-Dichlorobenzene 0.281 J F2 50.0 53.01 ug/L 105 79-128
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene 3.12 F2 50.0 55.93 ug/L 106 78-126
1,1-Dichloroethane 0.674 J 50.0 53.33 ug/L 105 71-139
1,2-Dichloroethane <0.200 50.0 52.66 ug/L 105 64-136
1,1-Dichloroethene <0.250 50.0 61.67 ug/L 123 70-142
1,2-Dichloropropane 0.311 J 50.0 52.72 ug/L 105 67-131
Ethylbenzene <0.190 F2 50.0 54.97 ug/L 110 79-139
2-Hexanone <1.28 F2 250 268.4 ug/L 107 50-150
Iodomethane <1.50 50.0 61.77 ug/L 124 34-191
Methylene Chloride <0.220 50.0 52.52 ug/L 105 64-139
4-Methyl-2-pentanone (MIBK)<0.810 F2 250 266.0 ug/L 106 50-147
Styrene <0.280 50.0 53.86 ug/L 108 61-148
1,1,1,2-Tetrachloroethane <0.150 F2 50.0 56.41 ug/L 113 73-141
1,1,2,2-Tetrachloroethane <0.190 50.0 52.71 ug/L 105 56-143
Tetrachloroethene <0.140 F2 50.0 59.14 ug/L 118 72-145
Tetrahydrofuran <0.820 F2 100 106.0 ug/L 106 34-133
Toluene <0.170 F2 50.0 55.81 ug/L 112 75-136
trans-1,4-Dichloro-2-butene <0.460 50.0 50.09 ug/L 100 29-156
trans-1,2-Dichloroethene <0.230 50.0 55.55 ug/L 111 66-143
trans-1,3-Dichloropropene <0.170 F2 50.0 55.63 ug/L 111 59-135
1,1,1-Trichloroethane <0.190 50.0 58.97 ug/L 118 76-149
1,1,2-Trichloroethane <0.190 F2 50.0 54.39 ug/L 109 74-134
Trichloroethene <0.200 50.0 58.73 ug/L 117 73-144
Trichlorofluoromethane <0.210 * F1 50.0 72.42 F1 ug/L 145 58-139
1,2,3-Trichloropropane <0.230 50.0 52.48 ug/L 105 53-144
Vinyl acetate <1.71 F2 100 118.1 ug/L 118 37-154
Vinyl chloride 0.324 J 50.0 61.11 ug/L 122 56-129
Xylenes, Total <0.580 F2 100 108.1 ug/L 108 74-141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
MS MS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
97Toluene-d8 (Surr)70 -130
Client Sample ID: MW-01 OldLab Sample ID: 490-90364-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
Acetone <2.66 250 229.8 ug/L 92 45-141 19 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 430.2 ug/L 86 50-148 14 18
Benzene 0.603 J 50.0 49.17 ug/L 97 75-133 15 17
Bromochloromethane <0.150 50.0 47.21 ug/L 94 67-139 15 17
Bromodichloromethane <0.170 50.0 47.53 ug/L 95 70-140 17 18
Bromoform <0.290 * F2 50.0 54.76 F2 ug/L 110 42-147 19 16
Bromomethane <0.350 50.0 56.45 ug/L 113 16-163 10 50
2-Butanone (MEK)<2.64 250 238.3 ug/L 95 50-138 17 19
TestAmerica Nashville
Page 22 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-01 OldLab Sample ID: 490-90364-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294861
Carbon disulfide <0.220 50.0 49.01 ug/L 98 48-152 15 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 50.0 54.94 ug/L 110 62-164 16 19
Chlorobenzene 1.77 F2 50.0 47.29 F2 ug/L 91 80-129 17 14
Chloroethane 0.810 J 50.0 52.70 ug/L 104 58-137 12 20
Chloroform <0.230 50.0 47.77 ug/L 96 66-138 15 18
Chloromethane <0.360 50.0 44.25 ug/L 89 10-169 16 31
cis-1,2-Dichloroethene 1.97 50.0 48.50 ug/L 93 68-138 15 17
cis-1,3-Dichloropropene <0.170 F2 50.0 46.17 F2 ug/L 92 71-141 17 15
Dibromochloromethane <0.250 F2 50.0 48.73 F2 ug/L 97 66-140 18 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 42.37 ug/L 85 52-126 20 24
1,2-Dibromoethane (EDB)<0.210 F2 50.0 46.43 F2 ug/L 93 75-137 16 15
Dibromomethane <0.450 50.0 47.15 ug/L 94 58-140 16 16
1,2-Dichlorobenzene 0.281 J F2 50.0 43.87 F2 ug/L 87 79-128 19 15
1,4-Dichlorobenzene 3.12 F2 50.0 46.15 F2 ug/L 86 78-126 19 15
1,1-Dichloroethane 0.674 J 50.0 47.85 ug/L 94 71-139 11 17
1,2-Dichloroethane <0.200 50.0 44.80 ug/L 90 64-136 16 17
1,1-Dichloroethene <0.250 50.0 52.01 ug/L 104 70-142 17 17
1,2-Dichloropropane 0.311 J 50.0 45.66 ug/L 91 67-131 14 17
Ethylbenzene <0.190 F2 50.0 46.40 F2 ug/L 93 79-139 17 15
2-Hexanone <1.28 F2 250 222.9 F2 ug/L 89 50-150 19 15
Iodomethane <1.50 50.0 54.78 ug/L 110 34-191 12 23
Methylene Chloride <0.220 50.0 45.52 ug/L 91 64-139 14 17
4-Methyl-2-pentanone (MIBK)<0.810 F2 250 220.3 F2 ug/L 88 50-147 19 17
Styrene <0.280 50.0 45.27 ug/L 91 61-148 17 24
1,1,1,2-Tetrachloroethane <0.150 F2 50.0 47.50 F2 ug/L 95 73-141 17 16
1,1,2,2-Tetrachloroethane <0.190 50.0 43.66 ug/L 87 56-143 19 20
Tetrachloroethene <0.140 F2 50.0 49.31 F2 ug/L 99 72-145 18 16
Tetrahydrofuran <0.820 F2 100 87.81 F2 ug/L 88 34-133 19 18
Toluene <0.170 F2 50.0 47.45 F2 ug/L 95 75-136 16 15
trans-1,4-Dichloro-2-butene <0.460 50.0 43.40 ug/L 87 29-156 14 26
trans-1,2-Dichloroethene <0.230 50.0 48.04 ug/L 96 66-143 15 16
trans-1,3-Dichloropropene <0.170 F2 50.0 46.60 F2 ug/L 93 59-135 18 14
1,1,1-Trichloroethane <0.190 50.0 51.11 ug/L 102 76-149 14 17
1,1,2-Trichloroethane <0.190 F2 50.0 45.18 F2 ug/L 90 74-134 19 15
Trichloroethene <0.200 50.0 50.00 ug/L 100 73-144 16 17
Trichlorofluoromethane <0.210 * F1 50.0 62.15 ug/L 124 58-139 15 18
1,2,3-Trichloropropane <0.230 50.0 43.83 ug/L 88 53-144 18 19
Vinyl acetate <1.71 F2 100 94.54 F2 ug/L 95 37-154 22 21
Vinyl chloride 0.324 J 50.0 54.17 ug/L 108 56-129 12 17
Xylenes, Total <0.580 F2 100 89.80 F2 ug/L 90 74-141 18 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
MSD MSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
97Toluene-d8 (Surr)70 -130
TestAmerica Nashville
Page 23 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 6010C - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-293000/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 296210 Prep Batch: 293000
RL MDL
Arsenic <8.60 10.0 8.60 ug/L 10/26/15 15:40 11/05/15 19:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<5.00 5.0010.0 ug/L 10/26/15 15:40 11/05/15 19:36 1Barium
<0.500 0.5001.00 ug/L 10/26/15 15:40 11/05/15 19:36 1Cadmium
<3.00 3.005.00 ug/L 10/26/15 15:40 11/05/15 19:36 1Chromium
<2.00 2.005.00 ug/L 10/26/15 15:40 11/05/15 19:36 1Lead
<5.00 5.0010.0 ug/L 10/26/15 15:40 11/05/15 19:36 1Selenium
<3.00 3.005.00 ug/L 10/26/15 15:40 11/05/15 19:36 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-293000/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 296210 Prep Batch: 293000
Arsenic 100 101.7 ug/L 102 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 100 104.0 ug/L 104 80-120
Cadmium 100 103.0 ug/L 103 80-120
Chromium 100 99.30 ug/L 99 80-120
Lead 100 106.9 ug/L 107 80-120
Selenium 100 99.50 ug/L 100 80-120
Silver 100 95.30 ug/L 95 80-120
Client Sample ID: Matrix SpikeLab Sample ID: 490-90332-D-11-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 296210 Prep Batch: 293000
Arsenic <8.60 100 102.4 ug/L 102 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 13.6 100 115.9 ug/L 102 75-125
Cadmium <0.500 100 100.2 ug/L 100 75-125
Chromium <3.00 100 99.90 ug/L 100 75-125
Lead 4.10 J 100 110.6 ug/L 107 75-125
Selenium <5.00 100 99.60 ug/L 100 75-125
Silver <3.00 100 94.10 ug/L 94 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-90332-D-11-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 296210 Prep Batch: 293000
Arsenic <8.60 100 102.8 ug/L 103 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 13.6 100 114.5 ug/L 101 75-125 1 20
Cadmium <0.500 100 99.90 ug/L 100 75-125 0 20
Chromium <3.00 100 98.90 ug/L 99 75-125 1 20
Lead 4.10 J 100 108.0 ug/L 104 75-125 2 20
Selenium <5.00 100 98.70 ug/L 99 75-125 1 20
Silver <3.00 100 94.70 ug/L 95 75-125 1 20
TestAmerica Nashville
Page 24 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-293324/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294762 Prep Batch: 293324
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:23 10/30/15 17:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-293324/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294762 Prep Batch: 293324
Mercury 1.00 0.8734 ug/L 87 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-293324/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294762 Prep Batch: 293324
Mercury 1.00 0.8296 ug/L 83 80-120 5 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-90252-G-4-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294762 Prep Batch: 293324
Mercury <0.100 F1 1.00 0.4049 F1 ug/L 40 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-90252-G-4-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294762 Prep Batch: 293324
Mercury <0.100 F1 1.00 0.3686 F1 ug/L 37 75-125 9 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-293337/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294166 Prep Batch: 293337
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/27/15 17:38 10/29/15 16:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-293337/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294166 Prep Batch: 293337
Mercury 1.00 1.020 ug/L 102 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-90368-A-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294166 Prep Batch: 293337
Mercury <0.100 1.00 0.9311 ug/L 93 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
TestAmerica Nashville
Page 25 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-90368-A-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 294166 Prep Batch: 293337
Mercury <0.100 1.00 0.9092 ug/L 91 75-125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
Page 26 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
GC/MS VOA
Analysis Batch: 294861
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-90364-1 MW-01 Old Total/NA
Water 8260B490-90364-1 MS MW-01 Old Total/NA
Water 8260B490-90364-1 MSD MW-01 Old Total/NA
Water 8260B490-90364-2 MW-02 Old Total/NA
Water 8260B490-90364-3 MW-03 Old Total/NA
Water 8260B490-90364-4 MW-04 Old Total/NA
Water 8260B490-90364-5 BG-Spring Old Total/NA
Water 8260B490-90364-6 Trip Blank Total/NA
Water 8260BLCS 490-294861/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-294861/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-294861/7 Method Blank Total/NA
Metals
Prep Batch: 293000
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-90332-D-11-B MS Matrix Spike Total/NA
Water 3010A490-90332-D-11-C MSD Matrix Spike Duplicate Total/NA
Water 3010A490-90364-1 MW-01 Old Total/NA
Water 3010A490-90364-2 MW-02 Old Total/NA
Water 3010A490-90364-3 MW-03 Old Total/NA
Water 3010A490-90364-4 MW-04 Old Total/NA
Water 3010A490-90364-5 BG-Spring Old Total/NA
Water 3010ALCS 490-293000/2-A Lab Control Sample Total/NA
Water 3010AMB 490-293000/1-A Method Blank Total/NA
Prep Batch: 293324
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-90252-G-4-C MS Matrix Spike Total/NA
Water 7470A490-90252-G-4-D MSD Matrix Spike Duplicate Total/NA
Water 7470A490-90364-1 MW-01 Old Total/NA
Water 7470ALCS 490-293324/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-293324/3-A Lab Control Sample Dup Total/NA
Water 7470AMB 490-293324/1-A Method Blank Total/NA
Prep Batch: 293337
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-90364-2 MW-02 Old Total/NA
Water 7470A490-90364-3 MW-03 Old Total/NA
Water 7470A490-90364-4 MW-04 Old Total/NA
Water 7470A490-90364-5 BG-Spring Old Total/NA
Water 7470A490-90368-A-1-B MS Matrix Spike Total/NA
Water 7470A490-90368-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 7470ALCS 490-293337/2-A Lab Control Sample Total/NA
Water 7470AMB 490-293337/1-A Method Blank Total/NA
Analysis Batch: 294166
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 293337490-90364-2 MW-02 Old Total/NA
Water 7470A 293337490-90364-3 MW-03 Old Total/NA
TestAmerica Nashville
Page 27 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Metals (Continued)
Analysis Batch: 294166 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 293337490-90368-A-1-B MS Matrix Spike Total/NA
Water 7470A 293337490-90368-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 7470A 293337LCS 490-293337/2-A Lab Control Sample Total/NA
Water 7470A 293337MB 490-293337/1-A Method Blank Total/NA
Analysis Batch: 294762
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 293324490-90252-G-4-C MS Matrix Spike Total/NA
Water 7470A 293324490-90252-G-4-D MSD Matrix Spike Duplicate Total/NA
Water 7470A 293324490-90364-1 MW-01 Old Total/NA
Water 7470A 293337490-90364-4 MW-04 Old Total/NA
Water 7470A 293337490-90364-5 BG-Spring Old Total/NA
Water 7470A 293324LCS 490-293324/2-A Lab Control Sample Total/NA
Water 7470A 293324LCSD 490-293324/3-A Lab Control Sample Dup Total/NA
Water 7470A 293324MB 490-293324/1-A Method Blank Total/NA
Analysis Batch: 296210
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010C 293000490-90332-D-11-B MS Matrix Spike Total/NA
Water 6010C 293000490-90332-D-11-C MSD Matrix Spike Duplicate Total/NA
Water 6010C 293000490-90364-1 MW-01 Old Total/NA
Water 6010C 293000490-90364-2 MW-02 Old Total/NA
Water 6010C 293000490-90364-3 MW-03 Old Total/NA
Water 6010C 293000490-90364-4 MW-04 Old Total/NA
Water 6010C 293000490-90364-5 BG-Spring Old Total/NA
Water 6010C 293000LCS 490-293000/2-A Lab Control Sample Total/NA
Water 6010C 293000MB 490-293000/1-A Method Blank Total/NA
TestAmerica Nashville
Page 28 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90364-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: MW-01 Old Lab Sample ID: 490-90364-1
Matrix: WaterDate Collected: 10/22/15 09:45
Date Received: 10/23/15 10:00
Analysis 8260B MJH11/02/15 18:221 TAL NSH294861
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 293000 10/26/15 15:40 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 296210 11/05/15 20:16 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 293324 10/27/15 17:23 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 294762 10/30/15 18:09 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-02 Old Lab Sample ID: 490-90364-2
Matrix: WaterDate Collected: 10/22/15 12:50
Date Received: 10/23/15 10:00
Analysis 8260B MJH11/02/15 18:481 TAL NSH294861
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 293000 10/26/15 15:40 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 296210 11/05/15 20:20 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 293337 10/27/15 17:38 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 294166 10/29/15 16:23 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-03 Old Lab Sample ID: 490-90364-3
Matrix: WaterDate Collected: 10/22/15 12:16
Date Received: 10/23/15 10:00
Analysis 8260B MJH11/02/15 19:141 TAL NSH294861
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 293000 10/26/15 15:40 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 296210 11/05/15 20:25 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 293337 10/27/15 17:38 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 294166 10/29/15 16:26 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-04 Old Lab Sample ID: 490-90364-4
Matrix: WaterDate Collected: 10/22/15 11:16
Date Received: 10/23/15 10:00
Analysis 8260B MJH11/02/15 19:411 TAL NSH294861
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 293000 10/26/15 15:40 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 296210 11/05/15 20:29 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 293337 10/27/15 17:38 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 294762 10/30/15 18:56 NJB TAL NSHTotal/NA 30 mL 30 mL
TestAmerica Nashville
Page 29 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90364-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: BG-Spring Old Lab Sample ID: 490-90364-5
Matrix: WaterDate Collected: 10/22/15 13:29
Date Received: 10/23/15 10:00
Analysis 8260B MJH11/02/15 20:081 TAL NSH294861
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 293000 10/26/15 15:40 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 296210 11/05/15 20:34 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 293337 10/27/15 17:38 RDF TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 294762 10/30/15 18:59 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: Trip Blank Lab Sample ID: 490-90364-6
Matrix: WaterDate Collected: 10/22/15 01:01
Date Received: 10/23/15 10:00
Analysis 8260B MJH11/02/15 17:551 TAL NSH294861
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 30 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Method Summary
TestAmerica Job ID: 490-90364-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010CMetals (ICP)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 31 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-90364-1
Project/Site: Madison Co Closed Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-15
TestAmerica Nashville
Page 32 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 33 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 34 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-90364-1
Login Number: 90364
Question Answer Comment
Creator: Buckingham, Paul
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
Page 35 of 35 11/6/2015
1
2
3
4
5
6
7
8
9
10
11
12
13

APPENDIX C

Environmental Monitoring Reporting Form
and
Electronic Submittal of Environmental
Data Deliverable
5802Oct2015 (Electronic Submittal Only)
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-MW01OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-34-3 75 1,1-Dichloroethane 0.674 ug/L J 8260B 0.240 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 95-50-1 69 1,2-Dichlorobenzene 0.281 ug/L J 8260B 0.190 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 78-87-5 82 1,2-Dichloropropane 0.311 ug/L J 8260B 0.250 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 106-46-7 71 1,4-Dichlorobenzene 3.12 ug/L 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 10.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 67-64-1 3 Acetone 2.66 ug/L U 8260B 2.66 25.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 7440-39-3 15 Barium 395 ug/L 6010C 5.00 10.0 100 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 71-43-2 16 Benzene 0.603 ug/L J 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 7440-43-9 34 Cadmium 0.500 ug/L U 6010C 0.500 1.00 1 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 108-90-7 39 Chlorobenzene 1.77 ug/L J 8260B 0.180 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-00-3 41 Chloroethane 0.810 ug/L J 8260B 0.360 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 7440-47-3 51 Chromium 4.90 ug/L J 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 156-59-2 78 cis-1,2-Dichloroethene 1.97 ug/L J 8260B 0.210 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/22/2015 11/8/2014 387
58-02 5802-MW01OLD 100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/22/2015 11/8/2014 387
58-02 5802-MW01OLD 7439-92-1 131 Lead 11.0 ug/L 6010C 2.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/22/2015 10/27/2015 10/30/2015 387
58-02 5802-MW01OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 7782-49-2 183 Selenium 5.00 ug/L U 6010C 5.00 10.0 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW01OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 109-99-9 458 Tetrahydrofuran 0.820 ug/L U 8260B 0.820 10.0 NE 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/22/2015 11/2/2015 387
Page 1 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-MW01OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 75-01-4 211 Vinyl chloride 0.324 ug/L J 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 1330-20-7 346 Xylene (Total)0.580 ug/L U 8260B 0.580 3.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW01OLD 7782-44-7 356 Dissolved Oxygen 3.18 mg/L 10/22/2015
58-02 5802-MW01OLD SW336 336 Oxygen Reduction Potential 74.7 mV 10/22/2015
58-02 5802-MW01OLD SW320 320 pH 6.33 SU 10/22/2015 5445
58-02 5802-MW01OLD SW323 323 Specific Conductivity 427 µS 10/22/2015
58-02 5802-MW01OLD SW325 325 Temperature 13.54 °C 10/22/2015
58-02 5802-MW01OLD SW330 330 Turbidity 124.6 NTU 10/22/2015
58-02 5802-MW01OLD SW318 318 Depth to Water 6.56 ft TOC 10/22/2015
58-02 5802-MW01OLD SW411 411 Total Well Depth 20.82 ft TOC 10/22/2015
58-02 5802-MW02OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-34-3 75 1,1-Dichloroethane 0.612 ug/L J 8260B 0.240 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 106-46-7 71 1,4-Dichlorobenzene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 10.0 100 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 67-64-1 3 Acetone 2.66 ug/L U 8260B 2.66 25.0 100 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 7440-39-3 15 Barium 46.7 ug/L J 6010C 5.00 10.0 100 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 71-43-2 16 Benzene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 7440-43-9 34 Cadmium 0.500 ug/L U 6010C 0.500 1.00 1 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 108-90-7 39 Chlorobenzene 0.180 ug/L U 8260B 0.180 1.00 3 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-00-3 41 Chloroethane 0.360 ug/L U 8260B 0.360 1.00 10 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 7440-47-3 51 Chromium 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/02/2015 387
Page 2 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-MW02OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 7439-92-1 131 Lead 4.80 ug/L J 6010C 2.00 5.00 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/22/2015 10/27/2015 10/29/2015 387
58-02 5802-MW02OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 7782-49-2 183 Selenium 5.00 ug/L U 6010C 5.00 10.0 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-MW02OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/22/2015 11/02/2015 387
58-03 5802-MW02OLD 109-99-9 458 Tetrahydrofuran 0.820 ug/L U 8260B 0.820 10.0 NE 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 1330-20-7 346 Xylene (Total)0.580 ug/L U 8260B 0.580 3.00 5 1 10/22/2015 11/02/2015 387
58-02 5802-MW02OLD 7782-44-7 356 Dissolved Oxygen 7.28 mg/L 10/22/2015
58-02 5802-MW02OLD SW336 336 Oxygen Reduction Potential 115.4 mV 10/22/2015
58-02 5802-MW02OLD SW320 320 pH 6.80 SU 10/22/2015 5445
58-02 5802-MW02OLD SW323 323 Specific Conductivity 191 µS 10/22/2015
58-02 5802-MW02OLD SW325 325 Temperature 17.28 °C 10/22/2015
58-02 5802-MW02OLD SW330 330 Turbidity 31.38 NTU 10/22/2015
58-02 5802-MW02OLD SW318 318 Depth to Water 8.11 ft TOC 10/22/2015
58-02 5802-MW02OLD SW411 411 Total Well Depth 43.35 ft TOC 10/22/2015
58-02 5802-MW03OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-34-3 75 1,1-Dichloroethane 0.240 ug/L U 8260B 0.240 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 106-46-7 71 1,4-Dichlorobenzene 2.69 ug/L 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 10.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 67-64-1 3 Acetone 3.04 ug/L J 8260B 2.66 25.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW03OLD 7440-39-3 15 Barium 887 ug/L 6010C 5.00 10.0 100 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW03OLD 71-43-2 16 Benzene 0.749 ug/L J 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/22/2015 11/2/2015 387
Page 3 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-MW03OLD 7440-43-9 34 Cadmium 0.500 ug/L U 6010C 0.500 1.00 1 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW03OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 108-90-7 39 Chlorobenzene 3.98 ug/L 8260B 0.180 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-00-3 41 Chloroethane 0.865 ug/L J 8260B 0.360 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 7440-47-3 51 Chromium 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW03OLD 156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 100-41-4 110 Ethylbenzene 0.210 ug/L J 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 7439-92-1 131 Lead 15.8 ug/L 6010C 2.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW03OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/22/2015 10/27/2015 10/29/2015 387
58-02 5802-MW03OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 7782-49-2 183 Selenium 5.70 ug/L J 6010C 5.00 10.0 10 1 10/22/2015 10/26/2015 11/2/2015 387
58-02 5802-MW03OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/2/2015 387
58-02 5802-MW03OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/22/2015 11/2/2015 387
3417-TP 5802-MW03OLD 109-99-9 458 Tetrahydrofuran 0.820 ug/L U 8260B 0.820 10.0 NE 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 1330-20-7 346 Xylene (Total)1.21 ug/L J 8260B 0.580 3.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW03OLD 7782-44-7 356 Dissolved Oxygen 0.410 mg/L 10/22/2015
58-02 5802-MW03OLD SW336 336 Oxygen Reduction Potential -3.60 mV 10/22/2015
58-02 5802-MW03OLD SW320 320 pH 6.32 SU 10/22/2015 5445
58-02 5802-MW03OLD SW323 323 Specific Conductivity 959 µS 10/22/2015
58-02 5802-MW03OLD SW325 325 Temperature 20.22 °C 10/22/2015
58-02 5802-MW03OLD SW330 330 Turbidity 24.51 NTU 10/22/2015
58-02 5802-MW03OLD SW318 318 Depth to Water 47.23 ft TOC 10/22/2015
58-02 5802-MW03OLD SW411 411 Total Well Depth 52.32 ft TOC 10/22/2015
58-02 5802-MW04OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 75-34-3 75 1,1-Dichloroethane 0.540 ug/L J 8260B 0.240 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/22/2015 11/2/2015 387
Page 4 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-MW04OLD 106-46-7 71 1,4-Dichlorobenzene 0.878 ug/L J 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 10.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 67-64-1 3 Acetone 5.65 ug/L J 8260B 2.66 25.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 7440-39-3 15 Barium 872 ug/L 6010C 5.00 10.0 100 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 71-43-2 16 Benzene 0.354 ug/L J 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 7440-43-9 34 Cadmium 0.500 ug/L U 6010C 0.500 1.00 1 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 108-90-7 39 Chlorobenzene 1.72 ug/L J 8260B 0.180 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 75-00-3 41 Chloroethane 0.576 ug/L J 8260B 0.360 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 7440-47-3 51 Chromium 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 156-59-2 78 cis-1,2-Dichloroethene 0.841 ug/L J 8260B 0.210 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 100-41-4 110 Ethylbenzene 0.357 ug/L J 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 7439-92-1 131 Lead 8.40 ug/L J 6010C 2.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/22/2015 10/27/2015 10/30/2015 387
58-02 5802-MW04OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 7782-49-2 183 Selenium 5.80 ug/L J 6010C 5.00 10.0 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/22/2015 10/26/2015 11/5/2015 387
58-02 5802-MW04OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/22/2015 11/2/2015 387
58-03 5802-MW04OLD 109-99-9 458 Tetrahydrofuran 2.37 ug/L J 8260B 0.820 10.0 NE 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-MW04OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/22/2015 11/8/2014 387
58-02 5802-MW04OLD 75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/8/2014 387
58-02 5802-MW04OLD 1330-20-7 346 Xylene (Total)2.26 ug/L J 8260B 0.580 3.00 5 1 10/22/2015 11/8/2014 387
58-02 5802-MW04OLD 7782-44-7 356 Dissolved Oxygen 2.77 mg/L 10/22/2015
58-02 5802-MW04OLD SW336 336 Oxygen Reduction Potential 177.1 mV 10/22/2015
58-02 5802-MW04OLD SW320 320 pH 6.25 SU 10/22/2015 5445
58-02 5802-MW04OLD SW323 323 Specific Conductivity 879 µS 10/22/2015
58-02 5802-MW04OLD SW325 325 Temperature 19.24 °C 10/22/2015
58-02 5802-MW04OLD SW330 330 Turbidity 4.75 NTU 10/22/2015
58-02 5802-MW04OLD SW318 318 Depth to Water 48.07 ft TOC 10/22/2015
Page 5 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-MW04OLD SW411 411 Total Well Depth 93.15 ft TOC 10/22/2015
58-02 5802-BGSPRINGOLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.15 ug/L U 8260B 0.15 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 71-55-6 200 1,1,1-Trichloroethane 0.19 ug/L U 8260B 0.19 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 79-34-5 200 1,1,2,2-Tetrachloroethane 0.19 ug/L U 8260B 0.19 1 3 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 79-00-5 200 1,1,2-Trichloroethane 0.19 ug/L U 8260B 0.19 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-34-3 200 1,1-Dichloroethane 0.24 ug/L U 8260B 0.24 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-35-4 200 1,1-Dichloroethene 0.25 ug/L U 8260B 0.25 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 96-18-4 200 1,2,3-Trichloropropane 0.23 ug/L U 8260B 0.23 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 96-12-8 200 1,2-Dibromo-3-chloropropane 0.94 ug/L U 8260B 0.94 10 13 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 106-93-4 200 1,2-Dibromoethane 0.21 ug/L U 8260B 0.21 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 107-06-2 200 1,2-Dichloroethane 0.2 ug/L U 8260B 0.2 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 78-87-5 200 1,2-Dichloropropane 0.25 ug/L U 8260B 0.25 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 591-78-6 200 2-Hexanone 1.28 ug/L U 8260B 1.28 10 50 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 108-10-1 200 4-Methyl-2-pentanone 0.81 ug/L U 8260B 0.81 10 100 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 67-64-1 200 Acetone 2.66 ug/L U 8260B 2.66 25 100 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 107-13-1 200 Acrylonitrile 0.5 ug/L U 8260B 0.5 10 200 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 7440-38-2 200 Arsenic 8.6 ug/L U 6010C 8.6 10 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 7440-39-3 200 Barium 430 ug/L 6010C 5 10 100 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 71-43-2 200 Benzene 0.2 ug/L U 8260B 0.2 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 74-97-5 200 Bromochloromethane 0.15 ug/L U 8260B 0.15 1 3 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-27-4 200 Bromodichloromethane 0.17 ug/L U 8260B 0.17 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-25-2 200 Bromoform 0.29 ug/L U *8260B 0.29 1 3 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 7440-43-9 200 Cadmium 0.5 ug/L U 6010C 0.5 1 1 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 75-15-0 200 Carbon disulfide 0.22 ug/L U 8260B 0.22 1 100 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 56-23-5 200 Carbon tetrachloride 0.18 ug/L U 8260B 0.18 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 108-90-7 200 Chlorobenzene 0.18 ug/L U 8260B 0.18 1 3 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-00-3 200 Chloroethane 0.36 ug/L U 8260B 0.36 1 10 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 67-66-3 200 Chloroform 0.23 ug/L U 8260B 0.23 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 7440-47-3 200 Chromium 59.7 ug/L 6010C 3 5 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 156-59-2 200 cis-1,2-Dichloroethene 0.21 ug/L U 8260B 0.21 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 10061-01-5 200 cis-1,3-Dichloropropene 0.17 ug/L U 8260B 0.17 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 124-48-1 200 Dibromochloromethane 0.25 ug/L U 8260B 0.25 1 3 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 100-41-4 200 Ethylbenzene 0.19 ug/L U 8260B 0.19 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 7439-92-1 200 Lead 26.7 ug/L 6010C 2 5 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 7439-97-6 200 Mercury 0.1 ug/L U 7470A 0.1 0.2 0.2 1 10/22/2015 10/27/2015 10/30/2015 387
58-02 5802-BGSPRINGOLD 74-83-9 200 Methyl bromide 0.35 ug/L U 8260B 0.35 1 10 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 74-87-3 200 Methyl chloride 0.36 ug/L U 8260B 0.36 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 78-93-3 200 Methyl ethyl ketone 2.64 ug/L U 8260B 2.64 50 100 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 74-88-4 200 Methyl iodide; Iodomethane 1.5 ug/L U 8260B 1.5 10 10 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 74-95-3 200 Methylene bromide 0.45 ug/L U 8260B 0.45 1 10 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-09-2 200 Methylene Chloride 0.22 ug/L U 8260B 0.22 5 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 95-50-1 200 o-Dichlorobenzene 0.19 ug/L U 8260B 0.19 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 106-46-7 200 p-Dichlorobenzene 0.17 ug/L U 8260B 0.17 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 7782-49-2 200 Selenium 5 ug/L U 6010C 5 10 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 7440-22-4 200 Silver 3 ug/L U 6010C 3 5 10 1 10/22/2015 10/26/2015 11/05/2015 387
58-02 5802-BGSPRINGOLD 100-42-5 200 Styrene 0.28 ug/L U 8260B 0.28 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 127-18-4 200 Tetrachloroethene 0.14 ug/L U 8260B 0.14 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 109-99-9 200 Tetrahydrofuran 0.82 ug/L U 8260B 0.82 10 NE 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 108-88-3 200 Toluene 0.17 ug/L U 8260B 0.17 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 156-60-5 200 trans-1,2-Dichloroethene 0.23 ug/L U 8260B 0.23 1 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 10061-02-6 200 trans-1,3-Dichloropropene 0.17 ug/L U 8260B 0.17 1 1 1 10/22/2015 11/02/2015 387
Page 6 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-BGSPRINGOLD 110-57-6 200 trans-1,4-Dichloro-2-butene 0.46 ug/L U 8260B 0.46 5 100 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 79-01-6 201 Trichloroethene 0.2 ug/L U 8260B 0.2 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-69-4 203 Trichlorofluoromethane 0.21 ug/L U *8260B 0.21 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10 50 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 75-01-4 211 Vinyl chloride 0.18 ug/L U 8260B 0.18 1 1 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 1330-20-7 346 Xylene (total)0.58 ug/L U 8260B 0.58 3 5 1 10/22/2015 11/02/2015 387
58-02 5802-BGSPRINGOLD 7782-44-7 356 Dissolved Oxygen 1.60 mg/L 10/22/2015
58-02 5802-BGSPRINGOLD SW336 336 Oxygen Reduction Potential 11.70 mV 10/22/2015
58-02 5802-BGSPRINGOLD SW320 320 pH 6.18 SU 10/22/2015 5445
58-02 5802-BGSPRINGOLD SW323 323 Specific Conductivity 212 µS 10/22/2015
58-02 5802-BGSPRINGOLD SW325 325 Temperature 16.08 °C 10/22/2015
58-02 5802-BGSPRINGOLD SW330 330 Turbidity 247.7 NTU 10/22/2015
58-02 5802-BGSPRINGOLD SW318 318 Depth to Water 12.56 ft TOC 10/22/2015
58-02 5802-BGSPRINGOLD SW411 411 Total Well Depth 14.25 ft TOC 10/22/2015
58-02 5802-SW01OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-34-3 75 1,1-Dichloroethane 0.240 ug/L U 8260B 0.240 1.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 106-46-7 71 1,4-Dichlorobenzene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 10.0 100 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 67-64-1 3 Acetone 2.66 ug/L U 8260B 2.66 25.0 100 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7440-39-3 15 Barium 63.2 ug/L J 6010C 5.00 10.0 100 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 71-43-2 16 Benzene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7440-43-9 34 Cadmium 0.500 ug/L U 6010C 0.500 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 108-90-7 39 Chlorobenzene 0.180 ug/L U 8260B 0.180 1.00 3 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-00-3 41 Chloroethane 0.360 ug/L U 8260B 0.360 1.00 10 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7440-47-3 51 Chromium 3.00 ug/L U 6010C 3.00 5.00 10 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/21/2015 10/26/2015 10/26/2015 387
58-02 5802-SW01OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/21/2015 10/26/2015 387
Page 7 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-SW01OLD 100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7439-92-1 131 Lead 2.00 ug/L U 6010C 2.00 5.00 10 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/21/2015 10/27/2015 387
58-02 5802-SW01OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7782-49-2 183 Selenium 5.00 ug/L U 6010C 5.00 10.0 10 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/21/2015 10/24/2015 10/26/2015 387
58-02 5802-SW01OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 109-99-9 458 Tetrahydrofuran 0.820 ug/L U 8260B 0.820 10.0 NE 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 1330-20-7 346 Xylene (Total)0.580 ug/L U 8260B 0.580 3.00 5 1 10/21/2015 10/26/2015 387
58-02 5802-SW01OLD 7782-44-7 356 Dissolved Oxygen 11.58 mg/L 10/21/2015
58-02 5802-SW01OLD SW336 336 Oxygen Reduction Potential 137.4 mV 10/21/2015
58-02 5802-SW01OLD SW320 320 pH 7.62 SU 10/21/2015 5445
58-02 5802-SW01OLD SW323 323 Specific Conductivity 171 µS 10/21/2015
58-02 5802-SW01OLD SW325 325 Temperature 12.74 °C 10/21/2015
58-02 5802-SW01OLD SW330 330 Turbidity 5.85 NTU 10/21/2015
58-02 5802-SW02OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 75-34-3 75 1,1-Dichloroethane 0.240 ug/L U 8260B 0.240 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.94 ug/L U 8260B 0.940 10.0 13 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 106-46-7 71 1,4-Dichlorobenzene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.81 ug/L U 8260B 0.810 10.0 100 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-SW02OLD 67-64-1 3 Acetone 2.66 ug/L U 8260B 2.66 25.0 100 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-SW02OLD 107-13-1 8 Acrylonitrile 0.5 ug/L U 8260B 0.500 10.0 200 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/21/2015 10/27/2015 387
58-02 5802-SW02OLD 7440-39-3 15 Barium 59.9 ug/L J 6010C 5.00 10.0 100 1 10/21/2015 10/27/2015 387
58-02 5802-SW02OLD 71-43-2 16 Benzene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-SW02OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 7440-43-9 34 Cadmium 0.5 ug/L U 6010C 0.500 1.00 1 1 10/21/2015 10/27/2015 387
Page 8 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-SW02OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-SW02OLD 108-90-7 39 Chlorobenzene 0.180 ug/L U 8260B 0.180 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 75-00-3 41 Chloroethane 0.360 ug/L U 8260B 0.360 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 7440-47-3 51 Chromium 3.00 ug/L U 6010C 3.00 5.00 10 1 10/21/2015 10/24/2015 10/27/2015 387
58-02 5802-SW02OLD 156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/21/2015 10/26/2015 10/24/2015 387
58-02 5802-SW02OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 7439-92-1 131 Lead 2.00 ug/L U 6010C 2.00 5.00 10 1 10/21/2015 10/27/2015 387
58-02 5802-SW02OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/21/2015 10/27/2015 387
58-02 5802-SW02OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 7782-49-2 183 Selenium 5.00 ug/L U 6010C 5.00 10.0 10 1 10/21/2015 10/24/2015 10/27/2015 387
58-02 5802-SW02OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/21/2015 10/24/2015 10/27/2015 387
58-02 5802-SW02OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.460 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 109-99-9 458 Tetrahydrofuran 0.82 ug/L U 8260B 0.820 10.0 NE 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.46 ug/L U 8260B 0.460 5.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 1330-20-7 346 Xylene (Total)0.58 ug/L U 8260B 0.580 3.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-SW02OLD 7782-44-7 356 Dissolved Oxygen 12.28 mg/L 10/21/2015
58-02 5802-SW02OLD SW336 336 Oxygen Reduction Potential 137.2 mV 10/21/2015
58-02 5802-SW02OLD SW320 320 pH 7.83 SU 10/21/2015 5445
58-02 5802-SW02OLD SW323 323 Specific Conductivity 191 µS 10/21/2015
58-02 5802-SW02OLD SW325 325 Temperature 9.94 °C 10/21/2015
58-02 5802-SW02OLD SW330 330 Turbidity 2.95 NTU 10/21/2015
58-02 5802-DW01OLD 630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 75-34-3 75 1,1-Dichloroethane 0.240 ug/L U 8260B 0.240 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 106-46-7 71 1,4-Dichlorobenzene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 10.0 50 1 10/21/2015 10/24/2015 387
Page 9 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-DW01OLD 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 10.0 100 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-DW01OLD 67-64-1 3 Acetone 2.66 ug/L U 8260B 2.66 25.0 100 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-DW01OLD 107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 7440-38-2 14 Arsenic 8.60 ug/L U 6010C 8.60 10.0 10 1 10/21/2015 10/27/2015 387
58-02 5802-DW01OLD 7440-39-3 15 Barium 215 ug/L 6010C 5.00 10.0 100 1 10/21/2015 10/27/2015 387
58-02 5802-DW01OLD 71-43-2 16 Benzene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-DW01OLD 75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 7440-43-9 34 Cadmium 0.500 ug/L U 6010C 0.500 1.00 1 1 10/21/2015 10/27/2015 387
58-02 5802-DW01OLD 75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 10/24/2015 387
58-02 5802-DW01OLD 108-90-7 39 Chlorobenzene 0.180 ug/L U 8260B 0.180 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 75-00-3 41 Chloroethane 0.360 ug/L U 8260B 0.360 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 7440-47-3 51 Chromium 3.20 ug/L J 6010C 3.00 5.00 10 1 10/21/2015 10/24/2015 10/27/2015 387
58-02 5802-DW01OLD 156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/21/2015 10/26/2015 10/24/2015 387
58-02 5802-DW01OLD 10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 7439-92-1 131 Lead 7.10 ug/L J 6010C 2.00 5.00 10 1 10/21/2015 10/27/2015 387
58-02 5802-DW01OLD 7439-97-6 132 Mercury 0.100 ug/L U 7470A 0.100 0.200 0.2 1 10/21/2015 10/27/2015 387
58-02 5802-DW01OLD 75-09-2 140 Methylene Chloride 0.220 ug/L U 8260B 0.220 5.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 7782-49-2 183 Selenium 5.00 ug/L U 6010C 5.00 10.0 10 1 10/21/2015 10/24/2015 10/27/2015 387
58-02 5802-DW01OLD 7440-22-4 184 Silver 3.00 ug/L U 6010C 3.00 5.00 10 1 10/21/2015 10/24/2015 10/27/2015 387
58-02 5802-DW01OLD 100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.460 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 109-99-9 458 Tetrahydrofuran 3.48 ug/L J 8260B 0.820 10.0 NE 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 1330-20-7 346 Xylene (Total)0.580 ug/L U 8260B 0.580 3.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-DW01OLD 7782-44-7 356 Dissolved Oxygen 5.56 mg/L 10/21/2015
58-02 5802-DW01OLD SW336 336 Oxygen Reduction Potential 183.0 mV 10/21/2015
58-02 5802-DW01OLD SW320 320 pH 6.39 SU 10/21/2015 5445
58-02 5802-DW01OLD SW323 323 Specific Conductivity 168 µS 10/21/2015
58-02 5802-DW01OLD SW325 325 Temperature 15.32 °C 10/21/2015
58-02 5802-DW01OLD SW330 330 Turbidity 4.84 NTU 10/21/2015
58-02 5802-TRIPBLANK (DW)630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
Page 10 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-TRIPBLANK (DW)75-34-3 75 1,1-Dichloroethane 0.240 ug/L U 8260B 0.240 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)106-46-7 71 1,4-Dichlorobenzene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 5.00 50 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 5.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)67-64-1 3 Acetone 6.31 ug/L J 8260B 2.66 25.0 100 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)71-43-2 16 Benzene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)108-90-7 39 Chlorobenzene 0.180 ug/L U 8260B 0.180 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-00-3 41 Chloroethane 0.360 ug/L U 8260B 0.360 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-09-2 140 Methylene Chloride 1.15 ug/L J 8260B 0.220 5.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/21/2015 10/24/2015 387
3417-TP 5802-TRIPBLANK (DW)109-99-9 458 Tetrahydrofuran 0.820 ug/L U 8260B 0.820 10.0 NE 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (DW)1330-20-7 346 Xylene (Total)0.580 ug/L U 8260B 0.580 3.00 5 1 10/21/2015 10/24/2015 387
58-02 5802-TRIPBLANK (CLOSED)630-20-6 190 1,1,1,2-Tetrachloroethane 0.150 ug/L U 8260B 0.150 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)71-55-6 200 1,1,1-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)79-34-5 191 1,1,2,2-Tetrachloroethane 0.190 ug/L U 8260B 0.190 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)79-00-5 202 1,1,2-Trichloroethane 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-34-3 75 1,1-Dichloroethane 0.240 ug/L U 8260B 0.240 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-35-4 77 1,1-Dichloroethene 0.250 ug/L U 8260B 0.250 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)96-18-4 206 1,2,3-Trichloropropane 0.230 ug/L U 8260B 0.230 1.00 1 1 10/22/2015 11/2/2015 387
Page 11 of 12
5802Oct2015EDD
FACILITY
PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
DILUTION
FACTOR COLLECT DATE
EXTRACTION
DATE
ANALYSIS
DATE
NC LABORATORY
CERTIFICATION
NUMBER
58-02 5802-TRIPBLANK (CLOSED)96-12-8 67 1,2-Dibromo-3-chloropropane 0.940 ug/L U 8260B 0.940 10.0 13 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)106-93-4 68 1,2-Dibromoethane (EDB)0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)95-50-1 69 1,2-Dichlorobenzene 0.190 ug/L U 8260B 0.190 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)107-06-2 76 1,2-Dichloroethane 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)78-87-5 82 1,2-Dichloropropane 0.250 ug/L U 8260B 0.250 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)106-46-7 71 1,4-Dichlorobenzene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)78-93-3 141 2-Butanone (MEK)2.64 ug/L U 8260B 2.64 50.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)591-78-6 124 2-Hexanone 1.28 ug/L U 8260B 1.28 5.00 50 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)108-10-1 147 4-Methyl-2-pentanone (MIBK)0.810 ug/L U 8260B 0.810 5.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)67-64-1 3 Acetone 10.20 ug/L J 8260B 10.00 25.0 100 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)107-13-1 8 Acrylonitrile 0.500 ug/L U 8260B 0.500 10.0 200 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)71-43-2 16 Benzene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)74-97-5 28 Bromochloromethane 0.150 ug/L U 8260B 0.150 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-27-4 29 Bromodichloromethane 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-25-2 30 Bromoform 0.290 ug/L U 8260B 0.290 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)74-83-9 136 Bromomethane 0.350 ug/L U 8260B 0.350 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-15-0 35 Carbon disulfide 0.220 ug/L U 8260B 0.220 1.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)56-23-5 36 Carbon tetrachloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)108-90-7 39 Chlorobenzene 0.180 ug/L U 8260B 0.180 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-00-3 41 Chloroethane 0.360 ug/L U 8260B 0.360 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)67-66-3 44 Chloroform 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)74-87-3 137 Chloromethane 0.360 ug/L U 8260B 0.360 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)156-59-2 78 cis-1,2-Dichloroethene 0.210 ug/L U 8260B 0.210 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)10061-01-5 86 cis-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)124-48-1 66 Dibromochloromethane 0.250 ug/L U 8260B 0.250 1.00 3 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)74-95-3 139 Dibromomethane 0.450 ug/L U 8260B 0.450 1.00 10 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)100-41-4 110 Ethylbenzene 0.190 ug/L U 8260B 0.190 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)74-88-4 142 Iodomethane 1.50 ug/L U 8260B 1.50 10.0 10 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-09-2 140 Methylene Chloride 1.45 ug/L J 8260B 0.220 5.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)100-42-5 186 Styrene 0.280 ug/L U 8260B 0.280 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)127-18-4 192 Tetrachloroethene 0.140 ug/L U 8260B 0.140 1.00 1 1 10/22/2015 11/2/2015 387
3417-TP 5802-TRIPBLANK (CLOSED)109-99-9 458 Tetrahydrofuran 0.820 ug/L U 8260B 0.820 10.0 NE 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)108-88-3 196 Toluene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)156-60-5 79 trans-1,2-Dichloroethene 0.230 ug/L U 8260B 0.230 1.00 5 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)10061-02-6 87 trans-1,3-Dichloropropene 0.170 ug/L U 8260B 0.170 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)110-57-6 73 trans-1,4-Dichloro-2-butene 0.460 ug/L U 8260B 0.460 5.00 100 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)79-01-6 201 Trichloroethene 0.200 ug/L U 8260B 0.200 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-69-4 203 Trichlorofluoromethane 0.210 ug/L U 8260B 0.210 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)108-05-4 210 Vinyl acetate 1.71 ug/L U 8260B 1.71 10.0 50 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)75-01-4 211 Vinyl chloride 0.180 ug/L U 8260B 0.180 1.00 1 1 10/22/2015 11/2/2015 387
58-02 5802-TRIPBLANK (CLOSED)1330-20-7 346 Xylene (Total)0.580 ug/L U 8260B 0.580 3.00 5 1 10/22/2015 11/2/2015 387
Page 12 of 12