Sidewalk Deve_LSI Reportcomp

Report of Limited Site
Investigation Services
Proposed Sidewalk Development Property
513 and 523 South Pitt Street
Greenville, Pitt County,North Carolina
May 27, 2016
Terracon Project No.
Prepared for:
The East Group, PA
Greenville, North Carolina
Prepared by:
Terracon Consultants, Inc.
Winterville, North Carolina
May 27, 2016
The East Group, PA
324 Evans Street
Greenville, NC 27858
Attention:Ms. Michelle Clements, PE
Senior Civil Engineer
Subject:Report of Limited Site Investigation Services
Proposed Sidewalk Development Property
513 and 523 South Pitt Street
Greenville, Pitt County, North Carolina
Terracon Project No: 72167043
Dear Ms. Clements:
Terracon Consultants, Inc. (Terracon) is pleased to submit our report of Limited Site Investigation
(LSI) services completed at the site referenced above. The report presents data from recent field
activities that included soil borings and the collection of soil and groundwater samples for
chemical analysis. The activities were completed to address a Recognized Environmental
Condition (REC) identified in our Phase I Environmental Site Assessment, Terracon Project
Number 72167027, dated April 15, 2016. Terracon conducted the LSI in general accordance with
our proposal, P72167041 dated April 25, 2016.
Terracon appreciates this opportunity to provide environmental engineering services. Should you
have any questions or require additional information, please do not hesitate to contact our office.
Sincerely,
Terracon Consultants, Inc.
Environmental Services
TABLE OF CONTENTS
ii
2.1 Standard of Care ................................................................................................ 2
2.2 Additional Scope Limitations ............................................................................ 2
2.3 Reliance .............................................................................................................. 3
5.1 Soil Sample Collection ...................................................................................... 4
5.2 Groundwater Sample Collection ....................................................................... 5
6.1 Soil Sample Results ........................................................................................... 6
6.2 Groundwater Sample Results ........................................................................... 7
APPENDIX A EXHIBITS
Exhibit 1 Topographic Vicinity Map
Exhibit 2 Site Diagram
APPENDIX B TABLES
APPENDIX C ANALYTICAL REPORT AND CHAIN OF CUSTODY
Responsive Resourceful Reliable
LIMITED SITE INVESTIGATION
PROPOSED SIDEWALK DEVELOPMENT PROPERTY
513 AND 523 SOUTH PITT STREET
GREENVILLE, PITT COUNTY, NORTH CAROLINA
Terracon Project No. 72167043
1.0 SITE DESCRIPTION
The site is located at 513 and 523 South Pitt Street in Greenville, Pitt County, North Carolina.
Based on information from the Pitt County Online Parcel Information System (OPIS), the site is
comprised of two adjoining parcels that total approximately 2.18 acres with Parcel ID Numbers
16544 and 11307. The subject site is currently developed as an asphalt parking lot with isolated
traffic islands.
Based on information obtained during the Phase I Environmental Site Assessment, several RECs
were observed in connection with the site:
A former filling station with gas tanks observed on Sanborn maps from 1929 to
1958.
A
1958.
A gas tank identified between the steam laundry building and the dry cleaning
building on the 1929 Sanborn map.
A
Sanborn map.
Soil borings were advanced and soil and groundwater samples were obtained in the vicinity of
the former filling station, the former dry cleaning building and the former automotive repair shop.
A Topographic Vicinity Map showing the site location as Exhibit 1 and a Site Diagram showing
the site layout with boring locations as Exhibit 2, is included in the appendix.
2.0 SCOPE OF SERVICES
Project information was obtained from our Phase I ESA performed for the subject site dated April
15, 2016, Terracon Project Number 72167027. The Phase I ESA was performed for The East
Group, PA.
Based on information obtained during the Phase I ESA, four RECs were found in connection with
the site:
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 2
The former filling station with gas tanks observed on Sanborn maps from 1929 to
1958.
T
to 1958.
The gas tank identified between the steam laundry building and the dry cleaning
building on the 1929 Sanborn map.
T
Sanborn map.
Based on the identified RECs, Terracon recommended
Soil and groundwater sampling at the site to evaluate if the site has been impacted
by the above referenced RECs.
The LSI was conducted to determine the presence or absence of indicator contaminants
associated with the RECs identified by the Phase I ESA. The scope of services was not intended
to identify every chemical possibly associated with the site. Similarly, the proposed scope was
not intended to determine the extent or magnitude of any existing contamination.
2.1 Standard of Care
the profession undertaken in similar studies in the same geographical area during the same time.
Terracon makes no warranties, either express or implied, regarding the findings, conclusions, or
recommendations. Please note that Terracon does not warrant the work of laboratories,
regulatory agencies, or other third parties supplying information used in the preparation of the
report. These LSI services were performed in accordance with the scope of work agreed with you,
our client, as reflected in our proposal and were not restricted by or intended to be in conformance
with ASTM E1903-11.
2.2 Additional Scope Limitations
Findings, conclusions, and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, nondetectable, or not present during these services. We cannot
represent that the site contains no hazardous substances, toxic materials, petroleum products, or
other latent conditions beyond those identified during this LSI. Subsurface conditions may vary
from those encountered at specific borings or wells or during other surveys, tests, assessments,
investigations, or exploratory services. The data, interpretations, findings, and our
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 3
recommendations are based solely upon data obtained at the time and within the scope of these
services.
2.3 Reliance
This report has been prepared for the exclusive use of The East Group, PA, and any authorization
for use or reliance by any other party (except a governmental entity having jurisdiction over the
site) is prohibited without the express written authorization of The East Group, PA and Terracon.
Any unauthorized distribution or reuse is at sole risk. Notwithstanding the
foregoing, reliance by authorized parties will be subject to the terms, conditions, and limitations
stated in the proposal,Agreement for Services. The limitation of liability
The East Group,
PA and all relying parties unless otherwise agreed in writing.
3.0 FIELD INVESTIGATION
Terracon conducted the fieldwork under a safety plan developed for this project. Work was
performed using United States Environmental Protection Agency (USEPA) Level D work attire
consisting of hard hats, safety glasses, protective gloves and protective boots. Prior to the start
of the subsurface investigation, Terracon contacted NC One Call and briefly met with
knowledgeable onsite personnel to locate the underground utilities.
As part of the LSI Services, Terracon performed the following tasks:
Mobilized to the site with a GPR subcontractor in order to scan the southern portion
of the site for orphan USTs associated with the former filling station.
Mobilized to the site with a drilling subcontractor to utilize a Geoprobe unit to
advance six borings in select areas onsite. Two borings were advanced in the
vicinity of the former automotive repair shop, two borings were advanced in the
vicinity of the former filling station and two borings were advanced in the vicinity of
the former dry cleaning building.
Advanced the six borings into the groundwater and a temporary well was installed
in each boring.
Screened the soils during the drilling operations using a photo ionization detector
(PID) in order to ascertain possible soil contamination.
Obtained six soil samples (one from each boring) from the soils that were field
screened to have the highest PID readings.
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 4
Obtained six groundwater samples (one from each temporary well) using a
peristaltic pump.
Analyzed the six soil samples and groundwater samples using EPA Method 8260
for volatiles and EPA Method 8270 for semi-volatiles.
Issued this LSI report of our findings.
4.0 GROUND PENETRATING RADAR (GPR) ASSESSMENT
Terracon mobilized to the site on May 6, 2016 in order to meet with our GPR subcontractor and
conduct the proposed GPR assessment. The GPR assessment was conducted in order to assist
in identifying the possible locations of orphan USTs that may still be located onsite and to assist
in the placement of borings.
The GPR subcontractor using a Geophysical Survey Systems, Inc. (GGSI) GPR Unit with a 400
megahertz (MHz) antenna conducted their services in the southern portion of the site in the vicinity
of the former filling station and gas tank observed near the former dry cleaning building. This
GPR device is typically capable of identifying objects at depths between 3 to 6 feet below land
surface.
The GPR subcontractor identified one area in the vicinity of the former filling station that appeared
to be an area of less dense soils, a possible indication of the location of a former UST basin. Soil
boring SB-3 was conducted in this area. Other anomalies or suspect areas were not identified
during the GPR assessment.
5.0 SAMPLE COLLECTION
May 11, 2016 under the supervision of Mr. Blake
Neel, Staff Scientist of Environmental Services with Terracon. Field activities included advancing
six borings using a Geoprobe unit, collecting six soil and groundwater samples from temporary
monitoring wells. These field activities are further discussed below. Please see Exhibit 2 in
Appendix A for our Site Diagram indicating boring locations.
5.1 Soil Sample Collection
Drilling services were performed by a State of North Carolina licensed driller using a track-
mounted Geoprobe unit under the supervision of a Terracon environmental professional. Soil
samples were collected using five-foot core barrel samplers with disposable clear plastic liners.
Drilling equipment was cleaned using a high pressure washer prior to beginning the project,
before beginning each boring, and at the conclusion of work.
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 5
Soil samples were collected continuously and observed to document soil lithology, color, moisture
content and sensory evidence of impairment. Generally, soils consisted of light brown and gray
slightly silty fine to medium sand.
The soil samples were field-screened using a pre-calibrated MiniRAE 2000 PID to indicate the
presence of VOCs. Each soil sample was divided into Ziploc® bags at approximately 2.5 foot
intervals prior to PID analysis.
At the discretion of onsite Terracon personnel along with PID readings recorded, Terracon
collected six soil samples from the following locations and intervals: SB-1 (Soil) was collected
between 15 17.5 vicinity of the former automotive repair shop;
SB-2 (Soil) was collected between 15 17.5 vicinity of the former automotive repair
shop; SB-y of the former filling station;
SB-vicinity of the former filling station; SB-5
vicinity of the former dry cleaning building and
gas tank; SB-6 in the vicinity of the former dry
cleaning building and gas tank.
Groundwater was encountered in each boring around 18 feet below land surface.
Each soil sample was collected using gloved hands. Gloves were changed at each sample
collection point. The soil samples selected for laboratory analysis were placed in laboratory
prepared containers and placed in a cooler with ice.
5.2 Groundwater Sample Collection
Terracon collected six groundwater samples, one from each boring location.
Groundwater samples were collected using a peristaltic pump and disposable tubing from
temporary wells installed by a direct push method using the . The temporary
groundwater monitoring wells were 1-inch diameter wells installed to a depth of approximately 20
feet below land surface. Each temporary well consisted of a ten foot section of 0.010-inch
machine slotted PVC well screen with a ten foot flush joint PVC riser. The temporary wells were
backfilled with pre-sieved silica sand pack from the bottom of the boring to approximately 2 feet
above the top of the well screen.
Prior to groundwater sample collection, each temporary well was purged until the groundwater
was relatively clear of suspended sediment.
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 6
Groundwater samples were then collected using disposable tubing and a peristaltic pump.
Disposable gloves were used and changed at each sample location. Groundwater samples were
placed into laboratory prepared jars, and placed in a cooler with ice.
The sample cooler containing both soil and groundwater samples and a completed chain-of-
custody form was relinquished to Pace Analytical, Inc., an analytical laboratory in Huntersville,
NC for standard turnaround.
Following sample collection, soil borings were properly abandoned using boring cuttings.
Temporary wells were abandoned by removing the well screen and filling the boreholes with a
cement/bentonite slurry from the bottom of the borings to within approximately one foot of ground
surface using a tremmie pipe. The remaining borehole space was filled with sand and topped
with asphalt patch where applicable.
6.0 ANALYTICAL RESULTS
The soil samples and groundwater samples were analyzed for volatiles using EPA Method 8260
and semi-volatiles using EPA Method 8270.
Laboratory results are summarized in Section 6.1 and 6.2 of this report. The executed chain-of-
custody form and laboratory data sheets are provided in Appendix B.
6.1 Soil Sample Results
The following summarizes the results of the soil sampling and analysis:
SB-6, collected in the vicinity of the former dry cleaning building and a former gas
tank was analyzed to contain 1-Methylnaphthalene, p-Isopropyltoluene and
Naphthalene above NCDEQs Soil-to-Water Maximum Contaminant
Concentrations.
Constituents in soil samples SB-1, SB-2, SB-3, SB-4, and SB-5 were analyzed to be non-detect
(ND) and below NCDEQs Soil-to-Water Maximum Contaminant Concentrations.
Please see Table 1 for a comparison of SB-6 soil analytical results to NCDEQ Soil-to-Water
Maximum Contaminant Concentrations.
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 7
6.2 Groundwater Sample Results
The groundwater samples were analyzed for volatile organics using EPA Method 8260 and semi-
volatiles using EPA Method 8270.
The following summarizes the results of the groundwater sampling and analysis:
GW-1 and GW-2, located in the vicinity of the former automotive repair shop was
analyzed to contain cis-1,2-Dichloroethene, Tetrachloroethene (PCE) and
Trichloroethene (TCE) above NCDEQs 2L groundwater standards.
Target contamination constituents in the groundwater samples collected from GW-3, GW-4, GW-
5 and GW-6 -were below the labor
detection limits.
Please see Table 2 for a comparison of groundwater analytical results to NCDEQ
Groundwater Quality Standards.
7.0 INVESTIGATION DERIVED WASTES
Soil cuttings, purge water, and decontamination fluids generated during this assessment were
discarded on the site at or near the point of generation. Disposable sampling materials including
gloves, soil liners, and PVC well screen and casing were collected and discarded in a solid waste
container.
8.0 CONCLUSIONS
Based on the scope of services described in this report and subject to the limitations described
herein, Terracon concludes the following.
During the course of this LSI, Terracon collected six soil samples and six
groundwater samples from the subject site to address RECs identified in our 2016
Phase I ESA report.
Soil Boring, SB-6, collected in the vicinity of the former dry cleaning building and a
former gas tank was analyzed to contain 1-Methylnaphthalene, p-Isopropyltoluene
and Naphthalene above NCDEQs Soil-to-Water Maximum Contaminant
Concentrations.
GW-1 and GW-2, located in the vicinity of the former automotive repair shop was
analyzed to contain cis-1,2-Dichloroethene, Tetrachloroethene (PCE) and
Trichloroethene (TCE) above NCDEQs 2L groundwater standards.
Report of Limited Site Investigation Services
Proposed Sidewalk Development Property Greenville, NC
May 27, 2016 Terracon Project No. 72167043
Responsive Resourceful Reliable 8
9.0 RECOMMENDATIONS
Based on the laboratory analytical results from the soil and groundwater samples collected during
this investigation, Terracon recommends a copy of this report be submitted to the NCDEQ
Brownfields Program for review and potential acceptance into the program.
10.0 GENERAL COMMENTS
The analysis and opinions expressed in this report are based upon data obtained from the borings
and temporary monitoring wells installed at the indicated location and from any other information
discussed in this report. This report does not reflect variations in subsurface chemistry,
stratigraphy or of geohydrology which may occur between borings or across the site. Actual
subsurface conditions may vary and may not become evident without further exploration.
This report is prepared for the exclusive use of our client for specific application to the project
discussed and has been prepared in accordance with generally accepted environmental
engineering practices. No warranties, express or implied, are intended or made. In the event any
changes in the nature or location of observed conditions outlined in this report are found, this
report cannot be considered valid unless these changes are reviewed and the opinions of this
report are modified or verified in writing by Terracon.
If there are any questions regarding this report or if we may be of further assistance, please do
not hesitate to contact us.
APPENDIX A EXHIBITS
Exhibit 1 Topographic Map
Exhibit 2 Site Diagram w/ Boring Locations
APPENDIX B TABLES
APPENDIX B ANALYTICAL REPORT AND CHAIN OF
CUSTODY
#=CL#
May 20, 2016
LIMS USE: FR - BLAKE NEEL
LIMS OBJECT ID: 92297335
92297335
Project:
Pace Project No.:
RE:
Blake Neel
Terracon Consultants
314 Beacon Dr
Winterville, NC 28590
SIDEWALK DEVELOPMENT
Dear Blake Neel:
Enclosed are the analytical results for sample(s) received by the laboratory on May 12, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 99
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 99
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Lab ID Sample ID Matrix Date Collected Date Received
92297335001 GW-1 Water 05/11/16 07:30 05/12/16 09:35
92297335002 GW-2 Water 05/11/16 07:55 05/12/16 09:35
92297335003 GW-3 Water 05/11/16 09:50 05/12/16 09:35
92297335004 GW-4 Water 05/11/16 09:36 05/12/16 09:35
92297335005 GW-5 Water 05/11/16 10:15 05/12/16 09:35
92297335006 GW-6 Water 05/11/16 10:35 05/12/16 09:35
92297335007 SB-1 Solid 05/11/16 11:23 05/12/16 09:35
92297335008 SB-2 Solid 05/11/16 11:29 05/12/16 09:35
92297335009 SB-3 Solid 05/11/16 11:35 05/12/16 09:35
92297335010 SB-4 Solid 05/11/16 11:41 05/12/16 09:35
92297335011 SB-5 Solid 05/11/16 11:47 05/12/16 09:35
92297335012 SB-6 Solid 05/11/16 11:52 05/12/16 09:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 99
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92297335001 GW-1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CNB
92297335002 GW-2 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CNB
92297335003 GW-3 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CNB
92297335004 GW-4 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CNB
92297335005 GW-5 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CNB
92297335006 GW-6 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CNB
92297335007 SB-1 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92297335008 SB-2 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92297335009 SB-3 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92297335010 SB-4 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92297335011 SB-5 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92297335012 SB-6 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-1 Lab ID: 92297335001 Collected: 05/11/16 07:30 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/17/16 02:06 83-32-905/14/16 13:3010.0 1
Acenaphthylene ND ug/L 05/17/16 02:06 208-96-805/14/16 13:3010.0 1
Aniline ND ug/L 05/17/16 02:06 62-53-305/14/16 13:3010.0 1
Anthracene ND ug/L 05/17/16 02:06 120-12-705/14/16 13:3010.0 1
Benzo(a)anthracene ND ug/L 05/17/16 02:06 56-55-305/14/16 13:3010.0 1
Benzo(a)pyrene ND ug/L 05/17/16 02:06 50-32-805/14/16 13:3010.0 1
Benzo(b)fluoranthene ND ug/L 05/17/16 02:06 205-99-205/14/16 13:3010.0 1
Benzo(g,h,i)perylene ND ug/L 05/17/16 02:06 191-24-205/14/16 13:3010.0 1
Benzo(k)fluoranthene ND ug/L 05/17/16 02:06 207-08-905/14/16 13:3010.0 1
Benzoic Acid ND ug/L 05/17/16 02:06 65-85-005/14/16 13:3050.0 1
Benzyl alcohol ND ug/L 05/17/16 02:06 100-51-605/14/16 13:3020.0 1
4-Bromophenylphenyl ether ND ug/L 05/17/16 02:06 101-55-305/14/16 13:3010.0 1
Butylbenzylphthalate ND ug/L 05/17/16 02:06 85-68-705/14/16 13:3010.0 1
4-Chloro-3-methylphenol ND ug/L 05/17/16 02:06 59-50-705/14/16 13:3020.0 1
4-Chloroaniline ND ug/L 05/17/16 02:06 106-47-805/14/16 13:3020.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/17/16 02:06 111-91-105/14/16 13:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/17/16 02:06 111-44-405/14/16 13:3010.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/17/16 02:06 108-60-105/14/16 13:3010.0 1
2-Chloronaphthalene ND ug/L 05/17/16 02:06 91-58-705/14/16 13:3010.0 1
2-Chlorophenol ND ug/L 05/17/16 02:06 95-57-805/14/16 13:3010.0 1
4-Chlorophenylphenyl ether ND ug/L 05/17/16 02:06 7005-72-305/14/16 13:3010.0 1
Chrysene ND ug/L 05/17/16 02:06 218-01-905/14/16 13:3010.0 1
Dibenz(a,h)anthracene ND ug/L 05/17/16 02:06 53-70-305/14/16 13:3010.0 1
Dibenzofuran ND ug/L 05/17/16 02:06 132-64-905/14/16 13:3010.0 1
1,2-Dichlorobenzene ND ug/L 05/17/16 02:06 95-50-105/14/16 13:3010.0 1
1,3-Dichlorobenzene ND ug/L 05/17/16 02:06 541-73-105/14/16 13:3010.0 1
1,4-Dichlorobenzene ND ug/L 05/17/16 02:06 106-46-705/14/16 13:3010.0 1
3,3'-Dichlorobenzidine ND ug/L 05/17/16 02:06 91-94-105/14/16 13:3020.0 1
2,4-Dichlorophenol ND ug/L 05/17/16 02:06 120-83-205/14/16 13:3010.0 1
Diethylphthalate ND ug/L 05/17/16 02:06 84-66-205/14/16 13:3010.0 1
2,4-Dimethylphenol ND ug/L 05/17/16 02:06 105-67-905/14/16 13:3010.0 1
Dimethylphthalate ND ug/L 05/17/16 02:06 131-11-305/14/16 13:3010.0 1
Di-n-butylphthalate ND ug/L 05/17/16 02:06 84-74-205/14/16 13:3010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/17/16 02:06 534-52-105/14/16 13:3020.0 1
2,4-Dinitrophenol ND ug/L 05/17/16 02:06 51-28-505/14/16 13:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/17/16 02:06 121-14-205/14/16 13:3010.0 1
2,6-Dinitrotoluene ND ug/L 05/17/16 02:06 606-20-205/14/16 13:3010.0 1
Di-n-octylphthalate ND ug/L 05/17/16 02:06 117-84-005/14/16 13:3010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/17/16 02:06 117-81-705/14/16 13:306.0 1
Fluoranthene ND ug/L 05/17/16 02:06 206-44-005/14/16 13:3010.0 1
Fluorene ND ug/L 05/17/16 02:06 86-73-705/14/16 13:3010.0 1
Hexachloro-1,3-butadiene ND ug/L 05/17/16 02:06 87-68-305/14/16 13:3010.0 1
Hexachlorobenzene ND ug/L 05/17/16 02:06 118-74-105/14/16 13:3010.0 1
Hexachlorocyclopentadiene ND ug/L 05/17/16 02:06 77-47-405/14/16 13:3010.0 1
Hexachloroethane ND ug/L 05/17/16 02:06 67-72-105/14/16 13:3010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/17/16 02:06 193-39-505/14/16 13:3010.0 1
Isophorone ND ug/L 05/17/16 02:06 78-59-105/14/16 13:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-1 Lab ID: 92297335001 Collected: 05/11/16 07:30 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 05/17/16 02:06 90-12-005/14/16 13:3010.0 1
2-Methylnaphthalene ND ug/L 05/17/16 02:06 91-57-605/14/16 13:3010.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/17/16 02:06 95-48-705/14/16 13:3010.0 1
3&4-Methylphenol(m&p Cresol)13.4 ug/L 05/17/16 02:0605/14/16 13:3010.0 1
Naphthalene ND ug/L 05/17/16 02:06 91-20-305/14/16 13:3010.0 1
2-Nitroaniline ND ug/L 05/17/16 02:06 88-74-405/14/16 13:3050.0 1
3-Nitroaniline ND ug/L 05/17/16 02:06 99-09-205/14/16 13:3050.0 1
4-Nitroaniline ND ug/L 05/17/16 02:06 100-01-605/14/16 13:3020.0 1
Nitrobenzene ND ug/L 05/17/16 02:06 98-95-305/14/16 13:3010.0 1
2-Nitrophenol ND ug/L 05/17/16 02:06 88-75-505/14/16 13:3010.0 1
4-Nitrophenol ND ug/L 05/17/16 02:06 100-02-705/14/16 13:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/17/16 02:06 62-75-905/14/16 13:3010.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/17/16 02:06 621-64-705/14/16 13:3010.0 1
N-Nitrosodiphenylamine ND ug/L 05/17/16 02:06 86-30-605/14/16 13:3010.0 1
Pentachlorophenol ND ug/L 05/17/16 02:06 87-86-505/14/16 13:3025.0 1
Phenanthrene ND ug/L 05/17/16 02:06 85-01-805/14/16 13:3010.0 1
Phenol ND ug/L 05/17/16 02:0605/14/16 13:3010.0 1
Pyrene ND ug/L 05/17/16 02:06 129-00-005/14/16 13:3010.0 1
1,2,4-Trichlorobenzene ND ug/L 05/17/16 02:06 120-82-105/14/16 13:3010.0 1
2,4,5-Trichlorophenol ND ug/L 05/17/16 02:06 95-95-405/14/16 13:3010.0 1
2,4,6-Trichlorophenol ND ug/L 05/17/16 02:06 88-06-205/14/16 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)35 %05/17/16 02:06 4165-60-005/14/16 13:3021-110 1
2-Fluorobiphenyl (S)35 %05/17/16 02:06 321-60-805/14/16 13:3027-110 1
Terphenyl-d14 (S)39 %05/17/16 02:06 1718-51-005/14/16 13:3031-107 1
Phenol-d6 (S)24 %05/17/16 02:06 13127-88-305/14/16 13:3010-110 1
2-Fluorophenol (S)27 %05/17/16 02:06 367-12-405/14/16 13:3012-110 1
2,4,6-Tribromophenol (S)41 %05/17/16 02:06 118-79-605/14/16 13:3027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/16/16 11:13 67-64-125.0 1
Benzene ND ug/L 05/16/16 11:13 71-43-21.0 1
Bromobenzene ND ug/L 05/16/16 11:13 108-86-11.0 1
Bromochloromethane ND ug/L 05/16/16 11:13 74-97-51.0 1
Bromodichloromethane ND ug/L 05/16/16 11:13 75-27-41.0 1
Bromoform ND ug/L 05/16/16 11:13 75-25-21.0 1
Bromomethane ND ug/L 05/16/16 11:13 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/16/16 11:13 78-93-35.0 1
Carbon tetrachloride ND ug/L 05/16/16 11:13 56-23-51.0 1
Chlorobenzene ND ug/L 05/16/16 11:13 108-90-71.0 1
Chloroethane ND ug/L 05/16/16 11:13 75-00-31.0 1
Chloroform ND ug/L 05/16/16 11:13 67-66-31.0 1
Chloromethane ND ug/L 05/16/16 11:13 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/16/16 11:13 95-49-81.0 1
4-Chlorotoluene ND ug/L 05/16/16 11:13 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/16/16 11:13 96-12-82.0 1
Dibromochloromethane ND ug/L 05/16/16 11:13 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-1 Lab ID: 92297335001 Collected: 05/11/16 07:30 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 05/16/16 11:13 106-93-41.0 1
Dibromomethane ND ug/L 05/16/16 11:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/16/16 11:13 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/16/16 11:13 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/16/16 11:13 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 05/16/16 11:13 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/16/16 11:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/16/16 11:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/16/16 11:13 75-35-41.0 1
cis-1,2-Dichloroethene 86.9 ug/L 05/16/16 11:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/16/16 11:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/16/16 11:13 78-87-51.0 1
1,3-Dichloropropane ND ug/L 05/16/16 11:13 142-28-91.0 1
2,2-Dichloropropane ND ug/L 05/16/16 11:13 594-20-71.0 1
1,1-Dichloropropene ND ug/L 05/16/16 11:13 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 05/16/16 11:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/16/16 11:13 10061-02-61.0 1
Diisopropyl ether ND ug/L 05/16/16 11:13 108-20-31.0 1
Ethylbenzene ND ug/L 05/16/16 11:13 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 05/16/16 11:13 87-68-31.0 1
2-Hexanone ND ug/L 05/16/16 11:13 591-78-65.0 1
p-Isopropyltoluene ND ug/L 05/16/16 11:13 99-87-61.0 1
Methylene Chloride ND ug/L 05/16/16 11:13 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/16/16 11:13 108-10-15.0 1
Methyl-tert-butyl ether 1.4 ug/L 05/16/16 11:13 1634-04-41.0 1
Naphthalene ND ug/L 05/16/16 11:13 91-20-31.0 1
Styrene ND ug/L 05/16/16 11:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/16/16 11:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/16/16 11:13 79-34-51.0 1
Tetrachloroethene 9.6 ug/L 05/16/16 11:13 127-18-41.0 1
Toluene ND ug/L 05/16/16 11:13 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 05/16/16 11:13 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 05/16/16 11:13 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 05/16/16 11:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/16/16 11:13 79-00-51.0 1
Trichloroethene 18.9 ug/L 05/16/16 11:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/16/16 11:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/16/16 11:13 96-18-41.0 1
Vinyl acetate ND ug/L 05/16/16 11:13 108-05-42.0 1
Vinyl chloride ND ug/L 05/16/16 11:13 75-01-41.0 1
Xylene (Total)ND ug/L 05/16/16 11:13 1330-20-72.0 1
m&p-Xylene ND ug/L 05/16/16 11:13 179601-23-12.0 1
o-Xylene ND ug/L 05/16/16 11:13 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %05/16/16 11:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/16/16 11:13 17060-07-070-130 1
Toluene-d8 (S)99 %05/16/16 11:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-2 Lab ID: 92297335002 Collected: 05/11/16 07:55 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/17/16 02:36 83-32-905/14/16 13:3010.0 1
Acenaphthylene ND ug/L 05/17/16 02:36 208-96-805/14/16 13:3010.0 1
Aniline ND ug/L 05/17/16 02:36 62-53-305/14/16 13:3010.0 1
Anthracene ND ug/L 05/17/16 02:36 120-12-705/14/16 13:3010.0 1
Benzo(a)anthracene ND ug/L 05/17/16 02:36 56-55-305/14/16 13:3010.0 1
Benzo(a)pyrene ND ug/L 05/17/16 02:36 50-32-805/14/16 13:3010.0 1
Benzo(b)fluoranthene ND ug/L 05/17/16 02:36 205-99-205/14/16 13:3010.0 1
Benzo(g,h,i)perylene ND ug/L 05/17/16 02:36 191-24-205/14/16 13:3010.0 1
Benzo(k)fluoranthene ND ug/L 05/17/16 02:36 207-08-905/14/16 13:3010.0 1
Benzoic Acid ND ug/L 05/17/16 02:36 65-85-005/14/16 13:3050.0 1
Benzyl alcohol ND ug/L 05/17/16 02:36 100-51-605/14/16 13:3020.0 1
4-Bromophenylphenyl ether ND ug/L 05/17/16 02:36 101-55-305/14/16 13:3010.0 1
Butylbenzylphthalate ND ug/L 05/17/16 02:36 85-68-705/14/16 13:3010.0 1
4-Chloro-3-methylphenol ND ug/L 05/17/16 02:36 59-50-705/14/16 13:3020.0 1
4-Chloroaniline ND ug/L 05/17/16 02:36 106-47-805/14/16 13:3020.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/17/16 02:36 111-91-105/14/16 13:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/17/16 02:36 111-44-405/14/16 13:3010.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/17/16 02:36 108-60-105/14/16 13:3010.0 1
2-Chloronaphthalene ND ug/L 05/17/16 02:36 91-58-705/14/16 13:3010.0 1
2-Chlorophenol ND ug/L 05/17/16 02:36 95-57-805/14/16 13:3010.0 1
4-Chlorophenylphenyl ether ND ug/L 05/17/16 02:36 7005-72-305/14/16 13:3010.0 1
Chrysene ND ug/L 05/17/16 02:36 218-01-905/14/16 13:3010.0 1
Dibenz(a,h)anthracene ND ug/L 05/17/16 02:36 53-70-305/14/16 13:3010.0 1
Dibenzofuran ND ug/L 05/17/16 02:36 132-64-905/14/16 13:3010.0 1
1,2-Dichlorobenzene ND ug/L 05/17/16 02:36 95-50-105/14/16 13:3010.0 1
1,3-Dichlorobenzene ND ug/L 05/17/16 02:36 541-73-105/14/16 13:3010.0 1
1,4-Dichlorobenzene ND ug/L 05/17/16 02:36 106-46-705/14/16 13:3010.0 1
3,3'-Dichlorobenzidine ND ug/L 05/17/16 02:36 91-94-105/14/16 13:3020.0 1
2,4-Dichlorophenol ND ug/L 05/17/16 02:36 120-83-205/14/16 13:3010.0 1
Diethylphthalate ND ug/L 05/17/16 02:36 84-66-205/14/16 13:3010.0 1
2,4-Dimethylphenol ND ug/L 05/17/16 02:36 105-67-905/14/16 13:3010.0 1
Dimethylphthalate ND ug/L 05/17/16 02:36 131-11-305/14/16 13:3010.0 1
Di-n-butylphthalate ND ug/L 05/17/16 02:36 84-74-205/14/16 13:3010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/17/16 02:36 534-52-105/14/16 13:3020.0 1
2,4-Dinitrophenol ND ug/L 05/17/16 02:36 51-28-505/14/16 13:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/17/16 02:36 121-14-205/14/16 13:3010.0 1
2,6-Dinitrotoluene ND ug/L 05/17/16 02:36 606-20-205/14/16 13:3010.0 1
Di-n-octylphthalate ND ug/L 05/17/16 02:36 117-84-005/14/16 13:3010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/17/16 02:36 117-81-705/14/16 13:306.0 1
Fluoranthene ND ug/L 05/17/16 02:36 206-44-005/14/16 13:3010.0 1
Fluorene ND ug/L 05/17/16 02:36 86-73-705/14/16 13:3010.0 1
Hexachloro-1,3-butadiene ND ug/L 05/17/16 02:36 87-68-305/14/16 13:3010.0 1
Hexachlorobenzene ND ug/L 05/17/16 02:36 118-74-105/14/16 13:3010.0 1
Hexachlorocyclopentadiene ND ug/L 05/17/16 02:36 77-47-405/14/16 13:3010.0 1
Hexachloroethane ND ug/L 05/17/16 02:36 67-72-105/14/16 13:3010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/17/16 02:36 193-39-505/14/16 13:3010.0 1
Isophorone ND ug/L 05/17/16 02:36 78-59-105/14/16 13:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-2 Lab ID: 92297335002 Collected: 05/11/16 07:55 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 05/17/16 02:36 90-12-005/14/16 13:3010.0 1
2-Methylnaphthalene ND ug/L 05/17/16 02:36 91-57-605/14/16 13:3010.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/17/16 02:36 95-48-705/14/16 13:3010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/17/16 02:3605/14/16 13:3010.0 1
Naphthalene ND ug/L 05/17/16 02:36 91-20-305/14/16 13:3010.0 1
2-Nitroaniline ND ug/L 05/17/16 02:36 88-74-405/14/16 13:3050.0 1
3-Nitroaniline ND ug/L 05/17/16 02:36 99-09-205/14/16 13:3050.0 1
4-Nitroaniline ND ug/L 05/17/16 02:36 100-01-605/14/16 13:3020.0 1
Nitrobenzene ND ug/L 05/17/16 02:36 98-95-305/14/16 13:3010.0 1
2-Nitrophenol ND ug/L 05/17/16 02:36 88-75-505/14/16 13:3010.0 1
4-Nitrophenol ND ug/L 05/17/16 02:36 100-02-705/14/16 13:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/17/16 02:36 62-75-905/14/16 13:3010.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/17/16 02:36 621-64-705/14/16 13:3010.0 1
N-Nitrosodiphenylamine ND ug/L 05/17/16 02:36 86-30-605/14/16 13:3010.0 1
Pentachlorophenol ND ug/L 05/17/16 02:36 87-86-505/14/16 13:3025.0 1
Phenanthrene ND ug/L 05/17/16 02:36 85-01-805/14/16 13:3010.0 1
Phenol ND ug/L 05/17/16 02:3605/14/16 13:3010.0 1
Pyrene ND ug/L 05/17/16 02:36 129-00-005/14/16 13:3010.0 1
1,2,4-Trichlorobenzene ND ug/L 05/17/16 02:36 120-82-105/14/16 13:3010.0 1
2,4,5-Trichlorophenol ND ug/L 05/17/16 02:36 95-95-405/14/16 13:3010.0 1
2,4,6-Trichlorophenol ND ug/L 05/17/16 02:36 88-06-205/14/16 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)79 %05/17/16 02:36 4165-60-005/14/16 13:3021-110 1
2-Fluorobiphenyl (S)72 %05/17/16 02:36 321-60-805/14/16 13:3027-110 1
Terphenyl-d14 (S)82 %05/17/16 02:36 1718-51-005/14/16 13:3031-107 1
Phenol-d6 (S)22 %05/17/16 02:36 13127-88-305/14/16 13:3010-110 1
2-Fluorophenol (S)35 %05/17/16 02:36 367-12-405/14/16 13:3012-110 1
2,4,6-Tribromophenol (S)73 %05/17/16 02:36 118-79-605/14/16 13:3027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/16/16 11:30 67-64-125.0 1
Benzene ND ug/L 05/16/16 11:30 71-43-21.0 1
Bromobenzene ND ug/L 05/16/16 11:30 108-86-11.0 1
Bromochloromethane ND ug/L 05/16/16 11:30 74-97-51.0 1
Bromodichloromethane ND ug/L 05/16/16 11:30 75-27-41.0 1
Bromoform ND ug/L 05/16/16 11:30 75-25-21.0 1
Bromomethane ND ug/L 05/16/16 11:30 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/16/16 11:30 78-93-35.0 1
Carbon tetrachloride ND ug/L 05/16/16 11:30 56-23-51.0 1
Chlorobenzene ND ug/L 05/16/16 11:30 108-90-71.0 1
Chloroethane ND ug/L 05/16/16 11:30 75-00-31.0 1
Chloroform ND ug/L 05/16/16 11:30 67-66-31.0 1
Chloromethane ND ug/L 05/16/16 11:30 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/16/16 11:30 95-49-81.0 1
4-Chlorotoluene ND ug/L 05/16/16 11:30 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/16/16 11:30 96-12-82.0 1
Dibromochloromethane ND ug/L 05/16/16 11:30 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-2 Lab ID: 92297335002 Collected: 05/11/16 07:55 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 05/16/16 11:30 106-93-41.0 1
Dibromomethane ND ug/L 05/16/16 11:30 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/16/16 11:30 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/16/16 11:30 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/16/16 11:30 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 05/16/16 11:30 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/16/16 11:30 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/16/16 11:30 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/16/16 11:30 75-35-41.0 1
cis-1,2-Dichloroethene 120 ug/L 05/16/16 11:30 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/16/16 11:30 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/16/16 11:30 78-87-51.0 1
1,3-Dichloropropane ND ug/L 05/16/16 11:30 142-28-91.0 1
2,2-Dichloropropane ND ug/L 05/16/16 11:30 594-20-71.0 1
1,1-Dichloropropene ND ug/L 05/16/16 11:30 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 05/16/16 11:30 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/16/16 11:30 10061-02-61.0 1
Diisopropyl ether ND ug/L 05/16/16 11:30 108-20-31.0 1
Ethylbenzene ND ug/L 05/16/16 11:30 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 05/16/16 11:30 87-68-31.0 1
2-Hexanone ND ug/L 05/16/16 11:30 591-78-65.0 1
p-Isopropyltoluene ND ug/L 05/16/16 11:30 99-87-61.0 1
Methylene Chloride ND ug/L 05/16/16 11:30 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/16/16 11:30 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 05/16/16 11:30 1634-04-41.0 1
Naphthalene ND ug/L 05/16/16 11:30 91-20-31.0 1
Styrene ND ug/L 05/16/16 11:30 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/16/16 11:30 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/16/16 11:30 79-34-51.0 1
Tetrachloroethene 15.8 ug/L 05/16/16 11:30 127-18-41.0 1
Toluene ND ug/L 05/16/16 11:30 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 05/16/16 11:30 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 05/16/16 11:30 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 05/16/16 11:30 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/16/16 11:30 79-00-51.0 1
Trichloroethene 23.8 ug/L 05/16/16 11:30 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/16/16 11:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/16/16 11:30 96-18-41.0 1
Vinyl acetate ND ug/L 05/16/16 11:30 108-05-42.0 1
Vinyl chloride ND ug/L 05/16/16 11:30 75-01-41.0 1
Xylene (Total)ND ug/L 05/16/16 11:30 1330-20-72.0 1
m&p-Xylene ND ug/L 05/16/16 11:30 179601-23-12.0 1
o-Xylene ND ug/L 05/16/16 11:30 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/16/16 11:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %05/16/16 11:30 17060-07-070-130 1
Toluene-d8 (S)100 %05/16/16 11:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-3 Lab ID: 92297335003 Collected: 05/11/16 09:50 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/18/16 10:31 83-32-905/14/16 13:3010.0 1
Acenaphthylene ND ug/L 05/18/16 10:31 208-96-805/14/16 13:3010.0 1
Aniline ND ug/L 05/18/16 10:31 62-53-305/14/16 13:3010.0 1
Anthracene ND ug/L 05/18/16 10:31 120-12-705/14/16 13:3010.0 1
Benzo(a)anthracene ND ug/L 05/18/16 10:31 56-55-305/14/16 13:3010.0 1
Benzo(a)pyrene ND ug/L 05/18/16 10:31 50-32-805/14/16 13:3010.0 1
Benzo(b)fluoranthene ND ug/L 05/18/16 10:31 205-99-205/14/16 13:3010.0 1
Benzo(g,h,i)perylene ND ug/L 05/18/16 10:31 191-24-205/14/16 13:3010.0 1
Benzo(k)fluoranthene ND ug/L 05/18/16 10:31 207-08-905/14/16 13:3010.0 1
Benzoic Acid ND ug/L 05/18/16 10:31 65-85-005/14/16 13:3050.0 1
Benzyl alcohol ND ug/L 05/18/16 10:31 100-51-605/14/16 13:3020.0 1
4-Bromophenylphenyl ether ND ug/L 05/18/16 10:31 101-55-305/14/16 13:3010.0 1
Butylbenzylphthalate ND ug/L 05/18/16 10:31 85-68-705/14/16 13:3010.0 1
4-Chloro-3-methylphenol ND ug/L 05/18/16 10:31 59-50-705/14/16 13:3020.0 1
4-Chloroaniline ND ug/L 05/18/16 10:31 106-47-805/14/16 13:3020.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/18/16 10:31 111-91-105/14/16 13:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/18/16 10:31 111-44-405/14/16 13:3010.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/18/16 10:31 108-60-105/14/16 13:3010.0 1
2-Chloronaphthalene ND ug/L 05/18/16 10:31 91-58-705/14/16 13:3010.0 1
2-Chlorophenol ND ug/L 05/18/16 10:31 95-57-805/14/16 13:3010.0 1
4-Chlorophenylphenyl ether ND ug/L 05/18/16 10:31 7005-72-305/14/16 13:3010.0 1
Chrysene ND ug/L 05/18/16 10:31 218-01-905/14/16 13:3010.0 1
Dibenz(a,h)anthracene ND ug/L 05/18/16 10:31 53-70-305/14/16 13:3010.0 1
Dibenzofuran ND ug/L 05/18/16 10:31 132-64-905/14/16 13:3010.0 1
1,2-Dichlorobenzene ND ug/L 05/18/16 10:31 95-50-105/14/16 13:3010.0 1
1,3-Dichlorobenzene ND ug/L 05/18/16 10:31 541-73-105/14/16 13:3010.0 1
1,4-Dichlorobenzene ND ug/L 05/18/16 10:31 106-46-705/14/16 13:3010.0 1
3,3'-Dichlorobenzidine ND ug/L 05/18/16 10:31 91-94-105/14/16 13:3020.0 1
2,4-Dichlorophenol ND ug/L 05/18/16 10:31 120-83-205/14/16 13:3010.0 1
Diethylphthalate ND ug/L 05/18/16 10:31 84-66-205/14/16 13:3010.0 1
2,4-Dimethylphenol ND ug/L 05/18/16 10:31 105-67-905/14/16 13:3010.0 1
Dimethylphthalate ND ug/L 05/18/16 10:31 131-11-305/14/16 13:3010.0 1
Di-n-butylphthalate ND ug/L 05/18/16 10:31 84-74-205/14/16 13:3010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/18/16 10:31 534-52-105/14/16 13:3020.0 1
2,4-Dinitrophenol ND ug/L 05/18/16 10:31 51-28-505/14/16 13:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/18/16 10:31 121-14-205/14/16 13:3010.0 1
2,6-Dinitrotoluene ND ug/L 05/18/16 10:31 606-20-205/14/16 13:3010.0 1
Di-n-octylphthalate ND ug/L 05/18/16 10:31 117-84-005/14/16 13:3010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/18/16 10:31 117-81-705/14/16 13:306.0 1
Fluoranthene ND ug/L 05/18/16 10:31 206-44-005/14/16 13:3010.0 1
Fluorene ND ug/L 05/18/16 10:31 86-73-705/14/16 13:3010.0 1
Hexachloro-1,3-butadiene ND ug/L 05/18/16 10:31 87-68-305/14/16 13:3010.0 1
Hexachlorobenzene ND ug/L 05/18/16 10:31 118-74-105/14/16 13:3010.0 1
Hexachlorocyclopentadiene ND ug/L 05/18/16 10:31 77-47-405/14/16 13:3010.0 1
Hexachloroethane ND ug/L 05/18/16 10:31 67-72-105/14/16 13:3010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/18/16 10:31 193-39-505/14/16 13:3010.0 1
Isophorone ND ug/L 05/18/16 10:31 78-59-105/14/16 13:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-3 Lab ID: 92297335003 Collected: 05/11/16 09:50 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 05/18/16 10:31 90-12-005/14/16 13:3010.0 1
2-Methylnaphthalene ND ug/L 05/18/16 10:31 91-57-605/14/16 13:3010.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/18/16 10:31 95-48-705/14/16 13:3010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/18/16 10:3105/14/16 13:3010.0 1
Naphthalene ND ug/L 05/18/16 10:31 91-20-305/14/16 13:3010.0 1
2-Nitroaniline ND ug/L 05/18/16 10:31 88-74-405/14/16 13:3050.0 1
3-Nitroaniline ND ug/L 05/18/16 10:31 99-09-205/14/16 13:3050.0 1
4-Nitroaniline ND ug/L 05/18/16 10:31 100-01-605/14/16 13:3020.0 1
Nitrobenzene ND ug/L 05/18/16 10:31 98-95-305/14/16 13:3010.0 1
2-Nitrophenol ND ug/L 05/18/16 10:31 88-75-505/14/16 13:3010.0 1
4-Nitrophenol ND ug/L 05/18/16 10:31 100-02-705/14/16 13:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/18/16 10:31 62-75-905/14/16 13:3010.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/18/16 10:31 621-64-705/14/16 13:3010.0 1
N-Nitrosodiphenylamine ND ug/L 05/18/16 10:31 86-30-605/14/16 13:3010.0 1
Pentachlorophenol ND ug/L 05/18/16 10:31 87-86-505/14/16 13:3025.0 1
Phenanthrene ND ug/L 05/18/16 10:31 85-01-805/14/16 13:3010.0 1
Phenol ND ug/L 05/18/16 10:3105/14/16 13:3010.0 1
Pyrene ND ug/L 05/18/16 10:31 129-00-005/14/16 13:3010.0 1
1,2,4-Trichlorobenzene ND ug/L 05/18/16 10:31 120-82-105/14/16 13:3010.0 1
2,4,5-Trichlorophenol ND ug/L 05/18/16 10:31 95-95-405/14/16 13:3010.0 1
2,4,6-Trichlorophenol ND ug/L 05/18/16 10:31 88-06-205/14/16 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)77 %05/18/16 10:31 4165-60-005/14/16 13:3021-110 1
2-Fluorobiphenyl (S)77 %05/18/16 10:31 321-60-805/14/16 13:3027-110 1
Terphenyl-d14 (S)88 %05/18/16 10:31 1718-51-005/14/16 13:3031-107 1
Phenol-d6 (S)23 %05/18/16 10:31 13127-88-305/14/16 13:3010-110 1
2-Fluorophenol (S)36 %05/18/16 10:31 367-12-405/14/16 13:3012-110 1
2,4,6-Tribromophenol (S)74 %05/18/16 10:31 118-79-605/14/16 13:3027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/16/16 10:05 67-64-125.0 1
Benzene ND ug/L 05/16/16 10:05 71-43-21.0 1
Bromobenzene ND ug/L 05/16/16 10:05 108-86-11.0 1
Bromochloromethane ND ug/L 05/16/16 10:05 74-97-51.0 1
Bromodichloromethane ND ug/L 05/16/16 10:05 75-27-41.0 1
Bromoform ND ug/L 05/16/16 10:05 75-25-21.0 1
Bromomethane ND ug/L 05/16/16 10:05 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/16/16 10:05 78-93-35.0 1
Carbon tetrachloride ND ug/L 05/16/16 10:05 56-23-51.0 1
Chlorobenzene ND ug/L 05/16/16 10:05 108-90-71.0 1
Chloroethane ND ug/L 05/16/16 10:05 75-00-31.0 1
Chloroform ND ug/L 05/16/16 10:05 67-66-31.0 1
Chloromethane ND ug/L 05/16/16 10:05 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/16/16 10:05 95-49-81.0 1
4-Chlorotoluene ND ug/L 05/16/16 10:05 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/16/16 10:05 96-12-82.0 1
Dibromochloromethane ND ug/L 05/16/16 10:05 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-3 Lab ID: 92297335003 Collected: 05/11/16 09:50 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 05/16/16 10:05 106-93-41.0 1
Dibromomethane ND ug/L 05/16/16 10:05 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/16/16 10:05 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/16/16 10:05 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/16/16 10:05 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 05/16/16 10:05 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/16/16 10:05 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/16/16 10:05 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/16/16 10:05 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/16/16 10:05 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/16/16 10:05 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/16/16 10:05 78-87-51.0 1
1,3-Dichloropropane ND ug/L 05/16/16 10:05 142-28-91.0 1
2,2-Dichloropropane ND ug/L 05/16/16 10:05 594-20-71.0 1
1,1-Dichloropropene ND ug/L 05/16/16 10:05 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 05/16/16 10:05 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/16/16 10:05 10061-02-61.0 1
Diisopropyl ether ND ug/L 05/16/16 10:05 108-20-31.0 1
Ethylbenzene ND ug/L 05/16/16 10:05 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 05/16/16 10:05 87-68-31.0 1
2-Hexanone ND ug/L 05/16/16 10:05 591-78-65.0 1
p-Isopropyltoluene ND ug/L 05/16/16 10:05 99-87-61.0 1
Methylene Chloride ND ug/L 05/16/16 10:05 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/16/16 10:05 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 05/16/16 10:05 1634-04-41.0 1
Naphthalene ND ug/L 05/16/16 10:05 91-20-31.0 1
Styrene ND ug/L 05/16/16 10:05 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/16/16 10:05 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/16/16 10:05 79-34-51.0 1
Tetrachloroethene ND ug/L 05/16/16 10:05 127-18-41.0 1
Toluene ND ug/L 05/16/16 10:05 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 05/16/16 10:05 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 05/16/16 10:05 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 05/16/16 10:05 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/16/16 10:05 79-00-51.0 1
Trichloroethene ND ug/L 05/16/16 10:05 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/16/16 10:05 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/16/16 10:05 96-18-41.0 1
Vinyl acetate ND ug/L 05/16/16 10:05 108-05-42.0 1
Vinyl chloride ND ug/L 05/16/16 10:05 75-01-41.0 1
Xylene (Total)ND ug/L 05/16/16 10:05 1330-20-72.0 1
m&p-Xylene ND ug/L 05/16/16 10:05 179601-23-12.0 1
o-Xylene ND ug/L 05/16/16 10:05 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/16/16 10:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %05/16/16 10:05 17060-07-070-130 1
Toluene-d8 (S)100 %05/16/16 10:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-4 Lab ID: 92297335004 Collected: 05/11/16 09:36 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/17/16 17:11 83-32-905/14/16 13:3010.0 1
Acenaphthylene ND ug/L 05/17/16 17:11 208-96-805/14/16 13:3010.0 1
Aniline ND ug/L 05/17/16 17:11 62-53-305/14/16 13:3010.0 1
Anthracene ND ug/L 05/17/16 17:11 120-12-705/14/16 13:3010.0 1
Benzo(a)anthracene ND ug/L 05/17/16 17:11 56-55-305/14/16 13:3010.0 1
Benzo(a)pyrene ND ug/L 05/17/16 17:11 50-32-805/14/16 13:3010.0 1
Benzo(b)fluoranthene ND ug/L 05/17/16 17:11 205-99-205/14/16 13:3010.0 1
Benzo(g,h,i)perylene ND ug/L 05/17/16 17:11 191-24-205/14/16 13:3010.0 1
Benzo(k)fluoranthene ND ug/L 05/17/16 17:11 207-08-905/14/16 13:3010.0 1
Benzoic Acid ND ug/L 05/17/16 17:11 65-85-005/14/16 13:3050.0 1
Benzyl alcohol ND ug/L 05/17/16 17:11 100-51-605/14/16 13:3020.0 1
4-Bromophenylphenyl ether ND ug/L 05/17/16 17:11 101-55-305/14/16 13:3010.0 1
Butylbenzylphthalate ND ug/L 05/17/16 17:11 85-68-705/14/16 13:3010.0 1
4-Chloro-3-methylphenol ND ug/L 05/17/16 17:11 59-50-705/14/16 13:3020.0 1
4-Chloroaniline ND ug/L 05/17/16 17:11 106-47-805/14/16 13:3020.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/17/16 17:11 111-91-105/14/16 13:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/17/16 17:11 111-44-405/14/16 13:3010.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/17/16 17:11 108-60-105/14/16 13:3010.0 1
2-Chloronaphthalene ND ug/L 05/17/16 17:11 91-58-705/14/16 13:3010.0 1
2-Chlorophenol ND ug/L 05/17/16 17:11 95-57-805/14/16 13:3010.0 1
4-Chlorophenylphenyl ether ND ug/L 05/17/16 17:11 7005-72-305/14/16 13:3010.0 1
Chrysene ND ug/L 05/17/16 17:11 218-01-905/14/16 13:3010.0 1
Dibenz(a,h)anthracene ND ug/L 05/17/16 17:11 53-70-305/14/16 13:3010.0 1
Dibenzofuran ND ug/L 05/17/16 17:11 132-64-905/14/16 13:3010.0 1
1,2-Dichlorobenzene ND ug/L 05/17/16 17:11 95-50-105/14/16 13:3010.0 1
1,3-Dichlorobenzene ND ug/L 05/17/16 17:11 541-73-105/14/16 13:3010.0 1
1,4-Dichlorobenzene ND ug/L 05/17/16 17:11 106-46-705/14/16 13:3010.0 1
3,3'-Dichlorobenzidine ND ug/L 05/17/16 17:11 91-94-105/14/16 13:3020.0 1
2,4-Dichlorophenol ND ug/L 05/17/16 17:11 120-83-205/14/16 13:3010.0 1
Diethylphthalate ND ug/L 05/17/16 17:11 84-66-205/14/16 13:3010.0 1
2,4-Dimethylphenol ND ug/L 05/17/16 17:11 105-67-905/14/16 13:3010.0 1
Dimethylphthalate ND ug/L 05/17/16 17:11 131-11-305/14/16 13:3010.0 1
Di-n-butylphthalate ND ug/L 05/17/16 17:11 84-74-205/14/16 13:3010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/17/16 17:11 534-52-105/14/16 13:3020.0 1
2,4-Dinitrophenol ND ug/L 05/17/16 17:11 51-28-505/14/16 13:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/17/16 17:11 121-14-205/14/16 13:3010.0 1
2,6-Dinitrotoluene ND ug/L 05/17/16 17:11 606-20-205/14/16 13:3010.0 1
Di-n-octylphthalate ND ug/L 05/17/16 17:11 117-84-005/14/16 13:3010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/17/16 17:11 117-81-705/14/16 13:306.0 1
Fluoranthene ND ug/L 05/17/16 17:11 206-44-005/14/16 13:3010.0 1
Fluorene ND ug/L 05/17/16 17:11 86-73-705/14/16 13:3010.0 1
Hexachloro-1,3-butadiene ND ug/L 05/17/16 17:11 87-68-305/14/16 13:3010.0 1
Hexachlorobenzene ND ug/L 05/17/16 17:11 118-74-105/14/16 13:3010.0 1
Hexachlorocyclopentadiene ND ug/L 05/17/16 17:11 77-47-405/14/16 13:3010.0 1
Hexachloroethane ND ug/L 05/17/16 17:11 67-72-105/14/16 13:3010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/17/16 17:11 193-39-505/14/16 13:3010.0 1
Isophorone ND ug/L 05/17/16 17:11 78-59-105/14/16 13:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-4 Lab ID: 92297335004 Collected: 05/11/16 09:36 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 05/17/16 17:11 90-12-005/14/16 13:3010.0 1
2-Methylnaphthalene ND ug/L 05/17/16 17:11 91-57-605/14/16 13:3010.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/17/16 17:11 95-48-705/14/16 13:3010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/17/16 17:1105/14/16 13:3010.0 1
Naphthalene ND ug/L 05/17/16 17:11 91-20-305/14/16 13:3010.0 1
2-Nitroaniline ND ug/L 05/17/16 17:11 88-74-405/14/16 13:3050.0 1
3-Nitroaniline ND ug/L 05/17/16 17:11 99-09-205/14/16 13:3050.0 1
4-Nitroaniline ND ug/L 05/17/16 17:11 100-01-605/14/16 13:3020.0 1
Nitrobenzene ND ug/L 05/17/16 17:11 98-95-305/14/16 13:3010.0 1
2-Nitrophenol ND ug/L 05/17/16 17:11 88-75-505/14/16 13:3010.0 1
4-Nitrophenol ND ug/L 05/17/16 17:11 100-02-705/14/16 13:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/17/16 17:11 62-75-905/14/16 13:3010.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/17/16 17:11 621-64-705/14/16 13:3010.0 1
N-Nitrosodiphenylamine ND ug/L 05/17/16 17:11 86-30-605/14/16 13:3010.0 1
Pentachlorophenol ND ug/L 05/17/16 17:11 87-86-505/14/16 13:3025.0 1
Phenanthrene ND ug/L 05/17/16 17:11 85-01-805/14/16 13:3010.0 1
Phenol ND ug/L 05/17/16 17:1105/14/16 13:3010.0 1
Pyrene ND ug/L 05/17/16 17:11 129-00-005/14/16 13:3010.0 1
1,2,4-Trichlorobenzene ND ug/L 05/17/16 17:11 120-82-105/14/16 13:3010.0 1
2,4,5-Trichlorophenol ND ug/L 05/17/16 17:11 95-95-405/14/16 13:3010.0 1
2,4,6-Trichlorophenol ND ug/L 05/17/16 17:11 88-06-205/14/16 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)82 %05/17/16 17:11 4165-60-005/14/16 13:3021-110 1
2-Fluorobiphenyl (S)79 %05/17/16 17:11 321-60-805/14/16 13:3027-110 1
Terphenyl-d14 (S)85 %05/17/16 17:11 1718-51-005/14/16 13:3031-107 1
Phenol-d6 (S)26 %05/17/16 17:11 13127-88-305/14/16 13:3010-110 1
2-Fluorophenol (S)40 %05/17/16 17:11 367-12-405/14/16 13:3012-110 1
2,4,6-Tribromophenol (S)74 %05/17/16 17:11 118-79-605/14/16 13:3027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/16/16 10:22 67-64-125.0 1
Benzene ND ug/L 05/16/16 10:22 71-43-21.0 1
Bromobenzene ND ug/L 05/16/16 10:22 108-86-11.0 1
Bromochloromethane ND ug/L 05/16/16 10:22 74-97-51.0 1
Bromodichloromethane ND ug/L 05/16/16 10:22 75-27-41.0 1
Bromoform ND ug/L 05/16/16 10:22 75-25-21.0 1
Bromomethane ND ug/L 05/16/16 10:22 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/16/16 10:22 78-93-35.0 1
Carbon tetrachloride ND ug/L 05/16/16 10:22 56-23-51.0 1
Chlorobenzene ND ug/L 05/16/16 10:22 108-90-71.0 1
Chloroethane ND ug/L 05/16/16 10:22 75-00-31.0 1
Chloroform ND ug/L 05/16/16 10:22 67-66-31.0 1
Chloromethane ND ug/L 05/16/16 10:22 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/16/16 10:22 95-49-81.0 1
4-Chlorotoluene ND ug/L 05/16/16 10:22 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/16/16 10:22 96-12-82.0 1
Dibromochloromethane ND ug/L 05/16/16 10:22 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-4 Lab ID: 92297335004 Collected: 05/11/16 09:36 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 05/16/16 10:22 106-93-41.0 1
Dibromomethane ND ug/L 05/16/16 10:22 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/16/16 10:22 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/16/16 10:22 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/16/16 10:22 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 05/16/16 10:22 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/16/16 10:22 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/16/16 10:22 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/16/16 10:22 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/16/16 10:22 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/16/16 10:22 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/16/16 10:22 78-87-51.0 1
1,3-Dichloropropane ND ug/L 05/16/16 10:22 142-28-91.0 1
2,2-Dichloropropane ND ug/L 05/16/16 10:22 594-20-71.0 1
1,1-Dichloropropene ND ug/L 05/16/16 10:22 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 05/16/16 10:22 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/16/16 10:22 10061-02-61.0 1
Diisopropyl ether ND ug/L 05/16/16 10:22 108-20-31.0 1
Ethylbenzene ND ug/L 05/16/16 10:22 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 05/16/16 10:22 87-68-31.0 1
2-Hexanone ND ug/L 05/16/16 10:22 591-78-65.0 1
p-Isopropyltoluene ND ug/L 05/16/16 10:22 99-87-61.0 1
Methylene Chloride ND ug/L 05/16/16 10:22 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/16/16 10:22 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 05/16/16 10:22 1634-04-41.0 1
Naphthalene ND ug/L 05/16/16 10:22 91-20-31.0 1
Styrene ND ug/L 05/16/16 10:22 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/16/16 10:22 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/16/16 10:22 79-34-51.0 1
Tetrachloroethene ND ug/L 05/16/16 10:22 127-18-41.0 1
Toluene ND ug/L 05/16/16 10:22 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 05/16/16 10:22 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 05/16/16 10:22 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 05/16/16 10:22 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/16/16 10:22 79-00-51.0 1
Trichloroethene ND ug/L 05/16/16 10:22 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/16/16 10:22 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/16/16 10:22 96-18-41.0 1
Vinyl acetate ND ug/L 05/16/16 10:22 108-05-42.0 1
Vinyl chloride ND ug/L 05/16/16 10:22 75-01-41.0 1
Xylene (Total)ND ug/L 05/16/16 10:22 1330-20-72.0 1
m&p-Xylene ND ug/L 05/16/16 10:22 179601-23-12.0 1
o-Xylene ND ug/L 05/16/16 10:22 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/16/16 10:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %05/16/16 10:22 17060-07-070-130 1
Toluene-d8 (S)100 %05/16/16 10:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-5 Lab ID: 92297335005 Collected: 05/11/16 10:15 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/18/16 13:02 83-32-905/16/16 12:1410.0 1
Acenaphthylene ND ug/L 05/18/16 13:02 208-96-805/16/16 12:1410.0 1
Aniline ND ug/L 05/18/16 13:02 62-53-305/16/16 12:1410.0 1
Anthracene ND ug/L 05/18/16 13:02 120-12-705/16/16 12:1410.0 1
Benzo(a)anthracene ND ug/L 05/18/16 13:02 56-55-305/16/16 12:1410.0 1
Benzo(a)pyrene ND ug/L 05/18/16 13:02 50-32-805/16/16 12:1410.0 1
Benzo(b)fluoranthene ND ug/L 05/18/16 13:02 205-99-205/16/16 12:1410.0 1
Benzo(g,h,i)perylene ND ug/L 05/18/16 13:02 191-24-205/16/16 12:1410.0 1
Benzo(k)fluoranthene ND ug/L 05/18/16 13:02 207-08-905/16/16 12:1410.0 1
Benzoic Acid ND ug/L 05/18/16 13:02 65-85-0 L205/16/16 12:1450.0 1
Benzyl alcohol ND ug/L 05/18/16 13:02 100-51-605/16/16 12:1420.0 1
4-Bromophenylphenyl ether ND ug/L 05/18/16 13:02 101-55-305/16/16 12:1410.0 1
Butylbenzylphthalate ND ug/L 05/18/16 13:02 85-68-705/16/16 12:1410.0 1
4-Chloro-3-methylphenol ND ug/L 05/18/16 13:02 59-50-705/16/16 12:1420.0 1
4-Chloroaniline ND ug/L 05/18/16 13:02 106-47-805/16/16 12:1420.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/18/16 13:02 111-91-105/16/16 12:1410.0 1
bis(2-Chloroethyl) ether ND ug/L 05/18/16 13:02 111-44-405/16/16 12:1410.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/18/16 13:02 108-60-105/16/16 12:1410.0 1
2-Chloronaphthalene ND ug/L 05/18/16 13:02 91-58-705/16/16 12:1410.0 1
2-Chlorophenol ND ug/L 05/18/16 13:02 95-57-805/16/16 12:1410.0 1
4-Chlorophenylphenyl ether ND ug/L 05/18/16 13:02 7005-72-305/16/16 12:1410.0 1
Chrysene ND ug/L 05/18/16 13:02 218-01-905/16/16 12:1410.0 1
Dibenz(a,h)anthracene ND ug/L 05/18/16 13:02 53-70-305/16/16 12:1410.0 1
Dibenzofuran ND ug/L 05/18/16 13:02 132-64-905/16/16 12:1410.0 1
1,2-Dichlorobenzene ND ug/L 05/18/16 13:02 95-50-105/16/16 12:1410.0 1
1,3-Dichlorobenzene ND ug/L 05/18/16 13:02 541-73-105/16/16 12:1410.0 1
1,4-Dichlorobenzene ND ug/L 05/18/16 13:02 106-46-705/16/16 12:1410.0 1
3,3'-Dichlorobenzidine ND ug/L 05/18/16 13:02 91-94-105/16/16 12:1420.0 1
2,4-Dichlorophenol ND ug/L 05/18/16 13:02 120-83-205/16/16 12:1410.0 1
Diethylphthalate ND ug/L 05/18/16 13:02 84-66-205/16/16 12:1410.0 1
2,4-Dimethylphenol ND ug/L 05/18/16 13:02 105-67-905/16/16 12:1410.0 1
Dimethylphthalate ND ug/L 05/18/16 13:02 131-11-305/16/16 12:1410.0 1
Di-n-butylphthalate ND ug/L 05/18/16 13:02 84-74-205/16/16 12:1410.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/18/16 13:02 534-52-105/16/16 12:1420.0 1
2,4-Dinitrophenol ND ug/L 05/18/16 13:02 51-28-505/16/16 12:1450.0 1
2,4-Dinitrotoluene ND ug/L 05/18/16 13:02 121-14-205/16/16 12:1410.0 1
2,6-Dinitrotoluene ND ug/L 05/18/16 13:02 606-20-205/16/16 12:1410.0 1
Di-n-octylphthalate ND ug/L 05/18/16 13:02 117-84-005/16/16 12:1410.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/18/16 13:02 117-81-705/16/16 12:146.0 1
Fluoranthene ND ug/L 05/18/16 13:02 206-44-005/16/16 12:1410.0 1
Fluorene ND ug/L 05/18/16 13:02 86-73-705/16/16 12:1410.0 1
Hexachloro-1,3-butadiene ND ug/L 05/18/16 13:02 87-68-305/16/16 12:1410.0 1
Hexachlorobenzene ND ug/L 05/18/16 13:02 118-74-105/16/16 12:1410.0 1
Hexachlorocyclopentadiene ND ug/L 05/18/16 13:02 77-47-405/16/16 12:1410.0 1
Hexachloroethane ND ug/L 05/18/16 13:02 67-72-105/16/16 12:1410.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/18/16 13:02 193-39-505/16/16 12:1410.0 1
Isophorone ND ug/L 05/18/16 13:02 78-59-105/16/16 12:1410.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-5 Lab ID: 92297335005 Collected: 05/11/16 10:15 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 05/18/16 13:02 90-12-005/16/16 12:1410.0 1
2-Methylnaphthalene ND ug/L 05/18/16 13:02 91-57-605/16/16 12:1410.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/18/16 13:02 95-48-705/16/16 12:1410.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/18/16 13:0205/16/16 12:1410.0 1
Naphthalene ND ug/L 05/18/16 13:02 91-20-305/16/16 12:1410.0 1
2-Nitroaniline ND ug/L 05/18/16 13:02 88-74-405/16/16 12:1450.0 1
3-Nitroaniline ND ug/L 05/18/16 13:02 99-09-205/16/16 12:1450.0 1
4-Nitroaniline ND ug/L 05/18/16 13:02 100-01-605/16/16 12:1420.0 1
Nitrobenzene ND ug/L 05/18/16 13:02 98-95-305/16/16 12:1410.0 1
2-Nitrophenol ND ug/L 05/18/16 13:02 88-75-505/16/16 12:1410.0 1
4-Nitrophenol ND ug/L 05/18/16 13:02 100-02-705/16/16 12:1450.0 1
N-Nitrosodimethylamine ND ug/L 05/18/16 13:02 62-75-905/16/16 12:1410.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/18/16 13:02 621-64-705/16/16 12:1410.0 1
N-Nitrosodiphenylamine ND ug/L 05/18/16 13:02 86-30-605/16/16 12:1410.0 1
Pentachlorophenol ND ug/L 05/18/16 13:02 87-86-505/16/16 12:1425.0 1
Phenanthrene ND ug/L 05/18/16 13:02 85-01-805/16/16 12:1410.0 1
Phenol ND ug/L 05/18/16 13:0205/16/16 12:1410.0 1
Pyrene ND ug/L 05/18/16 13:02 129-00-005/16/16 12:1410.0 1
1,2,4-Trichlorobenzene ND ug/L 05/18/16 13:02 120-82-105/16/16 12:1410.0 1
2,4,5-Trichlorophenol ND ug/L 05/18/16 13:02 95-95-405/16/16 12:1410.0 1
2,4,6-Trichlorophenol ND ug/L 05/18/16 13:02 88-06-205/16/16 12:1410.0 1
Surrogates
Nitrobenzene-d5 (S)79 %05/18/16 13:02 4165-60-005/16/16 12:1421-110 1
2-Fluorobiphenyl (S)78 %05/18/16 13:02 321-60-805/16/16 12:1427-110 1
Terphenyl-d14 (S)82 %05/18/16 13:02 1718-51-005/16/16 12:1431-107 1
Phenol-d6 (S)26 %05/18/16 13:02 13127-88-305/16/16 12:1410-110 1
2-Fluorophenol (S)40 %05/18/16 13:02 367-12-405/16/16 12:1412-110 1
2,4,6-Tribromophenol (S)69 %05/18/16 13:02 118-79-605/16/16 12:1427-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/17/16 01:40 67-64-125.0 1
Benzene ND ug/L 05/17/16 01:40 71-43-21.0 1
Bromobenzene ND ug/L 05/17/16 01:40 108-86-11.0 1
Bromochloromethane ND ug/L 05/17/16 01:40 74-97-51.0 1
Bromodichloromethane ND ug/L 05/17/16 01:40 75-27-41.0 1
Bromoform ND ug/L 05/17/16 01:40 75-25-21.0 1
Bromomethane ND ug/L 05/17/16 01:40 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/17/16 01:40 78-93-35.0 1
Carbon tetrachloride ND ug/L 05/17/16 01:40 56-23-51.0 1
Chlorobenzene ND ug/L 05/17/16 01:40 108-90-71.0 1
Chloroethane ND ug/L 05/17/16 01:40 75-00-31.0 1
Chloroform ND ug/L 05/17/16 01:40 67-66-31.0 1
Chloromethane ND ug/L 05/17/16 01:40 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/17/16 01:40 95-49-81.0 1
4-Chlorotoluene ND ug/L 05/17/16 01:40 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/17/16 01:40 96-12-82.0 1
Dibromochloromethane ND ug/L 05/17/16 01:40 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-5 Lab ID: 92297335005 Collected: 05/11/16 10:15 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 05/17/16 01:40 106-93-41.0 1
Dibromomethane ND ug/L 05/17/16 01:40 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/17/16 01:40 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/17/16 01:40 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/17/16 01:40 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 05/17/16 01:40 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/17/16 01:40 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/17/16 01:40 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/17/16 01:40 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/17/16 01:40 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/17/16 01:40 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/17/16 01:40 78-87-51.0 1
1,3-Dichloropropane ND ug/L 05/17/16 01:40 142-28-91.0 1
2,2-Dichloropropane ND ug/L 05/17/16 01:40 594-20-71.0 1
1,1-Dichloropropene ND ug/L 05/17/16 01:40 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 05/17/16 01:40 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/17/16 01:40 10061-02-61.0 1
Diisopropyl ether ND ug/L 05/17/16 01:40 108-20-31.0 1
Ethylbenzene ND ug/L 05/17/16 01:40 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 05/17/16 01:40 87-68-31.0 1
2-Hexanone ND ug/L 05/17/16 01:40 591-78-65.0 1
p-Isopropyltoluene ND ug/L 05/17/16 01:40 99-87-61.0 1
Methylene Chloride ND ug/L 05/17/16 01:40 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/17/16 01:40 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 05/17/16 01:40 1634-04-41.0 1
Naphthalene ND ug/L 05/17/16 01:40 91-20-31.0 1
Styrene ND ug/L 05/17/16 01:40 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/17/16 01:40 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/17/16 01:40 79-34-51.0 1
Tetrachloroethene ND ug/L 05/17/16 01:40 127-18-41.0 1
Toluene ND ug/L 05/17/16 01:40 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 05/17/16 01:40 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 05/17/16 01:40 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 05/17/16 01:40 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/17/16 01:40 79-00-51.0 1
Trichloroethene ND ug/L 05/17/16 01:40 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/17/16 01:40 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/17/16 01:40 96-18-41.0 1
Vinyl acetate ND ug/L 05/17/16 01:40 108-05-42.0 1
Vinyl chloride ND ug/L 05/17/16 01:40 75-01-41.0 1
Xylene (Total)ND ug/L 05/17/16 01:40 1330-20-72.0 1
m&p-Xylene ND ug/L 05/17/16 01:40 179601-23-12.0 1
o-Xylene ND ug/L 05/17/16 01:40 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/17/16 01:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %05/17/16 01:40 17060-07-070-130 1
Toluene-d8 (S)100 %05/17/16 01:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-6 Lab ID: 92297335006 Collected: 05/11/16 10:35 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/17/16 17:41 83-32-905/14/16 13:3010.0 1
Acenaphthylene ND ug/L 05/17/16 17:41 208-96-805/14/16 13:3010.0 1
Aniline ND ug/L 05/17/16 17:41 62-53-305/14/16 13:3010.0 1
Anthracene ND ug/L 05/17/16 17:41 120-12-705/14/16 13:3010.0 1
Benzo(a)anthracene ND ug/L 05/17/16 17:41 56-55-305/14/16 13:3010.0 1
Benzo(a)pyrene ND ug/L 05/17/16 17:41 50-32-805/14/16 13:3010.0 1
Benzo(b)fluoranthene ND ug/L 05/17/16 17:41 205-99-205/14/16 13:3010.0 1
Benzo(g,h,i)perylene ND ug/L 05/17/16 17:41 191-24-205/14/16 13:3010.0 1
Benzo(k)fluoranthene ND ug/L 05/17/16 17:41 207-08-905/14/16 13:3010.0 1
Benzoic Acid ND ug/L 05/17/16 17:41 65-85-005/14/16 13:3050.0 1
Benzyl alcohol ND ug/L 05/17/16 17:41 100-51-605/14/16 13:3020.0 1
4-Bromophenylphenyl ether ND ug/L 05/17/16 17:41 101-55-305/14/16 13:3010.0 1
Butylbenzylphthalate ND ug/L 05/17/16 17:41 85-68-705/14/16 13:3010.0 1
4-Chloro-3-methylphenol ND ug/L 05/17/16 17:41 59-50-705/14/16 13:3020.0 1
4-Chloroaniline ND ug/L 05/17/16 17:41 106-47-805/14/16 13:3020.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/17/16 17:41 111-91-105/14/16 13:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/17/16 17:41 111-44-405/14/16 13:3010.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/17/16 17:41 108-60-105/14/16 13:3010.0 1
2-Chloronaphthalene ND ug/L 05/17/16 17:41 91-58-705/14/16 13:3010.0 1
2-Chlorophenol ND ug/L 05/17/16 17:41 95-57-805/14/16 13:3010.0 1
4-Chlorophenylphenyl ether ND ug/L 05/17/16 17:41 7005-72-305/14/16 13:3010.0 1
Chrysene ND ug/L 05/17/16 17:41 218-01-905/14/16 13:3010.0 1
Dibenz(a,h)anthracene ND ug/L 05/17/16 17:41 53-70-305/14/16 13:3010.0 1
Dibenzofuran ND ug/L 05/17/16 17:41 132-64-905/14/16 13:3010.0 1
1,2-Dichlorobenzene ND ug/L 05/17/16 17:41 95-50-105/14/16 13:3010.0 1
1,3-Dichlorobenzene ND ug/L 05/17/16 17:41 541-73-105/14/16 13:3010.0 1
1,4-Dichlorobenzene ND ug/L 05/17/16 17:41 106-46-705/14/16 13:3010.0 1
3,3'-Dichlorobenzidine ND ug/L 05/17/16 17:41 91-94-105/14/16 13:3020.0 1
2,4-Dichlorophenol ND ug/L 05/17/16 17:41 120-83-205/14/16 13:3010.0 1
Diethylphthalate ND ug/L 05/17/16 17:41 84-66-205/14/16 13:3010.0 1
2,4-Dimethylphenol ND ug/L 05/17/16 17:41 105-67-905/14/16 13:3010.0 1
Dimethylphthalate ND ug/L 05/17/16 17:41 131-11-305/14/16 13:3010.0 1
Di-n-butylphthalate ND ug/L 05/17/16 17:41 84-74-205/14/16 13:3010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/17/16 17:41 534-52-105/14/16 13:3020.0 1
2,4-Dinitrophenol ND ug/L 05/17/16 17:41 51-28-505/14/16 13:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/17/16 17:41 121-14-205/14/16 13:3010.0 1
2,6-Dinitrotoluene ND ug/L 05/17/16 17:41 606-20-205/14/16 13:3010.0 1
Di-n-octylphthalate ND ug/L 05/17/16 17:41 117-84-005/14/16 13:3010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/17/16 17:41 117-81-705/14/16 13:306.0 1
Fluoranthene ND ug/L 05/17/16 17:41 206-44-005/14/16 13:3010.0 1
Fluorene ND ug/L 05/17/16 17:41 86-73-705/14/16 13:3010.0 1
Hexachloro-1,3-butadiene ND ug/L 05/17/16 17:41 87-68-305/14/16 13:3010.0 1
Hexachlorobenzene ND ug/L 05/17/16 17:41 118-74-105/14/16 13:3010.0 1
Hexachlorocyclopentadiene ND ug/L 05/17/16 17:41 77-47-405/14/16 13:3010.0 1
Hexachloroethane ND ug/L 05/17/16 17:41 67-72-105/14/16 13:3010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/17/16 17:41 193-39-505/14/16 13:3010.0 1
Isophorone ND ug/L 05/17/16 17:41 78-59-105/14/16 13:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-6 Lab ID: 92297335006 Collected: 05/11/16 10:35 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 05/17/16 17:41 90-12-005/14/16 13:3010.0 1
2-Methylnaphthalene ND ug/L 05/17/16 17:41 91-57-605/14/16 13:3010.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/17/16 17:41 95-48-705/14/16 13:3010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/17/16 17:4105/14/16 13:3010.0 1
Naphthalene ND ug/L 05/17/16 17:41 91-20-305/14/16 13:3010.0 1
2-Nitroaniline ND ug/L 05/17/16 17:41 88-74-405/14/16 13:3050.0 1
3-Nitroaniline ND ug/L 05/17/16 17:41 99-09-205/14/16 13:3050.0 1
4-Nitroaniline ND ug/L 05/17/16 17:41 100-01-605/14/16 13:3020.0 1
Nitrobenzene ND ug/L 05/17/16 17:41 98-95-305/14/16 13:3010.0 1
2-Nitrophenol ND ug/L 05/17/16 17:41 88-75-505/14/16 13:3010.0 1
4-Nitrophenol ND ug/L 05/17/16 17:41 100-02-705/14/16 13:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/17/16 17:41 62-75-905/14/16 13:3010.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/17/16 17:41 621-64-705/14/16 13:3010.0 1
N-Nitrosodiphenylamine ND ug/L 05/17/16 17:41 86-30-605/14/16 13:3010.0 1
Pentachlorophenol ND ug/L 05/17/16 17:41 87-86-505/14/16 13:3025.0 1
Phenanthrene ND ug/L 05/17/16 17:41 85-01-805/14/16 13:3010.0 1
Phenol ND ug/L 05/17/16 17:4105/14/16 13:3010.0 1
Pyrene ND ug/L 05/17/16 17:41 129-00-005/14/16 13:3010.0 1
1,2,4-Trichlorobenzene ND ug/L 05/17/16 17:41 120-82-105/14/16 13:3010.0 1
2,4,5-Trichlorophenol ND ug/L 05/17/16 17:41 95-95-405/14/16 13:3010.0 1
2,4,6-Trichlorophenol ND ug/L 05/17/16 17:41 88-06-205/14/16 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)77 %05/17/16 17:41 4165-60-005/14/16 13:3021-110 1
2-Fluorobiphenyl (S)76 %05/17/16 17:41 321-60-805/14/16 13:3027-110 1
Terphenyl-d14 (S)53 %05/17/16 17:41 1718-51-005/14/16 13:3031-107 1
Phenol-d6 (S)25 %05/17/16 17:41 13127-88-305/14/16 13:3010-110 1
2-Fluorophenol (S)38 %05/17/16 17:41 367-12-405/14/16 13:3012-110 1
2,4,6-Tribromophenol (S)71 %05/17/16 17:41 118-79-605/14/16 13:3027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/16/16 12:04 67-64-125.0 1
Benzene ND ug/L 05/16/16 12:04 71-43-21.0 1
Bromobenzene ND ug/L 05/16/16 12:04 108-86-11.0 1
Bromochloromethane ND ug/L 05/16/16 12:04 74-97-51.0 1
Bromodichloromethane ND ug/L 05/16/16 12:04 75-27-41.0 1
Bromoform ND ug/L 05/16/16 12:04 75-25-21.0 1
Bromomethane ND ug/L 05/16/16 12:04 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/16/16 12:04 78-93-35.0 1
Carbon tetrachloride ND ug/L 05/16/16 12:04 56-23-51.0 1
Chlorobenzene ND ug/L 05/16/16 12:04 108-90-71.0 1
Chloroethane ND ug/L 05/16/16 12:04 75-00-31.0 1
Chloroform ND ug/L 05/16/16 12:04 67-66-31.0 1
Chloromethane ND ug/L 05/16/16 12:04 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/16/16 12:04 95-49-81.0 1
4-Chlorotoluene ND ug/L 05/16/16 12:04 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/16/16 12:04 96-12-82.0 1
Dibromochloromethane ND ug/L 05/16/16 12:04 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: GW-6 Lab ID: 92297335006 Collected: 05/11/16 10:35 Received: 05/12/16 09:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 05/16/16 12:04 106-93-41.0 1
Dibromomethane ND ug/L 05/16/16 12:04 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/16/16 12:04 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/16/16 12:04 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/16/16 12:04 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 05/16/16 12:04 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/16/16 12:04 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/16/16 12:04 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/16/16 12:04 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/16/16 12:04 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/16/16 12:04 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/16/16 12:04 78-87-51.0 1
1,3-Dichloropropane ND ug/L 05/16/16 12:04 142-28-91.0 1
2,2-Dichloropropane ND ug/L 05/16/16 12:04 594-20-71.0 1
1,1-Dichloropropene ND ug/L 05/16/16 12:04 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 05/16/16 12:04 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/16/16 12:04 10061-02-61.0 1
Diisopropyl ether ND ug/L 05/16/16 12:04 108-20-31.0 1
Ethylbenzene ND ug/L 05/16/16 12:04 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 05/16/16 12:04 87-68-31.0 1
2-Hexanone ND ug/L 05/16/16 12:04 591-78-65.0 1
p-Isopropyltoluene 8.6 ug/L 05/16/16 12:04 99-87-61.0 1
Methylene Chloride ND ug/L 05/16/16 12:04 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/16/16 12:04 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 05/16/16 12:04 1634-04-41.0 1
Naphthalene 4.7 ug/L 05/16/16 12:04 91-20-31.0 1
Styrene ND ug/L 05/16/16 12:04 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/16/16 12:04 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/16/16 12:04 79-34-51.0 1
Tetrachloroethene ND ug/L 05/16/16 12:04 127-18-41.0 1
Toluene ND ug/L 05/16/16 12:04 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 05/16/16 12:04 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 05/16/16 12:04 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 05/16/16 12:04 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/16/16 12:04 79-00-51.0 1
Trichloroethene ND ug/L 05/16/16 12:04 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/16/16 12:04 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/16/16 12:04 96-18-41.0 1
Vinyl acetate ND ug/L 05/16/16 12:04 108-05-42.0 1
Vinyl chloride ND ug/L 05/16/16 12:04 75-01-41.0 1
Xylene (Total)ND ug/L 05/16/16 12:04 1330-20-72.0 1
m&p-Xylene ND ug/L 05/16/16 12:04 179601-23-12.0 1
o-Xylene ND ug/L 05/16/16 12:04 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/16/16 12:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %05/16/16 12:04 17060-07-070-130 1
Toluene-d8 (S)101 %05/16/16 12:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-1 Lab ID: 92297335007 Collected: 05/11/16 11:23 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/17/16 10:38 83-32-905/13/16 10:133501
Acenaphthylene ND ug/kg 05/17/16 10:38 208-96-805/13/16 10:133501
Aniline ND ug/kg 05/17/16 10:38 62-53-305/13/16 10:133501
Anthracene ND ug/kg 05/17/16 10:38 120-12-705/13/16 10:133501
Benzo(a)anthracene ND ug/kg 05/17/16 10:38 56-55-305/13/16 10:133501
Benzo(a)pyrene ND ug/kg 05/17/16 10:38 50-32-805/13/16 10:133501
Benzo(b)fluoranthene ND ug/kg 05/17/16 10:38 205-99-205/13/16 10:133501
Benzo(g,h,i)perylene ND ug/kg 05/17/16 10:38 191-24-205/13/16 10:133501
Benzo(k)fluoranthene ND ug/kg 05/17/16 10:38 207-08-905/13/16 10:133501
Benzoic Acid ND ug/kg 05/17/16 10:38 65-85-005/13/16 10:1317501
Benzyl alcohol ND ug/kg 05/17/16 10:38 100-51-605/13/16 10:137001
4-Bromophenylphenyl ether ND ug/kg 05/17/16 10:38 101-55-305/13/16 10:133501
Butylbenzylphthalate ND ug/kg 05/17/16 10:38 85-68-705/13/16 10:133501
4-Chloro-3-methylphenol ND ug/kg 05/17/16 10:38 59-50-705/13/16 10:137001
4-Chloroaniline ND ug/kg 05/17/16 10:38 106-47-805/13/16 10:1317501
bis(2-Chloroethoxy)methane ND ug/kg 05/17/16 10:38 111-91-105/13/16 10:133501
bis(2-Chloroethyl) ether ND ug/kg 05/17/16 10:38 111-44-405/13/16 10:133501
bis(2-Chloroisopropyl) ether ND ug/kg 05/17/16 10:38 108-60-105/13/16 10:133501
2-Chloronaphthalene ND ug/kg 05/17/16 10:38 91-58-705/13/16 10:133501
2-Chlorophenol ND ug/kg 05/17/16 10:38 95-57-805/13/16 10:133501
4-Chlorophenylphenyl ether ND ug/kg 05/17/16 10:38 7005-72-305/13/16 10:133501
Chrysene ND ug/kg 05/17/16 10:38 218-01-905/13/16 10:133501
Dibenz(a,h)anthracene ND ug/kg 05/17/16 10:38 53-70-305/13/16 10:133501
Dibenzofuran ND ug/kg 05/17/16 10:38 132-64-905/13/16 10:133501
1,2-Dichlorobenzene ND ug/kg 05/17/16 10:38 95-50-105/13/16 10:133501
1,3-Dichlorobenzene ND ug/kg 05/17/16 10:38 541-73-105/13/16 10:133501
1,4-Dichlorobenzene ND ug/kg 05/17/16 10:38 106-46-705/13/16 10:133501
3,3'-Dichlorobenzidine ND ug/kg 05/17/16 10:38 91-94-105/13/16 10:1317501
2,4-Dichlorophenol ND ug/kg 05/17/16 10:38 120-83-205/13/16 10:133501
Diethylphthalate ND ug/kg 05/17/16 10:38 84-66-205/13/16 10:133501
2,4-Dimethylphenol ND ug/kg 05/17/16 10:38 105-67-905/13/16 10:133501
Dimethylphthalate ND ug/kg 05/17/16 10:38 131-11-305/13/16 10:133501
Di-n-butylphthalate ND ug/kg 05/17/16 10:38 84-74-205/13/16 10:133501
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/16 10:38 534-52-105/13/16 10:137001
2,4-Dinitrophenol ND ug/kg 05/17/16 10:38 51-28-505/13/16 10:1317501
2,4-Dinitrotoluene ND ug/kg 05/17/16 10:38 121-14-205/13/16 10:133501
2,6-Dinitrotoluene ND ug/kg 05/17/16 10:38 606-20-205/13/16 10:133501
Di-n-octylphthalate ND ug/kg 05/17/16 10:38 117-84-005/13/16 10:133501
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/16 10:38 117-81-705/13/16 10:133501
Fluoranthene ND ug/kg 05/17/16 10:38 206-44-005/13/16 10:133501
Fluorene ND ug/kg 05/17/16 10:38 86-73-705/13/16 10:133501
Hexachloro-1,3-butadiene ND ug/kg 05/17/16 10:38 87-68-305/13/16 10:133501
Hexachlorobenzene ND ug/kg 05/17/16 10:38 118-74-105/13/16 10:133501
Hexachlorocyclopentadiene ND ug/kg 05/17/16 10:38 77-47-405/13/16 10:133501
Hexachloroethane ND ug/kg 05/17/16 10:38 67-72-105/13/16 10:133501
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/16 10:38 193-39-505/13/16 10:133501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-1 Lab ID: 92297335007 Collected: 05/11/16 11:23 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 05/17/16 10:38 78-59-105/13/16 10:133501
1-Methylnaphthalene ND ug/kg 05/17/16 10:38 90-12-005/13/16 10:133501
2-Methylnaphthalene ND ug/kg 05/17/16 10:38 91-57-605/13/16 10:133501
2-Methylphenol(o-Cresol)ND ug/kg 05/17/16 10:38 95-48-705/13/16 10:133501
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/17/16 10:3805/13/16 10:133501
Naphthalene ND ug/kg 05/17/16 10:38 91-20-305/13/16 10:133501
2-Nitroaniline ND ug/kg 05/17/16 10:38 88-74-405/13/16 10:1317501
3-Nitroaniline ND ug/kg 05/17/16 10:38 99-09-205/13/16 10:1317501
4-Nitroaniline ND ug/kg 05/17/16 10:38 100-01-605/13/16 10:137001
Nitrobenzene ND ug/kg 05/17/16 10:38 98-95-305/13/16 10:133501
2-Nitrophenol ND ug/kg 05/17/16 10:38 88-75-505/13/16 10:133501
4-Nitrophenol ND ug/kg 05/17/16 10:38 100-02-705/13/16 10:1317501
N-Nitrosodimethylamine ND ug/kg 05/17/16 10:38 62-75-905/13/16 10:133501
N-Nitroso-di-n-propylamine ND ug/kg 05/17/16 10:38 621-64-705/13/16 10:133501
N-Nitrosodiphenylamine ND ug/kg 05/17/16 10:38 86-30-605/13/16 10:133501
Pentachlorophenol ND ug/kg 05/17/16 10:38 87-86-505/13/16 10:1317501
Phenanthrene ND ug/kg 05/17/16 10:38 85-01-805/13/16 10:133501
Phenol ND ug/kg 05/17/16 10:3805/13/16 10:133501
Pyrene ND ug/kg 05/17/16 10:38 129-00-005/13/16 10:133501
1,2,4-Trichlorobenzene ND ug/kg 05/17/16 10:38 120-82-105/13/16 10:133501
2,4,5-Trichlorophenol ND ug/kg 05/17/16 10:38 95-95-405/13/16 10:133501
2,4,6-Trichlorophenol ND ug/kg 05/17/16 10:38 88-06-205/13/16 10:133501
Surrogates
Nitrobenzene-d5 (S)76 %05/17/16 10:38 4165-60-005/13/16 10:1323-110 1
2-Fluorobiphenyl (S)74 %05/17/16 10:38 321-60-805/13/16 10:1330-110 1
Terphenyl-d14 (S)86 %05/17/16 10:38 1718-51-005/13/16 10:1328-110 1
Phenol-d6 (S)72 %05/17/16 10:38 13127-88-305/13/16 10:1322-110 1
2-Fluorophenol (S)69 %05/17/16 10:38 367-12-405/13/16 10:1313-110 1
2,4,6-Tribromophenol (S)93 %05/17/16 10:38 118-79-605/13/16 10:1327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 05/13/16 21:47 67-64-199.5 1
Benzene ND ug/kg 05/13/16 21:47 71-43-25.0 1
Bromobenzene ND ug/kg 05/13/16 21:47 108-86-15.0 1
Bromochloromethane ND ug/kg 05/13/16 21:47 74-97-55.0 1
Bromodichloromethane ND ug/kg 05/13/16 21:47 75-27-45.0 1
Bromoform ND ug/kg 05/13/16 21:47 75-25-25.0 1
Bromomethane ND ug/kg 05/13/16 21:47 74-83-99.9 1
2-Butanone (MEK)ND ug/kg 05/13/16 21:47 78-93-399.5 1
n-Butylbenzene ND ug/kg 05/13/16 21:47 104-51-85.0 1
sec-Butylbenzene ND ug/kg 05/13/16 21:47 135-98-85.0 1
tert-Butylbenzene ND ug/kg 05/13/16 21:47 98-06-65.0 1
Carbon tetrachloride ND ug/kg 05/13/16 21:47 56-23-55.0 1
Chlorobenzene ND ug/kg 05/13/16 21:47 108-90-75.0 1
Chloroethane ND ug/kg 05/13/16 21:47 75-00-3 M19.9 1
Chloroform ND ug/kg 05/13/16 21:47 67-66-35.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-1 Lab ID: 92297335007 Collected: 05/11/16 11:23 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 05/13/16 21:47 74-87-3 M19.9 1
2-Chlorotoluene ND ug/kg 05/13/16 21:47 95-49-85.0 1
4-Chlorotoluene ND ug/kg 05/13/16 21:47 106-43-45.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/13/16 21:47 96-12-85.0 1
Dibromochloromethane ND ug/kg 05/13/16 21:47 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/kg 05/13/16 21:47 106-93-45.0 1
Dibromomethane ND ug/kg 05/13/16 21:47 74-95-35.0 1
1,2-Dichlorobenzene ND ug/kg 05/13/16 21:47 95-50-15.0 1
1,3-Dichlorobenzene ND ug/kg 05/13/16 21:47 541-73-15.0 1
1,4-Dichlorobenzene ND ug/kg 05/13/16 21:47 106-46-75.0 1
Dichlorodifluoromethane ND ug/kg 05/13/16 21:47 75-71-8 M19.9 1
1,1-Dichloroethane ND ug/kg 05/13/16 21:47 75-34-35.0 1
1,2-Dichloroethane ND ug/kg 05/13/16 21:47 107-06-25.0 1
1,1-Dichloroethene ND ug/kg 05/13/16 21:47 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/kg 05/13/16 21:47 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/kg 05/13/16 21:47 156-60-55.0 1
1,2-Dichloropropane ND ug/kg 05/13/16 21:47 78-87-55.0 1
1,3-Dichloropropane ND ug/kg 05/13/16 21:47 142-28-95.0 1
2,2-Dichloropropane ND ug/kg 05/13/16 21:47 594-20-75.0 1
1,1-Dichloropropene ND ug/kg 05/13/16 21:47 563-58-65.0 1
cis-1,3-Dichloropropene ND ug/kg 05/13/16 21:47 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/kg 05/13/16 21:47 10061-02-65.0 1
Diisopropyl ether ND ug/kg 05/13/16 21:47 108-20-35.0 1
Ethylbenzene ND ug/kg 05/13/16 21:47 100-41-45.0 1
Hexachloro-1,3-butadiene ND ug/kg 05/13/16 21:47 87-68-35.0 1
2-Hexanone ND ug/kg 05/13/16 21:47 591-78-649.7 1
Isopropylbenzene (Cumene)ND ug/kg 05/13/16 21:47 98-82-85.0 1
p-Isopropyltoluene ND ug/kg 05/13/16 21:47 99-87-65.0 1
Methylene Chloride ND ug/kg 05/13/16 21:47 75-09-2 M119.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/13/16 21:47 108-10-149.7 1
Methyl-tert-butyl ether ND ug/kg 05/13/16 21:47 1634-04-45.0 1
Naphthalene ND ug/kg 05/13/16 21:47 91-20-35.0 1
n-Propylbenzene ND ug/kg 05/13/16 21:47 103-65-15.0 1
Styrene ND ug/kg 05/13/16 21:47 100-42-55.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/13/16 21:47 630-20-65.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/13/16 21:47 79-34-55.0 1
Tetrachloroethene ND ug/kg 05/13/16 21:47 127-18-45.0 1
Toluene ND ug/kg 05/13/16 21:47 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/kg 05/13/16 21:47 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/kg 05/13/16 21:47 120-82-15.0 1
1,1,1-Trichloroethane ND ug/kg 05/13/16 21:47 71-55-65.0 1
1,1,2-Trichloroethane ND ug/kg 05/13/16 21:47 79-00-55.0 1
Trichloroethene ND ug/kg 05/13/16 21:47 79-01-65.0 1
Trichlorofluoromethane ND ug/kg 05/13/16 21:47 75-69-45.0 1
1,2,3-Trichloropropane ND ug/kg 05/13/16 21:47 96-18-45.0 1
1,2,4-Trimethylbenzene ND ug/kg 05/13/16 21:47 95-63-65.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-1 Lab ID: 92297335007 Collected: 05/11/16 11:23 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 05/13/16 21:47 108-67-85.0 1
Vinyl acetate ND ug/kg 05/13/16 21:47 108-05-449.7 1
Vinyl chloride ND ug/kg 05/13/16 21:47 75-01-4 M19.9 1
Xylene (Total)ND ug/kg 05/13/16 21:47 1330-20-79.9 1
m&p-Xylene ND ug/kg 05/13/16 21:47 179601-23-19.9 1
o-Xylene ND ug/kg 05/13/16 21:47 95-47-65.0 1
Surrogates
Toluene-d8 (S)100 %05/13/16 21:47 2037-26-570-130 1
4-Bromofluorobenzene (S)106 %05/13/16 21:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)77 %05/13/16 21:47 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 5.7 %05/13/16 07:550.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-2 Lab ID: 92297335008 Collected: 05/11/16 11:29 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/17/16 18:10 83-32-905/13/16 10:133501
Acenaphthylene ND ug/kg 05/17/16 18:10 208-96-805/13/16 10:133501
Aniline ND ug/kg 05/17/16 18:10 62-53-305/13/16 10:133501
Anthracene ND ug/kg 05/17/16 18:10 120-12-705/13/16 10:133501
Benzo(a)anthracene ND ug/kg 05/17/16 18:10 56-55-305/13/16 10:133501
Benzo(a)pyrene ND ug/kg 05/17/16 18:10 50-32-805/13/16 10:133501
Benzo(b)fluoranthene ND ug/kg 05/17/16 18:10 205-99-205/13/16 10:133501
Benzo(g,h,i)perylene ND ug/kg 05/17/16 18:10 191-24-205/13/16 10:133501
Benzo(k)fluoranthene ND ug/kg 05/17/16 18:10 207-08-905/13/16 10:133501
Benzoic Acid ND ug/kg 05/17/16 18:10 65-85-005/13/16 10:1317501
Benzyl alcohol ND ug/kg 05/17/16 18:10 100-51-605/13/16 10:137001
4-Bromophenylphenyl ether ND ug/kg 05/17/16 18:10 101-55-305/13/16 10:133501
Butylbenzylphthalate ND ug/kg 05/17/16 18:10 85-68-705/13/16 10:133501
4-Chloro-3-methylphenol ND ug/kg 05/17/16 18:10 59-50-705/13/16 10:137001
4-Chloroaniline ND ug/kg 05/17/16 18:10 106-47-805/13/16 10:1317501
bis(2-Chloroethoxy)methane ND ug/kg 05/17/16 18:10 111-91-105/13/16 10:133501
bis(2-Chloroethyl) ether ND ug/kg 05/17/16 18:10 111-44-405/13/16 10:133501
bis(2-Chloroisopropyl) ether ND ug/kg 05/17/16 18:10 108-60-105/13/16 10:133501
2-Chloronaphthalene ND ug/kg 05/17/16 18:10 91-58-705/13/16 10:133501
2-Chlorophenol ND ug/kg 05/17/16 18:10 95-57-805/13/16 10:133501
4-Chlorophenylphenyl ether ND ug/kg 05/17/16 18:10 7005-72-305/13/16 10:133501
Chrysene ND ug/kg 05/17/16 18:10 218-01-905/13/16 10:133501
Dibenz(a,h)anthracene ND ug/kg 05/17/16 18:10 53-70-305/13/16 10:133501
Dibenzofuran ND ug/kg 05/17/16 18:10 132-64-905/13/16 10:133501
1,2-Dichlorobenzene ND ug/kg 05/17/16 18:10 95-50-105/13/16 10:133501
1,3-Dichlorobenzene ND ug/kg 05/17/16 18:10 541-73-105/13/16 10:133501
1,4-Dichlorobenzene ND ug/kg 05/17/16 18:10 106-46-705/13/16 10:133501
3,3'-Dichlorobenzidine ND ug/kg 05/17/16 18:10 91-94-105/13/16 10:1317501
2,4-Dichlorophenol ND ug/kg 05/17/16 18:10 120-83-205/13/16 10:133501
Diethylphthalate ND ug/kg 05/17/16 18:10 84-66-205/13/16 10:133501
2,4-Dimethylphenol ND ug/kg 05/17/16 18:10 105-67-905/13/16 10:133501
Dimethylphthalate ND ug/kg 05/17/16 18:10 131-11-305/13/16 10:133501
Di-n-butylphthalate ND ug/kg 05/17/16 18:10 84-74-205/13/16 10:133501
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/16 18:10 534-52-105/13/16 10:137001
2,4-Dinitrophenol ND ug/kg 05/17/16 18:10 51-28-505/13/16 10:1317501
2,4-Dinitrotoluene ND ug/kg 05/17/16 18:10 121-14-205/13/16 10:133501
2,6-Dinitrotoluene ND ug/kg 05/17/16 18:10 606-20-205/13/16 10:133501
Di-n-octylphthalate ND ug/kg 05/17/16 18:10 117-84-005/13/16 10:133501
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/16 18:10 117-81-705/13/16 10:133501
Fluoranthene ND ug/kg 05/17/16 18:10 206-44-005/13/16 10:133501
Fluorene ND ug/kg 05/17/16 18:10 86-73-705/13/16 10:133501
Hexachloro-1,3-butadiene ND ug/kg 05/17/16 18:10 87-68-305/13/16 10:133501
Hexachlorobenzene ND ug/kg 05/17/16 18:10 118-74-105/13/16 10:133501
Hexachlorocyclopentadiene ND ug/kg 05/17/16 18:10 77-47-405/13/16 10:133501
Hexachloroethane ND ug/kg 05/17/16 18:10 67-72-105/13/16 10:133501
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/16 18:10 193-39-505/13/16 10:133501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-2 Lab ID: 92297335008 Collected: 05/11/16 11:29 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 05/17/16 18:10 78-59-105/13/16 10:133501
1-Methylnaphthalene ND ug/kg 05/17/16 18:10 90-12-005/13/16 10:133501
2-Methylnaphthalene ND ug/kg 05/17/16 18:10 91-57-605/13/16 10:133501
2-Methylphenol(o-Cresol)ND ug/kg 05/17/16 18:10 95-48-705/13/16 10:133501
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/17/16 18:1005/13/16 10:133501
Naphthalene ND ug/kg 05/17/16 18:10 91-20-305/13/16 10:133501
2-Nitroaniline ND ug/kg 05/17/16 18:10 88-74-405/13/16 10:1317501
3-Nitroaniline ND ug/kg 05/17/16 18:10 99-09-205/13/16 10:1317501
4-Nitroaniline ND ug/kg 05/17/16 18:10 100-01-605/13/16 10:137001
Nitrobenzene ND ug/kg 05/17/16 18:10 98-95-305/13/16 10:133501
2-Nitrophenol ND ug/kg 05/17/16 18:10 88-75-505/13/16 10:133501
4-Nitrophenol ND ug/kg 05/17/16 18:10 100-02-705/13/16 10:1317501
N-Nitrosodimethylamine ND ug/kg 05/17/16 18:10 62-75-905/13/16 10:133501
N-Nitroso-di-n-propylamine ND ug/kg 05/17/16 18:10 621-64-705/13/16 10:133501
N-Nitrosodiphenylamine ND ug/kg 05/17/16 18:10 86-30-605/13/16 10:133501
Pentachlorophenol ND ug/kg 05/17/16 18:10 87-86-505/13/16 10:1317501
Phenanthrene ND ug/kg 05/17/16 18:10 85-01-805/13/16 10:133501
Phenol ND ug/kg 05/17/16 18:1005/13/16 10:133501
Pyrene ND ug/kg 05/17/16 18:10 129-00-005/13/16 10:133501
1,2,4-Trichlorobenzene ND ug/kg 05/17/16 18:10 120-82-105/13/16 10:133501
2,4,5-Trichlorophenol ND ug/kg 05/17/16 18:10 95-95-405/13/16 10:133501
2,4,6-Trichlorophenol ND ug/kg 05/17/16 18:10 88-06-205/13/16 10:133501
Surrogates
Nitrobenzene-d5 (S)79 %05/17/16 18:10 4165-60-005/13/16 10:1323-110 1
2-Fluorobiphenyl (S)76 %05/17/16 18:10 321-60-805/13/16 10:1330-110 1
Terphenyl-d14 (S)85 %05/17/16 18:10 1718-51-005/13/16 10:1328-110 1
Phenol-d6 (S)75 %05/17/16 18:10 13127-88-305/13/16 10:1322-110 1
2-Fluorophenol (S)73 %05/17/16 18:10 367-12-405/13/16 10:1313-110 1
2,4,6-Tribromophenol (S)90 %05/17/16 18:10 118-79-605/13/16 10:1327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 05/13/16 22:07 67-64-193.4 1
Benzene ND ug/kg 05/13/16 22:07 71-43-24.7 1
Bromobenzene ND ug/kg 05/13/16 22:07 108-86-14.7 1
Bromochloromethane ND ug/kg 05/13/16 22:07 74-97-54.7 1
Bromodichloromethane ND ug/kg 05/13/16 22:07 75-27-44.7 1
Bromoform ND ug/kg 05/13/16 22:07 75-25-24.7 1
Bromomethane ND ug/kg 05/13/16 22:07 74-83-99.3 1
2-Butanone (MEK)ND ug/kg 05/13/16 22:07 78-93-393.4 1
n-Butylbenzene ND ug/kg 05/13/16 22:07 104-51-84.7 1
sec-Butylbenzene ND ug/kg 05/13/16 22:07 135-98-84.7 1
tert-Butylbenzene ND ug/kg 05/13/16 22:07 98-06-64.7 1
Carbon tetrachloride ND ug/kg 05/13/16 22:07 56-23-54.7 1
Chlorobenzene ND ug/kg 05/13/16 22:07 108-90-74.7 1
Chloroethane ND ug/kg 05/13/16 22:07 75-00-39.3 1
Chloroform ND ug/kg 05/13/16 22:07 67-66-34.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-2 Lab ID: 92297335008 Collected: 05/11/16 11:29 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 05/13/16 22:07 74-87-39.3 1
2-Chlorotoluene ND ug/kg 05/13/16 22:07 95-49-84.7 1
4-Chlorotoluene ND ug/kg 05/13/16 22:07 106-43-44.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/13/16 22:07 96-12-84.7 1
Dibromochloromethane ND ug/kg 05/13/16 22:07 124-48-14.7 1
1,2-Dibromoethane (EDB)ND ug/kg 05/13/16 22:07 106-93-44.7 1
Dibromomethane ND ug/kg 05/13/16 22:07 74-95-34.7 1
1,2-Dichlorobenzene ND ug/kg 05/13/16 22:07 95-50-14.7 1
1,3-Dichlorobenzene ND ug/kg 05/13/16 22:07 541-73-14.7 1
1,4-Dichlorobenzene ND ug/kg 05/13/16 22:07 106-46-74.7 1
Dichlorodifluoromethane ND ug/kg 05/13/16 22:07 75-71-89.3 1
1,1-Dichloroethane ND ug/kg 05/13/16 22:07 75-34-34.7 1
1,2-Dichloroethane ND ug/kg 05/13/16 22:07 107-06-24.7 1
1,1-Dichloroethene ND ug/kg 05/13/16 22:07 75-35-44.7 1
cis-1,2-Dichloroethene ND ug/kg 05/13/16 22:07 156-59-24.7 1
trans-1,2-Dichloroethene ND ug/kg 05/13/16 22:07 156-60-54.7 1
1,2-Dichloropropane ND ug/kg 05/13/16 22:07 78-87-54.7 1
1,3-Dichloropropane ND ug/kg 05/13/16 22:07 142-28-94.7 1
2,2-Dichloropropane ND ug/kg 05/13/16 22:07 594-20-74.7 1
1,1-Dichloropropene ND ug/kg 05/13/16 22:07 563-58-64.7 1
cis-1,3-Dichloropropene ND ug/kg 05/13/16 22:07 10061-01-54.7 1
trans-1,3-Dichloropropene ND ug/kg 05/13/16 22:07 10061-02-64.7 1
Diisopropyl ether ND ug/kg 05/13/16 22:07 108-20-34.7 1
Ethylbenzene ND ug/kg 05/13/16 22:07 100-41-44.7 1
Hexachloro-1,3-butadiene ND ug/kg 05/13/16 22:07 87-68-34.7 1
2-Hexanone ND ug/kg 05/13/16 22:07 591-78-646.7 1
Isopropylbenzene (Cumene)ND ug/kg 05/13/16 22:07 98-82-84.7 1
p-Isopropyltoluene ND ug/kg 05/13/16 22:07 99-87-64.7 1
Methylene Chloride ND ug/kg 05/13/16 22:07 75-09-218.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/13/16 22:07 108-10-146.7 1
Methyl-tert-butyl ether ND ug/kg 05/13/16 22:07 1634-04-44.7 1
Naphthalene ND ug/kg 05/13/16 22:07 91-20-34.7 1
n-Propylbenzene ND ug/kg 05/13/16 22:07 103-65-14.7 1
Styrene ND ug/kg 05/13/16 22:07 100-42-54.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/13/16 22:07 630-20-64.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/13/16 22:07 79-34-54.7 1
Tetrachloroethene ND ug/kg 05/13/16 22:07 127-18-44.7 1
Toluene ND ug/kg 05/13/16 22:07 108-88-34.7 1
1,2,3-Trichlorobenzene ND ug/kg 05/13/16 22:07 87-61-64.7 1
1,2,4-Trichlorobenzene ND ug/kg 05/13/16 22:07 120-82-14.7 1
1,1,1-Trichloroethane ND ug/kg 05/13/16 22:07 71-55-64.7 1
1,1,2-Trichloroethane ND ug/kg 05/13/16 22:07 79-00-54.7 1
Trichloroethene ND ug/kg 05/13/16 22:07 79-01-64.7 1
Trichlorofluoromethane ND ug/kg 05/13/16 22:07 75-69-44.7 1
1,2,3-Trichloropropane ND ug/kg 05/13/16 22:07 96-18-44.7 1
1,2,4-Trimethylbenzene ND ug/kg 05/13/16 22:07 95-63-64.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-2 Lab ID: 92297335008 Collected: 05/11/16 11:29 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 05/13/16 22:07 108-67-84.7 1
Vinyl acetate ND ug/kg 05/13/16 22:07 108-05-446.7 1
Vinyl chloride ND ug/kg 05/13/16 22:07 75-01-49.3 1
Xylene (Total)ND ug/kg 05/13/16 22:07 1330-20-79.3 1
m&p-Xylene ND ug/kg 05/13/16 22:07 179601-23-19.3 1
o-Xylene ND ug/kg 05/13/16 22:07 95-47-64.7 1
Surrogates
Toluene-d8 (S)100 %05/13/16 22:07 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %05/13/16 22:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)77 %05/13/16 22:07 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 5.7 %05/13/16 07:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-3 Lab ID: 92297335009 Collected: 05/11/16 11:35 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/17/16 19:11 83-32-905/13/16 10:133571
Acenaphthylene ND ug/kg 05/17/16 19:11 208-96-805/13/16 10:133571
Aniline ND ug/kg 05/17/16 19:11 62-53-305/13/16 10:133571
Anthracene ND ug/kg 05/17/16 19:11 120-12-705/13/16 10:133571
Benzo(a)anthracene ND ug/kg 05/17/16 19:11 56-55-305/13/16 10:133571
Benzo(a)pyrene ND ug/kg 05/17/16 19:11 50-32-805/13/16 10:133571
Benzo(b)fluoranthene ND ug/kg 05/17/16 19:11 205-99-205/13/16 10:133571
Benzo(g,h,i)perylene ND ug/kg 05/17/16 19:11 191-24-205/13/16 10:133571
Benzo(k)fluoranthene ND ug/kg 05/17/16 19:11 207-08-905/13/16 10:133571
Benzoic Acid ND ug/kg 05/17/16 19:11 65-85-005/13/16 10:1317901
Benzyl alcohol ND ug/kg 05/17/16 19:11 100-51-605/13/16 10:137151
4-Bromophenylphenyl ether ND ug/kg 05/17/16 19:11 101-55-305/13/16 10:133571
Butylbenzylphthalate ND ug/kg 05/17/16 19:11 85-68-705/13/16 10:133571
4-Chloro-3-methylphenol ND ug/kg 05/17/16 19:11 59-50-705/13/16 10:137151
4-Chloroaniline ND ug/kg 05/17/16 19:11 106-47-805/13/16 10:1317901
bis(2-Chloroethoxy)methane ND ug/kg 05/17/16 19:11 111-91-105/13/16 10:133571
bis(2-Chloroethyl) ether ND ug/kg 05/17/16 19:11 111-44-405/13/16 10:133571
bis(2-Chloroisopropyl) ether ND ug/kg 05/17/16 19:11 108-60-105/13/16 10:133571
2-Chloronaphthalene ND ug/kg 05/17/16 19:11 91-58-705/13/16 10:133571
2-Chlorophenol ND ug/kg 05/17/16 19:11 95-57-805/13/16 10:133571
4-Chlorophenylphenyl ether ND ug/kg 05/17/16 19:11 7005-72-305/13/16 10:133571
Chrysene ND ug/kg 05/17/16 19:11 218-01-905/13/16 10:133571
Dibenz(a,h)anthracene ND ug/kg 05/17/16 19:11 53-70-305/13/16 10:133571
Dibenzofuran ND ug/kg 05/17/16 19:11 132-64-905/13/16 10:133571
1,2-Dichlorobenzene ND ug/kg 05/17/16 19:11 95-50-105/13/16 10:133571
1,3-Dichlorobenzene ND ug/kg 05/17/16 19:11 541-73-105/13/16 10:133571
1,4-Dichlorobenzene ND ug/kg 05/17/16 19:11 106-46-705/13/16 10:133571
3,3'-Dichlorobenzidine ND ug/kg 05/17/16 19:11 91-94-105/13/16 10:1317901
2,4-Dichlorophenol ND ug/kg 05/17/16 19:11 120-83-205/13/16 10:133571
Diethylphthalate ND ug/kg 05/17/16 19:11 84-66-205/13/16 10:133571
2,4-Dimethylphenol ND ug/kg 05/17/16 19:11 105-67-905/13/16 10:133571
Dimethylphthalate ND ug/kg 05/17/16 19:11 131-11-305/13/16 10:133571
Di-n-butylphthalate ND ug/kg 05/17/16 19:11 84-74-205/13/16 10:133571
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/16 19:11 534-52-105/13/16 10:137151
2,4-Dinitrophenol ND ug/kg 05/17/16 19:11 51-28-505/13/16 10:1317901
2,4-Dinitrotoluene ND ug/kg 05/17/16 19:11 121-14-205/13/16 10:133571
2,6-Dinitrotoluene ND ug/kg 05/17/16 19:11 606-20-205/13/16 10:133571
Di-n-octylphthalate ND ug/kg 05/17/16 19:11 117-84-005/13/16 10:133571
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/16 19:11 117-81-705/13/16 10:133571
Fluoranthene ND ug/kg 05/17/16 19:11 206-44-005/13/16 10:133571
Fluorene ND ug/kg 05/17/16 19:11 86-73-705/13/16 10:133571
Hexachloro-1,3-butadiene ND ug/kg 05/17/16 19:11 87-68-305/13/16 10:133571
Hexachlorobenzene ND ug/kg 05/17/16 19:11 118-74-105/13/16 10:133571
Hexachlorocyclopentadiene ND ug/kg 05/17/16 19:11 77-47-405/13/16 10:133571
Hexachloroethane ND ug/kg 05/17/16 19:11 67-72-105/13/16 10:133571
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/16 19:11 193-39-505/13/16 10:133571
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-3 Lab ID: 92297335009 Collected: 05/11/16 11:35 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 05/17/16 19:11 78-59-105/13/16 10:133571
1-Methylnaphthalene ND ug/kg 05/17/16 19:11 90-12-005/13/16 10:133571
2-Methylnaphthalene ND ug/kg 05/17/16 19:11 91-57-605/13/16 10:133571
2-Methylphenol(o-Cresol)ND ug/kg 05/17/16 19:11 95-48-705/13/16 10:133571
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/17/16 19:1105/13/16 10:133571
Naphthalene ND ug/kg 05/17/16 19:11 91-20-305/13/16 10:133571
2-Nitroaniline ND ug/kg 05/17/16 19:11 88-74-405/13/16 10:1317901
3-Nitroaniline ND ug/kg 05/17/16 19:11 99-09-205/13/16 10:1317901
4-Nitroaniline ND ug/kg 05/17/16 19:11 100-01-605/13/16 10:137151
Nitrobenzene ND ug/kg 05/17/16 19:11 98-95-305/13/16 10:133571
2-Nitrophenol ND ug/kg 05/17/16 19:11 88-75-505/13/16 10:133571
4-Nitrophenol ND ug/kg 05/17/16 19:11 100-02-705/13/16 10:1317901
N-Nitrosodimethylamine ND ug/kg 05/17/16 19:11 62-75-905/13/16 10:133571
N-Nitroso-di-n-propylamine ND ug/kg 05/17/16 19:11 621-64-705/13/16 10:133571
N-Nitrosodiphenylamine ND ug/kg 05/17/16 19:11 86-30-605/13/16 10:133571
Pentachlorophenol ND ug/kg 05/17/16 19:11 87-86-505/13/16 10:1317901
Phenanthrene ND ug/kg 05/17/16 19:11 85-01-805/13/16 10:133571
Phenol ND ug/kg 05/17/16 19:1105/13/16 10:133571
Pyrene ND ug/kg 05/17/16 19:11 129-00-005/13/16 10:133571
1,2,4-Trichlorobenzene ND ug/kg 05/17/16 19:11 120-82-105/13/16 10:133571
2,4,5-Trichlorophenol ND ug/kg 05/17/16 19:11 95-95-405/13/16 10:133571
2,4,6-Trichlorophenol ND ug/kg 05/17/16 19:11 88-06-205/13/16 10:133571
Surrogates
Nitrobenzene-d5 (S)68 %05/17/16 19:11 4165-60-005/13/16 10:1323-110 1
2-Fluorobiphenyl (S)62 %05/17/16 19:11 321-60-805/13/16 10:1330-110 1
Terphenyl-d14 (S)64 %05/17/16 19:11 1718-51-005/13/16 10:1328-110 1
Phenol-d6 (S)63 %05/17/16 19:11 13127-88-305/13/16 10:1322-110 1
2-Fluorophenol (S)62 %05/17/16 19:11 367-12-405/13/16 10:1313-110 1
2,4,6-Tribromophenol (S)76 %05/17/16 19:11 118-79-605/13/16 10:1327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 05/13/16 22:28 67-64-11241
Benzene ND ug/kg 05/13/16 22:28 71-43-26.2 1
Bromobenzene ND ug/kg 05/13/16 22:28 108-86-16.2 1
Bromochloromethane ND ug/kg 05/13/16 22:28 74-97-56.2 1
Bromodichloromethane ND ug/kg 05/13/16 22:28 75-27-46.2 1
Bromoform ND ug/kg 05/13/16 22:28 75-25-26.2 1
Bromomethane ND ug/kg 05/13/16 22:28 74-83-912.4 1
2-Butanone (MEK)ND ug/kg 05/13/16 22:28 78-93-31241
n-Butylbenzene ND ug/kg 05/13/16 22:28 104-51-86.2 1
sec-Butylbenzene ND ug/kg 05/13/16 22:28 135-98-86.2 1
tert-Butylbenzene ND ug/kg 05/13/16 22:28 98-06-66.2 1
Carbon tetrachloride ND ug/kg 05/13/16 22:28 56-23-56.2 1
Chlorobenzene ND ug/kg 05/13/16 22:28 108-90-76.2 1
Chloroethane ND ug/kg 05/13/16 22:28 75-00-312.4 1
Chloroform ND ug/kg 05/13/16 22:28 67-66-36.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-3 Lab ID: 92297335009 Collected: 05/11/16 11:35 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 05/13/16 22:28 74-87-312.4 1
2-Chlorotoluene ND ug/kg 05/13/16 22:28 95-49-86.2 1
4-Chlorotoluene ND ug/kg 05/13/16 22:28 106-43-46.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/13/16 22:28 96-12-86.2 1
Dibromochloromethane ND ug/kg 05/13/16 22:28 124-48-16.2 1
1,2-Dibromoethane (EDB)ND ug/kg 05/13/16 22:28 106-93-46.2 1
Dibromomethane ND ug/kg 05/13/16 22:28 74-95-36.2 1
1,2-Dichlorobenzene ND ug/kg 05/13/16 22:28 95-50-16.2 1
1,3-Dichlorobenzene ND ug/kg 05/13/16 22:28 541-73-16.2 1
1,4-Dichlorobenzene ND ug/kg 05/13/16 22:28 106-46-76.2 1
Dichlorodifluoromethane ND ug/kg 05/13/16 22:28 75-71-812.4 1
1,1-Dichloroethane ND ug/kg 05/13/16 22:28 75-34-36.2 1
1,2-Dichloroethane ND ug/kg 05/13/16 22:28 107-06-26.2 1
1,1-Dichloroethene ND ug/kg 05/13/16 22:28 75-35-46.2 1
cis-1,2-Dichloroethene ND ug/kg 05/13/16 22:28 156-59-26.2 1
trans-1,2-Dichloroethene ND ug/kg 05/13/16 22:28 156-60-56.2 1
1,2-Dichloropropane ND ug/kg 05/13/16 22:28 78-87-56.2 1
1,3-Dichloropropane ND ug/kg 05/13/16 22:28 142-28-96.2 1
2,2-Dichloropropane ND ug/kg 05/13/16 22:28 594-20-76.2 1
1,1-Dichloropropene ND ug/kg 05/13/16 22:28 563-58-66.2 1
cis-1,3-Dichloropropene ND ug/kg 05/13/16 22:28 10061-01-56.2 1
trans-1,3-Dichloropropene ND ug/kg 05/13/16 22:28 10061-02-66.2 1
Diisopropyl ether ND ug/kg 05/13/16 22:28 108-20-36.2 1
Ethylbenzene ND ug/kg 05/13/16 22:28 100-41-46.2 1
Hexachloro-1,3-butadiene ND ug/kg 05/13/16 22:28 87-68-36.2 1
2-Hexanone ND ug/kg 05/13/16 22:28 591-78-662.0 1
Isopropylbenzene (Cumene)ND ug/kg 05/13/16 22:28 98-82-86.2 1
p-Isopropyltoluene ND ug/kg 05/13/16 22:28 99-87-66.2 1
Methylene Chloride ND ug/kg 05/13/16 22:28 75-09-224.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/13/16 22:28 108-10-162.0 1
Methyl-tert-butyl ether ND ug/kg 05/13/16 22:28 1634-04-46.2 1
Naphthalene ND ug/kg 05/13/16 22:28 91-20-36.2 1
n-Propylbenzene ND ug/kg 05/13/16 22:28 103-65-16.2 1
Styrene ND ug/kg 05/13/16 22:28 100-42-56.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/13/16 22:28 630-20-66.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/13/16 22:28 79-34-56.2 1
Tetrachloroethene ND ug/kg 05/13/16 22:28 127-18-46.2 1
Toluene ND ug/kg 05/13/16 22:28 108-88-36.2 1
1,2,3-Trichlorobenzene ND ug/kg 05/13/16 22:28 87-61-66.2 1
1,2,4-Trichlorobenzene ND ug/kg 05/13/16 22:28 120-82-16.2 1
1,1,1-Trichloroethane ND ug/kg 05/13/16 22:28 71-55-66.2 1
1,1,2-Trichloroethane ND ug/kg 05/13/16 22:28 79-00-56.2 1
Trichloroethene ND ug/kg 05/13/16 22:28 79-01-66.2 1
Trichlorofluoromethane ND ug/kg 05/13/16 22:28 75-69-46.2 1
1,2,3-Trichloropropane ND ug/kg 05/13/16 22:28 96-18-46.2 1
1,2,4-Trimethylbenzene ND ug/kg 05/13/16 22:28 95-63-66.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-3 Lab ID: 92297335009 Collected: 05/11/16 11:35 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 05/13/16 22:28 108-67-86.2 1
Vinyl acetate ND ug/kg 05/13/16 22:28 108-05-462.0 1
Vinyl chloride ND ug/kg 05/13/16 22:28 75-01-412.4 1
Xylene (Total)ND ug/kg 05/13/16 22:28 1330-20-712.4 1
m&p-Xylene ND ug/kg 05/13/16 22:28 179601-23-112.4 1
o-Xylene ND ug/kg 05/13/16 22:28 95-47-66.2 1
Surrogates
Toluene-d8 (S)98 %05/13/16 22:28 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %05/13/16 22:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)82 %05/13/16 22:28 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 7.7 %05/13/16 07:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-4 Lab ID: 92297335010 Collected: 05/11/16 11:41 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/18/16 15:02 83-32-905/13/16 10:133601
Acenaphthylene ND ug/kg 05/18/16 15:02 208-96-805/13/16 10:133601
Aniline ND ug/kg 05/18/16 15:02 62-53-305/13/16 10:133601
Anthracene ND ug/kg 05/18/16 15:02 120-12-705/13/16 10:133601
Benzo(a)anthracene ND ug/kg 05/18/16 15:02 56-55-305/13/16 10:133601
Benzo(a)pyrene ND ug/kg 05/18/16 15:02 50-32-805/13/16 10:133601
Benzo(b)fluoranthene ND ug/kg 05/18/16 15:02 205-99-205/13/16 10:133601
Benzo(g,h,i)perylene ND ug/kg 05/18/16 15:02 191-24-205/13/16 10:133601
Benzo(k)fluoranthene ND ug/kg 05/18/16 15:02 207-08-905/13/16 10:133601
Benzoic Acid ND ug/kg 05/18/16 15:02 65-85-005/13/16 10:1318001
Benzyl alcohol ND ug/kg 05/18/16 15:02 100-51-605/13/16 10:137191
4-Bromophenylphenyl ether ND ug/kg 05/18/16 15:02 101-55-305/13/16 10:133601
Butylbenzylphthalate ND ug/kg 05/18/16 15:02 85-68-705/13/16 10:133601
4-Chloro-3-methylphenol ND ug/kg 05/18/16 15:02 59-50-705/13/16 10:137191
4-Chloroaniline ND ug/kg 05/18/16 15:02 106-47-805/13/16 10:1318001
bis(2-Chloroethoxy)methane ND ug/kg 05/18/16 15:02 111-91-105/13/16 10:133601
bis(2-Chloroethyl) ether ND ug/kg 05/18/16 15:02 111-44-405/13/16 10:133601
bis(2-Chloroisopropyl) ether ND ug/kg 05/18/16 15:02 108-60-105/13/16 10:133601
2-Chloronaphthalene ND ug/kg 05/18/16 15:02 91-58-705/13/16 10:133601
2-Chlorophenol ND ug/kg 05/18/16 15:02 95-57-805/13/16 10:133601
4-Chlorophenylphenyl ether ND ug/kg 05/18/16 15:02 7005-72-305/13/16 10:133601
Chrysene ND ug/kg 05/18/16 15:02 218-01-905/13/16 10:133601
Dibenz(a,h)anthracene ND ug/kg 05/18/16 15:02 53-70-305/13/16 10:133601
Dibenzofuran ND ug/kg 05/18/16 15:02 132-64-905/13/16 10:133601
1,2-Dichlorobenzene ND ug/kg 05/18/16 15:02 95-50-105/13/16 10:133601
1,3-Dichlorobenzene ND ug/kg 05/18/16 15:02 541-73-105/13/16 10:133601
1,4-Dichlorobenzene ND ug/kg 05/18/16 15:02 106-46-705/13/16 10:133601
3,3'-Dichlorobenzidine ND ug/kg 05/18/16 15:02 91-94-105/13/16 10:1318001
2,4-Dichlorophenol ND ug/kg 05/18/16 15:02 120-83-205/13/16 10:133601
Diethylphthalate ND ug/kg 05/18/16 15:02 84-66-205/13/16 10:133601
2,4-Dimethylphenol ND ug/kg 05/18/16 15:02 105-67-905/13/16 10:133601
Dimethylphthalate ND ug/kg 05/18/16 15:02 131-11-305/13/16 10:133601
Di-n-butylphthalate ND ug/kg 05/18/16 15:02 84-74-205/13/16 10:133601
4,6-Dinitro-2-methylphenol ND ug/kg 05/18/16 15:02 534-52-105/13/16 10:137191
2,4-Dinitrophenol ND ug/kg 05/18/16 15:02 51-28-505/13/16 10:1318001
2,4-Dinitrotoluene ND ug/kg 05/18/16 15:02 121-14-205/13/16 10:133601
2,6-Dinitrotoluene ND ug/kg 05/18/16 15:02 606-20-205/13/16 10:133601
Di-n-octylphthalate ND ug/kg 05/18/16 15:02 117-84-005/13/16 10:133601
bis(2-Ethylhexyl)phthalate ND ug/kg 05/18/16 15:02 117-81-705/13/16 10:133601
Fluoranthene ND ug/kg 05/18/16 15:02 206-44-005/13/16 10:133601
Fluorene ND ug/kg 05/18/16 15:02 86-73-705/13/16 10:133601
Hexachloro-1,3-butadiene ND ug/kg 05/18/16 15:02 87-68-305/13/16 10:133601
Hexachlorobenzene ND ug/kg 05/18/16 15:02 118-74-105/13/16 10:133601
Hexachlorocyclopentadiene ND ug/kg 05/18/16 15:02 77-47-405/13/16 10:133601
Hexachloroethane ND ug/kg 05/18/16 15:02 67-72-105/13/16 10:133601
Indeno(1,2,3-cd)pyrene ND ug/kg 05/18/16 15:02 193-39-505/13/16 10:133601
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-4 Lab ID: 92297335010 Collected: 05/11/16 11:41 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 05/18/16 15:02 78-59-105/13/16 10:133601
1-Methylnaphthalene ND ug/kg 05/18/16 15:02 90-12-005/13/16 10:133601
2-Methylnaphthalene ND ug/kg 05/18/16 15:02 91-57-605/13/16 10:133601
2-Methylphenol(o-Cresol)ND ug/kg 05/18/16 15:02 95-48-705/13/16 10:133601
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/18/16 15:0205/13/16 10:133601
Naphthalene ND ug/kg 05/18/16 15:02 91-20-305/13/16 10:133601
2-Nitroaniline ND ug/kg 05/18/16 15:02 88-74-405/13/16 10:1318001
3-Nitroaniline ND ug/kg 05/18/16 15:02 99-09-205/13/16 10:1318001
4-Nitroaniline ND ug/kg 05/18/16 15:02 100-01-605/13/16 10:137191
Nitrobenzene ND ug/kg 05/18/16 15:02 98-95-305/13/16 10:133601
2-Nitrophenol ND ug/kg 05/18/16 15:02 88-75-505/13/16 10:133601
4-Nitrophenol ND ug/kg 05/18/16 15:02 100-02-705/13/16 10:1318001
N-Nitrosodimethylamine ND ug/kg 05/18/16 15:02 62-75-905/13/16 10:133601
N-Nitroso-di-n-propylamine ND ug/kg 05/18/16 15:02 621-64-705/13/16 10:133601
N-Nitrosodiphenylamine ND ug/kg 05/18/16 15:02 86-30-605/13/16 10:133601
Pentachlorophenol ND ug/kg 05/18/16 15:02 87-86-505/13/16 10:1318001
Phenanthrene ND ug/kg 05/18/16 15:02 85-01-805/13/16 10:133601
Phenol ND ug/kg 05/18/16 15:0205/13/16 10:133601
Pyrene ND ug/kg 05/18/16 15:02 129-00-005/13/16 10:133601
1,2,4-Trichlorobenzene ND ug/kg 05/18/16 15:02 120-82-105/13/16 10:133601
2,4,5-Trichlorophenol ND ug/kg 05/18/16 15:02 95-95-405/13/16 10:133601
2,4,6-Trichlorophenol ND ug/kg 05/18/16 15:02 88-06-205/13/16 10:133601
Surrogates
Nitrobenzene-d5 (S)74 %05/18/16 15:02 4165-60-005/13/16 10:1323-110 1
2-Fluorobiphenyl (S)70 %05/18/16 15:02 321-60-805/13/16 10:1330-110 1
Terphenyl-d14 (S)80 %05/18/16 15:02 1718-51-005/13/16 10:1328-110 1
Phenol-d6 (S)70 %05/18/16 15:02 13127-88-305/13/16 10:1322-110 1
2-Fluorophenol (S)68 %05/18/16 15:02 367-12-405/13/16 10:1313-110 1
2,4,6-Tribromophenol (S)83 %05/18/16 15:02 118-79-605/13/16 10:1327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 05/13/16 22:48 67-64-11321
Benzene ND ug/kg 05/13/16 22:48 71-43-26.6 1
Bromobenzene ND ug/kg 05/13/16 22:48 108-86-16.6 1
Bromochloromethane ND ug/kg 05/13/16 22:48 74-97-56.6 1
Bromodichloromethane ND ug/kg 05/13/16 22:48 75-27-46.6 1
Bromoform ND ug/kg 05/13/16 22:48 75-25-26.6 1
Bromomethane ND ug/kg 05/13/16 22:48 74-83-913.2 1
2-Butanone (MEK)ND ug/kg 05/13/16 22:48 78-93-31321
n-Butylbenzene ND ug/kg 05/13/16 22:48 104-51-86.6 1
sec-Butylbenzene ND ug/kg 05/13/16 22:48 135-98-86.6 1
tert-Butylbenzene ND ug/kg 05/13/16 22:48 98-06-66.6 1
Carbon tetrachloride ND ug/kg 05/13/16 22:48 56-23-56.6 1
Chlorobenzene ND ug/kg 05/13/16 22:48 108-90-76.6 1
Chloroethane ND ug/kg 05/13/16 22:48 75-00-313.2 1
Chloroform ND ug/kg 05/13/16 22:48 67-66-36.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-4 Lab ID: 92297335010 Collected: 05/11/16 11:41 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 05/13/16 22:48 74-87-313.2 1
2-Chlorotoluene ND ug/kg 05/13/16 22:48 95-49-86.6 1
4-Chlorotoluene ND ug/kg 05/13/16 22:48 106-43-46.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/13/16 22:48 96-12-86.6 1
Dibromochloromethane ND ug/kg 05/13/16 22:48 124-48-16.6 1
1,2-Dibromoethane (EDB)ND ug/kg 05/13/16 22:48 106-93-46.6 1
Dibromomethane ND ug/kg 05/13/16 22:48 74-95-36.6 1
1,2-Dichlorobenzene ND ug/kg 05/13/16 22:48 95-50-16.6 1
1,3-Dichlorobenzene ND ug/kg 05/13/16 22:48 541-73-16.6 1
1,4-Dichlorobenzene ND ug/kg 05/13/16 22:48 106-46-76.6 1
Dichlorodifluoromethane ND ug/kg 05/13/16 22:48 75-71-813.2 1
1,1-Dichloroethane ND ug/kg 05/13/16 22:48 75-34-36.6 1
1,2-Dichloroethane ND ug/kg 05/13/16 22:48 107-06-26.6 1
1,1-Dichloroethene ND ug/kg 05/13/16 22:48 75-35-46.6 1
cis-1,2-Dichloroethene ND ug/kg 05/13/16 22:48 156-59-26.6 1
trans-1,2-Dichloroethene ND ug/kg 05/13/16 22:48 156-60-56.6 1
1,2-Dichloropropane ND ug/kg 05/13/16 22:48 78-87-56.6 1
1,3-Dichloropropane ND ug/kg 05/13/16 22:48 142-28-96.6 1
2,2-Dichloropropane ND ug/kg 05/13/16 22:48 594-20-76.6 1
1,1-Dichloropropene ND ug/kg 05/13/16 22:48 563-58-66.6 1
cis-1,3-Dichloropropene ND ug/kg 05/13/16 22:48 10061-01-56.6 1
trans-1,3-Dichloropropene ND ug/kg 05/13/16 22:48 10061-02-66.6 1
Diisopropyl ether ND ug/kg 05/13/16 22:48 108-20-36.6 1
Ethylbenzene ND ug/kg 05/13/16 22:48 100-41-46.6 1
Hexachloro-1,3-butadiene ND ug/kg 05/13/16 22:48 87-68-36.6 1
2-Hexanone ND ug/kg 05/13/16 22:48 591-78-665.8 1
Isopropylbenzene (Cumene)ND ug/kg 05/13/16 22:48 98-82-86.6 1
p-Isopropyltoluene ND ug/kg 05/13/16 22:48 99-87-66.6 1
Methylene Chloride ND ug/kg 05/13/16 22:48 75-09-226.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/13/16 22:48 108-10-165.8 1
Methyl-tert-butyl ether ND ug/kg 05/13/16 22:48 1634-04-46.6 1
Naphthalene ND ug/kg 05/13/16 22:48 91-20-36.6 1
n-Propylbenzene ND ug/kg 05/13/16 22:48 103-65-16.6 1
Styrene ND ug/kg 05/13/16 22:48 100-42-56.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/13/16 22:48 630-20-66.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/13/16 22:48 79-34-56.6 1
Tetrachloroethene ND ug/kg 05/13/16 22:48 127-18-46.6 1
Toluene ND ug/kg 05/13/16 22:48 108-88-36.6 1
1,2,3-Trichlorobenzene ND ug/kg 05/13/16 22:48 87-61-66.6 1
1,2,4-Trichlorobenzene ND ug/kg 05/13/16 22:48 120-82-16.6 1
1,1,1-Trichloroethane ND ug/kg 05/13/16 22:48 71-55-66.6 1
1,1,2-Trichloroethane ND ug/kg 05/13/16 22:48 79-00-56.6 1
Trichloroethene ND ug/kg 05/13/16 22:48 79-01-66.6 1
Trichlorofluoromethane ND ug/kg 05/13/16 22:48 75-69-46.6 1
1,2,3-Trichloropropane ND ug/kg 05/13/16 22:48 96-18-46.6 1
1,2,4-Trimethylbenzene ND ug/kg 05/13/16 22:48 95-63-66.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-4 Lab ID: 92297335010 Collected: 05/11/16 11:41 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 05/13/16 22:48 108-67-86.6 1
Vinyl acetate ND ug/kg 05/13/16 22:48 108-05-465.8 1
Vinyl chloride ND ug/kg 05/13/16 22:48 75-01-413.2 1
Xylene (Total)ND ug/kg 05/13/16 22:48 1330-20-713.2 1
m&p-Xylene ND ug/kg 05/13/16 22:48 179601-23-113.2 1
o-Xylene ND ug/kg 05/13/16 22:48 95-47-66.6 1
Surrogates
Toluene-d8 (S)100 %05/13/16 22:48 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %05/13/16 22:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %05/13/16 22:48 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.2 %05/13/16 07:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-5 Lab ID: 92297335011 Collected: 05/11/16 11:47 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/17/16 20:13 83-32-905/13/16 10:133581
Acenaphthylene ND ug/kg 05/17/16 20:13 208-96-805/13/16 10:133581
Aniline ND ug/kg 05/17/16 20:13 62-53-305/13/16 10:133581
Anthracene ND ug/kg 05/17/16 20:13 120-12-705/13/16 10:133581
Benzo(a)anthracene ND ug/kg 05/17/16 20:13 56-55-305/13/16 10:133581
Benzo(a)pyrene ND ug/kg 05/17/16 20:13 50-32-805/13/16 10:133581
Benzo(b)fluoranthene ND ug/kg 05/17/16 20:13 205-99-205/13/16 10:133581
Benzo(g,h,i)perylene ND ug/kg 05/17/16 20:13 191-24-205/13/16 10:133581
Benzo(k)fluoranthene ND ug/kg 05/17/16 20:13 207-08-905/13/16 10:133581
Benzoic Acid ND ug/kg 05/17/16 20:13 65-85-005/13/16 10:1317901
Benzyl alcohol ND ug/kg 05/17/16 20:13 100-51-605/13/16 10:137171
4-Bromophenylphenyl ether ND ug/kg 05/17/16 20:13 101-55-305/13/16 10:133581
Butylbenzylphthalate ND ug/kg 05/17/16 20:13 85-68-705/13/16 10:133581
4-Chloro-3-methylphenol ND ug/kg 05/17/16 20:13 59-50-705/13/16 10:137171
4-Chloroaniline ND ug/kg 05/17/16 20:13 106-47-805/13/16 10:1317901
bis(2-Chloroethoxy)methane ND ug/kg 05/17/16 20:13 111-91-105/13/16 10:133581
bis(2-Chloroethyl) ether ND ug/kg 05/17/16 20:13 111-44-405/13/16 10:133581
bis(2-Chloroisopropyl) ether ND ug/kg 05/17/16 20:13 108-60-105/13/16 10:133581
2-Chloronaphthalene ND ug/kg 05/17/16 20:13 91-58-705/13/16 10:133581
2-Chlorophenol ND ug/kg 05/17/16 20:13 95-57-805/13/16 10:133581
4-Chlorophenylphenyl ether ND ug/kg 05/17/16 20:13 7005-72-305/13/16 10:133581
Chrysene ND ug/kg 05/17/16 20:13 218-01-905/13/16 10:133581
Dibenz(a,h)anthracene ND ug/kg 05/17/16 20:13 53-70-305/13/16 10:133581
Dibenzofuran ND ug/kg 05/17/16 20:13 132-64-905/13/16 10:133581
1,2-Dichlorobenzene ND ug/kg 05/17/16 20:13 95-50-105/13/16 10:133581
1,3-Dichlorobenzene ND ug/kg 05/17/16 20:13 541-73-105/13/16 10:133581
1,4-Dichlorobenzene ND ug/kg 05/17/16 20:13 106-46-705/13/16 10:133581
3,3'-Dichlorobenzidine ND ug/kg 05/17/16 20:13 91-94-105/13/16 10:1317901
2,4-Dichlorophenol ND ug/kg 05/17/16 20:13 120-83-205/13/16 10:133581
Diethylphthalate ND ug/kg 05/17/16 20:13 84-66-205/13/16 10:133581
2,4-Dimethylphenol ND ug/kg 05/17/16 20:13 105-67-905/13/16 10:133581
Dimethylphthalate ND ug/kg 05/17/16 20:13 131-11-305/13/16 10:133581
Di-n-butylphthalate ND ug/kg 05/17/16 20:13 84-74-205/13/16 10:133581
4,6-Dinitro-2-methylphenol ND ug/kg 05/17/16 20:13 534-52-105/13/16 10:137171
2,4-Dinitrophenol ND ug/kg 05/17/16 20:13 51-28-505/13/16 10:1317901
2,4-Dinitrotoluene ND ug/kg 05/17/16 20:13 121-14-205/13/16 10:133581
2,6-Dinitrotoluene ND ug/kg 05/17/16 20:13 606-20-205/13/16 10:133581
Di-n-octylphthalate ND ug/kg 05/17/16 20:13 117-84-005/13/16 10:133581
bis(2-Ethylhexyl)phthalate ND ug/kg 05/17/16 20:13 117-81-705/13/16 10:133581
Fluoranthene ND ug/kg 05/17/16 20:13 206-44-005/13/16 10:133581
Fluorene ND ug/kg 05/17/16 20:13 86-73-705/13/16 10:133581
Hexachloro-1,3-butadiene ND ug/kg 05/17/16 20:13 87-68-305/13/16 10:133581
Hexachlorobenzene ND ug/kg 05/17/16 20:13 118-74-105/13/16 10:133581
Hexachlorocyclopentadiene ND ug/kg 05/17/16 20:13 77-47-405/13/16 10:133581
Hexachloroethane ND ug/kg 05/17/16 20:13 67-72-105/13/16 10:133581
Indeno(1,2,3-cd)pyrene ND ug/kg 05/17/16 20:13 193-39-505/13/16 10:133581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-5 Lab ID: 92297335011 Collected: 05/11/16 11:47 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 05/17/16 20:13 78-59-105/13/16 10:133581
1-Methylnaphthalene ND ug/kg 05/17/16 20:13 90-12-005/13/16 10:133581
2-Methylnaphthalene ND ug/kg 05/17/16 20:13 91-57-605/13/16 10:133581
2-Methylphenol(o-Cresol)ND ug/kg 05/17/16 20:13 95-48-705/13/16 10:133581
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/17/16 20:1305/13/16 10:133581
Naphthalene ND ug/kg 05/17/16 20:13 91-20-305/13/16 10:133581
2-Nitroaniline ND ug/kg 05/17/16 20:13 88-74-405/13/16 10:1317901
3-Nitroaniline ND ug/kg 05/17/16 20:13 99-09-205/13/16 10:1317901
4-Nitroaniline ND ug/kg 05/17/16 20:13 100-01-605/13/16 10:137171
Nitrobenzene ND ug/kg 05/17/16 20:13 98-95-305/13/16 10:133581
2-Nitrophenol ND ug/kg 05/17/16 20:13 88-75-505/13/16 10:133581
4-Nitrophenol ND ug/kg 05/17/16 20:13 100-02-705/13/16 10:1317901
N-Nitrosodimethylamine ND ug/kg 05/17/16 20:13 62-75-905/13/16 10:133581
N-Nitroso-di-n-propylamine ND ug/kg 05/17/16 20:13 621-64-705/13/16 10:133581
N-Nitrosodiphenylamine ND ug/kg 05/17/16 20:13 86-30-605/13/16 10:133581
Pentachlorophenol ND ug/kg 05/17/16 20:13 87-86-505/13/16 10:1317901
Phenanthrene ND ug/kg 05/17/16 20:13 85-01-805/13/16 10:133581
Phenol ND ug/kg 05/17/16 20:1305/13/16 10:133581
Pyrene ND ug/kg 05/17/16 20:13 129-00-005/13/16 10:133581
1,2,4-Trichlorobenzene ND ug/kg 05/17/16 20:13 120-82-105/13/16 10:133581
2,4,5-Trichlorophenol ND ug/kg 05/17/16 20:13 95-95-405/13/16 10:133581
2,4,6-Trichlorophenol ND ug/kg 05/17/16 20:13 88-06-205/13/16 10:133581
Surrogates
Nitrobenzene-d5 (S)67 %05/17/16 20:13 4165-60-005/13/16 10:1323-110 1
2-Fluorobiphenyl (S)63 %05/17/16 20:13 321-60-805/13/16 10:1330-110 1
Terphenyl-d14 (S)81 %05/17/16 20:13 1718-51-005/13/16 10:1328-110 1
Phenol-d6 (S)69 %05/17/16 20:13 13127-88-305/13/16 10:1322-110 1
2-Fluorophenol (S)66 %05/17/16 20:13 367-12-405/13/16 10:1313-110 1
2,4,6-Tribromophenol (S)83 %05/17/16 20:13 118-79-605/13/16 10:1327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 05/13/16 23:09 67-64-176.1 1
Benzene ND ug/kg 05/13/16 23:09 71-43-23.8 1
Bromobenzene ND ug/kg 05/13/16 23:09 108-86-13.8 1
Bromochloromethane ND ug/kg 05/13/16 23:09 74-97-53.8 1
Bromodichloromethane ND ug/kg 05/13/16 23:09 75-27-43.8 1
Bromoform ND ug/kg 05/13/16 23:09 75-25-23.8 1
Bromomethane ND ug/kg 05/13/16 23:09 74-83-97.6 1
2-Butanone (MEK)ND ug/kg 05/13/16 23:09 78-93-376.1 1
n-Butylbenzene ND ug/kg 05/13/16 23:09 104-51-83.8 1
sec-Butylbenzene ND ug/kg 05/13/16 23:09 135-98-83.8 1
tert-Butylbenzene ND ug/kg 05/13/16 23:09 98-06-63.8 1
Carbon tetrachloride ND ug/kg 05/13/16 23:09 56-23-53.8 1
Chlorobenzene ND ug/kg 05/13/16 23:09 108-90-73.8 1
Chloroethane ND ug/kg 05/13/16 23:09 75-00-37.6 1
Chloroform ND ug/kg 05/13/16 23:09 67-66-33.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-5 Lab ID: 92297335011 Collected: 05/11/16 11:47 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 05/13/16 23:09 74-87-3 M17.6 1
2-Chlorotoluene ND ug/kg 05/13/16 23:09 95-49-83.8 1
4-Chlorotoluene ND ug/kg 05/13/16 23:09 106-43-43.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/13/16 23:09 96-12-83.8 1
Dibromochloromethane ND ug/kg 05/13/16 23:09 124-48-13.8 1
1,2-Dibromoethane (EDB)ND ug/kg 05/13/16 23:09 106-93-43.8 1
Dibromomethane ND ug/kg 05/13/16 23:09 74-95-33.8 1
1,2-Dichlorobenzene ND ug/kg 05/13/16 23:09 95-50-13.8 1
1,3-Dichlorobenzene ND ug/kg 05/13/16 23:09 541-73-13.8 1
1,4-Dichlorobenzene ND ug/kg 05/13/16 23:09 106-46-73.8 1
Dichlorodifluoromethane ND ug/kg 05/13/16 23:09 75-71-8 M17.6 1
1,1-Dichloroethane ND ug/kg 05/13/16 23:09 75-34-33.8 1
1,2-Dichloroethane ND ug/kg 05/13/16 23:09 107-06-23.8 1
1,1-Dichloroethene ND ug/kg 05/13/16 23:09 75-35-43.8 1
cis-1,2-Dichloroethene ND ug/kg 05/13/16 23:09 156-59-23.8 1
trans-1,2-Dichloroethene ND ug/kg 05/13/16 23:09 156-60-53.8 1
1,2-Dichloropropane ND ug/kg 05/13/16 23:09 78-87-53.8 1
1,3-Dichloropropane ND ug/kg 05/13/16 23:09 142-28-93.8 1
2,2-Dichloropropane ND ug/kg 05/13/16 23:09 594-20-73.8 1
1,1-Dichloropropene ND ug/kg 05/13/16 23:09 563-58-63.8 1
cis-1,3-Dichloropropene ND ug/kg 05/13/16 23:09 10061-01-53.8 1
trans-1,3-Dichloropropene ND ug/kg 05/13/16 23:09 10061-02-6 M13.8 1
Diisopropyl ether ND ug/kg 05/13/16 23:09 108-20-33.8 1
Ethylbenzene ND ug/kg 05/13/16 23:09 100-41-43.8 1
Hexachloro-1,3-butadiene ND ug/kg 05/13/16 23:09 87-68-33.8 1
2-Hexanone ND ug/kg 05/13/16 23:09 591-78-638.1 1
Isopropylbenzene (Cumene)ND ug/kg 05/13/16 23:09 98-82-83.8 1
p-Isopropyltoluene ND ug/kg 05/13/16 23:09 99-87-63.8 1
Methylene Chloride ND ug/kg 05/13/16 23:09 75-09-2 M115.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/13/16 23:09 108-10-138.1 1
Methyl-tert-butyl ether ND ug/kg 05/13/16 23:09 1634-04-43.8 1
Naphthalene ND ug/kg 05/13/16 23:09 91-20-33.8 1
n-Propylbenzene ND ug/kg 05/13/16 23:09 103-65-13.8 1
Styrene ND ug/kg 05/13/16 23:09 100-42-53.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/13/16 23:09 630-20-63.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/13/16 23:09 79-34-53.8 1
Tetrachloroethene ND ug/kg 05/13/16 23:09 127-18-43.8 1
Toluene ND ug/kg 05/13/16 23:09 108-88-33.8 1
1,2,3-Trichlorobenzene ND ug/kg 05/13/16 23:09 87-61-63.8 1
1,2,4-Trichlorobenzene ND ug/kg 05/13/16 23:09 120-82-1 M13.8 1
1,1,1-Trichloroethane ND ug/kg 05/13/16 23:09 71-55-63.8 1
1,1,2-Trichloroethane ND ug/kg 05/13/16 23:09 79-00-53.8 1
Trichloroethene ND ug/kg 05/13/16 23:09 79-01-63.8 1
Trichlorofluoromethane ND ug/kg 05/13/16 23:09 75-69-43.8 1
1,2,3-Trichloropropane ND ug/kg 05/13/16 23:09 96-18-43.8 1
1,2,4-Trimethylbenzene ND ug/kg 05/13/16 23:09 95-63-63.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 41 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-5 Lab ID: 92297335011 Collected: 05/11/16 11:47 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 05/13/16 23:09 108-67-83.8 1
Vinyl acetate ND ug/kg 05/13/16 23:09 108-05-438.1 1
Vinyl chloride ND ug/kg 05/13/16 23:09 75-01-4 M17.6 1
Xylene (Total)ND ug/kg 05/13/16 23:09 1330-20-77.6 1
m&p-Xylene ND ug/kg 05/13/16 23:09 179601-23-17.6 1
o-Xylene ND ug/kg 05/13/16 23:09 95-47-63.8 1
Surrogates
Toluene-d8 (S)99 %05/13/16 23:09 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %05/13/16 23:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %05/13/16 23:09 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 7.9 %05/13/16 07:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-6 Lab ID: 92297335012 Collected: 05/11/16 11:52 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/18/16 15:33 83-32-905/13/16 10:133591
Acenaphthylene ND ug/kg 05/18/16 15:33 208-96-805/13/16 10:133591
Aniline ND ug/kg 05/18/16 15:33 62-53-305/13/16 10:133591
Anthracene ND ug/kg 05/18/16 15:33 120-12-705/13/16 10:133591
Benzo(a)anthracene ND ug/kg 05/18/16 15:33 56-55-305/13/16 10:133591
Benzo(a)pyrene ND ug/kg 05/18/16 15:33 50-32-805/13/16 10:133591
Benzo(b)fluoranthene ND ug/kg 05/18/16 15:33 205-99-205/13/16 10:133591
Benzo(g,h,i)perylene ND ug/kg 05/18/16 15:33 191-24-205/13/16 10:133591
Benzo(k)fluoranthene ND ug/kg 05/18/16 15:33 207-08-905/13/16 10:133591
Benzoic Acid ND ug/kg 05/18/16 15:33 65-85-005/13/16 10:1317901
Benzyl alcohol ND ug/kg 05/18/16 15:33 100-51-605/13/16 10:137181
4-Bromophenylphenyl ether ND ug/kg 05/18/16 15:33 101-55-305/13/16 10:133591
Butylbenzylphthalate ND ug/kg 05/18/16 15:33 85-68-705/13/16 10:133591
4-Chloro-3-methylphenol ND ug/kg 05/18/16 15:33 59-50-705/13/16 10:137181
4-Chloroaniline ND ug/kg 05/18/16 15:33 106-47-805/13/16 10:1317901
bis(2-Chloroethoxy)methane ND ug/kg 05/18/16 15:33 111-91-105/13/16 10:133591
bis(2-Chloroethyl) ether ND ug/kg 05/18/16 15:33 111-44-405/13/16 10:133591
bis(2-Chloroisopropyl) ether ND ug/kg 05/18/16 15:33 108-60-105/13/16 10:133591
2-Chloronaphthalene ND ug/kg 05/18/16 15:33 91-58-705/13/16 10:133591
2-Chlorophenol ND ug/kg 05/18/16 15:33 95-57-805/13/16 10:133591
4-Chlorophenylphenyl ether ND ug/kg 05/18/16 15:33 7005-72-305/13/16 10:133591
Chrysene ND ug/kg 05/18/16 15:33 218-01-905/13/16 10:133591
Dibenz(a,h)anthracene ND ug/kg 05/18/16 15:33 53-70-305/13/16 10:133591
Dibenzofuran ND ug/kg 05/18/16 15:33 132-64-905/13/16 10:133591
1,2-Dichlorobenzene ND ug/kg 05/18/16 15:33 95-50-105/13/16 10:133591
1,3-Dichlorobenzene ND ug/kg 05/18/16 15:33 541-73-105/13/16 10:133591
1,4-Dichlorobenzene ND ug/kg 05/18/16 15:33 106-46-705/13/16 10:133591
3,3'-Dichlorobenzidine ND ug/kg 05/18/16 15:33 91-94-105/13/16 10:1317901
2,4-Dichlorophenol ND ug/kg 05/18/16 15:33 120-83-205/13/16 10:133591
Diethylphthalate ND ug/kg 05/18/16 15:33 84-66-205/13/16 10:133591
2,4-Dimethylphenol ND ug/kg 05/18/16 15:33 105-67-905/13/16 10:133591
Dimethylphthalate ND ug/kg 05/18/16 15:33 131-11-305/13/16 10:133591
Di-n-butylphthalate ND ug/kg 05/18/16 15:33 84-74-205/13/16 10:133591
4,6-Dinitro-2-methylphenol ND ug/kg 05/18/16 15:33 534-52-105/13/16 10:137181
2,4-Dinitrophenol ND ug/kg 05/18/16 15:33 51-28-505/13/16 10:1317901
2,4-Dinitrotoluene ND ug/kg 05/18/16 15:33 121-14-205/13/16 10:133591
2,6-Dinitrotoluene ND ug/kg 05/18/16 15:33 606-20-205/13/16 10:133591
Di-n-octylphthalate ND ug/kg 05/18/16 15:33 117-84-005/13/16 10:133591
bis(2-Ethylhexyl)phthalate ND ug/kg 05/18/16 15:33 117-81-705/13/16 10:133591
Fluoranthene ND ug/kg 05/18/16 15:33 206-44-005/13/16 10:133591
Fluorene ND ug/kg 05/18/16 15:33 86-73-705/13/16 10:133591
Hexachloro-1,3-butadiene ND ug/kg 05/18/16 15:33 87-68-305/13/16 10:133591
Hexachlorobenzene ND ug/kg 05/18/16 15:33 118-74-105/13/16 10:133591
Hexachlorocyclopentadiene ND ug/kg 05/18/16 15:33 77-47-405/13/16 10:133591
Hexachloroethane ND ug/kg 05/18/16 15:33 67-72-105/13/16 10:133591
Indeno(1,2,3-cd)pyrene ND ug/kg 05/18/16 15:33 193-39-505/13/16 10:133591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 43 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-6 Lab ID: 92297335012 Collected: 05/11/16 11:52 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 05/18/16 15:33 78-59-105/13/16 10:133591
1-Methylnaphthalene 362 ug/kg 05/18/16 15:33 90-12-005/13/16 10:133591
2-Methylnaphthalene 503 ug/kg 05/18/16 15:33 91-57-605/13/16 10:133591
2-Methylphenol(o-Cresol)ND ug/kg 05/18/16 15:33 95-48-705/13/16 10:133591
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/18/16 15:3305/13/16 10:133591
Naphthalene 659 ug/kg 05/18/16 15:33 91-20-305/13/16 10:133591
2-Nitroaniline ND ug/kg 05/18/16 15:33 88-74-405/13/16 10:1317901
3-Nitroaniline ND ug/kg 05/18/16 15:33 99-09-205/13/16 10:1317901
4-Nitroaniline ND ug/kg 05/18/16 15:33 100-01-605/13/16 10:137181
Nitrobenzene ND ug/kg 05/18/16 15:33 98-95-305/13/16 10:133591
2-Nitrophenol ND ug/kg 05/18/16 15:33 88-75-505/13/16 10:133591
4-Nitrophenol ND ug/kg 05/18/16 15:33 100-02-705/13/16 10:1317901
N-Nitrosodimethylamine ND ug/kg 05/18/16 15:33 62-75-905/13/16 10:133591
N-Nitroso-di-n-propylamine ND ug/kg 05/18/16 15:33 621-64-705/13/16 10:133591
N-Nitrosodiphenylamine ND ug/kg 05/18/16 15:33 86-30-605/13/16 10:133591
Pentachlorophenol ND ug/kg 05/18/16 15:33 87-86-505/13/16 10:1317901
Phenanthrene ND ug/kg 05/18/16 15:33 85-01-805/13/16 10:133591
Phenol ND ug/kg 05/18/16 15:3305/13/16 10:133591
Pyrene ND ug/kg 05/18/16 15:33 129-00-005/13/16 10:133591
1,2,4-Trichlorobenzene ND ug/kg 05/18/16 15:33 120-82-105/13/16 10:133591
2,4,5-Trichlorophenol ND ug/kg 05/18/16 15:33 95-95-405/13/16 10:133591
2,4,6-Trichlorophenol ND ug/kg 05/18/16 15:33 88-06-205/13/16 10:133591
Surrogates
Nitrobenzene-d5 (S)94 %05/18/16 15:33 4165-60-005/13/16 10:1323-110 1
2-Fluorobiphenyl (S)73 %05/18/16 15:33 321-60-805/13/16 10:1330-110 1
Terphenyl-d14 (S)77 %05/18/16 15:33 1718-51-005/13/16 10:1328-110 1
Phenol-d6 (S)86 %05/18/16 15:33 13127-88-305/13/16 10:1322-110 1
2-Fluorophenol (S)67 %05/18/16 15:33 367-12-405/13/16 10:1313-110 1
2,4,6-Tribromophenol (S)97 %05/18/16 15:33 118-79-605/13/16 10:1327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 05/15/16 19:58 67-64-1290025
Benzene ND ug/kg 05/15/16 19:58 71-43-214525
Bromobenzene ND ug/kg 05/15/16 19:58 108-86-114525
Bromochloromethane ND ug/kg 05/15/16 19:58 74-97-514525
Bromodichloromethane ND ug/kg 05/15/16 19:58 75-27-414525
Bromoform ND ug/kg 05/15/16 19:58 75-25-214525
Bromomethane ND ug/kg 05/15/16 19:58 74-83-929025
2-Butanone (MEK)ND ug/kg 05/15/16 19:58 78-93-3290025
n-Butylbenzene 203 ug/kg 05/15/16 19:58 104-51-814525
sec-Butylbenzene 187 ug/kg 05/15/16 19:58 135-98-814525
tert-Butylbenzene ND ug/kg 05/15/16 19:58 98-06-614525
Carbon tetrachloride ND ug/kg 05/15/16 19:58 56-23-514525
Chlorobenzene ND ug/kg 05/15/16 19:58 108-90-714525
Chloroethane ND ug/kg 05/15/16 19:58 75-00-329025
Chloroform ND ug/kg 05/15/16 19:58 67-66-314525
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-6 Lab ID: 92297335012 Collected: 05/11/16 11:52 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 05/15/16 19:58 74-87-329025
2-Chlorotoluene ND ug/kg 05/15/16 19:58 95-49-814525
4-Chlorotoluene ND ug/kg 05/15/16 19:58 106-43-414525
1,2-Dibromo-3-chloropropane ND ug/kg 05/15/16 19:58 96-12-814525
Dibromochloromethane ND ug/kg 05/15/16 19:58 124-48-114525
1,2-Dibromoethane (EDB)ND ug/kg 05/15/16 19:58 106-93-414525
Dibromomethane ND ug/kg 05/15/16 19:58 74-95-314525
1,2-Dichlorobenzene ND ug/kg 05/15/16 19:58 95-50-114525
1,3-Dichlorobenzene ND ug/kg 05/15/16 19:58 541-73-114525
1,4-Dichlorobenzene ND ug/kg 05/15/16 19:58 106-46-714525
Dichlorodifluoromethane ND ug/kg 05/15/16 19:58 75-71-829025
1,1-Dichloroethane ND ug/kg 05/15/16 19:58 75-34-314525
1,2-Dichloroethane ND ug/kg 05/15/16 19:58 107-06-214525
1,1-Dichloroethene ND ug/kg 05/15/16 19:58 75-35-414525
cis-1,2-Dichloroethene ND ug/kg 05/15/16 19:58 156-59-214525
trans-1,2-Dichloroethene ND ug/kg 05/15/16 19:58 156-60-514525
1,2-Dichloropropane ND ug/kg 05/15/16 19:58 78-87-514525
1,3-Dichloropropane ND ug/kg 05/15/16 19:58 142-28-914525
2,2-Dichloropropane ND ug/kg 05/15/16 19:58 594-20-714525
1,1-Dichloropropene ND ug/kg 05/15/16 19:58 563-58-614525
cis-1,3-Dichloropropene ND ug/kg 05/15/16 19:58 10061-01-514525
trans-1,3-Dichloropropene ND ug/kg 05/15/16 19:58 10061-02-614525
Diisopropyl ether ND ug/kg 05/15/16 19:58 108-20-314525
Ethylbenzene ND ug/kg 05/15/16 19:58 100-41-414525
Hexachloro-1,3-butadiene ND ug/kg 05/15/16 19:58 87-68-314525
2-Hexanone ND ug/kg 05/15/16 19:58 591-78-6145025
Isopropylbenzene (Cumene)ND ug/kg 05/15/16 19:58 98-82-814525
p-Isopropyltoluene 213 ug/kg 05/15/16 19:58 99-87-614525
Methylene Chloride ND ug/kg 05/15/16 19:58 75-09-258025
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/15/16 19:58 108-10-1145025
Methyl-tert-butyl ether ND ug/kg 05/15/16 19:58 1634-04-414525
Naphthalene ND ug/kg 05/15/16 19:58 91-20-314525
n-Propylbenzene ND ug/kg 05/15/16 19:58 103-65-114525
Styrene ND ug/kg 05/15/16 19:58 100-42-514525
1,1,1,2-Tetrachloroethane ND ug/kg 05/15/16 19:58 630-20-614525
1,1,2,2-Tetrachloroethane ND ug/kg 05/15/16 19:58 79-34-514525
Tetrachloroethene ND ug/kg 05/15/16 19:58 127-18-414525
Toluene ND ug/kg 05/15/16 19:58 108-88-314525
1,2,3-Trichlorobenzene ND ug/kg 05/15/16 19:58 87-61-614525
1,2,4-Trichlorobenzene ND ug/kg 05/15/16 19:58 120-82-114525
1,1,1-Trichloroethane ND ug/kg 05/15/16 19:58 71-55-614525
1,1,2-Trichloroethane ND ug/kg 05/15/16 19:58 79-00-514525
Trichloroethene ND ug/kg 05/15/16 19:58 79-01-614525
Trichlorofluoromethane ND ug/kg 05/15/16 19:58 75-69-414525
1,2,3-Trichloropropane ND ug/kg 05/15/16 19:58 96-18-414525
1,2,4-Trimethylbenzene 937 ug/kg 05/15/16 19:58 95-63-614525
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Sample: SB-6 Lab ID: 92297335012 Collected: 05/11/16 11:52 Received: 05/12/16 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene 248 ug/kg 05/15/16 19:58 108-67-814525
Vinyl acetate ND ug/kg 05/15/16 19:58 108-05-4145025
Vinyl chloride ND ug/kg 05/15/16 19:58 75-01-429025
Xylene (Total)ND ug/kg 05/15/16 19:58 1330-20-729025
m&p-Xylene ND ug/kg 05/15/16 19:58 179601-23-129025
o-Xylene ND ug/kg 05/15/16 19:58 95-47-614525
Surrogates
Toluene-d8 (S)98 %05/15/16 19:58 2037-26-5 D370-130 25
4-Bromofluorobenzene (S)96 %05/15/16 19:58 460-00-470-130 25
1,2-Dichloroethane-d4 (S)100 %05/15/16 19:58 17060-07-070-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.1 %05/13/16 07:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36854
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92297335001, 92297335002, 92297335003, 92297335004, 92297335006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734319
Associated Lab Samples:92297335001, 92297335002, 92297335003, 92297335004, 92297335006
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/16/16 03:49
1,1,1-Trichloroethane ug/L ND 1.0 05/16/16 03:49
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/16/16 03:49
1,1,2-Trichloroethane ug/L ND 1.0 05/16/16 03:49
1,1-Dichloroethane ug/L ND 1.0 05/16/16 03:49
1,1-Dichloroethene ug/L ND 1.0 05/16/16 03:49
1,1-Dichloropropene ug/L ND 1.0 05/16/16 03:49
1,2,3-Trichlorobenzene ug/L ND 1.0 05/16/16 03:49
1,2,3-Trichloropropane ug/L ND 1.0 05/16/16 03:49
1,2,4-Trichlorobenzene ug/L ND 1.0 05/16/16 03:49
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/16/16 03:49
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/16/16 03:49
1,2-Dichlorobenzene ug/L ND 1.0 05/16/16 03:49
1,2-Dichloroethane ug/L ND 1.0 05/16/16 03:49
1,2-Dichloropropane ug/L ND 1.0 05/16/16 03:49
1,3-Dichlorobenzene ug/L ND 1.0 05/16/16 03:49
1,3-Dichloropropane ug/L ND 1.0 05/16/16 03:49
1,4-Dichlorobenzene ug/L ND 1.0 05/16/16 03:49
2,2-Dichloropropane ug/L ND 1.0 05/16/16 03:49
2-Butanone (MEK)ug/L ND 5.0 05/16/16 03:49
2-Chlorotoluene ug/L ND 1.0 05/16/16 03:49
2-Hexanone ug/L ND 5.0 05/16/16 03:49
4-Chlorotoluene ug/L ND 1.0 05/16/16 03:49
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/16/16 03:49
Acetone ug/L ND 25.0 05/16/16 03:49
Benzene ug/L ND 1.0 05/16/16 03:49
Bromobenzene ug/L ND 1.0 05/16/16 03:49
Bromochloromethane ug/L ND 1.0 05/16/16 03:49
Bromodichloromethane ug/L ND 1.0 05/16/16 03:49
Bromoform ug/L ND 1.0 05/16/16 03:49
Bromomethane ug/L ND 2.0 05/16/16 03:49
Carbon tetrachloride ug/L ND 1.0 05/16/16 03:49
Chlorobenzene ug/L ND 1.0 05/16/16 03:49
Chloroethane ug/L ND 1.0 05/16/16 03:49
Chloroform ug/L ND 1.0 05/16/16 03:49
Chloromethane ug/L ND 1.0 05/16/16 03:49
cis-1,2-Dichloroethene ug/L ND 1.0 05/16/16 03:49
cis-1,3-Dichloropropene ug/L ND 1.0 05/16/16 03:49
Dibromochloromethane ug/L ND 1.0 05/16/16 03:49
Dibromomethane ug/L ND 1.0 05/16/16 03:49
Dichlorodifluoromethane ug/L ND 1.0 05/16/16 03:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734319
Associated Lab Samples:92297335001, 92297335002, 92297335003, 92297335004, 92297335006
Matrix: Water
Analyzed
Diisopropyl ether ug/L ND 1.0 05/16/16 03:49
Ethylbenzene ug/L ND 1.0 05/16/16 03:49
Hexachloro-1,3-butadiene ug/L ND 1.0 05/16/16 03:49
m&p-Xylene ug/L ND 2.0 05/16/16 03:49
Methyl-tert-butyl ether ug/L ND 1.0 05/16/16 03:49
Methylene Chloride ug/L ND 2.0 05/16/16 03:49
Naphthalene ug/L ND 1.0 05/16/16 03:49
o-Xylene ug/L ND 1.0 05/16/16 03:49
p-Isopropyltoluene ug/L ND 1.0 05/16/16 03:49
Styrene ug/L ND 1.0 05/16/16 03:49
Tetrachloroethene ug/L ND 1.0 05/16/16 03:49
Toluene ug/L ND 1.0 05/16/16 03:49
trans-1,2-Dichloroethene ug/L ND 1.0 05/16/16 03:49
trans-1,3-Dichloropropene ug/L ND 1.0 05/16/16 03:49
Trichloroethene ug/L ND 1.0 05/16/16 03:49
Trichlorofluoromethane ug/L ND 1.0 05/16/16 03:49
Vinyl acetate ug/L ND 2.0 05/16/16 03:49
Vinyl chloride ug/L ND 1.0 05/16/16 03:49
Xylene (Total)ug/L ND 2.0 05/16/16 03:49
1,2-Dichloroethane-d4 (S)%97 70-130 05/16/16 03:49
4-Bromofluorobenzene (S)%100 70-130 05/16/16 03:49
Toluene-d8 (S)%100 70-130 05/16/16 03:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734320LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.650 101 70-130
1,1,1-Trichloroethane ug/L 50.250 100 70-130
1,1,2,2-Tetrachloroethane ug/L 48.350 97 70-130
1,1,2-Trichloroethane ug/L 47.650 95 70-130
1,1-Dichloroethane ug/L 47.650 95 70-130
1,1-Dichloroethene ug/L 50.750 101 70-132
1,1-Dichloropropene ug/L 49.050 98 70-130
1,2,3-Trichlorobenzene ug/L 51.850 104 70-135
1,2,3-Trichloropropane ug/L 49.450 99 70-130
1,2,4-Trichlorobenzene ug/L 51.250 102 70-134
1,2-Dibromo-3-chloropropane ug/L 50.250 100 70-130
1,2-Dibromoethane (EDB)ug/L 52.550 105 70-130
1,2-Dichlorobenzene ug/L 50.450 101 70-130
1,2-Dichloroethane ug/L 45.850 92 70-130
1,2-Dichloropropane ug/L 46.850 94 70-130
1,3-Dichlorobenzene ug/L 49.250 98 70-130
1,3-Dichloropropane ug/L 46.850 94 70-130
1,4-Dichlorobenzene ug/L 49.850 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734320LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 44.550 89 58-145
2-Butanone (MEK)ug/L 97.4100 97 70-145
2-Chlorotoluene ug/L 50.150 100 70-130
2-Hexanone ug/L 99.3100 99 70-144
4-Chlorotoluene ug/L 49.850 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 98.2100 98 70-140
Acetone ug/L 95.0100 95 50-175
Benzene ug/L 48.050 96 70-130
Bromobenzene ug/L 49.250 98 70-130
Bromochloromethane ug/L 49.550 99 70-130
Bromodichloromethane ug/L 48.650 97 70-130
Bromoform ug/L 51.350 103 70-130
Bromomethane ug/L 42.650 85 54-130
Carbon tetrachloride ug/L 53.250 106 70-132
Chlorobenzene ug/L 51.050 102 70-130
Chloroethane ug/L 47.150 94 64-134
Chloroform ug/L 48.250 96 70-130
Chloromethane ug/L 42.750 85 64-130
cis-1,2-Dichloroethene ug/L 48.150 96 70-131
cis-1,3-Dichloropropene ug/L 47.750 95 70-130
Dibromochloromethane ug/L 50.250 100 70-130
Dibromomethane ug/L 49.050 98 70-131
Dichlorodifluoromethane ug/L 44.850 90 56-130
Diisopropyl ether ug/L 46.950 94 70-130
Ethylbenzene ug/L 49.250 98 70-130
Hexachloro-1,3-butadiene ug/L 52.650 105 70-130
m&p-Xylene ug/L 98.3100 98 70-130
Methyl-tert-butyl ether ug/L 49.350 99 70-130
Methylene Chloride ug/L 46.950 94 63-130
Naphthalene ug/L 50.350 101 70-138
o-Xylene ug/L 48.850 98 70-130
p-Isopropyltoluene ug/L 48.650 97 70-130
Styrene ug/L 51.750 103 70-130
Tetrachloroethene ug/L 47.350 95 70-130
Toluene ug/L 48.550 97 70-130
trans-1,2-Dichloroethene ug/L 51.150 102 70-130
trans-1,3-Dichloropropene ug/L 47.350 95 70-132
Trichloroethene ug/L 48.550 97 70-130
Trichlorofluoromethane ug/L 49.650 99 62-133
Vinyl acetate ug/L 107100 107 66-157
Vinyl chloride ug/L 48.550 97 50-150
Xylene (Total)ug/L 147150 98 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734321MATRIX SPIKE SAMPLE:
MSSpike
Result
92297635010
1,1,1,2-Tetrachloroethane ug/L 20.620 103 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.620 98 70-130ND
1,1,2-Trichloroethane ug/L 20.620 103 70-130ND
1,1-Dichloroethane ug/L 21.320 106 70-130ND
1,1-Dichloroethene ug/L 23.420 117 70-166ND
1,1-Dichloropropene ug/L 21.820 109 70-130ND
1,2,3-Trichlorobenzene ug/L 20.820 104 70-130ND
1,2,3-Trichloropropane ug/L 21.320 106 70-130ND
1,2,4-Trichlorobenzene ug/L 20.720 104 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.720 109 70-130ND
1,2-Dichlorobenzene ug/L 21.320 107 70-130ND
1,2-Dichloroethane ug/L 20.020 100 70-130ND
1,2-Dichloropropane ug/L 20.820 104 70-130ND
1,3-Dichlorobenzene ug/L 21.520 107 70-130ND
1,3-Dichloropropane ug/L 19.820 99 70-130ND
1,4-Dichlorobenzene ug/L 21.120 105 70-130ND
2,2-Dichloropropane ug/L 17.220 86 70-130ND
2-Butanone (MEK)ug/L 42.040 105 70-130ND
2-Chlorotoluene ug/L 21.720 109 70-130ND
2-Hexanone ug/L 42.140 105 70-130ND
4-Chlorotoluene ug/L 21.320 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.440 106 70-130ND
Acetone ug/L 44.140 110 70-130ND
Benzene ug/L 29.220 110 70-1487.3
Bromobenzene ug/L 21.220 106 70-130ND
Bromochloromethane ug/L 21.620 108 70-130ND
Bromodichloromethane ug/L 21.120 106 70-130ND
Bromoform ug/L 20.020 100 70-130ND
Bromomethane ug/L 16.020 80 70-130ND
Carbon tetrachloride ug/L 24.220 121 70-130ND
Chlorobenzene ug/L 22.220 111 70-146ND
Chloroethane ug/L 21.820 109 70-130ND
Chloroform ug/L 21.520 107 70-130ND
Chloromethane ug/L 18.920 94 70-130ND
cis-1,2-Dichloroethene ug/L 21.320 106 70-130ND
cis-1,3-Dichloropropene ug/L 20.320 101 70-130ND
Dibromochloromethane ug/L 20.020 100 70-130ND
Dibromomethane ug/L 21.020 105 70-130ND
Dichlorodifluoromethane ug/L 21.820 109 70-130ND
Diisopropyl ether ug/L 20.720 104 70-130ND
Ethylbenzene ug/L 21.320 106 70-130ND
Hexachloro-1,3-butadiene ug/L 21.720 108 70-130ND
m&p-Xylene ug/L 42.340 106 70-130ND
Methyl-tert-butyl ether ug/L 21.220 106 70-130ND
Methylene Chloride ug/L 19.620 98 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734321MATRIX SPIKE SAMPLE:
MSSpike
Result
92297635010
Naphthalene ug/L 25.820 106 70-1304.7
o-Xylene ug/L 23.520 104 70-1302.7
p-Isopropyltoluene ug/L 21.620 108 70-130ND
Styrene ug/L 21.420 107 70-130ND
Tetrachloroethene ug/L 20.120 100 70-130ND
Toluene ug/L 22.220 110 70-155ND
trans-1,2-Dichloroethene ug/L 22.220 111 70-130ND
trans-1,3-Dichloropropene ug/L 19.720 98 70-130ND
Trichloroethene ug/L 21.720 108 69-151ND
Trichlorofluoromethane ug/L 23.120 116 70-130ND
Vinyl acetate ug/L 34.440 86 70-130ND
Vinyl chloride ug/L 22.320 112 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297635015
1734322SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L .61J 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297635015
1734322SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%97 298
4-Bromofluorobenzene (S)%100 1102
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36861
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92297335005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734967
Associated Lab Samples:92297335005
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/16/16 16:36
1,1,1-Trichloroethane ug/L ND 1.0 05/16/16 16:36
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/16/16 16:36
1,1,2-Trichloroethane ug/L ND 1.0 05/16/16 16:36
1,1-Dichloroethane ug/L ND 1.0 05/16/16 16:36
1,1-Dichloroethene ug/L ND 1.0 05/16/16 16:36
1,1-Dichloropropene ug/L ND 1.0 05/16/16 16:36
1,2,3-Trichlorobenzene ug/L ND 1.0 05/16/16 16:36
1,2,3-Trichloropropane ug/L ND 1.0 05/16/16 16:36
1,2,4-Trichlorobenzene ug/L ND 1.0 05/16/16 16:36
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/16/16 16:36
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/16/16 16:36
1,2-Dichlorobenzene ug/L ND 1.0 05/16/16 16:36
1,2-Dichloroethane ug/L ND 1.0 05/16/16 16:36
1,2-Dichloropropane ug/L ND 1.0 05/16/16 16:36
1,3-Dichlorobenzene ug/L ND 1.0 05/16/16 16:36
1,3-Dichloropropane ug/L ND 1.0 05/16/16 16:36
1,4-Dichlorobenzene ug/L ND 1.0 05/16/16 16:36
2,2-Dichloropropane ug/L ND 1.0 05/16/16 16:36
2-Butanone (MEK)ug/L ND 5.0 05/16/16 16:36
2-Chlorotoluene ug/L ND 1.0 05/16/16 16:36
2-Hexanone ug/L ND 5.0 05/16/16 16:36
4-Chlorotoluene ug/L ND 1.0 05/16/16 16:36
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/16/16 16:36
Acetone ug/L ND 25.0 05/16/16 16:36
Benzene ug/L ND 1.0 05/16/16 16:36
Bromobenzene ug/L ND 1.0 05/16/16 16:36
Bromochloromethane ug/L ND 1.0 05/16/16 16:36
Bromodichloromethane ug/L ND 1.0 05/16/16 16:36
Bromoform ug/L ND 1.0 05/16/16 16:36
Bromomethane ug/L ND 2.0 05/16/16 16:36
Carbon tetrachloride ug/L ND 1.0 05/16/16 16:36
Chlorobenzene ug/L ND 1.0 05/16/16 16:36
Chloroethane ug/L ND 1.0 05/16/16 16:36
Chloroform ug/L ND 1.0 05/16/16 16:36
Chloromethane ug/L ND 1.0 05/16/16 16:36
cis-1,2-Dichloroethene ug/L ND 1.0 05/16/16 16:36
cis-1,3-Dichloropropene ug/L ND 1.0 05/16/16 16:36
Dibromochloromethane ug/L ND 1.0 05/16/16 16:36
Dibromomethane ug/L ND 1.0 05/16/16 16:36
Dichlorodifluoromethane ug/L ND 1.0 05/16/16 16:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734967
Associated Lab Samples:92297335005
Matrix: Water
Analyzed
Diisopropyl ether ug/L ND 1.0 05/16/16 16:36
Ethylbenzene ug/L ND 1.0 05/16/16 16:36
Hexachloro-1,3-butadiene ug/L ND 1.0 05/16/16 16:36
m&p-Xylene ug/L ND 2.0 05/16/16 16:36
Methyl-tert-butyl ether ug/L ND 1.0 05/16/16 16:36
Methylene Chloride ug/L ND 2.0 05/16/16 16:36
Naphthalene ug/L ND 1.0 05/16/16 16:36
o-Xylene ug/L ND 1.0 05/16/16 16:36
p-Isopropyltoluene ug/L ND 1.0 05/16/16 16:36
Styrene ug/L ND 1.0 05/16/16 16:36
Tetrachloroethene ug/L ND 1.0 05/16/16 16:36
Toluene ug/L ND 1.0 05/16/16 16:36
trans-1,2-Dichloroethene ug/L ND 1.0 05/16/16 16:36
trans-1,3-Dichloropropene ug/L ND 1.0 05/16/16 16:36
Trichloroethene ug/L ND 1.0 05/16/16 16:36
Trichlorofluoromethane ug/L ND 1.0 05/16/16 16:36
Vinyl acetate ug/L ND 2.0 05/16/16 16:36
Vinyl chloride ug/L ND 1.0 05/16/16 16:36
Xylene (Total)ug/L ND 2.0 05/16/16 16:36
1,2-Dichloroethane-d4 (S)%99 70-130 05/16/16 16:36
4-Bromofluorobenzene (S)%101 70-130 05/16/16 16:36
Toluene-d8 (S)%101 70-130 05/16/16 16:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734968LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.750 95 70-130
1,1,1-Trichloroethane ug/L 48.650 97 70-130
1,1,2,2-Tetrachloroethane ug/L 45.450 91 70-130
1,1,2-Trichloroethane ug/L 46.750 93 70-130
1,1-Dichloroethane ug/L 46.250 92 70-130
1,1-Dichloroethene ug/L 51.550 103 70-132
1,1-Dichloropropene ug/L 49.150 98 70-130
1,2,3-Trichlorobenzene ug/L 50.350 101 70-135
1,2,3-Trichloropropane ug/L 44.950 90 70-130
1,2,4-Trichlorobenzene ug/L 52.050 104 70-134
1,2-Dibromo-3-chloropropane ug/L 47.250 94 70-130
1,2-Dibromoethane (EDB)ug/L 50.450 101 70-130
1,2-Dichlorobenzene ug/L 49.050 98 70-130
1,2-Dichloroethane ug/L 45.350 91 70-130
1,2-Dichloropropane ug/L 46.950 94 70-130
1,3-Dichlorobenzene ug/L 49.750 99 70-130
1,3-Dichloropropane ug/L 45.150 90 70-130
1,4-Dichlorobenzene ug/L 49.050 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734968LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 50.850 102 58-145
2-Butanone (MEK)ug/L 93.2100 93 70-145
2-Chlorotoluene ug/L 50.350 101 70-130
2-Hexanone ug/L 92.6100 93 70-144
4-Chlorotoluene ug/L 49.150 98 70-130
4-Methyl-2-pentanone (MIBK)ug/L 96.0100 96 70-140
Acetone ug/L 90.8100 91 50-175
Benzene ug/L 47.650 95 70-130
Bromobenzene ug/L 48.850 98 70-130
Bromochloromethane ug/L 49.550 99 70-130
Bromodichloromethane ug/L 48.550 97 70-130
Bromoform ug/L 48.750 97 70-130
Bromomethane ug/L 40.450 81 54-130
Carbon tetrachloride ug/L 53.150 106 70-132
Chlorobenzene ug/L 49.650 99 70-130
Chloroethane ug/L 49.350 99 64-134
Chloroform ug/L 48.250 96 70-130
Chloromethane ug/L 41.250 82 64-130
cis-1,2-Dichloroethene ug/L 48.250 96 70-131
cis-1,3-Dichloropropene ug/L 48.750 97 70-130
Dibromochloromethane ug/L 47.950 96 70-130
Dibromomethane ug/L 47.750 95 70-131
Dichlorodifluoromethane ug/L 49.550 99 56-130
Diisopropyl ether ug/L 47.350 95 70-130
Ethylbenzene ug/L 48.250 96 70-130
Hexachloro-1,3-butadiene ug/L 53.450 107 70-130
m&p-Xylene ug/L 96.1100 96 70-130
Methyl-tert-butyl ether ug/L 48.750 97 70-130
Methylene Chloride ug/L 46.650 93 63-130
Naphthalene ug/L 49.650 99 70-138
o-Xylene ug/L 47.450 95 70-130
p-Isopropyltoluene ug/L 49.850 100 70-130
Styrene ug/L 49.950 100 70-130
Tetrachloroethene ug/L 46.850 94 70-130
Toluene ug/L 48.950 98 70-130
trans-1,2-Dichloroethene ug/L 50.650 101 70-130
trans-1,3-Dichloropropene ug/L 48.250 96 70-132
Trichloroethene ug/L 47.450 95 70-130
Trichlorofluoromethane ug/L 51.950 104 62-133
Vinyl acetate ug/L 106100 106 66-157
Vinyl chloride ug/L 49.350 99 50-150
Xylene (Total)ug/L 144150 96 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734969MATRIX SPIKE SAMPLE:
MSSpike
Result
92297512010
1,1,1,2-Tetrachloroethane ug/L 21302000 106 70-130ND
1,1,1-Trichloroethane ug/L 22502000 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19202000 96 70-130ND
1,1,2-Trichloroethane ug/L 20502000 102 70-130ND
1,1-Dichloroethane ug/L 21002000 105 70-130ND
1,1-Dichloroethene ug/L 22902000 115 70-166ND
1,1-Dichloropropene ug/L 22402000 112 70-130ND
1,2,3-Trichlorobenzene ug/L 21002000 105 70-130ND
1,2,3-Trichloropropane ug/L 20102000 100 70-130ND
1,2,4-Trichlorobenzene ug/L 21202000 106 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19702000 98 70-130ND
1,2-Dibromoethane (EDB)ug/L 21902000 109 70-130ND
1,2-Dichlorobenzene ug/L 21102000 105 70-130ND
1,2-Dichloroethane ug/L 19902000 99 70-130ND
1,2-Dichloropropane ug/L 19802000 99 70-130ND
1,3-Dichlorobenzene ug/L 21502000 108 70-130ND
1,3-Dichloropropane ug/L 19702000 99 70-130ND
1,4-Dichlorobenzene ug/L 21502000 107 70-130ND
2,2-Dichloropropane ug/L 20202000 101 70-130ND
2-Butanone (MEK)ug/L 39804000 100 70-130ND
2-Chlorotoluene ug/L 22902000 114 70-130ND
2-Hexanone ug/L 40704000 100 70-130ND
4-Chlorotoluene ug/L 21702000 108 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40904000 102 70-130ND
Acetone ug/L 37204000 93 70-130ND
Benzene ug/L 30902000 105 70-1480.99 mg/L
Bromobenzene ug/L 21702000 108 70-130ND
Bromochloromethane ug/L 21902000 110 70-130ND
Bromodichloromethane ug/L 20302000 101 70-130ND
Bromoform ug/L 20302000 101 70-130ND
Bromomethane ug/L 17202000 86 70-130ND
Carbon tetrachloride ug/L 23502000 118 70-130ND
Chlorobenzene ug/L 22202000 111 70-146ND
Chloroethane ug/L 21802000 109 70-130ND
Chloroform ug/L 21602000 108 70-130ND
Chloromethane ug/L 19702000 98 70-130ND
cis-1,2-Dichloroethene ug/L 21202000 106 70-130ND
cis-1,3-Dichloropropene ug/L 20802000 104 70-130ND
Dibromochloromethane ug/L 20302000 101 70-130ND
Dibromomethane ug/L 21402000 107 70-130ND
Dichlorodifluoromethane ug/L 21102000 106 70-130ND
Diisopropyl ether ug/L 20602000 103 70-130ND
Ethylbenzene ug/L 38902000 107 70-1301.8 mg/L
Hexachloro-1,3-butadiene ug/L 22502000 113 70-130ND
m&p-Xylene ug/L 128004000 103 70-1308.7 mg/L
Methyl-tert-butyl ether ug/L 21002000 105 70-130ND
Methylene Chloride ug/L 20402000 102 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734969MATRIX SPIKE SAMPLE:
MSSpike
Result
92297512010
Naphthalene ug/L 27802000 104 70-130693
o-Xylene ug/L 62102000 101 70-1304.2 mg/L
p-Isopropyltoluene ug/L 22202000 109 70-130ND
Styrene ug/L 22502000 112 70-130ND
Tetrachloroethene ug/L 20302000 102 70-130ND
Toluene ug/L 126002000 91 70-15510.8 mg/L
trans-1,2-Dichloroethene ug/L 22802000 114 70-130ND
trans-1,3-Dichloropropene ug/L 20002000 100 70-130ND
Trichloroethene ug/L 21102000 106 69-151ND
Trichlorofluoromethane ug/L 23302000 117 70-130ND
Vinyl acetate ug/L 44004000 110 70-130ND
Vinyl chloride ug/L 22102000 111 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297512020
1734970SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L 9860 3 3010.2 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297512020
1734970SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L 204 2 30200
Ethylbenzene ug/L 1290 3 301.3 mg/L
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L 3910 6 304.2 mg/L
Methyl-tert-butyl ether ug/L 1810 2 301.8 mg/L
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L 434 2 30424
o-Xylene ug/L 110 6 300.12 mg/L
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 1540 4 301.6 mg/L
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L 4020 6 304.3 mg/L
1,2-Dichloroethane-d4 (S)%98 098
4-Bromofluorobenzene (S)%99 3102
Toluene-d8 (S)%101 199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36811
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92297335007, 92297335008, 92297335009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1733738
Associated Lab Samples:92297335007, 92297335008, 92297335009
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.0 05/13/16 15:20
1,1,1-Trichloroethane ug/kg ND 4.0 05/13/16 15:20
1,1,2,2-Tetrachloroethane ug/kg ND 4.0 05/13/16 15:20
1,1,2-Trichloroethane ug/kg ND 4.0 05/13/16 15:20
1,1-Dichloroethane ug/kg ND 4.0 05/13/16 15:20
1,1-Dichloroethene ug/kg ND 4.0 05/13/16 15:20
1,1-Dichloropropene ug/kg ND 4.0 05/13/16 15:20
1,2,3-Trichlorobenzene ug/kg ND 4.0 05/13/16 15:20
1,2,3-Trichloropropane ug/kg ND 4.0 05/13/16 15:20
1,2,4-Trichlorobenzene ug/kg ND 4.0 05/13/16 15:20
1,2,4-Trimethylbenzene ug/kg ND 4.0 05/13/16 15:20
1,2-Dibromo-3-chloropropane ug/kg ND 4.0 05/13/16 15:20
1,2-Dibromoethane (EDB)ug/kg ND 4.0 05/13/16 15:20
1,2-Dichlorobenzene ug/kg ND 4.0 05/13/16 15:20
1,2-Dichloroethane ug/kg ND 4.0 05/13/16 15:20
1,2-Dichloropropane ug/kg ND 4.0 05/13/16 15:20
1,3,5-Trimethylbenzene ug/kg ND 4.0 05/13/16 15:20
1,3-Dichlorobenzene ug/kg ND 4.0 05/13/16 15:20
1,3-Dichloropropane ug/kg ND 4.0 05/13/16 15:20
1,4-Dichlorobenzene ug/kg ND 4.0 05/13/16 15:20
2,2-Dichloropropane ug/kg ND 4.0 05/13/16 15:20
2-Butanone (MEK)ug/kg ND 80.4 05/13/16 15:20
2-Chlorotoluene ug/kg ND 4.0 05/13/16 15:20
2-Hexanone ug/kg ND 40.2 05/13/16 15:20
4-Chlorotoluene ug/kg ND 4.0 05/13/16 15:20
4-Methyl-2-pentanone (MIBK)ug/kg ND 40.2 05/13/16 15:20
Acetone ug/kg ND 80.4 05/13/16 15:20
Benzene ug/kg ND 4.0 05/13/16 15:20
Bromobenzene ug/kg ND 4.0 05/13/16 15:20
Bromochloromethane ug/kg ND 4.0 05/13/16 15:20
Bromodichloromethane ug/kg ND 4.0 05/13/16 15:20
Bromoform ug/kg ND 4.0 05/13/16 15:20
Bromomethane ug/kg ND 8.0 05/13/16 15:20
Carbon tetrachloride ug/kg ND 4.0 05/13/16 15:20
Chlorobenzene ug/kg ND 4.0 05/13/16 15:20
Chloroethane ug/kg ND 8.0 05/13/16 15:20
Chloroform ug/kg ND 4.0 05/13/16 15:20
Chloromethane ug/kg ND 8.0 05/13/16 15:20
cis-1,2-Dichloroethene ug/kg ND 4.0 05/13/16 15:20
cis-1,3-Dichloropropene ug/kg ND 4.0 05/13/16 15:20
Dibromochloromethane ug/kg ND 4.0 05/13/16 15:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1733738
Associated Lab Samples:92297335007, 92297335008, 92297335009
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 4.0 05/13/16 15:20
Dichlorodifluoromethane ug/kg ND 8.0 05/13/16 15:20
Diisopropyl ether ug/kg ND 4.0 05/13/16 15:20
Ethylbenzene ug/kg ND 4.0 05/13/16 15:20
Hexachloro-1,3-butadiene ug/kg ND 4.0 05/13/16 15:20
Isopropylbenzene (Cumene)ug/kg ND 4.0 05/13/16 15:20
m&p-Xylene ug/kg ND 8.0 05/13/16 15:20
Methyl-tert-butyl ether ug/kg ND 4.0 05/13/16 15:20
Methylene Chloride ug/kg ND 16.1 05/13/16 15:20
n-Butylbenzene ug/kg ND 4.0 05/13/16 15:20
n-Propylbenzene ug/kg ND 4.0 05/13/16 15:20
Naphthalene ug/kg ND 4.0 05/13/16 15:20
o-Xylene ug/kg ND 4.0 05/13/16 15:20
p-Isopropyltoluene ug/kg ND 4.0 05/13/16 15:20
sec-Butylbenzene ug/kg ND 4.0 05/13/16 15:20
Styrene ug/kg ND 4.0 05/13/16 15:20
tert-Butylbenzene ug/kg ND 4.0 05/13/16 15:20
Tetrachloroethene ug/kg ND 4.0 05/13/16 15:20
Toluene ug/kg ND 4.0 05/13/16 15:20
trans-1,2-Dichloroethene ug/kg ND 4.0 05/13/16 15:20
trans-1,3-Dichloropropene ug/kg ND 4.0 05/13/16 15:20
Trichloroethene ug/kg ND 4.0 05/13/16 15:20
Trichlorofluoromethane ug/kg ND 4.0 05/13/16 15:20
Vinyl acetate ug/kg ND 40.2 05/13/16 15:20
Vinyl chloride ug/kg ND 8.0 05/13/16 15:20
Xylene (Total)ug/kg ND 8.0 05/13/16 15:20
1,2-Dichloroethane-d4 (S)%80 70-132 05/13/16 15:20
4-Bromofluorobenzene (S)%101 70-130 05/13/16 15:20
Toluene-d8 (S)%102 70-130 05/13/16 15:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733739LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 50.348.9 103 74-137
1,1,1-Trichloroethane ug/kg 46.048.9 94 67-140
1,1,2,2-Tetrachloroethane ug/kg 42.348.9 86 72-141
1,1,2-Trichloroethane ug/kg 45.848.9 94 78-138
1,1-Dichloroethane ug/kg 44.648.9 91 69-134
1,1-Dichloroethene ug/kg 44.948.9 92 67-138
1,1-Dichloropropene ug/kg 46.748.9 95 69-139
1,2,3-Trichlorobenzene ug/kg 48.148.9 98 70-146
1,2,3-Trichloropropane ug/kg 47.748.9 98 69-144
1,2,4-Trichlorobenzene ug/kg 46.748.9 96 68-148
1,2,4-Trimethylbenzene ug/kg 47.448.9 97 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733739LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 47.448.9 97 65-140
1,2-Dibromoethane (EDB)ug/kg 49.848.9 102 77-135
1,2-Dichlorobenzene ug/kg 47.448.9 97 77-141
1,2-Dichloroethane ug/kg 44.148.9 90 65-137
1,2-Dichloropropane ug/kg 47.348.9 97 72-136
1,3,5-Trimethylbenzene ug/kg 47.148.9 96 76-133
1,3-Dichlorobenzene ug/kg 47.748.9 98 74-138
1,3-Dichloropropane ug/kg 49.148.9 100 71-139
1,4-Dichlorobenzene ug/kg 48.048.9 98 76-138
2,2-Dichloropropane ug/kg 46.148.9 94 68-137
2-Butanone (MEK)ug/kg 92.4J97.8 94 58-147
2-Chlorotoluene ug/kg 46.448.9 95 73-139
2-Hexanone ug/kg 97.897.8 100 62-145
4-Chlorotoluene ug/kg 45.548.9 93 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 95.297.8 97 64-149
Acetone ug/kg 83.1J97.8 85 53-153
Benzene ug/kg 46.248.9 94 73-135
Bromobenzene ug/kg 47.948.9 98 75-133
Bromochloromethane ug/kg 44.948.9 92 73-134
Bromodichloromethane ug/kg 47.848.9 98 71-135
Bromoform ug/kg 48.248.9 99 66-141
Bromomethane ug/kg 46.7 F348.9 96 53-160
Carbon tetrachloride ug/kg 46.648.9 95 60-145
Chlorobenzene ug/kg 46.948.9 96 78-130
Chloroethane ug/kg 48.448.9 99 64-149
Chloroform ug/kg 45.648.9 93 70-134
Chloromethane ug/kg 43.748.9 89 52-150
cis-1,2-Dichloroethene ug/kg 44.448.9 91 70-133
cis-1,3-Dichloropropene ug/kg 49.348.9 101 68-134
Dibromochloromethane ug/kg 51.448.9 105 71-138
Dibromomethane ug/kg 44.348.9 90 74-130
Dichlorodifluoromethane ug/kg 41.848.9 85 40-160
Diisopropyl ether ug/kg 47.048.9 96 69-141
Ethylbenzene ug/kg 45.348.9 93 75-133
Hexachloro-1,3-butadiene ug/kg 44.748.9 91 68-143
Isopropylbenzene (Cumene)ug/kg 45.748.9 93 76-143
m&p-Xylene ug/kg 91.597.8 93 75-136
Methyl-tert-butyl ether ug/kg 44.548.9 91 68-144
Methylene Chloride ug/kg 42.848.9 88 45-154
n-Butylbenzene ug/kg 46.148.9 94 72-137
n-Propylbenzene ug/kg 44.948.9 92 76-136
Naphthalene ug/kg 47.448.9 97 68-151
o-Xylene ug/kg 44.848.9 92 76-141
p-Isopropyltoluene ug/kg 45.148.9 92 76-140
sec-Butylbenzene ug/kg 45.648.9 93 79-139
Styrene ug/kg 47.048.9 96 79-137
tert-Butylbenzene ug/kg 42.148.9 86 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733739LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 43.548.9 89 71-138
Toluene ug/kg 44.248.9 90 74-131
trans-1,2-Dichloroethene ug/kg 45.548.9 93 67-135
trans-1,3-Dichloropropene ug/kg 48.448.9 99 65-146
Trichloroethene ug/kg 50.348.9 103 67-135
Trichlorofluoromethane ug/kg 44.948.9 92 59-144
Vinyl acetate ug/kg 49.1 F397.8 50 40-160
Vinyl chloride ug/kg 44.848.9 92 56-141
Xylene (Total)ug/kg 136147 93 76-137
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734270MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335007
1,1,1,2-Tetrachloroethane ug/kg 17.619.2 92 70-130ND
1,1,1-Trichloroethane ug/kg 16.519.2 86 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 18.319.2 95 70-130ND
1,1,2-Trichloroethane ug/kg 16.219.2 85 70-130ND
1,1-Dichloroethane ug/kg 16.319.2 85 70-130ND
1,1-Dichloroethene ug/kg 14.619.2 76 49-180ND
1,1-Dichloropropene ug/kg 16.619.2 86 70-130ND
1,2,3-Trichlorobenzene ug/kg 16.419.2 85 70-130ND
1,2,3-Trichloropropane ug/kg 17.619.2 92 70-130ND
1,2,4-Trichlorobenzene ug/kg 16.019.2 83 70-130ND
1,2,4-Trimethylbenzene ug/kg 17.719.2 92 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 17.619.2 92 70-130ND
1,2-Dibromoethane (EDB)ug/kg 18.019.2 94 70-130ND
1,2-Dichlorobenzene ug/kg 17.119.2 89 70-130ND
1,2-Dichloroethane ug/kg 15.919.2 83 70-130ND
1,2-Dichloropropane ug/kg 16.419.2 86 70-130ND
1,3,5-Trimethylbenzene ug/kg 17.719.2 92 70-130ND
1,3-Dichlorobenzene ug/kg 17.419.2 91 70-130ND
1,3-Dichloropropane ug/kg 17.419.2 91 70-130ND
1,4-Dichlorobenzene ug/kg 17.219.2 90 70-130ND
2,2-Dichloropropane ug/kg 16.119.2 84 70-130ND
2-Butanone (MEK)ug/kg 34.8J38.4 91 70-130ND
2-Chlorotoluene ug/kg 17.319.2 90 70-130ND
2-Hexanone ug/kg 35.2J38.4 92 70-130ND
4-Chlorotoluene ug/kg 17.319.2 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 35.2J38.4 92 70-130ND
Acetone ug/kg 48.8J38.4 87 70-130ND
Benzene ug/kg 16.519.2 86 50-166ND
Bromobenzene ug/kg 17.619.2 92 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734270MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335007
Bromochloromethane ug/kg 15.619.2 81 70-130ND
Bromodichloromethane ug/kg 16.619.2 86 70-130ND
Bromoform ug/kg 17.419.2 91 70-130ND
Bromomethane ug/kg 13.419.2 70 70-130ND
Carbon tetrachloride ug/kg 16.019.2 83 70-130ND
Chlorobenzene ug/kg 17.719.2 92 43-169ND
Chloroethane ug/kg 13.2 M119.2 69 70-130ND
Chloroform ug/kg 16.619.2 86 70-130ND
Chloromethane ug/kg 4.9J M119.2 25 70-130ND
cis-1,2-Dichloroethene ug/kg 16.419.2 85 70-130ND
cis-1,3-Dichloropropene ug/kg 16.819.2 87 70-130ND
Dibromochloromethane ug/kg 17.119.2 89 70-130ND
Dibromomethane ug/kg 16.219.2 85 70-130ND
Dichlorodifluoromethane ug/kg ND M119.2 7 70-130ND
Diisopropyl ether ug/kg 16.419.2 86 70-130ND
Ethylbenzene ug/kg 18.019.2 94 70-130ND
Hexachloro-1,3-butadiene ug/kg 15.719.2 82 70-130ND
Isopropylbenzene (Cumene)ug/kg 17.719.2 93 70-130ND
m&p-Xylene ug/kg 35.538.4 93 70-130ND
Methyl-tert-butyl ether ug/kg 16.319.2 85 70-130ND
Methylene Chloride ug/kg 15.3J M119.2 54 70-130ND
n-Butylbenzene ug/kg 17.919.2 93 70-130ND
n-Propylbenzene ug/kg 17.819.2 93 70-130ND
Naphthalene ug/kg 18.619.2 97 70-130ND
o-Xylene ug/kg 17.019.2 88 70-130ND
p-Isopropyltoluene ug/kg 17.819.2 93 70-130ND
sec-Butylbenzene ug/kg 18.019.2 94 70-130ND
Styrene ug/kg 17.319.2 90 70-130ND
tert-Butylbenzene ug/kg 16.119.2 84 70-130ND
Tetrachloroethene ug/kg 15.519.2 81 70-130ND
Toluene ug/kg 17.119.2 88 52-163ND
trans-1,2-Dichloroethene ug/kg 16.119.2 84 70-130ND
trans-1,3-Dichloropropene ug/kg 16.219.2 85 70-130ND
Trichloroethene ug/kg 16.219.2 84 49-167ND
Trichlorofluoromethane ug/kg 13.819.2 72 70-130ND
Vinyl acetate ug/kg 36.6J38.4 95 70-130ND
Vinyl chloride ug/kg 8.1J M119.2 42 70-130ND
1,2-Dichloroethane-d4 (S)%108 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297113001
1734269SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297113001
1734269SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 19.1J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297113001
1734269SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%108 7676
4-Bromofluorobenzene (S)%94 4099
Toluene-d8 (S)%98 4598
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36812
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92297335010, 92297335011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1733740
Associated Lab Samples:92297335010, 92297335011
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.7 05/13/16 15:00
1,1,1-Trichloroethane ug/kg ND 4.7 05/13/16 15:00
1,1,2,2-Tetrachloroethane ug/kg ND 4.7 05/13/16 15:00
1,1,2-Trichloroethane ug/kg ND 4.7 05/13/16 15:00
1,1-Dichloroethane ug/kg ND 4.7 05/13/16 15:00
1,1-Dichloroethene ug/kg ND 4.7 05/13/16 15:00
1,1-Dichloropropene ug/kg ND 4.7 05/13/16 15:00
1,2,3-Trichlorobenzene ug/kg ND 4.7 05/13/16 15:00
1,2,3-Trichloropropane ug/kg ND 4.7 05/13/16 15:00
1,2,4-Trichlorobenzene ug/kg ND 4.7 05/13/16 15:00
1,2,4-Trimethylbenzene ug/kg ND 4.7 05/13/16 15:00
1,2-Dibromo-3-chloropropane ug/kg ND 4.7 05/13/16 15:00
1,2-Dibromoethane (EDB)ug/kg ND 4.7 05/13/16 15:00
1,2-Dichlorobenzene ug/kg ND 4.7 05/13/16 15:00
1,2-Dichloroethane ug/kg ND 4.7 05/13/16 15:00
1,2-Dichloropropane ug/kg ND 4.7 05/13/16 15:00
1,3,5-Trimethylbenzene ug/kg ND 4.7 05/13/16 15:00
1,3-Dichlorobenzene ug/kg ND 4.7 05/13/16 15:00
1,3-Dichloropropane ug/kg ND 4.7 05/13/16 15:00
1,4-Dichlorobenzene ug/kg ND 4.7 05/13/16 15:00
2,2-Dichloropropane ug/kg ND 4.7 05/13/16 15:00
2-Butanone (MEK)ug/kg ND 94.7 05/13/16 15:00
2-Chlorotoluene ug/kg ND 4.7 05/13/16 15:00
2-Hexanone ug/kg ND 47.3 05/13/16 15:00
4-Chlorotoluene ug/kg ND 4.7 05/13/16 15:00
4-Methyl-2-pentanone (MIBK)ug/kg ND 47.3 05/13/16 15:00
Acetone ug/kg ND 94.7 05/13/16 15:00
Benzene ug/kg ND 4.7 05/13/16 15:00
Bromobenzene ug/kg ND 4.7 05/13/16 15:00
Bromochloromethane ug/kg ND 4.7 05/13/16 15:00
Bromodichloromethane ug/kg ND 4.7 05/13/16 15:00
Bromoform ug/kg ND 4.7 05/13/16 15:00
Bromomethane ug/kg ND 9.5 05/13/16 15:00
Carbon tetrachloride ug/kg ND 4.7 05/13/16 15:00
Chlorobenzene ug/kg ND 4.7 05/13/16 15:00
Chloroethane ug/kg ND 9.5 05/13/16 15:00
Chloroform ug/kg ND 4.7 05/13/16 15:00
Chloromethane ug/kg ND 9.5 05/13/16 15:00
cis-1,2-Dichloroethene ug/kg ND 4.7 05/13/16 15:00
cis-1,3-Dichloropropene ug/kg ND 4.7 05/13/16 15:00
Dibromochloromethane ug/kg ND 4.7 05/13/16 15:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1733740
Associated Lab Samples:92297335010, 92297335011
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 4.7 05/13/16 15:00
Dichlorodifluoromethane ug/kg ND 9.5 05/13/16 15:00
Diisopropyl ether ug/kg ND 4.7 05/13/16 15:00
Ethylbenzene ug/kg ND 4.7 05/13/16 15:00
Hexachloro-1,3-butadiene ug/kg ND 4.7 05/13/16 15:00
Isopropylbenzene (Cumene)ug/kg ND 4.7 05/13/16 15:00
m&p-Xylene ug/kg ND 9.5 05/13/16 15:00
Methyl-tert-butyl ether ug/kg ND 4.7 05/13/16 15:00
Methylene Chloride ug/kg ND 18.9 05/13/16 15:00
n-Butylbenzene ug/kg ND 4.7 05/13/16 15:00
n-Propylbenzene ug/kg ND 4.7 05/13/16 15:00
Naphthalene ug/kg ND 4.7 05/13/16 15:00
o-Xylene ug/kg ND 4.7 05/13/16 15:00
p-Isopropyltoluene ug/kg ND 4.7 05/13/16 15:00
sec-Butylbenzene ug/kg ND 4.7 05/13/16 15:00
Styrene ug/kg ND 4.7 05/13/16 15:00
tert-Butylbenzene ug/kg ND 4.7 05/13/16 15:00
Tetrachloroethene ug/kg ND 4.7 05/13/16 15:00
Toluene ug/kg ND 4.7 05/13/16 15:00
trans-1,2-Dichloroethene ug/kg ND 4.7 05/13/16 15:00
trans-1,3-Dichloropropene ug/kg ND 4.7 05/13/16 15:00
Trichloroethene ug/kg ND 4.7 05/13/16 15:00
Trichlorofluoromethane ug/kg ND 4.7 05/13/16 15:00
Vinyl acetate ug/kg ND 47.3 05/13/16 15:00
Vinyl chloride ug/kg ND 9.5 05/13/16 15:00
Xylene (Total)ug/kg ND 9.5 05/13/16 15:00
1,2-Dichloroethane-d4 (S)%80 70-132 05/13/16 15:00
4-Bromofluorobenzene (S)%104 70-130 05/13/16 15:00
Toluene-d8 (S)%102 70-130 05/13/16 15:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733742LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 42.643.5 98 74-137
1,1,1-Trichloroethane ug/kg 39.243.5 90 67-140
1,1,2,2-Tetrachloroethane ug/kg 32.343.5 74 72-141
1,1,2-Trichloroethane ug/kg 38.843.5 89 78-138
1,1-Dichloroethane ug/kg 39.443.5 91 69-134
1,1-Dichloroethene ug/kg 39.743.5 91 67-138
1,1-Dichloropropene ug/kg 41.343.5 95 69-139
1,2,3-Trichlorobenzene ug/kg 39.943.5 92 70-146
1,2,3-Trichloropropane ug/kg 37.943.5 87 69-144
1,2,4-Trichlorobenzene ug/kg 39.943.5 92 68-148
1,2,4-Trimethylbenzene ug/kg 41.443.5 95 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733742LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 36.043.5 83 65-140
1,2-Dibromoethane (EDB)ug/kg 42.543.5 98 77-135
1,2-Dichlorobenzene ug/kg 39.643.5 91 77-141
1,2-Dichloroethane ug/kg 37.943.5 87 65-137
1,2-Dichloropropane ug/kg 40.943.5 94 72-136
1,3,5-Trimethylbenzene ug/kg 41.543.5 96 76-133
1,3-Dichlorobenzene ug/kg 41.043.5 94 74-138
1,3-Dichloropropane ug/kg 40.843.5 94 71-139
1,4-Dichlorobenzene ug/kg 40.843.5 94 76-138
2,2-Dichloropropane ug/kg 40.843.5 94 68-137
2-Butanone (MEK)ug/kg 78.1J87 90 58-147
2-Chlorotoluene ug/kg 39.843.5 92 73-139
2-Hexanone ug/kg 78.887 91 62-145
4-Chlorotoluene ug/kg 39.943.5 92 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 77.487 89 64-149
Acetone ug/kg 71J87 82 53-153
Benzene ug/kg 41.243.5 95 73-135
Bromobenzene ug/kg 41.643.5 96 75-133
Bromochloromethane ug/kg 38.243.5 88 73-134
Bromodichloromethane ug/kg 41.743.5 96 71-135
Bromoform ug/kg 37.943.5 87 66-141
Bromomethane ug/kg 46.0 F343.5 106 53-160
Carbon tetrachloride ug/kg 41.643.5 96 60-145
Chlorobenzene ug/kg 41.143.5 94 78-130
Chloroethane ug/kg 41.643.5 96 64-149
Chloroform ug/kg 40.643.5 93 70-134
Chloromethane ug/kg 37.443.5 86 52-150
cis-1,2-Dichloroethene ug/kg 38.743.5 89 70-133
cis-1,3-Dichloropropene ug/kg 42.343.5 97 68-134
Dibromochloromethane ug/kg 43.143.5 99 71-138
Dibromomethane ug/kg 39.643.5 91 74-130
Dichlorodifluoromethane ug/kg 37.043.5 85 40-160
Diisopropyl ether ug/kg 40.943.5 94 69-141
Ethylbenzene ug/kg 40.443.5 93 75-133
Hexachloro-1,3-butadiene ug/kg 39.443.5 91 68-143
Isopropylbenzene (Cumene)ug/kg 39.843.5 91 76-143
m&p-Xylene ug/kg 81.087 93 75-136
Methyl-tert-butyl ether ug/kg 37.643.5 86 68-144
Methylene Chloride ug/kg 37.743.5 87 45-154
n-Butylbenzene ug/kg 40.443.5 93 72-137
n-Propylbenzene ug/kg 39.643.5 91 76-136
Naphthalene ug/kg 38.843.5 89 68-151
o-Xylene ug/kg 39.143.5 90 76-141
p-Isopropyltoluene ug/kg 39.743.5 91 76-140
sec-Butylbenzene ug/kg 40.243.5 92 79-139
Styrene ug/kg 40.543.5 93 79-137
tert-Butylbenzene ug/kg 36.143.5 83 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733742LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 38.543.5 89 71-138
Toluene ug/kg 39.843.5 91 74-131
trans-1,2-Dichloroethene ug/kg 40.343.5 93 67-135
trans-1,3-Dichloropropene ug/kg 41.643.5 96 65-146
Trichloroethene ug/kg 46.743.5 107 67-135
Trichlorofluoromethane ug/kg 39.543.5 91 59-144
Vinyl acetate ug/kg 36.7J F3874240-160
Vinyl chloride ug/kg 39.143.5 90 56-141
Xylene (Total)ug/kg 120130 92 76-137
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734272MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335011
1,1,1,2-Tetrachloroethane ug/kg 14.716.9 87 70-130ND
1,1,1-Trichloroethane ug/kg 14.616.9 87 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 14.216.9 84 70-130ND
1,1,2-Trichloroethane ug/kg 13.516.9 80 70-130ND
1,1-Dichloroethane ug/kg 14.116.9 83 70-130ND
1,1-Dichloroethene ug/kg 13.016.9 77 49-180ND
1,1-Dichloropropene ug/kg 14.516.9 86 70-130ND
1,2,3-Trichlorobenzene ug/kg 11.816.9 70 70-130ND
1,2,3-Trichloropropane ug/kg 14.816.9 88 70-130ND
1,2,4-Trichlorobenzene ug/kg 11.4 M116.9 67 70-130ND
1,2,4-Trimethylbenzene ug/kg 15.616.9 92 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 13.716.9 81 70-130ND
1,2-Dibromoethane (EDB)ug/kg 13.816.9 81 70-130ND
1,2-Dichlorobenzene ug/kg 13.516.9 80 70-130ND
1,2-Dichloroethane ug/kg 13.816.9 82 70-130ND
1,2-Dichloropropane ug/kg 14.816.9 87 70-130ND
1,3,5-Trimethylbenzene ug/kg 15.916.9 94 70-130ND
1,3-Dichlorobenzene ug/kg 13.516.9 80 70-130ND
1,3-Dichloropropane ug/kg 14.416.9 85 70-130ND
1,4-Dichlorobenzene ug/kg 13.116.9 77 70-130ND
2,2-Dichloropropane ug/kg 14.516.9 86 70-130ND
2-Butanone (MEK)ug/kg 32.3J33.9 96 70-130ND
2-Chlorotoluene ug/kg 14.916.9 88 70-130ND
2-Hexanone ug/kg 28.9J33.9 86 70-130ND
4-Chlorotoluene ug/kg 14.016.9 83 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 31.9J33.9 94 70-130ND
Acetone ug/kg 47.9J33.9 82 70-130ND
Benzene ug/kg 14.916.9 88 50-166ND
Bromobenzene ug/kg 13.916.9 82 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
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Page 69 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734272MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335011
Bromochloromethane ug/kg 12.816.9 76 70-130ND
Bromodichloromethane ug/kg 13.416.9 79 70-130ND
Bromoform ug/kg 12.516.9 74 70-130ND
Bromomethane ug/kg 12.716.9 75 70-130ND
Carbon tetrachloride ug/kg 13.916.9 82 70-130ND
Chlorobenzene ug/kg 14.016.9 83 43-169ND
Chloroethane ug/kg 11.816.9 70 70-130ND
Chloroform ug/kg 14.616.9 86 70-130ND
Chloromethane ug/kg 4.8J M116.9 28 70-130ND
cis-1,2-Dichloroethene ug/kg 13.216.9 78 70-130ND
cis-1,3-Dichloropropene ug/kg 12.916.9 76 70-130ND
Dibromochloromethane ug/kg 13.416.9 79 70-130ND
Dibromomethane ug/kg 13.216.9 78 70-130ND
Dichlorodifluoromethane ug/kg ND M116.9 8 70-130ND
Diisopropyl ether ug/kg 15.716.9 93 70-130ND
Ethylbenzene ug/kg 14.616.9 87 70-130ND
Hexachloro-1,3-butadiene ug/kg 13.816.9 82 70-130ND
Isopropylbenzene (Cumene)ug/kg 15.016.9 89 70-130ND
m&p-Xylene ug/kg 29.333.9 86 70-130ND
Methyl-tert-butyl ether ug/kg 15.316.9 90 70-130ND
Methylene Chloride ug/kg 14.1J M116.9 57 70-130ND
n-Butylbenzene ug/kg 14.716.9 87 70-130ND
n-Propylbenzene ug/kg 15.116.9 89 70-130ND
Naphthalene ug/kg 13.616.9 80 70-130ND
o-Xylene ug/kg 14.616.9 86 70-130ND
p-Isopropyltoluene ug/kg 15.616.9 92 70-130ND
sec-Butylbenzene ug/kg 15.816.9 93 70-130ND
Styrene ug/kg 13.316.9 79 70-130ND
tert-Butylbenzene ug/kg 14.416.9 85 70-130ND
Tetrachloroethene ug/kg 13.216.9 78 70-130ND
Toluene ug/kg 14.716.9 84 52-163ND
trans-1,2-Dichloroethene ug/kg 13.416.9 79 70-130ND
trans-1,3-Dichloropropene ug/kg 11.6 M116.9 69 70-130ND
Trichloroethene ug/kg 13.916.9 82 49-167ND
Trichlorofluoromethane ug/kg 12.116.9 71 70-130ND
Vinyl acetate ug/kg 28.8J33.9 85 70-130ND
Vinyl chloride ug/kg 7.1J M116.9 42 70-130ND
1,2-Dichloroethane-d4 (S)%106 70-132
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297335010
1734271SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297335010
1734271SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297335010
1734271SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 4.5J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%112 986
4-Bromofluorobenzene (S)%96 3799
Toluene-d8 (S)%98 36100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36846
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92297335012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734296
Associated Lab Samples:92297335012
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.8 05/15/16 14:20
1,1,1-Trichloroethane ug/kg ND 4.8 05/15/16 14:20
1,1,2,2-Tetrachloroethane ug/kg ND 4.8 05/15/16 14:20
1,1,2-Trichloroethane ug/kg ND 4.8 05/15/16 14:20
1,1-Dichloroethane ug/kg ND 4.8 05/15/16 14:20
1,1-Dichloroethene ug/kg ND 4.8 05/15/16 14:20
1,1-Dichloropropene ug/kg ND 4.8 05/15/16 14:20
1,2,3-Trichlorobenzene ug/kg ND 4.8 05/15/16 14:20
1,2,3-Trichloropropane ug/kg ND 4.8 05/15/16 14:20
1,2,4-Trichlorobenzene ug/kg ND 4.8 05/15/16 14:20
1,2,4-Trimethylbenzene ug/kg ND 4.8 05/15/16 14:20
1,2-Dibromo-3-chloropropane ug/kg ND 4.8 05/15/16 14:20
1,2-Dibromoethane (EDB)ug/kg ND 4.8 05/15/16 14:20
1,2-Dichlorobenzene ug/kg ND 4.8 05/15/16 14:20
1,2-Dichloroethane ug/kg ND 4.8 05/15/16 14:20
1,2-Dichloropropane ug/kg ND 4.8 05/15/16 14:20
1,3,5-Trimethylbenzene ug/kg ND 4.8 05/15/16 14:20
1,3-Dichlorobenzene ug/kg ND 4.8 05/15/16 14:20
1,3-Dichloropropane ug/kg ND 4.8 05/15/16 14:20
1,4-Dichlorobenzene ug/kg ND 4.8 05/15/16 14:20
2,2-Dichloropropane ug/kg ND 4.8 05/15/16 14:20
2-Butanone (MEK)ug/kg ND 96.0 05/15/16 14:20
2-Chlorotoluene ug/kg ND 4.8 05/15/16 14:20
2-Hexanone ug/kg ND 48.0 05/15/16 14:20
4-Chlorotoluene ug/kg ND 4.8 05/15/16 14:20
4-Methyl-2-pentanone (MIBK)ug/kg ND 48.0 05/15/16 14:20
Acetone ug/kg ND 96.0 05/15/16 14:20
Benzene ug/kg ND 4.8 05/15/16 14:20
Bromobenzene ug/kg ND 4.8 05/15/16 14:20
Bromochloromethane ug/kg ND 4.8 05/15/16 14:20
Bromodichloromethane ug/kg ND 4.8 05/15/16 14:20
Bromoform ug/kg ND 4.8 05/15/16 14:20
Bromomethane ug/kg ND 9.6 05/15/16 14:20
Carbon tetrachloride ug/kg ND 4.8 05/15/16 14:20
Chlorobenzene ug/kg ND 4.8 05/15/16 14:20
Chloroethane ug/kg ND 9.6 05/15/16 14:20
Chloroform ug/kg ND 4.8 05/15/16 14:20
Chloromethane ug/kg ND 9.6 05/15/16 14:20
cis-1,2-Dichloroethene ug/kg ND 4.8 05/15/16 14:20
cis-1,3-Dichloropropene ug/kg ND 4.8 05/15/16 14:20
Dibromochloromethane ug/kg ND 4.8 05/15/16 14:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734296
Associated Lab Samples:92297335012
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 4.8 05/15/16 14:20
Dichlorodifluoromethane ug/kg ND 9.6 05/15/16 14:20
Diisopropyl ether ug/kg ND 4.8 05/15/16 14:20
Ethylbenzene ug/kg ND 4.8 05/15/16 14:20
Hexachloro-1,3-butadiene ug/kg ND 4.8 05/15/16 14:20
Isopropylbenzene (Cumene)ug/kg ND 4.8 05/15/16 14:20
m&p-Xylene ug/kg ND 9.6 05/15/16 14:20
Methyl-tert-butyl ether ug/kg ND 4.8 05/15/16 14:20
Methylene Chloride ug/kg ND 19.2 05/15/16 14:20
n-Butylbenzene ug/kg ND 4.8 05/15/16 14:20
n-Propylbenzene ug/kg ND 4.8 05/15/16 14:20
Naphthalene ug/kg ND 4.8 05/15/16 14:20
o-Xylene ug/kg ND 4.8 05/15/16 14:20
p-Isopropyltoluene ug/kg ND 4.8 05/15/16 14:20
sec-Butylbenzene ug/kg ND 4.8 05/15/16 14:20
Styrene ug/kg ND 4.8 05/15/16 14:20
tert-Butylbenzene ug/kg ND 4.8 05/15/16 14:20
Tetrachloroethene ug/kg ND 4.8 05/15/16 14:20
Toluene ug/kg ND 4.8 05/15/16 14:20
trans-1,2-Dichloroethene ug/kg ND 4.8 05/15/16 14:20
trans-1,3-Dichloropropene ug/kg ND 4.8 05/15/16 14:20
Trichloroethene ug/kg ND 4.8 05/15/16 14:20
Trichlorofluoromethane ug/kg ND 4.8 05/15/16 14:20
Vinyl acetate ug/kg ND 48.0 05/15/16 14:20
Vinyl chloride ug/kg ND 9.6 05/15/16 14:20
Xylene (Total)ug/kg ND 9.6 05/15/16 14:20
1,2-Dichloroethane-d4 (S)%110 70-132 05/15/16 14:20
4-Bromofluorobenzene (S)%92 70-130 05/15/16 14:20
Toluene-d8 (S)%100 70-130 05/15/16 14:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734297LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 44.242.8 103 74-137
1,1,1-Trichloroethane ug/kg 41.442.8 97 67-140
1,1,2,2-Tetrachloroethane ug/kg 39.842.8 93 72-141
1,1,2-Trichloroethane ug/kg 42.142.8 98 78-138
1,1-Dichloroethane ug/kg 41.942.8 98 69-134
1,1-Dichloroethene ug/kg 42.942.8 100 67-138
1,1-Dichloropropene ug/kg 42.342.8 99 69-139
1,2,3-Trichlorobenzene ug/kg 44.342.8 104 70-146
1,2,3-Trichloropropane ug/kg 44.042.8 103 69-144
1,2,4-Trichlorobenzene ug/kg 44.142.8 103 68-148
1,2,4-Trimethylbenzene ug/kg 45.142.8 105 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734297LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 44.142.8 103 65-140
1,2-Dibromoethane (EDB)ug/kg 45.942.8 107 77-135
1,2-Dichlorobenzene ug/kg 43.842.8 102 77-141
1,2-Dichloroethane ug/kg 40.642.8 95 65-137
1,2-Dichloropropane ug/kg 41.442.8 97 72-136
1,3,5-Trimethylbenzene ug/kg 44.242.8 103 76-133
1,3-Dichlorobenzene ug/kg 44.542.8 104 74-138
1,3-Dichloropropane ug/kg 43.842.8 102 71-139
1,4-Dichlorobenzene ug/kg 44.142.8 103 76-138
2,2-Dichloropropane ug/kg 42.142.8 98 68-137
2-Butanone (MEK)ug/kg 86.785.6 101 58-147
2-Chlorotoluene ug/kg 43.542.8 102 73-139
2-Hexanone ug/kg 90.785.6 106 62-145
4-Chlorotoluene ug/kg 43.442.8 101 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 92.585.6 108 64-149
Acetone ug/kg 81.8J85.6 96 53-153
Benzene ug/kg 42.342.8 99 73-135
Bromobenzene ug/kg 45.042.8 105 75-133
Bromochloromethane ug/kg 40.342.8 94 73-134
Bromodichloromethane ug/kg 42.042.8 98 71-135
Bromoform ug/kg 43.742.8 102 66-141
Bromomethane ug/kg 52.542.8 123 53-160
Carbon tetrachloride ug/kg 42.542.8 99 60-145
Chlorobenzene ug/kg 42.742.8 100 78-130
Chloroethane ug/kg 47.542.8 111 64-149
Chloroform ug/kg 40.942.8 95 70-134
Chloromethane ug/kg 39.142.8 91 52-150
cis-1,2-Dichloroethene ug/kg 41.442.8 97 70-133
cis-1,3-Dichloropropene ug/kg 44.042.8 103 68-134
Dibromochloromethane ug/kg 43.942.8 102 71-138
Dibromomethane ug/kg 42.042.8 98 74-130
Dichlorodifluoromethane ug/kg 40.742.8 95 40-160
Diisopropyl ether ug/kg 42.642.8 100 69-141
Ethylbenzene ug/kg 43.242.8 101 75-133
Hexachloro-1,3-butadiene ug/kg 41.142.8 96 68-143
Isopropylbenzene (Cumene)ug/kg 43.042.8 100 76-143
m&p-Xylene ug/kg 84.585.6 99 75-136
Methyl-tert-butyl ether ug/kg 43.442.8 101 68-144
Methylene Chloride ug/kg 41.142.8 96 45-154
n-Butylbenzene ug/kg 44.642.8 104 72-137
n-Propylbenzene ug/kg 43.542.8 102 76-136
Naphthalene ug/kg 49.642.8 116 68-151
o-Xylene ug/kg 41.642.8 97 76-141
p-Isopropyltoluene ug/kg 43.742.8 102 76-140
sec-Butylbenzene ug/kg 43.542.8 102 79-139
Styrene ug/kg 43.642.8 102 79-137
tert-Butylbenzene ug/kg 39.842.8 93 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734297LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 38.942.8 91 71-138
Toluene ug/kg 41.642.8 97 74-131
trans-1,2-Dichloroethene ug/kg 42.842.8 100 67-135
trans-1,3-Dichloropropene ug/kg 43.542.8 102 65-146
Trichloroethene ug/kg 44.142.8 103 67-135
Trichlorofluoromethane ug/kg 45.142.8 105 59-144
Vinyl acetate ug/kg 38.7J85.6 45 40-160
Vinyl chloride ug/kg 44.742.8 104 56-141
Xylene (Total)ug/kg 126128 98 76-137
1,2-Dichloroethane-d4 (S)%107 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734542MATRIX SPIKE SAMPLE:
MSSpike
Result
92297075013
1,1,1,2-Tetrachloroethane ug/kg 21.223.1 92 70-130ND
1,1,1-Trichloroethane ug/kg 21.123.1 92 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 21.923.1 95 70-130ND
1,1,2-Trichloroethane ug/kg 21.623.1 94 70-130ND
1,1-Dichloroethane ug/kg 20.923.1 91 70-130ND
1,1-Dichloroethene ug/kg 21.923.1 95 49-180ND
1,1-Dichloropropene ug/kg 22.423.1 97 70-130ND
1,2,3-Trichlorobenzene ug/kg 20.923.1 90 70-130ND
1,2,3-Trichloropropane ug/kg 22.023.1 96 70-130ND
1,2,4-Trichlorobenzene ug/kg 21.123.1 91 70-130ND
1,2,4-Trimethylbenzene ug/kg 28.023.1 121 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 21.623.1 93 70-130ND
1,2-Dibromoethane (EDB)ug/kg 23.523.1 102 70-130ND
1,2-Dichlorobenzene ug/kg 21.623.1 94 70-130ND
1,2-Dichloroethane ug/kg 21.123.1 91 70-130ND
1,2-Dichloropropane ug/kg 21.623.1 93 70-130ND
1,3,5-Trimethylbenzene ug/kg 24.623.1 107 70-130ND
1,3-Dichlorobenzene ug/kg 22.223.1 96 70-130ND
1,3-Dichloropropane ug/kg 22.423.1 97 70-130ND
1,4-Dichlorobenzene ug/kg 22.623.1 98 70-130ND
2,2-Dichloropropane ug/kg 20.623.1 90 70-130ND
2-Butanone (MEK)ug/kg 47.2J46.1 102 70-130ND
2-Chlorotoluene ug/kg 22.923.1 99 70-130ND
2-Hexanone ug/kg 47.2J46.1 102 70-130ND
4-Chlorotoluene ug/kg 22.423.1 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 47.6J46.1 103 70-130ND
Acetone ug/kg 76.3J46.1 126 70-130ND
Benzene ug/kg 22.623.1 98 50-166ND
Bromobenzene ug/kg 23.023.1 100 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1734542MATRIX SPIKE SAMPLE:
MSSpike
Result
92297075013
Bromochloromethane ug/kg 19.923.1 86 70-130ND
Bromodichloromethane ug/kg 20.723.1 90 70-130ND
Bromoform ug/kg 20.523.1 89 70-130ND
Bromomethane ug/kg 26.323.1 114 70-130ND
Carbon tetrachloride ug/kg 20.723.1 90 70-130ND
Chlorobenzene ug/kg 22.123.1 96 43-169ND
Chloroethane ug/kg 24.923.1 108 70-130ND
Chloroform ug/kg 20.923.1 90 70-130ND
Chloromethane ug/kg 19.823.1 86 70-130ND
cis-1,2-Dichloroethene ug/kg 21.223.1 92 70-130ND
cis-1,3-Dichloropropene ug/kg 21.323.1 92 70-130ND
Dibromochloromethane ug/kg 21.323.1 92 70-130ND
Dibromomethane ug/kg 21.923.1 95 70-130ND
Dichlorodifluoromethane ug/kg 20.723.1 90 70-130ND
Diisopropyl ether ug/kg 21.923.1 95 70-130ND
Ethylbenzene ug/kg 23.523.1 102 70-130ND
Hexachloro-1,3-butadiene ug/kg 21.923.1 95 70-130ND
Isopropylbenzene (Cumene)ug/kg 22.923.1 99 70-130ND
m&p-Xylene ug/kg 49.046.1 106 70-130ND
Methyl-tert-butyl ether ug/kg 22.223.1 96 70-130ND
Methylene Chloride ug/kg 21.9J23.1 95 70-130ND
n-Butylbenzene ug/kg 24.223.1 105 70-130ND
n-Propylbenzene ug/kg 23.923.1 104 70-130ND
Naphthalene ug/kg 31.3 M123.1 136 70-130ND
o-Xylene ug/kg 23.823.1 103 70-130ND
p-Isopropyltoluene ug/kg 23.823.1 103 70-130ND
sec-Butylbenzene ug/kg 23.823.1 103 70-130ND
Styrene ug/kg 22.023.1 95 70-130ND
tert-Butylbenzene ug/kg 21.023.1 91 70-130ND
Tetrachloroethene ug/kg 20.523.1 89 70-130ND
Toluene ug/kg 23.123.1 100 52-163ND
trans-1,2-Dichloroethene ug/kg 21.823.1 94 70-130ND
trans-1,3-Dichloropropene ug/kg 20.723.1 90 70-130ND
Trichloroethene ug/kg 21.723.1 94 49-167ND
Trichlorofluoromethane ug/kg 22.223.1 97 70-130ND
Vinyl acetate ug/kg 47.6J46.1 103 70-130ND
Vinyl chloride ug/kg 22.723.1 99 70-130ND
1,2-Dichloroethane-d4 (S)%105 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297075012
1734541SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297075012
1734541SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 62.9J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297075012
1734541SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 1.7J 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%107 13114
4-Bromofluorobenzene (S)%98 2097
Toluene-d8 (S)%99 1999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/42565
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92297335007, 92297335008, 92297335009, 92297335010, 92297335011, 92297335012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1733277
Associated Lab Samples:92297335007, 92297335008, 92297335009, 92297335010, 92297335011, 92297335012
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 05/16/16 09:50
1,2-Dichlorobenzene ug/kg ND 330 05/16/16 09:50
1,3-Dichlorobenzene ug/kg ND 330 05/16/16 09:50
1,4-Dichlorobenzene ug/kg ND 330 05/16/16 09:50
1-Methylnaphthalene ug/kg ND 330 05/16/16 09:50
2,4,5-Trichlorophenol ug/kg ND 330 05/16/16 09:50
2,4,6-Trichlorophenol ug/kg ND 330 05/16/16 09:50
2,4-Dichlorophenol ug/kg ND 330 05/16/16 09:50
2,4-Dimethylphenol ug/kg ND 330 05/16/16 09:50
2,4-Dinitrophenol ug/kg ND 1650 05/16/16 09:50
2,4-Dinitrotoluene ug/kg ND 330 05/16/16 09:50
2,6-Dinitrotoluene ug/kg ND 330 05/16/16 09:50
2-Chloronaphthalene ug/kg ND 330 05/16/16 09:50
2-Chlorophenol ug/kg ND 330 05/16/16 09:50
2-Methylnaphthalene ug/kg ND 330 05/16/16 09:50
2-Methylphenol(o-Cresol)ug/kg ND 330 05/16/16 09:50
2-Nitroaniline ug/kg ND 1650 05/16/16 09:50
2-Nitrophenol ug/kg ND 330 05/16/16 09:50
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 05/16/16 09:50
3,3'-Dichlorobenzidine ug/kg ND 1650 05/16/16 09:50
3-Nitroaniline ug/kg ND 1650 05/16/16 09:50
4,6-Dinitro-2-methylphenol ug/kg ND 660 05/16/16 09:50
4-Bromophenylphenyl ether ug/kg ND 330 05/16/16 09:50
4-Chloro-3-methylphenol ug/kg ND 660 05/16/16 09:50
4-Chloroaniline ug/kg ND 1650 05/16/16 09:50
4-Chlorophenylphenyl ether ug/kg ND 330 05/16/16 09:50
4-Nitroaniline ug/kg ND 660 05/16/16 09:50
4-Nitrophenol ug/kg ND 1650 05/16/16 09:50
Acenaphthene ug/kg ND 330 05/16/16 09:50
Acenaphthylene ug/kg ND 330 05/16/16 09:50
Aniline ug/kg ND 330 05/16/16 09:50
Anthracene ug/kg ND 330 05/16/16 09:50
Benzo(a)anthracene ug/kg ND 330 05/16/16 09:50
Benzo(a)pyrene ug/kg ND 330 05/16/16 09:50
Benzo(b)fluoranthene ug/kg ND 330 05/16/16 09:50
Benzo(g,h,i)perylene ug/kg ND 330 05/16/16 09:50
Benzo(k)fluoranthene ug/kg ND 330 05/16/16 09:50
Benzoic Acid ug/kg ND 1650 05/16/16 09:50
Benzyl alcohol ug/kg ND 660 05/16/16 09:50
bis(2-Chloroethoxy)methane ug/kg ND 330 05/16/16 09:50
bis(2-Chloroethyl) ether ug/kg ND 330 05/16/16 09:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1733277
Associated Lab Samples:92297335007, 92297335008, 92297335009, 92297335010, 92297335011, 92297335012
Matrix: Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 05/16/16 09:50
bis(2-Ethylhexyl)phthalate ug/kg ND 330 05/16/16 09:50
Butylbenzylphthalate ug/kg ND 330 05/16/16 09:50
Chrysene ug/kg ND 330 05/16/16 09:50
Di-n-butylphthalate ug/kg ND 330 05/16/16 09:50
Di-n-octylphthalate ug/kg ND 330 05/16/16 09:50
Dibenz(a,h)anthracene ug/kg ND 330 05/16/16 09:50
Dibenzofuran ug/kg ND 330 05/16/16 09:50
Diethylphthalate ug/kg ND 330 05/16/16 09:50
Dimethylphthalate ug/kg ND 330 05/16/16 09:50
Fluoranthene ug/kg ND 330 05/16/16 09:50
Fluorene ug/kg ND 330 05/16/16 09:50
Hexachloro-1,3-butadiene ug/kg ND 330 05/16/16 09:50
Hexachlorobenzene ug/kg ND 330 05/16/16 09:50
Hexachlorocyclopentadiene ug/kg ND 330 05/16/16 09:50
Hexachloroethane ug/kg ND 330 05/16/16 09:50
Indeno(1,2,3-cd)pyrene ug/kg ND 330 05/16/16 09:50
Isophorone ug/kg ND 330 05/16/16 09:50
N-Nitroso-di-n-propylamine ug/kg ND 330 05/16/16 09:50
N-Nitrosodimethylamine ug/kg ND 330 05/16/16 09:50
N-Nitrosodiphenylamine ug/kg ND 330 05/16/16 09:50
Naphthalene ug/kg ND 330 05/16/16 09:50
Nitrobenzene ug/kg ND 330 05/16/16 09:50
Pentachlorophenol ug/kg ND 1650 05/16/16 09:50
Phenanthrene ug/kg ND 330 05/16/16 09:50
Phenol ug/kg ND 330 05/16/16 09:50
Pyrene ug/kg ND 330 05/16/16 09:50
2,4,6-Tribromophenol (S)%80 27-110 05/16/16 09:50
2-Fluorobiphenyl (S)%82 30-110 05/16/16 09:50
2-Fluorophenol (S)%76 13-110 05/16/16 09:50
Nitrobenzene-d5 (S)%80 23-110 05/16/16 09:50
Phenol-d6 (S)%77 22-110 05/16/16 09:50
Terphenyl-d14 (S)%95 28-110 05/16/16 09:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733278LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13701670 82 36-120
1,2-Dichlorobenzene ug/kg 12501670 75 41-120
1,3-Dichlorobenzene ug/kg 12701670 76 66-120
1,4-Dichlorobenzene ug/kg 12401670 75 42-120
1-Methylnaphthalene ug/kg 13401670 80 40-120
2,4,5-Trichlorophenol ug/kg 14201670 85 37-120
2,4,6-Trichlorophenol ug/kg 14801670 89 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733278LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 14101670 85 33-120
2,4-Dimethylphenol ug/kg 14201670 85 36-120
2,4-Dinitrophenol ug/kg 46808330 56 22-121
2,4-Dinitrotoluene ug/kg 14701670 88 60-120
2,6-Dinitrotoluene ug/kg 14101670 84 54-120
2-Chloronaphthalene ug/kg 13401670 80 41-120
2-Chlorophenol ug/kg 13401670 80 39-120
2-Methylnaphthalene ug/kg 12701670 76 26-120
2-Methylphenol(o-Cresol)ug/kg 13301670 80 41-120
2-Nitroaniline ug/kg 30403330 91 45-120
2-Nitrophenol ug/kg 13601670 81 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 12901670 78 35-120
3,3'-Dichlorobenzidine ug/kg 27303330 82 16-125
3-Nitroaniline ug/kg 27303330 82 45-120
4,6-Dinitro-2-methylphenol ug/kg 27603330 83 46-120
4-Bromophenylphenyl ether ug/kg 14601670 87 36-120
4-Chloro-3-methylphenol ug/kg 29403330 88 37-120
4-Chloroaniline ug/kg 26703330 80 35-120
4-Chlorophenylphenyl ether ug/kg 14701670 88 30-120
4-Nitroaniline ug/kg 27703330 83 48-120
4-Nitrophenol ug/kg 82408330 99 43-120
Acenaphthene ug/kg 13201670 79 46-120
Acenaphthylene ug/kg 13301670 80 46-120
Aniline ug/kg 12001670 72 33-120
Anthracene ug/kg 12801670 77 63-120
Benzo(a)anthracene ug/kg 14201670 85 61-120
Benzo(a)pyrene ug/kg 15401670 92 59-120
Benzo(b)fluoranthene ug/kg 15401670 92 55-120
Benzo(g,h,i)perylene ug/kg 17101670 102 57-120
Benzo(k)fluoranthene ug/kg 15301670 92 56-120
Benzoic Acid ug/kg 43208330 52 13-120
Benzyl alcohol ug/kg 27003330 81 34-120
bis(2-Chloroethoxy)methane ug/kg 13401670 81 21-120
bis(2-Chloroethyl) ether ug/kg 12801670 77 25-120
bis(2-Chloroisopropyl) ether ug/kg 10801670 65 13-120
bis(2-Ethylhexyl)phthalate ug/kg 15401670 92 56-123
Butylbenzylphthalate ug/kg 15401670 92 57-120
Chrysene ug/kg 14101670 85 64-120
Di-n-butylphthalate ug/kg 14801670 89 58-120
Di-n-octylphthalate ug/kg 14101670 84 47-121
Dibenz(a,h)anthracene ug/kg 17301670 104 56-120
Dibenzofuran ug/kg 14701670 88 43-120
Diethylphthalate ug/kg 15501670 93 55-120
Dimethylphthalate ug/kg 15401670 92 54-120
Fluoranthene ug/kg 13201670 79 61-120
Fluorene ug/kg 14201670 85 51-120
Hexachloro-1,3-butadiene ug/kg 14201670 85 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733278LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 14301670 86 53-120
Hexachlorocyclopentadiene ug/kg 14301670 86 18-150
Hexachloroethane ug/kg 12901670 77 39-120
Indeno(1,2,3-cd)pyrene ug/kg 17801670 107 58-120
Isophorone ug/kg 13301670 80 38-120
N-Nitroso-di-n-propylamine ug/kg 12201670 73 30-120
N-Nitrosodimethylamine ug/kg 10001670 60 32-120
N-Nitrosodiphenylamine ug/kg 12701670 76 50-120
Naphthalene ug/kg 12501670 75 38-120
Nitrobenzene ug/kg 13401670 81 37-120
Pentachlorophenol ug/kg 29703330 89 10-120
Phenanthrene ug/kg 13201670 79 62-120
Phenol ug/kg 13301670 80 37-120
Pyrene ug/kg 14001670 84 63-120
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%82 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%82 23-110
Phenol-d6 (S)%81 22-110
Terphenyl-d14 (S)%92 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1733279MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335007
1,2,4-Trichlorobenzene ug/kg 12901770 73 18-119ND
1,2-Dichlorobenzene ug/kg 12501770 71 50-110ND
1,3-Dichlorobenzene ug/kg 12801770 72 27-110ND
1,4-Dichlorobenzene ug/kg 12601770 71 28-110ND
1-Methylnaphthalene ug/kg 12701770 72 24-116ND
2,4,5-Trichlorophenol ug/kg 15501770 88 28-110ND
2,4,6-Trichlorophenol ug/kg 15901770 90 17-117ND
2,4-Dichlorophenol ug/kg 14101770 80 21-128ND
2,4-Dimethylphenol ug/kg 13001770 74 10-120ND
2,4-Dinitrophenol ug/kg 43008830 49 10-107ND
2,4-Dinitrotoluene ug/kg 15301770 87 36-109ND
2,6-Dinitrotoluene ug/kg 14701770 83 32-110ND
2-Chloronaphthalene ug/kg 13201770 75 30-107ND
2-Chlorophenol ug/kg 13401770 76 14-106ND
2-Methylnaphthalene ug/kg 12401770 70 10-135ND
2-Methylphenol(o-Cresol)ug/kg 13301770 75 10-124ND
2-Nitroaniline ug/kg 30003530 85 26-116ND
2-Nitrophenol ug/kg 13101770 74 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 13501770 76 10-109ND
3,3'-Dichlorobenzidine ug/kg 30103530 85 10-150ND
3-Nitroaniline ug/kg 28203530 80 22-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1733279MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335007
4,6-Dinitro-2-methylphenol ug/kg 26403530 75 13-121ND
4-Bromophenylphenyl ether ug/kg 14501770 82 31-109ND
4-Chloro-3-methylphenol ug/kg 30403530 86 13-128ND
4-Chloroaniline ug/kg 26003530 73 18-102ND
4-Chlorophenylphenyl ether ug/kg 15101770 85 29-112ND
4-Nitroaniline ug/kg 28903530 82 16-111ND
4-Nitrophenol ug/kg 86508830 98 14-135ND
Acenaphthene ug/kg 13501770 76 26-114ND
Acenaphthylene ug/kg 13801770 78 32-108ND
Aniline ug/kg 11901770 67 10-107ND
Anthracene ug/kg 12901770 73 32-111ND
Benzo(a)anthracene ug/kg 13901770 78 25-117ND
Benzo(a)pyrene ug/kg 15201770 86 25-106ND
Benzo(b)fluoranthene ug/kg 15001770 85 24-110ND
Benzo(g,h,i)perylene ug/kg 17201770 97 19-112ND
Benzo(k)fluoranthene ug/kg 14901770 84 24-114ND
Benzoic Acid ug/kg 56808830 64 10-110ND
Benzyl alcohol ug/kg 27803530 79 24-106ND
bis(2-Chloroethoxy)methane ug/kg 13301770 75 13-119ND
bis(2-Chloroethyl) ether ug/kg 12901770 73 10-134ND
bis(2-Chloroisopropyl) ether ug/kg 11001770 62 10-113ND
bis(2-Ethylhexyl)phthalate ug/kg 15501770 88 10-125ND
Butylbenzylphthalate ug/kg 15401770 87 18-110ND
Chrysene ug/kg 13601770 77 30-110ND
Di-n-butylphthalate ug/kg 14901770 84 19-112ND
Di-n-octylphthalate ug/kg 15401770 87 17-105ND
Dibenz(a,h)anthracene ug/kg 17401770 98 23-111ND
Dibenzofuran ug/kg 15101770 86 35-103ND
Diethylphthalate ug/kg 16201770 91 27-113ND
Dimethylphthalate ug/kg 16201770 92 26-111ND
Fluoranthene ug/kg 13101770 74 33-109ND
Fluorene ug/kg 14501770 82 32-113ND
Hexachloro-1,3-butadiene ug/kg 13101770 74 16-116ND
Hexachlorobenzene ug/kg 14201770 81 27-120ND
Hexachlorocyclopentadiene ug/kg 12601770 71 10-108ND
Hexachloroethane ug/kg 12701770 72 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 18301770 104 10-122ND
Isophorone ug/kg 13501770 76 28-114ND
N-Nitroso-di-n-propylamine ug/kg 12701770 72 27-113ND
N-Nitrosodimethylamine ug/kg 10201770 57 10-109ND
N-Nitrosodiphenylamine ug/kg 13001770 74 10-128ND
Naphthalene ug/kg 12201770 69 25-110ND
Nitrobenzene ug/kg 13301770 75 18-114ND
Pentachlorophenol ug/kg 32303530 91 10-122ND
Phenanthrene ug/kg 13101770 74 30-114ND
Phenol ug/kg 13401770 76 11-102ND
Pyrene ug/kg 13401770 76 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 84 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1733279MATRIX SPIKE SAMPLE:
MSSpike
Result
92297335007
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%74 30-110
2-Fluorophenol (S)%75 13-110
Nitrobenzene-d5 (S)%74 23-110
Phenol-d6 (S)%77 22-110
Terphenyl-d14 (S)%81 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297335008
1733280SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297335008
1733280SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Chloroisopropyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%88 390
2-Fluorobiphenyl (S)%74 276
2-Fluorophenol (S)%70 373
Nitrobenzene-d5 (S)%77 379
Phenol-d6 (S)%71 575
Terphenyl-d14 (S)%86 185
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/42582
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples: 92297335001, 92297335002, 92297335003, 92297335004, 92297335006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734221
Associated Lab Samples:92297335001, 92297335002, 92297335003, 92297335004, 92297335006
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 05/16/16 19:09
1,2-Dichlorobenzene ug/L ND 10.0 05/16/16 19:09
1,3-Dichlorobenzene ug/L ND 10.0 05/16/16 19:09
1,4-Dichlorobenzene ug/L ND 10.0 05/16/16 19:09
1-Methylnaphthalene ug/L ND 10.0 05/16/16 19:09
2,4,5-Trichlorophenol ug/L ND 10.0 05/16/16 19:09
2,4,6-Trichlorophenol ug/L ND 10.0 05/16/16 19:09
2,4-Dichlorophenol ug/L ND 10.0 05/16/16 19:09
2,4-Dimethylphenol ug/L ND 10.0 05/16/16 19:09
2,4-Dinitrophenol ug/L ND 50.0 05/16/16 19:09
2,4-Dinitrotoluene ug/L ND 10.0 05/16/16 19:09
2,6-Dinitrotoluene ug/L ND 10.0 05/16/16 19:09
2-Chloronaphthalene ug/L ND 10.0 05/16/16 19:09
2-Chlorophenol ug/L ND 10.0 05/16/16 19:09
2-Methylnaphthalene ug/L ND 10.0 05/16/16 19:09
2-Methylphenol(o-Cresol)ug/L ND 10.0 05/16/16 19:09
2-Nitroaniline ug/L ND 50.0 05/16/16 19:09
2-Nitrophenol ug/L ND 10.0 05/16/16 19:09
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 05/16/16 19:09
3,3'-Dichlorobenzidine ug/L ND 20.0 05/16/16 19:09
3-Nitroaniline ug/L ND 50.0 05/16/16 19:09
4,6-Dinitro-2-methylphenol ug/L ND 20.0 05/16/16 19:09
4-Bromophenylphenyl ether ug/L ND 10.0 05/16/16 19:09
4-Chloro-3-methylphenol ug/L ND 20.0 05/16/16 19:09
4-Chloroaniline ug/L ND 20.0 05/16/16 19:09
4-Chlorophenylphenyl ether ug/L ND 10.0 05/16/16 19:09
4-Nitroaniline ug/L ND 20.0 05/16/16 19:09
4-Nitrophenol ug/L ND 50.0 05/16/16 19:09
Acenaphthene ug/L ND 10.0 05/16/16 19:09
Acenaphthylene ug/L ND 10.0 05/16/16 19:09
Aniline ug/L ND 10.0 05/16/16 19:09
Anthracene ug/L ND 10.0 05/16/16 19:09
Benzo(a)anthracene ug/L ND 10.0 05/16/16 19:09
Benzo(a)pyrene ug/L ND 10.0 05/16/16 19:09
Benzo(b)fluoranthene ug/L ND 10.0 05/16/16 19:09
Benzo(g,h,i)perylene ug/L ND 10.0 05/16/16 19:09
Benzo(k)fluoranthene ug/L ND 10.0 05/16/16 19:09
Benzoic Acid ug/L ND 50.0 05/16/16 19:09
Benzyl alcohol ug/L ND 20.0 05/16/16 19:09
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/16/16 19:09
bis(2-Chloroethyl) ether ug/L ND 10.0 05/16/16 19:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734221
Associated Lab Samples:92297335001, 92297335002, 92297335003, 92297335004, 92297335006
Matrix: Water
Analyzed
bis(2-Chloroisopropyl) ether ug/L ND 10.0 05/16/16 19:09
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 05/16/16 19:09
Butylbenzylphthalate ug/L ND 10.0 05/16/16 19:09
Chrysene ug/L ND 10.0 05/16/16 19:09
Di-n-butylphthalate ug/L ND 10.0 05/16/16 19:09
Di-n-octylphthalate ug/L ND 10.0 05/16/16 19:09
Dibenz(a,h)anthracene ug/L ND 10.0 05/16/16 19:09
Dibenzofuran ug/L ND 10.0 05/16/16 19:09
Diethylphthalate ug/L ND 10.0 05/16/16 19:09
Dimethylphthalate ug/L ND 10.0 05/16/16 19:09
Fluoranthene ug/L ND 10.0 05/16/16 19:09
Fluorene ug/L ND 10.0 05/16/16 19:09
Hexachloro-1,3-butadiene ug/L ND 10.0 05/16/16 19:09
Hexachlorobenzene ug/L ND 10.0 05/16/16 19:09
Hexachlorocyclopentadiene ug/L ND 10.0 05/16/16 19:09
Hexachloroethane ug/L ND 10.0 05/16/16 19:09
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 05/16/16 19:09
Isophorone ug/L ND 10.0 05/16/16 19:09
N-Nitroso-di-n-propylamine ug/L ND 10.0 05/16/16 19:09
N-Nitrosodimethylamine ug/L ND 10.0 05/16/16 19:09
N-Nitrosodiphenylamine ug/L ND 10.0 05/16/16 19:09
Naphthalene ug/L ND 10.0 05/16/16 19:09
Nitrobenzene ug/L ND 10.0 05/16/16 19:09
Pentachlorophenol ug/L ND 25.0 05/16/16 19:09
Phenanthrene ug/L ND 10.0 05/16/16 19:09
Phenol ug/L ND 10.0 05/16/16 19:09
Pyrene ug/L ND 10.0 05/16/16 19:09
2,4,6-Tribromophenol (S)%84 27-110 05/16/16 19:09
2-Fluorobiphenyl (S)%74 27-110 05/16/16 19:09
2-Fluorophenol (S)%35 12-110 05/16/16 19:09
Nitrobenzene-d5 (S)%72 21-110 05/16/16 19:09
Phenol-d6 (S)%24 10-110 05/16/16 19:09
Terphenyl-d14 (S)%108 31-107 S305/16/16 19:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734222LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 30.950 62 31-120
1,2-Dichlorobenzene ug/L 28.350 57 38-120
1,3-Dichlorobenzene ug/L 27.350 55 30-122
1,4-Dichlorobenzene ug/L 27.150 54 37-120
1-Methylnaphthalene ug/L 34.050 68 34-113
2,4,5-Trichlorophenol ug/L 39.650 79 43-113
2,4,6-Trichlorophenol ug/L 37.550 75 42-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734222LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/L 33.450 67 30-120
2,4-Dimethylphenol ug/L 35.650 71 29-111
2,4-Dinitrophenol ug/L 128250 51 19-132
2,4-Dinitrotoluene ug/L 52.450 105 58-128
2,6-Dinitrotoluene ug/L 50.750 101 54-129
2-Chloronaphthalene ug/L 37.550 75 43-117
2-Chlorophenol ug/L 31.050 62 37-120
2-Methylnaphthalene ug/L 32.450 65 33-120
2-Methylphenol(o-Cresol)ug/L 29.150 58 31-120
2-Nitroaniline ug/L 71.8100 72 48-121
2-Nitrophenol ug/L 32.950 66 25-116
3&4-Methylphenol(m&p Cresol)ug/L 24.750 49 23-120
3,3'-Dichlorobenzidine ug/L 103100 103 10-154
3-Nitroaniline ug/L 86.7100 87 43-115
4,6-Dinitro-2-methylphenol ug/L 69.5100 70 44-124
4-Bromophenylphenyl ether ug/L 45.650 91 34-113
4-Chloro-3-methylphenol ug/L 80.0100 80 31-110
4-Chloroaniline ug/L 66.7100 67 20-120
4-Chlorophenylphenyl ether ug/L 43.350 87 34-116
4-Nitroaniline ug/L 93.7100 94 46-128
4-Nitrophenol ug/L 65.3250 26 11-120
Acenaphthene ug/L 36.450 73 48-114
Acenaphthylene ug/L 37.450 75 48-112
Aniline ug/L 26.950 54 26-120
Anthracene ug/L 38.550 77 57-118
Benzo(a)anthracene ug/L 43.450 87 56-121
Benzo(a)pyrene ug/L 45.250 90 55-127
Benzo(b)fluoranthene ug/L 48.150 96 53-128
Benzo(g,h,i)perylene ug/L 52.850 106 54-125
Benzo(k)fluoranthene ug/L 41.950 84 51-123
Benzoic Acid ug/L 49.8J250 20 10-120
Benzyl alcohol ug/L 62.3100 62 27-120
bis(2-Chloroethoxy)methane ug/L 32.950 66 32-120
bis(2-Chloroethyl) ether ug/L 33.150 66 33-111
bis(2-Chloroisopropyl) ether ug/L 34.950 70 15-120
bis(2-Ethylhexyl)phthalate ug/L 44.950 90 50-145
Butylbenzylphthalate ug/L 48.950 98 54-138
Chrysene ug/L 42.450 85 58-127
Di-n-butylphthalate ug/L 49.850 100 56-125
Di-n-octylphthalate ug/L 54.050 108 50-134
Dibenz(a,h)anthracene ug/L 56.650 113 53-129
Dibenzofuran ug/L 41.550 83 45-120
Diethylphthalate ug/L 47.150 94 53-120
Dimethylphthalate ug/L 46.250 92 55-116
Fluoranthene ug/L 44.150 88 57-125
Fluorene ug/L 42.250 84 53-118
Hexachloro-1,3-butadiene ug/L 28.850 58 23-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734222LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 50.950 102 49-116
Hexachlorocyclopentadiene ug/L 33.250 66 26-158
Hexachloroethane ug/L 25.550 51 30-114
Indeno(1,2,3-cd)pyrene ug/L 57.350 115 55-128
Isophorone ug/L 32.450 65 31-118
N-Nitroso-di-n-propylamine ug/L 34.150 68 32-119
N-Nitrosodimethylamine ug/L 15.450 31 13-120
N-Nitrosodiphenylamine ug/L 37.150 74 43-120
Naphthalene ug/L 29.750 59 32-120
Nitrobenzene ug/L 29.250 58 33-110
Pentachlorophenol ug/L 89.4100 89 10-137
Phenanthrene ug/L 38.350 77 57-117
Phenol ug/L 15.950 32 10-120
Pyrene ug/L 37.850 76 55-122
2,4,6-Tribromophenol (S)%S011927-110
2-Fluorobiphenyl (S)%66 27-110
2-Fluorophenol (S)%31 12-110
Nitrobenzene-d5 (S)%61 21-110
Phenol-d6 (S)%26 10-110
Terphenyl-d14 (S)%92 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/42595
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples: 92297335005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734776
Associated Lab Samples:92297335005
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 05/18/16 11:31
1,2-Dichlorobenzene ug/L ND 10.0 05/18/16 11:31
1,3-Dichlorobenzene ug/L ND 10.0 05/18/16 11:31
1,4-Dichlorobenzene ug/L ND 10.0 05/18/16 11:31
1-Methylnaphthalene ug/L ND 10.0 05/18/16 11:31
2,4,5-Trichlorophenol ug/L ND 10.0 05/18/16 11:31
2,4,6-Trichlorophenol ug/L ND 10.0 05/18/16 11:31
2,4-Dichlorophenol ug/L ND 10.0 05/18/16 11:31
2,4-Dimethylphenol ug/L ND 10.0 05/18/16 11:31
2,4-Dinitrophenol ug/L ND 50.0 05/18/16 11:31
2,4-Dinitrotoluene ug/L ND 10.0 05/18/16 11:31
2,6-Dinitrotoluene ug/L ND 10.0 05/18/16 11:31
2-Chloronaphthalene ug/L ND 10.0 05/18/16 11:31
2-Chlorophenol ug/L ND 10.0 05/18/16 11:31
2-Methylnaphthalene ug/L ND 10.0 05/18/16 11:31
2-Methylphenol(o-Cresol)ug/L ND 10.0 05/18/16 11:31
2-Nitroaniline ug/L ND 50.0 05/18/16 11:31
2-Nitrophenol ug/L ND 10.0 05/18/16 11:31
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 05/18/16 11:31
3,3'-Dichlorobenzidine ug/L ND 20.0 05/18/16 11:31
3-Nitroaniline ug/L ND 50.0 05/18/16 11:31
4,6-Dinitro-2-methylphenol ug/L ND 20.0 05/18/16 11:31
4-Bromophenylphenyl ether ug/L ND 10.0 05/18/16 11:31
4-Chloro-3-methylphenol ug/L ND 20.0 05/18/16 11:31
4-Chloroaniline ug/L ND 20.0 05/18/16 11:31
4-Chlorophenylphenyl ether ug/L ND 10.0 05/18/16 11:31
4-Nitroaniline ug/L ND 20.0 05/18/16 11:31
4-Nitrophenol ug/L ND 50.0 05/18/16 11:31
Acenaphthene ug/L ND 10.0 05/18/16 11:31
Acenaphthylene ug/L ND 10.0 05/18/16 11:31
Aniline ug/L ND 10.0 05/18/16 11:31
Anthracene ug/L ND 10.0 05/18/16 11:31
Benzo(a)anthracene ug/L ND 10.0 05/18/16 11:31
Benzo(a)pyrene ug/L ND 10.0 05/18/16 11:31
Benzo(b)fluoranthene ug/L ND 10.0 05/18/16 11:31
Benzo(g,h,i)perylene ug/L ND 10.0 05/18/16 11:31
Benzo(k)fluoranthene ug/L ND 10.0 05/18/16 11:31
Benzoic Acid ug/L ND 50.0 05/18/16 11:31
Benzyl alcohol ug/L ND 20.0 05/18/16 11:31
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/18/16 11:31
bis(2-Chloroethyl) ether ug/L ND 10.0 05/18/16 11:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 91 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1734776
Associated Lab Samples:92297335005
Matrix: Water
Analyzed
bis(2-Chloroisopropyl) ether ug/L ND 10.0 05/18/16 11:31
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 05/18/16 11:31
Butylbenzylphthalate ug/L ND 10.0 05/18/16 11:31
Chrysene ug/L ND 10.0 05/18/16 11:31
Di-n-butylphthalate ug/L ND 10.0 05/18/16 11:31
Di-n-octylphthalate ug/L ND 10.0 05/18/16 11:31
Dibenz(a,h)anthracene ug/L ND 10.0 05/18/16 11:31
Dibenzofuran ug/L ND 10.0 05/18/16 11:31
Diethylphthalate ug/L ND 10.0 05/18/16 11:31
Dimethylphthalate ug/L ND 10.0 05/18/16 11:31
Fluoranthene ug/L ND 10.0 05/18/16 11:31
Fluorene ug/L ND 10.0 05/18/16 11:31
Hexachloro-1,3-butadiene ug/L ND 10.0 05/18/16 11:31
Hexachlorobenzene ug/L ND 10.0 05/18/16 11:31
Hexachlorocyclopentadiene ug/L ND 10.0 05/18/16 11:31
Hexachloroethane ug/L ND 10.0 05/18/16 11:31
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 05/18/16 11:31
Isophorone ug/L ND 10.0 05/18/16 11:31
N-Nitroso-di-n-propylamine ug/L ND 10.0 05/18/16 11:31
N-Nitrosodimethylamine ug/L ND 10.0 05/18/16 11:31
N-Nitrosodiphenylamine ug/L ND 10.0 05/18/16 11:31
Naphthalene ug/L ND 10.0 05/18/16 11:31
Nitrobenzene ug/L ND 10.0 05/18/16 11:31
Pentachlorophenol ug/L ND 25.0 05/18/16 11:31
Phenanthrene ug/L ND 10.0 05/18/16 11:31
Phenol ug/L ND 10.0 05/18/16 11:31
Pyrene ug/L ND 10.0 05/18/16 11:31
2,4,6-Tribromophenol (S)%73 27-110 05/18/16 11:31
2-Fluorobiphenyl (S)%75 27-110 05/18/16 11:31
2-Fluorophenol (S)%41 12-110 05/18/16 11:31
Nitrobenzene-d5 (S)%78 21-110 05/18/16 11:31
Phenol-d6 (S)%28 10-110 05/18/16 11:31
Terphenyl-d14 (S)%76 31-107 05/18/16 11:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734777LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1734778
1,2,4-Trichlorobenzene ug/L 28.750 57 31-1206030.1 5 30
1,2-Dichlorobenzene ug/L 25.550 51 38-1205527.5 8 30
1,3-Dichlorobenzene ug/L 24.150 48 30-1225226.1 8 30
1,4-Dichlorobenzene ug/L 24.650 49 37-1205226.2 6 30
1-Methylnaphthalene ug/L 32.550 65 34-1136834.1 5 30
2,4,5-Trichlorophenol ug/L 39.450 79 43-1137537.7 4 30
2,4,6-Trichlorophenol ug/L 39.850 80 42-1207537.3 7 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734777LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1734778
2,4-Dichlorophenol ug/L 38.350 77 30-1207637.8 1 30
2,4-Dimethylphenol ug/L 38.350 77 29-1117838.9 1 30
2,4-Dinitrophenol ug/L 141 R12505619-1322870.6 67 30
2,4-Dinitrotoluene ug/L 41.850 84 58-1288843.9 5 30
2,6-Dinitrotoluene ug/L 41.050 82 54-1298442.0 2 30
2-Chloronaphthalene ug/L 35.850 72 43-1177637.9 6 30
2-Chlorophenol ug/L 33.950 68 37-1207135.4 4 30
2-Methylnaphthalene ug/L 30.350 61 33-1206532.5 7 30
2-Methylphenol(o-Cresol)ug/L 30.650 61 31-1206231.1 1 30
2-Nitroaniline ug/L 76.9100 77 48-1218281.7 6 30
2-Nitrophenol ug/L 38.450 77 25-1167537.7 2 30
3&4-Methylphenol(m&p Cresol)ug/L 26.150 52 23-1205226.0 0 30
3,3'-Dichlorobenzidine ug/L 81.3100 81 10-1548585.2 5 30
3-Nitroaniline ug/L 74.9100 75 43-1158180.8 8 30
4,6-Dinitro-2-methylphenol ug/L 83.1100 83 44-1246767.4 21 30
4-Bromophenylphenyl ether ug/L 36.450 73 34-1137638.0 4 30
4-Chloro-3-methylphenol ug/L 74.5100 74 31-1107676.5 3 30
4-Chloroaniline ug/L 73.7100 74 20-1207777.4 5 30
4-Chlorophenylphenyl ether ug/L 39.450 79 34-1168341.5 5 30
4-Nitroaniline ug/L 80.0100 80 46-1288585.0 6 30
4-Nitrophenol ug/L 89.5250 36 11-1203073.8 19 30
Acenaphthene ug/L 36.150 72 48-1147738.6 7 30
Acenaphthylene ug/L 36.650 73 48-1127738.5 5 30
Aniline ug/L 30.350 61 26-1206633.0 9 30
Anthracene ug/L 35.450 71 57-1187537.5 6 30
Benzo(a)anthracene ug/L 40.550 81 56-1218642.8 5 30
Benzo(a)pyrene ug/L 44.750 89 55-1279346.5 4 30
Benzo(b)fluoranthene ug/L 42.450 85 53-1289145.3 7 30
Benzo(g,h,i)perylene ug/L 46.750 93 54-1259848.9 5 30
Benzo(k)fluoranthene ug/L 45.550 91 51-1239547.6 4 30
Benzoic Acid ug/L 62.1 L02502510-120717.6J 30
Benzyl alcohol ug/L 65.2100 65 27-1206868.1 4 30
bis(2-Chloroethoxy)methane ug/L 40.550 81 32-1208441.9 3 30
bis(2-Chloroethyl) ether ug/L 39.150 78 33-1118341.6 6 30
bis(2-Chloroisopropyl) ether ug/L 41.650 83 15-1208944.3 6 30
bis(2-Ethylhexyl)phthalate ug/L 45.050 90 50-1459246.2 3 30
Butylbenzylphthalate ug/L 44.650 89 54-1389246.1 3 30
Chrysene ug/L 40.950 82 58-1278542.5 4 30
Di-n-butylphthalate ug/L 41.550 83 56-1258743.6 5 30
Di-n-octylphthalate ug/L 42.350 85 50-1348542.4 0 30
Dibenz(a,h)anthracene ug/L 48.550 97 53-12910050.0 3 30
Dibenzofuran ug/L 40.150 80 45-1208542.6 6 30
Diethylphthalate ug/L 42.050 84 53-1208743.7 4 30
Dimethylphthalate ug/L 42.150 84 55-1169045.1 7 30
Fluoranthene ug/L 38.450 77 57-1258140.3 5 30
Fluorene ug/L 38.250 76 53-1188140.5 6 30
Hexachloro-1,3-butadiene ug/L 24.850 50 23-1205226.2 5 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1734777LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1734778
Hexachlorobenzene ug/L 36.050 72 49-1167638.2 6 30
Hexachlorocyclopentadiene ug/L 22.850 46 26-1584522.6 1 30
Hexachloroethane ug/L 22.650 45 30-1144924.6 8 30
Indeno(1,2,3-cd)pyrene ug/L 47.750 95 55-12810150.3 5 30
Isophorone ug/L 39.750 79 31-1188341.4 4 30
N-Nitroso-di-n-propylamine ug/L 36.750 73 32-1197738.7 5 30
N-Nitrosodimethylamine ug/L 23.050 46 13-1204723.7 3 30
N-Nitrosodiphenylamine ug/L 34.950 70 43-1207436.8 5 30
Naphthalene ug/L 30.650 61 32-1206431.8 4 30
Nitrobenzene ug/L 40.050 80 33-1108240.9 2 30
Pentachlorophenol ug/L 66.4100 66 10-1375757.0 15 30
Phenanthrene ug/L 36.650 73 57-1177838.8 6 30
Phenol ug/L 16.250 32 10-1203417.2 6 30
Pyrene ug/L 38.550 77 55-1228241.1 7 30
2,4,6-Tribromophenol (S)%80 27-11074
2-Fluorobiphenyl (S)%80 27-11081
2-Fluorophenol (S)%43 12-11042
Nitrobenzene-d5 (S)%81 21-11082
Phenol-d6 (S)%31 10-11030
Terphenyl-d14 (S)%72 31-10767
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/9045
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92297335007, 92297335008, 92297335009, 92297335010, 92297335011, 92297335012
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297232013
1732542SAMPLE DUPLICATE:
Percent Moisture %12.0 10 2513.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92297324013
1732543SAMPLE DUPLICATE:
Percent Moisture %11.0 1 2511.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 99
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.Results unaffected by high bias.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 99
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92297335
SIDEWALK DEVELOPMENT
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92297335007 OEXT/42565 MSSV/12253SB-1 EPA 3546 EPA 8270
92297335008 OEXT/42565 MSSV/12253SB-2 EPA 3546 EPA 8270
92297335009 OEXT/42565 MSSV/12253SB-3 EPA 3546 EPA 8270
92297335010 OEXT/42565 MSSV/12253SB-4 EPA 3546 EPA 8270
92297335011 OEXT/42565 MSSV/12253SB-5 EPA 3546 EPA 8270
92297335012 OEXT/42565 MSSV/12253SB-6 EPA 3546 EPA 8270
92297335001 OEXT/42582 MSSV/12258GW-1 EPA 3510 EPA 8270
92297335002 OEXT/42582 MSSV/12258GW-2 EPA 3510 EPA 8270
92297335003 OEXT/42582 MSSV/12258GW-3 EPA 3510 EPA 8270
92297335004 OEXT/42582 MSSV/12258GW-4 EPA 3510 EPA 8270
92297335005 OEXT/42595 MSSV/12271GW-5 EPA 3510 EPA 8270
92297335006 OEXT/42582 MSSV/12258GW-6 EPA 3510 EPA 8270
92297335001 MSV/36854GW-1 EPA 8260
92297335002 MSV/36854GW-2 EPA 8260
92297335003 MSV/36854GW-3 EPA 8260
92297335004 MSV/36854GW-4 EPA 8260
92297335005 MSV/36861GW-5 EPA 8260
92297335006 MSV/36854GW-6 EPA 8260
92297335007 MSV/36811SB-1 EPA 8260
92297335008 MSV/36811SB-2 EPA 8260
92297335009 MSV/36811SB-3 EPA 8260
92297335010 MSV/36812SB-4 EPA 8260
92297335011 MSV/36812SB-5 EPA 8260
92297335012 MSV/36846SB-6 EPA 8260
92297335007 PMST/9045SB-1 ASTM D2974-87
92297335008 PMST/9045SB-2 ASTM D2974-87
92297335009 PMST/9045SB-3 ASTM D2974-87
92297335010 PMST/9045SB-4 ASTM D2974-87
92297335011 PMST/9045SB-5 ASTM D2974-87
92297335012 PMST/9045SB-6 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2016 11:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 99
Page 98 of 99
Page 99 of 99