5103_JohnstonCounty_GWMReportOctober_DIN26919_20160115

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October 2015 Semi-Annual Groundwater Monitoring

Johnston County Landfill Facility
Solid Waste Permit No. 51-03

Prepared for:

Johnston County Department of Public Utilities
309 East Market Street
Smithfield, North Carolina

January 2016

Prepared by:

© 2016 Smith Gardner, Inc.
This document is intended for the sole use of the client for which it was prepared and
for the purpose agreed upon by the client and Smith Gardner, Inc.

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Johnston County Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January 2016 Table of Contents Page i
Johnston County Landfill
Smithfield, North Carolina

October 2015 Semi-Annual Groundwater Monitoring Report

Table of Contents
Page

1.0 INTRODUCTION ......................................................................................................... 1 
2.0 SITE GEOLOGY ........................................................................................................... 1 
3.0 SAMPLING LOCATIONS ............................................................................................ 1 
4.0 SAMPLING PROCEDURES ......................................................................................... 2 
5.0 FIELD AND LABORATORY RESULTS .......................................................................... 2 
5.1 Field Results .............................................................................................................. 2 
5.2 Laboratory Analysis ................................................................................................... 2 
5.3 Laboratory Results .................................................................................................... 3 
5.3.1 Inorganic Constituents .................................................................................. 3 
5.3.2 Organic Constituents .................................................................................... 4 
5.3.3 Surface Water Results .................................................................................. 4 
5.3.4 Leachate Analysis ......................................................................................... 4 
5.3.5 Leachate Lagoon Wells ................................................................................. 4 
6.0 SITE ASSESSMENT/REMEDIAL ACTION .................................................................... 4 
7.0 STATISTICAL ANALYSIS ............................................................................................ 5 
8.0 GROUNDWATER CHARACTERIZATION ...................................................................... 5 
9.0 CONCLUSIONS .......................................................................................................... 5 

FIGURES
Figure 1 Potentiometric Surface Map – April 2015

TABLES
Table 1 Monitoring Network Details
Table 2 Groundwater Elevations & Velocities
Table 3 Field Parameter Data
Table 4 Detected Inorganic Constituents
Table 5 Detected Organic Constituents
Table 6 Leachate Summary

APPENDICES
Appendix A Monitoring Well Information
Appendix B Laboratory Analytical Report
Appendix C Time vs. Concentration Graphs

Johnston County Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January 2016 Table of Contents Page ii

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Johnston County Phase 1-4A Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January2016 Page 1

1.0 INTRODUCTION
Smith Gardner, Inc. (S+G) is pleased to present the semi-annual sampling report for the
Johnston County Landfill facility, Solid Waste Permit #51-03. The landfill facility consists of an
active C&D landfill, closed Municipal Solid Waste (MSW) unlined landfill units Phases 1-4,
closed Subtitle-D MSW landfill Phase 5, and active MSW Phase 4A. Phase 4A currently accepts
MSW in a double-lined landfill located as a “piggy back” over the closed, unlined Phases 3 & 4.

The Johnston County Landfill is required to submit semi-annual groundwater monitoring
reports in accordance with Solid Waste Section Rule 15A NCAC 13B .1632. The current permit
to operate1 for this facility was issued 9/28/2009. This report presents the semi-annual
groundwater monitoring results for the event conducted October 26-30 and November 4 & 9,
2015.

Previously, the C&D, Phases 1-4 and 4A, and Phase 5 units were each reported separately.
However, the monitoring network was revised in the updated Water Quality Monitoring Plan
(WQMP)2, included in the 2014 Permit Renewal Application3, which established a single report
for the facility rather than separate reports for each landfill unit.

This report includes a field procedure summary, laboratory analyses, time vs. concentration
graphs and groundwater characterization for the facility.
2.0 SITE GEOLOGY
The Johnston County Landfill Facility is underlain by Middendorf Formation sediments
deposited largely in a deltaic system. According to Geology of the Carolinas (Horton/Zullo,
1991) the Middendorf Formation comprises unfossiliferous, interbedded, thin clay and sand.
The stratigraphy tends to be discontinuous indicating lenticular sediment deposits. Most
sediments range from silty clay to coarse clayey sand and gravel with thin dense clay lenses.
There are occasional concretions of iron oxide minerals that form hard thin layers within the
sand layers. In general, the unconsolidated sediments logged during drilling events at the site
contained medium to coarse sands with some silts and clays. The Middendorf Formation is
underlain by the highly weathered metamorphic rocks of the Carolina Slate Belt.

Topography controls the Middendorf Formation thickness, with the bottom being relatively flat-
lying at elevations of approximately 170 fmsl4. The unconsolidated sediment thickness ranges
from approximately 65 feet to less than 10 feet in the lower elevations surrounding the landfill.

3.0 SAMPLING LOCATIONS

1 Johnston County MSW & C&D Landfill Permit to Operate, Facility Permit No. 51-03. NCDENR, Ed
Mussler, III, PE. September 28, 2009. Doc ID: 8483.
2 Water Quality Monitoring Plan, Johnston County Landfill, Revised March 2014 by Smith Gardner, Inc.
3 Johnston County C&D Permit Renewal, January 2014, Smith Gardner, Inc.
4 fmsl = feet above mean sea level
Johnston County Phase 1-4A Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January2016 Page 2

The groundwater monitoring network comprises 19 well monitoring locations, five of which are
categorized as assessment well monitoring locations, five surface water locations, located both
up and downstream from the landfill on Middle Creek, four monitoring wells for the leachate
lagoon and four leachate collection locations. Monitoring well MW-5-1 serves as the
background well for the site. A trip blank (TB) and equipment blank (EB) were also included
with this event for quality control.

Table 1 presents the monitoring network details including well construction information and
the primary monitoring focus. Sampling locations are shown on Figure 1. Monitoring well
construction information is presented in Appendix A.
4.0 SAMPLING PROCEDURES
The sampling event, performed by trained personnel from Johnston County Landfill on October
26-30 and November 4 & 9, 2015, was conducted in accordance with the approved site Water
Quality Monitoring Plan2. Sampling methods followed the protocol outlined in the North
Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities (NCDENR,
DWM). The depth to water in each well was gauged prior to purging and sampling.
Groundwater elevation data is presented in Table 2.

Samples were collected by Johnston County personnel in laboratory prepared containers for the
specified analytical procedures. Samples were collected from dedicated pumps in wells where
these are installed, or by using new factory sealed teflon bailers in wells without pumps.
Groundwater samples were properly preserved, placed on ice and transported to a NC certified
laboratory facility within the specified holding times for each analysis.
5.0 FIELD AND LABORATORY RESULTS
5.1 Field Results
Temperature, pH, turbidity and specific conductance were measured in the field via
direct read instruments. In general, field parameter results remained consistent with
previously reported sampling events. Field parameter results are summarized in Table
3.
5.2 Laboratory Analysis
Collected samples were transported to Prism Laboratories, Inc., a North Carolina
certified laboratory (NC Certification #402) located in Charlotte, NC for analysis;
including Appendix I metals, VOC’s, BOD, COD, TSS, phosphorous, ammonia, nitrate and
sulfate. Laboratory analysis was conducted via the SWS approved methods listed in the
laboratory report.

During this event the lead and chromium concentrationswere re-analyzed by the lab at
the request of the county due to reported detections uncharacteristic with historical
sampling results.

Johnston County Phase 1-4A Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January2016 Page 3

The laboratory analytical report is included as Appendix B.
5.3 Laboratory Results
Laboratory analytical results were compared with the 15A NCAC 2L 0200 Groundwater
Standard (2L Standard), Solid Waste Section Groundwater Protection (GWP) Standards,
NC DWM Solid Waste Section Limits (SWSL) 5 and Federal Maximum Contaminant Limits
(MCL). Surface water results were compared with the NCAC 2B Standard for Class C
waters (2B Standard).

Prism defined “J” values as “detected but below the Reporting Limit (RL); therefore,
result is an estimated concentration.” Values below the Reporting Limit (BRL) are
considered non-detected.

This event there was several noteworthy issues with the sampling results. Regarding
inorganic results chromium was blank qualified in a majority of the samples. According
to the lab definition the analyte was detected in the associated blank at a concentration
>1/2 RL. Chromium and lead were also requested to be re-analyzed by the County for
MW-9C due to abnormal concentrations in the initial lab results.

Acetone and 2-Butanone (Methyl Ethyl Ketone) were reported in both the equipment and
field blank samples. Additionally, these two parameters were reported in the majority of
collected samples, even at locations with no historic detections, and at approximately
the same concentrations.

Based on these issues, it is likely some laboratory results are not representative of
groundwater chemistry for the Johnston County landfill this event.
5.3.1 Inorganic Constituents
No inorganic constituents were detected above their 2L Standard this event.

Two inorganic constituents were detected above their GWP Standard.

 Cobalt (CDMW-6, CDMW-7, CDMW-8, CDMW-9D, MW-6, MW-7B, MW-8D,
MW-9C, MW-11, MW-12B, MW-5-1, MW-5-2, MW5-5 and MW-5-6)
 Vanadium (MW-7B and MW-9C)

Turbidity levels (Table 3) may have biased the inorganic concentrations for select
well samples high. The influence of turbidity on inorganic results at this site was
characterized in the Revised Groundwater Assessment Report6 which compared
analytical results of filtered and unfiltered samples. This report concluded that

5 New Guidelines for electronic submittal of environmental monitoring data memo, NCDENR DWM, Solid
Waste Section, October 27, 2006.
6 G. N. Richardson and Associates, Inc., Revised Ground Water Assessment Report Proposed Johnston
County C&D Landfill, February 2005.
Johnston County Phase 1-4A Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January2016 Page 4

inorganic constituents in the natural soils yielded biased-high total inorganic
results when samples were turbid.

Detected inorganic constituents are presented in Table 4.
5.3.2 Organic Constituents
Seven volatile organic constituents were detected above their 2L Standards.
These results are consistent with historical results previously associated with
the unlined landfills at the facility.

 1,1-Dichloroethane (CDMW-9D and MW-11);
 1,2-Dichloroethane (CDMW-9D);
 1,2-Dichloropropane (CDMW-9D and MW5-2);
 1,4-Dichlorobenzene (CDMW-9D and MW-12B);
 Benzene (CDMW-9D);
 Tetrachloroethene (CDMW-9D); and
 Vinyl Chloride (CDMW-9D)

Organic constituent detections are summarized in Table 5.
5.3.3 Surface Water Results
No inorganic constituents were reported at concentrations above their 2B
Standards. 2-Butanone was a reported detection in all surface water samples
this event, however, it is likely not from the landfill due to similar concentrations
reported in samples from across the landfill and in multiple blanks. Available
analytical results are summarized in Tables 4 and 5, respectively.
5.3.4 Leachate Analysis
Leachate samples were collected from the C&D leachate collection system, the
Phase 4A leachate collection system and leak detection zone and the Ph.5
leachate collection system. A summary of constituents detected in the leachate
is included in Table 6.
5.3.5 Leachate Lagoon Wells
The leachate lagoon wells (LL-1 through LL-4) are positioned around the
leachate storage pond located in the northwestern portion of the facility.
Samples from leachate lagoon wells this event had reported concentrations of 2-
butanone and acetone; two common laboratory contaminants that are present in
the majority of samples and several blanks for this event, therefore are not
considered originating from the landfill. Analytical results are provided in Table
6.
6.0 SITE ASSESSMENT/REMEDIAL ACTION
Johnston County Phase 1-4A Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January2016 Page 5

The Johnston County lined C&D landfill, and the Phase 4A landfill were constructed as “piggy-
back” landfills that partially covers the side-slopes of the existing unlined Phase 3 MSW landfill.
. The remedial action plan includes construction of several lined “piggy-back” cells and a
partial geomembrane cover to limit rainwater infiltration into the unlined waste mass. When
remedial action is completed approximately 70 to 75% of the Phase 3 and 4 landfills will be
covered to reduce infiltration and the production of uncontrolled leachate.
7.0 STATISTICAL ANALYSIS
Statistical analysis is not performed for the site in accordance with the site WQMP and NC Solid
Waste Section Rule 15A NCAC 13B .1632.
8.0 GROUNDWATER CHARACTERIZATION
A potentiometric surface map was prepared from groundwater data collected during this event.
Data indicates groundwater is flowing generally to the north towards Middle Creek, which is
consistent with groundwater flow patterns previously detected for the site. The potentiometric
surface map is included as Figure 1.

Groundwater flow velocities during the sampling event were calculated using the equation:
V = Ki/n

where
K = hydraulic conductivity
i = groundwater gradient
n = porosity

Available groundwater flow velocities ranged from 0.023 ft/day (MW-11) to 0.857 ft/day (MW-9C).
Average flow velocity this event was 0.254 ft/day. These calculated flow velocities are included
in Table 2.
9.0 CONCLUSIONS
Despite, multiple blank detections and likely un-representative detections for several
constituents; data and analyses for the Johnston County Landfill shows generally stable
groundwater quality and indicating that impact remains from the unlined landfills and is not due
to current waste disposal activities. Constituent concentration graphs over time indicate the
concentrations of constituents detected at the site remain generally stable.

Elevated inorganic constituents are likely due to naturally occurring concentrations in the soils
and bedrock at the site and increased sample turbidity which can bias laboratory results high.
This is supported by the results of the Revised Groundwater Assessment Report completed in
2005.

Please note that remedial strategies are ongoing at the site. The Phase 4A landfill unit (a
double-lined landfill designed as a “piggy-back” over unlined Phases 3 and 4), was implemented
as a presumptive remedy to reduce rainwater infiltration into the unlined landfills. Additionally,
Johnston County Phase 1-4A Landfill October 2015 Semi-Annual Groundwater Monitoring Report
January2016 Page 6

a lined C&D landfill was constructed over part of Phase 3 to further reduce rainwater infiltration
and leachate production. These strategies are expected to help improve groundwater quality
over time.

The next semi-annual sampling event is tentatively scheduled for April 2016. Results will be
reported after a laboratory data review.

FIGURE

October 2015 Semi-Annual Monitoring Report
Johnston County Landfill
NC Solid Waste Permit No. 51-03

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October 2015 Semi-Annual Monitoring Report
Johnston County Landfill
NC Solid Waste Permit No. 51-03

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r
i
n
g

L
o
c
a
t
i
o
n
LL
-
2

N
A

3
5
.
5
2
3
3

7
8
.
4
3
4
5

1
4
8
.
1
0

1
5
0
.
3
3

N
A

N
A

N
A

N
A

L
e
a
c
h
a
t
e

L
a
g
o
o
n

M
o
n
i
t
o
r
i
n
g

L
o
c
a
t
i
o
n
LL
-
3

N
A

3
5
.
5
2
3
6

7
8
.
4
3
5
0

1
4
9
.
0
3

1
5
1
.
5
7

N
A

N
A

N
A

N
A

L
e
a
c
h
a
t
e

L
a
g
o
o
n

M
o
n
i
t
o
r
i
n
g

L
o
c
a
t
i
o
n
LL
-
4

N
A

3
5
.
5
2
3
1

7
8
.
4
3
5
9

1
3
6
.
4
4

1
3
8
.
8
1

N
A

N
A

N
A

N
A

L
e
a
c
h
a
t
e

L
a
g
o
o
n

M
o
n
i
t
o
r
i
n
g

L
o
c
a
t
i
o
n
Pr
o
p
o
s
e
d

G
r
o
u
n
d
w
a
t
e
r

A
s
s
e
s
s
m
e
n
t

M
o
n
i
t
o
r
i
n
g

N
e
t
w
o
r
k
MW
-
6

6
/
1
4
/
1
9
9
1

3
5
.
5
2
0
0

7
8
.
4
2
4
1

1
6
1
.
7
8

1
6
6
.
6
0

5
0

1
1
1
.
7
8

3
0
-
5
0

s
l
a
t
e
MW
-
7
B

9
/
1
0
/
1
9
9
3

3
5
.
5
2
1
5

7
8
.
4
2
6
0

1
2
7
.
8
4

1
2
9
.
8
4

1
8

1
0
9
.
8
4

6
-
1
6

s
a
p
r
o
l
i
t
e
MW
-
1
1

9
/
1
5
/
1
9
9
4

3
5
.
5
2
0
8

7
8
.
4
2
9
8

1
3
4
.
0
0

1
4
4
.
3
2

2
5

1
0
9
.
0
0

1
4
-
2
4

c
l
a
y
e
y

s
i
l
t
MW
-
1
2
B

4
/
2
4
/
1
9
9
7

3
5
.
5
2
0
9

7
8
.
4
2
4
4

1
5
3
.
8
2

1
5
6
.
1
2

3
8

1
1
5
.
8
2

2
1
.
5
-
3
6
.
5

P
W
R

-

s
l
a
t
e
MW
-
1
4
D

6
/
2
6
/
2
0
0
3

3
5
.
5
2
1
9

7
8
.
4
2
6
2

1
2
5
.
5
0

1
2
8
.
6
6

3
1

9
4
.
5
0

2
6
-
3
1

m
e
t
a
m
u
d
s
t
o
n
e
Su
r
f
a
c
e

W
a
t
e
r

M
o
n
i
t
o
r
i
n
g

L
o
c
a
t
i
o
n
s
CD
S
W
-
1

N
A

3
5
.
5
1
7
7

7
8
.
4
2
0
7

N
A

N
A

N
A

N
A

N
A

N
A
SW
P
T
-
1

N
A

3
5
.
5
1
3
5

7
8
.
4
3
3
5

N
A

N
A

N
A

N
A

N
A

N
A
SW
P
T
-
2

N
A

3
5
.
5
1
9
2

7
8
.
4
3
1
2

N
A

N
A

N
A

N
A

N
A

N
A
SW
5
-
1

N
A

3
5
.
5
1
8
2

7
8
.
4
3
8
2

N
A

N
A

N
A

N
A

N
A

N
A
SW
5
-
2

N
A

3
5
.
5
1
8
3

7
8
.
4
1
9
4

N
A

N
A

N
A

N
A

N
A

N
A
Le
a
c
h
a
t
e

M
o
n
i
t
o
r
i
n
g

L
o
c
a
t
i
o
n
s
Ph
a
s
e

5

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

M
o
n
i
t
o
r
s

P
h
a
s
e

5

L
e
a
c
h
a
t
e
Ph
a
s
e

4
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

M
o
n
i
t
o
r
s

P
h
a
s
e

4
A

L
e
a
c
h
a
t
e
Ph
a
s
e

4
A

W
i
t
n
e
s
s

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

M
o
n
i
t
o
r
s

P
h
a
s
e

4
A

L
e
a
k

D
e
t
e
c
t
i
o
n

Z
o
n
e

(
d
o
u
b
l
e

l
i
n
e
r
)
C&
D

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

N
A

M
o
n
i
t
o
r
s

C
&
D

L
a
n
d
f
i
l
l

L
e
a
c
h
a
t
e
NA

=

N
o
t

A
v
a
i
l
a
b
l
e
*
G
r
o
u
n
d
s
u
r
f
a
c
e

e
s
t
i
m
a
t
e
d

f
r
o
m

t
o
p
o
g
r
a
p
h
y

s
h
o
w
n

o
n

F
i
g
u
r
e

1
H:
\
P
r
o
j
e
c
t
s
\
G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g
\
2
.

G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g

R
e
p
o
r
t
s
\
J
o
h
n
s
t
o
n
\
2
0
.

J
o
h
n
s
t
o
n

5
-
2
0
1
5
\
m
a
y

1
5
-
J
o
h
n
s
t
o
n
_
t
a
b
l
e
s

Th
i
s

p
a
g
e

i
n
t
e
n
t
i
o
n
a
l
l
y

l
e
f
t

b
l
a
n
k
.

Ta
b
l
e

2
Gr
o
u
n
d
w
a
t
e
r

E
l
e
v
a
t
i
o
n
s

&

V
e
l
o
c
i
t
i
e
s
Jo
h
n
s
t
o
n

C
o
u
n
t
y

L
a
n
d
f
i
l
l
Oc
t
o
b
e
r

2
6
-
3
0

a
n
d

N
o
v
e
m
b
e
r

4

&

9
,

2
0
1
5
By: LMH Date: 07/15/2015
TO
C

W
a
t
e
r

G
r
o
u
n
d
w
a
t
e
r

H
y
d
r
a
u
l
i
c
We
l
l

L
a
t
i
t
u
d
e

L
o
n
g
i
t
u
d
e

E
l
e
v
a
t
i
o
n

L
e
v
e
l

E
l
e
v
a
t
i
o
n

C
o
n
d
u
c
t
i
v
i
t
y

P
o
r
o
s
i
t
y

G
r
a
d
i
e
n
t

V
e
l
o
c
i
t
y
(f
e
e
t
)

(
f
e
e
t
)

(
f
e
e
t
)

(
f
t
/
d
a
y
)

(
%
)

(
f
t
/
f
t
)

(
f
t
/
d
a
y
)
CD
M
W
-
3

3
5
.
5
1
7
7

7
8
.
4
2
1
3

1
7
0
.
6
5
32
.
5
2
13
8
.
1
3

0
.
2
3
2

0
.
2
5

0
.
2
3
7
4

0
.
2
2
0
CD
M
W
-
4

3
5
.
5
1
8
1

7
8
.
4
2
1
3

1
7
2
.
8
4
30
.
4
5
14
2
.
3
9

0
.
2
3
2

0
.
2
5

0
.
0
9
5
1

0
.
0
8
8
CD
M
W
-
6

3
5
.
5
1
8
3

7
8
.
4
2
2
1

1
6
2
.
1
2
9.
7
3
15
2
.
3
9

0
.
2
3
2

0
.
2
5

0
.
0
7
9
7

0
.
0
7
4
CD
M
W
-
7

3
5
.
5
1
6
6

7
8
.
4
2
2
9

1
7
5
.
2
7
12
.
6
0
16
2
.
6
7

0
.
2
3
2

0
.
2
5

0
.
0
2
9
7

0
.
0
2
8
CD
M
W
-
8

3
5
.
5
1
9
5

7
8
.
4
2
2
8

1
2
7
.
4
1
4.
7
4
12
2
.
6
7

0
.
2
3
2

0
.
2
5

0
.
1
2
2
2

0
.
1
1
3
CD
M
W
-
9
D
*

3
5
.
5
1
8
9

7
8
.
4
2
3
1

1
6
0
.
7
1
15
.
1
8
14
5
.
5
3

n
a

n
a

n
a

N
A
MW
-
6

A
35
.
5
2
0
0

7
8
.
4
2
4
1

1
6
6
.
6
0
36
.
8
1
12
9
.
7
9

1
.
8
2
9

0
.
2

0
.
0
5
6
7

0
.
5
1
9
MW
-
7
B

A
35
.
5
2
1
5

7
8
.
4
2
6
0

1
2
9
.
8
4
4.
3
3
12
5
.
5
1

n
a

n
a

n
a

N
A
MW
-
8
D
*
35
.
5
2
1
4

7
8
.
4
2
8
0

1
5
3
.
4
4
5.
6
6
14
7
.
7
8

1
.
5
7
0

n
a

n
a

N
A
MW
-
9
C

3
5
.
5
1
7
9

7
8
.
4
3
1
2

1
6
7
.
8
9
12
.
7
2
15
5
.
1
7

4
.
7
0
9

0
.
2

0
.
0
3
7
2

0
.
8
7
5
MW
-
1
1

A
35
.
5
2
0
8

7
8
.
4
2
9
8

1
4
4
.
3
2
9.
0
1
13
5
.
3
1

0
.
1
4
8

0
.
2

0
.
0
3
1
3

0
.
0
2
3
MW
-
1
2
B

A
35
.
5
2
0
9

7
8
.
4
2
4
4

1
5
6
.
1
4
29
.
3
0
12
6
.
8
4

n
a

n
a

n
a

n
a
MW
-
1
4
D

A *
35
.
5
2
1
9

7
8
.
4
2
6
2

1
2
8
.
6
6
7.
7
2
12
0
.
9
4

n
a

n
a

n
a

n
a
MW
-
1
5
D
*

3
5
.
5
2
1
9

7
8
.
4
2
6
9

1
2
8
.
7
0
8.
3
1
12
0
.
3
9

n
a

n
a

n
a

n
a
MW
-
1
6
D
*

3
5
.
5
2
1
8

7
8
.
4
2
7
6

1
3
3
.
9
6
7.
7
2
12
6
.
2
4

n
a

n
a

n
a

n
a
MW
-
5
-
1

3
5
.
5
1
2
7

7
8
.
4
3
0
7

2
3
2
.
1
7
23
.
6
2
20
8
.
5
5

2
.
2
7
5

0
.
2

0
.
0
2
4
4

0
.
2
7
8
MW
-
5
-
2

3
5
.
5
1
4
0

7
8
.
4
3
2
9

2
0
6
.
7
7
6.
6
3
20
0
.
1
4

5
.
2
4
7

0
.
2

0
.
0
2
4
7

0
.
6
4
9
MW
-
5
-
5

3
5
.
5
1
7
6

7
8
.
4
3
3
9

1
8
5
.
4
2
13
.
5
6
17
1
.
8
6

0
.
2
6
1

0
.
2

0
.
0
3
2
1

0
.
0
4
2
MW
-
5
-
6

3
5
.
5
1
8
0

7
8
.
4
3
3
1

1
9
9
.
1
1
31
.
6
1
16
7
.
5
0

0
.
3
6
6

0
.
2

0
.
0
7
8
9

0
.
1
4
4
No
t
e
s
:

V
e
l
o
c
i
t
y

C
a
l
c
u
l
a
t
e
d

f
r
o
m

V
=
K
*
i
/
n

H
y
d
r
a
u
l
i
c

C
o
n
d
u
c
t
i
v
i
t
y

d
a
t
a

f
r
o
m

s
l
u
g

t
e
s
t
i
n
g

V
=

v
e
l
o
c
i
t
y

P
o
r
o
s
i
t
y

v
a
l
u
e
s

a
s
s
u
m
e
d

f
r
o
m

G
r
o
u
n
d
w
a
t
e
r

&

W
e
l
l
s

(
D
r
i
s
c
o
l
l
)
K
=

H
y
d
r
a
u
l
i
c

C
o
n
d
u
c
t
i
v
i
t
y
na

=

n
o
t

a
v
a
i
l
a
b
l
e
i
=

G
r
a
d
i
e
n
t

A

=

A
s
s
e
s
s
m
e
n
t

M
o
n
i
t
o
r
i
n
g

N
e
t
w
o
r
k
n
=

P
o
r
o
s
i
t
y

*

D
e
e
p

w
e
l
l
s

n
o
t

i
n
c
l
u
d
e
d

i
n

g
r
a
d
i
e
n
t

c
a
l
c
u
l
a
t
i
o
n
H:
\
P
r
o
j
e
c
t
s
\
G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g
\
2
.

G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g

R
e
p
o
r
t
s
\
J
o
h
n
s
t
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Table 3
Field Parameter Data
Johnston County Landfill
October 26-30 and November 4 & 9 , 2015
By: MG
Date: 12/16/2015
Well Temperature
(°Celsius)
Turbidity
(NTU)pH
Specific
Conductivity
(uS/cm)
CDMW-3 16.3 6.83 5.36 24.4
CDMW-4 16.6 4.98 5.81 55.6
CDMW-6 17 295 6.03 81
CDMW-7 18.3 116 4.6 285.4
CDMW-8 17.2 22.6 4.79 126.2
CDMW-9D 18.5 12.2 5.51 288.1
MW-6 A 18.6 12.4 5.96 349.6
MW-7B A 17.4 20.3 5.76 950
MW-8D 19 3.98 5.9 398.8
MW-9C 16.4 122 4.97 114
MW-11 A 18.2 4.28 6.44 200.8
MW-12B A 18.9 5.93 5.77 452.2
MW-14D A 17.5 1.54 6.73 1041
MW-15D 18.6 3.29 6.82 312.1
MW-16D 18.4 6.71 5.59 227.7
MW-5-1 18.4 26.8 4.15 211.9
MW-5-2 17.3 48.9 4.04 303.9
MW-5-5 18.7 2.87 4.40 129.3
MW-5-6 18.2 7.17 4.47 75.7
C&D Leachate 19.1 167 6.30 1998
Ph 4A - Leak Detection 21.9 76.2 5.69 517
Ph 4A Leachate Collection 25.2 17.2 6.91 9,720
Phase 5 Direct Leachate 19.7 56.7 6.41 3023
Lagoon Lchte.#1 18.4 4.51 5.31 108.8
Lagoon Lchte. #2 17.4 13.6 5.53 129.4
Lagoon Lchte. #3 17.8 6.28 5.39 61.3
Lagoon Lchte. #4 16.5 21.9 5.55 105.1
CDSW-1 14.0 5.94 6.89 69
SWPT-1 17.4 3.24 6.53 226
SWPT-2 17.0 4.05 6.81 103
SW5 – 1 15.1 7.85 6.15 304.3
SW5 – 2 14.6 3.98 5.88 165
Notes:
A - Assessment Monitoring Network
Data collected by Kevin Shields & Darren Donnelly of Johnston County Department of Solid
Waste Services.
H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Johnston\20. Johnston 5-2015\may 15-Johnston_tables
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9
,

2
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5
By:LMH 07/08/2015
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9
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2
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5
By:MG Date:12/30/2015
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4

J

1
.
8

J

0
.
7
6

J
Se
l
e
n
i
u
m

u
g
/
l

7
.
1

1
1

0
.
7

J

2
.
2

2
.
4

N
D

N
D

N
D
Si
l
v
e
r

u
g
/
l

0
.
0
4
8

J

0
.
0
9
8

J

0
.
0
4
6

J

0
.
0
1
4

J

0
.
0
1
5

J

0
.
0
2

J

0
.
0
1
4

J

0
.
0
1
8

J
Th
a
l
l
i
u
m

u
g
/
l

0
.
0
5

J

0
.
0
4

J

0
.
0
5
2

J

0
.
2
3

J

0
.
0
3
3

J

0
.
0
3

J

0
.
0
2
3

J

0
.
0
2
4

J
Va
n
a
d
i
u
m

u
g
/
l

6
.
9

1
5

5
.
8

6
.
4

N
D

N
D

N
D

N
D
Zi
n
c

u
g
/
l

7
.
4

J

3
5

5
2

8
.
6

J

2
.
9

J

2
.
9

J

1
.
8

J

1
.
4

J
1,
1
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e

u
g
/
l

0
.
9
4

N
D

N
D

N
D

N
D

N
D

N
D

N
D
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e

u
g
/
l

N
D

0
.
6
5

3
.
5

N
D

N
D

N
D

N
D

N
D
1,
2

-

D
i
c
h
l
o
r
o
p
r
o
p
a
n
e

u
g
/
l

N
D

N
D

0
.
9
8

N
D

N
D

N
D

N
D

N
D
1,
4
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e

u
g
/
l

1
2

N
D

1
5

3

N
D

N
D

N
D

N
D
2-
B
u
t
a
n
o
n
e

u
g
/
l

N
D

4
5

1
1
0

1
.
7

J

2
.
6

J

2
.
1

J

2
.
8

J

2
.
2

J
2-
H
e
x
a
n
o
n
e

u
g
/
l

N
D

1
3

1
.
4

J

N
D

N
D

N
D

N
D

N
D
Ac
e
t
o
n
e

u
g
/
l

4
2

1
8
0

1
7
0

2
9

1
8

1
6

1
8

1
6
Be
n
z
e
n
e

u
g
/
l

7
.
9

7
.
2

1
8

2
.
3

N
D

N
D

N
D

N
D
H:
\
P
r
o
j
e
c
t
s
\
G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g
\
2
.

G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g

R
e
p
o
r
t
s
\
J
o
h
n
s
t
o
n
\
2
0
.

J
o
h
n
s
t
o
n

5
-
2
0
1
5
\
m
a
y

1
5
-
J
o
h
n
s
t
o
n
_
t
a
b
l
e
s
8 of 9
Ta
b
l
e

6
Le
a
c
h
a
t
e

S
u
m
m
a
r
y
Jo
h
n
s
t
o
n

C
o
u
n
t
y

L
a
n
d
f
i
l
l
Oc
t
o
b
e
r

2
6
-
3
0
,

a
n
d

N
o
v
e
m
b
e
r

4

&

9
,

2
0
1
5
By:MG Date:12/30/2015
Pa
r
a
m
e
t
e
r

U
n
i
t
Ph

5

-

Le
a
c
h
a
t
e
Ph

4
A

Le
a
c
h
a
t
e

Co
l
l
e
c
t
i
o
n
Ph
a
s
e

4
A
-
Le
a
k

De
t
e
c
t
i
o
n
C&
D

Le
a
c
h
a
t
e
Le
a
c
h
a
t
e

La
g
o
o
n

#
1
Le
a
c
h
a
t
e

La
g
o
o
n

#
2
Le
a
c
h
a
t
e

La
g
o
o
n

#
3
Leachate Lagoon #4
Ch
l
o
r
o
b
e
n
z
e
n
e

u
g
/
l

N
D

1
.
6

3
.
6

2
.
3

N
D

N
D

N
D

N
D
Ch
l
o
r
o
e
t
h
a
n
e

u
g
/
l

0
.
5
9

N
D

0
.
7
9

N
D

N
D

N
D

N
D

N
D
Ch
l
o
r
o
m
e
t
h
a
n
e

u
g
/
l

N
D

2
.
9

N
D

N
D

N
D

N
D

N
D

N
D
Ci
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e

u
g
/
l

0
.
8

1
.
4

8
.
2

3
.
4

N
D

N
D

N
D

N
D
Et
h
y
l
b
e
n
z
e
n
e

u
g
/
l

2
7

1
9

5
8

0
.
7

N
D

N
D

N
D

N
D
Me
t
h
y
l

I
s
o
b
u
t
y
l

K
e
t
o
n
e

u
g
/
l

1
.
6

J

3
.
6

J

1
2

N
D

N
D

N
D

N
D

N
D
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e

u
g
/
l

N
D

N
D

1
.
4

N
D

N
D

N
D

N
D

N
D
St
y
r
e
n
e

u
g
/
l

1
.
4

0
.
5
2

1
.
5

N
D

N
D

N
D

N
D

N
D
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e

u
g
/
l

N
D

N
D

0
.
6

N
D

N
D

N
D

N
D

N
D
Te
t
r
a
h
y
d
r
o
f
u
r
a
n

u
g
/
l

3
8
0

5
0
0

9
3
0

4
4

N
D

N
D

N
D

N
D
To
l
u
e
n
e

u
g
/
l

1
6

1
6

5
4

0
.
5
7

N
D

N
D

N
D

N
D
o-
X
y
l
e
n
e
s

u
g
/
l

1
0

1
1

2
8

N
D

N
D

N
D

N
D

N
D
m,
p
-
X
y
l
e
n
e
s

u
g
/
l

4
9

2
6

6
5

N
D

N
D

N
D

N
D

N
D
Xy
l
e
n
e
s
,

t
o
t
a
l
ug
/
l

5
9

3
7

9
3

N
D

N
D

N
D

N
D

N
D
Vi
n
y
l

C
h
l
o
r
i
d
e

u
g
/
l

1
.
6

1
.
3

4
.
6

2
.
3

N
D

N
D

N
D

N
D
NO
T
E
S
:

1.

P
h

5

-

L
e
a
c
h
a
t
e

s
a
m
p
l
e

o
b
t
a
i
n
e
d

f
r
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m

t
h
e

m
a
n
h
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l
e

d
o
w
n
g
r
a
d
i
e
n
t

f
r
o
m

t
h
e

n
o
r
t
h

e
n
d
2.

P
h
a
s
e

4
A

L
e
a
k

D
e
t
e
c
t
i
o
n

s
a
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p
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o
b
t
a
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d

a
t

t
h
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p
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p

s
t
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t
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n

v
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u
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t

a
t

t
h
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n
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t
h

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n
d

o
f

P
h
a
s
e

4
A
3.

P
h
a
s
e

4
A

L
e
a
c
h
a
t
e

C
o
l
l
e
c
t
i
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n

s
a
m
p
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o
b
t
a
i
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d

a
t

t
h
e

c
o
l
l
e
c
t
i
o
n

r
i
s
e
r

l
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c
a
t
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d

a
t

t
h
e

n
o
r
t
h

e
n
d

o
f

P
h
a
s
e

4
A
J
=

D
e
f
i
n
e
d

b
y

P
R
I
S
M

a
s

"
d
e
t
e
c
t
e
d

b
u
t

b
e
l
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w

t
h
e

r
e
p
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t
i
n
g

l
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m
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t

(
p
r
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s
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d

i
n

l
a
b

r
e
p
o
r
t
)
;

t
h
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f
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,

r
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s
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l
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i
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a
n

e
s
t
i
m
a
t
e
d

c
oncentration."
NA

=

P
a
r
a
m
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t
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r

N
o
t

A
n
a
l
y
z
e
d
ND

=

P
a
r
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m
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t
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r

N
o
t

D
e
t
e
c
t
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d
Da
t
a

f
r
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m

P
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L
a
b
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r
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t
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r
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s
,

I
n
c
.

P
r
i
s
m

W
o
r
k

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r
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r

#
s
:

5
1
0
0
5
2
7
,

5
1
0
0
5
2
8
,

5
1
1
0
0
3
7
,

5
1
1
0
0
3
8
,

5
1
1
0
0
8
4

a
n
d

5
1
1
0
1
8
7
H:
\
P
r
o
j
e
c
t
s
\
G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g
\
2
.

G
r
o
u
n
d
w
a
t
e
r

M
o
n
i
t
o
r
i
n
g

R
e
p
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r
t
s
\
J
o
h
n
s
t
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n
\
2
0
.

J
o
h
n
s
t
o
n

5
-
2
0
1
5
\
m
a
y

1
5
-
J
o
h
n
s
t
o
n
_
t
a
b
l
e
s
9 of 9
Ta
b
l
e

7
St
a
t
i
s
t
i
c
a
l

A
n
a
l
y
s
i
s

S
u
m
m
a
r
y
Jo
h
n
s
t
o
n

C
o
u
n
t
y

L
a
n
d
f
i
l
l
Oc
t
o
b
e
r

1
3
-
2
0
,

2
0
1
4
By: MG Date: 5/20/2013
Lo
c
a
t
i
o
n

P
a
r
a
m
e
t
e
r

R
e
s
u
l
t
2L

St
a
n
d
a
r
d
Te
s
t

U
n
i
t
s
%N
D

T
e
s
t
St
a
t
i
s
t
i
c
a
l
l
y

Si
g
n
i
f
i
c
a
n
t
?
2n
d

s
t
a
t
i
s
t
i
c
a
l

An
a
l
y
s
i
s

T
e
s
t
CD
M
W
-
9
D

A
r
s
e
n
i
c

1
9

1
0

u
g
/
l

5
2
.
6
3

P
P

N

-

-
CD
M
W
-
6

C
h
r
o
m
i
u
m

1
1

1
0

u
g
/
l

0

P
P

N

-

-
CD
M
W
-
9
D

1
,
1
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e

8
.
6

6

u
g
/
l

1
0
.
5
3

P
P

N

-

-
CD
M
W
-
9
D

1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e

0
.
6
1

0
.
4

u
g
/
l

8
9
.
4
7

P
o
s

N

-

-
CD
M
W
-
9
D

1
,
2
-
D
i
c
h
l
o
r
o
p
r
o
p
a
n
e

1
.
9

0
.
6

u
g
/
l

2
1
.
0
5

P
P

N

-

-
CD
M
W
-
9
D

1
,
4
-
D
i
c
h
l
o
r
o
b
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n
z
e
n
e

8
.
4

6

u
g
/
l

2
1
.
0
5

P
P

N
CD
M
W
-
9
D

B
e
n
z
e
n
e

1
.
6

1

u
g
/
l

1
5
.
7
9

P
P

N

-

-
CD
M
W
-
9
D

T
e
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e

1
.
5

0
.
7

u
g
/
l

2
1
.
0
5

P
P

N

-

-
CD
M
W
-
9
D

V
i
n
y
l

C
h
l
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r
i
d
e

2
.
1

0
.
0
3

u
g
/
l

3
6
.
8
4

P
P

N

-

-
No
t
e
:
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D

P
e
r
c
e
n
t

n
o
n
-
d
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c
t
s
PP

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c

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I
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t
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r
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l

A
n
a
l
y
s
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s

(
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t
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r
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l
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)
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s

P
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s
s
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n

P
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d
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c
t
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n

L
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t

(
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n
t
e
r
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l
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)
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a
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g

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c
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s

s
t
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t
i
s
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c
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l

s
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g
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f
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c
a
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e
.
MW
-
5
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1

w
a
s

u
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e
d

a
s

t
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e

b
a
c
k
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w
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f
v
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G
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w
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M
o
n
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r
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\
2
.

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r
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u
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d
w
a
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r

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n
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g

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p
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\
J
o
h
n
s
t
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\
2
1
.

J
o
h
n
s
t
o
n

1
1
-
2
0
1
5
\
o
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Appendix A
Monitoring Well Information

October 2015 Semi-Annual Monitoring Report
Johnston County Landfill
NC Solid Waste Permit No. 51-03

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Appendix B
Laboratory Analytical Report

October 2015 Semi-Annual Monitoring Report
Johnston County Landfill
NC Solid Waste Permit No. 51-03

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Johnston County 
Department of Solid Waste Services
Mailing Address: P.O. Box 2263 // Physical Address: 680 County Home Rd.
Smithfield, NC 27577
Phone: [phone] // Fax: [phone]

November 10th, 2015 

“Fall 2015” Groundwater Sampling Event – Johnston County Landfill Facility 


Field Measurements from Detection & Assessment Well Monitoring, to include Lagoon Wells, Surface Water 
Points and Leachate/Leak Detection Points: 

In‐House Data & Sample Collector: Kevin J. Shields  

 Monitoring Well & Surface Water Event Duration: 10/26/15 through 10/30/15 
 Leachate/Leak Detection Points were sampled on the afternoons of 11/4/15 & 11/9/15** 

Detection Monitoring Wells: Dedicated.  

Well  ID # Static Water Level (ft.)        
(DTW) 
Temperature (Celsius) Turbidity    
(NTU) 
pH Specific Conductance (uS/cm)
MW – 5‐1 23.62 18.4 26.8 4.15 211.9 
MW – 5‐2 6.63 17.3 48.9 4.04 303.9 
MW – 5‐5 13.56 18.7 2.87 4.40 129.3 
MW – 5‐6 31.61 18.2 7.17 4.47 75.7 

Detection Monitoring Wells: Non‐Dedicated.  

Well  ID # Static Water 
Level (ft.)      
(DTW) 
Depth to 
Bottom of 
Well (ft.) 
Amount 
Bailed 
(Liters) 
Temperature 
(Celsius) 
Turbidity    
(NTU) 
pH Specific Conductance 
(uS/cm) 
CDMW – 3 32.52 38.75 12 16.3 6.83 5.36 24.4 
CDMW – 4 30.45 47.33 32 16.6 4.98 5.81 55.6 
CDMW – 6 9.73 37.07 51 17.0 295 6.03 81.0 
CDMW – 7 12.60 29.81 33 18.3 116 4.60 285.4 
CDMW – 8 4.74 12.00 14* 17.2 22.6 4.79 126.2 
CDMW – 9D 15.18 47.95 61 18.5 12.2 5.51 288.1 
MW – 8D 5.66 36.02 57 19.0 3.98 5.90 398.8 
MW – 9C 12.72 16.61 5* 16.4 122 4.97 114.0 
MW – 15D 8.31 27.00 35 18.6 3.29 6.82 312.1 
MW – 16D 7.72 26.15 35 18.4 6.71 5.59 227.7 

Page 


Assessment Monitoring Wells: Dedicated and Non‐Dedicated.  

Well  ID # Static 
Water 
Level 
(f )
Depth to 
Bottom of 
Well (ft.) 
Amount 
Bailed 
(Liters) 
Temperature 
(Celsius) 
Turbidity    
(NTU) 
pH Specific Conductance 
(uS/cm) 
MW – 6 36.81 N/A N/A 18.6 12.4 5.96 349.6 
MW – 7B 4.33 18.61 26 17.4 20.3 5.76 950 
MW – 11 9.01 N/A N/A 18.2 4.28 6.44 200.8 
MW – 12B 29.30 N/A N/A 18.9 5.93 5.77 452.2 
MW – 14D 7.72 33.89 49 17.5 1.54 6.73 1041 

Leachate Lagoon Monitoring Wells:  

Well  ID # Static Water Level (ft.)      
(DTW) 
Temperature (Celsius) Turbidity    (NTU)pH Specific Conductance (uS/cm)
LL # 1 19.95 18.4 4.51 5.31 108.8 
LL # 2 19.00 17.4 13.6 5.53 129.4 
LL # 3 21.70 17.8 6.28 5.39 61.3 
LL # 4 11.32 16.5 21.9 5.55 105.1 

Surface Water Points:  

Surface Water Point ID # Temperature 
(Celsius) 
Turbidity    
(NTU) 
pH Specific Conductance (uS/cm) 
SW 5 – 1 (Phase 5) 15.1 7.85 6.15 304.3 
SW 5 – 2 (Phase 5) 14.6 3.98 5.88 165.0 
CDSW – 1 (C & D) 14.0 5.94 6.89 69.0 
SW – 1A (Phases 1‐ 4) 17.4 3.24 6.53 226.0 
SW – 2   (Phases 1‐ 4) 17.0 4.05 6.81 103.0 

Leachate and Leak Detection Points:  

Leachate & Detection Points 

Temperature 
(Celsius) 
Turbidity    
(NTU) 
pH Specific Conductance (uS/cm) 
C & D 19.1 167 6.30 1998 
Phase 5 19.7 56.7 6.41 3023 
Phase 4A Collection 25.2 17.2 6.91 9720 
Phase 4A Leak Detection 21.9 76.2 5.69 517 

Legend: ID # = Identification number 
               DTW = Depth to water from top of PVC casing. 
*Denotes Bailed Dry 

Page 


Summary: 

A modification to our previous sampling schedule was realized during the semi‐annual “Spring Event” of 2014. This 
was the year 2015’s fall continuance of that change. The only difference this time being that the designated 
“Assessment Well” network was sampled for Appendix I parameters versus the Appendix II requirements of the 
spring. Accordingly, all groundwater monitoring wells, Detection and Assessment, during this event were sampled 
for Appendix I constituents. 

On 10/26/15, sampling was performed on SWPT’s 5‐1 and 5‐2. Also, Detection Well #’s 5‐1, 5‐2, 5‐5 and 5‐6 were 
purged and sampled. In the afternoon, Lagoon Well #’s LL‐1, LL‐2, LL‐3 and LL‐4 were also completed. Lastly, 
Detection Wells CDMW‐8 and CDMW‐9D were bailed for the next day’s sampling.  

On the following day, 10/27/15, CDMW‐8 and CDMW‐9D were sampled along with CDSW‐1 and Detection Well 
#’s CDMW‐6, CDMW‐3, CDMW‐4 and CDMW‐7. I started late as there was a period of rain early in the morning. In 
addition, there were spotty moments of rain throughout the day but it did not prevent sampling procedures from 
being completed. However, at the end of the afternoon the rain grew heavier and more persistent.  

Due to somewhat heavy rain on Wednesday, 10/28/15, I was not able to sample. 

On 10/29/15, SWPT–2, SWPT‐1A, Assessment Well # 14D, and Detection Well #’s MW‐15D, MW‐16D, & MW‐8D 
were bailed and sampled. Also, on the afternoon of this day, Detection Well # 9C was bailed for the next day’s 
sampling. 

On 10/30/15, Detection Well # 9C was sampled first thing in the morning. Following this, Assessment Well #’s 
MW‐7B, MW‐11, MW‐12 & MW‐6 were bailed/purged and sampled.  

On 11/1/15 I could not perform leachate sampling because of persistent rain where I had concern with 
vial/container contamination/dilution with rainwater. On 11/4/15 I sampled the Phase 4A Collection Leachate 
Point along with the Phase 4A Detection well. Finally, on 11/9/15 I was able to complete event sampling on the 
remaining leachate points, the Phase 5 manhole and the C & D riser.   

** It should be mentioned that leachate samples, of which all include BOD & Nitrate, were only able to be        
retrieved on Monday afternoons and Wednesday afternoons. This was due to the aforementioned 48‐Hour short 
hold parameters; a slight conflict the laboratory courier’s schedule and the required relay to Prism’s facility in 
Charlotte, NC. 

Comments: 

- Field parameters included: Static water level readings for dedicated wells; depth to water and depth to 
bottom readings, with water volume bailed, for non‐dedicated wells; temperature; turbidity; pH and specific 
conductance.  

- All well casings were in good physical and mechanical condition. 

- All wells both dedicated and non‐dedicated were purged or bailed, respectively, in accordance with North 
Carolina State guidelines prior to sampling. 

- Water retrieved from both CDMW‐6 was cloudy white. 

- Water retrieved from MW‐7B, even after being bailed at the 3X volume requirement, varied in quality 
between cloudy white, to clear, then back to muddy. 
Page 


- CDMW‐ 8 again bailed dry near the completion of its required 3X volume; however, recovered adequately to 
be sampled the following day. 

- Leachate Lagoon Well # 1 (LL #1) exhibited poor recovery characteristics but was able to provide enough 
water for sampling. 

- MW‐9C, during this event exhibited extremely poor recovery characteristics and scarcely provided sufficient 
water volume to be sampled the following day.  

- Water retrieved from MW‐8D and MW‐16D again emitted a sulfur odor.  

- On the first day of the event, 10/26/15, ambient air temperatures ranged from ~55F in the morning and 
only rose to the low 60’s in the afternoon. The entire day was under partly cloudy skies. As mentioned 
earlier, 10/27/15 began rainy and then cleared before 09:00. It remained overcast with periods of light rain 
until around 15:30 when it began to rain harder. The temperature for the day remained about 55F.  
10/28/15 saw persistent rain. No sampling could be performed. On 10/29/15 the sun returned with 
temperatures beginning in the mid 60’s and raising to the mid 70’s in the afternoon. On 10/30/15, the day 
was again sunny. Temperatures in the morning were in the low 50’s and increased to about 60F at midday 
when we finished sampling. As I mentioned earlier, I was only able to sample short hold parameters (BOD & 
Nitrate) on Monday afternoons and Wednesday afternoons. In view of this, and unfortunately, there was a 
heavy rain event on Monday, 11/2/15, which prevented me from sampling any leachate points, which 
include these analytes. On 11/4/15, in the afternoon, when I sampled the 4A Collection and 4A Detection 
points, the sky was overcast with a temperature of ~ 65F. However, on the afternoon of 11/9/15, when I 
completed the leachate sampling for the C & D and Phase 5 cells, there was a steady but light rain with a 
temperature of ~ 58F. Nonetheless, the rainfall was not hard enough to compromise sampling procedures. 

- After each sampling day, all sample containers were placed on ice and maintained this way until the pickup 
was made. Prism’s courier retrieved the sample coolers on 10/27/15, 11/2/15, 11/4/15 and 11/9/15.  

- I was assisted during the event by Mr. Darren C. Donnelly of the Johnston County Department of Solid 
Waste Services. 

At each Detection Well, Assessment Well, Lagoon Well and Surface Water Point, the following containers were 
filled for their corresponding analytes as prescribed in Appendix I of 40 CFR Part 258: 

 (4) 40‐ml glass vials – EPA 8260B VOC’s (2 preserved w/HCl & 2 unpreserved). 
 (1) 250‐ml plastic bottle– 6020A Metals (preserved w/HNO3) via 3010C digestion. 

At each Leachate Point, the following containers were filled for their corresponding analytes:   

 (4) 40‐ml glass vials – EPA 8260B VOC’s (2 preserved w/HCl & 2 unpreserved) – Appendix I list.  
 (1) 250‐ml plastic bottle – 6020A Metals (preserved w/HNO3) via 3010C digestion – Appendix I list. 
 (1) 1 liter plastic bottle – BOD (no preservative). 
 (1) 1 liter plastic bottle – Sulfate, Nitrate and TSS (no preservative). 
 (1) 500 ml plastic bottle – COD, NH3 and Total Phosphorus (preserved w/H2SO4). 

Kevin J. Shields 
Johnston County Department of Solid Waste Services 
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
12/01/2015
Johnston County Dept. of Public Utilities
Kevin Shields
P. O. Box 2263
Smithfield, NC NC 27577
Project: Phase 5 Leachate and C&D Leachate
Project No.: 51-03
Lab Submittal Date: 11/10/2015
Prism Work Order: 5110187
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A Greater than 30% difference between dilutions.
Aa Original analysis performed within hold time. Dilution performed outside of hold time.
B Analyte is found in the associated blank at a concentration >1/2 RL.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 20
Sample Receipt Summary
12/01/2015
Prism Work Order: 5110187
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5110187-01 11/09/15Ph 5 Leachate 11/10/15Water
5110187-02 11/09/15C&D Leachate 11/10/15Water
5110187-03 11/09/15Trip Blanks 11/10/15Water
5110187-04 11/09/15Equipment Blanks 11/10/15Water
Samples were received in good condition at 0.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 20
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5110187
12/01/2015
Summary of Detections
71 J ug/L5110187-01 Ph 5 Leachate Nitrate as N 9056A
3700 ug/L5110187-01 Ph 5 Leachate Sulfate 9056A
17000 ug/L5110187-01 Ph 5 Leachate Biochemical Oxygen Demand SM5210 B
280000 ug/L5110187-01 Ph 5 Leachate Chemical Oxygen Demand SM5220 D
1200 ug/L5110187-01 Ph 5 Leachate Phosphorus-Total SM4500-P F
120000 ug/L5110187-01 Ph 5 Leachate Total Suspended Solids SM 2540 D
100000 ug/L5110187-01 Ph 5 Leachate Ammonia as N SM4500-NH3 G
0.96 J ug/L5110187-01 Ph 5 Leachate Antimony 6020A
12 ug/L5110187-01 Ph 5 Leachate Arsenic 6020A
250 ug/L5110187-01 Ph 5 Leachate Barium 6020A
0.023 J ug/L5110187-01 Ph 5 Leachate Cadmium 6020A
4.7 B ug/L5110187-01 Ph 5 Leachate Chromium 6020A
3.9 ug/L5110187-01 Ph 5 Leachate Cobalt 6020A
1.6 J ug/L5110187-01 Ph 5 Leachate Copper 6020A
0.54 J ug/L5110187-01 Ph 5 Leachate Lead 6020A
21 ug/L5110187-01 Ph 5 Leachate Nickel 6020A
7.1 ug/L5110187-01 Ph 5 Leachate Selenium 6020A
0.048 J ug/L5110187-01 Ph 5 Leachate Silver 6020A
0.050 J ug/L5110187-01 Ph 5 Leachate Thallium 6020A
6.9 ug/L5110187-01 Ph 5 Leachate Vanadium 6020A
7.4 J ug/L5110187-01 Ph 5 Leachate Zinc 6020A
0.94 ug/L5110187-01 Ph 5 Leachate 1,1-Dichloroethane 8260B
12 ug/L5110187-01 Ph 5 Leachate 1,4-Dichlorobenzene 8260B
42 ug/L5110187-01 Ph 5 Leachate Acetone 8260B
7.9 ug/L5110187-01 Ph 5 Leachate Benzene 8260B
0.59 ug/L5110187-01 Ph 5 Leachate Chloroethane 8260B
0.80 ug/L5110187-01 Ph 5 Leachate cis-1,2-Dichloroethylene 8260B
27 ug/L5110187-01 Ph 5 Leachate Ethylbenzene 8260B
49 ug/L5110187-01 Ph 5 Leachate m,p-Xylenes 8260B
1.6 J ug/L5110187-01 Ph 5 Leachate Methyl Isobutyl Ketone 8260B
10 ug/L5110187-01 Ph 5 Leachate o-Xylene 8260B
1.4 ug/L5110187-01 Ph 5 Leachate Styrene 8260B
380 Aa ug/L5110187-01 Ph 5 Leachate Tetrahydrofuran 8260B
16 ug/L5110187-01 Ph 5 Leachate Toluene 8260B
1.6 ug/L5110187-01 Ph 5 Leachate Vinyl chloride 8260B
59 ug/L5110187-01 Ph 5 Leachate Xylenes, total 8260B
260 ug/L5110187-02 C&D Leachate Nitrate as N 9056A
150000 ug/L5110187-02 C&D Leachate Sulfate 9056A
16000 A ug/L5110187-02 C&D Leachate Biochemical Oxygen Demand SM5210 B
210000 ug/L5110187-02 C&D Leachate Chemical Oxygen Demand SM5220 D
210 ug/L5110187-02 C&D Leachate Phosphorus-Total SM4500-P F
160000 ug/L5110187-02 C&D Leachate Total Suspended Solids SM 2540 D
27000 ug/L5110187-02 C&D Leachate Ammonia as N SM4500-NH3 G
0.18 J ug/L5110187-02 C&D Leachate Antimony 6020A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 20
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5110187
12/01/2015
Summary of Detections
12 ug/L5110187-02 C&D Leachate Arsenic 6020A
180 ug/L5110187-02 C&D Leachate Barium 6020A
0.057 J ug/L5110187-02 C&D Leachate Beryllium 6020A
0.035 J ug/L5110187-02 C&D Leachate Cadmium 6020A
7.8 B ug/L5110187-02 C&D Leachate Chromium 6020A
35 ug/L5110187-02 C&D Leachate Cobalt 6020A
3.2 J ug/L5110187-02 C&D Leachate Copper 6020A
0.93 J ug/L5110187-02 C&D Leachate Lead 6020A
4.8 ug/L5110187-02 C&D Leachate Nickel 6020A
2.2 ug/L5110187-02 C&D Leachate Selenium 6020A
0.014 J ug/L5110187-02 C&D Leachate Silver 6020A
0.23 J ug/L5110187-02 C&D Leachate Thallium 6020A
6.4 ug/L5110187-02 C&D Leachate Vanadium 6020A
8.6 J ug/L5110187-02 C&D Leachate Zinc 6020A
3.0 ug/L5110187-02 C&D Leachate 1,4-Dichlorobenzene 8260B
29 ug/L5110187-02 C&D Leachate Acetone 8260B
2.3 ug/L5110187-02 C&D Leachate Benzene 8260B
2.3 ug/L5110187-02 C&D Leachate Chlorobenzene 8260B
3.4 ug/L5110187-02 C&D Leachate cis-1,2-Dichloroethylene 8260B
0.70 ug/L5110187-02 C&D Leachate Ethylbenzene 8260B
1.7 J ug/L5110187-02 C&D Leachate Methyl Ethyl Ketone (2-Butanone)8260B
44 ug/L5110187-02 C&D Leachate Tetrahydrofuran 8260B
0.57 ug/L5110187-02 C&D Leachate Toluene 8260B
2.3 ug/L5110187-02 C&D Leachate Vinyl chloride 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Ph 5 Leachate
Prism Sample ID: 5110187-01
Prism Work Order: 5110187
Time Collected: 11/09/15 12:40
Time Submitted: 11/10/15 08:40
51-03
Anions by Ion Chromatography
71 9056A P5K0215110011/10/15 19:12 CDEJug/L 37Nitrate as N
3700 9056A P5K02151100011/10/15 19:12 CDEug/L 380Sulfate
General Chemistry Parameters
17000 SM5210 B P5K03161440011/11/15 12:38 EGCug/LBiochemical Oxygen Demand
280000 SM5220 D P5K036515000011/18/15 11:45 CDLug/L 7300Chemical Oxygen Demand
1200 SM4500-P F P5K035615011/19/15 9:19 CLBug/L 13Phosphorus-Total
120000 SM 2540 D P5K027712500011/13/15 9:40 EGCug/L 800Total Suspended Solids
100000 SM4500-NH3 G P5K02142002000011/12/15 10:10 CLBug/L 1800Ammonia as N
Total Metals
0.96 6020A P5K033111.0 11/20/15 15:43 gmartJug/L 0.069Antimony
12 6020A P5K033111.0 11/20/15 15:43 gmartug/L 0.29Arsenic
250 6020A P5K033115.0 11/20/15 15:43 gmartug/L 0.041Barium
BRL 6020A P5K033111.0 11/20/15 15:43 gmartug/L 0.047Beryllium
0.023 6020A P5K033111.0 11/20/15 15:43 gmartJug/L 0.019Cadmium
4.7 6020A P5K033111.0 11/20/15 15:43 gmartBug/L 0.51Chromium
3.9 6020A P5K033111.0 11/20/15 15:43 gmartug/L 0.013Cobalt
1.6 6020A P5K033115.0 11/20/15 15:43 gmartJug/L 0.44Copper
0.54 6020A P5K033111.0 11/20/15 15:43 gmartJug/L 0.020Lead
21 6020A P5K033112.0 11/20/15 15:43 gmartug/L 0.053Nickel
7.1 6020A P5K033111.0 11/20/15 15:43 gmartug/L 0.35Selenium
0.048 6020A P5K033111.0 11/20/15 15:43 gmartJug/L 0.011Silver
0.050 6020A P5K033111.0 11/20/15 15:43 gmartJug/L 0.0093Thallium
6.9 6020A P5K033115.0 11/20/15 15:43 gmartug/L 2.5Vanadium
7.4 6020A P5K033111011/20/15 15:43 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0661,1,2-Trichloroethane
0.94 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K044611.0 11/20/15 19:26 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K044612.0 11/20/15 19:26 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.111,2-Dichloropropane
12 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.0501,4-Dichlorobenzene
42 8260B P5K044615.0 11/20/15 19:26 KDMug/L 0.31Acetone
BRL 8260B P5K044612011/20/15 19:26 KDMug/L 0.20Acrylonitrile
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Ph 5 Leachate
Prism Sample ID: 5110187-01
Prism Work Order: 5110187
Time Collected: 11/09/15 12:40
Time Submitted: 11/10/15 08:40
51-03
7.9 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.048Benzene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.14Bromochloromethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.062Bromodichloromethane
BRL 8260B P5K044611.0 11/20/15 19:26 KDMug/L 0.040Bromoform
BRL 8260B P5K044611.0 11/20/15 19:26 KDMug/L 0.18Bromomethane
BRL 8260B P5K044615.0 11/20/15 19:26 KDMug/L 0.075Carbon disulfide
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.062Chlorobenzene
0.59 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.22Chloroethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.076Chloroform
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.079Chloromethane
0.80 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.081Dibromochloromethane
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.065Dibromomethane
27 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.061Ethylbenzene
49 8260B P5K044611.0 11/20/15 19:26 KDMug/L 0.12m,p-Xylenes
BRL 8260B P5K044615.0 11/20/15 19:26 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5K044615.0 11/20/15 19:26 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K044615.0 11/20/15 19:26 KDMug/L 0.33Methyl Iodide
1.6 8260B P5K044615.0 11/20/15 19:26 KDMJug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K044611.0 11/20/15 19:26 KDMug/L 0.083Methylene Chloride
10 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.044o-Xylene
1.4 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.047Styrene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.098Tetrachloroethylene
380 8260B P5K04461010011/24/15 16:16 KDMAaug/L 1.6Tetrahydrofuran
16 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.044Toluene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K044611011/20/15 19:26 KDMug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.078Trichloroethylene
BRL 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P5K044612.0 11/20/15 19:26 KDMug/L 0.060Vinyl acetate
1.6 8260B P5K044610.50 11/20/15 19:26 KDMug/L 0.097Vinyl chloride
59 8260B P5K044613.0 11/20/15 19:26 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124101 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-12396 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: C&D Leachate
Prism Sample ID: 5110187-02
Prism Work Order: 5110187
Time Collected: 11/09/15 14:09
Time Submitted: 11/10/15 08:40
51-03
Anions by Ion Chromatography
260 9056A P5K0215110011/10/15 19:29 CDEug/L 37Nitrate as N
150000 9056A P5K02151100011/10/15 19:29 CDEug/L 380Sulfate
General Chemistry Parameters
16000 SM5210 B P5K03161440011/11/15 12:38 EGCAug/LBiochemical Oxygen Demand
210000 SM5220 D P5K036615000011/18/15 11:45 CDLug/L 7300Chemical Oxygen Demand
210 SM4500-P F P5K035615011/19/15 9:19 CLBug/L 13Phosphorus-Total
160000 SM 2540 D P5K02771620011/13/15 9:40 EGCug/L 800Total Suspended Solids
27000 SM4500-NH3 G P5K021420200011/12/15 10:10 CLBug/L 180Ammonia as N
Total Metals
0.18 6020A P5K033111.0 11/20/15 15:46 gmartJug/L 0.069Antimony
12 6020A P5K033111.0 11/20/15 15:46 gmartug/L 0.29Arsenic
180 6020A P5K033115.0 11/20/15 15:46 gmartug/L 0.041Barium
0.057 6020A P5K033111.0 11/20/15 15:46 gmartJug/L 0.047Beryllium
0.035 6020A P5K033111.0 11/20/15 15:46 gmartJug/L 0.019Cadmium
7.8 6020A P5K033111.0 11/20/15 15:46 gmartBug/L 0.51Chromium
35 6020A P5K033111.0 11/20/15 15:46 gmartug/L 0.013Cobalt
3.2 6020A P5K033115.0 11/20/15 15:46 gmartJug/L 0.44Copper
0.93 6020A P5K033111.0 11/20/15 15:46 gmartJug/L 0.020Lead
4.8 6020A P5K033112.0 11/20/15 15:46 gmartug/L 0.053Nickel
2.2 6020A P5K033111.0 11/20/15 15:46 gmartug/L 0.35Selenium
0.014 6020A P5K033111.0 11/20/15 15:46 gmartJug/L 0.011Silver
0.23 6020A P5K033111.0 11/20/15 15:46 gmartJug/L 0.0093Thallium
6.4 6020A P5K033115.0 11/20/15 15:46 gmartug/L 2.5Vanadium
8.6 6020A P5K033111011/20/15 15:46 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K044611.0 11/20/15 19:51 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K044612.0 11/20/15 19:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.111,2-Dichloropropane
3.0 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.0501,4-Dichlorobenzene
29 8260B P5K044615.0 11/20/15 19:51 KDMug/L 0.31Acetone
BRL 8260B P5K044612011/20/15 19:51 KDMug/L 0.20Acrylonitrile
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: C&D Leachate
Prism Sample ID: 5110187-02
Prism Work Order: 5110187
Time Collected: 11/09/15 14:09
Time Submitted: 11/10/15 08:40
51-03
2.3 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.048Benzene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.14Bromochloromethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.062Bromodichloromethane
BRL 8260B P5K044611.0 11/20/15 19:51 KDMug/L 0.040Bromoform
BRL 8260B P5K044611.0 11/20/15 19:51 KDMug/L 0.18Bromomethane
BRL 8260B P5K044615.0 11/20/15 19:51 KDMug/L 0.075Carbon disulfide
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.11Carbon Tetrachloride
2.3 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.062Chlorobenzene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.22Chloroethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.076Chloroform
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.079Chloromethane
3.4 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.081Dibromochloromethane
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.065Dibromomethane
0.70 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.061Ethylbenzene
BRL 8260B P5K044611.0 11/20/15 19:51 KDMug/L 0.12m,p-Xylenes
BRL 8260B P5K044615.0 11/20/15 19:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
1.7 8260B P5K044615.0 11/20/15 19:51 KDMJug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K044615.0 11/20/15 19:51 KDMug/L 0.33Methyl Iodide
BRL 8260B P5K044615.0 11/20/15 19:51 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K044611.0 11/20/15 19:51 KDMug/L 0.083Methylene Chloride
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.044o-Xylene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.047Styrene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.098Tetrachloroethylene
44 8260B P5K044611011/20/15 19:51 KDMug/L 0.16Tetrahydrofuran
0.57 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.044Toluene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K044611011/20/15 19:51 KDMug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.078Trichloroethylene
BRL 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P5K044612.0 11/20/15 19:51 KDMug/L 0.060Vinyl acetate
2.3 8260B P5K044610.50 11/20/15 19:51 KDMug/L 0.097Vinyl chloride
BRL 8260B P5K044613.0 11/20/15 19:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124102 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Trip Blanks
Prism Sample ID: 5110187-03
Prism Work Order: 5110187
Time Collected: 11/09/15 00:00
Time Submitted: 11/10/15 08:40
51-03
Volatile Organic Compounds by GC/MS
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K044611.0 11/20/15 16:54 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K044612.0 11/20/15 16:54 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P5K044615.0 11/20/15 16:54 KDMug/L 0.31Acetone
BRL 8260B P5K044612011/20/15 16:54 KDMug/L 0.20Acrylonitrile
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.048Benzene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.14Bromochloromethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.062Bromodichloromethane
BRL 8260B P5K044611.0 11/20/15 16:54 KDMug/L 0.040Bromoform
BRL 8260B P5K044611.0 11/20/15 16:54 KDMug/L 0.18Bromomethane
BRL 8260B P5K044615.0 11/20/15 16:54 KDMug/L 0.075Carbon disulfide
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.062Chlorobenzene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.22Chloroethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.076Chloroform
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.079Chloromethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.081Dibromochloromethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.065Dibromomethane
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.061Ethylbenzene
BRL 8260B P5K044611.0 11/20/15 16:54 KDMug/L 0.12m,p-Xylenes
BRL 8260B P5K044615.0 11/20/15 16:54 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5K044615.0 11/20/15 16:54 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K044615.0 11/20/15 16:54 KDMug/L 0.33Methyl Iodide
BRL 8260B P5K044615.0 11/20/15 16:54 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K044611.0 11/20/15 16:54 KDMug/L 0.083Methylene Chloride
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.044o-Xylene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.047Styrene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P5K044611011/20/15 16:54 KDMug/L 0.16Tetrahydrofuran
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.044Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Trip Blanks
Prism Sample ID: 5110187-03
Prism Work Order: 5110187
Time Collected: 11/09/15 00:00
Time Submitted: 11/10/15 08:40
51-03
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K044611011/20/15 16:54 KDMug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.078Trichloroethylene
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P5K044612.0 11/20/15 16:54 KDMug/L 0.060Vinyl acetate
BRL 8260B P5K044610.50 11/20/15 16:54 KDMug/L 0.097Vinyl chloride
BRL 8260B P5K044613.0 11/20/15 16:54 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124101 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Equipment Blanks
Prism Sample ID: 5110187-04
Prism Work Order: 5110187
Time Collected: 11/09/15 16:04
Time Submitted: 11/10/15 08:40
51-03
Volatile Organic Compounds by GC/MS
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K044611.0 11/20/15 17:19 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K044612.0 11/20/15 17:19 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P5K044615.0 11/20/15 17:19 KDMug/L 0.31Acetone
BRL 8260B P5K044612011/20/15 17:19 KDMug/L 0.20Acrylonitrile
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.048Benzene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.14Bromochloromethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.062Bromodichloromethane
BRL 8260B P5K044611.0 11/20/15 17:19 KDMug/L 0.040Bromoform
BRL 8260B P5K044611.0 11/20/15 17:19 KDMug/L 0.18Bromomethane
BRL 8260B P5K044615.0 11/20/15 17:19 KDMug/L 0.075Carbon disulfide
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.062Chlorobenzene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.22Chloroethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.076Chloroform
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.079Chloromethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.081Dibromochloromethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.065Dibromomethane
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.061Ethylbenzene
BRL 8260B P5K044611.0 11/20/15 17:19 KDMug/L 0.12m,p-Xylenes
BRL 8260B P5K044615.0 11/20/15 17:19 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5K044615.0 11/20/15 17:19 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K044615.0 11/20/15 17:19 KDMug/L 0.33Methyl Iodide
BRL 8260B P5K044615.0 11/20/15 17:19 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K044611.0 11/20/15 17:19 KDMug/L 0.083Methylene Chloride
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.044o-Xylene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.047Styrene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P5K044611011/20/15 17:19 KDMug/L 0.16Tetrahydrofuran
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.044Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 20
Laboratory Report
12/01/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Equipment Blanks
Prism Sample ID: 5110187-04
Prism Work Order: 5110187
Time Collected: 11/09/15 16:04
Time Submitted: 11/10/15 08:40
51-03
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K044611011/20/15 17:19 KDMug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.078Trichloroethylene
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P5K044612.0 11/20/15 17:19 KDMug/L 0.060Vinyl acetate
BRL 8260B P5K044610.50 11/20/15 17:19 KDMug/L 0.097Vinyl chloride
BRL 8260B P5K044613.0 11/20/15 17:19 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-12398 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 20
12/1/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110187
Time Submitted: 11/10/2015 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5K0446 - 5030B
Blank (P5K0446-BLK1)Prepared & Analyzed: 11/20/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 20
12/1/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110187
Time Submitted: 11/10/2015 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5K0446 - 5030B
Blank (P5K0446-BLK1)Prepared & Analyzed: 11/20/15
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10351.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.7
ug/L 50.00 77-123Surrogate: Toluene-d8 9748.5
LCS (P5K0446-BS1)Prepared & Analyzed: 11/20/15
1,1-Dichloroethylene ug/L20.9 0.50 20.00 70-154105
Benzene ug/L21.1 0.50 20.00 77-128105
Chlorobenzene ug/L21.5 0.50 20.00 78-119107
Toluene ug/L21.1 0.50 20.00 76-131106
Trichloroethylene ug/L21.6 0.50 20.00 77-133108
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 77-123Surrogate: Toluene-d8 10250.8
LCS Dup (P5K0446-BSD1)Prepared & Analyzed: 11/20/15
1,1-Dichloroethylene ug/L20.3 0.50 20.00 2070-154101 3
Benzene ug/L20.5 0.50 20.00 2077-128102 3
Chlorobenzene ug/L21.3 0.50 20.00 2078-119106 0.9
Toluene ug/L20.8 0.50 20.00 2076-131104 1
Trichloroethylene ug/L21.0 0.50 20.00 2077-133105 3
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.5
ug/L 50.00 77-123Surrogate: Toluene-d8 10351.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 20
12/1/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110187
Time Submitted: 11/10/2015 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5K0331 - 3005A
Blank (P5K0331-BLK1)Prepared: 11/17/15 Analyzed: 11/18/15
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L0.325 5.0 J
Beryllium ug/LBRL1.0
Cadmium ug/LBRL1.0
Chromium ug/L1.17 1.0 B
Cobalt ug/LBRL1.0
Copper ug/LBRL5.0
Lead ug/L0.168 1.0 J
Nickel ug/L0.0713 2.0 J
Selenium ug/LBRL1.0
Silver ug/L0.0167 1.0 J
Thallium ug/L0.0757 1.0 J
Vanadium ug/LBRL5.0
Zinc ug/LBRL10
LCS (P5K0331-BS1)Prepared: 11/17/15 Analyzed: 11/18/15
Antimony ug/L95.2 1.0 100.0 80-12095
Arsenic ug/L97.0 1.0 100.0 80-12097
Barium ug/L99.9 5.0 100.0 80-120100
Beryllium ug/L97.8 1.0 100.0 80-12098
Cadmium ug/L97.1 1.0 100.0 80-12097
Chromium ug/L99.4 1.0 100.0 B80-12099
Cobalt ug/L97.8 1.0 100.0 80-12098
Copper ug/L1005.0 100.0 80-120100
Lead ug/L1001.0 100.0 80-120100
Nickel ug/L99.6 2.0 100.0 80-120100
Selenium ug/L93.8 1.0 100.0 80-12094
Silver ug/L97.2 1.0 100.0 80-12097
Thallium ug/L98.7 1.0 100.0 80-12099
Vanadium ug/L95.9 5.0 100.0 80-12096
Zinc ug/L95.3 10 100.0 80-12095
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 20
12/1/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110187
Time Submitted: 11/10/2015 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P5K0215 - NO PREP
Blank (P5K0215-BLK1)Prepared & Analyzed: 11/10/15
Nitrate as N ug/LBRL100
Sulfate ug/LBRL1000
LCS (P5K0215-BS1)Prepared & Analyzed: 11/10/15
Nitrate as N ug/L3770100 4000 80-12094
Sulfate ug/L386001000 40200 80-12096
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 20
12/1/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110187
Time Submitted: 11/10/2015 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5K0214 - NO PREP
Blank (P5K0214-BLK1)Prepared: 11/11/15 Analyzed: 11/12/15
Ammonia as N ug/LBRL100
LCS (P5K0214-BS1)Prepared: 11/11/15 Analyzed: 11/12/15
Ammonia as N ug/L2490100 2500 90-110100
Batch P5K0277 - NO PREP
Blank (P5K0277-BLK1)Prepared & Analyzed: 11/13/15
Total Suspended Solids ug/LBRL5000
LCS (P5K0277-BS1)Prepared & Analyzed: 11/13/15
Total Suspended Solids ug/L4800005000 477000 90-110101
Duplicate (P5K0277-DUP1)Prepared & Analyzed: 11/13/15 Source: 5110187-01
Total Suspended Solids ug/L1200005000 120000 207
Batch P5K0316 - NO PREP
Blank (P5K0316-BLK1)Prepared & Analyzed: 11/11/15
Biochemical Oxygen Demand ug/L25.0 2000 J
LCS (P5K0316-BS1)Prepared & Analyzed: 11/11/15
Biochemical Oxygen Demand ug/L2060002000 198000 84.6-115.4104
Duplicate (P5K0316-DUP1)Prepared & Analyzed: 11/11/15 Source: 5110187-01
Biochemical Oxygen Demand ug/L188002000 17500 307
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 20
12/1/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Phase 5 Leachate and C&D
Leachate
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110187
Time Submitted: 11/10/2015 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5K0356 - SM4500-PB5
Blank (P5K0356-BLK1)Prepared: 11/18/15 Analyzed: 11/19/15
Phosphorus-Total ug/LBRL50
LCS (P5K0356-BS1)Prepared: 11/18/15 Analyzed: 11/19/15
Phosphorus-Total ug/L1930 50 2000 90-11097
Batch P5K0365 - NO PREP
Blank (P5K0365-BLK1)Prepared & Analyzed: 11/18/15
Chemical Oxygen Demand ug/LBRL50000
LCS (P5K0365-BS1)Prepared & Analyzed: 11/18/15
Chemical Oxygen Demand ug/L50500050000 500000 90-110101
Batch P5K0366 - NO PREP
Blank (P5K0366-BLK1)Prepared & Analyzed: 11/18/15
Chemical Oxygen Demand ug/LBRL50000
LCS (P5K0366-BS1)Prepared & Analyzed: 11/18/15
Chemical Oxygen Demand ug/L50800050000 500000 90-110102
Sample Extraction Data
Prep Method: SM4500-PB5
Lab Number Batch Date/TimeInitialFinal
P5K03565110187-01 11/18/15 11:3050 50mL mL
P5K03565110187-02 11/18/15 11:3050 50mL mL
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P5K03315110187-01 11/17/15 8:4550 50mL mL
P5K03315110187-02 11/17/15 8:4550 50mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P5K04465110187-01 11/20/15 8:1210 10mL mL
P5K04465110187-01 11/20/15 8:1210 10mL mL
P5K04465110187-02 11/20/15 8:1210 10mL mL
P5K04465110187-03 11/20/15 8:1210 10mL mL
P5K04465110187-04 11/20/15 8:1210 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 20
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
12/04/2015
Johnston County Dept. of Public Utilities
Kevin Shields
P. O. Box 2263
Smithfield, NC NC 27577
Project: Detect.Monitor. Networks & SWPTs
Project No.: 51-03
Lab Submittal Date: 11/03/2015
Prism Work Order: 5110038
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
This is a Revised Report and supercedes the original laboratory report dated 12/1/15. Lead and Chromium
reanalyzed at the request of the client on Sample ID MW-9C.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 32
Sample Receipt Summary
12/04/2015
Prism Work Order: 5110038
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5110038-01 10/29/15SWPT-2 11/03/15Water
5110038-02 10/29/15SWPT-1A 11/03/15Water
5110038-03 10/29/15MW-14D 11/03/15Water
5110038-04 10/29/15MW-15D 11/03/15Water
5110038-05 10/29/15MW-16D 11/03/15Water
5110038-06 10/30/15MW-9C 11/03/15Water
5110038-07 10/30/15Field Blank 11/03/15Water
5110038-08 10/30/15Trip Blank 11/03/15Water
Samples were received in good condition at 0.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 32
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5110038
12/04/2015
Summary of Detections
0.73 J ug/L5110038-01 SWPT-2 Arsenic 6020A
25 ug/L5110038-01 SWPT-2 Barium 6020A
0.019 J ug/L5110038-01 SWPT-2 Cadmium 6020A
1.1 B ug/L5110038-01 SWPT-2 Chromium 6020A
0.36 J ug/L5110038-01 SWPT-2 Cobalt 6020A
1.1 J ug/L5110038-01 SWPT-2 Copper 6020A
0.41 J ug/L5110038-01 SWPT-2 Lead 6020A
0.98 J ug/L5110038-01 SWPT-2 Nickel 6020A
0.032 J ug/L5110038-01 SWPT-2 Thallium 6020A
2.6 J ug/L5110038-01 SWPT-2 Zinc 6020A
31 ug/L5110038-01 SWPT-2 Acetone 8260B
4.7 J ug/L5110038-01 SWPT-2 Methyl Ethyl Ketone (2-Butanone)8260B
0.29 J ug/L5110038-02 SWPT-1A Arsenic 6020A
26 ug/L5110038-02 SWPT-1A Barium 6020A
1.2 B ug/L5110038-02 SWPT-1A Chromium 6020A
0.51 J ug/L5110038-02 SWPT-1A Cobalt 6020A
1.2 J ug/L5110038-02 SWPT-1A Copper 6020A
0.36 J ug/L5110038-02 SWPT-1A Lead 6020A
1.8 J ug/L5110038-02 SWPT-1A Nickel 6020A
0.026 J ug/L5110038-02 SWPT-1A Thallium 6020A
3.0 J ug/L5110038-02 SWPT-1A Zinc 6020A
77 ug/L5110038-02 SWPT-1A Acetone 8260B
0.52 ug/L5110038-02 SWPT-1A Chloromethane 8260B
1.1 J ug/L5110038-02 SWPT-1A Methyl Butyl Ketone (2-Hexanone)8260B
12 ug/L5110038-02 SWPT-1A Methyl Ethyl Ketone (2-Butanone)8260B
0.81 J ug/L5110038-03 MW-14D Arsenic 6020A
2.8 J ug/L5110038-03 MW-14D Barium 6020A
0.18 J ug/L5110038-03 MW-14D Cadmium 6020A
1.0 B ug/L5110038-03 MW-14D Chromium 6020A
0.34 J ug/L5110038-03 MW-14D Cobalt 6020A
0.79 J ug/L5110038-03 MW-14D Copper 6020A
0.31 J ug/L5110038-03 MW-14D Lead 6020A
0.65 J ug/L5110038-03 MW-14D Nickel 6020A
3.9 ug/L5110038-03 MW-14D Selenium 6020A
0.065 J ug/L5110038-03 MW-14D Silver 6020A
0.023 J ug/L5110038-03 MW-14D Thallium 6020A
1.3 J ug/L5110038-03 MW-14D Zinc 6020A
3.0 ug/L5110038-03 MW-14D 1,1-Dichloroethane 8260B
0.56 ug/L5110038-03 MW-14D 1,2-Dichloropropane 8260B
2.5 ug/L5110038-03 MW-14D 1,4-Dichlorobenzene 8260B
23 ug/L5110038-03 MW-14D Acetone 8260B
4.5 ug/L5110038-03 MW-14D Chlorobenzene 8260B
2.5 ug/L5110038-03 MW-14D cis-1,2-Dichloroethylene 8260B
3.2 J ug/L5110038-03 MW-14D Methyl Ethyl Ketone (2-Butanone)8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 32
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5110038
12/04/2015
Summary of Detections
1.1 ug/L5110038-04 MW-15D Arsenic 6020A
23 ug/L5110038-04 MW-15D Barium 6020A
1.3 B ug/L5110038-04 MW-15D Chromium 6020A
0.47 J ug/L5110038-04 MW-15D Cobalt 6020A
0.52 J ug/L5110038-04 MW-15D Copper 6020A
0.42 J ug/L5110038-04 MW-15D Lead 6020A
1.4 J ug/L5110038-04 MW-15D Nickel 6020A
0.021 J ug/L5110038-04 MW-15D Thallium 6020A
2.9 J ug/L5110038-04 MW-15D Zinc 6020A
20 ug/L5110038-04 MW-15D Acetone 8260B
3.0 J ug/L5110038-04 MW-15D Methyl Ethyl Ketone (2-Butanone)8260B
62 ug/L5110038-05 MW-16D Barium 6020A
0.15 J ug/L5110038-05 MW-16D Beryllium 6020A
2.9 B ug/L5110038-05 MW-16D Chromium 6020A
0.42 J ug/L5110038-05 MW-16D Cobalt 6020A
0.67 J ug/L5110038-05 MW-16D Copper 6020A
0.34 J ug/L5110038-05 MW-16D Lead 6020A
1.1 J ug/L5110038-05 MW-16D Nickel 6020A
0.52 J ug/L5110038-05 MW-16D Selenium 6020A
0.013 J ug/L5110038-05 MW-16D Thallium 6020A
4.5 J ug/L5110038-05 MW-16D Zinc 6020A
43 ug/L5110038-05 MW-16D Acetone 8260B
0.73 J ug/L5110038-05 MW-16D Methyl Butyl Ketone (2-Hexanone)8260B
6.0 ug/L5110038-05 MW-16D Methyl Ethyl Ketone (2-Butanone)8260B
0.93 J ug/L5110038-06 MW-9C Arsenic 6020A
33 ug/L5110038-06 MW-9C Barium 6020A
1.0 ug/L5110038-06 MW-9C Beryllium 6020A
0.077 J ug/L5110038-06 MW-9C Cadmium 6020A
12 B ug/L5110038-06 MW-9C Chromium 6020A
28 ug/L5110038-06 MW-9C Cobalt 6020A
21 ug/L5110038-06 MW-9C Copper 6020A
10 ug/L5110038-06 MW-9C Lead 6020A
36 ug/L5110038-06 MW-9C Nickel 6020A
1.1 ug/L5110038-06 MW-9C Selenium 6020A
0.055 J ug/L5110038-06 MW-9C Silver 6020A
0.061 J ug/L5110038-06 MW-9C Thallium 6020A
6.4 ug/L5110038-06 MW-9C Vanadium 6020A
130 ug/L5110038-06 MW-9C Zinc 6020A
8.6 ug/L5110038-06 MW-9C Acetone 8260B
1.8 J ug/L5110038-06 MW-9C Methyl Ethyl Ketone (2-Butanone)8260B
12 B ug/L5110038-06RE1 MW-9C Chromium 6020A
10 ug/L5110038-06RE1 MW-9C Lead 6020A
8.5 ug/L5110038-06RE2 MW-9C Chromium 6020A
8.2 ug/L5110038-07 Field Blank Acetone 8260B
1.1 J ug/L5110038-07 Field Blank Methyl Ethyl Ketone (2-Butanone)8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 32
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: SWPT-2
Prism Sample ID: 5110038-01
Prism Work Order: 5110038
Time Collected: 10/29/15 08:49
Time Submitted: 11/03/15 08:25
51-03
Total Metals
BRL 6020A P5K018111.0 11/12/15 16:20 gmartug/L 0.069Antimony
0.73 6020A P5K018111.0 11/12/15 16:20 gmartJug/L 0.29Arsenic
25 6020A P5K018115.0 11/12/15 16:20 gmartug/L 0.041Barium
BRL 6020A P5K018111.0 11/12/15 16:20 gmartug/L 0.047Beryllium
0.019 6020A P5K018111.0 11/12/15 16:20 gmartJug/L 0.019Cadmium
1.1 6020A P5K032911.0 11/17/15 17:39 gmartBug/L 0.51Chromium
0.36 6020A P5K018111.0 11/12/15 16:20 gmartJug/L 0.013Cobalt
1.1 6020A P5K018115.0 11/12/15 16:20 gmartJug/L 0.44Copper
0.41 6020A P5K018111.0 11/12/15 16:20 gmartJug/L 0.020Lead
0.98 6020A P5K018112.0 11/12/15 16:20 gmartJug/L 0.053Nickel
BRL 6020A P5K018111.0 11/12/15 16:20 gmartug/L 0.35Selenium
BRL 6020A P5K018111.0 11/12/15 16:20 gmartug/L 0.011Silver
0.032 6020A P5K018111.0 11/12/15 16:20 gmartJug/L 0.0093Thallium
BRL 6020A P5K018115.0 11/12/15 16:20 gmartug/L 2.5Vanadium
2.6 6020A P5K018111011/12/15 16:20 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 16:54 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 16:54 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.0501,4-Dichlorobenzene
31 8260B P5K027115.0 11/12/15 16:54 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 16:54 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 16:54 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 16:54 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 16:54 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.076Chloroform
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: SWPT-2
Prism Sample ID: 5110038-01
Prism Work Order: 5110038
Time Collected: 10/29/15 08:49
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.079Chloromethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 16:54 CGPug/L 0.12m,p-Xylenes
BRL 8260B P5K027115.0 11/12/15 16:54 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
4.7 8260B P5K027115.0 11/12/15 16:54 CGPJug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 16:54 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 16:54 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 16:54 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 16:54 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.044Toluene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 16:54 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 16:54 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 16:54 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 16:54 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: SWPT-1A
Prism Sample ID: 5110038-02
Prism Work Order: 5110038
Time Collected: 10/29/15 09:27
Time Submitted: 11/03/15 08:25
51-03
Total Metals
BRL 6020A P5K018111.0 11/12/15 16:25 gmartug/L 0.069Antimony
0.29 6020A P5K018111.0 11/12/15 16:25 gmartJug/L 0.29Arsenic
26 6020A P5K018115.0 11/12/15 16:25 gmartug/L 0.041Barium
BRL 6020A P5K018111.0 11/12/15 16:25 gmartug/L 0.047Beryllium
BRL 6020A P5K018111.0 11/12/15 16:25 gmartug/L 0.019Cadmium
1.2 6020A P5K032911.0 11/17/15 17:42 gmartBug/L 0.51Chromium
0.51 6020A P5K018111.0 11/12/15 16:25 gmartJug/L 0.013Cobalt
1.2 6020A P5K018115.0 11/12/15 16:25 gmartJug/L 0.44Copper
0.36 6020A P5K018111.0 11/12/15 16:25 gmartJug/L 0.020Lead
1.8 6020A P5K018112.0 11/12/15 16:25 gmartJug/L 0.053Nickel
BRL 6020A P5K018111.0 11/12/15 16:25 gmartug/L 0.35Selenium
BRL 6020A P5K018111.0 11/12/15 16:25 gmartug/L 0.011Silver
0.026 6020A P5K018111.0 11/12/15 16:25 gmartJug/L 0.0093Thallium
BRL 6020A P5K018115.0 11/12/15 16:25 gmartug/L 2.5Vanadium
3.0 6020A P5K018111011/12/15 16:25 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 17:20 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 17:20 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.0501,4-Dichlorobenzene
77 8260B P5K027115.0 11/12/15 17:20 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 17:20 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 17:20 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 17:20 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 17:20 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.076Chloroform
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: SWPT-1A
Prism Sample ID: 5110038-02
Prism Work Order: 5110038
Time Collected: 10/29/15 09:27
Time Submitted: 11/03/15 08:25
51-03
0.52 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.079Chloromethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 17:20 CGPug/L 0.12m,p-Xylenes
1.1 8260B P5K027115.0 11/12/15 17:20 CGPJug/L 0.065Methyl Butyl Ketone (2-Hexanone)
12 8260B P5K027115.0 11/12/15 17:20 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 17:20 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 17:20 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 17:20 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 17:20 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.044Toluene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 17:20 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 17:20 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 17:20 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 17:20 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-14D
Prism Sample ID: 5110038-03
Prism Work Order: 5110038
Time Collected: 10/29/15 11:35
Time Submitted: 11/03/15 08:25
51-03
Total Metals
BRL 6020A P5K018111.0 11/12/15 16:30 gmartug/L 0.069Antimony
0.81 6020A P5K018111.0 11/12/15 16:30 gmartJug/L 0.29Arsenic
2.8 6020A P5K018115.0 11/12/15 16:30 gmartJug/L 0.041Barium
BRL 6020A P5K018111.0 11/12/15 16:30 gmartug/L 0.047Beryllium
0.18 6020A P5K018111.0 11/12/15 16:30 gmartJug/L 0.019Cadmium
1.0 6020A P5K032911.0 11/17/15 17:46 gmartBug/L 0.51Chromium
0.34 6020A P5K018111.0 11/12/15 16:30 gmartJug/L 0.013Cobalt
0.79 6020A P5K018115.0 11/12/15 16:30 gmartJug/L 0.44Copper
0.31 6020A P5K018111.0 11/12/15 16:30 gmartJug/L 0.020Lead
0.65 6020A P5K018112.0 11/12/15 16:30 gmartJug/L 0.053Nickel
3.9 6020A P5K018111.0 11/12/15 16:30 gmartug/L 0.35Selenium
0.065 6020A P5K018111.0 11/12/15 16:30 gmartJug/L 0.011Silver
0.023 6020A P5K018111.0 11/12/15 16:30 gmartJug/L 0.0093Thallium
BRL 6020A P5K018115.0 11/12/15 16:30 gmartug/L 2.5Vanadium
1.3 6020A P5K018111011/12/15 16:30 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0661,1,2-Trichloroethane
3.0 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 17:46 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 17:46 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0661,2-Dichloroethane
0.56 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.111,2-Dichloropropane
2.5 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.0501,4-Dichlorobenzene
23 8260B P5K027115.0 11/12/15 17:46 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 17:46 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 17:46 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 17:46 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 17:46 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.11Carbon Tetrachloride
4.5 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.076Chloroform
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-14D
Prism Sample ID: 5110038-03
Prism Work Order: 5110038
Time Collected: 10/29/15 11:35
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.079Chloromethane
2.5 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 17:46 CGPug/L 0.12m,p-Xylenes
BRL 8260B P5K027115.0 11/12/15 17:46 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
3.2 8260B P5K027115.0 11/12/15 22:30 CGPJug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 17:46 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 17:46 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 17:46 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 17:46 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.044Toluene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 17:46 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 17:46 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 17:46 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 17:46 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-15D
Prism Sample ID: 5110038-04
Prism Work Order: 5110038
Time Collected: 10/29/15 12:02
Time Submitted: 11/03/15 08:25
51-03
Total Metals
BRL 6020A P5K018111.0 11/12/15 16:34 gmartug/L 0.069Antimony
1.1 6020A P5K018111.0 11/12/15 16:34 gmartug/L 0.29Arsenic
23 6020A P5K018115.0 11/12/15 16:34 gmartug/L 0.041Barium
BRL 6020A P5K018111.0 11/12/15 16:34 gmartug/L 0.047Beryllium
BRL 6020A P5K018111.0 11/12/15 16:34 gmartug/L 0.019Cadmium
1.3 6020A P5K032911.0 11/17/15 17:49 gmartBug/L 0.51Chromium
0.47 6020A P5K018111.0 11/12/15 16:34 gmartJug/L 0.013Cobalt
0.52 6020A P5K018115.0 11/12/15 16:34 gmartJug/L 0.44Copper
0.42 6020A P5K018111.0 11/12/15 16:34 gmartJug/L 0.020Lead
1.4 6020A P5K018112.0 11/12/15 16:34 gmartJug/L 0.053Nickel
BRL 6020A P5K018111.0 11/12/15 16:34 gmartug/L 0.35Selenium
BRL 6020A P5K018111.0 11/12/15 16:34 gmartug/L 0.011Silver
0.021 6020A P5K018111.0 11/12/15 16:34 gmartJug/L 0.0093Thallium
BRL 6020A P5K018115.0 11/12/15 16:34 gmartug/L 2.5Vanadium
2.9 6020A P5K018111011/12/15 16:34 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 18:11 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 18:11 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.0501,4-Dichlorobenzene
20 8260B P5K027115.0 11/12/15 18:11 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 18:11 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 18:11 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 18:11 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 18:11 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.076Chloroform
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-15D
Prism Sample ID: 5110038-04
Prism Work Order: 5110038
Time Collected: 10/29/15 12:02
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.079Chloromethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 18:11 CGPug/L 0.12m,p-Xylenes
BRL 8260B P5K027115.0 11/12/15 18:11 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
3.0 8260B P5K027115.0 11/12/15 18:11 CGPJug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 18:11 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 18:11 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 18:11 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 18:11 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.044Toluene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 18:11 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 18:11 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 18:11 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 18:11 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-16D
Prism Sample ID: 5110038-05
Prism Work Order: 5110038
Time Collected: 10/29/15 12:46
Time Submitted: 11/03/15 08:25
51-03
Total Metals
BRL 6020A P5K018111.0 11/12/15 16:38 gmartug/L 0.069Antimony
BRL 6020A P5K018111.0 11/12/15 16:38 gmartug/L 0.29Arsenic
62 6020A P5K018115.0 11/12/15 16:38 gmartug/L 0.041Barium
0.15 6020A P5K018111.0 11/12/15 16:38 gmartJug/L 0.047Beryllium
BRL 6020A P5K018111.0 11/12/15 16:38 gmartug/L 0.019Cadmium
2.9 6020A P5K032911.0 11/17/15 17:53 gmartBug/L 0.51Chromium
0.42 6020A P5K018111.0 11/12/15 16:38 gmartJug/L 0.013Cobalt
0.67 6020A P5K018115.0 11/12/15 16:38 gmartJug/L 0.44Copper
0.34 6020A P5K018111.0 11/12/15 16:38 gmartJug/L 0.020Lead
1.1 6020A P5K018112.0 11/12/15 16:38 gmartJug/L 0.053Nickel
0.52 6020A P5K018111.0 11/12/15 16:38 gmartJug/L 0.35Selenium
BRL 6020A P5K018111.0 11/12/15 16:38 gmartug/L 0.011Silver
0.013 6020A P5K018111.0 11/12/15 16:38 gmartJug/L 0.0093Thallium
BRL 6020A P5K018115.0 11/12/15 16:38 gmartug/L 2.5Vanadium
4.5 6020A P5K018111011/12/15 16:38 gmartJug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 18:37 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 18:37 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.0501,4-Dichlorobenzene
43 8260B P5K027115.0 11/12/15 18:37 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 18:37 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 18:37 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 18:37 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 18:37 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.076Chloroform
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-16D
Prism Sample ID: 5110038-05
Prism Work Order: 5110038
Time Collected: 10/29/15 12:46
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.079Chloromethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 18:37 CGPug/L 0.12m,p-Xylenes
0.73 8260B P5K027115.0 11/12/15 18:37 CGPJug/L 0.065Methyl Butyl Ketone (2-Hexanone)
6.0 8260B P5K027115.0 11/12/15 18:37 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 18:37 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 18:37 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 18:37 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 18:37 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.044Toluene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 18:37 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 18:37 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 18:37 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 18:37 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12998 %Dibromofluoromethane
77-12393 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-9C
Prism Sample ID: 5110038-06
Prism Work Order: 5110038
Time Collected: 10/30/15 08:51
Time Submitted: 11/03/15 08:25
51-03
Total Metals
BRL 6020A P5K018111.0 11/12/15 16:51 gmartug/L 0.069Antimony
0.93 6020A P5K018111.0 11/12/15 16:51 gmartJug/L 0.29Arsenic
33 6020A P5K018115.0 11/12/15 16:51 gmartug/L 0.041Barium
1.0 6020A P5K018111.0 11/12/15 16:51 gmartug/L 0.047Beryllium
0.077 6020A P5K018111.0 11/12/15 16:51 gmartJug/L 0.019Cadmium
12 6020A P5K032911.0 11/17/15 18:04 gmartBug/L 0.51Chromium
28 6020A P5K018111.0 11/12/15 16:51 gmartug/L 0.013Cobalt
21 6020A P5K018115.0 11/12/15 16:51 gmartug/L 0.44Copper
10 6020A P5K018111.0 11/12/15 16:51 gmartug/L 0.020Lead
36 6020A P5K018112.0 11/12/15 16:51 gmartug/L 0.053Nickel
1.1 6020A P5K018111.0 11/12/15 16:51 gmartug/L 0.35Selenium
0.055 6020A P5K018111.0 11/12/15 16:51 gmartJug/L 0.011Silver
0.061 6020A P5K018111.0 11/12/15 16:51 gmartJug/L 0.0093Thallium
6.4 6020A P5K018115.0 11/12/15 16:51 gmartug/L 2.5Vanadium
130 6020A P5K018111011/12/15 16:51 gmartug/L 0.98Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K028811.0 11/13/15 13:16 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K028812.0 11/13/15 13:16 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.0501,4-Dichlorobenzene
8.6 8260B P5K028815.0 11/13/15 13:16 CGPug/L 0.31Acetone
BRL 8260B P5K028812011/13/15 13:16 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.048Benzene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K028811.0 11/13/15 13:16 CGPug/L 0.040Bromoform
BRL 8260B P5K028811.0 11/13/15 13:16 CGPug/L 0.18Bromomethane
BRL 8260B P5K028815.0 11/13/15 13:16 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.22Chloroethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.076Chloroform
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-9C
Prism Sample ID: 5110038-06
Prism Work Order: 5110038
Time Collected: 10/30/15 08:51
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.079Chloromethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.065Dibromomethane
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K028811.0 11/13/15 13:16 CGPug/L 0.12m,p-Xylenes
BRL 8260B P5K028815.0 11/13/15 13:16 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
1.8 8260B P5K028815.0 11/13/15 13:16 CGPJug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K028815.0 11/13/15 13:16 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K028815.0 11/13/15 13:16 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K028811.0 11/13/15 13:16 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.044o-Xylene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.047Styrene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K028811011/13/15 13:16 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.044Toluene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K028811011/13/15 13:16 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K028812.0 11/13/15 13:16 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K028810.50 11/13/15 13:16 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K028813.0 11/13/15 13:16 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-12398 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-9C
Prism Sample ID: 5110038-06RE1
Prism Work Order: 5110038
Time Collected: 10/30/15 08:51
Time Submitted: 11/03/15 08:25
51-03
Total Metals
12 6020A P5K050511.0 11/24/15 17:46 gmartBug/L 0.51Chromium
10 6020A P5L003011.0 12/2/15 19:50 gmartug/L 0.020Lead
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: MW-9C
Prism Sample ID: 5110038-06RE2
Prism Work Order: 5110038
Time Collected: 10/30/15 08:51
Time Submitted: 11/03/15 08:25
51-03
Total Metals
8.5 6020A P5L003011.0 12/2/15 19:50 gmartug/L 0.51Chromium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Field Blank
Prism Sample ID: 5110038-07
Prism Work Order: 5110038
Time Collected: 10/30/15 13:02
Time Submitted: 11/03/15 08:25
51-03
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 13:51 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 13:51 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.0501,4-Dichlorobenzene
8.2 8260B P5K027115.0 11/12/15 13:51 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 13:51 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 13:51 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 13:51 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 13:51 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.076Chloroform
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.079Chloromethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 13:51 CGPug/L 0.12m,p-Xylenes
BRL 8260B P5K027115.0 11/12/15 13:51 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
1.1 8260B P5K027115.0 11/12/15 13:51 CGPJug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 13:51 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 13:51 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 13:51 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 13:51 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.044Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Field Blank
Prism Sample ID: 5110038-07
Prism Work Order: 5110038
Time Collected: 10/30/15 13:02
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 13:51 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 13:51 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 13:51 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 13:51 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Trip Blank
Prism Sample ID: 5110038-08
Prism Work Order: 5110038
Time Collected: 10/30/15 00:00
Time Submitted: 11/03/15 08:25
51-03
Volatile Organic Compounds by GC/MS
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0611,1,1-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0661,1,2-Trichloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0831,1-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0831,1-Dichloroethylene
BRL 8260B P5K027111.0 11/12/15 14:17 CGPug/L 0.141,2,3-Trichloropropane
BRL 8260B P5K027112.0 11/12/15 14:17 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0511,2-Dibromoethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0761,2-Dichlorobenzene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0661,2-Dichloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.111,2-Dichloropropane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.0501,4-Dichlorobenzene
BRL 8260B P5K027115.0 11/12/15 14:17 CGPug/L 0.31Acetone
BRL 8260B P5K027112011/12/15 14:17 CGPug/L 0.20Acrylonitrile
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.048Benzene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.14Bromochloromethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.062Bromodichloromethane
BRL 8260B P5K027111.0 11/12/15 14:17 CGPug/L 0.040Bromoform
BRL 8260B P5K027111.0 11/12/15 14:17 CGPug/L 0.18Bromomethane
BRL 8260B P5K027115.0 11/12/15 14:17 CGPug/L 0.075Carbon disulfide
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.11Carbon Tetrachloride
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.062Chlorobenzene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.22Chloroethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.076Chloroform
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.079Chloromethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.081Dibromochloromethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.065Dibromomethane
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.061Ethylbenzene
BRL 8260B P5K027111.0 11/12/15 14:17 CGPug/L 0.12m,p-Xylenes
BRL 8260B P5K027115.0 11/12/15 14:17 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5K027115.0 11/12/15 14:17 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5K027115.0 11/12/15 14:17 CGPug/L 0.33Methyl Iodide
BRL 8260B P5K027115.0 11/12/15 14:17 CGPug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P5K027111.0 11/12/15 14:17 CGPug/L 0.083Methylene Chloride
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.044o-Xylene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.047Styrene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.098Tetrachloroethylene
BRL 8260B P5K027111011/12/15 14:17 CGPug/L 0.16Tetrahydrofuran
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.044Toluene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 32
Laboratory Report
12/04/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
P. O. Box 2263 Project No.:
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Sample Matrix: Water
Client Sample ID: Trip Blank
Prism Sample ID: 5110038-08
Prism Work Order: 5110038
Time Collected: 10/30/15 00:00
Time Submitted: 11/03/15 08:25
51-03
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P5K027111011/12/15 14:17 CGPug/L 0.12trans-1,4-Dichloro-2-butene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.078Trichloroethylene
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.062Trichlorofluoromethane
BRL 8260B P5K027112.0 11/12/15 14:17 CGPug/L 0.060Vinyl acetate
BRL 8260B P5K027110.50 11/12/15 14:17 CGPug/L 0.097Vinyl chloride
BRL 8260B P5K027113.0 11/12/15 14:17 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-12996 %Dibromofluoromethane
77-12396 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 32
12/4/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110038
Time Submitted: 11/3/2015 8:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5K0271 - 5030B
Blank (P5K0271-BLK1)Prepared & Analyzed: 11/12/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 32
12/4/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110038
Time Submitted: 11/3/2015 8:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5K0271 - 5030B
Blank (P5K0271-BLK1)Prepared & Analyzed: 11/12/15
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9648.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9849.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9748.3
LCS (P5K0271-BS1)Prepared & Analyzed: 11/12/15
1,1-Dichloroethylene ug/L22.9 0.50 20.00 70-154115
Benzene ug/L21.8 0.50 20.00 77-128109
Chlorobenzene ug/L20.3 0.50 20.00 78-119101
Toluene ug/L21.6 0.50 20.00 76-131108
Trichloroethylene ug/L22.4 0.50 20.00 77-133112
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9848.9
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.6
ug/L 50.00 77-123Surrogate: Toluene-d8 9748.5
LCS Dup (P5K0271-BSD1)Prepared & Analyzed: 11/12/15
1,1-Dichloroethylene ug/L22.0 0.50 20.00 2070-154110 4
Benzene ug/L21.1 0.50 20.00 2077-128105 3
Chlorobenzene ug/L20.1 0.50 20.00 2078-119100 1
Toluene ug/L20.9 0.50 20.00 2076-131105 3
Trichloroethylene ug/L21.6 0.50 20.00 2077-133108 4
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9849.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9748.5
ug/L 50.00 77-123Surrogate: Toluene-d8 9848.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 32
12/4/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110038
Time Submitted: 11/3/2015 8:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5K0288 - 5030B
Blank (P5K0288-BLK1)Prepared & Analyzed: 11/13/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 32
12/4/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110038
Time Submitted: 11/3/2015 8:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5K0288 - 5030B
Blank (P5K0288-BLK1)Prepared & Analyzed: 11/13/15
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10150.3
ug/L 50.00 77-123Surrogate: Toluene-d8 9848.8
LCS (P5K0288-BS1)Prepared & Analyzed: 11/13/15
1,1-Dichloroethylene ug/L20.8 0.50 20.00 70-154104
Benzene ug/L20.8 0.50 20.00 77-128104
Chlorobenzene ug/L21.8 0.50 20.00 78-119109
Toluene ug/L21.3 0.50 20.00 76-131106
Trichloroethylene ug/L21.3 0.50 20.00 77-133106
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.3
ug/L 50.00 77-123Surrogate: Toluene-d8 10552.3
LCS Dup (P5K0288-BSD1)Prepared & Analyzed: 11/13/15
1,1-Dichloroethylene ug/L19.9 0.50 20.00 2070-154100 4
Benzene ug/L20.0 0.50 20.00 2077-128100 4
Chlorobenzene ug/L21.2 0.50 20.00 2078-119106 3
Toluene ug/L20.5 0.50 20.00 2076-131102 4
Trichloroethylene ug/L20.3 0.50 20.00 2077-133102 5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10050.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10451.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10652.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 32
12/4/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110038
Time Submitted: 11/3/2015 8:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5K0181 - 3005A
Blank (P5K0181-BLK1)Prepared: 11/10/15 Analyzed: 11/12/15
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L0.455 5.0 J
Beryllium ug/L0.0533 1.0 J
Cadmium ug/LBRL1.0
Cobalt ug/LBRL1.0
Copper ug/LBRL5.0
Lead ug/L0.195 1.0 J
Nickel ug/L0.410 2.0 J
Selenium ug/LBRL1.0
Silver ug/LBRL1.0
Thallium ug/L0.0423 1.0 J
Vanadium ug/LBRL5.0
Zinc ug/LBRL10
LCS (P5K0181-BS1)Prepared: 11/10/15 Analyzed: 11/12/15
Antimony ug/L96.6 1.0 100.0 80-12097
Arsenic ug/L95.2 1.0 100.0 80-12095
Barium ug/L98.7 5.0 100.0 80-12099
Beryllium ug/L1021.0 100.0 80-120102
Cadmium ug/L98.7 1.0 100.0 80-12099
Cobalt ug/L98.2 1.0 100.0 80-12098
Copper ug/L1005.0 100.0 80-120100
Lead ug/L98.7 1.0 100.0 80-12099
Nickel ug/L1002.0 100.0 80-120100
Selenium ug/L94.3 1.0 100.0 80-12094
Silver ug/L97.0 1.0 100.0 80-12097
Thallium ug/L96.5 1.0 100.0 80-12097
Vanadium ug/L95.6 5.0 100.0 80-12096
Zinc ug/L95.3 10 100.0 80-12095
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 32
12/4/15
Level II QC Report
P. O. Box 2263 Project No: 51-03
Project: Detect.Monitor. Networks &
SWPTs
Johnston County Dept. of Public Utilities
Smithfield, NC NC 27577
Attn: Kevin Shields
Prism Work Order: 5110038
Time Submitted: 11/3/2015 8:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P5K0329 - 3005A
Blank (P5K0329-BLK1)Prepared & Analyzed: 11/17/15
Chromium ug/L0.723 1.0 B, J
LCS (P5K0329-BS1)Prepared & Analyzed: 11/17/15
Chromium ug/L95.1 1.0 100.0 B80-12095
Batch P5K0505 - 3005A
Blank (P5K0505-BLK1)Prepared & Analyzed: 11/24/15
Chromium ug/L0.656 1.0 B, J
LCS (P5K0505-BS1)Prepared & Analyzed: 11/24/15
Chromium ug/L97.2 1.0 100.0 B80-12097
Batch P5L0030 - 3005A
Blank (P5L0030-BLK1)Prepared & Analyzed: 12/02/15
Chromium ug/LBRL1.0
Lead ug/L0.105 1.0 J
LCS (P5L0030-BS1)Prepared & Analyzed: 12/02/15
Chromium ug/L92.7 1.0 100.0 80-12093
Lead ug/L98.7 1.0 100.0 80-12099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 32
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P5K03295110038-01 11/17/15 8:4550 50mL mL
P5K01815110038-01 11/10/15 10:2450 50mL mL
P5K01815110038-02 11/10/15 10:2450 50mL mL
P5K03295110038-02 11/17/15 8:4550 50mL mL
P5K01815110038-03 11/10/15 10:2450 50mL mL
P5K03295110038-03 11/17/15 8:4550 50mL mL
P5K01815110038-04 11/10/15 10:2450 50mL mL
P5K03295110038-04 11/17/15 8:4550 50mL mL
P5K03295110038-05 11/17/15 8:4550 50mL mL
P5K01815110038-05 11/10/15 10:2450 50mL mL
P5K01815110038-06 11/10/15 10:2450 50mL mL
P5K03295110038-06 11/17/15 8:4550 50mL mL
P5L00305110038-06RE1 12/02/15 7:5050 50mL mL
P5K05055110038-06RE1 11/24/15 9:2050 50mL mL
P5L00305110038-06RE2 12/02/15 7:5050 50mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P5K02715110038-01 11/12/15 8:4210 10mL mL
P5K02715110038-02 11/12/15 8:4210 10mL mL
P5K02715110038-03 11/12/15 8:4210 10mL mL
P5K02715110038-03 11/12/15 8:4210 10mL mL
P5K02715110038-04 11/12/15 8:4210 10mL mL
P5K02715110038-05 11/12/15 8:4210 10mL mL
P5K02885110038-06 11/13/15 8:3310 10mL mL
P5K02715110038-07 11/12/15 8:4210 10mL mL
P5K02715110038-08 11/12/15 8:4210 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 32
Page 31 of 32
Page 32 of 32

Appendix C
Time vs. Concentration Graphs

October 2015 Semi-Annual Monitoring Report
Johnston County Landfill
NC Solid Waste Permit No. 51-03

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(
p
p
b
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0510152025303540
MW
-
7
B
MW
-
9
C
2
/
2
5
/
1
9
9
9
7
/
1
4
/
2
0
0
1
1
2
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1
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2
0
0
3
4
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1
9
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0
0
6
9
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8
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3
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1
1
6/11/2013 10/30/2015
Pa
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1
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(
p
p
b
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05101520
MW
-
1
1
CD
M
W
-
9
D
9
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2
9
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9
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4
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10/24/2012 10/30/2015
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(
p
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b
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012345
8
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8
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6
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2
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1/29/2014 10/27/2015
Pa
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1
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(
p
p
b
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0123456
MW
-
5
-
2
CD
M
W
-
9
D
7
/
2
6
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1
9
9
7
3
/
4
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8
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1
0
3/18/2013 10/27/2015
Pa
g
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1
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4
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(
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05101520
CD
M
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-
9
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7
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3/21/2013 10/30/2015
Pa
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1
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012345
8
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0
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1/29/2014 10/27/2015
Pa
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1
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(
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012345
8
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1
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1/29/2014 10/27/2015
Pa
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1
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(
p
p
b
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0246810
8
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1
9
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2
0
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3
5
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1
6
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2
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8
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3
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2
0
1
2
1/29/2014 10/27/2015

Th
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