5802_MadisonCountyMSWLF_GWMonitoring_DIN27131_20160413

Prepared for
Madison County, North Carolina
Project Number 2313.1301

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Spring 2016 Semiannual
Water Quality Monitoring Report
Madison County Closed
Solid Waste Facility
Madison County, North Carolina
Permit No. 58-02
July 6, 2016

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page ii
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx

Spring 2016 Semiannual
Water Quality Monitoring Report
Madison County Closed
Solid Waste Facility
Madison County, North Carolina
Permit No. 58-02
July 6, 2016

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page iii
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx

Table of Contents
1.0 Introduction .................................................................................................................... 1
2.0 Methods ......................................................................................................................... 2
2.1 Groundwater Purging and Sampling Methods ..............................................................2
2.1.1 Monitoring Well Sampling Methods ..................................................................2
2.1.2 Domestic Well Sampling Methods ....................................................................3
2.1.3 Surface Water Sampling Methods ....................................................................3
2.2 Sample Handling, Documentation, and Analysis...........................................................3
3.0 Findings .......................................................................................................................... 4
3.1 Analytical Results ..........................................................................................................4
3.1.1 Groundwater Monitoring Wells .........................................................................4
3.1.2 Surface Water ...................................................................................................5
4.0 Site Hydrogeology ........................................................................................................... 7
5.0 Summary ........................................................................................................................ 8
5.1 Future Activities .............................................................................................................8
6.0 References ..................................................................................................................... 9

Figures
1. Site Location Map
2. Sample Location Map
Tables
1. Summary of Laboratory Analyses Performed on Samples
2. Summary of Detected Constituents
Appendices
A. Sampling Logs and Equipment Documentation and Instrument Calibration Data Sheets
B. Report of Laboratory Analysis and Chain-of-Custody Documentation
C. Environmental Monitoring Reporting Form and Electronic Submittal of Environmental Monitoring
Data 5802Apr2016 (Electronic Only)
Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 1
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
1.0 Introduction
The Madison County Solid Waste Department maintains a closed municipal solid waste landfill (Closed
Landfill) (the Site) located near the intersection of US Highway 25/70 Bypass and Long Branch Road (State
Route 1582) in Madison County, North Carolina. The general Site location is presented on Figure 1.
The Closed Landfill is permitted by the North Carolina Department of Environmental Quality (DEQ), Division
of Waste Management (DWM) under Permit No. 58-02, which requires semiannual monitoring of
groundwater and surface water quality.
This report is being submitted in accordance with monitoring requirements for closed landfills as stipulated
in the DEQ DWM Permit No. 58-02 issued to the Madison County Solid Waste Department and with
regulations codified in the DEQ Solid Waste Management (SWM) Rules Title 15A, Subchapter 13B,
Section .1600, of the North Carolina Administrative Code.
This report describes the first groundwater and surface water quality monitoring event performed in 2016.
The water quality monitoring network for the Closed Landfill consists of four compliance monitoring wells
(MW-01 OLD, MW-02 OLD, MW-03 OLD, and MW-04 OLD), a background groundwater quality sampling
location (BG SPRING OLD), and two surface water sampling locations—SW-01 OLD (upstream) and SW-02
OLD (downstream)—located along Profitt Branch. See Figure 2 for all approximate sampling locations.

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 2
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
2.0 Methods
Groundwater samples, surface water samples, and one domestic well sample were collected at the Closed
Landfill by Altamont Environmental, Inc. (Altamont) personnel on April 13 and 14, 2016 (see Appendices A
and B) at the approximate sampling locations depicted on Figure 2.
The water sample collected from background sampling location BG SPRING OLD is treated as a groundwater
sample for the following reasons:
 Groundwater does not discharge to the ground surface at the sampling point.
 Construction of the sample point is similar to that of a temporary monitoring well or piezometer and
is located upslope and upgradient of a springhead.
 The sampling point is constructed of a polyvinyl chloride (PVC) casing extending below ground
surface and has a screened interval from which groundwater is collected and recharges.
2.1 Groundwater Purging and Sampling Methods
2.1.1 Monitoring Well Sampling Methods
2.1.1.1 Monitoring Wells MW-01 OLD, MW-02 OLD, and BG SPRING OLD
Prior to collecting groundwater samples from the monitoring wells, the static water level and the total well
depth were measured and recorded in order to calculate the well’s volume. At each sample location, an
initial round of field parameters consisting of pH, specific conductivity (SC), dissolved oxygen (DO), oxidation-
reduction potential (ORP), turbidity, and temperature was measured and recorded. Water-level
measurements and field parameters are included on the sampling logs (Appendix A). Groundwater
monitoring wells MW-01 OLD and MW-02 OLD and sampling point BG SPRING OLD were then purged using a
new disposable polyethylene bailer. As each consecutive well volume was removed with the bailer, an
additional round of groundwater parameters was recorded. Each well was purged until a minimum of three
well volumes were removed and field parameters stabilized or until the well had been bailed dry. Wells that
were bailed dry were allowed to recharge prior to collecting one final round of field parameters and the
groundwater sample.
2.1.1.2 Monitoring Wells MW-03 OLD and MW-04 OLD
Monitoring wells MW-03 OLD and MW-04 OLD were purged and sampled using low-flow techniques in
accordance with the procedures described in Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures, United States Environmental Protection Agency (EPA), Groundwater Issues (Puls and Barcelona
1996). During purging, pH, SC, DO, ORP, turbidity, and temperature were measured and recorded
approximately every 3 minutes. Well purging continued until these parameters stabilized for three
consecutive readings. The required stabilization criteria are as follows:
 pH values within +/- 0.1 pH unit
 SC values within +/- 3 percent
 Temperature, DO, and turbidity values within +/- 10 percent
 ORP values within +/- 10 millivolts
Following stabilization of these parameters, a groundwater sample was collected by a technician wearing a
new pair of non-reactive nitrile gloves. Each sample was placed directly into laboratory-supplied sample
containers. Low-flow sampling logs are included in Appendix A.
Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 3
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
2.1.2 Domestic Well Sampling Methods
Altamont personnel sampled one domestic well (DW-01 OLD) owned by Mrs. J.V. Edwards on April 13, 2016.
The well was purged and sampled using the dedicated pump existing in the well. Groundwater was accessed
from a spigot in the basement of Mrs. J. V. Edwards’ house because a spigot does not exist at the wellhead.
Altamont personnel recorded one round of field parameters initially at the start of the purge and then one
round for every 10 gallons purged from the well. Prior to sample collection, a total of 30 gallons of water was
purged from the well. Field parameters are presented in Appendix A. A groundwater sample was collected
from the domestic well using laboratory-supplied sample containers by a technician wearing a new pair of
disposable nitrile gloves. The sample was identified as DW-01.
2.1.3 Surface Water Sampling Methods
Surface water samples SW-01 OLD and SW-02 OLD were collected at designated locations along Profitt
Branch, which flows adjacent to the southern Site boundary in a west-to-east direction (Figure 2). The
surface water sample collected at the SW-01 OLD location is assumed to represent surface water quality
upstream of the Closed Landfill, and the surface water sample collected at the SW-02 OLD location is
assumed to represent surface water quality downstream of the Closed Landfill. One set of field parameters,
including temperature, pH, SC, DO, ORP, and turbidity, was measured and recorded at each surface water
sampling location prior to sample collection (Appendix A). One surface water sample was collected from each
sampling location using laboratory-supplied sample containers by a technician wearing a new pair of
disposable nitrile gloves.
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to water quality sampling at the Closed Landfill
sampling locations are provided on the sampling logs provided in Appendix A. Following sample collection,
groundwater and surface water samples were immediately placed on ice in sample coolers for transport to
TestAmerica Laboratories, Inc. (TestAmerica), a laboratory certified in North Carolina and located in
Nashville, Tennessee. Altamont submitted the water samples collected from the monitoring wells and the
surface water sampling locations to TestAmerica for analysis as follows:
 Appendix I volatile organic compounds (VOCs) using EPA Approved Method 8260B
 Eight Resource Conservation and Recovery Act (RCRA) metals using EPA Approved Methods 6010D
and 7470A
A summary of laboratory analyses performed on samples is provided in Table 1. A trip blank, provided by the
laboratory and stored in the sample cooler, was analyzed for Appendix I VOCs. Proper chain-of-custody
documentation procedures were followed during collection and transport of each sample. The laboratory
analytical reports and chain-of-custody documentation are included in Appendix B. Water-level
measurements and field parameters are included in Appendix A and in the Electronic Data Deliverable (EDD)
in Appendix C.
Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 4
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
3.0 Findings
3.1 Analytical Results
The field parameter data and laboratory analytical results for the groundwater, surface water, and trip blank
samples collected at the Closed Landfill are included in Appendices A and B, respectively, in hard copy, and
also as Appendix C in the EDD format specified by the DEQ Solid Waste Section (SWS) of the DWM (most
recently updated on May 5, 2010).
As stipulated in the DWM documents referenced above, non-detections were reported at the method
detection limit (MDL), and all concentrations exceeding the applicable laboratory-specific MDL were reported
and appropriately qualified (see Table 2). The MDL is the minimum concentration of a substance that can be
measured and reported by a laboratory with 99 percent confidence that the analyte concentration is greater
than zero. All detections were compared to analyte-specific Solid Waste Section Limits (SWSLs) established
by the SWS. The SWSL is the lowest concentration of an analyte in a sample that can be quantitatively
determined with suitable precision and accuracy. If the reported concentration is above the laboratory MDL
and below the method reporting limit (MRL), the analytical result is qualified by the laboratory as estimated
and is flagged with a “J” qualifier (J-flag). The MRL is the minimum concentration of a target analyte that can
be accurately determined by the referenced method and is listed in the “Report Limit” (RL) column in the
TestAmerica report of laboratory analysis (see Appendix B). If the reported concentration is greater than the
laboratory MRL and less than the SWSL, the analytical result is qualified by Altamont as estimated and is
flagged with a “J” qualifier (italicized J-flag).
Detected concentrations of analytes in groundwater samples were compared to current groundwater quality
standards specified in Title 15A, NCAC, Subchapter 2L .0202, and are referred to as 2L standards. Detected
concentrations of analytes in groundwater with no established 2L standards were compared to the interim
maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with Title
15A, NCAC, Subchapter 02L .0202 [c]), if established. Detections of analytes in surface water samples were
compared to Title 15A, NCAC, Subchapter 2B .0200 surface water quality standards (2B standards).
Concentrations below respective SWSLs are not discussed in the text of this report unless they exceed their
contaminant-specific 2L or 2B water quality standard, as defined below.
Table 2 presents the summary of laboratory analytical results for detected constituents. The summary
outlines constituents that were detected above applicable SWSLs, as well as constituents detected at
concentrations that exceeded their respective 2L standards (including IMACs, if applicable) or 2B standards.
In the EDD (see Appendix C), the identification of a well (“WELL ID”) consists of the name of the well
prefaced by the un-hyphenated permit number for the facility. For example, monitoring well MW-01 OLD is
identified on the tables as 5802-MW01OLD. In the tables, figures, and text of this report, however, the
identification of a well consists only of the name of the well and does not include the permit number for the
facility.
3.1.1 Groundwater Monitoring Wells
The following sections summarize the results of laboratory and field parameter analyses of groundwater
samples.
3.1.1.1 RCRA Metals
Seven metals were detected in groundwater samples collected from one or more monitoring wells (see Table
2). Six of these metals (barium, cadmium, chromium, copper, lead, and nickel) were detected at
concentrations greater than their respective SWSLs (see Table 2). The concentration of barium exceeded its
2L standard in the samples collected from monitoring wells MW-03 OLD and MW-04 OLD (see Table 2).
Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 5
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
Chromium concentrations exceeded the 2L standard in samples collected from BG SPRING OLD. Detected
metals above 2L standards could be naturally occurring.
3.1.1.2 Appendix I VOCs
Thirteen VOCs were detected in groundwater samples collected from one or more monitoring wells. Four
VOCs (1,4-dichlorobenzene, benzene, chlorobenzene, and ethylbenzene) were detected in excess of their
respective SWSLs in one or more monitoring wells (see Table 2). Benzene was detected at a concentration in
excess of the 2L standard in MW-01 OLD and MW-03 OLD. Acetone was detected in two of the samples
collected from the monitoring wells, as well as in the trip blank. Due to the trip blank detection, it is likely
that detection of this VOC was due to laboratory contamination. Trans-1,2-dichloroethene was also detected
in the trip blank, although it was not detected in any of the samples collected from the monitoring wells.
3.1.1.3 Field Parameters
The pH readings obtained on April 14, 2016 from all monitoring wells, except for MW-02 OLD, were outside
the range for pH (6.5 to 8.5 Standard Units [SU]) specified in the 2L standard (see Table 2).
The remaining parameters measured in the field have no established groundwater quality standards and are
therefore not discussed in this section.
3.1.2 Surface Water
The following sections summarize the results of laboratory and field parameter analyses of surface water
samples SW-01 OLD and SW-02 OLD.
3.1.2.1 RCRA Metals
Barium was detected at concentrations below the SWSL in both SW-01 OLD and SW-02 OLD (see Table 2).
These concentrations were well below the applicable 2B standard.
3.1.2.2 Appendix I VOCs
Xylene (total) was detected in the upstream surface water sample (SW-01 OLD) at a concentration below its
SWSL and well below the 2B standard.
3.1.2.3 Field Parameters
The pH readings collected from both surface water sample locations were within the pH 2B standard range
established at 6.0 to 9.0 SU.
The turbidity readings collected from SW-01 OLD and SW-02 OLD were 3.09 NTUs and 7.53 NTUs,
respectively. Both readings are within the 2B standard of 50 NTUs.
DO was recorded outside of the 2B standard for both surface water samples collected. The established 2B
standard for DO in class C waters is “greater than 5.0 mg/L.” Collected DO readings were 4.78 mg/L and
4.36 mg/L for surface water samples SW-01 OLD and SW-02 OLD, respectively.
The remaining parameters measured in the field have no established surface water quality standards and
are therefore not discussed in this section.
3.1.3 Drinking Water
The following sections summarize the results of laboratory and field parameter analyses of the drinking
water sample DW-01 OLD.
Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 6
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
3.1.3.1 RCRA Metals
Three metals were detected in DW-01 OLD (Table 2). Barium and copper were detected above their
respective SWSLs. All three detected metals had concentrations below applicable 2L standards.
3.1.3.2 Appendix I VOCs
There were no VOCs detected in DW-01 OLD.
3.1.3.3 Field Parameters
The recorded pH reading for DW-01 OLD was 6.31 SU, which is outside the established 2L standard.
The remaining parameters measured have no established groundwater quality standards and are therefore
not discussed in this section.

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 7
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
4.0 Site Hydrogeology
Groundwater levels were measured in the four monitoring wells (MW-01 OLD, MW-02 OLD, MW-03 OLD, and
MW-04 OLD) at the Closed Landfill at depths of approximately 5.93 feet below ground surface (ft-bgs), 7.85
ft-bgs, 41.13 ft-bgs, and 41.91 ft-bgs, respectively (Appendix A).
Monitoring wells MW-03 OLD and MW-04 OLD are installed in bedrock east of the Edwards/Madison County
property line near the top of a ridge within the landfill parcel. Monitoring wells MW-01 OLD and MW-02 OLD
are located in topographic drainages and are screened in the water table aquifer. Locations of monitoring
wells at the Site are not situated such that groundwater flow direction may be accurately calculated based
on data from these wells. However, within the unconsolidated soil, the shallow groundwater is interpreted to
generally flow in directions that mimic topography, which is generally southward toward Profitt Branch. The
Site is situated on the southwest side of a knoll with an elevation of approximately 2,100 feet above mean
sea level and drains to Profitt Branch.

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 8
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
5.0 Summary
Altamont completed the first semiannual water quality monitoring event of 2016 at the Madison County
Closed Solid Waste Landfill on April 13 and 14, 2016.
Table 2 of this report, sampling logs (Appendix A), TestAmerica Reports of Laboratory Analysis (Appendix B),
and the EDD spreadsheet (Appendix C) provide detailed analytical results and field data related to
groundwater and surface water quality at the Closed Landfill.
5.1 Future Activities
Altamont has discussed the exceedances of applicable water quality standards with Madison County.
Altamont will continue to measure field parameters and collect water quality samples from groundwater and
surface water monitoring points associated with the Closed Landfill. Water quality samples will be submitted
to a North Carolina-certified laboratory for analysis for RCRA metals and Appendix I VOCs on a semiannual
basis. The next sampling event is scheduled for October 2016.

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-02, Madison County, North Carolina Page 9
P:\Madison County\Reports\2016\Spring\5802 - Closed\FINAL 5802Apr2016 Semiannual Water Quality Report.docx
6.0 References
DENR DWM Solid Waste Section (SWS). October 27, 2006. New Guidelines for Electronic Submittal of
Environmental Monitoring Data.
DENR DWM SWS. February 23, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding
New Guidelines for Electronic Submittal of Environmental Data.

FIGURES

Site Location











1





¦
@A@A
@A
@A
@A
@A#*
#*








Profitt Bran
c
h
U
n
n
a
m
e
d

T
r
i
b
u
t
a
r
y
Unnamed Trib
u
t
a
r
y
























20
5
5
204
5
206
5
2035
20
2
5
2
0
7
5
20
1
5
2005
208
5
1
9
9
5
2
0
9
5
2105
2115
1985
21252135
1975
21452155
2165
1965
2175
2185
1955
2195
2205 2215
2225
2245
2
2
3
5
2255
1945
2265
227
5
1935
1925
2285
229
5
2305
1915
231
5
21
8
5
2055
2
0
7
5
2035
2055
2105
2085
2145
2175
2045
21
1
5
2115
2035
2
0
6
5
2125
2145
2035
20
3
5
2
1
2
5
21
0
5
2115
21
3
5
20
3
5
1975
21
7
5












¦











#*
@A 





TABLES

Table 1
Summary of Laboratory Analyses Performed on Samples
Madison County Closed Municipal Solid Waste Landfill, Madison County, North Carolina
GROUNDWATER SAMPLES
VOCs RCRA Metals
EPA 8260B EPA 6010D
EPA 7470A
58-02 MW-01 OLD 04/14/2016 X X
58-02 MW-02 OLD 04/14/2016 X X
58-02 MW-03 OLD 04/14/2016 X X
58-02 MW-04 OLD 04/14/2016 X X
58-02 BG SPRING OLD 04/14/2016 X X
58-02 DW-01 OLD 04/13/2016 X X
SURFACE WATER SAMPLES
VOCs RCRA Metals
EPA 8260B EPA 6010D
EPA 7470A
58-02 SW-1 OLD 04/13/2016 X X
58-02 SW-2 OLD 04/13/2016 X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
58-02 TRIP BLANK 4/13/2016 X
Notes:
VOCs Volatile organic compounds. Analyses include Appendix I constituents per 40 CFR Part 258.
FACILITY
PERMIT SAMPLE ID COLLECT DATE
FACILITY
PERMIT WELL ID COLLECT DATE
FACILITY
PERMIT SAMPLE ID COLLECT DATE
P:\Madison County\Analytical & Data\Water\2016\58-02 Closed\Tables\5802April2016_Tables Page 1 of 1
Table 2
Summary of Detected Constituents
Madison County Closed Municipal Solid Waste Landfill, Madison County, North Carolina
Metals VOCs (Appendix I)Field Parameters
Lab Certification 387 387 5445 (pH only)
Lab Method EPA 6010D EPA 8260B
Parameter Barium Cadmium Chromium Copper Lead Nickel Selenium
1,1-
Dichloro-
ethane
1,2-
Dichloro-
benzene
1,2-
Dichloro-
propane
1,4-
Dichloro-
benzene
Acetone Benzene Chloro-
benzene
Chloro-
ethane
cis-1,2-
Dichloro-
ethene
Ethyl-
benzene
Methyl Ethyl
Ketone
trans-1,2-
dichloro-
ethene
Trichloro-
ethene
Xylene
(Total) pH Turbidity Dissolved
Oxygen
CAS Number 7440-39-3 7440-39-3 7440-47-3 7440-50-8 7439-92-1 7440-02-0 7782-49-2 75-34-3 95-50-1 78-87-5 106-46-7 67-64-1 71-43-2 108-90-7 75-00-3 156-59-2 100-41-4 78-93-3 156-60-5 79-01-6 1330-20-7 SW320 SW330 7782-44-7
SWS ID 15 34 51 54 131 152 183 75 69 82 71 3 16 39 41 78 110 141 79 201 346 320 330 356
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU mg/L
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Monitoring Well Samples
MW-01 OLD 04/14/2016 459 0.500 U 5.7 J 7.3 J 7.0 J 11.2 J 7.0 J 1.69 J 0.345 J 0.372 J 4.79 2.66 U 1.30 2.58 J 1.75 J 3.94 J 0.190 U 2.64 U 0.230 U 0.392 J 0.580 U 6.11 115 2.88
MW-02 OLD 04/14/2016 49.1 J 0.500 U 3.00 U 5.00 U 2.00 U 3.00 U 5.00 U 0.589 J 0.190 U 0.250 U 0.170 U 3.13 J 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 2.64 U 0.230 U 0.200 U 0.580 U 7.41 8.53 5.62
MW-03 OLD 04/14/2016 1,060 0.500 U 3.00 U 5.00 U 13.8 15.7 J 7.3 J 0.240 U 0.190 U 0.250 U 4.40 2.66 U 1.72 6.66 0.781 J 0.210 U 1.03 2.64 U 0.230 U 0.200 U 0.580 U 6.32 2.33 0.30
MW-04 OLD 04/14/2016 864 0.500 U 3.00 U 12.8 4.2 J 82.6 7.5 J 0.267 J 0.190 U 0.250 U 1.64 4.33 J 0.320 J 3.10 0.679 J 0.287 J 0.190 U 3.85 J 0.230 U 0.200 U 0.787 J 6.20 14.7 0.82
BG SPRING OLD 04/14/2016 356 1.90 30.8 39.6 7.9 J 40.6 J 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 2.64 U 0.230 U 0.200 U 0.580 U 5.88 137 2.79
Domestic Well Samples
DW-01 OLD 04/13/2016 219 0.500 U 3.00 U 57 6.7 J 3.00 U 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 2.64 U 0.230 U 0.200 U 0.580 U 6.31 2.80 3.83
Surface Water Samples
SW-01 OLD 04/13/2016 78.1 J 0.500 U 3.00 U 5.00 U 2.00 U 3.00 U 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 2.64 U 0.230 U 0.200 U 0.838 J 7.06 3.09 4.78
SW-02 OLD 04/13/2016 54.5 J 0.500 U 3.00 U 5.00 U 2.00 U 3.00 U 5.00 U 0.240 U 0.190 U 0.250 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 2.64 U 0.230 U 0.200 U 0.580 U 7.38 7.53 4.36
Quality Control Samples
TRIP BLANK 04/13/2016 NA NA NA NA NA NA NA 0.240 U 0.190 U 0.250 U 0.170 U 8.20 J 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 2.64 U 0.828 J 0.200 U 0.580 U NA NA NA
MDL 5.00 0.500 3.00 5.00 2.00 3.00 5.00 0.240 0.190 0.250 0.170 2.66 0.200 0.180 0.360 0.210 0.190 2.640 0.230 0.200 0.580 NA NA NA
MRL 10.0 1.00 5.0 10.0 5.0 10.0 10.0 1.0 1.0 1.0 1.0 25.0 1.0 1.0 1.0 1.0 1.0 50.0 1.0 1.0 3.0 NA NA NE
SWSL 100 1.00 10 10 10 50 10 5 5 1 1 100 1 3 10 5 1 100 5 1 5 NE NE NE
2L 700 2.00 10 1,000 15 100 20 6 20 0.6 6 6,000 1 50 3,000 70 600 4,000 100 3 500 6.5-8.5 NE NE
IMAC NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE 60 NE NE NE NE NE NE NE NE
GWPS NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
2B 200,000 0.15 35 2.7 0.54 16 5 100 470 15 100 2,000 51 140 NE 720 97 750,000 10,000 3 670 6.0-9.0 50 > 5.0
Notes:
Detections Only detected constituents are listed on this table. Please refer to the TestAmerica laboratory analysis reports for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID The Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, and milligrams per liter (mg/L) for dissolved oxygen.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL.
J Assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
2L
IMAC Interim Maximum Allowable Concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
GWPS
2B
NE Not Established
NA Not Applicable
459 Indicates a result in exceedance of the SWSL.
1.30 Indicates a result in exceedance of the 2L, IMAC, GWP, or 2B standard.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ (amended April 1,
2013).
"GWPS" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from the NC DEQ Solid Waste Section Environmental Monitoring List (last
updated June 13, 2011). GWPS is used only if 2L or IMAC standards are not established for specific constituent.
"2B" indicates surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards" (last amended
March, 2016) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
P:\Madison County\Analytical & Data\Water\2016\58-02 Closed\Tables\5802April2016_Tables Page 1 of 1

APPENDICES

APPENDIX A

Sampling Logs and
Equipment Documentation
and Instrument Calibration Data Sheets

APPENDIX B

Report of Laboratory Analysis
and Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-101753-1
Client Project/Site: Madison Co Closed Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
4/26/2016 4:54:10 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
TestAmerica Job ID: 490-101753-1
Page 2 of 45 TestAmerica Nashville4/26/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
1
2
3
4
5
6
7
8
9
10
11
12
13
Sample Summary
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-101753-1 MW-01 OLD Water 04/14/16 09:50 04/15/16 10:30
490-101753-2 MW-02 OLD Water 04/14/16 13:20 04/15/16 10:30
490-101753-3 MW-03 OLD Water 04/14/16 11:28 04/15/16 10:30
490-101753-4 MW-04 OLD Water 04/14/16 12:22 04/15/16 10:30
490-101753-5 BG Springs OLD Water 04/14/16 13:55 04/15/16 10:30
490-101753-6 SW-01 OLD Water 04/13/16 15:15 04/15/16 10:30
490-101753-7 SW-02 OLD Water 04/13/16 15:30 04/15/16 10:30
490-101753-8 DW-01 OLD Water 04/13/16 14:57 04/15/16 10:30
490-101753-9 Trip Blank Water 04/13/16 00:01 04/15/16 10:30
TestAmerica Nashville
Page 3 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101753-1
Project/Site: Madison Co Closed Landfill
Job ID: 490-101753-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-101753-1
Comments
No additional comments.
Receipt
The samples were received on 4/15/2016 10:30 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 5.1º C.
GC/MS VOA
Method(s) 8260B: Sample was received with approximately 0.1ml of headspace. Trip Blank (490-101753-9)
Method(s) 8260B: The method blank for analytical batch 490-333637 contained Carbon disulfide above the method detection limit. This
target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not
performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Definitions/Glossary
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-1Client Sample ID: MW-01 OLD
Matrix: WaterDate Collected: 04/14/16 09:50
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 22:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/21/16 22:51 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 22:51 1Benzene1.30
1.00 0.150 ug/L 04/21/16 22:51 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 22:51 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 22:51 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 22:51 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 22:51 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 22:51 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 22:51 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 22:51 1Chlorobenzene2.58
1.00 0.360 ug/L 04/21/16 22:51 1Chloroethane1.75
1.00 0.230 ug/L 04/21/16 22:51 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 22:51 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 22:51 1cis-1,2-Dichloroethene 3.94
1.00 0.170 ug/L 04/21/16 22:51 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 22:51 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 22:51 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 22:51 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 22:51 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 22:51 11,2-Dichlorobenzene 0.345 J
1.00 0.170 ug/L 04/21/16 22:51 11,4-Dichlorobenzene 4.79
1.00 0.240 ug/L 04/21/16 22:51 11,1-Dichloroethane 1.69
1.00 0.200 ug/L 04/21/16 22:51 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 22:51 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 22:51 11,2-Dichloropropane 0.372 J
1.00 0.190 ug/L 04/21/16 22:51 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 22:51 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 22:51 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 22:51 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 22:51 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 22:51 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 22:51 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 22:51 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 22:51 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/21/16 22:51 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 22:51 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 22:51 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 22:51 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 22:51 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 22:51 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 22:51 1Trichloroethene0.392 J
1.00 0.210 ug/L 04/21/16 22:51 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 22:51 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 22:51 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 22:51 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 22:51 1Xylenes, Total <0.580
TestAmerica Nashville
Page 6 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-1Client Sample ID: MW-01 OLD
Matrix: WaterDate Collected: 04/14/16 09:50
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)106 70-130 04/21/16 22:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)107 04/21/16 22:51 170-130
1,2-Dichloroethane-d4 (Surr)118 04/21/16 22:51 170-130
Toluene-d8 (Surr)99 04/21/16 22:51 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/21/16 20:27 04/23/16 17:18 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:18 1Barium0.459
0.00100 0.000500 mg/L 04/21/16 20:27 04/23/16 17:18 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:18 1Chromium0.00570
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:18 1Copper0.00730 J
0.00500 0.00200 mg/L 04/21/16 20:27 04/23/16 17:18 1Lead0.00700
0.0100 0.00300 mg/L 04/21/16 20:27 04/23/16 17:18 1Nickel0.0112
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:18 1Selenium0.00700 J
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:18 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 7 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-2Client Sample ID: MW-02 OLD
Matrix: WaterDate Collected: 04/14/16 13:20
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 3.13 J 25.0 2.66 ug/L 04/21/16 23:20 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/21/16 23:20 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 23:20 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 23:20 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 23:20 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 23:20 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 23:20 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 23:20 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 23:20 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 23:20 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 23:20 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 23:20 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 23:20 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 23:20 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 23:20 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 23:20 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 23:20 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 23:20 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 23:20 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 23:20 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 23:20 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 23:20 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 23:20 11,1-Dichloroethane 0.589 J
1.00 0.200 ug/L 04/21/16 23:20 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 23:20 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 23:20 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 23:20 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 23:20 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 23:20 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 23:20 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 23:20 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 23:20 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 23:20 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 23:20 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 23:20 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/21/16 23:20 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 23:20 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 23:20 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 23:20 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 23:20 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 23:20 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 23:20 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 23:20 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 23:20 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 23:20 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 23:20 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 23:20 1Xylenes, Total <0.580
TestAmerica Nashville
Page 8 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-2Client Sample ID: MW-02 OLD
Matrix: WaterDate Collected: 04/14/16 13:20
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)106 70-130 04/21/16 23:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)103 04/21/16 23:20 170-130
1,2-Dichloroethane-d4 (Surr)116 04/21/16 23:20 170-130
Toluene-d8 (Surr)102 04/21/16 23:20 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/21/16 20:27 04/23/16 17:22 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:22 1Barium0.0491
0.00100 0.000500 mg/L 04/21/16 20:27 04/23/16 17:22 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:22 1Chromium<0.00300
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:22 1Copper<0.00500
0.00500 0.00200 mg/L 04/21/16 20:27 04/23/16 17:22 1Lead<0.00200
0.0100 0.00300 mg/L 04/21/16 20:27 04/23/16 17:22 1Nickel<0.00300
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:22 1Selenium<0.00500
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:22 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 9 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-3Client Sample ID: MW-03 OLD
Matrix: WaterDate Collected: 04/14/16 11:28
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 23:48 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/21/16 23:48 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 23:48 1Benzene1.72
1.00 0.150 ug/L 04/21/16 23:48 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 23:48 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 23:48 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 23:48 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 23:48 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 23:48 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 23:48 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 23:48 1Chlorobenzene6.66
1.00 0.360 ug/L 04/21/16 23:48 1Chloroethane0.781 J
1.00 0.230 ug/L 04/21/16 23:48 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 23:48 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 23:48 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 23:48 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 23:48 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 23:48 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 23:48 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 23:48 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 23:48 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 23:48 11,4-Dichlorobenzene 4.40
1.00 0.240 ug/L 04/21/16 23:48 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 23:48 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 23:48 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 23:48 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 23:48 1Ethylbenzene1.03
10.0 1.28 ug/L 04/21/16 23:48 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 23:48 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 23:48 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 23:48 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 23:48 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 23:48 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 23:48 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 23:48 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/21/16 23:48 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 23:48 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 23:48 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 23:48 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 23:48 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 23:48 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 23:48 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 23:48 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 23:48 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 23:48 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 23:48 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 23:48 1Xylenes, Total <0.580
TestAmerica Nashville
Page 10 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-3Client Sample ID: MW-03 OLD
Matrix: WaterDate Collected: 04/14/16 11:28
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)102 70-130 04/21/16 23:48 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 04/21/16 23:48 170-130
1,2-Dichloroethane-d4 (Surr)115 04/21/16 23:48 170-130
Toluene-d8 (Surr)100 04/21/16 23:48 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/21/16 20:27 04/23/16 17:26 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:26 1Barium1.06
0.00100 0.000500 mg/L 04/21/16 20:27 04/23/16 17:26 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:26 1Chromium<0.00300
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:26 1Copper<0.00500
0.00500 0.00200 mg/L 04/21/16 20:27 04/23/16 17:26 1Lead0.0138
0.0100 0.00300 mg/L 04/21/16 20:27 04/23/16 17:26 1Nickel0.0157
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:26 1Selenium0.00730 J
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:26 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 19:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 11 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-4Client Sample ID: MW-04 OLD
Matrix: WaterDate Collected: 04/14/16 12:22
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 4.33 J 25.0 2.66 ug/L 04/22/16 00:16 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/22/16 00:16 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/22/16 00:16 1Benzene0.320 J
1.00 0.150 ug/L 04/22/16 00:16 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/22/16 00:16 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/22/16 00:16 1Bromoform<0.290
1.00 0.350 ug/L 04/22/16 00:16 1Bromomethane<0.350
50.0 2.64 ug/L 04/22/16 00:16 12-Butanone (MEK)3.85 J
1.00 0.220 ug/L 04/22/16 00:16 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/22/16 00:16 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/22/16 00:16 1Chlorobenzene3.10
1.00 0.360 ug/L 04/22/16 00:16 1Chloroethane0.679 J
1.00 0.230 ug/L 04/22/16 00:16 1Chloroform<0.230
1.00 0.360 ug/L 04/22/16 00:16 1Chloromethane<0.360
1.00 0.210 ug/L 04/22/16 00:16 1cis-1,2-Dichloroethene 0.287 J
1.00 0.170 ug/L 04/22/16 00:16 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/22/16 00:16 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/22/16 00:16 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/22/16 00:16 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/22/16 00:16 1Dibromomethane<0.450
1.00 0.190 ug/L 04/22/16 00:16 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/22/16 00:16 11,4-Dichlorobenzene 1.64
1.00 0.240 ug/L 04/22/16 00:16 11,1-Dichloroethane 0.267 J
1.00 0.200 ug/L 04/22/16 00:16 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/22/16 00:16 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/22/16 00:16 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/22/16 00:16 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/22/16 00:16 12-Hexanone <1.28
10.0 1.50 ug/L 04/22/16 00:16 1Iodomethane<1.50
5.00 1.00 ug/L 04/22/16 00:16 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/22/16 00:16 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/22/16 00:16 1Styrene<0.280
1.00 0.150 ug/L 04/22/16 00:16 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/22/16 00:16 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/22/16 00:16 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/22/16 00:16 1Toluene<0.170
5.00 0.460 ug/L 04/22/16 00:16 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/22/16 00:16 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/22/16 00:16 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/22/16 00:16 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/22/16 00:16 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/22/16 00:16 1Trichloroethene<0.200
1.00 0.210 ug/L 04/22/16 00:16 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/22/16 00:16 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/22/16 00:16 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/22/16 00:16 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/22/16 00:16 1Xylenes, Total 0.787 J
TestAmerica Nashville
Page 12 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-4Client Sample ID: MW-04 OLD
Matrix: WaterDate Collected: 04/14/16 12:22
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)105 70-130 04/22/16 00:16 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)108 04/22/16 00:16 170-130
1,2-Dichloroethane-d4 (Surr)116 04/22/16 00:16 170-130
Toluene-d8 (Surr)100 04/22/16 00:16 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/21/16 20:27 04/23/16 17:30 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:30 1Barium0.864
0.00100 0.000500 mg/L 04/21/16 20:27 04/23/16 17:30 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:30 1Chromium<0.00300
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:30 1Copper0.0128
0.00500 0.00200 mg/L 04/21/16 20:27 04/23/16 17:30 1Lead0.00420 J
0.0100 0.00300 mg/L 04/21/16 20:27 04/23/16 17:30 1Nickel0.0826
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:30 1Selenium0.00750 J
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:30 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 19:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 13 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-5Client Sample ID: BG Springs OLD
Matrix: WaterDate Collected: 04/14/16 13:55
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 22:23 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/21/16 22:23 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 22:23 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 22:23 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 22:23 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 22:23 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 22:23 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 22:23 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 22:23 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 22:23 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 22:23 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 22:23 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 22:23 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 22:23 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 22:23 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 22:23 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 22:23 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 22:23 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 22:23 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 22:23 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 22:23 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 22:23 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 22:23 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 22:23 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 22:23 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 22:23 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 22:23 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 22:23 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 22:23 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 22:23 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 22:23 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 22:23 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 22:23 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 22:23 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 22:23 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/21/16 22:23 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 22:23 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 22:23 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 22:23 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 22:23 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 22:23 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 22:23 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 22:23 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 22:23 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 22:23 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 22:23 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 22:23 1Xylenes, Total <0.580
TestAmerica Nashville
Page 14 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-5Client Sample ID: BG Springs OLD
Matrix: WaterDate Collected: 04/14/16 13:55
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)105 70-130 04/21/16 22:23 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 04/21/16 22:23 170-130
1,2-Dichloroethane-d4 (Surr)114 04/21/16 22:23 170-130
Toluene-d8 (Surr)101 04/21/16 22:23 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/21/16 20:27 04/23/16 17:35 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:35 1Barium0.356
0.00100 0.000500 mg/L 04/21/16 20:27 04/23/16 17:35 1Cadmium0.00190
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:35 1Chromium0.0308
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:35 1Copper0.0396
0.00500 0.00200 mg/L 04/21/16 20:27 04/23/16 17:35 1Lead0.00790
0.0100 0.00300 mg/L 04/21/16 20:27 04/23/16 17:35 1Nickel0.0406
0.0100 0.00500 mg/L 04/21/16 20:27 04/23/16 17:35 1Selenium<0.00500
0.00500 0.00300 mg/L 04/21/16 20:27 04/23/16 17:35 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 19:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 15 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-6Client Sample ID: SW-01 OLD
Matrix: WaterDate Collected: 04/13/16 15:15
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/22/16 00:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/22/16 00:45 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/22/16 00:45 1Benzene<0.200
1.00 0.150 ug/L 04/22/16 00:45 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/22/16 00:45 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/22/16 00:45 1Bromoform<0.290
1.00 0.350 ug/L 04/22/16 00:45 1Bromomethane<0.350
50.0 2.64 ug/L 04/22/16 00:45 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/22/16 00:45 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/22/16 00:45 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/22/16 00:45 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/22/16 00:45 1Chloroethane<0.360
1.00 0.230 ug/L 04/22/16 00:45 1Chloroform<0.230
1.00 0.360 ug/L 04/22/16 00:45 1Chloromethane<0.360
1.00 0.210 ug/L 04/22/16 00:45 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/22/16 00:45 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/22/16 00:45 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/22/16 00:45 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/22/16 00:45 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/22/16 00:45 1Dibromomethane<0.450
1.00 0.190 ug/L 04/22/16 00:45 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/22/16 00:45 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/22/16 00:45 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/22/16 00:45 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/22/16 00:45 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/22/16 00:45 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/22/16 00:45 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/22/16 00:45 12-Hexanone <1.28
10.0 1.50 ug/L 04/22/16 00:45 1Iodomethane<1.50
5.00 1.00 ug/L 04/22/16 00:45 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/22/16 00:45 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/22/16 00:45 1Styrene<0.280
1.00 0.150 ug/L 04/22/16 00:45 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/22/16 00:45 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/22/16 00:45 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/22/16 00:45 1Toluene<0.170
5.00 0.460 ug/L 04/22/16 00:45 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/22/16 00:45 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/22/16 00:45 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/22/16 00:45 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/22/16 00:45 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/22/16 00:45 1Trichloroethene<0.200
1.00 0.210 ug/L 04/22/16 00:45 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/22/16 00:45 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/22/16 00:45 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/22/16 00:45 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/22/16 00:45 1Xylenes, Total 0.838 J
TestAmerica Nashville
Page 16 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-6Client Sample ID: SW-01 OLD
Matrix: WaterDate Collected: 04/13/16 15:15
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)106 70-130 04/22/16 00:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)112 04/22/16 00:45 170-130
1,2-Dichloroethane-d4 (Surr)118 04/22/16 00:45 170-130
Toluene-d8 (Surr)101 04/22/16 00:45 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 16:45 04/21/16 12:30 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:30 1Barium0.0781
0.00100 0.000500 mg/L 04/20/16 16:45 04/21/16 12:30 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 16:45 04/21/16 12:30 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:30 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 16:45 04/21/16 12:30 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 16:45 04/21/16 12:30 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:30 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 16:45 04/21/16 12:30 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 19:14 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 17 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-7Client Sample ID: SW-02 OLD
Matrix: WaterDate Collected: 04/13/16 15:30
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/22/16 01:13 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/22/16 01:13 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/22/16 01:13 1Benzene<0.200
1.00 0.150 ug/L 04/22/16 01:13 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/22/16 01:13 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/22/16 01:13 1Bromoform<0.290
1.00 0.350 ug/L 04/22/16 01:13 1Bromomethane<0.350
50.0 2.64 ug/L 04/22/16 01:13 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/22/16 01:13 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/22/16 01:13 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/22/16 01:13 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/22/16 01:13 1Chloroethane<0.360
1.00 0.230 ug/L 04/22/16 01:13 1Chloroform<0.230
1.00 0.360 ug/L 04/22/16 01:13 1Chloromethane<0.360
1.00 0.210 ug/L 04/22/16 01:13 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/22/16 01:13 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/22/16 01:13 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/22/16 01:13 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/22/16 01:13 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/22/16 01:13 1Dibromomethane<0.450
1.00 0.190 ug/L 04/22/16 01:13 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/22/16 01:13 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/22/16 01:13 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/22/16 01:13 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/22/16 01:13 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/22/16 01:13 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/22/16 01:13 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/22/16 01:13 12-Hexanone <1.28
10.0 1.50 ug/L 04/22/16 01:13 1Iodomethane<1.50
5.00 1.00 ug/L 04/22/16 01:13 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/22/16 01:13 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/22/16 01:13 1Styrene<0.280
1.00 0.150 ug/L 04/22/16 01:13 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/22/16 01:13 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/22/16 01:13 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/22/16 01:13 1Toluene<0.170
5.00 0.460 ug/L 04/22/16 01:13 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/22/16 01:13 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/22/16 01:13 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/22/16 01:13 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/22/16 01:13 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/22/16 01:13 1Trichloroethene<0.200
1.00 0.210 ug/L 04/22/16 01:13 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/22/16 01:13 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/22/16 01:13 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/22/16 01:13 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/22/16 01:13 1Xylenes, Total <0.580
TestAmerica Nashville
Page 18 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-7Client Sample ID: SW-02 OLD
Matrix: WaterDate Collected: 04/13/16 15:30
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)105 70-130 04/22/16 01:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)111 04/22/16 01:13 170-130
1,2-Dichloroethane-d4 (Surr)117 04/22/16 01:13 170-130
Toluene-d8 (Surr)101 04/22/16 01:13 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 16:45 04/21/16 12:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:34 1Barium0.0545
0.00100 0.000500 mg/L 04/20/16 16:45 04/21/16 12:34 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 16:45 04/21/16 12:34 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:34 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 16:45 04/21/16 12:34 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 16:45 04/21/16 12:34 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:34 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 16:45 04/21/16 12:34 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:01 04/19/16 17:46 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 19 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-8Client Sample ID: DW-01 OLD
Matrix: WaterDate Collected: 04/13/16 14:57
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/22/16 01:42 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/22/16 01:42 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/22/16 01:42 1Benzene<0.200
1.00 0.150 ug/L 04/22/16 01:42 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/22/16 01:42 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/22/16 01:42 1Bromoform<0.290
1.00 0.350 ug/L 04/22/16 01:42 1Bromomethane<0.350
50.0 2.64 ug/L 04/22/16 01:42 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/22/16 01:42 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/22/16 01:42 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/22/16 01:42 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/22/16 01:42 1Chloroethane<0.360
1.00 0.230 ug/L 04/22/16 01:42 1Chloroform<0.230
1.00 0.360 ug/L 04/22/16 01:42 1Chloromethane<0.360
1.00 0.210 ug/L 04/22/16 01:42 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/22/16 01:42 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/22/16 01:42 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/22/16 01:42 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/22/16 01:42 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/22/16 01:42 1Dibromomethane<0.450
1.00 0.190 ug/L 04/22/16 01:42 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/22/16 01:42 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/22/16 01:42 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/22/16 01:42 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/22/16 01:42 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/22/16 01:42 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/22/16 01:42 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/22/16 01:42 12-Hexanone <1.28
10.0 1.50 ug/L 04/22/16 01:42 1Iodomethane<1.50
5.00 1.00 ug/L 04/22/16 01:42 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/22/16 01:42 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/22/16 01:42 1Styrene<0.280
1.00 0.150 ug/L 04/22/16 01:42 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/22/16 01:42 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/22/16 01:42 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/22/16 01:42 1Toluene<0.170
5.00 0.460 ug/L 04/22/16 01:42 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/22/16 01:42 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/22/16 01:42 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/22/16 01:42 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/22/16 01:42 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/22/16 01:42 1Trichloroethene<0.200
1.00 0.210 ug/L 04/22/16 01:42 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/22/16 01:42 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/22/16 01:42 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/22/16 01:42 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/22/16 01:42 1Xylenes, Total <0.580
TestAmerica Nashville
Page 20 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-8Client Sample ID: DW-01 OLD
Matrix: WaterDate Collected: 04/13/16 14:57
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)107 70-130 04/22/16 01:42 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)111 04/22/16 01:42 170-130
1,2-Dichloroethane-d4 (Surr)114 04/22/16 01:42 170-130
Toluene-d8 (Surr)100 04/22/16 01:42 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 16:45 04/21/16 12:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:39 1Barium0.219
0.00100 0.000500 mg/L 04/20/16 16:45 04/21/16 12:39 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 16:45 04/21/16 12:39 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:39 1Copper0.0570
0.00500 0.00200 mg/L 04/20/16 16:45 04/21/16 12:39 1Lead0.00670
0.0100 0.00300 mg/L 04/20/16 16:45 04/21/16 12:39 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 16:45 04/21/16 12:39 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 16:45 04/21/16 12:39 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:01 04/19/16 17:48 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
TestAmerica Nashville
Page 21 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-9Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/13/16 00:01
Date Received: 04/15/16 10:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 8.20 J 25.0 2.66 ug/L 04/21/16 21:54 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/21/16 21:54 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 21:54 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 21:54 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 21:54 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 21:54 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 21:54 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 21:54 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 21:54 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 21:54 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 21:54 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 21:54 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 21:54 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 21:54 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 21:54 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 21:54 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 21:54 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 21:54 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 21:54 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 21:54 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 21:54 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 21:54 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 21:54 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 21:54 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 21:54 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 21:54 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 21:54 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 21:54 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 21:54 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 21:54 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 21:54 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 21:54 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 21:54 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 21:54 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 21:54 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/21/16 21:54 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 21:54 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 21:54 1trans-1,2-Dichloroethene 0.828 J
1.00 0.170 ug/L 04/21/16 21:54 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 21:54 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 21:54 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 21:54 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 21:54 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 21:54 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 21:54 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 21:54 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 21:54 1Xylenes, Total <0.580
TestAmerica Nashville
Page 22 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-101753-9Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/13/16 00:01
Date Received: 04/15/16 10:30
4-Bromofluorobenzene (Surr)107 70-130 04/21/16 21:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)104 04/21/16 21:54 170-130
1,2-Dichloroethane-d4 (Surr)112 04/21/16 21:54 170-130
Toluene-d8 (Surr)100 04/21/16 21:54 170-130
TestAmerica Nashville
Page 23 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-333637/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 21:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 04/21/16 21:26 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/21/16 21:26 1Benzene
<0.150 0.1501.00 ug/L 04/21/16 21:26 1Bromochloromethane
<0.170 0.1701.00 ug/L 04/21/16 21:26 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/21/16 21:26 1Bromoform
<0.350 0.3501.00 ug/L 04/21/16 21:26 1Bromomethane
<2.64 2.6450.0 ug/L 04/21/16 21:26 12-Butanone (MEK)
0.4830 J 0.2201.00 ug/L 04/21/16 21:26 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/21/16 21:26 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/21/16 21:26 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/21/16 21:26 1Chloroethane
<0.230 0.2301.00 ug/L 04/21/16 21:26 1Chloroform
<0.360 0.3601.00 ug/L 04/21/16 21:26 1Chloromethane
<0.210 0.2101.00 ug/L 04/21/16 21:26 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/21/16 21:26 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/21/16 21:26 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/21/16 21:26 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/21/16 21:26 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/21/16 21:26 1Dibromomethane
<0.190 0.1901.00 ug/L 04/21/16 21:26 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/21/16 21:26 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/21/16 21:26 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/21/16 21:26 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/21/16 21:26 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/21/16 21:26 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/21/16 21:26 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/21/16 21:26 12-Hexanone
<1.50 1.5010.0 ug/L 04/21/16 21:26 1Iodomethane
<1.00 1.005.00 ug/L 04/21/16 21:26 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/21/16 21:26 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/21/16 21:26 1Styrene
<0.150 0.1501.00 ug/L 04/21/16 21:26 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/21/16 21:26 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/21/16 21:26 1Tetrachloroethene
<0.170 0.1701.00 ug/L 04/21/16 21:26 1Toluene
<0.460 0.4605.00 ug/L 04/21/16 21:26 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/21/16 21:26 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/21/16 21:26 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 04/21/16 21:26 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/21/16 21:26 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/21/16 21:26 1Trichloroethene
<0.210 0.2101.00 ug/L 04/21/16 21:26 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/21/16 21:26 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/21/16 21:26 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/21/16 21:26 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/21/16 21:26 1Xylenes, Total
TestAmerica Nashville
Page 24 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-333637/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
4-Bromofluorobenzene (Surr)106 70-130 04/21/16 21:26 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
107 04/21/16 21:26 1Dibromofluoromethane (Surr)70 -130
111 04/21/16 21:26 11,2-Dichloroethane-d4 (Surr)70 -130
101 04/21/16 21:26 1Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333637/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
Acetone 250 295.5 ug/L 118 39 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 577.0 ug/L 115 63 -135
Benzene 50.0 51.41 ug/L 103 70 -130
Bromochloromethane 50.0 53.91 ug/L 108 70 -130
Bromodichloromethane 50.0 55.40 ug/L 111 70 -130
Bromoform 50.0 51.83 ug/L 104 70 -137
Bromomethane 50.0 49.56 ug/L 99 53 -150
2-Butanone (MEK)250 291.7 ug/L 117 55 -143
Carbon disulfide 50.0 50.13 ug/L 100 64 -135
Carbon tetrachloride 50.0 52.73 ug/L 105 70 -147
Chlorobenzene 50.0 51.38 ug/L 103 70 -130
Chloroethane 50.0 51.71 ug/L 103 60 -138
Chloroform 50.0 55.01 ug/L 110 70 -130
Chloromethane 50.0 47.08 ug/L 94 33 -150
cis-1,2-Dichloroethene 50.0 58.85 ug/L 118 70 -130
cis-1,3-Dichloropropene 50.0 57.16 ug/L 114 70 -133
Dibromochloromethane 50.0 53.66 ug/L 107 70 -133
1,2-Dibromo-3-Chloropropane 50.0 50.69 ug/L 101 45 -138
1,2-Dibromoethane (EDB)50.0 51.71 ug/L 103 70 -130
Dibromomethane 50.0 52.65 ug/L 105 70 -130
1,2-Dichlorobenzene 50.0 52.18 ug/L 104 70 -130
1,4-Dichlorobenzene 50.0 52.16 ug/L 104 70 -130
1,1-Dichloroethane 50.0 57.87 ug/L 116 70 -130
1,2-Dichloroethane 50.0 60.20 ug/L 120 70 -130
1,1-Dichloroethene 50.0 52.43 ug/L 105 70 -132
1,2-Dichloropropane 50.0 50.68 ug/L 101 70 -130
Ethylbenzene 50.0 54.22 ug/L 108 70 -130
2-Hexanone 250 282.5 ug/L 113 54 -142
Iodomethane 50.0 61.80 ug/L 124 40 -150
Methylene Chloride 50.0 52.58 ug/L 105 70 -130
4-Methyl-2-pentanone (MIBK)250 284.7 ug/L 114 60 -137
Styrene 50.0 57.16 ug/L 114 70 -130
1,1,1,2-Tetrachloroethane 50.0 51.09 ug/L 102 70 -130
1,1,2,2-Tetrachloroethane 50.0 52.00 ug/L 104 69 -131
Tetrachloroethene 50.0 50.79 ug/L 102 70 -130
Toluene 50.0 52.97 ug/L 106 70 -130
trans-1,4-Dichloro-2-butene 50.0 56.53 ug/L 113 41 -150
trans-1,2-Dichloroethene 50.0 58.24 ug/L 116 70 -130
TestAmerica Nashville
Page 25 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333637/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
trans-1,3-Dichloropropene 50.0 58.91 ug/L 118 63 -142
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 53.66 ug/L 107 70 -135
1,1,2-Trichloroethane 50.0 52.65 ug/L 105 70 -130
Trichloroethene 50.0 51.26 ug/L 103 70 -130
Trichlorofluoromethane 50.0 57.71 ug/L 115 59 -150
1,2,3-Trichloropropane 50.0 56.99 ug/L 114 70 -131
Vinyl acetate 100 110.6 ug/L 111 54 -146
Vinyl chloride 50.0 50.97 ug/L 102 57 -137
Xylenes, Total 100 111.9 ug/L 112 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1051,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-333637/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
Acetone 250 286.9 ug/L 115 39 -150 3 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 562.6 ug/L 113 63 -135 3 16
Benzene 50.0 50.18 ug/L 100 70 -130 2 12
Bromochloromethane 50.0 53.29 ug/L 107 70 -130 1 16
Bromodichloromethane 50.0 53.97 ug/L 108 70 -130 3 14
Bromoform 50.0 51.44 ug/L 103 70 -137 1 14
Bromomethane 50.0 48.60 ug/L 97 53 -150 2 19
2-Butanone (MEK)250 286.4 ug/L 115 55 -143 2 19
Carbon disulfide 50.0 49.12 ug/L 98 64 -135 2 16
Carbon tetrachloride 50.0 50.79 ug/L 102 70 -147 4 16
Chlorobenzene 50.0 50.83 ug/L 102 70 -130 1 12
Chloroethane 50.0 50.27 ug/L 101 60 -138 3 15
Chloroform 50.0 53.99 ug/L 108 70 -130 2 14
Chloromethane 50.0 45.27 ug/L 91 33 -150 4 20
cis-1,2-Dichloroethene 50.0 57.19 ug/L 114 70 -130 3 15
cis-1,3-Dichloropropene 50.0 57.13 ug/L 114 70 -133 0 15
Dibromochloromethane 50.0 52.76 ug/L 106 70 -133 2 13
1,2-Dibromo-3-Chloropropane 50.0 48.45 ug/L 97 45 -138 5 19
1,2-Dibromoethane (EDB)50.0 52.60 ug/L 105 70 -130 2 13
Dibromomethane 50.0 52.11 ug/L 104 70 -130 1 14
1,2-Dichlorobenzene 50.0 51.71 ug/L 103 70 -130 1 12
1,4-Dichlorobenzene 50.0 51.59 ug/L 103 70 -130 1 12
1,1-Dichloroethane 50.0 56.02 ug/L 112 70 -130 3 17
1,2-Dichloroethane 50.0 58.39 ug/L 117 70 -130 3 13
1,1-Dichloroethene 50.0 50.66 ug/L 101 70 -132 3 20
1,2-Dichloropropane 50.0 50.02 ug/L 100 70 -130 1 15
Ethylbenzene 50.0 54.47 ug/L 109 70 -130 0 12
TestAmerica Nashville
Page 26 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-333637/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
2-Hexanone 250 279.3 ug/L 112 54 -142 1 17
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Iodomethane 50.0 59.89 ug/L 120 40 -150 3 20
Methylene Chloride 50.0 50.57 ug/L 101 70 -130 4 15
4-Methyl-2-pentanone (MIBK)250 285.6 ug/L 114 60 -137 0 21
Styrene 50.0 57.06 ug/L 114 70 -130 0 12
1,1,1,2-Tetrachloroethane 50.0 50.78 ug/L 102 70 -130 1 13
1,1,2,2-Tetrachloroethane 50.0 51.73 ug/L 103 69 -131 1 15
Tetrachloroethene 50.0 50.78 ug/L 102 70 -130 0 17
Toluene 50.0 52.68 ug/L 105 70 -130 1 13
trans-1,4-Dichloro-2-butene 50.0 53.46 ug/L 107 41 -150 6 20
trans-1,2-Dichloroethene 50.0 57.44 ug/L 115 70 -130 1 15
trans-1,3-Dichloropropene 50.0 60.06 ug/L 120 63 -142 2 13
1,1,1-Trichloroethane 50.0 52.33 ug/L 105 70 -135 3 15
1,1,2-Trichloroethane 50.0 51.78 ug/L 104 70 -130 2 13
Trichloroethene 50.0 50.96 ug/L 102 70 -130 1 14
Trichlorofluoromethane 50.0 55.06 ug/L 110 59 -150 5 22
1,2,3-Trichloropropane 50.0 54.50 ug/L 109 70 -131 4 14
Vinyl acetate 100 106.2 ug/L 106 54 -146 4 20
Vinyl chloride 50.0 50.67 ug/L 101 57 -137 1 15
Xylenes, Total 100 111.4 ug/L 111 70 -132 0 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1041,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: BG Springs OLDLab Sample ID: 490-101753-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
Acetone <2.66 250 289.2 ug/L 116 39 -150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 580.0 ug/L 116 50 -135
Benzene <0.200 50.0 50.96 ug/L 102 55 -147
Bromochloromethane <0.150 50.0 55.83 ug/L 112 59 -132
Bromodichloromethane <0.170 50.0 57.44 ug/L 115 70 -140
Bromoform <0.290 50.0 53.37 ug/L 107 53 -150
Bromomethane <0.350 50.0 47.63 ug/L 95 30 -150
2-Butanone (MEK)<2.64 250 291.4 ug/L 117 50 -143
Carbon disulfide <0.220 50.0 43.53 ug/L 87 35 -150
Carbon tetrachloride <0.180 50.0 55.47 ug/L 111 56 -150
Chlorobenzene <0.180 50.0 52.72 ug/L 105 70 -130
Chloroethane <0.360 50.0 52.40 ug/L 105 58 -141
Chloroform <0.230 50.0 57.16 ug/L 114 66 -138
Chloromethane <0.360 50.0 45.49 ug/L 91 10 -150
cis-1,2-Dichloroethene <0.210 50.0 59.10 ug/L 118 68 -131
cis-1,3-Dichloropropene <0.170 50.0 57.21 ug/L 114 70 -133
TestAmerica Nashville
Page 27 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: BG Springs OLDLab Sample ID: 490-101753-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
Dibromochloromethane <0.250 50.0 54.87 ug/L 110 66 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane <0.940 50.0 48.09 ug/L 96 38 -138
1,2-Dibromoethane (EDB)<0.210 50.0 52.44 ug/L 105 65 -137
Dibromomethane <0.450 50.0 54.08 ug/L 108 70 -130
1,2-Dichlorobenzene <0.190 50.0 53.72 ug/L 107 70 -130
1,4-Dichlorobenzene <0.170 50.0 52.82 ug/L 106 70 -130
1,1-Dichloroethane <0.240 50.0 60.37 ug/L 121 61 -139
1,2-Dichloroethane <0.200 50.0 60.62 ug/L 121 64 -136
1,1-Dichloroethene <0.250 50.0 53.57 ug/L 107 54 -150
1,2-Dichloropropane <0.250 50.0 53.28 ug/L 107 67 -130
Ethylbenzene <0.190 50.0 55.71 ug/L 111 65 -139
2-Hexanone <1.28 250 284.4 ug/L 114 44 -150
Iodomethane <1.50 50.0 60.51 ug/L 121 34 -150
Methylene Chloride <1.00 50.0 51.92 ug/L 104 64 -130
4-Methyl-2-pentanone (MIBK)<0.810 250 292.1 ug/L 117 50 -140
Styrene <0.280 50.0 58.72 ug/L 117 70 -130
1,1,1,2-Tetrachloroethane <0.150 50.0 52.88 ug/L 106 70 -130
1,1,2,2-Tetrachloroethane <0.190 50.0 53.33 ug/L 107 56 -145
Tetrachloroethene <0.140 50.0 52.03 ug/L 104 57 -138
Toluene <0.170 50.0 53.56 ug/L 107 64 -136
trans-1,4-Dichloro-2-butene <0.460 50.0 50.49 ug/L 101 39 -150
trans-1,2-Dichloroethene <0.230 50.0 58.17 ug/L 116 59 -143
trans-1,3-Dichloropropene <0.170 50.0 58.28 ug/L 117 63 -142
1,1,1-Trichloroethane <0.190 50.0 56.82 ug/L 114 68 -144
1,1,2-Trichloroethane <0.190 50.0 53.63 ug/L 107 70 -130
Trichloroethene <0.200 50.0 52.03 ug/L 104 63 -135
Trichlorofluoromethane <0.210 50.0 60.32 ug/L 121 44 -150
1,2,3-Trichloropropane <0.230 50.0 54.22 ug/L 108 65 -131
Vinyl acetate <1.71 100 115.8 ug/L 116 43 -146
Vinyl chloride <0.180 50.0 52.25 ug/L 104 57 -150
Xylenes, Total <0.580 100 114.5 ug/L 115 69 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
MS MS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1081,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: BG Springs OLDLab Sample ID: 490-101753-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
Acetone <2.66 250 287.8 ug/L 115 39 -150 0 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 562.3 ug/L 112 50 -135 3 17
Benzene <0.200 50.0 48.84 ug/L 98 55 -147 4 50
Bromochloromethane <0.150 50.0 52.50 ug/L 105 59 -132 6 17
Bromodichloromethane <0.170 50.0 54.37 ug/L 109 70 -140 5 18
TestAmerica Nashville
Page 28 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: BG Springs OLDLab Sample ID: 490-101753-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333637
Bromoform <0.290 50.0 52.54 ug/L 105 53 -150 2 30
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromomethane <0.350 50.0 45.97 ug/L 92 30 -150 4
2-Butanone (MEK)<2.64 250 278.4 ug/L 111 50 -143 5 19
Carbon disulfide <0.220 50.0 40.01 ug/L 80 35 -150 8 21
Carbon tetrachloride <0.180 50.0 52.56 ug/L 105 56 -150 5 19
Chlorobenzene <0.180 50.0 50.99 ug/L 102 70 -130 3 14
Chloroethane <0.360 50.0 47.14 ug/L 94 58 -141 11 20
Chloroform <0.230 50.0 52.96 ug/L 106 66 -138 8 18
Chloromethane <0.360 50.0 40.67 ug/L 81 10 -150 11 31
cis-1,2-Dichloroethene <0.210 50.0 55.61 ug/L 111 68 -131 6 17
cis-1,3-Dichloropropene <0.170 50.0 55.94 ug/L 112 70 -133 2 15
Dibromochloromethane <0.250 50.0 54.13 ug/L 108 66 -140 1 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 49.52 ug/L 99 38 -138 3 24
1,2-Dibromoethane (EDB)<0.210 50.0 52.91 ug/L 106 65 -137 1 15
Dibromomethane <0.450 50.0 51.82 ug/L 104 70 -130 4 16
1,2-Dichlorobenzene <0.190 50.0 51.96 ug/L 104 70 -130 3 15
1,4-Dichlorobenzene <0.170 50.0 51.49 ug/L 103 70 -130 3 15
1,1-Dichloroethane <0.240 50.0 56.27 ug/L 113 61 -139 7 17
1,2-Dichloroethane <0.200 50.0 58.30 ug/L 117 64 -136 4 17
1,1-Dichloroethene <0.250 50.0 48.86 ug/L 98 54 -150 9 20
1,2-Dichloropropane <0.250 50.0 50.41 ug/L 101 67 -130 6 17
Ethylbenzene <0.190 50.0 53.73 ug/L 107 65 -139 4 15
2-Hexanone <1.28 250 285.9 ug/L 114 44 -150 1 17
Iodomethane <1.50 50.0 57.37 ug/L 115 34 -150 5 23
Methylene Chloride <1.00 50.0 49.96 ug/L 100 64 -130 4 17
4-Methyl-2-pentanone (MIBK)<0.810 250 295.2 ug/L 118 50 -140 1 21
Styrene <0.280 50.0 56.58 ug/L 113 70 -130 4 24
1,1,1,2-Tetrachloroethane <0.150 50.0 51.87 ug/L 104 70 -130 2 16
1,1,2,2-Tetrachloroethane <0.190 50.0 53.59 ug/L 107 56 -145 0 20
Tetrachloroethene <0.140 50.0 49.47 ug/L 99 57 -138 5 17
Toluene <0.170 50.0 51.92 ug/L 104 64 -136 3 15
trans-1,4-Dichloro-2-butene <0.460 50.0 52.21 ug/L 104 39 -150 3 26
trans-1,2-Dichloroethene <0.230 50.0 54.04 ug/L 108 59 -143 7 16
trans-1,3-Dichloropropene <0.170 50.0 57.86 ug/L 116 63 -142 1 14
1,1,1-Trichloroethane <0.190 50.0 53.66 ug/L 107 68 -144 6 17
1,1,2-Trichloroethane <0.190 50.0 53.50 ug/L 107 70 -130 0 15
Trichloroethene <0.200 50.0 49.10 ug/L 98 63 -135 6 17
Trichlorofluoromethane <0.210 50.0 57.83 ug/L 116 44 -150 4 22
1,2,3-Trichloropropane <0.230 50.0 53.62 ug/L 107 65 -131 1 19
Vinyl acetate <1.71 100 112.8 ug/L 113 43 -146 3 21
Vinyl chloride <0.180 50.0 47.93 ug/L 96 57 -150 9 17
Xylenes, Total <0.580 100 109.3 ug/L 109 69 -132 5 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
MSD MSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
1051,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
TestAmerica Nashville
Page 29 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-333247/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333546 Prep Batch: 333247
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 16:45 04/21/16 10:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 04/20/16 16:45 04/21/16 10:30 1Barium
<0.000500 0.0005000.00100 mg/L 04/20/16 16:45 04/21/16 10:30 1Cadmium
<0.00300 0.003000.00500 mg/L 04/20/16 16:45 04/21/16 10:30 1Chromium
<0.00500 0.005000.0100 mg/L 04/20/16 16:45 04/21/16 10:30 1Copper
<0.00200 0.002000.00500 mg/L 04/20/16 16:45 04/21/16 10:30 1Lead
<0.00300 0.003000.0100 mg/L 04/20/16 16:45 04/21/16 10:30 1Nickel
<0.00500 0.005000.0100 mg/L 04/20/16 16:45 04/21/16 10:30 1Selenium
<0.00300 0.003000.00500 mg/L 04/20/16 16:45 04/21/16 10:30 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333247/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333546 Prep Batch: 333247
Arsenic 0.0500 0.04090 mg/L 82 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.031 mg/L 102 80 -120
Cadmium 0.0500 0.04960 mg/L 99 80 -120
Chromium 0.200 0.1980 mg/L 99 80 -120
Copper 0.250 0.2599 mg/L 104 80 -120
Lead 0.0500 0.05130 mg/L 103 80 -120
Nickel 0.500 0.5140 mg/L 103 80 -120
Selenium 0.0500 0.05130 mg/L 103 80 -120
Silver 0.0500 0.04840 mg/L 97 80 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-333247/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333546 Prep Batch: 333247
Arsenic 0.0500 0.04720 mg/L 94 80 -120 14 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Barium 2.00 2.059 mg/L 103 80 -120 1 20
Cadmium 0.0500 0.05020 mg/L 100 80 -120 1 20
Chromium 0.200 0.1997 mg/L 100 80 -120 1 20
Copper 0.250 0.2602 mg/L 104 80 -120 0 20
Lead 0.0500 0.05230 mg/L 105 80 -120 2 20
Nickel 0.500 0.5204 mg/L 104 80 -120 1 20
Selenium 0.0500 0.05240 mg/L 105 80 -120 2 20
Silver 0.0500 0.04910 mg/L 98 80 -120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 240-63616-H-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333546 Prep Batch: 333247
Arsenic 0.0809 0.0500 0.1317 mg/L 102 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0164 2.00 2.062 mg/L 102 75 -125
Cadmium <0.000500 0.0500 0.05010 mg/L 100 75 -125
Chromium <0.00300 0.200 0.1999 mg/L 100 75 -125
TestAmerica Nashville
Page 30 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 240-63616-H-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333546 Prep Batch: 333247
Copper 0.0337 0.250 0.3187 mg/L 114 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Lead <0.00200 0.0500 0.05190 mg/L 104 75 -125
Nickel <0.00300 0.500 0.5154 mg/L 103 75 -125
Selenium <0.00500 0.0500 0.05280 mg/L 106 75 -125
Silver <0.00300 0.0500 0.04960 mg/L 99 75 -125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 240-63616-H-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333546 Prep Batch: 333247
Arsenic 0.0809 0.0500 0.1368 mg/L 112 75 -125 4 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0164 2.00 2.076 mg/L 103 75 -125 1 20
Cadmium <0.000500 0.0500 0.05050 mg/L 101 75 -125 1 20
Chromium <0.00300 0.200 0.2023 mg/L 101 75 -125 1 20
Copper 0.0337 0.250 0.2966 mg/L 105 75 -125 7 20
Lead <0.00200 0.0500 0.05310 mg/L 106 75 -125 2 20
Nickel <0.00300 0.500 0.5179 mg/L 104 75 -125 0 20
Selenium <0.00500 0.0500 0.05120 mg/L 102 75 -125 3 20
Silver <0.00300 0.0500 0.05000 mg/L 100 75 -125 1 20
Client Sample ID: Method BlankLab Sample ID: MB 490-333658/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334222 Prep Batch: 333658
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/21/16 20:27 04/23/16 16:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 04/21/16 20:27 04/23/16 16:19 1Barium
<0.000500 0.0005000.00100 mg/L 04/21/16 20:27 04/23/16 16:19 1Cadmium
<0.00300 0.003000.00500 mg/L 04/21/16 20:27 04/23/16 16:19 1Chromium
<0.00500 0.005000.0100 mg/L 04/21/16 20:27 04/23/16 16:19 1Copper
<0.00200 0.002000.00500 mg/L 04/21/16 20:27 04/23/16 16:19 1Lead
<0.00300 0.003000.0100 mg/L 04/21/16 20:27 04/23/16 16:19 1Nickel
<0.00500 0.005000.0100 mg/L 04/21/16 20:27 04/23/16 16:19 1Selenium
<0.00300 0.003000.00500 mg/L 04/21/16 20:27 04/23/16 16:19 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333658/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334222 Prep Batch: 333658
Arsenic 0.0500 0.04820 mg/L 96 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.096 mg/L 105 80 -120
Cadmium 0.0500 0.05150 mg/L 103 80 -120
Chromium 0.200 0.2045 mg/L 102 80 -120
Copper 0.250 0.2547 mg/L 102 80 -120
Lead 0.0500 0.05390 mg/L 108 80 -120
Nickel 0.500 0.5257 mg/L 105 80 -120
Selenium 0.0500 0.05090 mg/L 102 80 -120
TestAmerica Nashville
Page 31 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333658/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334222 Prep Batch: 333658
Silver 0.0500 0.05050 mg/L 101 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-333658/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334222 Prep Batch: 333658
Arsenic 0.0500 0.04700 mg/L 94 80 -120 3 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Barium 2.00 2.082 mg/L 104 80 -120 1 20
Cadmium 0.0500 0.05090 mg/L 102 80 -120 1 20
Chromium 0.200 0.2024 mg/L 101 80 -120 1 20
Copper 0.250 0.2551 mg/L 102 80 -120 0 20
Lead 0.0500 0.05360 mg/L 107 80 -120 1 20
Nickel 0.500 0.5216 mg/L 104 80 -120 1 20
Selenium 0.0500 0.04990 mg/L 100 80 -120 2 20
Silver 0.0500 0.05020 mg/L 100 80 -120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-101722-D-33-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334222 Prep Batch: 333658
Arsenic 0.0521 0.0500 0.09930 mg/L 94 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 1.54 2.00 3.443 mg/L 95 75 -125
Cadmium 0.00550 0.0500 0.05070 mg/L 90 75 -125
Chromium 0.156 0.200 0.3495 mg/L 97 75 -125
Copper 0.398 0.250 0.6438 mg/L 98 75 -125
Lead 0.794 0.0500 0.8644 4 mg/L 140 75 -125
Nickel 0.158 0.500 0.6098 mg/L 90 75 -125
Selenium 0.0117 F1 0.0500 0.04880 F1 mg/L 74 75 -125
Silver <0.00300 0.0500 0.04870 mg/L 97 75 -125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101722-D-33-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334222 Prep Batch: 333658
Arsenic 0.0521 0.0500 0.09540 mg/L 87 75 -125 4 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 1.54 2.00 3.445 mg/L 95 75 -125 0 20
Cadmium 0.00550 0.0500 0.05040 mg/L 90 75 -125 1 20
Chromium 0.156 0.200 0.3556 mg/L 100 75 -125 2 20
Copper 0.398 0.250 0.6462 mg/L 99 75 -125 0 20
Lead 0.794 0.0500 0.8665 4 mg/L 144 75 -125 0 20
Nickel 0.158 0.500 0.6144 mg/L 91 75 -125 1 20
Selenium 0.0117 F1 0.0500 0.05440 mg/L 85 75 -125 11 20
Silver <0.00300 0.0500 0.04880 mg/L 98 75 -125 0 20
TestAmerica Nashville
Page 32 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-332626/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333029 Prep Batch: 332626
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:01 04/19/16 17:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332626/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333111 Prep Batch: 332626
Mercury 1.00 0.9104 ug/L 91 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-101722-D-25-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333029 Prep Batch: 332626
Mercury <0.100 F1 1.00 0.7559 ug/L 76 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101722-D-25-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333029 Prep Batch: 332626
Mercury <0.100 F1 1.00 0.7084 F1 ug/L 71 75 -125 6 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-332627/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333029 Prep Batch: 332627
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/19/16 06:05 04/19/16 18:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332627/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333111 Prep Batch: 332627
Mercury 1.00 0.9287 ug/L 93 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-101629-M-2-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333029 Prep Batch: 332627
Mercury <0.100 F1 1.00 0.4732 F1 ug/L 47 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101629-M-2-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333029 Prep Batch: 332627
Mercury <0.100 F1 1.00 0.4872 F1 ug/L 49 75 -125 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
Page 33 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
TestAmerica Nashville
Page 34 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
GC/MS VOA
Analysis Batch: 333637
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-101753-1 MW-01 OLD Total/NA
Water 8260B490-101753-2 MW-02 OLD Total/NA
Water 8260B490-101753-3 MW-03 OLD Total/NA
Water 8260B490-101753-4 MW-04 OLD Total/NA
Water 8260B490-101753-5 BG Springs OLD Total/NA
Water 8260B490-101753-5 MS BG Springs OLD Total/NA
Water 8260B490-101753-5 MSD BG Springs OLD Total/NA
Water 8260B490-101753-6 SW-01 OLD Total/NA
Water 8260B490-101753-7 SW-02 OLD Total/NA
Water 8260B490-101753-8 DW-01 OLD Total/NA
Water 8260B490-101753-9 Trip Blank Total/NA
Water 8260BLCS 490-333637/5 Lab Control Sample Total/NA
Water 8260BLCSD 490-333637/6 Lab Control Sample Dup Total/NA
Water 8260BMB 490-333637/9 Method Blank Total/NA
Metals
Prep Batch: 332626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-101722-D-25-B MS Matrix Spike Total/NA
Water 7470A490-101722-D-25-C MSD Matrix Spike Duplicate Total/NA
Water 7470A490-101753-7 SW-02 OLD Total/NA
Water 7470A490-101753-8 DW-01 OLD Total/NA
Water 7470ALCS 490-332626/2-A Lab Control Sample Total/NA
Water 7470AMB 490-332626/1-A Method Blank Total/NA
Prep Batch: 332627
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-101629-M-2-B MS Matrix Spike Total/NA
Water 7470A490-101629-M-2-C MSD Matrix Spike Duplicate Total/NA
Water 7470A490-101753-1 MW-01 OLD Total/NA
Water 7470A490-101753-2 MW-02 OLD Total/NA
Water 7470A490-101753-3 MW-03 OLD Total/NA
Water 7470A490-101753-4 MW-04 OLD Total/NA
Water 7470A490-101753-5 BG Springs OLD Total/NA
Water 7470A490-101753-6 SW-01 OLD Total/NA
Water 7470ALCS 490-332627/2-A Lab Control Sample Total/NA
Water 7470AMB 490-332627/1-A Method Blank Total/NA
Analysis Batch: 333029
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 332627490-101629-M-2-B MS Matrix Spike Total/NA
Water 7470A 332627490-101629-M-2-C MSD Matrix Spike Duplicate Total/NA
Water 7470A 332626490-101722-D-25-B MS Matrix Spike Total/NA
Water 7470A 332626490-101722-D-25-C MSD Matrix Spike Duplicate Total/NA
Water 7470A 332627490-101753-1 MW-01 OLD Total/NA
Water 7470A 332627490-101753-2 MW-02 OLD Total/NA
Water 7470A 332627490-101753-3 MW-03 OLD Total/NA
Water 7470A 332627490-101753-4 MW-04 OLD Total/NA
Water 7470A 332627490-101753-5 BG Springs OLD Total/NA
TestAmerica Nashville
Page 35 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Metals (Continued)
Analysis Batch: 333029 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 332627490-101753-6 SW-01 OLD Total/NA
Water 7470A 332626490-101753-7 SW-02 OLD Total/NA
Water 7470A 332626490-101753-8 DW-01 OLD Total/NA
Water 7470A 332626MB 490-332626/1-A Method Blank Total/NA
Water 7470A 332627MB 490-332627/1-A Method Blank Total/NA
Analysis Batch: 333111
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 332626LCS 490-332626/2-A Lab Control Sample Total/NA
Water 7470A 332627LCS 490-332627/2-A Lab Control Sample Total/NA
Prep Batch: 333247
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A240-63616-H-1-B MS Matrix Spike Total/NA
Water 3010A240-63616-H-1-C MSD Matrix Spike Duplicate Total/NA
Water 3010A490-101753-6 SW-01 OLD Total/NA
Water 3010A490-101753-7 SW-02 OLD Total/NA
Water 3010A490-101753-8 DW-01 OLD Total/NA
Water 3010ALCS 490-333247/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-333247/3-A Lab Control Sample Dup Total/NA
Water 3010AMB 490-333247/1-A Method Blank Total/NA
Analysis Batch: 333546
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 333247240-63616-H-1-B MS Matrix Spike Total/NA
Water 6010D 333247240-63616-H-1-C MSD Matrix Spike Duplicate Total/NA
Water 6010D 333247490-101753-6 SW-01 OLD Total/NA
Water 6010D 333247490-101753-7 SW-02 OLD Total/NA
Water 6010D 333247490-101753-8 DW-01 OLD Total/NA
Water 6010D 333247LCS 490-333247/2-A Lab Control Sample Total/NA
Water 6010D 333247LCSD 490-333247/3-A Lab Control Sample Dup Total/NA
Water 6010D 333247MB 490-333247/1-A Method Blank Total/NA
Prep Batch: 333658
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-101722-D-33-C MS Matrix Spike Total/NA
Water 3010A490-101722-D-33-D MSD Matrix Spike Duplicate Total/NA
Water 3010A490-101753-1 MW-01 OLD Total/NA
Water 3010A490-101753-2 MW-02 OLD Total/NA
Water 3010A490-101753-3 MW-03 OLD Total/NA
Water 3010A490-101753-4 MW-04 OLD Total/NA
Water 3010A490-101753-5 BG Springs OLD Total/NA
Water 3010ALCS 490-333658/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-333658/3-A Lab Control Sample Dup Total/NA
Water 3010AMB 490-333658/1-A Method Blank Total/NA
Analysis Batch: 334222
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 333658490-101722-D-33-C MS Matrix Spike Total/NA
Water 6010D 333658490-101722-D-33-D MSD Matrix Spike Duplicate Total/NA
Water 6010D 333658490-101753-1 MW-01 OLD Total/NA
TestAmerica Nashville
Page 36 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Metals (Continued)
Analysis Batch: 334222 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 333658490-101753-2 MW-02 OLD Total/NA
Water 6010D 333658490-101753-3 MW-03 OLD Total/NA
Water 6010D 333658490-101753-4 MW-04 OLD Total/NA
Water 6010D 333658490-101753-5 BG Springs OLD Total/NA
Water 6010D 333658LCS 490-333658/2-A Lab Control Sample Total/NA
Water 6010D 333658LCSD 490-333658/3-A Lab Control Sample Dup Total/NA
Water 6010D 333658MB 490-333658/1-A Method Blank Total/NA
TestAmerica Nashville
Page 37 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101753-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: MW-01 OLD Lab Sample ID: 490-101753-1
Matrix: WaterDate Collected: 04/14/16 09:50
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/21/16 22:511 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333658 04/21/16 20:27 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 334222 04/23/16 17:18 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332627 04/19/16 06:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 19:03 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-02 OLD Lab Sample ID: 490-101753-2
Matrix: WaterDate Collected: 04/14/16 13:20
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/21/16 23:201 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333658 04/21/16 20:27 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 334222 04/23/16 17:22 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332627 04/19/16 06:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 19:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-03 OLD Lab Sample ID: 490-101753-3
Matrix: WaterDate Collected: 04/14/16 11:28
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/21/16 23:481 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333658 04/21/16 20:27 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 334222 04/23/16 17:26 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332627 04/19/16 06:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 19:07 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-04 OLD Lab Sample ID: 490-101753-4
Matrix: WaterDate Collected: 04/14/16 12:22
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/22/16 00:161 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333658 04/21/16 20:27 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 334222 04/23/16 17:30 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332627 04/19/16 06:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 19:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
TestAmerica Nashville
Page 38 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101753-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: BG Springs OLD Lab Sample ID: 490-101753-5
Matrix: WaterDate Collected: 04/14/16 13:55
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/21/16 22:231 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333658 04/21/16 20:27 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 334222 04/23/16 17:35 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332627 04/19/16 06:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 19:12 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: SW-01 OLD Lab Sample ID: 490-101753-6
Matrix: WaterDate Collected: 04/13/16 15:15
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/22/16 00:451 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333247 04/20/16 16:45 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333546 04/21/16 12:30 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332627 04/19/16 06:05 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 19:14 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: SW-02 OLD Lab Sample ID: 490-101753-7
Matrix: WaterDate Collected: 04/13/16 15:30
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/22/16 01:131 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333247 04/20/16 16:45 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333546 04/21/16 12:34 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332626 04/19/16 06:01 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 17:46 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: DW-01 OLD Lab Sample ID: 490-101753-8
Matrix: WaterDate Collected: 04/13/16 14:57
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/22/16 01:421 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333247 04/20/16 16:45 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333546 04/21/16 12:39 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332626 04/19/16 06:01 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 333029 04/19/16 17:48 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
TestAmerica Nashville
Page 39 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101753-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: Trip Blank Lab Sample ID: 490-101753-9
Matrix: WaterDate Collected: 04/13/16 00:01
Date Received: 04/15/16 10:30
Analysis 8260B JRV04/21/16 21:541 TAL NSH333637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 40 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Method Summary
TestAmerica Job ID: 490-101753-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Closed Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 41 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101753-1
Project/Site: Madison Co Closed Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
TestAmerica Nashville
Page 42 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 43 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 44 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-101753-1
Login Number: 101753
Question Answer Comment
Creator: Huskey, Adam
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
FalseContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
Page 45 of 45 4/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13

APPENDIX C

Environmental Monitoring Reporting Form
and
Electronic Submittal of Environmental
Monitoring Data
5802Apr2016 (Electronic only)