19039_Oneida Mill_PIIR_20131002

•
•
•
PHASE II ENVIRONMENTAL SITE ASSESSMENT
ONEIDA MILLS
219 W. HARDEN STREET
GRAHAM, ALAMANCE COUNTY, NORTH CAROLINA
GEC JOB NO. 130524.241
PREPARED FOR
BRIDGELANDDEVELOPMENT
7000 PEACHTREE DUNWOODY ROAD, NE
SUITE 4-100
ATLANTA, GEORGIA 30328
ATTN: MR. STEVE MUNIER
PREPARED BY
GEOTECHNICAL & ENVIRONMENTAL CONSULTANTS, INC.
514 HILLCREST INDUSTRIAL BOULEVARD
MACON, GEORGIA 31204
[phone]
OCTOBER 2, 2013
GEC
•
•
•
October 2, 2013
Mr. Steve Munier
Bridgeland Development
GEC
GEOTECHNICAL -----&-----ENVIRONMENTAL
CONSULTANTS, INC
7000 Peachtree Dunwoody Road, NE
Suite 4-100
Atlanta, Georgia 30328
SUBJECT: Report of Phase II Environmental Site Assessment and
Evaluation of Remediation Standards
Oneida Mills
219 W. Harden Street
Graham, Alamance County, North Carolina
GEC Job No. 130524.241
Dear Mr. Munier:
Geotechnical & Environmental Consultants, Inc. (GEC) has completed a Phase II Environmental Site
Assessment of the above referenced site. The following report details our scope of work for the Phase II
services, our protocol for intrusive sampling and laboratory analysis of physical media, laboratory analytical
results, and our conclusions relative to the work performed.
GEC appreciates the opportunity to provide our professional services to you. If you have any questions
concerning this report, or if we can be of further assistance, please feel free to contact our office.
Sincerely,
GEOTECHNICAL & ENVIRONMENTAL CONSULTANTS, INC.
Thomas E. Driver, P.E
President
North Carolina Reg. No. 19125
514 Hillcrest Industrial Boulevard, Macon, GA 31204 • Phone: [phone] • Fax: [phone]
5031 Milgen Court, Columbus, GA 31907 • Phone: [phone] • Fax: [phone]
•
•
•
TABLE OF CONTENTS
ONEIDA MILLS
219 W. HARDEN STREET
GRAHAM, ALAMANCE COUNTY, NORTH CAROLINA
GEC JOB NO. 130524.241
PAGE#
1.0 INTRODUCTION
2.0 REVIEW OF EXISTING DATA
3.0 SOIL AND GROUNDWATER SAMPLING
4.0 VAPOR MONITORING
5.0 LABORATORY RESULTS
6.0 FINDINGS
7.0 CONCLUSIONS AND RECOMMENDATIONS
8.0 QUALIFICATIONS OF REPORT
APPENDICES
APPENDIX 1: Figure 1: Site Location Map
Sample Location Plan
APPENDIX2:
APPENDIX3:
APPENDIX4:
Figure 2:
Tables
Laboratory Analytical Report
Chains of Custody
Former Reports by Others
1
1
3
5
5
5
6
6
•
•
•
1.0 INTRODUCTION
Geotechnical and Environmental Consultants, Inc. (GEC) was retained by Mr. Steve Munier with
Bridgeland Development to perform a Phase II Environmental Site Assessment (ESA) for the
Proposed Oneida Mills project located at 316 N. West Street in Graham, North Carolina. The
purpose of the work performed at the site was to address and evaluate contamination of the
subsurface from past on-site operations as a cotton mill. The sample locations were determined based
on prior reports by others on the site and a site reconnaissance of the property. This study focuses on
soil, vapor, and groundwater sampling and testing only. Asbestos and lead based paint testing
reports have been issued under separate cover. The GEC study is focused on the actual property
being developed and does not evaluate any off site properties.
GEC performed the collection of eight soil samples, three vapor monitoring tests, and the installation
of one temporary groundwater monitoring well on the site. All subsurface media (soil), air, and
groundwater test locations were sampled and analyzed for constituents appropriate to the concerns at
this site. This report details the work performed at the site, provides the results of the analytical data,
and presents our conclusions and recommendations about the data obtained during the performance
of this Phase II ESA.
2.0 REVIEW OF EXISTING DATA
GEC reviewed readily available reports by others on the site in the form of a prior Phase I ESA on
the property and reports provided by the North Carolina Department of Environment and Natural
Resources (DENR). The following are brief summaries of selected reports.
Notification of Removal of Underground Storage Tank. April 5, 1989
This report was addressed to the DENR and was performed by GSX Tank Management, Inc. for
Kayser-Roth and provides prior notification of the removal of one 11,000-gallon UST at the site.
UST Closure Report, July 17,1989
This report was addressed to the DENR and was performed by GSX Tank Management for Kayser-
Roth and provides the results of the UST removal ( 11,000 gallon UST) at the site. The results of soil
testing below the UST indicated that the extraction was "clean" (had no indication of contamination).
The excavation was backfilled with new "clean" fill material.
Final Report Submittal Documenting Soil Remediation Operations, November 15, 1993
This report was addressed to DENR and was performed by Four Seasons Environmental for the
Kayser-Roth Corporation to document remediation operations associated with the removal of
petroleum contaminated soil from area around above ground storage tank excavations. The soil
remediation operations were conducted in the vicinity of the former location of one 12,000-gallon
1
GEC
• AST and one 7 ,500-gallon AST last containing #5 fuel oil. The ASTs were taken out of service in
November of 1992. The remediation was performed after the submittal of a Comprehensive Site
Assessment Report and the performance of soil and groundwater sampling. Significant soil
contamination was encountered, but no groundwater contamination. The area of remediation was
located "between a boiler house connected to the northern section of the yam warehouse and the
southern section of the warehouse" as shown in the attached report (Appendix 4 ). The approximate
size of the final remediation excavation was 4 7' x29' x 12 'to 17' deep. Over 1,000 tons of petroleum-
impacted soil was removed from the site, as well as over 80 tons of debris (concrete and piping). The
consultant recommended that the site work be considered for a clean closure. A site closure/no
further action approval letter was submitted to Kayser-Roth by DENR on July 25, 2004.
•
•
Comprehensive Site Assessment Report, March 16, 2000
This report was addressed to DENR and was performed by Aquaterra Engineering, Inc. for Kayser-
Roth Corporation. In March of 1999, Aquaterra performed limited soil and groundwater sampling
activities at the site. The areas of concern were the former location of an 11,000 gallon gasoline
Underground Storage Tank (UST) and associated pump island, as well as an area of soil impacted by
two ASTs (see above report description). Soil and groundwater sampling was performed and
additional monitoring wells were installed. The UST had been previously removed in 1989, and soil
samples collected did not indicate that a release had occurred. VOCs were detected in the soil from
two of the monitoring wells installed, but none of the constituents exceeded the "remediation goals
for each compound". Both shallow and deep groundwater monitoring wells were installed at the site.
Several of the shallow wells installed, exhibited volatiles contamination, perchloroethylene (PCE)
and trichloroethylene (TCE) (typical dry cleaning contaminants) above the established groundwater
quality standards. The deep monitoring well exhibited levels of PCE above the regulatory standard.
The results of the study were that "it appears that the horizontal extent of the shallow ground water
contamination has been defined to the north and east and appears to be confmed to the subject site"
and that "Due to the lack of potential receptors, the availability of municipal water, the lack of a
known impacted soil source, and the relatively small contaminant plume, Aquaterra feels that natural
attenuation is the appropriate remedy for this site".
Corrective Action Plan, April, 2002
This report was addressed to DENR and was performed by Waters Edge Environmental, LLC
(Waters Edge) for Kayser-Roth Corporation. Waters Edge was formerly known as Aquaterra
Engineering. The report suggests that additional wells were installed in April of 2001, with
additional sampling in 2002, and both soil and groundwater contamination were encountered. The
soil contamination existed as elevated VOCs in the soil around well MW-2, which is located in the
west portion of the site near the existing concrete pads without roof. The contaminants of concern
for both the soil and groundwater were Tetracholorethene (same as PCE), Trichloroethene (same as
TCE), Cloroform, and 1,1,1,-Trichloroethane. It was recommended that the corrective action at the
site consist of a dual phase extraction system .
2
GEC
• Ground Water Sampling Report, .January 2006
This report was the latest of several groundwater monitoring reports reviewed by GEC for the site.
The report was prepared by Waters Edge and submitted to DENR on behalf of Kayser-Roth. The
report includes the results of periodic groundwater monitoring at the site. The test results indicated
that contamination remains on the site for the following tested constituents: Benzene,
Tetrachloroethene, and Trichloroethene. The conclusion of the report was that the most elevated
groundwater contamination remains in the vicinity of monitor well MW-2 and that the source of
benzene contamination in the well is unknown. The report states that the plume is reasonably well
defined and appears to have multiple sources; and that consideration should be given to evaluate
natural attenuation as a viable remediation alternative. No DENR response was provided to GEC,
and this is the last monitoring event that GEC reviewed.
Prioritzation Assessment Report, Impressive Cleaners . .June 15, 2010
This report is on the adjacent facility across W. Harden Street, south of the site. The report was
written by Hart & Hickman and performed for the DENR for a release that has occurred at the
Impressive Cleaners Dry Cleaning operation. Based on the isoconcentration maps included in the
report, it appears that PCE contamination is inferred to enter upon the subject 219 W. Harden Street
property. Therefore it appears that the former Oneida Mills site has been impacted by an off site
• property.
•
Discussion of Prior Reports
In addition to the above reports, it is our understanding that the site is listed on the Inactive
Hazardous Waste Branch of DENR listing for sites that have been reported as contaminated. The
listing is due to the presence of chlorinated compounds in the soil and groundwater at the site. No
information other than the above was available relative to the site listing.
Based on our review of the above reports, there is soil and groundwater contamination on the
property that has been reported to the appropriate state agency (DENR) for evaluation and oversight.
The liability for these past reported releases should remain with the responsible parties of the release,
mainly Kayser-Roth.lt is our understanding that Kayser-Roth is a currently operating entity.
The Phase IT sampling and testing program performed by GEC was designed to evaluate some of
those areas not previously evaluated and/or to further augment the testing previously performed.
There are a number of monitoring wells in existence on the property. GEC made no attempt to
sample or otherwise tamper with any existing wells on the site.
3.0 SOIL AND GROUNDWATER SAMPLING
In order to specifically address the concerns posed by the former operations on the subject property
3
GEC
• and concerns indicated by the previous assessments at the site, GEC performed soil sampling at eight
locations and groundwater sampling at one location on September 11 and 12, 2013. The sample
locations are depicted on Figure 2 in Appendix I. A description of the sample locations is as follows:
•
•
B-1 through B-3:
B-4:
B-5:
B-6:
B-7 and B-8:
MW-2:
Area of the former electrical transformers on the site.
Former Boiler room, sample collected below slab near floor drains.
Area near the smokestack on the site.
Former warehouse, sample collected below slab.
Grassed area where former "Drug House", "Waste House", and "Oil Room"
were once located.
Temporary monitoring well near where former boiler room was located and
in an area in northeast portion of site not formerly evaluated.
Soil Samples B-2, B-7, and B-8 were collected using a skid-steer loader-mounted GeoProbe rig. The
GeoProbe advanced the probe-holes into the subsurface at the site. The former studies on the site
were used to assist in the determination of sampling locations and were found on areas not
previously evaluated. The probe holes were advanced using hydraulic pressure/pneumatic vibration.
This system permits continual sampling of soils throughout the entirety of the advancement of the
probe-hole. The other samples were collected using a hand auger.
All probes and other downhole apparatus were thoroughly decontaminated prior to introduction into
the subsurface. On-site personnel wore new disposable latex or nitrile gloves when handling any
tooling or sampling equipment in order to prevent cross-contamination of laboratory samples. All
soil samples were collected at a depth of two feet below grade.
Each probe hole was advanced to a depth of four feet below the ground surface. The soil was
assessed for sensory evidence of contamination, and the top two to three feet of each probe sample
was submitted for analysis.
The soil samples were placed in laboratory-supplied, vapor and fluid tight containers, labeled,
preserved on ice, and delivered via overnight commercial carrier to Environmental Science
Corporation (ESC) for analytical testing. The constituents of concern for each soil sample were
based on by products of former operations in the vicinity of each sample and former assessments
conducted at the site. Soil sample analysis included one or more of the following test methods:
volatile organic compounds (VOCs) utilizing EPA method 8260B; semi-volatile organic compounds
(SVOCs) utilizing EPA method 82700; PCBs utilizing EPA method 8082; mercury using EPA
method 7471, and Appendix I metals utilizing EPA method 6010C.
One of the probe holes was converted to a temporary monitoring well (MW-2) at a depth of25 feet
below the ground surface. Groundwater was encountered at approximately 16 feet below the ground
surface at the time of sampling. Following the completion of the advancement of the probe-hole, a
temporary monitoring well was installed at the location with a 1 "-outer diameter PVC pipe with 10
feet of 0.01 0" machine-slotted screen extending from the bottom of each well. A sand ftlter pack was
4
GEC
• installed in the annulus of the well from the bottom of the screen to approximately 0.5 to 1 foot
above the top of the screened interval to allow for filtration of silt and sediment from the surrounding
disturbed soil. A bentonite seal was placed over the top of the sand pack. Two well volumes of
groundwater was purged from the well utilizing a low-flow peristaltic pump prior to sample
collection to allow for equilibration of the groundwater in the well with the surrounding aquifer and
to remove silt and sediment from the well. Refer to Figure 2 in Appendix 1 for the locations of the
temporary monitoring well.
•
•
The groundwater sample was placed in laboratory-supplied, vapor and fluid tight containers, labeled,
preserved on ice, and delivered to ESC for analytical testing. The groundwater sample collected
from the temporary monitoring well was analyzed for VOCs utilizing EPA method 8260 and SVOCs
utilizing EPA method 82700.
4.0 VAPOR MONITORING
Three vapor monitoring samples were collected at the site, one in each of buildings 1 and 2, and the
third in the area of a former warehouse. We note that the sample collected in the former warehouse
was near the well location MW-2 that was installed by others, which is the area where the highest
contamination has been documented at the site. All samples were collected through a boring
installed after coring through the concrete slab at each location. The borings were installed to
approximately four feet below the ground surface, and a one-inch PVC temporary monitoring well
was installed in the borehole. The PVC included a screened interval extending from the bottom of
the borehole with a riser extending to the ground surface. Pea gravel was installed around the
screened interval. A sand layer was placed above the pea gravel, and the sampling point was sealed
with a bentonite layer to aid in containing the subsurface gases. The location was fitted with a cap
with a sealed hose attachment and was left in place for at least four hours to allow underground gases
to equilibrate within. The vapor was sampled by connecting the ppbRae TM to the hose attachment.
The ppbRae was connected to a Tedlar bag, and the bag was filled as the "Rae" extracted the air
from the sampling point.
5.0 LABORATORY RESULTS
All samples were shipped overnight via FED EX to ESC. Copies of the original laboratory chain of
custodies are included in Appendix 3. The results of the laboratory analyses are summarized in tables
provided in Appendix 2 with actual laboratory results in the ESC report. As there were no
groundwater exceedances above the detected limit, there is no groundwater results table.
6.0 FINDINGS
GEC has completed a Phase II Environmental Site Assessment at the property located at 219 West
Harden Street in Graham, North Carolina. Based on the analytical results from the soil and
groundwater samples taken at the site, the following is noted:
5
GEC
•
•
•
• All soil test results above laboratory detection levels are required to be reported to the
NCDENR.
• Soil exceedance of the Preliminary Soil Remediation Goals, as established by the NCDENR
Inactive Hazardous Sites Branch was exhibited by arsenic, benzo(a)Anthracene,
benzo(a)pyrene, benzo(k)fluoranthene, and indeno(l,2,3-c,d)pyrene.
• The groundwater sampling results were all BDL for the constituents evaluated.
• Vapor testing results indicated signs of some volatile organic compounds, at the site;
however, the samples collected within the building were well below NCDENR Preliminary
Acceptable Soil Gas Concentrations and OSHA permissible exposure limits (PELs).
7.0 CONCLUSIONS AND RECOMMENDATIONS
The site is reportable to the NCDENR Inactive Hazardous Sites Branch because some of the metals,
volatiles, semi volatiles, and PCB levels were above the laboratory detection limits. The reporting
must be done within 90 days of property ownership to meet the NCDENR requirements. The
notification should be performed in the form of a Remedial Investigation Work Plan. NCDENR will
review the information submitted and provide comment on the report and plan of action. We note
that the work performed during the Phase II evaluation will need to be supplemented with additional
sampling prior to the Remedial Investigation Work Plan being submitted.
We note that, although a number of samples had constituents above laboratory detection levels, there
were only a few exceedances above the listed Preliminary Residential Health-Based Soil
Remediation Goals (PSRG) for metals, which was in the form of Arsenic. During the preparation of
the work plan, Arsenic background levels sampling will be performed in the area to determine the
level of "natural" occurring arsenic in the soil. It is anticipated that arsenic remediation will not
ultimately be necessary at the site or that it will be limited, based on the current levels encountered.
However, additional sampling at the site may encounter higher levels.
We also note that, although a number of samples had constituents above laboratory detection levels,
there were few exceedances above the listed Preliminary Residential Health-Based Soil Remediation
Goals (PSRG) for volatiles and semi-volatiles. These constituents are not naturally occurring and we
anticipate that some soil remediation will be necessary for these compounds. The Remedial
Investigation Work Plan noted above will contain additional sampling and analysis with which to
establish the soil remediation, if any that may be directed by NCDENR.
8.0 QUALIFICATIONS OF REPORT
This report is intended for the sole use of Bridgeland Development and their representatives. GEC is
not responsible for opinions, conclusions, or recommendations made by others based on the fmdings
in this report. The conclusions presented in this report are our professional opinions based on our
6
GEC
•
•
•
findings obtained in accordance with customary practices, principles, and methodologies utilized in
the fields of environmental science and engineering.
Since no assessment can absolutely deny the existence of hazardous materials, existing hazardous
materials can escape detection using the customary methods. The conclusions of this environmental
assessment are based on conditions as observed on our site visits. Future changes in environmental
conditions and site characteristics may occur with the passage of time in which case the conclusions
of this report may have to be re-evaluated .
7
GEC
•
APPENDIX!
•
•
GEC
I
~''''f'''--fN~ ~''t''$'
I
118
P.woNGLC7f
MARKET STREET
== 811 :..=:=n
PAY!O~MA
IUI!.£)ING.
IIUILDIHG t1
HARDEN STREET
I 60' 120' 240' J6o' 480'
FIGURE 1: SITE MAP
ONEIDA MILLS LOFTS
SCALE: 1" = 120'
G EC S14HILLCRESTINDUSTRIALBLVD.
GEOTECHNICAL MACON, GEORGIA 31204
--& 47&-7S7-l606 (F.x) 47&-757-1608
ENVIRONMENTAL· WWW.GECONSULTANTS.COM
GRAHAM, ALAMANCE COUNTY, NORTH CAROLINA
GEC JOB NO. 130524.241 CONSULTANTS, INC.
I
PMIONQL.Of
I
al~. ~ CONCMTE W ~
• B·7
MARKET STREET
811 _=::=n
PAVIONIM
IIUII.£IINIO 112
HARDEN STREET
¥f2
8UIUIINGIJ1
Stdg,1-
Vaw ..
"
Key to s.t'nples Colleded
• Grota1dwater Monitoring Wei
• Soil Sample Location
.A Vapor Tett Location
··"t'"" --,
iN} I o 60' 120' 240• 36o• 480' ~'''f''<'
FIGURE 2: SAMPLE LOCATION PLAN
ONEIDA MILLS LOFTS
GRAHAM, ALAMANCE COUNTY, NORTH CAROLINA
GEC JOB NO. 130524.241
SCALE: 1" = 120'
G EC Sl4HILLCRESTINDUSTRIALBLVD.
GEOTECHNICAL MACON, GEORGIA 31204
--" 47J..757-t~ (Fax) 47&-7S7-t601 ENVIRONMENTAL WWW.GECONSULTANTS.COM
CONSULTANTS. INC.
•
APPENDIX2
•
•
GEC
•
Table 1
Oneida Mills Soil Sampling Data
GEC Project Number·
PSRG* ,_ .
lA ---1, 6.1 E·01
Barium 3.0E+03
~dmium 1.4 E+01
~hromium 2.4 E+04
Lead 4.0E+02
Merc:urv 2.0E+02
Selenium 7.8 E+01
Silver 7.8 E+01
PSRG* ,_ ..
~etone 1.2 E+04
Benzo (a) anthracene 1.5 E-01
Benzo (a) pyrene 1.5E-02
~o(b)ftuonudhene 1.5 E-01
Benzo (g,h,i) perytene -Benzo·(k) ftuoranthene 1.5 E+OO
Chrysene 1.5E+01
Fluoranthene 4.6E+02
lndeno (1,2,3-c:d) pyrene 1.5 E.01
~nthrene **
pyrene -PCB 1260 1.0 E+OO
B-1 B-2
1.6 BDL
140 250
BDL BDL
49 95
2.2 9.2
BDL SOL
4.3 7.0
BDL BDL
B-1 B-2
BDL BDL
BDL 0.082
BOL 0.07
BOL 0.1
BOL BOL
BOL BDL
SOL 0.1
0.054 0.19
BOL BDL
BOL 0.087
0.049 0.17
0.034 BDL
•
MW-2 B-3 8-4 B-5 B-6
BOL BOl 38" 3.2 5.5
250 210 70 40 110
BOL BDL BOL BDL BDL
61.0 39 14 33.0 41
1.8 14 52 9.0 38
BDL BDL 0.053 0.036 0.049
7.3 12 7.0 6.1 5.1
BDL BOL BOL BDL BDL
MW-2 B--3 B-4 B-5 B-6.
BOL SOL SOL BOL BDL
SOL SOL BDL SOL BOL
BDL SOL BDL BDL BOL
BOL SOL BDL BDL 0.22
BOL SOL BOL BDL BOL
BDL BOL BDL BDL SOL
BOL BDL BDL SOL 0.22
SOL BDL BDL BDL 0.42
BDL BDL BDL BDL BDL
SOL SOL BDL BDL 0.34
BOL BDL SOL BDL 0.33
BDL 0.024 BDL BDL BDL
*NCDENR Inactive HazardOus Sites BranCh Preliminary Re$idential Health Based Soil Remediation Goal. July 2013
**Not Listed
•
B-7 B-8
4.0 12
120 270
3.0 1.8
37.0 14
70.0 83
0.044 0.054
4.2 5.3
BOL BOL
B-7 B-8
0.091 BOL
BDL 6~1
BDL 6.2
0.2?_ 7.0
BDL 4.4
BDL 2.2
0.24 6.2
0.4 8.9
BOL '3.1
0.22 3.9
0.34 10
BOL BOL
• Ta~
Oaeida Mills Vapor Sampliag Data
130524.240
I
, . . . •· .. . ·t 'll·iilliD-8 ··t·· '»'ililillif '} CoJIP(JrJNb.· •. ;.<~·.· ·:;~!:. · .. i& ·. ';c;~1.· .... . . . ·. ·.. .•• . ,.i•. : ' t.·· .. ' ·~.'2.::. ' <.i( .•
~· I 67 I 41 I 45
.·~ . 1 6.1 I 1.7 I 2.2
1~B~ I I 7.8
Ctlrliiit Dlsul/ill! ..
·~····
~-';,..~.;.&.. .. .. ~; ''-'J!aURtfXIIII ...••.
i;s...~
'~· •.• ~;:p ·i
~:,
'~ .ur -,--.. ,-, --;--:;:-· .. ' ' ..u!Jtt!!l! ' " -IFHt!XIIIie , . ·
·Mettillf1liO.ifWldi; .. \,;;:Z~)Iiiililfiliic''. ••.; ::
•. z;:J-~?
L:"C:--'(.~li~f'l.
~ ~, .J.rriilliDie~' ., .. · ...
·. ·~U.,#.ll'iil'"··"·c..:.~.•• "'''-·~·,, "''·L
··tfi~eJ~
20
1.3
450
5.2
2.3
62
4.9
4.1
15
2.2
24
7.9
25 -6.9
3.3
18
ALL USOLTS in ug/m3
.62
. 92
210
1.1
1.2
1.6
4.8
22
4.1
6.1
T.2
.65
3.7
6.5
8.1
1.0
1.0
.42
.48
290
1.6
. 69
.43
1.1
3.9
2.8
12
7.8
8.5
1.8
.68
5.7
1.3
OSHA I TR*
PELs
1()()() 6.4£+04
10 3.1E+01
1 4.2£+(){}
20 1.46£+03
50 1.1£+01
1()() 1.88E+02
3()() ••
50 ••
1()()() ••
100 9.7£+01
NIA. •
1000 1.46£+03
1000 ••
500 ••
500 ••
NIA. ••
200 ••
400 ••
NIA. ••
2()() &34E+OJ
NIA. J.46E+Ol
NIA. ••
2.0E+02
2.1 I 2.0£+02
*Preliminary Acceptable soil-gas concentration per
NCDENR IHSB Residential Screening Table, July 2012
**None Listed
•
•
APPENDIX3
•
•
GEC
•
Soil & Ground Water Results
•
•
GEC
•
•
•
-ESC
YOUR LIIB OF CHOICE
Tom Driver
GEC -t-lacon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Report sunlinar:Y
.. ·.·.:. <-:·· .· · .. · ..
Thursday Sept:~~er 26, 2013
Report Nuin}:)19,r: L657552
Sample~ B.ece4.ved: 09/14/13
Client P~Qject: 130524.240
Descri tion: Oneida Mill Site
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax {615) 758-5859
Tax J.D. 62-0814289
Est. 1970
The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call .
Entire Report Reviewed By:
Laboratory Certification Numbers
A2LA -1461-01, AIHA -100789, AL -40660, CA -01157CA, CT -PH-0197, FL-E87487, GA-923, IN -C-TN-01 KY -90010, KYUST -0016, NC-ENV375/DW21704/BI0041, NO -R-l40. NJ -TN002, NJ NELAP -TN002, SC -84004, TN -2006, VA -460132, WV -233, AZ -0612 MN-047-999-395l NY-11742L WI-998093910L NV-TN006032011-1, TX -T104704245-1-3, OK -9~15, PA -68-fr29i91 IA Lab #364
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
Note: Tbe use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.
This report may not be reproduced, except in full, without written approval fro~ ESC Lab sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures! 060302, 060303, and 060304.
Page 1 of 43
•
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -1-dacon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received September 14, 2013
Description Oneida Mill Site
Sample ID B-7
CoUected By Todd Peterman Collection Date 09/12/13 15:40
Parameter
Total Solids
14ercury
Arsenic
Barium
Cadmium Chromium
Lead Selenium
Silver
Volatile Organics
Acetone Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane Bromoform
Bromomethane Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane Chloroform
Chloromethane
Oibromomethane 1,2-Dichlorobenzene
1,4-Dichlorobenzen~
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene 1,2-Dich1oropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene Ethylbenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry Result
77.6
0.044
4.0
120
3.0 37.
70. 4.2
BDL
0.091
BDL
BDL
BDL
BDL DOL
DOL DOL
BDL
DOL DOL
BDL BDL
BDL
8DL 80L
· 8DL
8DL
8DL
8DL
BDL
BDL
BDL 8DL
BDL
DOL BDL
Det. Limit -Practical Quantitation Limit(PQL)
Det. Limit Units
0.100 t
0.026 mq/kq
1.3 mq/kq
0.32 mq/kq
0.32 mq/kq
0.64 mq/kq
0.32 mq/kq
1.3 mq/kq
0.64 mq/kq
0.064 mg/kg
0.013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0064 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mq/kq
0.0064 mg/kg
0.0064 mg/kg
0.0032 mg/kg
0.0013 mg/kg
0.0013 mq/kq
0.0013 mq/kg
0.0032 mg/kg
0.0013 mq/kq
0.0013 mq/kq
0.0013 mq/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mq/kq 0.0013 mq/kq
12065 Lebanon Rd •
Mt. Juliet, Ttl 37122
[phone]
1-800-767-5859 Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-0l
Site ID GRAHAH, NC
Project t : 130524.240
Method Date Analyst
2540 G-20 09/18/13 0940 KDW
7471 CAF 09/17/13 1355
60108 ALT 09/25/13 2002
60108 ALT 09/25/13 2002 60108 ALT 09/25/13 2002
60108 ALT 09/25/13 2002
60108 ALT 09/25/13 2002
60108 ALT 09/25/13 2002
60108 ALT 09/25/13 2002
82608
82608
82608
82608
82608 82608
82608 82608
82608
82608
82608
82608 82608
82608
82608 82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608 82608
09/19/13 1402 RB 09/19/13 1402 RB
09/19/13 1402 RB
09/19/13 1402 RB
09/19/13 1402 R8 09/19/13 1402 R8
09/19/13 1402 R8 09/19/13 1402 R8
09/19/13 1402 R8
09/19/13 1402 RB
09/19/13 1402 RB
09/19/13 1402 RB 09/19/13 1402 RB
09/19/13 1402 R8 09/19/13 1402 RB
09/19/13 1402 R8
09/19/13 1402 RB 09/19/13 1402 RB
09/19/13 1402 RB
09/19/13 1402 RB 09/19/13 1402 RB
09/19/13 1402 RB
09/19/13 1402 RB 09/19/13 1402 RB
09/19/13 1402 RB
09/19/13 1402 RB 09/19/13 1402 RB
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-3951 NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 2 of 43
•
•
•
.-ESC
YOUR LIIO OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -!~aeon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-'7
Todd Peterman
09/12/13 15:40
Parameter Dry Result
2-Hexanone Iodomethane
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene 1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane Tetrachloroethane
Toluene
1,1,1-Trichloroethane
1,11 2-Trichloroethane
Trichloroethane
Trichlorofluoromethane 1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride Xylenes, Total
Surrogate Recovery
Toluene-dB Dibromofluoromethane
a,a,a-Trifluorotoluene
4-Bromofluorobenzene
Polychlorinated Biphenyls PCB 1016
PCB 1221 PCB 1232
PCB 1242
PCB 1248
PCB 1254
PCB 1260
PCBs Surrogates
Decachlorobiphenyl
Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaptithene Acenaphthylene
Anthracene
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
BDL BDL
BDL
BOL BDL
BOL BDL
BOL
93.6 91.4
95.8
69.4
BDL
BDL
BDL BDL
BDL BDL
80L
85.8
94.0
BOL 80L
BDL
Det. Limit -Practical Quantitation Limit(PQL)
Det. Limit Units
0.013 mg/kg
0.013 mg/kg
0.013 mg/kg
0.0064 mg/kg
0.013 mg/kg
0.0013 mg/kg 0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0064 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013
0.0064 0.0032
0.013
mg/kg
mg/kg mg/kg
mg/kg
0.0013 mg/kg
0.0039 mg/kg
% Rec.
% Rec.
% Rec.
% Rec.
0.022 mg/kg
0.022 mg/kg
0.022 mg/kg
0.022 mg/kg
0.022 mg/kg
0.022 mg/kg
0.022 mg/kg
% Rec.
% Rec.
0.21 mg/kg 0.21
0.21
mg/kg
mg/kg
12065 Lebanon Rd .
Ht. Juliet, Ttf 37122 [phone]
1-900-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-01
Site IO GRAHAI~, NC
Project i : 130524.240
Method Date Analyst
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB 8260B 09/19/13 1402 RB
8260B 09/19/13 1402 RB 8260B 09/19/13 1402 RB
82608 09/19/13 1402 RB
8260B 09/19/13 1402 RB
8260B 09/19/13 1402 RB
8260B 09/19/13 1402 RB
8260B 09/19/13 1402 RB 8260B 09/19/13 1402 RB
8260B 09/19/13 1402 RB 8260B 09/19/13 1402 RB 82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
82608 09/19/13 1402 RB
8082 09/20/13 1251 NO
8082 09/20/13 1251 NO 8082 09/20/13 1251 NO
8082 09/20/13 1251 ND
8082 09/20/13 1251 NO
8082 09/20/13 1251 NO
8082 09/20/13 1251 ND
8082 09/20/13 1251 ND
8082 09/20/13 1251 ND
82700 09/17/13 0707 KMF
82700 09/17/13 070'7 KMF
82700 09/1'7/13 0707 KMF
Laboratory Certification Numbers: AIHA-100789, AL-40660, CA-I-2327, CT-PH-019'7, FL -E87487, GA-923, IN -C-TN-01
KY -90010 1 KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, I~N -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Page 3 of 43
•
•
YOUR LAD OF CHOICE
REPORT OF ANALYSIS Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-7
Todd Pete~:man
09/12/13 15:40
Parameter DJ:Y Result Oet. Limit
Benzidine
Benzo(a)anthracene Benzo(b)fluoranthene
Benzo(k)fluoranthene Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-ch1orethoxy)methane Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether 2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene Dibenz(a,h)anthracene
3,3-Dichlorobenzidine 2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate Diethyl phthalate
Dimethyl phthalate Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene Acid Extractables
Results listed are dry weight basis.
BDL -Below Detection Limit
BOL
BDL 0.27
BDL
BDL BDL
BOL
BOL BDL
BDL
BDL
BDL
0.24 BDL
BDL BDL
BDL
0.40
BOL
BDL
BDL BDL
BOL
BDL BDL
BDL
BDL BDL
BDL
BDL
0.22
BDL BDL
BDL BDL
BDL
BDL
0.34
BDL
Det. Limit -Practical Quantitation Limit(PQL)
2.1
0.21
0.21
0.21
0.21 0.21
2.1
2.1
2.1
2.1
0.21
2.1
0.21
0.21
2.1
2.1 2.1
0.21
0.21
2.1
2.1 2.1
2.1
0.21 2.1
0.21 2.1
2.1
2.1
2.1
0.21
2.1
2.1
2.1
2.1 2.1
2.1 0.21
2.1
Units
mg/kq
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/k.g
mg/kg
mg/kg
mg/kg
mg/kg
12065 Lebanon Rd.
Ht. Juliet, Ttl 37122
{615) 758-5858
1-800-767-5859
Fax [phone]
Tax !.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample * L657552-01
Site ID GRAHA14, NC
Project i : 130524.240
Method Date Analyst
82700 09/17/13 0707 K~IF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF 82700 09/17/13 0707 KMF 82700 09/17/13 0707 Kt4F
82700 09/17/13 0707 KMF 82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF 82700 09/17/13 0707 Kl4F
82700 09/17/13 0707 KMF
82700 09/17/13 0707 Kl4F
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF 82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF 82700 09/17/13 0707 Kt4F
82700 09/17/13 0707 Kt4F
82700 09/17/13 0707 KMF 82700 09/17/13 0707 Kt4F
82700 09/17/13 0707 KMF
82700 09/17/13 0707 Kt4F 82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF 82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF 82700 09/17/13 0707 KMF
82700 09/17/13 0707 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYOST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233 AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 4 of 43
•
•
YOUR LAO OF CHOICE:
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-7
Todd Peterman 09/12/13 15:40
Parameter Dry Result Det. Limit
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol 4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5 2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d14
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
BDL BDL
BDL BDL
BDL
BDL BDL
BDL
66.1
68.6
81.6 95.5
95.6
84.2
Det. Limit -Practical Quantitation Limit(PQL)
2.1
2.1
2.1
2.1 2.1
2.1 2.1
2.1
2.1
2.1
2.1
Units
mg/kq mq/kq
mg/kq
mg/kq mq/kq
mq/kq mq/kq
mq/kq
mq/kq
mq/kq
mq/kq
' Rec.
' Rec.
' Rec .
' Rec.
' Rec.
' Rec.
12065 Lebanon Rd.
14t. Juliet, Til 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample II L657552-01
Site ID GRAHAM, NC
Project # : 130524.240
Method Date Analyst
82700 09/17/13 0707 I<MF 82700 09/17/13 0707 I<MF
82700 09/17/13 0707 I<MF 82700 09/17/13 0707 I<MF 82700 09/17/13 0707 KMF
82700 09/17/13 0707 I<MF 82700 09/17/13 0707 IG-IF
82700 09/17/13 0707 I<MF
82700 09/17/13 0707 Kl-iF
82700 09/17/13 0707 Kl~F
82700 09/17/13 0707 KHF
82700 09/17/13 0707 l<MF
82700 09/17/13 0707 I<MF
82700 09/17/13 0707 I<MF
82700 09/17/13 0707 l<MF
82700 09/17/13 0707 I<MF 82700 09/17/13 0707 Kl~F
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -887487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO-R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, tm -047-999-395, NY -11742, NJ-TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/26/13 15:16 Printed: 09/26/13 15:17
Page 5 of 43
•
•
•
.-ESC
Y 0 U R L A 13 0 F" C H 0 I C E
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received September 14, 2013
Description Oneida Mill Site
Sample ID B-1
Collected By Todd Peterman
Collection Date 09/11/13 11: OS
Parameter
Total Solids
Mercury
Arsenic
Barium
Cadmium Chromium
Lead
Selenium
Silver
Volatile Organics
Acetone Acrylonitrile
Benzene
8romoch1oromethane
Bromodichloromethane Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Ch1orobenzene Chlorodibromomethane
Chloroethane Chloroform
Chloromethane
Oibromomethane 1,2-0ich1orobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene 1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene Ethylbenzene
Results listed are dry weight basis.
8DL -Below Detection Limit
Dry Result
73.6
BDL
1.6
140
BDL
49. 2.2
4.3 BDL
BDL BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL BDL
8DL
8DL 80L
80L
8DL
8DL
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit(PQL)
Det. Limit units
0.100 '
0.027 mg/kg
1.4 mg/kg
0.34 mg/kg
0.34 mg/kg
0.68 mg/kg 0.34 mg/kg
1.4 mg/kg 0.68 mg/kg
0.071 mg/kg
0.014 mg/kg
0.0014 mq/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0071 mg/kg
0.0014 mg/kq
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0071 mg/kg
0.0071 mg/kg
0.0036 mg/kg
0.0014 mg/kg
0.0014 mg/kg "0.0014 mg/kg
0.0036 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mq/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
12065 Lebanon Rd . Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I : L657552-02
Site ID GRAHAM, NC
Project t : 130524.240
l.fethod Date Analyst
2540 G-20 09/18/13 0941 KDW
7471
60108 60108
60108 60108
60108
6010B 60108
82608
82608
82608 82608
8260B
82608 82608
82608 8260B
8260B
8260B
8260B
8260B
82608 8260B
8260B 8260B
82608
8260B 82608
82608
82608
82608
82608
82608 82608
82608
09/18/13 1013 CAF
09/25/13 2005 ALT
09/25/13 2005 ALT
09/25/13 2005 ALT
09/25/13 2005 ALT
09/25/13 2005 ALT 09/25/13 2005 ALT
09/25/13 2005 ALT
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB 09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
09/18/13 1655 RB
Laboratory certification Numbers: AIHA -100789, AL -40660, CA -I-2327, CT-PK-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST -0016, NC-ENV37S,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 6 of 43
•
•
•
.-ESC
YOUR LAD OF CHOICE
REPORT OF ANALYSIS
Tom Driver GEC -t4acon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-1
Todd Peterman
09/11/13 11: 05
Parameter Dry Result Det. Limit
2-Hexanone Iodomethane
2-Butanone (MEK) Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene 1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethane
Toluene
1,1,1-Trichloroethane 1,1,2-Trichloroethane
Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylenes, Total
Surrogate Recovery Toluene-dB
Dibromofluoromethane
a,a,a-Trifluorotoluene 4-Bromofluorobenzene
Polychlorinated Biphenyls
PCB 1016
PCB 1221 PCB 1232
PCB 1242 PCB 1248
PCB 1254
PCB 1260
PCBs Surrogates Decachlorobiphenyl
Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaphthene Acenaphthylene
Anthracene
Results listed are dry weiqht basis.
SOL -Below Detection Limit
BDL
BDL
BDL BOL
BOL
BDL BDL
BOL BOL
BDL BDL
BOL
BDL BDL
BDL
BDL BDL
BDL
103.
108.
105. 102.
BDL
BDL BDL
BOL BOL
BDL
0.034
82.4
94.4
BOL
BOL
BDL
Oet. Limit -Practical Quantitation Limit(PQL)
0.014
0.014
0.014
0.0071
0.014
0.0014 0.0014
0.0014 0.0014
0.0071
0.0014 0.0014
0.0014
0.0071
0.0036
0.014
0.0014
0.0043
0.023
0.023 0.023
0.023
0.023 0.023
0.023
0.045 0.045
0.045
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kq
mg/kg
mg/kg
mg/kq
mq/kg mq/kg
mg/kq
% Rec.
% Rec.
\ Rec. \ Rec.
mg/kq
mg/kg mg/kg
mg/kg mg/kg
mq/kg
mg/kq
ts Rec.
ts Rec.
mglkq mg/kq
mq/kg
12065 Lebanon Rd •
Mt. Juliet, Til 37122 [phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample • L657552-02
Site ID GRAHAl4, NC
Project # : 130524.240
Method Date Analyst
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB 8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
82608 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8260B 09/18/13 1655 RB
8082 09/20/13 1301 NO
8082 09/20/13 1301 ND
8082 09/20/13 1301 ND
8082 09/20/13 1301 NO
8082 09/20/13 1301 ND
8082 09/20/13 1301 ND
8082 09/20/13 1301 NO
8082 09/20/13 1301 NO
8082 09/20/13 1301 NO
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KHF
82700 09/17/13 0540 KMF
Laboratory Certification Numbers: AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233 AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 7 of 43
•
•
•
YOUR LAO OF CHOICE
REFORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
1-lacon, GA 31204
Date Received Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-1
Todd Peterman
09/11/13 11:05
Parameter orx Result
Benzidine BOL
Benzo(a)anthracene BOL
Benzo(blfluoranthene BOL
Benzo(k)fluoranthene BOL
Benzo(g,h,i)perylene BOL
Benzo(a)pyrene BOL
Bis(2-chlorethoxy)methane BDL
Bis(2-chloroethyl)ether BOL
Bis(2-chloroisopropyl)ether BOL
4-Bromophenyl-phenylether BDL
2-Chloronaphthalene BOL
4-Chlorophenyl-phenylether BDL
Chrysene BDL
Dibenz(a,h)anthracene BDL
3,3-Dichlorobenzidine BDL
2,4-Dinitrotoluene BOL
2,6-Dinitrotoluene BOL
Fluoranthene 0.054
Fluorene BDL
Hexachlorobenzene BDL
Hexachloro-1,3-butadiene BDL
Hexachlorocyclopentadiene BDL
Hexachloroethane BDL
Indeno{l,2,3-cd)pyrene BDL
Isophorone BDL
Naphthalene BDL
Nitrobenzene BDL
n-Nitrosodimethylamine BDL
n-Nitrosodiphenylamine BDL
n-Nitrosodi-n-propy1amine BDL
Phenanthrene BDL
Benzylbutyl phthalate BDL
Bis(2-ethylhexyl)phthalate BDL
Di-n-butyl phthalate BDL
Diethyl phthalate BDL
Dimethyl phthalate BDL
Di-n-octyl phthalate BOL
Pyrene 0.049
1,2,4-Trichlorobenzene BDL
Acid Extractables
Results listed are dry weight basis.
BDL -Below Detection Limit
Oet. Limit -Practical Quantitation Limit{PQL)
Det. Limit Units
0.45 mg/kg
0.045 mg/kg
0.045 mg/kg
0.045 mg/kg
0.045 mg/kg
0.045 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.045 mg/kg
0.45 mq/kg
0.045 mg/kg 0.045 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.045 mg/kg
0.045 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.045 mg/kg
0.45 mg/kg
0.045 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.045 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg
0.45 mg/kg 0.45 mg/kg
0.45 mg/kg
0.045 mg/kg
0.45 mg/kg
12065 Lebanon Rd . Mt. Juliet, Til 37122
[phone]
1-800-767-5859 Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-02
Site ID GRAHAl-1, NC
Project I : 130524.240
Method Date Analxst
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 Kf.IF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KI•IF
82700 09/17/13 0540 Kf.IF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KI4F
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KI-IF
8270D 09/11/13 0540 KMF
8270D 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 KI~F
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KI-IF
82700 09/17/13 0540 KI~F
82700 09/17/13 0540 KI~F
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
Laboratory Certification Numbers: IN -C-TN-01 AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923,
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, wv-
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 8 of 43
233
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -!~aeon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
s-1
Todd Peterman 09/11/13 11:05
Parameter Dry Result Det. Limit
4-Ch1oro-3-methylphenol
2-Ch1orophenol 2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-24nethylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitropheno1
Pentachlorophenol
Phenol 2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d14
Results listed are dry weight basis.
SOL -Below Detection Limit
BDL
BOL
BOL SOL
SOL
SOL BDL
BDL
BDL
BOL
BDL
56.3 61.7
64.9
79.1 85.5
63.5
Det. Limit -Practical Quantitation Limit(PQL)
0.45
0.45 0.45
0.45
0.45
0.45
0.45 0.45
0.45
0.45 0.45
Units
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
' Rec.
' Rec.
' Rec •
' Rec.
' Rec.
' Rec.
12065 Lebanon Rd . Mt. Juliet, TN 31122
[phone]
1-800-761-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-02
Site ID GRAHAt~, NC
Project I : 130524.240
Method Date Analyst
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/1'1 /13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
8270D 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KMF
82700 09/17/13 0540 KI~F
82700 09/17/13 0540 KI~F
82700 09/17/13 0540 Kt~F
82700 09/17/13 0540 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA-1-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/26/13 15:16 Printed: 09/26/13 15:17
Page 9 of 43
•
•
•
YOUR LAO OF CHOICE
REPORT OF ANALYSIS
Tom Driver GEC -14acon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
MW-2
Todd Peterman 09/12/13 14:40
Parameter or:.: Result
Total Solids 68.5
Mercury 8DL
Arsenic BDL
Barium 250
Cadmium BOL
Chromium 61.
Lead 1.8
Selenium 7.3
Silver BDL
Volatile Organics
Acetone BDL
Acrylonitrile BDL
Benzene BDL
Bromochloromethane BDL
Bromodichloromethane BDL
Bromoform BDL
Bromomethane 8DL
Carbon disulfide BDL
Carbon tetrachloride 8DL
Chlorobenzene BDL
Chlorodibromomethane 8DL
Chloroethane BDL
Chloroform BDL
Chloromethane BDL
Dibromomethane BDL
1,2-Dichlorobenzene BDL
1,4-Dichlorobenzene BDL
trans-1,4-Dichloro-2-butene BDL
1,1-Dichloroethane BDL
1,2-Dichloroethane BDL
1,1-Dichloroethene BDL
cis-1,2-Dichloroethene BDL
trans-1,2-Dichloroethene BDL
1,2-Dichloropropane BDL
cis-1,3-Dichloropropene BDL
trans-1,3-Dichloropropene BDL
Ethylbenzene BDL
Results listed are dry weight basis. BDL -Below Detection Limit
Det. Limit -Practical Quantitation Limit(PQL)
Oet. Limit Units
0.100 '
0.029 mg/kg
1.4 mg/kg
0.36 mq/kg
0.36 mg/kg
0.73 mg/kg
0.36 mq/kg
1.4 mg/kg
0.73 mg/kg
0.073 mg/kg
0.014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0073 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0073 mg/kg
0.0073 mg/kg
0.0036 mg/kg
0.0014 mq/kg
0.0014 mg/kg
0.0014 mg/kg
0.0036 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg 0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
12065 Lebanon Rd •
Mt. Juliet, Ttl 31122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample f L657552-03
Site ID GRAHAM, NC
Project I : 130524.240
1-!ethod Date Anal:.:st
2540 G-20 09/18/13 0941 KDW
7471 09/17/13 1358 CAF
6010B 09/25/13 2007 ALT
60108 09/25/13 2007 ALT
60108 09/25/13 2007 ALT
60108 09/25/13 2007 ALT
6010B 09/25/13 2007 ALT
60108 09/25/13 2007 ALT
60108 09/25/13 2007 ALT
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 R8
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 R8
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608. 09/19/13 2050 RB
82608 09/19/13 2050 R8
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
Laboratory Certification Numbers:
-100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 AIHA
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, wv -
AZ -0612, MN -047-999-395, NY -11742, NJ-TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 10 of 43
233
•
•
•
YOUR LAB OF CHOICI:
REPORT OF ANALYSIS
Tom Driver GEC -Macon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
MW-2
Todd Peterman 09/12/13 14:40
Parameter Dry Result Det. Limit
2-Hexanone Iodomethane
2-Butanone (MEK) Methylene Chloride
4-Methyl-2-pentanone (l4IBK)
styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethane
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane Trichloroethane
Trichlorofluoromethane 1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride Xylenes, Total
Surrogate Recovery
Toluene-d8 Oibromofluoromethane
a,a,a-Trifluorotoluene 4-Bromofluorobenzene
Polychlorinated Biphenyls
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254 PCB 1260
PCBs Surrogates Oecachlorobiphenyl
Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaphthene Acenaphthy1ene
Anthracene
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
BDL BDL
BDL
BDL
BOL
BDL BDL
BDL
BDL
BDL
BOL
BOL BOL
BOL
BDL
98.4 90.4
103.
100.
BDL
BOL
BDL
BDL
BOL ·
BDL
BDL
73.4 90.9
BDL
BDL
BDL
Oet. Limit -Practical Quantitation Limit(PQL)
0.014
0.014
0.014
0.0073 0.014
0.0014
0.0014 0.0014
0.0014
0.0073
0.0014
0.0014
0.0014
0.0073
0.0036 0.014
0.0014
0.0044
0.025
0.025
0.025
0.025
0.025
0.025
0.025
0.048
0.048
0.048
Units
mg/kg mg/kg
mg/kg
mg/kg mq/kq
mg/kq
mq/kq
mg/kg
mg/kg
mq/kq
mq/kq
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mq/kq
% Rec.
% Rec.
% Rec.
% Rec.
mq/kq
mg/kg
mq/kq
mq/kq
mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
mg/kg
mg/kg mg/kg
12065 Lebanon Rd •
Mt. Juliet, TN 37122
{615) 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-081~289
Est. 1970
September 26,2013
ESC Sample * L657552-03
Site ID GRAHA14, NC
Project # : 130524.240
l~ethod Date Analyst
8260B 09/19/13 2050 RB
8260B 09/19/13 2050 RB 8260B 09/19/13 2050 RB
8260B 09/19/13 2050 RB
82608 09/19/13 2050 RB 82608 09/19/13 2050 RB
82608 09/19/13 2050 RB 82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 R8
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
9260B 09/19/13 2050 RB 92608 09/19/13 2050 RB
92608 09/19/13 2050 RB
9260B 09/19/13 2050 RB
82608 09/19/13 2050 RB
9260B 09/19/13 2050 RB
82608 09/19/13 2050 RB
82608 09/19/13 2050 RB
8082 09/20/13 1332 NO 8082 09/20/13 1332 NO
8082 09/20/13 1332 NO
9082 09/20/13 1332 NO
9082 09/20/13 1332 NO
8082 09/20/13 1332 NO
8082 09/20/13 1332 NO
9082 09/20/13 1332 NO 8082 09/20/13 1332 NO
82700 09/17/13 0116 Kl4F
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST-0016, NC -ENV375,DW21704, NO-R-140, SC-84004, TN-2006, VA-00109, WV-233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Paqe 11 of 43
•
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
MW-2
Todd Peterman
09/12/13 14:40
Parameter Dry Result Det. Limit
Benzidine Benzo(a)anthracene
Benzo(b)fluoranthene Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether Bis(2-chloroisopropyl}ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene 3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone Naphthalene
Nitrobenzene n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate Dimethyl phthalate
Di-n-octyl phthalate
Pyrene 1,2,4-Trichlorobenzene
Acid Extractables
Results listed are dry weight basis. BDL -Below Detection Limit
BDL BDL
BDL
BDL
BDL
BDL
BDL BOL
BDL BOL
BOL
BOL BDL
BDL
BDL BDL
BDL
BOL BDL
BOL
BDL BDL
BDL BDL
BDL
BDL BOL
BOL BOL
BOL
BOL BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit{PQL)
0.49 0.048
0.048
0.048
0.048
0.048
0.49 0.49
0.49 0.49
0.048
0.49 0.048
0.048
0.49
0.49
0.49
0.048 0.048
0.49 0.49
0.49
0.49
0.048
0.49
0.048
0.49
0.49 0.49
0.49
0.048
0.49
0.49
0.49
0.49
0.49 0.49
0.048
0.49
Units
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kg mg/kg
mg/kg mg/kg
12065 Lebanon Rd . Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0914299
Est. 1970
September 26,2013
ESC Sample # L657552-03
Site ID GRAHAH, NC
Project # : 130524.240
Method Date Analyst
82700 09/17/13 0116 KI4F
82700 09/17/13 0116 Kl4F
82700 09/17/13 0116 KMF
82700 09/17/13 0116 Kl.fF
82700 09/17/13 0116 Kl4F
82700 09/17/13 0116 Kl4F
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
9270D 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 Kl4F
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
82700 09/17/13 0116 Kl•IF
82700 09/17/13 0116 IG!F
82700 09/17/13 0116 KMF
82700 09/17/13 0116 Kf.IF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
82700 09/17/13 0116 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 12 of 43
•
•
•
YOUR LAO OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
MW-2
Todd Peterman 09/12/13 14:40
Parameter Dry Result Det. Limit
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol
2-Nitrophenol 4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5 2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d14
Results listed are dry weight basis. BDL -Below Detection Limit
BDL
BDL BOL
BDL
BDL BDL
BDL BDL
BDL
BDL
BDL
59.4
62.1
62.0
72.3
83.5
68.6
Det. Limit -Practical Quantitation Limit(PQL)
0.49
0.49
0.49
0.49
0.49 0.49
0.49 0.49
0.49
0.49
0.49
Units
mq/kq
mq/kq mq/kq
mq/kq
mq/kq
mq/kq
mq/kq mq/kq
mq/kq
mq/kq
mq/kq
' Rec.
' Rec.
' Rec.
' Rec.
' Rec.
' Rec.
12065 Lebanon Rd . Mt. Juliet, TN 37122
{6151 759-5859
1-800-767-5859 Fax [phone]
Tax l.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-03
Site ID GRAHAM, NC
Project * : 130524.240
Method Date Analyst
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF 8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF 8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
8270D 09/17/13 0116 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,0W21704, NO-R-140, SC -84004, TN -2006, VA-00109, WV-233
AZ -0612, 14N -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted Reported: 09/26/13 15:16 Printed: 09/26/13 15:17
Page 13 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
Tom Driver
GE<: -Macon, GA 51<1 Hillcrest Industrial Blvd.
Mac:on, GA 31204
Date Received Septesnber 14, 2013
De:~cription Oneida lUll Site
SaJnple ID MW-2
Collected By Todd Peterman Collection Date 09/12/13 14:45
!,!;rameter
Volatile Organics
,ll.cetone
;~~ocrylonitrile
:Benzene
:Bromochloromethane
Bromodichloromethane
Bromoform Bromomethane
Carbon disulfide Carbon tetrachloride
Ch1orobenzene
Chlorodibromomethane
Chloroethane
Chloroform Chloromethane
1,2-Dibromo-3-Ch1oropropane
1,2-Dibromoethane
Dibromomethane 1,2-Dichlorobenzene
1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene 1,2-Dich1oropropane
cis-1,3-Dichloropropene trans-1,3-0ichloropropene
Ethylbenzene
2-Hexanone
Iodomethane
2-Butanone (MEK) Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene 1,1,1,2-Tetrach1oroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
BJ)L -Below Detection Limit
REPORT OF ANALYSIS
Result Det. Limit Units
BDL 50. ug/1 8DL 10. ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 5.0 ug/1
8DL 1.0 ug/1
BDL 1.0 ug/1
BDL 1.0 ug/1
8DL 1.0 ug/1
8DL 5.0 uq/1
BDL 5.0 ug/1
8DL 2.5 ug/1
8DL 5.0 uq/1
8DL 1.0 ug/1
BDL 1.0 ug/1
8DL 1.0 ug/1 8DL 1.0 ug/1
BDL 2.5 ug/1 8DL 1.0 ug/1
BDL 1.0 ug/1
8DL 1.0 ug/1
BDL 1.0 ug/1
BDL 1.0 ug/1
BDL 1.0 ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 10. ug/1
BDL 10. ug/1 8DL 10. ug/1
8DL 5.0 ug/1
8DL 10. ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 1.0 ug/1
8DL 5.0 ug/1
oe,t. Limit -Practical Quantitation Limit (PQL)
12065 Lebanon Rd •
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.O, 62-0814289
Est. 1970
September 26,2013
ESC Sample • L657552-04
Site ID GRAHAM, NC
Project It : 130524.240
Method Date/Time Analyst
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 R8
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 R8
82608 09/18/13 0149 RB
82608 09/18/13 0149 R8
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 R8
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 RB
82608 09/18/13 0149 R8
82608 09/18/13 0149 R8
82608 09/18/13 0149 R8
82608 09/18/13 0149 RB
82608 09/18/13 0149 R8
82608 09/18/13 0149 R8
82608 09/18/13 0149 R8
82608 09/18/13 0149 RB
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Page 14 of 43
Oil.
1
1 1
1
1 1
1
1
1
1 1
1
1
1
1
1
1
1 1
1
1 1
1
1
1
1 1
1 1
1
1
1
1
1
1
1 1
1
1
•
•
•
-ESC
YOUR LAI3 OF CHOICE
ToDl Driver
GE<: -Macon, GA 51'1 Hillcrest Industrial Blvd.
Macon, GA 31204
Da 1:e Received
De11cription
September 14, 2013
Oneida Mill Site
Sample IO MW-2
Collected By
Collection Date
Pa:rameter
Todd Peterman
09/12/13 14:45
1,1,1-Trichloroethane
1,1,2-Trichloroethane
•rr ichloroethene
•rrichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
'Vinyl chloride
:ltylenes, Total Su.rroqate Recovery
·roluene-d8 Dibromofluoromethane
4-Bromofluorobenzene
Base/Neutral Extractables
Acenaphthene
Acenaphthy1ene
Anthracene
Benzidine
Benzo(a)anthracene Benzo(b)fluoranthene
Benzo(k)fluoranthene Benzo(q,h,i)perylene
Benzo (a) pyrene
Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether 2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene Dibenz{a,h)anthracene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene 2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
BCIL -Below Detection Limit
RE~ORT OF ANALYSIS
Result Oet. Limit Units
BDL 1.0 uq/1 BOL 1.0 uq/1
BOL 1.0 uq/1
BOL 5.0 uq/1
BOL 2.5 uq/1
BOL 10. uq/1
BOL 1.0 uq/1
BDL 3.0 uq/1
102. \ Rec.
94.4 \ Rec.
104. \ Rec.
BOL 1.0 uq/1
BOL 1.0 uq/1
BOL 1.0 uq/1
BDL 10. uq/1
BDL 1.0 uq/1
BOL 1.0 uq/1
BDL 1.0 uq/1
BDL 1.0 uq/1
BDL 1.0 uq/1
BOL 10. ug/1
BDL 10. uq/1
BOL 10. uq/1
BOL 10. uq/1
BOL 1.0 uq/1
BOL 10. uq/1
BOL 1.0 uq/1
BOL 1.0 uq/1
BOL 10. uq/1
BOL 10. uq/1
BOL 10. uq/1
BOL 1.0 uq/1
BOL 1.0 uq/1
BOL 1.0 uq/1
BOL 10. uq/1
BOL 10. uq/l
BOL 10. uq/l
Oe1t. Limit -Practical Quantitation Limit (I?QL)
12065 Lebanon Rd. Ht. Juliet, TN 37122
(6151 758-5858
1-800-7 67-585 9
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I
Site ID
Project II :
L657552-04
GRAHAl~, NC
130524.240
Method Date/Time Analyst Oil.
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82608 09/18/13 0149
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
8270D 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
82700 09/18/13 0721
RB RB
RB
RB RB
RB
RB
RB
RB
RB
RB
KMF
KMF KMF
KMF KMF
KMF KMF
KMF
KMF KMF
Kl~F
KMF
KMF
KMF Kl4F
Kl-1F
KMF
Kl-1F
KHF
KMF KMF
KMF
KHF
KMF
KMF KMF
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Page 15 of 43
•
•
•
YOUR LAB OF CHOICE
Tom Driver
GEC: -Macon, GA
SU Hillcrest Industrial Blvd.
t~ac:on, GA 31204
Date Received September 14, 2013
De~1cription Oneida Mill Site
Scut~ple IO t~lf-2
ColLlected By Todd Peterman
Collection Date 09/12/13 14:45
~'!J~ameter
:rndeno(1,2,3-cd)pyrene
:rsophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
l~enzylbutyl phthalate
Bis(2-ethylhexyl)phthalate IDi-n-butyl phthalate
ll>iethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
l?yrene
1,2,4-Trichlorobenzene Acid Extractables
4-Ch1oro-3-methylphenol
2-Chlorophenol 2,4-0ichlorophenol
2,4-0imethylphenol 4,6-0initro-2-methylphenol
2,4-0initrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol Phenol
2,4,6-Trichlorophenol
Surrogate Recovery 2-Fluorophenol
Phenol-dS
Nitrobenzene-d5 2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Te:rphenyl-dl4
BIJIL -Below Detection Limit
REPORT OF ANALYSIS
Result Det. Limit Units
BDL 1.0 ug/1
BOL 10. ug/1
BOL 1.0 ug/1
BDL 10. ug/1
BOL 10. ug/1 BOL 10. ug/1
BOL 10. ug/1
BOL 1.0 ug/1 BDL 3.0 ug/1
SOL 3.0 ug/1 SOL 3.0 ug/1
BOL 3.0 ug/1
BOL 3.0 uq/1 SOL 3.0 ug/1
BOL 1.0 uq/1
BOL 10. ug/1
BOL 10. ug/1
SOL 10. ug/1 BOL 10. ug/1
SOL 10. ug/1 BOL 10. ug/1
BDL 10. ug/1
BDL 10. ug/1
BDL 10. ug/1
BDL 10. ug/1 BOL 10. ug/1 BOL 10. ug/1
37 .s· \ Rec.
25.4 \ Rec.
81.7 !fs Rec. 84.6 !fs Rec. 98.8 !fs Rec.
80.5 \ Rec.
Det. Limit -l?ractical Quantitation Limit(PQL)
12065 Lebanon Rd .
Mt. Juliet, Tll 37122
[phone]
1-800-767-5859
Fax [phone]
Tax 1.0. 62-0814289
Est. 1970
September 26,2013
ESC Seulple t : L657552-04
Site to GRAHAM, NC
Project I : 130524.240
Method Date/Time Analyst
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 Kl.fF 82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF 82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF 82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF 82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF 82700 09/18/13 0121 Kl.fF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF 82700 09/18/13 0721 Kl4F
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 Kl.fF
82700 09/18/13 0721 KMF
82700 09/18/13 0721 l(l.tF
Laboratory Certification Numbers: AIHA -100789 1 AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
Oil.
1
1
1
1
1
1 1
1
1
1
1 1
1
1 1
1
1
1 1
1 1
1
1
1
1
1 1
1
1
1 1
1
1
KY -90010, KYUST-0016, NC -ENV375,DW21704 1 NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, •m -047-999-395, NY -11742, NJ-TN002 1 WI -998093910 Nc•tes:
The reported analytical results relate only to the sample submitted
This report shall not be reproduced, except in full, without the written approval from ESC.
All samples analyzed in accordance with 40 CFR, Part 136.3
Reported: 09/26/13 15:16 Printed: 09/26/13 15:17
Page 16 of 43
•
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver GEC -Macon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received september 14, 2013
Description Oneida Mill Site
Sample ID B-5
Collected By Todd Peterman
Collection Date 09/12/13 13:15
Parameter
Total Solids
Mercury
Arsenic
Barium Cadmium
Chromium
Lead
Selenium
Silver
Volatile Organics
Acetone Acrylonitrile
Benzene
Bromochloromethane Bromodich1oromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene Chlorodibromomethane
Chloroethane Chloroform
Chloromethane
Dibromomethane 1,2-Dichlorobenzene
1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene 1,2-Dichloropropane
cis-1,3-0ichloropropene
trans-1,3-Dichloropropene Ethylbenzene
Results listed are dry weight basis.
8DL -Below Detection Limit
Dry Result
69.1
0.036
3.2
40. BDL
33.
9.0 6.1
BDL
BDL BDL
BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL BDL
BDL
BDL BDL
BDL
BOL
BOL
BOL BDL
BDL
BDL BDL
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit(PQL)
Oet. Limit Units
0.100 '
0.029 mq/kq
1.4 mq/kq
0.36 mq/kq 0.36 mq/kq o. 72 mq/kq
0.36 mq/kq
1.4 mq/kq
0.72 mg/kg
0.072 mq/kq
0.014 mq/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mq/kg
0.0014 mg/kg
0.0072 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0072 mg/kg
0.0072 mg/kg
0.0036 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0036 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg 0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg 0.0014 mg/kg
12065 Lebanon Rd .
11t. Juliet, TU 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-05
Site ID GRAHAM, NC
Project I : 130524.240
Method Date Analyst
2540 G-20 09/18/13 0941 KOW
7471
60108
60108 60108
60108
60108
60108
60108
82608 82608
82608
82608
82608 82608
8260B
82608
82608
82608 82608
82608 82608
82608
82608 82608
82608
8260B
82608
82608 82608
82608
82608 82608
82608
82608 82608
09/17/13 1401 CAF
09/25/13 2012 ALT
09/25/13 2012 ALT 09/25/13 2012 ALT
09/25/13 2012 ALT
09/25/13 2012 ALT
09/25/13 2012 ALT
09/25/13 2012 ALT
09/19/13 1602 RB 09/19/13 1602 R8
09/19/13 1602 RB
09/19/13 1602 RB 09/19/13 1602 RB
09/19/13 1602 R8
09/19/13 1602 R8 09/19/13 1602 R8
09/19/13 1602 R8
09/19/13 1602 RB 09/19/13 1602 RB
09/19/13 1602 RB 09/19/13 1602 RB
09/19/13 1602 R8
09/19/13 1602 RB
09/19/13 1602 RB
09/19/13 1602 RB 09/19/13 1602 RB
09/19/13 1602 RB
09/19/13 1602 RB 09/19/13 1602 RB
09/19/13 1602 RB
09/19/13 1602 RB 09/19/13 1602 R8
09/19/13 1602 RB
09/19/13 1602 RB 09/19/13 1602 R8
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, ND -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 17 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS Tom Driver
GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida !.fill Site
B-5
Todd Peterman
09/12/13 13:15
Parameter Dry Result
2-Hexanone
Iodomethane 2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK) Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethane
Toluene 1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethane Trichlorofluoromethane
1,2,3-Trich1oropropane
Vinyl acetate
Vinyl chloride
Xylenes, Total Surrogate Recovery
Toluene-dO
Dibromofluoromethane a,a,a-Trifluorotoluene
4-Bromofluorobenzene
Polychlorinated Biphenyls
PCB 1016 PCB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254 PCB 1260
PCBs Surrogates
Decachlorobiphenyl Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaphthene
Acenaphthylene Anthracene
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL BDL
BOL
BDL
BDL BDL
BDL
BDL BDL
BOL BDL
BDL
BDL BDL
BDL BDL
BDL
BDL
99.5
94.6 101.
102.
BDL
BDL BDL
BDL
BDL
BDL
BDL
92.1 101.
BDL
BOL BDL
Det. Limit -Practical Quantitation Limit(PQL)
Det. Limit Units
0.014
0.014 0.014
0.0072
mq/kg
mq/kg mq/kg
mq/kg
0.014 0.0014
0.0014
0.0014 0.0014
0.0072 0.0014
mg/kg mq/kg
mq/kg
mg/kg mq/kg
mg/kg mq/kg
0.0014 mq/kg
0.0014 mq/kg 0.0072 mq/kq
0.0036 mg/kg 0.014 mg/kg
0.0014 mg/kg
0.0043 mq/kg
% Rec.
% Rec.
% Rec.
% Rec.
0.025
0.025 0.025
0.025
0.025
0.025
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mq/kg
0.025 mg/kg
\ Rec.
\ Rec.
0.048 mg/kg
0.048 mq/kg
0.048 mg/kg
12065 Lebanon Rd •
Mt. Juliet, TN 37122
1615) 758-5858
1-800-767-5959
Fax [phone]
Tax 1.0. 62-0914299
Est. 1970
September 26,2013
ESC Sample i : L657552-05
Site ID GRAHAM, NC
Project II : 130524.240
Method Date Analyst
82608 09/19/13 1602 RB
8260B 09/19/13 1602 RB
8260B 09/19/13 1602 RB
82608 09/19/13 1602 RB
8260B 09/19/13 1602 RB 8260B 09/19/13 1602 RB
82608 09/19/13 1602 RB
8260B 09/19/13 1602 RB 82608 09/19/13 1602 RB
82608 09/19/13 1602 RB
82608 09/19/13 1602 RB
82608 09/19/13 1602 RB
82608 09/19/13 1602 RB 8260B 09/19/13 1602 RB
82608 09/19/13 1602 RB 82608 09/19/13 1602 RB 82608 09/19/13 1602 RB
82608 09/19/13 1602 RB
82608 09/19/13 1602 RB
82608 09/19/13 1602 RB 82608 09/19/13 1602 RB
8260B 09/19/13 1602 RB
8082 09/20/13 1342 NO
8082 09/20/13 1342 NO 8082 09/20/13 1342 ND
8082 09/20/13 1342 NO
8082 09/20/13 1342 NO
8082 09/20/13 1342 NO
8082 09/20/13 1342 NO
8082 09/20/13 1342 NO 8082 09/20/13 1342 NO
82700 09/17/13 0518 KHF
82700 09/17/13 0518 KHF
82700 09/17/13 0518 Kt4F
Laboratory Certification ttumbers:
AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST-0016, NC-ENV375,0W21704, NO-R-140, SC-84004, TN -2006, VA-00109, WV-233
AZ -0612, MN -047-999-395, NY -117421 NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 18 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
14acon, GA 31204
Date Received Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
B-5
Todd Peterman 09/12/13 13:15
Parameter Dry Result Oet. Limit
Benzidine
Benzo(a)anthracene
Benzo(b)f1uoranthene
Benzo(k)f1uoranthene Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether 4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chloropheny1-phenylether
Chrysene
Oibenz(a,h)anthracene
3,3-Dichlorobenzidine 2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene Fluorene
Hexachlorobenzene Hexachloro-1,3-butadiene
Hexachlorocyc1opentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine
Phenanthrene Benzylbutyl phthalate
Bis(2-ethylhexyllphthalate
Di-n-butyl phthalate
Oiethyl phthalate
Dimethyl phthalate Oi-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene Acid Extractables
Results listed are dry weight basis.
BOL -Below Detection Limit
BOL BOL
BDL
BDL BOL
BOL BDL
BDL
BDL BDL
BDL
BOL
BDL
BOL BDL
BOL
BOL
BDL
BDL
BOL BDL
BDL
BOL
BOL
BDL BDL
BDL
BOL BDL
BOL
BOL
BOL
BOL BOL
BOL BOL
BDL
BOL
BOL
Det. Limit -Practical Quantitation Limit(PQL)
0.48
0.048
0.048 0.048
0.048
0.048 0.48
0.48
0.48
0.48
0.048
0.48
0.048
0.048 0.48
0.48
0.48 0.048
0.048
0.48
0.48
0.48
0.48
0.048
0.48 0.048
0.48
0.48
0.48
0.48 0.048
0.48
0.48 0.48
0.48
0.48 0.48
0.048
0.48
Units
mg/kg
IIUJ/kg
mg/kg
DUJ/kg mg/kg
mg/kg
mq/kg
mg/kg
mq/k!f mq/kg
mq/kg mg/kg
mq/kg mg/kq
mq/kg
mq/kq
mq/kq
mq/kq
mq/kg
mq/kq
mg/kg
mq/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kg mg/kg
mg/kg mq/kg
mq/kg
mq/kq
mg/kq
mq/kq
mq/kq
mq/kg
12065 Lebanon Rd .
Mt. Juliet, TN 37122 [phone]
1-800-767-5859
Fax [phone]
Tax l.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-05
Site ID GRAHAM, NC
Project I : 130524.240
Method Date Analyst
8270D 09/17/13 0518 KMF
82700 09/11/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/11/13 0518 KMF
82700 09/17/13 0518 I<l4F
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KI~F
82700 09/17/13 0518 KI~F
8270D 09/17/13 0518 K14F
8270D 09/17/13 0518 Kl~F
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 I<l4F
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17113 0518 KMF
82700 09/17/13 0518 I<14F
82700 09/17/13 0518 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST -0016, NC -ENV375,DW21704, NO-R-140, SC -84004, TN -2006, VA-00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 19 of 43
•
•
•
.-ESC
YOUR Lf\B OF CHOlCE
REPORT OF ANALYSIS
Tom Driver GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-5
Todd Peterman
09/12/13 13:15
Parameter Dry Result Det. Limit
4-Chloro-3-methylphenol 2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5 Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d14
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL BDL
BDL
BDL
BDL
BDL
BOL
BDL BDL
BDL
BDL
73.1
67.4
70.0
82.1
99.8
77 .B
Det. Limit-Practical Quantitation Limit(PQLJ
0.48
0.48
0.48
0.48
0.48
0.48
0.48
0.48 0.48
0.48
0.48
Units
mg/kq
mg/kg
mg/kg
mq/kq
mq/kq mg/kq
mq/kq
mq/kg mq/kq
mg/kg
mg/kg
' Rec.
' Rec •
' Rec.
' Rec.
' Rec.
9s Rec.
1206~ Lebanon Rd .
Ht. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax r.o. 62-0814289
Est. 1970
September 26,2013
ESC Sample • L657552-05
Site IO GRAHAM, NC
Project t : 130524.240
Method Date Analyst
82700 09/17/13 0518 KMF
8270D 09/17/13 0518 KMF 82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 l<MF
82700 09/17/13 0519 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 IGIF
82700 09/17/13 0518 KMF
82700 09/17/13 0518 KMF
82700 09/17/13 0519 l<t~F
92700 09/17/13 0519 KMF
8270D 09/17/13 0519 KMF
92700 09/17/13 0518 KMF
9270D 09/17/13 0518 l<t~F
82700 09/17/13 0519 KMF
Laboratory Certification Numbers: AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E97487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,0W21704, ND -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY-11742, NJ-TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Reported: 09/26/13 15:16 Printed: 09/26/13 15:17
Page 20 of 43
•
•
•
YOUR Ll\0 OF CHOICE
Tom Driver
GEC -l.facon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received September 14, 2013
Description oneida Mill Site
Sample ID B-4
Collected By Todd Peterman
Collection Date 09/11/13 12:00
REPORT OF ANALYSIS
12065 Lebanon Rd .
Mt. Juliet, Til 37122
[phone]
1-800-767-5859 Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample # L657552-06
Site IO GRAHAM, NC
Project * : 130524.240
Parameter Dr:£ Result Det. Limit Units Method Date Anal:£st
Total Solids 77.3 0.100 ' 2540 G-20 09/18/13 0942 KDW
Mercury 0.053 0.026 mg/kg 7471 09/17/13 1404 CAF
Arsenic 38. 1.3 mg/kg 60108 09/25/13 2016 ALT
Barium 70. 0.32 mg/kg 60108 09/25/13 2016 ALT
Cadmium BDL 0.32 mg/kg 60108 09/25/13 2016 ALT Chromium 14. 0.65 mg/kg 60108 09/25/13 2016 ALT
Lead 52. 0.32 mg/kg 60108 09/25/13 2016 ALT Selenium 7.0 1.3 mg/kg 60108 09/25/13 2016 ALT
Silver BDL 0.65 mg/kg 60108 09/25/13 2016 ALT
Volatile Organics
Acetone BDL 0.065 mg/kg 82608 09/19/13 1619 RB Acrylonitrile BDL 0.013 mg/kg 82608 09/19/13 1619 RB Benzene BDL 0.0013 mg/kg 82608 09/19/13 1619 RB
8romochloromethane BDL 0.0013 mg/kg 82608 09/19/13 1619 RB
Bromodichloromethane BDL 0.0013 mg/kg 82608 09/19/13 1619 R8 Bromoform BDL 0.0013 mg/kg 82608 09/19/13 1619 RB
Bromomethane BDL 0.0065 mg/kg 82608 09/19/13 1619 RB Carbon disulfide BDL 0.0013 mg/kg 8260B 09/19/13 1619 RB Carbon tetrachloride BDL 0.0013 mg/kg 82608 09/19/13 1619 RB
Chlorobenzene BDL 0.0013 mg/kg 82608 09/19/13 1619 RB Chlorodibromomethane BDL 0.0013 mg/kg 82608 09/19/13 1619 RB
Chloroethane BDL 0.0065 mg/kg 82608 09/19/13 1619 RB Chloroform BDL 0.0065 mg/kg 8260B 09/19/13 1619 RB
Chloromethane 8DL 0.0032 mg/kg 82608 09/19/13 1619 R8
Dibromomethane BDL 0.0013 mg/kg 8260B 09/19/13 1619 RB 1,2-Dich1orobenzene BDL 0.0013 mg/kg 8260B 09/19/13 1619 RB
1,4-Dichlorobenzene BDL 0.0013 mg/kg 8260B 09/19/13 1619 RB
trans-1,4-Dich1oro-2-butene BDL 0.0032 mg/kg 8260B 09/19/13 1619 RB
1,1-Dich1oroethane 8DL 0.0013 mg/kg 82608 09/19/13 1619 RB
1,2-Dichloroethane 8DL 0.0013 mg/kg 8260B 09/19/13 1619 RB 1,1-Dichloroethene 8DL 0.0013 mg/kg 8260B 09/19/13 1619 RB cis-1,2-Dichloroethene 8DL 0.0013 mg/kg 82608 09/19/13 1619 RB trans-1,2-Dichloroethene 8DL 0.0013 mg/kg 82608 09/19/13 1619 RB 1,2-Dich1oropropane 8DL 0.0013 mg/kg 8260B 09/19/13 1619 RB
cis-1,3-Dichloropropene BDL 0.0013 mg/kg 8260B 09/19/13 1619 RB
trans-1,3-Dichloropropene BOL 0.0013 mg/kg 82608 09/19/13 1619 RB Ethylbenzene 8DL 0.0013 mg/kg 82608 09/19/13 1619 RB
Results listed are dry weiqht basis.
BDL -Below Detection Limit Det. Limit -Practical Quantitation Limit(PQL)
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,0W21704, NO -R-140, SC -84004, TN -2006, VA -00109, wv -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Paqe 21 of 43
•
•
•
-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
B-4
Todd Peterman 09/11/13 12:00
Parameter Dry Result Det. Limit
2-Hexanone
Iodomethane
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane Tetrachloroethane
Toluene 1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane Vinyl acetate
Vinyl chloride
Xylenes, Total Surrogate Recovery
Toluene-d8
Dibromofluoromethane a,a,a-Trifluorotoluene
4-Bromofluorobenzene
Polychlorinated Biphenyls
PCB 1016 PCB 1221
PCB 1232
PCB 1242
. PCB 1248
PCB 1254
PCB 1260
PCBs Surrogates
Decachlorobiphenyl Tetrachloro-m-xylene
Base/Neutral Extractables Acenaphthene
Acenaphthylene
Anthracene
Results listed are dry weight basis. BDL -Below Detection Limit
BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL
97.9
94.7
97.7 85.7
BDL
BDL BDL
BDL BDL
BDL
BDL
77.8
97.8
BOL
BOL
BDL
oet. Limit -Practical Quantitation Limit(PQL)
0.013
0.013
0.013
0.0065
0.013
0.0013
0.0013
0.0013 0.0013
0.0065 0.0013
0.0013
0.0013
0.0065
0.0032 0.013
0.0013
0.0039
0.022
0.022 0.022
0.022 0.022
0.022
0.022
0.043
0.043
0.043
Units
mg/kg
mg/kg
mg/kg
mg/kg
mq/kq mg/kq
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mq/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
% Rec.
% Rec.
mg/kg mg/kg
mg/kg
mq/kq
mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
mg/kg
mg/kg
mg/kg
12065 Lebanon Rd. Mt. Juliet, TN 37122
[phone]
l-800-767-5859
Fax [phone]
Tax I.O. 62-0814289
Est. 1970
September 26,2013
ESC Sample * L657552-06
Site ID GRAHAM, NC
Project # : 130524.240
Method Date Analyst
82608 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
82608 09/19/13 1619 RB
82608 09/19/13 1619 RB
92608 09/19/13 1619 RB 8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB 8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8260B 09/19/13 1619 RB
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO
8082 09/20/13 1352 NO 8082 09/20/13 1352 llO
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST -0016, NC-ENV375,DW21704, NO -R-140, SC-84004, TN-2006, VA-00109, WV-233
AZ -0612, MN -047-999-395, NY -11742, NJ -rN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 22 of 43
•
•
•
YOUR LAS OF CHOICE
REPORT OF ANALYSIS
Tom Driver
G&C -Macon, GA 514 Hillcrest Industrial Blvd.
!«aeon, GA 31204
Date Received Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
B-4
Todd Peterman
09/11/13 12: 00
Parameter Dry Result Oet. Limit
Benzidine Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(q,h,i)perylene
Benzo(a)pyrene
Bis(2-cblorethoxy)methane Bis(2-cbloroethyl}ether
Bis(2-chloroisopropyl)etber 4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chloropbenyl-pbenylether
Chrysene
Dibenz(a,h)anthracene 3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene Fluorene
Hexacblorobenzene Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isopborone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylbexyl)phthalate Di-n-butyl phthalate
Diethyl phthalate Dimethyl phthalate
Di-n-octyl phthalate
Pyrene 1,2,4-Trichlorobenzene
Acid Extractables
Results listed are dry weiqht basis.
BDL -Below Detection Limit
BOL
BDL
BDL
SOL
BDL BDL
BOL
SOL
BOL
BOL
BOL BOL
BDL BOL
BDL
BDL
BOL
SOL
SOL
SOL
SOL
SOL BOL
BOL BOL
SOL
BDL BDL
SOL
BOL
BOL
BDL BDL
BDL
BDL
BDL
BOL
BOL
BDL
Det. Limit -Practical Quantitation Limit{PQL)
0.43
0.043
0.043 0.043
0.043 0.043
0.43
0.43
0.43
0.43 0.043
0.43
0.043 0.043
0.43
0.43
0.43
0.043
0.043
0.43
0. 43 0.43
0.43
0.043 0.43
0.043
0.43 0.43
0.43 0.43
0.043
0.43 0.43
0.43
0.43
0.43
0.43 0.043
0.43
units
mq/kg
mg/kq mq/kq
mq/kg
mq/kg
mg/kg
mq/kg
mq/kq
mq/kq
mq/kq mq/kq
mq/kg
mq/kq
mg/kg
mg/kq mq/kg
mq/kq
mq/'kq
mq/kq
mq/kg
mq/'kq mq/kq
mq/kq
mg/kq
mg/kq
mq/kq
mq/'kq
mq/kq
mq/kq mq/kg
mq/kq mq/kg
mq/kg
mq/kq mg/kq
mg/kq
mq/kq mq/kq
mg/kq
12065 Lebanon Rd • Mt. Juliet, TN 37122
(6151 758-5858
l-800-7 67-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample * L657552-06
Site IO GRAHAM, NC
Project ' : 130524.240
t4ethod Date Analyst
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KI-IF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
8270D 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
8270D 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 Kl~F
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
8270D 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
8270D 09/17/13 0602 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -&87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233 AZ -0612, 14N -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Paqe 23 of 43
•
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -l.Jacon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By Collection Date
September 14, 2013 Oneida Mill Site
B-4
Todd Peterman 09/ll/13 12:00
Par:ameter Dr:y Result Det. Limit
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
21 4-Dimethylphenol 4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitr:ophenol 4-Nitrophenol
Pentachlorophenol Phenol
2,4,6-Trichlorophenol
Surrogate Recover:y
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5 2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-dl4
Results listed are dr:y weight basis.
BOL -Below Detection Limit
BDL
BDL BDL
BOL
BDL
BDL
BOL
BDL
BDL
BDL BDL
73.9 73.7
77.4
83.5 100.
70.6
Det. Limit -Practical Quantitation Limit(PQL)
0.43
0.43 0.43
0.43
0.43
0.43
0.43
0.43
0.43
0.43 0.43
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
% Rec.
% Rec •
% Rec.
% Rec.
% Rec.
% Rec.
12065 Lebanon Rd .
Mt. Juliet, TN 37122
[phone]
t-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September: 26,2013
ESC Sample • L657552-06
Site ID GRARAM, NC
Pr:oject i : 130524.240
Method Date Analyst
82700 09/17/13 0602 KMF
8270D 09/17/13 0602 KMF 82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF 82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF 82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF 8270D 09/17/13 0602 KMF
82700 09/17/13 0602 Kl.fF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
82700 09/17/13 0602 KMF
Laboratory Certification Numbers:
AIHA -100789, AL-40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY-90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA-00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be r:eproduced, except in full, without the written approval from ESC.
The reported analytical r:esults relate only to the sample submitted Reported: 09/26/13 15:16 Printed: 09/26/13 15:18
Page 24 of 43
•
•
•
YOUR LAU OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received September 14, 2013
Description Oneida lUll Site
Sample ID B-2
Collected By Todd Peterman Collection Date 09/11/13 10: 45
Parameter
Total Solids
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Volatile Organics
Acetone
Acrylonitrile Benzene
Bromochloromethane
Bromodichloromethane Bromoform
Bromomethane Carbon disulfide
Carbon tetrachloride Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Dibromomethane 1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene 1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethy1ben;~ene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry Result
64.3
BDL
BDL
250
BDL
95.
9.2 7.0
BDL
BDL
80L 80L
80L
BDL BDL
BDL
BDL
BDL
BDL 8DL
8DL
BDL BDL
BDL
8DL
BDL
8DL
8DL
BDL
8DL 8DL
BDL
BDL
8DL
BDL
8DL
Det. Limit -Practical Quantitation Limit{PQL)
Oet. Limit Units
0.100 '
0.031 mg/kg
3.1 mg/kg
0.78 mg/kg
0.78 mg/kg
1.6 mg/kg
0.78 mg/kg
3.1 mg/kg
1.6 mg/kg
0.078 mg/kg
0.016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg 0.0016 mg/kg
0.0078 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg 0.0016 mg/kg
0.0078 mg/kg
0.0078 mg/kg 0.0039 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0039 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
0.0016 mg/kg
12065 Lebanon Rd •
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample It : L657552-07
Site ID GRAHAM, NC
Project t : 130524.240
Method Date Analyst
2540 G-20 09/18/13 0942 KDW
7471
60108
60108
60108 60108
60108
60108
60108
82608
82608 82608
82608
82608
82608
82608
82608
8260B
82608 82608
82608
82608 82608
82608
82608
82608
82608
82608
82608
82608 82608
82608
82608
82608
8260B
82608
09/17/13 1407 CAF
09/25/13 2053 ALT
09/25/13 2053 ALT
09/25/13 2053 ALT
09/25/13 2053 ALT
09/25/13 2053 ALT
09/25/13 2053 ALT
09/25/13 2053 ALT
09/19/13 1637 RB
09/19/13 1637 RB 09/19/13 1637 RB
09/19/13 1637 R8
09/19/13 1637 RB 09/19/13 1637 RB
09/19/13 1637 RB 09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB 09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB 09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB 09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB
09/19/13 1637 RB 09/19/13 1637 RB
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -&87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC-ENV375,DW21704, ND-R-140 1 SC-84004, TN-2006, VA-00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Paqe 25 of 43
•
•
•
YOUR L/18 OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
B-2
Todd Peterman 09/11/13 10:45
Parameter Dry Result Det. Limit
2-Hexanone
Iodomethane 2-Butanone (MEK}
Methylene Chloride
4-Methyl-2-pentanone (MIBK}
Styrene 1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrach1oroethane
Tetrachloroethane Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylenes, Total Surrogate Recovery
Toluene-dB Dibromof1uoromethane
a,a,a-Trifluorotoluene
4-Bromofluorobenzene
Polychlorinated Biphenyls PCB 1016
PCB 1221
PCB 1232 PCB 1242
PCB 1248
PCB 1254
PCB 1260
PCBs Surrogates Decachlorobipheny1
Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaphthene
Acenaphthylene Anthracene
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL
BDL
97.0 93.9
100.
103.
BDL
BDL
BDL BDL
BDL
BDL
BDL
87.7
102.
BDL
BDL BDL
Det. Limit-Practical Quantitation Limit(PQL)
0.016 0.016
0.016
0.0078
0.016
0.0016 0.0016
0.0016
0.0016 0.0078
0.0016
0.0016
0.0016
0.0078 0.0039
0.016
0.0016 0.0047
0.026
0.026
0.026 0.026
0.026
0.026
0.026
0.051
0.051 0.051
Units
mq/kq
mq/kq
mq/kq mq/kq
mq/kq
mq!kq mg/kq
mg/kq
mg/kq
mg/kq
mg/kq
mg/kq
mg/kq
mg/kg mg/kg
mg/kg
mg/kg mg/kq
't Rec.
't Rec.
't Rec.
't Rec.
mq/kq
mq/kq mq/kg
mg/kg
mg/kg
mg/kg
mq/kg
't Rec.
% Rec.
mg/kq mq/kq
mg/kg
12065 Lebanon Rd .
Mt. Juliet, Ttl 31122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample i L657552-07
Site ID GRAHAl4, NC
Project # : 130524.240
t4ethod Date Analyst
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
82608 09/19/13 1637 RB
82608 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
82608 09/19/13 1637 RB
82608 09/19/13 1637 RB
82608 09/19/13 1637 RB
82608 09/19/13 1637 RB
8260B 09/19/13 1637 RB
82608 09/19/13 1637 RB
82608 09/19/13 1637 RB
82608 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB
8260B 09/19/13 1637 RB 8260B 09/19/13 1637 RB
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8082 09/20/13 1403 ND
8270D 09/17/13 0623 KMF
8270D 09/17/13 0623 KlolF
8270D 09/17/13 0623 KMF
Laboratory certification Numbers:
AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, ND -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Page 26 of 43
•
•
•
ltESC
YOUR LAB OF CHOICE:
REPORT OF ANALYSIS
Tom Driver
GEC -14acon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-2
Todd Peterman
09/11/13 10:45
Parameter Dry Result Det. Limit
Benzidine Benzo(a}anthracene
Benzo(b}fluoranthene Benzo(k}fluoranthene
Benzo(g,h,i}perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether
Bis{2-ch1oroisopropyl}ether. 4-Bromophenyl-phenylether
2-Chloronaphthalene 4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-0initrotoluene
l!'luoranthene
Fluorene
Hexachlorobenzene Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL 0.082
0.10 BDL
BOL
0.070
BOL
BOL
BDL BOL
BDL BDL
0.10
BDL
BDL
BDL
BDL
0.19
BDL
BDL BDL
BDL
BDL BDL
BDL BDL
BDL
BDL
BDL
BDL 0.087
BDL
BDL
BDL
BDL
BDL
BDL
0.17 BDL
Det. Limit -Practical Quantitation Limit(PQL)
0.52 0.051
0.051
0.051 0.051
0.051
0.52 0.52
0.52 0.52
0.051
0.52
0.051
0.051
0.52
0.52
0.52
0.051
0.051
0.52 0.52
0.52
0.52 0.051
0.52
0.051 0.52
0.52 0.52
0.52 0.051
0.52
0.52 0.52
0.52
0.52
0.52
0.051
0.52
Units
mg/kq mq/kq
mg/kq mq/kq
mq/kq
mq/kq
mg/kg
mg/kg
mq/kq mq/kg
mg/kg
mq/kq mg/kq
mq/kq mq/kg
mq/kg
mq/kg mg/kq
mg/kg
mq/kg mg/kq
mg/kg mg/kg
mq/kg
mq/kq mg/kg
mq/kg
mg/kg
mq/kg
mq/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kg
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
FaK [phone]
TaK I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample It L657552-07
Site ID GRAHAt-1, NC
Project . : 130524.240
Method Date Analyst
8270D 09/17/13 0623 KME' 8270D 09/17/13 0623 KME'
82700 09/17/13 0623 KME' 82700 09/17/13 0623 KME'
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
8270D 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF 82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF 82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF 82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KME'
82700 09/17/13 0623 KME'
8270D 09/17/13 0623 KME' 8270D 09/17/13 0623 KME'
82700 09/17/13 0623 KME'
82700 09/17/13 0623 KME'
82700 09/17/13 0623 KME'
82700 09/17/13 0623 KME' 82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF 8270D 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 Kl-lF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 Kl4E'
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,DW21704, ND -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY-11742, NJ-TN002 1 WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Page 27 of 43
•
•
YOUR LAO OP CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
!~aeon, GA 31204
Date Received Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
B-2
Todd Peterman
09/11/13 10:45
Parameter Dry Result Det. Limit
4-Chloro-3-methylphenol
2-Chlorophenol 2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol 4-Nitrophenol
Pentachlorophenol
Phenol 2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5 2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-dl4
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
67.7
65.9
70.6
74.3
81.3
61.8
Det. Limit -Practical Quantitation Limit(PQL)
0.52
0.52
0.52
0.52
0.52
0.52
0.52
0.52
0.52 0.52
0.52
Units
mg/kq
mg/kg
mg/kq
mg/kg
mg/kq
mq/kq
mg/kg
mg/kq
mg/kq mg/kg
mg/kq
' Rec.
' Rec •
' Rec.
' Rec.
' Rec.
' Rec.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-07
Site ID GRAH.Al-1, NC
Project # : 130524.240
l~ethod Date Analyst
8270D 09/17/13 0623 KMF
82700 09/17/13 0623 Kt·IF 82700 09/17/13 0623 Kt~F
8270D 09/17/13 0623 IGIF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF
82700 09/17/13 0623 Kt4E'
82700 09/17/13 0623 Kt4F
82700 09/17/13 0623 KME'
82700 09/17/13 0623 Kt4F
82700 09/17/13 0623 Kt~E'
82700 09/17/13 0623 KMF
82700 09/17/13 0623 KMF 82700 09/17/13 0623 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375 1 DW21704, NO -R-140, SC -840041 TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, UY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted Reported: 09/26/13 15:16 Printed: 09/26/13 15:18
Page 28 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received September 14, 2013
Description Oneida Mill Site
Sample ID B-3
Collected By Todd Peterman
Collection Date 09/11/13 11:20
Parameter
Total Solids
Mercury
Arsenic Barium
Cadmium
Chromium
Lead
Selenium Silver
Volatile Organics Acetone
Acrylonitrile
Benzene Bromochloromethane
Bromodichloromethane
Bromoform Bromomethane
Carbon disulfide Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane Chloroethane
Chloroform
Chloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dich1oro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dich1oropropene
Ethylbenzene
Results listed are dry weight basis. BDL -Below Detection Limit
Dry Result
72.0
BDL
BDL
210
BDL
39. 14.
12. BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
BDL BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit(PQL)
Det. Limit Units
0.100 '
0.028 mg/kg
6.9 mg/kg
1.7 mg/kg
1.7 mg/kg
3.5 mg/kg
1.7 mg/kg
6.9 mg/kg
3.5 mg/kg
0.069 mg/kq
0.014 mq/kq
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0069 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0069 mg/kg
0.0069 mg/kg
0.0035 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0035 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
0. 0014 mg/kg
0. 0014 mg/kg
0.0014 mg/kg
0.0014 mg/kg
12065 Lebanon Rd •
Mt. Juliet, Tll 37122
[phone]
1-800-767-5859
Fax [phone]
Tax r.o. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-08
Site ID GRAHAH, NC
Project I : 130524.240
Method Date Analyst
2540 G-20 09/18/13 0942 KDW
7471 CAF 09/17/13 1410
60108 ALT 09/26/13 1337
6010B ALT 09/26/13 1337
60108 ALT 09/26/13 1337
60108 ALT 09/26/13 1337
60108 ALT 09/26/13 1337
6010B ALT 09/26/13 1337
60108 ALT 09/26/13 1337
82608
82608
82608
82608
82608
82608
82608
82608 82608
82608 82608
82608
8260B
82608
82608
82608
8260B
82608
82608 82608
8260B
8260B 8260B
82608
82608
82608
82608
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB 09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 R8 09/19/13 1654 RB
09/19/13 1654 R8
09/19/13 1654 RB
09/19/13 1654 R8
09/19/13 1654 RB 09/19/13 1654 R8
09/19/13 1654 RB
09/19/13 1654 RB 09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
09/19/13 1654 RB
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL-E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 29 of 43
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver GEC -Macon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-3
Todd Peterman 09/11/13 11:20
Parameter Dry Result Det. Limit
2-Hexanone Iodomethane
2-Butanone (MEK) Methylene Chloride
4-l.fethyl-2-pentanone (14IBK)
Styrene 1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene 1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylenes, Total
Surrogate Recovery
Toluene-dB
Dibromofluoromethane a,a,a-Trifluorotoluene
4-Bromofluorobenzene
Polychlorinated Biphenyls
PCB 1016
PCB 1221
PCB 1232
PCB 1242 PCB 1248
PCB 1254
PCB 1260'
PCBs Surrogates
Decachlorobiphenyl
Tetrachloro-m-xylene
Base/Neutral Extractables Acenaphthene
Acenaphthylene
Anthracene
Results listed are dry weight basis. 80L -Below Detection Limit
BDL BDL
BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL BDL
BDL BDL
BDL
BDL
BDL
99.4 95.1
102.
97.9
BDL
BDL
BDL
BDL
BDL BDL
0.024
92.6
103.
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit(PQL)
0.014 0.014
0.014 0.0069
0.014
0.0014
0.0014
0.0014
0.0014 0.0069
0.0014 0.0014
0.0014
0.0069 0.0035
0.014
0.0014
0.0042
0.024
0.024
0.024
0.024 0.024
0.024
0.024
0.046 0.046
0.046
Units
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
% Rec.
% Rec.
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
mg/kg
mg/kg
mg/kg
12065 Lebanon Rd.
Mt. Juliet, Til 37122
(6151 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0914299
Est. 1970
September 26,2013
ESC Sample f. : L657552-08
Site ID GRAHAI4, NC
Project I : 130524.240
14ethod Date Analyst
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
8260B 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 R8
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
8260B 09/19/13 1654 RB
8260B 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
82608 09/19/13 1654 RB
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
8082 09/20/13 1413 ND
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KI4F
82700 09/17/13 0645 KI4F
Laboratory Certification Numbers: AIHA -1007891 AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST -0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN -2006, VA-00109, WV-233
AZ -0612, MN -047-999-395, NY -11742, NJ-TN002, WI -998093910
Note: This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 30 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida 14111 Site
B-3
Todd Peterman
09/11/13 11:20
Parameter Dry Result Det. Limit
Benzidine
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene Dibenz(a,h)anthracene
3,3-Dichlorobenzidine 2,4-Dinitrotoluene
2,6-Dinitrotoluene
ll'luoranthene
Fluorene Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene Isophorone
Naphthalene
Nitrobenzene n-Nitrosodimethylamine
n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
Results listed are dry weight basis. BDL -Below Detection Limit
BDL
BDL
BDL
BDL
BOL
BDL
BOL
BOL BOL
BDL
BDL BOL
BOL BDL
BOL
BOL BOL
BOL
BOL BOL
BOL
BOL
BDL
BOL BOL
BOL
BOL
BOL
BOL
BOL BDL
BDL
BDL
BDL
BDL BDL
BDL BDL
BDL
Det. Limit -Practical Quantitation Limit(PQL)
0.46
0.046 0.046
0.046
0.046 0.046
0.46
0.46 0.46
0.46
0.046
0.46
0.046 0.046
0.46
0.46 0.46
0.046
0.046 0.46
0.46
0.46
0.46
0.046 0.46
0.046
0.46 0.46 o. 46
0.46 0.046
0.46
0.46
0.46
0.46 0.46
0.46 0.046
0. 46
Units
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kq
mg/kg mq/kg
mg/kq mg/kg
mg/kg
mg/kg mq/kg
mq/kg
mq/kg mq/kq
mq/kg
mg/kg mq/kq
mq/kg
mg/kq mq/kq
mq/kq mg/kq
mq/kq
mq/kq mq/kg
mq/kq
mq/kq mq/kg
mq/kg mq/kq
mq/kg
12065 Lebanon Rd .
}lt. Juliet, TN 37122 [phone]
1-900-767-5859
rax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample It L657552-08
Site ID GRAHAM, NC
Project i : 130524.240
l~ethod Date Analyst
8270D 09/17/13 0645 KHF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
8270D 09/17/13 0645 KMII'
82700 09/17/13 0645 KMII'
82700 09/17/13 0645 KMII'
82'700 09/17/13 0645 KMF
82'700 09/17/13 0645 KMII' 82700 09/17/13 0645 KMII'
82700 09/17/13 0645 KMII'
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMII'
82700 09/17/13 0645 KMF 82700 09/17/13 0645 KMF
82'700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF 82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82'700 09/17/13 0645 KMF 82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF 8270D 09/17/13 0645 Kt.fF
82700 09/17/13 0645 KI4F
82700 09/17/13 0645 KI4F
82700 09/17/13 0645 KMF
82700 09/17/13 0645 Kt4F
82700 09/17/13 0645 KMF
82'700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 K~IF
82700 09/17/13 0645 KMF
82'700 09/17/13 0645 KMF
Laboratory Certification Numbers: AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, II'L -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Page 31 of 43
•
•
•
.-ESC
YOUR LAO OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida 14ill Site
B-3
Todd Peterman 09/11/13 11:20
Parameter Dry Result Oet. Limit
4-Chloro-3-methylphenol
2-Ch1orophenol 2,4-Dichloropheno1
2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol Phenol-d5
Nitrobenzene-d5 2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl.-d14
Results listed are dry weight basis.
BDL -Bel.ow Detection Limit
BDL
BDL BDL
BDL BDL
BDL
BDL
BDL
BDL BDL
BDL
61.8 62.9
63.8 74.5
88.4
65.8
Det. Limit -Practical Quantitation Limit(PQL)
0.46
0.46 0.46
0.46
0.46 0.46
0.46 0.46
0.46
0.46
0.46
Units
mg/kg
mg/kg mq/kg
mq/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
% Rec.
% Rec .
% Rec.
% Rec.
% Rec.
% Rec.
12065 Lebanon Rd .
Mt. Juliet, Ttl 37122
[phone]
1-800-767-5959
Fax [phone]
Tax I.O. 62-0814289
Est. 1970
September 26,2013
ESC Sample i L657552-08
Site ID GRAHAH, NC
Project It : 130524.240
Method Date Analyst
82700 09/17/13 0645 KI4F
82700 09/17/13 0645 KHF 82700 09/17/13 0645 KMF
82700 09/17/13 0645 KI4F
82700 09/17/13 0645 KMF 82700 09/17/13 0645 KI4F
82700 09/17/13 0645 KI4F 82700 09/17/13 0645 KMF
8270D 09/17/13 0645 KI4F
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF 82700 09/17/13 0645 Kl·lF
82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF 82700 09/17/13 0645 KMF
82700 09/17/13 0645 KMF
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY-90010, KYUST -0016, NC-ENV375,DW21704, NO-R-140, SC-84004, TN -2006, VA-00109, WV-233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical resul.ts relate only to the sampl.e submitted
Reported: 09/26/13 15:16 Printed: 09/26/13 15:18
Page 32 of 43
•
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received September 14, 2013
Description Oneida Mill Site
Sample ID B-6
Collected By Todd Peterman
Collection Date 09/12/13 13:55
Parameter
Total Solids
Mercury
Arsenic Barium
Cadmium
Chromium Lead
Selenium
Silver
Volatile Organics
Acetone
Acrylonitrile Benzene
8romochloromethane
Bromodichloromethane
Bromoform Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform Chloromethane
Dibromomethane
1,2-Dichlorobenzene 1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry Result
76.1
0.049
5.5
110
8DL
41. 38.
5.1
8DL
8DL
BDL
BDL BDL
BDL
BDL
BDL
BDL
BDL 8DL
BOL
BDL
80L
8DL
80L
8DL BOL
8DL
BDL
BDL
BOL
BOL
BOL
BOL
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit{PQL)
Det. Limit Units
0.100 ' 0.026 mg/kg
1.3 mq/kg
0.33 mg/kg
0.33 mg/kg
0.66 mg/kg 0.33 mq/kg
1.3 mg/kg
0.66 mq/kg
0.066 mg/kg 0.013 mg/kg
0.0013 mq/k<;j
0.0013 mg/kg
0.0013 mg/kg
0.0013 mq/kg
0.0066 mq/kg
0.0013 mg/kg
0.0013 mg/kg 0.0013 mg/kg
0.0013 mg/kg
0.0066 mg/kg
0.0066 mq/kg
0.0033 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg 0.0033 mg/kg
0.0013 mg/kg
0.0013 mg/kg 0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mq/kq
12065 Lebanon Rd .
11t. Juliet, TN 37122
[phone]
1-900-767-5859
Fax [phone]
Tax I.D. 62-0914299
Est. 1970
September 26,2013
ESC Sample I L657552-09
Site ID GRAHAM, NC
Project t : 130524.240
Method Date Analyst
2540 G-20 09/18/13 0942 KDW
7471 09/18/13 1016 CAF
60108 09/26/13 1305 ALT
60108 09/26/13 1305 ALT
60108 09/26/13 1305 ALT
60108 09/26/13 1305 ALT 60108 09/26/13 1305 ALT
60108 09/26/13 1305 ALT
60108 09/26/13 1305 ALT
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB 82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB
82608 09/18/13 1715 RB 8260B 09/18/13 1715 R8
82608 09/18/13 1715 R8
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
Laboratory Certification Numbers: AIHA -100789, AL -40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST -0016, NC-ENV375,DW21704, NO -R-140, SC-84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 33 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received Description
Sample ID
Collected By Collection Date
September 14, 2013 Oneida !~ill Site
8-6
Todd Peterman
09/12/13 13:55
• Parameter Dry Result Det. Limit
2-Hexanone
Iodomethane
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK) Styrene .
1,1,1,2-Tetrachloroethane 1,1,2,2-Tetxachloroethane
Tetrachloroethane
Toluene
1,1,1-Trichloroethane
1,1,2-Txichloroethane
Trichloroethane
Trichlorofluoromethane
1,2,3-Trich1oropropane Vinyl acetate
Vinyl chloride
Xylenes, Total Surroqate Recovery
Toluene-dB
Dibromofluoromethane
a,a,a-Trifluorotoluene
4-Bromofluorobenzene
Polychlorinated Biphenyls
PCB 1016 PCB 1221
PCB 1232 PCB 1242
PCB 1248
PCB 1254
PCB 1260
PCBs Surrogates
Decachlorobiphenyl Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaphthene
Acenaphthylene Anthracene
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL BDL
BDL
BDL
BDL
BDL
BDL BDL
BDL BDL
BDL
8DL
BDL
BDL
BDL
BDL
BDL
102.
105. 107.
94.4
BDL
BDL
BDL
BOL BDL
BDL
BDL
81.4 101.
BDL
BDL BDL
Det. Limit -Practical Quantitation Limit(PQL)
0.013
0.013 0.013
0.0066
0.013
0.0013
0.0013
0.0013 0.0013
0.0066 0.0013
0.0013
0.0013 0.0066
0.0033
0.013
0.0013
0.0039
0.022
0.022
0.022
0.022 0.022
0.022
0.022
0.22
0.22
0.22
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kq
mq/kq
mg/kg
' Rec.
' Rec.
' Rec.
' Rec.
mq/kq
mq/kq
mg/kq
mq/kq mq/kq
mq/kq
mq/kq
% Rec.
% Rec.
mq/kq
mq/kq
mglkq
12065 Lebanon Rd .
Mt. Juliet, TN 31122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample It L657552-09
Site ID GRAHAM, NC
Project I : 130524.240
Method Date Analyst
8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB 8260B 09/18/13 1715 RB 8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB 8260B 09/18/13 1715 RB
8260B 09/18/13 1715 RB 82608 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB 82608 09/18/13 1715 RB 82608 09/18/13 1715 RB
82608 09/18/13 1715 RB 82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB
82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB 82608 09/18/13 1715 RB
8260B 09/18/13 1715 RB
8082 09/23/13 1514 ~m
8082 09/23/13 1514 NO
8082 09/23/13 1514 llD
8082 09/23/13 1514 NO 8082 09/23/13 1514 llD
8082 09/23/13 1514 NO
8082 09/23/13 1514 NO
8082 09/23/13 1514 NO
8082 09/23/13 1514 NO
82700 09/17/13 0728 Kl~F
82700 09/17/13 0728 Kl~F
82700 09/17/13 0728 Kl~F
Laboratory Certification Numbers: AIHA -100789, AL -40660, CA -I-2327, CT-PH-01971 FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYOST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -20061 VA -00109, WV -233 AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 34 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Tom Driver GEC -Macon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample 10
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-6
Todd Peterman
09/12/13 13:55
Parameter Dry Result Oet. Limit
Benzidine
Benzo(a)anthracene
Benzo(b)fluoranthene Benzo(k)fluoranthene
Benzo(g,h,i)perylene Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene 3,3-Dichlorobenzidine
2,4-Dinitrotoluene 2,6-Dinitrotoluene
Fluoranthene
Fluorene Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene Hexachloroethane
Indeno(l,2,3-cd)pyrene Isophorone
Naphthalene
Nitrobenzene n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate
Diethyl phthalate Dimethyl phthalate
Di-n-octyl phthalate
J?yrene
1,2,4-Trichloroben~ene
Acid Extractables
Results listed are dry weight basis. BDL -Below Detection Limit
BDL
BDL
0.22 BDL
BDI. BDL
BDI.
BDL
BDL
BDL
BDL
BDL
0.22
BDL BDL
BDL BDL
0.42
BDL BOL
BOL
BDL BDL
BDL BDL
BDL
BDL
BOL
BOL
BOL
0.34
BDL
BDL BDL
BDL BDL
BDL
0.33
BDL
Det. Limit -Practical Quantitation Limit(PQL)
2.2
0.22
0.22 0.22
0.22 0.22
2.2
2.2 2.2
2.2
0.22 2.2
0.22
0.22 2.2
2.2
2.2 0.22
0.22
2.2
2.2 2.2 2.2
0.22 2.2
0.22
2.2 2.2
2.2
2.2 0.22
2.2
2.2 2.2
2.2 2.2
2.2
0.22
2.2
Units
mg/kg
mg/kg mq/kq
mqlkq
mg/kg mq/kq
mg/kg
mg/kg
mg/kg
mq/kq
mg/kg mq/kq
mq/kq mq/kq
mq/kq
mq/kq
mq/kq
mq/kq
mq/kq
mqlkq
mq/kq mg/kg
mq/kq
mq/kq mq/kq
mg/kg
mq/kg
mq/kq
mq/kq
mq/kg
mg/kg
mg/kg
mq/kq mg/kg
mq/kq mg/kg
mq/kq mg/kg
mg/kg
12065 Lebanon Rd .
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax l.D. 62-0814269
Est. 1970
September 26,2013
ESC Sample ll L657552-09
Site ID GRAHA!-1, NC
Project It : 130524.240
Method Date Analyst
82700 09/17/13 0728 KI~F
82700 09/17/13 0728 Kl~F 8270D 09/17/13 0728 KMF 82700 09/17/13 0728 Kl~F
8270D 09/17/13 0728 KMF 82700 09/17/13 0728 KI4F
8270D 09/17/13 0728 KI4F
8270D 09/17/13 0728 KMF
8270D 09/17/13 0728 KI4F
8270D 09/17/13 0728 KMF
8270D 09/17/13 0728 KMF 8270D 09/17/13 0728 K~IF
8270D 09/17/13 0728 KMF 8270D 09/17/13 0728 KMF
8270D 09/17/13 0728 KMF
8270D 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
8270D 09/17/13 0728 KMJ:'
82700 09/17/13 0728 KMr
8270D 09/17/13 0728 KMr
82700 09/17/13 0728 KMr 82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF 82700 09/17/13 0728 KMF
8270D 09/17/13 0728 KMF
8270D 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 Kl~F
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
8270D 09/17/13 0728 Kl4F 8270D 09/17/13 0728 KMF
8270D 09/17/13 0728 Kt~r
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA-923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,0W21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted
Paqe 35 of 43
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-6
Todd Petennan
09/12/13 13:55
Parameter Dry Result Det. Limit
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol Pentachlorophenol
Phenol 2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-dl4
Results listed are dry weight basis. BOL -Below Detection Limit
BDL BDL
BDL BOL
BDL BDL
BDL
BDL BDL
BDL BDL
59.8
61.6
71.9
89.4
78.0
78.1
Det. Limit-Practical Quantitation Limit(PQL)
2.2
2.2
2.2 2.2
2.2
2.2
2.2
2.2 2.2
2.2
2.2
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/ltg
mq/kg
mg/kg mg/kg
mg/ltg
mg/kg
' Rec.
' Rec.
' Rec.
' Rec.
' Rec.
' Rec.
12065 Lebanon Rd .
Mt. Juliet, Til 37122
(6151 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample it L657552-09
Site ID GRAHAM, NC
Project . : 130524.240
Method Date Analyst
82700 09/17/13 0728 KMF 82700 09/17/13 0728 KMF
82700 09/17/13 0728 KI~F 82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF
82700 09/17/13 0728 Kl·IF 82700 09/17/13 0728 KMF
82700 09/17/13 0728 Kl·IF
82700 09/17113 0728 Kl4F
82700 09/17/13 0728 KMF
82700 09/17/13 0728 KMF 82700 09/17/13 0728 Kl~F
82700 09/17/13 0728 KI~F
82700 09/17/13 0728 KMF 82700 09/17/13 0728 Kt~F
Laboratory Certification Numbers: AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, ND -R-140, SC -84004, TN -2006, VA -00109, WV -233 AZ -0612, l4N -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/26/13 15:16 Printed: 09/26/13 15:18
Page 36 of 43
•
•
•
-ESC
YOUR LJ\B OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received September 14, 2013
Oeser iption Oneida Mill Site
Sample ID 8-8
Collected By Todd Peterman Collection Date 09/12/13 00:00
Parameter
Total Solids
Mercury
Arsenic
Barium Cadmium
Chromium
Lead Selenium
Silver
Volatile Organics
Acetone
Acrylonitrile Benzene
Bromochloromethane
Bromodichloromethane Bromoform
8romomethane Carbon disulfide
Carbon tetrachloride
Chlorobenzene Chlorodibromomethane
Chloroethane Chloroform
Chloromethane
Dibromomethane 1,2-Dichlorobenzene
1,4-0ichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene 1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene Ethylbenzene
Results listed are dry weight basis.
8DL -Below Detection Limit
Dry Result
77.3
0.054
12.
270
1.8 14.
83.
5.3 8DL
BDL
BDL BDL
BDL
BDL
BDL
BDL
BDL BDL
BDL
BDL
BDL
80L 8DL
8DL 80L
8DL
BDL
8DL
8DL
BDL
8DL
8DL
8DL BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit(PQL)
Det. Limit Units
0.100 ' 0.026 mg/kg
1.3 mg/kg
0.32 mg/kg
0.32 mg/kg 0.65 mg/kg
0.32 mg/kg
1.3 mg/kg 0.65 mg/kg
0.065 mg/kg
0.013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0065 mg/kg
0.0013 mg/kg 0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0065 mg/kg
0.0065 mg/kg 0.0032 mg/kg
0.0013 mg/kg
0.0013 mg/kg 0.0013 mg/kg-
0.0032 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
0.0013 mg/kg
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-900-767-5859
Fax [phone]
Tax I.D. 62-0814299
Est. 1970
September 26,2013
ESC Sample i L657552-l0
Site ID GRAHAI.f, NC
Project t : 130524.240
Method Date Analyst
2540 G-20 09/18/13 0942 KDW
7471 09/18/13 1033 CAF
60108
60108
60108 60108
60108 60108
60108
8260B
82608 82608
82608
82608
82608
82608
82608 82608
82608
82608
82608
82608 82608
82608
82608 82608
82608 8260B
8260B
82608
82608
82608
82608 82608
82608
82608
09/26/13 1310 ALT
09/26/13 1310 ALT
09/26/13 1310 ALT 09/26/13 1310 ALT
09/26/13 1310 ALT 09/26/13 1310 ALT
09/26/13 1310 ALT
09/18/13 1555 R8
09/18/13 1555 RB 09/18/13 1555 R8
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB 09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB 09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB 09/18/13 1555 RB
09/18/13 1555 R8 09/18/13 1555 R8
09/18/13 1555 R8
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB
09/18/13 1555 RB 09/18/13 1555 R8
09/18/13 1555 RB
09/18/13 1555 RB
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, l-IN -047-999-395, NY -11742, NJ -TN002, WI -998093910
uote:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 37 of 43
•
•
•
.-ESC
YOUR LA() OF CHOICE
REPORT OF ANALYSIS
Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd. 14acon, GA 31204 ·
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013 Oneida Mill Site
B-8
Todd Peterman 09/12/13 00:00
Parameter Dry Result Det. Limit
2-Hexanone
Iodomethane 2-8utanone {MEK)
Methylene Chloride
4-Methyl-2-pentanone (l~IBK) Styrene
1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane
Tetrachloroethene Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane 'l'richloroethene
'l'richlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylenes, Total
Surrogate Recovery
Toluene-dB
Dibromofluoromethane
a,a,a-Trifluorotoluene
4-8romofluorobenzene
Polychlorinated Biphenyls
PCB 1016 PCB 1221
PCB 1232 PCB 1242
PCB 1248
PCB 1254 PCB 1260
PCBs Surrogates
Decachlorobiphenyl Tetrachloro-m-xylene
Base/Neutral Extractables
Acenaphthene
Acenaphthylene Anthracene
Results listed are dry weight basis,
BDL -Below Detection Limit
80L
8DL BDL
BDL
BDL BDL
BDL BDL
8DL BDL
BDL
BDL BDL
BDL
BDL BDL
BDL
BDL
92.1
114.
98.6
39.2
BDL BDL
BDL
BDL
BDL
BDL
BDL
82.3 93.1
BDL
BDL
BDL
Det. Limit -Practical Quantitation Limit{PQL)
0.013
0.013 0.013
0.0065
0.013 0.0013
0.0013 0.0013
0.0013
0.0065
0.0013
0.0013
0.0013 0.0065
0.0032 0.013
0.0013
0.0039
0.022 0.022
0.022
0.022
0.022
0.022
0.022
2.1
2.1
2.1
On its
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
% Rec.
% Rec.
mg/kg mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
% Rec.
% Rec.
mg/kg
mg/kg
mg/kg
12065 Lebanon Rd .
Mt. Juliet, Ttl 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample i L657552-10
Site ID GRAHAM, NC
Project t : 130524.240
Method Date Analyst
82608 09/18/13 1555 RB
82608 09/18/13 1555 RB 82608 09/18/13 1555 R8
82608 09/18/13 1555 RB
8260B 09/18/13 1555 RB 82608 09/18/13 1555 RB
82608 09/18/13 1555 RB 82608 09/19/13 1555 RB
82608 09/18/13 1555 RB
82608 09/18/13 1555 RB
8260B 09/19/13 1555 RB
82608 09/18/13 1555 RB
92608 09/18/13 1555 RB 8260B 09/18/13 1555 RB
8260B 09/18/13 1555 RB 82608 09/18/13 1555 RB
82608 09/18/13 1555 RB
8260B 09/18/13 1555 R8
8260B 09/18/13 1555 RB
8260B 09/18/13 1555 RB
82608 09/18/13 1555 RB
8260B 09/18/13 1555 RB
8082 09/23/13 1525 NO 8082 09/23/13 1525 ND
8082 09/23/13 1525 NO
8082 09/23/13 1525 NO
8082 09/23/13 1525 ND
8082 09/23/13 1525 NO
8082 09/23/13 1525 NO
8082 09/23/13 1525 NO 8082 09/23/13 1525 ND
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUS'l' -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 38 of 43
•
•
•
.-ESC
YOUR LAS OF CHOICE
REPORT OF ANALYSIS
Tom Driver GEC -Macon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By Collection Date
September 14, 2013
Oneida Mill Site
B-8
Todd Peterman 09/12/13 00:00
Parameter Dry Result Det. Limit
Benzidine
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether Chrysene
Dibenz(a,h)anthracene
3,3-Dichlorobenzidine 2,4-0initrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
6.1
7.0
2.2 4.4
6.2
BOL
BOL
BDL
BDL
BDL
BOL
6.2
BDL
BDL BDL
BDL
8.9 BDL
BDL
BDL
BDL
BDL
3.9
BDL BDL
BDL
BDL
BDL
BDL
3.9
BDL
BDL
BDL BOL
BDL BDL
10.
BDL
Det. Limit-Practical Quantitation Limit(PQL)
22.
2.1
2.1
2.1 2.1
2.1
22. 22.
22.
22.
2.1
22.
2.1 2.1
22. 22.
22.
2.1 2.1
22.
22.
22.
22. 2.1
22.
2.1 22.
22.
22.
22.
2.1
22. 22.
22. 22.
22.
22. 2.1
22.
Units
mg/kg
mg/kg
mg/kg
mg/kg
!D-9'/kg mq/kq
mg/kq mq/kq
mq/kq
mq/kq
mg/kg
mg/kq
mg/kq
mg/kg
mg/kq mg/kq
mg/kq
mg/kg mg/kg
mg/kg
mg/kg
mq/kq
mg/kg
mg/kg
mq/kg
mq/kq mq/kg
mq/kg
mg/kg
mg/kg
mg/kq
mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kq
1206S Lebanon Rd •
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
FaK [phone]
TaK I.D. 62-0814289
Est. 1970
September 26,2013
ESC Sample i L657552-10
Site IO GRAHAM, NC
Project i : 130524.240
14ethod Date Analyst
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KI4F
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KI4F
82700 09/20/13 1349 KMF
8270D 09/20/13 1349 Kl4F 8270D 09/20/13 1349 KMF
8270D 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KI4F
82700 09/20/13 1349 KI4F
8270D 09/20/13 1349 Kt-JF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KI4F
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KJ.lF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01 KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -84004, TN -2006, VA -00109, WV -233
AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910 Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 39 of 43
•
•
•
YOUR LAB OF CHOICE
REPORT OF ANALYSIS Tom Driver
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
Sample ID
Collected By
Collection Date
September 14, 2013
Oneida Mill Site
B-8
Todd Peterman
09/12/13 00:00
Parameter Dry Result Det. Limit
4-Chloro-3-methy1phenol
2-Chlorophenol 2,4-0ichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol 2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl 2,4,6-Tribromophenol
p-Terphenyl-d14
Results listed are dry weight basis. BDL -Below Detection Limit
BDL
BOL
BOL BOL
BDL BDL
BDL
BDL
BDL
BOL BDL
55.0
63.5 67.0
82.9
58.0 105.
Det. Limit -Practical Quantitation Limit{PQL}
22.
22.
22. 22.
22.
22. 22.
22.
22.
22.
22.
Units
mg/kg
mg/kg
mg/kg mg/kg
mg/kg mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mg/kg
' Rec.
' Rec.
' Rec .
' Rec.
' Rec.
' Rec.
12065 Lebanon Rd •
Mt. Juliet, TN 37122
(6151 758-5858
1-800-767-5859
Fax [phone]
Tax 1.0. 62-0814289
Est. 1970
September 26,2013
ESC Sample I L657552-10
Site ID GRAHAM, NC
Project . : 130524.240
Method Date Analyst
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMI!'
82700 09/20/13 1349 KMI!'
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF 82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
82700 09/20/13 1349 KMF
Laboratory Certification Numbers:
AIHA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, NO -R-140, SC -840041 TN -2006, VA -00109, WV -233 AZ -0612, MN -047-999-395, NY -11742, NJ -TN002, WI -998093910
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/26/13 15:16 Printed: 09/26/13 15:18
Page 40 of 43
Attachment A • List of Analytes with QC Qualifiers
Sample Work Sample Run
Number Group Typ~ Analyte ID Qualifier
L657552-01 WG682021 SAMP Bem:idine R2818366 J
WG682596 SAMP Acetone R2819960 J6J3
WG682596 SAMP Acrylonitrile R2819960 J3
WG682596 SAMP Benzene R2819960 J3
WG682596 SAMP Bromochloromethane R2819960 J6J3
WG682596 SAMP Bromodichloromethane R2819960 J6J3
WG682596 SAMP Bromoform R2819960 J6J3
WG682596 SAMP Bromoll\ethane R2819960 J3
WG682596 SAMP Carbon disulfide R2819960 J6J3
WG682596 SAMP Carbon tetrachloride R2819960 J3
WG682596 SAMP Chlorobem:ene R2819960 J6J3
WG682596 SAMP Chlorodibromomethane R2819960 J6J3
WG682596 SAMP Chloroethane R2819960 J3
WG682596 SAMP Chloroform R2819960 J3
WG682596 SAMP ChlorOD\ethane R2819960 J3
WG682596 SAMP Dibromomethane R2819960 J6J3
WG682596 SAM!? 1,2-Dichlorobenzene R2819960 J6J3
WG682596 SAM!? 1,4-Dichlorobenzene R2819960 J6J3
WG682596 SAHP trans-1,4-Dichloro-2-butene R2819960 J6J3
WG682596 SAM!? 1,1-Dichloroethane R2819960 JJ
WG682596 SA!~ I? 1,2-Dichloroethane R2819960 J6J3
WG682596 SAM!? 1,1-Dichloroethene R2819960 J3
WG682596 SAMP cis-1,2-Dichloroethene R2819960 J6J3
WG682596 SAMP trans-1,2-Dichloroethene R2819960 J3
WG682596 SAMP 1,2-Dichloropropane R2819960 J3
WG682596 S~P cis-1,3-Dichloropropene R2819960 J6J3
WG682596 SAI4P trans-1,3-Dichloropropene R2819960 J6J3
WG682596 SA14P Ethylbenzene R2819960 J3
WG682596 SAMP 2-Hexanone R2819960 J3
WG682596 SAMP Iodomethane R2819960 J3
WG682596 SAMP 2-Butanone (MEK) R2819960 J3
WG682596 SAMP Methylene Chloride R2819960 J3
WG682596 SAMP 4-Methyl-2-pentanone (14IBK) R2819960 J3 • WG682596 SAMP Styrene R2819960 J6J3
WG682596 SAMP 1,1,1,2-Tetrachloroethane R2819960 J3
WG682596 SAMP 1,1,2,2-Tetrachloroethane R2819960 J3
WG682596 SAMP Tetrachloroethane R2819960 J3
WG682596 SAMP Toluene R2819960 J3
WG682596 SAI4P 1,1,1-Trichloroethane R2819960 J3
WG682596 SAMP 1,1,2-Trichloroethane R2819960 J3
WG682596 SAMP Trichloroethene R2819960 J3
WG682596 SAMP Trichlorofluoromethane R2819960 J3
WG682596 SAI4P 1,2,3-Trichloropropane R2819960 J3
WG682596 SAMP Vinyl acetate R2819960 J6J3
WG682596 SAMP Vinyl chloride R2819960 J3
WG682596 SAMP Xylenes, Total R2819960 J3
WG682596 S~P 4-Bromofluorobenzene R2819960 J2
L657552-02 WG682021 SAMP Benzidine R2818366 J
L657552-03 WG682021 S~P Benzidine R2818366 J
L657552-04 WG682325 S~P Benzidine R2818791 J
L657552-05 WG682021 SAMP Benzidine R2818366 J
L657552-06 WG682021 SAMP Benzidine R2818366 J
L657552-07 WG682353 SAMP Arsenic R2827162 0
WG682353 SAMP Cadmiwu R2827162 0
WG682353 SAMP Silver R2827162 0
WG682021 SAMP Benzidine R2818366 J
L657552-08 WG682354 SAMP Arsenic R2827882 0
WG682354 SAMP Cadmium R2827882 0
WG682354 SAMP Silver R2827882 0
WG682021 SAMP Benzidine R2818366 J
L657552-09 WG682021 SAMP Benzidine R2818366 J
L657552-10 WG682233 SAMP Mercury R2819043 Pl
WG682399 SAMP Anthracene R2821343 J3
WG682399 SAMP Bis(2-chloroethyl)ether R2821343 J3
WG682399 SAMP Bis(2-chloroisopropyl)ether R2821343 J3
WG682399 SAMP 4-Bromophenyl-phenylether R2821343 J3
WG682399 SAMP 2,6-Dinitrotoluene R2821343 J3
WG682399 SAI4P Fluoranthene R2821343 J3
WG682399 S~P Hexachloro-1,3-butadiene R2821343 J3
Page 41 of 43 •
Attachment A • List of Analytes with QC Qualifiers
Sample work Sample Run
Number Group Type Analyte ID Qualifier
WG682399 SAMP Hexachloroethane R2821343 J3
WG682399 SAMP Isophorone R2821343 J3
WG682399 SAMP Naphthalene R2821343 J3
WG682399 SAMP Nitrobenzene R2821343 J3
WG682399 SAMP n-Nitrosodimethylamine R2821343 J3
WG682399 SAMP n-Nitrosodiphenylamine R2821343 J3
WG682399 SAMP n-Nitrosodi-n-propylamine R2821343 J3
WG682399 SAMP Phenanthrene R2821343 J3
WG682399 SAMP Benzylbutyl phthalate R2821343 J3
WG682399 SAMP Bis(2-ethylhexyl)phthalate R2821343 J3
WG682399 SAMP Di-n-butyl phthalate R2821343 J3
WG682399 SAl~P Pyrene R2821343 J3
WG682399 SAl~P 1,2,4-Trichlorobenzene R2821343 J3
WG682399 SAl~P 4-Chloro-3-methylphenol R2821343 J3
WG682399 SAl~P 2-Chlorophenol R2821343 J3
WG682399 SAl·lP 2,4-Dichlorophenol R2821343 J3
WG682399 SA14P 2,4-Dimethylphenol R2821343 J3
WG682399 SA14P 2-Nitrophenol R2821343 J3
WG682399 SA14P 4-Nitrophenol R2821343 J3
WG682399 SAMP Phenol R2821343 J3
WG682399 SAMP 2,4,6-Trichlorophenol R2821343 J3
WG682399 SAMP 2-Fluorophenol R2821343 J7
WG682399 SAMP Phenol-d5 R2821343 J7
WG682399 SAMP Nitrobenzene-d5 R2821343 J7
WG682399 SAMP 2-Fluorobiphenyl R2821343 J7
WG682399 SAMP 2,4,6-Tribromophenol R2821343 J7
WG682399 SAMP p-Terphenyl-d14 R2821343 J7
WG682373 SAMP Acrylonitrile R2819381 J6J3
WG682373 SAMP Benzene R2819381 J6J3
WG682373 SAMP Bromochloromethane R2819381 J6J3
WG682373 SAMP Bromodichloromethane R2819381 J6J3
WG682373 SAMP Bromoform R2819381 J6J3
WG682373 SAM[' Bromomethane R2819381 J3 • WG682373 SA14P Carbon disulfide R2819381 J6J3
WG682373 SAMP Chlorobenzene R2819381 J6J3
WG682373 SAMP Chlorodibromomethane R2819381 J6J3
WG682373 SAMP Chloroethane R2819381 J6
WG682373 SAMP Chloroform R2819381 J6J3
WG682373 SAMP Dibromomethane R2819381 J6J3
WG682373 SAM[' 1,2-Dichlorobenzene R2819381 J6J3
WG682373 SAM[' 1,4-Dichlorobenzene R28l9381 J6J3
WG682373 SAMP trans-1,4-Dich1oro-2-butene R2819381 J6J3
WG682373 SAMP 1,1-Dichloroethane R2819381 J6J3
WG682373 SJU.I£1 1,2-Dichloroethane R2819381 J6J3
WG682373 SAMP cis-1,2-Dichloroethene R2819381 J6J3
WG682373 SA14P trans-1,2-Dichloroethene R2819381 J6J3
WG682373 SA14P 1,2-Dichloropropane R2819381 J6J3
WG682373 SA14P cis-1,3-Dichloropropene R2819381 J6J3
WG682373 SA14P trans-1,3-Dichloropropene R2819381 J6J3
WG682373 SA14P Ethylbenzene R2819381 J6J3
WG682373 SJU.lP 2-Hexanone R2819381 J6J3
WG682373 SA14P Iodomethane R2819381 J6J3
WG682373 SA14P 2-Butanone (l4EK) R2819381 J3
WG682373 SAMP Methylene Chloride R2819381 J6J3
WG682373 SA14P 4-Methyl-2-pentanone (MIBK) R2819381 J6J3
WG682373 SA14P Styrene R2819381 J6J3
WG682373 SAlol[' 1,1,1,2-Tetrachloroethane R2819381 J6J3
WG682373 SAMP 1,1,2,2-Tetrachloroethane R2819381 J6J3
WG682373 SAMP Tetrachloroethane R2819381 J6J3
WG682373 SAMP Toluene R2819381 J6J3
WG682373 SAMP 1,1,2-Trichloroethane R2819381 J6J3
WG682373 SAMP Trichloroethane R2819381 J6J3
WG682373 SAMP 1,2,3-Trichloropropane R2819381 J6J3
WG682373 SAI~P Vinyl acetate R2819381 J6J3
WG682373 SAMP Xylenes, Total R2819381 J3J6
WG682373 SAMP 4-Bromofluorobenzene R2819381 J2
• Page 42 of 43
•
•
•
Qualifier
J
J2
J3
J6
J7
0
Pl
Attachment B
Explanation of QC Qualifier Codes
Meaning
(EPA) -Estimated value below the lowest calibration point. Confidence
correlates with concentration.
Surrogate recovery limits have been exceeded; values are outside lower control limits
The associated batch QC was outside the established quality control range for precision.
The sample matrix interfered with the ability to make any accurate
determination; spike value is low
Surrogate recovery cannot be used for control limit evaluation due to
dilution.
(ESC) Sample diluted due to matrix interferences that impaired the ability
to make an accurate analytical determination. The detection limit is
elevated in order to reflect the necessary dilution.
RPD value not applicable for sample concentrations less than 5 times the
reporting limit.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy -The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc.
Precision -The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate -Organic compounds that are similar in chemical composition, extraction,
and chromatography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC -Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 43 of 43
• Summary of Remarks For Samples
09/26/13 at 15:18:17
l':rinted
TSR Siqninq Reports: 350
RS -Desired TAT
Always include HG on AP2 metals
Sample: L657552-0l Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-02 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-03 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-04 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-05 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 Rl?T Date: 09/26/13 15:16
Sample: L657552-06 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-07 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-08 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-09 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
Sample: L657552-10 Account: GEOSCIGA Received: 09/14/13 09:00 Due Date: 09/23/13 00:00 RPT Date: 09/26/13 15:16
•
•
--~--~---•
GEC-Macon, GA
iCMp BIGilbe lr.·.'\1\ ~'f ~ .J e ('
IDesc.rit~tion: Onekla MW Site
I'UII!IIl.~.ll
/"';0 5;.~ '1•;+ .'1g,
ltlolt
Rush1. (uti MUST k J~.~atlficdt
-$;lftle 0.,. ·-~-·-·-...lGOIII _N*'Illllar----1~
_ Td J111r "--·-·..50llt -111-.~-·--~-··~
Coii'\PI~ l llUix • I Depth
ss
ss
tlitll:
• -Macon,GA
/('• ..... (, .....
Wi
514 Hillcrest Industrial Blvd.
tMacon, GA 312Q4.3412
Rush? .fbb MUST Be Notified}
_5.JJuo;r, .. DOK
_llleot O.y ............. ~··~···· ... 1<l0l'
_'rwoDII)' -···--···-"·...s:'lili _lb-M~r .. --.. -·-·..l5"
Comp/GAD I M:atrilt •
ss
ss
ss
ss
ss
ss
ss
ss
ss
ss
SS ·Sail GW ·Gll:llll"'liwllltcr WW • 'W;ute'lo'.ltcr DW • Drinkinc W;:tu:c OT-Other ___ _
• •
•
ESC
S•C•t•E•N•C•E·S
NON-CONFORMANCE FORM
Login No.: _..:../.J)..::.S.;;...!7~$!aS":...:'~....:__ __
Date: 2 · I '1 ~ 17::.
Evaluated by: ,;t1 L~..rc-
CIIent: .Gf:Of.(j G 4
Non-Conformance (check applicable Items)
0 Parametcr(s} past holding time
0 Improper t~mperature
o Improper container type
o Improper preseiVatlon
o Container ltd not intact
fft~gin Clarmcat1on Needed
0 Chain of custody is incomplete
0 Chain of Custody is missing (see below)
0 Bmken contalner{s) (See below)
o Broken container: sufficient sample
volume remains for analysis requested (See below)
If no COC: Rmlv~d b)·---.......,--~-
Datet Time:. ___ _
Ttmp:~. Cont. Rec_pff:~­
c t'edexo UPS QSWA t:• Oth~:r __
Trackln3# _____ _
Comments: R ~t' ,· -(.v<(. J
~ s' 13 hlo·l
l.ogitt Instructions:
u Insufficient packing material around container
o lnsuffldent packing matl!rillllnslde coolu
o Improper handllr.g by carrier (fed Ex 1 UPS I Courier
o S;~mple was frozen
, i d · del •. .J-· I f
Client Informed b@ email I fax I voice 111 II
Client contact: _ ~tV.
•
Vapor Results
•
•
GEC
•
•
•
.-ESC
YOUR LI\S OF CHOICE
Todd Peterman GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Re!)ort SUJlllllC\ry
Thursd.:tY September 19, 2013
Report Number: 1657882
Samples Received: 09/17/13
Clie~t Projec~: 130254~240
·: < ... ::. . .
Descri tion: Oneida Mills
12065 Lebanon Rd •
Mt. Juliet, TN 37122
(615} 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call .
Entire Report Reviewed By:
Laboratory Ce1·tilication Numbers
A2LA-1461-01, AIHA-100789, AL-40660, CA-01157CA, CT-PH-0197, FL-E87487, GA-923, IN -C-TN-01, KY-90010, KYUST-0016, NC -ENV375/DW21704/BI0041, NO -R-140. NJ -TN002, NJ NELAP -TN002, SC -84004, TN -2006, VA -460132, NV -233, AZ -0612,
MN -047-999-395i NY -11742, WI -998093910, NV -TN000032011-1, TX -T104704245-1-3, OK -9915, PA -68-02979, IA Lab #364
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
Note: Tho use of the preparatory EPA !{ethod 3511 is not approved or endorsed by the CA ELAP.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 9
•
•
•
.-ESC
YOUR LAO OF CHOICE
Todd Peterman GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received september 17,
Description Oneida Mills
Sample IO BLDG 1
Collected By Todd Peterman
Collection Date 09/11/13 09: 50
Parameter
Volatile Organics
Acetone
Allyl chloride Benzene
Benzyl Chloride
Bromodichloromethane Bromoform
Bromomethane
1,3-Butadiene
carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform Chloromethane
2-Chloroto1uene
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane 1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene 1,2-Dichloroethane
1,1-Dichloroethane 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene 1,4-Dioxane
Ethanol
Ethylbenzene 4-Ethyltoluene
Trichlorofluoromethane Dichlorodifluorornethane
1,1,2-Trichlorotrifluoroethane
1,2-Dichlorotetrafluoroethane
Heptane
Hexachloro-1,3-butadiene n-Hexane
Isopropylbenzene
Methylene Chloride
Methyl Butyl Ketone
ROLl ~ ppbv , RDL2 = ug/m3
Note:
REPORT OF ANALYSIS
2013
Cast 14ol Wght ROLl RDL2
67-64-1 58.1 2.50 5.90
107-05-1 76.53 0.400 1.30 71-43-2 78.1 0.400 1.30
100-44-7 127 0.400 2.10
75-27-4 164 0.400 2.70 75-25-2 253 1.20 12.0
74-83-9 94.9 0.400 1.60
106-99-0 54.1 4.00 8.90
75-15-0 76.1 0.400 1.20
56-23-5 154 0.400 2.50
108-90-7 113 0.400 1.80
75-00-3 64.5 0.400 1.10
67-66-3 119 0.400 1.90 74-87-3 50.5 0.400 0.830
95-49-8 126 0.400 2.10
110-82-7 84.2 0.400 1.40 124-48-1 208 0.400 3.40
106-93-4 188 0.400 3.10
95-50-1 147 0,400 2.40
541-73-1 147 0.400 2.40
106-46-7 147 0.400 2.40 107-06-2 99 0.400 1. 60
75-34-3 98 0.400 1.60
75-35-4 96.9 0.400 1.60
156-59-2 96.9 0.400 1.60
156-60-5 96.9 0.400 1.60
78-87-5 113 0.400 1.80 10061-01-5 111 0.400 1.80
10061-02-6 ill 0.400 1.80
123-91-1 88.1 0.400 1.40
64-17-5 46.1 1.26 2.40
100-41-4 106 0.400 l. 70
622-96-8 120 0.400 2.00
75-69-4 137.4 0.400 2.20
75-11-8 120.92 0.400 2.00 76-13-1 187.4 0.400 3.10
76-14-2 171 0.400 2.80
142-82-5 100 0.400 1.60
87-68-3 261 1.26 13.0 110-54-3 86.2 0.400 1.40 98-82-8 120.2 0.400 2.00
75-09-2 84.9 0.400 1.40 591-78-6 100 2.50 10.0
Units are based on (STP) -Standard Temperature and Pressure
September 19,
ESC Sample t
Site ID
Project t :
ppbv ug/m3
28. 67. < 0.40 < 1. 3 1.9 6.1
< 0.40 < 2.1 < 0.40 < 2.7 < 1.2 < 12. < 0.40 < 1.6 < 4.0 < 8.9 6.5 20.
< 0.40 < 2.5 < 0.40 < 1.8 < 0.40 < 1.1 < 0.40 < 1.9 0.63 1.3 < 0.40 < 2.1
< 0.40 < 1.4
< 0.40 < 3.4
< 0.40 < 3.1
< 0.40 < 2.4
< 0.40 < 2.4
< 0.40 < 2.4
< 0.40 < 1.6
< 0.40 < 1.6
< 0.40 < 1.6
< 0.40 < 1.6
< 0.40 < 1.6
< 0.40 < 1.8 < 0.40 < 1.8
< 0.40 < 1.8 < 0.40 < 1. 4 240 450
1.2 5.2 0.47 2.3
11. 62. 1.0 4.9 < 0.40 < 3.1 < 0.40 < 2.8
1.0 4.1
< 1.3 < 13.
4.2 15. < 0.40 < 2.0
0.64 2.2 < 2.5 < 10.
The reported analytical results relate only to the sample submitted.
12065 Lebanon Rd •
l~t. Juliet, TN 37122
[phone] l-800-167-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1910
2013
L657882-01
GRAHAM, NC
130254.240
Method Date
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
This report shall not be reproduced, except in full, without the written approval from ESC,
Reported: 09/19/13 16:19 Printed: 09/19/13 16:20
Page 2 of 9
Oil.
2
2
2 2
2 2
2
2
2
2
2
2
2 2
2
2
2
2
2
2
2 2
2
2 2
2
2
2
2
2
2
2 2
2 2
2
2
2
2 2
2
2
2
•
•
•
-ESC
YOUR LAB OF CHOICE:
REPORT OF ANALYSIS Todd Peterman
GEC -J;facon, GA 514 Hillcrest Industrial Blvd.
J;facon, GA 31204
Date Received
Description September 17, 2013 Oneida Hills
Sample ID
Collected By Collection Date
BLDG 1
Todd Peterman
09/11/13 09: 50
Parameter
2-Butanone (MEK)
4-Methyl-2-pentanone (1-IIBK)
Methyl methacrylate
MTBE
Naphthalene 2-Propanol
Propene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethylene Tetrahydrofuran
Toluene
1,2,4-Trich1orobenzene
1,1,1-Trich1oroethane
1,1,2-Trichloroethane Trichloroethylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride Vinyl Bromide
Vinyl acetate
m&p-Xylene o-Xylene
1,4-Bromofluorobenzene
ROLl s ppbv , RDL2 = ug/m3
Note:
Caslt
78-93-3
108-10-1
80-62-6
1634-04-4
91-20-3 67-63-0
115-07-1
100-42-5 79-34-5
127-18-4 109-99-9
108-88-3
120-82-1 11-55-6
79-00-5
79-01-6
95-63-6
108-67-8
540-84-1
75-01-4
593-60-2
108-05-4
1330-20-7
95-47-6 460-00-4
Mol Wght ROLl
72.1 2.50
100.1 2.50
100.12 0.400
88.1 0.400
128 1.26 60.1 2.50
42.1 0.800
104 0.400 168 0.400
166 0.400 72.1 0.400
92.1 0.400
181 1.26 133 0.400
133 0.400
131 0.400 120 0.400
120 0.400
114.22 0.400 62.5 0.400
106.95 0.400
86.1 0.400
106 0.800
106 0.400
Units are based on (STP) -Standard Temperature and Pressure
RDL2
7.40
10.0
1.60 1. 40
6.60
6.10 1. 40
1.70 2.70
2.70
1.20
1.50
9.30 2.20
2.20
2.10 2.00
2.00
1.90
1.00
1. 70
1.40
3.50
1. 70
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(6151 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 19, 2013
ESC Sample It
Site ID
Project It :
ppbv uq/m3
< 2.5 < 7.4
< 2.5 < 10.
< 0.40 < 1.6 < 0.40 < 1.4
< 1.3 < 6.6
9.9 24. 4.6 7.9
< 0.40 < 1.7 < 0.40 < 2.7
< 0.40 < 2.7 < 0.40 < 1.2
6.7 25.
< 1.3 < 9.3 < 0.40 < 2.2
< 0.40 < 2.2
< 0.40 < 2.1 1.4 6.9
< 0.40 < 2.0
0.70 3.3 < 0.40 < 1.0
< 0.40 < 1. 7 < 0.40 < 1.4
4.2 18.
1.5 6.5
96 ' Rec.
L657882-01
GRAHAl~, NC
130254.240
Method Date
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/19/13 16:19 Printed: 09/19/13 16:20
Page 3 of 9
Oil.
2
2
2
2
2 2
2
2 2
2 2
2
2
2
2
2 2
2
2
2
2
2
2
2
2
•
•
•
-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS Todd Peterman
GEC -1-lacon, GA
514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
September 17, 2013
oneida Mills
Sample ID
Collected By
Collection Date
Parameter
Volatile Organics
Acetone Allyl chloride
Benzene
Benzyl Chloride
BLDG 2
Todd Peterman
09/11/13 10:10
Bromodichloromethane
Bromoform
Bromomethane
1, 3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane Chloroform
Chloromethane
2-Chlorotoluene Cyclohexane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene 1,4-Dichlorobenzene
1,2-0ichloroethane
1,1-0ichloroethane
1,1-0ichloroethene
cis-1,2-Dichloroethene
trans-1,2-0ichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,4-Dioxane
Ethanol Ethylbenzene
4-Ethyltoluene
Trichlorof1uoromethane
Oichlorodifluoromethane
1,1,2-Trich1orotrifluoroethane
1,2-Dichlorotetrafluoroethane
Heptane Hexachloro-1,3-butadiene
n-Hexane
Isopropylbenzene
Methylene Chloride
t4ethyl Butyl Ketone
ROLl m ppbv , RDL2 .. ug/m3 Note:
Cas I
67-64-1
107-05-1
71-43-2
100-44-7 75-27-4
75-25-2
74-83-9
106-99-0
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8 110-82-7
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
107-06-2
75-34-3 75-35-4
156-59-2
156-60-5 78-87-5
10061-01-5
10061-02-6
123-91-1
64-17-5
100-41-4
622-96-8
75-69-4 75-71-8
76-13-1
76-14-2
142-82-5
87-68-3 110-54-3
98-82-8 75-09-2
591-78-6
l~ol Wght ROLl RDL2
58.1 2.50 5.90
76.53 0.400 1.30 78.1 0.400 1.30
127 0.400 2.10
164 0.400 2.70
253 1.20 12.0
94.9 0.400 1.60
54.1 4.00 8.90
76.1 0.400 1.20
154 0.400 2.50
113 0.400 1.80 64.5 0.400 1.10
119 0.400 1.90 50.5 0.400 0.830
126 0.400 2.10
84.2 0.400 1.40 208 0.400 3.40
188 0.400 3.10 147 0.400 2.40
147 0.400 2.40
147 0.400 2.40
99 0.400 1.60
98 0.400 1.60
96.9 0.400 1.60
96.9 0.400 1.60
96.9 0.400 1.60 113 0.400 1.80 111 0.400 1. 80
111 0.400 1.80
88.1 0.400 1.40 46.1 1.26 2.40
106 0.400 1. 70 120 0.400 2.00
137.4 0.400 2.20 120.92 0.400 2.00
187.4 0.400 3.10
171 0.400 2.80 100 0.400 1.60
261 1.26 13.0 86.2 0.400 1.40
120.2 0.400 2.00 84.9 0.400 1. 40 100 2.50 10.0
Units are based on (STP} -Standard Temperature and Pressure
12065 Lebanon Rd.
14t. Juliet, Ttl 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 19, 2013
ESC Sample lt
Site ID
Project I :
ppbv uq/m3
41. 97. < 0.40 < 1.3 1.7 5.4 < 0.40 < 2.1 < 0.40 < 2.7 < 1.2 < 12. < 0.40 < 1.6 < 4.0 < 8.9 7.8 24. < 0.40 < 2.5 < 0.40 < 1. 8
< 0.40 < 1.1 < 0.40 < 1. 9
0.62 1.3
< 0.40 < 2.1
0.92 3.2 < 0.40 < 3.4 < 0.40 < 3.1 < 0.40 < 2.4 < 0.40 < 2.4 < 0.40 < 2.4 < 0.40 < 1.6
< 0.40 < 1.6 < 0.40 < 1.6
< 0.40 < 1. 6 < o. 40 < 1. 6 < 0.40 < 1.8 < 0.40 < 1.8 < 0.40 < 1.8 < 0.40 < 1. 4
210 400
1.1 4.8
< 0.40 < 2.0
0.41 2.3
1.2 5.9 < 0.40 < 3.1 < 0.40 < 2.8
1.6 6.5 < 1.3 < 13.
4.8 17.
< 0.40 < 2.0 < 0.40 < 1.4 < 2.5 < 10.
L657882-02
GRAHAM, NC
130254.240
Method Date
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/19/13 16:19 Printed: 09/19/13 16:20
Page 4 of 9
Oil.
2
2 2
2
2 2
2
2
2
2
2
2
2
2
2
2 2
2
2
2
2 2
2 2
2
2 2
2
2
2
2
2
2
2 2
2
2
2
2 2
2 2
2
•
•
•
YOUR LAEl OF CHOICE
REPORT OF ANALYSIS
Todd Peterman
GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
September 17, 2013
Oneida ~tills
BLDG 2 Sample ID
Collected By
Collection Date
Todd Peterman
09/11/13 10:10
Parameter
2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK)
Methyl methacrylate MTBE
Naphthalene
2-Propanol Propene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethylene
Tetrahydrofuran
Toluene
1,2,4-Trichloroben~ene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene
1,2,4-Trimethy1benzene 1,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl Bromide
Vinyl acetate
m&p-Xylene
o-Xylene 1,4-Bromofluorobenzene
RDL1 ~ ppbv , RDL2 = uq/m3 Note:
Cast
78-93-3 108-10-1
80-62-6
1634-04-4
91-20-3
67-63-0 115-07-1
100-42-5
79-34-5 127-18-4
109-99-9
108-88-3
120-82-1
11-55-6
79-00-5
79-01-6
95-63-6
108-67-8
540-84-1
75-01-4 593-60-2
108-05-4
1330-20-7
95-47-6
460-00-4
Mol Wght ROLl
72.1 2.50 100.1 2.50
100.12 0.400
88.1 0.400
128 1.26
60.1 2.50 42.1 0.800
104 0.400
168 0.400 166 0.400
72.1 0.400
92.1 0.400
181 1.26
133 0.400 133 0.400
131 0.400
120 0.400 120 0.400
114.22 0.400
62.5 0.400 106.95 0.400
86.1 0.400
106 0.800
106 0.400
Units are based on (STP) -Standard Temperature and Pressure
RDL2
7.40 10.0
1.60
1.40
6.60
6.10 1.40
1. 70
2.70 2.70
1.20
1.50 9.30
2.20
2.20
2.10
2.00
2.00
1.90
1.00
l. 70
1.40
3.50
l. 70
12065 Lebanon Rd.
Ht. Juliet, Tll 31122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 19, 2013
ESC Sample It
Site ID
Project t :
ppbv uq/m3
< 2.5 < 1.4 < 2.5 < 10.
< 0.40 < 1.6
< 0.40 < 1.4 < 1.3 < 6.6
22. 54.
4.1 7.1 < 0.40 < 1.7 < 0.40 < 2.7 < 0.40 < 2.7 < 0.40 < 1.2
6.1 23. < 1.3 < 9.3 < 0.40 < 2.2 < 0.40 < 2.2
< 0.40 < 2.1
1.2 5.9 < 0.40 < 2.0 0.65 3.0 < 0.40 < 1. 0 < 0.40 < 1. 7 < 0.40 < 1.4 3.1 16.
1.3 5.6
94.1 % Rec.
L657882-02
GRAHAI4, NC
130254.240
Method Date
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13 T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
T0-15 09/19/13
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/19/13 16:19 Printed: 09/19/13 16:20
Page 5 of 9
Dil.
2 2
2
2
2
2
2
2
2 2
2
2
2
2 2
2
2
2
2
2
2
2
2
2
2
•
•
•
.-ESC
YOUR LAO OF CHOICE
REPORT OF ANALYSIS
Todd Peterman
GEC -Macon, GA
514 Hillcrest Industrial Blvd. Macon, GA 31204
Date Received
Description
September 17, 2013
Oneida Mills
Sample ID
Collected By
Collection Date
Parameter
Volatile Organics
Acetone
Allyl chloride Benzene
Benzyl Chloride
WHSE fH
Todd Peterman
09/11/13 10:20
Brornodichloromethane Bromoform
Bromomethane
1,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochlorornethane
1,2-Dibromoethane 1,2-Dich1orobenzene
1,3-Dich1orobenzene
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dich1oroethane
1,1-Dichloroethene cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dich1oropropene
trans-1,3-Dichloropropene
1,4-Dioxane
Ethanol Ethy1benzene
4-Ethyltoluene
Trichlorofluoromethane Dichlorodifluoromethane
1,1,2-Trichlorotrifluoroethane
1,2-Dichlorotetrafluoroethane
Heptane
Hexach1oro-1,3-butadiene n-Hexane
Isopropylbenzene
Methylene Chloride
Methyl Butyl Ketone
ROLl = ppbv , RDL2 "" uq/m3 Note:
Cas I
67-64-1
107-05-1
71-43-2
100-44-7
75-27-4 75-25-2
74-83-9
106-99-0 75-15-0
56-23-5
108-90-7
75-00-3
67-66-3 74-87-3
95-49-8
110-82-7 124-49-1
106-93-4
95-50-1
541-73-1
106-46-7
107-06-2
75-34-3
75-35-4 156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
123-91-1
64-17-5
100-41-4
622-96-8
75-69-4 75-71-B
76-13-1
76-14-2
142-92-5
87-68-3
110-54-3
98-92-8
75-09-2 591-78-6
1-!ol Wght ROLl ROL2
58.1 2.50 5.90
76.53 0.400 1.30
79.1 0.400 1.30
127 0.400 2.10
164 0.400 2.70
253 1.20 12.0
94.9 0.400 1.60
54.1 4.00 8.90 76.1 0.400 1.20
154 0.400 2.50
113 0.400 l. 80
64.5 0.400 1.10
119 0.400 1.90 50.5 0.400 0.830
126 0.400 2.10
84.2 0.400 1.40 208 0.400 3.40
198 0.400 3.10
147 0.400 2.40
147 0.400 2.40
147 0.400 2.40
99 0.400 1.60
98 0.400 1.60
96.9 0.400 1.60
96.9 0.400 1.60
96.9 0.400 1.60
113 0.400 1. 80 111 0.400 1.80
111 0.400 1.80 88.1 0.400 1.40
46.1 1.26 2.40
106 0.400 1.70
120 0.400 2.00
137.4 0.400 2.20 120.92 0.400 2.00
187.4 0.400 3.10
171 0.400 2.80
100 0.400 1.60
261 1.26 13.0
86.2 0.400 1. 40
120.2 0.400 2.00
84.9 0.400 1.40 100 2.50 10.0
Units are based on (STI?) -Standard Temperature and Pressure
12065 Lebanon Rd .
l~t. Juliet, TN 37122
[phone]
1-800-767-5859 Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 19, 2013
ESC Sample f. : L657982-03
Site ID GRAHAl~, NC
Project i : 130254.240
ppbv uq/m3 Method Date
45. 110 T0-15 09/19/13
< 0.40 < 1.3 T0-15 09/19/13
2.2 7.0 T0-15 09/19/13
< 0.40 < 2.1 T0-15 09/19/13
< 0.40 < 2.7 T0-15 09/19/13 < 1.2 < 12. T0-15 09/19/13
< 0.40 < 1.6 T0-15 09/19/13 < 4.0 < 9.9 T0-15 09/19/13
8.1 25. T0-15 09/19/13
< 0.40 < 2.5 T0-15 09/19/13
< 0.40 < 1. 8 T0-15 09/19/13
< 0.40 < 1.1 T0-15 09/19/13
< 0.40 < 1. 9 T0-15 09/19/13
1.0 2.1 T0-15 09/19/13
< 0.40 < 2.1 T0-15 09/19/13
0.42 1.4 T0-15 09/19/13
< 0.40 < 3.4 T0-15 09/19/13
< 0.40 < 3.1 T0-15 09/19/13 < 0.40 < 2.4 T0-15 09/19/13
0.48 2.9 T0-15 09/19/13 < 0.40 < 2.4 T0-15 09/19/13
< 0.40 < 1.6 T0-15 09/19/13
< 0.40 < 1.6 T0-15 09/19/13
< 0.40 < 1. 6 T0-15 09/19/13
'( 0.40 < 1.6 T0-15 09/19/13
< 0.40 < 1.6 T0-15 09/19/13 < 0.40 < 1.8 T0-15 09/19/13
< 0.40 < 1.8 T0-15 09/19/13 < 0.40 < 1.8 T0-15 09/19/13
< 0.40 < l. 4 T0-15 09/19/13
290 550 T0-15 09/19/13
1.6 6.9 T0-15 09/19/13
0.69 3.4 T0-15 09/19/13
0.43 2.4 T0-15 09/19/13 1.1 5.4 T0-15 09/19/13
< 0.40 < 3.1 T0-15 09/19/13
< 0.40 < 2.8 T0-15 09/19/13
1.1 4.5 T0-15 09/19/13
< 1.3 < 13. T0-15 09/19/13
3.9 14. T0-15 09/19/13
< 0.40 < 2.0 T0-15 09/19/13
< 0.40 < 1. 4 T0-15 09/19/13 < 2.5 < 10. T0-15 09/19/13
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/19/13 16:19 Printed: 09/19/13 16:20
Paqe 6 of 9
Dil.
2
2 2
2
2 2
2
2
2
2
2
2
2 2
2
2
2
2
2
2
2 2
2
2 2
2 2
2 2
2
2
2
2
2 2
2
2
2
2
2
2
2 2
•
•
•
.-ESC
YOUR LAB OF CHOICE
REPORT OF ANALYSIS
Todd Peterman
GEC -Macon, GA 514 Hillcrest Industrial Blvd.
Macon, GA 31204
Date Received
Description
September 17, 2013
oneida Mills
Sample ID
Collected By
Collection Date
WHSE 11
Todd Peterman
09/11/13 10:20
Parameter
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK) Methyl methacrylate
~IT BE
Naphthalene 2-Propanol
Propene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethylene Tetrahydrofuran
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene 1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene 2,2,4-Trimethylpentane
Vinyl chloride
Vinyl Bromide
Vinyl acetate
m&p-Xylene o-Xylene
1,4-Bromofluorobenzene
ROLl a ppbv , RDL2 ~ uq/m3 Note:
Cas I
78-93-3
108-10-1
80-62-6
1634-04-4
91-20-3 67-63-0
115-07-1
100-42-5
79-34-5
127-18-4
109-99-9
108-88-3
120-82-l
71-55-6
79-00-5
79-01-6 95-63-6
108-67-8
540-84-1
75-01-4
593-60-2 108-05-4
1330-20-7 95-47-6
460-00-4
~lol Wqht ROLl
72.1 2.50
100.1 2.50
100.12 0.400
88.1 0.400
128 1.26
60.1 2.50
42.1 0.800
104 0.400
168 0.400
166 0.400
72.1 0.400
92.1 0.400
181 1.26
133 0.400
133 0.400 131 0.400
120 0.400
120 0.400 114.22 0.400
62.5 0.400
106.95 0.400
86.1 0.400
106 0.800 106 0.400
Units are based on (STP) -Standard Temperature and Pressure
RDL2
7.40
10.0
1.60
1.40
6.60 6.10
l. 40
1.70
2.70
2.70
1.20
1.50
9.30
2.20
2.20
2.10 2.00
2.00
1.90
1.00
1. 70
1.40
3.50 1. 70
12065 Lebanon Rd •
Ht. Juliet, Ttl 37122
(615) 7511-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 19, 2013
ESC Sample I : L657882-03
Site ID GRAHAM, NC
Project I : 130254.240
ppbv uq/m3 Method Date
2.8 8.3 T0-15 09/19/13 < 2.5 < 10. T0-15 09/19/13
< 0.40 < 1.6 T0-15 09/19/13 < 0.40 < 1.4 T0-15 09/19/13
< 1.3 < 6.6 T0-15 09/19/13
12. 29. T0-15 09/19/13
7.8 13. T0-15 09/19/13
< 0.40 < l. 7 T0-15 09/19/13 < 0.40 < 2.7 T0-15 09/19/13 < 0.40 < 2.7 T0-15 09/19/13
< 0.40 < 1.2 T0-15 09/19/13
8.5 32. T0-15 09/19/13 < 1.3 < 9.3 T0-15 09/19/13
< 0.40 < 2.2 T0-15 09/19/13 < 0.40 < 2.2 T0-15 09/19/13
< 0.40 < 2.1 T0-15 09/19/13
1.8 8.8 T0-15 09/19/13
0.45 2.2 T0-15 09/19/13
0.68 3.2 T0-15 09/19/13 < 0.40 < 1. 0 T0-15 09/19/13 < 0.40 < 1. 7 T0-15 09/19/13
< 0.40 < 1. 4 T0-15 09/19/13
5.7 25. T0-15 09/19/13
2.1 9.1 T0-15 09/19/13
96.2 % Rec. T0-15 09/19/13
The reported analytical results relate only to the sample submitted. This report shall not he reproduced, except in full, without the written approval from ESC.
Reported: 09/19/13 16:19 Printed: 09/19/13 16:20
Page 7 of 9
Oil.
2
2
2
2 2
2
2
2
2 2
2
2 2
2
2
2
2
2
2
2 2
2
2 2
2
• Attachment A
List of Analytes with QC Qualifiers
Sample work Sample Run
Number Group Type Analyte ID Qualifier
L657882-01 WG682548 SAMP Ethanol R2820126 E L657882-02 WG682548 SAMP Acetone R2820126 E
WG682548 SAMP Ethanol R2820126 E L657882-03 WG682548 SAM!? Acetone R2820126 E
WG682548 SAMP Ethanol R2820126 E
•
• Page 8 of 9
•
•
•
Qualifier t~eaning
Attachment B
Explanation of QC Qualifier codes
E GTL (EPA) -Greater than upper calibration limit: Actual value is known to be greater than the upper calibration range.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy -The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision -The agreement between a set of samples or between duplicate samples,
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate -Organic compounds that are similar in chemical composition, extraction, and chromatography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC -Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 9 of 9
•
•
•
TSR Signing Reports:
R5 -Desired TAT
350
Summary of Remarks For Samples Printed
09/19/13 at 16:20:23
Always include HG on AP2 metals
Sample: L657882-0l Account: GEOSCIGA Received: 09/17/13 09:00 Due Date:
Sample: L657882-02 Account: GEOSCIGA Received: 09/17/13 09:00 Due Date:
Sa.IIIple: L657882-03 Account: GEOSCIGA Received: 09/17/13 09:00 Due Date:
09/24/13 00:00 RPT Date: 09/19/13 16:19
09/24/13 00:00 RPT Date: 09/19/13 16:19
09/24/13 00:00 RPT Date: 09/19/13 16:19
•
APPENDIX 4
•
•
GEC
•
GSX-Notification of Removal of Underground Storage Tank
•
•
GEC
·~
~· --.... _.
·' GSX
April 5, 1989
Mr. Steve Williams
8025 North Pt. Blvd.
Suite 100
GSX Tank Management, Inc.
7630A South Rail Street
P.O. Box 71188
Chatleston, South CaroHna 29415
(803) ~2693 FAX [phone]
Winston-Salem, North Carolina 27106-3203 .
'
.-RECEIVED
·N.C. Dept NRCO
· APR 10 1qRg
:Wfn::~~"'-~?.fem
_Regional Office
RE: Notification of Removal of Underground storage Tan~ at Kayser Roth Hosiery in Graham, North carolina
Dear Mr. Williams:
Per our telephone conversation of April 5, 1989, this
letter serves as the required thirty (301 day notification that GSX Tank Management, Inc. 'GSX) wil remove one (l) 11,000-gallon underground gasol1ne storage tank at the ·
Kafser Roth Hosiery facility in Graham, North carolina.
Th~s project will be performed in accordance with all
local, state and federal regulations. We anticipate removing this tank beginning the week of May 8, 1989;
however, we will notify you of the exact date prior to
project startup.
If you have any questions concerning this project,
please feel free to contact me at your convenience at
[phone]. Rc;;;.y 1//~1(
Christopher M. Lock
Manager of Regulatory Affairs
adw
c.c.: Robert May, Kayser Roth
•
GSX -Closure Report
•
•
GEC
KAYSER-ROTH HOSIERY INC.
P.O. BOX 77077, GREENSBORO, NC 27417·7077 (919) 852·2030
July 17, 1989
Ms. Emily F. Gloeckler
N.C. Department of Natural Resources
and Community Development
Division of Environmental Management
8025 North Point Blvd.
Suite 100
Winston-Salem, NC 27106-3203
Dear Mr. Gloeckler:
' . • _ _..... _ _.......~a---.:. ... ~••.J.•o-.. --...
:R!CEJVED
!N.C. Dept. NRCO
~ JUL 1 8 1989
·wrnstori-sarom
:Regional Office
The attached "Closur~ Report11 contains assessment results for the removal she of
an 11,000 gallon underground gasoline storage tank at our Graham, North
Carolina, Transportation Iacility. :
Please advise us if further action or information is needed.
Sincerely,
KA YSER-R01H HOSIDRY, INC.
rJ,_,.L._.:j-~. ~ '7-
Robert E. May, Sr. Staff Engineer
Facilities Engmeering
REM/ng
Enclosure
cc: Ron Hodge -Graham Transportation
~lEW YORK OFFICE: 840 FIFTH AVENUE, NEW YORK, HY 10019 (212)60:HOOO
J{AYSER·RQTH HOSIERY. INC.
]'RANSPORTATION QMSION
219 WJ{ARDEN SJREET cRAHAM:NC 27253
CLOSURE KEPORT
mR BEMQYALOFUNQERQROUND
GASjlLINE STORAGE TANK
JULY 17, 1989
-•se-t -Je..--,r.·:~· !'",.,...., -----:&-=--~ • ''" l£111*. ,_REeevED .
N.C. :oept. NACO
JU~ 1 8 1989
Winston·Satem
Regional Office
•
GSX
July 10_, 1989
Mr. Robert May, Sr.
Senior Staff Engineer Kayser-Roth Hosiery, Inc.
Post Office Box 77077 GReensboro, NC 27417-7077
GSX Tank~nr,lnc.
7630 A South RalSlteet
P.O. Bole 71188
CJtsrlttston. Soulll Catoila 29415
[phone] FAX [phone]
RE: Underground Storage Tank Site Closure
Kayser-Roth, Graham, NC
Dear Mr. May:
On May 9, 1989, GSX Tank Management, Inc. removed and disposed of an 11,000 gallon undergro.und gasoline storage
tank at your facility in Graham, North Carolina. once the tank was excavated and removed! 3 soil samples were taken from the bottom of the excavat on at each end and in the
middle. The bottom of the excavation was at a level 12'i below the ground level. The samples were then composited
and transported to General Engineering Laboratories for. analysis. I have attached a copy of the chain of custody form and the analyses for your information. The result~
of the analyses.indicated that the excavation was clean• and the excavation was then backfilled using clean fill !
material. A map is attached showing the location of the tank removal site for submittal to the North Carolina :
Department of Natural Resources. ~
The 11,000 gallon gasoline tank was then transported
to the American TDS companr in Charlotte, NC for disposal.
A certificate of disposal s attached for your records.
GSX Tank Management, Inc. appreciates the op~ortunity to do the work for you and if you have any qu~s~~ons, ; please feel free to contact me at your conven~ence at : [phone]. . .
Respectfully yours,
~~p)y, /l)_ ~
Christopher M. Lock
Facility Manager
adw
GENERAL ENGINEERING LABORATORIES
Environmental Engineering and Analytical Services
Molly F. Greene
President
Gc:oree C. Greene, P.E.,I'h.D.
Vice Pruidcnl
SC RegiSirallon Xo. 9103
-·--·----CERTIFICATE OF ANALYSIS
Cl i en t: GSX TANK l'1ANAGEMENT
P. 0. BOX 71188
CHARLESTON , SC 29415
Con he t r MR. HIKE t-Ic CLLI'IG
cc/fc: GXTWBTEXI
Rtlta.std bY:
Laboratory Certtncatlon•:
FL B87JS6187294
NC 233 sc 10120
VA OOJSI
~ACIP Approved
---------------------------------------~----------------------------~-----------
Pa.rameter
Sample 10
Lab ID
Samp 1t Type
Date Rece i vtd:
Col lechd by :
KAYSER
ROTH
OS/11/89
89050746
15
,lJS/11/89
GXTM
-------------------------------------------------------------------~------------
BENZENE
ETHYLBENZENE
TOLUENE
XYLENE
EVAPORATIVE LOSS ~ 105 C
<10 ppb
<tO ppb
<JO ppb
<10 ppb
35 wt;{
2040 Savage Road • Charll~ston, SC 29414 ·, P. 0. Bo;~; 30712 • Charleston, SC 29417
-----------PhnnrfAO'\l<;'i/..!1!71 • '1:.-\Yt\'n':\"'.C.: .,.,o
"
. --~--
Page_of __
IOICill N-.1 Fli:ihly J'oi.lm$
? l I .,....; J.•. /~0'44 or,._.u ~::~ h(.'(-U.4i-
CollcacdBy ICompuy "
; I
~ I ( ,, c. ·.:....v,
CHAIN OF CUSTODY RECORD
General Engineering Laboralories •
2040 Sa~~ RQQ.d
CbariCSIClll, Soulb carolina 29414
PO BOll30712
Clllii'IC$1011, Soulb Carolina 29417
803-SS6-8171
SAMIUANALYSISREQUlm) ·IISCICIIIIIIIsareatoiiysp:rr~comn:;ormcij53-U~Fiir1'-/itfi&iliOU610~ • .-MIIvr _UL I I I I I I I I I I I l I I I t I L L +-,.fYkwcufdurctJM41..-pru.rud
/'v __, , . -. < . I ,."'), .. ·, \-·-1 .• .'\ • • • ' . , ... ·\~. : .. .g ~ ~ ~ I I ~1 l .! ! l!S ..r .... l . 'S I ... :5 ll'l~:J • li ~ ~ u I ~J i J '~ ~ ~ 1 • t j SAMPLEID DATE TIME il~~~~~'
--.-I
9-;:~) ~o-.L'-
Rellaquisbo4 by:
~;;;r;; ;;{[RaOQiby.
Dale I Time I Ra:ci"fecl.lly lab by. ~._ ~~-) .. , , .. : ,....
While • sample coJlector Yellow • file Pink • withJepon
... -. -. --. -·--I I I
Rdia~by:
Dale.· ·@--il'imc I RiiinarkS ··; . , ,. ~-.,,;,,"I !~h
I
! .
I
:t.c.---
BTcf )( D~.l.
L Jnn~e·-· J RceaYCdby.
\
.,
American TDS Company. Inc.
4600 Park Road -luite 1000
Charlotte, Korth carolina 28209
Phone: [phone]
CERTIFICATE· O·F D I. S P O~S A L
TRANSPORTATION
MIL2ACB
/po
TYPB OF TANK
&d
SIZE
~au
CONTD'l' IH GAL.
~I~ Tc: '
TANK :ID f
otz ::soe9t:ZB
The American TDS company, Ina. certifies that the above mentio~ed tanks
. i have been properly disposed of and the contents ·and sludges pro.cessed in .
full compliance with the Local, State and Federal regulations.
. .......!.------,------
..
lr.loll.loT.Iolll.
........ -·
........ t ·~e 'i:E·· ~~;·-~~;'.':-r d>
Y611NWMILAD'1.. •
llo.loiUol
Figure A-2. General-Site Layout, Graham, North Carolina Facility
'
MYII:It-IIOTM Cllal'l
''···· lila lit_, "®
Figure A-1 b. Site Location, Graham. North Carolina Facility
'